id	sid	tid	token	lemma	pos
eurjchem-570	1	1	untitled	untitle	VERB
eurjchem-570	1	2	european	european	PROPN
eurjchem-570	1	3	journal	journal	PROPN
eurjchem-570	1	4	of	of	ADP
eurjchem-570	1	5	chemistry	chemistry	NOUN
eurjchem-570	1	6	3	3	NUM
eurjchem-570	1	7	(	(	PUNCT
eurjchem-570	1	8	2	2	NUM
eurjchem-570	1	9	)	)	PUNCT
eurjchem-570	1	10	(	(	PUNCT
eurjchem-570	1	11	2012	2012	NUM
eurjchem-570	1	12	)	)	PUNCT
eurjchem-570	1	13	152‐155	152‐155	NUM
eurjchem-570	1	14	european	european	PROPN
eurjchem-570	1	15	journal	journal	PROPN
eurjchem-570	1	16	of	of	ADP
eurjchem-570	1	17	chemistry	chemistry	NOUN
eurjchem-570	1	18	issn	issn	PROPN
eurjchem-570	1	19	2153‐2249	2153‐2249	PROPN
eurjchem-570	1	20	(	(	PUNCT
eurjchem-570	1	21	print	print	NOUN
eurjchem-570	1	22	)	)	PUNCT
eurjchem-570	1	23	/	/	SYM
eurjchem-570	1	24	issn	issn	PROPN
eurjchem-570	1	25	2153‐2257	2153‐2257	NUM
eurjchem-570	1	26	(	(	PUNCT
eurjchem-570	1	27	online	online	ADJ
eurjchem-570	1	28	)	)	PUNCT
eurjchem-570	1	29			NOUN
eurjchem-570	1	30	2012	2012	NUM
eurjchem-570	1	31	eurjchem	eurjchem	PROPN
eurjchem-570	1	32	doi:10.5155	doi:10.5155	ADJ
eurjchem-570	1	33	/	/	SYM
eurjchem-570	1	34	eurjchem.3.2.152‐155.570	eurjchem.3.2.152‐155.570	NOUN
eurjchem-570	1	35	european	european	ADJ
eurjchem-570	1	36	journal	journal	PROPN
eurjchem-570	1	37	of	of	ADP
eurjchem-570	1	38	chemistry	chemistry	PROPN
eurjchem-570	1	39	journal	journal	PROPN
eurjchem-570	1	40	homepage	homepage	NOUN
eurjchem-570	1	41	:	:	PUNCT
eurjchem-570	1	42	www.eurjchem.com	www.eurjchem.com	X
eurjchem-570	1	43	development	development	NOUN
eurjchem-570	1	44	and	and	CCONJ
eurjchem-570	1	45	validation	validation	NOUN
eurjchem-570	1	46	of	of	ADP
eurjchem-570	1	47	a	a	DET
eurjchem-570	1	48	reversed‐phase	reversed‐phase	NOUN
eurjchem-570	1	49	column	column	NOUN
eurjchem-570	1	50	liquid	liquid	ADJ
eurjchem-570	1	51	chromatographic	chromatographic	ADJ
eurjchem-570	1	52	method	method	NOUN
eurjchem-570	1	53	for	for	ADP
eurjchem-570	1	54	simultaneous	simultaneous	ADJ
eurjchem-570	1	55	determination	determination	NOUN
eurjchem-570	1	56	of	of	ADP
eurjchem-570	1	57	two	two	NUM
eurjchem-570	1	58	novel	novel	ADJ
eurjchem-570	1	59	gliptins	gliptin	NOUN
eurjchem-570	1	60	in	in	ADP
eurjchem-570	1	61	their	their	PRON
eurjchem-570	1	62	binary	binary	ADJ
eurjchem-570	1	63	mixtures	mixture	NOUN
eurjchem-570	1	64	with	with	ADP
eurjchem-570	1	65	metformin	metformin	NOUN
eurjchem-570	1	66	mohammad	mohammad	PROPN
eurjchem-570	1	67	abdul‐azim	abdul‐azim	PROPN
eurjchem-570	1	68	mohammada	mohammada	PROPN
eurjchem-570	1	69	,	,	PUNCT
eurjchem-570	1	70	b	b	PROPN
eurjchem-570	1	71	,	,	PUNCT
eurjchem-570	1	72	ehab	ehab	PROPN
eurjchem-570	1	73	farouk	farouk	PROPN
eurjchem-570	1	74	elkadyb	elkadyb	PROPN
eurjchem-570	1	75	and	and	CCONJ
eurjchem-570	1	76	marwa	marwa	PROPN
eurjchem-570	1	77	ahmed	ahmed	PROPN
eurjchem-570	1	78	fouadb	fouadb	PROPN
eurjchem-570	1	79	,	,	PUNCT
eurjchem-570	1	80	*	*	PUNCT
eurjchem-570	1	81	a	a	DET
eurjchem-570	1	82	pharmaceutical	pharmaceutical	ADJ
eurjchem-570	1	83	chemistry	chemistry	NOUN
eurjchem-570	1	84	department	department	NOUN
eurjchem-570	1	85	,	,	PUNCT
eurjchem-570	1	86	faculty	faculty	NOUN
eurjchem-570	1	87	of	of	ADP
eurjchem-570	1	88	pharmacy	pharmacy	NOUN
eurjchem-570	1	89	,	,	PUNCT
eurjchem-570	1	90	umm	umm	INTJ
eurjchem-570	1	91	al‐qura	al‐qura	PROPN
eurjchem-570	1	92	university	university	PROPN
eurjchem-570	1	93	,	,	PUNCT
eurjchem-570	1	94	makkah	makkah	PROPN
eurjchem-570	1	95	al‐mokarama	al‐mokarama	PROPN
eurjchem-570	1	96	,	,	PUNCT
eurjchem-570	1	97	p.o	p.o	PROPN
eurjchem-570	1	98	.	.	PROPN
eurjchem-570	1	99	box	box	PROPN
eurjchem-570	1	100	715	715	NUM
eurjchem-570	1	101	,	,	PUNCT
eurjchem-570	1	102	kingdom	kingdom	NOUN
eurjchem-570	1	103	of	of	ADP
eurjchem-570	1	104	saudi	saudi	PROPN
eurjchem-570	1	105	arabia	arabia	PROPN
eurjchem-570	1	106	b	b	PROPN
eurjchem-570	1	107	pharmaceutical	pharmaceutical	ADJ
eurjchem-570	1	108	chemistry	chemistry	NOUN
eurjchem-570	1	109	department	department	NOUN
eurjchem-570	1	110	,	,	PUNCT
eurjchem-570	1	111	faculty	faculty	NOUN
eurjchem-570	1	112	of	of	ADP
eurjchem-570	1	113	pharmacy	pharmacy	NOUN
eurjchem-570	1	114	,	,	PUNCT
eurjchem-570	1	115	cairo	cairo	PROPN
eurjchem-570	1	116	university	university	PROPN
eurjchem-570	1	117	,	,	PUNCT
eurjchem-570	1	118	cairo	cairo	PROPN
eurjchem-570	1	119	,	,	PUNCT
eurjchem-570	1	120	11562	11562	NUM
eurjchem-570	1	121	,	,	PUNCT
eurjchem-570	1	122	egypt	egypt	PROPN
eurjchem-570	1	123	*	*	PUNCT
eurjchem-570	1	124	corresponding	correspond	VERB
eurjchem-570	1	125	author	author	NOUN
eurjchem-570	1	126	at	at	ADP
eurjchem-570	1	127	:	:	PUNCT
eurjchem-570	1	128	pharmaceutical	pharmaceutical	ADJ
eurjchem-570	1	129	chemistry	chemistry	NOUN
eurjchem-570	1	130	department	department	NOUN
eurjchem-570	1	131	,	,	PUNCT
eurjchem-570	1	132	faculty	faculty	NOUN
eurjchem-570	1	133	of	of	ADP
eurjchem-570	1	134	pharmacy	pharmacy	NOUN
eurjchem-570	1	135	,	,	PUNCT
eurjchem-570	1	136	cairo	cairo	PROPN
eurjchem-570	1	137	university	university	PROPN
eurjchem-570	1	138	,	,	PUNCT
eurjchem-570	1	139	cairo	cairo	PROPN
eurjchem-570	1	140	,	,	PUNCT
eurjchem-570	1	141	11562	11562	NUM
eurjchem-570	1	142	,	,	PUNCT
eurjchem-570	1	143	egypt	egypt	PROPN
eurjchem-570	1	144	.	.	PUNCT
eurjchem-570	2	1	tel	tel	PROPN
eurjchem-570	2	2	.	.	PUNCT
eurjchem-570	2	3	:	:	PUNCT
eurjchem-570	3	1	+2.012.22441198	+2.012.22441198	NOUN
eurjchem-570	3	2	;	;	PUNCT
eurjchem-570	3	3	fax	fax	NOUN
eurjchem-570	3	4	:	:	PUNCT
eurjchem-570	3	5	+2.02.24148452	+2.02.24148452	PROPN
eurjchem-570	3	6	.	.	PUNCT
eurjchem-570	3	7	e‐mail	e‐mail	PUNCT
eurjchem-570	4	1	address	address	NOUN
eurjchem-570	4	2	:	:	PUNCT
eurjchem-570	4	3	merro911@yahoo.com	merro911@yahoo.com	X
eurjchem-570	4	4	(	(	PUNCT
eurjchem-570	4	5	m.a	m.a	PROPN
eurjchem-570	4	6	.	.	PROPN
eurjchem-570	4	7	fouad	fouad	PROPN
eurjchem-570	4	8	)	)	PUNCT
eurjchem-570	4	9	.	.	PUNCT
eurjchem-570	5	1	article	article	NOUN
eurjchem-570	5	2	information	information	PROPN
eurjchem-570	5	3	abstract	abstract	ADV
eurjchem-570	5	4	received	receive	VERB
eurjchem-570	5	5	:	:	PUNCT
eurjchem-570	5	6	13	13	NUM
eurjchem-570	5	7	december	december	PROPN
eurjchem-570	5	8	2011	2011	NUM
eurjchem-570	5	9	accepted	accept	VERB
eurjchem-570	5	10	:	:	PUNCT
eurjchem-570	5	11	12	12	NUM
eurjchem-570	5	12	january	january	PROPN
eurjchem-570	5	13	2012	2012	NUM
eurjchem-570	5	14	online	online	NOUN
eurjchem-570	5	15	:	:	PUNCT
eurjchem-570	5	16	30	30	NUM
eurjchem-570	5	17	june	june	PROPN
eurjchem-570	5	18	2012	2012	NUM
eurjchem-570	5	19	keywords	keyword	VERB
eurjchem-570	5	20	a	a	DET
eurjchem-570	5	21	new	new	ADJ
eurjchem-570	5	22	,	,	PUNCT
eurjchem-570	5	23	simple	simple	ADJ
eurjchem-570	5	24	,	,	PUNCT
eurjchem-570	5	25	accurate	accurate	ADJ
eurjchem-570	5	26	,	,	PUNCT
eurjchem-570	5	27	and	and	CCONJ
eurjchem-570	5	28	precise	precise	ADJ
eurjchem-570	5	29	liquid	liquid	ADJ
eurjchem-570	5	30	chromatographic	chromatographic	ADJ
eurjchem-570	5	31	method	method	NOUN
eurjchem-570	5	32	has	have	AUX
eurjchem-570	5	33	been	be	AUX
eurjchem-570	5	34	developed	develop	VERB
eurjchem-570	5	35	and	and	CCONJ
eurjchem-570	5	36	validated	validate	VERB
eurjchem-570	5	37	for	for	ADP
eurjchem-570	5	38	the	the	DET
eurjchem-570	5	39	determination	determination	NOUN
eurjchem-570	5	40	of	of	ADP
eurjchem-570	5	41	two	two	NUM
eurjchem-570	5	42	novel	novel	ADJ
eurjchem-570	5	43	dipeptidylpeptidase‐4	dipeptidylpeptidase‐4	NOUN
eurjchem-570	5	44	(	(	PUNCT
eurjchem-570	5	45	dpp‐4	dpp‐4	NOUN
eurjchem-570	5	46	)	)	PUNCT
eurjchem-570	5	47	inhibitors	inhibitor	NOUN
eurjchem-570	5	48	;	;	PUNCT
eurjchem-570	5	49	namely	namely	ADV
eurjchem-570	5	50	vildagliptin	vildagliptin	NOUN
eurjchem-570	5	51	(	(	PUNCT
eurjchem-570	5	52	vlg	vlg	PROPN
eurjchem-570	5	53	)	)	PUNCT
eurjchem-570	5	54	and	and	CCONJ
eurjchem-570	5	55	saxagliptin	saxagliptin	PROPN
eurjchem-570	5	56	hcl	hcl	PROPN
eurjchem-570	5	57	(	(	PUNCT
eurjchem-570	5	58	sxg	sxg	NOUN
eurjchem-570	5	59	)	)	PUNCT
eurjchem-570	5	60	simultaneously	simultaneously	ADV
eurjchem-570	5	61	in	in	ADP
eurjchem-570	5	62	their	their	PRON
eurjchem-570	5	63	binary	binary	ADJ
eurjchem-570	5	64	mixtures	mixture	NOUN
eurjchem-570	5	65	with	with	ADP
eurjchem-570	5	66	metformin	metformin	PROPN
eurjchem-570	5	67	hcl	hcl	PROPN
eurjchem-570	5	68	(	(	PUNCT
eurjchem-570	5	69	met	meet	VERB
eurjchem-570	5	70	)	)	PUNCT
eurjchem-570	5	71	.	.	PUNCT
eurjchem-570	6	1	chromatographic	chromatographic	ADJ
eurjchem-570	6	2	separation	separation	NOUN
eurjchem-570	6	3	was	be	AUX
eurjchem-570	6	4	achieved	achieve	VERB
eurjchem-570	6	5	on	on	ADP
eurjchem-570	6	6	an	an	DET
eurjchem-570	6	7	inertsil	inertsil	NOUN
eurjchem-570	6	8	®	®	NOUN
eurjchem-570	6	9	cn‐3	cn‐3	NOUN
eurjchem-570	6	10	column	column	NOUN
eurjchem-570	6	11	(	(	PUNCT
eurjchem-570	6	12	250	250	NUM
eurjchem-570	6	13	mm	mm	NOUN
eurjchem-570	6	14	x	x	SYM
eurjchem-570	6	15	4.6	4.6	NUM
eurjchem-570	6	16	mm	mm	NOUN
eurjchem-570	6	17	,	,	PUNCT
eurjchem-570	6	18	5	5	NUM
eurjchem-570	6	19	µm	µm	NOUN
eurjchem-570	6	20	)	)	PUNCT
eurjchem-570	6	21	.	.	PUNCT
eurjchem-570	7	1	isocratic	isocratic	ADJ
eurjchem-570	7	2	elution	elution	NOUN
eurjchem-570	7	3	using	use	VERB
eurjchem-570	7	4	a	a	DET
eurjchem-570	7	5	mobile	mobile	ADJ
eurjchem-570	7	6	phase	phase	NOUN
eurjchem-570	7	7	of	of	ADP
eurjchem-570	7	8	potassium	potassium	NOUN
eurjchem-570	7	9	dihydrogen	dihydrogen	NOUN
eurjchem-570	7	10	phosphate	phosphate	NOUN
eurjchem-570	7	11	buffer	buffer	NOUN
eurjchem-570	7	12	ph	ph	NOUN
eurjchem-570	7	13	(	(	PUNCT
eurjchem-570	7	14	4.6	4.6	NUM
eurjchem-570	7	15	)	)	PUNCT
eurjchem-570	7	16	‐	‐	ADJ
eurjchem-570	7	17	acetonitrile	acetonitrile	NOUN
eurjchem-570	7	18	(	(	PUNCT
eurjchem-570	7	19	15:85	15:85	NUM
eurjchem-570	7	20	,	,	PUNCT
eurjchem-570	7	21	v	v	NOUN
eurjchem-570	7	22	:	:	SYM
eurjchem-570	7	23	v	v	NOUN
eurjchem-570	7	24	)	)	PUNCT
eurjchem-570	7	25	at	at	ADP
eurjchem-570	7	26	a	a	DET
eurjchem-570	7	27	flow	flow	NOUN
eurjchem-570	7	28	rate	rate	NOUN
eurjchem-570	7	29	of	of	ADP
eurjchem-570	7	30	1	1	NUM
eurjchem-570	7	31	ml	ml	NOUN
eurjchem-570	7	32	/	/	SYM
eurjchem-570	7	33	min	min	NOUN
eurjchem-570	7	34	with	with	ADP
eurjchem-570	7	35	uv	uv	NOUN
eurjchem-570	7	36	detection	detection	NOUN
eurjchem-570	7	37	at	at	ADP
eurjchem-570	7	38	208	208	NUM
eurjchem-570	7	39	nm	nm	NOUN
eurjchem-570	7	40	was	be	AUX
eurjchem-570	7	41	performed	perform	VERB
eurjchem-570	7	42	.	.	PUNCT
eurjchem-570	8	1	the	the	DET
eurjchem-570	8	2	liquid	liquid	ADJ
eurjchem-570	8	3	chromatographic	chromatographic	ADJ
eurjchem-570	8	4	method	method	NOUN
eurjchem-570	8	5	was	be	AUX
eurjchem-570	8	6	used	use	VERB
eurjchem-570	8	7	for	for	ADP
eurjchem-570	8	8	the	the	DET
eurjchem-570	8	9	simultaneous	simultaneous	ADJ
eurjchem-570	8	10	determination	determination	NOUN
eurjchem-570	8	11	of	of	ADP
eurjchem-570	8	12	either	either	DET
eurjchem-570	8	13	vlg	vlg	PROPN
eurjchem-570	8	14	,	,	PUNCT
eurjchem-570	8	15	sxg	sxg	NOUN
eurjchem-570	8	16	and	and	CCONJ
eurjchem-570	8	17	met	meet	VERB
eurjchem-570	8	18	in	in	ADP
eurjchem-570	8	19	the	the	DET
eurjchem-570	8	20	range	range	NOUN
eurjchem-570	8	21	of	of	ADP
eurjchem-570	8	22	5‐200	5‐200	PROPN
eurjchem-570	8	23	,	,	PUNCT
eurjchem-570	8	24	0.5‐20	0.5‐20	NUM
eurjchem-570	8	25	and	and	CCONJ
eurjchem-570	8	26	50‐2000	50‐2000	NUM
eurjchem-570	8	27	μg	μg	NOUN
eurjchem-570	8	28	/	/	SYM
eurjchem-570	8	29	ml	ml	PROPN
eurjchem-570	8	30	,	,	PUNCT
eurjchem-570	8	31	respectively	respectively	ADV
eurjchem-570	8	32	.	.	PUNCT
eurjchem-570	9	1	the	the	DET
eurjchem-570	9	2	methods	method	NOUN
eurjchem-570	9	3	developed	develop	VERB
eurjchem-570	9	4	were	be	AUX
eurjchem-570	9	5	satisfactorily	satisfactorily	ADV
eurjchem-570	9	6	applied	apply	VERB
eurjchem-570	9	7	to	to	ADP
eurjchem-570	9	8	the	the	DET
eurjchem-570	9	9	analysis	analysis	NOUN
eurjchem-570	9	10	of	of	ADP
eurjchem-570	9	11	the	the	DET
eurjchem-570	9	12	pharmaceutical	pharmaceutical	NOUN
eurjchem-570	9	13	formulations	formulation	NOUN
eurjchem-570	9	14	and	and	CCONJ
eurjchem-570	9	15	proved	prove	VERB
eurjchem-570	9	16	to	to	PART
eurjchem-570	9	17	be	be	AUX
eurjchem-570	9	18	specific	specific	ADJ
eurjchem-570	9	19	and	and	CCONJ
eurjchem-570	9	20	accurate	accurate	ADJ
eurjchem-570	9	21	for	for	ADP
eurjchem-570	9	22	the	the	DET
eurjchem-570	9	23	quality	quality	NOUN
eurjchem-570	9	24	control	control	NOUN
eurjchem-570	9	25	of	of	ADP
eurjchem-570	9	26	the	the	DET
eurjchem-570	9	27	cited	cite	VERB
eurjchem-570	9	28	drugs	drug	NOUN
eurjchem-570	9	29	in	in	ADP
eurjchem-570	9	30	pharmaceutical	pharmaceutical	ADJ
eurjchem-570	9	31	dosage	dosage	NOUN
eurjchem-570	9	32	forms	form	NOUN
eurjchem-570	9	33	.	.	PUNCT
eurjchem-570	10	1	metformin	metformin	NOUN
eurjchem-570	10	2	saxagliptin	saxagliptin	PROPN
eurjchem-570	10	3	vildagliptin	vildagliptin	PROPN
eurjchem-570	10	4	isocratic	isocratic	PROPN
eurjchem-570	10	5	elution	elution	NOUN
eurjchem-570	10	6	pharmaceutical	pharmaceutical	NOUN
eurjchem-570	10	7	preparation	preparation	NOUN
eurjchem-570	10	8	reversed‐phase	reversed‐phase	NOUN
eurjchem-570	10	9	liquid	liquid	ADJ
eurjchem-570	10	10	chromatography	chromatography	NOUN
eurjchem-570	10	11	1	1	NUM
eurjchem-570	10	12	.	.	PUNCT
eurjchem-570	11	1	introduction	introduction	NOUN
eurjchem-570	11	2	vildagliptin	vildagliptin	NOUN
eurjchem-570	11	3	(	(	PUNCT
eurjchem-570	11	4	vdg	vdg	NOUN
eurjchem-570	11	5	)	)	PUNCT
eurjchem-570	11	6	,	,	PUNCT
eurjchem-570	11	7	s‐1‐[n‐(3‐hydroxy‐1‐adamantyl	s‐1‐[n‐(3‐hydroxy‐1‐adamantyl	PROPN
eurjchem-570	11	8	)	)	PUNCT
eurjchem-570	11	9	glycyl	glycyl	NOUN
eurjchem-570	11	10	]	]	PUNCT
eurjchem-570	11	11	pyrrolidine‐2‐carbonitrile	pyrrolidine‐2‐carbonitrile	NUM
eurjchem-570	11	12	(	(	PUNCT
eurjchem-570	11	13	figure	figure	NOUN
eurjchem-570	11	14	1	1	NUM
eurjchem-570	11	15	)	)	PUNCT
eurjchem-570	11	16	,	,	PUNCT
eurjchem-570	11	17	is	be	AUX
eurjchem-570	11	18	an	an	DET
eurjchem-570	11	19	oral	oral	ADJ
eurjchem-570	11	20	hypoglycemic	hypoglycemic	ADJ
eurjchem-570	11	21	drug	drug	NOUN
eurjchem-570	11	22	of	of	ADP
eurjchem-570	11	23	the	the	DET
eurjchem-570	11	24	dipeptidylpeptidase‐4	dipeptidylpeptidase‐4	PROPN
eurjchem-570	11	25	(	(	PUNCT
eurjchem-570	11	26	dpp‐4	dpp‐4	NOUN
eurjchem-570	11	27	)	)	PUNCT
eurjchem-570	11	28	inhibitor	inhibitor	NOUN
eurjchem-570	11	29	class	class	NOUN
eurjchem-570	11	30	[	[	X
eurjchem-570	11	31	1	1	NUM
eurjchem-570	11	32	]	]	PUNCT
eurjchem-570	11	33	.	.	PUNCT
eurjchem-570	12	1	dpp‐4	dpp‐4	NOUN
eurjchem-570	12	2	inhibitors	inhibitor	NOUN
eurjchem-570	12	3	represent	represent	VERB
eurjchem-570	12	4	a	a	DET
eurjchem-570	12	5	new	new	ADJ
eurjchem-570	12	6	therapeutic	therapeutic	ADJ
eurjchem-570	12	7	approach	approach	NOUN
eurjchem-570	12	8	to	to	ADP
eurjchem-570	12	9	the	the	DET
eurjchem-570	12	10	treatment	treatment	NOUN
eurjchem-570	12	11	of	of	ADP
eurjchem-570	12	12	type	type	NOUN
eurjchem-570	12	13	2	2	NUM
eurjchem-570	12	14	diabetes	diabetes	NOUN
eurjchem-570	12	15	[	[	X
eurjchem-570	12	16	2	2	NUM
eurjchem-570	12	17	]	]	PUNCT
eurjchem-570	12	18	.	.	PUNCT
eurjchem-570	13	1	literature	literature	NOUN
eurjchem-570	13	2	survey	survey	NOUN
eurjchem-570	13	3	reveals	reveal	VERB
eurjchem-570	13	4	that	that	SCONJ
eurjchem-570	13	5	only	only	ADV
eurjchem-570	13	6	one	one	NUM
eurjchem-570	13	7	spectrophotometric	spectrophotometric	ADJ
eurjchem-570	13	8	method	method	NOUN
eurjchem-570	13	9	[	[	X
eurjchem-570	13	10	3	3	NUM
eurjchem-570	13	11	]	]	PUNCT
eurjchem-570	13	12	and	and	CCONJ
eurjchem-570	13	13	one	one	NUM
eurjchem-570	13	14	chroma‐	chroma‐	NUM
eurjchem-570	13	15	tographic	tographic	ADJ
eurjchem-570	13	16	method	method	NOUN
eurjchem-570	13	17	was	be	AUX
eurjchem-570	13	18	reported	report	VERB
eurjchem-570	13	19	for	for	ADP
eurjchem-570	13	20	the	the	DET
eurjchem-570	13	21	determination	determination	NOUN
eurjchem-570	13	22	of	of	ADP
eurjchem-570	13	23	vdg	vdg	NOUN
eurjchem-570	13	24	in	in	ADP
eurjchem-570	13	25	the	the	DET
eurjchem-570	13	26	presence	presence	NOUN
eurjchem-570	13	27	of	of	ADP
eurjchem-570	13	28	its	its	PRON
eurjchem-570	13	29	synthetic	synthetic	ADJ
eurjchem-570	13	30	intermediate	intermediate	NOUN
eurjchem-570	13	31	[	[	X
eurjchem-570	13	32	4	4	NUM
eurjchem-570	13	33	]	]	PUNCT
eurjchem-570	13	34	.	.	PUNCT
eurjchem-570	14	1	saxagliptin	saxagliptin	PROPN
eurjchem-570	14	2	(	(	PUNCT
eurjchem-570	14	3	sxg	sxg	NOUN
eurjchem-570	14	4	)	)	PUNCT
eurjchem-570	14	5	,	,	PUNCT
eurjchem-570	14	6	(	(	PUNCT
eurjchem-570	14	7	1s,3s,5s)‐2‐[(2s)‐2‐amino‐2‐(3‐hydroxy	1s,3s,5s)‐2‐[(2s)‐2‐amino‐2‐(3‐hydroxy	NUM
eurjchem-570	14	8	‐1‐adamantyl)acetyl]‐	‐1‐adamantyl)acetyl]‐	NOUN
eurjchem-570	14	9	2‐azabicyclo	2‐azabicyclo	NUM
eurjchem-570	15	1	[	[	X
eurjchem-570	15	2	3.1.0	3.1.0	NUM
eurjchem-570	15	3	]	]	X
