id	sid	tid	token	lemma	pos
eurjchem-591	1	1	untitled	untitle	VERB
eurjchem-591	1	2	european	european	PROPN
eurjchem-591	1	3	journal	journal	PROPN
eurjchem-591	1	4	of	of	ADP
eurjchem-591	1	5	chemistry	chemistry	NOUN
eurjchem-591	1	6	3	3	NUM
eurjchem-591	1	7	(	(	PUNCT
eurjchem-591	1	8	1	1	NUM
eurjchem-591	1	9	)	)	PUNCT
eurjchem-591	1	10	(	(	PUNCT
eurjchem-591	1	11	2012	2012	NUM
eurjchem-591	1	12	)	)	PUNCT
eurjchem-591	1	13	37‐39	37‐39	PROPN
eurjchem-591	1	14	european	european	PROPN
eurjchem-591	1	15	journal	journal	PROPN
eurjchem-591	1	16	of	of	ADP
eurjchem-591	1	17	chemistry	chemistry	NOUN
eurjchem-591	1	18	issn	issn	PROPN
eurjchem-591	1	19	2153‐2249	2153‐2249	PROPN
eurjchem-591	1	20	(	(	PUNCT
eurjchem-591	1	21	print	print	NOUN
eurjchem-591	1	22	)	)	PUNCT
eurjchem-591	1	23	/	/	SYM
eurjchem-591	1	24	issn	issn	PROPN
eurjchem-591	1	25	2153‐2257	2153‐2257	NUM
eurjchem-591	1	26	(	(	PUNCT
eurjchem-591	1	27	online	online	ADJ
eurjchem-591	1	28	)	)	PUNCT
eurjchem-591	1	29			NOUN
eurjchem-591	1	30	2012	2012	NUM
eurjchem-591	1	31	eurjchem	eurjchem	PROPN
eurjchem-591	1	32	doi:10.5155	doi:10.5155	PROPN
eurjchem-591	1	33	/	/	SYM
eurjchem-591	1	34	eurjchem.3.1.37‐39.591	eurjchem.3.1.37‐39.591	PROPN
eurjchem-591	1	35	european	european	PROPN
eurjchem-591	1	36	journal	journal	PROPN
eurjchem-591	1	37	of	of	ADP
eurjchem-591	1	38	chemistry	chemistry	PROPN
eurjchem-591	1	39	journal	journal	PROPN
eurjchem-591	1	40	homepage	homepage	NOUN
eurjchem-591	1	41	:	:	PUNCT
eurjchem-591	2	1	www.eurjchem.com	www.eurjchem.com	X
eurjchem-591	2	2	crystal	crystal	NOUN
eurjchem-591	2	3	and	and	CCONJ
eurjchem-591	2	4	molecular	molecular	ADJ
eurjchem-591	2	5	structure	structure	NOUN
eurjchem-591	2	6	of	of	ADP
eurjchem-591	2	7	bis(4‐bromo‐n‐(diethylcarbamothioyl)benzamido)nickel(ii	bis(4‐bromo‐n‐(diethylcarbamothioyl)benzamido)nickel(ii	ADJ
eurjchem-591	2	8	)	)	PUNCT
eurjchem-591	2	9	complex	complex	ADJ
eurjchem-591	2	10	gun	gun	NOUN
eurjchem-591	2	11	binzeta	binzeta	NOUN
eurjchem-591	2	12	,	,	PUNCT
eurjchem-591	2	13	*	*	PROPN
eurjchem-591	2	14	,	,	PUNCT
eurjchem-591	2	15	ulrich	ulrich	PROPN
eurjchem-591	2	16	flörkeb	flörkeb	PROPN
eurjchem-591	2	17	,	,	PUNCT
eurjchem-591	2	18	nevzat	nevzat	VERB
eurjchem-591	2	19	külcüc	külcüc	PROPN
eurjchem-591	2	20	and	and	CCONJ
eurjchem-591	2	21	hakan	hakan	PROPN
eurjchem-591	2	22	arslanc	arslanc	PROPN
eurjchem-591	2	23	a	a	DET
eurjchem-591	2	24	science	science	NOUN
eurjchem-591	2	25	education	education	NOUN
eurjchem-591	2	26	,	,	PUNCT
eurjchem-591	2	27	faculty	faculty	NOUN
eurjchem-591	2	28	of	of	ADP
eurjchem-591	2	29	education	education	NOUN
eurjchem-591	2	30	,	,	PUNCT
eurjchem-591	2	31	mersin	mersin	PROPN
eurjchem-591	2	32	university	university	PROPN
eurjchem-591	2	33	,	,	PUNCT
eurjchem-591	2	34	mersin	mersin	PROPN
eurjchem-591	2	35	,	,	PUNCT
eurjchem-591	2	36	tr‐33169	tr‐33169	PROPN
eurjchem-591	2	37	,	,	PUNCT
eurjchem-591	2	38	turkey	turkey	PROPN
eurjchem-591	2	39	b	b	PROPN
eurjchem-591	2	40	department	department	PROPN
eurjchem-591	2	41	of	of	ADP
eurjchem-591	2	42	chemistry	chemistry	NOUN
eurjchem-591	2	43	,	,	PUNCT
eurjchem-591	2	44	university	university	NOUN
eurjchem-591	2	45	of	of	ADP
eurjchem-591	2	46	paderborn	paderborn	ADJ
eurjchem-591	2	47	,	,	PUNCT
eurjchem-591	2	48	paderborn	paderborn	ADJ
eurjchem-591	2	49	,	,	PUNCT
eurjchem-591	2	50	d‐33098	d‐33098	PROPN
eurjchem-591	2	51	,	,	PUNCT
eurjchem-591	2	52	germany	germany	PROPN
eurjchem-591	2	53	c	c	PROPN
eurjchem-591	2	54	department	department	PROPN
eurjchem-591	2	55	of	of	ADP
eurjchem-591	2	56	chemistry	chemistry	NOUN
eurjchem-591	2	57	,	,	PUNCT
eurjchem-591	2	58	faculty	faculty	NOUN
eurjchem-591	2	59	of	of	ADP
eurjchem-591	2	60	arts	art	NOUN
eurjchem-591	2	61	and	and	CCONJ
eurjchem-591	2	62	science	science	PROPN
eurjchem-591	2	63	,	,	PUNCT
eurjchem-591	2	64	mersin	mersin	PROPN
eurjchem-591	2	65	university	university	PROPN
eurjchem-591	2	66	,	,	PUNCT
eurjchem-591	2	67	mersin	mersin	PROPN
eurjchem-591	2	68	,	,	PUNCT
eurjchem-591	2	69	tr‐33343	tr‐33343	PROPN
eurjchem-591	2	70	,	,	PUNCT
eurjchem-591	2	71	turkey	turkey	NOUN
eurjchem-591	2	72	*	*	PUNCT
eurjchem-591	2	73	corresponding	correspond	VERB
eurjchem-591	2	74	author	author	NOUN
eurjchem-591	2	75	at	at	ADP
eurjchem-591	2	76	:	:	PUNCT
eurjchem-591	2	77	science	science	NOUN
eurjchem-591	2	78	education	education	NOUN
eurjchem-591	2	79	,	,	PUNCT
eurjchem-591	2	80	faculty	faculty	NOUN
eurjchem-591	2	81	of	of	ADP
eurjchem-591	2	82	education	education	NOUN
eurjchem-591	2	83	,	,	PUNCT
eurjchem-591	2	84	mersin	mersin	PROPN
eurjchem-591	2	85	university	university	PROPN
eurjchem-591	2	86	,	,	PUNCT
eurjchem-591	2	87	mersin	mersin	PROPN
eurjchem-591	2	88	,	,	PUNCT
eurjchem-591	2	89	tr‐33169	tr‐33169	PROPN
eurjchem-591	2	90	,	,	PUNCT
eurjchem-591	2	91	turkey	turkey	NOUN
eurjchem-591	2	92	.	.	PUNCT
eurjchem-591	3	1	tel	tel	PROPN
eurjchem-591	3	2	.	.	PUNCT
eurjchem-591	3	3	:	:	PUNCT
eurjchem-591	4	1	+90.532.2701917	+90.532.2701917	NUM
eurjchem-591	4	2	;	;	PUNCT
eurjchem-591	4	3	fax	fax	NOUN
eurjchem-591	4	4	:	:	PUNCT
eurjchem-591	4	5	+90.324.3610047	+90.324.3610047	NUM
eurjchem-591	4	6	.	.	PUNCT
eurjchem-591	4	7	e‐mail	e‐mail	PUNCT
eurjchem-591	4	8	address	address	NOUN
eurjchem-591	4	9	:	:	PUNCT
eurjchem-591	4	10	polatgun@gmail.com	polatgun@gmail.com	X
eurjchem-591	4	11	(	(	PUNCT
eurjchem-591	4	12	g.	g.	PROPN
eurjchem-591	4	13	binzet	binzet	PROPN
eurjchem-591	4	14	)	)	PUNCT
eurjchem-591	4	15	.	.	PUNCT
eurjchem-591	5	1	article	article	NOUN
eurjchem-591	5	2	information	information	PROPN
eurjchem-591	5	3	abstract	abstract	ADV
eurjchem-591	5	4	received	receive	VERB
eurjchem-591	5	5	:	:	PUNCT
eurjchem-591	5	6	31	31	NUM
eurjchem-591	5	7	january	january	PROPN
eurjchem-591	5	8	2012	2012	NUM
eurjchem-591	5	9	received	receive	VERB
eurjchem-591	5	10	in	in	ADP
eurjchem-591	5	11	revised	revise	VERB
eurjchem-591	5	12	form	form	NOUN
eurjchem-591	5	13	:	:	PUNCT
eurjchem-591	5	14	06	06	NUM
eurjchem-591	5	15	february	february	PROPN
eurjchem-591	5	16	2012	2012	NUM
eurjchem-591	5	17	accepted	accept	VERB
eurjchem-591	5	18	:	:	PUNCT
eurjchem-591	5	19	06	06	NUM
eurjchem-591	5	20	february	february	PROPN
eurjchem-591	5	21	2012	2012	NUM
eurjchem-591	5	22	online	online	NOUN
eurjchem-591	5	23	:	:	PUNCT
eurjchem-591	5	24	31	31	NUM
eurjchem-591	5	25	march	march	NOUN
eurjchem-591	5	26	2012	2012	NUM
eurjchem-591	5	27	keywords	keyword	NOUN
eurjchem-591	5	28	we	we	PRON
eurjchem-591	5	29	report	report	VERB
eurjchem-591	5	30	the	the	DET
eurjchem-591	5	31	synthesis	synthesis	NOUN
eurjchem-591	5	32	of	of	ADP
eurjchem-591	5	33	bis(4‐bromo‐n‐(diethylcarbamothioyl)benzamido)nickel(ii	bis(4‐bromo‐n‐(diethylcarbamothioyl)benzamido)nickel(ii	ADJ
eurjchem-591	5	34	)	)	PUNCT
eurjchem-591	5	35	complex	complex	NOUN
eurjchem-591	5	36	of	of	ADP
eurjchem-591	5	37	an	an	DET
eurjchem-591	5	38	benzoylthiourea	benzoylthiourea	NOUN
eurjchem-591	5	39	derivative	derivative	NOUN
eurjchem-591	5	40	formulated	formulate	VERB
eurjchem-591	5	41	as	as	ADP
eurjchem-591	5	42	c24h28br2nin4o2s2	c24h28br2nin4o2s2	PROPN
eurjchem-591	5	43	.	.	PUNCT
eurjchem-591	6	1	the	the	DET
eurjchem-591	6	2	structure	structure	NOUN
eurjchem-591	6	3	of	of	ADP
eurjchem-591	6	4	compound	compound	NOUN
eurjchem-591	6	5	has	have	AUX
eurjchem-591	6	6	been	be	AUX
eurjchem-591	6	7	determined	determine	VERB
eurjchem-591	6	8	by	by	ADP
eurjchem-591	6	9	single‐crystal	single‐crystal	ADJ
eurjchem-591	6	10	x‐ray	x‐ray	PROPN
eurjchem-591	6	11	diffraction	diffraction	NOUN
eurjchem-591	6	12	analysis	analysis	NOUN
eurjchem-591	6	13	.	.	PUNCT
eurjchem-591	7	1	it	it	PRON
eurjchem-591	7	2	crystallizes	crystallize	VERB
eurjchem-591	7	3	in	in	ADP
eurjchem-591	7	4	the	the	DET
eurjchem-591	7	5	monoclinic	monoclinic	ADJ
eurjchem-591	7	6	space	space	NOUN
eurjchem-591	7	7	group	group	NOUN
eurjchem-591	7	8	,	,	PUNCT
eurjchem-591	7	9	p21	p21	PROPN
eurjchem-591	7	10	/	/	SYM
eurjchem-591	7	11	c	c	PROPN
eurjchem-591	7	12	with	with	ADP
eurjchem-591	7	13	unit	unit	NOUN
eurjchem-591	7	14	cell	cell	NOUN
eurjchem-591	7	15	dimensions	dimension	NOUN
eurjchem-591	7	16	of	of	ADP
eurjchem-591	7	17	a	a	DET
eurjchem-591	7	18	=	=	SYM
eurjchem-591	7	19	12.9099(17	12.9099(17	NUM
eurjchem-591	7	20	)	)	PUNCT
eurjchem-591	7	21	å	å	PROPN
eurjchem-591	7	22	,	,	PUNCT
eurjchem-591	7	23	b	b	X
eurjchem-591	7	24	=	=	SYM
eurjchem-591	7	25	15.264(2	15.264(2	NUM
eurjchem-591	7	26	)	)	PUNCT
eurjchem-591	8	1	å	å	NOUN
eurjchem-591	8	2	,	,	PUNCT
eurjchem-591	8	3	c	c	NOUN
eurjchem-591	8	4	=	=	SYM
eurjchem-591	8	5	14.0287(19	14.0287(19	NUM
eurjchem-591	8	6	)	)	PUNCT
eurjchem-591	8	7	å	å	NOUN
eurjchem-591	8	8	,	,	PUNCT
eurjchem-591	8	9	β	β	X
eurjchem-591	8	10	=	=	SYM
eurjchem-591	8	11	92.140(4)o	92.140(4)o	NUM
eurjchem-591	8	12	and	and	CCONJ
eurjchem-591	8	13	v	v	NOUN
eurjchem-591	8	14	=	=	SYM
eurjchem-591	8	15	2762.5(6	2762.5(6	NUM
eurjchem-591	8	16	)	)	PUNCT
eurjchem-591	8	17	å3	å3	PROPN
eurjchem-591	8	18	.	.	PUNCT
eurjchem-591	9	1	in	in	ADP
eurjchem-591	9	2	this	this	DET
eurjchem-591	9	3	compound	compound	NOUN
eurjchem-591	9	4	,	,	PUNCT
eurjchem-591	9	5	the	the	DET
eurjchem-591	9	6	nickel	nickel	NOUN
eurjchem-591	9	7	atom	atom	NOUN
eurjchem-591	9	8	is	be	AUX
eurjchem-591	9	9	coordinated	coordinate	VERB
eurjchem-591	9	10	by	by	ADP
eurjchem-591	9	11	two	two	NUM
eurjchem-591	9	12	sulphur	sulphur	NOUN
eurjchem-591	9	13	and	and	CCONJ
eurjchem-591	9	14	two	two	NUM
eurjchem-591	9	15	oxygen	oxygen	NOUN
eurjchem-591	9	16	atoms	atom	NOUN
eurjchem-591	9	17	from	from	ADP
eurjchem-591	9	18	two	two	NUM
eurjchem-591	9	19	4‐bromo‐n‐	4‐bromo‐n‐	NUM
eurjchem-591	9	20	(	(	PUNCT
eurjchem-591	10	1	diethylcarbamothioyl)benzamide	diethylcarbamothioyl)benzamide	ADJ
eurjchem-591	10	2	molecules	molecule	NOUN
eurjchem-591	10	3	forming	form	VERB
eurjchem-591	10	4	an	an	DET
eurjchem-591	10	5	distorted	distort	VERB
eurjchem-591	10	6	square‐planar	square‐planar	NOUN
eurjchem-591	10	7	geometry	geometry	NOUN
eurjchem-591	10	8	.	.	PUNCT
eurjchem-591	11	1	thiourea	thiourea	NOUN
eurjchem-591	11	2	benzamide	benzamide	PROPN
eurjchem-591	11	3	nickel	nickel	NOUN
eurjchem-591	11	4	complex	complex	ADJ
eurjchem-591	11	5	benzoylthiourea	benzoylthiourea	NOUN
eurjchem-591	11	6	crystal	crystal	NOUN
eurjchem-591	11	7	structure	structure	NOUN
eurjchem-591	11	8	single	single	PROPN
eurjchem-591	11	9	crystal	crystal	NOUN
eurjchem-591	11	10	x‐ray	x‐ray	PROPN
eurjchem-591	11	11	diffraction	diffraction	PROPN
eurjchem-591	11	12	1	1	NUM
eurjchem-591	11	13	.	.	PUNCT
eurjchem-591	11	14	introduction	introduction	NOUN
