id	sid	tid	token	lemma	pos
eurjchem-562	1	1	untitled	untitle	VERB
eurjchem-562	1	2	european	european	PROPN
eurjchem-562	1	3	journal	journal	PROPN
eurjchem-562	1	4	of	of	ADP
eurjchem-562	1	5	chemistry	chemistry	NOUN
eurjchem-562	1	6	3	3	NUM
eurjchem-562	1	7	(	(	PUNCT
eurjchem-562	1	8	2	2	NUM
eurjchem-562	1	9	)	)	PUNCT
eurjchem-562	1	10	(	(	PUNCT
eurjchem-562	1	11	2012	2012	NUM
eurjchem-562	1	12	)	)	PUNCT
eurjchem-562	1	13	179‐185	179‐185	NUM
eurjchem-562	1	14	european	european	ADJ
eurjchem-562	1	15	journal	journal	PROPN
eurjchem-562	1	16	of	of	ADP
eurjchem-562	1	17	chemistry	chemistry	NOUN
eurjchem-562	1	18	issn	issn	PROPN
eurjchem-562	1	19	2153‐2249	2153‐2249	PROPN
eurjchem-562	1	20	(	(	PUNCT
eurjchem-562	1	21	print	print	NOUN
eurjchem-562	1	22	)	)	PUNCT
eurjchem-562	1	23	/	/	SYM
eurjchem-562	1	24	issn	issn	PROPN
eurjchem-562	1	25	2153‐2257	2153‐2257	NUM
eurjchem-562	1	26	(	(	PUNCT
eurjchem-562	1	27	online	online	ADJ
eurjchem-562	1	28	)	)	PUNCT
eurjchem-562	1	29			NOUN
eurjchem-562	1	30	2012	2012	NUM
eurjchem-562	1	31	eurjchem	eurjchem	PROPN
eurjchem-562	1	32	doi:10.5155	doi:10.5155	PROPN
eurjchem-562	1	33	/	/	SYM
eurjchem-562	1	34	eurjchem.3.2.179‐185.562	eurjchem.3.2.179‐185.562	ADJ
eurjchem-562	1	35	european	european	ADJ
eurjchem-562	1	36	journal	journal	PROPN
eurjchem-562	1	37	of	of	ADP
eurjchem-562	1	38	chemistry	chemistry	PROPN
eurjchem-562	1	39	journal	journal	PROPN
eurjchem-562	1	40	homepage	homepage	NOUN
eurjchem-562	1	41	:	:	PUNCT
eurjchem-562	1	42	www.eurjchem.com	www.eurjchem.com	X
eurjchem-562	1	43	tetra‐n‐butylammonium	tetra‐n‐butylammonium	NOUN
eurjchem-562	1	44	fluoride‐mediated	fluoride‐mediated	ADJ
eurjchem-562	1	45	dimerization	dimerization	NOUN
eurjchem-562	1	46	of	of	ADP
eurjchem-562	1	47	(	(	PUNCT
eurjchem-562	1	48	α‐methylbenzylidene)malononitriles	α‐methylbenzylidene)malononitrile	NOUN
eurjchem-562	1	49	to	to	PART
eurjchem-562	1	50	form	form	VERB
eurjchem-562	1	51	polyfunctional	polyfunctional	ADJ
eurjchem-562	1	52	5,6‐dihydropyridines	5,6‐dihydropyridine	NOUN
eurjchem-562	1	53	derivatives	derivative	NOUN
eurjchem-562	1	54	under	under	ADP
eurjchem-562	1	55	solvent‐free	solvent‐free	NOUN
eurjchem-562	1	56	conditions	condition	NOUN
eurjchem-562	1	57	abdul	abdul	PROPN
eurjchem-562	1	58	hameed	hameed	PROPN
eurjchem-562	1	59	*	*	PROPN
eurjchem-562	1	60	,	,	PUNCT
eurjchem-562	1	61	ayaz	ayaz	PROPN
eurjchem-562	1	62	anwar	anwar	PROPN
eurjchem-562	1	63	,	,	PUNCT
eurjchem-562	1	64	sammer	sammer	PROPN
eurjchem-562	1	65	yousaf	yousaf	PROPN
eurjchem-562	1	66	,	,	PUNCT
eurjchem-562	1	67	khalid	khalid	PROPN
eurjchem-562	1	68	mohammed	mohammed	PROPN
eurjchem-562	1	69	khan	khan	PROPN
eurjchem-562	1	70	and	and	CCONJ
eurjchem-562	1	71	fatima	fatima	PROPN
eurjchem-562	1	72	zahra	zahra	PROPN
eurjchem-562	1	73	basha	basha	PROPN
eurjchem-562	1	74	husein	husein	PROPN
eurjchem-562	1	75	ebrahim	ebrahim	PROPN
eurjchem-562	1	76	jamal	jamal	PROPN
eurjchem-562	1	77	research	research	PROPN
eurjchem-562	1	78	institute	institute	PROPN
eurjchem-562	1	79	of	of	ADP
eurjchem-562	1	80	chemistry	chemistry	PROPN
eurjchem-562	1	81	,	,	PUNCT
eurjchem-562	1	82	international	international	ADJ
eurjchem-562	1	83	center	center	NOUN
eurjchem-562	1	84	for	for	ADP
eurjchem-562	1	85	chemical	chemical	NOUN
eurjchem-562	1	86	and	and	CCONJ
eurjchem-562	1	87	biological	biological	ADJ
eurjchem-562	1	88	sciences	science	NOUN
eurjchem-562	1	89	,	,	PUNCT
eurjchem-562	1	90	university	university	PROPN
eurjchem-562	1	91	of	of	ADP
eurjchem-562	1	92	karachi	karachi	PROPN
eurjchem-562	1	93	,	,	PUNCT
eurjchem-562	1	94	karachi	karachi	PROPN
eurjchem-562	1	95	,	,	PUNCT
eurjchem-562	1	96	75270	75270	NUM
eurjchem-562	1	97	,	,	PUNCT
eurjchem-562	1	98	pakistan	pakistan	PROPN
eurjchem-562	1	99	*	*	PUNCT
eurjchem-562	1	100	corresponding	correspond	VERB
eurjchem-562	1	101	author	author	NOUN
eurjchem-562	1	102	at	at	ADP
eurjchem-562	1	103	:	:	PUNCT
eurjchem-562	1	104	husein	husein	PROPN
eurjchem-562	1	105	ebrahim	ebrahim	PROPN
eurjchem-562	1	106	jamal	jamal	PROPN
eurjchem-562	1	107	research	research	PROPN
eurjchem-562	1	108	institute	institute	PROPN
eurjchem-562	1	109	of	of	ADP
eurjchem-562	1	110	chemistry	chemistry	PROPN
eurjchem-562	1	111	,	,	PUNCT
eurjchem-562	1	112	international	international	ADJ
eurjchem-562	1	113	center	center	NOUN
eurjchem-562	1	114	for	for	ADP
eurjchem-562	1	115	chemical	chemical	NOUN
eurjchem-562	1	116	and	and	CCONJ
eurjchem-562	1	117	biological	biological	ADJ
eurjchem-562	1	118	sciences	science	NOUN
eurjchem-562	1	119	,	,	PUNCT
eurjchem-562	1	120	university	university	PROPN
eurjchem-562	1	121	of	of	ADP
eurjchem-562	1	122	karachi	karachi	PROPN
eurjchem-562	1	123	,	,	PUNCT
eurjchem-562	1	124	karachi	karachi	PROPN
eurjchem-562	1	125	,	,	PUNCT
eurjchem-562	1	126	75270	75270	NUM
eurjchem-562	1	127	,	,	PUNCT
eurjchem-562	1	128	pakistan	pakistan	PROPN
eurjchem-562	1	129	.	.	PUNCT
eurjchem-562	2	1	tel	tel	PROPN
eurjchem-562	2	2	.	.	PUNCT
eurjchem-562	2	3	:	:	PUNCT
eurjchem-562	3	1	+92.219.9261701‐2	+92.219.9261701‐2	PROPN
eurjchem-562	3	2	/	/	SYM
eurjchem-562	3	3	ext	ext	NOUN
eurjchem-562	3	4	.	.	PROPN
eurjchem-562	3	5	240	240	NUM
eurjchem-562	3	6	;	;	PUNCT
eurjchem-562	3	7	fax	fax	NOUN
eurjchem-562	3	8	:	:	PUNCT
eurjchem-562	3	9	+92.213.4819018	+92.213.4819018	NUM
eurjchem-562	3	10	.	.	PUNCT
eurjchem-562	3	11	e‐mail	e‐mail	PUNCT
eurjchem-562	4	1	address	address	NOUN
eurjchem-562	4	2	:	:	PUNCT
eurjchem-562	4	3	abdul.hameed@iccs.edu	abdul.hameed@iccs.edu	PROPN
eurjchem-562	4	4	(	(	PUNCT
eurjchem-562	4	5	a.	a.	NOUN
eurjchem-562	4	6	hameed	hameed	PROPN
eurjchem-562	4	7	)	)	PUNCT
eurjchem-562	4	8	.	.	PUNCT
eurjchem-562	5	1	article	article	NOUN
eurjchem-562	5	2	information	information	PROPN
eurjchem-562	5	3	abstract	abstract	ADV
eurjchem-562	5	4	received	receive	VERB
eurjchem-562	5	5	:	:	PUNCT
eurjchem-562	5	6	25	25	NUM
eurjchem-562	5	7	november	november	PROPN
eurjchem-562	5	8	2011	2011	NUM
eurjchem-562	5	9	received	receive	VERB
eurjchem-562	5	10	in	in	ADP
eurjchem-562	5	11	revised	revise	VERB
eurjchem-562	5	12	form	form	NOUN
eurjchem-562	5	13	:	:	PUNCT
eurjchem-562	5	14	09	09	NUM
eurjchem-562	5	15	january	january	PROPN
eurjchem-562	5	16	2012	2012	NUM
eurjchem-562	5	17	accepted	accept	VERB
eurjchem-562	5	18	:	:	PUNCT
eurjchem-562	5	19	09	09	NUM
eurjchem-562	5	20	january	january	PROPN
eurjchem-562	5	21	2012	2012	NUM
eurjchem-562	5	22	online	online	NOUN
eurjchem-562	5	23	:	:	PUNCT
eurjchem-562	5	24	30	30	NUM
eurjchem-562	5	25	june	june	PROPN
eurjchem-562	5	26	2012	2012	NUM
eurjchem-562	5	27	keywords	keyword	VERB
eurjchem-562	5	28	a	a	DET
eurjchem-562	5	29	series	series	NOUN
eurjchem-562	5	30	of	of	ADP
eurjchem-562	5	31	polyfunctional	polyfunctional	ADJ
eurjchem-562	5	32	dihydropyridine	dihydropyridine	NOUN
eurjchem-562	5	33	28‐46	28‐46	NUM
eurjchem-562	5	34	were	be	AUX
eurjchem-562	5	35	prepared	prepare	VERB
eurjchem-562	5	36	via	via	ADP
eurjchem-562	5	37	dimerization	dimerization	NOUN
eurjchem-562	5	38	of	of	ADP
eurjchem-562	5	39	readily	readily	ADV
eurjchem-562	5	40	available	available	ADJ
eurjchem-562	5	41	substituted	substitute	VERB
eurjchem-562	5	42	(	(	PUNCT
eurjchem-562	5	43	‐methylbenzylidene)‐malononitriles	‐methylbenzylidene)‐malononitrile	NOUN
eurjchem-562	5	44	10‐27	10‐27	NOUN
eurjchem-562	5	45	by	by	ADP
eurjchem-562	5	46	treating	treat	VERB
eurjchem-562	5	47	with	with	ADP
eurjchem-562	5	48	neat	neat	ADJ
eurjchem-562	5	49	tbaf.3h2o	tbaf.3h2o	NOUN
eurjchem-562	5	50	under	under	ADP
eurjchem-562	5	51	solvent‐free	solvent‐free	NOUN
eurjchem-562	5	52	conditions	condition	NOUN
eurjchem-562	5	53	at	at	ADP
eurjchem-562	5	54	85‐90	85‐90	NUM
eurjchem-562	5	55	oc	oc	NOUN
eurjchem-562	5	56	.	.	PUNCT
eurjchem-562	6	1	all	all	DET
eurjchem-562	6	2	the	the	DET
eurjchem-562	6	3	dimers	dimer	NOUN
eurjchem-562	6	4	28‐46	28‐46	NUM
eurjchem-562	6	5	were	be	AUX
eurjchem-562	6	6	obtained	obtain	VERB
eurjchem-562	6	7	in	in	ADP
eurjchem-562	6	8	high	high	ADJ
eurjchem-562	6	9	yield	yield	NOUN
eurjchem-562	6	10	from	from	ADP
eurjchem-562	6	11	their	their	PRON
eurjchem-562	6	12	corresponding	corresponding	ADJ
eurjchem-562	6	13	substituted	substitute	VERB
eurjchem-562	6	14	alkylidenemalononitriles	alkylidenemalononitrile	NOUN
eurjchem-562	6	15	except	except	SCONJ
eurjchem-562	6	16	in	in	ADP
eurjchem-562	6	17	the	the	DET
eurjchem-562	6	18	case	case	NOUN
eurjchem-562	6	19	of	of	ADP
eurjchem-562	6	20	2‐chloro	2‐chloro	NUM
eurjchem-562	6	21	(	(	PUNCT
eurjchem-562	6	22	15	15	NUM
eurjchem-562	6	23	)	)	PUNCT
eurjchem-562	6	24	,	,	PUNCT
eurjchem-562	6	25	2‐hydroxy	2‐hydroxy	NUM
eurjchem-562	6	26	(	(	PUNCT
eurjchem-562	6	27	21	21	NUM
eurjchem-562	6	28	)	)	PUNCT
eurjchem-562	6	29	,	,	PUNCT
eurjchem-562	6	30	and	and	CCONJ
eurjchem-562	6	31	2‐nitro	2‐nitro	NUM
eurjchem-562	6	32	(	(	PUNCT
eurjchem-562	6	33	26	26	NUM
eurjchem-562	6	34	)	)	PUNCT
eurjchem-562	6	35	substituted	substitute	VERB
eurjchem-562	6	36	alkylidenemalononitriles	alkylidenemalononitrile	NOUN
eurjchem-562	6	37	where	where	SCONJ
eurjchem-562	6	38	the	the	DET
eurjchem-562	6	39	reaction	reaction	NOUN
eurjchem-562	6	40	was	be	AUX
eurjchem-562	6	41	unsuccessful	unsuccessful	ADJ
eurjchem-562	6	42	due	due	ADP
eurjchem-562	6	43	to	to	ADP
eurjchem-562	6	44	the	the	DET
eurjchem-562	6	45	steric	steric	ADJ
eurjchem-562	6	46	interaction	interaction	NOUN
eurjchem-562	6	47	between	between	ADP
eurjchem-562	6	48	methylene	methylene	NOUN
eurjchem-562	6	49	group	group	NOUN
eurjchem-562	6	50	and	and	CCONJ
eurjchem-562	6	51	the	the	DET
eurjchem-562	6	52	substituents	substituent	NOUN
eurjchem-562	6	53	present	present	ADJ
eurjchem-562	6	54	at	at	ADP
eurjchem-562	6	55	ortho	ortho	PROPN
eurjchem-562	6	56	position	position	NOUN
eurjchem-562	6	57	.	.	PUNCT
eurjchem-562	7	1	the	the	DET
eurjchem-562	7	2	x‐ray	x‐ray	PROPN
eurjchem-562	7	3	crystallographic	crystallographic	ADJ
eurjchem-562	7	4	studies	study	NOUN
eurjchem-562	7	5	of	of	ADP
eurjchem-562	7	6	compounds	compound	NOUN
eurjchem-562	7	7	28	28	NUM
eurjchem-562	7	8	and	and	CCONJ
eurjchem-562	7	9	30	30	NUM
eurjchem-562	7	10	were	be	AUX
eurjchem-562	7	11	carried	carry	VERB
eurjchem-562	7	12	out	out	ADP
eurjchem-562	7	13	to	to	PART
eurjchem-562	7	14	confirm	confirm	VERB
eurjchem-562	7	15	the	the	DET
eurjchem-562	7	16	structure	structure	NOUN
eurjchem-562	7	17	of	of	ADP
eurjchem-562	7	18	dimerized	dimerize	VERB
eurjchem-562	7	19	product	product	NOUN
eurjchem-562	7	20	.	.	PUNCT
eurjchem-562	8	1	the	the	DET
eurjchem-562	8	2	method	method	NOUN
eurjchem-562	8	3	is	be	AUX
eurjchem-562	8	4	eco‐	eco‐	X
eurjchem-562	8	5	friendly	friendly	ADJ
eurjchem-562	8	6	and	and	CCONJ
eurjchem-562	8	7	wider	wide	ADJ
eurjchem-562	8	8	is	be	AUX
eurjchem-562	8	9	scope	scope	NOUN
eurjchem-562	8	10	to	to	PART
eurjchem-562	8	11	prepare	prepare	VERB
eurjchem-562	8	12	a	a	DET
eurjchem-562	8	13	range	range	NOUN
eurjchem-562	8	14	of	of	ADP
eurjchem-562	8	15	substituted	substitute	VERB
eurjchem-562	8	16	dihydropyridine	dihydropyridine	NOUN
eurjchem-562	8	17	derivatives	derivative	NOUN
eurjchem-562	8	18	28‐	28‐	NUM
eurjchem-562	8	19	46	46	NUM
eurjchem-562	8	20	.	.	PUNCT
eurjchem-562	9	1	dimerization	dimerization	NOUN
eurjchem-562	9	2	x‐ray	x‐ray	ADJ
eurjchem-562	9	3	crystallography	crystallography	NOUN
eurjchem-562	9	4	solvent‐free	solvent‐free	NOUN
eurjchem-562	9	5	conditions	condition	NOUN
eurjchem-562	9	6	alkylidenemalononitrile	alkylidenemalononitrile	ADJ
eurjchem-562	9	7	acetophenone	acetophenone	NOUN
eurjchem-562	9	8	derivatives	derivative	NOUN
eurjchem-562	9	9	knoevenagel	knoevenagel	NOUN
eurjchem-562	9	10	condensation	condensation	NOUN
eurjchem-562	9	11	1	1	NUM
eurjchem-562	9	12	.	.	PUNCT
eurjchem-562	10	1	introduction	introduction	NOUN
eurjchem-562	10	2	alkylidenemalononitriles	alkylidenemalononitrile	NOUN
eurjchem-562	10	3	are	be	AUX
eurjchem-562	10	4	important	important	ADJ
eurjchem-562	10	5	class	class	NOUN
eurjchem-562	10	6	of	of	ADP
eurjchem-562	10	7	compounds	compound	NOUN
eurjchem-562	10	8	in	in	ADP
eurjchem-562	10	9	organic	organic	ADJ
eurjchem-562	10	10	chemistry	chemistry	NOUN
eurjchem-562	10	11	.	.	PUNCT
eurjchem-562	11	1	they	they	PRON
eurjchem-562	11	2	are	be	AUX
eurjchem-562	11	3	derived	derive	VERB
eurjchem-562	11	4	from	from	ADP
eurjchem-562	11	5	acetophenone	acetophenone	NOUN
eurjchem-562	11	6	derivatives	derivative	NOUN
eurjchem-562	11	7	via	via	ADP
eurjchem-562	11	8	knoevenagel	knoevenagel	NOUN
eurjchem-562	11	9	condensation	condensation	NOUN
eurjchem-562	11	10	[	[	X
eurjchem-562	11	11	1‐3	1‐3	X
eurjchem-562	11	12	]	]	PUNCT
eurjchem-562	11	13	and	and	CCONJ
eurjchem-562	11	14	frequently	frequently	ADV
eurjchem-562	11	15	used	use	VERB
eurjchem-562	11	16	in	in	ADP
eurjchem-562	11	17	the	the	DET
eurjchem-562	11	18	preparation	preparation	NOUN
eurjchem-562	11	19	of	of	ADP
eurjchem-562	11	20	many	many	ADJ
eurjchem-562	11	21	medicinally	medicinally	ADV
eurjchem-562	11	22	important	important	ADJ
eurjchem-562	11	23	heterocyclic	heterocyclic	ADJ
eurjchem-562	11	24	compounds	compound	NOUN
eurjchem-562	11	25	.	.	PUNCT
eurjchem-562	12	1	pyridine	pyridine	NOUN
eurjchem-562	12	2	ring	ring	NOUN
eurjchem-562	12	3	containing	contain	VERB
eurjchem-562	12	4	compounds	compound	NOUN
eurjchem-562	12	5	are	be	AUX
eurjchem-562	12	6	also	also	ADV
eurjchem-562	12	7	important	important	ADJ
eurjchem-562	12	8	class	class	NOUN
eurjchem-562	12	9	of	of	ADP
eurjchem-562	12	10	the	the	DET
eurjchem-562	12	11	heterocyclic	heterocyclic	ADJ
eurjchem-562	12	12	compounds	compound	NOUN
eurjchem-562	12	13	,	,	PUNCT
eurjchem-562	12	14	which	which	PRON
eurjchem-562	12	15	are	be	AUX
eurjchem-562	12	16	frequently	frequently	ADV
eurjchem-562	12	17	used	use	VERB
eurjchem-562	12	18	in	in	ADP
eurjchem-562	12	19	the	the	DET
eurjchem-562	12	20	many	many	ADJ
eurjchem-562	12	21	fields	field	NOUN
eurjchem-562	12	22	including	include	VERB
eurjchem-562	12	23	medicinal	medicinal	ADJ
eurjchem-562	12	24	chemistry	chemistry	NOUN
eurjchem-562	12	25	,	,	PUNCT
eurjchem-562	12	26	agro	agro	NOUN
eurjchem-562	12	27	chemicals	chemical	NOUN
eurjchem-562	12	28	etc	etc	X
eurjchem-562	12	29	.	.	PUNCT
eurjchem-562	13	1	[	[	X
eurjchem-562	13	2	4	4	NUM
eurjchem-562	13	3	]	]	PUNCT
eurjchem-562	13	4	.	.	PUNCT
eurjchem-562	13	5	pyridine	pyridine	NOUN
eurjchem-562	13	6	ring	ring	NOUN
eurjchem-562	13	7	is	be	AUX
eurjchem-562	13	8	the	the	DET
eurjchem-562	13	9	basic	basic	ADJ
eurjchem-562	13	10	unit	unit	NOUN
eurjchem-562	13	11	in	in	ADP
eurjchem-562	13	12	many	many	ADJ
eurjchem-562	13	13	known	know	VERB
eurjchem-562	13	14	natural	natural	ADJ
eurjchem-562	13	15	products	product	NOUN
eurjchem-562	13	16	and	and	CCONJ
eurjchem-562	13	17	medicinally	medicinally	ADV
eurjchem-562	13	18	important	important	ADJ
eurjchem-562	13	19	compounds	compound	NOUN
eurjchem-562	13	20	[	[	X
eurjchem-562	13	21	5	5	NUM
eurjchem-562	13	22	]	]	PUNCT
eurjchem-562	13	23	.	.	PUNCT
eurjchem-562	14	1	for	for	ADP
eurjchem-562	14	2	example	example	NOUN
eurjchem-562	14	3	,	,	PUNCT
eurjchem-562	14	4	nifedipine	nifedipine	NOUN
eurjchem-562	14	5	1	1	NUM
eurjchem-562	14	6	and	and	CCONJ
eurjchem-562	14	7	its	its	PRON
eurjchem-562	14	8	different	different	ADJ
eurjchem-562	14	9	derivatives4	derivatives4	NOUN
eurjchem-562	14	10	contains	contain	VERB
eurjchem-562	14	11	pyridine	pyridine	NOUN
eurjchem-562	14	12	core	core	NOUN
eurjchem-562	14	13	ring	ring	NOUN
eurjchem-562	14	14	in	in	ADP
eurjchem-562	14	15	their	their	PRON
eurjchem-562	14	16	structure	structure	NOUN
eurjchem-562	14	17	(	(	PUNCT
eurjchem-562	14	18	figure	figure	NOUN
eurjchem-562	14	19	1	1	NUM
eurjchem-562	14	20	)	)	PUNCT
eurjchem-562	14	21	.	.	PUNCT
eurjchem-562	15	1	these	these	DET
eurjchem-562	15	2	compounds	compound	NOUN
eurjchem-562	15	3	show	show	VERB
eurjchem-562	15	4	significant	significant	ADJ
eurjchem-562	15	5	biological	biological	ADJ
eurjchem-562	15	6	potential	potential	NOUN
eurjchem-562	15	7	against	against	ADP
eurjchem-562	15	8	cardiovascular	cardiovascular	ADJ
eurjchem-562	15	9	diseases	disease	NOUN
eurjchem-562	15	10	(	(	PUNCT
eurjchem-562	15	11	calcium	calcium	NOUN
eurjchem-562	15	12	antagonist	antagonist	NOUN
eurjchem-562	15	13	)	)	PUNCT
eurjchem-562	16	1	[	[	X
eurjchem-562	16	2	5,6	5,6	NUM
eurjchem-562	16	3	]	]	PUNCT
eurjchem-562	16	4	.	.	PUNCT
eurjchem-562	17	1	many	many	ADJ
eurjchem-562	17	2	research	research	NOUN
eurjchem-562	17	3	groups	group	NOUN
eurjchem-562	17	4	are	be	AUX
eurjchem-562	17	5	involved	involve	VERB
eurjchem-562	17	6	in	in	ADP
eurjchem-562	17	7	the	the	DET
eurjchem-562	17	8	synthesis	synthesis	NOUN
eurjchem-562	17	9	of	of	ADP
eurjchem-562	17	10	useful	useful	ADJ
eurjchem-562	17	11	pyridine	pyridine	NOUN
eurjchem-562	17	12	derivatives	derivative	NOUN
eurjchem-562	17	13	possessing	possess	VERB
eurjchem-562	17	14	significant	significant	ADJ
eurjchem-562	17	15	biological	biological	ADJ
eurjchem-562	17	16	potential	potential	NOUN
eurjchem-562	17	17	.	.	PUNCT
eurjchem-562	18	1	our	our	PRON
eurjchem-562	18	2	group	group	NOUN
eurjchem-562	18	3	is	be	AUX
eurjchem-562	18	4	also	also	ADV
eurjchem-562	18	5	interested	interested	ADJ
eurjchem-562	18	6	in	in	ADP
eurjchem-562	18	7	the	the	DET
eurjchem-562	18	8	synthesis	synthesis	NOUN
eurjchem-562	18	9	of	of	ADP
eurjchem-562	18	10	potentially	potentially	ADV
eurjchem-562	18	11	useful	useful	ADJ
eurjchem-562	18	12	pyridine	pyridine	ADJ
eurjchem-562	18	13	derivatives	derivative	NOUN
eurjchem-562	18	14	via	via	ADP
eurjchem-562	18	15	efficient	efficient	ADJ
eurjchem-562	18	16	,	,	PUNCT
eurjchem-562	18	17	cost‐effective	cost‐effective	ADJ
eurjchem-562	18	18	and	and	CCONJ
eurjchem-562	18	19	scalable	scalable	ADJ
eurjchem-562	18	20	methods	method	NOUN
eurjchem-562	18	21	.	.	PUNCT
eurjchem-562	19	1	it	it	PRON
eurjchem-562	19	2	is	be	AUX
eurjchem-562	19	3	envisaged	envisage	VERB
eurjchem-562	19	4	that	that	SCONJ
eurjchem-562	19	5	preparation	preparation	NOUN
eurjchem-562	19	6	of	of	ADP
eurjchem-562	19	7	polyfunctional	polyfunctional	ADJ
eurjchem-562	19	8	5,6‐pyridine	5,6‐pyridine	NUM
eurjchem-562	19	9	derivatives	derivative	NOUN
eurjchem-562	19	10	i.e.	i.e.	X
eurjchem-562	19	11	compound	compound	NOUN
eurjchem-562	19	12	2	2	NUM
eurjchem-562	19	13	would	would	AUX
eurjchem-562	19	14	carry	carry	VERB
eurjchem-562	19	15	significant	significant	ADJ
eurjchem-562	19	16	biological	biological	ADJ
eurjchem-562	19	17	interests	interest	NOUN
eurjchem-562	19	18	(	(	PUNCT
eurjchem-562	19	19	figure	figure	NOUN
eurjchem-562	19	20	1	1	NUM
eurjchem-562	19	21	)	)	PUNCT
eurjchem-562	19	22	.	.	PUNCT
eurjchem-562	20	1	towards	towards	ADP
eurjchem-562	20	2	our	our	PRON
eurjchem-562	20	3	interest	interest	NOUN
eurjchem-562	20	4	,	,	PUNCT
eurjchem-562	20	5	readily	readily	ADV
eurjchem-562	20	6	available	available	ADJ
eurjchem-562	20	7	alkylidenemalononitriles	alkylidenemalononitrile	NOUN
eurjchem-562	20	8	10‐27	10‐27	NUM
eurjchem-562	20	9	were	be	AUX
eurjchem-562	20	10	selected	select	VERB
eurjchem-562	20	11	as	as	ADP
eurjchem-562	20	12	suitable	suitable	ADJ
eurjchem-562	20	13	candidates	candidate	NOUN
eurjchem-562	20	14	due	due	ADP
eurjchem-562	20	15	to	to	ADP
eurjchem-562	20	16	the	the	DET
eurjchem-562	20	17	reactive	reactive	ADJ
eurjchem-562	20	18	nature	nature	NOUN
eurjchem-562	20	19	of	of	ADP
eurjchem-562	20	20	the	the	DET
eurjchem-562	20	21	dicyanoolefin	dicyanoolefin	NOUN
eurjchem-562	20	22	and	and	CCONJ
eurjchem-562	20	23	the	the	DET
eurjchem-562	20	24	acidic	acidic	ADJ
eurjchem-562	20	25	nature	nature	NOUN
eurjchem-562	20	26	of	of	ADP
eurjchem-562	20	27	the	the	DET
eurjchem-562	20	28	methyl	methyl	NOUN
eurjchem-562	20	29	group	group	NOUN
eurjchem-562	20	30	.	.	PUNCT
eurjchem-562	21	1	both	both	PRON
eurjchem-562	21	2	of	of	ADP
eurjchem-562	21	3	these	these	DET
eurjchem-562	21	4	functionalities	functionality	NOUN
eurjchem-562	21	5	are	be	AUX
eurjchem-562	21	6	very	very	ADV
eurjchem-562	21	7	advantageous	advantageous	ADJ
eurjchem-562	21	8	in	in	ADP
eurjchem-562	21	9	promoting	promote	VERB
eurjchem-562	21	10	the	the	DET
eurjchem-562	21	11	dimerization	dimerization	NOUN
eurjchem-562	21	12	reaction	reaction	NOUN
eurjchem-562	21	13	to	to	PART
eurjchem-562	21	14	prepare	prepare	VERB
eurjchem-562	21	15	desired	desire	VERB
eurjchem-562	21	16	5,6‐dihydropyridine	5,6‐dihydropyridine	NUM
eurjchem-562	21	17	derivatives	derivative	NOUN
eurjchem-562	21	18	28‐46	28‐46	NUM
eurjchem-562	21	19	(	(	PUNCT
eurjchem-562	21	20	scheme	scheme	NOUN
eurjchem-562	21	21	1	1	NUM
eurjchem-562	21	22	)	)	PUNCT
eurjchem-562	21	23	.	.	PUNCT
eurjchem-562	22	1	previously	previously	ADV
eurjchem-562	22	2	,	,	PUNCT
eurjchem-562	22	3	dunkel	dunkel	NOUN
eurjchem-562	22	4	and	and	CCONJ
eurjchem-562	22	5	heb	heb	NOUN
eurjchem-562	22	6	(	(	PUNCT
eurjchem-562	22	7	1997	1997	NUM
eurjchem-562	22	8	)	)	PUNCT
eurjchem-562	23	1	[	[	X
eurjchem-562	23	2	7	7	X
eurjchem-562	23	3	]	]	PUNCT
eurjchem-562	23	4	reported	report	VERB
eurjchem-562	23	5	the	the	DET
eurjchem-562	23	6	synthesis	synthesis	NOUN
eurjchem-562	23	7	of	of	ADP
eurjchem-562	23	8	different	different	ADJ
eurjchem-562	23	9	dicyano	dicyano	NOUN
eurjchem-562	23	10	substituted	substitute	VERB
eurjchem-562	23	11	dimers	dimer	NOUN
eurjchem-562	23	12	in	in	ADP
eurjchem-562	23	13	the	the	DET
eurjchem-562	23	14	presence	presence	NOUN
eurjchem-562	23	15	of	of	ADP
eurjchem-562	23	16	dimcarb	dimcarb	NOUN
eurjchem-562	23	17	(	(	PUNCT
eurjchem-562	23	18	dimethylamine	dimethylamine	NOUN
eurjchem-562	23	19	carbondioxide	carbondioxide	NOUN
eurjchem-562	23	20	complex	complex	NOUN
eurjchem-562	23	21	)	)	PUNCT
eurjchem-562	23	22	,	,	PUNCT
eurjchem-562	23	23	whilst	whilst	SCONJ
eurjchem-562	23	24	abdelrazak	abdelrazak	NOUN
eurjchem-562	23	25	et	et	PROPN
eurjchem-562	23	26	al	al	PROPN
eurjchem-562	23	27	.	.	PROPN
eurjchem-562	24	1	(	(	PUNCT
eurjchem-562	24	2	2011	2011	NUM
eurjchem-562	24	3	)	)	PUNCT
eurjchem-562	25	1	[	[	X
eurjchem-562	25	2	8	8	NUM
eurjchem-562	25	3	]	]	PUNCT
eurjchem-562	25	4	carried	carry	VERB
eurjchem-562	25	5	out	out	ADP
eurjchem-562	25	6	the	the	DET
eurjchem-562	25	7	dimerization	dimerization	NOUN
eurjchem-562	25	8	of	of	ADP
eurjchem-562	25	9	phenyl	phenyl	NOUN
eurjchem-562	25	10	alkylidenemalononitrile	alkylidenemalononitrile	NOUN
eurjchem-562	25	11	in	in	ADP
eurjchem-562	25	12	ethanol	ethanol	NOUN
eurjchem-562	25	13	by	by	ADP
eurjchem-562	25	14	using	use	VERB
eurjchem-562	25	15	excessive	excessive	ADJ
eurjchem-562	25	16	amount	amount	NOUN
eurjchem-562	25	17	of	of	ADP
eurjchem-562	25	18	naoet	naoet	NOUN
eurjchem-562	25	19	to	to	PART
eurjchem-562	25	20	complete	complete	VERB
eurjchem-562	25	21	the	the	DET
eurjchem-562	25	22	reaction	reaction	NOUN
eurjchem-562	25	23	.	.	PUNCT
eurjchem-562	26	1	however	however	ADV
eurjchem-562	26	2	,	,	PUNCT
eurjchem-562	26	3	we	we	PRON
eurjchem-562	26	4	have	have	AUX
eurjchem-562	26	5	developed	develop	VERB
eurjchem-562	26	6	a	a	DET
eurjchem-562	26	7	novel	novel	ADJ
eurjchem-562	26	8	solvent‐free	solvent‐free	NOUN
eurjchem-562	26	9	method	method	NOUN
eurjchem-562	26	10	,	,	PUNCT
eurjchem-562	26	11	where	where	SCONJ
eurjchem-562	26	12	reaction	reaction	NOUN
eurjchem-562	26	13	is	be	AUX
eurjchem-562	26	14	mediated	mediate	VERB
eurjchem-562	26	15	by	by	ADP
eurjchem-562	26	16	tbaf.3h2o	tbaf.3h2o	PROPN
eurjchem-562	26	17	(	(	PUNCT
eurjchem-562	26	18	tetrabutylammonium	tetrabutylammonium	NOUN
eurjchem-562	26	19	fluoride	fluoride	NOUN
eurjchem-562	26	20	trihydrate	trihydrate	NOUN
eurjchem-562	26	21	)	)	PUNCT
eurjchem-562	26	22	to	to	PART
eurjchem-562	26	23	produce	produce	VERB
eurjchem-562	26	24	highly	highly	ADV
eurjchem-562	26	25	functionalized	functionalize	VERB
eurjchem-562	26	26	compound	compound	NOUN
eurjchem-562	26	27	8	8	NUM
eurjchem-562	26	28	.	.	PUNCT
eurjchem-562	27	1	these	these	DET
eurjchem-562	27	2	conditions	condition	NOUN
eurjchem-562	27	3	are	be	AUX
eurjchem-562	27	4	eco‐friendly	eco‐friendly	ADV
eurjchem-562	27	5	,	,	PUNCT
eurjchem-562	27	6	wider	wide	ADJ
eurjchem-562	27	7	in	in	ADP
eurjchem-562	27	8	scope	scope	NOUN
eurjchem-562	27	9	and	and	CCONJ
eurjchem-562	27	10	free	free	ADJ
eurjchem-562	27	11	of	of	ADP
eurjchem-562	27	12	anhydrous	anhydrous	ADJ
eurjchem-562	27	13	environment	environment	NOUN
eurjchem-562	27	14	.	.	PUNCT
eurjchem-562	28	1	we	we	PRON
eurjchem-562	28	2	have	have	AUX
eurjchem-562	28	3	explored	explore	VERB
eurjchem-562	28	4	this	this	DET
eurjchem-562	28	5	method	method	NOUN
eurjchem-562	28	6	on	on	ADP
eurjchem-562	28	7	a	a	DET
eurjchem-562	28	8	range	range	NOUN
eurjchem-562	28	9	of	of	ADP
eurjchem-562	28	10	different	different	ADJ
eurjchem-562	28	11	substituted	substitute	VERB
eurjchem-562	28	12	alkylidenemalononitriles	alkylidenemalononitrile	NOUN
eurjchem-562	28	13	10‐27	10‐27	NUM
eurjchem-562	28	14	and	and	CCONJ
eurjchem-562	28	15	synthesized	synthesize	VERB
eurjchem-562	28	16	different	different	ADJ
eurjchem-562	28	17	dihydropyridine	dihydropyridine	NOUN
eurjchem-562	28	18	derivatives	derivative	NOUN
eurjchem-562	28	19	28‐46	28‐46	NUM
eurjchem-562	28	20	.	.	PUNCT
eurjchem-562	29	1	figure	figure	NOUN
eurjchem-562	29	2	1	1	NUM
eurjchem-562	29	3	.	.	X
eurjchem-562	29	4	nifedipine	nifedipine	PROPN
eurjchem-562	29	5	and	and	CCONJ
eurjchem-562	29	6	related	relate	VERB
eurjchem-562	29	7	polyfunctional	polyfunctional	ADJ
eurjchem-562	29	8	pyridine	pyridine	ADJ
eurjchem-562	29	9	derivatives	derivative	NOUN
eurjchem-562	29	10	.	.	PUNCT
eurjchem-562	30	1	tbaf	tbaf	PROPN
eurjchem-562	30	2	(	(	PUNCT
eurjchem-562	30	3	tetrabutylammonium	tetrabutylammonium	NOUN
eurjchem-562	30	4	fluoride	fluoride	NOUN
eurjchem-562	30	5	)	)	PUNCT
eurjchem-562	30	6	is	be	AUX
eurjchem-562	30	7	commonly	commonly	ADV
eurjchem-562	30	8	used	use	VERB
eurjchem-562	30	9	as	as	ADP
eurjchem-562	30	10	desylating	desylate	VERB
eurjchem-562	30	11	agent	agent	NOUN
eurjchem-562	30	12	in	in	ADP
eurjchem-562	30	13	organic	organic	ADJ
eurjchem-562	30	14	reactions	reaction	NOUN
eurjchem-562	30	15	[	[	X
eurjchem-562	30	16	9	9	NUM
eurjchem-562	30	17	]	]	PUNCT
eurjchem-562	30	18	.	.	PUNCT
eurjchem-562	31	1	however	however	ADV
eurjchem-562	31	2	,	,	PUNCT
eurjchem-562	31	3	in	in	ADP
eurjchem-562	31	4	last	last	ADJ
eurjchem-562	31	5	few	few	ADJ
eurjchem-562	31	6	years	year	NOUN
eurjchem-562	31	7	chemists	chemist	NOUN
eurjchem-562	31	8	have	have	AUX
eurjchem-562	31	9	explored	explore	VERB
eurjchem-562	31	10	many	many	ADJ
eurjchem-562	31	11	utilities	utility	NOUN
eurjchem-562	31	12	of	of	ADP
eurjchem-562	31	13	this	this	DET
eurjchem-562	31	14	reagent	reagent	NOUN
eurjchem-562	31	15	which	which	PRON
eurjchem-562	31	16	involves	involve	VERB
eurjchem-562	31	17	nucleophilic	nucleophilic	ADJ
eurjchem-562	31	18	substitution	substitution	NOUN
eurjchem-562	31	19	to	to	PART
eurjchem-562	31	20	synthesize	synthesize	VERB
eurjchem-562	31	21	organo‐	organo‐	ADP
eurjchem-562	31	22	fluoro	fluoro	NOUN
eurjchem-562	31	23	compounds	compound	NOUN
eurjchem-562	31	24	[	[	X
eurjchem-562	31	25	10	10	NUM
eurjchem-562	31	26	]	]	PUNCT
eurjchem-562	31	27	,	,	PUNCT
eurjchem-562	31	28	cyclization	cyclization	NOUN
eurjchem-562	31	29	reactions	reaction	NOUN
eurjchem-562	31	30	to	to	PART
eurjchem-562	31	31	produce	produce	VERB
eurjchem-562	31	32	different	different	ADJ
eurjchem-562	31	33	heterocyclic	heterocyclic	NOUN
eurjchem-562	31	34	rings	ring	NOUN
eurjchem-562	31	35	systems	system	NOUN
eurjchem-562	31	36	via	via	ADP
eurjchem-562	31	37	5‐exo‐dig	5‐exo‐dig	NUM
eurjchem-562	31	38	cyclization	cyclization	NOUN
eurjchem-562	31	39	or	or	CCONJ
eurjchem-562	31	40	6‐endo‐dig	6‐endo‐dig	NUM
eurjchem-562	31	41	cyclization	cyclization	NOUN
eurjchem-562	31	42	[	[	X
eurjchem-562	31	43	11‐13	11‐13	VERB
eurjchem-562	31	44	]	]	PUNCT
eurjchem-562	31	45	,	,	PUNCT
eurjchem-562	31	46	oxidation	oxidation	NOUN
eurjchem-562	31	47	of	of	ADP
eurjchem-562	31	48	aromatic	aromatic	ADJ
eurjchem-562	31	49	aldehydes	aldehyde	NOUN
eurjchem-562	31	50	to	to	ADP
eurjchem-562	31	51	benzoic	benzoic	ADJ
eurjchem-562	31	52	acid	acid	NOUN
eurjchem-562	31	53	[	[	X
eurjchem-562	31	54	14	14	NUM
eurjchem-562	31	55	]	]	X
eurjchem-562	32	1	[	[	X
eurjchem-562	32	2	3	3	NUM
eurjchem-562	32	3	+	+	NOUN
eurjchem-562	32	4	2]‐cycloaddition	2]‐cycloaddition	NOUN
eurjchem-562	32	5	(	(	PUNCT
eurjchem-562	32	6	click	click	VERB
eurjchem-562	32	7	chemistry	chemistry	NOUN
eurjchem-562	32	8	)	)	PUNCT
eurjchem-562	33	1	[	[	X
eurjchem-562	33	2	15	15	NUM
eurjchem-562	33	3	]	]	PUNCT
eurjchem-562	33	4	and	and	CCONJ
eurjchem-562	33	5	[	[	X
eurjchem-562	33	6	4	4	NUM
eurjchem-562	33	7	+	+	NUM
eurjchem-562	33	8	2]‐cycloaddition	2]‐cycloaddition	NOUN
eurjchem-562	33	9	[	[	X
eurjchem-562	33	10	16	16	NUM
eurjchem-562	33	11	]	]	PUNCT
eurjchem-562	33	12	.	.	PUNCT
eurjchem-562	34	1	180	180	NUM
eurjchem-562	34	2	hameed	hameed	NOUN
eurjchem-562	34	3	et	et	PROPN
eurjchem-562	34	4	al	al	PROPN
eurjchem-562	34	5	.	.	PUNCT
eurjchem-562	34	6	/	/	SYM
eurjchem-562	34	7	european	european	PROPN
eurjchem-562	34	8	journal	journal	PROPN
eurjchem-562	34	9	of	of	ADP
eurjchem-562	34	10	chemistry	chemistry	NOUN
eurjchem-562	34	11	3	3	NUM
eurjchem-562	34	12	(	(	PUNCT
eurjchem-562	34	13	2	2	NUM
eurjchem-562	34	14	)	)	PUNCT
eurjchem-562	34	15	(	(	PUNCT
eurjchem-562	34	16	2012	2012	NUM
eurjchem-562	34	17	)	)	PUNCT
eurjchem-562	34	18	179‐185	179‐185	NUM
eurjchem-562	34	19	scheme	scheme	NOUN
eurjchem-562	34	20	1	1	NUM
eurjchem-562	34	21	homoallyl	homoallyl	NOUN
eurjchem-562	34	22	coupling	coupling	NOUN
eurjchem-562	34	23	of	of	ADP
eurjchem-562	34	24	aryl	aryl	NOUN
eurjchem-562	34	25	halides	halide	NOUN
eurjchem-562	34	26	[	[	X
eurjchem-562	34	27	17	17	NUM
eurjchem-562	34	28	]	]	PUNCT
eurjchem-562	34	29	,	,	PUNCT
eurjchem-562	34	30	activation	activation	NOUN
eurjchem-562	34	31	of	of	ADP
eurjchem-562	34	32	epoxide	epoxide	NOUN
eurjchem-562	34	33	ring	ring	NOUN
eurjchem-562	34	34	opening	opening	NOUN
eurjchem-562	34	35	with	with	ADP
eurjchem-562	34	36	aryl	aryl	NOUN
eurjchem-562	34	37	sulfonamide	sulfonamide	NOUN
eurjchem-562	34	38	to	to	PART
eurjchem-562	34	39	form	form	VERB
eurjchem-562	34	40	morpholine	morpholine	ADJ
eurjchem-562	34	41	derivatives	derivative	NOUN
eurjchem-562	34	42	[	[	X
eurjchem-562	34	43	18	18	NUM
eurjchem-562	34	44	]	]	PUNCT
eurjchem-562	34	45	and	and	CCONJ
eurjchem-562	34	46	n‐arylation	n‐arylation	NUM
eurjchem-562	34	47	of	of	ADP
eurjchem-562	34	48	benzazoles	benzazole	NOUN
eurjchem-562	34	49	[	[	X
eurjchem-562	34	50	19	19	NUM
eurjchem-562	34	51	]	]	PUNCT
eurjchem-562	34	52	are	be	AUX
eurjchem-562	34	53	some	some	DET
eurjchem-562	34	54	other	other	ADJ
eurjchem-562	34	55	applications	application	NOUN
eurjchem-562	34	56	of	of	ADP
eurjchem-562	34	57	tbaf	tbaf	NOUN