eurjchem-570	15	4	hexane‐3‐carbo‐	hexane‐3‐carbo‐	NOUN
eurjchem-570	15	5	nitrile	nitrile	NOUN
eurjchem-570	15	6	(	(	PUNCT
eurjchem-570	15	7	figure	figure	NOUN
eurjchem-570	15	8	1	1	NUM
eurjchem-570	15	9	)	)	PUNCT
eurjchem-570	15	10	,	,	PUNCT
eurjchem-570	15	11	is	be	AUX
eurjchem-570	15	12	another	another	DET
eurjchem-570	15	13	new	new	ADJ
eurjchem-570	15	14	dipeptidylpeptidase‐4	dipeptidylpeptidase‐4	NOUN
eurjchem-570	15	15	(	(	PUNCT
eurjchem-570	15	16	dpp‐4	dpp‐4	NOUN
eurjchem-570	15	17	)	)	PUNCT
eurjchem-570	15	18	inhibitor	inhibitor	NOUN
eurjchem-570	16	1	[	[	X
eurjchem-570	16	2	5	5	NUM
eurjchem-570	16	3	]	]	PUNCT
eurjchem-570	16	4	.	.	PUNCT
eurjchem-570	17	1	sxg	sxg	PROPN
eurjchem-570	17	2	was	be	AUX
eurjchem-570	17	3	recently	recently	ADV
eurjchem-570	17	4	approved	approve	VERB
eurjchem-570	17	5	for	for	ADP
eurjchem-570	17	6	the	the	DET
eurjchem-570	17	7	treatment	treatment	NOUN
eurjchem-570	17	8	of	of	ADP
eurjchem-570	17	9	type	type	NOUN
eurjchem-570	17	10	2	2	NUM
eurjchem-570	17	11	diabetes	diabetes	NOUN
eurjchem-570	17	12	mellitus	mellitus	NOUN
eurjchem-570	18	1	[	[	X
eurjchem-570	18	2	6	6	NUM
eurjchem-570	18	3	]	]	PUNCT
eurjchem-570	18	4	.	.	PUNCT
eurjchem-570	19	1	literature	literature	NOUN
eurjchem-570	19	2	survey	survey	NOUN
eurjchem-570	19	3	reveals	reveal	VERB
eurjchem-570	19	4	that	that	SCONJ
eurjchem-570	19	5	only	only	ADV
eurjchem-570	19	6	one	one	NUM
eurjchem-570	19	7	lc‐ms	lc‐ms	NUM
eurjchem-570	19	8	/	/	SYM
eurjchem-570	19	9	ms	ms	NOUN
eurjchem-570	20	1	[	[	X
eurjchem-570	20	2	7	7	NUM
eurjchem-570	20	3	]	]	PUNCT
eurjchem-570	20	4	has	have	AUX
eurjchem-570	20	5	been	be	AUX
eurjchem-570	20	6	reported	report	VERB
eurjchem-570	20	7	for	for	ADP
eurjchem-570	20	8	sxg	sxg	NOUN
eurjchem-570	20	9	.	.	PUNCT
eurjchem-570	21	1	besides	besides	SCONJ
eurjchem-570	21	2	,	,	PUNCT
eurjchem-570	21	3	another	another	DET
eurjchem-570	21	4	lc	lc	NOUN
eurjchem-570	21	5	method	method	NOUN
eurjchem-570	21	6	with	with	ADP
eurjchem-570	21	7	uv	uv	NOUN
eurjchem-570	21	8	detection	detection	NOUN
eurjchem-570	21	9	[	[	X
eurjchem-570	21	10	8	8	NUM
eurjchem-570	21	11	]	]	PUNCT
eurjchem-570	21	12	and	and	CCONJ
eurjchem-570	21	13	a	a	DET
eurjchem-570	21	14	spectrophotometric	spectrophotometric	ADJ
eurjchem-570	21	15	method	method	NOUN
eurjchem-570	21	16	[	[	X
eurjchem-570	21	17	9	9	NUM
eurjchem-570	21	18	]	]	PUNCT
eurjchem-570	21	19	have	have	AUX
eurjchem-570	21	20	been	be	AUX
eurjchem-570	21	21	reported	report	VERB
eurjchem-570	21	22	for	for	ADP
eurjchem-570	21	23	the	the	DET
eurjchem-570	21	24	determination	determination	NOUN
eurjchem-570	21	25	of	of	ADP
eurjchem-570	21	26	the	the	DET
eurjchem-570	21	27	drug	drug	NOUN
eurjchem-570	21	28	.	.	PUNCT
eurjchem-570	22	1	metformin	metformin	NOUN
eurjchem-570	22	2	hydrochloride	hydrochloride	NOUN
eurjchem-570	22	3	(	(	PUNCT
eurjchem-570	22	4	met	meet	VERB
eurjchem-570	22	5	)	)	PUNCT
eurjchem-570	22	6	,	,	PUNCT
eurjchem-570	22	7	n	n	CCONJ
eurjchem-570	22	8	,	,	PUNCT
eurjchem-570	22	9	n‐dimethylimido‐	n‐dimethylimido‐	PRON
eurjchem-570	22	10	dicarbonimidic	dicarbonimidic	PROPN
eurjchem-570	22	11	diamide	diamide	NOUN
eurjchem-570	22	12	(	(	PUNCT
eurjchem-570	22	13	figure	figure	NOUN
eurjchem-570	22	14	1	1	NUM
eurjchem-570	22	15	)	)	PUNCT
eurjchem-570	22	16	,	,	PUNCT
eurjchem-570	22	17	is	be	AUX
eurjchem-570	22	18	a	a	DET
eurjchem-570	22	19	biguanide	biguanide	NOUN
eurjchem-570	22	20	hypoglycemic	hypoglycemic	ADJ
eurjchem-570	22	21	drug	drug	NOUN
eurjchem-570	22	22	that	that	PRON
eurjchem-570	22	23	is	be	AUX
eurjchem-570	22	24	regarded	regard	VERB
eurjchem-570	22	25	as	as	ADP
eurjchem-570	22	26	the	the	DET
eurjchem-570	22	27	main	main	ADJ
eurjchem-570	22	28	drug	drug	NOUN
eurjchem-570	22	29	in	in	ADP
eurjchem-570	22	30	mixed	mixed	ADJ
eurjchem-570	22	31	therapies	therapy	NOUN
eurjchem-570	22	32	of	of	ADP
eurjchem-570	22	33	oral	oral	ADJ
eurjchem-570	22	34	hypoglycemics	hypoglycemic	NOUN
eurjchem-570	22	35	.	.	PUNCT
eurjchem-570	23	1	literature	literature	NOUN
eurjchem-570	23	2	survey	survey	NOUN
eurjchem-570	23	3	reveals	reveal	VERB
eurjchem-570	23	4	that	that	SCONJ
eurjchem-570	23	5	some	some	DET
eurjchem-570	23	6	methods	method	NOUN
eurjchem-570	23	7	have	have	AUX
eurjchem-570	23	8	been	be	AUX
eurjchem-570	23	9	reported	report	VERB
eurjchem-570	23	10	for	for	ADP
eurjchem-570	23	11	determination	determination	NOUN
eurjchem-570	23	12	of	of	ADP
eurjchem-570	23	13	met	meet	VERB
eurjchem-570	23	14	in	in	ADP
eurjchem-570	23	15	mixtures	mixture	NOUN
eurjchem-570	23	16	including	include	VERB
eurjchem-570	23	17	lc	lc	PROPN
eurjchem-570	23	18	/	/	SYM
eurjchem-570	23	19	ms	ms	PROPN
eurjchem-570	23	20	/	/	SYM
eurjchem-570	23	21	ms	ms	NOUN
eurjchem-570	24	1	[	[	X
eurjchem-570	24	2	10	10	NUM
eurjchem-570	24	3	]	]	PUNCT
eurjchem-570	24	4	and	and	CCONJ
eurjchem-570	24	5	hplc	hplc	PROPN
eurjchem-570	25	1	[	[	X
eurjchem-570	25	2	11‐14	11‐14	NUM
eurjchem-570	25	3	]	]	PUNCT
eurjchem-570	25	4	.	.	PUNCT
eurjchem-570	26	1	due	due	ADP
eurjchem-570	26	2	to	to	ADP
eurjchem-570	26	3	the	the	DET
eurjchem-570	26	4	lack	lack	NOUN
eurjchem-570	26	5	of	of	ADP
eurjchem-570	26	6	reported	report	VERB
eurjchem-570	26	7	lc	lc	PROPN
eurjchem-570	26	8	methods	method	NOUN
eurjchem-570	26	9	describing	describe	VERB
eurjchem-570	26	10	determination	determination	NOUN
eurjchem-570	26	11	of	of	ADP
eurjchem-570	26	12	the	the	DET
eurjchem-570	26	13	mixtures	mixture	NOUN
eurjchem-570	26	14	under	under	ADP
eurjchem-570	26	15	investigation	investigation	NOUN
eurjchem-570	26	16	,	,	PUNCT
eurjchem-570	26	17	it	it	PRON
eurjchem-570	26	18	was	be	AUX
eurjchem-570	26	19	deemed	deem	VERB
eurjchem-570	26	20	useful	useful	ADJ
eurjchem-570	26	21	to	to	PART
eurjchem-570	26	22	develop	develop	VERB
eurjchem-570	26	23	simple	simple	ADJ
eurjchem-570	26	24	,	,	PUNCT
eurjchem-570	26	25	sensitive	sensitive	ADJ
eurjchem-570	26	26	and	and	CCONJ
eurjchem-570	26	27	selective	selective	ADJ
eurjchem-570	26	28	lc	lc	NOUN
eurjchem-570	26	29	method	method	NOUN
eurjchem-570	26	30	that	that	PRON
eurjchem-570	26	31	could	could	AUX
eurjchem-570	26	32	be	be	AUX
eurjchem-570	26	33	useful	useful	ADJ
eurjchem-570	26	34	for	for	ADP
eurjchem-570	26	35	the	the	DET
eurjchem-570	26	36	simultaneous	simultaneous	ADJ
eurjchem-570	26	37	determination	determination	NOUN
eurjchem-570	26	38	of	of	ADP
eurjchem-570	26	39	vdg	vdg	NOUN
eurjchem-570	26	40	and	and	CCONJ
eurjchem-570	26	41	met	meet	VERB
eurjchem-570	26	42	or	or	CCONJ
eurjchem-570	26	43	the	the	DET
eurjchem-570	26	44	simultaneous	simultaneous	ADJ
eurjchem-570	26	45	determination	determination	NOUN
eurjchem-570	26	46	of	of	ADP
eurjchem-570	26	47	sxg	sxg	NOUN
eurjchem-570	26	48	and	and	CCONJ
eurjchem-570	26	49	met	meet	VERB
eurjchem-570	26	50	.	.	PUNCT
eurjchem-570	27	1	the	the	DET
eurjchem-570	27	2	proposed	propose	VERB
eurjchem-570	27	3	method	method	NOUN
eurjchem-570	27	4	was	be	AUX
eurjchem-570	27	5	designed	design	VERB
eurjchem-570	27	6	to	to	PART
eurjchem-570	27	7	be	be	AUX
eurjchem-570	27	8	suitable	suitable	ADJ
eurjchem-570	27	9	for	for	ADP
eurjchem-570	27	10	the	the	DET
eurjchem-570	27	11	quality	quality	NOUN
eurjchem-570	27	12	assessment	assessment	NOUN
eurjchem-570	27	13	of	of	ADP
eurjchem-570	27	14	these	these	DET
eurjchem-570	27	15	mixtures	mixture	NOUN
eurjchem-570	27	16	in	in	ADP
eurjchem-570	27	17	pharmaceutical	pharmaceutical	ADJ
eurjchem-570	27	18	preparations	preparation	NOUN
eurjchem-570	27	19	.	.	PUNCT
eurjchem-570	28	1	(	(	PUNCT
eurjchem-570	28	2	a	a	X
eurjchem-570	28	3	)	)	PUNCT
eurjchem-570	28	4	(	(	PUNCT
eurjchem-570	28	5	b	b	X
eurjchem-570	28	6	)	)	PUNCT
eurjchem-570	28	7	(	(	PUNCT
eurjchem-570	28	8	c	c	X
eurjchem-570	28	9	)	)	PUNCT
eurjchem-570	28	10	figure	figure	NOUN
eurjchem-570	28	11	1	1	NUM
eurjchem-570	28	12	.	.	PUNCT
eurjchem-570	29	1	chemical	chemical	NOUN
eurjchem-570	29	2	structures	structure	NOUN
eurjchem-570	29	3	of	of	ADP
eurjchem-570	29	4	vildagliptin	vildagliptin	NOUN
eurjchem-570	29	5	(	(	PUNCT
eurjchem-570	29	6	a	a	NOUN
eurjchem-570	29	7	)	)	PUNCT
eurjchem-570	29	8	,	,	PUNCT
eurjchem-570	29	9	saxagliptin	saxagliptin	NOUN
eurjchem-570	29	10	(	(	PUNCT
eurjchem-570	29	11	b	b	NOUN
eurjchem-570	29	12	)	)	PUNCT
eurjchem-570	29	13	and	and	CCONJ
eurjchem-570	29	14	metformin	metformin	NOUN
eurjchem-570	29	15	(	(	PUNCT
eurjchem-570	29	16	c	c	NOUN
eurjchem-570	29	17	)	)	PUNCT
eurjchem-570	29	18	.	.	PUNCT
eurjchem-570	30	1	2	2	X
eurjchem-570	30	2	.	.	X
eurjchem-570	30	3	experimental	experimental	ADJ
eurjchem-570	30	4	2.1	2.1	NUM
eurjchem-570	30	5	.	.	PUNCT
eurjchem-570	31	1	instrumentation	instrumentation	NOUN
eurjchem-570	31	2	the	the	DET
eurjchem-570	31	3	hplc	hplc	NOUN
eurjchem-570	31	4	system	system	NOUN
eurjchem-570	31	5	consisted	consist	VERB
eurjchem-570	31	6	of	of	ADP
eurjchem-570	31	7	a	a	DET
eurjchem-570	31	8	schimadzu	schimadzu	NOUN
eurjchem-570	31	9	lc‐20	lc‐20	NOUN
eurjchem-570	31	10	at	at	ADP
eurjchem-570	31	11	liquid	liquid	ADJ
eurjchem-570	31	12	chromatograph	chromatograph	NOUN
eurjchem-570	31	13	(	(	PUNCT
eurjchem-570	31	14	japan	japan	PROPN
eurjchem-570	31	15	)	)	PUNCT
eurjchem-570	31	16	using	use	VERB
eurjchem-570	31	17	an	an	DET
eurjchem-570	31	18	inertsil	inertsil	NOUN
eurjchem-570	31	19	®	®	NOUN
eurjchem-570	31	20	cn‐3	cn‐3	NOUN
eurjchem-570	31	21	column	column	NOUN
eurjchem-570	31	22	(	(	PUNCT
eurjchem-570	31	23	250	250	NUM
eurjchem-570	31	24	mm	mm	NOUN
eurjchem-570	31	25	x	x	SYM
eurjchem-570	31	26	4.6	4.6	NUM
eurjchem-570	31	27	mm	mm	NOUN
eurjchem-570	31	28	,	,	PUNCT
eurjchem-570	31	29	5	5	NUM
eurjchem-570	31	30	µm	µm	NOUN
eurjchem-570	31	31	)	)	PUNCT
eurjchem-570	31	32	.	.	PUNCT
eurjchem-570	32	1	the	the	DET
eurjchem-570	32	2	system	system	NOUN
eurjchem-570	32	3	was	be	AUX
eurjchem-570	32	4	equipped	equip	VERB
eurjchem-570	32	5	with	with	ADP
eurjchem-570	32	6	a	a	DET
eurjchem-570	32	7	uv‐	uv‐	ADJ
eurjchem-570	32	8	visible	visible	ADJ
eurjchem-570	32	9	detector	detector	NOUN
eurjchem-570	32	10	(	(	PUNCT
eurjchem-570	32	11	spd‐20a	spd‐20a	PROPN
eurjchem-570	32	12	,	,	PUNCT
eurjchem-570	32	13	japan	japan	PROPN
eurjchem-570	32	14	)	)	PUNCT
eurjchem-570	32	15	and	and	CCONJ
eurjchem-570	32	16	an	an	DET
eurjchem-570	32	17	autosampler	autosampler	NOUN
eurjchem-570	32	18	(	(	PUNCT
eurjchem-570	32	19	sil‐20a	sil‐20a	PROPN
eurjchem-570	32	20	,	,	PUNCT
eurjchem-570	32	21	mohammad	mohammad	PROPN
eurjchem-570	32	22	et	et	PROPN
eurjchem-570	32	23	al	al	PROPN
eurjchem-570	32	24	.	.	PUNCT
eurjchem-570	32	25	/	/	SYM
eurjchem-570	32	26	european	european	PROPN
eurjchem-570	32	27	journal	journal	PROPN
eurjchem-570	32	28	of	of	ADP
eurjchem-570	32	29	chemistry	chemistry	NOUN
eurjchem-570	32	30	3	3	NUM
eurjchem-570	32	31	(	(	PUNCT
eurjchem-570	32	32	2	2	NUM
eurjchem-570	32	33	)	)	PUNCT
eurjchem-570	32	34	(	(	PUNCT
eurjchem-570	32	35	2012	2012	NUM
eurjchem-570	32	36	)	)	PUNCT
eurjchem-570	32	37	152‐155	152‐155	PROPN
eurjchem-570	32	38	153	153	NUM
eurjchem-570	32	39	schimadzu	schimadzu	NOUN
eurjchem-570	32	40	,	,	PUNCT
eurjchem-570	32	41	japan	japan	PROPN
eurjchem-570	32	42	)	)	PUNCT
eurjchem-570	32	43	.	.	PUNCT
eurjchem-570	33	1	an	an	PRON
eurjchem-570	33	2	elma	elma	PROPN
eurjchem-570	33	3	s100	s100	PROPN
eurjchem-570	33	4	ultrasonic	ultrasonic	ADJ
eurjchem-570	33	5	processor	processor	NOUN
eurjchem-570	33	6	model	model	NOUN
eurjchem-570	33	7	kbk	kbk	PROPN
eurjchem-570	33	8	4200	4200	NUM
eurjchem-570	33	9	(	(	PUNCT
eurjchem-570	33	10	germany	germany	PROPN
eurjchem-570	33	11	)	)	PUNCT
eurjchem-570	33	12	was	be	AUX
eurjchem-570	33	13	used	use	VERB
eurjchem-570	33	14	for	for	ADP
eurjchem-570	33	15	the	the	DET
eurjchem-570	33	16	degassing	degassing	NOUN
eurjchem-570	33	17	of	of	ADP
eurjchem-570	33	18	the	the	DET
eurjchem-570	33	19	mobile	mobile	ADJ
eurjchem-570	33	20	phases	phase	NOUN
eurjchem-570	33	21	.	.	PUNCT
eurjchem-570	34	1	2.2	2.2	NUM
eurjchem-570	34	2	.	.	PUNCT
eurjchem-570	34	3	reagents	reagent	NOUN
eurjchem-570	34	4	and	and	CCONJ
eurjchem-570	34	5	reference	reference	NOUN
eurjchem-570	34	6	samples	sample	VERB
eurjchem-570	34	7	pharmaceutical	pharmaceutical	ADJ
eurjchem-570	34	8	grade	grade	NOUN
eurjchem-570	34	9	vdg	vdg	NOUN
eurjchem-570	34	10	,	,	PUNCT
eurjchem-570	34	11	certified	certify	VERB
eurjchem-570	34	12	to	to	PART
eurjchem-570	34	13	contain	contain	VERB
eurjchem-570	34	14	99.70	99.70	NUM
eurjchem-570	34	15	%	%	NOUN
eurjchem-570	34	16	and	and	CCONJ
eurjchem-570	34	17	eucreas	eucreas	ADJ
eurjchem-570	34	18	®	®	NOUN
eurjchem-570	34	19	tablets	tablet	NOUN
eurjchem-570	34	20	,	,	PUNCT
eurjchem-570	34	21	nominally	nominally	ADV
eurjchem-570	34	22	containing	contain	VERB
eurjchem-570	34	23	50	50	NUM
eurjchem-570	34	24	mg	mg	NOUN
eurjchem-570	34	25	vdg	vdg	NOUN
eurjchem-570	34	26	and	and	CCONJ
eurjchem-570	34	27	500	500	NUM
eurjchem-570	34	28	mg	mg	NOUN
eurjchem-570	34	29	of	of	ADP
eurjchem-570	34	30	met	meet	VERB
eurjchem-570	34	31	per	per	ADP
eurjchem-570	34	32	tablet	tablet	NOUN
eurjchem-570	34	33	,	,	PUNCT
eurjchem-570	34	34	were	be	AUX
eurjchem-570	34	35	supplied	supply	VERB
eurjchem-570	34	36	from	from	ADP
eurjchem-570	34	37	novartis	novartis	PROPN
eurjchem-570	34	38	europharm	europharm	NOUN
eurjchem-570	34	39	limited	limit	VERB
eurjchem-570	34	40	company	company	NOUN
eurjchem-570	34	41	(	(	PUNCT
eurjchem-570	34	42	london	london	PROPN
eurjchem-570	34	43	,	,	PUNCT
eurjchem-570	34	44	united	united	ADJ
eurjchem-570	34	45	kingdom	kingdom	PROPN
eurjchem-570	34	46	)	)	PUNCT
eurjchem-570	34	47	.	.	PUNCT
eurjchem-570	35	1	pharmaceutical	pharmaceutical	PROPN
eurjchem-570	35	2	grade	grade	PROPN
eurjchem-570	35	3	sxg	sxg	NOUN
eurjchem-570	35	4	,	,	PUNCT
eurjchem-570	35	5	certified	certify	VERB
eurjchem-570	35	6	to	to	PART
eurjchem-570	35	7	contain	contain	VERB
eurjchem-570	35	8	99.85	99.85	NUM
eurjchem-570	35	9	%	%	NOUN
eurjchem-570	35	10	and	and	CCONJ
eurjchem-570	35	11	kombiglyze	kombiglyze	NOUN
eurjchem-570	35	12	®	®	NOUN
eurjchem-570	35	13	tablets	tablet	NOUN
eurjchem-570	35	14	,	,	PUNCT
eurjchem-570	35	15	nominally	nominally	ADV
eurjchem-570	35	16	containing	contain	VERB
eurjchem-570	35	17	5.58	5.58	NUM
eurjchem-570	35	18	mg	mg	NOUN
eurjchem-570	35	19	of	of	ADP
eurjchem-570	35	20	sxg	sxg	NOUN
eurjchem-570	35	21	and	and	CCONJ
eurjchem-570	35	22	500	500	NUM
eurjchem-570	35	23	mg	mg	NOUN
eurjchem-570	35	24	of	of	ADP
eurjchem-570	35	25	met	meet	VERB
eurjchem-570	35	26	per	per	ADP
eurjchem-570	35	27	tablet	tablet	NOUN
eurjchem-570	35	28	,	,	PUNCT
eurjchem-570	35	29	were	be	AUX
eurjchem-570	35	30	supplied	supply	VERB
eurjchem-570	35	31	by	by	ADP
eurjchem-570	35	32	bristol‐myers	bristol‐myer	NOUN
eurjchem-570	35	33	squibb/	squibb/	PROPN
eurjchem-570	35	34	astrazeneca	astrazeneca	NOUN
eurjchem-570	35	35	eeig	eeig	NOUN
eurjchem-570	35	36	(	(	PUNCT
eurjchem-570	35	37	united	united	ADJ
eurjchem-570	35	38	kingdom	kingdom	PROPN
eurjchem-570	35	39	)	)	PUNCT
eurjchem-570	35	40	.	.	PUNCT
eurjchem-570	36	1	pharmaceutical	pharmaceutical	PROPN
eurjchem-570	36	2	grade	grade	NOUN
eurjchem-570	36	3	met	meet	VERB
eurjchem-570	36	4	,	,	PUNCT
eurjchem-570	36	5	certified	certify	VERB
eurjchem-570	36	6	to	to	PART
eurjchem-570	36	7	contain	contain	VERB
eurjchem-570	36	8	99.79	99.79	NUM
eurjchem-570	36	9	%	%	NOUN
eurjchem-570	36	10	was	be	AUX
eurjchem-570	36	11	supplied	supply	VERB
eurjchem-570	36	12	by	by	ADP
eurjchem-570	36	13	chemical	chemical	NOUN
eurjchem-570	36	14	industries	industry	NOUN
eurjchem-570	36	15	development	development	NOUN
eurjchem-570	36	16	(	(	PUNCT
eurjchem-570	36	17	cid	cid	PROPN
eurjchem-570	36	18	)	)	PUNCT
eurjchem-570	36	19	co.	co.	PROPN
eurjchem-570	36	20	(	(	PUNCT
eurjchem-570	36	21	giza	giza	PROPN
eurjchem-570	36	22	,	,	PUNCT
eurjchem-570	36	23	egypt	egypt	PROPN
eurjchem-570	36	24	)	)	PUNCT
eurjchem-570	36	25	.	.	PUNCT
eurjchem-570	37	1	methanol	methanol	NOUN
eurjchem-570	37	2	(	(	PUNCT
eurjchem-570	37	3	hipersolv	hipersolv	NOUN
eurjchem-570	37	4	for	for	ADP
eurjchem-570	37	5	hplc	hplc	NOUN
eurjchem-570	37	6	)	)	PUNCT
eurjchem-570	37	7	,	,	PUNCT
eurjchem-570	37	8	acetonitrile	acetonitrile	NOUN
eurjchem-570	37	9	(	(	PUNCT
eurjchem-570	37	10	hipersolv	hipersolv	NOUN
eurjchem-570	37	11	)	)	PUNCT
eurjchem-570	37	12	,	,	PUNCT
eurjchem-570	37	13	potassium	potassium	NOUN
eurjchem-570	37	14	dihydrogen	dihydrogen	NOUN
eurjchem-570	37	15	phosphate	phosphate	NOUN
eurjchem-570	37	16	and	and	CCONJ
eurjchem-570	37	17	orthophosphoric	orthophosphoric	ADJ
eurjchem-570	37	18	acid	acid	NOUN
eurjchem-570	37	19	(	(	PUNCT
eurjchem-570	37	20	85	85	NUM
eurjchem-570	37	21	%	%	NOUN
eurjchem-570	37	22	)	)	PUNCT
eurjchem-570	37	23	were	be	AUX
eurjchem-570	37	24	obtained	obtain	VERB
eurjchem-570	37	25	from	from	ADP
eurjchem-570	37	26	vwr	vwr	PROPN
eurjchem-570	37	27	chemicals	chemical	NOUN
eurjchem-570	37	28	(	(	PUNCT
eurjchem-570	37	29	pool	pool	NOUN
