id	sid	tid	token	lemma	pos
eurjchem-518	1	1	untitled	untitle	VERB
eurjchem-518	1	2	european	european	PROPN
eurjchem-518	1	3	journal	journal	PROPN
eurjchem-518	1	4	of	of	ADP
eurjchem-518	1	5	chemistry	chemistry	NOUN
eurjchem-518	1	6	3	3	NUM
eurjchem-518	1	7	(	(	PUNCT
eurjchem-518	1	8	1	1	NUM
eurjchem-518	1	9	)	)	PUNCT
eurjchem-518	1	10	(	(	PUNCT
eurjchem-518	1	11	2012	2012	NUM
eurjchem-518	1	12	)	)	PUNCT
eurjchem-518	1	13	65‐70	65‐70	NOUN
eurjchem-518	1	14	european	european	PROPN
eurjchem-518	1	15	journal	journal	PROPN
eurjchem-518	1	16	of	of	ADP
eurjchem-518	1	17	chemistry	chemistry	NOUN
eurjchem-518	1	18	issn	issn	PROPN
eurjchem-518	1	19	2153‐2249	2153‐2249	PROPN
eurjchem-518	1	20	(	(	PUNCT
eurjchem-518	1	21	print	print	NOUN
eurjchem-518	1	22	)	)	PUNCT
eurjchem-518	1	23	/	/	SYM
eurjchem-518	1	24	issn	issn	PROPN
eurjchem-518	1	25	2153‐2257	2153‐2257	NUM
eurjchem-518	1	26	(	(	PUNCT
eurjchem-518	1	27	online	online	ADJ
eurjchem-518	1	28	)	)	PUNCT
eurjchem-518	1	29			NOUN
eurjchem-518	1	30	2012	2012	NUM
eurjchem-518	1	31	eurjchem	eurjchem	PROPN
eurjchem-518	1	32	doi:10.5155	doi:10.5155	PROPN
eurjchem-518	1	33	/	/	SYM
eurjchem-518	1	34	eurjchem.3.1.65‐70.518	eurjchem.3.1.65‐70.518	PROPN
eurjchem-518	1	35	european	european	PROPN
eurjchem-518	1	36	journal	journal	PROPN
eurjchem-518	1	37	of	of	ADP
eurjchem-518	1	38	chemistry	chemistry	PROPN
eurjchem-518	1	39	journal	journal	PROPN
eurjchem-518	1	40	homepage	homepage	NOUN
eurjchem-518	1	41	:	:	PUNCT
eurjchem-518	1	42	www.eurjchem.com	www.eurjchem.com	X
eurjchem-518	1	43	synthesis	synthesis	NOUN
eurjchem-518	1	44	of	of	ADP
eurjchem-518	1	45	novel	novel	ADJ
eurjchem-518	1	46	2‐propenoyl	2‐propenoyl	PROPN
eurjchem-518	1	47	amides	amide	NOUN
eurjchem-518	1	48	,	,	PUNCT
eurjchem-518	1	49	esters	ester	NOUN
eurjchem-518	1	50	,	,	PUNCT
eurjchem-518	1	51	heterocyclic	heterocyclic	ADJ
eurjchem-518	1	52	compounds	compound	NOUN
eurjchem-518	1	53	and	and	CCONJ
eurjchem-518	1	54	their	their	PRON
eurjchem-518	1	55	screening	screening	NOUN
eurjchem-518	1	56	as	as	ADP
eurjchem-518	1	57	antifungal	antifungal	ADJ
eurjchem-518	1	58	and	and	CCONJ
eurjchem-518	1	59	antibacterial	antibacterial	ADJ
eurjchem-518	1	60	agents	agent	NOUN
eurjchem-518	1	61	ahmed	ahme	VERB
eurjchem-518	1	62	el‐ziatya	el‐ziatya	PROPN
eurjchem-518	1	63	,	,	PUNCT
eurjchem-518	1	64	*	*	SYM
eurjchem-518	1	65	,	,	PUNCT
eurjchem-518	1	66	abdelaal	abdelaal	PROPN
eurjchem-518	1	67	abdalha	abdalha	NOUN
eurjchem-518	1	68	,	,	PUNCT
eurjchem-518	1	69	ashraf	ashraf	PROPN
eurjchem-518	1	70	hameda	hameda	PROPN
eurjchem-518	1	71	,	,	PUNCT
eurjchem-518	1	72	sayed	say	VERB
eurjchem-518	1	73	shibab	shibab	PROPN
eurjchem-518	1	74	and	and	CCONJ
eurjchem-518	1	75	abdelhafed	abdelhafe	VERB
eurjchem-518	1	76	abdullhaa	abdullhaa	NOUN
eurjchem-518	1	77	a	a	DET
eurjchem-518	1	78	chemistry	chemistry	NOUN
eurjchem-518	1	79	department	department	NOUN
eurjchem-518	1	80	,	,	PUNCT
eurjchem-518	1	81	faculty	faculty	NOUN
eurjchem-518	1	82	of	of	ADP
eurjchem-518	1	83	science	science	NOUN
eurjchem-518	1	84	,	,	PUNCT
eurjchem-518	1	85	ain	ain	PROPN
eurjchem-518	1	86	shams	shams	PROPN
eurjchem-518	1	87	university	university	PROPN
eurjchem-518	1	88	,	,	PUNCT
eurjchem-518	1	89	abbassia	abbassia	NOUN
eurjchem-518	1	90	11566	11566	NUM
eurjchem-518	1	91	,	,	PUNCT
eurjchem-518	1	92	cairo	cairo	PROPN
eurjchem-518	1	93	,	,	PUNCT
eurjchem-518	1	94	egypt	egypt	PROPN
eurjchem-518	1	95	b	b	PROPN
eurjchem-518	1	96	chemistry	chemistry	NOUN
eurjchem-518	1	97	department	department	NOUN
eurjchem-518	1	98	,	,	PUNCT
eurjchem-518	1	99	faculty	faculty	NOUN
eurjchem-518	1	100	of	of	ADP
eurjchem-518	1	101	science	science	NOUN
eurjchem-518	1	102	and	and	CCONJ
eurjchem-518	1	103	hummanities	hummanitie	NOUN
eurjchem-518	1	104	,	,	PUNCT
eurjchem-518	1	105	shaqra	shaqra	PROPN
eurjchem-518	1	106	university	university	PROPN
eurjchem-518	1	107	,	,	PUNCT
eurjchem-518	1	108	11962	11962	NUM
eurjchem-518	1	109	,	,	PUNCT
eurjchem-518	1	110	harmala	harmala	PROPN
eurjchem-518	1	111	,	,	PUNCT
eurjchem-518	1	112	saudia	saudia	PROPN
eurjchem-518	1	113	arabia	arabia	PROPN
eurjchem-518	1	114	*	*	PUNCT
eurjchem-518	1	115	corresponding	correspond	VERB
eurjchem-518	1	116	author	author	NOUN
eurjchem-518	1	117	at	at	ADP
eurjchem-518	1	118	:	:	PUNCT
eurjchem-518	1	119	chemistry	chemistry	NOUN
eurjchem-518	1	120	department	department	NOUN
eurjchem-518	1	121	,	,	PUNCT
eurjchem-518	1	122	faculty	faculty	NOUN
eurjchem-518	1	123	of	of	ADP
eurjchem-518	1	124	science	science	NOUN
eurjchem-518	1	125	,	,	PUNCT
eurjchem-518	1	126	ain	ain	PROPN
eurjchem-518	1	127	shams	shams	PROPN
eurjchem-518	1	128	university	university	PROPN
eurjchem-518	1	129	,	,	PUNCT
eurjchem-518	1	130	abbassia	abbassia	NOUN
eurjchem-518	1	131	11566	11566	NUM
eurjchem-518	1	132	,	,	PUNCT
eurjchem-518	1	133	cairo	cairo	PROPN
eurjchem-518	1	134	,	,	PUNCT
eurjchem-518	1	135	egypt	egypt	PROPN
eurjchem-518	1	136	.	.	PUNCT
eurjchem-518	2	1	tel	tel	PROPN
eurjchem-518	2	2	.	.	PUNCT
eurjchem-518	2	3	:	:	PUNCT
eurjchem-518	3	1	+202.2.4831836	+202.2.4831836	NUM
eurjchem-518	3	2	;	;	PUNCT
eurjchem-518	3	3	fax	fax	NOUN
eurjchem-518	3	4	:	:	PUNCT
eurjchem-518	3	5	+202.2.4831836	+202.2.4831836	NUM
eurjchem-518	3	6	.	.	PUNCT
eurjchem-518	3	7	e‐mail	e‐mail	PUNCT
eurjchem-518	4	1	address	address	NOUN
eurjchem-518	4	2	:	:	PUNCT
eurjchem-518	4	3	ahm512@sci.asu.edu.eg	ahm512@sci.asu.edu.eg	PROPN
eurjchem-518	4	4	(	(	PUNCT
eurjchem-518	4	5	a.	a.	PROPN
eurjchem-518	4	6	el‐ziaty	el‐ziaty	PROPN
eurjchem-518	4	7	)	)	PUNCT
eurjchem-518	4	8	.	.	PUNCT
eurjchem-518	5	1	article	article	NOUN
eurjchem-518	5	2	information	information	PROPN
eurjchem-518	5	3	abstract	abstract	ADV
eurjchem-518	5	4	received	receive	VERB
eurjchem-518	5	5	:	:	PUNCT
eurjchem-518	5	6	03	03	NUM
eurjchem-518	5	7	september	september	PROPN
eurjchem-518	5	8	2011	2011	NUM
eurjchem-518	5	9	received	receive	VERB
eurjchem-518	5	10	in	in	ADP
eurjchem-518	5	11	revised	revise	VERB
eurjchem-518	5	12	form	form	NOUN
eurjchem-518	5	13	:	:	PUNCT
eurjchem-518	5	14	26	26	NUM
eurjchem-518	5	15	september	september	PROPN
eurjchem-518	5	16	2011	2011	NUM
eurjchem-518	5	17	accepted	accept	VERB
eurjchem-518	5	18	:	:	PUNCT
eurjchem-518	5	19	26	26	NUM
eurjchem-518	5	20	september	september	PROPN
eurjchem-518	5	21	2011	2011	NUM
eurjchem-518	5	22	online	online	NOUN
eurjchem-518	5	23	:	:	PUNCT
eurjchem-518	5	24	31	31	NUM
eurjchem-518	5	25	march	march	NOUN
eurjchem-518	5	26	2012	2012	NUM
eurjchem-518	5	27	keywords	keyword	NOUN
eurjchem-518	5	28	compound	compound	VERB
eurjchem-518	5	29	,	,	PUNCT
eurjchem-518	5	30	2‐cyano‐3‐(2ˊ,4ˊ‐dichlorophenyl)‐2‐prpoenoyl	2‐cyano‐3‐(2ˊ,4ˊ‐dichlorophenyl)‐2‐prpoenoyl	ADJ
eurjchem-518	5	31	chloride	chloride	NOUN
eurjchem-518	5	32	,	,	PUNCT
eurjchem-518	5	33	3	3	NUM
eurjchem-518	5	34	,	,	PUNCT
eurjchem-518	5	35	was	be	AUX
eurjchem-518	5	36	reacted	react	VERB
eurjchem-518	5	37	with	with	ADP
eurjchem-518	5	38	nitrogen	nitrogen	NOUN
eurjchem-518	5	39	,	,	PUNCT
eurjchem-518	5	40	sulfur	sulfur	NOUN
eurjchem-518	5	41	,	,	PUNCT
eurjchem-518	5	42	and	and	CCONJ
eurjchem-518	5	43	oxygen	oxygen	NOUN
eurjchem-518	5	44	nucleophilic	nucleophilic	ADJ
eurjchem-518	5	45	reagents	reagent	NOUN
eurjchem-518	5	46	to	to	PART
eurjchem-518	5	47	give	give	VERB
eurjchem-518	5	48	new	new	ADJ
eurjchem-518	5	49	2‐propenoyl	2‐propenoyl	ADJ
eurjchem-518	5	50	amide	amide	NOUN
eurjchem-518	5	51	and	and	CCONJ
eurjchem-518	5	52	ester	ester	NOUN
eurjchem-518	5	53	derivatives	derivative	NOUN
eurjchem-518	5	54	.	.	PUNCT
eurjchem-518	6	1	some	some	PRON
eurjchem-518	6	2	of	of	ADP
eurjchem-518	6	3	these	these	DET
eurjchem-518	6	4	derivatives	derivative	NOUN
eurjchem-518	6	5	were	be	AUX
eurjchem-518	6	6	cyclized	cyclize	VERB
eurjchem-518	6	7	under	under	ADP
eurjchem-518	6	8	the	the	DET
eurjchem-518	6	9	reaction	reaction	NOUN
eurjchem-518	6	10	conditions	condition	NOUN
eurjchem-518	6	11	and/or	and/or	CCONJ
eurjchem-518	6	12	with	with	ADP
eurjchem-518	6	13	pocl3	pocl3	NOUN
eurjchem-518	6	14	or	or	CCONJ
eurjchem-518	6	15	ac2o	ac2o	PROPN
eurjchem-518	6	16	to	to	PART
eurjchem-518	6	17	give	give	VERB
eurjchem-518	6	18	new	new	ADJ
eurjchem-518	6	19	derivatives	derivative	NOUN
eurjchem-518	6	20	of	of	ADP
eurjchem-518	6	21	heterocyclic	heterocyclic	ADJ
eurjchem-518	6	22	systems	system	NOUN
eurjchem-518	6	23	.	.	PUNCT
eurjchem-518	7	1	some	some	PRON
eurjchem-518	7	2	of	of	ADP
eurjchem-518	7	3	these	these	DET
eurjchem-518	7	4	compounds	compound	NOUN
eurjchem-518	7	5	were	be	AUX
eurjchem-518	7	6	tested	test	VERB
eurjchem-518	7	7	as	as	ADP
eurjchem-518	7	8	antibacterial	antibacterial	ADJ
eurjchem-518	7	9	and	and	CCONJ
eurjchem-518	7	10	antifungal	antifungal	ADJ
eurjchem-518	7	11	agents	agent	NOUN
eurjchem-518	7	12	.	.	PUNCT
eurjchem-518	8	1	oxadiazole	oxadiazole	NOUN
eurjchem-518	8	2	benzoxazinone	benzoxazinone	NOUN
eurjchem-518	8	3	pyridopyrimidine	pyridopyrimidine	NOUN
eurjchem-518	8	4	2‐propenoyl	2‐propenoyl	ADJ
eurjchem-518	8	5	amide	amide	NOUN
eurjchem-518	8	6	2‐propenoyl	2‐propenoyl	PROPN
eurjchem-518	8	7	chloride	chloride	NOUN
eurjchem-518	8	8	antibacterial	antibacterial	ADJ
eurjchem-518	8	9	activities	activity	NOUN
eurjchem-518	8	10	1	1	NUM
eurjchem-518	8	11	.	.	PUNCT
eurjchem-518	9	1	introduction	introduction	NOUN
eurjchem-518	9	2	the	the	DET
eurjchem-518	9	3	recent	recent	ADJ
eurjchem-518	9	4	wide	wide	ADJ
eurjchem-518	9	5	importance	importance	NOUN
eurjchem-518	9	6	of	of	ADP
eurjchem-518	9	7	2‐propenoylamides	2‐propenoylamide	NOUN
eurjchem-518	9	8	[	[	X
eurjchem-518	9	9	1,2	1,2	NUM
eurjchem-518	9	10	]	]	PUNCT
eurjchem-518	9	11	,	,	PUNCT
eurjchem-518	9	12	2‐	2‐	NUM
eurjchem-518	9	13	propenoates	propenoate	NOUN
eurjchem-518	9	14	[	[	X
eurjchem-518	9	15	3‐6	3‐6	NUM
eurjchem-518	9	16	]	]	PUNCT
eurjchem-518	9	17	,	,	PUNCT
eurjchem-518	9	18	besides	besides	ADV
eurjchem-518	9	19	,	,	PUNCT
eurjchem-518	9	20	the	the	DET
eurjchem-518	9	21	interesting	interesting	ADJ
eurjchem-518	9	22	biological	biological	ADJ
eurjchem-518	9	23	and	and	CCONJ
eurjchem-518	9	24	pharmacological	pharmacological	ADJ
eurjchem-518	9	25	activities	activity	NOUN
eurjchem-518	9	26	of	of	ADP
eurjchem-518	9	27	many	many	ADJ
eurjchem-518	9	28	heterocyclic	heterocyclic	ADJ
eurjchem-518	9	29	systems	system	NOUN
eurjchem-518	9	30	,	,	PUNCT
eurjchem-518	9	31	like	like	INTJ
eurjchem-518	9	32	,	,	PUNCT
eurjchem-518	9	33	benzoxazoles	benzoxazole	NOUN
eurjchem-518	9	34	[	[	X
eurjchem-518	9	35	7	7	NUM
eurjchem-518	9	36	]	]	PUNCT
eurjchem-518	9	37	,	,	PUNCT
eurjchem-518	9	38	pyrimidines	pyrimidine	VERB
eurjchem-518	9	39	[	[	X
eurjchem-518	9	40	8	8	NUM
eurjchem-518	9	41	]	]	PUNCT
eurjchem-518	9	42	,	,	PUNCT
eurjchem-518	9	43	pyridopyrimidines	pyridopyrimidine	VERB
eurjchem-518	9	44	[	[	X
eurjchem-518	9	45	9	9	NUM
eurjchem-518	9	46	]	]	PUNCT
eurjchem-518	9	47	,	,	PUNCT
eurjchem-518	9	48	oxazoles	oxazole	NOUN
eurjchem-518	10	1	[	[	X
eurjchem-518	10	2	10	10	NUM
eurjchem-518	10	3	]	]	PUNCT
eurjchem-518	10	4	,	,	PUNCT
eurjchem-518	10	5	benzoxazines	benzoxazine	VERB
eurjchem-518	10	6	[	[	X
eurjchem-518	10	7	11,12	11,12	NUM
eurjchem-518	10	8	]	]	PUNCT
eurjchem-518	10	9	,	,	PUNCT
eurjchem-518	10	10	oxadiazoles	oxadiazole	NOUN
eurjchem-518	10	11	[	[	X
eurjchem-518	10	12	13	13	NUM
eurjchem-518	10	13	]	]	PUNCT
eurjchem-518	10	14	and	and	CCONJ
eurjchem-518	10	15	pyrazoles	pyrazole	VERB
eurjchem-518	10	16	[	[	X
eurjchem-518	10	17	14	14	NUM
eurjchem-518	10	18	]	]	PUNCT
eurjchem-518	10	19	encourage	encourage	VERB
eurjchem-518	10	20	the	the	DET
eurjchem-518	10	21	authors	author	NOUN
eurjchem-518	10	22	to	to	PART
eurjchem-518	10	23	gather	gather	VERB
eurjchem-518	10	24	these	these	DET
eurjchem-518	10	25	moieties	moiety	NOUN
eurjchem-518	10	26	hoping	hope	VERB
eurjchem-518	10	27	to	to	PART
eurjchem-518	10	28	produce	produce	VERB
eurjchem-518	10	29	a	a	DET
eurjchem-518	10	30	valuable	valuable	ADJ
eurjchem-518	10	31	new	new	ADJ
eurjchem-518	10	32	compounds	compound	NOUN
eurjchem-518	10	33	of	of	ADP
eurjchem-518	10	34	expected	expect	VERB
eurjchem-518	10	35	antibacterial	antibacterial	ADJ
eurjchem-518	10	36	and	and	CCONJ
eurjchem-518	10	37	antifungal	antifungal	ADJ
eurjchem-518	10	38	activity	activity	NOUN
eurjchem-518	10	39	.	.	PUNCT
eurjchem-518	11	1	we	we	PRON
eurjchem-518	11	2	report	report	VERB
eurjchem-518	11	3	here	here	ADV
eurjchem-518	11	4	the	the	DET
eurjchem-518	11	5	synthesis	synthesis	NOUN
eurjchem-518	11	6	of	of	ADP
eurjchem-518	11	7	2‐propenoyl	2‐propenoyl	PROPN
eurjchem-518	11	8	amides	amide	NOUN
eurjchem-518	11	9	,	,	PUNCT
eurjchem-518	11	10	2‐propenoyl	2‐propenoyl	ADJ
eurjchem-518	11	11	esters	ester	NOUN
eurjchem-518	11	12	and	and	CCONJ
eurjchem-518	11	13	some	some	DET
eurjchem-518	11	14	heterocyclic	heterocyclic	ADJ
eurjchem-518	11	15	systems	system	NOUN
eurjchem-518	11	16	by	by	ADP
eurjchem-518	11	17	developed	develop	VERB
eurjchem-518	11	18	,	,	PUNCT
eurjchem-518	11	19	simple	simple	ADJ
eurjchem-518	11	20	convenient	convenient	ADJ
eurjchem-518	11	21	and	and	CCONJ
eurjchem-518	11	22	efficient	efficient	ADJ
eurjchem-518	11	23	procedure	procedure	NOUN
eurjchem-518	11	24	.	.	PUNCT
eurjchem-518	12	1	also	also	ADV
eurjchem-518	12	2	this	this	DET
eurjchem-518	12	3	modified	modify	VERB
eurjchem-518	12	4	method	method	NOUN
eurjchem-518	12	5	is	be	AUX
eurjchem-518	12	6	fast	fast	ADJ
eurjchem-518	12	7	,	,	PUNCT
eurjchem-518	12	8	cheap	cheap	ADJ
eurjchem-518	12	9	and	and	CCONJ
eurjchem-518	12	10	unequivocal	unequivocal	ADJ
eurjchem-518	12	11	preparation	preparation	NOUN
eurjchem-518	12	12	with	with	ADP
eurjchem-518	12	13	improved	improved	ADJ
eurjchem-518	12	14	yields	yield	NOUN
eurjchem-518	12	15	.	.	PUNCT
eurjchem-518	13	1	2	2	X
eurjchem-518	13	2	.	.	X
eurjchem-518	13	3	experimental	experimental	ADJ
eurjchem-518	13	4	2.1	2.1	NUM
eurjchem-518	13	5	.	.	PUNCT
eurjchem-518	14	1	instrumentation	instrumentation	NOUN
eurjchem-518	14	2	melting	melting	NOUN
eurjchem-518	14	3	points	point	NOUN
eurjchem-518	14	4	were	be	AUX
eurjchem-518	14	5	taken	take	VERB
eurjchem-518	14	6	on	on	ADP
eurjchem-518	14	7	griffin	griffin	NOUN
eurjchem-518	14	8	and	and	CCONJ
eurjchem-518	14	9	geory	geory	NOUN
eurjchem-518	14	10	melting	melting	NOUN
eurjchem-518	14	11	point	point	NOUN
eurjchem-518	14	12	apparatus	apparatus	NOUN
eurjchem-518	14	13	and	and	CCONJ
eurjchem-518	14	14	are	be	AUX
eurjchem-518	14	15	uncorrected	uncorrecte	VERB
eurjchem-518	14	16	.	.	PUNCT
eurjchem-518	15	1	ft‐ir	ft‐ir	ADJ
eurjchem-518	15	2	spectra	spectra	PROPN
eurjchem-518	15	3	were	be	AUX
eurjchem-518	15	4	recorded	record	VERB
eurjchem-518	15	5	on	on	ADP
eurjchem-518	15	6	pye	pye	PROPN
eurjchem-518	15	7	unicam	unicam	ADV
eurjchem-518	15	8	sp	sp	ADP
eurjchem-518	15	9	1200	1200	NUM
eurjchem-518	15	10	spectrophotometer	spectrophotometer	NOUN
eurjchem-518	15	11	using	use	VERB
eurjchem-518	15	12	the	the	DET
eurjchem-518	15	13	kbr	kbr	PROPN
eurjchem-518	15	14	wafer	wafer	NOUN
eurjchem-518	15	15	technique	technique	NOUN
eurjchem-518	15	16	.	.	PUNCT
eurjchem-518	16	1	1h	1h	NUM
eurjchem-518	16	2	nmr	nmr	PROPN
eurjchem-518	16	3	spectra	spectra	NOUN
eurjchem-518	16	4	were	be	AUX
eurjchem-518	16	5	determined	determine	VERB
eurjchem-518	16	6	on	on	ADP
eurjchem-518	16	7	varian	varian	PROPN
eurjchem-518	16	8	gemini	gemini	PROPN
eurjchem-518	16	9	300	300	NUM
eurjchem-518	16	10	mhz	mhz	NOUN
eurjchem-518	16	11	using	use	VERB
eurjchem-518	16	12	tms	tms	PROPN
eurjchem-518	16	13	as	as	ADP
eurjchem-518	16	14	internal	internal	ADJ
eurjchem-518	16	15	standard	standard	NOUN
eurjchem-518	16	16	.	.	PUNCT
eurjchem-518	17	1	all	all	DET
eurjchem-518	17	2	chemical	chemical	ADJ
eurjchem-518	17	3	shifts	shift	NOUN
eurjchem-518	17	4	(	(	PUNCT
eurjchem-518	17	5	δ	δ	NOUN
eurjchem-518	17	6	)	)	PUNCT
eurjchem-518	17	7	are	be	AUX
eurjchem-518	17	8	expressed	express	VERB
eurjchem-518	17	9	in	in	ADP
eurjchem-518	17	10	ppm	ppm	NOUN
eurjchem-518	17	11	.	.	PUNCT
eurjchem-518	18	1	all	all	DET
eurjchem-518	18	2	the	the	DET
eurjchem-518	18	3	nh	nh	PROPN
eurjchem-518	18	4	or	or	CCONJ
eurjchem-518	18	5	oh	oh	NUM
eurjchem-518	18	6	protons	proton	NOUN
eurjchem-518	18	7	are	be	AUX
eurjchem-518	18	8	exchangeable	exchangeable	ADJ
eurjchem-518	18	9	on	on	ADP
eurjchem-518	18	10	addition	addition	NOUN
eurjchem-518	18	11	of	of	ADP
eurjchem-518	18	12	d2o	d2o	NOUN
eurjchem-518	18	13	.	.	PUNCT
eurjchem-518	19	1	the	the	DET
eurjchem-518	19	2	elemental	elemental	ADJ
eurjchem-518	19	3	analyses	analysis	NOUN
eurjchem-518	19	4	were	be	AUX
eurjchem-518	19	5	investigated	investigate	VERB
eurjchem-518	19	6	by	by	ADP
eurjchem-518	19	7	elemental	elemental	ADJ
eurjchem-518	19	8	analyzer	analyzer	PROPN
eurjchem-518	19	9	vario	vario	PROPN
eurjchem-518	19	10	el	el	PROPN
eurjchem-518	19	11	iii	iii	PROPN
eurjchem-518	19	12	.	.	PROPN
eurjchem-518	19	13	2.2	2.2	NUM
eurjchem-518	19	14	.	.	PUNCT
eurjchem-518	20	1	syntheses	synthesis	NOUN
eurjchem-518	20	2	2.2.1	2.2.1	NUM
eurjchem-518	20	3	.	.	PUNCT
eurjchem-518	21	1	2‐cyano‐3‐(2ˊ,4ˊ‐dichlorophenyl)acryloyl	2‐cyano‐3‐(2ˊ,4ˊ‐dichlorophenyl)acryloyl	NUM
eurjchem-518	21	2	chloride	chloride	NOUN
eurjchem-518	21	3	(	(	PUNCT
eurjchem-518	21	4	3	3	NUM
eurjchem-518	21	5	)	)	PUNCT
eurjchem-518	21	6	a	a	DET
eurjchem-518	21	7	mixture	mixture	NOUN
eurjchem-518	21	8	of	of	ADP
eurjchem-518	21	9	2	2	NUM
eurjchem-518	21	10	(	(	PUNCT
eurjchem-518	21	11	10	10	NUM
eurjchem-518	21	12	g	g	NOUN
eurjchem-518	21	13	)	)	PUNCT
eurjchem-518	21	14	and	and	CCONJ
eurjchem-518	21	15	thionyl	thionyl	VERB
eurjchem-518	21	16	chloride	chloride	NOUN
eurjchem-518	21	17	(	(	PUNCT
eurjchem-518	21	18	15	15	NUM
eurjchem-518	21	19	ml	ml	NOUN
eurjchem-518	21	20	)	)	PUNCT
eurjchem-518	21	21	was	be	AUX
eurjchem-518	21	22	heated	heat	VERB
eurjchem-518	21	23	on	on	ADP
eurjchem-518	21	24	water	water	NOUN
eurjchem-518	21	25	bath	bath	NOUN
eurjchem-518	21	26	for	for	ADP
eurjchem-518	21	27	3	3	NUM
eurjchem-518	21	28	hours	hour	NOUN
eurjchem-518	21	29	.	.	PUNCT
eurjchem-518	22	1	the	the	DET
eurjchem-518	22	2	excess	excess	ADJ
eurjchem-518	22	3	thionyl	thionyl	ADJ
eurjchem-518	22	4	chloride	chloride	NOUN
eurjchem-518	22	5	was	be	AUX
eurjchem-518	22	6	distilled	distil	VERB
eurjchem-518	22	7	under	under	ADP
eurjchem-518	22	8	reduced	reduced	ADJ
eurjchem-518	22	9	pressure	pressure	NOUN
eurjchem-518	22	10	;	;	PUNCT
eurjchem-518	22	11	the	the	DET
eurjchem-518	22	12	solid	solid	ADJ
eurjchem-518	22	13	separated	separate	VERB
eurjchem-518	22	14	was	be	AUX
eurjchem-518	22	15	collected	collect	VERB
eurjchem-518	22	16	,	,	PUNCT
eurjchem-518	22	17	triturated	triturate	VERB
eurjchem-518	22	18	with	with	ADP
eurjchem-518	22	19	petroleum	petroleum	NOUN
eurjchem-518	22	20	ether	ether	NOUN
eurjchem-518	22	21	40‐60	40‐60	NUM
eurjchem-518	22	22	c	c	PROPN
eurjchem-518	22	23	,	,	PUNCT
eurjchem-518	22	24	dried	dry	VERB
eurjchem-518	22	25	and	and	CCONJ
eurjchem-518	22	26	recrystallized	recrystallize	VERB
eurjchem-518	22	27	from	from	ADP
eurjchem-518	22	28	benzene	benzene	NOUN
eurjchem-518	22	29	to	to	PART
eurjchem-518	22	30	give	give	VERB
eurjchem-518	22	31	3	3	NUM
eurjchem-518	22	32	(	(	PUNCT
eurjchem-518	22	33	scheme	scheme	NOUN
eurjchem-518	22	34	1	1	NUM
eurjchem-518	22	35	)	)	PUNCT
eurjchem-518	22	36	.	.	PUNCT
eurjchem-518	23	1	yellow	yellow	ADJ
eurjchem-518	23	2	.	.	PUNCT
eurjchem-518	23	3	yield	yield	NOUN
eurjchem-518	23	4	:	:	PUNCT
eurjchem-518	23	5	90	90	NUM
eurjchem-518	23	6	%	%	NOUN
eurjchem-518	23	7	.	.	PUNCT
eurjchem-518	24	1	m.p	m.p	PROPN
eurjchem-518	24	2	.	.	PROPN
eurjchem-518	24	3	:	:	PUNCT
eurjchem-518	24	4	88‐90	88‐90	PROPN
eurjchem-518	24	5	oc	oc	PROPN
eurjchem-518	24	6	.	.	PUNCT
eurjchem-518	25	1	ft‐ir	ft‐ir	NOUN
eurjchem-518	25	2	(	(	PUNCT
eurjchem-518	25	3	kbr	kbr	PROPN
eurjchem-518	25	4	,	,	PUNCT
eurjchem-518	25	5	ν	ν	PROPN
eurjchem-518	25	6	,	,	PUNCT
eurjchem-518	25	7	cm‐1	cm‐1	PROPN
eurjchem-518	25	8	):	):	PUNCT
eurjchem-518	25	9	2205	2205	NUM
eurjchem-518	25	10	(	(	PUNCT
eurjchem-518	25	11	c≡n	c≡n	PROPN
eurjchem-518	25	12	)	)	PUNCT
eurjchem-518	25	13	,	,	PUNCT
eurjchem-518	25	14	1738	1738	NUM
eurjchem-518	25	15	(	(	PUNCT
eurjchem-518	25	16	c	c	NOUN
eurjchem-518	25	17	=	=	NOUN
eurjchem-518	25	18	o	o	NOUN
eurjchem-518	25	19	)	)	PUNCT
eurjchem-518	25	20	.	.	PUNCT
eurjchem-518	26	1	1h	1h	NUM
eurjchem-518	26	2	nmr	nmr	NOUN
eurjchem-518	26	3	(	(	PUNCT
eurjchem-518	26	4	300	300	NUM
eurjchem-518	26	5	mhz	mhz	NOUN
eurjchem-518	26	6	,	,	PUNCT
eurjchem-518	26	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-518	26	8	,	,	PUNCT
eurjchem-518	26	9	δ	δ	PROPN
eurjchem-518	26	10	,	,	PUNCT
eurjchem-518	26	11	ppm	ppm	NUM
eurjchem-518	26	12	):	):	PUNCT
eurjchem-518	26	13	8.39	8.39	NUM
eurjchem-518	26	14	(	(	PUNCT
eurjchem-518	26	15	s	s	PROPN
eurjchem-518	26	16	,	,	PUNCT
eurjchem-518	26	17	1h	1h	NUM
eurjchem-518	26	18	,	,	PUNCT
eurjchem-518	26	19	=	=	NOUN
eurjchem-518	26	20	ch	ch	NOUN
eurjchem-518	26	21	)	)	PUNCT
eurjchem-518	26	22	,	,	PUNCT
eurjchem-518	26	23	8.04	8.04	NUM
eurjchem-518	26	24	(	(	PUNCT
eurjchem-518	26	25	d	d	PROPN
eurjchem-518	26	26	,	,	PUNCT
eurjchem-518	26	27	1h	1h	NUM
eurjchem-518	26	28	,	,	PUNCT
eurjchem-518	26	29	j	j	PROPN
eurjchem-518	26	30	=	=	PROPN
eurjchem-518	26	31	8.4	8.4	NUM
eurjchem-518	26	32	hz	hz	NOUN
eurjchem-518	26	33	,	,	PUNCT
eurjchem-518	26	34	ar‐h	ar‐h	PROPN