eurjchem-591	11	15	in	in	ADP
eurjchem-591	11	16	recent	recent	ADJ
eurjchem-591	11	17	years	year	NOUN
eurjchem-591	11	18	,	,	PUNCT
eurjchem-591	11	19	there	there	PRON
eurjchem-591	11	20	has	have	AUX
eurjchem-591	11	21	been	be	AUX
eurjchem-591	11	22	considerable	considerable	ADJ
eurjchem-591	11	23	interest	interest	NOUN
eurjchem-591	11	24	in	in	ADP
eurjchem-591	11	25	benzoylthiourea	benzoylthiourea	PROPN
eurjchem-591	11	26	compounds	compound	NOUN
eurjchem-591	11	27	.	.	PUNCT
eurjchem-591	12	1	this	this	PRON
eurjchem-591	12	2	is	be	AUX
eurjchem-591	12	3	due	due	ADJ
eurjchem-591	12	4	to	to	ADP
eurjchem-591	12	5	the	the	DET
eurjchem-591	12	6	fact	fact	NOUN
eurjchem-591	12	7	that	that	SCONJ
eurjchem-591	12	8	these	these	DET
eurjchem-591	12	9	compounds	compound	NOUN
eurjchem-591	12	10	have	have	AUX
eurjchem-591	12	11	demonstrated	demonstrate	VERB
eurjchem-591	12	12	remarkable	remarkable	ADJ
eurjchem-591	12	13	pharmacological	pharmacological	ADJ
eurjchem-591	12	14	characteristics	characteristic	NOUN
eurjchem-591	12	15	.	.	PUNCT
eurjchem-591	13	1	many	many	ADJ
eurjchem-591	13	2	benzoylthiourea	benzoylthiourea	PROPN
eurjchem-591	13	3	compounds	compound	NOUN
eurjchem-591	13	4	have	have	AUX
eurjchem-591	13	5	been	be	AUX
eurjchem-591	13	6	tested	test	VERB
eurjchem-591	13	7	for	for	ADP
eurjchem-591	13	8	their	their	PRON
eurjchem-591	13	9	in	in	X
eurjchem-591	13	10	vitro	vitro	X
eurjchem-591	13	11	activity	activity	NOUN
eurjchem-591	13	12	against	against	ADP
eurjchem-591	13	13	a	a	DET
eurjchem-591	13	14	large	large	ADJ
eurjchem-591	13	15	variety	variety	NOUN
eurjchem-591	13	16	of	of	ADP
eurjchem-591	13	17	tumor	tumor	NOUN
eurjchem-591	13	18	lines	line	NOUN
eurjchem-591	13	19	and	and	CCONJ
eurjchem-591	13	20	have	have	AUX
eurjchem-591	13	21	been	be	AUX
eurjchem-591	13	22	found	find	VERB
eurjchem-591	13	23	to	to	PART
eurjchem-591	13	24	be	be	AUX
eurjchem-591	13	25	as	as	ADV
eurjchem-591	13	26	effective	effective	ADJ
eurjchem-591	13	27	or	or	CCONJ
eurjchem-591	13	28	better	well	ADJ
eurjchem-591	13	29	than	than	ADP
eurjchem-591	13	30	traditional	traditional	ADJ
eurjchem-591	13	31	heavy	heavy	ADJ
eurjchem-591	13	32	metal	metal	NOUN
eurjchem-591	13	33	anticancer	anticancer	NOUN
eurjchem-591	13	34	drugs	drug	NOUN
eurjchem-591	13	35	such	such	ADJ
eurjchem-591	13	36	as	as	ADP
eurjchem-591	13	37	cis‐platin	cis‐platin	PROPN
eurjchem-591	13	38	[	[	X
eurjchem-591	13	39	1	1	NUM
eurjchem-591	13	40	]	]	PUNCT
eurjchem-591	13	41	.	.	PUNCT
eurjchem-591	14	1	some	some	DET
eurjchem-591	14	2	acylthiourea	acylthiourea	PROPN
eurjchem-591	14	3	derivatives	derivative	NOUN
eurjchem-591	14	4	exhibit	exhibit	VERB
eurjchem-591	14	5	antiviral	antiviral	NOUN
eurjchem-591	14	6	[	[	X
eurjchem-591	14	7	2	2	NUM
eurjchem-591	14	8	]	]	PUNCT
eurjchem-591	14	9	,	,	PUNCT
eurjchem-591	14	10	antibacterial	antibacterial	ADJ
eurjchem-591	14	11	[	[	X
eurjchem-591	14	12	3	3	NUM
eurjchem-591	14	13	]	]	PUNCT
eurjchem-591	14	14	,	,	PUNCT
eurjchem-591	14	15	antifungal	antifungal	PROPN
eurjchem-591	15	1	[	[	X
eurjchem-591	15	2	4	4	NUM
eurjchem-591	15	3	]	]	PUNCT
eurjchem-591	15	4	,	,	PUNCT
eurjchem-591	15	5	antihelmintic	antihelmintic	ADJ
eurjchem-591	15	6	[	[	X
eurjchem-591	15	7	5,6	5,6	NUM
eurjchem-591	15	8	]	]	PUNCT
eurjchem-591	15	9	,	,	PUNCT
eurjchem-591	15	10	herbicidal	herbicidal	NOUN
eurjchem-591	15	11	[	[	X
eurjchem-591	15	12	7	7	NUM
eurjchem-591	15	13	]	]	PUNCT
eurjchem-591	15	14	,	,	PUNCT
eurjchem-591	15	15	activities	activity	NOUN
eurjchem-591	15	16	.	.	PUNCT
eurjchem-591	16	1	1,3‐dialkyl	1,3‐dialkyl	NUM
eurjchem-591	16	2	or	or	CCONJ
eurjchem-591	16	3	diaryl	diaryl	NOUN
eurjchem-591	16	4	thioureas	thiourea	NOUN
eurjchem-591	16	5	exhibit	exhibit	VERB
eurjchem-591	16	6	significant	significant	ADJ
eurjchem-591	16	7	antifungal	antifungal	ADJ
eurjchem-591	16	8	activity	activity	NOUN
eurjchem-591	16	9	against	against	ADP
eurjchem-591	16	10	plant	plant	NOUN
eurjchem-591	16	11	pathogens	pathogen	NOUN
eurjchem-591	16	12	pyricularia	pyricularia	NOUN
eurjchem-591	16	13	oryzae	oryzae	NOUN
eurjchem-591	16	14	and	and	CCONJ
eurjchem-591	16	15	drechslera	drechslera	NOUN
eurjchem-591	16	16	oryzae	oryzae	NOUN
eurjchem-591	16	17	[	[	X
eurjchem-591	16	18	8	8	NUM
eurjchem-591	16	19	]	]	PUNCT
eurjchem-591	16	20	.	.	PUNCT
eurjchem-591	17	1	furthermore	furthermore	ADV
eurjchem-591	17	2	,	,	PUNCT
eurjchem-591	17	3	thiourea	thiourea	NOUN
eurjchem-591	17	4	and	and	CCONJ
eurjchem-591	17	5	its	its	PRON
eurjchem-591	17	6	derivatives	derivative	NOUN
eurjchem-591	17	7	are	be	AUX
eurjchem-591	17	8	a	a	DET
eurjchem-591	17	9	well‐known	well‐known	ADJ
eurjchem-591	17	10	class	class	NOUN
eurjchem-591	17	11	of	of	ADP
eurjchem-591	17	12	excellent	excellent	ADJ
eurjchem-591	17	13	ligands	ligand	NOUN
eurjchem-591	17	14	for	for	ADP
eurjchem-591	17	15	transition	transition	NOUN
eurjchem-591	17	16	metals	metal	NOUN
eurjchem-591	17	17	,	,	PUNCT
eurjchem-591	17	18	which	which	PRON
eurjchem-591	17	19	also	also	ADV
eurjchem-591	17	20	exhibit	exhibit	VERB
eurjchem-591	17	21	redox	redox	ADJ
eurjchem-591	17	22	activity	activity	NOUN
eurjchem-591	17	23	with	with	ADP
eurjchem-591	17	24	reducible	reducible	ADJ
eurjchem-591	17	25	metal	metal	NOUN
eurjchem-591	17	26	ions	ion	NOUN
eurjchem-591	17	27	to	to	PART
eurjchem-591	17	28	make	make	VERB
eurjchem-591	17	29	the	the	DET
eurjchem-591	17	30	reaction	reaction	NOUN
eurjchem-591	17	31	systems	system	NOUN
eurjchem-591	17	32	complicated	complicate	VERB
eurjchem-591	17	33	[	[	X
eurjchem-591	17	34	9‐11	9‐11	NUM
eurjchem-591	17	35	]	]	X
eurjchem-591	17	36	.	.	PUNCT
eurjchem-591	18	1	moreover	moreover	ADV
eurjchem-591	18	2	,	,	PUNCT
eurjchem-591	18	3	ion	ion	NOUN
eurjchem-591	18	4	selective	selective	ADJ
eurjchem-591	18	5	electrodes	electrode	NOUN
eurjchem-591	18	6	for	for	ADP
eurjchem-591	18	7	pb(ii	pb(ii	NOUN
eurjchem-591	18	8	)	)	PUNCT
eurjchem-591	18	9	based	base	VERB
eurjchem-591	18	10	on	on	ADP
eurjchem-591	18	11	benzoylthioureido	benzoylthioureido	NOUN
eurjchem-591	18	12	derivatives	derivative	NOUN
eurjchem-591	18	13	as	as	SCONJ
eurjchem-591	18	14	ionophores	ionophore	NOUN
eurjchem-591	18	15	have	have	AUX
eurjchem-591	18	16	been	be	AUX
eurjchem-591	18	17	formulated	formulate	VERB
eurjchem-591	18	18	[	[	X
eurjchem-591	18	19	12	12	NUM
eurjchem-591	18	20	]	]	PUNCT
eurjchem-591	18	21	.	.	PUNCT
eurjchem-591	19	1	our	our	PRON
eurjchem-591	19	2	group	group	NOUN
eurjchem-591	19	3	has	have	AUX
eurjchem-591	19	4	studied	study	VERB
eurjchem-591	19	5	the	the	DET
eurjchem-591	19	6	synthesis	synthesis	NOUN
eurjchem-591	19	7	[	[	X
eurjchem-591	19	8	13‐20	13‐20	NUM
eurjchem-591	19	9	]	]	PUNCT
eurjchem-591	19	10	,	,	PUNCT
eurjchem-591	19	11	charac‐	charac‐	PROPN
eurjchem-591	19	12	terization	terization	PROPN
eurjchem-591	19	13	,	,	PUNCT
eurjchem-591	19	14	crystal	crystal	NOUN
eurjchem-591	19	15	structure	structure	NOUN
eurjchem-591	19	16	[	[	X
eurjchem-591	19	17	21‐26	21‐26	X
eurjchem-591	19	18	]	]	X
eurjchem-591	19	19	,	,	PUNCT
eurjchem-591	19	20	thermal	thermal	ADJ
eurjchem-591	19	21	behavior	behavior	NOUN
eurjchem-591	19	22	[	[	X
eurjchem-591	19	23	26	26	NUM
eurjchem-591	19	24	,	,	PUNCT
eurjchem-591	19	25	27	27	NUM
eurjchem-591	19	26	]	]	PUNCT
eurjchem-591	19	27	and	and	CCONJ
eurjchem-591	19	28	antimicrobial	antimicrobial	ADJ
eurjchem-591	19	29	activity	activity	NOUN
eurjchem-591	19	30	[	[	X
eurjchem-591	19	31	28	28	NUM
eurjchem-591	19	32	,	,	PUNCT
eurjchem-591	19	33	29	29	NUM
eurjchem-591	19	34	]	]	PUNCT
eurjchem-591	19	35	of	of	ADP
eurjchem-591	19	36	some	some	DET
eurjchem-591	19	37	substitute	substitute	NOUN
eurjchem-591	19	38	benzoylthiourea	benzoylthiourea	NOUN
eurjchem-591	19	39	derivatives	derivative	NOUN
eurjchem-591	19	40	and	and	CCONJ
eurjchem-591	19	41	their	their	PRON
eurjchem-591	19	42	metal	metal	NOUN
eurjchem-591	19	43	complexes	complex	NOUN
eurjchem-591	19	44	.	.	PUNCT
eurjchem-591	20	1	in	in	ADP
eurjchem-591	20	2	the	the	DET
eurjchem-591	20	3	present	present	ADJ
eurjchem-591	20	4	work	work	NOUN
eurjchem-591	20	5	,	,	PUNCT
eurjchem-591	20	6	we	we	PRON
eurjchem-591	20	7	report	report	VERB
eurjchem-591	20	8	the	the	DET
eurjchem-591	20	9	crystal	crystal	NOUN
eurjchem-591	20	10	structure	structure	NOUN
eurjchem-591	20	11	of	of	ADP
eurjchem-591	20	12	bis(4‐bromo‐	bis(4‐bromo‐	PUNCT
eurjchem-591	20	13	n‐(diethylcarbamothioyl)benzamido)nickel(ii	n‐(diethylcarbamothioyl)benzamido)nickel(ii	NOUN
eurjchem-591	20	14	)	)	PUNCT
eurjchem-591	20	15	complex	complex	NOUN
eurjchem-591	20	16	.	.	PUNCT
eurjchem-591	21	1	2	2	X
eurjchem-591	21	2	.	.	X
eurjchem-591	21	3	experimental	experimental	ADJ
eurjchem-591	21	4	2.1	2.1	NUM
eurjchem-591	21	5	.	.	PUNCT
eurjchem-591	22	1	instrumentation	instrumentation	NOUN
eurjchem-591	22	2	melting	melting	NOUN
eurjchem-591	22	3	points	point	NOUN
eurjchem-591	22	4	were	be	AUX
eurjchem-591	22	5	measured	measure	VERB
eurjchem-591	22	6	on	on	ADP
eurjchem-591	22	7	an	an	DET
eurjchem-591	22	8	electrothermal	electrothermal	ADJ
eurjchem-591	22	9	model	model	NOUN
eurjchem-591	22	10	9200	9200	NUM
eurjchem-591	22	11	and	and	CCONJ
eurjchem-591	22	12	are	be	AUX
eurjchem-591	22	13	uncorrected	uncorrecte	VERB
eurjchem-591	22	14	.	.	PUNCT
eurjchem-591	23	1	elemental	elemental	ADJ
eurjchem-591	23	2	analyses	analysis	NOUN
eurjchem-591	23	3	were	be	AUX
eurjchem-591	23	4	carried	carry	VERB
eurjchem-591	23	5	out	out	ADP
eurjchem-591	23	6	with	with	ADP
eurjchem-591	23	7	a	a	DET
eurjchem-591	23	8	leco	leco	PROPN
eurjchem-591	23	9	chns‐932	chns‐932	VERB
eurjchem-591	23	10	elemental	elemental	ADJ
eurjchem-591	23	11	analyzer	analyzer	NOUN
eurjchem-591	23	12	.	.	PUNCT
eurjchem-591	24	1	fourier	fourier	PROPN
eurjchem-591	24	2	transform	transform	VERB
eurjchem-591	24	3	infrared	infrared	ADJ
eurjchem-591	24	4	spectra	spectra	PROPN
eurjchem-591	24	5	(	(	PUNCT
eurjchem-591	24	6	ftir	ftir	PROPN
eurjchem-591	24	7	)	)	PUNCT
eurjchem-591	24	8	were	be	AUX
eurjchem-591	24	9	recorded	record	VERB
eurjchem-591	24	10	in	in	ADP
eurjchem-591	24	11	kbr	kbr	PROPN
eurjchem-591	24	12	pellets	pellet	NOUN
eurjchem-591	24	13	using	use	VERB
eurjchem-591	24	14	a	a	DET
eurjchem-591	24	15	winfirst	winfirst	ADJ
eurjchem-591	24	16	satellite	satellite	NOUN
eurjchem-591	24	17	ftir	ftir	PROPN
eurjchem-591	24	18	spectrometer	spectrometer	NOUN
eurjchem-591	24	19	.	.	PUNCT
eurjchem-591	25	1	1h	1h	NUM
eurjchem-591	25	2	nmr	nmr	PROPN
eurjchem-591	25	3	spectra	spectra	NOUN
eurjchem-591	25	4	were	be	AUX
eurjchem-591	25	5	recorded	record	VERB
eurjchem-591	25	6	on	on	ADP
eurjchem-591	25	7	a	a	DET