eurjchem-562	34	58	in	in	ADP
eurjchem-562	34	59	organic	organic	ADJ
eurjchem-562	34	60	chemistry	chemistry	NOUN
eurjchem-562	34	61	.	.	PUNCT
eurjchem-562	35	1	thus	thus	ADV
eurjchem-562	35	2	,	,	PUNCT
eurjchem-562	35	3	we	we	PRON
eurjchem-562	35	4	explored	explore	VERB
eurjchem-562	35	5	tbaf.3h2o	tbaf.3h2o	NOUN
eurjchem-562	35	6	as	as	ADP
eurjchem-562	35	7	a	a	DET
eurjchem-562	35	8	base	base	NOUN
eurjchem-562	35	9	for	for	ADP
eurjchem-562	35	10	the	the	DET
eurjchem-562	35	11	dimerization	dimerization	NOUN
eurjchem-562	35	12	of	of	ADP
eurjchem-562	35	13	alkylidenemalononitriles	alkylidenemalononitrile	NOUN
eurjchem-562	35	14	10‐27	10‐27	NUM
eurjchem-562	35	15	under	under	ADP
eurjchem-562	35	16	solvent‐free	solvent‐free	NOUN
eurjchem-562	35	17	conditions	condition	NOUN
eurjchem-562	35	18	.	.	PUNCT
eurjchem-562	36	1	2	2	X
eurjchem-562	36	2	.	.	X
eurjchem-562	36	3	experimental	experimental	ADJ
eurjchem-562	36	4	all	all	DET
eurjchem-562	36	5	the	the	DET
eurjchem-562	36	6	acetophenone	acetophenone	NOUN
eurjchem-562	36	7	derivatives	derivative	NOUN
eurjchem-562	36	8	and	and	CCONJ
eurjchem-562	36	9	other	other	ADJ
eurjchem-562	36	10	starting	start	VERB
eurjchem-562	36	11	materials	material	NOUN
eurjchem-562	36	12	were	be	AUX
eurjchem-562	36	13	used	use	VERB
eurjchem-562	36	14	without	without	ADP
eurjchem-562	36	15	purification	purification	NOUN
eurjchem-562	36	16	unless	unless	SCONJ
eurjchem-562	36	17	otherwise	otherwise	ADV
eurjchem-562	36	18	stated	state	VERB
eurjchem-562	36	19	.	.	PUNCT
eurjchem-562	37	1	infrared	infrared	PROPN
eurjchem-562	37	2	spectra	spectra	PROPN
eurjchem-562	37	3	were	be	AUX
eurjchem-562	37	4	recorded	record	VERB
eurjchem-562	37	5	on	on	ADP
eurjchem-562	37	6	shimadzu	shimadzu	PROPN
eurjchem-562	37	7	ftir	ftir	PROPN
eurjchem-562	37	8	8900	8900	NUM
eurjchem-562	37	9	spectrometer	spectrometer	NOUN
eurjchem-562	37	10	and	and	CCONJ
eurjchem-562	37	11	1h	1h	NUM
eurjchem-562	37	12	nmr	nmr	NOUN
eurjchem-562	37	13	spectra	spectra	NOUN
eurjchem-562	37	14	were	be	AUX
eurjchem-562	37	15	obtained	obtain	VERB
eurjchem-562	37	16	on	on	ADP
eurjchem-562	37	17	bruker	bruker	NOUN
eurjchem-562	37	18	300	300	NUM
eurjchem-562	37	19	mhz	mhz	NOUN
eurjchem-562	37	20	and	and	CCONJ
eurjchem-562	37	21	400	400	NUM
eurjchem-562	37	22	mhz	mhz	ADJ
eurjchem-562	37	23	spectrometers	spectrometer	NOUN
eurjchem-562	37	24	.	.	PUNCT
eurjchem-562	38	1	coupling	couple	VERB
eurjchem-562	38	2	constant	constant	ADJ
eurjchem-562	38	3	were	be	AUX
eurjchem-562	38	4	calculated	calculate	VERB
eurjchem-562	38	5	in	in	ADP
eurjchem-562	38	6	hertz	hertz	NOUN
eurjchem-562	38	7	(	(	PUNCT
eurjchem-562	38	8	hz	hz	PROPN
eurjchem-562	38	9	)	)	PUNCT
eurjchem-562	38	10	.	.	PUNCT
eurjchem-562	39	1	mass	mass	PROPN
eurjchem-562	39	2	spectra	spectra	PROPN
eurjchem-562	39	3	were	be	AUX
eurjchem-562	39	4	obtained	obtain	VERB
eurjchem-562	39	5	at	at	ADP
eurjchem-562	39	6	jeol	jeol	PROPN
eurjchem-562	39	7	ms	ms	PROPN
eurjchem-562	39	8	route	route	PROPN
eurjchem-562	39	9	600	600	NUM
eurjchem-562	39	10	h	h	NOUN
eurjchem-562	39	11	spectrometer	spectrometer	NOUN
eurjchem-562	39	12	by	by	ADP
eurjchem-562	39	13	using	use	VERB
eurjchem-562	39	14	electron	electron	NOUN
eurjchem-562	39	15	impact	impact	NOUN
eurjchem-562	39	16	(	(	PUNCT
eurjchem-562	39	17	ei+	ei+	NOUN
eurjchem-562	39	18	)	)	PUNCT
eurjchem-562	39	19	techniques	technique	NOUN
eurjchem-562	39	20	.	.	PUNCT
eurjchem-562	40	1	hrms	hrm	NOUN
eurjchem-562	40	2	was	be	AUX
eurjchem-562	40	3	carried	carry	VERB
eurjchem-562	40	4	out	out	ADP
eurjchem-562	40	5	at	at	ADP
eurjchem-562	40	6	thermo	thermo	NOUN
eurjchem-562	40	7	finnigan	finnigan	NOUN
eurjchem-562	40	8	mat	mat	PROPN
eurjchem-562	40	9	95xp	95xp	ADJ
eurjchem-562	40	10	instrument	instrument	NOUN
eurjchem-562	40	11	.	.	PUNCT
eurjchem-562	41	1	single	single	ADJ
eurjchem-562	41	2	crystal	crystal	PROPN
eurjchem-562	41	3	x‐ray	x‐ray	PROPN
eurjchem-562	41	4	diffraction	diffraction	PROPN
eurjchem-562	41	5	data	datum	NOUN
eurjchem-562	41	6	was	be	AUX
eurjchem-562	41	7	collected	collect	VERB
eurjchem-562	41	8	on	on	ADP
eurjchem-562	41	9	bruker	bruker	PROPN
eurjchem-562	41	10	smart	smart	PROPN
eurjchem-562	41	11	apex	apex	PROPN
eurjchem-562	41	12	ii	ii	PROPN
eurjchem-562	41	13	,	,	PUNCT
eurjchem-562	41	14	ccd	ccd	PROPN
eurjchem-562	41	15	4‐k	4‐k	PROPN
eurjchem-562	41	16	area	area	NOUN
eurjchem-562	41	17	detector	detector	NOUN
eurjchem-562	41	18	diffractometer	diffractometer	NOUN
eurjchem-562	41	19	.	.	PUNCT
eurjchem-562	42	1	data	datum	NOUN
eurjchem-562	42	2	reductions	reduction	NOUN
eurjchem-562	42	3	were	be	AUX
eurjchem-562	42	4	performed	perform	VERB
eurjchem-562	42	5	by	by	ADP
eurjchem-562	42	6	using	use	VERB
eurjchem-562	42	7	saint	saint	NOUN
eurjchem-562	42	8	program	program	NOUN
eurjchem-562	42	9	and	and	CCONJ
eurjchem-562	42	10	refined	refine	VERB
eurjchem-562	42	11	by	by	ADP
eurjchem-562	42	12	full‐matrix	full‐matrix	NOUN
eurjchem-562	42	13	least	least	ADJ
eurjchem-562	42	14	squares	square	NOUN
eurjchem-562	42	15	on	on	ADP
eurjchem-562	42	16	f2	f2	PROPN
eurjchem-562	42	17	by	by	ADP
eurjchem-562	42	18	using	use	VERB
eurjchem-562	42	19	the	the	DET
eurjchem-562	42	20	shelxtl‐pc	shelxtl‐pc	PROPN
eurjchem-562	42	21	package	package	NOUN
eurjchem-562	42	22	[	[	X
eurjchem-562	42	23	20	20	NUM
eurjchem-562	42	24	]	]	PUNCT
eurjchem-562	42	25	.	.	PUNCT
eurjchem-562	43	1	the	the	DET
eurjchem-562	43	2	figures	figure	NOUN
eurjchem-562	43	3	were	be	AUX
eurjchem-562	43	4	plotted	plot	VERB
eurjchem-562	43	5	with	with	ADP
eurjchem-562	43	6	the	the	DET
eurjchem-562	43	7	aid	aid	NOUN
eurjchem-562	43	8	of	of	ADP
eurjchem-562	43	9	ortep	ortep	NOUN
eurjchem-562	43	10	program	program	NOUN
eurjchem-562	43	11	[	[	X
eurjchem-562	43	12	21	21	NUM
eurjchem-562	43	13	]	]	PUNCT
eurjchem-562	43	14	.	.	PUNCT
eurjchem-562	44	1	the	the	DET
eurjchem-562	44	2	merck	merck	PROPN
eurjchem-562	44	3	silica	silica	NOUN
eurjchem-562	44	4	gel	gel	NOUN
eurjchem-562	44	5	60	60	NUM
eurjchem-562	44	6	was	be	AUX
eurjchem-562	44	7	used	use	VERB
eurjchem-562	44	8	for	for	ADP
eurjchem-562	44	9	column	column	NOUN
eurjchem-562	44	10	chromatography	chromatography	NOUN
eurjchem-562	44	11	.	.	PUNCT
eurjchem-562	45	1	2.1	2.1	NUM
eurjchem-562	45	2	.	.	PUNCT
eurjchem-562	45	3	general	general	ADJ
eurjchem-562	45	4	procedure	procedure	NOUN
eurjchem-562	45	5	for	for	ADP
eurjchem-562	45	6	the	the	DET
eurjchem-562	45	7	synthesis	synthesis	NOUN
eurjchem-562	45	8	of	of	ADP
eurjchem-562	45	9	polyfunctional	polyfunctional	ADJ
eurjchem-562	45	10	5,6‐dihydropyridine	5,6‐dihydropyridine	NUM
eurjchem-562	45	11	derivatives	derivative	NOUN
eurjchem-562	45	12	(	(	PUNCT
eurjchem-562	45	13	28‐46	28‐46	NUM
eurjchem-562	45	14	)	)	PUNCT
eurjchem-562	45	15	in	in	ADP
eurjchem-562	45	16	a	a	DET
eurjchem-562	45	17	typical	typical	ADJ
eurjchem-562	45	18	reaction	reaction	NOUN
eurjchem-562	45	19	,	,	PUNCT
eurjchem-562	45	20	an	an	DET
eurjchem-562	45	21	oven	oven	NOUN
eurjchem-562	45	22	dried	dry	VERB
eurjchem-562	45	23	screw‐capped	screw‐cappe	VERB
eurjchem-562	45	24	vial	vial	ADJ
eurjchem-562	45	25	having	have	VERB
eurjchem-562	45	26	magnetic	magnetic	ADJ
eurjchem-562	45	27	stirrer	stirrer	ADJ
eurjchem-562	45	28	bar	bar	NOUN
eurjchem-562	45	29	was	be	AUX
eurjchem-562	45	30	charged	charge	VERB
eurjchem-562	45	31	with	with	ADP
eurjchem-562	45	32	alkylidene‐	alkylidene‐	PROPN
eurjchem-562	45	33	malononitrile	malononitrile	PROPN
eurjchem-562	45	34	(	(	PUNCT
eurjchem-562	45	35	10‐27	10‐27	NOUN
eurjchem-562	45	36	)	)	PUNCT
eurjchem-562	45	37	(	(	PUNCT
eurjchem-562	45	38	1.0	1.0	NUM
eurjchem-562	45	39	equiv	equiv	NOUN
eurjchem-562	45	40	)	)	PUNCT
eurjchem-562	45	41	and	and	CCONJ
eurjchem-562	45	42	neat	neat	ADJ
eurjchem-562	45	43	tbaf.3h2o	tbaf.3h2o	NOUN
eurjchem-562	45	44	(	(	PUNCT
eurjchem-562	45	45	1.0	1.0	NUM
eurjchem-562	45	46	equiv	equiv	NOUN
eurjchem-562	45	47	)	)	PUNCT
eurjchem-562	45	48	.	.	PUNCT
eurjchem-562	46	1	the	the	DET
eurjchem-562	46	2	reaction	reaction	NOUN
eurjchem-562	46	3	mixture	mixture	NOUN
eurjchem-562	46	4	was	be	AUX
eurjchem-562	46	5	then	then	ADV
eurjchem-562	46	6	heated	heat	VERB
eurjchem-562	46	7	at	at	ADP
eurjchem-562	46	8	85‐90	85‐90	NUM
eurjchem-562	46	9	°	°	SCONJ
eurjchem-562	46	10	c	c	PROPN
eurjchem-562	46	11	with	with	ADP
eurjchem-562	46	12	constant	constant	ADJ
eurjchem-562	46	13	stirring	stirring	NOUN
eurjchem-562	46	14	for	for	ADP
eurjchem-562	46	15	15	15	NUM
eurjchem-562	46	16	h.	h.	NOUN
eurjchem-562	46	17	the	the	DET
eurjchem-562	46	18	completion	completion	NOUN
eurjchem-562	46	19	of	of	ADP
eurjchem-562	46	20	the	the	DET
eurjchem-562	46	21	reaction	reaction	NOUN
eurjchem-562	46	22	was	be	AUX
eurjchem-562	46	23	monitored	monitor	VERB
eurjchem-562	46	24	by	by	ADP
eurjchem-562	46	25	thin	thin	ADJ
eurjchem-562	46	26	layer	layer	NOUN
eurjchem-562	46	27	chromatography	chromatography	NOUN
eurjchem-562	46	28	(	(	PUNCT
eurjchem-562	46	29	tlc	tlc	NOUN
eurjchem-562	46	30	)	)	PUNCT
eurjchem-562	46	31	analysis	analysis	NOUN
eurjchem-562	46	32	.	.	PUNCT
eurjchem-562	47	1	the	the	DET
eurjchem-562	47	2	reaction	reaction	NOUN
eurjchem-562	47	3	mixture	mixture	NOUN
eurjchem-562	47	4	was	be	AUX
eurjchem-562	47	5	cooled	cool	VERB
eurjchem-562	47	6	to	to	ADP
eurjchem-562	47	7	room	room	NOUN
eurjchem-562	47	8	temperature	temperature	NOUN
eurjchem-562	47	9	and	and	CCONJ
eurjchem-562	47	10	diluted	dilute	VERB
eurjchem-562	47	11	with	with	ADP
eurjchem-562	47	12	dioxane	dioxane	NOUN
eurjchem-562	47	13	(	(	PUNCT
eurjchem-562	47	14	2‐3	2‐3	NUM
eurjchem-562	47	15	ml	ml	NOUN
eurjchem-562	47	16	)	)	PUNCT
eurjchem-562	47	17	and	and	CCONJ
eurjchem-562	47	18	then	then	ADV
eurjchem-562	47	19	1.0	1.0	NUM
eurjchem-562	47	20	m	m	NOUN
eurjchem-562	47	21	hcl	hcl	PROPN
eurjchem-562	47	22	(	(	PUNCT
eurjchem-562	47	23	100	100	NUM
eurjchem-562	47	24	ml	ml	NOUN
eurjchem-562	47	25	)	)	PUNCT
eurjchem-562	47	26	aqueous	aqueous	ADJ
eurjchem-562	47	27	solution	solution	NOUN
eurjchem-562	47	28	to	to	PART
eurjchem-562	47	29	remove	remove	VERB
eurjchem-562	47	30	excess	excess	ADJ
eurjchem-562	47	31	tbaf	tbaf	ADJ
eurjchem-562	47	32	.	.	PUNCT
eurjchem-562	48	1	the	the	DET
eurjchem-562	48	2	resulting	result	VERB
eurjchem-562	48	3	mixture	mixture	NOUN
eurjchem-562	48	4	was	be	AUX
eurjchem-562	48	5	stirred	stir	VERB
eurjchem-562	48	6	for	for	ADP
eurjchem-562	48	7	additional	additional	ADJ
eurjchem-562	48	8	5	5	NUM
eurjchem-562	48	9	min	min	NOUN
eurjchem-562	48	10	and	and	CCONJ
eurjchem-562	48	11	then	then	ADV
eurjchem-562	48	12	formed	form	VERB
eurjchem-562	48	13	precipitate	precipitate	NOUN
eurjchem-562	48	14	was	be	AUX
eurjchem-562	48	15	filtered	filter	VERB
eurjchem-562	48	16	and	and	CCONJ
eurjchem-562	48	17	washed	wash	VERB
eurjchem-562	48	18	with	with	ADP
eurjchem-562	48	19	more	more	ADJ
eurjchem-562	48	20	1.0	1.0	NUM
eurjchem-562	48	21	m	m	NOUN
eurjchem-562	48	22	hcl	hcl	PROPN
eurjchem-562	48	23	to	to	PART
eurjchem-562	48	24	give	give	VERB
eurjchem-562	48	25	the	the	DET
eurjchem-562	48	26	pure	pure	ADJ
eurjchem-562	48	27	compounds	compound	NOUN
eurjchem-562	48	28	28‐46	28‐46	NUM
eurjchem-562	48	29	in	in	ADP
eurjchem-562	48	30	good	good	ADJ
eurjchem-562	48	31	to	to	ADP
eurjchem-562	48	32	excellent	excellent	ADJ
eurjchem-562	48	33	yield	yield	NOUN
eurjchem-562	48	34	(	(	PUNCT
eurjchem-562	48	35	52	52	NUM
eurjchem-562	48	36	to	to	PART
eurjchem-562	48	37	95	95	NUM
eurjchem-562	48	38	%	%	NOUN
eurjchem-562	48	39	)	)	PUNCT
eurjchem-562	48	40	.	.	PUNCT
eurjchem-562	49	1	the	the	DET
eurjchem-562	49	2	structure	structure	NOUN
eurjchem-562	49	3	of	of	ADP
eurjchem-562	49	4	these	these	DET
eurjchem-562	49	5	compounds	compound	NOUN
eurjchem-562	49	6	28‐46	28‐46	NUM
eurjchem-562	49	7	was	be	AUX
eurjchem-562	49	8	confirmed	confirm	VERB
eurjchem-562	49	9	by	by	ADP
eurjchem-562	49	10	using	use	VERB
eurjchem-562	49	11	different	different	ADJ
eurjchem-562	49	12	spectroscopic	spectroscopic	ADJ
eurjchem-562	49	13	techniques	technique	NOUN
eurjchem-562	49	14	including	include	VERB
eurjchem-562	49	15	1h	1h	NUM
eurjchem-562	49	16	nmr	nmr	NOUN
eurjchem-562	49	17	,	,	PUNCT
eurjchem-562	49	18	13c	13c	NOUN
eurjchem-562	49	19	nmr	nmr	NOUN
eurjchem-562	49	20	,	,	PUNCT
eurjchem-562	49	21	ei‐hrms	ei‐hrm	NOUN
eurjchem-562	49	22	and	and	CCONJ
eurjchem-562	49	23	ir	ir	PROPN
eurjchem-562	49	24	spectroscopy	spectroscopy	NOUN
eurjchem-562	49	25	.	.	PUNCT
eurjchem-562	50	1	2‐(3‐cyano‐6‐methyl‐4,6‐diphenyl‐5,6‐dihydropyridin‐2(1h)‐	2‐(3‐cyano‐6‐methyl‐4,6‐diphenyl‐5,6‐dihydropyridin‐2(1h)‐	PROPN
eurjchem-562	50	2	ylidene)malono‐nitrile	ylidene)malono‐nitrile	PROPN
eurjchem-562	50	3	(	(	PUNCT
eurjchem-562	50	4	28	28	NUM
eurjchem-562	50	5	):	):	PUNCT
eurjchem-562	50	6	brown	brown	ADJ
eurjchem-562	50	7	solid	solid	NOUN
eurjchem-562	50	8	.	.	PUNCT
eurjchem-562	50	9	yield	yield	NOUN
eurjchem-562	50	10	:	:	PUNCT
eurjchem-562	50	11	98	98	NUM
eurjchem-562	50	12	%	%	NOUN
eurjchem-562	50	13	.	.	PUNCT
eurjchem-562	51	1	m.p	m.p	PROPN
eurjchem-562	51	2	.	.	PROPN
eurjchem-562	51	3	:	:	PUNCT
eurjchem-562	52	1	193‐	193‐	NUM
eurjchem-562	52	2	195	195	NUM
eurjchem-562	52	3	oc	oc	NOUN
eurjchem-562	52	4	[	[	X
eurjchem-562	52	5	lit	lit	ADJ
eurjchem-562	52	6	.	.	PUNCT
eurjchem-562	53	1	[	[	X
eurjchem-562	53	2	7	7	NUM
eurjchem-562	53	3	]	]	SYM
eurjchem-562	53	4	:	:	PUNCT
eurjchem-562	53	5	201‐203	201‐203	NUM
eurjchem-562	53	6	°	°	ADP
eurjchem-562	53	7	c	c	NOUN
eurjchem-562	53	8	)	)	PUNCT
eurjchem-562	53	9	.	.	PUNCT
eurjchem-562	54	1	ir	ir	PROPN
eurjchem-562	54	2	(	(	PUNCT
eurjchem-562	54	3	kbr	kbr	PROPN
eurjchem-562	54	4	,	,	PUNCT
eurjchem-562	54	5	νmax	νmax	NOUN
eurjchem-562	54	6	,	,	PUNCT
eurjchem-562	54	7	cm‐1	cm‐1	PROPN
eurjchem-562	54	8	):	):	PUNCT
eurjchem-562	54	9	3448	3448	NUM
eurjchem-562	54	10	(	(	PUNCT
eurjchem-562	54	11	nh	nh	NOUN
eurjchem-562	54	12	)	)	PUNCT
eurjchem-562	54	13	,	,	PUNCT
eurjchem-562	54	14	2925	2925	NUM
eurjchem-562	54	15	,	,	PUNCT
eurjchem-562	54	16	2215	2215	NUM
eurjchem-562	54	17	,	,	PUNCT
eurjchem-562	54	18	1598	1598	NUM
eurjchem-562	54	19	,	,	PUNCT
eurjchem-562	54	20	1546	1546	NUM
eurjchem-562	54	21	,	,	PUNCT
eurjchem-562	54	22	1445	1445	NUM
eurjchem-562	54	23	,	,	PUNCT
eurjchem-562	54	24	1257	1257	NUM
eurjchem-562	54	25	.	.	PUNCT
eurjchem-562	55	1	1h	1h	NUM
eurjchem-562	55	2	nmr	nmr	NOUN
eurjchem-562	55	3	(	(	PUNCT
eurjchem-562	55	4	300	300	NUM
eurjchem-562	55	5	mhz	mhz	NOUN
eurjchem-562	55	6	,	,	PUNCT
eurjchem-562	55	7	cdcl3	cdcl3	PROPN
eurjchem-562	55	8	,	,	PUNCT
eurjchem-562	55	9	δ	δ	PROPN
eurjchem-562	55	10	,	,	PUNCT
eurjchem-562	55	11	ppm	ppm	NOUN
eurjchem-562	55	12	):	):	PUNCT
eurjchem-562	55	13	7.50‐7.40	7.50‐7.40	NUM
eurjchem-562	55	14	(	(	PUNCT
eurjchem-562	55	15	6h	6h	NUM
eurjchem-562	55	16	,	,	PUNCT
eurjchem-562	55	17	m	m	PROPN
eurjchem-562	55	18	,	,	PUNCT
eurjchem-562	55	19	arh	arh	ADJ
eurjchem-562	55	20	)	)	PUNCT
eurjchem-562	55	21	,	,	PUNCT
eurjchem-562	55	22	7.35	7.35	NUM
eurjchem-562	55	23	(	(	PUNCT
eurjchem-562	55	24	2h	2h	NUM
eurjchem-562	55	25	app	app	X
eurjchem-562	55	26	d	d	PROPN
eurjchem-562	55	27	,	,	PUNCT
eurjchem-562	55	28	j	j	PROPN
eurjchem-562	55	29	=	=	SYM
eurjchem-562	55	30	8.0	8.0	NUM
eurjchem-562	55	31	hz	hz	NOUN
eurjchem-562	55	32	,	,	PUNCT
eurjchem-562	55	33	arh	arh	ADJ
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eurjchem-562	55	35	,	,	PUNCT
eurjchem-562	55	36	7.24	7.24	NUM
eurjchem-562	55	37	(	(	PUNCT
eurjchem-562	55	38	2h	2h	NUM
eurjchem-562	55	39	app	app	X
eurjchem-562	55	40	d	d	PROPN
eurjchem-562	55	41	,	,	PUNCT
eurjchem-562	55	42	j	j	PROPN
eurjchem-562	56	1	=	=	SYM
eurjchem-562	56	2	8.0	8.0	NUM
eurjchem-562	56	3	hz	hz	NOUN
eurjchem-562	56	4	,	,	PUNCT
eurjchem-562	56	5	arh	arh	ADJ
eurjchem-562	56	6	)	)	PUNCT
eurjchem-562	56	7	,	,	PUNCT
eurjchem-562	56	8	6.58	6.58	NUM
eurjchem-562	56	9	(	(	PUNCT
eurjchem-562	56	10	1h	1h	NUM
eurjchem-562	56	11	,	,	PUNCT
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eurjchem-562	56	13	,	,	PUNCT
eurjchem-562	56	14	nh	nh	PROPN
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eurjchem-562	56	16	,	,	PUNCT
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eurjchem-562	56	18	(	(	PUNCT
eurjchem-562	56	19	1h	1h	NUM
eurjchem-562	56	20	,	,	PUNCT
eurjchem-562	56	21	d	d	PROPN
eurjchem-562	56	22	,	,	PUNCT
eurjchem-562	56	23	j	j	PROPN
eurjchem-562	57	1	=	=	SYM
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eurjchem-562	57	3	hz	hz	NOUN
eurjchem-562	57	4	,	,	PUNCT
eurjchem-562	57	5	ch2	ch2	PROPN
eurjchem-562	57	6	)	)	PUNCT
eurjchem-562	57	7	,	,	PUNCT
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eurjchem-562	57	9	(	(	PUNCT
eurjchem-562	57	10	1h	1h	NUM
eurjchem-562	57	11	,	,	PUNCT
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eurjchem-562	57	13	,	,	PUNCT
eurjchem-562	57	14	j	j	PROPN
eurjchem-562	58	1	=	=	SYM
eurjchem-562	59	1	18.0	18.0	NUM
eurjchem-562	60	1	hz	hz	NOUN
eurjchem-562	60	2	,	,	PUNCT
eurjchem-562	60	3	ch2	ch2	PROPN
eurjchem-562	60	4	)	)	PUNCT
eurjchem-562	60	5	,	,	PUNCT
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eurjchem-562	60	7	(	(	PUNCT
eurjchem-562	60	8	3h	3h	NUM
eurjchem-562	60	9	.	.	PUNCT
eurjchem-562	61	1	s	s	X
eurjchem-562	61	2	,	,	PUNCT
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eurjchem-562	61	4	)	)	PUNCT
eurjchem-562	61	5	.	.	PUNCT
eurjchem-562	62	1	13c	13c	NOUN
eurjchem-562	62	2	nmr	nmr	NOUN
eurjchem-562	62	3	(	(	PUNCT
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eurjchem-562	62	5	mhz	mhz	NOUN
eurjchem-562	62	6	,	,	PUNCT
eurjchem-562	62	7	cdcl3	cdcl3	PROPN
eurjchem-562	62	8	,	,	PUNCT
eurjchem-562	62	9	δ	δ	PROPN
eurjchem-562	62	10	,	,	PUNCT
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eurjchem-562	62	12	):	):	PUNCT
eurjchem-562	62	13	166.5	166.5	NUM
eurjchem-562	62	14	,	,	PUNCT
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eurjchem-562	62	16	,	,	PUNCT
eurjchem-562	62	17	141.3	141.3	NUM
eurjchem-562	62	18	,	,	PUNCT
eurjchem-562	62	19	135.5	135.5	NUM
eurjchem-562	62	20	,	,	PUNCT
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eurjchem-562	62	22	,	,	PUNCT
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eurjchem-562	62	24	,	,	PUNCT
eurjchem-562	62	25	129.2	129.2	NUM
eurjchem-562	62	26	,	,	PUNCT
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eurjchem-562	62	28	,	,	PUNCT
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eurjchem-562	62	30	,	,	PUNCT
eurjchem-562	62	31	124.4	124.4	NUM
eurjchem-562	62	32	,	,	PUNCT
eurjchem-562	62	33	114.6	114.6	NUM
eurjchem-562	62	34	,	,	PUNCT
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eurjchem-562	62	36	,	,	PUNCT
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eurjchem-562	62	38	,	,	PUNCT
eurjchem-562	62	39	102.0	102.0	NUM
eurjchem-562	62	40	,	,	PUNCT
eurjchem-562	62	41	56.8	56.8	NUM
eurjchem-562	62	42	,	,	PUNCT
eurjchem-562	62	43	54.2	54.2	NUM
eurjchem-562	62	44	,	,	PUNCT
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eurjchem-562	62	46	,	,	PUNCT
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eurjchem-562	62	48	.	.	PUNCT
eurjchem-562	62	49	hrms	hrm	VERB
eurjchem-562	62	50	calcd	calcd	NOUN
eurjchem-562	62	51	.	.	PUNCT
eurjchem-562	63	1	for	for	ADP
eurjchem-562	63	2	c22h16n4	c22h16n4	PROPN
eurjchem-562	63	3	(	(	PUNCT
eurjchem-562	63	4	m	m	PROPN
eurjchem-562	63	5	):	):	PUNCT
eurjchem-562	63	6	336.1375	336.1375	NUM
eurjchem-562	63	7	,	,	PUNCT
eurjchem-562	63	8	found	find	VERB
eurjchem-562	63	9	:	:	PUNCT
eurjchem-562	63	10	336.1355	336.1355	NUM
eurjchem-562	63	11	.	.	PUNCT
eurjchem-562	64	1	the	the	DET
eurjchem-562	64	2	data	datum	NOUN
eurjchem-562	64	3	are	be	AUX
eurjchem-562	64	4	identical	identical	ADJ
eurjchem-562	64	5	to	to	ADP
eurjchem-562	64	6	those	those	PRON
eurjchem-562	64	7	previously	previously	ADV
eurjchem-562	64	8	reported	report	VERB
eurjchem-562	64	9	[	[	X
eurjchem-562	64	10	8	8	NUM
eurjchem-562	64	11	]	]	PUNCT
eurjchem-562	64	12	.	.	PUNCT
eurjchem-562	65	1	x‐ray	x‐ray	PROPN
eurjchem-562	65	2	crystallographic	crystallographic	ADJ
eurjchem-562	65	3	data	datum	NOUN
eurjchem-562	65	4	:	:	PUNCT
eurjchem-562	65	5	c22h16n4	c22h16n4	PROPN
eurjchem-562	65	6	,	,	PUNCT
eurjchem-562	65	7	(	(	PUNCT
eurjchem-562	65	8	mr	mr	PROPN
eurjchem-562	65	9	=	=	PROPN
eurjchem-562	65	10	336.39	336.39	NUM
eurjchem-562	65	11	g	g	NOUN
eurjchem-562	65	12	/	/	SYM
eurjchem-562	65	13	mol	mol	NOUN
eurjchem-562	65	14	)	)	PUNCT
eurjchem-562	65	15	,	,	PUNCT
eurjchem-562	65	16	monoclinic	monoclinic	ADJ
eurjchem-562	65	17	,	,	PUNCT
eurjchem-562	65	18	space	space	NOUN
eurjchem-562	65	19	group	group	NOUN
eurjchem-562	65	20	p21	p21	PROPN
eurjchem-562	65	21	/	/	SYM
eurjchem-562	65	22	c	c	PROPN
eurjchem-562	65	23	,	,	PUNCT
eurjchem-562	65	24	a	a	PRON
eurjchem-562	65	25	=	=	X
eurjchem-562	65	26	6.4827(6	6.4827(6	NUM
eurjchem-562	65	27	)	)	PUNCT
eurjchem-562	66	1	å	å	NOUN
eurjchem-562	66	2	,	,	PUNCT
eurjchem-562	66	3	b	b	X
eurjchem-562	66	4	=	=	SYM
eurjchem-562	66	5	16.2837(16	16.2837(16	NUM
eurjchem-562	66	6	)	)	PUNCT
eurjchem-562	66	7	å	å	NOUN
eurjchem-562	66	8	,	,	PUNCT
eurjchem-562	66	9	c	c	X
eurjchem-562	66	10	=	=	SYM
eurjchem-562	66	11	17.8649(17	17.8649(17	NUM
eurjchem-562	66	12	)	)	PUNCT
eurjchem-562	66	13	å	å	NOUN
eurjchem-562	66	14	,	,	PUNCT
eurjchem-562	66	15	α	α	NOUN
eurjchem-562	66	16	=	=	SYM
eurjchem-562	66	17	90	90	NUM
eurjchem-562	66	18	◦	◦	NOUN
eurjchem-562	66	19	,	,	PUNCT
eurjchem-562	66	20	β	β	X
eurjchem-562	66	21	=	=	SYM
eurjchem-562	66	22	100.047(2	100.047(2	NUM
eurjchem-562	66	23	)	)	PUNCT
eurjchem-562	66	24	◦	◦	NOUN
eurjchem-562	66	25	,	,	PUNCT
eurjchem-562	66	26	v	v	NOUN
eurjchem-562	66	27	=	=	SYM
eurjchem-562	66	28	1856.9(3)å	1856.9(3)å	PROPN
eurjchem-562	66	29	3	3	NUM
eurjchem-562	66	30	,	,	PUNCT
eurjchem-562	66	31	z	z	NOUN
eurjchem-562	66	32	=	=	SYM
eurjchem-562	66	33	4	4	NUM
eurjchem-562	66	34	,	,	PUNCT
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eurjchem-562	66	36	=	=	SYM
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eurjchem-562	66	38	mg	mg	PROPN
eurjchem-562	66	39	/	/	SYM
eurjchem-562	66	40	m3	m3	PROPN
eurjchem-562	66	41	,	,	PUNCT
eurjchem-562	66	42	f(000	f(000	PROPN
eurjchem-562	66	43	)	)	PUNCT
eurjchem-562	66	44	=	=	SYM
eurjchem-562	66	45	704	704	NUM
eurjchem-562	66	46	,	,	PUNCT
eurjchem-562	66	47	μ(mokα	μ(mokα	NOUN
eurjchem-562	66	48	=	=	SYM
eurjchem-562	66	49	0.71073	0.71073	NUM
eurjchem-562	66	50	å	å	NOUN
eurjchem-562	66	51	,	,	PUNCT
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eurjchem-562	66	54	min	min	PROPN
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eurjchem-562	66	56	:	:	PUNCT
eurjchem-562	66	57	0.9891/0.9656	0.9891/0.9656	NUM
eurjchem-562	66	58	,	,	PUNCT
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eurjchem-562	66	60	dimensions	dimension	NOUN
eurjchem-562	66	61	:	:	PUNCT
eurjchem-562	67	1	0.48	0.48	NUM
eurjchem-562	67	2	x	x	SYM
eurjchem-562	67	3	0.19	0.19	NUM
eurjchem-562	67	4	x	x	SYM
eurjchem-562	67	5	0.15	0.15	NUM
eurjchem-562	67	6	,	,	PUNCT
eurjchem-562	67	7	1.70o	1.70o	NUM
eurjchem-562	67	8	<	<	X
eurjchem-562	67	9			X
eurjchem-562	67	10	<	<	X
eurjchem-562	67	11	25.5o	25.5o	NUM
eurjchem-562	67	12	,	,	PUNCT
eurjchem-562	67	13	10830	10830	NUM
eurjchem-562	67	14	reflections	reflection	NOUN
eurjchem-562	67	15	were	be	AUX
eurjchem-562	67	16	collected	collect	VERB
eurjchem-562	67	17	,	,	PUNCT
eurjchem-562	67	18	of	of	ADP
eurjchem-562	67	19	which	which	PRON
eurjchem-562	67	20	3442	3442	NUM
eurjchem-562	67	21	reflections	reflection	NOUN
eurjchem-562	67	22	were	be	AUX
eurjchem-562	67	23	observed	observe	VERB
eurjchem-562	67	24	(	(	PUNCT
eurjchem-562	67	25	rint	rint	NOUN
eurjchem-562	67	26	=	=	SYM
eurjchem-562	67	27	0.0248	0.0248	NUM
eurjchem-562	67	28	)	)	PUNCT
eurjchem-562	67	29	.	.	PUNCT
eurjchem-562	68	1	the	the	DET
eurjchem-562	68	2	r	r	NOUN
eurjchem-562	68	3	values	value	NOUN
eurjchem-562	68	4	were	be	AUX
eurjchem-562	68	5	:	:	PUNCT
eurjchem-562	68	6	r1	r1	PROPN
eurjchem-562	68	7	=	=	PUNCT
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eurjchem-562	68	9	,	,	PUNCT
eurjchem-562	68	10	wr2	wr2	PROPN
eurjchem-562	68	11	=	=	PROPN
eurjchem-562	68	12	0.1043	0.1043	NUM
eurjchem-562	68	13	for	for	ADP
eurjchem-562	68	14	i	i	PRON
eurjchem-562	68	15			PROPN
eurjchem-562	68	16	2(i	2(i	NUM
eurjchem-562	68	17	)	)	PUNCT
eurjchem-562	68	18	,	,	PUNCT
eurjchem-562	68	19	and	and	CCONJ
eurjchem-562	68	20	r1	r1	PROPN
eurjchem-562	68	21	=	=	SYM
eurjchem-562	68	22	0.0634	0.0634	PROPN
eurjchem-562	68	23	,	,	PUNCT
eurjchem-562	68	24	wr2	wr2	PROPN
eurjchem-562	68	25	=	=	PROPN
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eurjchem-562	68	27	for	for	ADP
eurjchem-562	68	28	all	all	DET
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eurjchem-562	68	30	;	;	PUNCT
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eurjchem-562	68	33	min	min	PROPN
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eurjchem-562	68	37	:	:	PUNCT
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eurjchem-562	68	39	e	e	X
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eurjchem-562	68	41	.	.	PROPN
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eurjchem-562	69	4	29	29	NUM
eurjchem-562	69	5	):	):	PUNCT
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eurjchem-562	69	9	.	.	PUNCT
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eurjchem-562	69	11	:	:	PUNCT
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eurjchem-562	69	13	%	%	NOUN
eurjchem-562	69	14	.	.	PUNCT
eurjchem-562	70	1	m.p	m.p	PROPN
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eurjchem-562	70	3	:	:	PUNCT
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eurjchem-562	71	2	oc	oc	PROPN
eurjchem-562	71	3	.	.	PROPN
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eurjchem-562	71	5	(	(	PUNCT
eurjchem-562	71	6	kbr	kbr	PROPN
eurjchem-562	71	7	,	,	PUNCT
eurjchem-562	71	8	νmax	νmax	NOUN
eurjchem-562	71	9	,	,	PUNCT
eurjchem-562	71	10	cm‐1	cm‐1	PROPN
eurjchem-562	71	11	):	):	PUNCT
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eurjchem-562	71	13	(	(	PUNCT
eurjchem-562	71	14	nh	nh	NOUN
eurjchem-562	71	15	)	)	PUNCT
eurjchem-562	71	16	,	,	PUNCT
eurjchem-562	71	17	3279	3279	NUM
eurjchem-562	71	18	,	,	PUNCT
eurjchem-562	71	19	2923	2923	NUM
eurjchem-562	71	20	,	,	PUNCT
eurjchem-562	71	21	2214	2214	NUM
eurjchem-562	71	22	,	,	PUNCT
eurjchem-562	71	23	1591	1591	NUM
eurjchem-562	71	24	,	,	PUNCT
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eurjchem-562	71	26	,	,	PUNCT
eurjchem-562	71	27	1259	1259	NUM
eurjchem-562	71	28	.	.	PUNCT
eurjchem-562	72	1	1h	1h	NUM
eurjchem-562	72	2	nmr	nmr	NOUN
eurjchem-562	72	3	(	(	PUNCT
eurjchem-562	72	4	300	300	NUM
eurjchem-562	72	5	mhz	mhz	NOUN
eurjchem-562	72	6	,	,	PUNCT
eurjchem-562	72	7	cdcl3	cdcl3	PROPN
eurjchem-562	72	8	,	,	PUNCT
eurjchem-562	72	9	δ	δ	PROPN
eurjchem-562	72	10	,	,	PUNCT
eurjchem-562	72	11	ppm	ppm	NUM
eurjchem-562	72	12	):	):	PUNCT
eurjchem-562	72	13	7.32	7.32	NUM
eurjchem-562	72	14	(	(	PUNCT
eurjchem-562	72	15	2h	2h	NUM
eurjchem-562	72	16	,	,	PUNCT
eurjchem-562	72	17	d	d	NOUN
eurjchem-562	72	18	,	,	PUNCT
eurjchem-562	72	19	j	j	PROPN
eurjchem-562	72	20	=	=	PROPN
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eurjchem-562	72	22	hz	hz	NOUN
eurjchem-562	72	23	,	,	PUNCT
eurjchem-562	72	24	arh	arh	ADJ
eurjchem-562	72	25	)	)	PUNCT
eurjchem-562	72	26	,	,	PUNCT
eurjchem-562	73	1	7.25‐7.18	7.25‐7.18	NUM
eurjchem-562	73	2	(	(	PUNCT
eurjchem-562	73	3	4h	4h	NUM
eurjchem-562	73	4	,	,	PUNCT
eurjchem-562	73	5	m	m	PROPN
eurjchem-562	73	6	,	,	PUNCT
eurjchem-562	73	7	arh	arh	ADJ
eurjchem-562	73	8	)	)	PUNCT
eurjchem-562	73	9	,	,	PUNCT
eurjchem-562	73	10	6.11	6.11	NUM
eurjchem-562	73	11	(	(	PUNCT
eurjchem-562	73	12	2h	2h	NUM
eurjchem-562	73	13	,	,	PUNCT
eurjchem-562	73	14	d	d	NOUN
eurjchem-562	73	15	,	,	PUNCT
eurjchem-562	73	16	j	j	PROPN
eurjchem-562	73	17	=	=	SYM
eurjchem-562	73	18	8.0	8.0	NUM
eurjchem-562	73	19	hz	hz	NOUN
eurjchem-562	73	20	,	,	PUNCT
eurjchem-562	73	21	arh	arh	ADJ
eurjchem-562	73	22	)	)	PUNCT
eurjchem-562	73	23	,	,	PUNCT
eurjchem-562	73	24	6.50	6.50	NUM
eurjchem-562	73	25	(	(	PUNCT
eurjchem-562	73	26	1h	1h	NUM
eurjchem-562	73	27	,	,	PUNCT
eurjchem-562	73	28	br	br	PROPN
eurjchem-562	73	29	s	s	PROPN
eurjchem-562	73	30	,	,	PUNCT
eurjchem-562	73	31	nh	nh	PROPN
eurjchem-562	73	32	)	)	PUNCT
eurjchem-562	73	33	,	,	PUNCT
eurjchem-562	73	34	3.46	3.46	NUM
eurjchem-562	73	35	(	(	PUNCT
eurjchem-562	73	36	1h	1h	NUM
eurjchem-562	73	37	,	,	PUNCT
eurjchem-562	73	38	d	d	PROPN
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eurjchem-562	73	46	,	,	PUNCT
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eurjchem-562	73	80	3h	3h	NUM
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eurjchem-562	74	2	,	,	PUNCT
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eurjchem-562	74	5	.	.	PUNCT
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eurjchem-562	75	53	.	.	PUNCT
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eurjchem-562	76	4	m	m	PROPN
eurjchem-562	76	5	):	):	PUNCT
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eurjchem-562	76	9	:	:	PUNCT
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eurjchem-562	76	11	.	.	NOUN
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eurjchem-562	77	3	(	(	PUNCT
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eurjchem-562	77	5	):	):	PUNCT
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eurjchem-562	77	9	.	.	PUNCT
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eurjchem-562	77	11	:	:	PUNCT
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eurjchem-562	80	3	(	(	PUNCT
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eurjchem-562	80	19	,	,	PUNCT
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eurjchem-562	80	21	=	=	SYM
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eurjchem-562	80	24	,	,	PUNCT
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eurjchem-562	80	30	,	,	PUNCT
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eurjchem-562	80	37	,	,	PUNCT
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eurjchem-562	81	4	,	,	PUNCT
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eurjchem-562	81	12	(	(	PUNCT
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eurjchem-562	81	17	,	,	PUNCT
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eurjchem-562	82	1	=	=	SYM
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eurjchem-562	82	4	,	,	PUNCT
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eurjchem-562	82	8	arh	arh	ADJ
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eurjchem-562	82	20	,	,	PUNCT
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eurjchem-562	83	1	=	=	SYM