eurjchem-518	26	35	)	)	PUNCT
eurjchem-518	26	36	,	,	PUNCT
eurjchem-518	26	37	7.77	7.77	NUM
eurjchem-518	26	38	(	(	PUNCT
eurjchem-518	26	39	s	s	PROPN
eurjchem-518	26	40	,	,	PUNCT
eurjchem-518	26	41	1h	1h	NUM
eurjchem-518	26	42	,	,	PUNCT
eurjchem-518	26	43	ar‐h	ar‐h	NOUN
eurjchem-518	26	44	)	)	PUNCT
eurjchem-518	26	45	7.60	7.60	NUM
eurjchem-518	26	46	(	(	PUNCT
eurjchem-518	26	47	d	d	PROPN
eurjchem-518	26	48	,	,	PUNCT
eurjchem-518	26	49	1h	1h	NUM
eurjchem-518	26	50	,	,	PUNCT
eurjchem-518	26	51	j	j	PROPN
eurjchem-518	26	52	=	=	PROPN
eurjchem-518	26	53	8.4	8.4	NUM
eurjchem-518	26	54	hz	hz	NOUN
eurjchem-518	26	55	,	,	PUNCT
eurjchem-518	26	56	ar‐h	ar‐h	PROPN
eurjchem-518	26	57	)	)	PUNCT
eurjchem-518	26	58	.	.	PUNCT
eurjchem-518	27	1	anal	anal	PROPN
eurjchem-518	27	2	.	.	PUNCT
eurjchem-518	27	3	calcd	calcd	NOUN
eurjchem-518	27	4	.	.	PUNCT
eurjchem-518	28	1	for	for	ADP
eurjchem-518	28	2	c10h4cl3no	c10h4cl3no	PROPN
eurjchem-518	28	3	:	:	PUNCT
eurjchem-518	28	4	c	c	X
eurjchem-518	28	5	,	,	PUNCT
eurjchem-518	28	6	46.42	46.42	NUM
eurjchem-518	28	7	;	;	PUNCT
eurjchem-518	28	8	h	h	NOUN
eurjchem-518	28	9	,	,	PUNCT
eurjchem-518	28	10	1.55	1.55	NUM
eurjchem-518	28	11	;	;	PUNCT
eurjchem-518	28	12	n	n	CCONJ
eurjchem-518	28	13	,	,	PUNCT
eurjchem-518	28	14	5.38	5.38	NUM
eurjchem-518	28	15	.	.	PUNCT
eurjchem-518	28	16	found	find	VERB
eurjchem-518	28	17	:	:	PUNCT
eurjchem-518	29	1	c	c	X
eurjchem-518	29	2	,	,	PUNCT
eurjchem-518	29	3	45.89	45.89	NUM
eurjchem-518	29	4	;	;	PUNCT
eurjchem-518	29	5	h	h	NOUN
eurjchem-518	29	6	,	,	PUNCT
eurjchem-518	29	7	1.51	1.51	NUM
eurjchem-518	29	8	;	;	PUNCT
eurjchem-518	29	9	n	n	CCONJ
eurjchem-518	29	10	,	,	PUNCT
eurjchem-518	29	11	5.34	5.34	NUM
eurjchem-518	29	12	%	%	NOUN
eurjchem-518	29	13	.	.	PUNCT
eurjchem-518	30	1	2.2.2	2.2.2	X
eurjchem-518	30	2	.	.	PUNCT
eurjchem-518	30	3	general	general	ADJ
eurjchem-518	30	4	procedure	procedure	NOUN
eurjchem-518	30	5	for	for	ADP
eurjchem-518	30	6	the	the	DET
eurjchem-518	30	7	formation	formation	NOUN
eurjchem-518	30	8	of	of	ADP
eurjchem-518	30	9	compounds	compound	NOUN
eurjchem-518	30	10	4‐9	4‐9	NOUN
eurjchem-518	30	11	a	a	DET
eurjchem-518	30	12	mixture	mixture	NOUN
eurjchem-518	30	13	of	of	ADP
eurjchem-518	30	14	3	3	NUM
eurjchem-518	30	15	(	(	PUNCT
eurjchem-518	30	16	1.30	1.30	NUM
eurjchem-518	30	17	g	g	NOUN
eurjchem-518	30	18	,	,	PUNCT
eurjchem-518	30	19	0.005	0.005	NUM
eurjchem-518	30	20	mol	mol	NOUN
eurjchem-518	30	21	)	)	PUNCT
eurjchem-518	30	22	,	,	PUNCT
eurjchem-518	30	23	triethylamine	triethylamine	NOUN
eurjchem-518	30	24	(	(	PUNCT
eurjchem-518	30	25	0.505	0.505	NUM
eurjchem-518	30	26	g	g	NOUN
eurjchem-518	30	27	,	,	PUNCT
eurjchem-518	30	28	0.005	0.005	NUM
eurjchem-518	30	29	mol	mol	NOUN
eurjchem-518	30	30	)	)	PUNCT
eurjchem-518	30	31	,	,	PUNCT
eurjchem-518	30	32	and	and	CCONJ
eurjchem-518	30	33	phenol	phenol	NOUN
eurjchem-518	30	34	,	,	PUNCT
eurjchem-518	30	35	4‐chlorothiophenol	4‐chlorothiophenol	NOUN
eurjchem-518	30	36	,	,	PUNCT
eurjchem-518	30	37	4‐methoxyaniline	4‐methoxyaniline	NUM
eurjchem-518	30	38	,	,	PUNCT
eurjchem-518	30	39	4‐chloroaniline	4‐chloroaniline	NUM
eurjchem-518	30	40	,	,	PUNCT
eurjchem-518	30	41	4‐methylaniline	4‐methylaniline	NUM
eurjchem-518	30	42	(	(	PUNCT
eurjchem-518	30	43	0.005	0.005	NUM
eurjchem-518	30	44	mol	mol	NOUN
eurjchem-518	30	45	)	)	PUNCT
eurjchem-518	30	46	in	in	ADP
eurjchem-518	30	47	dry	dry	ADJ
eurjchem-518	30	48	benzene	benzene	NOUN
eurjchem-518	30	49	(	(	PUNCT
eurjchem-518	30	50	50	50	NUM
eurjchem-518	30	51	ml	ml	NOUN
eurjchem-518	30	52	)	)	PUNCT
eurjchem-518	30	53	was	be	AUX
eurjchem-518	30	54	refluxed	refluxe	VERB
eurjchem-518	30	55	for	for	ADP
eurjchem-518	30	56	2	2	NUM
eurjchem-518	30	57	hours	hour	NOUN
eurjchem-518	30	58	.	.	PUNCT
eurjchem-518	31	1	the	the	DET
eurjchem-518	31	2	solid	solid	ADJ
eurjchem-518	31	3	separated	separate	VERB
eurjchem-518	31	4	was	be	AUX
eurjchem-518	31	5	filtered	filter	VERB
eurjchem-518	31	6	,	,	PUNCT
eurjchem-518	31	7	washed	wash	VERB
eurjchem-518	31	8	with	with	ADP
eurjchem-518	31	9	water	water	NOUN
eurjchem-518	31	10	(	(	PUNCT
eurjchem-518	31	11	80	80	NUM
eurjchem-518	31	12	ml	ml	NOUN
eurjchem-518	31	13	)	)	PUNCT
eurjchem-518	31	14	,	,	PUNCT
eurjchem-518	31	15	dried	dry	VERB
eurjchem-518	31	16	and	and	CCONJ
eurjchem-518	31	17	recrystallized	recrystallize	VERB
eurjchem-518	31	18	from	from	ADP
eurjchem-518	31	19	toluene	toluene	NOUN
eurjchem-518	31	20	to	to	PART
eurjchem-518	31	21	give	give	VERB
eurjchem-518	31	22	4‐9	4‐9	NOUN
eurjchem-518	31	23	,	,	PUNCT
eurjchem-518	31	24	respectively	respectively	ADV
eurjchem-518	31	25	(	(	PUNCT
eurjchem-518	31	26	scheme	scheme	NOUN
eurjchem-518	31	27	2	2	NUM
eurjchem-518	31	28	)	)	PUNCT
eurjchem-518	31	29	.	.	PUNCT
eurjchem-518	32	1	phenyl	phenyl	NOUN
eurjchem-518	32	2	2‐cyano‐3‐(2,4‐dichlorophenyl	2‐cyano‐3‐(2,4‐dichlorophenyl	NUM
eurjchem-518	32	3	)	)	PUNCT
eurjchem-518	32	4	acrylate	acrylate	NOUN
eurjchem-518	32	5	(	(	PUNCT
eurjchem-518	32	6	4	4	NUM
eurjchem-518	32	7	):	):	PUNCT
eurjchem-518	32	8	yellow	yellow	ADJ
eurjchem-518	32	9	.	.	PUNCT
eurjchem-518	33	1	yield	yield	NOUN
eurjchem-518	33	2	:	:	PUNCT
eurjchem-518	33	3	75	75	NUM
eurjchem-518	33	4	%	%	NOUN
eurjchem-518	33	5	.	.	PUNCT
eurjchem-518	34	1	m.p	m.p	PROPN
eurjchem-518	34	2	.	.	PROPN
eurjchem-518	34	3	:	:	PUNCT
eurjchem-518	35	1	120‐122	120‐122	NUM
eurjchem-518	35	2	oc	oc	NOUN
eurjchem-518	35	3	.	.	PUNCT
eurjchem-518	35	4	ft‐ir	ft‐ir	NOUN
eurjchem-518	35	5	(	(	PUNCT
eurjchem-518	35	6	kbr	kbr	PROPN
eurjchem-518	35	7	,	,	PUNCT
eurjchem-518	35	8	ν	ν	PROPN
eurjchem-518	35	9	,	,	PUNCT
eurjchem-518	35	10	cm‐1	cm‐1	PROPN
eurjchem-518	35	11	):	):	PUNCT
eurjchem-518	35	12	2232	2232	NUM
eurjchem-518	35	13	(	(	PUNCT
eurjchem-518	35	14	c≡n	c≡n	PROPN
eurjchem-518	35	15	)	)	PUNCT
eurjchem-518	35	16	,	,	PUNCT
eurjchem-518	35	17	1743	1743	NUM
eurjchem-518	35	18	(	(	PUNCT
eurjchem-518	35	19	c	c	NOUN
eurjchem-518	35	20	=	=	NOUN
eurjchem-518	35	21	o	o	NOUN
eurjchem-518	35	22	)	)	PUNCT
eurjchem-518	35	23	.	.	PUNCT
eurjchem-518	36	1	1h	1h	NUM
eurjchem-518	36	2	nmr	nmr	NOUN
eurjchem-518	36	3	(	(	PUNCT
eurjchem-518	36	4	300	300	NUM
eurjchem-518	36	5	mhz	mhz	NOUN
eurjchem-518	36	6	,	,	PUNCT
eurjchem-518	36	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-518	36	8	,	,	PUNCT
eurjchem-518	36	9	δ	δ	PROPN
eurjchem-518	36	10	,	,	PUNCT
eurjchem-518	36	11	ppm	ppm	NUM
eurjchem-518	36	12	):	):	PUNCT
eurjchem-518	36	13	8.37	8.37	NUM
eurjchem-518	36	14	(	(	PUNCT
eurjchem-518	36	15	s	s	NOUN
eurjchem-518	36	16	1h	1h	NUM
eurjchem-518	36	17	,	,	PUNCT
eurjchem-518	36	18	=	=	NOUN
eurjchem-518	36	19	ch	ch	NOUN
eurjchem-518	36	20	)	)	PUNCT
eurjchem-518	36	21	,	,	PUNCT
eurjchem-518	36	22	8.16	8.16	NUM
eurjchem-518	36	23	(	(	PUNCT
eurjchem-518	36	24	d	d	PROPN
eurjchem-518	36	25	,	,	PUNCT
eurjchem-518	36	26	1h	1h	NUM
eurjchem-518	36	27	,	,	PUNCT
eurjchem-518	36	28	j	j	PROPN
eurjchem-518	36	29	=	=	PROPN
eurjchem-518	36	30	8.4	8.4	NUM
eurjchem-518	36	31	hz	hz	NOUN
eurjchem-518	36	32	,	,	PUNCT
eurjchem-518	36	33	ar‐h	ar‐h	NOUN
eurjchem-518	36	34	)	)	PUNCT
eurjchem-518	36	35	,	,	PUNCT
eurjchem-518	36	36	7.98	7.98	NUM
eurjchem-518	36	37	(	(	PUNCT
eurjchem-518	36	38	s	s	PROPN
eurjchem-518	36	39	,	,	PUNCT
eurjchem-518	36	40	1h	1h	NUM
eurjchem-518	36	41	,	,	PUNCT
eurjchem-518	36	42	ar‐h	ar‐h	NOUN
eurjchem-518	36	43	)	)	PUNCT
eurjchem-518	36	44	7.75	7.75	NUM
eurjchem-518	36	45	(	(	PUNCT
eurjchem-518	36	46	d	d	PROPN
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eurjchem-518	39	2	,	,	PUNCT
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eurjchem-518	40	2	)	)	PUNCT
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eurjchem-518	40	7	):	):	PUNCT
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eurjchem-518	40	9	.	.	PUNCT
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eurjchem-518	40	11	:	:	PUNCT
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eurjchem-518	41	36	=	=	PROPN
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eurjchem-518	41	42	,	,	PUNCT
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eurjchem-518	41	46	,	,	PUNCT
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eurjchem-518	41	51	,	,	PUNCT
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eurjchem-518	41	59	=	=	PROPN
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eurjchem-518	41	74	.	.	PUNCT
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eurjchem-518	42	4	.	.	PUNCT
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eurjchem-518	43	5	,	,	PUNCT
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eurjchem-518	43	9	,	,	PUNCT
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eurjchem-518	43	13	,	,	PUNCT
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eurjchem-518	43	17	:	:	PUNCT
eurjchem-518	44	1	c	c	X
eurjchem-518	44	2	,	,	PUNCT
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eurjchem-518	44	5	h	h	NOUN
eurjchem-518	44	6	,	,	PUNCT
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eurjchem-518	45	2	)	)	PUNCT
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eurjchem-518	45	4	(	(	PUNCT
eurjchem-518	45	5	6	6	NUM
eurjchem-518	45	6	):	):	PUNCT
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eurjchem-518	45	8	.	.	PUNCT
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eurjchem-518	46	2	:	:	PUNCT
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eurjchem-518	46	5	.	.	PUNCT
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eurjchem-518	47	3	:	:	PUNCT
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eurjchem-518	48	3	.	.	PUNCT
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eurjchem-518	48	5	(	(	PUNCT
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eurjchem-518	48	11	):	):	PUNCT
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eurjchem-518	48	15	)	)	PUNCT
eurjchem-518	48	16	,	,	PUNCT
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eurjchem-518	48	28	.	.	PUNCT
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eurjchem-518	49	30	,	,	PUNCT
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eurjchem-518	49	41	,	,	PUNCT
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eurjchem-518	49	45	,	,	PUNCT
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eurjchem-518	49	51	,	,	PUNCT
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eurjchem-518	49	55	,	,	PUNCT
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eurjchem-518	49	59	=	=	PROPN
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eurjchem-518	49	62	,	,	PUNCT
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eurjchem-518	49	65	,	,	PUNCT
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eurjchem-518	49	69	,	,	PUNCT
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eurjchem-518	49	74	,	,	PUNCT
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eurjchem-518	49	85	,	,	PUNCT
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eurjchem-518	49	88	,	,	PUNCT
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eurjchem-518	49	94	,	,	PUNCT
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eurjchem-518	49	97	8.4	8.4	NUM
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eurjchem-518	49	99	,	,	PUNCT
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eurjchem-518	49	102	,	,	PUNCT
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eurjchem-518	49	124	.	.	PUNCT
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eurjchem-518	51	5	,	,	PUNCT
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eurjchem-518	51	9	,	,	PUNCT
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eurjchem-518	51	13	,	,	PUNCT
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eurjchem-518	51	17	:	:	PUNCT
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eurjchem-518	52	2	,	,	PUNCT
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eurjchem-518	52	5	h	h	NOUN
eurjchem-518	52	6	,	,	PUNCT
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eurjchem-518	52	13	.	.	PUNCT
eurjchem-518	53	1	2‐cyano‐3‐(2,4‐dichlorophenyl)‐n‐4‐tolylacrylamide	2‐cyano‐3‐(2,4‐dichlorophenyl)‐n‐4‐tolylacrylamide	NUM
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eurjchem-518	53	3	7	7	NUM
eurjchem-518	53	4	):	):	PUNCT
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eurjchem-518	53	6	.	.	PUNCT
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eurjchem-518	54	2	:	:	PUNCT
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eurjchem-518	54	5	.	.	PUNCT
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eurjchem-518	55	3	:	:	PUNCT
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eurjchem-518	56	3	.	.	PUNCT
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eurjchem-518	56	5	(	(	PUNCT
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eurjchem-518	56	7	,	,	PUNCT
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eurjchem-518	56	9	,	,	PUNCT
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eurjchem-518	56	11	):	):	PUNCT
eurjchem-518	56	12	3342	3342	NUM
eurjchem-518	56	13	(	(	PUNCT
eurjchem-518	56	14	nh	nh	NOUN
eurjchem-518	56	15	)	)	PUNCT
eurjchem-518	56	16	,	,	PUNCT
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eurjchem-518	56	18	(	(	PUNCT
eurjchem-518	56	19	c≡n	c≡n	NOUN
eurjchem-518	56	20	)	)	PUNCT
eurjchem-518	56	21	,	,	PUNCT
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eurjchem-518	56	25	=	=	NOUN
eurjchem-518	56	26	o	o	NOUN
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eurjchem-518	56	28	.	.	PUNCT
eurjchem-518	57	1	1h	1h	NUM
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eurjchem-518	57	3	(	(	PUNCT
eurjchem-518	57	4	300	300	NUM
eurjchem-518	57	5	mhz	mhz	NOUN
eurjchem-518	57	6	,	,	PUNCT
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eurjchem-518	57	12	):	):	PUNCT
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eurjchem-518	57	16	,	,	PUNCT
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eurjchem-518	57	18	,	,	PUNCT
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eurjchem-518	57	20	)	)	PUNCT
eurjchem-518	57	21	,	,	PUNCT
eurjchem-518	57	22	8.36	8.36	NUM
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eurjchem-518	57	24	s	s	PROPN
eurjchem-518	57	25	,	,	PUNCT
eurjchem-518	57	26	1h	1h	NUM
eurjchem-518	57	27	,	,	PUNCT
eurjchem-518	57	28	=	=	NOUN
eurjchem-518	57	29	ch	ch	NOUN
eurjchem-518	57	30	)	)	PUNCT
eurjchem-518	57	31	,	,	PUNCT
eurjchem-518	57	32	8.0	8.0	NUM
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eurjchem-518	57	34	d	d	PROPN
eurjchem-518	57	35	,	,	PUNCT
eurjchem-518	57	36	1h	1h	NUM
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eurjchem-518	57	39	=	=	PROPN
eurjchem-518	57	40	8.4	8.4	NUM
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eurjchem-518	57	42	,	,	PUNCT
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eurjchem-518	57	44	)	)	PUNCT
eurjchem-518	57	45	,	,	PUNCT
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eurjchem-518	57	48	s	s	PROPN
eurjchem-518	57	49	,	,	PUNCT
eurjchem-518	57	50	1h	1h	NUM
eurjchem-518	57	51	,	,	PUNCT
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eurjchem-518	57	54	,	,	PUNCT
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eurjchem-518	57	58	,	,	PUNCT
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eurjchem-518	57	62	=	=	PROPN
eurjchem-518	57	63	8.4	8.4	NUM
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eurjchem-518	57	65	,	,	PUNCT
eurjchem-518	57	66	ar‐h	ar‐h	NOUN
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eurjchem-518	57	68	,	,	PUNCT
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eurjchem-518	57	76	=	=	PROPN
eurjchem-518	57	77	8.4	8.4	NUM
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eurjchem-518	57	82	,	,	PUNCT
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eurjchem-518	57	85	d	d	NOUN
eurjchem-518	57	86	,	,	PUNCT
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eurjchem-518	57	89	j	j	PROPN
eurjchem-518	57	90	=	=	PROPN
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eurjchem-518	57	96	,	,	PUNCT
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eurjchem-518	57	100	,	,	PUNCT
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eurjchem-518	57	102	,	,	PUNCT
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eurjchem-518	57	104	)	)	PUNCT
eurjchem-518	57	105	.	.	PUNCT
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eurjchem-518	58	2	.	.	PUNCT
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eurjchem-518	58	4	.	.	PUNCT
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eurjchem-518	59	5	,	,	PUNCT
eurjchem-518	59	6	61.65	61.65	NUM
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eurjchem-518	59	8	h	h	NOUN
eurjchem-518	59	9	,	,	PUNCT
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eurjchem-518	59	11	;	;	PUNCT
eurjchem-518	59	12	n	n	CCONJ
eurjchem-518	59	13	,	,	PUNCT
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eurjchem-518	59	17	:	:	PUNCT
eurjchem-518	60	1	c	c	X
eurjchem-518	60	2	,	,	PUNCT
eurjchem-518	60	3	61.60	61.60	NUM
eurjchem-518	60	4	;	;	PUNCT
eurjchem-518	60	5	h	h	NOUN
eurjchem-518	60	6	,	,	PUNCT
eurjchem-518	60	7	3.67	3.67	NUM
eurjchem-518	60	8	;	;	PUNCT
eurjchem-518	60	9	n	n	CCONJ
eurjchem-518	60	10	,	,	PUNCT
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eurjchem-518	60	12	%	%	NOUN
eurjchem-518	60	13	.	.	PUNCT
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eurjchem-518	61	2	)	)	PUNCT
eurjchem-518	61	3	acrylamide	acrylamide	NOUN
eurjchem-518	61	4	(	(	PUNCT
eurjchem-518	61	5	8)	8)	NUM
eurjchem-518	61	6	:	:	PUNCT
eurjchem-518	61	7	yellow	yellow	ADJ
eurjchem-518	61	8	.	.	PUNCT
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eurjchem-518	61	10	:	:	PUNCT
eurjchem-518	61	11	80	80	NUM
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eurjchem-518	61	13	.	.	PUNCT
eurjchem-518	62	1	m.p	m.p	PROPN
eurjchem-518	62	2	.	.	PROPN
eurjchem-518	62	3	:	:	PUNCT
eurjchem-518	63	1	158‐159	158‐159	PROPN
eurjchem-518	63	2	oc	oc	PROPN
eurjchem-518	63	3	.	.	PUNCT
eurjchem-518	63	4	ft‐ir	ft‐ir	NOUN
eurjchem-518	63	5	(	(	PUNCT
eurjchem-518	63	6	kbr	kbr	PROPN
eurjchem-518	63	7	,	,	PUNCT
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eurjchem-518	63	9	,	,	PUNCT
eurjchem-518	63	10	cm‐1	cm‐1	PROPN
eurjchem-518	63	11	):	):	PUNCT
eurjchem-518	63	12	3323	3323	NUM
eurjchem-518	63	13	(	(	PUNCT
eurjchem-518	63	14	nh	nh	NOUN
eurjchem-518	63	15	)	)	PUNCT
eurjchem-518	63	16	,	,	PUNCT
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eurjchem-518	63	18	(	(	PUNCT
eurjchem-518	63	19	c≡n	c≡n	PROPN
eurjchem-518	63	20	)	)	PUNCT
eurjchem-518	63	21	,	,	PUNCT
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eurjchem-518	63	24	c	c	NOUN
eurjchem-518	63	25	=	=	NOUN
eurjchem-518	63	26	o	o	NOUN
eurjchem-518	63	27	)	)	PUNCT
eurjchem-518	63	28	.	.	PUNCT
eurjchem-518	64	1	1h	1h	NUM
eurjchem-518	64	2	nmr	nmr	NOUN
eurjchem-518	64	3	(	(	PUNCT
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eurjchem-518	64	5	mhz	mhz	NOUN
eurjchem-518	64	6	,	,	PUNCT
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eurjchem-518	64	8	,	,	PUNCT
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eurjchem-518	64	10	,	,	PUNCT
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eurjchem-518	64	12	):	):	PUNCT
eurjchem-518	64	13	10.64	10.64	NUM
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eurjchem-518	64	16	,	,	PUNCT
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eurjchem-518	64	18	,	,	PUNCT
eurjchem-518	64	19	nh	nh	PROPN
eurjchem-518	64	20	)	)	PUNCT
eurjchem-518	64	21	,	,	PUNCT
eurjchem-518	64	22	8.39	8.39	NUM
eurjchem-518	64	23	(	(	PUNCT
eurjchem-518	64	24	s	s	NOUN
eurjchem-518	64	25	1h	1h	NUM
eurjchem-518	64	26	,	,	PUNCT
eurjchem-518	64	27	=	=	NOUN
eurjchem-518	64	28	ch	ch	NOUN
eurjchem-518	64	29	)	)	PUNCT
eurjchem-518	64	30	,	,	PUNCT
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eurjchem-518	64	34	,	,	PUNCT
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eurjchem-518	64	36	,	,	PUNCT
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eurjchem-518	64	38	=	=	PROPN
eurjchem-518	64	39	8.4	8.4	NUM
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eurjchem-518	64	41	,	,	PUNCT
eurjchem-518	64	42	ar‐h	ar‐h	NOUN
eurjchem-518	64	43	)	)	PUNCT
eurjchem-518	64	44	,	,	PUNCT
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eurjchem-518	64	46	(	(	PUNCT
eurjchem-518	64	47	s	s	PROPN
eurjchem-518	64	48	,	,	PUNCT
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eurjchem-518	64	50	,	,	PUNCT
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eurjchem-518	64	52	)	)	PUNCT
eurjchem-518	64	53	,	,	PUNCT
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eurjchem-518	64	56	d	d	PROPN
eurjchem-518	64	57	,	,	PUNCT
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eurjchem-518	64	59	,	,	PUNCT
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eurjchem-518	64	61	=	=	PROPN
eurjchem-518	64	62	8.4	8.4	NUM
eurjchem-518	64	63	hz	hz	NOUN
eurjchem-518	64	64	,	,	PUNCT
eurjchem-518	64	65	ar‐h	ar‐h	NOUN
eurjchem-518	64	66	)	)	PUNCT
eurjchem-518	64	67	,	,	PUNCT
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eurjchem-518	64	71	,	,	PUNCT
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eurjchem-518	64	73	,	,	PUNCT
eurjchem-518	64	74	ar‐h	ar‐h	PROPN
eurjchem-518	64	75	)	)	PUNCT
eurjchem-518	64	76	.	.	PUNCT