eurjchem-570	37	30	,	,	PUNCT
eurjchem-570	37	31	england	england	PROPN
eurjchem-570	37	32	)	)	PUNCT
eurjchem-570	37	33	.	.	PUNCT
eurjchem-570	38	1	bi‐distilled	bi‐distille	VERB
eurjchem-570	38	2	water	water	NOUN
eurjchem-570	38	3	was	be	AUX
eurjchem-570	38	4	produced	produce	VERB
eurjchem-570	38	5	in‐house	in‐house	NOUN
eurjchem-570	38	6	(	(	PUNCT
eurjchem-570	38	7	aquatron	aquatron	VERB
eurjchem-570	38	8	water	water	NOUN
eurjchem-570	38	9	still	still	ADV
eurjchem-570	38	10	,	,	PUNCT
eurjchem-570	38	11	a4000d	a4000d	PROPN
eurjchem-570	38	12	,	,	PUNCT
eurjchem-570	38	13	uk	uk	PROPN
eurjchem-570	38	14	)	)	PUNCT
eurjchem-570	38	15	.	.	PUNCT
eurjchem-570	39	1	membrane	membrane	NOUN
eurjchem-570	39	2	filters	filter	NOUN
eurjchem-570	39	3	0.45	0.45	NUM
eurjchem-570	39	4	µm	µm	NOUN
eurjchem-570	39	5	from	from	ADP
eurjchem-570	39	6	teknokroma	teknokroma	NOUN
eurjchem-570	39	7	(	(	PUNCT
eurjchem-570	39	8	barcelona	barcelona	PROPN
eurjchem-570	39	9	,	,	PUNCT
eurjchem-570	39	10	spain	spain	PROPN
eurjchem-570	39	11	)	)	PUNCT
eurjchem-570	39	12	were	be	AUX
eurjchem-570	39	13	used	use	VERB
eurjchem-570	39	14	.	.	PUNCT
eurjchem-570	40	1	all	all	DET
eurjchem-570	40	2	other	other	ADJ
eurjchem-570	40	3	chemicals	chemical	NOUN
eurjchem-570	40	4	and	and	CCONJ
eurjchem-570	40	5	reagents	reagent	NOUN
eurjchem-570	40	6	used	use	VERB
eurjchem-570	40	7	were	be	AUX
eurjchem-570	40	8	of	of	ADP
eurjchem-570	40	9	analytical	analytical	ADJ
eurjchem-570	40	10	grade	grade	NOUN
eurjchem-570	40	11	unless	unless	SCONJ
eurjchem-570	40	12	indicated	indicate	VERB
eurjchem-570	40	13	otherwise	otherwise	ADV
eurjchem-570	40	14	.	.	PUNCT
eurjchem-570	41	1	standard	standard	ADJ
eurjchem-570	41	2	stock	stock	NOUN
eurjchem-570	41	3	solutions	solution	NOUN
eurjchem-570	41	4	of	of	ADP
eurjchem-570	41	5	each	each	DET
eurjchem-570	41	6	drug	drug	NOUN
eurjchem-570	41	7	(	(	PUNCT
eurjchem-570	41	8	1	1	NUM
eurjchem-570	41	9	mg	mg	NUM
eurjchem-570	41	10	/	/	SYM
eurjchem-570	41	11	ml	ml	NOUN
eurjchem-570	41	12	)	)	PUNCT
eurjchem-570	41	13	were	be	AUX
eurjchem-570	41	14	prepared	prepare	VERB
eurjchem-570	41	15	by	by	ADP
eurjchem-570	41	16	dissolving	dissolve	VERB
eurjchem-570	41	17	100	100	NUM
eurjchem-570	41	18	mg	mg	ADP
eurjchem-570	41	19	of	of	ADP
eurjchem-570	41	20	the	the	DET
eurjchem-570	41	21	drug	drug	NOUN
eurjchem-570	41	22	in	in	ADP
eurjchem-570	41	23	methanol	methanol	NOUN
eurjchem-570	41	24	in	in	ADP
eurjchem-570	41	25	a	a	DET
eurjchem-570	41	26	100	100	NUM
eurjchem-570	41	27	ml	ml	NOUN
eurjchem-570	41	28	volumetric	volumetric	ADJ
eurjchem-570	41	29	flask	flask	NOUN
eurjchem-570	41	30	and	and	CCONJ
eurjchem-570	41	31	then	then	ADV
eurjchem-570	41	32	completed	complete	VERB
eurjchem-570	41	33	to	to	PART
eurjchem-570	41	34	volume	volume	VERB
eurjchem-570	41	35	with	with	ADP
eurjchem-570	41	36	methanol	methanol	NOUN
eurjchem-570	41	37	.	.	PUNCT
eurjchem-570	42	1	then	then	ADV
eurjchem-570	42	2	required	require	VERB
eurjchem-570	42	3	concentrations	concentration	NOUN
eurjchem-570	42	4	were	be	AUX
eurjchem-570	42	5	prepared	prepare	VERB
eurjchem-570	42	6	by	by	ADP
eurjchem-570	42	7	serial	serial	ADJ
eurjchem-570	42	8	dilutions	dilution	NOUN
eurjchem-570	42	9	with	with	ADP
eurjchem-570	42	10	methanol	methanol	NOUN
eurjchem-570	42	11	of	of	ADP
eurjchem-570	42	12	these	these	DET
eurjchem-570	42	13	stock	stock	NOUN
eurjchem-570	42	14	solutions	solution	NOUN
eurjchem-570	42	15	.	.	PUNCT
eurjchem-570	43	1	2.3	2.3	NUM
eurjchem-570	43	2	.	.	PUNCT
eurjchem-570	43	3	chromatographic	chromatographic	ADJ
eurjchem-570	43	4	conditions	condition	NOUN
eurjchem-570	43	5	chromatographic	chromatographic	ADJ
eurjchem-570	43	6	separation	separation	NOUN
eurjchem-570	43	7	was	be	AUX
eurjchem-570	43	8	achieved	achieve	VERB
eurjchem-570	43	9	on	on	ADP
eurjchem-570	43	10	an	an	DET
eurjchem-570	43	11	inertsil	inertsil	NOUN
eurjchem-570	43	12	®	®	NOUN
eurjchem-570	43	13	cn‐3	cn‐3	NOUN
eurjchem-570	43	14	column	column	NOUN
eurjchem-570	43	15	(	(	PUNCT
eurjchem-570	43	16	250	250	NUM
eurjchem-570	43	17	mm	mm	NOUN
eurjchem-570	43	18	x	x	SYM
eurjchem-570	43	19	4.6	4.6	NUM
eurjchem-570	43	20	mm	mm	NOUN
eurjchem-570	43	21	,	,	PUNCT
eurjchem-570	43	22	5	5	NUM
eurjchem-570	43	23	µm	µm	NOUN
eurjchem-570	43	24	)	)	PUNCT
eurjchem-570	43	25	.	.	PUNCT
eurjchem-570	44	1	isocratic	isocratic	ADJ
eurjchem-570	44	2	elution	elution	NOUN
eurjchem-570	44	3	using	use	VERB
eurjchem-570	44	4	a	a	DET
eurjchem-570	44	5	mobile	mobile	ADJ
eurjchem-570	44	6	phase	phase	NOUN
eurjchem-570	44	7	consisting	consist	VERB
eurjchem-570	44	8	of	of	ADP
eurjchem-570	44	9	potassium	potassium	NOUN
eurjchem-570	44	10	dihydrogen	dihydrogen	NOUN
eurjchem-570	44	11	phosphate	phosphate	NOUN
eurjchem-570	44	12	buffer	buffer	NOUN
eurjchem-570	44	13	ph	ph	NOUN
eurjchem-570	44	14	(	(	PUNCT
eurjchem-570	44	15	4.6	4.6	NUM
eurjchem-570	44	16	)	)	PUNCT
eurjchem-570	44	17	‐	‐	ADJ
eurjchem-570	44	18	acetonitrile	acetonitrile	NOUN
eurjchem-570	44	19	(	(	PUNCT
eurjchem-570	44	20	15:85	15:85	NUM
eurjchem-570	44	21	,	,	PUNCT
eurjchem-570	44	22	v	v	NOUN
eurjchem-570	44	23	:	:	SYM
eurjchem-570	44	24	v	v	NOUN
eurjchem-570	44	25	)	)	PUNCT
eurjchem-570	44	26	with	with	ADP
eurjchem-570	44	27	uv	uv	NOUN
eurjchem-570	44	28	detection	detection	NOUN
eurjchem-570	44	29	at	at	ADP
eurjchem-570	44	30	208	208	NUM
eurjchem-570	44	31	nm	nm	NOUN
eurjchem-570	44	32	was	be	AUX
eurjchem-570	44	33	performed	perform	VERB
eurjchem-570	44	34	.	.	PUNCT
eurjchem-570	45	1	the	the	DET
eurjchem-570	45	2	buffer	buffer	NOUN
eurjchem-570	45	3	solution	solution	NOUN
eurjchem-570	45	4	was	be	AUX
eurjchem-570	45	5	filtered	filter	VERB
eurjchem-570	45	6	through	through	ADP
eurjchem-570	45	7	0.45	0.45	NUM
eurjchem-570	45	8	µm	µm	ADP
eurjchem-570	45	9	membrane	membrane	NOUN
eurjchem-570	45	10	filter	filter	NOUN
eurjchem-570	45	11	and	and	CCONJ
eurjchem-570	45	12	degassed	degas	VERB
eurjchem-570	45	13	for	for	ADP
eurjchem-570	45	14	30	30	NUM
eurjchem-570	45	15	min	min	NOUN
eurjchem-570	45	16	in	in	ADP
eurjchem-570	45	17	an	an	DET
eurjchem-570	45	18	ultrasonic	ultrasonic	ADJ
eurjchem-570	45	19	bath	bath	NOUN
eurjchem-570	45	20	prior	prior	ADV
eurjchem-570	45	21	to	to	ADP
eurjchem-570	45	22	use	use	NOUN
eurjchem-570	45	23	.	.	PUNCT
eurjchem-570	46	1	the	the	DET
eurjchem-570	46	2	mobile	mobile	ADJ
eurjchem-570	46	3	phase	phase	NOUN
eurjchem-570	46	4	was	be	AUX
eurjchem-570	46	5	pumped	pump	VERB
eurjchem-570	46	6	through	through	ADP
eurjchem-570	46	7	the	the	DET
eurjchem-570	46	8	column	column	NOUN
eurjchem-570	46	9	at	at	ADP
eurjchem-570	46	10	a	a	DET
eurjchem-570	46	11	flow	flow	NOUN
eurjchem-570	46	12	rate	rate	NOUN
eurjchem-570	46	13	of	of	ADP
eurjchem-570	46	14	1	1	NUM
eurjchem-570	46	15	ml	ml	NOUN
eurjchem-570	46	16	/	/	SYM
eurjchem-570	46	17	min	min	NOUN
eurjchem-570	46	18	.	.	PROPN
eurjchem-570	46	19	analyses	analysis	NOUN
eurjchem-570	46	20	were	be	AUX
eurjchem-570	46	21	performed	perform	VERB
eurjchem-570	46	22	at	at	ADP
eurjchem-570	46	23	ambient	ambient	ADJ
eurjchem-570	46	24	temperature	temperature	NOUN
eurjchem-570	46	25	and	and	CCONJ
eurjchem-570	46	26	the	the	DET
eurjchem-570	46	27	injection	injection	NOUN
eurjchem-570	46	28	volume	volume	NOUN
eurjchem-570	46	29	was	be	AUX
eurjchem-570	46	30	25	25	NUM
eurjchem-570	46	31	µl	µl	NOUN
eurjchem-570	46	32	.	.	PUNCT
eurjchem-570	47	1	2.4	2.4	NUM
eurjchem-570	47	2	.	.	PUNCT
eurjchem-570	48	1	samples	sample	NOUN
eurjchem-570	48	2	’	'	PUNCT
eurjchem-570	48	3	preparation	preparation	NOUN
eurjchem-570	48	4	twenty	twenty	NUM
eurjchem-570	48	5	tablets	tablet	NOUN
eurjchem-570	48	6	of	of	ADP
eurjchem-570	48	7	each	each	DET
eurjchem-570	48	8	mixture	mixture	NOUN
eurjchem-570	48	9	were	be	AUX
eurjchem-570	48	10	weighed	weigh	VERB
eurjchem-570	48	11	.	.	PUNCT
eurjchem-570	49	1	an	an	DET
eurjchem-570	49	2	accurately	accurately	ADV
eurjchem-570	49	3	weighed	weigh	VERB
eurjchem-570	49	4	amount	amount	NOUN
eurjchem-570	49	5	of	of	ADP
eurjchem-570	49	6	the	the	DET
eurjchem-570	49	7	finely	finely	ADV
eurjchem-570	49	8	powdered	powder	VERB
eurjchem-570	49	9	eucreas	eucreas	ADJ
eurjchem-570	49	10	®	®	NOUN
eurjchem-570	49	11	tablets	tablet	NOUN
eurjchem-570	49	12	equivalent	equivalent	ADJ
eurjchem-570	49	13	to	to	ADP
eurjchem-570	49	14	100	100	NUM
eurjchem-570	49	15	mg	mg	ADP
eurjchem-570	49	16	of	of	ADP
eurjchem-570	49	17	vdg	vdg	NOUN
eurjchem-570	49	18	and	and	CCONJ
eurjchem-570	49	19	1000	1000	NUM
eurjchem-570	49	20	mg	mg	NOUN
eurjchem-570	49	21	of	of	ADP
eurjchem-570	49	22	met	meet	VERB
eurjchem-570	49	23	was	be	AUX
eurjchem-570	49	24	made	make	VERB
eurjchem-570	49	25	up	up	ADP
eurjchem-570	49	26	to	to	PART
eurjchem-570	49	27	100	100	NUM
eurjchem-570	49	28	ml	ml	NOUN
eurjchem-570	49	29	with	with	ADP
eurjchem-570	49	30	methanol	methanol	NOUN
eurjchem-570	49	31	.	.	PUNCT
eurjchem-570	50	1	an	an	DET
eurjchem-570	50	2	accurately	accurately	ADV
eurjchem-570	50	3	weighed	weigh	VERB
eurjchem-570	50	4	amount	amount	NOUN
eurjchem-570	50	5	of	of	ADP
eurjchem-570	50	6	the	the	DET
eurjchem-570	50	7	finely	finely	ADV
eurjchem-570	50	8	powdered	powdered	ADJ
eurjchem-570	50	9	kombiglyze	kombiglyze	NOUN
eurjchem-570	50	10	®	®	NOUN
eurjchem-570	50	11	tablets	tablet	NOUN
eurjchem-570	50	12	equivalent	equivalent	ADJ
eurjchem-570	50	13	to	to	ADP
eurjchem-570	50	14	11.16	11.16	NUM
eurjchem-570	50	15	mg	mg	NOUN
eurjchem-570	50	16	of	of	ADP
eurjchem-570	50	17	sxg	sxg	NOUN
eurjchem-570	50	18	and	and	CCONJ
eurjchem-570	50	19	1000	1000	NUM
eurjchem-570	50	20	mg	mg	NOUN
eurjchem-570	50	21	of	of	ADP
eurjchem-570	50	22	met	meet	VERB
eurjchem-570	50	23	were	be	AUX
eurjchem-570	50	24	made	make	VERB
eurjchem-570	50	25	up	up	ADP
eurjchem-570	50	26	to	to	PART
eurjchem-570	50	27	100	100	NUM
eurjchem-570	50	28	ml	ml	NOUN
eurjchem-570	50	29	with	with	ADP
eurjchem-570	50	30	methanol	methanol	NOUN
eurjchem-570	50	31	.	.	PUNCT
eurjchem-570	51	1	the	the	DET
eurjchem-570	51	2	solutions	solution	NOUN
eurjchem-570	51	3	were	be	AUX
eurjchem-570	51	4	filtered	filter	VERB
eurjchem-570	51	5	followed	follow	VERB
eurjchem-570	51	6	by	by	ADP
eurjchem-570	51	7	serial	serial	ADJ
eurjchem-570	51	8	dilution	dilution	NOUN
eurjchem-570	51	9	to	to	ADP
eurjchem-570	51	10	the	the	DET
eurjchem-570	51	11	required	require	VERB
eurjchem-570	51	12	concentrations	concentration	NOUN
eurjchem-570	51	13	for	for	ADP
eurjchem-570	51	14	each	each	DET
eurjchem-570	51	15	experiment	experiment	NOUN
eurjchem-570	51	16	.	.	PUNCT
eurjchem-570	52	1	2.5	2.5	NUM
eurjchem-570	52	2	.	.	PUNCT
eurjchem-570	52	3	procedure	procedure	NOUN
eurjchem-570	52	4	2.5.1	2.5.1	NUM
eurjchem-570	52	5	.	.	PUNCT
eurjchem-570	53	1	linearity	linearity	NOUN
eurjchem-570	53	2	and	and	CCONJ
eurjchem-570	53	3	repeatability	repeatability	NOUN
eurjchem-570	53	4	accurately	accurately	ADV
eurjchem-570	53	5	measured	measure	VERB
eurjchem-570	53	6	aliquots	aliquot	NOUN
eurjchem-570	53	7	of	of	ADP
eurjchem-570	53	8	working	work	VERB
eurjchem-570	53	9	standard	standard	ADJ
eurjchem-570	53	10	solutions	solution	NOUN
eurjchem-570	53	11	equivalent	equivalent	ADJ
eurjchem-570	53	12	to	to	ADP
eurjchem-570	53	13	50‐2000	50‐2000	NUM
eurjchem-570	53	14	µg	µg	CCONJ
eurjchem-570	53	15	vlg	vlg	PROPN
eurjchem-570	53	16	,	,	PUNCT
eurjchem-570	53	17	5.0‐200.0	5.0‐200.0	NUM
eurjchem-570	53	18	µg	µg	X
eurjchem-570	53	19	sxg	sxg	NOUN
eurjchem-570	54	1	and	and	CCONJ
eurjchem-570	54	2	0.5‐20.0	0.5‐20.0	ADJ
eurjchem-570	54	3	mg	mg	PROPN
eurjchem-570	54	4	met	meet	VERB
eurjchem-570	54	5	were	be	AUX
eurjchem-570	54	6	separately	separately	ADV
eurjchem-570	54	7	transferred	transfer	VERB
eurjchem-570	54	8	into	into	ADP
eurjchem-570	54	9	two	two	NUM
eurjchem-570	54	10	series	series	NOUN
eurjchem-570	54	11	of	of	ADP
eurjchem-570	54	12	10	10	NUM
eurjchem-570	54	13	ml	ml	NOUN
eurjchem-570	54	14	volumetric	volumetric	ADJ
eurjchem-570	54	15	flasks	flask	NOUN
eurjchem-570	54	16	and	and	CCONJ
eurjchem-570	54	17	then	then	ADV
eurjchem-570	54	18	completed	complete	VERB
eurjchem-570	54	19	to	to	PART
eurjchem-570	54	20	volume	volume	VERB
eurjchem-570	54	21	with	with	ADP
eurjchem-570	54	22	methanol	methanol	NOUN
eurjchem-570	54	23	.	.	PUNCT
eurjchem-570	55	1	a	a	DET
eurjchem-570	55	2	volume	volume	NOUN
eurjchem-570	55	3	of	of	ADP
eurjchem-570	55	4	25	25	NUM
eurjchem-570	55	5	µl	µl	NOUN
eurjchem-570	55	6	of	of	ADP
eurjchem-570	55	7	each	each	DET
eurjchem-570	55	8	solution	solution	NOUN
eurjchem-570	55	9	was	be	AUX
eurjchem-570	55	10	injected	inject	VERB
eurjchem-570	55	11	into	into	ADP
eurjchem-570	55	12	the	the	DET
eurjchem-570	55	13	chromatograph	chromatograph	NOUN
eurjchem-570	55	14	.	.	PUNCT
eurjchem-570	56	1	the	the	DET
eurjchem-570	56	2	chromatographic	chromatographic	ADJ
eurjchem-570	56	3	conditions	condition	NOUN
eurjchem-570	56	4	mentioned	mention	VERB
eurjchem-570	56	5	in	in	ADP
eurjchem-570	56	6	section	section	NOUN
eurjchem-570	56	7	2.3	2.3	NUM
eurjchem-570	56	8	.	.	PUNCT
eurjchem-570	56	9	including	include	VERB
eurjchem-570	56	10	the	the	DET
eurjchem-570	56	11	mobile	mobile	ADJ
eurjchem-570	56	12	phase	phase	NOUN
eurjchem-570	56	13	at	at	ADP
eurjchem-570	56	14	a	a	DET
eurjchem-570	56	15	flow	flow	NOUN
eurjchem-570	56	16	rate	rate	NOUN
eurjchem-570	56	17	1	1	NUM
eurjchem-570	56	18	ml	ml	NOUN
eurjchem-570	56	19	/	/	SYM
eurjchem-570	56	20	min	min	NOUN
eurjchem-570	56	21	,	,	PUNCT
eurjchem-570	56	22	detection	detection	NOUN
eurjchem-570	56	23	at	at	ADP
eurjchem-570	56	24	208	208	NUM
eurjchem-570	56	25	nm	nm	NOUN
eurjchem-570	56	26	and	and	CCONJ
eurjchem-570	56	27	run	run	VERB
eurjchem-570	56	28	time	time	NOUN
eurjchem-570	56	29	program	program	NOUN
eurjchem-570	56	30	for	for	ADP
eurjchem-570	56	31	12.5	12.5	NUM
eurjchem-570	56	32	min	min	NOUN
eurjchem-570	56	33	were	be	AUX
eurjchem-570	56	34	adjusted	adjust	VERB
eurjchem-570	56	35	.	.	PUNCT
eurjchem-570	57	1	a	a	DET
eurjchem-570	57	2	calibration	calibration	NOUN
eurjchem-570	57	3	curve	curve	NOUN
eurjchem-570	57	4	for	for	ADP
eurjchem-570	57	5	each	each	DET
eurjchem-570	57	6	drug	drug	NOUN
eurjchem-570	57	7	was	be	AUX
eurjchem-570	57	8	obtained	obtain	VERB
eurjchem-570	57	9	by	by	ADP
eurjchem-570	57	10	plotting	plot	VERB
eurjchem-570	57	11	area	area	NOUN
eurjchem-570	57	12	under	under	ADP
eurjchem-570	57	13	the	the	DET
eurjchem-570	57	14	peak	peak	NOUN
eurjchem-570	57	15	(	(	PUNCT
eurjchem-570	57	16	aup	aup	PROPN
eurjchem-570	57	17	)	)	PUNCT
eurjchem-570	57	18	against	against	ADP
eurjchem-570	57	19	concentration	concentration	NOUN
eurjchem-570	57	20	(	(	PUNCT
eurjchem-570	57	21	c	c	NOUN
eurjchem-570	57	22	)	)	PUNCT
eurjchem-570	57	23	.	.	PUNCT
eurjchem-570	58	1	the	the	DET
eurjchem-570	58	2	repeatability	repeatability	NOUN
eurjchem-570	58	3	of	of	ADP
eurjchem-570	58	4	the	the	DET
eurjchem-570	58	5	method	method	NOUN
eurjchem-570	58	6	was	be	AUX
eurjchem-570	58	7	assessed	assess	VERB
eurjchem-570	58	8	by	by	ADP
eurjchem-570	58	9	analyzing	analyze	VERB
eurjchem-570	58	10	a	a	DET
eurjchem-570	58	11	mixture	mixture	NOUN
eurjchem-570	58	12	containing	contain	VERB
eurjchem-570	58	13	100	100	NUM
eurjchem-570	58	14	µg	µg	NOUN
eurjchem-570	58	15	/	/	SYM
eurjchem-570	58	16	ml	ml	NOUN
eurjchem-570	58	17	of	of	ADP
eurjchem-570	58	18	vdg	vdg	NOUN
eurjchem-570	58	19	and	and	CCONJ
eurjchem-570	58	20	1000	1000	NUM
eurjchem-570	58	21	µg	µg	NOUN
eurjchem-570	58	22	/	/	SYM
eurjchem-570	58	23	ml	ml	NOUN
eurjchem-570	58	24	of	of	ADP
eurjchem-570	58	25	met	meet	VERB
eurjchem-570	58	26	,	,	PUNCT
eurjchem-570	58	27	and	and	CCONJ
eurjchem-570	58	28	another	another	DET
eurjchem-570	58	29	mixture	mixture	NOUN
eurjchem-570	58	30	containing	contain	VERB
eurjchem-570	58	31	11.16	11.16	NUM
eurjchem-570	58	32	µg	µg	NOUN
eurjchem-570	58	33	/	/	SYM
eurjchem-570	58	34	ml	ml	NOUN
eurjchem-570	58	35	of	of	ADP
eurjchem-570	58	36	sxg	sxg	NOUN
eurjchem-570	58	37	and	and	CCONJ
eurjchem-570	58	38	1000	1000	NUM
eurjchem-570	58	39	µg	µg	NOUN
eurjchem-570	58	40	/	/	SYM
eurjchem-570	58	41	ml	ml	NOUN
eurjchem-570	58	42	of	of	ADP
eurjchem-570	58	43	met	meet	VERB
eurjchem-570	58	44	(	(	PUNCT
eurjchem-570	58	45	n	n	NOUN
eurjchem-570	58	46	=	=	SYM
eurjchem-570	58	47	6	6	NUM
eurjchem-570	58	48	)	)	PUNCT
eurjchem-570	58	49	.	.	PUNCT
eurjchem-570	59	1	the	the	DET
eurjchem-570	59	2	%	%	NOUN
eurjchem-570	59	3	r.s.d	r.s.d	NOUN
eurjchem-570	59	4	.	.	PUNCT
eurjchem-570	60	1	for	for	ADP
eurjchem-570	60	2	the	the	DET
eurjchem-570	60	3	peak	peak	NOUN
eurjchem-570	60	4	area	area	NOUN
eurjchem-570	60	5	and	and	CCONJ
eurjchem-570	60	6	retention	retention	NOUN
eurjchem-570	60	7	time	time	NOUN
eurjchem-570	60	8	was	be	AUX
eurjchem-570	60	9	calculated	calculate	VERB
eurjchem-570	60	10	(	(	PUNCT
eurjchem-570	60	11	table	table	NOUN
eurjchem-570	60	12	1	1	NUM
eurjchem-570	60	13	and	and	CCONJ
eurjchem-570	60	14	2	2	NUM
eurjchem-570	60	15	)	)	PUNCT
eurjchem-570	60	16	.	.	PUNCT