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eurjchem-562	83	4	,	,	PUNCT
eurjchem-562	83	5	ch2	ch2	PROPN
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eurjchem-562	83	7	,	,	PUNCT
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eurjchem-562	83	15	=	=	SYM
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eurjchem-562	83	18	,	,	PUNCT
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eurjchem-562	83	21	,	,	PUNCT
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eurjchem-562	83	25	,	,	PUNCT
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eurjchem-562	83	27	,	,	PUNCT
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eurjchem-562	83	30	.	.	PUNCT
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eurjchem-562	84	3	(	(	PUNCT
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eurjchem-562	84	10	,	,	PUNCT
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eurjchem-562	84	16	,	,	PUNCT
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eurjchem-562	84	20	,	,	PUNCT
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eurjchem-562	84	22	,	,	PUNCT
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eurjchem-562	84	24	,	,	PUNCT
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eurjchem-562	84	26	,	,	PUNCT
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eurjchem-562	84	28	,	,	PUNCT
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eurjchem-562	84	30	,	,	PUNCT
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eurjchem-562	84	32	,	,	PUNCT
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eurjchem-562	84	36	,	,	PUNCT
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eurjchem-562	84	44	,	,	PUNCT
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eurjchem-562	84	50	,	,	PUNCT
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eurjchem-562	84	52	,	,	PUNCT
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eurjchem-562	84	54	,	,	PUNCT
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eurjchem-562	85	9	:	:	PUNCT
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eurjchem-562	89	19	,	,	PUNCT
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eurjchem-562	89	25	,	,	PUNCT
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eurjchem-562	89	31	,	,	PUNCT
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eurjchem-562	89	35	,	,	PUNCT
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eurjchem-562	89	42	,	,	PUNCT
eurjchem-562	89	43	f(000	f(000	PROPN
eurjchem-562	89	44	)	)	PUNCT
eurjchem-562	89	45	=	=	SYM
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eurjchem-562	89	47	,	,	PUNCT
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eurjchem-562	89	49	=	=	SYM
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eurjchem-562	89	51	å	å	NOUN
eurjchem-562	89	52	,	,	PUNCT
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eurjchem-562	89	57	:	:	PUNCT
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eurjchem-562	89	59	,	,	PUNCT
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eurjchem-562	89	62	:	:	PUNCT
eurjchem-562	90	1	0.51	0.51	NUM
eurjchem-562	90	2	x	x	SYM
eurjchem-562	90	3	0.31	0.31	NUM
eurjchem-562	90	4	x	x	SYM
eurjchem-562	90	5	0.17	0.17	NUM
eurjchem-562	90	6	,	,	PUNCT
eurjchem-562	90	7	1.42o	1.42o	NUM
eurjchem-562	90	8	<	<	X
eurjchem-562	90	9	hameed	hameed	PROPN
eurjchem-562	90	10	et	et	PROPN
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eurjchem-562	90	13	/	/	SYM
eurjchem-562	90	14	european	european	PROPN
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eurjchem-562	90	18	3	3	NUM
eurjchem-562	90	19	(	(	PUNCT
eurjchem-562	90	20	2	2	NUM
eurjchem-562	90	21	)	)	PUNCT
eurjchem-562	90	22	(	(	PUNCT
eurjchem-562	90	23	2012	2012	NUM
eurjchem-562	90	24	)	)	PUNCT
eurjchem-562	90	25	179‐185	179‐185	NUM
eurjchem-562	91	1	181	181	NUM
eurjchem-562	91	2			X
eurjchem-562	91	3	<	<	X
eurjchem-562	91	4	25.5	25.5	NUM
eurjchem-562	91	5	o	o	NOUN
eurjchem-562	91	6	,	,	PUNCT
eurjchem-562	91	7	10262	10262	NUM
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eurjchem-562	91	11	,	,	PUNCT
eurjchem-562	91	12	of	of	ADP
eurjchem-562	91	13	which	which	PRON
eurjchem-562	91	14	3372	3372	NUM
eurjchem-562	91	15	reflections	reflection	NOUN
eurjchem-562	91	16	were	be	AUX
eurjchem-562	91	17	observed	observe	VERB
eurjchem-562	91	18	(	(	PUNCT
eurjchem-562	91	19	rint	rint	NOUN
eurjchem-562	91	20	=	=	NOUN
eurjchem-562	91	21	0.0162	0.0162	NUM
eurjchem-562	91	22	)	)	PUNCT
eurjchem-562	91	23	.	.	PUNCT
eurjchem-562	92	1	the	the	DET
eurjchem-562	92	2	r	r	NOUN
eurjchem-562	92	3	values	value	NOUN
eurjchem-562	92	4	were	be	AUX
eurjchem-562	92	5	:	:	PUNCT
eurjchem-562	92	6	r1	r1	PROPN
eurjchem-562	92	7	=	=	SYM
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eurjchem-562	92	9	,	,	PUNCT
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eurjchem-562	92	11	=	=	PUNCT
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eurjchem-562	92	13	for	for	ADP
eurjchem-562	92	14	i	i	PRON
eurjchem-562	92	15			PROPN
eurjchem-562	92	16	2(i	2(i	NUM
eurjchem-562	92	17	)	)	PUNCT
eurjchem-562	92	18	,	,	PUNCT
eurjchem-562	92	19	and	and	CCONJ
eurjchem-562	92	20	r1	r1	PROPN
eurjchem-562	92	21	=	=	SYM
eurjchem-562	92	22	0.0434	0.0434	NUM
eurjchem-562	92	23	,	,	PUNCT
eurjchem-562	92	24	wr2	wr2	PROPN
eurjchem-562	92	25	=	=	PROPN
eurjchem-562	92	26	0.1031	0.1031	NUM
eurjchem-562	92	27	for	for	ADP
eurjchem-562	92	28	all	all	DET
eurjchem-562	92	29	data	datum	NOUN
eurjchem-562	92	30	;	;	PUNCT
eurjchem-562	92	31	max	max	PROPN
eurjchem-562	92	32	/	/	SYM
eurjchem-562	92	33	min	min	PROPN
eurjchem-562	92	34	residual	residual	ADJ
eurjchem-562	92	35	electron	electron	NOUN
eurjchem-562	92	36	density	density	NOUN
eurjchem-562	92	37	:	:	PUNCT
eurjchem-562	92	38	0.221/‐0.223	0.221/‐0.223	NUM
eurjchem-562	92	39	e	e	X
eurjchem-562	92	40	å−3	å−3	PROPN
eurjchem-562	92	41	.	.	PROPN
eurjchem-562	92	42	2‐(3‐cyano‐4,6‐bis(3‐fluorophenyl)‐6‐methyl‐5,6‐dihydro	2‐(3‐cyano‐4,6‐bis(3‐fluorophenyl)‐6‐methyl‐5,6‐dihydro	NUM
eurjchem-562	92	43	pyridin‐2(1h)‐ylidene)malononitrile	pyridin‐2(1h)‐ylidene)malononitrile	NOUN
eurjchem-562	92	44	(	(	PUNCT
eurjchem-562	92	45	31	31	NUM
eurjchem-562	92	46	):	):	PUNCT
eurjchem-562	92	47	yellow	yellow	ADJ
eurjchem-562	92	48	solid	solid	ADJ
eurjchem-562	92	49	.	.	PUNCT
eurjchem-562	93	1	yield	yield	NOUN
eurjchem-562	93	2	:	:	PUNCT
eurjchem-562	93	3	75	75	NUM
eurjchem-562	93	4	%	%	NOUN
eurjchem-562	93	5	.	.	PUNCT
eurjchem-562	94	1	m.p	m.p	PROPN
eurjchem-562	94	2	.	.	PROPN
eurjchem-562	94	3	:	:	PUNCT
eurjchem-562	95	1	130‐135	130‐135	NUM
eurjchem-562	95	2	oc	oc	PROPN
eurjchem-562	95	3	.	.	PROPN
eurjchem-562	95	4	ir	ir	PROPN
eurjchem-562	95	5	(	(	PUNCT
eurjchem-562	95	6	kbr	kbr	PROPN
eurjchem-562	95	7	,	,	PUNCT
eurjchem-562	95	8	νmax	νmax	NOUN
eurjchem-562	95	9	,	,	PUNCT
eurjchem-562	95	10	cm‐1	cm‐1	PROPN
eurjchem-562	95	11	):	):	PUNCT
eurjchem-562	95	12	3249	3249	NUM
eurjchem-562	95	13	(	(	PUNCT
eurjchem-562	95	14	nh	nh	NOUN
eurjchem-562	95	15	)	)	PUNCT
eurjchem-562	95	16	,	,	PUNCT
eurjchem-562	95	17	2222	2222	NUM
eurjchem-562	95	18	,	,	PUNCT
eurjchem-562	95	19	2204	2204	NUM
eurjchem-562	95	20	,	,	PUNCT
eurjchem-562	95	21	1614	1614	NUM
eurjchem-562	95	22	,	,	PUNCT
eurjchem-562	95	23	1584	1584	NUM
eurjchem-562	95	24	,	,	PUNCT
eurjchem-562	95	25	1487	1487	NUM
eurjchem-562	95	26	,	,	PUNCT
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eurjchem-562	95	28	,	,	PUNCT
eurjchem-562	95	29	1270	1270	NUM
eurjchem-562	95	30	.	.	PUNCT
eurjchem-562	96	1	1h	1h	NUM
eurjchem-562	96	2	nmr	nmr	NOUN
eurjchem-562	96	3	(	(	PUNCT
eurjchem-562	96	4	400	400	NUM
eurjchem-562	96	5	mhz	mhz	NOUN
eurjchem-562	96	6	,	,	PUNCT
eurjchem-562	96	7	cdcl3	cdcl3	PROPN
eurjchem-562	96	8	,	,	PUNCT
eurjchem-562	96	9	δ	δ	PROPN
eurjchem-562	96	10	,	,	PUNCT
eurjchem-562	96	11	ppm	ppm	NUM
eurjchem-562	96	12	):	):	PUNCT
eurjchem-562	96	13	7.45‐7.39	7.45‐7.39	NUM
eurjchem-562	96	14	(	(	PUNCT
eurjchem-562	96	15	2h	2h	NUM
eurjchem-562	96	16	,	,	PUNCT
eurjchem-562	96	17	m	m	NOUN
eurjchem-562	96	18	,	,	PUNCT
eurjchem-562	96	19	arh	arh	ADJ
eurjchem-562	96	20	)	)	PUNCT
eurjchem-562	96	21	,	,	PUNCT
eurjchem-562	96	22	7.22‐7.15	7.22‐7.15	NUM
eurjchem-562	96	23	(	(	PUNCT
eurjchem-562	96	24	2h	2h	NUM
eurjchem-562	96	25	,	,	PUNCT
eurjchem-562	96	26	m	m	NOUN
eurjchem-562	96	27	,	,	PUNCT
eurjchem-562	96	28	arh	arh	ADJ
eurjchem-562	96	29	)	)	PUNCT
eurjchem-562	96	30	,	,	PUNCT
eurjchem-562	96	31	7.07	7.07	NUM
eurjchem-562	96	32	(	(	PUNCT
eurjchem-562	96	33	1h	1h	NUM
eurjchem-562	96	34	,	,	PUNCT
eurjchem-562	96	35	app	app	X
eurjchem-562	96	36	td	td	NOUN
eurjchem-562	96	37	,	,	PUNCT
eurjchem-562	96	38	j	j	PROPN
eurjchem-562	96	39	=	=	SYM
eurjchem-562	96	40	8.0	8.0	NUM
eurjchem-562	96	41	hz	hz	NOUN
eurjchem-562	96	42	,	,	PUNCT
eurjchem-562	96	43	2.0	2.0	NUM
eurjchem-562	96	44	hz	hz	NOUN
eurjchem-562	96	45	,	,	PUNCT
eurjchem-562	96	46	arh	arh	ADJ
eurjchem-562	96	47	)	)	PUNCT
eurjchem-562	96	48	,	,	PUNCT
eurjchem-562	96	49	7.03‐6.99	7.03‐6.99	NUM
eurjchem-562	96	50	(	(	PUNCT
eurjchem-562	96	51	2h	2h	NUM
eurjchem-562	96	52	,	,	PUNCT
eurjchem-562	96	53	m	m	NOUN
eurjchem-562	96	54	,	,	PUNCT
eurjchem-562	96	55	arh	arh	ADJ
eurjchem-562	96	56	)	)	PUNCT
eurjchem-562	96	57	,	,	PUNCT
eurjchem-562	96	58	6.94	6.94	NUM
eurjchem-562	96	59	(	(	PUNCT
eurjchem-562	96	60	1h	1h	NUM
eurjchem-562	96	61	,	,	PUNCT
eurjchem-562	96	62	app	app	PROPN
eurjchem-562	96	63	dt	dt	PROPN
eurjchem-562	96	64	,	,	PUNCT
eurjchem-562	96	65	7.6	7.6	NUM
eurjchem-562	96	66	,	,	PUNCT
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eurjchem-562	96	68	,	,	PUNCT
eurjchem-562	96	69	arh	arh	ADJ
eurjchem-562	96	70	)	)	PUNCT
eurjchem-562	96	71	,	,	PUNCT
eurjchem-562	96	72	6.15	6.15	NUM
eurjchem-562	96	73	(	(	PUNCT
eurjchem-562	96	74	1h	1h	NUM
eurjchem-562	96	75	,	,	PUNCT
eurjchem-562	96	76	br	br	PROPN
eurjchem-562	96	77	s	s	PROPN
eurjchem-562	96	78	,	,	PUNCT
eurjchem-562	96	79	nh	nh	PROPN
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eurjchem-562	96	81	,	,	PUNCT
eurjchem-562	96	82	3.40	3.40	NUM
eurjchem-562	96	83	(	(	PUNCT
eurjchem-562	96	84	1h	1h	NUM
eurjchem-562	96	85	,	,	PUNCT
eurjchem-562	96	86	d	d	PROPN
eurjchem-562	96	87	,	,	PUNCT
eurjchem-562	96	88	j	j	PROPN
eurjchem-562	97	1	=	=	SYM
eurjchem-562	97	2	18	18	NUM
eurjchem-562	97	3	hz	hz	VERB
eurjchem-562	97	4	,	,	PUNCT
eurjchem-562	97	5	ch2	ch2	PROPN
eurjchem-562	97	6	)	)	PUNCT
eurjchem-562	97	7	,	,	PUNCT
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eurjchem-562	97	9	(	(	PUNCT
eurjchem-562	97	10	1h	1h	NUM
eurjchem-562	97	11	,	,	PUNCT
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eurjchem-562	97	13	,	,	PUNCT
eurjchem-562	97	14	j	j	PROPN
eurjchem-562	97	15	=	=	SYM
eurjchem-562	97	16	18	18	NUM
eurjchem-562	97	17	hz	hz	VERB
eurjchem-562	97	18	,	,	PUNCT
eurjchem-562	97	19	ch2	ch2	PROPN
eurjchem-562	97	20	)	)	PUNCT
eurjchem-562	97	21	,	,	PUNCT
eurjchem-562	97	22	1.79	1.79	NUM
eurjchem-562	97	23	(	(	PUNCT
eurjchem-562	97	24	3h	3h	NUM
eurjchem-562	97	25	,	,	PUNCT
eurjchem-562	97	26	s	s	X
eurjchem-562	97	27	,	,	PUNCT
eurjchem-562	97	28	ch3	ch3	PROPN
eurjchem-562	97	29	)	)	PUNCT
eurjchem-562	97	30	.	.	PUNCT
eurjchem-562	98	1	13c	13c	NOUN
eurjchem-562	98	2	nmr	nmr	NOUN
eurjchem-562	98	3	(	(	PUNCT
eurjchem-562	98	4	100	100	NUM
eurjchem-562	98	5	mhz	mhz	NOUN
eurjchem-562	98	6	,	,	PUNCT
eurjchem-562	98	7	cdcl3	cdcl3	PROPN
eurjchem-562	98	8	,	,	PUNCT
eurjchem-562	98	9	δ	δ	PROPN
eurjchem-562	98	10	,	,	PUNCT
eurjchem-562	98	11	ppm	ppm	NOUN
eurjchem-562	98	12	):	):	PUNCT
eurjchem-562	98	13	164.5	164.5	NUM
eurjchem-562	98	14	,	,	PUNCT
eurjchem-562	98	15	164.1	164.1	NUM
eurjchem-562	98	16	,	,	PUNCT
eurjchem-562	98	17	163.9	163.9	NUM
eurjchem-562	98	18	,	,	PUNCT
eurjchem-562	98	19	162.0	162.0	NUM
eurjchem-562	98	20	,	,	PUNCT
eurjchem-562	98	21	161.4	161.4	NUM
eurjchem-562	98	22	,	,	PUNCT
eurjchem-562	98	23	156.4	156.4	NUM
eurjchem-562	98	24	,	,	PUNCT
eurjchem-562	98	25	144.0	144.0	NUM
eurjchem-562	98	26	,	,	PUNCT
eurjchem-562	98	27	143.9	143.9	NUM
eurjchem-562	98	28	,	,	PUNCT
eurjchem-562	98	29	137.4	137.4	NUM
eurjchem-562	98	30	,	,	PUNCT
eurjchem-562	98	31	137.3	137.3	NUM
eurjchem-562	98	32	,	,	PUNCT
eurjchem-562	98	33	131.4	131.4	NUM
eurjchem-562	98	34	,	,	PUNCT
eurjchem-562	98	35	131.4	131.4	NUM
eurjchem-562	98	36	,	,	PUNCT
eurjchem-562	98	37	131.3	131.3	NUM
eurjchem-562	98	38	,	,	PUNCT
eurjchem-562	98	39	131.2	131.2	NUM
eurjchem-562	98	40	,	,	PUNCT
eurjchem-562	98	41	123.7	123.7	NUM
eurjchem-562	98	42	,	,	PUNCT
eurjchem-562	98	43	123.6	123.6	NUM
eurjchem-562	98	44	,	,	PUNCT
eurjchem-562	98	45	120.1	120.1	NUM
eurjchem-562	98	46	,	,	PUNCT
eurjchem-562	98	47	120.0	120.0	NUM
eurjchem-562	98	48	,	,	PUNCT
eurjchem-562	98	49	119.4	119.4	NUM
eurjchem-562	98	50	,	,	PUNCT
eurjchem-562	98	51	119.2	119.2	NUM
eurjchem-562	98	52	,	,	PUNCT
eurjchem-562	98	53	116.1	116.1	NUM
eurjchem-562	98	54	,	,	PUNCT
eurjchem-562	98	55	115.9	115.9	NUM
eurjchem-562	98	56	,	,	PUNCT
eurjchem-562	98	57	114.9	114.9	NUM
eurjchem-562	98	58	,	,	PUNCT
eurjchem-562	98	59	114.7	114.7	NUM
eurjchem-562	98	60	,	,	PUNCT
eurjchem-562	98	61	114.2	114.2	NUM
eurjchem-562	98	62	,	,	PUNCT
eurjchem-562	98	63	112.1	112.1	NUM
eurjchem-562	98	64	,	,	PUNCT
eurjchem-562	98	65	112.0	112.0	NUM
eurjchem-562	98	66	,	,	PUNCT
eurjchem-562	98	67	111.9	111.9	NUM
eurjchem-562	98	68	,	,	PUNCT
eurjchem-562	98	69	111.8	111.8	NUM
eurjchem-562	98	70	,	,	PUNCT
eurjchem-562	98	71	103.0	103.0	NUM
eurjchem-562	98	72	,	,	PUNCT
eurjchem-562	98	73	56.6	56.6	NUM
eurjchem-562	98	74	,	,	PUNCT
eurjchem-562	98	75	56.5	56.5	NUM
eurjchem-562	98	76	,	,	PUNCT
eurjchem-562	98	77	55.6	55.6	NUM
eurjchem-562	98	78	,	,	PUNCT
eurjchem-562	98	79	45.5	45.5	NUM
eurjchem-562	98	80	.	.	PUNCT
eurjchem-562	98	81	hrms	hrm	VERB
eurjchem-562	98	82	calcd	calcd	NOUN
eurjchem-562	98	83	.	.	PUNCT
eurjchem-562	99	1	for	for	ADP
eurjchem-562	99	2	c24h14f2n4	c24h14f2n4	PROPN
eurjchem-562	99	3	(	(	PUNCT
eurjchem-562	99	4	m	m	PROPN
eurjchem-562	99	5	):	):	PUNCT
eurjchem-562	99	6	372.1187	372.1187	NUM
eurjchem-562	99	7	,	,	PUNCT
eurjchem-562	99	8	found	find	VERB
eurjchem-562	99	9	:	:	PUNCT
eurjchem-562	99	10	372.1176	372.1176	NUM
eurjchem-562	99	11	.	.	PUNCT
eurjchem-562	100	1	2‐(3‐cyano‐4,6‐bis(4‐chlorophenyl)‐6‐methyl‐5,6‐dihydro	2‐(3‐cyano‐4,6‐bis(4‐chlorophenyl)‐6‐methyl‐5,6‐dihydro	NUM
eurjchem-562	100	2	pyridin‐2(1h)‐ylidene)malononitrile	pyridin‐2(1h)‐ylidene)malononitrile	NOUN
eurjchem-562	100	3	(	(	PUNCT
eurjchem-562	100	4	32	32	NUM
eurjchem-562	100	5	):	):	PUNCT
eurjchem-562	100	6	brown	brown	ADJ
eurjchem-562	100	7	solid	solid	ADJ
eurjchem-562	100	8	.	.	PUNCT
eurjchem-562	101	1	yield	yield	NOUN
eurjchem-562	101	2	:	:	PUNCT
eurjchem-562	101	3	90	90	NUM
eurjchem-562	101	4	%	%	NOUN
eurjchem-562	101	5	.	.	PUNCT
eurjchem-562	102	1	m.p	m.p	PROPN
eurjchem-562	102	2	.	.	PROPN
eurjchem-562	102	3	:	:	PUNCT
eurjchem-562	102	4	132‐135	132‐135	PROPN
eurjchem-562	102	5	oc	oc	VERB
eurjchem-562	102	6	.	.	PROPN
eurjchem-562	103	1	ir	ir	PROPN
eurjchem-562	103	2	(	(	PUNCT
eurjchem-562	103	3	kbr	kbr	PROPN
eurjchem-562	103	4	,	,	PUNCT
eurjchem-562	103	5	νmax	νmax	NOUN
eurjchem-562	103	6	,	,	PUNCT
eurjchem-562	103	7	cm‐1	cm‐1	PROPN
eurjchem-562	103	8	):	):	PUNCT
eurjchem-562	103	9	3449	3449	NUM
eurjchem-562	103	10	(	(	PUNCT
eurjchem-562	103	11	nh	nh	NOUN
eurjchem-562	103	12	)	)	PUNCT
eurjchem-562	103	13	,	,	PUNCT
eurjchem-562	103	14	2218	2218	NUM
eurjchem-562	103	15	,	,	PUNCT
eurjchem-562	103	16	1593	1593	NUM
eurjchem-562	103	17	,	,	PUNCT
eurjchem-562	103	18	1542	1542	NUM
eurjchem-562	103	19	,	,	PUNCT
eurjchem-562	103	20	1489	1489	NUM
eurjchem-562	103	21	,	,	PUNCT
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eurjchem-562	103	23	.	.	PUNCT
eurjchem-562	104	1	1h	1h	NUM
eurjchem-562	104	2	nmr	nmr	NOUN
eurjchem-562	104	3	(	(	PUNCT
eurjchem-562	104	4	300	300	NUM
eurjchem-562	104	5	mhz	mhz	NOUN
eurjchem-562	104	6	,	,	PUNCT
eurjchem-562	104	7	cdcl3	cdcl3	PROPN
eurjchem-562	104	8	,	,	PUNCT
eurjchem-562	104	9	δ	δ	PROPN
eurjchem-562	104	10	,	,	PUNCT
eurjchem-562	104	11	ppm	ppm	NUM
eurjchem-562	104	12	):	):	PUNCT
eurjchem-562	104	13	7.42	7.42	NUM
eurjchem-562	104	14	(	(	PUNCT
eurjchem-562	104	15	4h	4h	NUM
eurjchem-562	104	16	,	,	PUNCT
eurjchem-562	104	17	app	app	PROPN
eurjchem-562	104	18	t	t	PROPN
eurjchem-562	104	19	,	,	PUNCT
eurjchem-562	104	20	j	j	PROPN
eurjchem-562	104	21	=	=	SYM
eurjchem-562	104	22	8.8	8.8	NUM
eurjchem-562	104	23	hz	hz	NOUN
eurjchem-562	104	24	,	,	PUNCT
eurjchem-562	104	25	arh	arh	ADJ
eurjchem-562	104	26	)	)	PUNCT
eurjchem-562	104	27	,	,	PUNCT
eurjchem-562	104	28	7.22	7.22	NUM
eurjchem-562	104	29	(	(	PUNCT
eurjchem-562	104	30	2h	2h	NUM
eurjchem-562	104	31	,	,	PUNCT
eurjchem-562	104	32	d	d	NOUN
eurjchem-562	104	33	,	,	PUNCT
eurjchem-562	104	34	j=	j=	PROPN
eurjchem-562	104	35	8.7	8.7	NUM
eurjchem-562	104	36	hz	hz	NOUN
eurjchem-562	104	37	,	,	PUNCT
eurjchem-562	104	38	arh	arh	ADJ
eurjchem-562	104	39	)	)	PUNCT
eurjchem-562	104	40	,	,	PUNCT
eurjchem-562	104	41	7.16	7.16	NUM
eurjchem-562	104	42	(	(	PUNCT
eurjchem-562	104	43	2h	2h	NUM
eurjchem-562	104	44	,	,	PUNCT
eurjchem-562	104	45	d	d	NOUN
eurjchem-562	104	46	,	,	PUNCT
eurjchem-562	104	47	j	j	PROPN
eurjchem-562	105	1	=	=	SYM
eurjchem-562	105	2	8.7	8.7	NUM
eurjchem-562	105	3	hz	hz	NOUN
eurjchem-562	105	4	,	,	PUNCT
eurjchem-562	105	5	arh	arh	ADJ
eurjchem-562	105	6	)	)	PUNCT
eurjchem-562	105	7	,	,	PUNCT
eurjchem-562	105	8	6.43	6.43	NUM
eurjchem-562	105	9	(	(	PUNCT
eurjchem-562	105	10	1h	1h	NUM
eurjchem-562	105	11	,	,	PUNCT
eurjchem-562	105	12	br	br	PROPN
eurjchem-562	105	13	s	s	PROPN
eurjchem-562	105	14	,	,	PUNCT
eurjchem-562	105	15	nh	nh	PROPN
eurjchem-562	105	16	)	)	PUNCT
eurjchem-562	105	17	,	,	PUNCT
eurjchem-562	105	18	3.39	3.39	NUM
eurjchem-562	105	19	(	(	PUNCT
eurjchem-562	105	20	1h	1h	NUM
eurjchem-562	105	21	,	,	PUNCT
eurjchem-562	105	22	d	d	PROPN
eurjchem-562	105	23	,	,	PUNCT
eurjchem-562	105	24	j	j	PROPN
eurjchem-562	105	25	=	=	SYM
eurjchem-562	105	26	18	18	NUM
eurjchem-562	105	27	hz	hz	VERB
eurjchem-562	105	28	,	,	PUNCT
eurjchem-562	105	29	ch2	ch2	PROPN
eurjchem-562	105	30	)	)	PUNCT
eurjchem-562	105	31	,	,	PUNCT
eurjchem-562	105	32	3.15	3.15	NUM
eurjchem-562	105	33	(	(	PUNCT
eurjchem-562	105	34	1h	1h	NUM
eurjchem-562	105	35	,	,	PUNCT
eurjchem-562	105	36	d	d	PROPN
eurjchem-562	105	37	,	,	PUNCT
eurjchem-562	105	38	j	j	PROPN
eurjchem-562	105	39	=	=	SYM
eurjchem-562	105	40	18	18	NUM
eurjchem-562	105	41	hz	hz	VERB
eurjchem-562	105	42	,	,	PUNCT
eurjchem-562	105	43	ch2	ch2	PROPN
eurjchem-562	105	44	)	)	PUNCT
eurjchem-562	105	45	,	,	PUNCT
eurjchem-562	105	46	1.78	1.78	NUM
eurjchem-562	105	47	(	(	PUNCT
eurjchem-562	105	48	3h	3h	NUM
eurjchem-562	105	49	.	.	PUNCT
eurjchem-562	106	1	s	s	X
eurjchem-562	106	2	,	,	PUNCT
eurjchem-562	106	3	ch3	ch3	PROPN
eurjchem-562	106	4	)	)	PUNCT
eurjchem-562	106	5	.	.	PUNCT
eurjchem-562	107	1	13c	13c	NOUN
eurjchem-562	107	2	nmr	nmr	NOUN
eurjchem-562	107	3	(	(	PUNCT
eurjchem-562	107	4	100	100	NUM
eurjchem-562	107	5	mhz	mhz	NOUN
eurjchem-562	107	6	,	,	PUNCT
eurjchem-562	107	7	cdcl3	cdcl3	PROPN
eurjchem-562	107	8	,	,	PUNCT
eurjchem-562	107	9	δ	δ	PROPN
eurjchem-562	107	10	,	,	PUNCT
eurjchem-562	107	11	ppm	ppm	NOUN
eurjchem-562	107	12	):	):	PUNCT
eurjchem-562	107	13	164.9	164.9	NUM
eurjchem-562	107	14	,	,	PUNCT
eurjchem-562	107	15	156.9	156.9	NUM
eurjchem-562	107	16	,	,	PUNCT
eurjchem-562	107	17	139.9	139.9	NUM
eurjchem-562	107	18	,	,	PUNCT
eurjchem-562	107	19	138.8	138.8	NUM
eurjchem-562	107	20	,	,	PUNCT
eurjchem-562	107	21	134.7	134.7	NUM
eurjchem-562	107	22	,	,	PUNCT
eurjchem-562	107	23	133.7	133.7	NUM
eurjchem-562	107	24	,	,	PUNCT
eurjchem-562	107	25	129.6	129.6	NUM
eurjchem-562	107	26	,	,	PUNCT
eurjchem-562	107	27	129.6	129.6	NUM
eurjchem-562	107	28	,	,	PUNCT
eurjchem-562	107	29	129.3	129.3	NUM
eurjchem-562	107	30	,	,	PUNCT
eurjchem-562	107	31	125.9	125.9	NUM
eurjchem-562	107	32	,	,	PUNCT
eurjchem-562	107	33	114.5	114.5	NUM
eurjchem-562	107	34	,	,	PUNCT
eurjchem-562	107	35	112.6	112.6	NUM
eurjchem-562	107	36	,	,	PUNCT
eurjchem-562	107	37	112.6	112.6	NUM
eurjchem-562	107	38	,	,	PUNCT
eurjchem-562	107	39	102.2	102.2	NUM
eurjchem-562	107	40	,	,	PUNCT
eurjchem-562	107	41	56.6	56.6	NUM
eurjchem-562	107	42	,	,	PUNCT
eurjchem-562	107	43	54.4	54.4	NUM
eurjchem-562	107	44	,	,	PUNCT
eurjchem-562	107	45	45.3	45.3	NUM
eurjchem-562	107	46	,	,	PUNCT
eurjchem-562	107	47	29.3	29.3	NUM
eurjchem-562	107	48	.	.	PUNCT
eurjchem-562	107	49	hrms	hrm	VERB
eurjchem-562	107	50	calcd	calcd	NOUN
eurjchem-562	107	51	.	.	PUNCT
eurjchem-562	108	1	for	for	ADP
eurjchem-562	108	2	c22h14cl2n4	c22h14cl2n4	PROPN
eurjchem-562	108	3	(	(	PUNCT
eurjchem-562	108	4	m	m	PROPN
eurjchem-562	108	5	):	):	PUNCT
eurjchem-562	108	6	404.0596	404.0596	NUM
eurjchem-562	108	7	,	,	PUNCT
eurjchem-562	108	8	found	find	VERB
eurjchem-562	108	9	:	:	PUNCT
eurjchem-562	108	10	404.0571	404.0571	NUM
eurjchem-562	108	11	.	.	PUNCT
eurjchem-562	109	1	2‐(3‐cyano‐4,6‐bis(4‐bromophenyl)‐6‐methyl‐5,6‐dihydro	2‐(3‐cyano‐4,6‐bis(4‐bromophenyl)‐6‐methyl‐5,6‐dihydro	NUM
eurjchem-562	110	1	pyridin‐2(1h)‐ylidene)malononitrile	pyridin‐2(1h)‐ylidene)malononitrile	NOUN
eurjchem-562	110	2	(	(	PUNCT
eurjchem-562	110	3	34	34	NUM
eurjchem-562	110	4	):	):	PUNCT
eurjchem-562	110	5	dark	dark	ADJ
eurjchem-562	110	6	brown	brown	PROPN
eurjchem-562	110	7	solid	solid	ADJ
eurjchem-562	110	8	.	.	PUNCT
eurjchem-562	110	9	yield	yield	NOUN
eurjchem-562	110	10	:	:	PUNCT
eurjchem-562	110	11	90	90	NUM
eurjchem-562	110	12	%	%	NOUN
eurjchem-562	110	13	.	.	PUNCT
eurjchem-562	111	1	m.p	m.p	PROPN
eurjchem-562	111	2	.	.	PROPN
eurjchem-562	111	3	:	:	PUNCT
eurjchem-562	112	1	138‐140	138‐140	NUM
eurjchem-562	112	2	oc	oc	NOUN
eurjchem-562	112	3	.	.	PUNCT
eurjchem-562	112	4	ir	ir	PROPN
eurjchem-562	112	5	(	(	PUNCT
eurjchem-562	112	6	kbr	kbr	PROPN
eurjchem-562	112	7	,	,	PUNCT
eurjchem-562	112	8	νmax	νmax	NOUN
eurjchem-562	112	9	,	,	PUNCT
eurjchem-562	112	10	cm‐1	cm‐1	PROPN
eurjchem-562	112	11	):	):	PUNCT
eurjchem-562	112	12	3438	3438	NUM
eurjchem-562	112	13	(	(	PUNCT
eurjchem-562	112	14	nh	nh	NOUN
eurjchem-562	112	15	)	)	PUNCT
eurjchem-562	112	16	,	,	PUNCT
eurjchem-562	112	17	1591	1591	NUM
eurjchem-562	112	18	,	,	PUNCT
eurjchem-562	112	19	1544	1544	NUM
eurjchem-562	112	20	,	,	PUNCT
eurjchem-562	112	21	1429	1429	NUM
eurjchem-562	112	22	,	,	PUNCT
eurjchem-562	112	23	1259	1259	NUM
eurjchem-562	112	24	.	.	PUNCT
eurjchem-562	113	1	1h	1h	NUM
eurjchem-562	113	2	nmr	nmr	NOUN
eurjchem-562	113	3	(	(	PUNCT
eurjchem-562	113	4	400	400	NUM
eurjchem-562	113	5	mhz	mhz	NOUN
eurjchem-562	113	6	,	,	PUNCT
eurjchem-562	113	7	cdcl3	cdcl3	PROPN
eurjchem-562	113	8	,	,	PUNCT
eurjchem-562	113	9	δ	δ	PROPN
eurjchem-562	113	10	,	,	PUNCT
eurjchem-562	113	11	ppm	ppm	NOUN
eurjchem-562	113	12	):	):	PUNCT
eurjchem-562	113	13	7.56	7.56	NUM
eurjchem-562	113	14	(	(	PUNCT
eurjchem-562	113	15	4h	4h	NUM
eurjchem-562	113	16	,	,	PUNCT
eurjchem-562	113	17	app	app	PROPN
eurjchem-562	113	18	dd	dd	PROPN
eurjchem-562	113	19	,	,	PUNCT
eurjchem-562	113	20	j	j	PROPN
eurjchem-562	113	21	=	=	SYM
eurjchem-562	113	22	16	16	NUM
eurjchem-562	113	23	hz	hz	VERB
eurjchem-562	113	24	,	,	PUNCT
eurjchem-562	113	25	8.4	8.4	NUM
eurjchem-562	113	26	hz	hz	NOUN
eurjchem-562	113	27	,	,	PUNCT
eurjchem-562	113	28	arh	arh	ADJ
eurjchem-562	113	29	)	)	PUNCT
eurjchem-562	113	30	,	,	PUNCT
eurjchem-562	113	31	7.21	7.21	NUM
eurjchem-562	113	32	(	(	PUNCT
eurjchem-562	113	33	2h	2h	NUM
eurjchem-562	113	34	,	,	PUNCT
eurjchem-562	113	35	d	d	NOUN
eurjchem-562	113	36	,	,	PUNCT
eurjchem-562	113	37	j	j	PROPN
eurjchem-562	114	1	=	=	PROPN
eurjchem-562	114	2	8.4	8.4	NUM
eurjchem-562	114	3	hz	hz	NOUN
eurjchem-562	114	4	,	,	PUNCT
eurjchem-562	114	5	arh	arh	ADJ
eurjchem-562	114	6	)	)	PUNCT
eurjchem-562	114	7	,	,	PUNCT
eurjchem-562	114	8	7.09	7.09	NUM
eurjchem-562	114	9	(	(	PUNCT
eurjchem-562	114	10	2h	2h	NUM
eurjchem-562	114	11	,	,	PUNCT
eurjchem-562	114	12	d	d	NOUN
eurjchem-562	114	13	,	,	PUNCT
eurjchem-562	114	14	j	j	PROPN
eurjchem-562	114	15	=	=	PROPN
eurjchem-562	114	16	8.4	8.4	NUM
eurjchem-562	114	17	hz	hz	NOUN
eurjchem-562	114	18	,	,	PUNCT
eurjchem-562	114	19	arh	arh	ADJ
eurjchem-562	114	20	)	)	PUNCT
eurjchem-562	114	21	,	,	PUNCT
eurjchem-562	114	22	6.83	6.83	NUM
eurjchem-562	114	23	(	(	PUNCT
eurjchem-562	114	24	1h	1h	NUM
eurjchem-562	114	25	,	,	PUNCT
eurjchem-562	114	26	br	br	PROPN
eurjchem-562	114	27	s	s	PROPN
eurjchem-562	114	28	,	,	PUNCT
eurjchem-562	114	29	nh	nh	PROPN
eurjchem-562	114	30	)	)	PUNCT
eurjchem-562	114	31	,	,	PUNCT
eurjchem-562	114	32	3.38	3.38	NUM
eurjchem-562	114	33	(	(	PUNCT
eurjchem-562	114	34	1h	1h	NUM
eurjchem-562	114	35	,	,	PUNCT
eurjchem-562	114	36	d	d	PROPN
eurjchem-562	114	37	,	,	PUNCT
eurjchem-562	114	38	j	j	PROPN
eurjchem-562	114	39	=	=	SYM
eurjchem-562	114	40	18	18	NUM
eurjchem-562	114	41	hz	hz	VERB
eurjchem-562	114	42	,	,	PUNCT
eurjchem-562	114	43	ch2	ch2	PROPN
eurjchem-562	114	44	)	)	PUNCT
eurjchem-562	114	45	,	,	PUNCT
eurjchem-562	114	46	3.15	3.15	NUM
eurjchem-562	114	47	(	(	PUNCT
eurjchem-562	114	48	1h	1h	NUM
eurjchem-562	114	49	,	,	PUNCT
eurjchem-562	114	50	d	d	PROPN
eurjchem-562	114	51	,	,	PUNCT
eurjchem-562	114	52	j	j	PROPN
eurjchem-562	114	53	=	=	SYM
eurjchem-562	114	54	18	18	NUM
eurjchem-562	114	55	hz	hz	VERB
eurjchem-562	114	56	,	,	PUNCT
eurjchem-562	114	57	ch2	ch2	PROPN
eurjchem-562	114	58	)	)	PUNCT
eurjchem-562	114	59	,	,	PUNCT
eurjchem-562	114	60	1.77	1.77	NUM
eurjchem-562	114	61	(	(	PUNCT
eurjchem-562	114	62	3h	3h	NUM
eurjchem-562	114	63	,	,	PUNCT
eurjchem-562	114	64	s	s	X
eurjchem-562	114	65	,	,	PUNCT
eurjchem-562	114	66	ch3	ch3	PROPN
eurjchem-562	114	67	):	):	PUNCT
eurjchem-562	114	68	13c	13c	NOUN
eurjchem-562	114	69	nmr	nmr	NOUN
eurjchem-562	114	70	(	(	PUNCT
eurjchem-562	114	71	100	100	NUM
eurjchem-562	114	72	mhz	mhz	NOUN
eurjchem-562	114	73	,	,	PUNCT
eurjchem-562	114	74	cdcl3	cdcl3	PROPN
eurjchem-562	114	75	,	,	PUNCT
eurjchem-562	114	76	δ	δ	PROPN
eurjchem-562	114	77	,	,	PUNCT
eurjchem-562	114	78	ppm	ppm	NOUN
eurjchem-562	114	79	):	):	PUNCT
eurjchem-562	114	80	167.3	167.3	NUM
eurjchem-562	114	81	,	,	PUNCT
eurjchem-562	114	82	157.2	157.2	NUM
eurjchem-562	114	83	,	,	PUNCT
eurjchem-562	114	84	142.3	142.3	NUM
eurjchem-562	114	85	,	,	PUNCT
eurjchem-562	114	86	134.4	134.4	NUM
eurjchem-562	114	87	,	,	PUNCT
eurjchem-562	114	88	132.0	132.0	NUM
eurjchem-562	114	89	,	,	PUNCT
eurjchem-562	114	90	132.5	132.5	NUM
eurjchem-562	114	91	,	,	PUNCT
eurjchem-562	114	92	130.2	130.2	NUM
eurjchem-562	114	93	,	,	PUNCT
eurjchem-562	114	94	127.3	127.3	NUM
eurjchem-562	114	95	,	,	PUNCT
eurjchem-562	114	96	125.9	125.9	NUM
eurjchem-562	114	97	,	,	PUNCT
eurjchem-562	114	98	120.8	120.8	NUM
eurjchem-562	114	99	,	,	PUNCT
eurjchem-562	114	100	115.3	115.3	NUM
eurjchem-562	114	101	,	,	PUNCT
eurjchem-562	114	102	114.6	114.6	NUM
eurjchem-562	114	103	,	,	PUNCT
eurjchem-562	114	104	113.4	113.4	NUM
eurjchem-562	114	105	,	,	PUNCT
eurjchem-562	114	106	101.4	101.4	NUM
eurjchem-562	114	107	,	,	PUNCT
eurjchem-562	114	108	56.7	56.7	NUM
eurjchem-562	114	109	,	,	PUNCT
eurjchem-562	114	110	50.0	50.0	NUM
eurjchem-562	114	111	,	,	PUNCT
eurjchem-562	114	112	43.5	43.5	NUM
eurjchem-562	114	113	,	,	PUNCT
eurjchem-562	114	114	28.0	28.0	NUM
eurjchem-562	114	115	.	.	PUNCT
eurjchem-562	115	1	hrms	hrm	VERB
eurjchem-562	115	2	calcd	calcd	NOUN
eurjchem-562	115	3	.	.	PUNCT
eurjchem-562	116	1	for	for	ADP
eurjchem-562	116	2	c22h15br2n4	c22h15br2n4	PROPN
eurjchem-562	116	3	(	(	PUNCT
eurjchem-562	116	4	m+h	m+h	PROPN
eurjchem-562	116	5	):	):	PUNCT
eurjchem-562	116	6	492.9663	492.9663	NUM
eurjchem-562	116	7	,	,	PUNCT
eurjchem-562	116	8	found	find	VERB
eurjchem-562	116	9	:	:	PUNCT
eurjchem-562	116	10	492.9691	492.9691	NUM
eurjchem-562	116	11	.	.	PUNCT
eurjchem-562	117	1	2‐(3‐cyano‐4,6‐bis(3‐bromophenyl)‐6‐methyl‐5,6‐dihydro	2‐(3‐cyano‐4,6‐bis(3‐bromophenyl)‐6‐methyl‐5,6‐dihydro	NUM
eurjchem-562	117	2	pyridin‐2(1h)‐ylidene)malononitrile	pyridin‐2(1h)‐ylidene)malononitrile	NOUN
eurjchem-562	117	3	(	(	PUNCT
eurjchem-562	117	4	35	35	NUM
eurjchem-562	117	5	):	):	PUNCT
eurjchem-562	117	6	yellow	yellow	ADJ
eurjchem-562	117	7	solid	solid	ADJ
eurjchem-562	117	8	.	.	PUNCT
eurjchem-562	117	9	yield	yield	NOUN
eurjchem-562	117	10	:	:	PUNCT
eurjchem-562	117	11	84	84	NUM
eurjchem-562	117	12	%	%	NOUN
eurjchem-562	117	13	.	.	PUNCT
eurjchem-562	118	1	m.p	m.p	PROPN
eurjchem-562	118	2	.	.	PROPN
eurjchem-562	118	3	:	:	PUNCT
eurjchem-562	119	1	148‐150	148‐150	PROPN
eurjchem-562	119	2	oc	oc	PROPN
eurjchem-562	119	3	.	.	PROPN
eurjchem-562	120	1	ir	ir	PROPN
eurjchem-562	120	2	(	(	PUNCT
eurjchem-562	120	3	kbr	kbr	PROPN
eurjchem-562	120	4	,	,	PUNCT
eurjchem-562	120	5	νmax	νmax	NOUN
eurjchem-562	120	6	,	,	PUNCT
eurjchem-562	120	7	cm‐1	cm‐1	PROPN
eurjchem-562	120	8	):	):	PUNCT
eurjchem-562	120	9	3447	3447	NUM
eurjchem-562	120	10	(	(	PUNCT
eurjchem-562	120	11	nh	nh	NOUN
eurjchem-562	120	12	)	)	PUNCT
eurjchem-562	120	13	,	,	PUNCT
eurjchem-562	120	14	3285	3285	NUM
eurjchem-562	120	15	,	,	PUNCT
eurjchem-562	120	16	2220	2220	NUM
eurjchem-562	120	17	,	,	PUNCT
eurjchem-562	120	18	2190	2190	NUM
eurjchem-562	120	19	,	,	PUNCT
eurjchem-562	120	20	1585	1585	NUM
eurjchem-562	120	21	,	,	PUNCT
eurjchem-562	120	22	1560	1560	NUM
eurjchem-562	120	23	,	,	PUNCT
eurjchem-562	120	24	1433	1433	NUM
eurjchem-562	120	25	,	,	PUNCT
eurjchem-562	120	26	1408	1408	NUM
eurjchem-562	120	27	.	.	PUNCT
eurjchem-562	121	1	1h	1h	NUM
eurjchem-562	121	2	nmr	nmr	NOUN
eurjchem-562	121	3	(	(	PUNCT
eurjchem-562	121	4	400	400	NUM
eurjchem-562	121	5	mhz	mhz	NOUN
eurjchem-562	121	6	,	,	PUNCT
eurjchem-562	121	7	cdcl3	cdcl3	PROPN
eurjchem-562	121	8	,	,	PUNCT
eurjchem-562	121	9	δ	δ	PROPN
eurjchem-562	121	10	,	,	PUNCT
eurjchem-562	121	11	ppm	ppm	NUM
eurjchem-562	121	12	):	):	PUNCT
eurjchem-562	121	13	7.63	7.63	NUM
eurjchem-562	121	14	(	(	PUNCT
eurjchem-562	121	15	1h	1h	NUM
eurjchem-562	121	16	,	,	PUNCT
eurjchem-562	121	17	app	app	PROPN
eurjchem-562	121	18	dt	dt	PROPN
eurjchem-562	121	19	,	,	PUNCT
eurjchem-562	121	20	j	j	PROPN
eurjchem-562	121	21	=	=	PROPN
eurjchem-562	121	22	6.4	6.4	NUM
eurjchem-562	121	23	hz	hz	VERB
eurjchem-562	121	24	,	,	PUNCT
eurjchem-562	121	25	1.6	1.6	NUM
eurjchem-562	121	26	hz	hz	NOUN
eurjchem-562	121	27	,	,	PUNCT
eurjchem-562	121	28	arh	arh	ADJ
eurjchem-562	121	29	)	)	PUNCT
eurjchem-562	121	30	,	,	PUNCT
eurjchem-562	121	31	7.51	7.51	NUM
eurjchem-562	121	32	(	(	PUNCT
eurjchem-562	121	33	1h	1h	NUM
eurjchem-562	121	34	,	,	PUNCT
eurjchem-562	121	35	d	d	PROPN
eurjchem-562	121	36	,	,	PUNCT
eurjchem-562	121	37	j	j	PROPN
eurjchem-562	122	1	=	=	SYM
eurjchem-562	122	2	7.6	7.6	NUM
eurjchem-562	122	3	hz	hz	NOUN