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eurjchem-518	65	2	.	.	PUNCT
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eurjchem-518	65	4	.	.	PUNCT
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eurjchem-518	66	4	c	c	X
eurjchem-518	66	5	,	,	PUNCT
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eurjchem-518	66	9	,	,	PUNCT
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eurjchem-518	66	13	,	,	PUNCT
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eurjchem-518	66	17	:	:	PUNCT
eurjchem-518	67	1	c	c	X
eurjchem-518	67	2	,	,	PUNCT
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eurjchem-518	67	4	;	;	PUNCT
eurjchem-518	68	1	h	h	NOUN
eurjchem-518	68	2	,	,	PUNCT
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eurjchem-518	68	4	;	;	PUNCT
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eurjchem-518	68	6	,	,	PUNCT
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eurjchem-518	68	9	.	.	PUNCT
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eurjchem-518	69	2	)	)	PUNCT
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eurjchem-518	69	4	(	(	PUNCT
eurjchem-518	69	5	9	9	NUM
eurjchem-518	69	6	):	):	PUNCT
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eurjchem-518	69	8	.	.	PUNCT
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eurjchem-518	70	2	:	:	PUNCT
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eurjchem-518	70	5	.	.	PUNCT
eurjchem-518	71	1	m.p	m.p	PROPN
eurjchem-518	71	2	.	.	PROPN
eurjchem-518	71	3	:	:	PUNCT
eurjchem-518	72	1	176‐178	176‐178	NUM
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eurjchem-518	72	3	.	.	PUNCT
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eurjchem-518	72	5	(	(	PUNCT
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eurjchem-518	72	7	,	,	PUNCT
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eurjchem-518	72	9	,	,	PUNCT
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eurjchem-518	72	11	):	):	PUNCT
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eurjchem-518	72	13	(	(	PUNCT
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eurjchem-518	72	15	)	)	PUNCT
eurjchem-518	72	16	,	,	PUNCT
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eurjchem-518	72	19	c≡n	c≡n	PROPN
eurjchem-518	72	20	)	)	PUNCT
eurjchem-518	72	21	,	,	PUNCT
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eurjchem-518	72	25	=	=	NOUN
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eurjchem-518	72	28	.	.	PUNCT
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eurjchem-518	73	3	(	(	PUNCT
eurjchem-518	73	4	300	300	NUM
eurjchem-518	73	5	mhz	mhz	NOUN
eurjchem-518	73	6	,	,	PUNCT
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eurjchem-518	73	9	,	,	PUNCT
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eurjchem-518	73	11	,	,	PUNCT
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eurjchem-518	73	13	):	):	PUNCT
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eurjchem-518	73	17	,	,	PUNCT
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eurjchem-518	73	19	,	,	PUNCT
eurjchem-518	73	20	nh	nh	PROPN
eurjchem-518	73	21	)	)	PUNCT
eurjchem-518	73	22	,	,	PUNCT
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eurjchem-518	73	24	(	(	PUNCT
eurjchem-518	73	25	s	s	NOUN
eurjchem-518	73	26	1h	1h	NUM
eurjchem-518	73	27	,	,	PUNCT
eurjchem-518	73	28	=	=	NOUN
eurjchem-518	73	29	ch	ch	NOUN
eurjchem-518	73	30	)	)	PUNCT
eurjchem-518	73	31	,	,	PUNCT
eurjchem-518	73	32	8.09	8.09	NUM
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eurjchem-518	73	34	d	d	PROPN
eurjchem-518	73	35	,	,	PUNCT
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eurjchem-518	73	37	,	,	PUNCT
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eurjchem-518	73	39	=	=	PROPN
eurjchem-518	73	40	8.4	8.4	NUM
eurjchem-518	73	41	hz	hz	NOUN
eurjchem-518	73	42	,	,	PUNCT
eurjchem-518	73	43	ar‐h	ar‐h	NOUN
eurjchem-518	73	44	)	)	PUNCT
eurjchem-518	73	45	,	,	PUNCT
eurjchem-518	73	46	7.98	7.98	NUM
eurjchem-518	73	47	(	(	PUNCT
eurjchem-518	73	48	s	s	PROPN
eurjchem-518	73	49	,	,	PUNCT
eurjchem-518	73	50	1h	1h	NUM
eurjchem-518	73	51	,	,	PUNCT
eurjchem-518	73	52	ar‐h	ar‐h	NOUN
eurjchem-518	73	53	)	)	PUNCT
eurjchem-518	73	54	,	,	PUNCT
eurjchem-518	73	55	7.70	7.70	NUM
eurjchem-518	73	56	(	(	PUNCT
eurjchem-518	73	57	d	d	PROPN
eurjchem-518	73	58	,	,	PUNCT
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eurjchem-518	73	60	,	,	PUNCT
eurjchem-518	73	61	j	j	PROPN
eurjchem-518	73	62	=	=	PROPN
eurjchem-518	73	63	8.4	8.4	NUM
eurjchem-518	73	64	hz	hz	NOUN
eurjchem-518	73	65	,	,	PUNCT
eurjchem-518	73	66	ar‐h	ar‐h	NOUN
eurjchem-518	73	67	)	)	PUNCT
eurjchem-518	73	68	,	,	PUNCT
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eurjchem-518	73	70	(	(	PUNCT
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eurjchem-518	73	73	4h	4h	NOUN
eurjchem-518	73	74	,	,	PUNCT
eurjchem-518	73	75	ar‐h	ar‐h	PROPN
eurjchem-518	73	76	)	)	PUNCT
eurjchem-518	73	77	.	.	PUNCT
eurjchem-518	74	1	anal	anal	PROPN
eurjchem-518	74	2	.	.	PUNCT
eurjchem-518	74	3	calcd	calcd	NOUN
eurjchem-518	74	4	.	.	PUNCT
eurjchem-518	75	1	for	for	ADP
eurjchem-518	75	2	c15h9cl2n3o	c15h9cl2n3o	PROPN
eurjchem-518	75	3	:	:	PUNCT
eurjchem-518	75	4	c	c	X
eurjchem-518	75	5	,	,	PUNCT
eurjchem-518	75	6	56.63	56.63	NUM
eurjchem-518	75	7	;	;	PUNCT
eurjchem-518	75	8	h	h	X
eurjchem-518	75	9	,	,	PUNCT
eurjchem-518	75	10	2.85	2.85	NUM
eurjchem-518	75	11	;	;	PUNCT
eurjchem-518	75	12	n	n	CCONJ
eurjchem-518	75	13	,	,	PUNCT
eurjchem-518	75	14	13.21	13.21	NUM
eurjchem-518	75	15	.	.	PUNCT
eurjchem-518	75	16	found	find	VERB
eurjchem-518	75	17	:	:	PUNCT
eurjchem-518	76	1	c	c	X
eurjchem-518	76	2	,	,	PUNCT
eurjchem-518	76	3	56.59	56.59	NUM
eurjchem-518	76	4	;	;	PUNCT
eurjchem-518	76	5	h	h	NOUN
eurjchem-518	76	6	,	,	PUNCT
eurjchem-518	76	7	2.79	2.79	NUM
eurjchem-518	76	8	;	;	PUNCT
eurjchem-518	76	9	n	n	CCONJ
eurjchem-518	76	10	,	,	PUNCT
eurjchem-518	76	11	13.02	13.02	NUM
eurjchem-518	76	12	%	%	NOUN
eurjchem-518	76	13	.	.	PUNCT
eurjchem-518	77	1	2.2.3	2.2.3	X
eurjchem-518	77	2	.	.	X
eurjchem-518	77	3	n’‐(2‐cyano‐3‐(2,4‐dichlorophenyl)acryloyl	n’‐(2‐cyano‐3‐(2,4‐dichlorophenyl)acryloyl	NUM
eurjchem-518	77	4	)	)	PUNCT
eurjchem-518	77	5	benzohydrazide	benzohydrazide	NOUN
eurjchem-518	77	6	(	(	PUNCT
eurjchem-518	77	7	10	10	NUM
eurjchem-518	77	8	)	)	PUNCT
eurjchem-518	77	9	a	a	DET
eurjchem-518	77	10	mixture	mixture	NOUN
eurjchem-518	77	11	of	of	ADP
eurjchem-518	77	12	3	3	NUM
eurjchem-518	77	13	(	(	PUNCT
eurjchem-518	77	14	1.30	1.30	NUM
eurjchem-518	77	15	g	g	NOUN
eurjchem-518	77	16	,	,	PUNCT
eurjchem-518	77	17	0.005	0.005	NUM
eurjchem-518	77	18	mol	mol	NOUN
eurjchem-518	77	19	)	)	PUNCT
eurjchem-518	77	20	,	,	PUNCT
eurjchem-518	77	21	triethylamine	triethylamine	NOUN
eurjchem-518	77	22	(	(	PUNCT
eurjchem-518	77	23	0.505	0.505	NUM
eurjchem-518	77	24	g	g	NOUN
eurjchem-518	77	25	,	,	PUNCT
eurjchem-518	77	26	0.005	0.005	NUM
eurjchem-518	77	27	mol	mol	NOUN
eurjchem-518	77	28	)	)	PUNCT
eurjchem-518	77	29	and	and	CCONJ
eurjchem-518	77	30	benzoyl	benzoyl	ADJ
eurjchem-518	77	31	hydrazine	hydrazine	NOUN
eurjchem-518	77	32	(	(	PUNCT
eurjchem-518	77	33	0.68	0.68	NUM
eurjchem-518	77	34	g	g	NOUN
eurjchem-518	77	35	,	,	PUNCT
eurjchem-518	77	36	0.005	0.005	NUM
eurjchem-518	77	37	mol	mol	NOUN
eurjchem-518	77	38	)	)	PUNCT
eurjchem-518	77	39	in	in	ADP
eurjchem-518	77	40	dry	dry	ADJ
eurjchem-518	77	41	benzene	benzene	NOUN
eurjchem-518	77	42	(	(	PUNCT
eurjchem-518	77	43	50	50	NUM
eurjchem-518	77	44	ml	ml	NOUN
eurjchem-518	77	45	)	)	PUNCT
eurjchem-518	77	46	was	be	AUX
eurjchem-518	77	47	stired	stir	VERB
eurjchem-518	77	48	for	for	ADP
eurjchem-518	77	49	an	an	DET
eurjchem-518	77	50	hour	hour	NOUN
eurjchem-518	77	51	.	.	PUNCT
eurjchem-518	78	1	the	the	DET
eurjchem-518	78	2	solid	solid	ADJ
eurjchem-518	78	3	separated	separate	VERB
eurjchem-518	78	4	was	be	AUX
eurjchem-518	78	5	filtered	filter	VERB
eurjchem-518	78	6	,	,	PUNCT
eurjchem-518	78	7	washed	wash	VERB
eurjchem-518	78	8	with	with	ADP
eurjchem-518	78	9	water	water	NOUN
eurjchem-518	78	10	(	(	PUNCT
eurjchem-518	78	11	80	80	NUM
eurjchem-518	78	12	ml	ml	NOUN
eurjchem-518	78	13	)	)	PUNCT
eurjchem-518	78	14	,	,	PUNCT
eurjchem-518	78	15	dried	dry	VERB
eurjchem-518	78	16	and	and	CCONJ
eurjchem-518	78	17	recrystallized	recrystallize	VERB
eurjchem-518	78	18	from	from	ADP
eurjchem-518	78	19	toluene	toluene	NOUN
eurjchem-518	78	20	to	to	PART
eurjchem-518	78	21	give	give	VERB
eurjchem-518	78	22	10	10	NUM
eurjchem-518	78	23	(	(	PUNCT
eurjchem-518	78	24	scheme	scheme	NOUN
eurjchem-518	78	25	2	2	NUM
eurjchem-518	78	26	)	)	PUNCT
eurjchem-518	78	27	.	.	PUNCT
eurjchem-518	79	1	yellow	yellow	ADJ
eurjchem-518	79	2	.	.	PUNCT
eurjchem-518	79	3	yield	yield	NOUN
eurjchem-518	79	4	:	:	PUNCT
eurjchem-518	79	5	86	86	NUM
eurjchem-518	79	6	%	%	NOUN
eurjchem-518	79	7	.	.	PUNCT
eurjchem-518	80	1	m.p	m.p	PROPN
eurjchem-518	80	2	.	.	PROPN
eurjchem-518	80	3	:	:	PUNCT
eurjchem-518	81	1	180‐181	180‐181	NUM
eurjchem-518	81	2	oc	oc	PROPN
eurjchem-518	81	3	.	.	PUNCT
eurjchem-518	81	4	ft‐ir	ft‐ir	NOUN
eurjchem-518	81	5	(	(	PUNCT
eurjchem-518	81	6	kbr	kbr	PROPN
eurjchem-518	81	7	,	,	PUNCT
eurjchem-518	81	8	ν	ν	PROPN
eurjchem-518	81	9	,	,	PUNCT
eurjchem-518	81	10	cm‐1	cm‐1	PROPN
eurjchem-518	81	11	):	):	PUNCT
eurjchem-518	81	12	3188	3188	NUM
eurjchem-518	81	13	,	,	PUNCT
eurjchem-518	81	14	3209	3209	NUM
eurjchem-518	81	15	(	(	PUNCT
eurjchem-518	81	16	nh	nh	NOUN
eurjchem-518	81	17	)	)	PUNCT
eurjchem-518	81	18	,	,	PUNCT
eurjchem-518	81	19	2218	2218	NUM
eurjchem-518	81	20	(	(	PUNCT
eurjchem-518	81	21	c≡n	c≡n	PROPN
eurjchem-518	81	22	)	)	PUNCT
eurjchem-518	81	23	,	,	PUNCT
eurjchem-518	81	24	1675	1675	NUM
eurjchem-518	81	25	(	(	PUNCT
eurjchem-518	81	26	c	c	NOUN
eurjchem-518	81	27	=	=	NOUN
eurjchem-518	81	28	o	o	NOUN
eurjchem-518	81	29	)	)	PUNCT
eurjchem-518	81	30	.	.	PUNCT
eurjchem-518	82	1	1h	1h	NUM
eurjchem-518	82	2	nmr	nmr	NOUN
eurjchem-518	82	3	(	(	PUNCT
eurjchem-518	82	4	300	300	NUM
eurjchem-518	82	5	mhz	mhz	NOUN
eurjchem-518	82	6	,	,	PUNCT
eurjchem-518	82	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-518	82	8	,	,	PUNCT
eurjchem-518	82	9	δ	δ	PROPN
eurjchem-518	82	10	,	,	PUNCT
eurjchem-518	82	11	ppm	ppm	NUM
eurjchem-518	82	12	):	):	PUNCT
eurjchem-518	82	13	10.81	10.81	NUM
eurjchem-518	82	14	(	(	PUNCT
eurjchem-518	82	15	s	s	PROPN
eurjchem-518	82	16	,	,	PUNCT
eurjchem-518	82	17	1h	1h	NUM
eurjchem-518	82	18	,	,	PUNCT
eurjchem-518	82	19	nh	nh	PROPN
eurjchem-518	82	20	)	)	PUNCT
eurjchem-518	82	21	,	,	PUNCT
eurjchem-518	82	22	10.64	10.64	NUM
eurjchem-518	82	23	(	(	PUNCT
eurjchem-518	82	24	s	s	PROPN
eurjchem-518	82	25	,	,	PUNCT
eurjchem-518	82	26	1h	1h	NUM
eurjchem-518	82	27	,	,	PUNCT
eurjchem-518	82	28	nh	nh	PROPN
eurjchem-518	82	29	)	)	PUNCT
eurjchem-518	82	30	,	,	PUNCT
eurjchem-518	82	31	8.4	8.4	NUM
eurjchem-518	82	32	(	(	PUNCT
eurjchem-518	82	33	s	s	PROPN
eurjchem-518	82	34	,	,	PUNCT
eurjchem-518	82	35	1h	1h	NUM
eurjchem-518	82	36	,	,	PUNCT
eurjchem-518	82	37	=	=	NOUN
eurjchem-518	82	38	ch	ch	NOUN
eurjchem-518	82	39	)	)	PUNCT
eurjchem-518	82	40	,	,	PUNCT
eurjchem-518	82	41	7.89‐7.49	7.89‐7.49	X
eurjchem-518	82	42	(	(	PUNCT
eurjchem-518	82	43	m	m	PROPN
eurjchem-518	82	44	,	,	PUNCT
eurjchem-518	82	45	8h	8h	PROPN
eurjchem-518	82	46	ar‐h	ar‐h	PROPN
eurjchem-518	82	47	)	)	PUNCT
eurjchem-518	82	48	.	.	PUNCT
eurjchem-518	83	1	anal	anal	PROPN
eurjchem-518	83	2	.	.	PUNCT
eurjchem-518	83	3	calcd	calcd	NOUN
eurjchem-518	83	4	.	.	PUNCT
eurjchem-518	84	1	for	for	SCONJ
eurjchem-518	84	2	c17h11cl2n3o2	c17h11cl2n3o2	PROPN
eurjchem-518	84	3	:	:	PUNCT
eurjchem-518	84	4	c	c	X
eurjchem-518	84	5	,	,	PUNCT
eurjchem-518	84	6	56.69	56.69	NUM
eurjchem-518	84	7	;	;	PUNCT
eurjchem-518	84	8	h	h	NOUN
eurjchem-518	84	9	,	,	PUNCT
eurjchem-518	84	10	3.08	3.08	NUM
eurjchem-518	84	11	;	;	PUNCT
eurjchem-518	84	12	n	n	CCONJ
eurjchem-518	84	13	,	,	PUNCT
eurjchem-518	84	14	11.67	11.67	NUM
eurjchem-518	84	15	.	.	PUNCT
eurjchem-518	84	16	found	find	VERB
eurjchem-518	84	17	:	:	PUNCT
eurjchem-518	85	1	c	c	X
eurjchem-518	85	2	,	,	PUNCT
eurjchem-518	85	3	56.65	56.65	NUM
eurjchem-518	85	4	;	;	PUNCT
eurjchem-518	85	5	h	h	NOUN
eurjchem-518	85	6	,	,	PUNCT
eurjchem-518	85	7	2.99	2.99	NUM
eurjchem-518	85	8	;	;	PUNCT
eurjchem-518	85	9	n	n	CCONJ
eurjchem-518	85	10	,	,	PUNCT
eurjchem-518	85	11	11.61	11.61	NUM
eurjchem-518	85	12	%	%	NOUN
eurjchem-518	85	13	.	.	PUNCT
eurjchem-518	86	1	2.2.4	2.2.4	X
eurjchem-518	86	2	.	.	PUNCT
eurjchem-518	87	1	(	(	PUNCT
eurjchem-518	87	2	e)‐3‐(2,4‐ichlorophenyl)‐2‐(5‐phenyl‐1,3,4‐oxadiazol‐	e)‐3‐(2,4‐ichlorophenyl)‐2‐(5‐phenyl‐1,3,4‐oxadiazol‐	NOUN
eurjchem-518	87	3	2‐yl)acrylonitrile	2‐yl)acrylonitrile	NUM
eurjchem-518	87	4	(	(	PUNCT
eurjchem-518	87	5	11	11	NUM
eurjchem-518	87	6	)	)	PUNCT
eurjchem-518	87	7	a	a	DET
eurjchem-518	87	8	mixture	mixture	NOUN
eurjchem-518	87	9	of	of	ADP
eurjchem-518	87	10	10	10	NUM
eurjchem-518	87	11	(	(	PUNCT
eurjchem-518	87	12	1	1	NUM
eurjchem-518	87	13	g	g	NOUN
eurjchem-518	87	14	)	)	PUNCT
eurjchem-518	87	15	and	and	CCONJ
eurjchem-518	87	16	phosphorus	phosphorus	NOUN
eurjchem-518	87	17	oxychloride	oxychloride	NOUN
eurjchem-518	87	18	(	(	PUNCT
eurjchem-518	87	19	10	10	NUM
eurjchem-518	87	20	ml	ml	NOUN
eurjchem-518	87	21	)	)	PUNCT
eurjchem-518	87	22	was	be	AUX
eurjchem-518	87	23	heated	heat	VERB
eurjchem-518	87	24	on	on	ADP
eurjchem-518	87	25	water	water	NOUN
eurjchem-518	87	26	bath	bath	NOUN
eurjchem-518	87	27	for	for	ADP
eurjchem-518	87	28	6	6	NUM
eurjchem-518	87	29	hours	hour	NOUN
eurjchem-518	87	30	.	.	PUNCT
eurjchem-518	88	1	after	after	ADP
eurjchem-518	88	2	cooling	cool	VERB
eurjchem-518	88	3	the	the	DET
eurjchem-518	88	4	reaction	reaction	NOUN
eurjchem-518	88	5	mixture	mixture	NOUN
eurjchem-518	88	6	was	be	AUX
eurjchem-518	88	7	poured	pour	VERB
eurjchem-518	88	8	on	on	ADP
eurjchem-518	88	9	crushed	crush	VERB
eurjchem-518	88	10	ice	ice	NOUN
eurjchem-518	88	11	(	(	PUNCT
eurjchem-518	88	12	20	20	NUM
eurjchem-518	88	13	g	g	NOUN
eurjchem-518	88	14	)	)	PUNCT
eurjchem-518	88	15	.	.	PUNCT
eurjchem-518	89	1	the	the	DET
eurjchem-518	89	2	solid	solid	ADJ
eurjchem-518	89	3	separated	separate	VERB
eurjchem-518	89	4	was	be	AUX
eurjchem-518	89	5	filtered	filter	VERB
eurjchem-518	89	6	,	,	PUNCT
eurjchem-518	89	7	washed	wash	VERB
eurjchem-518	89	8	with	with	ADP
eurjchem-518	89	9	water	water	NOUN
eurjchem-518	89	10	(	(	PUNCT
eurjchem-518	89	11	50	50	NUM
eurjchem-518	89	12	ml	ml	NOUN
eurjchem-518	89	13	)	)	PUNCT
eurjchem-518	89	14	,	,	PUNCT
eurjchem-518	89	15	dried	dry	VERB
eurjchem-518	89	16	and	and	CCONJ
eurjchem-518	89	17	recrystallized	recrystallize	VERB
eurjchem-518	89	18	ftom	ftom	PROPN
eurjchem-518	89	19	ethanol	ethanol	NOUN
eurjchem-518	89	20	to	to	PART
eurjchem-518	89	21	give	give	VERB
eurjchem-518	89	22	11	11	NUM
eurjchem-518	89	23	(	(	PUNCT
eurjchem-518	89	24	scheme	scheme	NOUN
eurjchem-518	89	25	2	2	NUM
eurjchem-518	89	26	)	)	PUNCT
eurjchem-518	89	27	.	.	PUNCT
eurjchem-518	90	1	green	green	ADJ
eurjchem-518	90	2	.	.	PUNCT
eurjchem-518	90	3	yield	yield	NOUN
eurjchem-518	90	4	:	:	PUNCT
eurjchem-518	90	5	75	75	NUM
eurjchem-518	90	6	%	%	NOUN
eurjchem-518	90	7	.	.	PUNCT
eurjchem-518	91	1	m.p	m.p	PROPN
eurjchem-518	91	2	.	.	PROPN
eurjchem-518	91	3	:	:	PUNCT
eurjchem-518	92	1	176‐178	176‐178	NUM
eurjchem-518	92	2	oc	oc	NOUN
eurjchem-518	92	3	.	.	PUNCT
eurjchem-518	92	4	ft‐ir	ft‐ir	NOUN
eurjchem-518	92	5	(	(	PUNCT
eurjchem-518	92	6	kbr	kbr	PROPN
eurjchem-518	92	7	,	,	PUNCT
eurjchem-518	92	8	ν	ν	PROPN
eurjchem-518	92	9	,	,	PUNCT
eurjchem-518	92	10	cm‐1	cm‐1	PROPN
eurjchem-518	92	11	):	):	PUNCT
eurjchem-518	92	12	2205	2205	NUM
eurjchem-518	92	13	(	(	PUNCT
eurjchem-518	92	14	c≡n	c≡n	NOUN
eurjchem-518	92	15	)	)	PUNCT
eurjchem-518	92	16	.	.	PUNCT
eurjchem-518	93	1	1h	1h	NUM
eurjchem-518	93	2	nmr	nmr	NOUN
eurjchem-518	93	3	(	(	PUNCT
eurjchem-518	93	4	300	300	NUM
eurjchem-518	93	5	mhz	mhz	NOUN
eurjchem-518	93	6	,	,	PUNCT
eurjchem-518	93	7	cdcl3	cdcl3	PROPN
eurjchem-518	93	8	,	,	PUNCT
eurjchem-518	93	9	δ	δ	PROPN
eurjchem-518	93	10	,	,	PUNCT
eurjchem-518	93	11	ppm	ppm	NUM
eurjchem-518	93	12	):	):	PUNCT
eurjchem-518	93	13	8.56	8.56	NUM
eurjchem-518	93	14	(	(	PUNCT
eurjchem-518	93	15	s	s	PROPN
eurjchem-518	93	16	,	,	PUNCT
eurjchem-518	93	17	1h	1h	NUM
eurjchem-518	93	18	,	,	PUNCT
eurjchem-518	93	19	ar‐h	ar‐h	NOUN
eurjchem-518	93	20	)	)	PUNCT
eurjchem-518	93	21	8.27	8.27	NUM
eurjchem-518	93	22	(	(	PUNCT
eurjchem-518	93	23	d	d	PROPN
eurjchem-518	93	24	,	,	PUNCT
eurjchem-518	93	25	1h	1h	NUM
eurjchem-518	93	26	,	,	PUNCT
eurjchem-518	93	27	j	j	PROPN
eurjchem-518	93	28	=	=	PROPN
eurjchem-518	93	29	8.4	8.4	NUM
eurjchem-518	93	30	hz	hz	NOUN
eurjchem-518	93	31	,	,	PUNCT
eurjchem-518	93	32	ar‐h	ar‐h	PROPN
eurjchem-518	93	33	)	)	PUNCT
eurjchem-518	93	34	,	,	PUNCT
eurjchem-518	93	35	8.14	8.14	NUM
eurjchem-518	93	36	(	(	PUNCT
eurjchem-518	93	37	d	d	PROPN
eurjchem-518	93	38	,	,	PUNCT
eurjchem-518	93	39	1h	1h	NUM
eurjchem-518	93	40	,	,	PUNCT
eurjchem-518	93	41	j	j	PROPN
eurjchem-518	93	42	=	=	SYM
eurjchem-518	93	43	8.1	8.1	NUM
eurjchem-518	93	44	hz	hz	VERB
eurjchem-518	93	45	,	,	PUNCT
eurjchem-518	93	46	ar‐h	ar‐h	PROPN
eurjchem-518	93	47	)	)	PUNCT
eurjchem-518	93	48	,	,	PUNCT
eurjchem-518	93	49	7.54‐7.43	7.54‐7.43	NUM
eurjchem-518	93	50	(	(	PUNCT
eurjchem-518	93	51	m	m	PROPN
eurjchem-518	93	52	,	,	PUNCT
eurjchem-518	93	53	6h	6h	NUM
eurjchem-518	93	54	,	,	PUNCT
eurjchem-518	93	55	ar‐h	ar‐h	PROPN
eurjchem-518	93	56	,	,	PUNCT
eurjchem-518	93	57	5ph+1aryl	5ph+1aryl	NOUN
eurjchem-518	93	58	)	)	PUNCT
eurjchem-518	93	59	.	.	PUNCT
eurjchem-518	94	1	anal	anal	PROPN
eurjchem-518	94	2	.	.	PUNCT
eurjchem-518	94	3	calcd	calcd	NOUN
eurjchem-518	94	4	.	.	PUNCT
eurjchem-518	95	1	for	for	SCONJ
eurjchem-518	95	2	c17h9cl2n3o	c17h9cl2n3o	PROPN
eurjchem-518	95	3	:	:	PUNCT
eurjchem-518	95	4	c	c	X
eurjchem-518	95	5	,	,	PUNCT
eurjchem-518	95	6	59.67	59.67	NUM
eurjchem-518	95	7	;	;	PUNCT
eurjchem-518	95	8	h	h	NOUN
eurjchem-518	95	9	,	,	PUNCT
eurjchem-518	95	10	2.65	2.65	NUM
eurjchem-518	95	11	;	;	PUNCT
eurjchem-518	95	12	n	n	CCONJ
eurjchem-518	95	13	,	,	PUNCT
eurjchem-518	95	14	12.28	12.28	NUM
eurjchem-518	95	15	.	.	PUNCT
eurjchem-518	95	16	found	find	VERB
eurjchem-518	95	17	:	:	PUNCT
eurjchem-518	96	1	c	c	X
eurjchem-518	96	2	,	,	PUNCT
eurjchem-518	96	3	59.72	59.72	NUM
eurjchem-518	96	4	;	;	PUNCT
eurjchem-518	97	1	h	h	NOUN
eurjchem-518	97	2	,	,	PUNCT
eurjchem-518	97	3	2.61	2.61	NUM
eurjchem-518	97	4	;	;	PUNCT
eurjchem-518	97	5	n	n	CCONJ
eurjchem-518	97	6	,	,	PUNCT
eurjchem-518	97	7	12.33	12.33	NUM
eurjchem-518	97	8	%	%	NOUN
eurjchem-518	97	9	.	.	PUNCT
eurjchem-518	98	1	2.2.5	2.2.5	NUM
eurjchem-518	98	2	.	.	NUM
eurjchem-518	98	3	6‐(2,4‐dichlorophenyl)‐4‐hydroxy‐1‐methyl‐2‐thioxo‐	6‐(2,4‐dichlorophenyl)‐4‐hydroxy‐1‐methyl‐2‐thioxo‐	NUM
eurjchem-518	98	4	1,2‐dihydropyrimidine‐	1,2‐dihydropyrimidine‐	NUM
eurjchem-518	98	5	5‐carbonitrile	5‐carbonitrile	NUM
eurjchem-518	98	6	(	(	PUNCT
eurjchem-518	98	7	12	12	NUM
eurjchem-518	98	8	)	)	PUNCT
eurjchem-518	98	9	n‐methylthiourea	n‐methylthiourea	NUM
eurjchem-518	98	10	(	(	PUNCT
eurjchem-518	98	11	0.45	0.45	NUM
eurjchem-518	98	12	g	g	NOUN
eurjchem-518	98	13	,	,	PUNCT
eurjchem-518	98	14	0.005	0.005	NUM
eurjchem-518	98	15	mol	mol	NOUN
eurjchem-518	98	16	)	)	PUNCT
eurjchem-518	98	17	was	be	AUX
eurjchem-518	98	18	added	add	VERB
eurjchem-518	98	19	to	to	ADP
eurjchem-518	98	20	a	a	DET
eurjchem-518	98	21	solution	solution	NOUN
eurjchem-518	98	22	of	of	ADP
eurjchem-518	98	23	3	3	NUM
eurjchem-518	98	24	(	(	PUNCT
eurjchem-518	98	25	1.30	1.30	NUM
eurjchem-518	98	26	g	g	NOUN
eurjchem-518	98	27	,	,	PUNCT
eurjchem-518	98	28	0.005	0.005	NUM
eurjchem-518	98	29	mol	mol	NOUN
eurjchem-518	98	30	)	)	PUNCT
eurjchem-518	98	31	in	in	ADP
eurjchem-518	98	32	dry	dry	ADJ
eurjchem-518	98	33	benzene	benzene	NOUN
eurjchem-518	98	34	(	(	PUNCT
eurjchem-518	98	35	50	50	NUM
eurjchem-518	98	36	ml	ml	NOUN
eurjchem-518	98	37	)	)	PUNCT
eurjchem-518	98	38	and	and	CCONJ
eurjchem-518	98	39	triethylamine	triethylamine	NOUN
eurjchem-518	98	40	(	(	PUNCT
eurjchem-518	98	41	0.505	0.505	NUM
eurjchem-518	98	42	g	g	NOUN
eurjchem-518	98	43	,	,	PUNCT
eurjchem-518	98	44	0.005	0.005	NUM
eurjchem-518	98	45	mol	mol	NOUN
eurjchem-518	98	46	)	)	PUNCT
eurjchem-518	98	47	,	,	PUNCT
eurjchem-518	98	48	the	the	DET
eurjchem-518	98	49	reaction	reaction	NOUN
eurjchem-518	98	50	mixture	mixture	NOUN
eurjchem-518	98	51	was	be	AUX
eurjchem-518	98	52	refluxed	refluxe	VERB
eurjchem-518	98	53	for	for	ADP
eurjchem-518	98	54	one	one	NUM
eurjchem-518	98	55	hour	hour	NOUN
eurjchem-518	98	56	.	.	PUNCT
eurjchem-518	99	1	the	the	DET
eurjchem-518	99	2	solid	solid	ADJ
eurjchem-518	99	3	formed	form	VERB
eurjchem-518	99	4	was	be	AUX
eurjchem-518	99	5	collected	collect	VERB
eurjchem-518	99	6	,	,	PUNCT
eurjchem-518	99	7	washed	wash	VERB
eurjchem-518	99	8	with	with	ADP
eurjchem-518	99	9	water	water	NOUN
eurjchem-518	99	10	(	(	PUNCT
eurjchem-518	99	11	80	80	NUM
eurjchem-518	99	12	ml	ml	NOUN
eurjchem-518	99	13	)	)	PUNCT
eurjchem-518	99	14	,	,	PUNCT
eurjchem-518	99	15	dried	dry	VERB
eurjchem-518	99	16	and	and	CCONJ
eurjchem-518	99	17	recrystallized	recrystallize	VERB
eurjchem-518	99	18	from	from	ADP
eurjchem-518	99	19	ethanol	ethanol	NOUN
eurjchem-518	99	20	to	to	PART
eurjchem-518	99	21	give	give	VERB