eurjchem-570	61	1	table	table	NOUN
eurjchem-570	61	2	1	1	NUM
eurjchem-570	61	3	.	.	PUNCT
eurjchem-570	61	4	system	system	NOUN
eurjchem-570	61	5	suitability	suitability	NOUN
eurjchem-570	61	6	test	test	NOUN
eurjchem-570	61	7	for	for	ADP
eurjchem-570	61	8	the	the	DET
eurjchem-570	61	9	proposed	propose	VERB
eurjchem-570	61	10	lc	lc	NOUN
eurjchem-570	61	11	method	method	NOUN
eurjchem-570	61	12	for	for	ADP
eurjchem-570	61	13	the	the	DET
eurjchem-570	61	14	determination	determination	NOUN
eurjchem-570	61	15	of	of	ADP
eurjchem-570	61	16	vildagliptin	vildagliptin	NOUN
eurjchem-570	61	17	in	in	ADP
eurjchem-570	61	18	binary	binary	ADJ
eurjchem-570	61	19	mixture	mixture	NOUN
eurjchem-570	61	20	with	with	ADP
eurjchem-570	61	21	metformin	metformin	NOUN
eurjchem-570	61	22	.	.	PUNCT
eurjchem-570	62	1	item	item	PROPN
eurjchem-570	62	2	vdg	vdg	PROPN
eurjchem-570	62	3	met	meet	VERB
eurjchem-570	62	4	n	n	PRON
eurjchem-570	62	5	2135	2135	NUM
eurjchem-570	62	6	2975	2975	NUM
eurjchem-570	62	7	r	r	NOUN
eurjchem-570	62	8	3.1	3.1	NUM
eurjchem-570	62	9	3.1	3.1	NUM
eurjchem-570	62	10	t	t	NOUN
eurjchem-570	62	11	1.02	1.02	NUM
eurjchem-570	62	12	1.10	1.10	NUM
eurjchem-570	62	13	rsd%	rsd%	NOUN
eurjchem-570	62	14	of	of	ADP
eurjchem-570	62	15	peak	peak	NOUN
eurjchem-570	62	16	area	area	NOUN
eurjchem-570	62	17	(	(	PUNCT
eurjchem-570	62	18	6	6	NUM
eurjchem-570	62	19	injections	injection	NOUN
eurjchem-570	62	20	)	)	PUNCT
eurjchem-570	62	21	0.57	0.57	NUM
eurjchem-570	62	22	0.69	0.69	NUM
eurjchem-570	62	23	rsd%	rsd%	NOUN
eurjchem-570	62	24	of	of	ADP
eurjchem-570	62	25	retention	retention	NOUN
eurjchem-570	62	26	time	time	NOUN
eurjchem-570	62	27	(	(	PUNCT
eurjchem-570	62	28	6	6	NUM
eurjchem-570	62	29	injections	injection	NOUN
eurjchem-570	62	30	)	)	PUNCT
eurjchem-570	62	31	0.16	0.16	NUM
eurjchem-570	62	32	0.28	0.28	NUM
eurjchem-570	62	33	table	table	NOUN
eurjchem-570	62	34	2	2	NUM
eurjchem-570	62	35	.	.	PUNCT
eurjchem-570	62	36	system	system	NOUN
eurjchem-570	62	37	suitability	suitability	NOUN
eurjchem-570	62	38	test	test	NOUN
eurjchem-570	62	39	for	for	ADP
eurjchem-570	62	40	the	the	DET
eurjchem-570	62	41	proposed	propose	VERB
eurjchem-570	62	42	lc	lc	NOUN
eurjchem-570	62	43	method	method	NOUN
eurjchem-570	62	44	for	for	ADP
eurjchem-570	62	45	the	the	DET
eurjchem-570	62	46	determination	determination	NOUN
eurjchem-570	62	47	of	of	ADP
eurjchem-570	62	48	saxagliptin	saxagliptin	NOUN
eurjchem-570	62	49	in	in	ADP
eurjchem-570	62	50	binary	binary	ADJ
eurjchem-570	62	51	mixture	mixture	NOUN
eurjchem-570	62	52	with	with	ADP
eurjchem-570	62	53	metformin	metformin	PROPN
eurjchem-570	62	54	.	.	PUNCT
eurjchem-570	63	1	item	item	PROPN
eurjchem-570	63	2	sxg	sxg	PROPN
eurjchem-570	63	3	met	meet	VERB
eurjchem-570	63	4	n	n	PROPN
eurjchem-570	63	5	1811	1811	NUM
eurjchem-570	63	6	2835	2835	NUM
eurjchem-570	63	7	r	r	NOUN
eurjchem-570	63	8	3.9	3.9	NUM
eurjchem-570	63	9	3.9	3.9	NUM
eurjchem-570	63	10	t	t	NOUN
eurjchem-570	63	11	1.00	1.00	NUM
eurjchem-570	63	12	1.09	1.09	NUM
eurjchem-570	63	13	rsd%	rsd%	NOUN
eurjchem-570	63	14	of	of	ADP
eurjchem-570	63	15	peak	peak	NOUN
eurjchem-570	63	16	area	area	NOUN
eurjchem-570	63	17	(	(	PUNCT
eurjchem-570	63	18	6	6	NUM
eurjchem-570	63	19	injections	injection	NOUN
eurjchem-570	63	20	)	)	PUNCT
eurjchem-570	63	21	0.71	0.71	NUM
eurjchem-570	63	22	0.62	0.62	NUM
eurjchem-570	63	23	rsd%	rsd%	NOUN
eurjchem-570	63	24	of	of	ADP
eurjchem-570	63	25	retention	retention	NOUN
eurjchem-570	63	26	time	time	NOUN
eurjchem-570	63	27	(	(	PUNCT
eurjchem-570	63	28	6	6	NUM
eurjchem-570	63	29	injections	injection	NOUN
eurjchem-570	63	30	)	)	PUNCT
eurjchem-570	63	31	0.28	0.28	NUM
eurjchem-570	63	32	0.19	0.19	NUM
eurjchem-570	63	33	2.5.2	2.5.2	NUM
eurjchem-570	63	34	.	.	PUNCT
eurjchem-570	64	1	assay	assay	NOUN
eurjchem-570	64	2	of	of	ADP
eurjchem-570	64	3	drugs	drug	NOUN
eurjchem-570	64	4	in	in	ADP
eurjchem-570	64	5	laboratory	laboratory	NOUN
eurjchem-570	64	6	prepared	prepare	VERB
eurjchem-570	64	7	mixtures	mixture	NOUN
eurjchem-570	64	8	and	and	CCONJ
eurjchem-570	64	9	in	in	ADP
eurjchem-570	64	10	pharmaceutical	pharmaceutical	ADJ
eurjchem-570	64	11	preparations	preparation	NOUN
eurjchem-570	64	12	the	the	DET
eurjchem-570	64	13	procedure	procedure	NOUN
eurjchem-570	64	14	mentioned	mention	VERB
eurjchem-570	64	15	in	in	ADP
eurjchem-570	64	16	section	section	NOUN
eurjchem-570	64	17	2.5.1	2.5.1	NUM
eurjchem-570	64	18	was	be	AUX
eurjchem-570	64	19	repeated	repeat	VERB
eurjchem-570	64	20	using	use	VERB
eurjchem-570	64	21	two	two	NUM
eurjchem-570	64	22	sets	set	NOUN
eurjchem-570	64	23	of	of	ADP
eurjchem-570	64	24	laboratory	laboratory	NOUN
eurjchem-570	64	25	prepared	prepare	VERB
eurjchem-570	64	26	mixtures	mixture	NOUN
eurjchem-570	64	27	equivalent	equivalent	ADJ
eurjchem-570	64	28	to	to	ADP
eurjchem-570	64	29	100‐1450	100‐1450	NUM
eurjchem-570	64	30	µg	µg	VERB
eurjchem-570	64	31	/	/	SYM
eurjchem-570	64	32	ml	ml	VERB
eurjchem-570	64	33	met	meet	VERB
eurjchem-570	64	34	with	with	ADP
eurjchem-570	64	35	10‐145	10‐145	NUM
eurjchem-570	64	36	µg	µg	NOUN
eurjchem-570	64	37	/	/	SYM
eurjchem-570	64	38	ml	ml	ADP
eurjchem-570	64	39	vlg	vlg	NOUN
eurjchem-570	64	40	and	and	CCONJ
eurjchem-570	64	41	2‐13	2‐13	NUM
eurjchem-570	64	42	µg	µg	ADV
eurjchem-570	64	43	/	/	SYM
eurjchem-570	64	44	ml	ml	NOUN
eurjchem-570	64	45	sxg	sxg	NOUN
eurjchem-570	64	46	in	in	ADP
eurjchem-570	64	47	different	different	ADJ
eurjchem-570	64	48	concentration	concentration	NOUN
eurjchem-570	64	49	ratios	ratio	NOUN
eurjchem-570	64	50	.	.	PUNCT
eurjchem-570	65	1	for	for	ADP
eurjchem-570	65	2	the	the	DET
eurjchem-570	65	3	determination	determination	NOUN
eurjchem-570	65	4	of	of	ADP
eurjchem-570	65	5	the	the	DET
eurjchem-570	65	6	examined	examine	VERB
eurjchem-570	65	7	drugs	drug	NOUN
eurjchem-570	65	8	in	in	ADP
eurjchem-570	65	9	eucreas	eucreas	ADJ
eurjchem-570	65	10	®	®	NOUN
eurjchem-570	65	11	and	and	CCONJ
eurjchem-570	65	12	kombiglyze	kombiglyze	VERB
eurjchem-570	65	13	®	®	NOUN
eurjchem-570	65	14	tablets	tablet	NOUN
eurjchem-570	65	15	,	,	PUNCT
eurjchem-570	65	16	the	the	DET
eurjchem-570	65	17	samples	sample	NOUN
eurjchem-570	65	18	’	'	PUNCT
eurjchem-570	65	19	solutions	solution	NOUN
eurjchem-570	65	20	prepared	prepare	VERB
eurjchem-570	65	21	in	in	ADP
eurjchem-570	65	22	section	section	NOUN
eurjchem-570	65	23	2.4	2.4	NUM
eurjchem-570	65	24	were	be	AUX
eurjchem-570	65	25	serially	serially	ADV
eurjchem-570	65	26	diluted	dilute	VERB
eurjchem-570	65	27	to	to	PART
eurjchem-570	65	28	prepare	prepare	VERB
eurjchem-570	65	29	solutions	solution	NOUN
eurjchem-570	65	30	equivalent	equivalent	ADJ
eurjchem-570	65	31	to	to	ADP
eurjchem-570	65	32	15‐	15‐	NUM
eurjchem-570	65	33	75	75	NUM
eurjchem-570	65	34	and	and	CCONJ
eurjchem-570	65	35	150‐750	150‐750	NUM
eurjchem-570	65	36	µg	µg	NOUN
eurjchem-570	65	37	/	/	SYM
eurjchem-570	65	38	ml	ml	PROPN
eurjchem-570	65	39	of	of	ADP
eurjchem-570	65	40	vld	vld	PROPN
eurjchem-570	65	41	and	and	CCONJ
eurjchem-570	65	42	met	meet	VERB
eurjchem-570	65	43	,	,	PUNCT
eurjchem-570	65	44	respectively	respectively	ADV
eurjchem-570	65	45	;	;	PUNCT
eurjchem-570	65	46	and	and	CCONJ
eurjchem-570	65	47	equivalent	equivalent	ADJ
eurjchem-570	65	48	to	to	ADP
eurjchem-570	65	49	1.67‐8.37	1.67‐8.37	NUM
eurjchem-570	65	50	and	and	CCONJ
eurjchem-570	65	51	150‐750	150‐750	NUM
eurjchem-570	65	52	µg	µg	NOUN
eurjchem-570	65	53	/	/	SYM
eurjchem-570	65	54	ml	ml	NOUN
eurjchem-570	65	55	of	of	ADP
eurjchem-570	65	56	sxd	sxd	NOUN
eurjchem-570	65	57	and	and	CCONJ
eurjchem-570	65	58	met	meet	VERB
eurjchem-570	65	59	,	,	PUNCT
eurjchem-570	65	60	respectively	respectively	ADV
eurjchem-570	65	61	;	;	PUNCT
eurjchem-570	65	62	and	and	CCONJ
eurjchem-570	65	63	then	then	ADV
eurjchem-570	65	64	injected	inject	VERB
eurjchem-570	65	65	in	in	ADP
eurjchem-570	65	66	triplicates	triplicate	NOUN
eurjchem-570	65	67	.	.	PUNCT
eurjchem-570	66	1	the	the	DET
eurjchem-570	66	2	concentrations	concentration	NOUN
eurjchem-570	66	3	of	of	ADP
eurjchem-570	66	4	the	the	DET
eurjchem-570	66	5	examined	examine	VERB
eurjchem-570	66	6	drugs	drug	NOUN
eurjchem-570	66	7	were	be	AUX
eurjchem-570	66	8	calculated	calculate	VERB
eurjchem-570	66	9	by	by	ADP
eurjchem-570	66	10	the	the	DET
eurjchem-570	66	11	calibration	calibration	NOUN
eurjchem-570	66	12	equations	equation	NOUN
eurjchem-570	66	13	(	(	PUNCT
eurjchem-570	66	14	table	table	NOUN
eurjchem-570	66	15	3	3	NUM
eurjchem-570	66	16	)	)	PUNCT
eurjchem-570	66	17	.	.	PUNCT
eurjchem-570	67	1	3	3	X
eurjchem-570	67	2	.	.	NOUN
eurjchem-570	67	3	results	result	NOUN
eurjchem-570	67	4	and	and	CCONJ
eurjchem-570	67	5	discussion	discussion	VERB
eurjchem-570	67	6	the	the	DET
eurjchem-570	67	7	combinations	combination	NOUN
eurjchem-570	67	8	of	of	ADP
eurjchem-570	67	9	vdg	vdg	NOUN
eurjchem-570	67	10	or	or	CCONJ
eurjchem-570	67	11	sxg	sxg	NOUN
eurjchem-570	67	12	with	with	ADP
eurjchem-570	67	13	met	meet	VERB
eurjchem-570	67	14	are	be	AUX
eurjchem-570	67	15	new	new	ADJ
eurjchem-570	67	16	to	to	ADP
eurjchem-570	67	17	the	the	DET
eurjchem-570	67	18	market	market	NOUN
eurjchem-570	67	19	.	.	PUNCT
eurjchem-570	68	1	no	no	DET
eurjchem-570	68	2	previous	previous	ADJ
eurjchem-570	68	3	method	method	NOUN
eurjchem-570	68	4	was	be	AUX
eurjchem-570	68	5	reported	report	VERB
eurjchem-570	68	6	for	for	ADP
eurjchem-570	68	7	the	the	DET
eurjchem-570	68	8	lc	lc	NOUN
eurjchem-570	68	9	determination	determination	NOUN
eurjchem-570	68	10	of	of	ADP
eurjchem-570	68	11	vdg	vdg	NOUN
eurjchem-570	68	12	or	or	CCONJ
eurjchem-570	68	13	sxg	sxg	NOUN
eurjchem-570	68	14	in	in	ADP
eurjchem-570	68	15	their	their	PRON
eurjchem-570	68	16	binary	binary	ADJ
eurjchem-570	68	17	mixture	mixture	NOUN
eurjchem-570	68	18	with	with	ADP
eurjchem-570	68	19	met	meet	VERB
eurjchem-570	68	20	.	.	PUNCT
eurjchem-570	69	1	thus	thus	ADV
eurjchem-570	69	2	,	,	PUNCT
eurjchem-570	69	3	the	the	DET
eurjchem-570	69	4	aim	aim	NOUN
eurjchem-570	69	5	of	of	ADP
eurjchem-570	69	6	this	this	DET
eurjchem-570	69	7	work	work	NOUN
eurjchem-570	69	8	was	be	AUX
eurjchem-570	69	9	to	to	PART
eurjchem-570	69	10	develop	develop	VERB
eurjchem-570	69	11	a	a	DET
eurjchem-570	69	12	simple	simple	ADJ
eurjchem-570	69	13	,	,	PUNCT
eurjchem-570	69	14	accurate	accurate	ADJ
eurjchem-570	69	15	and	and	CCONJ
eurjchem-570	69	16	reproducible	reproducible	VERB
eurjchem-570	69	17	lc	lc	NOUN
eurjchem-570	69	18	method	method	NOUN
eurjchem-570	69	19	that	that	PRON
eurjchem-570	69	20	could	could	AUX
eurjchem-570	69	21	be	be	AUX
eurjchem-570	69	22	applied	apply	VERB
eurjchem-570	69	23	to	to	ADP
eurjchem-570	69	24	the	the	DET
eurjchem-570	69	25	simultaneous	simultaneous	ADJ
eurjchem-570	69	26	determination	determination	NOUN
eurjchem-570	69	27	of	of	ADP
eurjchem-570	69	28	vdg	vdg	NOUN
eurjchem-570	69	29	or	or	CCONJ
eurjchem-570	69	30	sxg	sxg	NOUN
eurjchem-570	69	31	with	with	ADP
eurjchem-570	69	32	met	meet	VERB
eurjchem-570	69	33	in	in	ADP
eurjchem-570	69	34	their	their	PRON
eurjchem-570	69	35	laboratory	laboratory	NOUN
eurjchem-570	69	36	prepared	prepare	VERB
eurjchem-570	69	37	mixtures	mixture	NOUN
eurjchem-570	69	38	or	or	CCONJ
eurjchem-570	69	39	pharmaceutical	pharmaceutical	NOUN
eurjchem-570	69	40	preparations	preparation	NOUN
eurjchem-570	69	41	of	of	ADP
eurjchem-570	69	42	these	these	DET
eurjchem-570	69	43	drugs	drug	NOUN
eurjchem-570	69	44	.	.	PUNCT
eurjchem-570	70	1	3.1	3.1	NUM
eurjchem-570	70	2	.	.	PUNCT
eurjchem-570	70	3	method	method	PROPN
eurjchem-570	70	4	development	development	NOUN
eurjchem-570	70	5	during	during	ADP
eurjchem-570	70	6	the	the	DET
eurjchem-570	70	7	optimization	optimization	NOUN
eurjchem-570	70	8	cycle	cycle	NOUN
eurjchem-570	70	9	,	,	PUNCT
eurjchem-570	70	10	several	several	ADJ
eurjchem-570	70	11	chromatographic	chromatographic	ADJ
eurjchem-570	70	12	conditions	condition	NOUN
eurjchem-570	70	13	were	be	AUX
eurjchem-570	70	14	attempted	attempt	VERB
eurjchem-570	70	15	using	use	VERB
eurjchem-570	70	16	an	an	DET
eurjchem-570	70	17	inertsil	inertsil	NOUN
eurjchem-570	70	18	®	®	NOUN
eurjchem-570	70	19	cn‐3	cn‐3	NOUN
eurjchem-570	70	20	column	column	NOUN
eurjchem-570	70	21	(	(	PUNCT
eurjchem-570	70	22	250	250	NUM
eurjchem-570	70	23	mm	mm	NOUN
eurjchem-570	70	24	x	x	SYM
eurjchem-570	70	25	4.6	4.6	NUM
eurjchem-570	70	26	mm	mm	NOUN
eurjchem-570	70	27	,	,	PUNCT
eurjchem-570	70	28	5	5	NUM
eurjchem-570	70	29	µm	µm	NOUN
eurjchem-570	70	30	)	)	PUNCT
eurjchem-570	70	31	.	.	PUNCT
eurjchem-570	71	1	recently	recently	ADV
eurjchem-570	71	2	,	,	PUNCT
eurjchem-570	71	3	cyano	cyano	NOUN
eurjchem-570	71	4	columns	column	NOUN
eurjchem-570	71	5	have	have	AUX
eurjchem-570	71	6	been	be	AUX
eurjchem-570	71	7	used	use	VERB
eurjchem-570	71	8	for	for	ADP
eurjchem-570	71	9	the	the	DET
eurjchem-570	71	10	separation	separation	NOUN
eurjchem-570	71	11	and	and	CCONJ
eurjchem-570	71	12	quantitation	quantitation	NOUN
eurjchem-570	71	13	of	of	ADP
eurjchem-570	71	14	drugs	drug	NOUN
eurjchem-570	71	15	[	[	X
eurjchem-570	71	16	15‐16	15‐16	NUM
eurjchem-570	71	17	]	]	X
eurjchem-570	71	18	.	.	PUNCT
eurjchem-570	72	1	various	various	ADJ
eurjchem-570	72	2	mobile	mobile	ADJ
eurjchem-570	72	3	phase	phase	NOUN
eurjchem-570	72	4	compositions	composition	NOUN
eurjchem-570	72	5	containing	contain	VERB
eurjchem-570	72	6	different	different	ADJ
eurjchem-570	72	7	ratios	ratio	NOUN
eurjchem-570	72	8	of	of	ADP
eurjchem-570	72	9	organic	organic	ADJ
eurjchem-570	72	10	and	and	CCONJ
eurjchem-570	72	11	aqueous	aqueous	ADJ
eurjchem-570	72	12	phases	phase	NOUN
eurjchem-570	72	13	were	be	AUX
eurjchem-570	72	14	tried	try	VERB
eurjchem-570	72	15	in	in	ADP
eurjchem-570	72	16	an	an	DET
eurjchem-570	72	17	isocratic	isocratic	ADJ
eurjchem-570	72	18	mode	mode	NOUN
eurjchem-570	72	19	.	.	PUNCT
eurjchem-570	73	1	it	it	PRON
eurjchem-570	73	2	was	be	AUX
eurjchem-570	73	3	found	find	VERB
eurjchem-570	73	4	that	that	SCONJ
eurjchem-570	73	5	85	85	NUM
eurjchem-570	73	6	%	%	NOUN
eurjchem-570	73	7	of	of	ADP
eurjchem-570	73	8	organic	organic	ADJ
eurjchem-570	73	9	modifier	modifier	NOUN
eurjchem-570	73	10	was	be	AUX
eurjchem-570	73	11	needed	need	VERB
eurjchem-570	73	12	to	to	PART
eurjchem-570	73	13	elute	elute	VERB
eurjchem-570	73	14	all	all	DET
eurjchem-570	73	15	peaks	peak	NOUN
eurjchem-570	73	16	within	within	ADP
eurjchem-570	73	17	10	10	NUM
eurjchem-570	73	18	min	min	NOUN
eurjchem-570	73	19	.	.	PROPN
eurjchem-570	73	20	acetonitrile	acetonitrile	NOUN
eurjchem-570	73	21	was	be	AUX
eurjchem-570	73	22	found	find	VERB
eurjchem-570	73	23	optimum	optimum	ADJ
eurjchem-570	73	24	for	for	ADP
eurjchem-570	73	25	the	the	DET
eurjchem-570	73	26	elution	elution	NOUN
eurjchem-570	73	27	.	.	PUNCT
eurjchem-570	74	1	besides	besides	SCONJ
eurjchem-570	74	2	,	,	PUNCT
eurjchem-570	74	3	different	different	ADJ
eurjchem-570	74	4	buffers	buffer	NOUN
eurjchem-570	74	5	at	at	ADP
eurjchem-570	74	6	different	different	ADJ
eurjchem-570	74	7	ph	ph	ADJ
eurjchem-570	74	8	values	value	NOUN
eurjchem-570	74	9	were	be	AUX
eurjchem-570	74	10	attempted	attempt	VERB
eurjchem-570	74	11	along	along	ADP
eurjchem-570	74	12	with	with	ADP
eurjchem-570	74	13	acetonitrile	acetonitrile	NOUN
eurjchem-570	74	14	.	.	PUNCT
eurjchem-570	75	1	therefore	therefore	ADV
eurjchem-570	75	2	,	,	PUNCT
eurjchem-570	75	3	a	a	DET
eurjchem-570	75	4	mobile	mobile	ADJ
eurjchem-570	75	5	phase	phase	NOUN
eurjchem-570	75	6	consisting	consist	VERB
eurjchem-570	75	7	of	of	ADP
eurjchem-570	75	8	potassium	potassium	NOUN
eurjchem-570	75	9	dihydrogen	dihydrogen	NOUN
eurjchem-570	75	10	phosphate	phosphate	NOUN
eurjchem-570	75	11	buffer	buffer	NOUN
eurjchem-570	75	12	ph	ph	NOUN
eurjchem-570	75	13	(	(	PUNCT
eurjchem-570	75	14	4.6	4.6	NUM
eurjchem-570	75	15	)	)	PUNCT
eurjchem-570	75	16	‐	‐	ADJ
eurjchem-570	75	17	acetonitrile	acetonitrile	NOUN
eurjchem-570	75	18	(	(	PUNCT
eurjchem-570	75	19	15:85	15:85	NUM
eurjchem-570	75	20	,	,	PUNCT
eurjchem-570	75	21	v	v	NOUN
eurjchem-570	75	22	:	:	SYM
eurjchem-570	75	23	v	v	NOUN
eurjchem-570	75	24	)	)	PUNCT
eurjchem-570	75	25	and	and	CCONJ
eurjchem-570	75	26	pumped	pump	VERB
eurjchem-570	75	27	at	at	ADP
eurjchem-570	75	28	a	a	DET
eurjchem-570	75	29	flow	flow	NOUN
eurjchem-570	75	30	rate	rate	NOUN
eurjchem-570	75	31	of	of	ADP
eurjchem-570	75	32	1.0	1.0	NUM
eurjchem-570	75	33	ml	ml	NOUN
eurjchem-570	75	34	/	/	SYM
eurjchem-570	75	35	min	min	NOUN
eurjchem-570	75	36	,	,	PUNCT
eurjchem-570	75	37	in	in	ADP
eurjchem-570	75	38	an	an	DET
eurjchem-570	75	39	isocratic	isocratic	ADJ
eurjchem-570	75	40	mode	mode	NOUN
eurjchem-570	75	41	,	,	PUNCT
eurjchem-570	75	42	gave	give	VERB
eurjchem-570	75	43	good	good	ADJ
eurjchem-570	75	44	separation	separation	NOUN
eurjchem-570	75	45	of	of	ADP
eurjchem-570	75	46	the	the	DET
eurjchem-570	75	47	three	three	NUM
eurjchem-570	75	48	drugs	drug	NOUN
eurjchem-570	75	49	.	.	PUNCT
eurjchem-570	76	1	due	due	ADP