eurjchem-562	122	4	,	,	PUNCT
eurjchem-562	122	5	arh	arh	ADJ
eurjchem-562	122	6	)	)	PUNCT
eurjchem-562	122	7	,	,	PUNCT
eurjchem-562	122	8	7.40	7.40	NUM
eurjchem-562	122	9	(	(	PUNCT
eurjchem-562	122	10	2h	2h	NUM
eurjchem-562	122	11	,	,	PUNCT
eurjchem-562	122	12	app	app	PROPN
eurjchem-562	122	13	d	d	PROPN
eurjchem-562	122	14	,	,	PUNCT
eurjchem-562	122	15	j	j	PROPN
eurjchem-562	122	16	=	=	PROPN
eurjchem-562	122	17	6.4	6.4	NUM
eurjchem-562	122	18	hz	hz	NOUN
eurjchem-562	122	19	,	,	PUNCT
eurjchem-562	122	20	arh	arh	ADJ
eurjchem-562	122	21	)	)	PUNCT
eurjchem-562	122	22	,	,	PUNCT
eurjchem-562	122	23	7.34‐7.30	7.34‐7.30	PROPN
eurjchem-562	122	24	(	(	PUNCT
eurjchem-562	122	25	h	h	NOUN
eurjchem-562	122	26	,	,	PUNCT
eurjchem-562	122	27	m	m	PROPN
eurjchem-562	122	28	,	,	PUNCT
eurjchem-562	122	29	arh	arh	ADJ
eurjchem-562	122	30	)	)	PUNCT
eurjchem-562	122	31	,	,	PUNCT
eurjchem-562	122	32	7.16	7.16	NUM
eurjchem-562	122	33	(	(	PUNCT
eurjchem-562	122	34	1h	1h	NUM
eurjchem-562	122	35	,	,	PUNCT
eurjchem-562	122	36	d	d	PROPN
eurjchem-562	122	37	,	,	PUNCT
eurjchem-562	122	38	j	j	PROPN
eurjchem-562	122	39	=	=	SYM
eurjchem-562	122	40	7.6	7.6	NUM
eurjchem-562	122	41	hz	hz	NOUN
eurjchem-562	122	42	,	,	PUNCT
eurjchem-562	122	43	arh	arh	ADJ
eurjchem-562	122	44	)	)	PUNCT
eurjchem-562	122	45	,	,	PUNCT
eurjchem-562	122	46	6.15	6.15	NUM
eurjchem-562	122	47	(	(	PUNCT
eurjchem-562	122	48	1h	1h	NUM
eurjchem-562	122	49	,	,	PUNCT
eurjchem-562	122	50	br	br	PROPN
eurjchem-562	122	51	s	s	PROPN
eurjchem-562	122	52	,	,	PUNCT
eurjchem-562	122	53	nh	nh	PROPN
eurjchem-562	122	54	)	)	PUNCT
eurjchem-562	122	55	,	,	PUNCT
eurjchem-562	122	56	3.39	3.39	NUM
eurjchem-562	122	57	(	(	PUNCT
eurjchem-562	122	58	1h	1h	NUM
eurjchem-562	122	59	,	,	PUNCT
eurjchem-562	122	60	d	d	PROPN
eurjchem-562	122	61	,	,	PUNCT
eurjchem-562	122	62	j	j	PROPN
eurjchem-562	123	1	=	=	SYM
eurjchem-562	123	2	18	18	NUM
eurjchem-562	123	3	hz	hz	VERB
eurjchem-562	123	4	,	,	PUNCT
eurjchem-562	123	5	ch2	ch2	PROPN
eurjchem-562	123	6	)	)	PUNCT
eurjchem-562	123	7	,	,	PUNCT
eurjchem-562	123	8	3.14	3.14	NUM
eurjchem-562	123	9	(	(	PUNCT
eurjchem-562	123	10	1h	1h	NUM
eurjchem-562	123	11	,	,	PUNCT
eurjchem-562	123	12	d	d	PROPN
eurjchem-562	123	13	,	,	PUNCT
eurjchem-562	123	14	j	j	PROPN
eurjchem-562	123	15	=	=	SYM
eurjchem-562	123	16	18	18	NUM
eurjchem-562	123	17	hz	hz	VERB
eurjchem-562	123	18	,	,	PUNCT
eurjchem-562	123	19	ch2	ch2	PROPN
eurjchem-562	123	20	)	)	PUNCT
eurjchem-562	123	21	,	,	PUNCT
eurjchem-562	123	22	1.79	1.79	NUM
eurjchem-562	123	23	(	(	PUNCT
eurjchem-562	123	24	3h	3h	NUM
eurjchem-562	123	25	,	,	PUNCT
eurjchem-562	123	26	s	s	X
eurjchem-562	123	27	,	,	PUNCT
eurjchem-562	123	28	ch3	ch3	PROPN
eurjchem-562	123	29	)	)	PUNCT
eurjchem-562	123	30	.	.	PUNCT
eurjchem-562	124	1	13c	13c	NOUN
eurjchem-562	124	2	nmr	nmr	NOUN
eurjchem-562	124	3	(	(	PUNCT
eurjchem-562	124	4	100	100	NUM
eurjchem-562	124	5	mhz	mhz	NOUN
eurjchem-562	124	6	,	,	PUNCT
eurjchem-562	124	7	cdcl3	cdcl3	PROPN
eurjchem-562	124	8	,	,	PUNCT
eurjchem-562	124	9	δ	δ	PROPN
eurjchem-562	124	10	,	,	PUNCT
eurjchem-562	124	11	ppm	ppm	NUM
eurjchem-562	124	12	):	):	PUNCT
eurjchem-562	124	13	163.9	163.9	NUM
eurjchem-562	124	14	,	,	PUNCT
eurjchem-562	124	15	156.2	156.2	NUM
eurjchem-562	124	16	,	,	PUNCT
eurjchem-562	124	17	143.6	143.6	NUM
eurjchem-562	124	18	,	,	PUNCT
eurjchem-562	124	19	173.3	173.3	NUM
eurjchem-562	124	20	,	,	PUNCT
eurjchem-562	124	21	135.2	135.2	NUM
eurjchem-562	124	22	,	,	PUNCT
eurjchem-562	124	23	132.2	132.2	NUM
eurjchem-562	124	24	,	,	PUNCT
eurjchem-562	124	25	131.1	131.1	NUM
eurjchem-562	124	26	,	,	PUNCT
eurjchem-562	124	27	130.8	130.8	NUM
eurjchem-562	124	28	,	,	PUNCT
eurjchem-562	124	29	130.4	130.4	NUM
eurjchem-562	124	30	,	,	PUNCT
eurjchem-562	124	31	127.8	127.8	NUM
eurjchem-562	124	32	,	,	PUNCT
eurjchem-562	124	33	126.4	126.4	NUM
eurjchem-562	124	34	,	,	PUNCT
eurjchem-562	124	35	123.8	123.8	NUM
eurjchem-562	124	36	,	,	PUNCT
eurjchem-562	124	37	123.4	123.4	NUM
eurjchem-562	124	38	,	,	PUNCT
eurjchem-562	124	39	123.1	123.1	NUM
eurjchem-562	124	40	,	,	PUNCT
eurjchem-562	124	41	114.1	114.1	NUM
eurjchem-562	124	42	,	,	PUNCT
eurjchem-562	124	43	111.9	111.9	NUM
eurjchem-562	124	44	,	,	PUNCT
eurjchem-562	124	45	111.8	111.8	NUM
eurjchem-562	124	46	,	,	PUNCT
eurjchem-562	124	47	103.2	103.2	NUM
eurjchem-562	124	48	,	,	PUNCT
eurjchem-562	124	49	56.5	56.5	NUM
eurjchem-562	124	50	,	,	PUNCT
eurjchem-562	124	51	55.8	55.8	NUM
eurjchem-562	124	52	,	,	PUNCT
eurjchem-562	124	53	45.4	45.4	NUM
eurjchem-562	124	54	,	,	PUNCT
eurjchem-562	124	55	29.2	29.2	NUM
eurjchem-562	124	56	.	.	PUNCT
eurjchem-562	125	1	hrms	hrm	VERB
eurjchem-562	125	2	calcd	calcd	NOUN
eurjchem-562	125	3	.	.	PUNCT
eurjchem-562	126	1	for	for	ADP
eurjchem-562	126	2	c22h15br2n4	c22h15br2n4	PROPN
eurjchem-562	126	3	(	(	PUNCT
eurjchem-562	126	4	m+h	m+h	PROPN
eurjchem-562	126	5	):	):	PUNCT
eurjchem-562	126	6	492.9663	492.9663	NUM
eurjchem-562	126	7	,	,	PUNCT
eurjchem-562	126	8	found	find	VERB
eurjchem-562	126	9	:	:	PUNCT
eurjchem-562	126	10	492.9691	492.9691	NUM
eurjchem-562	126	11	.	.	PUNCT
eurjchem-562	127	1	2‐(3‐cyano‐4,6‐bis(4‐iodophenyl)‐6‐methyl‐5,6‐dihydro	2‐(3‐cyano‐4,6‐bis(4‐iodophenyl)‐6‐methyl‐5,6‐dihydro	NUM
eurjchem-562	127	2	pyridin‐2(1h)‐ylidene)malononitrile	pyridin‐2(1h)‐ylidene)malononitrile	NOUN
eurjchem-562	127	3	(	(	PUNCT
eurjchem-562	127	4	36	36	NUM
eurjchem-562	127	5	):	):	PUNCT
eurjchem-562	127	6	yellow	yellow	ADJ
eurjchem-562	127	7	solid	solid	ADJ
eurjchem-562	127	8	.	.	PUNCT
eurjchem-562	127	9	yield	yield	NOUN
eurjchem-562	127	10	:	:	PUNCT
eurjchem-562	127	11	89	89	NUM
eurjchem-562	127	12	%	%	NOUN
eurjchem-562	127	13	.	.	PUNCT
eurjchem-562	128	1	mixture	mixture	NOUN
eurjchem-562	128	2	(	(	PUNCT
eurjchem-562	128	3	4/1	4/1	NUM
eurjchem-562	128	4	ratio	ratio	NOUN
eurjchem-562	128	5	)	)	PUNCT
eurjchem-562	128	6	of	of	ADP
eurjchem-562	128	7	36/47	36/47	NUM
eurjchem-562	128	8	.	.	PUNCT
eurjchem-562	129	1	ir	ir	PROPN
eurjchem-562	129	2	(	(	PUNCT
eurjchem-562	129	3	kbr	kbr	PROPN
eurjchem-562	129	4	,	,	PUNCT
eurjchem-562	129	5	νmax	νmax	NOUN
eurjchem-562	129	6	,	,	PUNCT
eurjchem-562	129	7	cm‐1	cm‐1	PROPN
eurjchem-562	129	8	):	):	PUNCT
eurjchem-562	129	9	3441	3441	NUM
eurjchem-562	129	10	(	(	PUNCT
eurjchem-562	129	11	nh	nh	NOUN
eurjchem-562	129	12	)	)	PUNCT
eurjchem-562	129	13	,	,	PUNCT
eurjchem-562	129	14	1589	1589	NUM
eurjchem-562	129	15	,	,	PUNCT
eurjchem-562	129	16	1548	1548	NUM
eurjchem-562	129	17	,	,	PUNCT
eurjchem-562	129	18	1429	1429	NUM
eurjchem-562	129	19	,	,	PUNCT
eurjchem-562	129	20	1261	1261	NUM
eurjchem-562	129	21	.	.	PUNCT
eurjchem-562	130	1	1h	1h	NUM
eurjchem-562	130	2	nmr	nmr	NOUN
eurjchem-562	130	3	(	(	PUNCT
eurjchem-562	130	4	300	300	NUM
eurjchem-562	130	5	mhz	mhz	NOUN
eurjchem-562	130	6	,	,	PUNCT
eurjchem-562	130	7	cdcl3	cdcl3	PROPN
eurjchem-562	130	8	,	,	PUNCT
eurjchem-562	130	9	δ	δ	PROPN
eurjchem-562	130	10	,	,	PUNCT
eurjchem-562	130	11	ppm	ppm	NUM
eurjchem-562	130	12	):	):	PUNCT
eurjchem-562	130	13	7.77	7.77	NUM
eurjchem-562	130	14	(	(	PUNCT
eurjchem-562	130	15	4h	4h	NUM
eurjchem-562	130	16	,	,	PUNCT
eurjchem-562	130	17	app	app	PROPN
eurjchem-562	130	18	dd	dd	PROPN
eurjchem-562	130	19	,	,	PUNCT
eurjchem-562	130	20	j	j	PROPN
eurjchem-562	130	21	=	=	SYM
eurjchem-562	130	22	17	17	NUM
eurjchem-562	130	23	hz	hz	VERB
eurjchem-562	130	24	,	,	PUNCT
eurjchem-562	130	25	8.8	8.8	NUM
eurjchem-562	130	26	hz	hz	NOUN
eurjchem-562	130	27	,	,	PUNCT
eurjchem-562	130	28	arh	arh	ADJ
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eurjchem-562	130	30	,	,	PUNCT
eurjchem-562	130	31	7.07	7.07	NUM
eurjchem-562	130	32	(	(	PUNCT
eurjchem-562	130	33	2h	2h	NUM
eurjchem-562	130	34	,	,	PUNCT
eurjchem-562	130	35	d	d	NOUN
eurjchem-562	130	36	,	,	PUNCT
eurjchem-562	130	37	j	j	PROPN
eurjchem-562	130	38	=	=	PROPN
eurjchem-562	130	39	8.4	8.4	NUM
eurjchem-562	130	40	hz	hz	NOUN
eurjchem-562	130	41	,	,	PUNCT
eurjchem-562	130	42	arh	arh	ADJ
eurjchem-562	130	43	)	)	PUNCT
eurjchem-562	130	44	,	,	PUNCT
eurjchem-562	130	45	6.96	6.96	NUM
eurjchem-562	130	46	(	(	PUNCT
eurjchem-562	130	47	2h	2h	NUM
eurjchem-562	130	48	,	,	PUNCT
eurjchem-562	130	49	d	d	NOUN
eurjchem-562	130	50	,	,	PUNCT
eurjchem-562	130	51	j	j	PROPN
eurjchem-562	130	52	=	=	SYM
eurjchem-562	130	53	8.8	8.8	NUM
eurjchem-562	130	54	hz	hz	NOUN
eurjchem-562	130	55	,	,	PUNCT
eurjchem-562	130	56	arh	arh	ADJ
eurjchem-562	130	57	)	)	PUNCT
eurjchem-562	130	58	,	,	PUNCT
eurjchem-562	130	59	6.41	6.41	NUM
eurjchem-562	130	60	(	(	PUNCT
eurjchem-562	130	61	1h	1h	NUM
eurjchem-562	130	62	,	,	PUNCT
eurjchem-562	130	63	br	br	PROPN
eurjchem-562	130	64	s	s	PROPN
eurjchem-562	130	65	,	,	PUNCT
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eurjchem-562	130	67	)	)	PUNCT
eurjchem-562	130	68	,	,	PUNCT
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eurjchem-562	130	71	1h	1h	NUM
eurjchem-562	130	72	,	,	PUNCT
eurjchem-562	130	73	d	d	PROPN
eurjchem-562	130	74	,	,	PUNCT
eurjchem-562	130	75	j	j	PROPN
eurjchem-562	130	76	=	=	SYM
eurjchem-562	130	77	18	18	NUM
eurjchem-562	130	78	hz	hz	VERB
eurjchem-562	130	79	,	,	PUNCT
eurjchem-562	130	80	ch2	ch2	PROPN
eurjchem-562	130	81	)	)	PUNCT
eurjchem-562	130	82	,	,	PUNCT
eurjchem-562	130	83	3.14	3.14	NUM
eurjchem-562	130	84	(	(	PUNCT
eurjchem-562	130	85	1h	1h	NUM
eurjchem-562	130	86	,	,	PUNCT
eurjchem-562	130	87	d	d	PROPN
eurjchem-562	130	88	,	,	PUNCT
eurjchem-562	130	89	j	j	PROPN
eurjchem-562	130	90	=	=	SYM
eurjchem-562	130	91	18	18	NUM
eurjchem-562	130	92	hz	hz	VERB
eurjchem-562	130	93	,	,	PUNCT
eurjchem-562	130	94	ch2	ch2	PROPN
eurjchem-562	130	95	)	)	PUNCT
eurjchem-562	130	96	,	,	PUNCT
eurjchem-562	130	97	1.77	1.77	NUM
eurjchem-562	130	98	(	(	PUNCT
eurjchem-562	130	99	3h	3h	NUM
eurjchem-562	130	100	.	.	PUNCT
eurjchem-562	131	1	s	s	X
eurjchem-562	131	2	,	,	PUNCT
eurjchem-562	131	3	ch3	ch3	PROPN
eurjchem-562	131	4	)	)	PUNCT
eurjchem-562	131	5	.	.	PUNCT
eurjchem-562	132	1	data	datum	NOUN
eurjchem-562	132	2	for	for	ADP
eurjchem-562	132	3	minor	minor	ADJ
eurjchem-562	132	4	isomer	isomer	NOUN
eurjchem-562	132	5	47	47	NUM
eurjchem-562	132	6	where	where	SCONJ
eurjchem-562	132	7	different	different	ADJ
eurjchem-562	132	8	from	from	ADP
eurjchem-562	132	9	major	major	ADJ
eurjchem-562	132	10	isomer	isomer	PROPN
eurjchem-562	132	11	36	36	NUM
eurjchem-562	132	12	,	,	PUNCT
eurjchem-562	132	13	7.75	7.75	NUM
eurjchem-562	132	14	(	(	PUNCT
eurjchem-562	132	15	4h	4h	NUM
eurjchem-562	132	16	,	,	PUNCT
eurjchem-562	132	17	app	app	PROPN
eurjchem-562	132	18	dd	dd	PROPN
eurjchem-562	132	19	,	,	PUNCT
eurjchem-562	132	20	j	j	PROPN
eurjchem-562	132	21	=	=	SYM
eurjchem-562	132	22	14	14	NUM
eurjchem-562	132	23	hz	hz	VERB
eurjchem-562	132	24	,	,	PUNCT
eurjchem-562	132	25	8.8	8.8	NUM
eurjchem-562	132	26	hz	hz	NOUN
eurjchem-562	132	27	,	,	PUNCT
eurjchem-562	132	28	arh	arh	ADJ
eurjchem-562	132	29	)	)	PUNCT
eurjchem-562	132	30	,	,	PUNCT
eurjchem-562	132	31	7.02	7.02	NUM
eurjchem-562	132	32	(	(	PUNCT
eurjchem-562	132	33	2h	2h	NUM
eurjchem-562	132	34	,	,	PUNCT
eurjchem-562	132	35	d	d	NOUN
eurjchem-562	132	36	,	,	PUNCT
eurjchem-562	132	37	j	j	PROPN
eurjchem-562	133	1	=	=	PROPN
eurjchem-562	133	2	8.4	8.4	NUM
eurjchem-562	133	3	hz	hz	NOUN
eurjchem-562	133	4	,	,	PUNCT
eurjchem-562	133	5	arh	arh	ADJ
eurjchem-562	133	6	)	)	PUNCT
eurjchem-562	133	7	,	,	PUNCT
eurjchem-562	133	8	6.88	6.88	NUM
eurjchem-562	133	9	(	(	PUNCT
eurjchem-562	133	10	2h	2h	NUM
eurjchem-562	133	11	,	,	PUNCT
eurjchem-562	133	12	d	d	NOUN
eurjchem-562	133	13	,	,	PUNCT
eurjchem-562	133	14	j	j	PROPN
eurjchem-562	133	15	=	=	SYM
eurjchem-562	133	16	9.0	9.0	NUM
eurjchem-562	133	17	,	,	PUNCT
eurjchem-562	133	18	arh	arh	ADJ
eurjchem-562	133	19	)	)	PUNCT
eurjchem-562	133	20	,	,	PUNCT
eurjchem-562	133	21	6.2	6.2	NUM
eurjchem-562	133	22	(	(	PUNCT
eurjchem-562	133	23	1h	1h	NUM
eurjchem-562	133	24	,	,	PUNCT
eurjchem-562	133	25	brs	br	VERB
eurjchem-562	133	26	,	,	PUNCT
eurjchem-562	133	27	c	c	NOUN
eurjchem-562	133	28	=	=	NOUN
eurjchem-562	133	29	ch	ch	NOUN
eurjchem-562	133	30	)	)	PUNCT
eurjchem-562	133	31	.	.	PUNCT
eurjchem-562	134	1	13c	13c	NOUN
eurjchem-562	134	2	nmr	nmr	NOUN
eurjchem-562	134	3	(	(	PUNCT
eurjchem-562	134	4	75	75	NUM
eurjchem-562	134	5	mhz	mhz	NOUN
eurjchem-562	134	6	,	,	PUNCT
eurjchem-562	134	7	cdcl3	cdcl3	PROPN
eurjchem-562	134	8	,	,	PUNCT
eurjchem-562	134	9	δ	δ	PROPN
eurjchem-562	134	10	,	,	PUNCT
eurjchem-562	134	11	ppm	ppm	NOUN
eurjchem-562	134	12	):	):	PUNCT
eurjchem-562	134	13	164.8	164.8	NUM
eurjchem-562	134	14	,	,	PUNCT
eurjchem-562	134	15	156.7	156.7	NUM
eurjchem-562	134	16	,	,	PUNCT
eurjchem-562	134	17	140.9	140.9	NUM
eurjchem-562	134	18	,	,	PUNCT
eurjchem-562	134	19	138.6	138.6	NUM
eurjchem-562	134	20	,	,	PUNCT
eurjchem-562	134	21	138.6	138.6	NUM
eurjchem-562	134	22	,	,	PUNCT
eurjchem-562	134	23	134.6	134.6	NUM
eurjchem-562	134	24	,	,	PUNCT
eurjchem-562	134	25	129.1	129.1	NUM
eurjchem-562	134	26	,	,	PUNCT
eurjchem-562	134	27	126.3	126.3	NUM
eurjchem-562	134	28	,	,	PUNCT
eurjchem-562	134	29	114.3	114.3	NUM
eurjchem-562	134	30	,	,	PUNCT
eurjchem-562	134	31	112.4	112.4	NUM
eurjchem-562	134	32	,	,	PUNCT
eurjchem-562	134	33	112.2	112.2	NUM
eurjchem-562	134	34	,	,	PUNCT
eurjchem-562	134	35	102.2	102.2	NUM
eurjchem-562	134	36	,	,	PUNCT
eurjchem-562	134	37	99.8	99.8	NUM
eurjchem-562	134	38	,	,	PUNCT
eurjchem-562	134	39	94.5	94.5	NUM
eurjchem-562	134	40	,	,	PUNCT
eurjchem-562	134	41	56.6	56.6	NUM
eurjchem-562	134	42	,	,	PUNCT
eurjchem-562	134	43	55.0	55.0	NUM
eurjchem-562	134	44	m	m	NOUN
eurjchem-562	134	45	,	,	PUNCT
eurjchem-562	134	46	45.1	45.1	NUM
eurjchem-562	134	47	,	,	PUNCT
eurjchem-562	134	48	29.3	29.3	NUM
eurjchem-562	134	49	.	.	PUNCT
eurjchem-562	134	50	hrms	hrm	VERB
eurjchem-562	134	51	calcd	calcd	NOUN
eurjchem-562	134	52	.	.	PUNCT
eurjchem-562	135	1	for	for	ADP
eurjchem-562	135	2	c22h14i2n4	c22h14i2n4	PROPN
eurjchem-562	135	3	(	(	PUNCT
eurjchem-562	135	4	m	m	PROPN
eurjchem-562	135	5	):	):	PUNCT
eurjchem-562	135	6	587.9308	587.9308	NUM
eurjchem-562	135	7	,	,	PUNCT
eurjchem-562	135	8	found	find	VERB
eurjchem-562	135	9	:	:	PUNCT
eurjchem-562	136	1	587.9291	587.9291	NUM
eurjchem-562	136	2	.	.	NOUN
eurjchem-562	136	3	2‐(3‐cyano‐4,6‐bis(4‐hydroxyphenyl)‐6‐methyl‐5,6‐dihydro	2‐(3‐cyano‐4,6‐bis(4‐hydroxyphenyl)‐6‐methyl‐5,6‐dihydro	NUM
eurjchem-562	136	4	pyridin‐2(1h)‐ylidene)malononitrile	pyridin‐2(1h)‐ylidene)malononitrile	NOUN
eurjchem-562	136	5	(	(	PUNCT
eurjchem-562	136	6	37	37	NUM
eurjchem-562	136	7	):	):	PUNCT
eurjchem-562	136	8	orange	orange	PROPN
eurjchem-562	136	9	solid	solid	PROPN
eurjchem-562	136	10	.	.	PUNCT
eurjchem-562	137	1	yield	yield	NOUN
eurjchem-562	137	2	:	:	PUNCT
eurjchem-562	137	3	75	75	NUM
eurjchem-562	137	4	%	%	NOUN
eurjchem-562	137	5	.	.	PUNCT
eurjchem-562	138	1	m.p	m.p	PROPN
eurjchem-562	138	2	.	.	PROPN
eurjchem-562	138	3	:	:	PUNCT
eurjchem-562	139	1	253‐255	253‐255	NUM
eurjchem-562	139	2	oc	oc	PROPN
eurjchem-562	139	3	.	.	PROPN
eurjchem-562	139	4	ir	ir	PROPN
eurjchem-562	139	5	(	(	PUNCT
eurjchem-562	139	6	kbr	kbr	PROPN
eurjchem-562	139	7	,	,	PUNCT
eurjchem-562	139	8	νmax	νmax	NOUN
eurjchem-562	139	9	,	,	PUNCT
eurjchem-562	139	10	cm‐1	cm‐1	PROPN
eurjchem-562	139	11	):	):	PUNCT
eurjchem-562	139	12	3382	3382	NUM
eurjchem-562	139	13	(	(	PUNCT
eurjchem-562	139	14	nh	nh	NOUN
eurjchem-562	139	15	)	)	PUNCT
eurjchem-562	139	16	,	,	PUNCT
eurjchem-562	139	17	1575	1575	NUM
eurjchem-562	139	18	,	,	PUNCT
eurjchem-562	139	19	1510	1510	NUM
eurjchem-562	139	20	,	,	PUNCT
eurjchem-562	139	21	1435	1435	NUM
eurjchem-562	139	22	,	,	PUNCT
eurjchem-562	139	23	1261	1261	NUM
eurjchem-562	139	24	.	.	PUNCT
eurjchem-562	140	1	1h	1h	NUM
eurjchem-562	140	2	nmr	nmr	NOUN
eurjchem-562	140	3	(	(	PUNCT
eurjchem-562	140	4	300	300	NUM
eurjchem-562	140	5	mhz	mhz	NOUN
eurjchem-562	140	6	,	,	PUNCT
eurjchem-562	140	7	dmso	dmso	NOUN
eurjchem-562	140	8	):	):	PUNCT
eurjchem-562	140	9	10.55	10.55	NUM
eurjchem-562	140	10	(	(	PUNCT
eurjchem-562	140	11	1h	1h	NUM
eurjchem-562	140	12	,	,	PUNCT
eurjchem-562	140	13	br	br	PROPN
eurjchem-562	140	14	s	s	PROPN
eurjchem-562	140	15	,	,	PUNCT
eurjchem-562	140	16	nh	nh	PROPN
eurjchem-562	140	17	)	)	PUNCT
eurjchem-562	140	18	,	,	PUNCT
eurjchem-562	140	19	9.55	9.55	NUM
eurjchem-562	140	20	(	(	PUNCT
eurjchem-562	140	21	1h	1h	NUM
eurjchem-562	140	22	,	,	PUNCT
eurjchem-562	140	23	br	br	PROPN
eurjchem-562	140	24	s	s	PROPN
eurjchem-562	140	25	,	,	PUNCT
eurjchem-562	140	26	aroh	aroh	NOUN
eurjchem-562	140	27	)	)	PUNCT
eurjchem-562	140	28	,	,	PUNCT
eurjchem-562	140	29	9.45	9.45	NUM
eurjchem-562	140	30	(	(	PUNCT
eurjchem-562	140	31	1h	1h	NUM
eurjchem-562	140	32	,	,	PUNCT
eurjchem-562	140	33	br	br	PROPN
eurjchem-562	140	34	s	s	PROPN
eurjchem-562	140	35	,	,	PUNCT
eurjchem-562	140	36	aroh	aroh	NOUN
eurjchem-562	140	37	)	)	PUNCT
eurjchem-562	140	38	,	,	PUNCT
eurjchem-562	140	39	7.50	7.50	NUM
eurjchem-562	140	40	(	(	PUNCT
eurjchem-562	140	41	2h	2h	NUM
eurjchem-562	140	42	,	,	PUNCT
eurjchem-562	140	43	d	d	NOUN
eurjchem-562	140	44	,	,	PUNCT
eurjchem-562	140	45	j	j	PROPN
eurjchem-562	140	46	=	=	SYM
eurjchem-562	140	47	8.7	8.7	NUM
eurjchem-562	140	48	hz	hz	NOUN
eurjchem-562	140	49	,	,	PUNCT
eurjchem-562	140	50	arh	arh	ADJ
eurjchem-562	140	51	)	)	PUNCT
eurjchem-562	140	52	,	,	PUNCT
eurjchem-562	140	53	7.17	7.17	NUM
eurjchem-562	140	54	(	(	PUNCT
eurjchem-562	140	55	2h	2h	NUM
eurjchem-562	140	56	,	,	PUNCT
eurjchem-562	140	57	d	d	NOUN
eurjchem-562	140	58	,	,	PUNCT
eurjchem-562	140	59	j	j	PROPN
eurjchem-562	140	60	=	=	PROPN
eurjchem-562	140	61	8.4	8.4	NUM
eurjchem-562	140	62	hz	hz	NOUN
eurjchem-562	140	63	,	,	PUNCT
eurjchem-562	140	64	arh	arh	ADJ
eurjchem-562	140	65	)	)	PUNCT
eurjchem-562	140	66	,	,	PUNCT
eurjchem-562	140	67	6.87	6.87	NUM
eurjchem-562	140	68	(	(	PUNCT
eurjchem-562	140	69	2h	2h	NUM
eurjchem-562	140	70	,	,	PUNCT
eurjchem-562	140	71	d	d	NOUN
eurjchem-562	140	72	,	,	PUNCT
eurjchem-562	140	73	j	j	PROPN
eurjchem-562	141	1	=	=	SYM
eurjchem-562	141	2	8.7	8.7	NUM
eurjchem-562	141	3	hz	hz	NOUN
eurjchem-562	141	4	,	,	PUNCT
eurjchem-562	141	5	arh	arh	ADJ
eurjchem-562	141	6	)	)	PUNCT
eurjchem-562	141	7	,	,	PUNCT
eurjchem-562	141	8	6.73	6.73	NUM
eurjchem-562	141	9	(	(	PUNCT
eurjchem-562	141	10	2h	2h	NUM
eurjchem-562	141	11	,	,	PUNCT
eurjchem-562	141	12	d	d	NOUN
eurjchem-562	141	13	,	,	PUNCT
eurjchem-562	141	14	j	j	PROPN
eurjchem-562	141	15	=	=	PROPN
eurjchem-562	141	16	8.4	8.4	NUM
eurjchem-562	141	17	hz	hz	NOUN
eurjchem-562	141	18	,	,	PUNCT
eurjchem-562	141	19	arh	arh	ADJ
eurjchem-562	141	20	)	)	PUNCT
eurjchem-562	141	21	,	,	PUNCT
eurjchem-562	141	22	3.75	3.75	NUM
eurjchem-562	141	23	(	(	PUNCT
eurjchem-562	141	24	1h	1h	NUM
eurjchem-562	141	25	,	,	PUNCT
eurjchem-562	141	26	d	d	PROPN
eurjchem-562	141	27	,	,	PUNCT
eurjchem-562	141	28	j=	j=	ADP
eurjchem-562	141	29	18	18	NUM
eurjchem-562	141	30	hz	hz	VERB
eurjchem-562	141	31	,	,	PUNCT
eurjchem-562	141	32	ch2	ch2	PROPN
eurjchem-562	141	33	)	)	PUNCT
eurjchem-562	141	34	,	,	PUNCT
eurjchem-562	141	35	3.14	3.14	NUM
eurjchem-562	141	36	(	(	PUNCT
eurjchem-562	141	37	1h	1h	NUM
eurjchem-562	141	38	,	,	PUNCT
eurjchem-562	141	39	d	d	PROPN
eurjchem-562	141	40	,	,	PUNCT
eurjchem-562	141	41	j=	j=	ADP
eurjchem-562	141	42	18	18	NUM
eurjchem-562	141	43	hz	hz	VERB
eurjchem-562	141	44	,	,	PUNCT
eurjchem-562	141	45	ch2	ch2	PROPN
eurjchem-562	141	46	)	)	PUNCT
eurjchem-562	141	47	,	,	PUNCT
eurjchem-562	141	48	1.65	1.65	NUM
eurjchem-562	141	49	(	(	PUNCT
eurjchem-562	141	50	3h	3h	NUM
eurjchem-562	141	51	,	,	PUNCT
eurjchem-562	141	52	s	s	X
eurjchem-562	141	53	,	,	PUNCT
eurjchem-562	141	54	ch3	ch3	PROPN
eurjchem-562	141	55	)	)	PUNCT
eurjchem-562	141	56	.	.	PUNCT
eurjchem-562	142	1	13c	13c	NOUN
eurjchem-562	142	2	nmr	nmr	NOUN
eurjchem-562	142	3	(	(	PUNCT
eurjchem-562	142	4	75	75	NUM
eurjchem-562	142	5	mhz	mhz	NOUN
eurjchem-562	142	6	,	,	PUNCT
eurjchem-562	142	7	dmso	dmso	NOUN
eurjchem-562	142	8	,	,	PUNCT
eurjchem-562	142	9	δ	δ	PROPN
eurjchem-562	142	10	,	,	PUNCT
eurjchem-562	142	11	ppm	ppm	NOUN
eurjchem-562	142	12	):	):	PUNCT
eurjchem-562	142	13	168.5	168.5	NUM
eurjchem-562	142	14	,	,	PUNCT
eurjchem-562	142	15	161.9	161.9	NUM
eurjchem-562	142	16	,	,	PUNCT
eurjchem-562	142	17	158.9	158.9	NUM
eurjchem-562	142	18	,	,	PUNCT
eurjchem-562	142	19	156.5	156.5	NUM
eurjchem-562	142	20	,	,	PUNCT
eurjchem-562	142	21	132.9	132.9	NUM
eurjchem-562	142	22	,	,	PUNCT
eurjchem-562	142	23	131.4	131.4	NUM
eurjchem-562	142	24	,	,	PUNCT
eurjchem-562	142	25	125.9	125.9	NUM
eurjchem-562	142	26	,	,	PUNCT
eurjchem-562	142	27	125.5	125.5	NUM
eurjchem-562	142	28	,	,	PUNCT
eurjchem-562	142	29	115.9	115.9	NUM
eurjchem-562	142	30	,	,	PUNCT
eurjchem-562	142	31	115.8	115.8	NUM
eurjchem-562	142	32	,	,	PUNCT
eurjchem-562	142	33	115.3	115.3	NUM
eurjchem-562	142	34	,	,	PUNCT
eurjchem-562	142	35	115.2	115.2	NUM
eurjchem-562	142	36	,	,	PUNCT
eurjchem-562	142	37	114.9	114.9	NUM
eurjchem-562	142	38	,	,	PUNCT
eurjchem-562	142	39	97.3	97.3	NUM
eurjchem-562	142	40	,	,	PUNCT
eurjchem-562	142	41	56.5	56.5	NUM
eurjchem-562	142	42	,	,	PUNCT
eurjchem-562	142	43	48.1	48.1	NUM
eurjchem-562	142	44	,	,	PUNCT
eurjchem-562	142	45	43.5	43.5	NUM
eurjchem-562	142	46	,	,	PUNCT
eurjchem-562	142	47	28.8	28.8	NUM
eurjchem-562	142	48	.	.	PUNCT
eurjchem-562	142	49	hrms	hrm	VERB
eurjchem-562	142	50	calcd	calcd	NOUN
eurjchem-562	142	51	.	.	PUNCT
eurjchem-562	143	1	for	for	ADP
eurjchem-562	143	2	c22h16n4o2	c22h16n4o2	PROPN
eurjchem-562	143	3	(	(	PUNCT
eurjchem-562	143	4	m	m	PROPN
eurjchem-562	143	5	):	):	PUNCT
eurjchem-562	143	6	368.1230	368.1230	NUM
eurjchem-562	143	7	,	,	PUNCT
eurjchem-562	143	8	found	find	VERB
eurjchem-562	143	9	:	:	PUNCT
eurjchem-562	143	10	368.1273	368.1273	NUM
eurjchem-562	143	11	.	.	NOUN
eurjchem-562	144	1	2‐(3‐cyano‐4,6‐bis(3‐hydroxyphenyl)‐6‐methyl‐5,6‐dihydro	2‐(3‐cyano‐4,6‐bis(3‐hydroxyphenyl)‐6‐methyl‐5,6‐dihydro	NUM
eurjchem-562	145	1	pyridin‐2(1h)‐ylidene)malononitrile	pyridin‐2(1h)‐ylidene)malononitrile	NOUN
eurjchem-562	145	2	(	(	PUNCT
eurjchem-562	145	3	38	38	NUM
eurjchem-562	145	4	):	):	PUNCT
eurjchem-562	145	5	yellow	yellow	ADJ
eurjchem-562	145	6	solid	solid	ADJ
eurjchem-562	145	7	.	.	PUNCT
eurjchem-562	146	1	yield	yield	NOUN
eurjchem-562	146	2	:	:	PUNCT
eurjchem-562	146	3	93	93	NUM
eurjchem-562	146	4	%	%	NOUN
eurjchem-562	146	5	.	.	PUNCT
eurjchem-562	147	1	m.p	m.p	PROPN
eurjchem-562	147	2	.	.	PROPN
eurjchem-562	147	3	:	:	PUNCT
eurjchem-562	148	1	270‐272	270‐272	NUM
eurjchem-562	148	2	oc	oc	NOUN
eurjchem-562	148	3	.	.	PROPN
eurjchem-562	148	4	ir	ir	PROPN
eurjchem-562	148	5	(	(	PUNCT
eurjchem-562	148	6	kbr	kbr	PROPN
eurjchem-562	148	7	,	,	PUNCT
eurjchem-562	148	8	νmax	νmax	NOUN
eurjchem-562	148	9	,	,	PUNCT
eurjchem-562	148	10	cm‐1	cm‐1	PROPN
eurjchem-562	148	11	):	):	PUNCT
eurjchem-562	148	12	3449	3449	NUM
eurjchem-562	148	13	(	(	PUNCT
eurjchem-562	148	14	nh	nh	NOUN
eurjchem-562	148	15	)	)	PUNCT
eurjchem-562	148	16	,	,	PUNCT
eurjchem-562	148	17	3250	3250	NUM
eurjchem-562	148	18	,	,	PUNCT
eurjchem-562	148	19	2213	2213	NUM
eurjchem-562	148	20	,	,	PUNCT
eurjchem-562	148	21	1594	1594	NUM
eurjchem-562	148	22	,	,	PUNCT
eurjchem-562	148	23	1451	1451	NUM
eurjchem-562	148	24	,	,	PUNCT
eurjchem-562	148	25	1429	1429	NUM
eurjchem-562	148	26	.	.	PUNCT
eurjchem-562	149	1	1h	1h	NUM
eurjchem-562	149	2	nmr	nmr	NOUN
eurjchem-562	149	3	(	(	PUNCT
eurjchem-562	149	4	300	300	NUM
eurjchem-562	149	5	mhz	mhz	NOUN
eurjchem-562	149	6	,	,	PUNCT
eurjchem-562	149	7	dmso	dmso	NOUN
eurjchem-562	149	8	,	,	PUNCT
eurjchem-562	149	9	δ	δ	PROPN
eurjchem-562	149	10	,	,	PUNCT
eurjchem-562	149	11	ppm	ppm	NOUN
eurjchem-562	149	12	):	):	PUNCT
eurjchem-562	149	13	9.92	9.92	NUM
eurjchem-562	149	14	(	(	PUNCT
eurjchem-562	149	15	1h	1h	NUM
eurjchem-562	149	16	,	,	PUNCT
eurjchem-562	149	17	br	br	PROPN
eurjchem-562	149	18	s	s	PROPN
eurjchem-562	149	19	,	,	PUNCT
eurjchem-562	149	20	nh	nh	PROPN
eurjchem-562	149	21	)	)	PUNCT
eurjchem-562	149	22	,	,	PUNCT
eurjchem-562	149	23	9.65	9.65	NUM
eurjchem-562	149	24	(	(	PUNCT
eurjchem-562	149	25	1h	1h	NUM
eurjchem-562	149	26	,	,	PUNCT
eurjchem-562	149	27	br	br	PROPN
eurjchem-562	149	28	s	s	PROPN
eurjchem-562	149	29	,	,	PUNCT
eurjchem-562	149	30	aroh	aroh	NOUN
eurjchem-562	149	31	)	)	PUNCT
eurjchem-562	149	32	,	,	PUNCT
eurjchem-562	149	33	9.55	9.55	NUM
eurjchem-562	149	34	(	(	PUNCT
eurjchem-562	149	35	1h	1h	NUM
eurjchem-562	149	36	,	,	PUNCT
eurjchem-562	149	37	br	br	PROPN
eurjchem-562	149	38	s	s	PROPN
eurjchem-562	149	39	,	,	PUNCT
eurjchem-562	149	40	aroh	aroh	NOUN
eurjchem-562	149	41	)	)	PUNCT
eurjchem-562	149	42	,	,	PUNCT
eurjchem-562	149	43	7.29	7.29	NUM
eurjchem-562	149	44	(	(	PUNCT
eurjchem-562	149	45	1h	1h	NUM
eurjchem-562	149	46	,	,	PUNCT
eurjchem-562	149	47	app	app	PROPN
eurjchem-562	149	48	t	t	PROPN
eurjchem-562	149	49	,	,	PUNCT
eurjchem-562	149	50	j	j	PROPN
eurjchem-562	150	1	=	=	SYM
eurjchem-562	150	2	7.8	7.8	NUM
eurjchem-562	150	3	hz	hz	NOUN
eurjchem-562	150	4	,	,	PUNCT
eurjchem-562	150	5	arh	arh	ADJ
eurjchem-562	150	6	)	)	PUNCT
eurjchem-562	150	7	,	,	PUNCT
eurjchem-562	150	8	7.18	7.18	NUM
eurjchem-562	150	9	(	(	PUNCT
eurjchem-562	150	10	1h	1h	NUM
eurjchem-562	150	11	,	,	PUNCT
eurjchem-562	150	12	app	app	PROPN
eurjchem-562	150	13	t	t	PROPN
eurjchem-562	150	14	,	,	PUNCT
eurjchem-562	150	15	j	j	PROPN
eurjchem-562	151	1	=	=	SYM
eurjchem-562	151	2	7.8	7.8	NUM
eurjchem-562	151	3	hz	hz	NOUN
eurjchem-562	151	4	,	,	PUNCT
eurjchem-562	151	5	arh	arh	ADJ
eurjchem-562	151	6	)	)	PUNCT
eurjchem-562	151	7	,	,	PUNCT
eurjchem-562	151	8	6.92	6.92	NUM
eurjchem-562	151	9	(	(	PUNCT
eurjchem-562	151	10	1h	1h	NUM
eurjchem-562	151	11	,	,	PUNCT
eurjchem-562	151	12	d	d	PROPN
eurjchem-562	151	13	,	,	PUNCT
eurjchem-562	151	14	j	j	PROPN
eurjchem-562	152	1	=	=	SYM
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eurjchem-562	152	3	hz	hz	NOUN
eurjchem-562	152	4	,	,	PUNCT
eurjchem-562	152	5	arh	arh	ADJ
eurjchem-562	152	6	)	)	PUNCT
eurjchem-562	152	7	,	,	PUNCT
eurjchem-562	152	8	6.85‐6.78	6.85‐6.78	NUM
eurjchem-562	152	9	(	(	PUNCT
eurjchem-562	152	10	3h	3h	NUM
eurjchem-562	152	11	,	,	PUNCT
eurjchem-562	152	12	m	m	PROPN
eurjchem-562	152	13	,	,	PUNCT
eurjchem-562	152	14	arh	arh	ADJ
eurjchem-562	152	15	)	)	PUNCT
eurjchem-562	152	16	)	)	PUNCT
eurjchem-562	152	17	,	,	PUNCT
eurjchem-562	152	18	6.70‐6.65	6.70‐6.65	NUM
eurjchem-562	152	19	(	(	PUNCT
eurjchem-562	152	20	2h	2h	NUM
eurjchem-562	152	21	,	,	PUNCT
eurjchem-562	152	22	m	m	NOUN
eurjchem-562	152	23	,	,	PUNCT
eurjchem-562	152	24	arh	arh	ADJ
eurjchem-562	152	25	)	)	PUNCT
eurjchem-562	152	26	,	,	PUNCT
eurjchem-562	152	27	3.61	3.61	NUM
eurjchem-562	152	28	(	(	PUNCT
eurjchem-562	152	29	1h	1h	NUM
eurjchem-562	152	30	,	,	PUNCT
eurjchem-562	152	31	d	d	PROPN
eurjchem-562	152	32	,	,	PUNCT
eurjchem-562	152	33	j=	j=	ADP
eurjchem-562	152	34	18	18	NUM
eurjchem-562	152	35	hz	hz	VERB
eurjchem-562	152	36	,	,	PUNCT
eurjchem-562	152	37	ch2	ch2	PROPN
eurjchem-562	152	38	)	)	PUNCT
eurjchem-562	152	39	,	,	PUNCT
eurjchem-562	152	40	3.27	3.27	NUM
eurjchem-562	152	41	(	(	PUNCT
eurjchem-562	152	42	1h	1h	NUM
eurjchem-562	152	43	,	,	PUNCT
eurjchem-562	152	44	d	d	PROPN
eurjchem-562	152	45	,	,	PUNCT
eurjchem-562	152	46	j=	j=	ADP
eurjchem-562	152	47	18	18	NUM
eurjchem-562	152	48	hz	hz	VERB
eurjchem-562	152	49	,	,	PUNCT
eurjchem-562	152	50	ch2	ch2	PROPN
eurjchem-562	152	51	)	)	PUNCT
eurjchem-562	152	52	,	,	PUNCT
eurjchem-562	152	53	1.67	1.67	NUM
eurjchem-562	152	54	(	(	PUNCT
eurjchem-562	152	55	3h	3h	NUM
eurjchem-562	152	56	,	,	PUNCT
eurjchem-562	152	57	s	s	X
eurjchem-562	152	58	,	,	PUNCT
eurjchem-562	152	59	ch3	ch3	PROPN
eurjchem-562	152	60	)	)	PUNCT
eurjchem-562	152	61	.	.	PUNCT
eurjchem-562	153	1	13c	13c	NOUN
eurjchem-562	153	2	nmr	nmr	NOUN
eurjchem-562	153	3	(	(	PUNCT
eurjchem-562	153	4	75	75	NUM
eurjchem-562	153	5	mhz	mhz	NOUN
eurjchem-562	153	6	,	,	PUNCT
eurjchem-562	153	7	dmso	dmso	NOUN
eurjchem-562	153	8	,	,	PUNCT
eurjchem-562	153	9	δ	δ	PROPN
eurjchem-562	153	10	,	,	PUNCT
eurjchem-562	153	11	ppm	ppm	NOUN
eurjchem-562	153	12	):	):	PUNCT
eurjchem-562	153	13	169.1	169.1	NUM
eurjchem-562	153	14	,	,	PUNCT
eurjchem-562	153	15	157.9	157.9	NUM
eurjchem-562	153	16	,	,	PUNCT
eurjchem-562	153	17	157.4	157.4	NUM
eurjchem-562	153	18	,	,	PUNCT
eurjchem-562	153	19	157.3	157.3	NUM
eurjchem-562	153	20	,	,	PUNCT
eurjchem-562	153	21	144.4	144.4	NUM
eurjchem-562	153	22	,	,	PUNCT
eurjchem-562	153	23	136.8	136.8	NUM
eurjchem-562	153	24	,	,	PUNCT
eurjchem-562	153	25	130.1	130.1	NUM
eurjchem-562	153	26	,	,	PUNCT
eurjchem-562	153	27	1	1	NUM
eurjchem-562	153	28	29.7	29.7	NUM
eurjchem-562	153	29	,	,	PUNCT
eurjchem-562	153	30	119.0	119.0	NUM
eurjchem-562	153	31	,	,	PUNCT
eurjchem-562	153	32	118.8	118.8	NUM
eurjchem-562	153	33	,	,	PUNCT
eurjchem-562	153	34	115.6	115.6	NUM
eurjchem-562	153	35	,	,	PUNCT
eurjchem-562	153	36	115.5	115.5	NUM
eurjchem-562	153	37	,	,	PUNCT
eurjchem-562	153	38	115.0	115.0	NUM
eurjchem-562	153	39	,	,	PUNCT
eurjchem-562	153	40	114.8	114.8	NUM
eurjchem-562	153	41	,	,	PUNCT
eurjchem-562	153	42	114.2	114.2	NUM
eurjchem-562	153	43	,	,	PUNCT
eurjchem-562	153	44	113.7	113.7	NUM
eurjchem-562	153	45	,	,	PUNCT
eurjchem-562	153	46	112.0	112.0	NUM
eurjchem-562	153	47	,	,	PUNCT
eurjchem-562	153	48	100.7	100.7	NUM
eurjchem-562	153	49	,	,	PUNCT
eurjchem-562	153	50	56.8	56.8	NUM
eurjchem-562	153	51	,	,	PUNCT
eurjchem-562	153	52	49.1	49.1	NUM
eurjchem-562	153	53	,	,	PUNCT
eurjchem-562	153	54	44.2	44.2	NUM
eurjchem-562	153	55	,	,	PUNCT
eurjchem-562	153	56	28.4	28.4	NUM
eurjchem-562	153	57	.	.	PUNCT
eurjchem-562	153	58	hrms	hrm	VERB
eurjchem-562	153	59	calcd	calcd	NOUN
eurjchem-562	153	60	.	.	PUNCT
eurjchem-562	154	1	for	for	ADP
eurjchem-562	154	2	c22h16n4o2	c22h16n4o2	PROPN
eurjchem-562	154	3	(	(	PUNCT
eurjchem-562	154	4	m	m	PROPN
eurjchem-562	154	5	):	):	PUNCT
eurjchem-562	154	6	368.1272	368.1272	NUM
eurjchem-562	154	7	,	,	PUNCT
eurjchem-562	154	8	found	find	VERB
eurjchem-562	154	9	:	:	PUNCT
eurjchem-562	154	10	368.1273	368.1273	NUM
eurjchem-562	154	11	.	.	PUNCT
eurjchem-562	155	1	2‐(3‐cyano‐4,6‐bis(4‐methoxyphenyl)‐6‐methyl‐5,6‐dihydro	2‐(3‐cyano‐4,6‐bis(4‐methoxyphenyl)‐6‐methyl‐5,6‐dihydro	NUM
eurjchem-562	155	2	pyridin‐2(1h)‐ylidene)malononitrile	pyridin‐2(1h)‐ylidene)malononitrile	NOUN
eurjchem-562	155	3	(	(	PUNCT
eurjchem-562	155	4	41	41	NUM
eurjchem-562	155	5	):	):	PUNCT
eurjchem-562	155	6	brown	brown	ADJ
eurjchem-562	155	7	solid	solid	NOUN
eurjchem-562	155	8	.	.	PUNCT
eurjchem-562	156	1	yield	yield	NOUN
eurjchem-562	156	2	:	:	PUNCT
eurjchem-562	156	3	77	77	NUM
eurjchem-562	156	4	%	%	NOUN
eurjchem-562	156	5	.	.	PUNCT
eurjchem-562	157	1	m.p	m.p	PROPN
eurjchem-562	157	2	.	.	PROPN
eurjchem-562	157	3	:	:	PUNCT
eurjchem-562	158	1	119‐121	119‐121	NUM