eurjchem-518	99	22	12	12	NUM
eurjchem-518	99	23	(	(	PUNCT
eurjchem-518	99	24	scheme	scheme	NOUN
eurjchem-518	99	25	2	2	NUM
eurjchem-518	99	26	)	)	PUNCT
eurjchem-518	99	27	.	.	PUNCT
eurjchem-518	100	1	yellow	yellow	ADJ
eurjchem-518	100	2	.	.	PUNCT
eurjchem-518	100	3	yield	yield	NOUN
eurjchem-518	100	4	:	:	PUNCT
eurjchem-518	100	5	80	80	NUM
eurjchem-518	100	6	%	%	NOUN
eurjchem-518	100	7	.	.	PUNCT
eurjchem-518	101	1	m.p	m.p	PROPN
eurjchem-518	101	2	.	.	PROPN
eurjchem-518	101	3	:	:	PUNCT
eurjchem-518	102	1	186‐188	186‐188	NUM
eurjchem-518	102	2	oc	oc	NOUN
eurjchem-518	102	3	.	.	PUNCT
eurjchem-518	102	4	ft‐ir	ft‐ir	NOUN
eurjchem-518	102	5	(	(	PUNCT
eurjchem-518	102	6	kbr	kbr	PROPN
eurjchem-518	102	7	,	,	PUNCT
eurjchem-518	102	8	ν	ν	PROPN
eurjchem-518	102	9	,	,	PUNCT
eurjchem-518	102	10	cm‐1	cm‐1	PROPN
eurjchem-518	102	11	):	):	PUNCT
eurjchem-518	102	12	3449	3449	NUM
eurjchem-518	102	13	(	(	PUNCT
eurjchem-518	102	14	oh	oh	INTJ
eurjchem-518	102	15	)	)	PUNCT
eurjchem-518	102	16	,	,	PUNCT
eurjchem-518	102	17	2211	2211	NUM
eurjchem-518	102	18	(	(	PUNCT
eurjchem-518	102	19	cn	cn	PROPN
eurjchem-518	102	20	)	)	PUNCT
eurjchem-518	102	21	,	,	PUNCT
eurjchem-518	102	22	1633	1633	NUM
eurjchem-518	102	23	(	(	PUNCT
eurjchem-518	102	24	c	c	NOUN
eurjchem-518	102	25	=	=	SYM
eurjchem-518	102	26	n	n	NUM
eurjchem-518	102	27	)	)	PUNCT
eurjchem-518	102	28	.	.	PUNCT
eurjchem-518	103	1	1h	1h	NUM
eurjchem-518	103	2	nmr	nmr	NOUN
eurjchem-518	103	3	(	(	PUNCT
eurjchem-518	103	4	300	300	NUM
eurjchem-518	103	5	mhz	mhz	NOUN
eurjchem-518	103	6	,	,	PUNCT
eurjchem-518	103	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-518	103	8	,	,	PUNCT
eurjchem-518	103	9	δ	δ	PROPN
eurjchem-518	103	10	,	,	PUNCT
eurjchem-518	103	11	ppm	ppm	NOUN
eurjchem-518	103	12	):	):	PUNCT
eurjchem-518	103	13	7.9	7.9	NUM
eurjchem-518	103	14	(	(	PUNCT
eurjchem-518	103	15	d	d	PROPN
eurjchem-518	103	16	,	,	PUNCT
eurjchem-518	103	17	1h	1h	NUM
eurjchem-518	103	18	,	,	PUNCT
eurjchem-518	103	19	j	j	PROPN
eurjchem-518	103	20	=	=	SYM
eurjchem-518	103	21	7.9	7.9	NUM
eurjchem-518	103	22	hz	hz	NOUN
eurjchem-518	103	23	,	,	PUNCT
eurjchem-518	103	24	ar‐h	ar‐h	PROPN
eurjchem-518	103	25	)	)	PUNCT
eurjchem-518	103	26	,	,	PUNCT
eurjchem-518	103	27	7.8	7.8	NUM
eurjchem-518	103	28	(	(	PUNCT
eurjchem-518	103	29	d	d	PROPN
eurjchem-518	103	30	,	,	PUNCT
eurjchem-518	103	31	1h	1h	NUM
eurjchem-518	103	32	,	,	PUNCT
eurjchem-518	103	33	j	j	PROPN
eurjchem-518	103	34	=	=	SYM
eurjchem-518	103	35	7.8	7.8	NUM
eurjchem-518	103	36	hz	hz	NOUN
eurjchem-518	103	37	,	,	PUNCT
eurjchem-518	103	38	ar‐h	ar‐h	PROPN
eurjchem-518	103	39	)	)	PUNCT
eurjchem-518	103	40	,	,	PUNCT
eurjchem-518	103	41	7.76	7.76	NUM
eurjchem-518	103	42	(	(	PUNCT
eurjchem-518	103	43	s	s	PROPN
eurjchem-518	103	44	,	,	PUNCT
eurjchem-518	103	45	1h	1h	NUM
eurjchem-518	103	46	,	,	PUNCT
eurjchem-518	103	47	ar‐h	ar‐h	NOUN
eurjchem-518	103	48	)	)	PUNCT
eurjchem-518	103	49	,	,	PUNCT
eurjchem-518	103	50	3.79	3.79	NUM
eurjchem-518	103	51	(	(	PUNCT
eurjchem-518	103	52	s	s	PROPN
eurjchem-518	103	53	,	,	PUNCT
eurjchem-518	103	54	3h	3h	NUM
eurjchem-518	103	55	,	,	PUNCT
eurjchem-518	103	56	nch3	nch3	PROPN
eurjchem-518	103	57	)	)	PUNCT
eurjchem-518	103	58	,	,	PUNCT
eurjchem-518	103	59	1.6	1.6	NUM
eurjchem-518	103	60	(	(	PUNCT
eurjchem-518	103	61	s	s	PROPN
eurjchem-518	103	62	,	,	PUNCT
eurjchem-518	103	63	1h	1h	NUM
eurjchem-518	103	64	,	,	PUNCT
eurjchem-518	103	65	oh	oh	INTJ
eurjchem-518	103	66	)	)	PUNCT
eurjchem-518	103	67	.	.	PUNCT
eurjchem-518	104	1	anal	anal	PROPN
eurjchem-518	104	2	.	.	PUNCT
eurjchem-518	104	3	calcd	calcd	NOUN
eurjchem-518	104	4	.	.	PUNCT
eurjchem-518	105	1	for	for	SCONJ
eurjchem-518	105	2	c12h7cl2n3os	c12h7cl2n3os	PROPN
eurjchem-518	105	3	:	:	PUNCT
eurjchem-518	105	4	c	c	NOUN
eurjchem-518	105	5	,	,	PUNCT
eurjchem-518	105	6	46.17	46.17	NUM
eurjchem-518	105	7	;	;	PUNCT
eurjchem-518	105	8	h	h	NOUN
eurjchem-518	105	9	,	,	PUNCT
eurjchem-518	105	10	2.26	2.26	NUM
eurjchem-518	105	11	;	;	PUNCT
eurjchem-518	105	12	n	n	CCONJ
eurjchem-518	105	13	,	,	PUNCT
eurjchem-518	105	14	13.46	13.46	NUM
eurjchem-518	105	15	.	.	PUNCT
eurjchem-518	105	16	found	find	VERB
eurjchem-518	105	17	:	:	PUNCT
eurjchem-518	106	1	c	c	X
eurjchem-518	106	2	,	,	PUNCT
eurjchem-518	106	3	45.81	45.81	NUM
eurjchem-518	106	4	;	;	PUNCT
eurjchem-518	106	5	h	h	NOUN
eurjchem-518	106	6	,	,	PUNCT
eurjchem-518	106	7	2.81	2.81	NUM
eurjchem-518	106	8	;	;	PUNCT
eurjchem-518	106	9	n	n	CCONJ
eurjchem-518	106	10	,	,	PUNCT
eurjchem-518	106	11	13.43	13.43	NUM
eurjchem-518	106	12	%	%	NOUN
eurjchem-518	106	13	.	.	PUNCT
eurjchem-518	107	1	2.2.6	2.2.6	NUM
eurjchem-518	107	2	.	.	NOUN
eurjchem-518	108	1	1‐(2‐cyano‐3‐(2,4‐dichlorophenyl)acryloyl)‐3‐	1‐(2‐cyano‐3‐(2,4‐dichlorophenyl)acryloyl)‐3‐	NUM
eurjchem-518	108	2	phenylurea	phenylurea	NOUN
eurjchem-518	108	3	(	(	PUNCT
eurjchem-518	108	4	13	13	NUM
eurjchem-518	108	5	)	)	PUNCT
eurjchem-518	108	6	a	a	DET
eurjchem-518	108	7	mixture	mixture	NOUN
eurjchem-518	108	8	of	of	ADP
eurjchem-518	108	9	3	3	NUM
eurjchem-518	108	10	(	(	PUNCT
eurjchem-518	108	11	1.30	1.30	NUM
eurjchem-518	108	12	g	g	NOUN
eurjchem-518	108	13	,	,	PUNCT
eurjchem-518	108	14	0.005	0.005	NUM
eurjchem-518	108	15	mol	mol	NOUN
eurjchem-518	108	16	)	)	PUNCT
eurjchem-518	108	17	,	,	PUNCT
eurjchem-518	108	18	triethylamine	triethylamine	NOUN
eurjchem-518	108	19	(	(	PUNCT
eurjchem-518	108	20	0.505	0.505	NUM
eurjchem-518	108	21	g	g	NOUN
eurjchem-518	108	22	,	,	PUNCT
eurjchem-518	108	23	0.005	0.005	NUM
eurjchem-518	108	24	mol	mol	NOUN
eurjchem-518	108	25	)	)	PUNCT
eurjchem-518	108	26	and	and	CCONJ
eurjchem-518	108	27	phenylurea	phenylurea	NOUN
eurjchem-518	108	28	(	(	PUNCT
eurjchem-518	108	29	0.681	0.681	NUM
eurjchem-518	108	30	g	g	NOUN
eurjchem-518	108	31	)	)	PUNCT
eurjchem-518	108	32	,	,	PUNCT
eurjchem-518	108	33	0.005	0.005	NUM
eurjchem-518	108	34	mol	mol	NOUN
eurjchem-518	108	35	)	)	PUNCT
eurjchem-518	108	36	in	in	ADP
eurjchem-518	108	37	dry	dry	ADJ
eurjchem-518	108	38	benzene	benzene	NOUN
eurjchem-518	108	39	(	(	PUNCT
eurjchem-518	108	40	50	50	NUM
eurjchem-518	108	41	ml	ml	NOUN
eurjchem-518	108	42	)	)	PUNCT
eurjchem-518	108	43	was	be	AUX
eurjchem-518	108	44	stirred	stir	VERB
eurjchem-518	108	45	for	for	ADP
eurjchem-518	108	46	2	2	NUM
eurjchem-518	108	47	hours	hour	NOUN
eurjchem-518	108	48	.	.	PUNCT
eurjchem-518	109	1	the	the	DET
eurjchem-518	109	2	separated	separate	VERB
eurjchem-518	109	3	solid	solid	ADJ
eurjchem-518	109	4	was	be	AUX
eurjchem-518	109	5	filtered	filter	VERB
eurjchem-518	109	6	,	,	PUNCT
eurjchem-518	109	7	washed	wash	VERB
eurjchem-518	109	8	with	with	ADP
eurjchem-518	109	9	water	water	NOUN
eurjchem-518	109	10	(	(	PUNCT
eurjchem-518	109	11	80	80	NUM
eurjchem-518	109	12	ml	ml	NOUN
eurjchem-518	109	13	)	)	PUNCT
eurjchem-518	109	14	,	,	PUNCT
eurjchem-518	109	15	dried	dry	VERB
eurjchem-518	109	16	and	and	CCONJ
eurjchem-518	109	17	recrystallized	recrystallize	VERB
eurjchem-518	109	18	from	from	ADP
eurjchem-518	109	19	benzene	benzene	NOUN
eurjchem-518	109	20	to	to	PART
eurjchem-518	109	21	give	give	VERB
eurjchem-518	109	22	13	13	NUM
eurjchem-518	109	23	(	(	PUNCT
eurjchem-518	109	24	scheme	scheme	NOUN
eurjchem-518	109	25	2	2	NUM
eurjchem-518	109	26	)	)	PUNCT
eurjchem-518	109	27	.	.	PUNCT
eurjchem-518	110	1	yellow	yellow	ADJ
eurjchem-518	110	2	.	.	PUNCT
eurjchem-518	110	3	yield	yield	NOUN
eurjchem-518	110	4	:	:	PUNCT
eurjchem-518	110	5	60	60	NUM
eurjchem-518	110	6	%	%	NOUN
eurjchem-518	110	7	.	.	PUNCT
eurjchem-518	111	1	m.p	m.p	PROPN
eurjchem-518	111	2	.	.	PROPN
eurjchem-518	111	3	:	:	PUNCT
eurjchem-518	112	1	180‐181	180‐181	NUM
eurjchem-518	112	2	oc	oc	PROPN
eurjchem-518	112	3	.	.	PUNCT
eurjchem-518	112	4	ft‐ir	ft‐ir	NOUN
eurjchem-518	112	5	(	(	PUNCT
eurjchem-518	112	6	kbr	kbr	PROPN
eurjchem-518	112	7	,	,	PUNCT
eurjchem-518	112	8	ν	ν	PROPN
eurjchem-518	112	9	,	,	PUNCT
eurjchem-518	112	10	cm‐1	cm‐1	PROPN
eurjchem-518	112	11	):	):	PUNCT
eurjchem-518	112	12	3231	3231	NUM
eurjchem-518	112	13	,	,	PUNCT
eurjchem-518	112	14	3129	3129	NUM
eurjchem-518	112	15	(	(	PUNCT
eurjchem-518	112	16	nh	nh	NOUN
eurjchem-518	112	17	)	)	PUNCT
eurjchem-518	112	18	,	,	PUNCT
eurjchem-518	112	19	2228	2228	NUM
eurjchem-518	112	20	(	(	PUNCT
eurjchem-518	112	21	c≡n	c≡n	PROPN
eurjchem-518	112	22	)	)	PUNCT
eurjchem-518	112	23	,	,	PUNCT
eurjchem-518	112	24	1704	1704	NUM
eurjchem-518	112	25	,	,	PUNCT
eurjchem-518	112	26	1660	1660	NUM
eurjchem-518	112	27	(	(	PUNCT
eurjchem-518	112	28	c	c	NOUN
eurjchem-518	112	29	=	=	NOUN
eurjchem-518	112	30	o	o	NOUN
eurjchem-518	112	31	)	)	PUNCT
eurjchem-518	112	32	.	.	PUNCT
eurjchem-518	113	1	1h	1h	NUM
eurjchem-518	113	2	nmr	nmr	NOUN
eurjchem-518	113	3	(	(	PUNCT
eurjchem-518	113	4	300	300	NUM
eurjchem-518	113	5	mhz	mhz	NOUN
eurjchem-518	113	6	,	,	PUNCT
eurjchem-518	113	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-518	113	8	,	,	PUNCT
eurjchem-518	113	9	δ	δ	PROPN
eurjchem-518	113	10	,	,	PUNCT
eurjchem-518	113	11	ppm	ppm	NUM
eurjchem-518	113	12	):	):	PUNCT
eurjchem-518	113	13	10.23	10.23	NUM
eurjchem-518	113	14	(	(	PUNCT
eurjchem-518	113	15	s	s	PROPN
eurjchem-518	113	16	,	,	PUNCT
eurjchem-518	113	17	1h	1h	NUM
eurjchem-518	113	18	,	,	PUNCT
eurjchem-518	113	19	nh	nh	PROPN
eurjchem-518	113	20	,	,	PUNCT
eurjchem-518	113	21	)	)	PUNCT
eurjchem-518	113	22	,	,	PUNCT
eurjchem-518	113	23	8.5	8.5	NUM
eurjchem-518	113	24	(	(	PUNCT
eurjchem-518	113	25	s	s	PROPN
eurjchem-518	113	26	,	,	PUNCT
eurjchem-518	113	27	1h	1h	NUM
eurjchem-518	113	28	,	,	PUNCT
eurjchem-518	113	29	=	=	NOUN
eurjchem-518	113	30	ch	ch	NOUN
eurjchem-518	113	31	)	)	PUNCT
eurjchem-518	113	32	,	,	PUNCT
eurjchem-518	113	33	8.06‐6.53	8.06‐6.53	NUM
eurjchem-518	113	34	(	(	PUNCT
eurjchem-518	113	35	m	m	PROPN
eurjchem-518	113	36	,	,	PUNCT
eurjchem-518	113	37	8h	8h	NUM
eurjchem-518	113	38	,	,	PUNCT
eurjchem-518	113	39	ar‐h	ar‐h	PROPN
eurjchem-518	113	40	)	)	PUNCT
eurjchem-518	113	41	,	,	PUNCT
eurjchem-518	113	42	5.8	5.8	NUM
eurjchem-518	113	43	(	(	PUNCT
eurjchem-518	113	44	s	s	PROPN
eurjchem-518	113	45	,	,	PUNCT
eurjchem-518	113	46	1h	1h	NUM
eurjchem-518	113	47	,	,	PUNCT
eurjchem-518	113	48	nh	nh	PROPN
eurjchem-518	113	49	)	)	PUNCT
eurjchem-518	113	50	.	.	PUNCT
eurjchem-518	114	1	anal	anal	PROPN
eurjchem-518	114	2	.	.	PUNCT
eurjchem-518	114	3	calcd	calcd	NOUN
eurjchem-518	114	4	.	.	PUNCT
eurjchem-518	115	1	for	for	SCONJ
eurjchem-518	115	2	c17h11cl2n3o2	c17h11cl2n3o2	PROPN
eurjchem-518	115	3	:	:	PUNCT
eurjchem-518	115	4	c	c	X
eurjchem-518	115	5	,	,	PUNCT
eurjchem-518	115	6	56.69	56.69	NUM
eurjchem-518	115	7	;	;	PUNCT
eurjchem-518	115	8	h	h	NOUN
eurjchem-518	115	9	,	,	PUNCT
eurjchem-518	115	10	3.08	3.08	NUM
eurjchem-518	115	11	;	;	PUNCT
eurjchem-518	115	12	n	n	CCONJ
eurjchem-518	115	13	,	,	PUNCT
eurjchem-518	115	14	11.67	11.67	NUM
eurjchem-518	115	15	.	.	PUNCT
eurjchem-518	115	16	found	find	VERB
eurjchem-518	115	17	:	:	PUNCT
eurjchem-518	116	1	c	c	X
eurjchem-518	116	2	,	,	PUNCT
eurjchem-518	116	3	56.62	56.62	NUM
eurjchem-518	116	4	;	;	PUNCT
eurjchem-518	117	1	h	h	NOUN
eurjchem-518	117	2	,	,	PUNCT
eurjchem-518	117	3	3.12	3.12	NUM
eurjchem-518	117	4	;	;	PUNCT
eurjchem-518	117	5	n	n	CCONJ
eurjchem-518	117	6	,	,	PUNCT
eurjchem-518	117	7	11.59	11.59	NUM
eurjchem-518	117	8	%	%	NOUN
eurjchem-518	117	9	.	.	PUNCT
eurjchem-518	118	1	2.2.7	2.2.7	X
eurjchem-518	118	2	.	.	PUNCT
eurjchem-518	119	1	synthesis	synthesis	NOUN
eurjchem-518	119	2	of	of	ADP
eurjchem-518	119	3	compounds	compound	NOUN
eurjchem-518	119	4	14	14	NUM
eurjchem-518	119	5	and	and	CCONJ
eurjchem-518	119	6	15	15	NUM
eurjchem-518	119	7	a	a	DET
eurjchem-518	119	8	mixture	mixture	NOUN
eurjchem-518	119	9	of	of	ADP
eurjchem-518	119	10	3	3	NUM
eurjchem-518	119	11	(	(	PUNCT
eurjchem-518	119	12	1.30	1.30	NUM
eurjchem-518	119	13	g	g	NOUN
eurjchem-518	119	14	,	,	PUNCT
eurjchem-518	119	15	0.005	0.005	NUM
eurjchem-518	119	16	mol	mol	NOUN
eurjchem-518	119	17	)	)	PUNCT
eurjchem-518	119	18	,	,	PUNCT
eurjchem-518	119	19	triethylamine	triethylamine	NOUN
eurjchem-518	119	20	(	(	PUNCT
eurjchem-518	119	21	0.505	0.505	NUM
eurjchem-518	119	22	g	g	NOUN
eurjchem-518	119	23	,	,	PUNCT
eurjchem-518	119	24	0.005	0.005	NUM
eurjchem-518	119	25	mol	mol	NOUN
eurjchem-518	119	26	)	)	PUNCT
eurjchem-518	119	27	and	and	CCONJ
eurjchem-518	119	28	2‐aminopyridine	2‐aminopyridine	NUM
eurjchem-518	119	29	(	(	PUNCT
eurjchem-518	119	30	0.47	0.47	NUM
eurjchem-518	119	31	g	g	NOUN
eurjchem-518	119	32	,	,	PUNCT
eurjchem-518	119	33	0.005	0.005	NUM
eurjchem-518	119	34	mol	mol	NOUN
eurjchem-518	119	35	)	)	PUNCT
eurjchem-518	119	36	in	in	ADP
eurjchem-518	119	37	dry	dry	ADJ
eurjchem-518	119	38	benzene	benzene	NOUN
eurjchem-518	119	39	(	(	PUNCT
eurjchem-518	119	40	50	50	NUM
eurjchem-518	119	41	ml	ml	NOUN
eurjchem-518	119	42	)	)	PUNCT
eurjchem-518	119	43	was	be	AUX
eurjchem-518	119	44	stirred	stir	VERB
eurjchem-518	119	45	for	for	ADP
eurjchem-518	119	46	2	2	NUM
eurjchem-518	119	47	hours	hour	NOUN
eurjchem-518	119	48	.	.	PUNCT
eurjchem-518	120	1	the	the	DET
eurjchem-518	120	2	separated	separate	VERB
eurjchem-518	120	3	solid	solid	ADJ
eurjchem-518	120	4	was	be	AUX
eurjchem-518	120	5	filtered	filter	VERB
eurjchem-518	120	6	,	,	PUNCT
eurjchem-518	120	7	washed	wash	VERB
eurjchem-518	120	8	with	with	ADP
eurjchem-518	120	9	water	water	NOUN
eurjchem-518	120	10	,	,	PUNCT
eurjchem-518	120	11	dried	dry	VERB
eurjchem-518	120	12	and	and	CCONJ
eurjchem-518	120	13	recrystallized	recrystallize	VERB
eurjchem-518	120	14	from	from	ADP
eurjchem-518	120	15	benzene	benzene	NOUN
eurjchem-518	120	16	to	to	PART
eurjchem-518	120	17	give	give	VERB
eurjchem-518	120	18	14	14	NUM
eurjchem-518	120	19	and	and	CCONJ
eurjchem-518	120	20	then	then	ADV
eurjchem-518	120	21	from	from	ADP
eurjchem-518	120	22	ethanol	ethanol	NOUN
eurjchem-518	120	23	to	to	PART
eurjchem-518	120	24	give	give	VERB
eurjchem-518	120	25	15	15	NUM
eurjchem-518	120	26	(	(	PUNCT
eurjchem-518	120	27	scheme	scheme	NOUN
eurjchem-518	120	28	2	2	NUM
eurjchem-518	120	29	)	)	PUNCT
eurjchem-518	120	30	.	.	PUNCT
eurjchem-518	121	1	2‐cyano‐3‐(2,4‐dichlorophenyl)‐n‐(pyridin‐2‐yl	2‐cyano‐3‐(2,4‐dichlorophenyl)‐n‐(pyridin‐2‐yl	NUM
eurjchem-518	121	2	)	)	PUNCT
eurjchem-518	121	3	acrylamide	acrylamide	NOUN
eurjchem-518	121	4	(	(	PUNCT
eurjchem-518	121	5	14	14	NUM
eurjchem-518	121	6	):	):	PUNCT
eurjchem-518	121	7	yellow	yellow	ADJ
eurjchem-518	121	8	.	.	PUNCT
eurjchem-518	122	1	yield	yield	NOUN
eurjchem-518	122	2	:	:	PUNCT
eurjchem-518	122	3	90	90	NUM
eurjchem-518	122	4	%	%	NOUN
eurjchem-518	122	5	.	.	PUNCT
eurjchem-518	123	1	m.p	m.p	PROPN
eurjchem-518	123	2	.	.	PROPN
eurjchem-518	123	3	:	:	PUNCT
eurjchem-518	124	1	210‐211	210‐211	NUM
eurjchem-518	124	2	oc	oc	X
eurjchem-518	124	3	.	.	PUNCT
eurjchem-518	124	4	ft‐ir	ft‐ir	NOUN
eurjchem-518	124	5	(	(	PUNCT
eurjchem-518	124	6	kbr	kbr	PROPN
eurjchem-518	124	7	,	,	PUNCT
eurjchem-518	124	8	ν	ν	PROPN
eurjchem-518	124	9	,	,	PUNCT
eurjchem-518	124	10	cm‐1	cm‐1	PROPN
eurjchem-518	124	11	):	):	PUNCT
eurjchem-518	124	12	3305	3305	NUM
eurjchem-518	124	13	(	(	PUNCT
eurjchem-518	124	14	nh	nh	NOUN
eurjchem-518	124	15	)	)	PUNCT
eurjchem-518	124	16	,	,	PUNCT
eurjchem-518	124	17	2216	2216	NUM
eurjchem-518	124	18	(	(	PUNCT
eurjchem-518	124	19	c≡n	c≡n	PROPN
eurjchem-518	124	20	)	)	PUNCT
eurjchem-518	124	21	,	,	PUNCT
eurjchem-518	124	22	1669	1669	NUM
eurjchem-518	124	23	(	(	PUNCT
eurjchem-518	124	24	c	c	NOUN
eurjchem-518	124	25	=	=	NOUN
eurjchem-518	124	26	o	o	NOUN
eurjchem-518	124	27	)	)	PUNCT
eurjchem-518	124	28	.	.	PUNCT
eurjchem-518	125	1	1h‐nmr	1h‐nmr	NUM
eurjchem-518	125	2	(	(	PUNCT
eurjchem-518	125	3	300	300	NUM
eurjchem-518	125	4	mhz	mhz	NOUN
eurjchem-518	125	5	,	,	PUNCT
eurjchem-518	125	6	dmso‐d6	dmso‐d6	PROPN
eurjchem-518	125	7	,	,	PUNCT
eurjchem-518	125	8	δ	δ	PROPN
eurjchem-518	125	9	,	,	PUNCT
eurjchem-518	125	10	ppm	ppm	NUM
eurjchem-518	125	11	):	):	PUNCT
eurjchem-518	125	12	8.3	8.3	NUM
eurjchem-518	125	13	(	(	PUNCT
eurjchem-518	125	14	s	s	PROPN
eurjchem-518	125	15	,	,	PUNCT
eurjchem-518	125	16	1h	1h	NUM
eurjchem-518	125	17	,	,	PUNCT
eurjchem-518	125	18	=	=	NOUN
eurjchem-518	125	19	ch	ch	NOUN
eurjchem-518	125	20	)	)	PUNCT
eurjchem-518	125	21	,	,	PUNCT
eurjchem-518	125	22	8.07	8.07	NUM
eurjchem-518	125	23	(	(	PUNCT
eurjchem-518	125	24	d	d	PROPN
eurjchem-518	125	25	,	,	PUNCT
eurjchem-518	125	26	1h	1h	NUM
eurjchem-518	125	27	,	,	PUNCT
eurjchem-518	125	28	j	j	PROPN
eurjchem-518	125	29	=	=	PROPN
eurjchem-518	125	30	8.4	8.4	NUM
eurjchem-518	125	31	hz	hz	NOUN
eurjchem-518	125	32	,	,	PUNCT
eurjchem-518	125	33	ar‐h	ar‐h	PROPN
eurjchem-518	125	34	)	)	PUNCT
eurjchem-518	125	35	,	,	PUNCT
eurjchem-518	125	36	6.03	6.03	NUM
eurjchem-518	125	37	(	(	PUNCT
eurjchem-518	125	38	m	m	PROPN
eurjchem-518	125	39	,	,	PUNCT
eurjchem-518	125	40	3h	3h	NUM
eurjchem-518	125	41	,	,	PUNCT
eurjchem-518	125	42	ar‐h	ar‐h	NOUN
eurjchem-518	125	43	)	)	PUNCT
eurjchem-518	125	44	,	,	PUNCT
eurjchem-518	125	45	7.6	7.6	NUM
eurjchem-518	125	46	(	(	PUNCT
eurjchem-518	125	47	s	s	PROPN
eurjchem-518	125	48	,	,	PUNCT
eurjchem-518	125	49	1h	1h	NUM
eurjchem-518	125	50	,	,	PUNCT
eurjchem-518	125	51	nh	nh	NOUN
eurjchem-518	125	52	)	)	PUNCT
eurjchem-518	125	53	6.7‐6.6	6.7‐6.6	NUM
eurjchem-518	125	54	(	(	PUNCT
eurjchem-518	125	55	m	m	PROPN
eurjchem-518	125	56	,	,	PUNCT
eurjchem-518	125	57	3h	3h	NUM
eurjchem-518	125	58	,	,	PUNCT
eurjchem-518	125	59	ar‐h	ar‐h	NOUN
eurjchem-518	125	60	)	)	PUNCT
eurjchem-518	125	61	.	.	PUNCT
eurjchem-518	126	1	anal	anal	PROPN
eurjchem-518	126	2	.	.	PUNCT
eurjchem-518	126	3	calcd	calcd	NOUN
eurjchem-518	126	4	.	.	PUNCT
eurjchem-518	127	1	for	for	ADP
eurjchem-518	127	2	c15h9cl2n3o	c15h9cl2n3o	PROPN
eurjchem-518	127	3	:	:	PUNCT
eurjchem-518	127	4	c	c	X
eurjchem-518	127	5	,	,	PUNCT
eurjchem-518	127	6	56.63	56.63	NUM
eurjchem-518	127	7	;	;	PUNCT
eurjchem-518	127	8	h	h	X
eurjchem-518	127	9	,	,	PUNCT
eurjchem-518	127	10	2.85	2.85	NUM
eurjchem-518	127	11	;	;	PUNCT
eurjchem-518	127	12	n	n	CCONJ
eurjchem-518	127	13	,	,	PUNCT
eurjchem-518	127	14	13.21	13.21	NUM
eurjchem-518	127	15	.	.	PUNCT
eurjchem-518	127	16	found	find	VERB
eurjchem-518	127	17	:	:	PUNCT
eurjchem-518	128	1	c	c	X
eurjchem-518	128	2	,	,	PUNCT
eurjchem-518	128	3	56.59	56.59	NUM
eurjchem-518	128	4	;	;	PUNCT
eurjchem-518	128	5	h	h	NOUN
eurjchem-518	128	6	,	,	PUNCT
eurjchem-518	128	7	2.89	2.89	NUM
eurjchem-518	128	8	;	;	PUNCT
eurjchem-518	128	9	n	n	CCONJ
eurjchem-518	128	10	,	,	PUNCT
eurjchem-518	128	11	13.28	13.28	NUM
eurjchem-518	128	12	%	%	NOUN
eurjchem-518	128	13	.	.	PUNCT
eurjchem-518	129	1	el‐ziaty	el‐ziaty	PROPN
eurjchem-518	129	2	et	et	PROPN
eurjchem-518	129	3	al	al	PROPN
eurjchem-518	129	4	.	.	PUNCT
eurjchem-518	129	5	/	/	SYM
eurjchem-518	129	6	european	european	PROPN
eurjchem-518	129	7	journal	journal	PROPN
eurjchem-518	129	8	of	of	ADP
eurjchem-518	129	9	chemistry	chemistry	NOUN
eurjchem-518	129	10	3	3	NUM
eurjchem-518	129	11	(	(	PUNCT
eurjchem-518	129	12	1	1	NUM
eurjchem-518	129	13	)	)	PUNCT
eurjchem-518	129	14	(	(	PUNCT
eurjchem-518	129	15	2012	2012	NUM
eurjchem-518	129	16	)	)	PUNCT
eurjchem-518	129	17	65‐70	65‐70	NOUN
eurjchem-518	129	18	67	67	NUM
eurjchem-518	129	19	3	3	NUM
eurjchem-518	129	20	ar	ar	NOUN
eurjchem-518	129	21	h	h	NOUN
eurjchem-518	129	22	cl	cl	NOUN
eurjchem-518	130	1	o	o	INTJ
eurjchem-518	130	2	cn	cn	PROPN
eurjchem-518	130	3	ar	ar	PROPN
eurjchem-518	130	4	h	h	PROPN
eurjchem-518	130	5	x	x	PROPN
eurjchem-518	131	1	o	o	PROPN
eurjchem-518	131	2	nc	nc	PROPN
eurjchem-518	131	3	ar/	ar/	PROPN
eurjchem-518	131	4	4	4	NUM
eurjchem-518	131	5	,	,	PUNCT
eurjchem-518	131	6	x	x	PUNCT
eurjchem-518	131	7	=	=	SYM
eurjchem-518	131	8	o	o	NOUN
eurjchem-518	131	9	;	;	PUNCT
eurjchem-518	131	10	ar/	ar/	NOUN
eurjchem-518	131	11	=	=	PUNCT
eurjchem-518	131	12	c6h5	c6h5	PROPN
eurjchem-518	131	13	5	5	NUM
eurjchem-518	131	14	,	,	PUNCT
eurjchem-518	131	15	x	x	PUNCT
eurjchem-518	131	16	=	=	SYM
eurjchem-518	131	17	s	s	X
eurjchem-518	131	18	;	;	PUNCT
eurjchem-518	131	19	ar/	ar/	NOUN
eurjchem-518	131	20	=	=	PUNCT
eurjchem-518	131	21	c6h4(4	c6h4(4	NOUN
eurjchem-518	131	22	-	-	PUNCT
eurjchem-518	131	23	cl	cl	NOUN
eurjchem-518	131	24	)	)	PUNCT
eurjchem-518	131	25	6	6	NUM
eurjchem-518	131	26	,	,	PUNCT
eurjchem-518	131	27	x	x	SYM
eurjchem-518	131	28	=	=	SYM
eurjchem-518	131	29	nh	nh	PROPN
eurjchem-518	131	30	;	;	PUNCT
eurjchem-518	131	31	ar/	ar/	NOUN
eurjchem-518	131	32	=	=	SYM
eurjchem-518	131	33	c6h4(p	c6h4(p	NOUN
eurjchem-518	131	34	-	-	PUNCT
eurjchem-518	131	35	och3	och3	ADJ
eurjchem-518	131	36	)	)	PUNCT
eurjchem-518	131	37	7	7	NUM
eurjchem-518	131	38	,	,	PUNCT
eurjchem-518	131	39	x	x	SYM
eurjchem-518	131	40	=	=	SYM
eurjchem-518	131	41	nh	nh	PROPN
eurjchem-518	131	42	;	;	PUNCT
eurjchem-518	131	43	ar/	ar/	NOUN
eurjchem-518	131	44	=	=	SYM
eurjchem-518	131	45	c6h4(p	c6h4(p	NOUN
eurjchem-518	131	46	-	-	PUNCT
eurjchem-518	131	47	ch3	ch3	NOUN
eurjchem-518	131	48	)	)	PUNCT
eurjchem-518	131	49	8	8	NUM
eurjchem-518	131	50	,	,	PUNCT
eurjchem-518	131	51	x	x	PUNCT
eurjchem-518	131	52	=	=	PUNCT
eurjchem-518	131	53	nh;.ar/	nh;.ar/	NOUN
eurjchem-518	131	54	=	=	NOUN
eurjchem-518	131	55	c6h4	c6h4	X
eurjchem-518	131	56	(	(	PUNCT
eurjchem-518	131	57	p	p	NOUN
eurjchem-518	131	58	-	-	PUNCT
eurjchem-518	131	59	cl	cl	NOUN
eurjchem-518	131	60	)	)	PUNCT
eurjchem-518	131	61	9	9	NUM
eurjchem-518	131	62	,	,	PUNCT