eurjchem-570	76	2	to	to	ADP
eurjchem-570	76	3	the	the	DET
eurjchem-570	76	4	poorly	poorly	ADV
eurjchem-570	76	5	absorbing	absorbing	ADJ
eurjchem-570	76	6	chromophores	chromophore	NOUN
eurjchem-570	76	7	in	in	ADP
eurjchem-570	76	8	the	the	DET
eurjchem-570	76	9	three	three	NUM
eurjchem-570	76	10	drugs	drug	NOUN
eurjchem-570	76	11	examined	examine	VERB
eurjchem-570	76	12	,	,	PUNCT
eurjchem-570	76	13	detection	detection	NOUN
eurjchem-570	76	14	was	be	AUX
eurjchem-570	76	15	carried	carry	VERB
eurjchem-570	76	16	out	out	ADP
eurjchem-570	76	17	at	at	ADP
eurjchem-570	76	18	208	208	NUM
eurjchem-570	76	19	nm	nm	NOUN
eurjchem-570	76	20	to	to	PART
eurjchem-570	76	21	obtain	obtain	VERB
eurjchem-570	76	22	sufficient	sufficient	ADJ
eurjchem-570	76	23	peak	peak	NOUN
eurjchem-570	76	24	intensity	intensity	NOUN
eurjchem-570	76	25	for	for	ADP
eurjchem-570	76	26	these	these	DET
eurjchem-570	76	27	drugs	drug	NOUN
eurjchem-570	76	28	.	.	PUNCT
eurjchem-570	77	1	the	the	DET
eurjchem-570	77	2	retention	retention	NOUN
eurjchem-570	77	3	times	time	NOUN
eurjchem-570	77	4	were	be	AUX
eurjchem-570	77	5	7.2	7.2	NUM
eurjchem-570	77	6	,	,	PUNCT
eurjchem-570	77	7	6.3	6.3	NUM
eurjchem-570	77	8	and	and	CCONJ
eurjchem-570	77	9	8.7	8.7	NUM
eurjchem-570	77	10	min	min	NOUN
eurjchem-570	77	11	for	for	ADP
eurjchem-570	77	12	vld	vld	PROPN
eurjchem-570	77	13	,	,	PUNCT
eurjchem-570	77	14	sxg	sxg	NOUN
eurjchem-570	77	15	and	and	CCONJ
eurjchem-570	77	16	met	meet	VERB
eurjchem-570	77	17	,	,	PUNCT
eurjchem-570	77	18	respectively	respectively	ADV
eurjchem-570	77	19	;	;	PUNCT
eurjchem-570	77	20	as	as	SCONJ
eurjchem-570	77	21	presented	present	VERB
eurjchem-570	77	22	in	in	ADP
eurjchem-570	77	23	figure	figure	NOUN
eurjchem-570	77	24	2	2	NUM
eurjchem-570	77	25	and	and	CCONJ
eurjchem-570	77	26	3	3	NUM
eurjchem-570	77	27	.	.	NOUN
eurjchem-570	77	28	154	154	NUM
eurjchem-570	77	29	mohammad	mohammad	PROPN
eurjchem-570	77	30	et	et	PROPN
eurjchem-570	77	31	al	al	PROPN
eurjchem-570	77	32	.	.	PUNCT
eurjchem-570	77	33	/	/	SYM
eurjchem-570	77	34	european	european	PROPN
eurjchem-570	77	35	journal	journal	PROPN
eurjchem-570	77	36	of	of	ADP
eurjchem-570	77	37	chemistry	chemistry	NOUN
eurjchem-570	77	38	3	3	NUM
eurjchem-570	77	39	(	(	PUNCT
eurjchem-570	77	40	2	2	NUM
eurjchem-570	77	41	)	)	PUNCT
eurjchem-570	77	42	(	(	PUNCT
eurjchem-570	77	43	2012	2012	NUM
eurjchem-570	77	44	)	)	PUNCT
eurjchem-570	77	45	152‐155	152‐155	NUM
eurjchem-570	77	46	table	table	NOUN
eurjchem-570	77	47	3	3	NUM
eurjchem-570	77	48	.	.	PUNCT
eurjchem-570	77	49	results	result	NOUN
eurjchem-570	77	50	obtained	obtain	VERB
eurjchem-570	77	51	by	by	ADP
eurjchem-570	77	52	lc	lc	PROPN
eurjchem-570	77	53	method	method	NOUN
eurjchem-570	77	54	for	for	ADP
eurjchem-570	77	55	the	the	DET
eurjchem-570	77	56	determination	determination	NOUN
eurjchem-570	77	57	of	of	ADP
eurjchem-570	77	58	metformin	metformin	NOUN
eurjchem-570	77	59	in	in	ADP
eurjchem-570	77	60	binary	binary	ADJ
eurjchem-570	77	61	mixture	mixture	NOUN
eurjchem-570	77	62	with	with	ADP
eurjchem-570	77	63	vildagliptin	vildagliptin	NOUN
eurjchem-570	77	64	or	or	CCONJ
eurjchem-570	77	65	saxagliptin	saxagliptin	NOUN
eurjchem-570	77	66	.	.	PUNCT
eurjchem-570	78	1	item	item	PROPN
eurjchem-570	78	2	metformin	metformin	PROPN
eurjchem-570	78	3	vildagliptin	vildagliptin	NOUN
eurjchem-570	78	4	saxagliptin	saxagliptin	NOUN
eurjchem-570	78	5	retention	retention	NOUN
eurjchem-570	78	6	time	time	NOUN
eurjchem-570	78	7	(	(	PUNCT
eurjchem-570	78	8	min	min	NOUN
eurjchem-570	78	9	)	)	PUNCT
eurjchem-570	78	10	8.7	8.7	NUM
eurjchem-570	78	11	7.2	7.2	NUM
eurjchem-570	78	12	6.3	6.3	NUM
eurjchem-570	78	13	wavelength	wavelength	NOUN
eurjchem-570	78	14	of	of	ADP
eurjchem-570	78	15	detection	detection	NOUN
eurjchem-570	78	16	208	208	NUM
eurjchem-570	78	17	nm	nm	NUM
eurjchem-570	78	18	208	208	NUM
eurjchem-570	78	19	nm	nm	NUM
eurjchem-570	78	20	208	208	NUM
eurjchem-570	78	21	nm	nm	ADJ
eurjchem-570	78	22	range	range	NOUN
eurjchem-570	78	23	of	of	ADP
eurjchem-570	78	24	linearity	linearity	NOUN
eurjchem-570	78	25	50‐2000	50‐2000	NUM
eurjchem-570	78	26	μg	μg	NOUN
eurjchem-570	78	27	/	/	SYM
eurjchem-570	78	28	ml	ml	NOUN
eurjchem-570	78	29	5‐200	5‐200	PROPN
eurjchem-570	78	30	μg	μg	PROPN
eurjchem-570	78	31	/	/	SYM
eurjchem-570	78	32	ml	ml	NOUN
eurjchem-570	78	33	0.5‐20	0.5‐20	NUM
eurjchem-570	78	34	μg	μg	NOUN
eurjchem-570	78	35	/	/	SYM
eurjchem-570	78	36	ml	ml	ADP
eurjchem-570	78	37	regression	regression	NOUN
eurjchem-570	78	38	equation	equation	NOUN
eurjchem-570	78	39	area	area	NOUN
eurjchem-570	78	40	x	x	NOUN
eurjchem-570	78	41	10‐6	10‐6	NUM
eurjchem-570	78	42	=	=	SYM
eurjchem-570	78	43	0.0528	0.0528	NUM
eurjchem-570	78	44	cμg	cμg	NOUN
eurjchem-570	78	45	/	/	SYM
eurjchem-570	78	46	ml	ml	NOUN
eurjchem-570	78	47	+	+	CCONJ
eurjchem-570	78	48	0.0231	0.0231	NUM
eurjchem-570	78	49	area	area	NOUN
eurjchem-570	78	50	x	x	SYM
eurjchem-570	78	51	10‐5	10‐5	NUM
eurjchem-570	78	52	=	=	SYM
eurjchem-570	78	53	0.1126	0.1126	NUM
eurjchem-570	78	54	cμg	cμg	NOUN
eurjchem-570	78	55	/	/	SYM
eurjchem-570	78	56	ml	ml	NOUN
eurjchem-570	78	57	+	+	CCONJ
eurjchem-570	78	58	0.4040	0.4040	NUM
eurjchem-570	78	59	area	area	NOUN
eurjchem-570	78	60	x	x	SYM
eurjchem-570	78	61	10‐5	10‐5	NUM
eurjchem-570	78	62	=	=	SYM
eurjchem-570	78	63	0.2415	0.2415	NUM
eurjchem-570	78	64	cμg	cμg	ADJ
eurjchem-570	78	65	/	/	SYM
eurjchem-570	78	66	ml	ml	NOUN
eurjchem-570	78	67	+	+	CCONJ
eurjchem-570	78	68	0.5112	0.5112	NUM
eurjchem-570	78	69	regression	regression	NOUN
eurjchem-570	78	70	coefficient	coefficient	NOUN
eurjchem-570	78	71	(	(	PUNCT
eurjchem-570	78	72	r2	r2	PROPN
eurjchem-570	78	73	)	)	PUNCT
eurjchem-570	78	74	0.9999	0.9999	NUM
eurjchem-570	78	75	0.9996	0.9996	NUM
eurjchem-570	78	76	0.9968	0.9968	NUM
eurjchem-570	78	77	lod	lod	PROPN
eurjchem-570	78	78	μg	μg	PROPN
eurjchem-570	78	79	/	/	SYM
eurjchem-570	78	80	ml	ml	PROPN
eurjchem-570	78	81	19.36	19.36	NUM
eurjchem-570	78	82	0.53	0.53	NUM
eurjchem-570	78	83	0.29	0.29	NUM
eurjchem-570	78	84	loq	loq	PROPN
eurjchem-570	78	85	μg	μg	PROPN
eurjchem-570	78	86	/	/	SYM
eurjchem-570	78	87	ml	ml	PROPN
eurjchem-570	78	88	46.54	46.54	NUM
eurjchem-570	78	89	1.78	1.78	NUM
eurjchem-570	78	90	0.48	0.48	NUM
eurjchem-570	78	91	sb	sb	PROPN
eurjchem-570	78	92	2.1	2.1	NUM
eurjchem-570	78	93	x	x	SYM
eurjchem-570	78	94	10‐4	10‐4	NUM
eurjchem-570	78	95	1.1	1.1	NUM
eurjchem-570	78	96	x	x	SYM
eurjchem-570	78	97	10‐3	10‐3	NUM
eurjchem-570	78	98	6.7	6.7	NUM
eurjchem-570	78	99	x	x	SYM
eurjchem-570	78	100	10‐2	10‐2	NUM
eurjchem-570	78	101	sa	sa	PROPN
eurjchem-570	78	102	2.7	2.7	NUM
eurjchem-570	78	103	x	x	SYM
eurjchem-570	78	104	10‐2	10‐2	NUM
eurjchem-570	78	105	0.15	0.15	NUM
eurjchem-570	78	106	0.58	0.58	NUM
eurjchem-570	78	107	confidence	confidence	NOUN
eurjchem-570	78	108	limit	limit	NOUN
eurjchem-570	78	109	of	of	ADP
eurjchem-570	78	110	the	the	DET
eurjchem-570	78	111	slope	slope	NOUN
eurjchem-570	78	112	0.0528	0.0528	NUM
eurjchem-570	78	113	±	±	NOUN
eurjchem-570	78	114	0.14	0.14	NUM
eurjchem-570	78	115	x	x	SYM
eurjchem-570	78	116	10‐2	10‐2	NUM
eurjchem-570	78	117	0.1126	0.1126	NUM
eurjchem-570	78	118	±	±	NUM
eurjchem-570	78	119	0.02	0.02	NUM
eurjchem-570	78	120	0.2415	0.2415	NUM
eurjchem-570	78	121	±	±	NOUN
eurjchem-570	78	122	0.14	0.14	NUM
eurjchem-570	78	123	confidence	confidence	NOUN
eurjchem-570	78	124	limit	limit	NOUN
eurjchem-570	78	125	of	of	ADP
eurjchem-570	78	126	the	the	DET
eurjchem-570	78	127	intercept	intercept	NOUN
eurjchem-570	78	128	0.0231	0.0231	NUM
eurjchem-570	78	129	±	±	NUM
eurjchem-570	78	130	0.05	0.05	NUM
eurjchem-570	78	131	x	x	SYM
eurjchem-570	78	132	10‐4	10‐4	NUM
eurjchem-570	78	133	0.4040	0.4040	NUM
eurjchem-570	78	134	±	±	NUM
eurjchem-570	78	135	0.44	0.44	NUM
eurjchem-570	78	136	x	x	SYM
eurjchem-570	79	1	10‐3	10‐3	NUM
eurjchem-570	79	2	0.5112	0.5112	NUM
eurjchem-570	79	3	±	±	NUM
eurjchem-570	79	4	3.43	3.43	NUM
eurjchem-570	79	5	x	x	SYM
eurjchem-570	79	6	10‐2	10‐2	NUM
eurjchem-570	79	7	standard	standard	ADJ
eurjchem-570	79	8	error	error	NOUN
eurjchem-570	79	9	of	of	ADP
eurjchem-570	79	10	the	the	DET
eurjchem-570	79	11	estimation	estimation	NOUN
eurjchem-570	79	12	0.341	0.341	NUM
eurjchem-570	79	13	0.186	0.186	NUM
eurjchem-570	79	14	0.489	0.489	NUM
eurjchem-570	79	15	intraday	intraday	NOUN
eurjchem-570	79	16	%	%	NOUN
eurjchem-570	79	17	r.s.d	r.s.d	NOUN
eurjchem-570	79	18	.	.	PUNCT
eurjchem-570	80	1	0.38‐0.87	0.38‐0.87	NUM
eurjchem-570	80	2	0.37‐0.68	0.37‐0.68	NUM
eurjchem-570	81	1	0.33‐0.57	0.33‐0.57	PROPN
eurjchem-570	81	2	interday	interday	NOUN
eurjchem-570	81	3	%	%	PROPN
eurjchem-570	81	4	r.s.d	r.s.d	PROPN
eurjchem-570	81	5	.	.	PUNCT
eurjchem-570	82	1	0.33‐1.22	0.33‐1.22	NUM
eurjchem-570	83	1	0.41‐1.51	0.41‐1.51	NOUN
eurjchem-570	83	2	0.54‐1.18	0.54‐1.18	PROPN
eurjchem-570	83	3	drug	drug	NOUN
eurjchem-570	83	4	in	in	ADP
eurjchem-570	83	5	lab	lab	NOUN
eurjchem-570	83	6	.	.	PUNCT
eurjchem-570	84	1	prepared	prepare	VERB
eurjchem-570	84	2	mixture	mixture	NOUN
eurjchem-570	84	3	100.12	100.12	NUM
eurjchem-570	84	4	±	±	NUM
eurjchem-570	84	5	0.99	0.99	NUM
eurjchem-570	84	6	99.49	99.49	NUM
eurjchem-570	84	7	±	±	NUM
eurjchem-570	84	8	0.90	0.90	NUM
eurjchem-570	84	9	100.30	100.30	NUM
eurjchem-570	84	10	±	±	NUM
eurjchem-570	84	11	1.25	1.25	NUM
eurjchem-570	84	12	drug	drug	NOUN
eurjchem-570	84	13	in	in	ADP
eurjchem-570	84	14	dosage	dosage	NOUN
eurjchem-570	84	15	form	form	NOUN
eurjchem-570	84	16	100.42	100.42	NUM
eurjchem-570	84	17	±	±	NUM
eurjchem-570	84	18	0.92	0.92	NUM
eurjchem-570	84	19	(	(	PUNCT
eurjchem-570	84	20	eucreas	eucreas	ADJ
eurjchem-570	84	21	®	®	NOUN
eurjchem-570	84	22	)	)	PUNCT
eurjchem-570	84	23	99.87	99.87	NUM
eurjchem-570	84	24	±	±	NUM
eurjchem-570	84	25	0.81	0.81	NUM
eurjchem-570	84	26	(	(	PUNCT
eurjchem-570	84	27	kombiglyze	kombiglyze	PROPN
eurjchem-570	84	28	®	®	NOUN
eurjchem-570	84	29	)	)	PUNCT
eurjchem-570	84	30	100.11	100.11	NUM
eurjchem-570	84	31	±	±	NUM
eurjchem-570	84	32	0.67	0.67	NUM
eurjchem-570	84	33	99.47	99.47	NUM
eurjchem-570	84	34	±	±	NUM
eurjchem-570	84	35	1.15	1.15	NUM
eurjchem-570	84	36	drug	drug	NOUN
eurjchem-570	84	37	added	add	VERB
eurjchem-570	84	38	100.83	100.83	NUM
eurjchem-570	84	39	±	±	NUM
eurjchem-570	84	40	1.30	1.30	NUM
eurjchem-570	84	41	(	(	PUNCT
eurjchem-570	84	42	eucreas	eucreas	ADJ
eurjchem-570	84	43	®	®	NOUN
eurjchem-570	84	44	)	)	PUNCT
eurjchem-570	84	45	100.17	100.17	NUM
eurjchem-570	84	46	±	±	NUM
eurjchem-570	84	47	0.86	0.86	NUM
eurjchem-570	84	48	(	(	PUNCT
eurjchem-570	84	49	kombiglyze	kombiglyze	PROPN
eurjchem-570	84	50	®	®	NOUN
eurjchem-570	84	51	)	)	PUNCT
eurjchem-570	84	52	100.53	100.53	NUM
eurjchem-570	84	53	±	±	NUM
eurjchem-570	84	54	0.89	0.89	NUM
eurjchem-570	84	55	100.64	100.64	NUM
eurjchem-570	84	56	±	±	NUM
eurjchem-570	84	57	1.40	1.40	NUM
eurjchem-570	84	58	figure	figure	NOUN
eurjchem-570	84	59	2	2	NUM
eurjchem-570	84	60	.	.	PUNCT
eurjchem-570	85	1	a	a	DET
eurjchem-570	85	2	typical	typical	ADJ
eurjchem-570	85	3	lc	lc	NOUN
eurjchem-570	85	4	chromatogram	chromatogram	NOUN
eurjchem-570	85	5	of	of	ADP
eurjchem-570	85	6	25	25	NUM
eurjchem-570	85	7	µl	µl	ADP
eurjchem-570	85	8	injector	injector	NOUN
eurjchem-570	85	9	of	of	ADP
eurjchem-570	85	10	eucreas	eucrea	NOUN
eurjchem-570	85	11	®	®	NOUN
eurjchem-570	85	12	sample	sample	NOUN
eurjchem-570	85	13	solution	solution	NOUN
eurjchem-570	85	14	containing	contain	VERB
eurjchem-570	85	15	(	(	PUNCT
eurjchem-570	85	16	a	a	PRON
eurjchem-570	85	17	)	)	PUNCT
eurjchem-570	85	18	metformin	metformin	NOUN
eurjchem-570	85	19	hydrochloride	hydrochloride	NOUN
eurjchem-570	85	20	(	(	PUNCT
eurjchem-570	85	21	400	400	NUM
eurjchem-570	85	22	µg	µg	NOUN
eurjchem-570	85	23	/	/	SYM
eurjchem-570	85	24	ml	ml	NOUN
eurjchem-570	85	25	)	)	PUNCT
eurjchem-570	85	26	and	and	CCONJ
eurjchem-570	85	27	(	(	PUNCT
eurjchem-570	85	28	b	b	NOUN
eurjchem-570	85	29	)	)	PUNCT
eurjchem-570	85	30	vildagliptin	vildagliptin	NOUN
eurjchem-570	85	31	(	(	PUNCT
eurjchem-570	85	32	40	40	NUM
eurjchem-570	85	33	µg	µg	NOUN
eurjchem-570	85	34	/	/	SYM
eurjchem-570	85	35	ml	ml	NOUN
eurjchem-570	85	36	)	)	PUNCT
eurjchem-570	85	37	.	.	PUNCT
eurjchem-570	86	1	figure	figure	VERB
eurjchem-570	86	2	3	3	NUM
eurjchem-570	86	3	.	.	PUNCT
eurjchem-570	87	1	a	a	DET
eurjchem-570	87	2	typical	typical	ADJ
eurjchem-570	87	3	lc	lc	NOUN
eurjchem-570	87	4	chromatogram	chromatogram	NOUN
eurjchem-570	87	5	of	of	ADP
eurjchem-570	87	6	25	25	NUM
eurjchem-570	87	7	µl	µl	ADP
eurjchem-570	87	8	injector	injector	NOUN
eurjchem-570	87	9	of	of	ADP
eurjchem-570	87	10	kombiglyze	kombiglyze	NOUN
eurjchem-570	87	11	®	®	NOUN
eurjchem-570	87	12	sample	sample	NOUN
eurjchem-570	87	13	solution	solution	NOUN
eurjchem-570	87	14	containing	contain	VERB
eurjchem-570	87	15	(	(	PUNCT
eurjchem-570	87	16	a	a	PRON
eurjchem-570	87	17	)	)	PUNCT
eurjchem-570	87	18	metformin	metformin	NOUN
eurjchem-570	87	19	hydrochloride	hydrochloride	NOUN
eurjchem-570	87	20	(	(	PUNCT
eurjchem-570	87	21	500	500	NUM
eurjchem-570	87	22	µg	µg	NOUN
eurjchem-570	87	23	/	/	SYM
eurjchem-570	87	24	ml	ml	NOUN
eurjchem-570	87	25	)	)	PUNCT
eurjchem-570	87	26	and	and	CCONJ
eurjchem-570	87	27	(	(	PUNCT
eurjchem-570	87	28	b	b	NOUN
eurjchem-570	87	29	)	)	PUNCT
eurjchem-570	87	30	saxagliptin	saxagliptin	NOUN
eurjchem-570	87	31	hydrochloride	hydrochloride	NOUN
eurjchem-570	87	32	(	(	PUNCT
eurjchem-570	87	33	5.58	5.58	NUM
eurjchem-570	87	34	µg	µg	NOUN
eurjchem-570	87	35	/	/	SYM
eurjchem-570	87	36	ml	ml	NOUN
eurjchem-570	87	37	)	)	PUNCT
eurjchem-570	87	38	.	.	PUNCT
eurjchem-570	88	1	3.2	3.2	NUM
eurjchem-570	88	2	.	.	PUNCT
eurjchem-570	89	1	system	system	NOUN
eurjchem-570	89	2	suitability	suitability	NOUN
eurjchem-570	89	3	tests	test	NOUN
eurjchem-570	89	4	according	accord	VERB
eurjchem-570	89	5	to	to	ADP
eurjchem-570	89	6	the	the	DET
eurjchem-570	89	7	united	united	PROPN
eurjchem-570	89	8	states	states	PROPN
eurjchem-570	89	9	pharmacopoeia	pharmacopoeia	PROPN
eurjchem-570	89	10	,	,	PUNCT
eurjchem-570	89	11	2007	2007	NUM
eurjchem-570	90	1	[	[	X
eurjchem-570	90	2	17	17	NUM
eurjchem-570	90	3	]	]	PUNCT
eurjchem-570	90	4	,	,	PUNCT
eurjchem-570	90	5	system	system	NOUN
eurjchem-570	90	6	suitability	suitability	NOUN
eurjchem-570	90	7	tests	test	NOUN
eurjchem-570	90	8	are	be	AUX
eurjchem-570	90	9	an	an	DET
eurjchem-570	90	10	integral	integral	ADJ
eurjchem-570	90	11	part	part	NOUN
eurjchem-570	90	12	of	of	ADP
eurjchem-570	90	13	liquid	liquid	ADJ
eurjchem-570	90	14	chromatographic	chromatographic	ADJ
eurjchem-570	90	15	methods	method	NOUN
eurjchem-570	90	16	in	in	ADP
eurjchem-570	90	17	the	the	DET
eurjchem-570	90	18	course	course	NOUN
eurjchem-570	90	19	of	of	ADP
eurjchem-570	90	20	optimizing	optimize	VERB
eurjchem-570	90	21	the	the	DET
eurjchem-570	90	22	conditions	condition	NOUN
eurjchem-570	90	23	of	of	ADP
eurjchem-570	90	24	the	the	DET
eurjchem-570	90	25	proposed	propose	VERB
eurjchem-570	90	26	method	method	NOUN
eurjchem-570	90	27	.	.	PUNCT
eurjchem-570	91	1	in	in	ADP
eurjchem-570	91	2	the	the	DET
eurjchem-570	91	3	proposed	propose	VERB
eurjchem-570	91	4	lc	lc	NOUN
eurjchem-570	91	5	method	method	NOUN
eurjchem-570	91	6	,	,	PUNCT
eurjchem-570	91	7	system	system	NOUN
eurjchem-570	91	8	suitability	suitability	NOUN
eurjchem-570	91	9	tests	test	NOUN
eurjchem-570	91	10	are	be	AUX
eurjchem-570	91	11	used	use	VERB
eurjchem-570	91	12	to	to	PART
eurjchem-570	91	13	verify	verify	VERB
eurjchem-570	91	14	that	that	DET
eurjchem-570	91	15	resolution	resolution	NOUN
eurjchem-570	91	16	and	and	CCONJ
eurjchem-570	91	17	reproducibility	reproducibility	NOUN
eurjchem-570	91	18	were	be	AUX
eurjchem-570	91	19	adequate	adequate	ADJ
eurjchem-570	91	20	for	for	ADP
eurjchem-570	91	21	analysis	analysis	NOUN
eurjchem-570	91	22	performed	perform	VERB
eurjchem-570	91	23	.	.	PUNCT
eurjchem-570	92	1	different	different	ADJ
eurjchem-570	92	2	parameters	parameter	NOUN
eurjchem-570	92	3	affecting	affect	VERB
eurjchem-570	92	4	the	the	DET
eurjchem-570	92	5	chromatographic	chromatographic	ADJ
eurjchem-570	92	6	separation	separation	NOUN
eurjchem-570	92	7	were	be	AUX
eurjchem-570	92	8	studied	study	VERB
eurjchem-570	92	9	.	.	PUNCT
eurjchem-570	93	1	the	the	DET
eurjchem-570	93	2	parameters	parameter	NOUN
eurjchem-570	93	3	of	of	ADP
eurjchem-570	93	4	this	this	DET
eurjchem-570	93	5	test	test	NOUN
eurjchem-570	93	6	are	be	AUX
eurjchem-570	93	7	column	column	NOUN
eurjchem-570	93	8	efficiency	efficiency	NOUN
eurjchem-570	93	9	(	(	PUNCT
eurjchem-570	93	10	number	number	NOUN
eurjchem-570	93	11	of	of	ADP
eurjchem-570	93	12	theoretical	theoretical	ADJ
eurjchem-570	93	13	plates	plate	NOUN
eurjchem-570	93	14	)	)	PUNCT
eurjchem-570	93	15	,	,	PUNCT
eurjchem-570	93	16	tailing	tail	VERB
eurjchem-570	93	17	of	of	ADP
eurjchem-570	93	18	chromatographic	chromatographic	ADJ
eurjchem-570	93	19	peak	peak	NOUN
eurjchem-570	93	20	,	,	PUNCT