eurjchem-562	158	2	oc	oc	NOUN
eurjchem-562	158	3	.	.	PROPN
eurjchem-562	158	4	ir	ir	PROPN
eurjchem-562	158	5	(	(	PUNCT
eurjchem-562	158	6	kbr	kbr	PROPN
eurjchem-562	158	7	,	,	PUNCT
eurjchem-562	158	8	νmax	νmax	NOUN
eurjchem-562	158	9	,	,	PUNCT
eurjchem-562	158	10	cm‐1	cm‐1	PROPN
eurjchem-562	158	11	):	):	PUNCT
eurjchem-562	158	12	3449	3449	NUM
eurjchem-562	158	13	(	(	PUNCT
eurjchem-562	158	14	nh	nh	NOUN
eurjchem-562	158	15	)	)	PUNCT
eurjchem-562	158	16	,	,	PUNCT
eurjchem-562	158	17	2926	2926	NUM
eurjchem-562	158	18	,	,	PUNCT
eurjchem-562	158	19	2212	2212	NUM
eurjchem-562	158	20	,	,	PUNCT
eurjchem-562	158	21	1510	1510	NUM
eurjchem-562	158	22	,	,	PUNCT
eurjchem-562	158	23	1459	1459	NUM
eurjchem-562	158	24	,	,	PUNCT
eurjchem-562	158	25	1259	1259	NUM
eurjchem-562	158	26	.	.	PUNCT
eurjchem-562	159	1	1h	1h	NUM
eurjchem-562	159	2	nmr	nmr	NOUN
eurjchem-562	159	3	(	(	PUNCT
eurjchem-562	159	4	300	300	NUM
eurjchem-562	159	5	mhz	mhz	NOUN
eurjchem-562	159	6	,	,	PUNCT
eurjchem-562	159	7	cdcl3	cdcl3	PROPN
eurjchem-562	159	8	,	,	PUNCT
eurjchem-562	159	9	δ	δ	PROPN
eurjchem-562	159	10	,	,	PUNCT
eurjchem-562	159	11	ppm	ppm	NUM
eurjchem-562	159	12	):	):	PUNCT
eurjchem-562	159	13	7.45	7.45	NUM
eurjchem-562	159	14	(	(	PUNCT
eurjchem-562	159	15	2h	2h	NUM
eurjchem-562	159	16	,	,	PUNCT
eurjchem-562	159	17	d	d	NOUN
eurjchem-562	159	18	,	,	PUNCT
eurjchem-562	159	19	j	j	PROPN
eurjchem-562	159	20	=	=	SYM
eurjchem-562	159	21	9.0	9.0	NUM
eurjchem-562	159	22	hz	hz	NOUN
eurjchem-562	159	23	,	,	PUNCT
eurjchem-562	159	24	arh	arh	ADJ
eurjchem-562	159	25	)	)	PUNCT
eurjchem-562	159	26	,	,	PUNCT
eurjchem-562	159	27	7.15	7.15	NUM
eurjchem-562	159	28	(	(	PUNCT
eurjchem-562	159	29	2h	2h	NUM
eurjchem-562	159	30	,	,	PUNCT
eurjchem-562	159	31	d	d	NOUN
eurjchem-562	159	32	,	,	PUNCT
eurjchem-562	159	33	j	j	PROPN
eurjchem-562	160	1	=	=	SYM
eurjchem-562	160	2	8.7	8.7	NUM
eurjchem-562	160	3	hz	hz	NOUN
eurjchem-562	160	4	,	,	PUNCT
eurjchem-562	160	5	arh	arh	ADJ
eurjchem-562	160	6	)	)	PUNCT
eurjchem-562	160	7	,	,	PUNCT
eurjchem-562	160	8	6.91	6.91	NUM
eurjchem-562	160	9	(	(	PUNCT
eurjchem-562	160	10	4h	4h	NUM
eurjchem-562	160	11	,	,	PUNCT
eurjchem-562	160	12	app	app	PROPN
eurjchem-562	160	13	t	t	PROPN
eurjchem-562	160	14	,	,	PUNCT
eurjchem-562	160	15	j	j	PROPN
eurjchem-562	161	1	=	=	SYM
eurjchem-562	161	2	9.4	9.4	NUM
eurjchem-562	161	3	hz	hz	NOUN
eurjchem-562	161	4	,	,	PUNCT
eurjchem-562	161	5	arh	arh	ADJ
eurjchem-562	161	6	)	)	PUNCT
eurjchem-562	161	7	,	,	PUNCT
eurjchem-562	161	8	6.73	6.73	NUM
eurjchem-562	161	9	(	(	PUNCT
eurjchem-562	161	10	1h	1h	NUM
eurjchem-562	161	11	,	,	PUNCT
eurjchem-562	161	12	br	br	PROPN
eurjchem-562	161	13	s	s	PROPN
eurjchem-562	161	14	,	,	PUNCT
eurjchem-562	161	15	nh	nh	PROPN
eurjchem-562	161	16	)	)	PUNCT
eurjchem-562	161	17	,	,	PUNCT
eurjchem-562	161	18	3.82	3.82	NUM
eurjchem-562	161	19	(	(	PUNCT
eurjchem-562	161	20	3h	3h	NUM
eurjchem-562	161	21	,	,	PUNCT
eurjchem-562	161	22	s	s	X
eurjchem-562	161	23	,	,	PUNCT
eurjchem-562	161	24	och3	och3	ADJ
eurjchem-562	161	25	)	)	PUNCT
eurjchem-562	161	26	,	,	PUNCT
eurjchem-562	161	27	3.78	3.78	NUM
eurjchem-562	161	28	(	(	PUNCT
eurjchem-562	161	29	3h	3h	NUM
eurjchem-562	161	30	,	,	PUNCT
eurjchem-562	161	31	s	s	X
eurjchem-562	161	32	,	,	PUNCT
eurjchem-562	161	33	och3	och3	ADJ
eurjchem-562	161	34	)	)	PUNCT
eurjchem-562	161	35	,	,	PUNCT
eurjchem-562	161	36	3.46	3.46	NUM
eurjchem-562	161	37	(	(	PUNCT
eurjchem-562	161	38	1h	1h	NUM
eurjchem-562	161	39	,	,	PUNCT
eurjchem-562	161	40	d	d	PROPN
eurjchem-562	161	41	,	,	PUNCT
eurjchem-562	161	42	j	j	PROPN
eurjchem-562	162	1	=	=	SYM
eurjchem-562	162	2	18	18	NUM
eurjchem-562	162	3	hz	hz	VERB
eurjchem-562	162	4	,	,	PUNCT
eurjchem-562	162	5	ch2	ch2	PROPN
eurjchem-562	162	6	)	)	PUNCT
eurjchem-562	162	7	,	,	PUNCT
eurjchem-562	162	8	3.05	3.05	NUM
eurjchem-562	162	9	(	(	PUNCT
eurjchem-562	162	10	1h	1h	NUM
eurjchem-562	162	11	,	,	PUNCT
eurjchem-562	162	12	d	d	PROPN
eurjchem-562	162	13	,	,	PUNCT
eurjchem-562	162	14	j	j	PROPN
eurjchem-562	162	15	=	=	SYM
eurjchem-562	162	16	18	18	NUM
eurjchem-562	162	17	hz	hz	VERB
eurjchem-562	162	18	,	,	PUNCT
eurjchem-562	162	19	ch2	ch2	PROPN
eurjchem-562	162	20	)	)	PUNCT
eurjchem-562	162	21	,	,	PUNCT
eurjchem-562	162	22	1.75	1.75	NUM
eurjchem-562	162	23	(	(	PUNCT
eurjchem-562	162	24	3h	3h	NUM
eurjchem-562	162	25	,	,	PUNCT
eurjchem-562	162	26	s	s	X
eurjchem-562	162	27	,	,	PUNCT
eurjchem-562	162	28	ch3	ch3	PROPN
eurjchem-562	162	29	)	)	PUNCT
eurjchem-562	162	30	.	.	PUNCT
eurjchem-562	163	1	13c	13c	NOUN
eurjchem-562	163	2	nmr	nmr	NOUN
eurjchem-562	163	3	(	(	PUNCT
eurjchem-562	163	4	100	100	NUM
eurjchem-562	163	5	mhz	mhz	NOUN
eurjchem-562	163	6	,	,	PUNCT
eurjchem-562	163	7	cdcl3	cdcl3	PROPN
eurjchem-562	163	8	,	,	PUNCT
eurjchem-562	163	9	δ	δ	PROPN
eurjchem-562	163	10	,	,	PUNCT
eurjchem-562	163	11	ppm	ppm	NOUN
eurjchem-562	163	12	):	):	PUNCT
eurjchem-562	163	13	165.8	165.8	NUM
eurjchem-562	163	14	,	,	PUNCT
eurjchem-562	163	15	163.2	163.2	NUM
eurjchem-562	163	16	,	,	PUNCT
eurjchem-562	163	17	159.5	159.5	NUM
eurjchem-562	163	18	,	,	PUNCT
eurjchem-562	163	19	157.9	157.9	NUM
eurjchem-562	163	20	,	,	PUNCT
eurjchem-562	163	21	133.2	133.2	NUM
eurjchem-562	163	22	,	,	PUNCT
eurjchem-562	163	23	130.5	130.5	NUM
eurjchem-562	163	24	,	,	PUNCT
eurjchem-562	163	25	127.4	127.4	NUM
eurjchem-562	163	26	,	,	PUNCT
eurjchem-562	163	27	125.7	125.7	NUM
eurjchem-562	163	28	,	,	PUNCT
eurjchem-562	163	29	114.9	114.9	NUM
eurjchem-562	163	30	,	,	PUNCT
eurjchem-562	163	31	114.7	114.7	NUM
eurjchem-562	163	32	,	,	PUNCT
eurjchem-562	163	33	114.6	114.6	NUM
eurjchem-562	163	34	,	,	PUNCT
eurjchem-562	163	35	113.6	113.6	NUM
eurjchem-562	163	36	,	,	PUNCT
eurjchem-562	163	37	113.0	113.0	NUM
eurjchem-562	163	38	,	,	PUNCT
eurjchem-562	163	39	99.4	99.4	NUM
eurjchem-562	163	40	,	,	PUNCT
eurjchem-562	163	41	56.4	56.4	NUM
eurjchem-562	163	42	,	,	PUNCT
eurjchem-562	163	43	55.6	55.6	NUM
eurjchem-562	163	44	,	,	PUNCT
eurjchem-562	163	45	55.4	55.4	NUM
eurjchem-562	163	46	,	,	PUNCT
eurjchem-562	163	47	55.0	55.0	NUM
eurjchem-562	163	48	,	,	PUNCT
eurjchem-562	163	49	45.4	45.4	NUM
eurjchem-562	163	50	,	,	PUNCT
eurjchem-562	163	51	29.2	29.2	NUM
eurjchem-562	163	52	.	.	PUNCT
eurjchem-562	164	1	hrms	hrm	VERB
eurjchem-562	164	2	calcd	calcd	NOUN
eurjchem-562	164	3	.	.	PUNCT
eurjchem-562	165	1	for	for	ADP
eurjchem-562	165	2	c24h20n4o2	c24h20n4o2	PROPN
eurjchem-562	165	3	(	(	PUNCT
eurjchem-562	165	4	m	m	PROPN
eurjchem-562	165	5	):	):	PUNCT
eurjchem-562	165	6	396.1586	396.1586	NUM
eurjchem-562	165	7	,	,	PUNCT
eurjchem-562	165	8	found	find	VERB
eurjchem-562	165	9	:	:	PUNCT
eurjchem-562	165	10	396.1515	396.1515	NUM
eurjchem-562	165	11	.	.	NOUN
eurjchem-562	165	12	2‐(3‐cyano‐4,6‐bis(3‐methoxyphenyl)‐6‐methyl‐5,6‐dihydro	2‐(3‐cyano‐4,6‐bis(3‐methoxyphenyl)‐6‐methyl‐5,6‐dihydro	NUM
eurjchem-562	166	1	pyridin‐2(1h)‐ylidene)malononitrile	pyridin‐2(1h)‐ylidene)malononitrile	NOUN
eurjchem-562	166	2	(	(	PUNCT
eurjchem-562	166	3	42	42	NUM
eurjchem-562	166	4	):	):	PUNCT
eurjchem-562	166	5	yellow	yellow	ADJ
eurjchem-562	166	6	solid	solid	ADJ
eurjchem-562	166	7	.	.	PUNCT
eurjchem-562	167	1	yield	yield	NOUN
eurjchem-562	167	2	:	:	PUNCT
eurjchem-562	167	3	80	80	NUM
eurjchem-562	167	4	%	%	NOUN
eurjchem-562	167	5	.	.	PUNCT
eurjchem-562	168	1	m.p	m.p	PROPN
eurjchem-562	168	2	.	.	PROPN
eurjchem-562	168	3	:	:	PUNCT
eurjchem-562	169	1	133‐135	133‐135	NUM
eurjchem-562	169	2	oc	oc	NOUN
eurjchem-562	169	3	.	.	PUNCT
eurjchem-562	169	4	ir	ir	PROPN
eurjchem-562	169	5	(	(	PUNCT
eurjchem-562	169	6	kbr	kbr	PROPN
eurjchem-562	169	7	,	,	PUNCT
eurjchem-562	169	8	νmax	νmax	NOUN
eurjchem-562	169	9	,	,	PUNCT
eurjchem-562	169	10	cm‐1	cm‐1	PROPN
eurjchem-562	169	11	):	):	PUNCT
eurjchem-562	169	12	3449	3449	NUM
eurjchem-562	169	13	(	(	PUNCT
eurjchem-562	169	14	nh	nh	NOUN
eurjchem-562	169	15	)	)	PUNCT
eurjchem-562	169	16	,	,	PUNCT
eurjchem-562	169	17	3284	3284	NUM
eurjchem-562	169	18	,	,	PUNCT
eurjchem-562	169	19	2212	2212	NUM
eurjchem-562	169	20	,	,	PUNCT
eurjchem-562	169	21	1598	1598	NUM
eurjchem-562	169	22	,	,	PUNCT
eurjchem-562	169	23	1427	1427	NUM
eurjchem-562	169	24	.	.	PUNCT
eurjchem-562	170	1	1h	1h	NUM
eurjchem-562	170	2	nmr	nmr	NOUN
eurjchem-562	170	3	(	(	PUNCT
eurjchem-562	170	4	300	300	NUM
eurjchem-562	170	5	mhz	mhz	NOUN
eurjchem-562	170	6	,	,	PUNCT
eurjchem-562	170	7	cdcl3	cdcl3	PROPN
eurjchem-562	170	8	,	,	PUNCT
eurjchem-562	170	9	δ	δ	PROPN
eurjchem-562	170	10	,	,	PUNCT
eurjchem-562	170	11	ppm	ppm	NOUN
eurjchem-562	170	12	):	):	PUNCT
eurjchem-562	170	13	7.34	7.34	NUM
eurjchem-562	170	14	(	(	PUNCT
eurjchem-562	170	15	2h	2h	NUM
eurjchem-562	170	16	,	,	PUNCT
eurjchem-562	170	17	app	app	PROPN
eurjchem-562	170	18	t	t	PROPN
eurjchem-562	170	19	,	,	PUNCT
eurjchem-562	170	20	j	j	PROPN
eurjchem-562	171	1	=	=	SYM
eurjchem-562	171	2	8.0	8.0	NUM
eurjchem-562	171	3	hz	hz	NOUN
eurjchem-562	171	4	,	,	PUNCT
eurjchem-562	171	5	arh	arh	ADJ
eurjchem-562	171	6	)	)	PUNCT
eurjchem-562	171	7	,	,	PUNCT
eurjchem-562	171	8	7.01	7.01	NUM
eurjchem-562	171	9	(	(	PUNCT
eurjchem-562	171	10	1h	1h	NUM
eurjchem-562	171	11	,	,	PUNCT
eurjchem-562	171	12	app	app	PROPN
eurjchem-562	171	13	dd	dd	PROPN
eurjchem-562	171	14	,	,	PUNCT
eurjchem-562	171	15	j	j	PROPN
eurjchem-562	172	1	=	=	SYM
eurjchem-562	172	2	8.0	8.0	NUM
eurjchem-562	172	3	hz	hz	NOUN
eurjchem-562	172	4	,	,	PUNCT
eurjchem-562	172	5	2.0	2.0	NUM
eurjchem-562	172	6	hz	hz	NOUN
eurjchem-562	172	7	,	,	PUNCT
eurjchem-562	172	8	arh	arh	ADJ
eurjchem-562	172	9	)	)	PUNCT
eurjchem-562	172	10	,	,	PUNCT
eurjchem-562	172	11	6.93	6.93	NUM
eurjchem-562	172	12	(	(	PUNCT
eurjchem-562	172	13	1h	1h	NUM
eurjchem-562	172	14	,	,	PUNCT
eurjchem-562	172	15	d	d	PROPN
eurjchem-562	172	16	,	,	PUNCT
eurjchem-562	172	17	j	j	PROPN
eurjchem-562	173	1	=	=	SYM
eurjchem-562	173	2	8.0	8.0	NUM
eurjchem-562	173	3	hz	hz	NOUN
eurjchem-562	173	4	,	,	PUNCT
eurjchem-562	173	5	arh	arh	ADJ
eurjchem-562	173	6	)	)	PUNCT
eurjchem-562	173	7	,	,	PUNCT
eurjchem-562	173	8	6.87‐6.79	6.87‐6.79	NUM
eurjchem-562	173	9	(	(	PUNCT
eurjchem-562	173	10	3h	3h	NUM
eurjchem-562	173	11	,	,	PUNCT
eurjchem-562	173	12	m	m	PROPN
eurjchem-562	173	13	,	,	PUNCT
eurjchem-562	173	14	arh	arh	ADJ
eurjchem-562	173	15	)	)	PUNCT
eurjchem-562	173	16	,	,	PUNCT
eurjchem-562	173	17	6.73	6.73	NUM
eurjchem-562	173	18	(	(	PUNCT
eurjchem-562	173	19	1h	1h	NUM
eurjchem-562	173	20	,	,	PUNCT
eurjchem-562	173	21	app	app	PROPN
eurjchem-562	173	22	t	t	PROPN
eurjchem-562	173	23	,	,	PUNCT
eurjchem-562	173	24	j	j	PROPN
eurjchem-562	173	25	=	=	SYM
eurjchem-562	173	26	2.1	2.1	NUM
eurjchem-562	173	27	hz	hz	NOUN
eurjchem-562	173	28	,	,	PUNCT
eurjchem-562	173	29	arh	arh	ADJ
eurjchem-562	173	30	)	)	PUNCT
eurjchem-562	173	31	,	,	PUNCT
eurjchem-562	173	32	6.38	6.38	NUM
eurjchem-562	173	33	(	(	PUNCT
eurjchem-562	173	34	1h	1h	NUM
eurjchem-562	173	35	,	,	PUNCT
eurjchem-562	173	36	br	br	PROPN
eurjchem-562	173	37	s	s	PROPN
eurjchem-562	173	38	,	,	PUNCT
eurjchem-562	173	39	nh	nh	PROPN
eurjchem-562	173	40	)	)	PUNCT
eurjchem-562	173	41	,	,	PUNCT
eurjchem-562	173	42	3.80	3.80	NUM
eurjchem-562	173	43	(	(	PUNCT
eurjchem-562	173	44	3h	3h	NUM
eurjchem-562	173	45	,	,	PUNCT
eurjchem-562	173	46	s	s	X
eurjchem-562	173	47	,	,	PUNCT
eurjchem-562	173	48	och3	och3	ADJ
eurjchem-562	173	49	)	)	PUNCT
eurjchem-562	173	50	,	,	PUNCT
eurjchem-562	173	51	3.79	3.79	NUM
eurjchem-562	173	52	(	(	PUNCT
eurjchem-562	173	53	3h	3h	NUM
eurjchem-562	173	54	,	,	PUNCT
eurjchem-562	173	55	s	s	X
eurjchem-562	173	56	,	,	PUNCT
eurjchem-562	173	57	och3	och3	ADJ
eurjchem-562	173	58	)	)	PUNCT
eurjchem-562	173	59	,	,	PUNCT
eurjchem-562	173	60	3.45	3.45	NUM
eurjchem-562	173	61	(	(	PUNCT
eurjchem-562	173	62	1h	1h	NUM
eurjchem-562	173	63	,	,	PUNCT
eurjchem-562	173	64	d	d	PROPN
eurjchem-562	173	65	,	,	PUNCT
eurjchem-562	173	66	j	j	PROPN
eurjchem-562	174	1	=	=	SYM
eurjchem-562	174	2	18	18	NUM
eurjchem-562	174	3	hz	hz	VERB
eurjchem-562	174	4	,	,	PUNCT
eurjchem-562	174	5	ch2	ch2	PROPN
eurjchem-562	174	6	)	)	PUNCT
eurjchem-562	174	7	,	,	PUNCT
eurjchem-562	174	8	3.11	3.11	NUM
eurjchem-562	174	9	(	(	PUNCT
eurjchem-562	174	10	1h	1h	NUM
eurjchem-562	174	11	,	,	PUNCT
eurjchem-562	174	12	d	d	PROPN
eurjchem-562	174	13	,	,	PUNCT
eurjchem-562	174	14	j	j	PROPN
eurjchem-562	174	15	=	=	SYM
eurjchem-562	174	16	18	18	NUM
eurjchem-562	174	17	hz	hz	VERB
eurjchem-562	174	18	,	,	PUNCT
eurjchem-562	174	19	ch2	ch2	PROPN
eurjchem-562	174	20	)	)	PUNCT
eurjchem-562	174	21	,	,	PUNCT
eurjchem-562	174	22	1.77	1.77	NUM
eurjchem-562	174	23	(	(	PUNCT
eurjchem-562	174	24	3h	3h	NUM
eurjchem-562	174	25	,	,	PUNCT
eurjchem-562	174	26	s	s	X
eurjchem-562	174	27	,	,	PUNCT
eurjchem-562	174	28	ch3	ch3	PROPN
eurjchem-562	174	29	)	)	PUNCT
eurjchem-562	174	30	.	.	PUNCT
eurjchem-562	175	1	13c	13c	NOUN
eurjchem-562	175	2	nmr	nmr	NOUN
eurjchem-562	175	3	(	(	PUNCT
eurjchem-562	175	4	75	75	NUM
eurjchem-562	175	5	mhz	mhz	NOUN
eurjchem-562	175	6	,	,	PUNCT
eurjchem-562	175	7	cdcl3	cdcl3	PROPN
eurjchem-562	175	8	,	,	PUNCT
eurjchem-562	175	9	δ	δ	PROPN
eurjchem-562	175	10	,	,	PUNCT
eurjchem-562	175	11	ppm	ppm	NOUN
eurjchem-562	175	12	):	):	PUNCT
eurjchem-562	175	13	166.3	166.3	NUM
eurjchem-562	175	14	,	,	PUNCT
eurjchem-562	175	15	160.3	160.3	NUM
eurjchem-562	175	16	,	,	PUNCT
eurjchem-562	175	17	157.1	157.1	NUM
eurjchem-562	175	18	,	,	PUNCT
eurjchem-562	175	19	143.0	143.0	NUM
eurjchem-562	175	20	,	,	PUNCT
eurjchem-562	175	21	136.7	136.7	NUM
eurjchem-562	175	22	,	,	PUNCT
eurjchem-562	175	23	130.3	130.3	NUM
eurjchem-562	175	24	,	,	PUNCT
eurjchem-562	175	25	120.2	120.2	NUM
eurjchem-562	175	26	,	,	PUNCT
eurjchem-562	175	27	118.2	118.2	NUM
eurjchem-562	175	28	,	,	PUNCT
eurjchem-562	175	29	116.6	116.6	NUM
eurjchem-562	175	30	,	,	PUNCT
eurjchem-562	175	31	114.6	114.6	NUM
eurjchem-562	175	32	,	,	PUNCT
eurjchem-562	175	33	113.2	113.2	NUM
eurjchem-562	175	34	,	,	PUNCT
eurjchem-562	175	35	112.8	112.8	NUM
eurjchem-562	175	36	,	,	PUNCT
eurjchem-562	175	37	112.7	112.7	NUM
eurjchem-562	175	38	,	,	PUNCT
eurjchem-562	175	39	112.5	112.5	NUM
eurjchem-562	175	40	,	,	PUNCT
eurjchem-562	175	41	111.5	111.5	NUM
eurjchem-562	175	42	,	,	PUNCT
eurjchem-562	175	43	101.9	101.9	NUM
eurjchem-562	175	44	,	,	PUNCT
eurjchem-562	175	45	67.1	67.1	NUM
eurjchem-562	175	46	,	,	PUNCT
eurjchem-562	175	47	56.7	56.7	NUM
eurjchem-562	175	48	,	,	PUNCT
eurjchem-562	175	49	55.5	55.5	NUM
eurjchem-562	175	50	,	,	PUNCT
eurjchem-562	175	51	55.4	55.4	NUM
eurjchem-562	175	52	,	,	PUNCT
eurjchem-562	175	53	45.5	45.5	NUM
eurjchem-562	175	54	,	,	PUNCT
eurjchem-562	175	55	29.3	29.3	NUM
eurjchem-562	175	56	.	.	PUNCT
eurjchem-562	175	57	hrms	hrm	VERB
eurjchem-562	175	58	calcd	calcd	NOUN
eurjchem-562	175	59	.	.	PUNCT
eurjchem-562	176	1	for	for	ADP
eurjchem-562	176	2	c24h21n4o2	c24h21n4o2	PROPN
eurjchem-562	176	3	(	(	PUNCT
eurjchem-562	176	4	m+h	m+h	NOUN
eurjchem-562	176	5	):	):	PUNCT
eurjchem-562	176	6	397.1665	397.1665	NUM
eurjchem-562	176	7	,	,	PUNCT
eurjchem-562	176	8	found	find	VERB
eurjchem-562	176	9	:	:	PUNCT
eurjchem-562	176	10	397.1638	397.1638	NUM
eurjchem-562	176	11	2‐(3‐cyano‐4,6‐bis(4‐nitrophenyl)‐6‐methyl‐5,6‐dihydro	2‐(3‐cyano‐4,6‐bis(4‐nitrophenyl)‐6‐methyl‐5,6‐dihydro	NUM
eurjchem-562	176	12	pyridin‐2(1h)‐ylidene)malononitrile	pyridin‐2(1h)‐ylidene)malononitrile	NOUN
eurjchem-562	176	13	(	(	PUNCT
eurjchem-562	176	14	43	43	NUM
eurjchem-562	176	15	):	):	PUNCT
eurjchem-562	176	16	brown	brown	ADJ
eurjchem-562	176	17	solid	solid	ADJ
eurjchem-562	176	18	.	.	PUNCT
eurjchem-562	177	1	mixture	mixture	NOUN
eurjchem-562	177	2	(	(	PUNCT
eurjchem-562	177	3	2/1	2/1	NUM
eurjchem-562	177	4	ratio	ratio	NOUN
eurjchem-562	177	5	)	)	PUNCT
eurjchem-562	177	6	of	of	ADP
eurjchem-562	177	7	43/48	43/48	NUM
eurjchem-562	177	8	.	.	PUNCT
eurjchem-562	178	1	ir	ir	PROPN
eurjchem-562	178	2	(	(	PUNCT
eurjchem-562	178	3	kbr	kbr	PROPN
eurjchem-562	178	4	,	,	PUNCT
eurjchem-562	178	5	νmax	νmax	NOUN
eurjchem-562	178	6	,	,	PUNCT
eurjchem-562	178	7	cm‐1	cm‐1	PROPN
eurjchem-562	178	8	):	):	PUNCT
eurjchem-562	178	9	3447	3447	NUM
eurjchem-562	178	10	(	(	PUNCT
eurjchem-562	178	11	nh	nh	NOUN
eurjchem-562	178	12	)	)	PUNCT
eurjchem-562	178	13	,	,	PUNCT
eurjchem-562	178	14	3419	3419	NUM
eurjchem-562	178	15	,	,	PUNCT
eurjchem-562	178	16	2963	2963	NUM
eurjchem-562	178	17	,	,	PUNCT
eurjchem-562	178	18	2928	2928	NUM
eurjchem-562	178	19	,	,	PUNCT
eurjchem-562	178	20	2188	2188	NUM
eurjchem-562	178	21	,	,	PUNCT
eurjchem-562	178	22	2160	2160	NUM
eurjchem-562	178	23	,	,	PUNCT
eurjchem-562	178	24	1596	1596	NUM
eurjchem-562	178	25	,	,	PUNCT
eurjchem-562	178	26	1520	1520	NUM
eurjchem-562	178	27	,	,	PUNCT
eurjchem-562	178	28	1453	1453	NUM
eurjchem-562	178	29	.	.	PUNCT
eurjchem-562	179	1	1h	1h	NUM
eurjchem-562	179	2	nmr	nmr	NOUN
eurjchem-562	179	3	(	(	PUNCT
eurjchem-562	179	4	300	300	NUM
eurjchem-562	179	5	mhz	mhz	NOUN
eurjchem-562	179	6	,	,	PUNCT
eurjchem-562	179	7	dmso	dmso	NOUN
eurjchem-562	179	8	,	,	PUNCT
eurjchem-562	179	9	δ	δ	PROPN
eurjchem-562	179	10	,	,	PUNCT
eurjchem-562	179	11	ppm	ppm	NUM
eurjchem-562	179	12	):	):	PUNCT
eurjchem-562	179	13	9.68	9.68	NUM
eurjchem-562	179	14	(	(	PUNCT
eurjchem-562	179	15	1h	1h	NUM
eurjchem-562	179	16	,	,	PUNCT
eurjchem-562	179	17	br	br	PROPN
eurjchem-562	179	18	s	s	PROPN
eurjchem-562	179	19	,	,	PUNCT
eurjchem-562	179	20	nh	nh	PROPN
eurjchem-562	179	21	)	)	PUNCT
eurjchem-562	179	22	,	,	PUNCT
eurjchem-562	179	23	8.30	8.30	NUM
eurjchem-562	179	24	(	(	PUNCT
eurjchem-562	179	25	2h	2h	NUM
eurjchem-562	179	26	,	,	PUNCT
eurjchem-562	179	27	dd	dd	NOUN
eurjchem-562	179	28	,	,	PUNCT
eurjchem-562	179	29	j	j	PROPN
eurjchem-562	179	30	=	=	SYM
eurjchem-562	179	31	9.0	9.0	NUM
eurjchem-562	179	32	hz	hz	NOUN
eurjchem-562	179	33	,	,	PUNCT
eurjchem-562	179	34	arh	arh	ADJ
eurjchem-562	179	35	)	)	PUNCT
eurjchem-562	179	36	,	,	PUNCT
eurjchem-562	179	37	8.26	8.26	NUM
eurjchem-562	179	38	(	(	PUNCT
eurjchem-562	179	39	2h	2h	NUM
eurjchem-562	179	40	,	,	PUNCT
eurjchem-562	179	41	d	d	NOUN
eurjchem-562	179	42	,	,	PUNCT
eurjchem-562	179	43	j	j	PROPN
eurjchem-562	179	44	=	=	SYM
eurjchem-562	179	45	9.0	9.0	NUM
eurjchem-562	179	46	hz	hz	NOUN
eurjchem-562	179	47	,	,	PUNCT
eurjchem-562	179	48	arh	arh	ADJ
eurjchem-562	179	49	)	)	PUNCT
eurjchem-562	179	50	,	,	PUNCT
eurjchem-562	179	51	7.73	7.73	NUM
eurjchem-562	179	52	(	(	PUNCT
eurjchem-562	179	53	2h	2h	NUM
eurjchem-562	179	54	d	d	SYM
eurjchem-562	179	55	j	j	X
eurjchem-562	179	56	=	=	SYM
eurjchem-562	179	57	9.0	9.0	NUM
eurjchem-562	179	58	hz	hz	NOUN
eurjchem-562	179	59	,	,	PUNCT
eurjchem-562	179	60	arh	arh	ADJ
eurjchem-562	179	61	)	)	PUNCT
eurjchem-562	179	62	,	,	PUNCT
eurjchem-562	179	63	7.62	7.62	NUM
eurjchem-562	179	64	(	(	PUNCT
eurjchem-562	179	65	2h	2h	NUM
eurjchem-562	179	66	,	,	PUNCT
eurjchem-562	179	67	d	d	NOUN
eurjchem-562	179	68	,	,	PUNCT
eurjchem-562	179	69	j	j	PROPN
eurjchem-562	179	70	=	=	SYM
eurjchem-562	179	71	9.0	9.0	NUM
eurjchem-562	179	72	hz	hz	NOUN
eurjchem-562	179	73	,	,	PUNCT
eurjchem-562	179	74	arh	arh	ADJ
eurjchem-562	179	75	)	)	PUNCT
eurjchem-562	179	76	,	,	PUNCT
eurjchem-562	179	77	3.70	3.70	NUM
eurjchem-562	179	78	(	(	PUNCT
eurjchem-562	179	79	1h	1h	NUM
eurjchem-562	179	80	,	,	PUNCT
eurjchem-562	179	81	d	d	PROPN
eurjchem-562	179	82	,	,	PUNCT
eurjchem-562	179	83	j	j	PROPN
eurjchem-562	179	84	=	=	SYM
eurjchem-562	179	85	18	18	NUM
eurjchem-562	179	86	hz	hz	VERB
eurjchem-562	179	87	,	,	PUNCT
eurjchem-562	179	88	ch2	ch2	PROPN
eurjchem-562	179	89	)	)	PUNCT
eurjchem-562	179	90	,	,	PUNCT
eurjchem-562	179	91	3.53	3.53	NUM
eurjchem-562	179	92	(	(	PUNCT
eurjchem-562	179	93	1h	1h	NUM
eurjchem-562	179	94	,	,	PUNCT
eurjchem-562	179	95	d	d	PROPN
eurjchem-562	179	96	,	,	PUNCT
eurjchem-562	179	97	j	j	PROPN
eurjchem-562	179	98	=	=	SYM
eurjchem-562	179	99	18	18	NUM
eurjchem-562	179	100	hz	hz	VERB
eurjchem-562	179	101	,	,	PUNCT
eurjchem-562	179	102	ch2	ch2	PROPN
eurjchem-562	179	103	)	)	PUNCT
eurjchem-562	179	104	,	,	PUNCT
eurjchem-562	179	105	1.77	1.77	NUM
eurjchem-562	179	106	(	(	PUNCT
eurjchem-562	179	107	3h	3h	NUM
eurjchem-562	179	108	,	,	PUNCT
eurjchem-562	179	109	s	s	X
eurjchem-562	179	110	,	,	PUNCT
eurjchem-562	179	111	ch3	ch3	PROPN
eurjchem-562	179	112	)	)	PUNCT
eurjchem-562	179	113	.	.	PUNCT
eurjchem-562	180	1	data	datum	NOUN
eurjchem-562	180	2	for	for	ADP
eurjchem-562	180	3	minor	minor	ADJ
eurjchem-562	180	4	isomer	isomer	NOUN
eurjchem-562	180	5	48	48	NUM
eurjchem-562	180	6	where	where	SCONJ
eurjchem-562	180	7	different	different	ADJ
eurjchem-562	180	8	from	from	ADP
eurjchem-562	180	9	major	major	ADJ
eurjchem-562	180	10	isomer	isomer	NOUN
eurjchem-562	180	11	43	43	NUM
eurjchem-562	180	12	,	,	PUNCT
eurjchem-562	180	13	8.19	8.19	NUM
eurjchem-562	180	14	(	(	PUNCT
eurjchem-562	180	15	4h	4h	NUM
eurjchem-562	180	16	,	,	PUNCT
eurjchem-562	180	17	dd	dd	PROPN
eurjchem-562	180	18	,	,	PUNCT
eurjchem-562	180	19	j	j	PROPN
eurjchem-562	180	20	=	=	SYM
eurjchem-562	180	21	8.7	8.7	NUM
eurjchem-562	180	22	hz	hz	VERB
eurjchem-562	180	23	,	,	PUNCT
eurjchem-562	180	24	5.4	5.4	NUM
eurjchem-562	180	25	hz	hz	NOUN
eurjchem-562	180	26	,	,	PUNCT
eurjchem-562	180	27	arh	arh	ADJ
eurjchem-562	180	28	)	)	PUNCT
eurjchem-562	180	29	,	,	PUNCT
eurjchem-562	180	30	7.68	7.68	NUM
eurjchem-562	180	31	(	(	PUNCT
eurjchem-562	180	32	2h	2h	NUM
eurjchem-562	180	33	,	,	PUNCT
eurjchem-562	180	34	d	d	NOUN
eurjchem-562	180	35	,	,	PUNCT
eurjchem-562	180	36	j	j	PROPN
eurjchem-562	181	1	=	=	SYM
eurjchem-562	181	2	9.0	9.0	NUM
eurjchem-562	181	3	hz	hz	NOUN
eurjchem-562	181	4	,	,	PUNCT
eurjchem-562	181	5	arh	arh	ADJ
eurjchem-562	181	6	)	)	PUNCT
eurjchem-562	181	7	,	,	PUNCT
eurjchem-562	181	8	7.60	7.60	NUM
eurjchem-562	181	9	(	(	PUNCT
eurjchem-562	181	10	2h	2h	NUM
eurjchem-562	181	11	,	,	PUNCT
eurjchem-562	181	12	d	d	NOUN
eurjchem-562	181	13	,	,	PUNCT
eurjchem-562	181	14	j	j	PROPN
eurjchem-562	181	15	=	=	SYM
eurjchem-562	181	16	9.0	9.0	NUM
eurjchem-562	181	17	hz	hz	VERB
eurjchem-562	181	18	arh	arh	PROPN
eurjchem-562	181	19	)	)	PUNCT
eurjchem-562	181	20	,	,	PUNCT
eurjchem-562	181	21	6.95	6.95	NUM
eurjchem-562	181	22	(	(	PUNCT
eurjchem-562	181	23	1h	1h	NUM
eurjchem-562	181	24	,	,	PUNCT
eurjchem-562	181	25	br	br	PROPN
eurjchem-562	181	26	s	s	PROPN
eurjchem-562	181	27	,	,	PUNCT
eurjchem-562	181	28	ch	ch	NOUN
eurjchem-562	181	29	=	=	NOUN
eurjchem-562	181	30	c	c	NOUN
eurjchem-562	181	31	)	)	PUNCT
eurjchem-562	181	32	,	,	PUNCT
eurjchem-562	181	33	1.61	1.61	NUM
eurjchem-562	181	34	(	(	PUNCT
eurjchem-562	181	35	3h	3h	NUM
eurjchem-562	181	36	,	,	PUNCT
eurjchem-562	181	37	s	s	X
eurjchem-562	181	38	,	,	PUNCT
eurjchem-562	181	39	ch3	ch3	PROPN
eurjchem-562	181	40	)	)	PUNCT
eurjchem-562	181	41	13c	13c	NOUN
eurjchem-562	181	42	nmr	nmr	NOUN
eurjchem-562	181	43	(	(	PUNCT
eurjchem-562	181	44	75	75	NUM
eurjchem-562	181	45	mhz	mhz	NOUN
eurjchem-562	181	46	,	,	PUNCT
eurjchem-562	181	47	dmso	dmso	NOUN
eurjchem-562	181	48	,	,	PUNCT
eurjchem-562	181	49	δ	δ	PROPN
eurjchem-562	181	50	,	,	PUNCT
eurjchem-562	181	51	ppm	ppm	NOUN
eurjchem-562	181	52	):	):	PUNCT
eurjchem-562	181	53	166.1	166.1	NUM
eurjchem-562	181	54	,	,	PUNCT
eurjchem-562	181	55	157.2	157.2	NUM
eurjchem-562	181	56	,	,	PUNCT
eurjchem-562	181	57	156.5	156.5	NUM
eurjchem-562	181	58	,	,	PUNCT
eurjchem-562	181	59	150.3	150.3	NUM
eurjchem-562	181	60	,	,	PUNCT
eurjchem-562	181	61	148.8	148.8	NUM
eurjchem-562	181	62	,	,	PUNCT
eurjchem-562	181	63	146.9	146.9	NUM
eurjchem-562	181	64	,	,	PUNCT
eurjchem-562	181	65	146.7	146.7	NUM
eurjchem-562	181	66	,	,	PUNCT
eurjchem-562	181	67	146.2	146.2	NUM
eurjchem-562	181	68	,	,	PUNCT
eurjchem-562	181	69	145.4	145.4	NUM
eurjchem-562	181	70	,	,	PUNCT
eurjchem-562	181	71	141.5	141.5	NUM
eurjchem-562	181	72	,	,	PUNCT
eurjchem-562	181	73	135.5	135.5	NUM
eurjchem-562	181	74	,	,	PUNCT
eurjchem-562	181	75	129.6	129.6	NUM
eurjchem-562	181	76	,	,	PUNCT
eurjchem-562	181	77	128.9	128.9	NUM
eurjchem-562	181	78	,	,	PUNCT
eurjchem-562	181	79	126.7	126.7	NUM
eurjchem-562	181	80	,	,	PUNCT
eurjchem-562	181	81	125.8	125.8	NUM
eurjchem-562	181	82	,	,	PUNCT
eurjchem-562	181	83	124.0	124.0	NUM
eurjchem-562	181	84	,	,	PUNCT
eurjchem-562	181	85	123.8	123.8	NUM
eurjchem-562	181	86	,	,	PUNCT
eurjchem-562	181	87	123.2	123.2	NUM
eurjchem-562	181	88	,	,	PUNCT
eurjchem-562	181	89	123.1	123.1	NUM
eurjchem-562	181	90	,	,	PUNCT
eurjchem-562	181	91	121.8	121.8	NUM
eurjchem-562	181	92	,	,	PUNCT
eurjchem-562	181	93	120.6	120.6	NUM
eurjchem-562	181	94	,	,	PUNCT
eurjchem-562	181	95	117.3	117.3	NUM
eurjchem-562	181	96	,	,	PUNCT
eurjchem-562	181	97	115.1	115.1	NUM
eurjchem-562	181	98	,	,	PUNCT
eurjchem-562	181	99	114.4	114.4	NUM
eurjchem-562	181	100	,	,	PUNCT
eurjchem-562	181	101	112.7	112.7	NUM
eurjchem-562	181	102	,	,	PUNCT
eurjchem-562	181	103	103.4	103.4	NUM
eurjchem-562	181	104	,	,	PUNCT
eurjchem-562	181	105	57.1	57.1	NUM
eurjchem-562	181	106	,	,	PUNCT
eurjchem-562	181	107	56.9	56.9	NUM
eurjchem-562	181	108	,	,	PUNCT
eurjchem-562	181	109	51.1	51.1	NUM
eurjchem-562	181	110	,	,	PUNCT
eurjchem-562	181	111	43.5	43.5	NUM
eurjchem-562	181	112	,	,	PUNCT
eurjchem-562	181	113	30.1	30.1	NUM
eurjchem-562	181	114	,	,	PUNCT
eurjchem-562	181	115	27.7	27.7	NUM
eurjchem-562	181	116	.	.	PUNCT
eurjchem-562	182	1	ms	ms	PROPN
eurjchem-562	182	2	(	(	PUNCT
eurjchem-562	182	3	esi	esi	ADJ
eurjchem-562	182	4	)	)	PUNCT
eurjchem-562	182	5	calcd	calcd	NOUN
eurjchem-562	182	6	.	.	PUNCT
eurjchem-562	183	1	for	for	ADP
eurjchem-562	183	2	c22h15n6o4	c22h15n6o4	PROPN
eurjchem-562	183	3	(	(	PUNCT
eurjchem-562	183	4	m+h	m+h	PROPN
eurjchem-562	183	5	):	):	PUNCT
eurjchem-562	183	6	427.1155	427.1155	NUM
eurjchem-562	183	7	,	,	PUNCT
eurjchem-562	183	8	found	find	VERB
eurjchem-562	183	9	:	:	PUNCT
eurjchem-562	183	10	427.1130	427.1130	NUM
eurjchem-562	183	11	.	.	PROPN
eurjchem-562	183	12	2‐(3‐cyano‐4,6‐bis(3‐nitrophenyl)‐6‐methyl‐5,6‐dihydro	2‐(3‐cyano‐4,6‐bis(3‐nitrophenyl)‐6‐methyl‐5,6‐dihydro	NUM
eurjchem-562	183	13	pyridin‐2(1h)‐ylidene)malononitrile	pyridin‐2(1h)‐ylidene)malononitrile	NOUN
eurjchem-562	183	14	(	(	PUNCT
eurjchem-562	183	15	44	44	NUM
eurjchem-562	183	16	):	):	PUNCT
eurjchem-562	183	17	brown	brown	ADJ
eurjchem-562	183	18	solid	solid	ADJ
eurjchem-562	183	19	.	.	PUNCT
eurjchem-562	184	1	yield	yield	NOUN
eurjchem-562	184	2	:	:	PUNCT
eurjchem-562	184	3	80	80	NUM
eurjchem-562	184	4	%	%	NOUN
eurjchem-562	184	5	.	.	PUNCT
eurjchem-562	185	1	mixture	mixture	NOUN
eurjchem-562	185	2	(	(	PUNCT
eurjchem-562	185	3	2/1	2/1	NUM
eurjchem-562	185	4	ratio	ratio	NOUN
eurjchem-562	185	5	)	)	PUNCT
eurjchem-562	185	6	of	of	ADP
eurjchem-562	185	7	44/49	44/49	NUM
eurjchem-562	185	8	.	.	PUNCT
eurjchem-562	186	1	ir	ir	PROPN
eurjchem-562	186	2	(	(	PUNCT
eurjchem-562	186	3	kbr	kbr	PROPN
eurjchem-562	186	4	,	,	PUNCT
eurjchem-562	186	5	νmax	νmax	NOUN
eurjchem-562	186	6	,	,	PUNCT
eurjchem-562	186	7	cm‐1	cm‐1	PROPN
eurjchem-562	186	8	):	):	PUNCT
eurjchem-562	186	9	3447	3447	NUM
eurjchem-562	186	10	(	(	PUNCT
eurjchem-562	186	11	nh	nh	NOUN
eurjchem-562	186	12	)	)	PUNCT
eurjchem-562	186	13	,	,	PUNCT
eurjchem-562	186	14	3382	3382	NUM
eurjchem-562	186	15	,	,	PUNCT
eurjchem-562	186	16	3266	3266	NUM
eurjchem-562	186	17	,	,	PUNCT
eurjchem-562	186	18	2219	2219	NUM
eurjchem-562	186	19	,	,	PUNCT
eurjchem-562	186	20	2202	2202	NUM
eurjchem-562	186	21	,	,	PUNCT
eurjchem-562	186	22	1612	1612	NUM
eurjchem-562	186	23	,	,	PUNCT
eurjchem-562	186	24	1523	1523	NUM
eurjchem-562	186	25	,	,	PUNCT
eurjchem-562	186	26	1437	1437	NUM
eurjchem-562	186	27	.	.	PUNCT
eurjchem-562	187	1	1h	1h	NUM
eurjchem-562	187	2	nmr	nmr	NOUN
eurjchem-562	187	3	(	(	PUNCT
eurjchem-562	187	4	300	300	NUM
eurjchem-562	187	5	mhz	mhz	NOUN
eurjchem-562	187	6	,	,	PUNCT
eurjchem-562	187	7	dmso	dmso	NOUN
eurjchem-562	187	8	,	,	PUNCT
eurjchem-562	187	9	δ	δ	PROPN
eurjchem-562	187	10	,	,	PUNCT
eurjchem-562	187	11	ppm	ppm	NOUN
eurjchem-562	187	12	):	):	PUNCT
eurjchem-562	187	13	9.84	9.84	NUM
eurjchem-562	187	14	(	(	PUNCT
eurjchem-562	187	15	1h	1h	NUM
eurjchem-562	187	16	,	,	PUNCT
eurjchem-562	187	17	br	br	PROPN
eurjchem-562	187	18	s	s	PROPN
eurjchem-562	187	19	,	,	PUNCT
eurjchem-562	187	20	nh	nh	PROPN
eurjchem-562	187	21	)	)	PUNCT
eurjchem-562	187	22	,	,	PUNCT
eurjchem-562	187	23	8.37	8.37	NUM
eurjchem-562	187	24	(	(	PUNCT
eurjchem-562	187	25	1h	1h	NUM
eurjchem-562	187	26	,	,	PUNCT
eurjchem-562	187	27	app	app	PROPN
eurjchem-562	187	28	dt	dt	PROPN
eurjchem-562	187	29	,	,	PUNCT
eurjchem-562	187	30	j	j	PROPN
eurjchem-562	187	31	=	=	SYM
eurjchem-562	187	32	8.0	8.0	NUM
eurjchem-562	187	33	hz	hz	NOUN
eurjchem-562	187	34	,	,	PUNCT
eurjchem-562	187	35	2.0	2.0	NUM
eurjchem-562	187	36	hz	hz	NOUN
eurjchem-562	187	37	,	,	PUNCT
eurjchem-562	187	38	arh	arh	ADJ
eurjchem-562	187	39	)	)	PUNCT
eurjchem-562	187	40	,	,	PUNCT
eurjchem-562	187	41	8.33	8.33	NUM
eurjchem-562	187	42	(	(	PUNCT
eurjchem-562	187	43	1h	1h	NUM
eurjchem-562	187	44	,	,	PUNCT
eurjchem-562	187	45	br	br	PROPN
eurjchem-562	187	46	s	s	PROPN
eurjchem-562	187	47	,	,	PUNCT
eurjchem-562	187	48	arh	arh	ADJ
eurjchem-562	187	49	)	)	PUNCT
eurjchem-562	187	50	,	,	PUNCT
eurjchem-562	187	51	8.26	8.26	NUM
eurjchem-562	187	52	(	(	PUNCT
eurjchem-562	187	53	2h	2h	NUM
eurjchem-562	187	54	,	,	PUNCT
eurjchem-562	187	55	app	app	PROPN
eurjchem-562	187	56	d	d	PROPN
eurjchem-562	187	57	,	,	PUNCT
eurjchem-562	187	58	j	j	PROPN
eurjchem-562	187	59	=	=	SYM
eurjchem-562	187	60	9.6	9.6	NUM
eurjchem-562	187	61	hz	hz	NOUN
eurjchem-562	187	62	,	,	PUNCT
eurjchem-562	187	63	arh	arh	ADJ
eurjchem-562	187	64	)	)	PUNCT
eurjchem-562	187	65	,	,	PUNCT
eurjchem-562	187	66	8.20‐8.13	8.20‐8.13	NUM
eurjchem-562	187	67	(	(	PUNCT
eurjchem-562	187	68	3h	3h	NUM
eurjchem-562	187	69	,	,	PUNCT
eurjchem-562	187	70	m	m	PROPN
eurjchem-562	187	71	,	,	PUNCT
eurjchem-562	187	72	arh	arh	ADJ
eurjchem-562	187	73	)	)	PUNCT
eurjchem-562	187	74	,	,	PUNCT
eurjchem-562	187	75	8.07	8.07	NUM
eurjchem-562	187	76	(	(	PUNCT
eurjchem-562	187	77	1h	1h	NUM
eurjchem-562	187	78	,	,	PUNCT
eurjchem-562	187	79	d	d	PROPN
eurjchem-562	187	80	,	,	PUNCT
eurjchem-562	187	81	j	j	PROPN
eurjchem-562	187	82	=	=	SYM
eurjchem-562	187	83	8.0	8.0	NUM
eurjchem-562	187	84	,	,	PUNCT
eurjchem-562	187	85	hz	hz	VERB
eurjchem-562	187	86	,	,	PUNCT
eurjchem-562	187	87	arh	arh	ADJ
eurjchem-562	187	88	)	)	PUNCT
eurjchem-562	187	89	,	,	PUNCT
eurjchem-562	187	90	7.94‐7.89	7.94‐7.89	NUM
eurjchem-562	187	91	(	(	PUNCT
eurjchem-562	187	92	2h	2h	NUM
eurjchem-562	187	93	,	,	PUNCT
eurjchem-562	187	94	m	m	NOUN
eurjchem-562	187	95	,	,	PUNCT
eurjchem-562	187	96	arh	arh	ADJ
eurjchem-562	187	97	)	)	PUNCT
eurjchem-562	187	98	,	,	PUNCT
eurjchem-562	187	99	7.84	7.84	NUM
eurjchem-562	187	100	(	(	PUNCT
eurjchem-562	187	101	1h	1h	NUM
eurjchem-562	187	102	,	,	PUNCT
eurjchem-562	187	103	app	app	PROPN