eurjchem-518	131	63	x	x	SYM
eurjchem-518	131	64	=	=	SYM
eurjchem-518	131	65	nh	nh	PROPN
eurjchem-518	131	66	;	;	PUNCT
eurjchem-518	131	67	ar/	ar/	NOUN
eurjchem-518	131	68	=	=	SYM
eurjchem-518	131	69	3	3	NUM
eurjchem-518	131	70	-	-	PUNCT
eurjchem-518	131	71	pyridyl	pyridyl	NOUN
eurjchem-518	131	72	4	4	NUM
eurjchem-518	131	73	-	-	SYM
eurjchem-518	131	74	9	9	NUM
eurjchem-518	131	75	ph	ph	PROPN
eurjchem-518	131	76	co	co	X
eurjchem-518	131	77	nh	nh	PROPN
eurjchem-518	131	78	nh	nh	PROPN
eurjchem-518	131	79	2	2	NUM
eurjchem-518	131	80	ar	ar	PROPN
eurjchem-518	131	81	h	h	NOUN
eurjchem-518	131	82	n	n	PRON
eurjchem-518	131	83	h	h	NOUN
eurjchem-518	132	1	o	o	INTJ
eurjchem-518	132	2	cn	cn	INTJ
eurjchem-518	132	3	10	10	NUM
eurjchem-518	132	4	po	po	NOUN
eurjchem-518	132	5	cl	cl	NOUN
eurjchem-518	132	6	3	3	NUM
eurjchem-518	132	7	nn	nn	NOUN
eurjchem-518	132	8	o	o	PROPN
eurjchem-518	132	9	ph	ph	PROPN
eurjchem-518	132	10	nc	nc	PROPN
eurjchem-518	132	11	11	11	NUM
eurjchem-518	132	12	ar	ar	PROPN
eurjchem-518	132	13	h	h	PROPN
eurjchem-518	132	14	nh	nh	PROPN
eurjchem-518	133	1	2csnhch	2csnhch	NUM
eurjchem-518	133	2	3	3	NUM
eurjchem-518	133	3	2	2	NUM
eurjchem-518	133	4	-	-	PUNCT
eurjchem-518	133	5	aminpryidine	aminpryidine	NOUN
eurjchem-518	133	6	n	n	CCONJ
eurjchem-518	133	7	n	n	ADV
eurjchem-518	134	1	oh	oh	INTJ
eurjchem-518	134	2	nc	nc	PROPN
eurjchem-518	134	3	ar	ar	PROPN
eurjchem-518	134	4	ch3	ch3	PROPN
eurjchem-518	134	5	s	s	PART
eurjchem-518	134	6	12	12	NUM
eurjchem-518	134	7	ar	ar	NOUN
eurjchem-518	134	8	h	h	PROPN
eurjchem-518	134	9	n	n	PRON
eurjchem-518	134	10	h	h	NOUN
eurjchem-518	135	1	o	o	INTJ
eurjchem-518	135	2	cn	cn	INTJ
eurjchem-518	136	1	o	o	PROPN
eurjchem-518	136	2	13	13	NUM
eurjchem-518	136	3	ar	ar	NOUN
eurjchem-518	136	4	h	h	NOUN
eurjchem-518	137	1	cn	cn	PROPN
eurjchem-518	137	2	o	o	PROPN
eurjchem-518	138	1	n	n	CCONJ
eurjchem-518	138	2	h	h	NOUN
eurjchem-518	139	1	n	n	ADV
eurjchem-518	139	2	14	14	NUM
eurjchem-518	139	3	+	+	CCONJ
eurjchem-518	139	4	n	n	CCONJ
eurjchem-518	139	5	n	n	PROPN
eurjchem-518	139	6	ar	ar	PROPN
eurjchem-518	139	7	nc	nc	PROPN
eurjchem-518	139	8	ho	ho	PROPN
eurjchem-518	139	9	15	15	NUM
eurjchem-518	139	10	ar	ar	NOUN
eurjchem-518	139	11	=	=	PUNCT
eurjchem-518	139	12	c6h3cl2(2,4	c6h3cl2(2,4	NOUN
eurjchem-518	139	13	)	)	PUNCT
eurjchem-518	140	1	n	n	NOUN
eurjchem-518	140	2	h	h	NOUN
eurjchem-518	140	3	ph	ph	NOUN
eurjchem-518	140	4	h	h	NOUN
eurjchem-518	140	5	n	n	PRON
eurjchem-518	140	6	ph	ph	NOUN
eurjchem-518	140	7	o	o	PROPN
eurjchem-518	140	8	scheme	scheme	NOUN
eurjchem-518	140	9	2	2	NUM
eurjchem-518	140	10	4‐(2,4‐dichlorophenyl)‐2‐hydroxy‐4h‐pyrimido[1,2‐a	4‐(2,4‐dichlorophenyl)‐2‐hydroxy‐4h‐pyrimido[1,2‐a	NOUN
eurjchem-518	140	11	]	]	X
eurjchem-518	140	12	pyrimidine‐3‐carbonitrile	pyrimidine‐3‐carbonitrile	PROPN
eurjchem-518	140	13	(	(	PUNCT
eurjchem-518	140	14	15	15	NUM
eurjchem-518	141	1	):	):	PUNCT
eurjchem-518	141	2	yellow	yellow	ADJ
eurjchem-518	141	3	.	.	PUNCT
eurjchem-518	141	4	yield	yield	NOUN
eurjchem-518	141	5	:	:	PUNCT
eurjchem-518	141	6	65	65	NUM
eurjchem-518	141	7	%	%	NOUN
eurjchem-518	141	8	.	.	PUNCT
eurjchem-518	142	1	m.p	m.p	PROPN
eurjchem-518	142	2	.	.	PROPN
eurjchem-518	142	3	:	:	PUNCT
eurjchem-518	143	1	152‐	152‐	NUM
eurjchem-518	143	2	153	153	NUM
eurjchem-518	143	3	oc	oc	NOUN
eurjchem-518	143	4	.	.	PUNCT
eurjchem-518	143	5	ft‐ir	ft‐ir	NOUN
eurjchem-518	143	6	(	(	PUNCT
eurjchem-518	143	7	kbr	kbr	PROPN
eurjchem-518	143	8	,	,	PUNCT
eurjchem-518	143	9	ν	ν	PROPN
eurjchem-518	143	10	,	,	PUNCT
eurjchem-518	143	11	cm‐1	cm‐1	PROPN
eurjchem-518	143	12	):	):	PUNCT
eurjchem-518	143	13	3444	3444	NUM
eurjchem-518	143	14	(	(	PUNCT
eurjchem-518	143	15	nh	nh	NOUN
eurjchem-518	143	16	)	)	PUNCT
eurjchem-518	143	17	,	,	PUNCT
eurjchem-518	143	18	2186	2186	NUM
eurjchem-518	143	19	(	(	PUNCT
eurjchem-518	143	20	c≡n	c≡n	PROPN
eurjchem-518	143	21	)	)	PUNCT
eurjchem-518	143	22	,	,	PUNCT
eurjchem-518	143	23	1681	1681	NUM
eurjchem-518	143	24	(	(	PUNCT
eurjchem-518	143	25	c	c	NOUN
eurjchem-518	143	26	=	=	NOUN
eurjchem-518	143	27	o	o	NOUN
eurjchem-518	143	28	)	)	PUNCT
eurjchem-518	143	29	.	.	PUNCT
eurjchem-518	144	1	1h	1h	NUM
eurjchem-518	144	2	nmr	nmr	NOUN
eurjchem-518	144	3	(	(	PUNCT
eurjchem-518	144	4	300	300	NUM
eurjchem-518	144	5	mhz	mhz	NOUN
eurjchem-518	144	6	,	,	PUNCT
eurjchem-518	144	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-518	144	8	,	,	PUNCT
eurjchem-518	144	9	δ	δ	PROPN
eurjchem-518	144	10	,	,	PUNCT
eurjchem-518	144	11	ppm	ppm	NUM
eurjchem-518	144	12	):	):	PUNCT
eurjchem-518	144	13	9.63	9.63	NUM
eurjchem-518	144	14	(	(	PUNCT
eurjchem-518	144	15	s	s	PROPN
eurjchem-518	144	16	,	,	PUNCT
eurjchem-518	144	17	1h	1h	NUM
eurjchem-518	144	18	,	,	PUNCT
eurjchem-518	144	19	oh	oh	INTJ
eurjchem-518	144	20	)	)	PUNCT
eurjchem-518	144	21	,	,	PUNCT
eurjchem-518	144	22	8.56	8.56	NUM
eurjchem-518	144	23	(	(	PUNCT
eurjchem-518	144	24	d	d	PROPN
eurjchem-518	144	25	,	,	PUNCT
eurjchem-518	144	26	1h	1h	NUM
eurjchem-518	144	27	,	,	PUNCT
eurjchem-518	144	28	j	j	PROPN
eurjchem-518	144	29	=	=	SYM
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eurjchem-518	144	31	hz	hz	ADJ
eurjchem-518	144	32	,	,	PUNCT
eurjchem-518	144	33	ar‐h	ar‐h	PROPN
eurjchem-518	144	34	)	)	PUNCT
eurjchem-518	144	35	,	,	PUNCT
eurjchem-518	144	36	7.8‐6.8	7.8‐6.8	NUM
eurjchem-518	144	37	(	(	PUNCT
eurjchem-518	144	38	m	m	PROPN
eurjchem-518	144	39	,	,	PUNCT
eurjchem-518	144	40	6h	6h	NUM
eurjchem-518	144	41	,	,	PUNCT
eurjchem-518	144	42	ar‐h	ar‐h	PROPN
eurjchem-518	144	43	)	)	PUNCT
eurjchem-518	144	44	,	,	PUNCT
eurjchem-518	144	45	5.9	5.9	NUM
eurjchem-518	144	46	(	(	PUNCT
eurjchem-518	144	47	s	s	PROPN
eurjchem-518	144	48	,	,	PUNCT
eurjchem-518	144	49	h	h	NOUN
eurjchem-518	144	50	,	,	PUNCT
eurjchem-518	144	51	benzylic	benzylic	ADJ
eurjchem-518	144	52	h	h	NOUN
eurjchem-518	144	53	)	)	PUNCT
eurjchem-518	144	54	.	.	PUNCT
eurjchem-518	145	1	anal	anal	PROPN
eurjchem-518	145	2	.	.	PUNCT
eurjchem-518	145	3	calcd	calcd	NOUN
eurjchem-518	145	4	.	.	PUNCT
eurjchem-518	146	1	for	for	ADP
eurjchem-518	146	2	c15h9cl2n3o	c15h9cl2n3o	PROPN
eurjchem-518	146	3	:	:	PUNCT
eurjchem-518	146	4	c	c	X
eurjchem-518	146	5	,	,	PUNCT
eurjchem-518	146	6	56.63	56.63	NUM
eurjchem-518	146	7	;	;	PUNCT
eurjchem-518	146	8	h	h	X
eurjchem-518	146	9	,	,	PUNCT
eurjchem-518	146	10	2.85	2.85	NUM
eurjchem-518	146	11	;	;	PUNCT
eurjchem-518	146	12	n	n	CCONJ
eurjchem-518	146	13	,	,	PUNCT
eurjchem-518	146	14	13.21	13.21	NUM
eurjchem-518	146	15	.	.	PUNCT
eurjchem-518	146	16	found	find	VERB
eurjchem-518	146	17	:	:	PUNCT
eurjchem-518	147	1	c	c	X
eurjchem-518	147	2	,	,	PUNCT
eurjchem-518	147	3	56.56	56.56	NUM
eurjchem-518	147	4	;	;	PUNCT
eurjchem-518	147	5	h	h	NOUN
eurjchem-518	147	6	,	,	PUNCT
eurjchem-518	147	7	2.93	2.93	NUM
eurjchem-518	147	8	;	;	PUNCT
eurjchem-518	147	9	n	n	CCONJ
eurjchem-518	147	10	,	,	PUNCT
eurjchem-518	147	11	13.21	13.21	NUM
eurjchem-518	147	12	%	%	NOUN
eurjchem-518	147	13	.	.	PUNCT
eurjchem-518	148	1	2.2.8	2.2.8	X
eurjchem-518	148	2	.	.	PUNCT
eurjchem-518	149	1	synthesis	synthesis	NOUN
eurjchem-518	149	2	of	of	ADP
eurjchem-518	149	3	compounds	compound	NOUN
eurjchem-518	149	4	16	16	NUM
eurjchem-518	149	5	and	and	CCONJ
eurjchem-518	149	6	17	17	NUM
eurjchem-518	149	7	thiosemicarbazide	thiosemicarbazide	NOUN
eurjchem-518	149	8	(	(	PUNCT
eurjchem-518	149	9	0.45	0.45	NUM
eurjchem-518	149	10	g	g	NOUN
eurjchem-518	149	11	,	,	PUNCT
eurjchem-518	149	12	0.005	0.005	NUM
eurjchem-518	149	13	mol	mol	NOUN
eurjchem-518	149	14	)	)	PUNCT
eurjchem-518	149	15	was	be	AUX
eurjchem-518	149	16	added	add	VERB
eurjchem-518	149	17	to	to	ADP
eurjchem-518	149	18	a	a	DET
eurjchem-518	149	19	solution	solution	NOUN
eurjchem-518	149	20	of	of	ADP
eurjchem-518	149	21	3	3	NUM
eurjchem-518	149	22	(	(	PUNCT
eurjchem-518	149	23	1.30	1.30	NUM
eurjchem-518	149	24	g	g	NOUN
eurjchem-518	149	25	,	,	PUNCT
eurjchem-518	149	26	0.005	0.005	NUM
eurjchem-518	149	27	mol	mol	NOUN
eurjchem-518	149	28	)	)	PUNCT
eurjchem-518	149	29	in	in	ADP
eurjchem-518	149	30	dioxane	dioxane	NOUN
eurjchem-518	149	31	(	(	PUNCT
eurjchem-518	149	32	20	20	NUM
eurjchem-518	149	33	ml	ml	NOUN
eurjchem-518	149	34	)	)	PUNCT
eurjchem-518	149	35	and	and	CCONJ
eurjchem-518	149	36	triethylamine	triethylamine	NOUN
eurjchem-518	149	37	(	(	PUNCT
eurjchem-518	149	38	0.505	0.505	NUM
eurjchem-518	149	39	g	g	NOUN
eurjchem-518	149	40	,	,	PUNCT
eurjchem-518	149	41	0.005	0.005	NUM
eurjchem-518	149	42	mol	mol	NOUN
eurjchem-518	149	43	)	)	PUNCT
eurjchem-518	149	44	.	.	PUNCT
eurjchem-518	150	1	the	the	DET
eurjchem-518	150	2	reaction	reaction	NOUN
eurjchem-518	150	3	mixture	mixture	NOUN
eurjchem-518	150	4	was	be	AUX
eurjchem-518	150	5	refluxed	refluxe	VERB
eurjchem-518	150	6	for	for	ADP
eurjchem-518	150	7	an	an	DET
eurjchem-518	150	8	hour	hour	NOUN
eurjchem-518	150	9	.	.	PUNCT
eurjchem-518	151	1	the	the	DET
eurjchem-518	151	2	solid	solid	ADJ
eurjchem-518	151	3	formed	form	VERB
eurjchem-518	151	4	was	be	AUX
eurjchem-518	151	5	ammonium	ammonium	NOUN
eurjchem-518	151	6	salt	salt	NOUN
eurjchem-518	151	7	,	,	PUNCT
eurjchem-518	151	8	the	the	DET
eurjchem-518	151	9	filtrate	filtrate	NOUN
eurjchem-518	151	10	was	be	AUX
eurjchem-518	151	11	concentrated	concentrate	VERB
eurjchem-518	151	12	,	,	PUNCT
eurjchem-518	151	13	and	and	CCONJ
eurjchem-518	151	14	the	the	DET
eurjchem-518	151	15	remaining	remain	VERB
eurjchem-518	151	16	semisolid	semisolid	NOUN
eurjchem-518	151	17	was	be	AUX
eurjchem-518	151	18	recrystallized	recrystallize	VERB
eurjchem-518	151	19	from	from	ADP
eurjchem-518	151	20	benzene	benzene	NOUN
eurjchem-518	151	21	to	to	PART
eurjchem-518	151	22	give	give	VERB
eurjchem-518	151	23	16	16	NUM
eurjchem-518	151	24	and	and	CCONJ
eurjchem-518	151	25	then	then	ADV
eurjchem-518	151	26	from	from	ADP
eurjchem-518	151	27	benzene	benzene	NOUN
eurjchem-518	151	28	/	/	SYM
eurjchem-518	151	29	ethanol	ethanol	NOUN
eurjchem-518	151	30	mixture	mixture	NOUN
eurjchem-518	151	31	to	to	PART
eurjchem-518	151	32	give	give	VERB
eurjchem-518	151	33	17	17	NUM
eurjchem-518	151	34	(	(	PUNCT
eurjchem-518	151	35	scheme	scheme	NOUN
eurjchem-518	151	36	3	3	NUM
eurjchem-518	151	37	)	)	PUNCT
eurjchem-518	151	38	1‐(2,4‐dichlorobenzylidene)thiosemicarbazide	1‐(2,4‐dichlorobenzylidene)thiosemicarbazide	NUM
eurjchem-518	151	39	(	(	PUNCT
eurjchem-518	151	40	16	16	NUM
eurjchem-518	151	41	)	)	PUNCT
eurjchem-518	151	42	the	the	DET
eurjchem-518	151	43	structure	structure	NOUN
eurjchem-518	151	44	was	be	AUX
eurjchem-518	151	45	confirmed	confirm	VERB
eurjchem-518	151	46	by	by	ADP
eurjchem-518	151	47	m.p	m.p	PROPN
eurjchem-518	151	48	.	.	PROPN
eurjchem-518	151	49	with	with	ADP
eurjchem-518	151	50	an	an	DET
eurjchem-518	151	51	authentic	authentic	ADJ
eurjchem-518	151	52	sample	sample	NOUN
eurjchem-518	151	53	[	[	X
eurjchem-518	151	54	15	15	NUM
eurjchem-518	151	55	]	]	PUNCT
eurjchem-518	151	56	.	.	PUNCT
eurjchem-518	152	1	4‐(2,4‐dichlorobenzylidene)‐3‐amino‐1h‐pyrazol‐5‐(4h)‐one	4‐(2,4‐dichlorobenzylidene)‐3‐amino‐1h‐pyrazol‐5‐(4h)‐one	NUM
eurjchem-518	152	2	(	(	PUNCT
eurjchem-518	152	3	17	17	NUM
eurjchem-518	152	4	):	):	PUNCT
eurjchem-518	152	5	reddish	reddish	ADJ
eurjchem-518	152	6	brown	brown	NOUN
eurjchem-518	152	7	.	.	PUNCT
eurjchem-518	153	1	yield	yield	NOUN
eurjchem-518	153	2	:	:	PUNCT
eurjchem-518	153	3	84	84	NUM
eurjchem-518	153	4	%	%	NOUN
eurjchem-518	153	5	.	.	PUNCT
eurjchem-518	154	1	m.p	m.p	PROPN
eurjchem-518	154	2	.	.	PROPN
eurjchem-518	154	3	:	:	PUNCT
eurjchem-518	155	1	150‐151	150‐151	NUM
eurjchem-518	155	2	oc	oc	PROPN
eurjchem-518	155	3	.	.	PUNCT
eurjchem-518	155	4	ft‐ir	ft‐ir	NOUN
eurjchem-518	155	5	(	(	PUNCT
eurjchem-518	155	6	kbr	kbr	PROPN
eurjchem-518	155	7	,	,	PUNCT
eurjchem-518	155	8	ν	ν	PROPN
eurjchem-518	155	9	,	,	PUNCT
eurjchem-518	155	10	cm‐1	cm‐1	PROPN
eurjchem-518	155	11	):	):	PUNCT
eurjchem-518	155	12	3179	3179	NUM
eurjchem-518	155	13	,	,	PUNCT
eurjchem-518	155	14	3263	3263	NUM
eurjchem-518	155	15	,	,	PUNCT
eurjchem-518	155	16	3369	3369	NUM
eurjchem-518	155	17	(	(	PUNCT
eurjchem-518	155	18	nh	nh	PROPN
eurjchem-518	155	19	,	,	PUNCT
eurjchem-518	155	20	nh2	nh2	PROPN
eurjchem-518	155	21	)	)	PUNCT
eurjchem-518	155	22	,	,	PUNCT
eurjchem-518	155	23	1645	1645	NUM
eurjchem-518	155	24	(	(	PUNCT
eurjchem-518	155	25	c	c	NOUN
eurjchem-518	155	26	=	=	NOUN
eurjchem-518	155	27	o	o	NOUN
eurjchem-518	155	28	)	)	PUNCT
eurjchem-518	155	29	,	,	PUNCT
eurjchem-518	155	30	1619(c	1619(c	NUM
eurjchem-518	155	31	=	=	SYM
eurjchem-518	155	32	n	n	NUM
eurjchem-518	155	33	)	)	PUNCT
eurjchem-518	155	34	.	.	PUNCT
eurjchem-518	156	1	1h	1h	NUM
eurjchem-518	156	2	nmr	nmr	NOUN
eurjchem-518	156	3	(	(	PUNCT
eurjchem-518	156	4	300	300	NUM
eurjchem-518	156	5	mhz	mhz	NOUN
eurjchem-518	156	6	,	,	PUNCT
eurjchem-518	156	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-518	156	8	,	,	PUNCT
eurjchem-518	156	9	δ	δ	PROPN
eurjchem-518	156	10	,	,	PUNCT
eurjchem-518	156	11	ppm	ppm	NUM
eurjchem-518	156	12	):	):	PUNCT
eurjchem-518	156	13	8.54	8.54	NUM
eurjchem-518	156	14	(	(	PUNCT
eurjchem-518	156	15	s	s	PROPN
eurjchem-518	156	16	,	,	PUNCT
eurjchem-518	156	17	1h	1h	NUM
eurjchem-518	156	18	,	,	PUNCT
eurjchem-518	156	19	nh	nh	PROPN
eurjchem-518	156	20	)	)	PUNCT
eurjchem-518	156	21	,	,	PUNCT
eurjchem-518	156	22	8.35	8.35	NUM
eurjchem-518	156	23	(	(	PUNCT
eurjchem-518	156	24	s	s	PROPN
eurjchem-518	156	25	,	,	PUNCT
eurjchem-518	156	26	1h	1h	NUM
eurjchem-518	156	27	,	,	PUNCT
eurjchem-518	156	28	=	=	NOUN
eurjchem-518	156	29	ch	ch	NOUN
eurjchem-518	156	30	)	)	PUNCT
eurjchem-518	156	31	,	,	PUNCT
eurjchem-518	156	32	7.4‐7.2	7.4‐7.2	NUM
eurjchem-518	156	33	(	(	PUNCT
eurjchem-518	156	34	m	m	PROPN
eurjchem-518	156	35	,	,	PUNCT
eurjchem-518	156	36	3h	3h	NUM
eurjchem-518	156	37	,	,	PUNCT
eurjchem-518	156	38	ar‐h	ar‐h	NOUN
eurjchem-518	156	39	)	)	PUNCT
eurjchem-518	156	40	,	,	PUNCT
eurjchem-518	156	41	4.4	4.4	NUM
eurjchem-518	156	42	(	(	PUNCT
eurjchem-518	156	43	s	s	PROPN
eurjchem-518	156	44	,	,	PUNCT
eurjchem-518	156	45	2h	2h	NUM
eurjchem-518	156	46	,	,	PUNCT
eurjchem-518	156	47	nh2	nh2	PROPN
eurjchem-518	156	48	)	)	PUNCT
eurjchem-518	156	49	.	.	PUNCT
eurjchem-518	157	1	anal	anal	PROPN
eurjchem-518	157	2	.	.	PUNCT
eurjchem-518	157	3	calcd	calcd	NOUN
eurjchem-518	157	4	.	.	PUNCT
eurjchem-518	158	1	for	for	SCONJ
eurjchem-518	158	2	c10h7cl2n3o	c10h7cl2n3o	NUM
eurjchem-518	158	3	:	:	PUNCT
eurjchem-518	158	4	c	c	X
eurjchem-518	158	5	,	,	PUNCT
eurjchem-518	158	6	46.90	46.90	NUM
eurjchem-518	158	7	;	;	PUNCT
eurjchem-518	158	8	h	h	NOUN
eurjchem-518	158	9	,	,	PUNCT
eurjchem-518	158	10	2.76	2.76	NUM
eurjchem-518	158	11	;	;	PUNCT
eurjchem-518	158	12	n	n	CCONJ
eurjchem-518	158	13	,	,	PUNCT
eurjchem-518	158	14	16.41	16.41	NUM
eurjchem-518	158	15	.	.	PUNCT
eurjchem-518	158	16	found	find	VERB
eurjchem-518	158	17	:	:	PUNCT
eurjchem-518	159	1	c	c	X
eurjchem-518	159	2	,	,	PUNCT
eurjchem-518	159	3	46.85	46.85	NUM
eurjchem-518	159	4	;	;	PUNCT
eurjchem-518	159	5	h	h	NOUN
eurjchem-518	159	6	,	,	PUNCT
eurjchem-518	159	7	2.71	2.71	NUM
eurjchem-518	159	8	;	;	PUNCT
eurjchem-518	159	9	n	n	CCONJ
eurjchem-518	159	10	,	,	PUNCT
eurjchem-518	159	11	16.38	16.38	NUM
eurjchem-518	159	12	%	%	NOUN
eurjchem-518	159	13	.	.	PUNCT
eurjchem-518	160	1	2.2.9	2.2.9	X
eurjchem-518	160	2	.	.	X
eurjchem-518	160	3	3‐(2,4‐dichlorophenyl)‐2‐(4,5‐dihydrooxazol‐2‐yl	3‐(2,4‐dichlorophenyl)‐2‐(4,5‐dihydrooxazol‐2‐yl	NUM
eurjchem-518	160	4	)	)	PUNCT
eurjchem-518	160	5	acrylonitrile	acrylonitrile	NOUN
eurjchem-518	160	6	(	(	PUNCT
eurjchem-518	160	7	18	18	NUM
eurjchem-518	160	8	)	)	PUNCT
eurjchem-518	160	9	a	a	DET
eurjchem-518	160	10	mixture	mixture	NOUN
eurjchem-518	160	11	of	of	ADP
eurjchem-518	160	12	3	3	NUM
eurjchem-518	160	13	(	(	PUNCT
eurjchem-518	160	14	1.30	1.30	NUM
eurjchem-518	160	15	g	g	NOUN
eurjchem-518	160	16	,	,	PUNCT
eurjchem-518	160	17	0.005	0.005	NUM
eurjchem-518	160	18	mol	mol	NOUN
eurjchem-518	160	19	)	)	PUNCT
eurjchem-518	160	20	,	,	PUNCT
eurjchem-518	160	21	triethylamine	triethylamine	NOUN
eurjchem-518	160	22	(	(	PUNCT
eurjchem-518	160	23	0.505	0.505	NUM
eurjchem-518	160	24	g	g	NOUN
eurjchem-518	160	25	,	,	PUNCT
eurjchem-518	160	26	0.005	0.005	NUM
eurjchem-518	160	27	mol	mol	NOUN
eurjchem-518	160	28	)	)	PUNCT
eurjchem-518	160	29	and	and	CCONJ
eurjchem-518	160	30	ethanolamine	ethanolamine	NOUN
eurjchem-518	160	31	(	(	PUNCT
eurjchem-518	160	32	0.305	0.305	NUM
eurjchem-518	160	33	g	g	NOUN
eurjchem-518	160	34	,	,	PUNCT
eurjchem-518	160	35	0.005	0.005	NUM
eurjchem-518	160	36	mol	mol	NOUN
eurjchem-518	160	37	)	)	PUNCT
eurjchem-518	160	38	in	in	ADP
eurjchem-518	160	39	dry	dry	ADJ
eurjchem-518	160	40	benzene	benzene	NOUN
eurjchem-518	160	41	(	(	PUNCT
eurjchem-518	160	42	50	50	NUM
eurjchem-518	160	43	ml	ml	NOUN
eurjchem-518	160	44	)	)	PUNCT
eurjchem-518	160	45	was	be	AUX
eurjchem-518	160	46	stirred	stir	VERB
eurjchem-518	160	47	for	for	ADP
eurjchem-518	160	48	2	2	NUM
eurjchem-518	160	49	hours	hour	NOUN
eurjchem-518	160	50	.	.	PUNCT
eurjchem-518	161	1	the	the	DET
eurjchem-518	161	2	separated	separate	VERB
eurjchem-518	161	3	solid	solid	ADJ
eurjchem-518	161	4	was	be	AUX
eurjchem-518	161	5	filtered	filter	VERB
eurjchem-518	161	6	,	,	PUNCT
eurjchem-518	161	7	washed	wash	VERB
eurjchem-518	161	8	with	with	ADP
eurjchem-518	161	9	water	water	NOUN
eurjchem-518	161	10	(	(	PUNCT
eurjchem-518	161	11	50	50	NUM
eurjchem-518	161	12	ml	ml	NOUN
eurjchem-518	161	13	)	)	PUNCT
eurjchem-518	161	14	,	,	PUNCT
eurjchem-518	161	15	dried	dry	VERB
eurjchem-518	161	16	and	and	CCONJ
eurjchem-518	161	17	recrystallized	recrystallize	VERB
eurjchem-518	161	18	from	from	ADP
eurjchem-518	161	19	ethanol	ethanol	NOUN
eurjchem-518	161	20	to	to	PART
eurjchem-518	161	21	give	give	VERB
eurjchem-518	161	22	18	18	NUM
eurjchem-518	161	23	(	(	PUNCT
eurjchem-518	161	24	scheme	scheme	NOUN
eurjchem-518	161	25	3	3	NUM
eurjchem-518	161	26	):	):	PUNCT
eurjchem-518	161	27	yellow	yellow	ADJ
eurjchem-518	161	28	.	.	PUNCT
eurjchem-518	162	1	yield	yield	NOUN
eurjchem-518	162	2	:	:	PUNCT
eurjchem-518	162	3	90	90	NUM
eurjchem-518	162	4	%	%	NOUN
eurjchem-518	162	5	.	.	PUNCT
eurjchem-518	163	1	m.p	m.p	PROPN
eurjchem-518	163	2	.	.	PROPN
eurjchem-518	163	3	:	:	PUNCT
eurjchem-518	164	1	220‐222	220‐222	NUM
eurjchem-518	164	2	oc	oc	PROPN
eurjchem-518	164	3	.	.	PUNCT
eurjchem-518	164	4	ft‐ir	ft‐ir	NOUN
eurjchem-518	164	5	(	(	PUNCT
eurjchem-518	164	6	kbr	kbr	PROPN
eurjchem-518	164	7	,	,	PUNCT
eurjchem-518	164	8	ν	ν	PROPN
eurjchem-518	164	9	,	,	PUNCT
eurjchem-518	164	10	cm‐1	cm‐1	PROPN
eurjchem-518	164	11	):	):	PUNCT
eurjchem-518	164	12	2209	2209	NUM
eurjchem-518	164	13	(	(	PUNCT
eurjchem-518	164	14	c≡n	c≡n	PROPN
eurjchem-518	164	15	)	)	PUNCT
eurjchem-518	164	16	,	,	PUNCT
eurjchem-518	164	17	1642	1642	NUM
eurjchem-518	164	18	(	(	PUNCT
eurjchem-518	164	19	c	c	NOUN
eurjchem-518	164	20	=	=	SYM
eurjchem-518	164	21	n	n	NUM
eurjchem-518	164	22	)	)	PUNCT
eurjchem-518	164	23	.	.	PUNCT
eurjchem-518	165	1	1h	1h	NUM
eurjchem-518	165	2	nmr	nmr	NOUN
eurjchem-518	165	3	(	(	PUNCT
eurjchem-518	165	4	300	300	NUM
eurjchem-518	165	5	mhz	mhz	NOUN
eurjchem-518	165	6	,	,	PUNCT
eurjchem-518	165	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-518	165	8	,	,	PUNCT
eurjchem-518	165	9	δ	δ	PROPN
eurjchem-518	165	10	,	,	PUNCT
eurjchem-518	165	11	ppm	ppm	NUM
eurjchem-518	165	12	):	):	PUNCT
eurjchem-518	165	13	7.77	7.77	NUM
eurjchem-518	165	14	(	(	PUNCT
eurjchem-518	165	15	s	s	PROPN
eurjchem-518	165	16	,	,	PUNCT
eurjchem-518	165	17	1h	1h	NUM
eurjchem-518	165	18	,	,	PUNCT
eurjchem-518	165	19	=	=	NOUN
eurjchem-518	165	20	ch	ch	NOUN
eurjchem-518	165	21	)	)	PUNCT
eurjchem-518	165	22	,	,	PUNCT
eurjchem-518	165	23	7.69‐7.40	7.69‐7.40	NUM
eurjchem-518	165	24	(	(	PUNCT
eurjchem-518	165	25	m	m	PROPN
eurjchem-518	165	26	,	,	PUNCT
eurjchem-518	165	27	3h	3h	NUM
eurjchem-518	165	28	,	,	PUNCT
eurjchem-518	165	29	ar‐h	ar‐h	NOUN
eurjchem-518	165	30	)	)	PUNCT
eurjchem-518	165	31	,	,	PUNCT
eurjchem-518	165	32	3.61	3.61	NUM
eurjchem-518	165	33	(	(	PUNCT
eurjchem-518	165	34	t	t	PROPN
eurjchem-518	165	35	,	,	PUNCT
eurjchem-518	165	36	2h	2h	NUM
eurjchem-518	165	37	,	,	PUNCT
eurjchem-518	165	38	j	j	PROPN
eurjchem-518	165	39	=	=	PROPN
eurjchem-518	165	40	6.90	6.90	NUM
eurjchem-518	165	41	hz	hz	NOUN
eurjchem-518	165	42	,	,	PUNCT
eurjchem-518	165	43	ch2‐o	ch2‐o	NOUN
eurjchem-518	165	44	)	)	PUNCT
eurjchem-518	165	45	,	,	PUNCT
eurjchem-518	165	46	1.84	1.84	NUM
eurjchem-518	165	47	(	(	PUNCT
eurjchem-518	165	48	t	t	PROPN
eurjchem-518	165	49	,	,	PUNCT
eurjchem-518	165	50	2h	2h	NUM
eurjchem-518	165	51	,	,	PUNCT
eurjchem-518	165	52	j	j	PROPN
eurjchem-518	165	53	=	=	PROPN
eurjchem-518	165	54	6.90	6.90	NUM
eurjchem-518	165	55	hz	hz	NOUN
eurjchem-518	165	56	,	,	PUNCT
eurjchem-518	165	57	n‐ch2	n‐ch2	PROPN
eurjchem-518	165	58	)	)	PUNCT
eurjchem-518	165	59	.	.	PUNCT
eurjchem-518	166	1	anal	anal	PROPN
eurjchem-518	166	2	.	.	PUNCT
eurjchem-518	166	3	calcd	calcd	NOUN
eurjchem-518	166	4	.	.	PUNCT
eurjchem-518	167	1	for	for	ADP
eurjchem-518	167	2	c12h8cl2n2o	c12h8cl2n2o	VERB
eurjchem-518	167	3	:	:	PUNCT
eurjchem-518	167	4	c	c	X
eurjchem-518	167	5	,	,	PUNCT
eurjchem-518	167	6	53.96	53.96	NUM
eurjchem-518	167	7	;	;	PUNCT
eurjchem-518	167	8	h	h	NOUN
eurjchem-518	167	9	,	,	PUNCT
eurjchem-518	167	10	3.02	3.02	NUM
eurjchem-518	167	11	;	;	PUNCT
eurjchem-518	167	12	n	n	CCONJ