eurjchem-570	93	21	peak	peak	NOUN
eurjchem-570	93	22	resolution	resolution	NOUN
eurjchem-570	93	23	factor	factor	NOUN
eurjchem-570	93	24	,	,	PUNCT
eurjchem-570	93	25	and	and	CCONJ
eurjchem-570	93	26	repeatability	repeatability	NOUN
eurjchem-570	93	27	as	as	ADP
eurjchem-570	93	28	%	%	NOUN
eurjchem-570	93	29	r.s.d	r.s.d	NOUN
eurjchem-570	93	30	.	.	PUNCT
eurjchem-570	94	1	of	of	ADP
eurjchem-570	94	2	peak	peak	NOUN
eurjchem-570	94	3	areas	area	NOUN
eurjchem-570	94	4	for	for	ADP
eurjchem-570	94	5	six	six	NUM
eurjchem-570	94	6	injections	injection	NOUN
eurjchem-570	94	7	and	and	CCONJ
eurjchem-570	94	8	reproducibility	reproducibility	NOUN
eurjchem-570	94	9	of	of	ADP
eurjchem-570	94	10	retention	retention	NOUN
eurjchem-570	94	11	times	time	NOUN
eurjchem-570	94	12	.	.	PUNCT
eurjchem-570	95	1	the	the	DET
eurjchem-570	95	2	results	result	NOUN
eurjchem-570	95	3	of	of	ADP
eurjchem-570	95	4	these	these	DET
eurjchem-570	95	5	tests	test	NOUN
eurjchem-570	95	6	are	be	AUX
eurjchem-570	95	7	listed	list	VERB
eurjchem-570	95	8	in	in	ADP
eurjchem-570	95	9	table	table	NOUN
eurjchem-570	95	10	1	1	NUM
eurjchem-570	95	11	and	and	CCONJ
eurjchem-570	95	12	2	2	NUM
eurjchem-570	95	13	.	.	NOUN
eurjchem-570	95	14	3.3	3.3	NUM
eurjchem-570	95	15	.	.	PUNCT
eurjchem-570	96	1	method	method	NOUN
eurjchem-570	96	2	validation	validation	NOUN
eurjchem-570	96	3	3.3.1	3.3.1	PROPN
eurjchem-570	96	4	.	.	PUNCT
eurjchem-570	97	1	linearity	linearity	NOUN
eurjchem-570	97	2	linearity	linearity	PROPN
eurjchem-570	97	3	was	be	AUX
eurjchem-570	97	4	studied	study	VERB
eurjchem-570	97	5	for	for	ADP
eurjchem-570	97	6	vdg	vdg	NOUN
eurjchem-570	97	7	,	,	PUNCT
eurjchem-570	97	8	sxg	sxg	ADJ
eurjchem-570	97	9	and	and	CCONJ
eurjchem-570	97	10	met	meet	VERB
eurjchem-570	97	11	.	.	PUNCT
eurjchem-570	98	1	a	a	DET
eurjchem-570	98	2	linear	linear	ADJ
eurjchem-570	98	3	relationship	relationship	NOUN
eurjchem-570	98	4	between	between	ADP
eurjchem-570	98	5	area	area	NOUN
eurjchem-570	98	6	under	under	ADP
eurjchem-570	98	7	the	the	DET
eurjchem-570	98	8	peak	peak	NOUN
eurjchem-570	98	9	(	(	PUNCT
eurjchem-570	98	10	aup	aup	PROPN
eurjchem-570	98	11	)	)	PUNCT
eurjchem-570	98	12	and	and	CCONJ
eurjchem-570	98	13	component	component	NOUN
eurjchem-570	98	14	concentration	concentration	NOUN
eurjchem-570	98	15	(	(	PUNCT
eurjchem-570	98	16	c	c	NOUN
eurjchem-570	98	17	)	)	PUNCT
eurjchem-570	98	18	was	be	AUX
eurjchem-570	98	19	obtained	obtain	VERB
eurjchem-570	98	20	.	.	PUNCT
eurjchem-570	99	1	the	the	DET
eurjchem-570	99	2	regression	regression	NOUN
eurjchem-570	99	3	equations	equation	NOUN
eurjchem-570	99	4	were	be	AUX
eurjchem-570	99	5	also	also	ADV
eurjchem-570	99	6	computed	compute	VERB
eurjchem-570	99	7	.	.	PUNCT
eurjchem-570	100	1	the	the	DET
eurjchem-570	100	2	linearity	linearity	NOUN
eurjchem-570	100	3	of	of	ADP
eurjchem-570	100	4	the	the	DET
eurjchem-570	100	5	calibration	calibration	NOUN
eurjchem-570	100	6	curves	curve	NOUN
eurjchem-570	100	7	were	be	AUX
eurjchem-570	100	8	validated	validate	VERB
eurjchem-570	100	9	by	by	ADP
eurjchem-570	100	10	the	the	DET
eurjchem-570	100	11	high	high	ADJ
eurjchem-570	100	12	value	value	NOUN
eurjchem-570	100	13	of	of	ADP
eurjchem-570	100	14	correlation	correlation	NOUN
eurjchem-570	100	15	coefficients	coefficient	NOUN
eurjchem-570	100	16	.	.	PUNCT
eurjchem-570	101	1	the	the	DET
eurjchem-570	101	2	analytical	analytical	ADJ
eurjchem-570	101	3	data	datum	NOUN
eurjchem-570	101	4	of	of	ADP
eurjchem-570	101	5	the	the	DET
eurjchem-570	101	6	calibration	calibration	NOUN
eurjchem-570	101	7	curves	curve	NOUN
eurjchem-570	101	8	including	include	VERB
eurjchem-570	101	9	standard	standard	ADJ
eurjchem-570	101	10	deviations	deviation	NOUN
eurjchem-570	101	11	for	for	ADP
eurjchem-570	101	12	the	the	DET
eurjchem-570	101	13	slope	slope	NOUN
eurjchem-570	101	14	and	and	CCONJ
eurjchem-570	101	15	intercept	intercept	PROPN
eurjchem-570	101	16	(	(	PUNCT
eurjchem-570	101	17	sb	sb	PROPN
eurjchem-570	101	18	,	,	PUNCT
eurjchem-570	101	19	sa	sa	PROPN
eurjchem-570	101	20	)	)	PUNCT
eurjchem-570	101	21	are	be	AUX
eurjchem-570	101	22	summarized	summarize	VERB
eurjchem-570	101	23	in	in	ADP
eurjchem-570	101	24	table	table	NOUN
eurjchem-570	101	25	3	3	NUM
eurjchem-570	101	26	.	.	NOUN
eurjchem-570	102	1	3.3.2	3.3.2	NUM
eurjchem-570	102	2	.	.	PUNCT
eurjchem-570	103	1	accuracy	accuracy	NOUN
eurjchem-570	103	2	accuracy	accuracy	NOUN
eurjchem-570	103	3	of	of	ADP
eurjchem-570	103	4	the	the	DET
eurjchem-570	103	5	results	result	NOUN
eurjchem-570	103	6	was	be	AUX
eurjchem-570	103	7	calculated	calculate	VERB
eurjchem-570	103	8	by	by	ADP
eurjchem-570	103	9	%	%	NOUN
eurjchem-570	103	10	recovery	recovery	NOUN
eurjchem-570	103	11	of	of	ADP
eurjchem-570	103	12	five	five	NUM
eurjchem-570	103	13	different	different	ADJ
eurjchem-570	103	14	samples	sample	NOUN
eurjchem-570	103	15	of	of	ADP
eurjchem-570	103	16	the	the	DET
eurjchem-570	103	17	laboratory	laboratory	NOUN
eurjchem-570	103	18	prepared	prepare	VERB
eurjchem-570	103	19	mixtures	mixture	NOUN
eurjchem-570	103	20	of	of	ADP
eurjchem-570	103	21	vld	vld	NOUN
eurjchem-570	103	22	and	and	CCONJ
eurjchem-570	103	23	sxg	sxg	NOUN
eurjchem-570	103	24	in	in	ADP
eurjchem-570	103	25	their	their	PRON
eurjchem-570	103	26	binary	binary	ADJ
eurjchem-570	103	27	mixture	mixture	NOUN
eurjchem-570	103	28	with	with	ADP
eurjchem-570	103	29	met	meet	VERB
eurjchem-570	103	30	and	and	CCONJ
eurjchem-570	103	31	also	also	ADV
eurjchem-570	103	32	by	by	ADP
eurjchem-570	103	33	standard	standard	ADJ
eurjchem-570	103	34	addition	addition	NOUN
eurjchem-570	103	35	technique	technique	NOUN
eurjchem-570	103	36	for	for	ADP
eurjchem-570	103	37	eucreas	eucreas	ADJ
eurjchem-570	103	38	®	®	NOUN
eurjchem-570	103	39	and	and	CCONJ
eurjchem-570	103	40	kombiglyze	kombiglyze	VERB
eurjchem-570	103	41	®	®	NOUN
eurjchem-570	103	42	tablets	tablet	NOUN
eurjchem-570	103	43	.	.	PUNCT
eurjchem-570	104	1	the	the	DET
eurjchem-570	104	2	results	result	NOUN
eurjchem-570	104	3	obtained	obtain	VERB
eurjchem-570	104	4	including	include	VERB
eurjchem-570	104	5	the	the	DET
eurjchem-570	104	6	mean	mean	NOUN
eurjchem-570	104	7	of	of	ADP
eurjchem-570	104	8	the	the	DET
eurjchem-570	104	9	recovery	recovery	NOUN
eurjchem-570	104	10	and	and	CCONJ
eurjchem-570	104	11	relative	relative	ADJ
eurjchem-570	104	12	standard	standard	ADJ
eurjchem-570	104	13	deviation	deviation	NOUN
eurjchem-570	104	14	are	be	AUX
eurjchem-570	104	15	displayed	display	VERB
eurjchem-570	104	16	in	in	ADP
eurjchem-570	104	17	table	table	NOUN
eurjchem-570	104	18	3	3	NUM
eurjchem-570	104	19	.	.	X
eurjchem-570	105	1	3.3.3	3.3.3	NUM
eurjchem-570	105	2	.	.	PUNCT
eurjchem-570	105	3	precision	precision	VERB
eurjchem-570	105	4	the	the	DET
eurjchem-570	105	5	repeatability	repeatability	NOUN
eurjchem-570	105	6	of	of	ADP
eurjchem-570	105	7	the	the	DET
eurjchem-570	105	8	method	method	NOUN
eurjchem-570	105	9	was	be	AUX
eurjchem-570	105	10	assessed	assess	VERB
eurjchem-570	105	11	by	by	ADP
eurjchem-570	105	12	analyzing	analyze	VERB
eurjchem-570	105	13	100	100	NUM
eurjchem-570	105	14	µg	µg	NOUN
eurjchem-570	105	15	/	/	SYM
eurjchem-570	105	16	ml	ml	NOUN
eurjchem-570	105	17	of	of	ADP
eurjchem-570	105	18	vlg	vlg	PROPN
eurjchem-570	105	19	,	,	PUNCT
eurjchem-570	105	20	11.16	11.16	NUM
eurjchem-570	105	21	µg	µg	NOUN
eurjchem-570	105	22	/	/	SYM
eurjchem-570	105	23	ml	ml	NOUN
eurjchem-570	105	24	of	of	ADP
eurjchem-570	105	25	sxg	sxg	NOUN
eurjchem-570	105	26	and	and	CCONJ
eurjchem-570	105	27	1000	1000	NUM
eurjchem-570	105	28	µg	µg	NOUN
eurjchem-570	105	29	/	/	SYM
eurjchem-570	105	30	ml	ml	NOUN
eurjchem-570	105	31	of	of	ADP
eurjchem-570	105	32	met	meet	VERB
eurjchem-570	105	33	(	(	PUNCT
eurjchem-570	105	34	n	n	NOUN
eurjchem-570	105	35	=	=	SYM
eurjchem-570	105	36	6	6	NUM
eurjchem-570	105	37	)	)	PUNCT
eurjchem-570	105	38	.	.	PUNCT
eurjchem-570	106	1	the	the	DET
eurjchem-570	106	2	values	value	NOUN
eurjchem-570	106	3	of	of	ADP
eurjchem-570	106	4	the	the	DET
eurjchem-570	106	5	precision	precision	NOUN
eurjchem-570	106	6	(	(	PUNCT
eurjchem-570	106	7	%	%	INTJ
eurjchem-570	106	8	r.s.d	r.s.d	NOUN
eurjchem-570	106	9	.	.	PUNCT
eurjchem-570	106	10	)	)	PUNCT
eurjchem-570	107	1	of	of	ADP
eurjchem-570	107	2	repeatability	repeatability	NOUN
eurjchem-570	107	3	,	,	PUNCT
eurjchem-570	107	4	inter‐day	inter‐day	NOUN
eurjchem-570	107	5	and	and	CCONJ
eurjchem-570	107	6	intra‐day	intra‐day	PROPN
eurjchem-570	107	7	precision	precision	NOUN
eurjchem-570	107	8	(	(	PUNCT
eurjchem-570	107	9	using	use	VERB
eurjchem-570	107	10	three	three	NUM
eurjchem-570	107	11	different	different	ADJ
eurjchem-570	107	12	concentrations	concentration	NOUN
eurjchem-570	107	13	in	in	ADP
eurjchem-570	107	14	triplicates	triplicate	NOUN
eurjchem-570	107	15	for	for	ADP
eurjchem-570	107	16	three	three	NUM
eurjchem-570	107	17	days	day	NOUN
eurjchem-570	107	18	)	)	PUNCT
eurjchem-570	107	19	are	be	AUX
eurjchem-570	107	20	displayed	display	VERB
eurjchem-570	107	21	in	in	ADP
eurjchem-570	107	22	table	table	NOUN
eurjchem-570	107	23	1‐3	1‐3	PROPN
eurjchem-570	107	24	.	.	PUNCT
eurjchem-570	108	1	3.3.4	3.3.4	NUM
eurjchem-570	108	2	.	.	PUNCT
eurjchem-570	108	3	specificity	specificity	NOUN
eurjchem-570	108	4	specificity	specificity	NOUN
eurjchem-570	108	5	is	be	AUX
eurjchem-570	108	6	the	the	DET
eurjchem-570	108	7	ability	ability	NOUN
eurjchem-570	108	8	of	of	ADP
eurjchem-570	108	9	the	the	DET
eurjchem-570	108	10	analytical	analytical	ADJ
eurjchem-570	108	11	method	method	NOUN
eurjchem-570	108	12	to	to	PART
eurjchem-570	108	13	measure	measure	VERB
eurjchem-570	108	14	the	the	DET
eurjchem-570	108	15	analyte	analyte	NOUN
eurjchem-570	108	16	response	response	NOUN
eurjchem-570	108	17	in	in	ADP
eurjchem-570	108	18	the	the	DET
eurjchem-570	108	19	presence	presence	NOUN
eurjchem-570	108	20	of	of	ADP
eurjchem-570	108	21	interferences	interference	NOUN
eurjchem-570	108	22	.	.	PUNCT
eurjchem-570	109	1	due	due	ADP
eurjchem-570	109	2	to	to	ADP
eurjchem-570	109	3	lack	lack	NOUN
eurjchem-570	109	4	of	of	ADP
eurjchem-570	109	5	the	the	DET
eurjchem-570	109	6	degradation	degradation	NOUN
eurjchem-570	109	7	profile	profile	NOUN
eurjchem-570	109	8	of	of	ADP
eurjchem-570	109	9	the	the	DET
eurjchem-570	109	10	studied	study	VERB
eurjchem-570	109	11	gliptins	gliptin	NOUN
eurjchem-570	109	12	,	,	PUNCT
eurjchem-570	109	13	interferences	interference	NOUN
eurjchem-570	109	14	due	due	ADP
eurjchem-570	109	15	to	to	ADP
eurjchem-570	109	16	the	the	DET
eurjchem-570	109	17	degradation	degradation	NOUN
eurjchem-570	109	18	products	product	NOUN
eurjchem-570	109	19	could	could	AUX
eurjchem-570	109	20	not	not	PART
eurjchem-570	109	21	be	be	AUX
eurjchem-570	109	22	studied	study	VERB
eurjchem-570	109	23	.	.	PUNCT
eurjchem-570	110	1	in	in	ADP
eurjchem-570	110	2	the	the	DET
eurjchem-570	110	3	present	present	ADJ
eurjchem-570	110	4	work	work	NOUN
eurjchem-570	110	5	,	,	PUNCT
eurjchem-570	110	6	specificity	specificity	NOUN
eurjchem-570	110	7	was	be	AUX
eurjchem-570	110	8	checked	check	VERB
eurjchem-570	110	9	by	by	ADP
eurjchem-570	110	10	analyzing	analyze	VERB
eurjchem-570	110	11	vdg	vdg	NOUN
eurjchem-570	110	12	with	with	ADP
eurjchem-570	110	13	met	meet	VERB
eurjchem-570	110	14	and	and	CCONJ
eurjchem-570	110	15	sxg	sxg	ADJ
eurjchem-570	110	16	with	with	ADP
eurjchem-570	110	17	met	meet	VERB
eurjchem-570	110	18	in	in	ADP
eurjchem-570	110	19	laboratory	laboratory	NOUN
eurjchem-570	110	20	prepared	prepare	VERB
eurjchem-570	110	21	mixtures	mixture	NOUN
eurjchem-570	110	22	.	.	PUNCT
eurjchem-570	111	1	good	good	ADJ
eurjchem-570	111	2	resolution	resolution	NOUN
eurjchem-570	111	3	and	and	CCONJ
eurjchem-570	111	4	absence	absence	NOUN
eurjchem-570	111	5	of	of	ADP
eurjchem-570	111	6	interference	interference	NOUN
eurjchem-570	111	7	between	between	ADP
eurjchem-570	111	8	drugs	drug	NOUN
eurjchem-570	111	9	being	be	AUX
eurjchem-570	111	10	analyzed	analyze	VERB
eurjchem-570	111	11	are	be	AUX
eurjchem-570	111	12	shown	show	VERB
eurjchem-570	111	13	in	in	ADP
eurjchem-570	111	14	figure	figure	NOUN
eurjchem-570	111	15	2	2	NUM
eurjchem-570	111	16	and	and	CCONJ
eurjchem-570	111	17	3	3	NUM
eurjchem-570	111	18	.	.	X
eurjchem-570	112	1	besides	besides	SCONJ
eurjchem-570	112	2	,	,	PUNCT
eurjchem-570	112	3	the	the	DET
eurjchem-570	112	4	chromatograms	chromatogram	NOUN
eurjchem-570	112	5	of	of	ADP
eurjchem-570	112	6	the	the	DET
eurjchem-570	112	7	pharmaceutical	pharmaceutical	ADJ
eurjchem-570	112	8	formulation	formulation	NOUN
eurjchem-570	112	9	samples	sample	NOUN
eurjchem-570	112	10	were	be	AUX
eurjchem-570	112	11	checked	check	VERB
eurjchem-570	112	12	for	for	ADP
eurjchem-570	112	13	the	the	DET
eurjchem-570	112	14	appearance	appearance	NOUN
eurjchem-570	112	15	of	of	ADP
eurjchem-570	112	16	any	any	DET
eurjchem-570	112	17	extra	extra	ADJ
eurjchem-570	112	18	peaks	peak	NOUN
eurjchem-570	112	19	.	.	PUNCT
eurjchem-570	113	1	no	no	DET
eurjchem-570	113	2	chromatographic	chromatographic	ADJ
eurjchem-570	113	3	interference	interference	NOUN
eurjchem-570	113	4	from	from	ADP
eurjchem-570	113	5	any	any	PRON
eurjchem-570	113	6	of	of	ADP
eurjchem-570	113	7	the	the	DET
eurjchem-570	113	8	excipients	excipient	NOUN
eurjchem-570	113	9	was	be	AUX
eurjchem-570	113	10	found	find	VERB
eurjchem-570	113	11	at	at	ADP
eurjchem-570	113	12	the	the	DET
eurjchem-570	113	13	retention	retention	NOUN
eurjchem-570	113	14	times	time	NOUN
eurjchem-570	113	15	of	of	ADP
eurjchem-570	113	16	the	the	DET
eurjchem-570	113	17	examined	examine	VERB
eurjchem-570	113	18	drugs	drug	NOUN
eurjchem-570	113	19	(	(	PUNCT
eurjchem-570	113	20	figure	figure	NOUN
eurjchem-570	113	21	2	2	NUM
eurjchem-570	113	22	and	and	CCONJ
eurjchem-570	113	23	3	3	NUM
eurjchem-570	113	24	)	)	PUNCT
eurjchem-570	113	25	.	.	PUNCT
eurjchem-570	114	1	mohammad	mohammad	PROPN
eurjchem-570	114	2	et	et	PROPN
eurjchem-570	114	3	al	al	PROPN
eurjchem-570	114	4	.	.	PUNCT
eurjchem-570	114	5	/	/	SYM
eurjchem-570	114	6	european	european	PROPN
eurjchem-570	114	7	journal	journal	PROPN
eurjchem-570	114	8	of	of	ADP
eurjchem-570	114	9	chemistry	chemistry	NOUN
eurjchem-570	114	10	3	3	NUM
eurjchem-570	114	11	(	(	PUNCT
eurjchem-570	114	12	2	2	NUM
eurjchem-570	114	13	)	)	PUNCT
eurjchem-570	114	14	(	(	PUNCT
eurjchem-570	114	15	2012	2012	NUM
eurjchem-570	114	16	)	)	PUNCT
eurjchem-570	114	17	152‐155	152‐155	NUM
eurjchem-570	114	18	155	155	NUM
eurjchem-570	114	19	table	table	NOUN
eurjchem-570	114	20	4	4	NUM
eurjchem-570	114	21	.	.	PUNCT
eurjchem-570	115	1	statistical	statistical	ADJ
eurjchem-570	115	2	comparison	comparison	NOUN
eurjchem-570	115	3	between	between	ADP
eurjchem-570	115	4	the	the	DET
eurjchem-570	115	5	results	result	NOUN
eurjchem-570	115	6	of	of	ADP
eurjchem-570	115	7	the	the	DET
eurjchem-570	115	8	proposed	propose	VERB
eurjchem-570	115	9	lc	lc	NOUN
eurjchem-570	115	10	method	method	NOUN
eurjchem-570	115	11	and	and	CCONJ
eurjchem-570	115	12	the	the	DET
eurjchem-570	115	13	reference	reference	NOUN
eurjchem-570	115	14	method	method	NOUN
eurjchem-570	115	15	for	for	ADP
eurjchem-570	115	16	the	the	DET
eurjchem-570	115	17	determination	determination	NOUN
eurjchem-570	115	18	of	of	ADP
eurjchem-570	115	19	metformin	metformin	NOUN
eurjchem-570	115	20	.	.	PUNCT
eurjchem-570	116	1	statistical	statistical	ADJ
eurjchem-570	116	2	term	term	NOUN
eurjchem-570	116	3	reference	reference	NOUN
eurjchem-570	116	4	methodb	methodb	NOUN
eurjchem-570	116	5	proposed	propose	VERB
eurjchem-570	116	6	method	method	NOUN
eurjchem-570	116	7	mean	mean	VERB
eurjchem-570	116	8	100.4	100.4	NUM
eurjchem-570	116	9	100.12	100.12	NUM
eurjchem-570	116	10	s.d	s.d	PROPN
eurjchem-570	116	11	.	.	PROPN
eurjchem-570	116	12	±	±	PROPN
eurjchem-570	116	13	0.28	0.28	NUM
eurjchem-570	116	14	0.99	0.99	NUM
eurjchem-570	116	15	s.e	s.e	PROPN
eurjchem-570	116	16	.	.	PROPN
eurjchem-570	116	17	±	±	PROPN
eurjchem-570	116	18	0.13	0.13	NUM
eurjchem-570	116	19	0.44	0.44	NUM
eurjchem-570	116	20	%	%	NOUN
eurjchem-570	116	21	r.s.d	r.s.d	NOUN
eurjchem-570	116	22	.	.	PUNCT
eurjchem-570	117	1	0.28	0.28	NUM
eurjchem-570	117	2	0.99	0.99	NUM
eurjchem-570	117	3	n	n	NOUN
eurjchem-570	117	4	5	5	NUM
eurjchem-570	117	5	5	5	NUM
eurjchem-570	117	6	v	v	ADP
eurjchem-570	117	7	0.08	0.08	NUM
eurjchem-570	117	8	0.98	0.98	NUM
eurjchem-570	117	9	t	t	NOUN
eurjchem-570	117	10	(	(	PUNCT
eurjchem-570	117	11	a	a	DET
eurjchem-570	117	12	2.306	2.306	NUM
eurjchem-570	117	13	)	)	PUNCT
eurjchem-570	117	14	‐	‐	NOUN
eurjchem-570	117	15	0.61	0.61	NUM
eurjchem-570	117	16	f	f	NOUN
eurjchem-570	117	17	(	(	PUNCT
eurjchem-570	117	18	a	a	DET
eurjchem-570	117	19	6.39	6.39	NUM
eurjchem-570	117	20	)	)	PUNCT
eurjchem-570	117	21	‐	‐	NOUN
eurjchem-570	117	22	0.08	0.08	NUM
eurjchem-570	117	23	a	a	DET
eurjchem-570	117	24	figures	figure	NOUN
eurjchem-570	117	25	in	in	ADP
eurjchem-570	117	26	parentheses	parenthesis	NOUN