eurjchem-562	187	104	d	d	PROPN
eurjchem-562	187	105	,	,	PUNCT
eurjchem-562	187	106	j	j	PROPN
eurjchem-562	187	107	=	=	SYM
eurjchem-562	187	108	3.6	3.6	NUM
eurjchem-562	187	109	hz	hz	NOUN
eurjchem-562	187	110	,	,	PUNCT
eurjchem-562	187	111	arh	arh	ADJ
eurjchem-562	187	112	)	)	PUNCT
eurjchem-562	187	113	,	,	PUNCT
eurjchem-562	187	114	7.80	7.80	NUM
eurjchem-562	187	115	182	182	NUM
eurjchem-562	187	116	hameed	hameed	NOUN
eurjchem-562	187	117	et	et	PROPN
eurjchem-562	187	118	al	al	PROPN
eurjchem-562	187	119	.	.	PUNCT
eurjchem-562	187	120	/	/	SYM
eurjchem-562	187	121	european	european	PROPN
eurjchem-562	187	122	journal	journal	PROPN
eurjchem-562	187	123	of	of	ADP
eurjchem-562	187	124	chemistry	chemistry	NOUN
eurjchem-562	187	125	3	3	NUM
eurjchem-562	187	126	(	(	PUNCT
eurjchem-562	187	127	2	2	NUM
eurjchem-562	187	128	)	)	PUNCT
eurjchem-562	187	129	(	(	PUNCT
eurjchem-562	187	130	2012	2012	NUM
eurjchem-562	188	1	)	)	PUNCT
eurjchem-562	188	2	179‐185	179‐185	NUM
eurjchem-562	188	3	figure	figure	NOUN
eurjchem-562	188	4	2	2	NUM
eurjchem-562	188	5	.	.	PUNCT
eurjchem-562	189	1	x‐ray	x‐ray	PROPN
eurjchem-562	189	2	crystallographic	crystallographic	ADJ
eurjchem-562	189	3	structures	structure	NOUN
eurjchem-562	189	4	of	of	ADP
eurjchem-562	189	5	acetophenone	acetophenone	NOUN
eurjchem-562	189	6	dimer	dimer	NOUN
eurjchem-562	189	7	28	28	NUM
eurjchem-562	189	8	and	and	CCONJ
eurjchem-562	189	9	4	4	NUM
eurjchem-562	189	10	fluoro	fluoro	NOUN
eurjchem-562	189	11	dimer	dimer	NOUN
eurjchem-562	189	12	30	30	NUM
eurjchem-562	189	13	.	.	PUNCT
eurjchem-562	190	1	(	(	PUNCT
eurjchem-562	190	2	1h	1h	NUM
eurjchem-562	190	3	,	,	PUNCT
eurjchem-562	190	4	d	d	PROPN
eurjchem-562	190	5	,	,	PUNCT
eurjchem-562	190	6	j	j	PROPN
eurjchem-562	190	7	=	=	SYM
eurjchem-562	190	8	8.0	8.0	NUM
eurjchem-562	190	9	hz	hz	NOUN
eurjchem-562	190	10	,	,	PUNCT
eurjchem-562	190	11	arh	arh	ADJ
eurjchem-562	190	12	)	)	PUNCT
eurjchem-562	190	13	,	,	PUNCT
eurjchem-562	190	14	7.74	7.74	NUM
eurjchem-562	190	15	(	(	PUNCT
eurjchem-562	190	16	1h	1h	NUM
eurjchem-562	190	17	,	,	PUNCT
eurjchem-562	190	18	d	d	PROPN
eurjchem-562	190	19	,	,	PUNCT
eurjchem-562	190	20	j	j	PROPN
eurjchem-562	191	1	=	=	SYM
eurjchem-562	191	2	8.0	8.0	NUM
eurjchem-562	191	3	hz	hz	NOUN
eurjchem-562	191	4	,	,	PUNCT
eurjchem-562	191	5	arh	arh	ADJ
eurjchem-562	191	6	)	)	PUNCT
eurjchem-562	191	7	,	,	PUNCT
eurjchem-562	191	8	7.70‐7.62	7.70‐7.62	NUM
eurjchem-562	191	9	(	(	PUNCT
eurjchem-562	191	10	3h	3h	NUM
eurjchem-562	191	11	,	,	PUNCT
eurjchem-562	191	12	m	m	PROPN
eurjchem-562	191	13	,	,	PUNCT
eurjchem-562	191	14	arh	arh	ADJ
eurjchem-562	191	15	)	)	PUNCT
eurjchem-562	191	16	,	,	PUNCT
eurjchem-562	191	17	,	,	PUNCT
eurjchem-562	191	18	3.90	3.90	NUM
eurjchem-562	191	19	(	(	PUNCT
eurjchem-562	191	20	1h	1h	NUM
eurjchem-562	191	21	,	,	PUNCT
eurjchem-562	191	22	d	d	PROPN
eurjchem-562	191	23	,	,	PUNCT
eurjchem-562	191	24	j	j	PROPN
eurjchem-562	192	1	=	=	SYM
eurjchem-562	192	2	18	18	NUM
eurjchem-562	192	3	hz	hz	VERB
eurjchem-562	192	4	,	,	PUNCT
eurjchem-562	192	5	ch2	ch2	PROPN
eurjchem-562	192	6	)	)	PUNCT
eurjchem-562	192	7	,	,	PUNCT
eurjchem-562	192	8	3.46	3.46	NUM
eurjchem-562	192	9	(	(	PUNCT
eurjchem-562	192	10	1h	1h	NUM
eurjchem-562	192	11	,	,	PUNCT
eurjchem-562	192	12	d	d	PROPN
eurjchem-562	192	13	,	,	PUNCT
eurjchem-562	192	14	j	j	PROPN
eurjchem-562	192	15	=	=	SYM
eurjchem-562	192	16	18	18	NUM
eurjchem-562	192	17	hz	hz	VERB
eurjchem-562	192	18	,	,	PUNCT
eurjchem-562	192	19	ch2	ch2	PROPN
eurjchem-562	192	20	)	)	PUNCT
eurjchem-562	192	21	,	,	PUNCT
eurjchem-562	192	22	1.78	1.78	NUM
eurjchem-562	192	23	(	(	PUNCT
eurjchem-562	192	24	3h	3h	NUM
eurjchem-562	192	25	,	,	PUNCT
eurjchem-562	192	26	s	s	X
eurjchem-562	192	27	,	,	PUNCT
eurjchem-562	192	28	ch3	ch3	PROPN
eurjchem-562	192	29	)	)	PUNCT
eurjchem-562	192	30	.	.	PUNCT
eurjchem-562	193	1	data	datum	NOUN
eurjchem-562	193	2	for	for	ADP
eurjchem-562	193	3	minor	minor	ADJ
eurjchem-562	193	4	isomer	isomer	NOUN
eurjchem-562	193	5	44	44	NUM
eurjchem-562	193	6	where	where	SCONJ
eurjchem-562	193	7	different	different	ADJ
eurjchem-562	193	8	from	from	ADP
eurjchem-562	193	9	major	major	ADJ
eurjchem-562	193	10	isomer	isomer	NOUN
eurjchem-562	193	11	49	49	NUM
eurjchem-562	193	12	,	,	PUNCT
eurjchem-562	193	13	6.97	6.97	NUM
eurjchem-562	193	14	(	(	PUNCT
eurjchem-562	193	15	1h	1h	NUM
eurjchem-562	193	16	,	,	PUNCT
eurjchem-562	193	17	br	br	PROPN
eurjchem-562	193	18	s	s	PROPN
eurjchem-562	193	19	,	,	PUNCT
eurjchem-562	193	20	ch	ch	NOUN
eurjchem-562	193	21	=	=	NOUN
eurjchem-562	193	22	c	c	NOUN
eurjchem-562	193	23	)	)	PUNCT
eurjchem-562	193	24	,	,	PUNCT
eurjchem-562	193	25	1.62	1.62	NUM
eurjchem-562	193	26	(	(	PUNCT
eurjchem-562	193	27	3h	3h	NUM
eurjchem-562	193	28	,	,	PUNCT
eurjchem-562	193	29	s	s	X
eurjchem-562	193	30	,	,	PUNCT
eurjchem-562	193	31	ch3	ch3	PROPN
eurjchem-562	193	32	)	)	PUNCT
eurjchem-562	193	33	.	.	PUNCT
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eurjchem-562	194	2	nmr	nmr	NOUN
eurjchem-562	194	3	(	(	PUNCT
eurjchem-562	194	4	75	75	NUM
eurjchem-562	194	5	mhz	mhz	NOUN
eurjchem-562	194	6	,	,	PUNCT
eurjchem-562	194	7	dmso	dmso	NOUN
eurjchem-562	194	8	,	,	PUNCT
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eurjchem-562	194	10	,	,	PUNCT
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eurjchem-562	194	12	):	):	PUNCT
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eurjchem-562	194	14	,	,	PUNCT
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eurjchem-562	194	16	,	,	PUNCT
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eurjchem-562	194	22	,	,	PUNCT
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eurjchem-562	194	24	,	,	PUNCT
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eurjchem-562	194	26	,	,	PUNCT
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eurjchem-562	194	28	,	,	PUNCT
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eurjchem-562	194	30	,	,	PUNCT
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eurjchem-562	194	32	,	,	PUNCT
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eurjchem-562	194	34	,	,	PUNCT
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eurjchem-562	194	36	,	,	PUNCT
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eurjchem-562	194	38	,	,	PUNCT
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eurjchem-562	194	40	,	,	PUNCT
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eurjchem-562	194	42	,	,	PUNCT
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eurjchem-562	194	44	,	,	PUNCT
eurjchem-562	194	45	126.1	126.1	NUM
eurjchem-562	194	46	,	,	PUNCT
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eurjchem-562	194	48	,	,	PUNCT
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eurjchem-562	194	50	,	,	PUNCT
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eurjchem-562	194	52	,	,	PUNCT
eurjchem-562	194	53	121.9	121.9	NUM
eurjchem-562	194	54	,	,	PUNCT
eurjchem-562	194	55	121.7	121.7	NUM
eurjchem-562	194	56	,	,	PUNCT
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eurjchem-562	194	58	,	,	PUNCT
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eurjchem-562	194	60	,	,	PUNCT
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eurjchem-562	194	62	,	,	PUNCT
eurjchem-562	194	63	116.4	116.4	NUM
eurjchem-562	194	64	,	,	PUNCT
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eurjchem-562	194	66	,	,	PUNCT
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eurjchem-562	194	68	,	,	PUNCT
eurjchem-562	194	69	112.9	112.9	NUM
eurjchem-562	194	70	,	,	PUNCT
eurjchem-562	194	71	103.2	103.2	NUM
eurjchem-562	194	72	,	,	PUNCT
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eurjchem-562	194	74	,	,	PUNCT
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eurjchem-562	194	76	,	,	PUNCT
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eurjchem-562	194	78	,	,	PUNCT
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eurjchem-562	194	82	calcd	calcd	NOUN
eurjchem-562	194	83	.	.	PUNCT
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eurjchem-562	195	2	c22h14n6o4	c22h14n6o4	PROPN
eurjchem-562	195	3	(	(	PUNCT
eurjchem-562	195	4	m	m	PROPN
eurjchem-562	195	5	):	):	PUNCT
eurjchem-562	195	6	426.1077	426.1077	NUM
eurjchem-562	195	7	,	,	PUNCT
eurjchem-562	195	8	found	find	VERB
eurjchem-562	195	9	:	:	PUNCT
eurjchem-562	196	1	426.1068	426.1068	NUM
eurjchem-562	196	2	.	.	PUNCT
eurjchem-562	196	3	2‐(3‐cyano‐4,6‐bis(6‐methoxynaphthalen‐2‐yl)‐6‐methyl‐5,6‐	2‐(3‐cyano‐4,6‐bis(6‐methoxynaphthalen‐2‐yl)‐6‐methyl‐5,6‐	PROPN
eurjchem-562	196	4	dihydropyridin‐2(1h)‐ylidene)malononitriles	dihydropyridin‐2(1h)‐ylidene)malononitriles	PROPN
eurjchem-562	196	5	(	(	PUNCT
eurjchem-562	196	6	46	46	NUM
eurjchem-562	196	7	):	):	PUNCT
eurjchem-562	196	8	brown	brown	ADJ
eurjchem-562	196	9	solid	solid	ADJ
eurjchem-562	196	10	.	.	PUNCT
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eurjchem-562	196	12	:	:	PUNCT
eurjchem-562	196	13	65	65	NUM
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eurjchem-562	196	15	.	.	PUNCT
eurjchem-562	197	1	m.p	m.p	PROPN
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eurjchem-562	198	3	.	.	PROPN
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eurjchem-562	199	2	(	(	PUNCT
eurjchem-562	199	3	kbr	kbr	PROPN
eurjchem-562	199	4	,	,	PUNCT
eurjchem-562	199	5	νmax	νmax	NOUN
eurjchem-562	199	6	,	,	PUNCT
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eurjchem-562	199	8	):	):	PUNCT
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eurjchem-562	199	10	(	(	PUNCT
eurjchem-562	199	11	nh	nh	NOUN
eurjchem-562	199	12	)	)	PUNCT
eurjchem-562	199	13	,	,	PUNCT
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eurjchem-562	199	15	,	,	PUNCT
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eurjchem-562	199	17	,	,	PUNCT
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eurjchem-562	199	19	,	,	PUNCT
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eurjchem-562	199	23	,	,	PUNCT
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eurjchem-562	199	25	,	,	PUNCT
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eurjchem-562	199	27	.	.	PUNCT
eurjchem-562	200	1	1h	1h	NUM
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eurjchem-562	200	3	(	(	PUNCT
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eurjchem-562	200	5	mhz	mhz	NOUN
eurjchem-562	200	6	,	,	PUNCT
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eurjchem-562	200	10	,	,	PUNCT
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eurjchem-562	200	12	):	):	PUNCT
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eurjchem-562	200	15	1h	1h	NUM
eurjchem-562	200	16	,	,	PUNCT
eurjchem-562	200	17	app	app	PROPN
eurjchem-562	200	18	d	d	PROPN
eurjchem-562	200	19	,	,	PUNCT
eurjchem-562	200	20	j	j	PROPN
eurjchem-562	200	21	=	=	SYM
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eurjchem-562	200	23	hz	hz	NOUN
eurjchem-562	200	24	,	,	PUNCT
eurjchem-562	200	25	arh	arh	ADJ
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eurjchem-562	200	27	,	,	PUNCT
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eurjchem-562	200	29	(	(	PUNCT
eurjchem-562	200	30	1h	1h	NUM
eurjchem-562	200	31	,	,	PUNCT
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eurjchem-562	200	33	d	d	PROPN
eurjchem-562	200	34	,	,	PUNCT
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eurjchem-562	200	36	=	=	SYM
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eurjchem-562	200	39	,	,	PUNCT
eurjchem-562	200	40	arh	arh	ADJ
eurjchem-562	200	41	)	)	PUNCT
eurjchem-562	200	42	,	,	PUNCT
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eurjchem-562	200	45	3h	3h	NUM
eurjchem-562	200	46	,	,	PUNCT
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eurjchem-562	200	49	,	,	PUNCT
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eurjchem-562	200	51	=	=	SYM
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eurjchem-562	200	54	,	,	PUNCT
eurjchem-562	200	55	arh	arh	ADJ
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eurjchem-562	200	57	,	,	PUNCT
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eurjchem-562	200	60	1h	1h	NUM
eurjchem-562	200	61	,	,	PUNCT
eurjchem-562	200	62	app	app	PROPN
eurjchem-562	200	63	d	d	PROPN
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eurjchem-562	200	66	=	=	SYM
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eurjchem-562	200	69	,	,	PUNCT
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eurjchem-562	200	72	,	,	PUNCT
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eurjchem-562	200	75	1h	1h	NUM
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eurjchem-562	201	4	,	,	PUNCT
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eurjchem-562	201	7	,	,	PUNCT
eurjchem-562	201	8	arh	arh	ADJ
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eurjchem-562	201	10	,	,	PUNCT
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eurjchem-562	201	13	1h	1h	NUM
eurjchem-562	201	14	,	,	PUNCT
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eurjchem-562	201	16	,	,	PUNCT
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eurjchem-562	202	1	=	=	SYM
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eurjchem-562	202	4	,	,	PUNCT
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eurjchem-562	202	7	,	,	PUNCT
eurjchem-562	202	8	arh	arh	ADJ
eurjchem-562	202	9	)	)	PUNCT
eurjchem-562	202	10	,	,	PUNCT
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eurjchem-562	202	13	2h	2h	NUM
eurjchem-562	202	14	,	,	PUNCT
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eurjchem-562	202	16	td	td	NOUN
eurjchem-562	202	17	,	,	PUNCT
eurjchem-562	202	18	j	j	PROPN
eurjchem-562	202	19	=	=	SYM
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eurjchem-562	202	21	hz	hz	VERB
eurjchem-562	202	22	,	,	PUNCT
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eurjchem-562	202	24	hz	hz	NOUN
eurjchem-562	202	25	,	,	PUNCT
eurjchem-562	202	26	arh	arh	ADJ
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eurjchem-562	202	28	,	,	PUNCT
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eurjchem-562	202	30	(	(	PUNCT
eurjchem-562	202	31	1h	1h	NUM
eurjchem-562	202	32	,	,	PUNCT
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eurjchem-562	202	34	,	,	PUNCT
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eurjchem-562	202	42	,	,	PUNCT
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eurjchem-562	202	85	j	j	PROPN
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eurjchem-562	203	3	hz	hz	VERB
eurjchem-562	203	4	,	,	PUNCT
eurjchem-562	203	5	ch2	ch2	PROPN
eurjchem-562	203	6	)	)	PUNCT
eurjchem-562	203	7	,	,	PUNCT
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eurjchem-562	203	13	,	,	PUNCT
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eurjchem-562	203	15	=	=	SYM
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eurjchem-562	203	17	hz	hz	VERB
eurjchem-562	203	18	,	,	PUNCT
eurjchem-562	203	19	ch2	ch2	PROPN
eurjchem-562	203	20	)	)	PUNCT
eurjchem-562	203	21	,	,	PUNCT
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eurjchem-562	203	23	(	(	PUNCT
eurjchem-562	203	24	3h	3h	NUM
eurjchem-562	203	25	,	,	PUNCT
eurjchem-562	203	26	s	s	X
eurjchem-562	203	27	,	,	PUNCT
eurjchem-562	203	28	ch3	ch3	PROPN
eurjchem-562	203	29	)	)	PUNCT
eurjchem-562	203	30	.	.	PUNCT
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eurjchem-562	204	2	nmr	nmr	NOUN
eurjchem-562	204	3	(	(	PUNCT
eurjchem-562	204	4	100	100	NUM
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eurjchem-562	204	6	,	,	PUNCT
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eurjchem-562	204	8	,	,	PUNCT
eurjchem-562	204	9	δ	δ	PROPN
eurjchem-562	204	10	,	,	PUNCT
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eurjchem-562	204	12	):	):	PUNCT
eurjchem-562	204	13	166.2	166.2	NUM
eurjchem-562	204	14	,	,	PUNCT
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eurjchem-562	204	20	,	,	PUNCT
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eurjchem-562	204	24	,	,	PUNCT
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eurjchem-562	204	26	,	,	PUNCT
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eurjchem-562	204	28	,	,	PUNCT
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eurjchem-562	204	30	,	,	PUNCT
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eurjchem-562	204	32	,	,	PUNCT
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eurjchem-562	204	34	,	,	PUNCT
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eurjchem-562	204	36	,	,	PUNCT
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eurjchem-562	204	38	,	,	PUNCT
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eurjchem-562	204	40	,	,	PUNCT
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eurjchem-562	204	42	,	,	PUNCT
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eurjchem-562	204	50	,	,	PUNCT
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eurjchem-562	204	52	,	,	PUNCT
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eurjchem-562	204	54	,	,	PUNCT
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eurjchem-562	204	56	,	,	PUNCT
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eurjchem-562	204	58	,	,	PUNCT
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eurjchem-562	204	62	,	,	PUNCT
eurjchem-562	204	63	100.8	100.8	NUM
eurjchem-562	204	64	,	,	PUNCT
eurjchem-562	204	65	56.8	56.8	NUM
eurjchem-562	204	66	,	,	PUNCT
eurjchem-562	204	67	55.5	55.5	NUM
eurjchem-562	204	68	,	,	PUNCT
eurjchem-562	204	69	55.4	55.4	NUM
eurjchem-562	204	70	,	,	PUNCT
eurjchem-562	204	71	53.9	53.9	NUM
eurjchem-562	204	72	,	,	PUNCT
eurjchem-562	204	73	45.4	45.4	NUM
eurjchem-562	204	74	,	,	PUNCT
eurjchem-562	204	75	29.2	29.2	NUM
eurjchem-562	204	76	.	.	PUNCT
eurjchem-562	205	1	hrms	hrm	VERB
eurjchem-562	205	2	calcd	calcd	NOUN
eurjchem-562	205	3	.	.	PUNCT
eurjchem-562	206	1	for	for	ADP
eurjchem-562	206	2	c32h24n4o2	c32h24n4o2	PROPN
eurjchem-562	206	3	(	(	PUNCT
eurjchem-562	206	4	m	m	PROPN
eurjchem-562	206	5	):	):	PUNCT
eurjchem-562	206	6	496.1939	496.1939	NUM
eurjchem-562	206	7	,	,	PUNCT
eurjchem-562	206	8	found	find	VERB
eurjchem-562	206	9	:	:	PUNCT
eurjchem-562	206	10	496.1912	496.1912	NUM
eurjchem-562	206	11	.	.	NOUN
eurjchem-562	207	1	3	3	X
eurjchem-562	207	2	.	.	NOUN
eurjchem-562	207	3	results	result	NOUN
eurjchem-562	207	4	and	and	CCONJ
eurjchem-562	207	5	discussion	discussion	NOUN
eurjchem-562	207	6	towards	towards	ADP
eurjchem-562	207	7	our	our	PRON
eurjchem-562	207	8	proposed	propose	VERB
eurjchem-562	207	9	synthetic	synthetic	ADJ
eurjchem-562	207	10	target	target	NOUN
eurjchem-562	207	11	,	,	PUNCT
eurjchem-562	207	12	we	we	PRON
eurjchem-562	207	13	required	require	VERB
eurjchem-562	207	14	to	to	PART
eurjchem-562	207	15	prepare	prepare	VERB
eurjchem-562	207	16	the	the	DET
eurjchem-562	207	17	alkylidenemalononitriles	alkylidenemalononitrile	NOUN
eurjchem-562	207	18	10‐27	10‐27	NUM
eurjchem-562	207	19	via	via	ADP
eurjchem-562	207	20	an	an	DET
eurjchem-562	207	21	appropriate	appropriate	ADJ
eurjchem-562	207	22	method	method	NOUN
eurjchem-562	207	23	to	to	PART
eurjchem-562	207	24	test	test	VERB
eurjchem-562	207	25	the	the	DET
eurjchem-562	207	26	tbaf	tbaf	ADJ
eurjchem-562	207	27	mediated	mediate	VERB
eurjchem-562	207	28	cyclization	cyclization	NOUN
eurjchem-562	207	29	conditions	condition	NOUN
eurjchem-562	207	30	to	to	PART
eurjchem-562	207	31	form	form	VERB
eurjchem-562	207	32	dicyano	dicyano	NOUN
eurjchem-562	207	33	substituted	substitute	VERB
eurjchem-562	207	34	dihydropyridine	dihydropyridine	NOUN
eurjchem-562	207	35	derivatives	derivative	NOUN
eurjchem-562	207	36	28‐46	28‐46	NUM
eurjchem-562	207	37	(	(	PUNCT
eurjchem-562	207	38	scheme	scheme	NOUN
eurjchem-562	207	39	1	1	NUM
eurjchem-562	207	40	)	)	PUNCT
eurjchem-562	207	41	.	.	PUNCT
eurjchem-562	208	1	the	the	DET
eurjchem-562	208	2	desired	desire	VERB
eurjchem-562	208	3	precursors	precursor	NOUN
eurjchem-562	208	4	10‐27	10‐27	NOUN
eurjchem-562	208	5	for	for	ADP
eurjchem-562	208	6	this	this	DET
eurjchem-562	208	7	purpose	purpose	NOUN
eurjchem-562	208	8	were	be	AUX
eurjchem-562	208	9	prepared	prepare	VERB
eurjchem-562	208	10	from	from	ADP
eurjchem-562	208	11	commercially	commercially	ADV
eurjchem-562	208	12	available	available	ADJ
eurjchem-562	208	13	substituted	substitute	VERB
eurjchem-562	208	14	acetophenone	acetophenone	NOUN
eurjchem-562	208	15	derivatives	derivative	NOUN
eurjchem-562	208	16	via	via	ADP
eurjchem-562	208	17	knoevenagel	knoevenagel	NOUN
eurjchem-562	208	18	condensation	condensation	NOUN
eurjchem-562	208	19	with	with	ADP
eurjchem-562	208	20	malononitrile	malononitrile	NOUN
eurjchem-562	208	21	by	by	ADP
eurjchem-562	208	22	following	follow	VERB
eurjchem-562	208	23	the	the	DET
eurjchem-562	208	24	procedure	procedure	NOUN
eurjchem-562	208	25	developed	develop	VERB
eurjchem-562	208	26	by	by	ADP
eurjchem-562	208	27	barnes	barnes	PROPN
eurjchem-562	208	28	et	et	PROPN
eurjchem-562	208	29	al	al	PROPN
eurjchem-562	208	30	.	.	PUNCT
eurjchem-562	209	1	[	[	X
eurjchem-562	209	2	2	2	X
eurjchem-562	209	3	]	]	PUNCT
eurjchem-562	209	4	in	in	ADP
eurjchem-562	209	5	good	good	ADJ
eurjchem-562	209	6	to	to	ADP
eurjchem-562	209	7	excellent	excellent	ADJ
eurjchem-562	209	8	yield	yield	NOUN
eurjchem-562	209	9	(	(	PUNCT
eurjchem-562	209	10	50	50	NUM
eurjchem-562	209	11	to	to	PART
eurjchem-562	209	12	95	95	NUM
eurjchem-562	209	13	%	%	NOUN
eurjchem-562	209	14	)	)	PUNCT
eurjchem-562	209	15	.	.	PUNCT
eurjchem-562	210	1	the	the	DET
eurjchem-562	210	2	successful	successful	ADJ
eurjchem-562	210	3	preparation	preparation	NOUN
eurjchem-562	210	4	of	of	ADP
eurjchem-562	210	5	alkylidenemalononitriles	alkylidenemalononitrile	NOUN
eurjchem-562	210	6	10‐	10‐	NUM
eurjchem-562	210	7	27	27	NUM
eurjchem-562	210	8	were	be	AUX
eurjchem-562	210	9	enabled	enable	VERB
eurjchem-562	210	10	us	we	PRON
eurjchem-562	210	11	to	to	PART
eurjchem-562	210	12	explore	explore	VERB
eurjchem-562	210	13	their	their	PRON
eurjchem-562	210	14	dimerization	dimerization	NOUN
eurjchem-562	210	15	under	under	ADP
eurjchem-562	210	16	solvent‐free	solvent‐free	NOUN
eurjchem-562	210	17	conditions	condition	NOUN
eurjchem-562	210	18	for	for	ADP
eurjchem-562	210	19	the	the	DET
eurjchem-562	210	20	preparation	preparation	NOUN
eurjchem-562	210	21	of	of	ADP
eurjchem-562	210	22	dicyano	dicyano	PROPN
eurjchem-562	210	23	substituted	substitute	VERB
eurjchem-562	210	24	dihydropyridine	dihydropyridine	NOUN
eurjchem-562	210	25	derivatives	derivative	NOUN
eurjchem-562	210	26	28‐46	28‐46	NUM
eurjchem-562	210	27	.	.	PUNCT
eurjchem-562	211	1	initially	initially	ADV
eurjchem-562	211	2	,	,	PUNCT
eurjchem-562	211	3	the	the	DET
eurjchem-562	211	4	phenyl	phenyl	NOUN
eurjchem-562	211	5	alkylidenemalononitrile	alkylidenemalononitrile	NOUN
eurjchem-562	211	6	10	10	NUM
eurjchem-562	211	7	was	be	AUX
eurjchem-562	211	8	treated	treat	VERB
eurjchem-562	211	9	with	with	ADP
eurjchem-562	211	10	neat	neat	ADJ
eurjchem-562	211	11	tbaf.3h2o	tbaf.3h2o	NOUN
eurjchem-562	211	12	under	under	ADP
eurjchem-562	211	13	solvent‐free	solvent‐free	NOUN
eurjchem-562	211	14	conditions	condition	NOUN
eurjchem-562	211	15	to	to	PART
eurjchem-562	211	16	get	get	VERB
eurjchem-562	211	17	the	the	DET
eurjchem-562	211	18	desire	desire	NOUN
eurjchem-562	211	19	dimerized	dimerize	VERB
eurjchem-562	211	20	product	product	NOUN
eurjchem-562	211	21	28	28	NUM
eurjchem-562	211	22	in	in	ADP
eurjchem-562	211	23	low	low	ADJ
eurjchem-562	211	24	yield	yield	NOUN
eurjchem-562	211	25	(	(	PUNCT
eurjchem-562	211	26	20	20	NUM
eurjchem-562	211	27	%	%	NOUN
eurjchem-562	211	28	)	)	PUNCT
eurjchem-562	211	29	having	have	VERB
eurjchem-562	211	30	molecular	molecular	ADJ
eurjchem-562	211	31	ion	ion	NOUN
eurjchem-562	211	32	peak	peak	NOUN
eurjchem-562	211	33	at	at	ADP
eurjchem-562	211	34	m	m	PROPN
eurjchem-562	211	35	/	/	SYM
eurjchem-562	211	36	z	z	NOUN
eurjchem-562	211	37	=	=	SYM
eurjchem-562	211	38	336	336	NUM
eurjchem-562	211	39	.	.	PUNCT
eurjchem-562	212	1	the	the	DET
eurjchem-562	212	2	next	next	ADJ
eurjchem-562	212	3	step	step	NOUN
eurjchem-562	212	4	involved	involve	VERB
eurjchem-562	212	5	,	,	PUNCT
eurjchem-562	212	6	was	be	AUX
eurjchem-562	212	7	the	the	DET
eurjchem-562	212	8	structure	structure	NOUN
eurjchem-562	212	9	elucidation	elucidation	NOUN
eurjchem-562	212	10	of	of	ADP
eurjchem-562	212	11	this	this	DET
eurjchem-562	212	12	new	new	ADJ
eurjchem-562	212	13	compound	compound	NOUN
eurjchem-562	212	14	.	.	PUNCT
eurjchem-562	213	1	there	there	PRON
eurjchem-562	213	2	are	be	VERB
eurjchem-562	213	3	different	different	ADJ
eurjchem-562	213	4	possibilities	possibility	NOUN
eurjchem-562	213	5	in	in	ADP
eurjchem-562	213	6	which	which	PRON
eurjchem-562	213	7	the	the	DET
eurjchem-562	213	8	alkylidenemalononitrile	alkylidenemalononitrile	NOUN
eurjchem-562	213	9	could	could	AUX
eurjchem-562	213	10	be	be	AUX
eurjchem-562	213	11	dimerized	dimerize	VERB
eurjchem-562	213	12	to	to	PART
eurjchem-562	213	13	give	give	VERB
eurjchem-562	213	14	different	different	ADJ
eurjchem-562	213	15	structures	structure	NOUN
eurjchem-562	213	16	as	as	SCONJ
eurjchem-562	213	17	shown	show	VERB
eurjchem-562	213	18	in	in	ADP
eurjchem-562	213	19	scheme	scheme	NOUN
eurjchem-562	213	20	1	1	NUM
eurjchem-562	213	21	.	.	PUNCT
eurjchem-562	214	1	the	the	DET
eurjchem-562	214	2	1h	1h	NUM
eurjchem-562	214	3	nmr	nmr	NOUN
eurjchem-562	214	4	spectra	spectra	NOUN
eurjchem-562	214	5	of	of	ADP
eurjchem-562	214	6	compound	compound	NOUN
eurjchem-562	214	7	28	28	NUM
eurjchem-562	214	8	showed	show	VERB
eurjchem-562	214	9	four	four	NUM
eurjchem-562	214	10	distinguished	distinguished	ADJ
eurjchem-562	214	11	signals	signal	NOUN
eurjchem-562	214	12	for	for	ADP
eurjchem-562	214	13	four	four	NUM
eurjchem-562	214	14	groups	group	NOUN
eurjchem-562	214	15	,	,	PUNCT
eurjchem-562	214	16	a	a	DET
eurjchem-562	214	17	)	)	PUNCT
eurjchem-562	214	18	singlet	singlet	NOUN
eurjchem-562	214	19	for	for	ADP
eurjchem-562	214	20	methyl	methyl	NOUN
eurjchem-562	214	21	group	group	NOUN
eurjchem-562	214	22	at	at	ADP
eurjchem-562	214	23	δh	δh	NOUN
eurjchem-562	214	24	=	=	SYM
eurjchem-562	214	25	1.79	1.79	NUM
eurjchem-562	214	26	,	,	PUNCT
eurjchem-562	214	27	b	b	NOUN
eurjchem-562	214	28	)	)	PUNCT
eurjchem-562	214	29	two	two	NUM
eurjchem-562	214	30	doublets	doublet	NOUN
eurjchem-562	214	31	for	for	ADP
eurjchem-562	214	32	two	two	NUM
eurjchem-562	214	33	non‐equivalent	non‐equivalent	ADJ
eurjchem-562	214	34	protons	proton	NOUN
eurjchem-562	214	35	of	of	ADP
eurjchem-562	214	36	methylene	methylene	NOUN
eurjchem-562	214	37	group	group	NOUN
eurjchem-562	214	38	at	at	ADP
eurjchem-562	214	39	δh	δh	ADP
eurjchem-562	214	40	=	=	SYM
eurjchem-562	214	41	3.49	3.49	NUM
eurjchem-562	214	42	,	,	PUNCT
eurjchem-562	214	43	3.15	3.15	NUM
eurjchem-562	214	44	,	,	PUNCT
eurjchem-562	214	45	c	c	NOUN
eurjchem-562	214	46	)	)	PUNCT
eurjchem-562	214	47	multiplet	multiplet	NOUN
eurjchem-562	214	48	for	for	ADP
eurjchem-562	214	49	aromatic	aromatic	ADJ
eurjchem-562	214	50	protons	proton	NOUN
eurjchem-562	214	51	between	between	ADP
eurjchem-562	214	52	7.24‐7.50	7.24‐7.50	PROPN
eurjchem-562	214	53	,	,	PUNCT
eurjchem-562	214	54	and	and	CCONJ
eurjchem-562	214	55	d	d	NOUN
eurjchem-562	214	56	)	)	PUNCT
eurjchem-562	214	57	broad	broad	ADJ
eurjchem-562	214	58	singlet	singlet	NOUN
eurjchem-562	214	59	for	for	ADP
eurjchem-562	214	60	nh	nh	PROPN
eurjchem-562	214	61	group	group	NOUN
eurjchem-562	214	62	at	at	ADP
eurjchem-562	214	63	δh	δh	ADP
eurjchem-562	214	64	=	=	SYM
eurjchem-562	214	65	6.58	6.58	NUM
eurjchem-562	214	66	ppm	ppm	NOUN
eurjchem-562	214	67	.	.	PUNCT
eurjchem-562	215	1	interestingly	interestingly	ADV
eurjchem-562	215	2	,	,	PUNCT
eurjchem-562	215	3	it	it	PRON
eurjchem-562	215	4	has	have	AUX
eurjchem-562	215	5	been	be	AUX
eurjchem-562	215	6	observed	observe	VERB
eurjchem-562	215	7	that	that	SCONJ
eurjchem-562	215	8	the	the	DET
eurjchem-562	215	9	value	value	NOUN
eurjchem-562	215	10	of	of	ADP
eurjchem-562	215	11	nh	nh	PROPN
eurjchem-562	215	12	group	group	NOUN
eurjchem-562	215	13	resonated	resonate	VERB
eurjchem-562	215	14	between	between	ADP
eurjchem-562	215	15	6.00	6.00	NUM
eurjchem-562	215	16	to	to	PART
eurjchem-562	215	17	9.50	9.50	NUM
eurjchem-562	215	18	ppm	ppm	NOUN
eurjchem-562	215	19	depends	depend	VERB
eurjchem-562	215	20	upon	upon	SCONJ
eurjchem-562	215	21	the	the	DET
eurjchem-562	215	22	solvent	solvent	NOUN
eurjchem-562	215	23	used	use	VERB
eurjchem-562	215	24	to	to	PART
eurjchem-562	215	25	run	run	VERB
eurjchem-562	215	26	the	the	DET
eurjchem-562	215	27	1h	1h	NUM
eurjchem-562	215	28	nmr	nmr	NOUN
eurjchem-562	215	29	spectrum	spectrum	NOUN
eurjchem-562	215	30	.	.	PUNCT
eurjchem-562	216	1	it	it	PRON
eurjchem-562	216	2	shifted	shift	VERB
eurjchem-562	216	3	towards	towards	ADP
eurjchem-562	216	4	downfield	downfield	NOUN
eurjchem-562	216	5	region	region	NOUN
eurjchem-562	216	6	when	when	SCONJ
eurjchem-562	216	7	1h	1h	NUM
eurjchem-562	216	8	nmr	nmr	NOUN
eurjchem-562	216	9	run	run	VERB
eurjchem-562	216	10	in	in	ADP
eurjchem-562	216	11	dmso	dmso	ADJ
eurjchem-562	216	12	solvent	solvent	NOUN
eurjchem-562	216	13	and	and	CCONJ
eurjchem-562	216	14	this	this	PRON
eurjchem-562	216	15	was	be	AUX
eurjchem-562	216	16	later	later	ADV
eurjchem-562	216	17	confirmed	confirm	VERB
eurjchem-562	216	18	by	by	ADP
eurjchem-562	216	19	obtaining	obtain	VERB
eurjchem-562	216	20	the	the	DET
eurjchem-562	216	21	1h	1h	NUM
eurjchem-562	216	22	nmr	nmr	NOUN
eurjchem-562	216	23	of	of	ADP
eurjchem-562	216	24	4‐fluoro	4‐fluoro	NUM
eurjchem-562	216	25	dimer	dimer	VERB
eurjchem-562	216	26	30	30	NUM
eurjchem-562	216	27	in	in	ADP
eurjchem-562	216	28	both	both	DET
eurjchem-562	216	29	cdcl3	cdcl3	NOUN
eurjchem-562	216	30	(	(	PUNCT
eurjchem-562	216	31	δh	δh	ADP
eurjchem-562	216	32	=	=	NUM
eurjchem-562	216	33	6.41	6.41	NUM
eurjchem-562	216	34	ppm	ppm	NOUN
eurjchem-562	216	35	)	)	PUNCT
eurjchem-562	216	36	and	and	CCONJ
eurjchem-562	216	37	dmso	dmso	NOUN
eurjchem-562	216	38	(	(	PUNCT
eurjchem-562	216	39	δh	δh	ADP
eurjchem-562	216	40	=	=	SYM
eurjchem-562	216	41	9.72	9.72	NUM
eurjchem-562	216	42	ppm	ppm	NOUN
eurjchem-562	216	43	)	)	PUNCT
eurjchem-562	216	44	.	.	PUNCT
eurjchem-562	217	1	the	the	DET
eurjchem-562	217	2	above	above	ADV
eurjchem-562	217	3	mentioned	mention	VERB
eurjchem-562	217	4	data	datum	NOUN
eurjchem-562	217	5	is	be	AUX
eurjchem-562	217	6	pretty	pretty	ADV
eurjchem-562	217	7	much	much	ADV
eurjchem-562	217	8	comparable	comparable	ADJ
eurjchem-562	217	9	with	with	ADP
eurjchem-562	217	10	the	the	DET
eurjchem-562	217	11	reported	report	VERB
eurjchem-562	217	12	data	datum	NOUN
eurjchem-562	217	13	of	of	ADP
eurjchem-562	217	14	structure	structure	NOUN