eurjchem-518	167	13	,	,	PUNCT
eurjchem-518	167	14	10.49	10.49	NUM
eurjchem-518	167	15	.	.	PUNCT
eurjchem-518	167	16	found	find	VERB
eurjchem-518	167	17	:	:	PUNCT
eurjchem-518	168	1	c	c	X
eurjchem-518	168	2	,	,	PUNCT
eurjchem-518	168	3	53.89	53.89	NUM
eurjchem-518	168	4	;	;	PUNCT
eurjchem-518	169	1	h	h	NOUN
eurjchem-518	169	2	,	,	PUNCT
eurjchem-518	169	3	2.98	2.98	NUM
eurjchem-518	169	4	;	;	PUNCT
eurjchem-518	169	5	n	n	CCONJ
eurjchem-518	169	6	,	,	PUNCT
eurjchem-518	169	7	10.51	10.51	NUM
eurjchem-518	169	8	%	%	NOUN
eurjchem-518	169	9	.	.	PUNCT
eurjchem-518	170	1	2.2.10	2.2.10	NUM
eurjchem-518	170	2	.	.	PUNCT
eurjchem-518	171	1	2‐(2‐cyano‐3‐(2,4‐dichlorophenyl)acrylamido	2‐(2‐cyano‐3‐(2,4‐dichlorophenyl)acrylamido	NUM
eurjchem-518	171	2	)	)	PUNCT
eurjchem-518	171	3	benzoic	benzoic	NOUN
eurjchem-518	171	4	acid	acid	NOUN
eurjchem-518	171	5	(	(	PUNCT
eurjchem-518	171	6	19	19	NUM
eurjchem-518	171	7	)	)	PUNCT
eurjchem-518	171	8	a	a	DET
eurjchem-518	171	9	mixture	mixture	NOUN
eurjchem-518	171	10	of	of	ADP
eurjchem-518	171	11	3	3	NUM
eurjchem-518	171	12	(	(	PUNCT
eurjchem-518	171	13	2.60	2.60	NUM
eurjchem-518	171	14	g	g	NOUN
eurjchem-518	171	15	,	,	PUNCT
eurjchem-518	171	16	0.01	0.01	NUM
eurjchem-518	171	17	mol	mol	NOUN
eurjchem-518	171	18	)	)	PUNCT
eurjchem-518	171	19	,	,	PUNCT
eurjchem-518	171	20	triethylamine	triethylamine	NOUN
eurjchem-518	171	21	(	(	PUNCT
eurjchem-518	171	22	1.01	1.01	NUM
eurjchem-518	171	23	g	g	NOUN
eurjchem-518	171	24	,	,	PUNCT
eurjchem-518	171	25	0.01	0.01	NUM
eurjchem-518	171	26	mol	mol	NOUN
eurjchem-518	171	27	)	)	PUNCT
eurjchem-518	171	28	and	and	CCONJ
eurjchem-518	171	29	anthranilic	anthranilic	ADJ
eurjchem-518	171	30	acid	acid	NOUN
eurjchem-518	171	31	(	(	PUNCT
eurjchem-518	171	32	1.37	1.37	NUM
eurjchem-518	171	33	g	g	NOUN
eurjchem-518	171	34	,	,	PUNCT
eurjchem-518	171	35	0.01	0.01	NUM
eurjchem-518	171	36	mol	mol	NOUN
eurjchem-518	171	37	)	)	PUNCT
eurjchem-518	171	38	in	in	ADP
eurjchem-518	171	39	dry	dry	ADJ
eurjchem-518	171	40	benzene	benzene	NOUN
eurjchem-518	171	41	(	(	PUNCT
eurjchem-518	171	42	100	100	NUM
eurjchem-518	171	43	ml	ml	NOUN
eurjchem-518	171	44	)	)	PUNCT
eurjchem-518	171	45	was	be	AUX
eurjchem-518	171	46	refluxed	refluxe	VERB
eurjchem-518	171	47	for	for	ADP
eurjchem-518	171	48	an	an	DET
eurjchem-518	171	49	hour	hour	NOUN
eurjchem-518	171	50	.	.	PUNCT
eurjchem-518	172	1	the	the	DET
eurjchem-518	172	2	solid	solid	ADJ
eurjchem-518	172	3	separated	separate	VERB
eurjchem-518	172	4	was	be	AUX
eurjchem-518	172	5	filtered	filter	VERB
eurjchem-518	172	6	,	,	PUNCT
eurjchem-518	172	7	washed	wash	VERB
eurjchem-518	172	8	with	with	ADP
eurjchem-518	172	9	water	water	NOUN
eurjchem-518	172	10	(	(	PUNCT
eurjchem-518	172	11	100	100	NUM
eurjchem-518	172	12	ml	ml	NOUN
eurjchem-518	172	13	)	)	PUNCT
eurjchem-518	172	14	,	,	PUNCT
eurjchem-518	172	15	dried	dry	VERB
eurjchem-518	172	16	and	and	CCONJ
eurjchem-518	172	17	recrystallized	recrystallize	VERB
eurjchem-518	172	18	from	from	ADP
eurjchem-518	172	19	benzento	benzento	ADP
eurjchem-518	172	20	give	give	VERB
eurjchem-518	172	21	19	19	NUM
eurjchem-518	172	22	(	(	PUNCT
eurjchem-518	172	23	scheme	scheme	NOUN
eurjchem-518	172	24	3	3	NUM
eurjchem-518	172	25	):	):	PUNCT
eurjchem-518	172	26	brown	brown	ADJ
eurjchem-518	172	27	.	.	PUNCT
eurjchem-518	173	1	yield	yield	NOUN
eurjchem-518	173	2	:	:	PUNCT
eurjchem-518	173	3	84	84	NUM
eurjchem-518	173	4	%	%	NOUN
eurjchem-518	173	5	.	.	PUNCT
eurjchem-518	174	1	m.p	m.p	PROPN
eurjchem-518	174	2	.	.	PROPN
eurjchem-518	174	3	:	:	PUNCT
eurjchem-518	175	1	172‐173	172‐173	NUM
eurjchem-518	175	2	oc	oc	NOUN
eurjchem-518	175	3	.	.	PUNCT
eurjchem-518	175	4	ft‐ir	ft‐ir	NOUN
eurjchem-518	175	5	(	(	PUNCT
eurjchem-518	175	6	kbr	kbr	PROPN
eurjchem-518	175	7	,	,	PUNCT
eurjchem-518	175	8	ν	ν	PROPN
eurjchem-518	175	9	,	,	PUNCT
eurjchem-518	175	10	cm‐1	cm‐1	PROPN
eurjchem-518	175	11	):	):	PUNCT
eurjchem-518	175	12	3359	3359	NUM
eurjchem-518	175	13	(	(	PUNCT
eurjchem-518	175	14	nh	nh	NOUN
eurjchem-518	175	15	)	)	PUNCT
eurjchem-518	175	16	,	,	PUNCT
eurjchem-518	175	17	2220	2220	NUM
eurjchem-518	175	18	(	(	PUNCT
eurjchem-518	175	19	c≡n	c≡n	NOUN
eurjchem-518	175	20	)	)	PUNCT
eurjchem-518	175	21	,	,	PUNCT
eurjchem-518	175	22	1689	1689	NUM
eurjchem-518	175	23	(	(	PUNCT
eurjchem-518	175	24	c	c	NOUN
eurjchem-518	175	25	=	=	NOUN
eurjchem-518	175	26	o	o	NOUN
eurjchem-518	175	27	)	)	PUNCT
eurjchem-518	175	28	.	.	PUNCT
eurjchem-518	176	1	1h	1h	NUM
eurjchem-518	176	2	nmr	nmr	NOUN
eurjchem-518	176	3	(	(	PUNCT
eurjchem-518	176	4	300	300	NUM
eurjchem-518	176	5	mhz	mhz	NOUN
eurjchem-518	176	6	,	,	PUNCT
eurjchem-518	176	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-518	176	8	,	,	PUNCT
eurjchem-518	176	9	δ	δ	PROPN
eurjchem-518	176	10	,	,	PUNCT
eurjchem-518	176	11	ppm	ppm	NUM
eurjchem-518	176	12	):	):	PUNCT
eurjchem-518	176	13	10.75	10.75	NUM
eurjchem-518	176	14	(	(	PUNCT
eurjchem-518	176	15	s	s	PROPN
eurjchem-518	176	16	,	,	PUNCT
eurjchem-518	176	17	1h	1h	NUM
eurjchem-518	176	18	,	,	PUNCT
eurjchem-518	176	19	cooh	cooh	NOUN
eurjchem-518	176	20	)	)	PUNCT
eurjchem-518	176	21	,	,	PUNCT
eurjchem-518	176	22	8.39	8.39	NUM
eurjchem-518	176	23	(	(	PUNCT
eurjchem-518	176	24	s	s	PROPN
eurjchem-518	176	25	,	,	PUNCT
eurjchem-518	176	26	1h	1h	NUM
eurjchem-518	176	27	,	,	PUNCT
eurjchem-518	176	28	=	=	NOUN
eurjchem-518	176	29	ch	ch	NOUN
eurjchem-518	176	30	)	)	PUNCT
eurjchem-518	176	31	,	,	PUNCT
eurjchem-518	176	32	8.07‐7.94	8.07‐7.94	NUM
eurjchem-518	176	33	(	(	PUNCT
eurjchem-518	176	34	m	m	PROPN
eurjchem-518	176	35	,	,	PUNCT
eurjchem-518	176	36	4h	4h	NUM
eurjchem-518	176	37	,	,	PUNCT
eurjchem-518	176	38	ar‐h	ar‐h	PROPN
eurjchem-518	176	39	)	)	PUNCT
eurjchem-518	176	40	,	,	PUNCT
eurjchem-518	176	41	7.89	7.89	NUM
eurjchem-518	176	42	(	(	PUNCT
eurjchem-518	176	43	s	s	PROPN
eurjchem-518	176	44	,	,	PUNCT
eurjchem-518	176	45	1h	1h	NUM
eurjchem-518	176	46	,	,	PUNCT
eurjchem-518	176	47	nh	nh	PROPN
eurjchem-518	176	48	)	)	PUNCT
eurjchem-518	176	49	,	,	PUNCT
eurjchem-518	176	50	7.81‐7.62	7.81‐7.62	NUM
eurjchem-518	176	51	(	(	PUNCT
eurjchem-518	176	52	m	m	PROPN
eurjchem-518	176	53	,	,	PUNCT
eurjchem-518	176	54	3h	3h	NUM
eurjchem-518	176	55	,	,	PUNCT
eurjchem-518	176	56	ar‐h	ar‐h	NOUN
eurjchem-518	176	57	)	)	PUNCT
eurjchem-518	176	58	.	.	PUNCT
eurjchem-518	177	1	anal	anal	PROPN
eurjchem-518	177	2	.	.	PUNCT
eurjchem-518	177	3	calcd	calcd	NOUN
eurjchem-518	177	4	.	.	PUNCT
eurjchem-518	178	1	for	for	ADP
eurjchem-518	178	2	c17h10cl2n2o3	c17h10cl2n2o3	PROPN
eurjchem-518	178	3	:	:	PUNCT
eurjchem-518	178	4	c	c	X
eurjchem-518	178	5	,	,	PUNCT
eurjchem-518	178	6	56.53	56.53	NUM
eurjchem-518	178	7	;	;	PUNCT
eurjchem-518	178	8	h	h	NOUN
eurjchem-518	178	9	,	,	PUNCT
eurjchem-518	178	10	2.79	2.79	NUM
eurjchem-518	178	11	;	;	PUNCT
eurjchem-518	178	12	n	n	CCONJ
eurjchem-518	178	13	,	,	PUNCT
eurjchem-518	178	14	7.76	7.76	NUM
eurjchem-518	178	15	.	.	PUNCT
eurjchem-518	178	16	found	find	VERB
eurjchem-518	178	17	:	:	PUNCT
eurjchem-518	179	1	c	c	X
eurjchem-518	179	2	,	,	PUNCT
eurjchem-518	179	3	56.68	56.68	NUM
eurjchem-518	179	4	;	;	PUNCT
eurjchem-518	179	5	h	h	NOUN
eurjchem-518	179	6	,	,	PUNCT
eurjchem-518	179	7	2.82	2.82	NUM
eurjchem-518	179	8	;	;	PUNCT
eurjchem-518	179	9	n	n	CCONJ
eurjchem-518	179	10	,	,	PUNCT
eurjchem-518	179	11	7.68	7.68	NUM
eurjchem-518	179	12	%	%	NOUN
eurjchem-518	179	13	.	.	PUNCT
eurjchem-518	180	1	68	68	NUM
eurjchem-518	180	2	el‐ziaty	el‐ziaty	PROPN
eurjchem-518	180	3	et	et	PROPN
eurjchem-518	180	4	al	al	PROPN
eurjchem-518	180	5	.	.	PUNCT
eurjchem-518	180	6	/	/	SYM
eurjchem-518	180	7	european	european	PROPN
eurjchem-518	180	8	journal	journal	PROPN
eurjchem-518	180	9	of	of	ADP
eurjchem-518	180	10	chemistry	chemistry	NOUN
eurjchem-518	180	11	3	3	NUM
eurjchem-518	180	12	(	(	PUNCT
eurjchem-518	180	13	1	1	NUM
eurjchem-518	180	14	)	)	PUNCT
eurjchem-518	180	15	(	(	PUNCT
eurjchem-518	180	16	2012	2012	NUM
eurjchem-518	180	17	)	)	PUNCT
eurjchem-518	180	18	65‐70	65‐70	NOUN
eurjchem-518	181	1	n	n	PRON
eurjchem-518	181	2	h	h	NOUN
eurjchem-518	181	3	2	2	NUM
eurjchem-518	181	4	n	n	NUM
eurjchem-518	181	5	h	h	NOUN
eurjchem-518	181	6	c	c	NOUN
eurjchem-518	181	7	s	s	PART
eurjchem-518	181	8	n	n	VERB
eurjchem-518	181	9	h	h	NOUN
eurjchem-518	181	10	2	2	NUM
eurjchem-518	181	11	an	an	DET
eurjchem-518	181	12	th	th	X
eurjchem-518	181	13	ran	run	VERB
eurjchem-518	181	14	ilic	ilic	PROPN
eurjchem-518	181	15	acid	acid	PROPN
eurjchem-518	181	16	scheme	scheme	NOUN
eurjchem-518	181	17	3	3	NUM
eurjchem-518	181	18	2.2.11	2.2.11	NUM
eurjchem-518	181	19	.	.	PUNCT
eurjchem-518	182	1	3‐(2,4‐dichlorophenyl)‐2‐(4‐oxo‐4h‐benzo[d][1,3	3‐(2,4‐dichlorophenyl)‐2‐(4‐oxo‐4h‐benzo[d][1,3	NUM
eurjchem-518	182	2	]	]	X
eurjchem-518	182	3	oxazin‐2‐yl)acrylonitrile	oxazin‐2‐yl)acrylonitrile	PROPN
eurjchem-518	182	4	(	(	PUNCT
eurjchem-518	182	5	20	20	NUM
eurjchem-518	182	6	)	)	PUNCT
eurjchem-518	182	7	a	a	DET
eurjchem-518	182	8	mixture	mixture	NOUN
eurjchem-518	182	9	of	of	ADP
eurjchem-518	182	10	19	19	NUM
eurjchem-518	182	11	(	(	PUNCT
eurjchem-518	182	12	2	2	NUM
eurjchem-518	182	13	g	g	NOUN
eurjchem-518	182	14	)	)	PUNCT
eurjchem-518	182	15	and	and	CCONJ
eurjchem-518	182	16	freshly	freshly	ADV
eurjchem-518	182	17	distilled	distil	VERB
eurjchem-518	182	18	acetic	acetic	ADJ
eurjchem-518	182	19	anhydride	anhydride	NOUN
eurjchem-518	182	20	(	(	PUNCT
eurjchem-518	182	21	5	5	NUM
eurjchem-518	182	22	ml	ml	NOUN
eurjchem-518	182	23	)	)	PUNCT
eurjchem-518	182	24	was	be	AUX
eurjchem-518	182	25	heated	heat	VERB
eurjchem-518	182	26	on	on	ADP
eurjchem-518	182	27	a	a	DET
eurjchem-518	182	28	water	water	NOUN
eurjchem-518	182	29	bath	bath	NOUN
eurjchem-518	182	30	for	for	ADP
eurjchem-518	182	31	6	6	NUM
eurjchem-518	182	32	hours	hour	NOUN
eurjchem-518	182	33	.	.	PUNCT
eurjchem-518	183	1	after	after	ADP
eurjchem-518	183	2	cooling	cool	VERB
eurjchem-518	183	3	the	the	DET
eurjchem-518	183	4	solid	solid	ADJ
eurjchem-518	183	5	separated	separate	VERB
eurjchem-518	183	6	was	be	AUX
eurjchem-518	183	7	collected	collect	VERB
eurjchem-518	183	8	,	,	PUNCT
eurjchem-518	183	9	washed	wash	VERB
eurjchem-518	183	10	with	with	ADP
eurjchem-518	183	11	dry	dry	ADJ
eurjchem-518	183	12	petroleum	petroleum	NOUN
eurjchem-518	183	13	ether	ether	NOUN
eurjchem-518	183	14	(	(	PUNCT
eurjchem-518	183	15	40‐60	40‐60	NUM
eurjchem-518	183	16	oc	oc	PROPN
eurjchem-518	183	17	)	)	PUNCT
eurjchem-518	183	18	,	,	PUNCT
eurjchem-518	183	19	dried	dry	VERB
eurjchem-518	183	20	and	and	CCONJ
eurjchem-518	183	21	recrystallized	recrystallize	VERB
eurjchem-518	183	22	from	from	ADP
eurjchem-518	183	23	ethanol	ethanol	NOUN
eurjchem-518	183	24	to	to	PART
eurjchem-518	183	25	give	give	VERB
eurjchem-518	183	26	20	20	NUM
eurjchem-518	183	27	(	(	PUNCT
eurjchem-518	183	28	scheme	scheme	NOUN
eurjchem-518	183	29	3	3	NUM
eurjchem-518	183	30	):	):	PUNCT
eurjchem-518	183	31	green	green	ADJ
eurjchem-518	183	32	.	.	PUNCT
eurjchem-518	184	1	yield	yield	NOUN
eurjchem-518	184	2	:	:	PUNCT
eurjchem-518	184	3	85	85	NUM
eurjchem-518	184	4	%	%	NOUN
eurjchem-518	184	5	.	.	PUNCT
eurjchem-518	185	1	m.p	m.p	PROPN
eurjchem-518	185	2	.	.	PROPN
eurjchem-518	185	3	:	:	PUNCT
eurjchem-518	186	1	172‐173	172‐173	NUM
eurjchem-518	186	2	oc	oc	NOUN
eurjchem-518	186	3	.	.	PUNCT
eurjchem-518	186	4	ft‐ir	ft‐ir	NOUN
eurjchem-518	186	5	(	(	PUNCT
eurjchem-518	186	6	kbr	kbr	PROPN
eurjchem-518	186	7	,	,	PUNCT
eurjchem-518	186	8	ν	ν	PROPN
eurjchem-518	186	9	,	,	PUNCT
eurjchem-518	186	10	cm‐1	cm‐1	PROPN
eurjchem-518	186	11	):	):	PUNCT
eurjchem-518	186	12	2205	2205	NUM
eurjchem-518	186	13	(	(	PUNCT
eurjchem-518	186	14	c≡n	c≡n	PROPN
eurjchem-518	186	15	)	)	PUNCT
eurjchem-518	186	16	,	,	PUNCT
eurjchem-518	186	17	1758	1758	NUM
eurjchem-518	186	18	(	(	PUNCT
eurjchem-518	186	19	c	c	NOUN
eurjchem-518	186	20	=	=	NOUN
eurjchem-518	186	21	o	o	NOUN
eurjchem-518	186	22	)	)	PUNCT
eurjchem-518	186	23	.	.	PUNCT
eurjchem-518	187	1	1h	1h	NUM
eurjchem-518	187	2	nmr	nmr	NOUN
eurjchem-518	187	3	(	(	PUNCT
eurjchem-518	187	4	300	300	NUM
eurjchem-518	187	5	mhz	mhz	NOUN
eurjchem-518	187	6	,	,	PUNCT
eurjchem-518	187	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-518	187	8	,	,	PUNCT
eurjchem-518	187	9	δ	δ	PROPN
eurjchem-518	187	10	,	,	PUNCT
eurjchem-518	187	11	ppm	ppm	NUM
eurjchem-518	187	12	):	):	PUNCT
eurjchem-518	187	13	8.52	8.52	NUM
eurjchem-518	187	14	(	(	PUNCT
eurjchem-518	187	15	s	s	PROPN
eurjchem-518	187	16	,	,	PUNCT
eurjchem-518	187	17	1h	1h	NUM
eurjchem-518	187	18	,	,	PUNCT
eurjchem-518	187	19	=	=	NOUN
eurjchem-518	187	20	ch	ch	NOUN
eurjchem-518	187	21	)	)	PUNCT
eurjchem-518	187	22	,	,	PUNCT
eurjchem-518	187	23	8.21‐7.94	8.21‐7.94	NUM
eurjchem-518	187	24	(	(	PUNCT
eurjchem-518	187	25	m	m	PROPN
eurjchem-518	187	26	,	,	PUNCT
eurjchem-518	187	27	3h	3h	NUM
eurjchem-518	187	28	,	,	PUNCT
eurjchem-518	187	29	ar‐h	ar‐h	NOUN
eurjchem-518	187	30	)	)	PUNCT
eurjchem-518	187	31	,	,	PUNCT
eurjchem-518	187	32	7.93‐7.96	7.93‐7.96	NUM
eurjchem-518	187	33	(	(	PUNCT
eurjchem-518	187	34	m	m	PROPN
eurjchem-518	187	35	,	,	PUNCT
eurjchem-518	187	36	4h	4h	NOUN
eurjchem-518	187	37	,	,	PUNCT
eurjchem-518	187	38	ar‐h	ar‐h	PROPN
eurjchem-518	187	39	)	)	PUNCT
eurjchem-518	187	40	.	.	PUNCT
eurjchem-518	188	1	anal	anal	PROPN
eurjchem-518	188	2	.	.	PUNCT
eurjchem-518	188	3	calcd	calcd	NOUN
eurjchem-518	188	4	.	.	PUNCT
eurjchem-518	189	1	for	for	ADP
eurjchem-518	189	2	c17h8cl2n2o2	c17h8cl2n2o2	ADJ
eurjchem-518	189	3	:	:	PUNCT
eurjchem-518	189	4	c	c	NOUN
eurjchem-518	189	5	,	,	PUNCT
eurjchem-518	189	6	59.50	59.50	NUM
eurjchem-518	189	7	;	;	PUNCT
eurjchem-518	189	8	h	h	NOUN
eurjchem-518	189	9	,	,	PUNCT
eurjchem-518	189	10	2.35	2.35	NUM
eurjchem-518	189	11	;	;	PUNCT
eurjchem-518	189	12	n	n	CCONJ
eurjchem-518	189	13	,	,	PUNCT
eurjchem-518	189	14	8.16	8.16	NUM
eurjchem-518	189	15	.	.	PUNCT
eurjchem-518	189	16	found	find	VERB
eurjchem-518	189	17	:	:	PUNCT
eurjchem-518	190	1	c	c	X
eurjchem-518	190	2	,	,	PUNCT
eurjchem-518	190	3	60.01	60.01	NUM
eurjchem-518	190	4	;	;	PUNCT
eurjchem-518	190	5	h	h	NOUN
eurjchem-518	190	6	,	,	PUNCT
eurjchem-518	190	7	2.33	2.33	NUM
eurjchem-518	190	8	;	;	PUNCT
eurjchem-518	190	9	n	n	CCONJ
eurjchem-518	190	10	,	,	PUNCT
eurjchem-518	190	11	8.19	8.19	NUM
eurjchem-518	190	12	%	%	NOUN
eurjchem-518	190	13	.	.	PUNCT
eurjchem-518	191	1	2.2.12	2.2.12	X
eurjchem-518	191	2	.	.	PUNCT
eurjchem-518	191	3	2‐cyano‐3‐(2,4‐dichlorophenyl)‐n‐(2‐hydroxy	2‐cyano‐3‐(2,4‐dichlorophenyl)‐n‐(2‐hydroxy	NUM
eurjchem-518	191	4	phenyl	phenyl	NOUN
eurjchem-518	191	5	)	)	PUNCT
eurjchem-518	191	6	acrylamide	acrylamide	NOUN
eurjchem-518	191	7	(	(	PUNCT
eurjchem-518	191	8	21	21	NUM
eurjchem-518	191	9	)	)	PUNCT
eurjchem-518	191	10	a	a	DET
eurjchem-518	191	11	mixture	mixture	NOUN
eurjchem-518	191	12	of	of	ADP
eurjchem-518	191	13	3	3	NUM
eurjchem-518	191	14	(	(	PUNCT
eurjchem-518	191	15	1.30	1.30	NUM
eurjchem-518	191	16	g	g	NOUN
eurjchem-518	191	17	,	,	PUNCT
eurjchem-518	191	18	0.005	0.005	NUM
eurjchem-518	191	19	mol	mol	NOUN
eurjchem-518	191	20	)	)	PUNCT
eurjchem-518	191	21	,	,	PUNCT
eurjchem-518	191	22	triethylamine	triethylamine	NOUN
eurjchem-518	191	23	(	(	PUNCT
eurjchem-518	191	24	0.505	0.505	NUM
eurjchem-518	191	25	g	g	NOUN
eurjchem-518	191	26	,	,	PUNCT
eurjchem-518	191	27	0.005	0.005	NUM
eurjchem-518	191	28	mol	mol	NOUN
eurjchem-518	191	29	)	)	PUNCT
eurjchem-518	191	30	and	and	CCONJ
eurjchem-518	191	31	2‐amino	2‐amino	NUM
eurjchem-518	191	32	phenol	phenol	NOUN
eurjchem-518	191	33	(	(	PUNCT
eurjchem-518	191	34	0.54	0.54	NUM
eurjchem-518	191	35	g	g	NOUN
eurjchem-518	191	36	,	,	PUNCT
eurjchem-518	191	37	0.005	0.005	NUM
eurjchem-518	191	38	mol	mol	NOUN
eurjchem-518	191	39	)	)	PUNCT
eurjchem-518	191	40	in	in	ADP
eurjchem-518	191	41	dry	dry	ADJ
eurjchem-518	191	42	benzene	benzene	NOUN
eurjchem-518	191	43	(	(	PUNCT
eurjchem-518	191	44	50	50	NUM
eurjchem-518	191	45	ml	ml	NOUN
eurjchem-518	191	46	)	)	PUNCT
eurjchem-518	191	47	was	be	AUX
eurjchem-518	191	48	refluxed	refluxe	VERB
eurjchem-518	191	49	for	for	ADP
eurjchem-518	191	50	an	an	DET
eurjchem-518	191	51	hour	hour	NOUN
eurjchem-518	191	52	.	.	PUNCT
eurjchem-518	192	1	the	the	DET
eurjchem-518	192	2	solid	solid	ADJ
eurjchem-518	192	3	separated	separate	VERB
eurjchem-518	192	4	was	be	AUX
eurjchem-518	192	5	filtered	filter	VERB
eurjchem-518	192	6	,	,	PUNCT
eurjchem-518	192	7	washed	wash	VERB
eurjchem-518	192	8	with	with	ADP
eurjchem-518	192	9	water	water	NOUN
eurjchem-518	192	10	(	(	PUNCT
eurjchem-518	192	11	80	80	NUM
eurjchem-518	192	12	ml	ml	NOUN
eurjchem-518	192	13	)	)	PUNCT
eurjchem-518	192	14	,	,	PUNCT
eurjchem-518	192	15	dried	dry	VERB
eurjchem-518	192	16	and	and	CCONJ
eurjchem-518	192	17	recrystallized	recrystallize	VERB
eurjchem-518	192	18	from	from	ADP
eurjchem-518	192	19	toluene	toluene	NOUN
eurjchem-518	192	20	to	to	PART
eurjchem-518	192	21	give	give	VERB
eurjchem-518	192	22	21	21	NUM
eurjchem-518	192	23	(	(	PUNCT
eurjchem-518	192	24	scheme	scheme	NOUN
eurjchem-518	192	25	3	3	NUM
eurjchem-518	192	26	)	)	PUNCT
eurjchem-518	192	27	yellow	yellow	ADJ
eurjchem-518	192	28	.	.	PUNCT
eurjchem-518	193	1	yield	yield	NOUN
eurjchem-518	193	2	:	:	PUNCT
eurjchem-518	193	3	92	92	NUM
eurjchem-518	193	4	%	%	NOUN
eurjchem-518	193	5	.	.	PUNCT
eurjchem-518	194	1	m.p	m.p	PROPN
eurjchem-518	194	2	.	.	PROPN
eurjchem-518	194	3	:	:	PUNCT
eurjchem-518	195	1	108‐110	108‐110	NUM
eurjchem-518	195	2	oc	oc	NOUN
eurjchem-518	195	3	.	.	PUNCT
eurjchem-518	195	4	ft‐ir	ft‐ir	NOUN
eurjchem-518	195	5	(	(	PUNCT
eurjchem-518	195	6	kbr	kbr	PROPN
eurjchem-518	195	7	,	,	PUNCT
eurjchem-518	195	8	ν	ν	PROPN
eurjchem-518	195	9	,	,	PUNCT
eurjchem-518	195	10	cm‐1	cm‐1	PROPN
eurjchem-518	195	11	):	):	PUNCT
eurjchem-518	195	12	3247	3247	NUM
eurjchem-518	195	13	,	,	PUNCT
eurjchem-518	195	14	3353	3353	NUM
eurjchem-518	195	15	(	(	PUNCT
eurjchem-518	195	16	nh	nh	NOUN
eurjchem-518	195	17	)	)	PUNCT
eurjchem-518	195	18	,	,	PUNCT
eurjchem-518	195	19	2213	2213	NUM
eurjchem-518	195	20	(	(	PUNCT
eurjchem-518	195	21	c≡n	c≡n	PROPN
eurjchem-518	195	22	)	)	PUNCT
eurjchem-518	195	23	,	,	PUNCT
eurjchem-518	195	24	1669	1669	NUM
eurjchem-518	195	25	(	(	PUNCT
eurjchem-518	195	26	c	c	NOUN
eurjchem-518	195	27	=	=	NOUN
eurjchem-518	195	28	o	o	NOUN
eurjchem-518	195	29	)	)	PUNCT
eurjchem-518	195	30	.	.	PUNCT
eurjchem-518	196	1	1h	1h	NUM
eurjchem-518	196	2	nmr	nmr	NOUN
eurjchem-518	196	3	(	(	PUNCT
eurjchem-518	196	4	300	300	NUM
eurjchem-518	196	5	mhz	mhz	NOUN
eurjchem-518	196	6	,	,	PUNCT
eurjchem-518	196	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-518	196	8	,	,	PUNCT
eurjchem-518	196	9	δ	δ	PROPN
eurjchem-518	196	10	,	,	PUNCT
eurjchem-518	196	11	ppm	ppm	NOUN
eurjchem-518	196	12	):	):	PUNCT
eurjchem-518	196	13	10.15	10.15	NUM
eurjchem-518	196	14	(	(	PUNCT
eurjchem-518	196	15	s	s	PROPN
eurjchem-518	196	16	,	,	PUNCT
eurjchem-518	196	17	1h	1h	NUM
eurjchem-518	196	18	,	,	PUNCT
eurjchem-518	196	19	nh	nh	PROPN
eurjchem-518	196	20	)	)	PUNCT
eurjchem-518	196	21	,	,	PUNCT
eurjchem-518	196	22	9.4	9.4	NUM
eurjchem-518	196	23	(	(	PUNCT
eurjchem-518	196	24	s	s	PROPN
eurjchem-518	196	25	,	,	PUNCT
eurjchem-518	196	26	1h	1h	NUM
eurjchem-518	196	27	,	,	PUNCT
eurjchem-518	196	28	oh	oh	INTJ
eurjchem-518	196	29	)	)	PUNCT
eurjchem-518	196	30	,	,	PUNCT
eurjchem-518	196	31	8.43	8.43	NUM
eurjchem-518	196	32	(	(	PUNCT
eurjchem-518	196	33	s	s	PROPN
eurjchem-518	196	34	,	,	PUNCT
eurjchem-518	196	35	1h	1h	NUM
eurjchem-518	196	36	,	,	PUNCT
eurjchem-518	196	37	=	=	NOUN
eurjchem-518	196	38	ch	ch	NOUN
eurjchem-518	196	39	)	)	PUNCT
eurjchem-518	196	40	,	,	PUNCT
eurjchem-518	196	41	8.10‐6.80	8.10‐6.80	NUM
eurjchem-518	196	42	(	(	PUNCT
eurjchem-518	196	43	m	m	PROPN
eurjchem-518	196	44	,	,	PUNCT
eurjchem-518	196	45	7h	7h	PROPN
eurjchem-518	196	46	,	,	PUNCT
eurjchem-518	196	47	ar‐h	ar‐h	NOUN
eurjchem-518	196	48	)	)	PUNCT
eurjchem-518	196	49	.	.	PUNCT
eurjchem-518	197	1	anal	anal	PROPN
eurjchem-518	197	2	.	.	PUNCT
eurjchem-518	197	3	calcd	calcd	NOUN
eurjchem-518	197	4	.	.	PUNCT
eurjchem-518	198	1	for	for	SCONJ
eurjchem-518	198	2	c16h10cl2n2o2	c16h10cl2n2o2	NOUN
eurjchem-518	198	3	:	:	PUNCT
eurjchem-518	198	4	c	c	X
eurjchem-518	198	5	,	,	PUNCT
eurjchem-518	198	6	57.68	57.68	NUM
eurjchem-518	198	7	;	;	PUNCT
eurjchem-518	198	8	h	h	NOUN
eurjchem-518	198	9	,	,	PUNCT
eurjchem-518	198	10	3.03	3.03	NUM
eurjchem-518	198	11	;	;	PUNCT
eurjchem-518	198	12	n	n	CCONJ
eurjchem-518	198	13	,	,	PUNCT
eurjchem-518	198	14	8.41	8.41	NUM
eurjchem-518	198	15	.	.	PUNCT
eurjchem-518	198	16	found	find	VERB
eurjchem-518	198	17	:	:	PUNCT
eurjchem-518	199	1	c	c	X
eurjchem-518	199	2	,	,	PUNCT
eurjchem-518	199	3	57.56	57.56	NUM
eurjchem-518	199	4	;	;	PUNCT
eurjchem-518	200	1	h	h	NOUN
eurjchem-518	200	2	,	,	PUNCT
eurjchem-518	200	3	2.98	2.98	NUM
eurjchem-518	200	4	;	;	PUNCT
eurjchem-518	200	5	n	n	CCONJ
eurjchem-518	200	6	,	,	PUNCT
eurjchem-518	200	7	8.32	8.32	NUM
eurjchem-518	200	8	%	%	NOUN
eurjchem-518	200	9	.	.	PUNCT
eurjchem-518	201	1	2.2.13	2.2.13	NUM
eurjchem-518	201	2	.	.	NOUN
eurjchem-518	201	3	2‐(benzo[d]oxazol‐2‐yl)‐3‐(2,4‐dichlorophenyl	2‐(benzo[d]oxazol‐2‐yl)‐3‐(2,4‐dichlorophenyl	X
eurjchem-518	201	4	)	)	PUNCT
eurjchem-518	201	5	acrylonitrile	acrylonitrile	NOUN
eurjchem-518	201	6	(	(	PUNCT
eurjchem-518	201	7	22	22	NUM
eurjchem-518	201	8	)	)	PUNCT
eurjchem-518	201	9	a	a	DET