eurjchem-570	117	27	are	be	AUX
eurjchem-570	117	28	the	the	DET
eurjchem-570	117	29	theoretical	theoretical	ADJ
eurjchem-570	117	30	t	t	NOUN
eurjchem-570	117	31	and	and	CCONJ
eurjchem-570	117	32	f	f	PROPN
eurjchem-570	117	33	values	value	NOUN
eurjchem-570	117	34	at	at	ADP
eurjchem-570	117	35	(	(	PUNCT
eurjchem-570	117	36	p=0.05	p=0.05	NOUN
eurjchem-570	117	37	)	)	PUNCT
eurjchem-570	117	38	.	.	PUNCT
eurjchem-570	118	1	b	b	X
eurjchem-570	118	2	reference	reference	NOUN
eurjchem-570	118	3	method	method	NOUN
eurjchem-570	118	4	for	for	ADP
eurjchem-570	118	5	the	the	DET
eurjchem-570	118	6	spectrophotometric	spectrophotometric	ADJ
eurjchem-570	118	7	determination	determination	NOUN
eurjchem-570	118	8	of	of	ADP
eurjchem-570	118	9	metformin	metformin	NOUN
eurjchem-570	118	10	in	in	ADP
eurjchem-570	118	11	the	the	DET
eurjchem-570	118	12	indian	indian	ADJ
eurjchem-570	118	13	pharmacopeia	pharmacopeia	NOUN
eurjchem-570	118	14	[	[	X
eurjchem-570	118	15	18	18	NUM
eurjchem-570	118	16	]	]	PUNCT
eurjchem-570	118	17	.	.	PUNCT
eurjchem-570	119	1	table	table	NOUN
eurjchem-570	119	2	5	5	NUM
eurjchem-570	119	3	.	.	PUNCT
eurjchem-570	120	1	statistical	statistical	ADJ
eurjchem-570	120	2	comparison	comparison	NOUN
eurjchem-570	120	3	between	between	ADP
eurjchem-570	120	4	the	the	DET
eurjchem-570	120	5	results	result	NOUN
eurjchem-570	120	6	of	of	ADP
eurjchem-570	120	7	the	the	DET
eurjchem-570	120	8	lc	lc	NOUN
eurjchem-570	120	9	method	method	NOUN
eurjchem-570	120	10	and	and	CCONJ
eurjchem-570	120	11	the	the	DET
eurjchem-570	120	12	reference	reference	NOUN
eurjchem-570	120	13	methods	method	NOUN
eurjchem-570	120	14	for	for	ADP
eurjchem-570	120	15	the	the	DET
eurjchem-570	120	16	determination	determination	NOUN
eurjchem-570	120	17	of	of	ADP
eurjchem-570	120	18	vildagliptin	vildagliptin	NOUN
eurjchem-570	120	19	and	and	CCONJ
eurjchem-570	120	20	saxagliptin	saxagliptin	NOUN
eurjchem-570	120	21	.	.	PUNCT
eurjchem-570	121	1	statistical	statistical	ADJ
eurjchem-570	121	2	term	term	NOUN
eurjchem-570	121	3	reference	reference	NOUN
eurjchem-570	121	4	method	method	NOUN
eurjchem-570	121	5	for	for	ADP
eurjchem-570	121	6	vildagliptin	vildagliptin	PROPN
eurjchem-570	121	7	b	b	PROPN
eurjchem-570	121	8	hplc	hplc	NOUN
eurjchem-570	121	9	method	method	NOUN
eurjchem-570	121	10	reference	reference	NOUN
eurjchem-570	121	11	method	method	NOUN
eurjchem-570	121	12	for	for	ADP
eurjchem-570	121	13	saxagliptinc	saxagliptinc	NOUN
eurjchem-570	121	14	hplc	hplc	NOUN
eurjchem-570	121	15	method	method	NOUN
eurjchem-570	121	16	mean	mean	VERB
eurjchem-570	121	17	100.01	100.01	NUM
eurjchem-570	121	18	99.49	99.49	NUM
eurjchem-570	121	19	100.20	100.20	NUM
eurjchem-570	121	20	100.3	100.3	NUM
eurjchem-570	121	21	s.d	s.d	PROPN
eurjchem-570	121	22	.	.	PROPN
eurjchem-570	121	23	±	±	PROPN
eurjchem-570	121	24	0.99	0.99	NUM
eurjchem-570	121	25	0.90	0.90	NUM
eurjchem-570	121	26	1.10	1.10	NUM
eurjchem-570	121	27	1.25	1.25	NUM
eurjchem-570	121	28	s.e	s.e	PROPN
eurjchem-570	121	29	.	.	PROPN
eurjchem-570	121	30	±	±	NUM
eurjchem-570	121	31	0.44	0.44	NUM
eurjchem-570	121	32	0.40	0.40	NUM
eurjchem-570	121	33	0.49	0.49	NUM
eurjchem-570	121	34	0.56	0.56	NUM
eurjchem-570	121	35	%	%	NOUN
eurjchem-570	121	36	rsd	rsd	PROPN
eurjchem-570	121	37	0.99	0.99	NUM
eurjchem-570	121	38	0.90	0.90	NUM
eurjchem-570	121	39	1.1	1.1	NUM
eurjchem-570	121	40	1.25	1.25	NUM
eurjchem-570	121	41	n	n	NOUN
eurjchem-570	121	42	5	5	NUM
eurjchem-570	121	43	5	5	NUM
eurjchem-570	121	44	5	5	NUM
eurjchem-570	121	45	5	5	NUM
eurjchem-570	121	46	v	v	ADP
eurjchem-570	121	47	0.98	0.98	NUM
eurjchem-570	121	48	0.81	0.81	NUM
eurjchem-570	121	49	1.21	1.21	NUM
eurjchem-570	121	50	1.56	1.56	NUM
eurjchem-570	121	51	t	t	NOUN
eurjchem-570	121	52	(	(	PUNCT
eurjchem-570	121	53	a	a	DET
eurjchem-570	121	54	2.306	2.306	NUM
eurjchem-570	121	55	)	)	PUNCT
eurjchem-570	121	56	‐	‐	NOUN
eurjchem-570	121	57	0.87	0.87	NUM
eurjchem-570	121	58	‐	‐	NOUN
eurjchem-570	121	59	0.13	0.13	NUM
eurjchem-570	121	60	f	f	NOUN
eurjchem-570	121	61	(	(	PUNCT
eurjchem-570	121	62	a	a	DET
eurjchem-570	121	63	6.39	6.39	NUM
eurjchem-570	121	64	)	)	PUNCT
eurjchem-570	121	65	‐	‐	NOUN
eurjchem-570	121	66	1.21	1.21	NUM
eurjchem-570	121	67	‐	‐	NOUN
eurjchem-570	121	68	0.78	0.78	NUM
eurjchem-570	121	69	a	a	DET
eurjchem-570	121	70	figures	figure	NOUN
eurjchem-570	121	71	in	in	ADP
eurjchem-570	121	72	parentheses	parenthesis	NOUN
eurjchem-570	121	73	are	be	AUX
eurjchem-570	121	74	the	the	DET
eurjchem-570	121	75	theoretical	theoretical	ADJ
eurjchem-570	121	76	t	t	NOUN
eurjchem-570	121	77	and	and	CCONJ
eurjchem-570	121	78	f	f	PROPN
eurjchem-570	121	79	values	value	NOUN
eurjchem-570	121	80	at	at	ADP
eurjchem-570	121	81	(	(	PUNCT
eurjchem-570	121	82	p=0.05	p=0.05	NOUN
eurjchem-570	121	83	)	)	PUNCT
eurjchem-570	121	84	.	.	PUNCT
eurjchem-570	122	1	b	b	X
eurjchem-570	122	2	reference	reference	NOUN
eurjchem-570	122	3	method	method	NOUN
eurjchem-570	122	4	:	:	PUNCT
eurjchem-570	122	5	aliquots	aliquot	NOUN
eurjchem-570	122	6	of	of	ADP
eurjchem-570	122	7	standard	standard	ADJ
eurjchem-570	122	8	solutions	solution	NOUN
eurjchem-570	122	9	in	in	ADP
eurjchem-570	122	10	distilled	distil	VERB
eurjchem-570	122	11	water	water	NOUN
eurjchem-570	122	12	containing	contain	VERB
eurjchem-570	122	13	5‐25	5‐25	NUM
eurjchem-570	122	14	μg	μg	NOUN
eurjchem-570	122	15	/	/	SYM
eurjchem-570	122	16	ml	ml	ADP
eurjchem-570	122	17	vdg	vdg	NOUN
eurjchem-570	122	18	were	be	AUX
eurjchem-570	122	19	measured	measure	VERB
eurjchem-570	122	20	at	at	ADP
eurjchem-570	122	21	208	208	NUM
eurjchem-570	122	22	nm	nm	NOUN
eurjchem-570	122	23	using	use	VERB
eurjchem-570	122	24	water	water	NOUN
eurjchem-570	122	25	as	as	ADP
eurjchem-570	122	26	a	a	DET
eurjchem-570	122	27	blank	blank	NOUN
eurjchem-570	123	1	[	[	X
eurjchem-570	123	2	3	3	NUM
eurjchem-570	123	3	]	]	PUNCT
eurjchem-570	123	4	.	.	PUNCT
eurjchem-570	124	1	c	c	PROPN
eurjchem-570	124	2	reference	reference	NOUN
eurjchem-570	124	3	method	method	NOUN
eurjchem-570	124	4	:	:	PUNCT
eurjchem-570	124	5	aliquots	aliquot	NOUN
eurjchem-570	124	6	of	of	ADP
eurjchem-570	124	7	standard	standard	ADJ
eurjchem-570	124	8	solutions	solution	NOUN
eurjchem-570	124	9	in	in	ADP
eurjchem-570	124	10	distilled	distil	VERB
eurjchem-570	124	11	water	water	NOUN
eurjchem-570	124	12	containing	contain	VERB
eurjchem-570	124	13	5‐40	5‐40	NUM
eurjchem-570	124	14	μg	μg	NOUN
eurjchem-570	124	15	/	/	SYM
eurjchem-570	124	16	ml	ml	NOUN
eurjchem-570	124	17	sxg	sxg	NOUN
eurjchem-570	124	18	were	be	AUX
eurjchem-570	124	19	measured	measure	VERB
eurjchem-570	124	20	at	at	ADP
eurjchem-570	124	21	208	208	NUM
eurjchem-570	124	22	nm	nm	NOUN
eurjchem-570	124	23	using	use	VERB
eurjchem-570	124	24	methanol	methanol	NOUN
eurjchem-570	124	25	as	as	ADP
eurjchem-570	124	26	a	a	DET
eurjchem-570	124	27	blank	blank	NOUN
eurjchem-570	125	1	[	[	X
eurjchem-570	125	2	8	8	NUM
eurjchem-570	125	3	]	]	PUNCT
eurjchem-570	125	4	.	.	PUNCT
eurjchem-570	126	1	in	in	ADP
eurjchem-570	126	2	addition	addition	NOUN
eurjchem-570	126	3	,	,	PUNCT
eurjchem-570	126	4	the	the	DET
eurjchem-570	126	5	chromatograms	chromatogram	NOUN
eurjchem-570	126	6	of	of	ADP
eurjchem-570	126	7	the	the	DET
eurjchem-570	126	8	drugs	drug	NOUN
eurjchem-570	126	9	in	in	ADP
eurjchem-570	126	10	the	the	DET
eurjchem-570	126	11	samples	sample	NOUN
eurjchem-570	126	12	’	'	PUNCT
eurjchem-570	126	13	solutions	solution	NOUN
eurjchem-570	126	14	were	be	AUX
eurjchem-570	126	15	found	find	VERB
eurjchem-570	126	16	identical	identical	ADJ
eurjchem-570	126	17	to	to	ADP
eurjchem-570	126	18	the	the	DET
eurjchem-570	126	19	chromatograms	chromatogram	NOUN
eurjchem-570	126	20	received	receive	VERB
eurjchem-570	126	21	by	by	ADP
eurjchem-570	126	22	the	the	DET
eurjchem-570	126	23	standard	standard	ADJ
eurjchem-570	126	24	solutions	solution	NOUN
eurjchem-570	126	25	at	at	ADP
eurjchem-570	126	26	the	the	DET
eurjchem-570	126	27	wavelengths	wavelength	NOUN
eurjchem-570	126	28	applied	apply	VERB
eurjchem-570	126	29	.	.	PUNCT
eurjchem-570	127	1	moreover	moreover	ADV
eurjchem-570	127	2	,	,	PUNCT
eurjchem-570	127	3	good	good	ADJ
eurjchem-570	127	4	results	result	NOUN
eurjchem-570	127	5	were	be	AUX
eurjchem-570	127	6	obtained	obtain	VERB
eurjchem-570	127	7	for	for	ADP
eurjchem-570	127	8	the	the	DET
eurjchem-570	127	9	determination	determination	NOUN
eurjchem-570	127	10	of	of	ADP
eurjchem-570	127	11	the	the	DET
eurjchem-570	127	12	cited	cite	VERB
eurjchem-570	127	13	drugs	drug	NOUN
eurjchem-570	127	14	in	in	ADP
eurjchem-570	127	15	the	the	DET
eurjchem-570	127	16	two	two	NUM
eurjchem-570	127	17	dosage	dosage	NOUN
eurjchem-570	127	18	forms	form	NOUN
eurjchem-570	127	19	,	,	PUNCT
eurjchem-570	127	20	table	table	NOUN
eurjchem-570	127	21	3	3	NUM
eurjchem-570	127	22	.	.	PUNCT
eurjchem-570	128	1	these	these	DET
eurjchem-570	128	2	results	result	NOUN
eurjchem-570	128	3	confirm	confirm	VERB
eurjchem-570	128	4	the	the	DET
eurjchem-570	128	5	absence	absence	NOUN
eurjchem-570	128	6	of	of	ADP
eurjchem-570	128	7	interference	interference	NOUN
eurjchem-570	128	8	from	from	ADP
eurjchem-570	128	9	other	other	ADJ
eurjchem-570	128	10	materials	material	NOUN
eurjchem-570	128	11	in	in	ADP
eurjchem-570	128	12	the	the	DET
eurjchem-570	128	13	pharmaceutical	pharmaceutical	NOUN
eurjchem-570	128	14	formulations	formulation	NOUN
eurjchem-570	128	15	and	and	CCONJ
eurjchem-570	128	16	therefore	therefore	ADV
eurjchem-570	128	17	confirm	confirm	VERB
eurjchem-570	128	18	the	the	DET
eurjchem-570	128	19	specificity	specificity	NOUN
eurjchem-570	128	20	of	of	ADP
eurjchem-570	128	21	the	the	DET
eurjchem-570	128	22	two	two	NUM
eurjchem-570	128	23	proposed	propose	VERB
eurjchem-570	128	24	methods	method	NOUN
eurjchem-570	128	25	.	.	PUNCT
eurjchem-570	129	1	3.3.5	3.3.5	X
eurjchem-570	129	2	.	.	PUNCT
eurjchem-570	129	3	robustness	robustness	NOUN
eurjchem-570	129	4	robustness	robustness	NOUN
eurjchem-570	129	5	was	be	AUX
eurjchem-570	129	6	performed	perform	VERB
eurjchem-570	129	7	by	by	ADP
eurjchem-570	129	8	deliberately	deliberately	ADV
eurjchem-570	129	9	changing	change	VERB
eurjchem-570	129	10	the	the	DET
eurjchem-570	129	11	chromatographic	chromatographic	ADJ
eurjchem-570	129	12	conditions	condition	NOUN
eurjchem-570	129	13	.	.	PUNCT
eurjchem-570	130	1	the	the	DET
eurjchem-570	130	2	most	most	ADV
eurjchem-570	130	3	important	important	ADJ
eurjchem-570	130	4	parameter	parameter	NOUN
eurjchem-570	130	5	to	to	PART
eurjchem-570	130	6	be	be	AUX
eurjchem-570	130	7	studied	study	VERB
eurjchem-570	130	8	was	be	AUX
eurjchem-570	130	9	the	the	DET
eurjchem-570	130	10	resolution	resolution	NOUN
eurjchem-570	130	11	factor	factor	NOUN
eurjchem-570	130	12	between	between	ADP
eurjchem-570	130	13	the	the	DET
eurjchem-570	130	14	peaks	peak	NOUN
eurjchem-570	130	15	of	of	ADP
eurjchem-570	130	16	vlg	vlg	PROPN
eurjchem-570	130	17	and	and	CCONJ
eurjchem-570	130	18	met	meet	VERB
eurjchem-570	130	19	and	and	CCONJ
eurjchem-570	130	20	also	also	ADV
eurjchem-570	130	21	between	between	ADP
eurjchem-570	130	22	the	the	DET
eurjchem-570	130	23	peaks	peak	NOUN
eurjchem-570	130	24	of	of	ADP
eurjchem-570	130	25	sxg	sxg	NOUN
eurjchem-570	130	26	and	and	CCONJ
eurjchem-570	130	27	met	meet	VERB
eurjchem-570	130	28	.	.	PUNCT
eurjchem-570	131	1	the	the	DET
eurjchem-570	131	2	flow	flow	NOUN
eurjchem-570	131	3	rate	rate	NOUN
eurjchem-570	131	4	of	of	ADP
eurjchem-570	131	5	the	the	DET
eurjchem-570	131	6	mobile	mobile	ADJ
eurjchem-570	131	7	phase	phase	NOUN
eurjchem-570	131	8	was	be	AUX
eurjchem-570	131	9	changed	change	VERB
eurjchem-570	131	10	from	from	ADP
eurjchem-570	131	11	1.0	1.0	NUM
eurjchem-570	131	12	ml	ml	NOUN
eurjchem-570	131	13	/	/	SYM
eurjchem-570	131	14	min	min	NOUN
eurjchem-570	131	15	to	to	PART
eurjchem-570	131	16	0.8	0.8	NUM
eurjchem-570	131	17	ml	ml	NOUN
eurjchem-570	131	18	/	/	SYM
eurjchem-570	131	19	min	min	NOUN
eurjchem-570	131	20	and	and	CCONJ
eurjchem-570	131	21	1.2	1.2	NUM
eurjchem-570	131	22	ml	ml	NOUN
eurjchem-570	131	23	/	/	SYM
eurjchem-570	131	24	min	min	NOUN
eurjchem-570	131	25	,	,	PUNCT
eurjchem-570	131	26	where	where	SCONJ
eurjchem-570	131	27	resolution	resolution	NOUN
eurjchem-570	131	28	factors	factor	NOUN
eurjchem-570	131	29	obtained	obtain	VERB
eurjchem-570	131	30	were	be	AUX
eurjchem-570	131	31	(	(	PUNCT
eurjchem-570	131	32	3.1‐3.9	3.1‐3.9	NUM
eurjchem-570	131	33	)	)	PUNCT
eurjchem-570	131	34	,	,	PUNCT
eurjchem-570	131	35	(	(	PUNCT
eurjchem-570	131	36	3.25‐4.11	3.25‐4.11	NUM
eurjchem-570	131	37	)	)	PUNCT
eurjchem-570	131	38	and	and	CCONJ
eurjchem-570	131	39	(	(	PUNCT
eurjchem-570	131	40	3.15‐3.87	3.15‐3.87	NUM
eurjchem-570	131	41	)	)	PUNCT
eurjchem-570	131	42	,	,	PUNCT
eurjchem-570	131	43	respectively	respectively	ADV
eurjchem-570	131	44	.	.	PUNCT
eurjchem-570	132	1	the	the	DET
eurjchem-570	132	2	organic	organic	ADJ
eurjchem-570	132	3	strength	strength	NOUN
eurjchem-570	132	4	was	be	AUX
eurjchem-570	132	5	changed	change	VERB
eurjchem-570	132	6	by	by	ADP
eurjchem-570	132	7	±%2	±%2	PROPN
eurjchem-570	132	8	,	,	PUNCT
eurjchem-570	132	9	where	where	SCONJ
eurjchem-570	132	10	resolution	resolution	NOUN
eurjchem-570	132	11	factors	factor	NOUN
eurjchem-570	132	12	obtained	obtain	VERB
eurjchem-570	132	13	were	be	AUX
eurjchem-570	132	14	(	(	PUNCT
eurjchem-570	132	15	3.1‐3.9	3.1‐3.9	NUM
eurjchem-570	132	16	)	)	PUNCT
eurjchem-570	132	17	,	,	PUNCT
eurjchem-570	132	18	(	(	PUNCT
eurjchem-570	132	19	3.22‐3.78	3.22‐3.78	NUM
eurjchem-570	132	20	)	)	PUNCT
eurjchem-570	132	21	and	and	CCONJ
eurjchem-570	132	22	(	(	PUNCT
eurjchem-570	132	23	3.1‐4.0	3.1‐4.0	NUM
eurjchem-570	132	24	)	)	PUNCT
eurjchem-570	132	25	respectively	respectively	ADV
eurjchem-570	132	26	.	.	PUNCT
eurjchem-570	133	1	finally	finally	ADV
eurjchem-570	133	2	,	,	PUNCT
eurjchem-570	133	3	a	a	DET
eurjchem-570	133	4	value	value	NOUN
eurjchem-570	133	5	of	of	ADP
eurjchem-570	133	6	ph	ph	NOUN
eurjchem-570	133	7	of	of	ADP
eurjchem-570	133	8	the	the	DET
eurjchem-570	133	9	phosphate	phosphate	ADJ
eurjchem-570	133	10	buffer	buffer	NOUN
eurjchem-570	133	11	was	be	AUX
eurjchem-570	133	12	varied	varied	ADJ
eurjchem-570	133	13	from	from	ADP
eurjchem-570	133	14	4.6	4.6	NUM
eurjchem-570	133	15	to	to	ADP
eurjchem-570	133	16	4.5	4.5	NUM
eurjchem-570	133	17	and	and	CCONJ
eurjchem-570	133	18	4.7	4.7	NUM
eurjchem-570	133	19	,	,	PUNCT
eurjchem-570	133	20	where	where	SCONJ
eurjchem-570	133	21	resolution	resolution	NOUN
eurjchem-570	133	22	factors	factor	NOUN
eurjchem-570	133	23	obtained	obtain	VERB
eurjchem-570	133	24	were	be	AUX
eurjchem-570	133	25	(	(	PUNCT
eurjchem-570	133	26	3.1‐	3.1‐	NUM
eurjchem-570	133	27	3.9	3.9	NUM
eurjchem-570	133	28	)	)	PUNCT
eurjchem-570	133	29	,	,	PUNCT
eurjchem-570	133	30	(	(	PUNCT
eurjchem-570	133	31	3.05‐4.25	3.05‐4.25	NOUN
eurjchem-570	133	32	)	)	PUNCT
eurjchem-570	133	33	and	and	CCONJ
eurjchem-570	133	34	(	(	PUNCT
eurjchem-570	133	35	2.95‐3.18	2.95‐3.18	NOUN
eurjchem-570	133	36	)	)	PUNCT
eurjchem-570	133	37	,	,	PUNCT
eurjchem-570	133	38	respectively	respectively	ADV
eurjchem-570	133	39	.	.	PUNCT
eurjchem-570	134	1	as	as	SCONJ
eurjchem-570	134	2	it	it	PRON
eurjchem-570	134	3	can	can	AUX
eurjchem-570	134	4	be	be	AUX
eurjchem-570	134	5	seen	see	VERB
eurjchem-570	134	6	from	from	ADP
eurjchem-570	134	7	these	these	DET
eurjchem-570	134	8	results	result	NOUN
eurjchem-570	134	9	,	,	PUNCT
eurjchem-570	134	10	good	good	ADJ
eurjchem-570	134	11	values	value	NOUN
eurjchem-570	134	12	of	of	ADP
eurjchem-570	134	13	the	the	DET
eurjchem-570	134	14	resolution	resolution	NOUN
eurjchem-570	134	15	factor	factor	NOUN
eurjchem-570	134	16	were	be	AUX
eurjchem-570	134	17	obtained	obtain	VERB
eurjchem-570	134	18	for	for	ADP
eurjchem-570	134	19	all	all	DET
eurjchem-570	134	20	these	these	DET
eurjchem-570	134	21	variations	variation	NOUN
eurjchem-570	134	22	,	,	PUNCT
eurjchem-570	134	23	indicating	indicate	VERB
eurjchem-570	134	24	good	good	ADJ
eurjchem-570	134	25	robustness	robustness	NOUN
eurjchem-570	134	26	of	of	ADP
eurjchem-570	134	27	the	the	DET
eurjchem-570	134	28	proposed	propose	VERB
eurjchem-570	134	29	lc	lc	NOUN
eurjchem-570	134	30	method	method	NOUN
eurjchem-570	134	31	.	.	PUNCT
eurjchem-570	135	1	3.3.6	3.3.6	X
eurjchem-570	135	2	.	.	PUNCT
eurjchem-570	136	1	limit	limit	NOUN
eurjchem-570	136	2	of	of	ADP
eurjchem-570	136	3	detection	detection	NOUN
eurjchem-570	136	4	and	and	CCONJ
eurjchem-570	136	5	limit	limit	NOUN
eurjchem-570	136	6	of	of	ADP
eurjchem-570	136	7	quantification	quantification	NOUN
eurjchem-570	136	8	limit	limit	NOUN
eurjchem-570	136	9	of	of	ADP
eurjchem-570	136	10	detection	detection	NOUN
eurjchem-570	136	11	(	(	PUNCT
eurjchem-570	136	12	lod	lod	PROPN
eurjchem-570	136	13	)	)	PUNCT
eurjchem-570	136	14	which	which	PRON
eurjchem-570	136	15	represents	represent	VERB
eurjchem-570	136	16	the	the	DET
eurjchem-570	136	17	concentration	concentration	NOUN