eurjchem-562	217	15	5	5	NUM
eurjchem-562	218	1	[	[	X
eurjchem-562	218	2	22,23	22,23	NOUN
eurjchem-562	218	3	]	]	PUNCT
eurjchem-562	218	4	and	and	CCONJ
eurjchem-562	218	5	structure	structure	NOUN
eurjchem-562	218	6	8	8	NUM
eurjchem-562	219	1	[	[	X
eurjchem-562	219	2	8	8	NUM
eurjchem-562	219	3	]	]	PUNCT
eurjchem-562	219	4	.	.	PUNCT
eurjchem-562	220	1	therefore	therefore	ADV
eurjchem-562	220	2	,	,	PUNCT
eurjchem-562	220	3	in	in	ADP
eurjchem-562	220	4	order	order	NOUN
eurjchem-562	220	5	to	to	PART
eurjchem-562	220	6	solve	solve	VERB
eurjchem-562	220	7	the	the	DET
eurjchem-562	220	8	structural	structural	ADJ
eurjchem-562	220	9	ambiguity	ambiguity	NOUN
eurjchem-562	220	10	,	,	PUNCT
eurjchem-562	220	11	the	the	DET
eurjchem-562	220	12	compound	compound	NOUN
eurjchem-562	220	13	was	be	AUX
eurjchem-562	220	14	treated	treat	VERB
eurjchem-562	220	15	with	with	ADP
eurjchem-562	220	16	naome	naome	NOUN
eurjchem-562	220	17	by	by	ADP
eurjchem-562	220	18	using	use	VERB
eurjchem-562	220	19	literature	literature	NOUN
eurjchem-562	220	20	procedure	procedure	NOUN
eurjchem-562	220	21	to	to	PART
eurjchem-562	220	22	produce	produce	VERB
eurjchem-562	220	23	compound	compound	NOUN
eurjchem-562	220	24	6	6	NUM
eurjchem-562	220	25	by	by	ADP
eurjchem-562	220	26	assuming	assume	VERB
eurjchem-562	220	27	the	the	DET
eurjchem-562	220	28	structure	structure	NOUN
eurjchem-562	220	29	5	5	NUM
eurjchem-562	220	30	of	of	ADP
eurjchem-562	220	31	the	the	DET
eurjchem-562	220	32	new	new	ADJ
eurjchem-562	220	33	compound	compound	NOUN
eurjchem-562	220	34	[	[	X
eurjchem-562	220	35	24	24	NUM
eurjchem-562	220	36	]	]	PUNCT
eurjchem-562	220	37	.	.	PUNCT
eurjchem-562	221	1	but	but	CCONJ
eurjchem-562	221	2	the	the	DET
eurjchem-562	221	3	experiment	experiment	NOUN
eurjchem-562	221	4	proved	prove	VERB
eurjchem-562	221	5	to	to	ADP
eurjchem-562	221	6	unsuccessful	unsuccessful	ADJ
eurjchem-562	221	7	and	and	CCONJ
eurjchem-562	221	8	we	we	PRON
eurjchem-562	221	9	would	would	AUX
eurjchem-562	221	10	not	not	PART
eurjchem-562	221	11	be	be	AUX
eurjchem-562	221	12	able	able	ADJ
eurjchem-562	221	13	to	to	PART
eurjchem-562	221	14	obtain	obtain	VERB
eurjchem-562	221	15	the	the	DET
eurjchem-562	221	16	desired	desire	VERB
eurjchem-562	221	17	compound	compound	NOUN
eurjchem-562	221	18	6	6	NUM
eurjchem-562	221	19	.	.	PUNCT
eurjchem-562	222	1	the	the	DET
eurjchem-562	222	2	reaction	reaction	NOUN
eurjchem-562	222	3	mixture	mixture	NOUN
eurjchem-562	222	4	became	become	VERB
eurjchem-562	222	5	very	very	ADV
eurjchem-562	222	6	sluggish	sluggish	ADJ
eurjchem-562	222	7	and	and	CCONJ
eurjchem-562	222	8	even	even	ADV
eurjchem-562	222	9	no	no	DET
eurjchem-562	222	10	starting	starting	NOUN
eurjchem-562	222	11	material	material	NOUN
eurjchem-562	222	12	was	be	AUX
eurjchem-562	222	13	recovered	recover	VERB
eurjchem-562	222	14	.	.	PUNCT
eurjchem-562	223	1	thus	thus	ADV
eurjchem-562	223	2	,	,	PUNCT
eurjchem-562	223	3	with	with	ADP
eurjchem-562	223	4	all	all	DET
eurjchem-562	223	5	these	these	DET
eurjchem-562	223	6	results	result	NOUN
eurjchem-562	223	7	,	,	PUNCT
eurjchem-562	223	8	the	the	DET
eurjchem-562	223	9	x‐ray	x‐ray	PROPN
eurjchem-562	223	10	crystallographic	crystallographic	ADJ
eurjchem-562	223	11	technique	technique	NOUN
eurjchem-562	223	12	became	become	VERB
eurjchem-562	223	13	obligatory	obligatory	ADJ
eurjchem-562	223	14	to	to	PART
eurjchem-562	223	15	establish	establish	VERB
eurjchem-562	223	16	the	the	DET
eurjchem-562	223	17	structure	structure	NOUN
eurjchem-562	223	18	of	of	ADP
eurjchem-562	223	19	this	this	DET
eurjchem-562	223	20	new	new	ADJ
eurjchem-562	223	21	dimer	dimer	NOUN
eurjchem-562	223	22	.	.	PUNCT
eurjchem-562	224	1	for	for	ADP
eurjchem-562	224	2	this	this	DET
eurjchem-562	224	3	purpose	purpose	NOUN
eurjchem-562	224	4	,	,	PUNCT
eurjchem-562	224	5	the	the	DET
eurjchem-562	224	6	compound	compound	NOUN
eurjchem-562	224	7	was	be	AUX
eurjchem-562	224	8	crystallized	crystallize	VERB
eurjchem-562	224	9	with	with	ADP
eurjchem-562	224	10	little	little	ADJ
eurjchem-562	224	11	effort	effort	NOUN
eurjchem-562	224	12	in	in	ADP
eurjchem-562	224	13	the	the	DET
eurjchem-562	224	14	mixture	mixture	NOUN
eurjchem-562	224	15	of	of	ADP
eurjchem-562	224	16	ethanol	ethanol	NOUN
eurjchem-562	224	17	/	/	SYM
eurjchem-562	224	18	h2o	h2o	NOUN
eurjchem-562	224	19	mixture	mixture	NOUN
eurjchem-562	224	20	and	and	CCONJ
eurjchem-562	224	21	then	then	ADV
eurjchem-562	224	22	x‐ray	x‐ray	PROPN
eurjchem-562	224	23	crystallographic	crystallographic	ADJ
eurjchem-562	224	24	structure	structure	NOUN
eurjchem-562	224	25	of	of	ADP
eurjchem-562	224	26	compound	compound	NOUN
eurjchem-562	224	27	28	28	NUM
eurjchem-562	224	28	was	be	AUX
eurjchem-562	224	29	then	then	ADV
eurjchem-562	224	30	obtained	obtain	VERB
eurjchem-562	224	31	which	which	PRON
eurjchem-562	224	32	clearly	clearly	ADV
eurjchem-562	224	33	showed	show	VERB
eurjchem-562	224	34	the	the	DET
eurjchem-562	224	35	attachment	attachment	NOUN
eurjchem-562	224	36	of	of	ADP
eurjchem-562	224	37	malononitrile	malononitrile	PROPN
eurjchem-562	224	38	group	group	NOUN
eurjchem-562	224	39	to	to	ADP
eurjchem-562	224	40	the	the	DET
eurjchem-562	224	41	c‐2	c‐2	NOUN
eurjchem-562	224	42	via	via	ADP
eurjchem-562	224	43	double	double	ADJ
eurjchem-562	224	44	bond	bond	NOUN
eurjchem-562	224	45	,	,	PUNCT
eurjchem-562	224	46	cyano	cyano	NOUN
eurjchem-562	224	47	group	group	NOUN
eurjchem-562	224	48	at	at	ADP
eurjchem-562	224	49	c‐3	c‐3	ADJ
eurjchem-562	224	50	position	position	NOUN
eurjchem-562	224	51	,	,	PUNCT
eurjchem-562	224	52	phenyl	phenyl	NOUN
eurjchem-562	224	53	ring	ring	NOUN
eurjchem-562	224	54	at	at	ADP
eurjchem-562	224	55	c‐4	c‐4	PROPN
eurjchem-562	224	56	position	position	NOUN
eurjchem-562	224	57	and	and	CCONJ
eurjchem-562	224	58	quaternary	quaternary	ADJ
eurjchem-562	224	59	center	center	NOUN
eurjchem-562	224	60	at	at	ADP
eurjchem-562	224	61	c‐6	c‐6	NOUN
eurjchem-562	224	62	position	position	NOUN
eurjchem-562	225	1	[	[	X
eurjchem-562	225	2	8	8	NUM
eurjchem-562	225	3	]	]	PUNCT
eurjchem-562	225	4	(	(	PUNCT
eurjchem-562	225	5	figure	figure	NOUN
eurjchem-562	225	6	2	2	NUM
eurjchem-562	225	7	)	)	PUNCT
eurjchem-562	225	8	.	.	PUNCT
eurjchem-562	226	1	the	the	DET
eurjchem-562	226	2	x‐ray	x‐ray	PROPN
eurjchem-562	226	3	crystallographic	crystallographic	ADJ
eurjchem-562	226	4	structure	structure	NOUN
eurjchem-562	226	5	of	of	ADP
eurjchem-562	226	6	the	the	DET
eurjchem-562	226	7	4‐flouro	4‐flouro	PROPN
eurjchem-562	226	8	30	30	NUM
eurjchem-562	226	9	derivative	derivative	NOUN
eurjchem-562	226	10	was	be	AUX
eurjchem-562	226	11	also	also	ADV
eurjchem-562	226	12	obtained	obtain	VERB
eurjchem-562	226	13	for	for	ADP
eurjchem-562	226	14	further	further	ADJ
eurjchem-562	226	15	verification	verification	NOUN
eurjchem-562	226	16	(	(	PUNCT
eurjchem-562	226	17	figure	figure	NOUN
eurjchem-562	226	18	2	2	NUM
eurjchem-562	226	19	)	)	PUNCT
eurjchem-562	226	20	.	.	PUNCT
eurjchem-562	227	1	all	all	DET
eurjchem-562	227	2	the	the	DET
eurjchem-562	227	3	spectroscopic	spectroscopic	ADJ
eurjchem-562	227	4	data	datum	NOUN
eurjchem-562	227	5	includes	include	VERB
eurjchem-562	227	6	1h	1h	NUM
eurjchem-562	227	7	nmr	nmr	NOUN
eurjchem-562	227	8	,	,	PUNCT
eurjchem-562	227	9	13c	13c	NOUN
eurjchem-562	227	10	nmr	nmr	NOUN
eurjchem-562	227	11	,	,	PUNCT
eurjchem-562	227	12	ir	ir	PROPN
eurjchem-562	227	13	and	and	CCONJ
eurjchem-562	227	14	mass	mass	PROPN
eurjchem-562	227	15	spectra	spectra	PROPN
eurjchem-562	227	16	showed	show	VERB
eurjchem-562	227	17	complete	complete	ADJ
eurjchem-562	227	18	agreement	agreement	NOUN
eurjchem-562	227	19	with	with	ADP
eurjchem-562	227	20	the	the	DET
eurjchem-562	227	21	structure	structure	NOUN
eurjchem-562	227	22	28	28	NUM
eurjchem-562	227	23	.	.	PUNCT
eurjchem-562	228	1	after	after	ADP
eurjchem-562	228	2	the	the	DET
eurjchem-562	228	3	confirmation	confirmation	NOUN
eurjchem-562	228	4	of	of	ADP
eurjchem-562	228	5	dimer	dimer	ADJ
eurjchem-562	228	6	structure	structure	NOUN
eurjchem-562	228	7	30	30	NUM
eurjchem-562	228	8	,	,	PUNCT
eurjchem-562	228	9	the	the	DET
eurjchem-562	228	10	reaction	reaction	NOUN
eurjchem-562	228	11	condition	condition	NOUN
eurjchem-562	228	12	was	be	AUX
eurjchem-562	228	13	optimized	optimize	VERB
eurjchem-562	228	14	to	to	PART
eurjchem-562	228	15	increase	increase	VERB
eurjchem-562	228	16	the	the	DET
eurjchem-562	228	17	yield	yield	NOUN
eurjchem-562	228	18	of	of	ADP
eurjchem-562	228	19	the	the	DET
eurjchem-562	228	20	reaction	reaction	NOUN
eurjchem-562	228	21	product	product	NOUN
eurjchem-562	228	22	.	.	PUNCT
eurjchem-562	229	1	initially	initially	ADV
eurjchem-562	229	2	,	,	PUNCT
eurjchem-562	229	3	the	the	DET
eurjchem-562	229	4	temperature	temperature	NOUN
eurjchem-562	229	5	reaction	reaction	NOUN
eurjchem-562	229	6	mixture	mixture	NOUN
eurjchem-562	229	7	was	be	AUX
eurjchem-562	229	8	raised	raise	VERB
eurjchem-562	229	9	from	from	ADP
eurjchem-562	229	10	35	35	NUM
eurjchem-562	229	11	to	to	PART
eurjchem-562	229	12	85	85	NUM
eurjchem-562	229	13	oc	oc	NOUN
eurjchem-562	229	14	and	and	CCONJ
eurjchem-562	229	15	proceeded	proceed	VERB
eurjchem-562	229	16	the	the	DET
eurjchem-562	229	17	reaction	reaction	NOUN
eurjchem-562	229	18	for	for	ADP
eurjchem-562	229	19	14	14	NUM
eurjchem-562	229	20	h	h	NOUN
eurjchem-562	229	21	until	until	SCONJ
eurjchem-562	229	22	tlc	tlc	NOUN
eurjchem-562	229	23	analysis	analysis	NOUN
eurjchem-562	229	24	showed	show	VERB
eurjchem-562	229	25	no	no	DET
eurjchem-562	229	26	starting	starting	NOUN
eurjchem-562	229	27	material	material	NOUN
eurjchem-562	229	28	.	.	PUNCT
eurjchem-562	230	1	the	the	DET
eurjchem-562	230	2	reaction	reaction	NOUN
eurjchem-562	230	3	mixture	mixture	NOUN
eurjchem-562	230	4	was	be	AUX
eurjchem-562	230	5	cooled	cool	VERB
eurjchem-562	230	6	and	and	CCONJ
eurjchem-562	230	7	quenched	quench	VERB
eurjchem-562	230	8	with	with	ADP
eurjchem-562	230	9	2.0	2.0	NUM
eurjchem-562	230	10	n	n	PRON
eurjchem-562	230	11	hcl	hcl	PROPN
eurjchem-562	230	12	to	to	PART
eurjchem-562	230	13	get	get	VERB
eurjchem-562	230	14	the	the	DET
eurjchem-562	230	15	compound	compound	NOUN
eurjchem-562	230	16	28	28	NUM
eurjchem-562	230	17	in	in	ADP
eurjchem-562	230	18	excellent	excellent	ADJ
eurjchem-562	230	19	yield	yield	NOUN
eurjchem-562	230	20	(	(	PUNCT
eurjchem-562	230	21	95	95	NUM
eurjchem-562	230	22	%	%	NOUN
eurjchem-562	230	23	)	)	PUNCT
eurjchem-562	230	24	as	as	ADP
eurjchem-562	230	25	a	a	DET
eurjchem-562	230	26	single	single	ADJ
eurjchem-562	230	27	product	product	NOUN
eurjchem-562	230	28	.	.	PUNCT
eurjchem-562	231	1	the	the	DET
eurjchem-562	231	2	isolated	isolated	ADJ
eurjchem-562	231	3	product	product	NOUN
eurjchem-562	231	4	28	28	NUM
eurjchem-562	231	5	was	be	AUX
eurjchem-562	231	6	found	find	VERB
eurjchem-562	231	7	to	to	PART
eurjchem-562	231	8	be	be	AUX
eurjchem-562	231	9	analytically	analytically	ADV
eurjchem-562	231	10	pure	pure	ADJ
eurjchem-562	231	11	>	>	ADP
eurjchem-562	231	12	95	95	NUM
eurjchem-562	231	13	%	%	NOUN
eurjchem-562	231	14	by	by	ADP
eurjchem-562	231	15	1h	1h	NUM
eurjchem-562	231	16	nmr	nmr	NOUN
eurjchem-562	231	17	spectroscopy	spectroscopy	NOUN
eurjchem-562	231	18	without	without	ADP
eurjchem-562	231	19	tedious	tedious	ADJ
eurjchem-562	231	20	silica	silica	NOUN
eurjchem-562	231	21	gel	gel	NOUN
eurjchem-562	231	22	column	column	NOUN
eurjchem-562	231	23	chromatography	chromatography	NOUN
eurjchem-562	231	24	.	.	PUNCT
eurjchem-562	232	1	the	the	DET
eurjchem-562	232	2	scope	scope	NOUN
eurjchem-562	232	3	of	of	ADP
eurjchem-562	232	4	the	the	DET
eurjchem-562	232	5	reaction	reaction	NOUN
eurjchem-562	232	6	was	be	AUX
eurjchem-562	232	7	further	far	ADV
eurjchem-562	232	8	explored	explore	VERB
eurjchem-562	232	9	to	to	PART
eurjchem-562	232	10	prepare	prepare	VERB
eurjchem-562	232	11	a	a	DET
eurjchem-562	232	12	range	range	NOUN
eurjchem-562	232	13	of	of	ADP
eurjchem-562	232	14	dihydropyridine	dihydropyridine	NOUN
eurjchem-562	232	15	derivatives	derivative	NOUN
eurjchem-562	232	16	28‐	28‐	NUM
eurjchem-562	232	17	46	46	NUM
eurjchem-562	232	18	in	in	ADP
eurjchem-562	232	19	good	good	ADJ
eurjchem-562	232	20	to	to	ADP
eurjchem-562	232	21	excellent	excellent	ADJ
eurjchem-562	232	22	yield	yield	NOUN
eurjchem-562	232	23	(	(	PUNCT
eurjchem-562	232	24	52	52	NUM
eurjchem-562	232	25	to	to	PART
eurjchem-562	232	26	98	98	NUM
eurjchem-562	232	27	%	%	NOUN
eurjchem-562	232	28	)	)	PUNCT
eurjchem-562	232	29	as	as	SCONJ
eurjchem-562	232	30	shown	show	VERB
eurjchem-562	232	31	in	in	ADP
eurjchem-562	232	32	the	the	DET
eurjchem-562	232	33	table	table	NOUN
eurjchem-562	232	34	1	1	NUM
eurjchem-562	232	35	.	.	PUNCT
eurjchem-562	232	36	hameed	hameed	PROPN
eurjchem-562	232	37	et	et	PROPN
eurjchem-562	232	38	al	al	PROPN
eurjchem-562	232	39	.	.	PUNCT
eurjchem-562	232	40	/	/	SYM
eurjchem-562	232	41	european	european	PROPN
eurjchem-562	232	42	journal	journal	PROPN
eurjchem-562	232	43	of	of	ADP
eurjchem-562	232	44	chemistry	chemistry	NOUN
eurjchem-562	232	45	3	3	NUM
eurjchem-562	232	46	(	(	PUNCT
eurjchem-562	232	47	2	2	NUM
eurjchem-562	232	48	)	)	PUNCT
eurjchem-562	232	49	(	(	PUNCT
eurjchem-562	232	50	2012	2012	NUM
eurjchem-562	232	51	)	)	PUNCT
eurjchem-562	232	52	179‐185	179‐185	NUM
eurjchem-562	232	53	183	183	NUM
eurjchem-562	232	54	table	table	NOUN
eurjchem-562	232	55	1	1	NUM
eurjchem-562	232	56	.	.	PUNCT
eurjchem-562	232	57	synthesis	synthesis	NOUN
eurjchem-562	232	58	of	of	ADP
eurjchem-562	232	59	functionalized	functionalized	ADJ
eurjchem-562	232	60	dicyano	dicyano	NOUN
eurjchem-562	232	61	substituted	substitute	VERB
eurjchem-562	232	62	dihydropyridine	dihydropyridine	NOUN
eurjchem-562	232	63	28‐46	28‐46	NUM
eurjchem-562	232	64	via	via	ADP
eurjchem-562	232	65	tbaf‐mediated	tbaf‐mediate	VERB
eurjchem-562	232	66	dimerization	dimerization	NOUN
eurjchem-562	232	67	.	.	PUNCT
eurjchem-562	233	1	entry	entry	NOUN
eurjchem-562	233	2	alkylidene‐malononitriles	alkylidene‐malononitrile	NOUN
eurjchem-562	233	3	dihydropyridine	dihydropyridine	NOUN
eurjchem-562	233	4	derivatives	derivative	NOUN
eurjchem-562	233	5	dihydropyridine	dihydropyridine	NOUN
eurjchem-562	233	6	derivatives	derivative	NOUN
eurjchem-562	233	7	isolated	isolate	VERB
eurjchem-562	233	8	yield	yield	NOUN
eurjchem-562	233	9	(	(	PUNCT
eurjchem-562	233	10	%	%	NOUN
eurjchem-562	233	11	)	)	PUNCT
eurjchem-562	233	12	1	1	NUM
eurjchem-562	233	13	‐	‐	NOUN
eurjchem-562	233	14	98	98	NUM
eurjchem-562	233	15	2	2	NUM
eurjchem-562	233	16	‐	‐	NOUN
eurjchem-562	233	17	95	95	NUM
eurjchem-562	233	18	3	3	NUM
eurjchem-562	233	19	n	n	NOUN
eurjchem-562	233	20	h	h	NOUN
eurjchem-562	234	1	cn	cn	INTJ
eurjchem-562	235	1	cn	cn	INTJ
eurjchem-562	235	2	cn	cn	INTJ
eurjchem-562	235	3	me	i	PRON
eurjchem-562	236	1	f	f	PROPN
eurjchem-562	236	2	f	f	PROPN
eurjchem-562	236	3	30	30	NUM
eurjchem-562	236	4	‐	‐	ADV
eurjchem-562	236	5	75	75	NUM
eurjchem-562	236	6	4	4	NUM
eurjchem-562	236	7	‐	‐	NOUN
eurjchem-562	236	8	75	75	NUM
eurjchem-562	236	9	5	5	NUM
eurjchem-562	236	10	‐	‐	ADV
eurjchem-562	236	11	90	90	NUM
eurjchem-562	236	12	6	6	NUM
eurjchem-562	236	13	‐	‐	NOUN
eurjchem-562	236	14	no	no	DET
eurjchem-562	236	15	reaction	reaction	NOUN
eurjchem-562	236	16	7	7	NUM
eurjchem-562	236	17	‐	‐	NOUN
eurjchem-562	236	18	90	90	NUM
eurjchem-562	236	19	8	8	NUM
eurjchem-562	236	20	n	n	PRON
eurjchem-562	236	21	h	h	NOUN
eurjchem-562	237	1	cn	cn	INTJ
eurjchem-562	237	2	cn	cn	INTJ
eurjchem-562	237	3	cn	cn	INTJ
eurjchem-562	237	4	me	i	PRON
eurjchem-562	237	5	br	br	INTJ
eurjchem-562	237	6	br	br	PROPN
eurjchem-562	237	7	35	35	NUM
eurjchem-562	237	8	‐	‐	NOUN
eurjchem-562	237	9	90	90	NUM
eurjchem-562	237	10	9	9	NUM
eurjchem-562	237	11	89	89	NUM
eurjchem-562	237	12	(	(	PUNCT
eurjchem-562	237	13	4:1	4:1	NUM
eurjchem-562	237	14	ratio	ratio	NOUN
eurjchem-562	237	15	)	)	PUNCT
eurjchem-562	237	16	184	184	NUM
eurjchem-562	237	17	hameed	hameed	NOUN
eurjchem-562	237	18	et	et	PROPN
eurjchem-562	237	19	al	al	PROPN
eurjchem-562	237	20	.	.	PUNCT
eurjchem-562	237	21	/	/	SYM
eurjchem-562	237	22	european	european	PROPN
eurjchem-562	237	23	journal	journal	PROPN
eurjchem-562	237	24	of	of	ADP
eurjchem-562	237	25	chemistry	chemistry	NOUN
eurjchem-562	237	26	3	3	NUM
eurjchem-562	237	27	(	(	PUNCT
eurjchem-562	237	28	2	2	NUM
eurjchem-562	237	29	)	)	PUNCT
eurjchem-562	237	30	(	(	PUNCT
eurjchem-562	237	31	2012	2012	NUM
eurjchem-562	237	32	)	)	PUNCT
eurjchem-562	237	33	179‐185	179‐185	NUM
eurjchem-562	237	34	table	table	NOUN
eurjchem-562	237	35	1	1	NUM
eurjchem-562	237	36	.	.	PUNCT
eurjchem-562	238	1	(	(	PUNCT
eurjchem-562	238	2	continued	continue	VERB
eurjchem-562	238	3	)	)	PUNCT
eurjchem-562	238	4	.	.	PUNCT
eurjchem-562	239	1	entry	entry	NOUN
eurjchem-562	239	2	alkylidene‐malononitriles	alkylidene‐malononitrile	NOUN
eurjchem-562	239	3	dihydropyridine	dihydropyridine	NOUN
eurjchem-562	239	4	derivatives	derivative	NOUN
eurjchem-562	239	5	dihydropyridine	dihydropyridine	NOUN
eurjchem-562	239	6	derivatives	derivative	NOUN
eurjchem-562	239	7	isolated	isolate	VERB
eurjchem-562	239	8	yield	yield	NOUN
eurjchem-562	239	9	(	(	PUNCT
eurjchem-562	239	10	%	%	NOUN
eurjchem-562	239	11	)	)	PUNCT
eurjchem-562	239	12	10	10	NUM
eurjchem-562	240	1	n	n	NUM
eurjchem-562	240	2	h	h	NOUN
eurjchem-562	241	1	cn	cn	INTJ
eurjchem-562	242	1	cn	cn	INTJ
eurjchem-562	242	2	cn	cn	INTJ
eurjchem-562	242	3	me	i	PRON
eurjchem-562	243	1	oh	oh	INTJ
eurjchem-562	243	2	ho	ho	INTJ
eurjchem-562	243	3	37	37	NUM
eurjchem-562	243	4	‐	‐	NOUN
eurjchem-562	243	5	75	75	NUM
eurjchem-562	243	6	11	11	NUM
eurjchem-562	243	7	‐	‐	NOUN
eurjchem-562	243	8	93	93	NUM
eurjchem-562	243	9	12	12	NUM
eurjchem-562	243	10	‐	‐	NOUN
eurjchem-562	243	11	no	no	DET
eurjchem-562	243	12	reaction	reaction	NOUN
eurjchem-562	243	13	13	13	NUM
eurjchem-562	243	14	n	n	NUM
eurjchem-562	244	1	h	h	NOUN
eurjchem-562	245	1	cn	cn	INTJ
eurjchem-562	246	1	cn	cn	INTJ
eurjchem-562	246	2	cn	cn	PROPN
eurjchem-562	246	3	me	i	PRON
eurjchem-562	246	4	ome	ome	INTJ
eurjchem-562	246	5	meo	meo	PROPN
eurjchem-562	246	6	41	41	NUM
eurjchem-562	246	7	‐	‐	NOUN
eurjchem-562	246	8	95	95	NUM
eurjchem-562	246	9	14	14	NUM
eurjchem-562	246	10	‐	‐	ADV
eurjchem-562	246	11	80	80	NUM
eurjchem-562	246	12	16	16	NUM
eurjchem-562	246	13	n	n	PRON
eurjchem-562	246	14	h	h	NOUN
eurjchem-562	247	1	cn	cn	INTJ
eurjchem-562	247	2	cn	cn	INTJ
eurjchem-562	248	1	cn	cn	PROPN
eurjchem-562	248	2	me	i	PRON
eurjchem-562	248	3	no2	no2	NOUN
eurjchem-562	248	4	o2n	o2n	NOUN
eurjchem-562	249	1	43	43	NUM
eurjchem-562	249	2	52	52	NUM
eurjchem-562	249	3	(	(	PUNCT
eurjchem-562	249	4	2:1	2:1	NUM
eurjchem-562	249	5	ratio	ratio	NOUN
eurjchem-562	249	6	)	)	PUNCT
eurjchem-562	249	7	17	17	NUM
eurjchem-562	249	8	n	n	PRON
eurjchem-562	249	9	h	h	NOUN
eurjchem-562	250	1	cn	cn	INTJ
eurjchem-562	251	1	cn	cn	INTJ
eurjchem-562	251	2	cn	cn	PROPN
eurjchem-562	251	3	me	i	PRON
eurjchem-562	251	4	o2n	o2n	PROPN
eurjchem-562	251	5	o2n	o2n	PROPN
eurjchem-562	251	6	44	44	NUM
eurjchem-562	251	7	80	80	NUM
eurjchem-562	251	8	(	(	PUNCT
eurjchem-562	251	9	4:1	4:1	NUM
eurjchem-562	251	10	ratio	ratio	NOUN
eurjchem-562	251	11	)	)	PUNCT
eurjchem-562	251	12	18	18	NUM
eurjchem-562	251	13	‐	‐	NOUN
eurjchem-562	251	14	no	no	DET
eurjchem-562	251	15	reaction	reaction	NOUN
eurjchem-562	251	16	19	19	NUM
eurjchem-562	251	17	‐	‐	NOUN
eurjchem-562	251	18	65	65	NUM
eurjchem-562	251	19	hameed	hameed	NOUN
eurjchem-562	251	20	et	et	PROPN
eurjchem-562	251	21	al	al	PROPN
eurjchem-562	251	22	.	.	PUNCT
eurjchem-562	251	23	/	/	SYM
eurjchem-562	251	24	european	european	PROPN
eurjchem-562	251	25	journal	journal	PROPN
eurjchem-562	251	26	of	of	ADP
eurjchem-562	251	27	chemistry	chemistry	NOUN
eurjchem-562	251	28	3	3	NUM
eurjchem-562	251	29	(	(	PUNCT
eurjchem-562	251	30	2	2	NUM
eurjchem-562	251	31	)	)	PUNCT
eurjchem-562	251	32	(	(	PUNCT
eurjchem-562	251	33	2012	2012	NUM
eurjchem-562	251	34	)	)	PUNCT
eurjchem-562	251	35	179‐185	179‐185	NUM
eurjchem-562	252	1	185	185	NUM
eurjchem-562	252	2	ar	ar	NOUN
eurjchem-562	253	1	h3c	h3c	PROPN
eurjchem-562	254	1	cn	cn	PROPN
eurjchem-562	254	2	cn	cn	PROPN
eurjchem-562	254	3	ar	ar	PROPN
eurjchem-562	254	4	h2c	h2c	PROPN
eurjchem-562	254	5	c	c	PROPN
eurjchem-562	254	6	cn	cn	PROPN
eurjchem-562	254	7	ar	ar	PROPN
eurjchem-562	255	1	h2c	h2c	PROPN
eurjchem-562	255	2	c	c	PROPN
eurjchem-562	255	3	cn	cn	PROPN
eurjchem-562	255	4	ar	ar	PROPN
eurjchem-562	255	5	ch3	ch3	PROPN
eurjchem-562	255	6	cn	cn	PROPN
eurjchem-562	255	7	nc	nc	PROPN
eurjchem-562	255	8	n	n	PROPN
eurjchem-562	255	9	h	h	NOUN
eurjchem-562	256	1	cn	cn	PROPN
eurjchem-562	256	2	cn	cn	PROPN
eurjchem-562	256	3	cn	cn	PROPN
eurjchem-562	256	4	ar	ar	PROPN
eurjchem-562	256	5	ar	ar	PROPN
eurjchem-562	256	6	me	i	PRON
eurjchem-562	256	7	h2c	h2c	X
eurjchem-562	256	8	c	c	PROPN
eurjchem-562	256	9	cn	cn	PROPN
eurjchem-562	256	10	ar	ar	PROPN
eurjchem-562	256	11	n	n	PROPN
eurjchem-562	256	12	tbaf	tbaf	ADJ
eurjchem-562	256	13	(	(	PUNCT
eurjchem-562	256	14	base	base	NOUN
eurjchem-562	256	15	)	)	PUNCT
eurjchem-562	256	16	-h+	-h+	NOUN
eurjchem-562	256	17	nn	nn	PROPN
eurjchem-562	256	18	ar	ar	PROPN
eurjchem-562	256	19	ch3	ch3	PROPN
eurjchem-562	256	20	cn	cn	PROPN
eurjchem-562	256	21	nc	nc	PROPN
eurjchem-562	256	22	me	me	PROPN
eurjchem-562	256	23	ar	ar	PROPN
eurjchem-562	256	24	h2c	h2c	PROPN
eurjchem-562	256	25	c	c	PROPN
eurjchem-562	256	26	cn	cn	PROPN
eurjchem-562	256	27	ar	ar	PROPN
eurjchem-562	256	28	n	n	PROPN
eurjchem-562	256	29	nc	nc	PROPN
eurjchem-562	256	30	cn	cn	PROPN
eurjchem-562	256	31	4	4	NUM
eurjchem-562	256	32	50	50	NUM
eurjchem-562	256	33	51	51	NUM
eurjchem-562	256	34	4	4	NUM
eurjchem-562	256	35	8	8	NUM
eurjchem-562	256	36	53	53	NUM
eurjchem-562	256	37	52	52	NUM
eurjchem-562	256	38	scheme	scheme	NOUN
eurjchem-562	256	39	2	2	NUM
eurjchem-562	256	40	the	the	DET
eurjchem-562	256	41	results	result	NOUN
eurjchem-562	256	42	presented	present	VERB
eurjchem-562	256	43	in	in	ADP
eurjchem-562	256	44	the	the	DET
eurjchem-562	256	45	table	table	NOUN
eurjchem-562	256	46	1	1	NUM
eurjchem-562	256	47	showed	show	VERB
eurjchem-562	256	48	that	that	SCONJ
eurjchem-562	256	49	in	in	ADP
eurjchem-562	256	50	almost	almost	ADV
eurjchem-562	256	51	all	all	PRON
eurjchem-562	256	52	cases	case	NOUN
eurjchem-562	256	53	we	we	PRON
eurjchem-562	256	54	have	have	AUX
eurjchem-562	256	55	only	only	ADV
eurjchem-562	256	56	obtained	obtain	VERB
eurjchem-562	256	57	dicyano	dicyano	ADV
eurjchem-562	256	58	substituted	substitute	VERB
eurjchem-562	256	59	dihydropyridine	dihydropyridine	NOUN
eurjchem-562	256	60	derivatives	derivative	NOUN
eurjchem-562	256	61	28‐46	28‐46	NUM
eurjchem-562	256	62	as	as	ADP
eurjchem-562	256	63	single	single	ADJ
eurjchem-562	256	64	product	product	NOUN
eurjchem-562	256	65	in	in	ADP
eurjchem-562	256	66	high	high	ADJ
eurjchem-562	256	67	yields	yield	NOUN
eurjchem-562	256	68	.	.	PUNCT
eurjchem-562	257	1	however	however	ADV
eurjchem-562	257	2	,	,	PUNCT
eurjchem-562	257	3	in	in	ADP
eurjchem-562	257	4	the	the	DET
eurjchem-562	257	5	case	case	NOUN
eurjchem-562	257	6	of	of	ADP
eurjchem-562	257	7	4‐iodo	4‐iodo	PROPN
eurjchem-562	257	8	18	18	NUM
eurjchem-562	257	9	,	,	PUNCT
eurjchem-562	257	10	4‐nitro	4‐nitro	NUM
eurjchem-562	257	11	24	24	NUM
eurjchem-562	257	12	and	and	CCONJ
eurjchem-562	257	13	3‐nitro	3‐nitro	NUM
eurjchem-562	257	14	25	25	NUM
eurjchem-562	257	15	derivatives	derivative	NOUN
eurjchem-562	257	16	,	,	PUNCT
eurjchem-562	257	17	an	an	DET
eurjchem-562	257	18	inseparable	inseparable	ADJ
eurjchem-562	257	19	mixture	mixture	NOUN
eurjchem-562	257	20	of	of	ADP
eurjchem-562	257	21	corresponding	correspond	VERB
eurjchem-562	257	22	dihydropyridines	dihydropyridine	NOUN
eurjchem-562	257	23	and	and	CCONJ
eurjchem-562	257	24	their	their	PRON
eurjchem-562	257	25	other	other	ADJ
eurjchem-562	257	26	derivatives	derivative	NOUN
eurjchem-562	257	27	were	be	AUX
eurjchem-562	257	28	obtained	obtain	VERB
eurjchem-562	257	29	in	in	ADP
eurjchem-562	257	30	4/1	4/1	NUM
eurjchem-562	257	31	to	to	ADP
eurjchem-562	257	32	2/1	2/1	NUM
eurjchem-562	257	33	ratio	ratio	NOUN
eurjchem-562	257	34	,	,	PUNCT
eurjchem-562	257	35	as	as	SCONJ
eurjchem-562	257	36	judged	judge	VERB
eurjchem-562	257	37	by	by	ADP
eurjchem-562	257	38	1h	1h	NUM
eurjchem-562	257	39	nmr	nmr	NOUN
eurjchem-562	257	40	spectroscopy	spectroscopy	NOUN
eurjchem-562	257	41	(	(	PUNCT
eurjchem-562	257	42	table	table	NOUN
eurjchem-562	257	43	1	1	NUM
eurjchem-562	257	44	)	)	PUNCT
eurjchem-562	257	45	.	.	PUNCT
eurjchem-562	258	1	the	the	DET
eurjchem-562	258	2	dimerization	dimerization	NOUN
eurjchem-562	258	3	of	of	ADP
eurjchem-562	258	4	2‐chloro	2‐chloro	NUM
eurjchem-562	258	5	15	15	NUM
eurjchem-562	258	6	ylidene	ylidene	NOUN
eurjchem-562	258	7	,	,	PUNCT
eurjchem-562	258	8	2‐hydroxy	2‐hydroxy	NUM
eurjchem-562	258	9	ylidene	ylidene	NOUN
eurjchem-562	258	10	21	21	NUM
eurjchem-562	258	11	and	and	CCONJ
eurjchem-562	258	12	2‐nitro	2‐nitro	NUM
eurjchem-562	258	13	ylidene	ylidene	NOUN
eurjchem-562	258	14	26	26	NUM
eurjchem-562	258	15	was	be	AUX
eurjchem-562	258	16	unsuccessful	unsuccessful	ADJ
eurjchem-562	258	17	which	which	PRON
eurjchem-562	258	18	could	could	AUX
eurjchem-562	258	19	be	be	AUX
eurjchem-562	258	20	possibly	possibly	ADV
eurjchem-562	258	21	due	due	ADJ
eurjchem-562	258	22	to	to	ADP
eurjchem-562	258	23	the	the	DET
eurjchem-562	258	24	steric	steric	ADJ
eurjchem-562	258	25	interaction	interaction	NOUN
eurjchem-562	258	26	of	of	ADP
eurjchem-562	258	27	methylene	methylene	NOUN
eurjchem-562	258	28	group	group	NOUN
eurjchem-562	258	29	,	,	PUNCT
eurjchem-562	258	30	generated	generate	VERB
eurjchem-562	258	31	in	in	ADP
eurjchem-562	258	32	situ	situ	ADJ
eurjchem-562	258	33	deprotonation	deprotonation	NOUN
eurjchem-562	258	34	by	by	ADP
eurjchem-562	258	35	tbaf	tbaf	PROPN
eurjchem-562	258	36	,	,	PUNCT
eurjchem-562	258	37	with	with	SCONJ
eurjchem-562	258	38	the	the	DET
eurjchem-562	258	39	hydroxy	hydroxy	PROPN
eurjchem-562	258	40	and	and	CCONJ
eurjchem-562	258	41	nitro	nitro	NOUN
eurjchem-562	258	42	substituents	substituent	NOUN
eurjchem-562	258	43	present	present	ADJ
eurjchem-562	258	44	at	at	ADP
eurjchem-562	258	45	2‐position	2‐position	NUM
eurjchem-562	258	46	of	of	ADP
eurjchem-562	258	47	the	the	DET
eurjchem-562	258	48	phenyl	phenyl	NOUN
eurjchem-562	258	49	ring	ring	NOUN
eurjchem-562	258	50	.	.	PUNCT
eurjchem-562	259	1	a	a	DET
eurjchem-562	259	2	plausible	plausible	ADJ
eurjchem-562	259	3	mechanism	mechanism	NOUN
eurjchem-562	259	4	of	of	ADP
eurjchem-562	259	5	this	this	DET
eurjchem-562	259	6	dimerization	dimerization	NOUN
eurjchem-562	259	7	has	have	AUX
eurjchem-562	259	8	been	be	AUX
eurjchem-562	259	9	outlined	outline	VERB
eurjchem-562	259	10	in	in	ADP
eurjchem-562	259	11	scheme	scheme	NOUN
eurjchem-562	259	12	2	2	NUM
eurjchem-562	259	13	.	.	PUNCT
eurjchem-562	260	1	the	the	DET
eurjchem-562	260	2	carbanion	carbanion	NOUN
eurjchem-562	260	3	50	50	NUM
eurjchem-562	260	4	,	,	PUNCT
eurjchem-562	260	5	generated	generate	VERB
eurjchem-562	260	6	by	by	ADP
eurjchem-562	260	7	the	the	DET
eurjchem-562	260	8	abstraction	abstraction	NOUN
eurjchem-562	260	9	of	of	ADP
eurjchem-562	260	10	proton	proton	NOUN
eurjchem-562	260	11	from	from	ADP
eurjchem-562	260	12	methyl	methyl	NOUN
eurjchem-562	260	13	group	group	NOUN
eurjchem-562	260	14	by	by	ADP
eurjchem-562	260	15	tbaf	tbaf	PROPN
eurjchem-562	260	16	which	which	PRON
eurjchem-562	260	17	acts	act	VERB
eurjchem-562	260	18	as	as	ADP
eurjchem-562	260	19	base	base	NOUN
eurjchem-562	260	20	,	,	PUNCT
eurjchem-562	260	21	rearrange	rearrange	VERB
eurjchem-562	260	22	itself	itself	PRON
eurjchem-562	260	23	to	to	ADP
eurjchem-562	260	24	keteneimine	keteneimine	PROPN
eurjchem-562	260	25	51	51	NUM
eurjchem-562	260	26	which	which	PRON
eurjchem-562	260	27	then	then	ADV
eurjchem-562	260	28	attacks	attack	VERB
eurjchem-562	260	29	to	to	PART
eurjchem-562	260	30	dicycano	dicycano	VERB
eurjchem-562	260	31	alkene	alkene	VERB
eurjchem-562	260	32	4	4	NUM
eurjchem-562	260	33	of	of	ADP
eurjchem-562	260	34	another	another	DET
eurjchem-562	260	35	molecule	molecule	NOUN
eurjchem-562	260	36	to	to	PART
eurjchem-562	260	37	afford	afford	VERB
eurjchem-562	260	38	intermediate	intermediate	ADJ
eurjchem-562	260	39	52	52	NUM
eurjchem-562	260	40	.	.	PUNCT
eurjchem-562	261	1	the	the	DET
eurjchem-562	261	2	intermediate	intermediate	ADJ
eurjchem-562	261	3	52	52	NUM
eurjchem-562	261	4	then	then	ADV
eurjchem-562	261	5	undergo	undergo	VERB
eurjchem-562	261	6	rearrangement	rearrangement	NOUN
eurjchem-562	261	7	to	to	PART
eurjchem-562	261	8	afford	afford	VERB
eurjchem-562	261	9	compound	compound	NOUN
eurjchem-562	261	10	53	53	NUM
eurjchem-562	261	11	,	,	PUNCT
eurjchem-562	261	12	which	which	PRON
eurjchem-562	261	13	on	on	ADP
eurjchem-562	261	14	cyclization	cyclization	NOUN
eurjchem-562	261	15	give	give	VERB
eurjchem-562	261	16	final	final	ADJ
eurjchem-562	261	17	product	product	NOUN
eurjchem-562	261	18	8	8	NUM
eurjchem-562	261	19	(	(	PUNCT
eurjchem-562	261	20	scheme	scheme	NOUN
eurjchem-562	261	21	2	2	NUM
eurjchem-562	261	22	)	)	PUNCT
eurjchem-562	262	1	[	[	X
eurjchem-562	262	2	7	7	NUM
eurjchem-562	262	3	,	,	PUNCT
eurjchem-562	262	4	8	8	NUM
eurjchem-562	262	5	]	]	PUNCT
eurjchem-562	262	6	.	.	PUNCT
eurjchem-562	263	1	4	4	X
eurjchem-562	263	2	.	.	X
eurjchem-562	263	3	conclusion	conclusion	NOUN
eurjchem-562	263	4	in	in	ADP
eurjchem-562	263	5	summary	summary	NOUN
eurjchem-562	263	6	,	,	PUNCT
eurjchem-562	263	7	we	we	PRON
eurjchem-562	263	8	have	have	AUX
eurjchem-562	263	9	successfully	successfully	ADV
eurjchem-562	263	10	developed	develop	VERB
eurjchem-562	263	11	a	a	DET
eurjchem-562	263	12	new	new	ADJ
eurjchem-562	263	13	broad	broad	ADJ
eurjchem-562	263	14	spectrum	spectrum	NOUN
eurjchem-562	263	15	,	,	PUNCT
eurjchem-562	263	16	eco‐friendly	eco‐friendly	ADV
eurjchem-562	263	17	method	method	NOUN
eurjchem-562	263	18	of	of	ADP
eurjchem-562	263	19	alkylidenemalononitriles	alkylidenemalononitrile	NOUN
eurjchem-562	263	20	10‐	10‐	NUM
eurjchem-562	263	21	27	27	NUM
eurjchem-562	263	22	dimerization	dimerization	NOUN
eurjchem-562	263	23	to	to	PART
eurjchem-562	263	24	form	form	VERB
eurjchem-562	263	25	the	the	DET
eurjchem-562	263	26	dihydropyridine	dihydropyridine	NOUN
eurjchem-562	263	27	derivative	derivative	NOUN
eurjchem-562	263	28	28‐46	28‐46	NUM
eurjchem-562	263	29	under	under	ADP
eurjchem-562	263	30	solvent‐free	solvent‐free	NOUN
eurjchem-562	263	31	conditions	condition	NOUN
eurjchem-562	263	32	.	.	PUNCT
eurjchem-562	264	1	tbaf	tbaf	PROPN
eurjchem-562	264	2	is	be	AUX
eurjchem-562	264	3	found	find	VERB
eurjchem-562	264	4	to	to	PART
eurjchem-562	264	5	be	be	AUX
eurjchem-562	264	6	an	an	DET
eurjchem-562	264	7	efficient	efficient	ADJ
eurjchem-562	264	8	base	base	NOUN