eurjchem-518	201	10	mixture	mixture	NOUN
eurjchem-518	201	11	of	of	ADP
eurjchem-518	201	12	21	21	NUM
eurjchem-518	201	13	(	(	PUNCT
eurjchem-518	201	14	1	1	NUM
eurjchem-518	201	15	g	g	NOUN
eurjchem-518	201	16	)	)	PUNCT
eurjchem-518	201	17	and	and	CCONJ
eurjchem-518	201	18	phosphorus	phosphorus	NOUN
eurjchem-518	201	19	oxychloride	oxychloride	NOUN
eurjchem-518	201	20	(	(	PUNCT
eurjchem-518	201	21	10	10	NUM
eurjchem-518	201	22	ml	ml	NOUN
eurjchem-518	201	23	)	)	PUNCT
eurjchem-518	201	24	was	be	AUX
eurjchem-518	201	25	heated	heat	VERB
eurjchem-518	201	26	on	on	ADP
eurjchem-518	201	27	water	water	NOUN
eurjchem-518	201	28	bath	bath	NOUN
eurjchem-518	201	29	for	for	ADP
eurjchem-518	201	30	6	6	NUM
eurjchem-518	201	31	hours	hour	NOUN
eurjchem-518	201	32	.	.	PUNCT
eurjchem-518	202	1	after	after	ADP
eurjchem-518	202	2	cooling	cool	VERB
eurjchem-518	202	3	the	the	DET
eurjchem-518	202	4	reaction	reaction	NOUN
eurjchem-518	202	5	mixture	mixture	NOUN
eurjchem-518	202	6	was	be	AUX
eurjchem-518	202	7	poured	pour	VERB
eurjchem-518	202	8	on	on	ADP
eurjchem-518	202	9	crushed	crush	VERB
eurjchem-518	202	10	ice	ice	NOUN
eurjchem-518	202	11	(	(	PUNCT
eurjchem-518	202	12	20	20	NUM
eurjchem-518	202	13	g	g	NOUN
eurjchem-518	202	14	)	)	PUNCT
eurjchem-518	202	15	.	.	PUNCT
eurjchem-518	203	1	the	the	DET
eurjchem-518	203	2	solid	solid	ADJ
eurjchem-518	203	3	separated	separate	VERB
eurjchem-518	203	4	was	be	AUX
eurjchem-518	203	5	filtered	filter	VERB
eurjchem-518	203	6	,	,	PUNCT
eurjchem-518	203	7	washed	wash	VERB
eurjchem-518	203	8	with	with	ADP
eurjchem-518	203	9	water	water	NOUN
eurjchem-518	203	10	(	(	PUNCT
eurjchem-518	203	11	50	50	NUM
eurjchem-518	203	12	ml	ml	NOUN
eurjchem-518	203	13	)	)	PUNCT
eurjchem-518	203	14	,	,	PUNCT
eurjchem-518	203	15	dried	dry	VERB
eurjchem-518	203	16	and	and	CCONJ
eurjchem-518	203	17	recrystallized	recrystallize	VERB
eurjchem-518	203	18	from	from	ADP
eurjchem-518	203	19	ethanol	ethanol	NOUN
eurjchem-518	203	20	to	to	PART
eurjchem-518	203	21	give	give	VERB
eurjchem-518	203	22	22	22	NUM
eurjchem-518	203	23	(	(	PUNCT
eurjchem-518	203	24	scheme	scheme	NOUN
eurjchem-518	203	25	3	3	NUM
eurjchem-518	203	26	)	)	PUNCT
eurjchem-518	203	27	.	.	PUNCT
eurjchem-518	204	1	green	green	ADJ
eurjchem-518	204	2	.	.	PUNCT
eurjchem-518	204	3	yield	yield	NOUN
eurjchem-518	204	4	:	:	PUNCT
eurjchem-518	204	5	82	82	NUM
eurjchem-518	204	6	%	%	NOUN
eurjchem-518	204	7	.	.	PUNCT
eurjchem-518	205	1	m.p	m.p	PROPN
eurjchem-518	205	2	.	.	PROPN
eurjchem-518	205	3	:	:	PUNCT
eurjchem-518	206	1	150‐152	150‐152	NUM
eurjchem-518	206	2	oc	oc	NOUN
eurjchem-518	206	3	.	.	PUNCT
eurjchem-518	206	4	ft‐ir	ft‐ir	NOUN
eurjchem-518	206	5	(	(	PUNCT
eurjchem-518	206	6	kbr	kbr	PROPN
eurjchem-518	206	7	,	,	PUNCT
eurjchem-518	206	8	ν	ν	PROPN
eurjchem-518	206	9	,	,	PUNCT
eurjchem-518	206	10	cm‐1	cm‐1	PROPN
eurjchem-518	206	11	):	):	PUNCT
eurjchem-518	206	12	2205	2205	NUM
eurjchem-518	206	13	(	(	PUNCT
eurjchem-518	206	14	c≡n	c≡n	PROPN
eurjchem-518	206	15	)	)	PUNCT
eurjchem-518	206	16	and	and	CCONJ
eurjchem-518	206	17	1622	1622	NUM
eurjchem-518	206	18	(	(	PUNCT
eurjchem-518	206	19	c	c	NOUN
eurjchem-518	206	20	=	=	SYM
eurjchem-518	206	21	n	n	CCONJ
eurjchem-518	206	22	)	)	PUNCT
eurjchem-518	206	23	1h	1h	NUM
eurjchem-518	206	24	nmr	nmr	NOUN
eurjchem-518	206	25	(	(	PUNCT
eurjchem-518	206	26	300	300	NUM
eurjchem-518	206	27	mhz	mhz	NOUN
eurjchem-518	206	28	,	,	PUNCT
eurjchem-518	206	29	dmso‐d6	dmso‐d6	PROPN
eurjchem-518	206	30	,	,	PUNCT
eurjchem-518	206	31	δ	δ	PROPN
eurjchem-518	206	32	,	,	PUNCT
eurjchem-518	206	33	ppm	ppm	NUM
eurjchem-518	206	34	):	):	PUNCT
eurjchem-518	206	35	8.6‐7.8	8.6‐7.8	NUM
eurjchem-518	206	36	(	(	PUNCT
eurjchem-518	206	37	m	m	PROPN
eurjchem-518	206	38	,	,	PUNCT
eurjchem-518	206	39	3h	3h	NUM
eurjchem-518	206	40	,	,	PUNCT
eurjchem-518	206	41	ar‐h	ar‐h	NOUN
eurjchem-518	206	42	)	)	PUNCT
eurjchem-518	206	43	,	,	PUNCT
eurjchem-518	206	44	7.43‐	7.43‐	NOUN
eurjchem-518	206	45	7.40	7.40	NUM
eurjchem-518	206	46	(	(	PUNCT
eurjchem-518	206	47	m	m	PROPN
eurjchem-518	206	48	,	,	PUNCT
eurjchem-518	206	49	4h	4h	NUM
eurjchem-518	206	50	,	,	PUNCT
eurjchem-518	206	51	ar‐h	ar‐h	PROPN
eurjchem-518	206	52	)	)	PUNCT
eurjchem-518	206	53	,	,	PUNCT
eurjchem-518	206	54	7.25	7.25	NUM
eurjchem-518	206	55	(	(	PUNCT
eurjchem-518	206	56	s	s	PROPN
eurjchem-518	206	57	,	,	PUNCT
eurjchem-518	206	58	1h	1h	NUM
eurjchem-518	206	59	,	,	PUNCT
eurjchem-518	206	60	=	=	NOUN
eurjchem-518	206	61	ch	ch	NOUN
eurjchem-518	206	62	)	)	PUNCT
eurjchem-518	206	63	.	.	PUNCT
eurjchem-518	207	1	anal	anal	PROPN
eurjchem-518	207	2	.	.	PUNCT
eurjchem-518	207	3	calcd	calcd	NOUN
eurjchem-518	207	4	.	.	PUNCT
eurjchem-518	208	1	for	for	ADP
eurjchem-518	208	2	c16h8cl2n2o	c16h8cl2n2o	VERB
eurjchem-518	208	3	:	:	PUNCT
eurjchem-518	208	4	c	c	X
eurjchem-518	208	5	,	,	PUNCT
eurjchem-518	208	6	60.98	60.98	NUM
eurjchem-518	208	7	;	;	PUNCT
eurjchem-518	208	8	h	h	NOUN
eurjchem-518	208	9	,	,	PUNCT
eurjchem-518	208	10	2.56	2.56	NUM
eurjchem-518	208	11	;	;	PUNCT
eurjchem-518	208	12	n	n	CCONJ
eurjchem-518	208	13	,	,	PUNCT
eurjchem-518	208	14	8.89	8.89	NUM
eurjchem-518	208	15	.	.	PUNCT
eurjchem-518	208	16	found	find	VERB
eurjchem-518	208	17	:	:	PUNCT
eurjchem-518	209	1	c	c	X
eurjchem-518	209	2	,	,	PUNCT
eurjchem-518	209	3	60.86	60.86	NUM
eurjchem-518	209	4	;	;	PUNCT
eurjchem-518	209	5	h	h	X
eurjchem-518	209	6	,	,	PUNCT
eurjchem-518	209	7	2.51	2.51	NUM
eurjchem-518	209	8	;	;	PUNCT
eurjchem-518	209	9	n	n	CCONJ
eurjchem-518	209	10	,	,	PUNCT
eurjchem-518	209	11	8.81	8.81	NUM
eurjchem-518	209	12	%	%	NOUN
eurjchem-518	209	13	.	.	PUNCT
eurjchem-518	210	1	2.3	2.3	NUM
eurjchem-518	210	2	.	.	PUNCT
eurjchem-518	211	1	antimicrobial	antimicrobial	ADJ
eurjchem-518	211	2	and	and	CCONJ
eurjchem-518	211	3	antifungal	antifungal	ADJ
eurjchem-518	211	4	activities	activity	NOUN
eurjchem-518	211	5	a	a	DET
eurjchem-518	211	6	filter	filter	NOUN
eurjchem-518	211	7	paper	paper	NOUN
eurjchem-518	211	8	sterilized	sterilize	VERB
eurjchem-518	211	9	disc	disc	NOUN
eurjchem-518	211	10	saturated	saturate	VERB
eurjchem-518	211	11	with	with	ADP
eurjchem-518	211	12	measured	measured	ADJ
eurjchem-518	211	13	quantity	quantity	NOUN
eurjchem-518	211	14	of	of	ADP
eurjchem-518	211	15	the	the	DET
eurjchem-518	211	16	sample	sample	NOUN
eurjchem-518	211	17	with	with	ADP
eurjchem-518	211	18	concentration	concentration	NOUN
eurjchem-518	211	19	of	of	ADP
eurjchem-518	211	20	20	20	NUM
eurjchem-518	211	21	mg	mg	NUM
eurjchem-518	211	22	/	/	SYM
eurjchem-518	211	23	ml	ml	PROPN
eurjchem-518	211	24	was	be	AUX
eurjchem-518	211	25	placed	place	VERB
eurjchem-518	211	26	on	on	ADP
eurjchem-518	211	27	a	a	DET
eurjchem-518	211	28	plate	plate	NOUN
eurjchem-518	211	29	containing	contain	VERB
eurjchem-518	211	30	solid	solid	ADJ
eurjchem-518	211	31	bacterial	bacterial	ADJ
eurjchem-518	211	32	medium	medium	NOUN
eurjchem-518	211	33	(	(	PUNCT
eurjchem-518	211	34	nutrient	nutrient	NOUN
eurjchem-518	211	35	agar	agar	NOUN
eurjchem-518	211	36	broth	broth	NOUN
eurjchem-518	211	37	)	)	PUNCT
eurjchem-518	211	38	or	or	CCONJ
eurjchem-518	211	39	fungal	fungal	ADJ
eurjchem-518	211	40	medium	medium	NOUN
eurjchem-518	211	41	(	(	PUNCT
eurjchem-518	211	42	dox	dox	NOUN
eurjchem-518	211	43	’s	’s	PART
eurjchem-518	211	44	medium	medium	NOUN
eurjchem-518	211	45	)	)	PUNCT
eurjchem-518	211	46	which	which	PRON
eurjchem-518	211	47	was	be	AUX
eurjchem-518	211	48	heavily	heavily	ADV
eurjchem-518	211	49	seeded	seeded	ADJ
eurjchem-518	211	50	with	with	ADP
eurjchem-518	211	51	the	the	DET
eurjchem-518	211	52	spore	spore	ADJ
eurjchem-518	211	53	suspension	suspension	NOUN
eurjchem-518	211	54	of	of	ADP
eurjchem-518	211	55	the	the	DET
eurjchem-518	211	56	tested	test	VERB
eurjchem-518	211	57	organism	organism	NOUN
eurjchem-518	211	58	.	.	PUNCT
eurjchem-518	212	1	after	after	ADP
eurjchem-518	212	2	incubation	incubation	NOUN
eurjchem-518	212	3	,	,	PUNCT
eurjchem-518	212	4	the	the	DET
eurjchem-518	212	5	diameter	diameter	NOUN
eurjchem-518	212	6	of	of	ADP
eurjchem-518	212	7	the	the	DET
eurjchem-518	212	8	clear	clear	ADJ
eurjchem-518	212	9	zone	zone	NOUN
eurjchem-518	212	10	of	of	ADP
eurjchem-518	212	11	inhibition	inhibition	NOUN
eurjchem-518	212	12	surrounding	surround	VERB
eurjchem-518	212	13	the	the	DET
eurjchem-518	212	14	sample	sample	NOUN
eurjchem-518	212	15	was	be	AUX
eurjchem-518	212	16	taken	take	VERB
eurjchem-518	212	17	as	as	ADP
eurjchem-518	212	18	a	a	DET
eurjchem-518	212	19	measure	measure	NOUN
eurjchem-518	212	20	of	of	ADP
eurjchem-518	212	21	the	the	DET
eurjchem-518	212	22	inhibitory	inhibitory	ADJ
eurjchem-518	212	23	power	power	NOUN
eurjchem-518	212	24	of	of	ADP
eurjchem-518	212	25	the	the	DET
eurjchem-518	212	26	sample	sample	NOUN
eurjchem-518	212	27	against	against	ADP
eurjchem-518	212	28	the	the	DET
eurjchem-518	212	29	particular	particular	ADJ
eurjchem-518	212	30	test	test	NOUN
eurjchem-518	212	31	organism	organism	NOUN
eurjchem-518	212	32	[	[	X
eurjchem-518	212	33	16‐19	16‐19	NUM
eurjchem-518	212	34	]	]	PUNCT
eurjchem-518	212	35	.	.	PUNCT
eurjchem-518	213	1	the	the	DET
eurjchem-518	213	2	selected	select	VERB
eurjchem-518	213	3	samples	sample	NOUN
eurjchem-518	213	4	were	be	AUX
eurjchem-518	213	5	screened	screen	VERB
eurjchem-518	213	6	against	against	ADP
eurjchem-518	213	7	gram‐positive	gram‐positive	ADJ
eurjchem-518	213	8	;	;	PUNCT
eurjchem-518	213	9	staphylococcus	staphylococcus	NOUN
eurjchem-518	213	10	aureus	aureus	PROPN
eurjchem-518	213	11	and	and	CCONJ
eurjchem-518	213	12	gram‐negative	gram‐negative	PROPN
eurjchem-518	213	13	escherichia	escherichia	NOUN
eurjchem-518	213	14	coli	coli	NOUN
eurjchem-518	213	15	.	.	PUNCT
eurjchem-518	214	1	antifungal	antifungal	ADJ
eurjchem-518	214	2	activity	activity	NOUN
eurjchem-518	214	3	was	be	AUX
eurjchem-518	214	4	tested	test	VERB
eurjchem-518	214	5	using	use	VERB
eurjchem-518	214	6	aspergillus	aspergillus	ADJ
eurjchem-518	214	7	flavus	flavus	NOUN
eurjchem-518	214	8	and	and	CCONJ
eurjchem-518	214	9	candida	candida	NOUN
eurjchem-518	214	10	albicans	albican	NOUN
eurjchem-518	214	11	(	(	PUNCT
eurjchem-518	214	12	table	table	NOUN
eurjchem-518	214	13	1	1	NUM
eurjchem-518	214	14	)	)	PUNCT
eurjchem-518	214	15	.	.	PUNCT
eurjchem-518	215	1	table	table	NOUN
eurjchem-518	215	2	1	1	NUM
eurjchem-518	215	3	.	.	PUNCT
eurjchem-518	216	1	the	the	DET
eurjchem-518	216	2	antimicrobial	antimicrobial	ADJ
eurjchem-518	216	3	and	and	CCONJ
eurjchem-518	216	4	antifungal	antifungal	ADJ
eurjchem-518	216	5	activities	activity	NOUN
eurjchem-518	216	6	of	of	ADP
eurjchem-518	216	7	the	the	DET
eurjchem-518	216	8	selected	select	VERB
eurjchem-518	216	9	compounds	compound	NOUN
eurjchem-518	216	10	*	*	NOUN
eurjchem-518	216	11	.	.	PUNCT
eurjchem-518	217	1	sample	sample	NOUN
eurjchem-518	217	2	escherichia	escherichia	NOUN
eurjchem-518	217	3	coli	coli	NOUN
eurjchem-518	217	4	staphylococcus	staphylococcus	NOUN
eurjchem-518	217	5	aureus	aureus	NOUN
eurjchem-518	217	6	aspergillus	aspergillus	NOUN
eurjchem-518	217	7	flavus	flavus	NOUN
eurjchem-518	217	8	candida	candida	NOUN
eurjchem-518	217	9	albicans	albican	VERB
eurjchem-518	217	10	4	4	NUM
eurjchem-518	217	11	13	13	NUM
eurjchem-518	217	12	12	12	NUM
eurjchem-518	217	13	0	0	NUM
eurjchem-518	217	14	0	0	NUM
eurjchem-518	217	15	5	5	NUM
eurjchem-518	217	16	16	16	NUM
eurjchem-518	217	17	20	20	NUM
eurjchem-518	217	18	0	0	NUM
eurjchem-518	217	19	0	0	NUM
eurjchem-518	217	20	6	6	NUM
eurjchem-518	217	21	10	10	NUM
eurjchem-518	217	22	13	13	NUM
eurjchem-518	217	23	0	0	NUM
eurjchem-518	217	24	0	0	NUM
eurjchem-518	217	25	7	7	NUM
eurjchem-518	217	26	13	13	NUM
eurjchem-518	217	27	13	13	NUM
eurjchem-518	217	28	0	0	NUM
eurjchem-518	217	29	0	0	NUM
eurjchem-518	217	30	9	9	NUM
eurjchem-518	217	31	10	10	NUM
eurjchem-518	217	32	11	11	NUM
eurjchem-518	217	33	0	0	NUM
eurjchem-518	217	34	0	0	NUM
eurjchem-518	217	35	10	10	NUM
eurjchem-518	217	36	17	17	NUM
eurjchem-518	217	37	15	15	NUM
eurjchem-518	217	38	0	0	NUM
eurjchem-518	217	39	13	13	NUM
eurjchem-518	217	40	12	12	NUM
eurjchem-518	217	41	19	19	NUM
eurjchem-518	217	42	18	18	NUM
eurjchem-518	217	43	0	0	NUM
eurjchem-518	217	44	12	12	NUM
eurjchem-518	217	45	17	17	NUM
eurjchem-518	217	46	13	13	NUM
eurjchem-518	217	47	15	15	NUM
eurjchem-518	217	48	0	0	NUM
eurjchem-518	217	49	0	0	NUM
eurjchem-518	217	50	tetracycline	tetracycline	NOUN
eurjchem-518	217	51	32	32	NUM
eurjchem-518	217	52	30	30	NUM
eurjchem-518	217	53	‐‐‐	‐‐‐	X
eurjchem-518	217	54	‐‐‐	‐‐‐	NOUN
eurjchem-518	217	55	amphotericin	amphotericin	ADP
eurjchem-518	217	56	b	b	PROPN
eurjchem-518	217	57	‐‐‐	‐‐‐	PROPN
eurjchem-518	217	58	‐‐‐	‐‐‐	NUM
eurjchem-518	217	59	16	16	NUM
eurjchem-518	217	60	18	18	NUM
eurjchem-518	217	61	dmso	dmso	NOUN
eurjchem-518	217	62	0	0	NUM
eurjchem-518	217	63	0	0	NUM
eurjchem-518	217	64	0	0	NUM
eurjchem-518	217	65	0	0	NUM
eurjchem-518	217	66	*	*	PUNCT
eurjchem-518	217	67	solvent	solvent	NOUN
eurjchem-518	217	68	:	:	PUNCT
eurjchem-518	217	69	chloroform	chloroform	NOUN
eurjchem-518	217	70	;	;	PUNCT
eurjchem-518	217	71	0	0	NUM
eurjchem-518	217	72	:	:	PUNCT
eurjchem-518	217	73	no	no	DET
eurjchem-518	217	74	activity	activity	NOUN
eurjchem-518	217	75	(	(	PUNCT
eurjchem-518	217	76	inhibition	inhibition	NOUN
eurjchem-518	217	77	zone	zone	NOUN
eurjchem-518	217	78	less	less	ADJ
eurjchem-518	217	79	than	than	ADP
eurjchem-518	217	80	7	7	NUM
eurjchem-518	217	81	mm	mm	NOUN
eurjchem-518	217	82	)	)	PUNCT
eurjchem-518	217	83	;	;	PUNCT
eurjchem-518	217	84	7‐10	7‐10	NUM
eurjchem-518	217	85	weak	weak	ADJ
eurjchem-518	217	86	activity	activity	NOUN
eurjchem-518	217	87	;	;	PUNCT
eurjchem-518	217	88	11‐15	11‐15	NUM
eurjchem-518	217	89	moderate	moderate	ADJ
eurjchem-518	217	90	activity	activity	NOUN
eurjchem-518	217	91	;	;	PUNCT
eurjchem-518	217	92	more	more	ADJ
eurjchem-518	217	93	than	than	ADP
eurjchem-518	217	94	15	15	NUM
eurjchem-518	217	95	strong	strong	ADJ
eurjchem-518	217	96	activity	activity	NOUN
eurjchem-518	217	97	.	.	PUNCT
eurjchem-518	218	1	el‐ziaty	el‐ziaty	PROPN
eurjchem-518	218	2	et	et	PROPN
eurjchem-518	218	3	al	al	PROPN
eurjchem-518	218	4	.	.	PUNCT
eurjchem-518	218	5	/	/	SYM
eurjchem-518	218	6	european	european	PROPN
eurjchem-518	218	7	journal	journal	PROPN
eurjchem-518	218	8	of	of	ADP
eurjchem-518	218	9	chemistry	chemistry	NOUN
eurjchem-518	218	10	3	3	NUM
eurjchem-518	218	11	(	(	PUNCT
eurjchem-518	218	12	1	1	NUM
eurjchem-518	218	13	)	)	PUNCT
eurjchem-518	218	14	(	(	PUNCT
eurjchem-518	218	15	2012	2012	NUM
eurjchem-518	218	16	)	)	PUNCT
eurjchem-518	218	17	65‐70	65‐70	NOUN
eurjchem-518	218	18	69	69	NUM
eurjchem-518	218	19	h	h	NOUN
eurjchem-518	218	20	ar	ar	PROPN
eurjchem-518	218	21	c	c	PROPN
eurjchem-518	218	22	n	n	PROPN
eurjchem-518	218	23	nh	nh	NOUN
eurjchem-518	219	1	o	o	X
eurjchem-518	219	2	s	s	VERB
eurjchem-518	219	3	hn	hn	PROPN
eurjchem-518	219	4	h3c	h3c	X
eurjchem-518	219	5	-h/+h	-h/+h	PROPN
eurjchem-518	219	6	n	n	CCONJ
eurjchem-518	219	7	nh	nh	PROPN
eurjchem-518	219	8	cn	cn	PROPN
eurjchem-518	219	9	ar	ar	PROPN
eurjchem-518	219	10	h3c	h3c	PROPN
eurjchem-518	219	11	s	s	PROPN
eurjchem-518	219	12	o	o	PROPN
eurjchem-518	219	13	n	n	CCONJ
eurjchem-518	219	14	nh	nh	NOUN
eurjchem-518	220	1	cn	cn	INTJ
eurjchem-518	220	2	o	o	PROPN
eurjchem-518	220	3	s	s	X
eurjchem-518	220	4	h3c	h3c	PROPN
eurjchem-518	220	5	ar	ar	PROPN
eurjchem-518	220	6	12	12	NUM
eurjchem-518	220	7	cn	cn	PROPN
eurjchem-518	220	8	h	h	PROPN
eurjchem-518	220	9	ar	ar	PROPN
eurjchem-518	220	10	cocl	cocl	PROPN
eurjchem-518	220	11	h2n	h2n	PROPN
eurjchem-518	221	1	n	n	DET
eurjchem-518	221	2	h	h	NOUN
eurjchem-518	221	3	s	s	AUX
eurjchem-518	221	4	ch3	ch3	PROPN
eurjchem-518	221	5	t.e.a	t.e.a	ADP
eurjchem-518	221	6	-hcl	-hcl	ADJ
eurjchem-518	221	7	3	3	NUM
eurjchem-518	221	8	-h2	-h2	SYM
eurjchem-518	221	9	n	n	CCONJ
eurjchem-518	221	10	n	n	ADV
eurjchem-518	221	11	cn	cn	INTJ
eurjchem-518	222	1	oh	oh	INTJ
eurjchem-518	222	2	s	s	NOUN
eurjchem-518	222	3	h3c	h3c	PROPN
eurjchem-518	222	4	ar	ar	NOUN
eurjchem-518	222	5	scheme	scheme	NOUN
eurjchem-518	222	6	4	4	NUM
eurjchem-518	222	7	scheme	scheme	NOUN
eurjchem-518	222	8	5	5	NUM
eurjchem-518	222	9	3	3	NUM
eurjchem-518	222	10	.	.	NOUN
eurjchem-518	222	11	results	result	NOUN
eurjchem-518	222	12	and	and	CCONJ
eurjchem-518	222	13	discussion	discussion	NOUN
eurjchem-518	222	14	in	in	ADP
eurjchem-518	222	15	continuation	continuation	NOUN
eurjchem-518	222	16	of	of	ADP
eurjchem-518	222	17	our	our	PRON
eurjchem-518	222	18	efforts	effort	NOUN
eurjchem-518	222	19	to	to	PART
eurjchem-518	222	20	study	study	VERB
eurjchem-518	222	21	the	the	DET
eurjchem-518	222	22	reactivity	reactivity	NOUN
eurjchem-518	222	23	of	of	ADP
eurjchem-518	222	24	2‐	2‐	NUM
eurjchem-518	222	25	propenoyl	propenoyl	NOUN
eurjchem-518	222	26	chlorides	chloride	NOUN
eurjchem-518	222	27	towards	towards	ADP
eurjchem-518	222	28	some	some	DET
eurjchem-518	222	29	nitrogen	nitrogen	NOUN
eurjchem-518	222	30	and	and	CCONJ
eurjchem-518	222	31	oxygen	oxygen	NOUN
eurjchem-518	222	32	nucleophilic	nucleophilic	ADJ
eurjchem-518	222	33	reagents	reagent	NOUN
eurjchem-518	222	34	[	[	X
eurjchem-518	222	35	20‐23	20‐23	NUM
eurjchem-518	222	36	]	]	PUNCT
eurjchem-518	222	37	,	,	PUNCT
eurjchem-518	222	38	we	we	PRON
eurjchem-518	222	39	reported	report	VERB
eurjchem-518	222	40	herein	herein	NOUN
eurjchem-518	222	41	,	,	PUNCT
eurjchem-518	222	42	the	the	DET
eurjchem-518	222	43	synthesis	synthesis	NOUN
eurjchem-518	222	44	of	of	ADP
eurjchem-518	222	45	a	a	DET
eurjchem-518	222	46	new	new	ADJ
eurjchem-518	222	47	compound	compound	NOUN
eurjchem-518	222	48	,	,	PUNCT
eurjchem-518	222	49	(	(	PUNCT
eurjchem-518	222	50	e)2‐cyano‐3‐(2,4‐dichloro	e)2‐cyano‐3‐(2,4‐dichloro	X
eurjchem-518	222	51	phenyl)acryloyl	phenyl)acryloyl	ADV
eurjchem-518	222	52	chloride	chloride	NOUN
eurjchem-518	222	53	3	3	NUM
eurjchem-518	222	54	via	via	ADP
eurjchem-518	222	55	the	the	DET
eurjchem-518	222	56	common	common	ADJ
eurjchem-518	222	57	route	route	NOUN
eurjchem-518	222	58	condensation	condensation	NOUN
eurjchem-518	222	59	of	of	ADP
eurjchem-518	222	60	2,4‐dichlorobenzaldehyde	2,4‐dichlorobenzaldehyde	NOUN
eurjchem-518	222	61	with	with	ADP
eurjchem-518	222	62	ethyl	ethyl	PROPN
eurjchem-518	222	63	cyanoacetate	cyanoacetate	NOUN
eurjchem-518	222	64	in	in	ADP
eurjchem-518	222	65	the	the	DET
eurjchem-518	222	66	presence	presence	NOUN
eurjchem-518	222	67	of	of	ADP
eurjchem-518	222	68	piperidine	piperidine	NOUN
eurjchem-518	222	69	,	,	PUNCT
eurjchem-518	222	70	to	to	PART
eurjchem-518	222	71	give	give	VERB
eurjchem-518	222	72	the	the	DET
eurjchem-518	222	73	corresponding	correspond	VERB
eurjchem-518	222	74	(	(	PUNCT
eurjchem-518	222	75	e)‐ethyl	e)‐ethyl	PROPN
eurjchem-518	222	76	2‐	2‐	NUM
eurjchem-518	222	77	cyano‐3‐(2,4‐dichlorophenyl	cyano‐3‐(2,4‐dichlorophenyl	PROPN
eurjchem-518	222	78	)	)	PUNCT
eurjchem-518	222	79	acrylate	acrylate	NOUN
eurjchem-518	222	80	,	,	PUNCT
eurjchem-518	222	81	1	1	NUM
eurjchem-518	222	82	,	,	PUNCT
eurjchem-518	222	83	[	[	X
eurjchem-518	222	84	24	24	NUM
eurjchem-518	222	85	]	]	PUNCT
eurjchem-518	222	86	.	.	PUNCT
eurjchem-518	223	1	hydrolysis	hydrolysis	NOUN
eurjchem-518	223	2	of	of	ADP
eurjchem-518	223	3	1	1	NUM
eurjchem-518	223	4	in	in	ADP
eurjchem-518	223	5	alcoholic	alcoholic	ADJ
eurjchem-518	223	6	solution	solution	NOUN
eurjchem-518	223	7	of	of	ADP
eurjchem-518	223	8	sodium	sodium	NOUN
eurjchem-518	223	9	hydroxide	hydroxide	NOUN
eurjchem-518	223	10	(	(	PUNCT
eurjchem-518	223	11	1:1	1:1	NUM
eurjchem-518	223	12	mole	mole	NOUN
eurjchem-518	223	13	)	)	PUNCT
eurjchem-518	223	14	gave	give	VERB
eurjchem-518	223	15	(	(	PUNCT
eurjchem-518	223	16	e)‐	e)‐	X
eurjchem-518	223	17	2‐cyano‐3‐(2,4‐dichlorophenyl)acrylic	2‐cyano‐3‐(2,4‐dichlorophenyl)acrylic	ADJ
eurjchem-518	223	18	acid	acid	NOUN
eurjchem-518	223	19	,	,	PUNCT
eurjchem-518	223	20	2	2	NUM
eurjchem-518	223	21	,	,	PUNCT
eurjchem-518	223	22	[	[	X
eurjchem-518	223	23	25	25	NUM
eurjchem-518	223	24	]	]	PUNCT
eurjchem-518	223	25	.	.	PUNCT
eurjchem-518	224	1	refluxing	refluxe	VERB
eurjchem-518	224	2	the	the	DET
eurjchem-518	224	3	acid	acid	NOUN
eurjchem-518	224	4	2	2	NUM
eurjchem-518	224	5	with	with	ADP
eurjchem-518	224	6	thionyl	thionyl	ADJ
eurjchem-518	224	7	chloride	chloride	NOUN
eurjchem-518	224	8	yielded	yield	VERB
eurjchem-518	224	9	the	the	DET
eurjchem-518	224	10	new	new	ADJ
eurjchem-518	224	11	acryloyl	acryloyl	ADV
eurjchem-518	224	12	chloride	chloride	NOUN
eurjchem-518	224	13	derivative	derivative	ADJ
eurjchem-518	224	14	3	3	NUM
eurjchem-518	224	15	in	in	ADP
eurjchem-518	224	16	good	good	ADJ
eurjchem-518	224	17	yield	yield	NOUN
eurjchem-518	224	18	(	(	PUNCT
eurjchem-518	224	19	scheme	scheme	NOUN
eurjchem-518	224	20	1	1	NUM
eurjchem-518	224	21	)	)	PUNCT
eurjchem-518	224	22	.	.	PUNCT
eurjchem-518	225	1	the	the	DET
eurjchem-518	225	2	acryloyl	acryloyl	PROPN
eurjchem-518	225	3	chloride	chloride	PROPN
eurjchem-518	225	4	derivative	derivative	ADJ
eurjchem-518	225	5	3	3	NUM
eurjchem-518	225	6	was	be	AUX
eurjchem-518	225	7	reacted	react	VERB
eurjchem-518	225	8	with	with	ADP
eurjchem-518	225	9	phenol	phenol	NOUN
eurjchem-518	225	10	,	,	PUNCT
eurjchem-518	225	11	4‐chlorothiophenol	4‐chlorothiophenol	NUM
eurjchem-518	225	12	and	and	CCONJ
eurjchem-518	225	13	primary	primary	ADJ
eurjchem-518	225	14	amines	amine	NOUN
eurjchem-518	225	15	such	such	ADJ
eurjchem-518	225	16	as	as	ADP