eurjchem-591	25	8	bruker	bruker	NOUN
eurjchem-591	25	9	dpx‐400	dpx‐400	NOUN
eurjchem-591	25	10	spectrometer	spectrometer	NOUN
eurjchem-591	25	11	at	at	ADP
eurjchem-591	25	12	400	400	NUM
eurjchem-591	25	13	mhz	mhz	NOUN
eurjchem-591	25	14	using	use	VERB
eurjchem-591	25	15	cdcl3	cdcl3	NOUN
eurjchem-591	25	16	as	as	ADP
eurjchem-591	25	17	the	the	DET
eurjchem-591	25	18	solvent	solvent	NOUN
eurjchem-591	25	19	,	,	PUNCT
eurjchem-591	25	20	with	with	ADP
eurjchem-591	25	21	tetramethylsilane	tetramethylsilane	VERB
eurjchem-591	25	22	as	as	ADP
eurjchem-591	25	23	internal	internal	ADJ
eurjchem-591	25	24	standard	standard	NOUN
eurjchem-591	25	25	.	.	PUNCT
eurjchem-591	26	1	the	the	DET
eurjchem-591	26	2	crystallographic	crystallographic	ADJ
eurjchem-591	26	3	data	datum	NOUN
eurjchem-591	26	4	of	of	ADP
eurjchem-591	26	5	bis(4‐bromo‐n‐	bis(4‐bromo‐n‐	PROPN
eurjchem-591	26	6	diethylcarbamothioyl	diethylcarbamothioyl	PROPN
eurjchem-591	26	7	)	)	PUNCT
eurjchem-591	26	8	benzamido)nickel(ii	benzamido)nickel(ii	NOUN
eurjchem-591	26	9	)	)	PUNCT
eurjchem-591	26	10	complex	complex	NOUN
eurjchem-591	26	11	were	be	AUX
eurjchem-591	26	12	recorded	record	VERB
eurjchem-591	26	13	on	on	ADP
eurjchem-591	26	14	a	a	DET
eurjchem-591	26	15	bruker	bruker	PROPN
eurjchem-591	26	16	axs	axs	PROPN
eurjchem-591	26	17	smart‐apex	smart‐apex	PROPN
eurjchem-591	26	18	diffractometer	diffractometer	NOUN
eurjchem-591	26	19	using	use	VERB
eurjchem-591	26	20	mok	mok	PROPN
eurjchem-591	26	21	radiation	radiation	NOUN
eurjchem-591	26	22	(	(	PUNCT
eurjchem-591	26	23			X
eurjchem-591	26	24	=	=	PUNCT
eurjchem-591	26	25	0.71073	0.71073	NUM
eurjchem-591	26	26	å	å	NOUN
eurjchem-591	26	27	)	)	PUNCT
eurjchem-591	26	28	at	at	ADP
eurjchem-591	26	29	t	t	NOUN
eurjchem-591	26	30	=	=	SYM
eurjchem-591	26	31	120(2	120(2	NUM
eurjchem-591	26	32	)	)	PUNCT
eurjchem-591	26	33	k.	k.	NOUN
eurjchem-591	27	1	the	the	DET
eurjchem-591	27	2	structure	structure	NOUN
eurjchem-591	27	3	was	be	AUX
eurjchem-591	27	4	solved	solve	VERB
eurjchem-591	27	5	by	by	ADP
eurjchem-591	27	6	direct	direct	ADJ
eurjchem-591	27	7	methods	method	NOUN
eurjchem-591	27	8	and	and	CCONJ
eurjchem-591	27	9	refined	refine	VERB
eurjchem-591	27	10	by	by	ADP
eurjchem-591	27	11	least	least	ADJ
eurjchem-591	27	12	square	square	ADJ
eurjchem-591	27	13	cycles	cycle	NOUN
eurjchem-591	27	14	.	.	PUNCT
eurjchem-591	28	1	the	the	DET
eurjchem-591	28	2	non‐hydrogen	non‐hydrogen	NOUN
eurjchem-591	28	3	atoms	atom	NOUN
eurjchem-591	28	4	were	be	AUX
eurjchem-591	28	5	refined	refine	VERB
eurjchem-591	28	6	anisotropically	anisotropically	ADV
eurjchem-591	28	7	.	.	PUNCT
eurjchem-591	29	1	all	all	DET
eurjchem-591	29	2	calculations	calculation	NOUN
eurjchem-591	29	3	were	be	AUX
eurjchem-591	29	4	performed	perform	VERB
eurjchem-591	29	5	using	use	VERB
eurjchem-591	29	6	the	the	DET
eurjchem-591	29	7	shelxtl‐97	shelxtl‐97	PROPN
eurjchem-591	29	8	package	package	NOUN
eurjchem-591	29	9	[	[	X
eurjchem-591	29	10	30	30	NUM
eurjchem-591	29	11	]	]	PUNCT
eurjchem-591	29	12	.	.	PUNCT
eurjchem-591	30	1	the	the	DET
eurjchem-591	30	2	crystallographic	crystallographic	ADJ
eurjchem-591	30	3	data	datum	NOUN
eurjchem-591	30	4	for	for	ADP
eurjchem-591	30	5	the	the	DET
eurjchem-591	30	6	complex	complex	NOUN
eurjchem-591	30	7	are	be	AUX
eurjchem-591	30	8	listed	list	VERB
eurjchem-591	30	9	in	in	ADP
eurjchem-591	30	10	table	table	NOUN
eurjchem-591	30	11	1	1	NUM
eurjchem-591	30	12	.	.	X
eurjchem-591	30	13	2.2	2.2	NUM
eurjchem-591	30	14	.	.	PUNCT
eurjchem-591	31	1	synthesis	synthesis	NOUN
eurjchem-591	31	2	of	of	ADP
eurjchem-591	31	3	bis(4‐bromo‐n‐(diethylcarbamothioyl	bis(4‐bromo‐n‐(diethylcarbamothioyl	PROPN
eurjchem-591	31	4	)	)	PUNCT
eurjchem-591	31	5	benzamido)nickel(ii	benzamido)nickel(ii	NOUN
eurjchem-591	31	6	)	)	PUNCT
eurjchem-591	31	7	complex	complex	ADJ
eurjchem-591	31	8	all	all	DET
eurjchem-591	31	9	chemicals	chemical	NOUN
eurjchem-591	31	10	were	be	AUX
eurjchem-591	31	11	used	use	VERB
eurjchem-591	31	12	as	as	SCONJ
eurjchem-591	31	13	obtained	obtain	VERB
eurjchem-591	31	14	from	from	ADP
eurjchem-591	31	15	merck	merck	NOUN
eurjchem-591	31	16	and	and	CCONJ
eurjchem-591	31	17	analytical‐grade	analytical‐grade	NOUN
eurjchem-591	31	18	solvents	solvent	NOUN
eurjchem-591	31	19	were	be	AUX
eurjchem-591	31	20	used	use	VERB
eurjchem-591	31	21	without	without	ADP
eurjchem-591	31	22	further	further	ADJ
eurjchem-591	31	23	purification	purification	NOUN
eurjchem-591	31	24	.	.	PUNCT
eurjchem-591	32	1	the	the	DET
eurjchem-591	32	2	bis(4‐bromo‐n‐(diethylcarbamothioyl)benz‐	bis(4‐bromo‐n‐(diethylcarbamothioyl)benz‐	PROPN
eurjchem-591	32	3	amido)nickel(ii	amido)nickel(ii	NOUN
eurjchem-591	32	4	)	)	PUNCT
eurjchem-591	32	5	complex	complex	NOUN
eurjchem-591	32	6	was	be	AUX
eurjchem-591	32	7	prepared	prepare	VERB
eurjchem-591	32	8	according	accord	VERB
eurjchem-591	32	9	to	to	ADP
eurjchem-591	32	10	the	the	DET
eurjchem-591	32	11	method	method	NOUN
eurjchem-591	32	12	described	describe	VERB
eurjchem-591	32	13	in	in	ADP
eurjchem-591	32	14	the	the	DET
eurjchem-591	32	15	literature	literature	NOUN
eurjchem-591	32	16	[	[	X
eurjchem-591	32	17	16	16	NUM
eurjchem-591	32	18	]	]	PUNCT
eurjchem-591	32	19	(	(	PUNCT
eurjchem-591	32	20	scheme	scheme	NOUN
eurjchem-591	32	21	1	1	NUM
eurjchem-591	32	22	)	)	PUNCT
eurjchem-591	32	23	.	.	PUNCT
eurjchem-591	33	1	4‐bromo‐n‐(diethylcarbamothioyl)benzamide	4‐bromo‐n‐(diethylcarbamothioyl)benzamide	PROPN
eurjchem-591	33	2	was	be	AUX
eurjchem-591	33	3	dissol‐	dissol‐	PRON
eurjchem-591	33	4	ved	ve	VERB
eurjchem-591	33	5	in	in	ADP
eurjchem-591	33	6	methanol	methanol	NOUN
eurjchem-591	33	7	(	(	PUNCT
eurjchem-591	33	8	30	30	NUM
eurjchem-591	33	9	ml	ml	NOUN
eurjchem-591	33	10	)	)	PUNCT
eurjchem-591	33	11	and	and	CCONJ
eurjchem-591	33	12	added	add	VERB
eurjchem-591	33	13	dropwise	dropwise	NOUN
eurjchem-591	33	14	to	to	ADP
eurjchem-591	33	15	nickel(ii	nickel(ii	PROPN
eurjchem-591	33	16	)	)	PUNCT
eurjchem-591	33	17	acetate	acetate	NOUN
eurjchem-591	33	18	,	,	PUNCT
eurjchem-591	33	19	ni(ch3coo)2	ni(ch3coo)2	PROPN
eurjchem-591	33	20	,	,	PUNCT
eurjchem-591	33	21	in	in	ADP
eurjchem-591	33	22	methanol	methanol	NOUN
eurjchem-591	33	23	(	(	PUNCT
eurjchem-591	33	24	30	30	NUM
eurjchem-591	33	25	ml	ml	NOUN
eurjchem-591	33	26	)	)	PUNCT
eurjchem-591	33	27	in	in	ADP
eurjchem-591	33	28	a	a	DET
eurjchem-591	33	29	1:2	1:2	NUM
eurjchem-591	33	30	ratio	ratio	NOUN
eurjchem-591	33	31	(	(	PUNCT
eurjchem-591	33	32	metal	metal	NOUN
eurjchem-591	33	33	:	:	PUNCT
eurjchem-591	33	34	ligand	ligand	NOUN
eurjchem-591	33	35	)	)	PUNCT
eurjchem-591	33	36	at	at	ADP
eurjchem-591	33	37	ph	ph	PROPN
eurjchem-591	33	38	>	>	PUNCT
eurjchem-591	33	39	7	7	NUM
eurjchem-591	33	40	and	and	CCONJ
eurjchem-591	33	41	the	the	DET
eurjchem-591	33	42	mixture	mixture	NOUN
eurjchem-591	33	43	was	be	AUX
eurjchem-591	33	44	stirred	stir	VERB
eurjchem-591	33	45	for	for	ADP
eurjchem-591	33	46	30	30	NUM
eurjchem-591	33	47	min	min	NOUN
eurjchem-591	33	48	at	at	ADP
eurjchem-591	33	49	room	room	NOUN
eurjchem-591	33	50	temperature	temperature	NOUN
eurjchem-591	33	51	.	.	PUNCT
eurjchem-591	34	1	during	during	ADP
eurjchem-591	34	2	the	the	DET
eurjchem-591	34	3	time	time	NOUN
eurjchem-591	34	4	,	,	PUNCT
eurjchem-591	34	5	the	the	DET
eurjchem-591	34	6	color	color	NOUN
eurjchem-591	34	7	of	of	ADP
eurjchem-591	34	8	the	the	DET
eurjchem-591	34	9	4‐	4‐	PROPN
eurjchem-591	34	10	bromo‐n‐(diethylcarbamothioyl)benzamide	bromo‐n‐(diethylcarbamothioyl)benzamide	PROPN
eurjchem-591	34	11	is	be	AUX
eurjchem-591	34	12	changed	change	VERB
eurjchem-591	34	13	white	white	ADJ
eurjchem-591	34	14	to	to	ADP
eurjchem-591	34	15	purple	purple	ADJ
eurjchem-591	34	16	.	.	PUNCT
eurjchem-591	35	1	the	the	DET
eurjchem-591	35	2	change	change	NOUN
eurjchem-591	35	3	in	in	ADP
eurjchem-591	35	4	color	color	NOUN
eurjchem-591	35	5	was	be	AUX
eurjchem-591	35	6	due	due	ADJ
eurjchem-591	35	7	to	to	PART
eurjchem-591	35	8	complete	complete	VERB
eurjchem-591	35	9	the	the	DET
eurjchem-591	35	10	reaction	reaction	NOUN
eurjchem-591	35	11	.	.	PUNCT
eurjchem-591	36	1	the	the	DET
eurjchem-591	36	2	change	change	NOUN
eurjchem-591	36	3	in	in	ADP
eurjchem-591	36	4	color	color	NOUN
eurjchem-591	36	5	was	be	AUX
eurjchem-591	36	6	due	due	ADJ
eurjchem-591	36	7	to	to	ADP
eurjchem-591	36	8	the	the	DET
eurjchem-591	36	9	interaction	interaction	NOUN
eurjchem-591	36	10	of	of	ADP
eurjchem-591	36	11	nicl2.6h2o	nicl2.6h2o	NOUN
eurjchem-591	36	12	with	with	ADP
eurjchem-591	36	13	the	the	DET
eurjchem-591	36	14	4‐bromo‐n‐(diethylcarbamothioyl	4‐bromo‐n‐(diethylcarbamothioyl	PROPN
eurjchem-591	36	15	)	)	PUNCT
eurjchem-591	36	16	benzamide	benzamide	NOUN
eurjchem-591	36	17	.	.	PUNCT
eurjchem-591	37	1	38	38	NUM
eurjchem-591	37	2	binzet	binzet	NOUN
eurjchem-591	37	3	et	et	PROPN
eurjchem-591	37	4	al	al	PROPN
eurjchem-591	37	5	.	.	PUNCT
eurjchem-591	37	6	/	/	SYM
eurjchem-591	37	7	european	european	PROPN
eurjchem-591	37	8	journal	journal	PROPN
eurjchem-591	37	9	of	of	ADP
eurjchem-591	37	10	chemistry	chemistry	NOUN
eurjchem-591	37	11	3	3	NUM
eurjchem-591	37	12	(	(	PUNCT
eurjchem-591	37	13	1	1	NUM
eurjchem-591	37	14	)	)	PUNCT
eurjchem-591	37	15	(	(	PUNCT
eurjchem-591	37	16	2012	2012	NUM
eurjchem-591	37	17	)	)	PUNCT
eurjchem-591	37	18	37‐39	37‐39	NOUN
eurjchem-591	37	19	scheme	scheme	VERB
eurjchem-591	37	20	1	1	NUM
eurjchem-591	37	21	the	the	DET
eurjchem-591	37	22	solid	solid	ADJ
eurjchem-591	37	23	complex	complex	NOUN
eurjchem-591	37	24	was	be	AUX
eurjchem-591	37	25	filtered	filter	VERB
eurjchem-591	37	26	and	and	CCONJ
eurjchem-591	37	27	recrystallized	recrystallize	VERB
eurjchem-591	37	28	from	from	ADP
eurjchem-591	37	29	an	an	DET
eurjchem-591	37	30	ethanol	ethanol	NOUN
eurjchem-591	37	31	:	:	PUNCT
eurjchem-591	37	32	dichloromethane	dichloromethane	NOUN
eurjchem-591	37	33	mixture	mixture	NOUN
eurjchem-591	37	34	(	(	PUNCT
eurjchem-591	37	35	1:2	1:2	NUM
eurjchem-591	37	36	)	)	PUNCT
eurjchem-591	37	37	(	(	PUNCT
eurjchem-591	37	38	scheme	scheme	NOUN
eurjchem-591	37	39	1	1	NUM
eurjchem-591	37	40	)	)	PUNCT
eurjchem-591	37	41	.	.	PUNCT
eurjchem-591	38	1	purple	purple	ADJ
eurjchem-591	38	2	precipitate	precipitate	NOUN
eurjchem-591	38	3	was	be	AUX
eurjchem-591	38	4	formed	form	VERB
eurjchem-591	38	5	crystal	crystal	NOUN
eurjchem-591	38	6	suitable	suitable	ADJ
eurjchem-591	38	7	for	for	ADP
eurjchem-591	38	8	x‐ray	x‐ray	PROPN
eurjchem-591	38	9	single	single	ADJ
eurjchem-591	38	10	crystal	crystal	PROPN
eurjchem-591	38	11	diffraction	diffraction	NOUN
eurjchem-591	38	12	.	.	PUNCT