eurjchem-562	264	9	for	for	ADP
eurjchem-562	264	10	promoting	promote	VERB
eurjchem-562	264	11	the	the	DET
eurjchem-562	264	12	reaction	reaction	NOUN
eurjchem-562	264	13	to	to	PART
eurjchem-562	264	14	desire	desire	VERB
eurjchem-562	264	15	products	product	NOUN
eurjchem-562	264	16	.	.	PUNCT
eurjchem-562	265	1	further	further	ADJ
eurjchem-562	265	2	work	work	NOUN
eurjchem-562	265	3	on	on	ADP
eurjchem-562	265	4	other	other	ADJ
eurjchem-562	265	5	kind	kind	NOUN
eurjchem-562	265	6	of	of	ADP
eurjchem-562	265	7	ylidenes	ylidene	NOUN
eurjchem-562	265	8	e.g.	e.g.	ADV
eurjchem-562	265	9	phch(cn)2	phch(cn)2	ADV
eurjchem-562	265	10	,	,	PUNCT
eurjchem-562	265	11	further	further	ADJ
eurjchem-562	265	12	chemical	chemical	NOUN
eurjchem-562	265	13	transformations	transformation	NOUN
eurjchem-562	265	14	on	on	ADP
eurjchem-562	265	15	above	above	ADP
eurjchem-562	265	16	mentioned	mention	VERB
eurjchem-562	265	17	dimers	dimer	NOUN
eurjchem-562	265	18	28‐46	28‐46	NUM
eurjchem-562	265	19	and	and	CCONJ
eurjchem-562	265	20	their	their	PRON
eurjchem-562	265	21	biological	biological	ADJ
eurjchem-562	265	22	properties	property	NOUN
eurjchem-562	265	23	are	be	AUX
eurjchem-562	265	24	under	under	ADP
eurjchem-562	265	25	progress	progress	NOUN
eurjchem-562	265	26	.	.	PUNCT
eurjchem-562	266	1	acknowledgements	acknowledgement	NOUN
eurjchem-562	266	2	we	we	PRON
eurjchem-562	266	3	are	be	AUX
eurjchem-562	266	4	thankful	thankful	ADJ
eurjchem-562	266	5	to	to	ADP
eurjchem-562	266	6	higher	high	ADJ
eurjchem-562	266	7	education	education	NOUN
eurjchem-562	266	8	commission	commission	NOUN
eurjchem-562	266	9	(	(	PUNCT
eurjchem-562	266	10	hec	hec	PROPN
eurjchem-562	266	11	)	)	PUNCT
eurjchem-562	266	12	,	,	PUNCT
eurjchem-562	266	13	pakistan	pakistan	PROPN
eurjchem-562	266	14	and	and	CCONJ
eurjchem-562	266	15	husein	husein	PROPN
eurjchem-562	266	16	ebrahim	ebrahim	PROPN
eurjchem-562	266	17	jamal	jamal	PROPN
eurjchem-562	266	18	research	research	PROPN
eurjchem-562	266	19	institute	institute	PROPN
eurjchem-562	266	20	of	of	ADP
eurjchem-562	266	21	chemistry	chemistry	PROPN
eurjchem-562	266	22	,	,	PUNCT
eurjchem-562	266	23	international	international	ADJ
eurjchem-562	266	24	center	center	NOUN
eurjchem-562	266	25	for	for	ADP
eurjchem-562	266	26	chemical	chemical	NOUN
eurjchem-562	266	27	and	and	CCONJ
eurjchem-562	266	28	biological	biological	ADJ
eurjchem-562	266	29	sciences	science	NOUN
eurjchem-562	266	30	,	,	PUNCT
eurjchem-562	266	31	university	university	PROPN
eurjchem-562	266	32	of	of	ADP
eurjchem-562	266	33	karachi	karachi	PROPN
eurjchem-562	266	34	,	,	PUNCT
eurjchem-562	266	35	karachi‐75270	karachi‐75270	PROPN
eurjchem-562	266	36	,	,	PUNCT
eurjchem-562	266	37	pakistan	pakistan	PROPN
eurjchem-562	266	38	for	for	ADP
eurjchem-562	266	39	providing	provide	VERB
eurjchem-562	266	40	financial	financial	ADJ
eurjchem-562	266	41	support	support	NOUN
eurjchem-562	266	42	.	.	PUNCT
eurjchem-562	267	1	supplementary	supplementary	ADJ
eurjchem-562	267	2	materials	material	NOUN
eurjchem-562	267	3	ccdc‐845736	ccdc‐845736	PROPN
eurjchem-562	267	4	(	(	PUNCT
eurjchem-562	267	5	28	28	NUM
eurjchem-562	267	6	)	)	PUNCT
eurjchem-562	267	7	and	and	CCONJ
eurjchem-562	267	8	845735	845735	NUM
eurjchem-562	267	9	(	(	PUNCT
eurjchem-562	267	10	30	30	NUM
eurjchem-562	267	11	)	)	PUNCT
eurjchem-562	267	12	contains	contain	VERB
eurjchem-562	267	13	the	the	DET
eurjchem-562	267	14	supplementary	supplementary	ADJ
eurjchem-562	267	15	crystallographic	crystallographic	ADJ
eurjchem-562	267	16	data	datum	NOUN
eurjchem-562	267	17	for	for	ADP
eurjchem-562	267	18	this	this	DET
eurjchem-562	267	19	paper	paper	NOUN
eurjchem-562	267	20	.	.	PUNCT
eurjchem-562	268	1	these	these	DET
eurjchem-562	268	2	data	datum	NOUN
eurjchem-562	268	3	can	can	AUX
eurjchem-562	268	4	be	be	AUX
eurjchem-562	268	5	obtained	obtain	VERB
eurjchem-562	268	6	free	free	ADJ
eurjchem-562	268	7	of	of	ADP
eurjchem-562	268	8	charge	charge	NOUN
eurjchem-562	268	9	via	via	ADP
eurjchem-562	268	10	www.ccdc.cam.ac.uk/data_request/cif	www.ccdc.cam.ac.uk/data_request/cif	NOUN
eurjchem-562	268	11	,	,	PUNCT
eurjchem-562	268	12	or	or	CCONJ
eurjchem-562	268	13	by	by	ADP
eurjchem-562	268	14	e‐mailing	e‐maile	VERB
eurjchem-562	268	15	data_request@ccdc.cam.ac.uk	data_request@ccdc.cam.ac.uk	VERB
eurjchem-562	268	16	,	,	PUNCT
eurjchem-562	268	17	or	or	CCONJ
eurjchem-562	268	18	by	by	ADP
eurjchem-562	268	19	contacting	contact	VERB
eurjchem-562	268	20	the	the	DET
eurjchem-562	268	21	cambridge	cambridge	PROPN
eurjchem-562	268	22	crystallographic	crystallographic	PROPN
eurjchem-562	268	23	data	data	PROPN
eurjchem-562	268	24	centre	centre	NOUN
eurjchem-562	268	25	,	,	PUNCT
eurjchem-562	268	26	12	12	NUM
eurjchem-562	268	27	union	union	NOUN
eurjchem-562	268	28	road	road	NOUN
eurjchem-562	268	29	,	,	PUNCT
eurjchem-562	268	30	cambridge	cambridge	PROPN
eurjchem-562	268	31	cb2	cb2	PROPN
eurjchem-562	268	32	1ez	1ez	PROPN
eurjchem-562	268	33	,	,	PUNCT
eurjchem-562	268	34	uk	uk	PROPN
eurjchem-562	268	35	;	;	PUNCT
eurjchem-562	268	36	fax	fax	NOUN
eurjchem-562	268	37	:	:	PUNCT
eurjchem-562	268	38	+44(0)1223‐336033	+44(0)1223‐336033	ADJ
eurjchem-562	268	39	.	.	PUNCT
eurjchem-562	268	40	references	reference	NOUN
eurjchem-562	268	41	[	[	X
eurjchem-562	268	42	1	1	NUM
eurjchem-562	268	43	]	]	PUNCT
eurjchem-562	268	44	.	.	PUNCT
eurjchem-562	269	1	knoevenagel	knoevenagel	PROPN
eurjchem-562	269	2	,	,	PUNCT
eurjchem-562	269	3	k.	k.	PROPN
eurjchem-562	269	4	ber	ber	PROPN
eurjchem-562	269	5	.	.	PUNCT
eurjchem-562	270	1	dtsch	dtsch	PROPN
eurjchem-562	270	2	.	.	PUNCT
eurjchem-562	271	1	chem	chem	NOUN
eurjchem-562	271	2	.	.	PUNCT
eurjchem-562	272	1	ges	ges	PROPN
eurjchem-562	272	2	.	.	PROPN
eurjchem-562	272	3	1988	1988	NUM
eurjchem-562	272	4	,	,	PUNCT
eurjchem-562	272	5	31	31	NUM
eurjchem-562	272	6	,	,	PUNCT
eurjchem-562	272	7	2596‐2619	2596‐2619	NUM
eurjchem-562	272	8	.	.	PUNCT
eurjchem-562	273	1	[	[	X
eurjchem-562	273	2	2	2	NUM
eurjchem-562	273	3	]	]	PUNCT
eurjchem-562	273	4	.	.	PUNCT
eurjchem-562	274	1	barnes	barnes	PROPN
eurjchem-562	274	2	,	,	PUNCT
eurjchem-562	274	3	d.	d.	PROPN
eurjchem-562	274	4	m.	m.	PROPN
eurjchem-562	274	5	;	;	PUNCT
eurjchem-562	274	6	haight	haight	PROPN
eurjchem-562	274	7	,	,	PUNCT
eurjchem-562	274	8	a.	a.	PROPN
eurjchem-562	274	9	r.	r.	PROPN
eurjchem-562	274	10	;	;	PUNCT
eurjchem-562	274	11	hameury	hameury	NOUN
eurjchem-562	274	12	,	,	PUNCT
eurjchem-562	274	13	t.	t.	PROPN
eurjchem-562	274	14	;	;	PUNCT
eurjchem-562	274	15	mclaughlin	mclaughlin	PROPN
eurjchem-562	274	16	,	,	PUNCT
eurjchem-562	274	17	m.	m.	NOUN
eurjchem-562	274	18	a.	a.	PROPN
eurjchem-562	274	19	;	;	PUNCT
eurjchem-562	274	20	mei	mei	PROPN
eurjchem-562	274	21	,	,	PUNCT
eurjchem-562	274	22	j.	j.	PROPN
eurjchem-562	274	23	;	;	PUNCT
eurjchem-562	274	24	tedrow	tedrow	PROPN
eurjchem-562	274	25	,	,	PUNCT
eurjchem-562	274	26	j.	j.	PROPN
eurjchem-562	274	27	s.	s.	PROPN
eurjchem-562	274	28	;	;	PUNCT
eurjchem-562	274	29	toma	toma	PROPN
eurjchem-562	274	30	,	,	PUNCT
eurjchem-562	274	31	j.	j.	PROPN
eurjchem-562	274	32	,	,	PUNCT
eurjchem-562	274	33	d.	d.	PROPN
eurjchem-562	274	34	r.	r.	PROPN
eurjchem-562	274	35	tetrahedron	tetrahedron	PROPN
eurjchem-562	274	36	2006	2006	NUM
eurjchem-562	274	37	,	,	PUNCT
eurjchem-562	274	38	62	62	NUM
eurjchem-562	274	39	,	,	PUNCT
eurjchem-562	274	40	11311‐11319	11311‐11319	NUM
eurjchem-562	274	41	.	.	PUNCT
eurjchem-562	275	1	[	[	X
eurjchem-562	275	2	3	3	NUM
eurjchem-562	275	3	]	]	PUNCT
eurjchem-562	275	4	.	.	PUNCT
eurjchem-562	276	1	sharif	sharif	PROPN
eurjchem-562	276	2	,	,	PUNCT
eurjchem-562	276	3	a.	a.	NOUN
eurjchem-562	276	4	;	;	PUNCT
eurjchem-562	276	5	ahmad	ahmad	PROPN
eurjchem-562	276	6	,	,	PUNCT
eurjchem-562	276	7	e.	e.	PROPN
eurjchem-562	276	8	;	;	PUNCT
eurjchem-562	276	9	munawar	munawar	PROPN
eurjchem-562	276	10	,	,	PUNCT
eurjchem-562	276	11	m.	m.	NOUN
eurjchem-562	276	12	a.	a.	NOUN
eurjchem-562	276	13	;	;	PUNCT
eurjchem-562	276	14	jabeen	jabeen	PROPN
eurjchem-562	276	15	,	,	PUNCT
eurjchem-562	276	16	s.	s.	PROPN
eurjchem-562	276	17	;	;	PUNCT
eurjchem-562	276	18	khan	khan	PROPN
eurjchem-562	276	19	,	,	PUNCT
eurjchem-562	276	20	m.	m.	PROPN
eurjchem-562	276	21	u.	u.	PROPN
eurjchem-562	276	22	a.	a.	PROPN
eurjchem-562	276	23	;	;	PUNCT
eurjchem-562	276	24	begum	begum	PROPN
eurjchem-562	276	25	,	,	PUNCT
eurjchem-562	276	26	r.	r.	PROPN
eurjchem-562	276	27	;	;	PUNCT
eurjchem-562	276	28	farrukh	farrukh	PROPN
eurjchem-562	276	29	,	,	PUNCT
eurjchem-562	276	30	a.	a.	NOUN
eurjchem-562	276	31	;	;	PUNCT
eurjchem-562	276	32	ashraf	ashraf	NOUN
eurjchem-562	276	33	,	,	PUNCT
eurjchem-562	276	34	m.	m.	NOUN
eurjchem-562	276	35	;	;	PUNCT
eurjchem-562	276	36	arshad	arshad	PROPN
eurjchem-562	276	37	,	,	PUNCT
eurjchem-562	276	38	s.	s.	PROPN
eurjchem-562	276	39	;	;	PUNCT
eurjchem-562	276	40	afza	afza	PROPN
eurjchem-562	276	41	,	,	PUNCT
eurjchem-562	276	42	n.	n.	PROPN
eurjchem-562	276	43	j.	j.	PROPN
eurjchem-562	276	44	chem	chem	PROPN
eurjchem-562	276	45	.	.	PUNCT
eurjchem-562	277	1	soc	soc	PROPN
eurjchem-562	277	2	.	.	PUNCT
eurjchem-562	278	1	pak	pak	PROPN
eurjchem-562	278	2	.	.	PROPN
eurjchem-562	279	1	2011	2011	NUM
eurjchem-562	279	2	,	,	PUNCT
eurjchem-562	279	3	33	33	NUM
eurjchem-562	279	4	,	,	PUNCT
eurjchem-562	279	5	578‐786	578‐786	NUM
eurjchem-562	279	6	.	.	PUNCT
eurjchem-562	280	1	[	[	X
eurjchem-562	280	2	4	4	NUM
eurjchem-562	280	3	]	]	PUNCT
eurjchem-562	280	4	.	.	PUNCT
eurjchem-562	280	5	bogdanowicz‐szwed	bogdanowicz‐szwe	VERB
eurjchem-562	280	6	,	,	PUNCT
eurjchem-562	280	7	k.	k.	PROPN
eurjchem-562	280	8	;	;	PUNCT
eurjchem-562	280	9	krasodomska	krasodomska	PROPN
eurjchem-562	280	10	,	,	PUNCT
eurjchem-562	280	11	m.	m.	NOUN
eurjchem-562	280	12	monatsh	monatsh	PROPN
eurjchem-562	280	13	.	.	PUNCT
eurjchem-562	281	1	chem	chem	PROPN
eurjchem-562	281	2	.	.	PUNCT
eurjchem-562	282	1	2006	2006	NUM
eurjchem-562	282	2	,	,	PUNCT
eurjchem-562	282	3	137	137	NUM
eurjchem-562	282	4	,	,	PUNCT
eurjchem-562	282	5	347‐355	347‐355	NUM
eurjchem-562	282	6	.	.	PUNCT
eurjchem-562	283	1	[	[	X
eurjchem-562	283	2	5	5	NUM
eurjchem-562	283	3	]	]	PUNCT
eurjchem-562	283	4	.	.	PUNCT
eurjchem-562	284	1	johnson	johnson	PROPN
eurjchem-562	284	2	,	,	PUNCT
eurjchem-562	284	3	d.	d.	PROPN
eurjchem-562	284	4	s.	s.	PROPN
eurjchem-562	284	5	;	;	PUNCT
eurjchem-562	284	6	li	li	PROPN
eurjchem-562	284	7	,	,	PUNCT
eurjchem-562	284	8	j.	j.	PROPN
eurjchem-562	284	9	j.	j.	PROPN
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eurjchem-562	284	11	art	art	NOUN
eurjchem-562	284	12	of	of	ADP
eurjchem-562	284	13	drug	drug	NOUN
eurjchem-562	284	14	synthesis	synthesis	NOUN
eurjchem-562	284	15	,	,	PUNCT
eurjchem-562	284	16	john	john	PROPN
eurjchem-562	284	17	wiley	wiley	PROPN
eurjchem-562	284	18	and	and	CCONJ
eurjchem-562	284	19	sons	son	NOUN
eurjchem-562	284	20	,	,	PUNCT
eurjchem-562	284	21	inc	inc	PROPN
eurjchem-562	284	22	.	.	PROPN
eurjchem-562	284	23	:	:	PUNCT
eurjchem-562	285	1	new	new	PROPN
eurjchem-562	285	2	jersey	jersey	PROPN
eurjchem-562	285	3	,	,	PUNCT
eurjchem-562	285	4	2007	2007	NUM
eurjchem-562	285	5	.	.	PUNCT
eurjchem-562	286	1	[	[	X
eurjchem-562	286	2	6	6	NUM
eurjchem-562	286	3	]	]	PUNCT
eurjchem-562	286	4	.	.	PUNCT
eurjchem-562	287	1	lichitsky	lichitsky	PROPN
eurjchem-562	287	2	,	,	PUNCT
eurjchem-562	287	3	b.	b.	PROPN
eurjchem-562	287	4	v.	v.	PROPN
eurjchem-562	287	5	;	;	PUNCT
eurjchem-562	287	6	dudinov	dudinov	PROPN
eurjchem-562	287	7	,	,	PUNCT
eurjchem-562	287	8	a.	a.	NOUN
eurjchem-562	287	9	a.	a.	NOUN
eurjchem-562	287	10	;	;	PUNCT
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eurjchem-562	287	12	,	,	PUNCT
eurjchem-562	287	13	m.	m.	NOUN
eurjchem-562	287	14	m.	m.	NOUN
eurjchem-562	287	15	arkivoc	arkivoc	PROPN
eurjchem-562	287	16	2001	2001	NUM
eurjchem-562	287	17	,	,	PUNCT
eurjchem-562	287	18	9	9	NUM
eurjchem-562	287	19	,	,	PUNCT
eurjchem-562	287	20	73‐	73‐	NUM
eurjchem-562	287	21	79	79	NUM
eurjchem-562	287	22	.	.	PUNCT
eurjchem-562	288	1	[	[	X
eurjchem-562	288	2	7	7	NUM
eurjchem-562	288	3	]	]	PUNCT
eurjchem-562	288	4	.	.	PUNCT
eurjchem-562	288	5	dunkel	dunkel	NOUN
eurjchem-562	288	6	,	,	PUNCT
eurjchem-562	288	7	s.	s.	PROPN
eurjchem-562	288	8	;	;	PUNCT
eurjchem-562	288	9	heb	heb	NOUN
eurjchem-562	288	10	,	,	PUNCT
eurjchem-562	288	11	u.	u.	PROPN
eurjchem-562	288	12	j.	j.	PROPN
eurjchem-562	288	13	prakt	prakt	PROPN
eurjchem-562	288	14	.	.	PUNCT
eurjchem-562	289	1	chem	chem	NOUN
eurjchem-562	289	2	.	.	PUNCT
eurjchem-562	290	1	1997	1997	NUM
eurjchem-562	290	2	,	,	PUNCT
eurjchem-562	290	3	339	339	NUM
eurjchem-562	290	4	,	,	PUNCT
eurjchem-562	290	5	414‐419	414‐419	NUM
eurjchem-562	290	6	.	.	PUNCT
eurjchem-562	291	1	[	[	X
eurjchem-562	291	2	8	8	NUM
eurjchem-562	291	3	]	]	SYM
eurjchem-562	291	4	.	.	PUNCT
eurjchem-562	291	5	abdelrazek	abdelrazek	PROPN
eurjchem-562	291	6	,	,	PUNCT
eurjchem-562	291	7	f.	f.	PROPN
eurjchem-562	291	8	m.	m.	PROPN
eurjchem-562	291	9	;	;	PUNCT
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eurjchem-562	291	11	,	,	PUNCT
eurjchem-562	291	12	m.	m.	PROPN
eurjchem-562	291	13	h.	h.	PROPN
eurjchem-562	291	14	;	;	PUNCT
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eurjchem-562	291	16	,	,	PUNCT
eurjchem-562	291	17	n.	n.	PROPN
eurjchem-562	291	18	a.	a.	PROPN
eurjchem-562	291	19	;	;	PUNCT
eurjchem-562	291	20	sobhy	sobhy	PROPN
eurjchem-562	291	21	,	,	PUNCT
eurjchem-562	291	22	n.	n.	PROPN
eurjchem-562	291	23	a.	a.	PROPN
eurjchem-562	291	24	;	;	PUNCT
eurjchem-562	292	1	metz	metz	PROPN
eurjchem-562	292	2	,	,	PUNCT
eurjchem-562	292	3	p.	p.	NOUN
eurjchem-562	292	4	;	;	PUNCT
eurjchem-562	292	5	jaeger	jaeger	NOUN
eurjchem-562	292	6	,	,	PUNCT
eurjchem-562	292	7	a.	a.	PROPN
eurjchem-562	292	8	j.	j.	PROPN
eurjchem-562	292	9	heterocyclic	heterocyclic	PROPN
eurjchem-562	292	10	chem	chem	PROPN
eurjchem-562	292	11	.	.	PUNCT
eurjchem-562	293	1	2010	2010	NUM
eurjchem-562	293	2	,	,	PUNCT
eurjchem-562	293	3	47	47	NUM
eurjchem-562	293	4	,	,	PUNCT
eurjchem-562	293	5	348‐388	348‐388	NUM
eurjchem-562	293	6	.	.	PUNCT
eurjchem-562	294	1	[	[	X
eurjchem-562	294	2	9	9	NUM
eurjchem-562	294	3	]	]	PUNCT
eurjchem-562	294	4	.	.	PUNCT
eurjchem-562	295	1	corey	corey	PROPN
eurjchem-562	295	2	,	,	PUNCT
eurjchem-562	295	3	e.	e.	PROPN
eurjchem-562	295	4	j.	j.	PROPN
eurjchem-562	295	5	;	;	PUNCT
eurjchem-562	295	6	snider	snider	PROPN
eurjchem-562	295	7	,	,	PUNCT
eurjchem-562	295	8	b.	b.	PROPN
eurjchem-562	295	9	b.	b.	PROPN
eurjchem-562	295	10	j.	j.	PROPN
eurjchem-562	295	11	am	am	PROPN
eurjchem-562	295	12	.	.	PUNCT
eurjchem-562	296	1	chem	chem	PROPN
eurjchem-562	296	2	.	.	PUNCT
eurjchem-562	297	1	soc	soc	PROPN
eurjchem-562	297	2	.	.	PUNCT
eurjchem-562	298	1	1972	1972	NUM
eurjchem-562	298	2	,	,	PUNCT
eurjchem-562	298	3	94	94	NUM
eurjchem-562	298	4	,	,	PUNCT
eurjchem-562	298	5	6190‐6192	6190‐6192	NUM
eurjchem-562	299	1	[	[	X
eurjchem-562	299	2	10	10	NUM
eurjchem-562	299	3	]	]	PUNCT
eurjchem-562	299	4	.	.	PUNCT
eurjchem-562	300	1	cox	cox	PROPN
eurjchem-562	300	2	,	,	PUNCT
eurjchem-562	300	3	d.	d.	PROPN
eurjchem-562	300	4	p.	p.	PROPN
eurjchem-562	300	5	;	;	PUNCT
eurjchem-562	300	6	terpinski	terpinski	PROPN
eurjchem-562	300	7	,	,	PUNCT
eurjchem-562	300	8	j.	j.	PROPN
eurjchem-562	300	9	;	;	PUNCT
eurjchem-562	300	10	lawrynowicz	lawrynowicz	PROPN
eurjchem-562	300	11	,	,	PUNCT
eurjchem-562	300	12	w.	w.	PROPN
eurjchem-562	300	13	j.	j.	PROPN
eurjchem-562	300	14	org	org	PROPN
eurjchem-562	300	15	.	.	PUNCT
eurjchem-562	300	16	chem	chem	PROPN
eurjchem-562	300	17	.	.	PUNCT
eurjchem-562	300	18	1984	1984	NUM
eurjchem-562	300	19	,	,	PUNCT
eurjchem-562	300	20	49	49	NUM
eurjchem-562	300	21	,	,	PUNCT
eurjchem-562	300	22	3216‐	3216‐	NUM
eurjchem-562	300	23	3219	3219	NUM
eurjchem-562	300	24	.	.	PUNCT
eurjchem-562	301	1	[	[	X
eurjchem-562	301	2	11	11	NUM
eurjchem-562	301	3	]	]	PUNCT
eurjchem-562	301	4	.	.	PUNCT
eurjchem-562	302	1	jacobi	jacobi	PROPN
eurjchem-562	302	2	,	,	PUNCT
eurjchem-562	302	3	p.	p.	NOUN
eurjchem-562	302	4	a.	a.	NOUN
eurjchem-562	302	5	;	;	PUNCT
eurjchem-562	302	6	brielmann	brielmann	PROPN
eurjchem-562	302	7	,	,	PUNCT
eurjchem-562	302	8	h.	h.	PROPN
eurjchem-562	302	9	l.	l.	PROPN
eurjchem-562	302	10	;	;	PUNCT
eurjchem-562	302	11	hauck	hauck	PROPN
eurjchem-562	302	12	,	,	PUNCT
eurjchem-562	302	13	s.	s.	PROPN
eurjchem-562	302	14	i.	i.	PROPN
eurjchem-562	302	15	j.	j.	PROPN
eurjchem-562	302	16	org	org	PROPN
eurjchem-562	302	17	.	.	PUNCT
eurjchem-562	302	18	chem	chem	PROPN
eurjchem-562	302	19	.	.	PUNCT
eurjchem-562	303	1	1996	1996	NUM
eurjchem-562	303	2	,	,	PUNCT
eurjchem-562	303	3	61	61	NUM
eurjchem-562	303	4	,	,	PUNCT
eurjchem-562	303	5	5013‐	5013‐	NUM
eurjchem-562	303	6	5023	5023	NUM
eurjchem-562	303	7	.	.	PUNCT
eurjchem-562	304	1	[	[	X
eurjchem-562	304	2	12	12	NUM
eurjchem-562	304	3	]	]	PUNCT
eurjchem-562	304	4	.	.	PUNCT
eurjchem-562	305	1	yasuhara	yasuhara	PROPN
eurjchem-562	305	2	,	,	PUNCT
eurjchem-562	305	3	a.	a.	NOUN
eurjchem-562	305	4	;	;	PUNCT
eurjchem-562	305	5	kanamori	kanamori	PROPN
eurjchem-562	305	6	,	,	PUNCT
eurjchem-562	305	7	y.	y.	PROPN
eurjchem-562	305	8	;	;	PUNCT
eurjchem-562	305	9	kaneko	kaneko	PROPN
eurjchem-562	305	10	,	,	PUNCT
eurjchem-562	305	11	m.	m.	NOUN
eurjchem-562	305	12	;	;	PUNCT
eurjchem-562	305	13	numata	numata	PROPN
eurjchem-562	305	14	,	,	PUNCT
eurjchem-562	305	15	a.	a.	NOUN
eurjchem-562	305	16	;	;	PUNCT
eurjchem-562	305	17	kondo	kondo	PROPN
eurjchem-562	305	18	,	,	PUNCT
eurjchem-562	305	19	y.	y.	PROPN
eurjchem-562	305	20	;	;	PUNCT
eurjchem-562	305	21	sakamoto	sakamoto	NOUN
eurjchem-562	305	22	,	,	PUNCT
eurjchem-562	305	23	t.	t.	PROPN
eurjchem-562	305	24	j.	j.	PROPN
eurjchem-562	305	25	chem	chem	PROPN
eurjchem-562	305	26	.	.	PUNCT
eurjchem-562	306	1	soc	soc	PROPN
eurjchem-562	306	2	.	.	PUNCT
eurjchem-562	306	3	,	,	PUNCT
eurjchem-562	306	4	perkin	perkin	PROPN
eurjchem-562	306	5	trans	trans	PROPN
eurjchem-562	306	6	.	.	PUNCT
eurjchem-562	307	1	i	i	PRON
eurjchem-562	307	2	1999	1999	NUM
eurjchem-562	307	3	,	,	PUNCT
eurjchem-562	307	4	529‐534	529‐534	NUM
eurjchem-562	307	5	.	.	PUNCT
eurjchem-562	308	1	[	[	X
eurjchem-562	308	2	13	13	NUM
eurjchem-562	308	3	]	]	PUNCT
eurjchem-562	308	4	.	.	PUNCT
eurjchem-562	309	1	hiroya	hiroya	PROPN
eurjchem-562	309	2	,	,	PUNCT
eurjchem-562	309	3	k.	k.	PROPN
eurjchem-562	309	4	;	;	PUNCT
eurjchem-562	309	5	jouka	jouka	PROPN
eurjchem-562	309	6	,	,	PUNCT
eurjchem-562	309	7	r.	r.	PROPN
eurjchem-562	309	8	;	;	PUNCT
eurjchem-562	309	9	kameda	kameda	PROPN
eurjchem-562	309	10	,	,	PUNCT
eurjchem-562	309	11	m.	m.	NOUN
eurjchem-562	309	12	;	;	PUNCT
eurjchem-562	309	13	yasuhara	yasuhara	PROPN
eurjchem-562	309	14	,	,	PUNCT
eurjchem-562	309	15	a.	a.	NOUN
eurjchem-562	309	16	;	;	PUNCT
eurjchem-562	309	17	sakamoto	sakamoto	NOUN
eurjchem-562	309	18	,	,	PUNCT
eurjchem-562	309	19	t.	t.	PROPN
eurjchem-562	309	20	tetrahedron	tetrahedron	NOUN
eurjchem-562	309	21	2001	2001	NUM
eurjchem-562	309	22	,	,	PUNCT
eurjchem-562	309	23	57	57	NUM
eurjchem-562	309	24	,	,	PUNCT
eurjchem-562	309	25	9697‐9710	9697‐9710	NUM
eurjchem-562	309	26	.	.	PUNCT
eurjchem-562	310	1	[	[	X
eurjchem-562	310	2	14	14	NUM
eurjchem-562	310	3	]	]	PUNCT
eurjchem-562	310	4	.	.	PUNCT
eurjchem-562	311	1	chung	chung	PROPN
eurjchem-562	311	2	,	,	PUNCT
eurjchem-562	311	3	k.	k.	PROPN
eurjchem-562	311	4	‐h	‐h	PROPN
eurjchem-562	311	5	.	.	PUNCT
eurjchem-562	311	6	;	;	PUNCT
eurjchem-562	311	7	moon	moon	PROPN
eurjchem-562	311	8	,	,	PUNCT
eurjchem-562	311	9	b.	b.	PROPN
eurjchem-562	312	1	‐c	‐c	PROPN
eurjchem-562	312	2	.	.	PUNCT
eurjchem-562	313	1	;	;	PUNCT
eurjchem-562	313	2	lim	lim	PROPN
eurjchem-562	313	3	,	,	PUNCT
eurjchem-562	313	4	c.	c.	PROPN
eurjchem-562	313	5	h.	h.	PROPN
eurjchem-562	313	6	;	;	PUNCT
eurjchem-562	313	7	kim	kim	PROPN
eurjchem-562	313	8	,	,	PUNCT
eurjchem-562	313	9	j.	j.	PROPN
eurjchem-562	313	10	p.	p.	PROPN
eurjchem-562	313	11	;	;	PUNCT
eurjchem-562	313	12	lee	lee	PROPN
eurjchem-562	313	13	,	,	PUNCT
eurjchem-562	313	14	j.	j.	PROPN
eurjchem-562	313	15	h.	h.	PROPN
eurjchem-562	313	16	;	;	PUNCT
eurjchem-562	313	17	chi	chi	PROPN
eurjchem-562	313	18	,	,	PUNCT
eurjchem-562	313	19	d.	d.	PROPN
eurjchem-562	313	20	y.	y.	PROPN
eurjchem-562	313	21	bull	bull	PROPN
eurjchem-562	313	22	.	.	PUNCT
eurjchem-562	314	1	korean	korean	ADJ
eurjchem-562	314	2	chem	chem	PROPN
eurjchem-562	314	3	.	.	PUNCT
eurjchem-562	315	1	soc	soc	PROPN
eurjchem-562	315	2	.	.	PUNCT
eurjchem-562	316	1	2006	2006	NUM
eurjchem-562	316	2	,	,	PUNCT
eurjchem-562	316	3	27	27	NUM
eurjchem-562	316	4	,	,	PUNCT
eurjchem-562	316	5	1203‐1205	1203‐1205	NUM
eurjchem-562	316	6	.	.	PUNCT
eurjchem-562	317	1	[	[	X
eurjchem-562	317	2	15	15	NUM
eurjchem-562	317	3	]	]	PUNCT
eurjchem-562	317	4	.	.	PUNCT
eurjchem-562	317	5	amantini	amantini	PROPN
eurjchem-562	317	6	,	,	PUNCT
eurjchem-562	317	7	d.	d.	PROPN
eurjchem-562	317	8	;	;	PUNCT
eurjchem-562	317	9	beleggia	beleggia	PROPN
eurjchem-562	317	10	,	,	PUNCT
eurjchem-562	317	11	r.	r.	PROPN
eurjchem-562	317	12	;	;	PUNCT
eurjchem-562	317	13	fringuelli	fringuelli	PROPN
eurjchem-562	317	14	,	,	PUNCT
eurjchem-562	317	15	f.	f.	PROPN
eurjchem-562	317	16	;	;	PUNCT
eurjchem-562	317	17	pizzo	pizzo	PROPN
eurjchem-562	317	18	,	,	PUNCT
eurjchem-562	317	19	f.	f.	PROPN
eurjchem-562	317	20	;	;	PUNCT
eurjchem-562	317	21	vaccaro	vaccaro	PROPN
eurjchem-562	317	22	,	,	PUNCT
eurjchem-562	317	23	l.	l.	PROPN
eurjchem-562	317	24	j.	j.	PROPN
eurjchem-562	317	25	org	org	PROPN
eurjchem-562	317	26	.	.	PUNCT
eurjchem-562	317	27	chem	chem	PROPN
eurjchem-562	317	28	.	.	PUNCT
eurjchem-562	318	1	2004	2004	NUM
eurjchem-562	318	2	,	,	PUNCT
eurjchem-562	318	3	69	69	NUM
eurjchem-562	318	4	,	,	PUNCT
eurjchem-562	318	5	2896‐2898	2896‐2898	NUM
eurjchem-562	318	6	.	.	PUNCT
eurjchem-562	319	1	[	[	X
eurjchem-562	319	2	16	16	NUM
eurjchem-562	319	3	]	]	PUNCT
eurjchem-562	319	4	.	.	PUNCT
eurjchem-562	320	1	alden‐danforth	alden‐danforth	PROPN
eurjchem-562	320	2	,	,	PUNCT
eurjchem-562	320	3	e.	e.	PROPN
eurjchem-562	320	4	;	;	PUNCT
eurjchem-562	320	5	scerba	scerba	NOUN
eurjchem-562	320	6	,	,	PUNCT
eurjchem-562	320	7	m.	m.	NOUN
eurjchem-562	320	8	t.	t.	PROPN
eurjchem-562	320	9	;	;	PUNCT
eurjchem-562	320	10	lectka	lectka	PROPN
eurjchem-562	320	11	,	,	PUNCT
eurjchem-562	320	12	t.	t.	PROPN
eurjchem-562	320	13	org	org	PROPN
eurjchem-562	320	14	.	.	PUNCT
eurjchem-562	321	1	lett	lett	PROPN
eurjchem-562	321	2	.	.	PROPN
eurjchem-562	321	3	2008	2008	NUM
eurjchem-562	321	4	,	,	PUNCT
eurjchem-562	321	5	10	10	NUM
eurjchem-562	321	6	,	,	PUNCT
eurjchem-562	321	7	4951‐	4951‐	NUM
eurjchem-562	321	8	4953	4953	NUM
eurjchem-562	321	9	.	.	PUNCT
eurjchem-562	322	1	[	[	X
eurjchem-562	322	2	17	17	NUM
eurjchem-562	322	3	]	]	SYM
eurjchem-562	322	4	.	.	PUNCT
eurjchem-562	322	5	albanese	albanese	PROPN
eurjchem-562	322	6	,	,	PUNCT
eurjchem-562	322	7	d.	d.	PROPN
eurjchem-562	322	8	;	;	PUNCT
eurjchem-562	322	9	landini	landini	PROPN
eurjchem-562	322	10	,	,	PUNCT
eurjchem-562	322	11	d.	d.	PROPN
eurjchem-562	322	12	;	;	PUNCT
eurjchem-562	322	13	penso	penso	PROPN
eurjchem-562	322	14	,	,	PUNCT
eurjchem-562	322	15	m.	m.	NOUN
eurjchem-562	322	16	;	;	PUNCT
eurjchem-562	322	17	petricci	petricci	PROPN
eurjchem-562	322	18	,	,	PUNCT
eurjchem-562	322	19	s.	s.	PROPN
eurjchem-562	322	20	synlett	synlett	PROPN
eurjchem-562	322	21	.	.	PUNCT
eurjchem-562	323	1	1999	1999	NUM
eurjchem-562	323	2	,	,	PUNCT
eurjchem-562	323	3	199‐200	199‐200	NUM
eurjchem-562	323	4	.	.	PUNCT
eurjchem-562	324	1	[	[	X
eurjchem-562	324	2	18	18	NUM
eurjchem-562	324	3	]	]	SYM
eurjchem-562	324	4	.	.	PUNCT
eurjchem-562	324	5	albanese	albanese	PROPN
eurjchem-562	324	6	,	,	PUNCT
eurjchem-562	324	7	d.	d.	PROPN
eurjchem-562	324	8	;	;	PUNCT
eurjchem-562	324	9	donghi	donghi	PROPN
eurjchem-562	324	10	,	,	PUNCT
eurjchem-562	324	11	a.	a.	NOUN
eurjchem-562	324	12	;	;	PUNCT
eurjchem-562	324	13	landini	landini	PROPN
eurjchem-562	324	14	,	,	PUNCT
eurjchem-562	324	15	d.	d.	PROPN
eurjchem-562	324	16	;	;	PUNCT
eurjchem-562	324	17	lupi	lupi	PROPN
eurjchem-562	324	18	,	,	PUNCT
eurjchem-562	324	19	v.	v.	PROPN
eurjchem-562	324	20	;	;	PUNCT
eurjchem-562	324	21	penso	penso	PROPN
eurjchem-562	324	22	,	,	PUNCT
eurjchem-562	324	23	m.	m.	NOUN
eurjchem-562	324	24	green	green	PROPN
eurjchem-562	324	25	chem	chem	PROPN
eurjchem-562	324	26	.	.	PUNCT
eurjchem-562	325	1	2003	2003	NUM
eurjchem-562	325	2	,	,	PUNCT
eurjchem-562	325	3	5	5	NUM
eurjchem-562	325	4	,	,	PUNCT
eurjchem-562	325	5	367‐369	367‐369	NUM
eurjchem-562	325	6	.	.	PUNCT
eurjchem-562	326	1	[	[	X
eurjchem-562	326	2	19	19	NUM
eurjchem-562	326	3	]	]	PUNCT
eurjchem-562	326	4	.	.	PUNCT
eurjchem-562	327	1	lee	lee	PROPN
eurjchem-562	327	2	,	,	PUNCT
eurjchem-562	327	3	h.	h.	PROPN
eurjchem-562	327	4	‐g	‐g	PROPN
eurjchem-562	327	5	.	.	PUNCT
eurjchem-562	327	6	;	;	PUNCT
eurjchem-562	327	7	won	win	VERB
eurjchem-562	327	8	,	,	PUNCT
eurjchem-562	327	9	j.	j.	PROPN
eurjchem-562	327	10	‐e	‐e	PROPN
eurjchem-562	327	11	.	.	PROPN
eurjchem-562	327	12	;	;	PUNCT
eurjchem-562	328	1	kim	kim	PROPN
eurjchem-562	328	2	,	,	PUNCT
eurjchem-562	328	3	m.	m.	NOUN
eurjchem-562	328	4	‐j	‐j	NOUN
eurjchem-562	328	5	.	.	PUNCT
eurjchem-562	328	6	;	;	PUNCT
eurjchem-562	328	7	park	park	PROPN
eurjchem-562	328	8	,	,	PUNCT
eurjchem-562	328	9	s.	s.	PROPN
eurjchem-562	328	10	‐e	‐e	PROPN
eurjchem-562	328	11	.	.	PROPN
eurjchem-562	328	12	;	;	PUNCT
eurjchem-562	328	13	jung	jung	PROPN
eurjchem-562	328	14	,	,	PUNCT
eurjchem-562	328	15	k.	k.	PROPN
eurjchem-562	328	16	‐j	‐j	PROPN
eurjchem-562	328	17	.	.	PROPN
eurjchem-562	328	18	;	;	PUNCT
eurjchem-562	328	19	kim	kim	PROPN
eurjchem-562	328	20	,	,	PUNCT
eurjchem-562	328	21	b.	b.	PROPN
eurjchem-562	328	22	r.	r.	PROPN
eurjchem-562	328	23	;	;	PUNCT
eurjchem-562	328	24	lee	lee	PROPN
eurjchem-562	328	25	,	,	PUNCT
eurjchem-562	328	26	s.	s.	PROPN
eurjchem-562	328	27	‐g	‐g	PROPN
eurjchem-562	328	28	.	.	PUNCT
eurjchem-562	328	29	;	;	PUNCT
eurjchem-562	329	1	yoon	yoon	PROPN
eurjchem-562	329	2	,	,	PUNCT
eurjchem-562	329	3	y.	y.	PROPN
eurjchem-562	329	4	‐j	‐j	NOUN
eurjchem-562	329	5	.	.	PUNCT
eurjchem-562	329	6	j.	j.	PROPN
eurjchem-562	329	7	org	org	PROPN
eurjchem-562	329	8	.	.	PUNCT
eurjchem-562	329	9	chem	chem	PROPN
eurjchem-562	329	10	.	.	PUNCT
eurjchem-562	330	1	2009	2009	NUM
eurjchem-562	330	2	,	,	PUNCT
eurjchem-562	330	3	74	74	NUM
eurjchem-562	330	4	,	,	PUNCT
eurjchem-562	330	5	5675‐5678	5675‐5678	NUM
eurjchem-562	330	6	.	.	PUNCT
eurjchem-562	331	1	[	[	X
eurjchem-562	331	2	20	20	NUM
eurjchem-562	331	3	]	]	PUNCT
eurjchem-562	331	4	.	.	PUNCT
eurjchem-562	332	1	sheldrick	sheldrick	NOUN
eurjchem-562	332	2	,	,	PUNCT
eurjchem-562	332	3	g.	g.	PROPN
eurjchem-562	332	4	m.	m.	PROPN
eurjchem-562	332	5	shelxtl	shelxtl	PROPN
eurjchem-562	332	6	/	/	SYM
eurjchem-562	332	7	pc	pc	NOUN
eurjchem-562	332	8	version	version	NOUN
eurjchem-562	332	9	5	5	NUM
eurjchem-562	332	10	.	.	NOUN
eurjchem-562	332	11	1	1	NUM
eurjchem-562	332	12	;	;	PUNCT
eurjchem-562	332	13	siemens	siemen	NOUN
eurjchem-562	332	14	analytical	analytical	ADJ
eurjchem-562	332	15	x‐ray	x‐ray	PROPN
eurjchem-562	332	16	instruments	instruments	PROPN
eurjchem-562	332	17	inc	inc	PROPN
eurjchem-562	332	18	.	.	PROPN
eurjchem-562	332	19	:	:	PUNCT
eurjchem-562	333	1	madison	madison	PROPN
eurjchem-562	333	2	,	,	PUNCT
eurjchem-562	333	3	wi	wi	PROPN
eurjchem-562	333	4	,	,	PUNCT
eurjchem-562	333	5	1997	1997	NUM
eurjchem-562	333	6	.	.	PUNCT
eurjchem-562	334	1	[	[	X
eurjchem-562	334	2	21	21	NUM
eurjchem-562	334	3	]	]	PUNCT
eurjchem-562	334	4	.	.	PUNCT
eurjchem-562	335	1	johnson	johnson	PROPN
eurjchem-562	335	2	,	,	PUNCT
eurjchem-562	335	3	c.	c.	PROPN
eurjchem-562	335	4	k.	k.	PROPN
eurjchem-562	335	5	ortepii	ortepii	PROPN
eurjchem-562	335	6	.	.	PUNCT
eurjchem-562	336	1	report	report	PROPN
eurjchem-562	336	2	ornl‐5138	ornl‐5138	PROPN
eurjchem-562	336	3	;	;	PUNCT
eurjchem-562	336	4	oak	oak	PROPN
eurjchem-562	336	5	ridge	ridge	PROPN
eurjchem-562	336	6	national	national	PROPN
eurjchem-562	336	7	laboratory	laboratory	PROPN
eurjchem-562	336	8	:	:	PUNCT
eurjchem-562	336	9	oak	oak	PROPN
eurjchem-562	336	10	ridge	ridge	PROPN
eurjchem-562	336	11	,	,	PUNCT
eurjchem-562	336	12	tn	tn	PROPN
eurjchem-562	336	13	,	,	PUNCT
eurjchem-562	336	14	1976	1976	NUM
eurjchem-562	336	15	.	.	PUNCT
eurjchem-562	337	1	[	[	X
eurjchem-562	337	2	22	22	NUM
eurjchem-562	337	3	]	]	PUNCT
eurjchem-562	337	4	.	.	PUNCT
eurjchem-562	338	1	nanjo	nanjo	PROPN
eurjchem-562	338	2	,	,	PUNCT
eurjchem-562	338	3	k.	k.	PROPN
eurjchem-562	338	4	;	;	PUNCT
eurjchem-562	338	5	suzuki	suzuki	PROPN
eurjchem-562	338	6	,	,	PUNCT
eurjchem-562	338	7	k.	k.	PROPN
eurjchem-562	338	8	;	;	PUNCT
eurjchem-562	338	9	sekiya	sekiya	NOUN
eurjchem-562	338	10	,	,	PUNCT
eurjchem-562	338	11	m.	m.	NOUN
eurjchem-562	338	12	chem	chem	NOUN
eurjchem-562	338	13	.	.	PUNCT
eurjchem-562	339	1	pharm	pharm	NOUN
eurjchem-562	339	2	.	.	PUNCT
eurjchem-562	340	1	bull	bull	PROPN
eurjchem-562	340	2	.	.	PUNCT
eurjchem-562	341	1	1977	1977	NUM
eurjchem-562	341	2	,	,	PUNCT
eurjchem-562	341	3	25	25	NUM
eurjchem-562	341	4	,	,	PUNCT
eurjchem-562	341	5	2396‐	2396‐	NUM
eurjchem-562	341	6	4000	4000	NUM
eurjchem-562	341	7	.	.	PUNCT
eurjchem-562	342	1	[	[	X
eurjchem-562	342	2	23	23	NUM
eurjchem-562	342	3	]	]	PUNCT
eurjchem-562	342	4	.	.	PUNCT
eurjchem-562	343	1	ohnishi	ohnishi	PROPN
eurjchem-562	343	2	,	,	PUNCT
eurjchem-562	343	3	y.	y.	PROPN
eurjchem-562	343	4	;	;	PUNCT
eurjchem-562	343	5	kagami	kagami	PROPN
eurjchem-562	343	6	,	,	PUNCT
eurjchem-562	343	7	m.	m.	NOUN
eurjchem-562	343	8	;	;	PUNCT
eurjchem-562	343	9	numakunai	numakunai	ADV
eurjchem-562	343	10	,	,	PUNCT
eurjchem-562	343	11	t.	t.	PROPN
eurjchem-562	343	12	;	;	PUNCT
eurjchem-562	343	13	ohno	ohno	PROPN
eurjchem-562	343	14	,	,	PUNCT
eurjchem-562	343	15	a.	a.	NOUN
eurjchem-562	343	16	chem	chem	PROPN
eurjchem-562	343	17	.	.	PUNCT
eurjchem-562	344	1	lett	lett	PROPN
eurjchem-562	344	2	.	.	PUNCT
eurjchem-562	345	1	1976	1976	NUM
eurjchem-562	345	2	,	,	PUNCT
eurjchem-562	345	3	915‐916	915‐916	NUM
eurjchem-562	345	4	.	.	PUNCT
eurjchem-562	346	1	[	[	X
eurjchem-562	346	2	24	24	NUM
eurjchem-562	346	3	]	]	PUNCT
eurjchem-562	346	4	.	.	PUNCT
eurjchem-562	347	1	quincoses	quincoses	PROPN
eurjchem-562	347	2	,	,	PUNCT
eurjchem-562	347	3	j.	j.	PROPN
eurjchem-562	347	4	;	;	PUNCT
eurjchem-562	347	5	peseke	peseke	PROPN
eurjchem-562	347	6	,	,	PUNCT
eurjchem-562	347	7	k.	k.	PROPN
eurjchem-562	347	8	quim	quim	PROPN
eurjchem-562	347	9	.	.	PUNCT
eurjchem-562	348	1	tecnol	tecnol	PROPN
eurjchem-562	348	2	.	.	PUNCT
eurjchem-562	349	1	quim	quim	PROPN
eurjchem-562	349	2	.	.	PUNCT
eurjchem-562	350	1	1978	1978	NUM
eurjchem-562	350	2	,	,	PUNCT
eurjchem-562	350	3	6	6	NUM
eurjchem-562	350	4	,	,	PUNCT
eurjchem-562	350	5	95‐102	95‐102	NUM
eurjchem-562	350	6	.	.	PUNCT