eurjchem-570	136	18	of	of	ADP
eurjchem-570	136	19	analyte	analyte	NOUN
eurjchem-570	136	20	at	at	ADP
eurjchem-570	136	21	s	s	PROPN
eurjchem-570	136	22	/	/	SYM
eurjchem-570	136	23	n	n	PRON
eurjchem-570	136	24	ratio	ratio	NOUN
eurjchem-570	136	25	of	of	ADP
eurjchem-570	136	26	3	3	NUM
eurjchem-570	136	27	and	and	CCONJ
eurjchem-570	136	28	limit	limit	NOUN
eurjchem-570	136	29	of	of	ADP
eurjchem-570	136	30	quantification	quantification	NOUN
eurjchem-570	136	31	(	(	PUNCT
eurjchem-570	136	32	loq	loq	PROPN
eurjchem-570	136	33	)	)	PUNCT
eurjchem-570	136	34	at	at	ADP
eurjchem-570	136	35	which	which	PRON
eurjchem-570	136	36	s	s	PROPN
eurjchem-570	136	37	/	/	SYM
eurjchem-570	136	38	n	n	PRON
eurjchem-570	136	39	is	be	AUX
eurjchem-570	136	40	10	10	NUM
eurjchem-570	136	41	were	be	AUX
eurjchem-570	136	42	determined	determine	VERB
eurjchem-570	136	43	experimentally	experimentally	ADV
eurjchem-570	136	44	for	for	ADP
eurjchem-570	136	45	the	the	DET
eurjchem-570	136	46	proposed	propose	VERB
eurjchem-570	136	47	methods	method	NOUN
eurjchem-570	136	48	and	and	CCONJ
eurjchem-570	136	49	results	result	NOUN
eurjchem-570	136	50	are	be	AUX
eurjchem-570	136	51	given	give	VERB
eurjchem-570	136	52	in	in	ADP
eurjchem-570	136	53	table	table	NOUN
eurjchem-570	136	54	3	3	NUM
eurjchem-570	136	55	.	.	PUNCT
eurjchem-570	137	1	3.3.7	3.3.7	NUM
eurjchem-570	137	2	.	.	PUNCT
eurjchem-570	138	1	statistical	statistical	ADJ
eurjchem-570	138	2	analysis	analysis	NOUN
eurjchem-570	138	3	statistical	statistical	ADJ
eurjchem-570	138	4	analysis	analysis	NOUN
eurjchem-570	138	5	of	of	ADP
eurjchem-570	138	6	the	the	DET
eurjchem-570	138	7	results	result	NOUN
eurjchem-570	138	8	obtained	obtain	VERB
eurjchem-570	138	9	by	by	ADP
eurjchem-570	138	10	the	the	DET
eurjchem-570	138	11	proposed	propose	VERB
eurjchem-570	138	12	methods	method	NOUN
eurjchem-570	138	13	and	and	CCONJ
eurjchem-570	138	14	the	the	DET
eurjchem-570	138	15	reference	reference	NOUN
eurjchem-570	138	16	methods	method	NOUN
eurjchem-570	138	17	for	for	ADP
eurjchem-570	138	18	each	each	DET
eurjchem-570	138	19	drug	drug	NOUN
eurjchem-570	138	20	were	be	AUX
eurjchem-570	138	21	carried	carry	VERB
eurjchem-570	138	22	out	out	ADP
eurjchem-570	138	23	by	by	ADP
eurjchem-570	138	24	“	"	PUNCT
eurjchem-570	138	25	spss	spss	ADJ
eurjchem-570	138	26	statistical	statistical	ADJ
eurjchem-570	138	27	package	package	NOUN
eurjchem-570	138	28	version	version	NOUN
eurjchem-570	138	29	11	11	NUM
eurjchem-570	138	30	”	"	PUNCT
eurjchem-570	138	31	.	.	PUNCT
eurjchem-570	139	1	the	the	DET
eurjchem-570	139	2	significant	significant	ADJ
eurjchem-570	139	3	difference	difference	NOUN
eurjchem-570	139	4	between	between	ADP
eurjchem-570	139	5	the	the	DET
eurjchem-570	139	6	reference	reference	NOUN
eurjchem-570	139	7	methods	method	NOUN
eurjchem-570	139	8	and	and	CCONJ
eurjchem-570	139	9	the	the	DET
eurjchem-570	139	10	described	describe	VERB
eurjchem-570	139	11	methods	method	NOUN
eurjchem-570	139	12	was	be	AUX
eurjchem-570	139	13	tested	test	VERB
eurjchem-570	139	14	by	by	ADP
eurjchem-570	139	15	one	one	NUM
eurjchem-570	139	16	way	way	NOUN
eurjchem-570	139	17	anova	anova	X
eurjchem-570	139	18	(	(	PUNCT
eurjchem-570	139	19	f‐test	f‐test	X
eurjchem-570	139	20	)	)	PUNCT
eurjchem-570	139	21	at	at	ADP
eurjchem-570	139	22	p	p	NOUN
eurjchem-570	139	23	=	=	NOUN
eurjchem-570	139	24	0.05	0.05	NUM
eurjchem-570	139	25	as	as	SCONJ
eurjchem-570	139	26	shown	show	VERB
eurjchem-570	139	27	in	in	ADP
eurjchem-570	139	28	table	table	NOUN
eurjchem-570	139	29	4	4	NUM
eurjchem-570	139	30	and	and	CCONJ
eurjchem-570	139	31	5	5	NUM
eurjchem-570	139	32	.	.	PUNCT
eurjchem-570	140	1	the	the	DET
eurjchem-570	140	2	test	test	NOUN
eurjchem-570	140	3	ascertained	ascertain	VERB
eurjchem-570	140	4	that	that	SCONJ
eurjchem-570	140	5	there	there	PRON
eurjchem-570	140	6	was	be	VERB
eurjchem-570	140	7	no	no	DET
eurjchem-570	140	8	significant	significant	ADJ
eurjchem-570	140	9	difference	difference	NOUN
eurjchem-570	140	10	among	among	ADP
eurjchem-570	140	11	the	the	DET
eurjchem-570	140	12	methods	method	NOUN
eurjchem-570	140	13	.	.	PUNCT
eurjchem-570	141	1	4	4	X
eurjchem-570	141	2	.	.	X
eurjchem-570	141	3	conclusion	conclusion	NOUN
eurjchem-570	141	4	a	a	DET
eurjchem-570	141	5	single	single	ADJ
eurjchem-570	141	6	lc	lc	NOUN
eurjchem-570	141	7	method	method	NOUN
eurjchem-570	141	8	can	can	AUX
eurjchem-570	141	9	be	be	AUX
eurjchem-570	141	10	applied	apply	VERB
eurjchem-570	141	11	to	to	ADP
eurjchem-570	141	12	the	the	DET
eurjchem-570	141	13	simultaneous	simultaneous	ADJ
eurjchem-570	141	14	determination	determination	NOUN
eurjchem-570	141	15	of	of	ADP
eurjchem-570	141	16	vdg	vdg	NOUN
eurjchem-570	141	17	and	and	CCONJ
eurjchem-570	141	18	sxg	sxg	ADJ
eurjchem-570	141	19	with	with	ADP
eurjchem-570	141	20	metformin	metformin	NOUN
eurjchem-570	141	21	.	.	PUNCT
eurjchem-570	142	1	the	the	DET
eurjchem-570	142	2	proposed	propose	VERB
eurjchem-570	142	3	lc	lc	NOUN
eurjchem-570	142	4	method	method	NOUN
eurjchem-570	142	5	has	have	VERB
eurjchem-570	142	6	the	the	DET
eurjchem-570	142	7	advantages	advantage	NOUN
eurjchem-570	142	8	of	of	ADP
eurjchem-570	142	9	simplicity	simplicity	NOUN
eurjchem-570	142	10	,	,	PUNCT
eurjchem-570	142	11	precision	precision	NOUN
eurjchem-570	142	12	,	,	PUNCT
eurjchem-570	142	13	accuracy	accuracy	NOUN
eurjchem-570	142	14	and	and	CCONJ
eurjchem-570	142	15	convenience	convenience	NOUN
eurjchem-570	142	16	for	for	ADP
eurjchem-570	142	17	the	the	DET
eurjchem-570	142	18	separation	separation	NOUN
eurjchem-570	142	19	and	and	CCONJ
eurjchem-570	142	20	quantization	quantization	NOUN
eurjchem-570	142	21	of	of	ADP
eurjchem-570	142	22	vdg	vdg	NOUN
eurjchem-570	142	23	or	or	CCONJ
eurjchem-570	142	24	sxg	sxg	NOUN
eurjchem-570	142	25	in	in	ADP
eurjchem-570	142	26	combination	combination	NOUN
eurjchem-570	142	27	with	with	ADP
eurjchem-570	142	28	met	meet	VERB
eurjchem-570	142	29	.	.	PUNCT
eurjchem-570	143	1	the	the	DET
eurjchem-570	143	2	method	method	NOUN
eurjchem-570	143	3	can	can	AUX
eurjchem-570	143	4	be	be	AUX
eurjchem-570	143	5	applied	apply	VERB
eurjchem-570	143	6	for	for	ADP
eurjchem-570	143	7	the	the	DET
eurjchem-570	143	8	determination	determination	NOUN
eurjchem-570	143	9	of	of	ADP
eurjchem-570	143	10	the	the	DET
eurjchem-570	143	11	cited	cite	VERB
eurjchem-570	143	12	drugs	drug	NOUN
eurjchem-570	143	13	in	in	ADP
eurjchem-570	143	14	tablets	tablet	NOUN
eurjchem-570	143	15	without	without	ADP
eurjchem-570	143	16	interference	interference	NOUN
eurjchem-570	143	17	from	from	ADP
eurjchem-570	143	18	the	the	DET
eurjchem-570	143	19	tablets	tablet	NOUN
eurjchem-570	143	20	’	'	PUNCT
eurjchem-570	143	21	inactive	inactive	ADJ
eurjchem-570	143	22	ingredients	ingredient	NOUN
eurjchem-570	143	23	.	.	PUNCT
eurjchem-570	144	1	the	the	DET
eurjchem-570	144	2	method	method	NOUN
eurjchem-570	144	3	was	be	AUX
eurjchem-570	144	4	validated	validate	VERB
eurjchem-570	144	5	showing	show	VERB
eurjchem-570	144	6	satisfactory	satisfactory	ADJ
eurjchem-570	144	7	data	datum	NOUN
eurjchem-570	144	8	for	for	ADP
eurjchem-570	144	9	all	all	DET
eurjchem-570	144	10	the	the	DET
eurjchem-570	144	11	method	method	NOUN
eurjchem-570	144	12	validation	validation	NOUN
eurjchem-570	144	13	parameters	parameter	NOUN
eurjchem-570	144	14	tested	test	VERB
eurjchem-570	144	15	.	.	PUNCT
eurjchem-570	145	1	thus	thus	ADV
eurjchem-570	145	2	,	,	PUNCT
eurjchem-570	145	3	the	the	DET
eurjchem-570	145	4	developed	develop	VERB
eurjchem-570	145	5	method	method	NOUN
eurjchem-570	145	6	can	can	AUX
eurjchem-570	145	7	be	be	AUX
eurjchem-570	145	8	conveniently	conveniently	ADV
eurjchem-570	145	9	used	use	VERB
eurjchem-570	145	10	by	by	ADP
eurjchem-570	145	11	quality	quality	NOUN
eurjchem-570	145	12	control	control	NOUN
eurjchem-570	145	13	laboratories	laboratory	NOUN
eurjchem-570	145	14	.	.	PUNCT
eurjchem-570	146	1	references	reference	NOUN
eurjchem-570	146	2	[	[	X
eurjchem-570	146	3	1	1	NUM
eurjchem-570	146	4	]	]	PUNCT
eurjchem-570	146	5	.	.	PUNCT
eurjchem-570	147	1	singh	singh	PROPN
eurjchem-570	147	2	,	,	PUNCT
eurjchem-570	147	3	s.	s.	PROPN
eurjchem-570	147	4	k.	k.	PROPN
eurjchem-570	147	5	;	;	PUNCT
eurjchem-570	147	6	manne	manne	PROPN
eurjchem-570	147	7	,	,	PUNCT
eurjchem-570	147	8	n.	n.	PROPN
eurjchem-570	147	9	;	;	PUNCT
eurjchem-570	147	10	pal	pal	NOUN
eurjchem-570	147	11	,	,	PUNCT
eurjchem-570	147	12	m.	m.	NOUN
eurjchem-570	147	13	beilstein	beilstein	PROPN
eurjchem-570	147	14	j.	j.	PROPN
eurjchem-570	147	15	org	org	PROPN
eurjchem-570	147	16	.	.	PUNCT
eurjchem-570	147	17	chem	chem	PROPN
eurjchem-570	147	18	.	.	PUNCT
eurjchem-570	148	1	2008	2008	NUM
eurjchem-570	148	2	,	,	PUNCT
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eurjchem-570	148	4	,	,	PUNCT
eurjchem-570	148	5	20‐20	20‐20	NUM
eurjchem-570	148	6	.	.	PUNCT
eurjchem-570	149	1	[	[	X
eurjchem-570	149	2	2	2	NUM
eurjchem-570	149	3	]	]	PUNCT
eurjchem-570	149	4	.	.	PUNCT
eurjchem-570	150	1	nirogi	nirogi	PROPN
eurjchem-570	150	2	,	,	PUNCT
eurjchem-570	150	3	r.	r.	PROPN
eurjchem-570	150	4	;	;	PUNCT
eurjchem-570	150	5	kandikere	kandikere	PROPN
eurjchem-570	150	6	,	,	PUNCT
eurjchem-570	150	7	v.	v.	PROPN
eurjchem-570	150	8	;	;	PUNCT
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eurjchem-570	150	10	,	,	PUNCT
eurjchem-570	150	11	k.	k.	PROPN
eurjchem-570	150	12	;	;	PUNCT
eurjchem-570	150	13	komarneni	komarneni	PROPN
eurjchem-570	150	14	,	,	PUNCT
eurjchem-570	150	15	p.	p.	NOUN
eurjchem-570	150	16	;	;	PUNCT
eurjchem-570	150	17	aleti	aleti	PROPN
eurjchem-570	150	18	,	,	PUNCT
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eurjchem-570	150	20	;	;	PUNCT
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eurjchem-570	150	22	,	,	PUNCT
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eurjchem-570	151	2	.	.	PUNCT
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eurjchem-570	152	2	,	,	PUNCT
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eurjchem-570	152	4	,	,	PUNCT
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eurjchem-570	152	6	.	.	PUNCT
eurjchem-570	153	1	[	[	X
eurjchem-570	153	2	3	3	NUM
eurjchem-570	153	3	]	]	PUNCT
eurjchem-570	153	4	.	.	PUNCT
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eurjchem-570	154	2	,	,	PUNCT
eurjchem-570	154	3	r.	r.	PROPN
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eurjchem-570	154	5	;	;	PUNCT
eurjchem-570	154	6	elkady	elkady	PROPN
eurjchem-570	154	7	,	,	PUNCT
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eurjchem-570	154	12	,	,	PUNCT
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eurjchem-570	154	16	.	.	PUNCT
eurjchem-570	155	1	j.	j.	PROPN
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eurjchem-570	155	3	.	.	PUNCT
eurjchem-570	156	1	sci	sci	PROPN
eurjchem-570	156	2	.	.	PROPN
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eurjchem-570	156	4	,	,	PUNCT
eurjchem-570	156	5	7(1	7(1	NUM
eurjchem-570	156	6	)	)	PUNCT
eurjchem-570	156	7	,	,	PUNCT
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eurjchem-570	156	9	.	.	PUNCT
eurjchem-570	157	1	[	[	X
eurjchem-570	157	2	4	4	NUM
eurjchem-570	157	3	]	]	PUNCT
eurjchem-570	157	4	.	.	PUNCT
eurjchem-570	158	1	el‐bagary	el‐bagary	PROPN
eurjchem-570	158	2	,	,	PUNCT
eurjchem-570	158	3	r.	r.	PROPN
eurjchem-570	158	4	i.	i.	PROPN
eurjchem-570	158	5	;	;	PUNCT
eurjchem-570	158	6	elkady	elkady	PROPN
eurjchem-570	158	7	,	,	PUNCT
eurjchem-570	158	8	e.	e.	PROPN
eurjchem-570	158	9	f.	f.	PROPN
eurjchem-570	158	10	;	;	PUNCT
eurjchem-570	158	11	ayoub	ayoub	PROPN
eurjchem-570	158	12	,	,	PUNCT
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eurjchem-570	160	4	,	,	PUNCT
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eurjchem-570	160	6	)	)	PUNCT
eurjchem-570	160	7	,	,	PUNCT
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eurjchem-570	160	9	.	.	PUNCT
eurjchem-570	161	1	[	[	X
eurjchem-570	161	2	5	5	NUM
eurjchem-570	161	3	]	]	PUNCT
eurjchem-570	161	4	.	.	PUNCT
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eurjchem-570	161	6	,	,	PUNCT
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eurjchem-570	161	8	;	;	PUNCT
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eurjchem-570	161	10	,	,	PUNCT
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eurjchem-570	161	12	;	;	PUNCT
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eurjchem-570	161	14	,	,	PUNCT
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eurjchem-570	161	16	;	;	PUNCT
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eurjchem-570	161	22	,	,	PUNCT
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eurjchem-570	161	24	;	;	PUNCT
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eurjchem-570	162	2	,	,	PUNCT
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eurjchem-570	162	4	,	,	PUNCT
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eurjchem-570	162	6	.	.	PUNCT
eurjchem-570	163	1	[	[	X
eurjchem-570	163	2	6	6	NUM
eurjchem-570	163	3	]	]	PUNCT
eurjchem-570	163	4	.	.	PUNCT
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eurjchem-570	164	2	,	,	PUNCT
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eurjchem-570	164	4	;	;	PUNCT
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eurjchem-570	165	2	,	,	PUNCT
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eurjchem-570	165	6	.	.	PUNCT
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eurjchem-570	166	2	7	7	NUM
eurjchem-570	166	3	]	]	PUNCT
eurjchem-570	166	4	.	.	PUNCT
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eurjchem-570	166	6	,	,	PUNCT
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eurjchem-570	166	8	;	;	PUNCT
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eurjchem-570	166	10	,	,	PUNCT
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eurjchem-570	166	12	;	;	PUNCT
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eurjchem-570	166	14	,	,	PUNCT
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eurjchem-570	166	16	;	;	PUNCT
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eurjchem-570	166	18	,	,	PUNCT
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eurjchem-570	166	22	,	,	PUNCT
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eurjchem-570	166	24	;	;	PUNCT
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eurjchem-570	166	30	.	.	PUNCT
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eurjchem-570	167	2	.	.	PUNCT
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eurjchem-570	168	2	,	,	PUNCT
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eurjchem-570	168	6	.	.	PUNCT
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eurjchem-570	169	3	]	]	PUNCT
eurjchem-570	169	4	.	.	PUNCT
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eurjchem-570	170	2	,	,	PUNCT
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eurjchem-570	170	4	;	;	PUNCT
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eurjchem-570	170	6	,	,	PUNCT
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eurjchem-570	171	3	.	.	PUNCT
eurjchem-570	172	1	pharm	pharm	PROPN
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eurjchem-570	173	2	.	.	PROPN
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eurjchem-570	173	4	,	,	PUNCT
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eurjchem-570	173	8	.	.	PUNCT
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eurjchem-570	174	3	]	]	PUNCT
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eurjchem-570	174	8	;	;	PUNCT
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eurjchem-570	174	16	;	;	PUNCT
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eurjchem-570	178	3	)	)	PUNCT
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eurjchem-570	178	5	,	,	PUNCT
eurjchem-570	178	6	25(3	25(3	NUM
eurjchem-570	178	7	)	)	PUNCT
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eurjchem-570	179	9	;	;	PUNCT
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eurjchem-570	179	11	,	,	PUNCT
eurjchem-570	179	12	i.	i.	PROPN
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eurjchem-570	181	2	,	,	PUNCT
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eurjchem-570	181	4	,	,	PUNCT
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eurjchem-570	182	1	[	[	X
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eurjchem-570	182	4	.	.	PUNCT
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eurjchem-570	183	2	,	,	PUNCT
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eurjchem-570	183	4	;	;	PUNCT
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eurjchem-570	183	6	,	,	PUNCT
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eurjchem-570	193	4	.	.	PUNCT
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eurjchem-570	198	2	,	,	PUNCT
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eurjchem-570	200	4	.	.	PUNCT
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