eurjchem-591	39	1	bis(4‐bromo‐n‐(diethylcarbamothioyl)benzamido	bis(4‐bromo‐n‐(diethylcarbamothioyl)benzamido	NOUN
eurjchem-591	39	2	)	)	PUNCT
eurjchem-591	40	1	nickel(ii	nickel(ii	ADJ
eurjchem-591	40	2	):	):	PUNCT
eurjchem-591	40	3	yield	yield	NOUN
eurjchem-591	40	4	:	:	PUNCT
eurjchem-591	40	5	82	82	NUM
eurjchem-591	40	6	%	%	NOUN
eurjchem-591	40	7	.	.	PUNCT
eurjchem-591	41	1	m.p	m.p	PROPN
eurjchem-591	41	2	.	.	PROPN
eurjchem-591	41	3	:	:	PUNCT
eurjchem-591	42	1	248‐250	248‐250	NUM
eurjchem-591	42	2	oc	oc	PROPN
eurjchem-591	42	3	.	.	PROPN
eurjchem-591	42	4	anal	anal	PROPN
eurjchem-591	42	5	.	.	PUNCT
eurjchem-591	42	6	calcd	calcd	NOUN
eurjchem-591	42	7	.	.	PUNCT
eurjchem-591	43	1	for	for	SCONJ
eurjchem-591	43	2	c24h28br2n4o2s2ni	c24h28br2n4o2s2ni	PROPN
eurjchem-591	43	3	:	:	PUNCT
eurjchem-591	43	4	c	c	X
eurjchem-591	43	5	,	,	PUNCT
eurjchem-591	43	6	41.95	41.95	NUM
eurjchem-591	43	7	;	;	PUNCT
eurjchem-591	43	8	h	h	NOUN
eurjchem-591	43	9	,	,	PUNCT
eurjchem-591	43	10	4.11	4.11	NUM
eurjchem-591	43	11	;	;	PUNCT
eurjchem-591	43	12	n	n	CCONJ
eurjchem-591	43	13	,	,	PUNCT
eurjchem-591	43	14	8.15	8.15	NUM
eurjchem-591	43	15	.	.	PUNCT
eurjchem-591	43	16	found	find	VERB
eurjchem-591	43	17	:	:	PUNCT
eurjchem-591	44	1	c	c	X
eurjchem-591	44	2	,	,	PUNCT
eurjchem-591	44	3	41.80	41.80	NUM
eurjchem-591	44	4	;	;	PUNCT
eurjchem-591	44	5	h	h	NOUN
eurjchem-591	44	6	,	,	PUNCT
eurjchem-591	44	7	4.05	4.05	NUM
eurjchem-591	44	8	;	;	PUNCT
eurjchem-591	44	9	n	n	CCONJ
eurjchem-591	44	10	,	,	PUNCT
eurjchem-591	44	11	8.16	8.16	NUM
eurjchem-591	44	12	%	%	NOUN
eurjchem-591	44	13	.	.	PUNCT
eurjchem-591	45	1	ft‐ir	ft‐ir	NOUN
eurjchem-591	45	2	(	(	PUNCT
eurjchem-591	45	3	kbr	kbr	PROPN
eurjchem-591	45	4	,	,	PUNCT
eurjchem-591	45	5	cm‐1	cm‐1	PROPN
eurjchem-591	45	6	):	):	PUNCT
eurjchem-591	45	7	2974	2974	NUM
eurjchem-591	45	8	,	,	PUNCT
eurjchem-591	45	9	2932	2932	NUM
eurjchem-591	45	10	,	,	PUNCT
eurjchem-591	45	11	2868	2868	NUM
eurjchem-591	45	12	(	(	PUNCT
eurjchem-591	45	13	ch	ch	NOUN
eurjchem-591	45	14	)	)	PUNCT
eurjchem-591	45	15	;	;	PUNCT
eurjchem-591	45	16	1581	1581	NUM
eurjchem-591	45	17	(	(	PUNCT
eurjchem-591	45	18	cn	cn	NOUN
eurjchem-591	45	19	)	)	PUNCT
eurjchem-591	45	20	,	,	PUNCT
eurjchem-591	45	21	1492	1492	NUM
eurjchem-591	45	22	(	(	PUNCT
eurjchem-591	45	23	c‐o	c‐o	NOUN
eurjchem-591	45	24	)	)	PUNCT
eurjchem-591	45	25	,	,	PUNCT
eurjchem-591	45	26	751	751	NUM
eurjchem-591	45	27	(	(	PUNCT
eurjchem-591	45	28	c‐br	c‐br	NOUN
eurjchem-591	45	29	)	)	PUNCT
eurjchem-591	45	30	.	.	PUNCT
eurjchem-591	46	1	1h	1h	NUM
eurjchem-591	46	2	nmr	nmr	NOUN
eurjchem-591	46	3	(	(	PUNCT
eurjchem-591	46	4	400	400	NUM
eurjchem-591	46	5	mhz	mhz	NOUN
eurjchem-591	46	6	,	,	PUNCT
eurjchem-591	46	7	cdcl3	cdcl3	PROPN
eurjchem-591	46	8	,	,	PUNCT
eurjchem-591	46	9	δ	δ	PROPN
eurjchem-591	46	10	,	,	PUNCT
eurjchem-591	46	11	ppm	ppm	NUM
eurjchem-591	46	12	):	):	PUNCT
eurjchem-591	46	13	7.96	7.96	NUM
eurjchem-591	46	14	(	(	PUNCT
eurjchem-591	46	15	d	d	PROPN
eurjchem-591	46	16	,	,	PUNCT
eurjchem-591	46	17	4h	4h	NUM
eurjchem-591	46	18	,	,	PUNCT
eurjchem-591	46	19	ar‐h	ar‐h	PROPN
eurjchem-591	46	20	)	)	PUNCT
eurjchem-591	46	21	,	,	PUNCT
eurjchem-591	46	22	7.52	7.52	NUM
eurjchem-591	46	23	(	(	PUNCT
eurjchem-591	46	24	d	d	PROPN
eurjchem-591	46	25	,	,	PUNCT
eurjchem-591	46	26	4h	4h	NUM
eurjchem-591	46	27	,	,	PUNCT
eurjchem-591	46	28	ar‐h	ar‐h	PROPN
eurjchem-591	46	29	)	)	PUNCT
eurjchem-591	46	30	,	,	PUNCT
eurjchem-591	46	31	3.57	3.57	NUM
eurjchem-591	46	32	(	(	PUNCT
eurjchem-591	46	33	m	m	PROPN
eurjchem-591	46	34	,	,	PUNCT
eurjchem-591	46	35	8h	8h	PROPN
eurjchem-591	46	36	,	,	PUNCT
eurjchem-591	46	37	n‐	n‐	NOUN
eurjchem-591	46	38	ch2	ch2	PROPN
eurjchem-591	46	39	)	)	PUNCT
eurjchem-591	46	40	,	,	PUNCT
eurjchem-591	46	41	1.48	1.48	NUM
eurjchem-591	46	42	(	(	PUNCT
eurjchem-591	46	43	m	m	PROPN
eurjchem-591	46	44	,	,	PUNCT
eurjchem-591	46	45	12h,‐ch3	12h,‐ch3	ADJ
eurjchem-591	46	46	)	)	PUNCT
eurjchem-591	46	47	.	.	PUNCT
eurjchem-591	47	1	table	table	NOUN
eurjchem-591	47	2	1	1	NUM
eurjchem-591	47	3	.	.	PUNCT
eurjchem-591	48	1	crystal	crystal	NOUN
eurjchem-591	48	2	data	datum	NOUN
eurjchem-591	48	3	and	and	CCONJ
eurjchem-591	48	4	structure	structure	NOUN
eurjchem-591	48	5	refinement	refinement	NOUN
eurjchem-591	48	6	for	for	ADP
eurjchem-591	48	7	the	the	DET
eurjchem-591	48	8	title	title	NOUN
eurjchem-591	48	9	compound	compound	NOUN
eurjchem-591	48	10	.	.	PUNCT
eurjchem-591	49	1	empirical	empirical	ADJ
eurjchem-591	49	2	formula	formula	NOUN
eurjchem-591	49	3	c24h28br2nin4o2s2	c24h28br2nin4o2s2	NOUN
eurjchem-591	49	4	formula	formula	NOUN
eurjchem-591	49	5	weight	weight	NOUN
eurjchem-591	49	6	687.15	687.15	NUM
eurjchem-591	49	7	temperature	temperature	NOUN
eurjchem-591	49	8	 	 	SPACE
eurjchem-591	49	9	/	/	SYM
eurjchem-591	49	10	 	 	SPACE
eurjchem-591	49	11	k	k	PROPN
eurjchem-591	49	12	120(2	120(2	NUM
eurjchem-591	49	13	)	)	PUNCT
eurjchem-591	49	14	crystal	crystal	NOUN
eurjchem-591	49	15	system	system	NOUN
eurjchem-591	49	16	monoclinic	monoclinic	ADJ
eurjchem-591	49	17	space	space	NOUN
eurjchem-591	49	18	group	group	NOUN
eurjchem-591	49	19	p21	p21	PROPN
eurjchem-591	49	20	/	/	SYM
eurjchem-591	49	21	c	c	PROPN
eurjchem-591	49	22	a	a	DET
eurjchem-591	49	23	 	 	SPACE
eurjchem-591	49	24	/	/	SYM
eurjchem-591	49	25	 	 	SPACE
eurjchem-591	49	26	å	å	PROPN
eurjchem-591	49	27	,	,	PUNCT
eurjchem-591	49	28	b	b	NOUN
eurjchem-591	49	29	 	 	SPACE
eurjchem-591	49	30	/	/	SYM
eurjchem-591	49	31	 	 	SPACE
eurjchem-591	49	32	å	å	PROPN
eurjchem-591	49	33	,	,	PUNCT
eurjchem-591	49	34	c	c	AUX
eurjchem-591	49	35	 	 	SPACE
eurjchem-591	49	36	/	/	SYM
eurjchem-591	49	37	 	 	SPACE
eurjchem-591	49	38	å	å	PROPN
eurjchem-591	49	39	12.9099(17	12.9099(17	NUM
eurjchem-591	49	40	)	)	PUNCT
eurjchem-591	49	41	,	,	PUNCT
eurjchem-591	49	42	15.264(2	15.264(2	NUM
eurjchem-591	49	43	)	)	PUNCT
eurjchem-591	49	44	,	,	PUNCT
eurjchem-591	49	45	14.0287(19	14.0287(19	NUM
eurjchem-591	49	46	)	)	PUNCT
eurjchem-591	49	47	β	β	NOUN
eurjchem-591	49	48	°	°	VERB
eurjchem-591	49	49	92.140(4	92.140(4	NOUN
eurjchem-591	49	50	)	)	PUNCT
eurjchem-591	49	51	volume	volume	NOUN
eurjchem-591	49	52	 	 	SPACE
eurjchem-591	49	53	/	/	SYM
eurjchem-591	49	54	 	 	SPACE
eurjchem-591	49	55	å3	å3	PROPN
eurjchem-591	49	56	2762.5(6	2762.5(6	NUM
eurjchem-591	49	57	)	)	PUNCT
eurjchem-591	49	58	z	z	NOUN
eurjchem-591	49	59	4	4	NUM
eurjchem-591	49	60	ρcalc	ρcalc	NOUN
eurjchem-591	49	61	.	.	PUNCT
eurjchem-591	49	62	 	 	SPACE
eurjchem-591	50	1	/	/	SYM
eurjchem-591	50	2	 	 	SPACE
eurjchem-591	50	3	mg	mg	PROPN
eurjchem-591	50	4	mm‐3	mm‐3	PROPN
eurjchem-591	51	1	1.652	1.652	NUM
eurjchem-591	51	2	μ	μ	NOUN
eurjchem-591	51	3	 	 	SPACE
eurjchem-591	51	4	/	/	SYM
eurjchem-591	51	5	 	 	SPACE
eurjchem-591	51	6	mm‐1	mm‐1	NOUN
eurjchem-591	51	7	3.775	3.775	NUM
eurjchem-591	51	8	f(000	f(000	NOUN
eurjchem-591	51	9	)	)	PUNCT
eurjchem-591	51	10	1384	1384	NUM
eurjchem-591	51	11	crystal	crystal	NOUN
eurjchem-591	51	12	size	size	NOUN
eurjchem-591	51	13	 	 	SPACE
eurjchem-591	51	14	/	/	SYM
eurjchem-591	51	15	 	 	SPACE
eurjchem-591	51	16	mm3	mm3	NOUN
eurjchem-591	51	17	0.26	0.26	NUM
eurjchem-591	51	18	x	x	SYM
eurjchem-591	51	19	0.26	0.26	NUM
eurjchem-591	51	20	x	x	SYM
eurjchem-591	51	21	0.09	0.09	NUM
eurjchem-591	51	22	2θ	2θ	NUM
eurjchem-591	51	23	range	range	NOUN
eurjchem-591	51	24	for	for	ADP
eurjchem-591	51	25	data	datum	NOUN
eurjchem-591	51	26	collection	collection	NOUN
eurjchem-591	51	27	1.58	1.58	NUM
eurjchem-591	51	28	to	to	ADP
eurjchem-591	51	29	27.88	27.88	NUM
eurjchem-591	51	30	°	°	PART
eurjchem-591	51	31	index	index	NOUN
eurjchem-591	51	32	ranges	range	NOUN
eurjchem-591	51	33	‐13	‐13	VERB
eurjchem-591	51	34	≤	≤	NUM
eurjchem-591	51	35	h	h	NOUN
eurjchem-591	51	36	≤	≤	NUM
eurjchem-591	51	37	16	16	NUM
eurjchem-591	51	38	,	,	PUNCT
eurjchem-591	51	39	‐18	‐18	NOUN
eurjchem-591	52	1	≤	≤	PROPN
eurjchem-591	52	2	k	k	PROPN
eurjchem-591	52	3	≤	≤	NUM
eurjchem-591	52	4	20	20	NUM
eurjchem-591	52	5	,	,	PUNCT
eurjchem-591	52	6	‐18	‐18	NOUN
eurjchem-591	52	7	≤	≤	PROPN
eurjchem-591	52	8	l	l	NOUN
eurjchem-591	52	9	≤	≤	NUM
eurjchem-591	52	10	18	18	NUM
eurjchem-591	52	11	reflections	reflection	NOUN
eurjchem-591	52	12	collected	collect	VERB
eurjchem-591	52	13	22583	22583	NUM
eurjchem-591	52	14	independent	independent	ADJ
eurjchem-591	52	15	reflections	reflection	NOUN
eurjchem-591	52	16	6579	6579	NUM
eurjchem-591	53	1	[	[	X
eurjchem-591	53	2	r(int	r(int	X
eurjchem-591	53	3	)	)	PUNCT
eurjchem-591	53	4	=	=	PUNCT
eurjchem-591	53	5	0.0607	0.0607	NUM
eurjchem-591	53	6	]	]	PUNCT
eurjchem-591	53	7	data	data	NOUN
eurjchem-591	53	8	/	/	SYM
eurjchem-591	53	9	restraints	restraint	NOUN
eurjchem-591	53	10	/	/	SYM
eurjchem-591	53	11	parameters	parameter	NOUN
eurjchem-591	53	12	6579/4/324	6579/4/324	NUM
eurjchem-591	53	13	goodness‐of‐fit	goodness‐of‐fit	NOUN
eurjchem-591	53	14	on	on	ADP
eurjchem-591	53	15	f2	f2	PROPN
eurjchem-591	53	16	1.026	1.026	NUM
eurjchem-591	53	17	final	final	ADJ
eurjchem-591	53	18	r	r	NOUN
eurjchem-591	53	19	indexes	index	NOUN
eurjchem-591	54	1	[	[	X
eurjchem-591	54	2	i>2σ	i>2σ	PROPN
eurjchem-591	54	3	(	(	PUNCT
eurjchem-591	54	4	i	i	NOUN
eurjchem-591	54	5	)	)	PUNCT
eurjchem-591	54	6	]	]	PUNCT
eurjchem-591	54	7	r1	r1	NOUN
eurjchem-591	54	8	=	=	SYM
eurjchem-591	54	9	0.0503	0.0503	NUM
eurjchem-591	54	10	,	,	PUNCT
eurjchem-591	54	11	wr2	wr2	PROPN
eurjchem-591	54	12	=	=	NOUN
eurjchem-591	54	13	0.1146	0.1146	NUM
eurjchem-591	54	14	final	final	ADJ
eurjchem-591	54	15	r	r	NOUN
eurjchem-591	54	16	indexes	index	NOUN
eurjchem-591	54	17	[	[	X
eurjchem-591	54	18	all	all	DET
eurjchem-591	54	19	data	datum	NOUN
eurjchem-591	54	20	]	]	PUNCT
eurjchem-591	54	21	r1	r1	PROPN
eurjchem-591	54	22	=	=	SYM
eurjchem-591	54	23	0.0901	0.0901	PROPN
eurjchem-591	54	24	,	,	PUNCT
eurjchem-591	54	25	wr2	wr2	PROPN
eurjchem-591	54	26	=	=	PROPN
eurjchem-591	54	27	0.1301	0.1301	NUM
eurjchem-591	54	28	largest	large	ADJ
eurjchem-591	54	29	diff	diff	NOUN
eurjchem-591	54	30	.	.	PUNCT
eurjchem-591	54	31	peak	peak	NOUN
eurjchem-591	54	32	/	/	SYM
eurjchem-591	54	33	hole	hole	NOUN
eurjchem-591	54	34	 	 	SPACE
eurjchem-591	54	35	/	/	SYM
eurjchem-591	54	36	 	 	SPACE
eurjchem-591	54	37	e	e	NOUN
eurjchem-591	54	38	å‐3	å‐3	NOUN
eurjchem-591	54	39	0.731	0.731	NUM
eurjchem-591	54	40	/	/	SYM
eurjchem-591	54	41	‐0.612	‐0.612	PROPN
eurjchem-591	54	42	3	3	NUM
eurjchem-591	54	43	.	.	NOUN
eurjchem-591	54	44	results	result	NOUN
eurjchem-591	54	45	and	and	CCONJ
eurjchem-591	54	46	discussion	discussion	VERB
eurjchem-591	54	47	the	the	DET
eurjchem-591	54	48	reaction	reaction	NOUN