eurjchem-518	225	17	,	,	PUNCT
eurjchem-518	225	18	4‐	4‐	NUM
eurjchem-518	225	19	methoxyaniline	methoxyaniline	NOUN
eurjchem-518	225	20	,	,	PUNCT
eurjchem-518	225	21	4‐methylaniline4chloroaniline	4‐methylaniline4chloroaniline	NOUN
eurjchem-518	225	22	and	and	CCONJ
eurjchem-518	225	23	3‐amino	3‐amino	NUM
eurjchem-518	225	24	pyridine	pyridine	NOUN
eurjchem-518	225	25	in	in	ADP
eurjchem-518	225	26	dry	dry	ADJ
eurjchem-518	225	27	benzene	benzene	NOUN
eurjchem-518	225	28	in	in	ADP
eurjchem-518	225	29	the	the	DET
eurjchem-518	225	30	presence	presence	NOUN
eurjchem-518	225	31	of	of	ADP
eurjchem-518	225	32	triethylamine	triethylamine	NOUN
eurjchem-518	225	33	to	to	PART
eurjchem-518	225	34	give	give	VERB
eurjchem-518	225	35	acrylate	acrylate	NOUN
eurjchem-518	225	36	,	,	PUNCT
eurjchem-518	225	37	thioacrylate	thioacrylate	NOUN
eurjchem-518	225	38	and	and	CCONJ
eurjchem-518	225	39	acrylamides	acrylamide	NOUN
eurjchem-518	225	40	,	,	PUNCT
eurjchem-518	225	41	4‐9	4‐9	NOUN
eurjchem-518	225	42	,	,	PUNCT
eurjchem-518	225	43	respectively	respectively	ADV
eurjchem-518	225	44	(	(	PUNCT
eurjchem-518	225	45	scheme	scheme	NOUN
eurjchem-518	225	46	2	2	NUM
eurjchem-518	225	47	)	)	PUNCT
eurjchem-518	225	48	.	.	PUNCT
eurjchem-518	226	1	on	on	ADP
eurjchem-518	226	2	the	the	DET
eurjchem-518	226	3	other	other	ADJ
eurjchem-518	226	4	hand	hand	NOUN
eurjchem-518	226	5	,	,	PUNCT
eurjchem-518	226	6	reaction	reaction	NOUN
eurjchem-518	226	7	of	of	ADP
eurjchem-518	226	8	the	the	DET
eurjchem-518	226	9	acryloyl	acryloyl	PROPN
eurjchem-518	226	10	chloride	chloride	NOUN
eurjchem-518	226	11	derivative	derivative	ADJ
eurjchem-518	226	12	3	3	NUM
eurjchem-518	226	13	with	with	ADP
eurjchem-518	226	14	benzoyl	benzoyl	ADJ
eurjchem-518	226	15	hydrazine	hydrazine	NOUN
eurjchem-518	226	16	as	as	ADP
eurjchem-518	226	17	a	a	DET
eurjchem-518	226	18	bifunctional	bifunctional	ADJ
eurjchem-518	226	19	nucleophile	nucleophile	NOUN
eurjchem-518	226	20	under	under	ADP
eurjchem-518	226	21	the	the	DET
eurjchem-518	226	22	same	same	ADJ
eurjchem-518	226	23	conditions	condition	NOUN
eurjchem-518	226	24	gave	give	VERB
eurjchem-518	226	25	the	the	DET
eurjchem-518	226	26	benzoyl	benzoyl	NOUN
eurjchem-518	226	27	hydrazide	hydrazide	NOUN
eurjchem-518	226	28	derivative	derivative	PROPN
eurjchem-518	226	29	10	10	NUM
eurjchem-518	226	30	which	which	PRON
eurjchem-518	226	31	underwent	undergo	VERB
eurjchem-518	226	32	ring	ring	NOUN
eurjchem-518	226	33	closure	closure	NOUN
eurjchem-518	226	34	upon	upon	SCONJ
eurjchem-518	226	35	heating	heat	VERB
eurjchem-518	226	36	with	with	ADP
eurjchem-518	226	37	pocl3	pocl3	NOUN
eurjchem-518	226	38	to	to	PART
eurjchem-518	226	39	give	give	VERB
eurjchem-518	226	40	the	the	DET
eurjchem-518	226	41	oxadiazole	oxadiazole	NOUN
eurjchem-518	226	42	derivative	derivative	ADJ
eurjchem-518	226	43	11	11	NUM
eurjchem-518	226	44	(	(	PUNCT
eurjchem-518	226	45	scheme	scheme	NOUN
eurjchem-518	226	46	2	2	NUM
eurjchem-518	226	47	)	)	PUNCT
eurjchem-518	226	48	.	.	PUNCT
eurjchem-518	227	1	when	when	SCONJ
eurjchem-518	227	2	the	the	DET
eurjchem-518	227	3	acryloyl	acryloyl	PROPN
eurjchem-518	227	4	chloride	chloride	NOUN
eurjchem-518	227	5	derivative	derivative	ADJ
eurjchem-518	227	6	3	3	NUM
eurjchem-518	227	7	was	be	AUX
eurjchem-518	227	8	allowed	allow	VERB
eurjchem-518	227	9	to	to	PART
eurjchem-518	227	10	react	react	VERB
eurjchem-518	227	11	with	with	ADP
eurjchem-518	227	12	methylthiourea	methylthiourea	NOUN
eurjchem-518	227	13	,	,	PUNCT
eurjchem-518	227	14	phenylurea	phenylurea	NOUN
eurjchem-518	227	15	and	and	CCONJ
eurjchem-518	227	16	2‐	2‐	NUM
eurjchem-518	227	17	aminopyridine	aminopyridine	NOUN
eurjchem-518	227	18	as	as	ADP
eurjchem-518	227	19	1,3‐binucleophilic	1,3‐binucleophilic	ADJ
eurjchem-518	227	20	reagents	reagent	NOUN
eurjchem-518	227	21	,	,	PUNCT
eurjchem-518	227	22	it	it	PRON
eurjchem-518	227	23	gave	give	VERB
eurjchem-518	227	24	the	the	DET
eurjchem-518	227	25	tetrahydropyrimidine‐2‐thione	tetrahydropyrimidine‐2‐thione	PROPN
eurjchem-518	227	26	derivative	derivative	ADJ
eurjchem-518	227	27	12	12	NUM
eurjchem-518	227	28	,	,	PUNCT
eurjchem-518	227	29	1‐acryloyl‐3‐	1‐acryloyl‐3‐	NUM
eurjchem-518	227	30	phenyl	phenyl	NOUN
eurjchem-518	227	31	urea	urea	NOUN
eurjchem-518	227	32	derivative	derivative	ADJ
eurjchem-518	227	33	13	13	NUM
eurjchem-518	227	34	and	and	CCONJ
eurjchem-518	227	35	a	a	DET
eurjchem-518	227	36	mixture	mixture	NOUN
eurjchem-518	227	37	of	of	ADP
eurjchem-518	227	38	acrylamide	acrylamide	ADJ
eurjchem-518	227	39	derivative	derivative	ADJ
eurjchem-518	227	40	14	14	NUM
eurjchem-518	227	41	and	and	CCONJ
eurjchem-518	227	42	pyridopyrimidine	pyridopyrimidine	NOUN
eurjchem-518	227	43	derivative	derivative	ADJ
eurjchem-518	227	44	15	15	NUM
eurjchem-518	227	45	,	,	PUNCT
eurjchem-518	227	46	respectively	respectively	ADV
eurjchem-518	227	47	(	(	PUNCT
eurjchem-518	227	48	scheme	scheme	NOUN
eurjchem-518	227	49	2	2	NUM
eurjchem-518	227	50	)	)	PUNCT
eurjchem-518	227	51	.	.	PUNCT
eurjchem-518	228	1	the	the	DET
eurjchem-518	228	2	formation	formation	NOUN
eurjchem-518	228	3	of	of	ADP
eurjchem-518	228	4	compound	compound	NOUN
eurjchem-518	228	5	12	12	NUM
eurjchem-518	228	6	can	can	AUX
eurjchem-518	228	7	be	be	AUX
eurjchem-518	228	8	represented	represent	VERB
eurjchem-518	228	9	by	by	ADP
eurjchem-518	228	10	the	the	DET
eurjchem-518	228	11	following	follow	VERB
eurjchem-518	228	12	pathway	pathway	NOUN
eurjchem-518	228	13	(	(	PUNCT
eurjchem-518	228	14	scheme	scheme	NOUN
eurjchem-518	228	15	4	4	NUM
eurjchem-518	228	16	)	)	PUNCT
eurjchem-518	228	17	.	.	PUNCT
eurjchem-518	229	1	the	the	DET
eurjchem-518	229	2	formation	formation	NOUN
eurjchem-518	229	3	of	of	ADP
eurjchem-518	229	4	compounds	compound	NOUN
eurjchem-518	229	5	14	14	NUM
eurjchem-518	229	6	and	and	CCONJ
eurjchem-518	229	7	15	15	NUM
eurjchem-518	229	8	can	can	AUX
eurjchem-518	229	9	be	be	AUX
eurjchem-518	229	10	explained	explain	VERB
eurjchem-518	229	11	by	by	ADP
eurjchem-518	229	12	the	the	DET
eurjchem-518	229	13	following	follow	VERB
eurjchem-518	229	14	pathway	pathway	NOUN
eurjchem-518	229	15	(	(	PUNCT
eurjchem-518	229	16	scheme	scheme	NOUN
eurjchem-518	229	17	5	5	NUM
eurjchem-518	229	18	)	)	PUNCT
eurjchem-518	229	19	.	.	PUNCT
eurjchem-518	230	1	when	when	SCONJ
eurjchem-518	230	2	the	the	DET
eurjchem-518	230	3	acryloyl	acryloyl	PROPN
eurjchem-518	230	4	chloride	chloride	NOUN
eurjchem-518	230	5	derivative	derivative	ADJ
eurjchem-518	230	6	3	3	NUM
eurjchem-518	230	7	was	be	AUX
eurjchem-518	230	8	allowed	allow	VERB
eurjchem-518	230	9	to	to	PART
eurjchem-518	230	10	react	react	VERB
eurjchem-518	230	11	with	with	ADP
eurjchem-518	230	12	thiosemicarbazide	thiosemicarbazide	NOUN
eurjchem-518	230	13	,	,	PUNCT
eurjchem-518	230	14	it	it	PRON
eurjchem-518	230	15	gave	give	VERB
eurjchem-518	230	16	a	a	DET
eurjchem-518	230	17	mixture	mixture	NOUN
eurjchem-518	230	18	of	of	ADP
eurjchem-518	230	19	the	the	DET
eurjchem-518	230	20	thiosemicarbazone	thiosemicarbazone	NOUN
eurjchem-518	230	21	16	16	NUM
eurjchem-518	230	22	and	and	CCONJ
eurjchem-518	230	23	the	the	DET
eurjchem-518	230	24	pyrazolone	pyrazolone	NOUN
eurjchem-518	230	25	derivative	derivative	NOUN
eurjchem-518	230	26	17	17	NUM
eurjchem-518	230	27	(	(	PUNCT
eurjchem-518	230	28	scheme	scheme	NOUN
eurjchem-518	230	29	3	3	NUM
eurjchem-518	230	30	)	)	PUNCT
eurjchem-518	230	31	.	.	PUNCT
eurjchem-518	231	1	the	the	DET
eurjchem-518	231	2	acryloyl	acryloyl	PROPN
eurjchem-518	231	3	derivative	derivative	ADJ
eurjchem-518	231	4	3	3	NUM
eurjchem-518	231	5	condensed	condense	VERB
eurjchem-518	231	6	with	with	ADP
eurjchem-518	231	7	ethanolamine	ethanolamine	NOUN
eurjchem-518	231	8	to	to	PART
eurjchem-518	231	9	give	give	VERB
eurjchem-518	231	10	the	the	DET
eurjchem-518	231	11	dihydrooxazole	dihydrooxazole	ADJ
eurjchem-518	231	12	derivative	derivative	ADJ
eurjchem-518	231	13	18	18	NUM
eurjchem-518	231	14	(	(	PUNCT
eurjchem-518	231	15	scheme	scheme	NOUN
eurjchem-518	231	16	3	3	NUM
eurjchem-518	231	17	)	)	PUNCT
eurjchem-518	231	18	.	.	PUNCT
eurjchem-518	232	1	2‐propenoyl	2‐propenoyl	ADJ
eurjchem-518	232	2	amide	amide	NOUN
eurjchem-518	232	3	19	19	NUM
eurjchem-518	232	4	was	be	AUX
eurjchem-518	232	5	prepared	prepare	VERB
eurjchem-518	232	6	by	by	ADP
eurjchem-518	232	7	condensation	condensation	NOUN
eurjchem-518	232	8	of	of	ADP
eurjchem-518	232	9	3	3	NUM
eurjchem-518	232	10	with	with	ADP
eurjchem-518	232	11	anthranilic	anthranilic	ADJ
eurjchem-518	232	12	acid	acid	NOUN
eurjchem-518	232	13	in	in	ADP
eurjchem-518	232	14	the	the	DET
eurjchem-518	232	15	presence	presence	NOUN
eurjchem-518	232	16	of	of	ADP
eurjchem-518	232	17	triethylamine	triethylamine	NOUN
eurjchem-518	232	18	(	(	PUNCT
eurjchem-518	232	19	tea	tea	NOUN
eurjchem-518	232	20	)	)	PUNCT
eurjchem-518	232	21	.	.	PUNCT
eurjchem-518	233	1	the	the	DET
eurjchem-518	233	2	structure	structure	NOUN
eurjchem-518	233	3	of	of	ADP
eurjchem-518	233	4	19	19	NUM
eurjchem-518	233	5	was	be	AUX
eurjchem-518	233	6	confirmed	confirm	VERB
eurjchem-518	233	7	chemically	chemically	ADV
eurjchem-518	233	8	by	by	ADP
eurjchem-518	233	9	ring	re	VERB
eurjchem-518	233	10	closure	closure	NOUN
eurjchem-518	233	11	using	use	VERB
eurjchem-518	233	12	acetic	acetic	ADJ
eurjchem-518	233	13	anhydride	anhydride	NOUN
eurjchem-518	233	14	whereby	whereby	SCONJ
eurjchem-518	233	15	the	the	DET
eurjchem-518	233	16	benzoxazinone	benzoxazinone	NOUN
eurjchem-518	233	17	20	20	NUM
eurjchem-518	233	18	was	be	AUX
eurjchem-518	233	19	obtained	obtain	VERB
eurjchem-518	233	20	(	(	PUNCT
eurjchem-518	233	21	scheme	scheme	NOUN
eurjchem-518	233	22	3	3	NUM
eurjchem-518	233	23	)	)	PUNCT
eurjchem-518	233	24	.	.	PUNCT
eurjchem-518	234	1	70	70	NUM
eurjchem-518	234	2	el‐ziaty	el‐ziaty	PROPN
eurjchem-518	234	3	et	et	PROPN
eurjchem-518	234	4	al	al	PROPN
eurjchem-518	234	5	.	.	PUNCT
eurjchem-518	234	6	/	/	SYM
eurjchem-518	234	7	european	european	PROPN
eurjchem-518	234	8	journal	journal	PROPN
eurjchem-518	234	9	of	of	ADP
eurjchem-518	234	10	chemistry	chemistry	NOUN
eurjchem-518	234	11	3	3	NUM
eurjchem-518	234	12	(	(	PUNCT
eurjchem-518	234	13	1	1	NUM
eurjchem-518	234	14	)	)	PUNCT
eurjchem-518	234	15	(	(	PUNCT
eurjchem-518	234	16	2012	2012	NUM
eurjchem-518	234	17	)	)	PUNCT
eurjchem-518	234	18	65‐70	65‐70	NOUN
eurjchem-518	235	1	n	n	PRON
eurjchem-518	235	2	h	h	NOUN
eurjchem-518	235	3	2	2	NUM
eurjchem-518	235	4	n	n	NUM
eurjchem-518	235	5	h	h	NOUN
eurjchem-518	235	6	c	c	NOUN
eurjchem-518	235	7	s	s	PART
eurjchem-518	235	8	n	n	ADP
eurjchem-518	235	9	h	h	NOUN
eurjchem-518	235	10	2	2	NUM
eurjchem-518	235	11	scheme	scheme	NOUN
eurjchem-518	235	12	6	6	NUM
eurjchem-518	235	13	the	the	DET
eurjchem-518	235	14	acrylamide	acrylamide	NOUN
eurjchem-518	235	15	derivative	derivative	ADJ
eurjchem-518	235	16	21	21	NUM
eurjchem-518	235	17	,	,	PUNCT
eurjchem-518	235	18	which	which	PRON
eurjchem-518	235	19	was	be	AUX
eurjchem-518	235	20	prepared	prepare	VERB
eurjchem-518	235	21	by	by	ADP
eurjchem-518	235	22	the	the	DET
eurjchem-518	235	23	reaction	reaction	NOUN
eurjchem-518	235	24	of	of	ADP
eurjchem-518	235	25	3	3	NUM
eurjchem-518	235	26	with	with	ADP
eurjchem-518	235	27	2‐aminophenol	2‐aminophenol	NUM
eurjchem-518	235	28	,	,	PUNCT
eurjchem-518	235	29	gave	give	VERB
eurjchem-518	235	30	the	the	DET
eurjchem-518	235	31	benzoxazole	benzoxazole	NOUN
eurjchem-518	235	32	derivative	derivative	NOUN
eurjchem-518	235	33	22	22	NUM
eurjchem-518	235	34	upon	upon	SCONJ
eurjchem-518	235	35	heating	heat	VERB
eurjchem-518	235	36	with	with	ADP
eurjchem-518	235	37	phosphorus	phosphorus	NOUN
eurjchem-518	235	38	oxychloride	oxychloride	NOUN
eurjchem-518	235	39	(	(	PUNCT
eurjchem-518	235	40	scheme	scheme	NOUN
eurjchem-518	235	41	3	3	NUM
eurjchem-518	235	42	)	)	PUNCT
eurjchem-518	235	43	.	.	PUNCT
eurjchem-518	236	1	the	the	DET
eurjchem-518	236	2	formation	formation	NOUN
eurjchem-518	236	3	of	of	ADP
eurjchem-518	236	4	compounds	compound	NOUN
eurjchem-518	236	5	16	16	NUM
eurjchem-518	236	6	and	and	CCONJ
eurjchem-518	236	7	17	17	NUM
eurjchem-518	236	8	can	can	AUX
eurjchem-518	236	9	be	be	AUX
eurjchem-518	236	10	represented	represent	VERB
eurjchem-518	236	11	by	by	ADP
eurjchem-518	236	12	the	the	DET
eurjchem-518	236	13	following	follow	VERB
eurjchem-518	236	14	pathway	pathway	NOUN
eurjchem-518	236	15	scheme	scheme	NOUN
eurjchem-518	236	16	6	6	NUM
eurjchem-518	236	17	.	.	NOUN
eurjchem-518	237	1	4	4	NUM
eurjchem-518	237	2	.	.	X
eurjchem-518	237	3	conclusion	conclusion	NOUN
eurjchem-518	237	4	2‐propenoyl	2‐propenoyl	NUM
eurjchem-518	237	5	derivatives	derivative	NOUN
eurjchem-518	237	6	and	and	CCONJ
eurjchem-518	237	7	some	some	DET
eurjchem-518	237	8	heterocyclic	heterocyclic	ADJ
eurjchem-518	237	9	compounds	compound	NOUN
eurjchem-518	237	10	with	with	ADP
eurjchem-518	237	11	antibacterial	antibacterial	ADJ
eurjchem-518	237	12	and	and	CCONJ
eurjchem-518	237	13	antifungal	antifungal	ADJ
eurjchem-518	237	14	activities	activity	NOUN
eurjchem-518	237	15	were	be	AUX
eurjchem-518	237	16	synthesized	synthesize	VERB
eurjchem-518	237	17	from	from	ADP
eurjchem-518	237	18	readily	readily	ADV
eurjchem-518	237	19	obtainable	obtainable	ADJ
eurjchem-518	237	20	starting	start	VERB
eurjchem-518	237	21	materials	material	NOUN
eurjchem-518	237	22	such	such	ADJ
eurjchem-518	237	23	as	as	ADP
eurjchem-518	237	24	2‐cyano‐3‐	2‐cyano‐3‐	PROPN
eurjchem-518	237	25	(	(	PUNCT
eurjchem-518	237	26	2ˊ,4ˊ‐dichlorophenyl)acryloyl	2ˊ,4ˊ‐dichlorophenyl)acryloyl	NUM
eurjchem-518	237	27	chloride	chloride	NOUN
eurjchem-518	237	28	,	,	PUNCT
eurjchem-518	237	29	3	3	NUM
eurjchem-518	237	30	.	.	X
eurjchem-518	238	1	acknowledgements	acknowledgement	NOUN
eurjchem-518	238	2	the	the	DET
eurjchem-518	238	3	best	good	ADJ
eurjchem-518	238	4	regards	regard	NOUN
eurjchem-518	238	5	for	for	ADP
eurjchem-518	238	6	the	the	DET
eurjchem-518	238	7	micro	micro	ADJ
eurjchem-518	238	8	analytical	analytical	ADJ
eurjchem-518	238	9	center	center	NOUN
eurjchem-518	238	10	,	,	PUNCT
eurjchem-518	238	11	cairo	cairo	PROPN
eurjchem-518	238	12	university	university	PROPN
eurjchem-518	238	13	,	,	PUNCT
eurjchem-518	238	14	egypt	egypt	PROPN
eurjchem-518	238	15	for	for	ADP
eurjchem-518	238	16	carrying	carry	VERB
eurjchem-518	238	17	out	out	ADP
eurjchem-518	238	18	the	the	DET
eurjchem-518	238	19	biological	biological	ADJ
eurjchem-518	238	20	activities	activity	NOUN
eurjchem-518	238	21	and	and	CCONJ
eurjchem-518	238	22	spectral	spectral	ADJ
eurjchem-518	238	23	studies	study	NOUN
eurjchem-518	238	24	references	reference	NOUN
eurjchem-518	238	25	[	[	X
eurjchem-518	238	26	1	1	NUM
eurjchem-518	238	27	]	]	PUNCT
eurjchem-518	238	28	.	.	PUNCT
eurjchem-518	239	1	santos	santos	PROPN
eurjchem-518	239	2	,	,	PUNCT
eurjchem-518	239	3	s.	s.	PROPN
eurjchem-518	239	4	a.	a.	PROPN
eurjchem-518	239	5	;	;	PUNCT
eurjchem-518	239	6	pereira	pereira	PROPN
eurjchem-518	239	7	,	,	PUNCT
eurjchem-518	239	8	n.	n.	PROPN
eurjchem-518	239	9	jr	jr	PROPN
eurjchem-518	239	10	.	.	PROPN
eurjchem-518	239	11	;	;	PUNCT
eurjchem-518	239	12	da	da	PROPN
eurjchem-518	239	13	silva	silva	PROPN
eurjchem-518	239	14	,	,	PUNCT
eurjchem-518	239	15	i.	i.	NOUN
eurjchem-518	239	16	m.	m.	PROPN
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eurjchem-518	239	21	i.	i.	PROPN
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eurjchem-518	239	27	a.	a.	PROPN
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eurjchem-518	240	2	,	,	PUNCT
eurjchem-518	240	3	39	39	NUM
eurjchem-518	240	4	,	,	PUNCT
eurjchem-518	240	5	2269‐2275	2269‐2275	NUM
eurjchem-518	240	6	.	.	PUNCT
eurjchem-518	241	1	[	[	X
eurjchem-518	241	2	2	2	NUM
eurjchem-518	241	3	]	]	PUNCT
eurjchem-518	241	4	.	.	PUNCT
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eurjchem-518	242	2	,	,	PUNCT
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eurjchem-518	242	5	;	;	PUNCT
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eurjchem-518	242	9	f.	f.	PROPN
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eurjchem-518	242	11	.	.	PUNCT
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eurjchem-518	243	3	chem	chem	PROPN
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eurjchem-518	244	2	,	,	PUNCT
eurjchem-518	244	3	13	13	NUM
eurjchem-518	244	4	,	,	PUNCT
eurjchem-518	244	5	5171‐5180	5171‐5180	NUM
eurjchem-518	244	6	.	.	PUNCT
eurjchem-518	245	1	[	[	X
eurjchem-518	245	2	3	3	NUM
eurjchem-518	245	3	]	]	PUNCT
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eurjchem-518	247	2	,	,	PUNCT
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eurjchem-518	247	4	,	,	PUNCT
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eurjchem-518	248	2	4	4	NUM
eurjchem-518	248	3	]	]	PUNCT
eurjchem-518	248	4	.	.	PUNCT
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eurjchem-518	249	4	;	;	PUNCT
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eurjchem-518	249	28	c.	c.	PROPN
eurjchem-518	249	29	;	;	PUNCT
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eurjchem-518	249	32	p.	p.	PROPN
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eurjchem-518	249	40	h.	h.	PROPN
eurjchem-518	249	41	;	;	PUNCT
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eurjchem-518	249	46	)	)	PUNCT
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eurjchem-518	250	2	5	5	NUM
eurjchem-518	250	3	]	]	PUNCT
eurjchem-518	250	4	.	.	PUNCT
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eurjchem-518	251	5	;	;	PUNCT
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eurjchem-518	251	12	s.	s.	PROPN
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eurjchem-518	251	15	,	,	PUNCT
eurjchem-518	251	16	m.	m.	PROPN
eurjchem-518	251	17	h.	h.	PROPN
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eurjchem-518	252	2	.	.	PUNCT
eurjchem-518	253	1	2005	2005	NUM
eurjchem-518	253	2	,	,	PUNCT
eurjchem-518	253	3	690(5	690(5	NUM
eurjchem-518	253	4	)	)	PUNCT
eurjchem-518	253	5	,	,	PUNCT
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eurjchem-518	253	7	.	.	PUNCT
eurjchem-518	254	1	[	[	X
eurjchem-518	254	2	6	6	NUM
eurjchem-518	254	3	]	]	PUNCT
eurjchem-518	254	4	.	.	PUNCT
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eurjchem-518	255	5	;	;	PUNCT
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eurjchem-518	255	25	;	;	PUNCT
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eurjchem-518	255	29	;	;	PUNCT
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eurjchem-518	255	42	,	,	PUNCT
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eurjchem-518	255	44	)	)	PUNCT
eurjchem-518	255	45	,	,	PUNCT
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eurjchem-518	256	3	]	]	PUNCT
eurjchem-518	256	4	.	.	PUNCT
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eurjchem-518	259	2	,	,	PUNCT
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eurjchem-518	259	4	)	)	PUNCT
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eurjchem-518	261	20	)	)	PUNCT
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eurjchem-518	262	3	]	]	PUNCT
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eurjchem-518	266	2	,	,	PUNCT
eurjchem-518	266	3	19(11	19(11	NUM
eurjchem-518	266	4	)	)	PUNCT
eurjchem-518	266	5	,	,	PUNCT
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eurjchem-518	267	3	]	]	PUNCT
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eurjchem-518	268	24	)	)	PUNCT
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eurjchem-518	269	3	]	]	PUNCT
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eurjchem-518	272	3	527(1‐3	527(1‐3	NOUN
eurjchem-518	272	4	)	)	PUNCT
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eurjchem-518	272	7	.	.	PUNCT
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eurjchem-518	273	2	12	12	NUM
eurjchem-518	273	3	]	]	PUNCT
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eurjchem-518	275	3	.	.	PUNCT
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eurjchem-518	276	2	,	,	PUNCT
eurjchem-518	276	3	269(1	269(1	NUM
eurjchem-518	276	4	)	)	PUNCT
eurjchem-518	276	5	,	,	PUNCT
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eurjchem-518	276	7	.	.	PUNCT
eurjchem-518	277	1	[	[	X
eurjchem-518	277	2	13	13	NUM
eurjchem-518	277	3	]	]	PUNCT
eurjchem-518	277	4	.	.	PUNCT
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eurjchem-518	280	2	.	.	PUNCT
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eurjchem-518	281	2	,	,	PUNCT
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eurjchem-518	281	4	)	)	PUNCT
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eurjchem-518	282	3	]	]	SYM
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eurjchem-518	285	2	.	.	PUNCT
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eurjchem-518	286	2	,	,	PUNCT
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eurjchem-518	286	4	)	)	PUNCT
eurjchem-518	286	5	,	,	PUNCT
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eurjchem-518	289	5	)	)	PUNCT
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eurjchem-518	292	2	17	17	NUM
eurjchem-518	292	3	]	]	PUNCT
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eurjchem-518	294	2	,	,	PUNCT
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eurjchem-518	302	2	20	20	NUM
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eurjchem-518	304	2	,	,	PUNCT
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