eurjchem-591	54	49	of	of	ADP
eurjchem-591	54	50	nickel(ii	nickel(ii	ADJ
eurjchem-591	54	51	)	)	PUNCT
eurjchem-591	54	52	acetate	acetate	NOUN
eurjchem-591	54	53	,	,	PUNCT
eurjchem-591	54	54	ni(ch3coo)2	ni(ch3coo)2	PROPN
eurjchem-591	54	55	,	,	PUNCT
eurjchem-591	54	56	with	with	ADP
eurjchem-591	54	57	two	two	NUM
eurjchem-591	54	58	equivalents	equivalent	NOUN
eurjchem-591	54	59	of	of	ADP
eurjchem-591	54	60	4‐bromo‐n‐(diethylcarbamothioyl)benzamide	4‐bromo‐n‐(diethylcarbamothioyl)benzamide	NOUN
eurjchem-591	54	61	in	in	ADP
eurjchem-591	54	62	methanol	methanol	NOUN
eurjchem-591	54	63	produces	produce	VERB
eurjchem-591	54	64	the	the	DET
eurjchem-591	54	65	potentially	potentially	ADV
eurjchem-591	54	66	bidentate	bidentate	ADJ
eurjchem-591	54	67	molecule	molecule	NOUN
eurjchem-591	54	68	bis(4‐	bis(4‐	PROPN
eurjchem-591	54	69	bromo‐n‐(diethylcarbamothioyl)benzamido)nickel(ii	bromo‐n‐(diethylcarbamothioyl)benzamido)nickel(ii	NOUN
eurjchem-591	54	70	)	)	PUNCT
eurjchem-591	54	71	complex	complex	ADJ
eurjchem-591	54	72	high	high	ADJ
eurjchem-591	54	73	yield	yield	NOUN
eurjchem-591	54	74	(	(	PUNCT
eurjchem-591	54	75	scheme	scheme	NOUN
eurjchem-591	54	76	1	1	NUM
eurjchem-591	54	77	)	)	PUNCT
eurjchem-591	54	78	,	,	PUNCT
eurjchem-591	54	79	as	as	ADP
eurjchem-591	54	80	an	an	DET
eurjchem-591	54	81	air‐stable	air‐stable	ADJ
eurjchem-591	54	82	purple	purple	NOUN
eurjchem-591	54	83	solid	solid	NOUN
eurjchem-591	54	84	.	.	PUNCT
eurjchem-591	55	1	the	the	DET
eurjchem-591	55	2	single	single	ADJ
eurjchem-591	55	3	crystals	crystal	NOUN
eurjchem-591	55	4	of	of	ADP
eurjchem-591	55	5	nickel(ii	nickel(ii	ADJ
eurjchem-591	55	6	)	)	PUNCT
eurjchem-591	55	7	complex	complex	NOUN
eurjchem-591	55	8	were	be	AUX
eurjchem-591	55	9	grown	grow	VERB
eurjchem-591	55	10	by	by	ADP
eurjchem-591	55	11	re‐crystallization	re‐crystallization	NOUN
eurjchem-591	55	12	from	from	ADP
eurjchem-591	55	13	an	an	DET
eurjchem-591	55	14	ethanol	ethanol	NOUN
eurjchem-591	55	15	:	:	PUNCT
eurjchem-591	55	16	dichloromethane	dichloromethane	NOUN
eurjchem-591	55	17	solution	solution	NOUN
eurjchem-591	55	18	mixture	mixture	NOUN
eurjchem-591	55	19	(	(	PUNCT
eurjchem-591	55	20	1:2	1:2	NUM
eurjchem-591	55	21	)	)	PUNCT
eurjchem-591	55	22	at	at	ADP
eurjchem-591	55	23	ambient	ambient	ADJ
eurjchem-591	55	24	temperature	temperature	NOUN
eurjchem-591	55	25	.	.	PUNCT
eurjchem-591	56	1	the	the	DET
eurjchem-591	56	2	ortep	ortep	NOUN
eurjchem-591	56	3	drawing	drawing	NOUN
eurjchem-591	56	4	of	of	ADP
eurjchem-591	56	5	complex	complex	NOUN
eurjchem-591	56	6	is	be	AUX
eurjchem-591	56	7	illustrated	illustrate	VERB
eurjchem-591	56	8	in	in	ADP
eurjchem-591	56	9	figure	figure	NOUN
eurjchem-591	56	10	1	1	NUM
eurjchem-591	56	11	and	and	CCONJ
eurjchem-591	56	12	some	some	DET
eurjchem-591	56	13	selected	select	VERB
eurjchem-591	56	14	bond	bond	NOUN
eurjchem-591	56	15	lengths	length	NOUN
eurjchem-591	56	16	and	and	CCONJ
eurjchem-591	56	17	angles	angle	NOUN
eurjchem-591	56	18	are	be	AUX
eurjchem-591	56	19	listed	list	VERB
eurjchem-591	56	20	in	in	ADP
eurjchem-591	56	21	table	table	NOUN
eurjchem-591	56	22	1	1	NUM
eurjchem-591	56	23	and	and	CCONJ
eurjchem-591	56	24	table	table	NOUN
eurjchem-591	56	25	2	2	NUM
eurjchem-591	56	26	.	.	PUNCT
eurjchem-591	57	1	in	in	ADP
eurjchem-591	57	2	this	this	DET
eurjchem-591	57	3	complex	complex	NOUN
eurjchem-591	57	4	,	,	PUNCT
eurjchem-591	57	5	the	the	DET
eurjchem-591	57	6	central	central	ADJ
eurjchem-591	57	7	ni(ii	ni(ii	PROPN
eurjchem-591	57	8	)	)	PUNCT
eurjchem-591	57	9	atom	atom	NOUN
eurjchem-591	57	10	is	be	AUX
eurjchem-591	57	11	a	a	DET
eurjchem-591	57	12	cis‐complex	cis‐complex	NOUN
eurjchem-591	57	13	with	with	ADP
eurjchem-591	57	14	slightly	slightly	ADV
eurjchem-591	57	15	distorted	distorted	ADJ
eurjchem-591	57	16	square	square	ADJ
eurjchem-591	57	17	planar	planar	ADJ
eurjchem-591	57	18	coordination	coordination	NOUN
eurjchem-591	57	19	.	.	PUNCT
eurjchem-591	58	1	in	in	ADP
eurjchem-591	58	2	this	this	DET
eurjchem-591	58	3	complex	complex	ADJ
eurjchem-591	58	4	center	center	NOUN
eurjchem-591	58	5	nickel	nickel	NOUN
eurjchem-591	58	6	atom	atom	NOUN
eurjchem-591	58	7	coordinated	coordinate	VERB
eurjchem-591	58	8	by	by	ADP
eurjchem-591	58	9	two	two	NUM
eurjchem-591	58	10	sulfur	sulfur	NOUN
eurjchem-591	58	11	and	and	CCONJ
eurjchem-591	58	12	two	two	NUM
eurjchem-591	58	13	oxygen	oxygen	NOUN
eurjchem-591	58	14	atoms	atom	NOUN
eurjchem-591	58	15	from	from	ADP
eurjchem-591	58	16	two	two	NUM
eurjchem-591	58	17	ligands	ligand	NOUN
eurjchem-591	58	18	.	.	PUNCT
eurjchem-591	59	1	the	the	DET
eurjchem-591	59	2	bond	bond	NOUN
eurjchem-591	59	3	lengths	length	NOUN
eurjchem-591	59	4	of	of	ADP
eurjchem-591	59	5	the	the	DET
eurjchem-591	59	6	carbonyl	carbonyl	NOUN
eurjchem-591	59	7	o1‐c6	o1‐c6	VERB
eurjchem-591	59	8	1.263(5	1.263(5	NUM
eurjchem-591	59	9	)	)	PUNCT
eurjchem-591	59	10	å	å	NOUN
eurjchem-591	59	11	;	;	PUNCT
eurjchem-591	59	12	o2‐c18	o2‐c18	NOUN
eurjchem-591	59	13	1.268(5	1.268(5	NUM
eurjchem-591	59	14	)	)	PUNCT
eurjchem-591	59	15	å	å	PROPN
eurjchem-591	59	16	and	and	CCONJ
eurjchem-591	59	17	thiocarbonyl	thiocarbonyl	VERB
eurjchem-591	59	18	s1‐c1	s1‐c1	NOUN
eurjchem-591	59	19	1.744(4	1.744(4	NUM
eurjchem-591	59	20	)	)	PUNCT
eurjchem-591	59	21	å	å	NOUN
eurjchem-591	59	22	;	;	PUNCT
eurjchem-591	59	23	s2‐c13	s2‐c13	NOUN
eurjchem-591	59	24	1.745(4	1.745(4	NUM
eurjchem-591	59	25	)	)	PUNCT
eurjchem-591	59	26	å	å	NOUN
eurjchem-591	59	27	groups	group	NOUN
eurjchem-591	59	28	lie	lie	VERB
eurjchem-591	59	29	between	between	ADP
eurjchem-591	59	30	those	those	PRON
eurjchem-591	59	31	for	for	ADP
eurjchem-591	59	32	double	double	ADJ
eurjchem-591	59	33	and	and	CCONJ
eurjchem-591	59	34	single	single	ADJ
eurjchem-591	59	35	bonds	bond	NOUN
eurjchem-591	59	36	.	.	PUNCT
eurjchem-591	60	1	the	the	DET
eurjchem-591	60	2	same	same	ADJ
eurjchem-591	60	3	behavior	behavior	NOUN
eurjchem-591	60	4	is	be	AUX
eurjchem-591	60	5	observed	observe	VERB
eurjchem-591	60	6	for	for	ADP
eurjchem-591	60	7	c‐n	c‐n	NOUN
eurjchem-591	60	8	bond	bond	NOUN
eurjchem-591	60	9	lengths	length	NOUN
eurjchem-591	60	10	.	.	PUNCT
eurjchem-591	61	1	c‐n	c‐n	VERB
eurjchem-591	61	2	bond	bond	NOUN
eurjchem-591	61	3	lengths	length	NOUN
eurjchem-591	61	4	for	for	ADP
eurjchem-591	61	5	the	the	DET
eurjchem-591	61	6	investigated	investigate	VERB
eurjchem-591	61	7	complex	complex	NOUN
eurjchem-591	61	8	is	be	AUX
eurjchem-591	61	9	shorter	short	ADJ
eurjchem-591	61	10	than	than	ADP
eurjchem-591	61	11	the	the	DET
eurjchem-591	61	12	average	average	ADJ
eurjchem-591	61	13	single	single	ADJ
eurjchem-591	61	14	c‐n	c‐n	PROPN
eurjchem-591	61	15	bond	bond	NOUN
eurjchem-591	61	16	length	length	NOUN
eurjchem-591	61	17	of	of	ADP
eurjchem-591	61	18	1.48	1.48	NUM
eurjchem-591	61	19	å	å	NOUN
eurjchem-591	61	20	,	,	PUNCT
eurjchem-591	61	21	being	be	AUX
eurjchem-591	61	22	c1‐n1	c1‐n1	NOUN
eurjchem-591	61	23	=	=	NOUN
eurjchem-591	61	24	1.335(5	1.335(5	NUM
eurjchem-591	61	25	)	)	PUNCT
eurjchem-591	61	26	å	å	NOUN
eurjchem-591	61	27	,	,	PUNCT
eurjchem-591	61	28	c6‐	c6‐	NOUN
eurjchem-591	61	29	n1=	n1=	PROPN
eurjchem-591	61	30	1.325(6	1.325(6	NUM
eurjchem-591	61	31	)	)	PUNCT
eurjchem-591	61	32	å	å	NOUN
eurjchem-591	61	33	,	,	PUNCT
eurjchem-591	61	34	c1‐n2	c1‐n2	X
eurjchem-591	61	35	=	=	SYM
eurjchem-591	61	36	1.334(6	1.334(6	NUM
eurjchem-591	61	37	)	)	PUNCT
eurjchem-591	61	38	å	å	NOUN
eurjchem-591	61	39	,	,	PUNCT
eurjchem-591	61	40	thus	thus	ADV
eurjchem-591	61	41	showing	show	VERB
eurjchem-591	61	42	varying	vary	VERB
eurjchem-591	61	43	degrees	degree	NOUN
eurjchem-591	61	44	of	of	ADP
eurjchem-591	61	45	double	double	ADJ
eurjchem-591	61	46	bond	bond	NOUN
eurjchem-591	61	47	character	character	NOUN
eurjchem-591	61	48	[	[	X
eurjchem-591	61	49	13‐27,33,34	13‐27,33,34	NUM
eurjchem-591	61	50	]	]	X
eurjchem-591	61	51	.	.	PUNCT
eurjchem-591	62	1	two	two	NUM
eurjchem-591	62	2	carbon	carbon	NOUN
eurjchem-591	62	3	atoms	atom	NOUN
eurjchem-591	62	4	of	of	ADP
eurjchem-591	62	5	one	one	NUM
eurjchem-591	62	6	of	of	ADP
eurjchem-591	62	7	the	the	DET
eurjchem-591	62	8	terminal	terminal	ADJ
eurjchem-591	62	9	ethyl	ethyl	PROPN
eurjchem-591	62	10	groups	group	NOUN
eurjchem-591	62	11	were	be	AUX
eurjchem-591	62	12	modelled	model	VERB
eurjchem-591	62	13	as	as	SCONJ
eurjchem-591	62	14	disordered	disorder	VERB
eurjchem-591	62	15	over	over	ADP
eurjchem-591	62	16	two	two	NUM
eurjchem-591	62	17	sites	site	NOUN
eurjchem-591	62	18	,	,	PUNCT
eurjchem-591	62	19	the	the	DET
eurjchem-591	62	20	ratio	ratio	NOUN
eurjchem-591	62	21	of	of	ADP
eurjchem-591	62	22	refined	refined	ADJ
eurjchem-591	62	23	occupancies	occupancy	NOUN
eurjchem-591	62	24	being	be	AUX
eurjchem-591	62	25	0.5:0.5	0.5:0.5	NUM
eurjchem-591	62	26	for	for	ADP
eurjchem-591	62	27	c141	c141	PRON
eurjchem-591	62	28	/	/	SYM
eurjchem-591	62	29	c151	c151	PROPN
eurjchem-591	62	30	:	:	PUNCT
eurjchem-591	62	31	c142	c142	NUM
eurjchem-591	62	32	/	/	SYM
eurjchem-591	62	33	c152	c152	PROPN
eurjchem-591	62	34	.	.	PUNCT
eurjchem-591	63	1	the	the	DET
eurjchem-591	63	2	c141‐c151	c141‐c151	PROPN
eurjchem-591	63	3	and	and	CCONJ
eurjchem-591	63	4	c141‐n4	c141‐n4	VERB
eurjchem-591	63	5	bond	bond	NOUN
eurjchem-591	63	6	lengths	length	NOUN
eurjchem-591	63	7	were	be	AUX
eurjchem-591	63	8	restrained	restrain	VERB
eurjchem-591	63	9	to	to	PART
eurjchem-591	63	10	be	be	AUX
eurjchem-591	63	11	equal	equal	ADJ
eurjchem-591	63	12	to	to	ADP
eurjchem-591	63	13	the	the	DET
eurjchem-591	63	14	c142‐c152	c142‐c152	PROPN
eurjchem-591	63	15	and	and	CCONJ
eurjchem-591	63	16	c142‐n4	c142‐n4	ADP
eurjchem-591	63	17	bond	bond	NOUN
eurjchem-591	63	18	lengths	length	NOUN
eurjchem-591	63	19	,	,	PUNCT
eurjchem-591	63	20	respectively	respectively	ADV
eurjchem-591	63	21	with	with	ADP
eurjchem-591	63	22	an	an	DET
eurjchem-591	63	23	effective	effective	ADJ
eurjchem-591	63	24	standard	standard	ADJ
eurjchem-591	63	25	deviation	deviation	NOUN
eurjchem-591	63	26	of	of	ADP
eurjchem-591	63	27	0.003	0.003	NUM
eurjchem-591	63	28	å	å	NOUN
eurjchem-591	63	29	.	.	PUNCT
eurjchem-591	64	1	h	h	NOUN
eurjchem-591	64	2	atoms	atom	NOUN
eurjchem-591	64	3	were	be	AUX
eurjchem-591	64	4	placed	place	VERB
eurjchem-591	64	5	in	in	ADP
eurjchem-591	64	6	calculated	calculate	VERB
eurjchem-591	64	7	positions	position	NOUN
eurjchem-591	64	8	and	and	CCONJ
eurjchem-591	64	9	refined	refine	VERB
eurjchem-591	64	10	as	as	ADP
eurjchem-591	64	11	riding	ride	VERB
eurjchem-591	64	12	,	,	PUNCT
eurjchem-591	64	13	with	with	ADP
eurjchem-591	64	14	uiso(h	uiso(h	NOUN
eurjchem-591	64	15	)	)	PUNCT
eurjchem-591	64	16	=	=	SYM
eurjchem-591	65	1	1.2ueq	1.2ueq	NUM
eurjchem-591	65	2	(	(	PUNCT
eurjchem-591	65	3	c	c	NOUN
eurjchem-591	65	4	)	)	PUNCT
eurjchem-591	65	5	or	or	CCONJ
eurjchem-591	65	6	1.5	1.5	NUM
eurjchem-591	65	7	ueq	ueq	NOUN
eurjchem-591	65	8	(	(	PUNCT
eurjchem-591	65	9	methyl	methyl	NOUN
eurjchem-591	65	10	c	c	NOUN
eurjchem-591	65	11	)	)	PUNCT
eurjchem-591	65	12	.	.	PUNCT
eurjchem-591	66	1	one	one	NUM
eurjchem-591	66	2	br	br	NOUN
eurjchem-591	66	3	atom	atom	NOUN
eurjchem-591	66	4	is	be	AUX
eurjchem-591	66	5	disordered	disorder	VERB
eurjchem-591	66	6	over	over	ADP
eurjchem-591	66	7	two	two	NUM
eurjchem-591	66	8	positions	position	NOUN
eurjchem-591	66	9	with	with	ADP
eurjchem-591	66	10	a	a	DET
eurjchem-591	66	11	refined	refined	ADJ
eurjchem-591	66	12	site‐occupancy	site‐occupancy	ADJ
eurjchem-591	66	13	ratio	ratio	NOUN
eurjchem-591	66	14	of	of	ADP
eurjchem-591	66	15	0.509(5):0.491	0.509(5):0.491	NUM
eurjchem-591	66	16	(	(	PUNCT
eurjchem-591	66	17	5	5	NUM
eurjchem-591	66	18	)	)	PUNCT
eurjchem-591	66	19	.	.	PUNCT
eurjchem-591	67	1	figure	figure	NOUN
eurjchem-591	67	2	1	1	NUM
eurjchem-591	67	3	.	.	PUNCT
eurjchem-591	68	1	a	a	DET
eurjchem-591	68	2	perspective	perspective	ADJ
eurjchem-591	68	3	view	view	NOUN
eurjchem-591	68	4	of	of	ADP
eurjchem-591	68	5	the	the	DET
eurjchem-591	68	6	title	title	NOUN
eurjchem-591	68	7	compound	compound	NOUN
eurjchem-591	68	8	,	,	PUNCT
eurjchem-591	68	9	with	with	ADP
eurjchem-591	68	10	atom‐numbering	atom‐numbere	VERB
eurjchem-591	68	11	scheme	scheme	NOUN
eurjchem-591	68	12	.	.	PUNCT
eurjchem-591	69	1	the	the	DET
eurjchem-591	69	2	crystal	crystal	NOUN
eurjchem-591	69	3	structure	structure	NOUN
eurjchem-591	69	4	is	be	AUX
eurjchem-591	69	5	stabilized	stabilize	VERB
eurjchem-591	69	6	by	by	ADP
eurjchem-591	69	7	weak	weak	ADJ
eurjchem-591	69	8	c‐h	c‐h	PROPN
eurjchem-591	69	9	…	…	SYM
eurjchem-591	69	10	s	s	NOUN
eurjchem-591	69	11	and	and	CCONJ
eurjchem-591	69	12	c‐	c‐	NOUN
eurjchem-591	69	13	h	h	NOUN
eurjchem-591	69	14	…	…	PUNCT
eurjchem-591	69	15	br	br	NOUN
eurjchem-591	69	16	hydrogen‐bonding	hydrogen‐bonde	VERB
eurjchem-591	69	17	interactions	interaction	NOUN
eurjchem-591	69	18	(	(	PUNCT
eurjchem-591	69	19	table	table	NOUN
eurjchem-591	69	20	4	4	NUM
eurjchem-591	69	21	)	)	PUNCT
eurjchem-591	69	22	.	.	PUNCT
eurjchem-591	70	1	table	table	NOUN
eurjchem-591	70	2	2	2	NUM
eurjchem-591	70	3	.	.	PUNCT
eurjchem-591	71	1	bond	bond	NOUN
eurjchem-591	71	2	lengths	length	NOUN
eurjchem-591	71	3	for	for	ADP
eurjchem-591	71	4	the	the	DET
eurjchem-591	71	5	title	title	NOUN
eurjchem-591	71	6	compound	compound	NOUN
eurjchem-591	71	7	.	.	PUNCT
eurjchem-591	72	1	atom	atom	NOUN
eurjchem-591	72	2	atom	atom	NOUN
eurjchem-591	72	3	length	length	NOUN
eurjchem-591	72	4	,	,	PUNCT
eurjchem-591	72	5	å	å	PROPN
eurjchem-591	72	6	ni1	ni1	PROPN
eurjchem-591	72	7	o1	o1	PROPN
eurjchem-591	72	8	1.852(3	1.852(3	NUM
eurjchem-591	72	9	)	)	PUNCT
eurjchem-591	72	10	ni1	ni1	PROPN
eurjchem-591	72	11	o2	o2	PROPN
eurjchem-591	72	12	1.854(3	1.854(3	NUM
eurjchem-591	72	13	)	)	PUNCT
eurjchem-591	72	14	ni1	ni1	PROPN
eurjchem-591	72	15	s1	s1	PROPN
eurjchem-591	72	16	2.1356(12	2.1356(12	NUM
eurjchem-591	72	17	)	)	PUNCT
eurjchem-591	73	1	ni1	ni1	NOUN
eurjchem-591	73	2	s2	s2	VERB
eurjchem-591	73	3	2.1405(12	2.1405(12	NUM
eurjchem-591	73	4	)	)	PUNCT
eurjchem-591	73	5	br2	br2	PROPN
eurjchem-591	73	6	c22	c22	PROPN
eurjchem-591	73	7	1.899(4	1.899(4	NUM
eurjchem-591	73	8	)	)	PUNCT
eurjchem-591	74	1	br11	br11	PROPN
eurjchem-591	74	2	c10	c10	VERB
eurjchem-591	74	3	1.980(6	1.980(6	PROPN
eurjchem-591	74	4	)	)	PUNCT
eurjchem-591	74	5	s1	s1	PROPN
eurjchem-591	74	6	c1	c1	PROPN
eurjchem-591	74	7	1.744(4	1.744(4	NUM
eurjchem-591	74	8	)	)	PUNCT
eurjchem-591	74	9	s2	s2	NOUN
eurjchem-591	74	10	c13	c13	X
eurjchem-591	74	11	1.745(4	1.745(4	NOUN
eurjchem-591	74	12	)	)	PUNCT
eurjchem-591	74	13	o1	o1	NOUN
eurjchem-591	74	14	c6	c6	NOUN
eurjchem-591	74	15	1.263(5	1.263(5	NUM
eurjchem-591	74	16	)	)	PUNCT
eurjchem-591	74	17	o2	o2	PROPN
eurjchem-591	74	18	c18	c18	NOUN
eurjchem-591	74	19	1.268(5	1.268(5	NUM
eurjchem-591	74	20	)	)	PUNCT
eurjchem-591	74	21	n1	n1	PROPN
eurjchem-591	74	22	c1	c1	PROPN
eurjchem-591	74	23	1.335(5	1.335(5	NUM
eurjchem-591	74	24	)	)	PUNCT
eurjchem-591	74	25	n1	n1	PROPN
eurjchem-591	74	26	c6	c6	PROPN
eurjchem-591	74	27	1.325(6	1.325(6	NUM
eurjchem-591	74	28	)	)	PUNCT
eurjchem-591	74	29	n2	n2	PROPN
eurjchem-591	74	30	c1	c1	PROPN
eurjchem-591	74	31	1.334(6	1.334(6	NUM
eurjchem-591	74	32	)	)	PUNCT
eurjchem-591	74	33	n2	n2	PROPN
eurjchem-591	74	34	c2	c2	PROPN
eurjchem-591	74	35	1.466(6	1.466(6	NUM
eurjchem-591	74	36	)	)	PUNCT
eurjchem-591	74	37	n2	n2	NOUN
eurjchem-591	74	38	c4	c4	NOUN
eurjchem-591	74	39	1.487(5	1.487(5	NUM
eurjchem-591	74	40	)	)	PUNCT
eurjchem-591	74	41	n3	n3	NOUN
eurjchem-591	74	42	c13	c13	PROPN
eurjchem-591	74	43	1.345(5	1.345(5	NUM
eurjchem-591	74	44	)	)	PUNCT
eurjchem-591	74	45	n3	n3	NOUN
eurjchem-591	74	46	c18	c18	NOUN
eurjchem-591	74	47	1.314(5	1.314(5	NUM
eurjchem-591	74	48	)	)	PUNCT
eurjchem-591	75	1	n4	n4	PROPN
eurjchem-591	75	2	c13	c13	PROPN
eurjchem-591	75	3	1.322(6	1.322(6	NUM
eurjchem-591	75	4	)	)	PUNCT
eurjchem-591	75	5	n4	n4	PROPN
eurjchem-591	75	6	c141	c141	PROPN
eurjchem-591	75	7	1.519(8	1.519(8	NUM
eurjchem-591	75	8	)	)	PUNCT
eurjchem-591	75	9	binzet	binzet	NOUN
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eurjchem-591	75	12	.	.	PUNCT
eurjchem-591	75	13	/	/	SYM
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eurjchem-591	75	18	3	3	NUM
eurjchem-591	75	19	(	(	PUNCT
eurjchem-591	75	20	1	1	NUM
eurjchem-591	75	21	)	)	PUNCT
eurjchem-591	75	22	(	(	PUNCT
eurjchem-591	75	23	2012	2012	NUM
eurjchem-591	75	24	)	)	PUNCT
eurjchem-591	75	25	37‐39	37‐39	NOUN
eurjchem-591	75	26	39	39	NUM
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eurjchem-591	75	28	3	3	NUM
eurjchem-591	75	29	.	.	PUNCT
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eurjchem-591	76	2	angles	angle	NOUN
eurjchem-591	76	3	for	for	ADP
eurjchem-591	76	4	the	the	DET
eurjchem-591	76	5	title	title	NOUN
eurjchem-591	76	6	compound	compound	NOUN
eurjchem-591	76	7	.	.	PUNCT
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eurjchem-591	77	2	atom	atom	NOUN
eurjchem-591	77	3	atom	atom	NOUN
eurjchem-591	77	4	angle	angle	NOUN
eurjchem-591	77	5	,	,	PUNCT
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eurjchem-591	77	7	o1	o1	PROPN
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eurjchem-591	77	9	o2	o2	PROPN
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eurjchem-591	77	11	)	)	PUNCT
eurjchem-591	77	12	o2	o2	PROPN
eurjchem-591	77	13	ni1	ni1	PROPN
eurjchem-591	77	14	s2	s2	PROPN
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eurjchem-591	77	16	)	)	PUNCT
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eurjchem-591	77	18	ni1	ni1	PROPN
eurjchem-591	77	19	s2	s2	PROPN
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eurjchem-591	77	21	)	)	PUNCT
eurjchem-591	77	22	o2	o2	PROPN
eurjchem-591	77	23	ni1	ni1	PROPN
eurjchem-591	77	24	s1	s1	PROPN
eurjchem-591	77	25	178.89(10	178.89(10	NUM
eurjchem-591	77	26	)	)	PUNCT
eurjchem-591	77	27	o1	o1	NOUN
eurjchem-591	77	28	ni1	ni1	PROPN
eurjchem-591	77	29	s1	s1	PROPN
eurjchem-591	77	30	94.90(10	94.90(10	NUM
eurjchem-591	77	31	)	)	PUNCT
eurjchem-591	77	32	s1	s1	PROPN
eurjchem-591	77	33	ni1	ni1	PROPN
eurjchem-591	77	34	s2	s2	PROPN
eurjchem-591	77	35	87.66(4	87.66(4	NUM
eurjchem-591	77	36	)	)	PUNCT
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eurjchem-591	77	38	s1	s1	PROPN
eurjchem-591	77	39	ni1	ni1	PROPN
eurjchem-591	77	40	107.99(16	107.99(16	NUM
eurjchem-591	77	41	)	)	PUNCT
eurjchem-591	77	42	c13	c13	PROPN
eurjchem-591	77	43	s2	s2	PROPN
eurjchem-591	77	44	ni1	ni1	PROPN
eurjchem-591	77	45	105.87(17	105.87(17	NUM
eurjchem-591	77	46	)	)	PUNCT
eurjchem-591	77	47	c6	c6	PROPN
eurjchem-591	77	48	o1	o1	PROPN
eurjchem-591	77	49	ni1	ni1	PROPN
eurjchem-591	77	50	133.4(3	133.4(3	NUM
eurjchem-591	77	51	)	)	PUNCT
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eurjchem-591	77	53	o2	o2	PROPN
eurjchem-591	77	54	ni1	ni1	PROPN
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eurjchem-591	77	56	)	)	PUNCT
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eurjchem-591	77	59	c1	c1	PROPN
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eurjchem-591	77	61	)	)	PUNCT
eurjchem-591	77	62	c1	c1	PROPN
eurjchem-591	77	63	n2	n2	PROPN
eurjchem-591	77	64	c2	c2	PROPN
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eurjchem-591	77	66	)	)	PUNCT
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eurjchem-591	77	68	n2	n2	PROPN
eurjchem-591	77	69	c4	c4	PROPN
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eurjchem-591	77	71	)	)	PUNCT
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eurjchem-591	77	73	n2	n2	PROPN
eurjchem-591	77	74	c4	c4	PROPN
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eurjchem-591	77	76	)	)	PUNCT
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eurjchem-591	77	79	c1	c1	PROPN
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eurjchem-591	77	81	)	)	PUNCT
eurjchem-591	77	82	c1	c1	PROPN
eurjchem-591	77	83	n2	n2	PROPN
eurjchem-591	77	84	c2	c2	PROPN
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eurjchem-591	77	86	)	)	PUNCT
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eurjchem-591	77	89	c4	c4	PROPN
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eurjchem-591	77	91	)	)	PUNCT
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eurjchem-591	77	93	n2	n2	PROPN
eurjchem-591	77	94	c4	c4	PROPN
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eurjchem-591	77	96	)	)	PUNCT
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eurjchem-591	77	99	n1	n1	PROPN
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eurjchem-591	77	101	)	)	PUNCT
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eurjchem-591	77	104	s1	s1	PROPN
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eurjchem-591	77	106	)	)	PUNCT
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eurjchem-591	77	111	)	)	PUNCT
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eurjchem-591	77	114	n1	n1	PROPN
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eurjchem-591	77	116	)	)	PUNCT
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eurjchem-591	77	118	c6	c6	PROPN
eurjchem-591	77	119	c7	c7	PROPN
eurjchem-591	77	120	114.8(5	114.8(5	X
eurjchem-591	77	121	)	)	PUNCT
eurjchem-591	77	122	n1	n1	PROPN
eurjchem-591	77	123	c6	c6	PROPN
eurjchem-591	77	124	c7	c7	PROPN
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eurjchem-591	77	126	)	)	PUNCT
eurjchem-591	77	127	n4	n4	PROPN
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eurjchem-591	77	129	n3	n3	PROPN
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eurjchem-591	77	131	)	)	PUNCT
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eurjchem-591	77	133	c13	c13	PROPN
eurjchem-591	77	134	s2	s2	PROPN
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eurjchem-591	77	136	)	)	PUNCT
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eurjchem-591	77	138	c13	c13	PROPN
eurjchem-591	77	139	s2	s2	PROPN
eurjchem-591	77	140	127.8(4	127.8(4	X
eurjchem-591	77	141	)	)	PUNCT
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eurjchem-591	77	146	)	)	PUNCT
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eurjchem-591	77	149	c18	c18	PROPN
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eurjchem-591	77	151	)	)	PUNCT
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eurjchem-591	77	154	c18	c18	NOUN
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eurjchem-591	77	156	)	)	PUNCT
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eurjchem-591	77	158	4	4	NUM
eurjchem-591	77	159	.	.	PUNCT
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eurjchem-591	78	5	title	title	NOUN
eurjchem-591	78	6	compound	compound	NOUN
eurjchem-591	78	7	.	.	PUNCT
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eurjchem-591	79	5	)	)	PUNCT
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eurjchem-591	79	9	)	)	PUNCT
eurjchem-591	79	10	,	,	PUNCT
eurjchem-591	79	11	å	å	PROPN
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eurjchem-591	79	13	)	)	PUNCT
eurjchem-591	79	14	,	,	PUNCT
eurjchem-591	79	15	å	å	PROPN
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eurjchem-591	79	17	,	,	PUNCT
eurjchem-591	79	18	o	o	PROPN
eurjchem-591	79	19	c(2	c(2	PROPN
eurjchem-591	79	20	)	)	PUNCT
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eurjchem-591	79	22	)	)	PUNCT
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eurjchem-591	79	24	)	)	PUNCT
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eurjchem-591	79	26	2.56	2.56	NUM
eurjchem-591	79	27	2.965(5	2.965(5	NUM
eurjchem-591	79	28	)	)	PUNCT
eurjchem-591	79	29	105	105	NUM
eurjchem-591	79	30	c(16	c(16	NOUN
eurjchem-591	79	31	)	)	PUNCT
eurjchem-591	79	32	h(16a	h(16a	NOUN
eurjchem-591	79	33	)	)	PUNCT
eurjchem-591	79	34	s(2	s(2	PROPN
eurjchem-591	79	35	)	)	PUNCT
eurjchem-591	79	36	0.99	0.99	NUM
eurjchem-591	79	37	2.53	2.53	NUM
eurjchem-591	79	38	2.951(6	2.951(6	NUM
eurjchem-591	79	39	)	)	PUNCT
eurjchem-591	79	40	106	106	NUM
eurjchem-591	79	41	c(3	c(3	PROPN
eurjchem-591	79	42	)	)	PUNCT
eurjchem-591	79	43	h(3a	h(3a	NOUN
eurjchem-591	79	44	)	)	PUNCT
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eurjchem-591	79	47	2.87	2.87	NUM
eurjchem-591	79	48	3.633(6	3.633(6	NUM
eurjchem-591	79	49	)	)	PUNCT
eurjchem-591	79	50	135	135	NUM
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eurjchem-591	79	52	code	code	NOUN
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eurjchem-591	79	54	i	i	PRON
eurjchem-591	79	55	:	:	PUNCT
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eurjchem-591	79	57	,	,	PUNCT
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eurjchem-591	79	59	,	,	PUNCT
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eurjchem-591	79	62	4	4	NUM
eurjchem-591	79	63	.	.	X
eurjchem-591	79	64	conclusion	conclusion	NOUN
eurjchem-591	79	65	in	in	ADP
eurjchem-591	79	66	this	this	DET
eurjchem-591	79	67	work	work	NOUN
eurjchem-591	79	68	,	,	PUNCT
eurjchem-591	79	69	bis(4‐bromo‐n‐(diethylcarbamothioyl	bis(4‐bromo‐n‐(diethylcarbamothioyl	PROPN
eurjchem-591	79	70	)	)	PUNCT
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eurjchem-591	80	2	(	(	PUNCT
eurjchem-591	80	3	ii	ii	NOUN
eurjchem-591	80	4	)	)	PUNCT
eurjchem-591	80	5	complex	complex	NOUN
eurjchem-591	80	6	has	have	AUX
eurjchem-591	80	7	been	be	AUX
eurjchem-591	80	8	synthesized	synthesize	VERB
eurjchem-591	80	9	according	accord	VERB
eurjchem-591	80	10	to	to	ADP
eurjchem-591	80	11	the	the	DET
eurjchem-591	80	12	previous	previous	ADJ
eurjchem-591	80	13	reports	report	NOUN
eurjchem-591	80	14	.	.	PUNCT
eurjchem-591	81	1	the	the	DET
eurjchem-591	81	2	crystal	crystal	NOUN
eurjchem-591	81	3	of	of	ADP
eurjchem-591	81	4	nickel(ii	nickel(ii	ADJ
eurjchem-591	81	5	)	)	PUNCT
eurjchem-591	81	6	complex	complex	NOUN
eurjchem-591	81	7	is	be	AUX
eurjchem-591	81	8	suitable	suitable	ADJ
eurjchem-591	81	9	for	for	ADP
eurjchem-591	81	10	x‐ray	x‐ray	PROPN
eurjchem-591	81	11	single	single	ADJ
eurjchem-591	81	12	crystal	crystal	PROPN
eurjchem-591	81	13	diffraction	diffraction	NOUN
eurjchem-591	81	14	analysis	analysis	NOUN
eurjchem-591	81	15	.	.	PUNCT
eurjchem-591	82	1	in	in	ADP
eurjchem-591	82	2	this	this	DET
eurjchem-591	82	3	nickel	nickel	NOUN
eurjchem-591	82	4	complex	complex	NOUN
eurjchem-591	82	5	,	,	PUNCT
eurjchem-591	82	6	the	the	DET
eurjchem-591	82	7	nickel	nickel	NOUN
eurjchem-591	82	8	atom	atom	NOUN
eurjchem-591	82	9	is	be	AUX
eurjchem-591	82	10	coordinated	coordinate	VERB
eurjchem-591	82	11	by	by	ADP
eurjchem-591	82	12	two	two	NUM
eurjchem-591	82	13	s	s	NOUN
eurjchem-591	82	14	atoms	atom	NOUN
eurjchem-591	82	15	and	and	CCONJ
eurjchem-591	82	16	two	two	NUM
eurjchem-591	82	17	o	o	NOUN
eurjchem-591	82	18	atoms	atom	NOUN
eurjchem-591	82	19	from	from	ADP
eurjchem-591	82	20	two	two	NUM
eurjchem-591	82	21	4‐bromo‐n‐(diethylcarbamothioyl	4‐bromo‐n‐(diethylcarbamothioyl	NUM
eurjchem-591	82	22	)	)	PUNCT
eurjchem-591	82	23	benzamide	benzamide	VERB
eurjchem-591	82	24	molecules	molecule	NOUN
eurjchem-591	82	25	.	.	PUNCT
eurjchem-591	83	1	acknowledgements	acknowledgement	NOUN
eurjchem-591	83	2	this	this	DET
eurjchem-591	83	3	work	work	NOUN
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eurjchem-591	83	6	by	by	ADP
eurjchem-591	83	7	mersin	mersin	PROPN
eurjchem-591	83	8	university	university	PROPN
eurjchem-591	83	9	research	research	NOUN
eurjchem-591	83	10	fund	fund	NOUN
eurjchem-591	83	11	(	(	PUNCT
eurjchem-591	83	12	project	project	NOUN
eurjchem-591	83	13	no	no	PRON
eurjchem-591	83	14	:	:	PUNCT
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eurjchem-591	83	16	)	)	PUNCT
eurjchem-591	83	17	.	.	PUNCT
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eurjchem-591	84	2	material	material	PROPN
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eurjchem-591	84	5	the	the	DET
eurjchem-591	84	6	supplementary	supplementary	ADJ
eurjchem-591	84	7	crystallographic	crystallographic	ADJ
eurjchem-591	84	8	data	datum	NOUN
eurjchem-591	84	9	for	for	ADP
eurjchem-591	84	10	this	this	DET
eurjchem-591	84	11	paper	paper	NOUN
eurjchem-591	84	12	.	.	PUNCT
eurjchem-591	85	1	these	these	DET
eurjchem-591	85	2	data	datum	NOUN
eurjchem-591	85	3	can	can	AUX
eurjchem-591	85	4	be	be	AUX
eurjchem-591	85	5	obtained	obtain	VERB
eurjchem-591	85	6	free	free	ADJ
eurjchem-591	85	7	of	of	ADP
eurjchem-591	85	8	charge	charge	NOUN
eurjchem-591	85	9	via	via	ADP
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eurjchem-591	85	16	,	,	PUNCT
eurjchem-591	85	17	or	or	CCONJ
eurjchem-591	85	18	by	by	ADP
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eurjchem-591	85	20	the	the	DET
eurjchem-591	85	21	cambridge	cambridge	PROPN
eurjchem-591	85	22	crystallographic	crystallographic	PROPN
eurjchem-591	85	23	data	data	PROPN
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eurjchem-591	85	25	,	,	PUNCT
eurjchem-591	85	26	12	12	NUM
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eurjchem-591	85	29	,	,	PUNCT
eurjchem-591	85	30	cambridge	cambridge	PROPN
eurjchem-591	85	31	cb2	cb2	PROPN
eurjchem-591	85	32	1ez	1ez	PROPN
eurjchem-591	85	33	,	,	PUNCT
eurjchem-591	85	34	uk	uk	PROPN
eurjchem-591	85	35	;	;	PUNCT
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eurjchem-591	85	37	:	:	PUNCT
eurjchem-591	85	38	+44(0)1223‐336033	+44(0)1223‐336033	ADJ
eurjchem-591	85	39	.	.	PUNCT
eurjchem-591	85	40	references	reference	NOUN
eurjchem-591	85	41	[	[	X
eurjchem-591	85	42	1	1	NUM
eurjchem-591	85	43	]	]	PUNCT
eurjchem-591	85	44	.	.	PUNCT
eurjchem-591	86	1	sacht	sacht	PROPN
eurjchem-591	86	2	,	,	PUNCT
eurjchem-591	86	3	c.	c.	PROPN
eurjchem-591	86	4	;	;	PUNCT
eurjchem-591	86	5	datt	datt	PROPN
eurjchem-591	86	6	,	,	PUNCT
eurjchem-591	86	7	m.	m.	PROPN
eurjchem-591	86	8	s.	s.	PROPN
eurjchem-591	86	9	;	;	PUNCT
eurjchem-591	86	10	otto	otto	PROPN
eurjchem-591	86	11	,	,	PUNCT
eurjchem-591	86	12	s.	s.	PROPN
eurjchem-591	86	13	;	;	PUNCT
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eurjchem-591	87	4	.	.	PUNCT
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eurjchem-591	88	2	.	.	PUNCT
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eurjchem-591	90	2	,	,	PUNCT
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eurjchem-591	90	4	,	,	PUNCT
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eurjchem-591	90	6	.	.	PUNCT
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eurjchem-591	91	3	]	]	PUNCT
eurjchem-591	91	4	.	.	PUNCT
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eurjchem-591	92	2	,	,	PUNCT
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eurjchem-591	92	6	,	,	PUNCT
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eurjchem-591	92	14	,	,	PUNCT
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eurjchem-591	92	18	,	,	PUNCT
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eurjchem-591	92	25	.	.	PUNCT
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eurjchem-591	93	2	.	.	PROPN
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eurjchem-591	93	4	.	.	PUNCT
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eurjchem-591	94	2	.	.	PUNCT
eurjchem-591	95	1	2006	2006	NUM
eurjchem-591	95	2	,	,	PUNCT
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eurjchem-591	95	4	,	,	PUNCT
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eurjchem-591	95	6	.	.	PUNCT
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eurjchem-591	96	3	]	]	PUNCT
eurjchem-591	96	4	.	.	PUNCT
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eurjchem-591	97	2	,	,	PUNCT
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eurjchem-591	97	4	;	;	PUNCT
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eurjchem-591	97	6	,	,	PUNCT
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eurjchem-591	97	8	;	;	PUNCT
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eurjchem-591	97	10	,	,	PUNCT
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eurjchem-591	97	12	;	;	PUNCT
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eurjchem-591	97	14	,	,	PUNCT
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eurjchem-591	97	17	.	.	PUNCT
eurjchem-591	98	1	j.	j.	PROPN
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eurjchem-591	98	3	.	.	PUNCT
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eurjchem-591	99	2	,	,	PUNCT
eurjchem-591	99	3	1(3	1(3	NUM
eurjchem-591	99	4	)	)	PUNCT
eurjchem-591	99	5	,	,	PUNCT
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eurjchem-591	99	7	205	205	NUM
eurjchem-591	99	8	.	.	PUNCT
eurjchem-591	100	1	[	[	X
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eurjchem-591	100	3	]	]	PUNCT
eurjchem-591	100	4	.	.	PUNCT
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eurjchem-591	101	2	,	,	PUNCT
eurjchem-591	101	3	s.	s.	PROPN
eurjchem-591	101	4	;	;	PUNCT
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eurjchem-591	101	6	,	,	PUNCT
eurjchem-591	101	7	n.	n.	PROPN
eurjchem-591	101	8	;	;	PUNCT
eurjchem-591	101	9	ali	ali	PROPN
eurjchem-591	101	10	,	,	PUNCT
eurjchem-591	101	11	m.	m.	NOUN
eurjchem-591	101	12	;	;	PUNCT
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eurjchem-591	101	14	,	,	PUNCT
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eurjchem-591	101	16	;	;	PUNCT
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eurjchem-591	101	18	,	,	PUNCT
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eurjchem-591	101	20	g.	g.	PROPN
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eurjchem-591	101	22	.	.	PUNCT
eurjchem-591	102	1	j.	j.	PROPN
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eurjchem-591	102	3	.	.	PUNCT
eurjchem-591	103	1	2010	2010	NUM
eurjchem-591	103	2	,	,	PUNCT
eurjchem-591	103	3	1(3	1(3	NUM
eurjchem-591	103	4	)	)	PUNCT
eurjchem-591	103	5	,	,	PUNCT
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eurjchem-591	103	7	.	.	PUNCT
eurjchem-591	104	1	[	[	X
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eurjchem-591	104	3	]	]	PUNCT
eurjchem-591	104	4	.	.	PUNCT
eurjchem-591	105	1	chow	chow	PROPN
eurjchem-591	105	2	,	,	PUNCT
eurjchem-591	105	3	a.	a.	PROPN
eurjchem-591	105	4	w.	w.	PROPN
eurjchem-591	105	5	u.	u.	PROPN
eurjchem-591	105	6	s.	s.	PROPN
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eurjchem-591	106	1	no	no	PROPN
eurjchem-591	106	2	.	.	PROPN
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eurjchem-591	106	4	.	.	PUNCT
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eurjchem-591	107	2	,	,	PUNCT
eurjchem-591	107	3	d.	d.	PROPN
eurjchem-591	107	4	c.	c.	PROPN
eurjchem-591	107	5	,	,	PUNCT
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eurjchem-591	107	8	u.	u.	PROPN
eurjchem-591	107	9	s.	s.	PROPN
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eurjchem-591	107	14	,	,	PUNCT
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eurjchem-591	107	16	.	.	PUNCT
eurjchem-591	108	1	[	[	X
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eurjchem-591	108	3	]	]	PUNCT
eurjchem-591	108	4	.	.	PUNCT
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eurjchem-591	109	2	,	,	PUNCT
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eurjchem-591	109	4	;	;	PUNCT
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eurjchem-591	109	6	,	,	PUNCT
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eurjchem-591	109	8	;	;	PUNCT
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eurjchem-591	109	10	,	,	PUNCT
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eurjchem-591	109	12	cs	cs	PROPN
eurjchem-591	109	13	patent	patent	PROPN
eurjchem-591	109	14	no	no	PROPN
eurjchem-591	109	15	.	.	PROPN
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eurjchem-591	109	17	.	.	PUNCT
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eurjchem-591	110	2	,	,	PUNCT
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eurjchem-591	110	11	,	,	PUNCT
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eurjchem-591	110	13	.	.	PUNCT
eurjchem-591	111	1	[	[	X
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eurjchem-591	111	3	]	]	PUNCT
eurjchem-591	111	4	.	.	PUNCT
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eurjchem-591	112	2	,	,	PUNCT
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eurjchem-591	112	5	;	;	PUNCT
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eurjchem-591	112	7	,	,	PUNCT
eurjchem-591	112	8	s.	s.	PROPN
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eurjchem-591	112	12	,	,	PUNCT
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eurjchem-591	112	14	,	,	PUNCT
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eurjchem-591	112	16	.	.	PUNCT
eurjchem-591	113	1	[	[	X
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eurjchem-591	113	3	]	]	PUNCT
eurjchem-591	113	4	.	.	PUNCT
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eurjchem-591	114	2	,	,	PUNCT
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eurjchem-591	114	4	;	;	PUNCT
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eurjchem-591	114	6	,	,	PUNCT
eurjchem-591	114	7	g.	g.	PROPN
eurjchem-591	114	8	;	;	PUNCT
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eurjchem-591	114	10	,	,	PUNCT
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eurjchem-591	114	12	;	;	PUNCT
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eurjchem-591	114	14	,	,	PUNCT
eurjchem-591	114	15	s.	s.	PROPN
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eurjchem-591	114	17	.	.	PUNCT
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eurjchem-591	115	2	.	.	PROPN
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eurjchem-591	115	4	,	,	PUNCT
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eurjchem-591	115	6	,	,	PUNCT
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eurjchem-591	115	8	.	.	PUNCT
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eurjchem-591	116	4	.	.	PUNCT
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eurjchem-591	117	2	,	,	PUNCT
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eurjchem-591	117	6	;	;	PUNCT
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eurjchem-591	117	9	,	,	PUNCT
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eurjchem-591	117	12	;	;	PUNCT
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eurjchem-591	117	14	,	,	PUNCT
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eurjchem-591	117	18	.	.	PUNCT
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eurjchem-591	118	2	.	.	PUNCT
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eurjchem-591	119	2	,	,	PUNCT
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eurjchem-591	119	4	,	,	PUNCT
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eurjchem-591	119	6	.	.	PUNCT
eurjchem-591	120	1	[	[	X
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eurjchem-591	120	3	]	]	PUNCT
eurjchem-591	120	4	.	.	PUNCT
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eurjchem-591	121	2	,	,	PUNCT
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eurjchem-591	121	5	;	;	PUNCT
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eurjchem-591	121	7	,	,	PUNCT
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eurjchem-591	121	11	.	.	PUNCT
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eurjchem-591	122	2	.	.	PUNCT
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eurjchem-591	123	2	.	.	PROPN
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eurjchem-591	123	4	,	,	PUNCT
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eurjchem-591	123	6	,	,	PUNCT
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eurjchem-591	123	8	.	.	PUNCT
eurjchem-591	124	1	[	[	X
eurjchem-591	124	2	11	11	NUM
eurjchem-591	124	3	]	]	PUNCT
eurjchem-591	124	4	.	.	PUNCT
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eurjchem-591	125	2	,	,	PUNCT
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eurjchem-591	125	7	,	,	PUNCT
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eurjchem-591	125	11	.	.	PUNCT
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eurjchem-591	126	2	.	.	PUNCT
eurjchem-591	127	1	1996	1996	NUM
eurjchem-591	127	2	,	,	PUNCT
eurjchem-591	127	3	35	35	NUM
eurjchem-591	127	4	,	,	PUNCT
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eurjchem-591	127	6	.	.	PUNCT
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eurjchem-591	128	3	]	]	PUNCT
eurjchem-591	128	4	.	.	PUNCT
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eurjchem-591	129	2	,	,	PUNCT
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eurjchem-591	129	4	;	;	PUNCT
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eurjchem-591	129	14	,	,	PUNCT
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eurjchem-591	129	22	.	.	PUNCT
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eurjchem-591	131	2	,	,	PUNCT
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eurjchem-591	131	4	,	,	PUNCT
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eurjchem-591	131	6	.	.	PUNCT
eurjchem-591	132	1	[	[	X
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eurjchem-591	132	3	]	]	SYM
eurjchem-591	132	4	.	.	PUNCT
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eurjchem-591	132	6	,	,	PUNCT
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eurjchem-591	132	9	;	;	PUNCT
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eurjchem-591	132	11	,	,	PUNCT
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eurjchem-591	132	13	;	;	PUNCT
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eurjchem-591	132	25	.	.	PUNCT
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eurjchem-591	133	2	.	.	PUNCT
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eurjchem-591	134	2	,	,	PUNCT
eurjchem-591	134	3	184(12	184(12	NUM
eurjchem-591	134	4	)	)	PUNCT
eurjchem-591	134	5	,	,	PUNCT
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eurjchem-591	134	7	.	.	PUNCT
eurjchem-591	135	1	[	[	X
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eurjchem-591	135	3	]	]	PUNCT
eurjchem-591	135	4	.	.	PUNCT
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eurjchem-591	136	2	,	,	PUNCT
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eurjchem-591	136	4	;	;	PUNCT
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eurjchem-591	136	6	,	,	PUNCT
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eurjchem-591	136	8	;	;	PUNCT
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eurjchem-591	137	2	.	.	PUNCT
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eurjchem-591	138	2	,	,	PUNCT
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eurjchem-591	138	4	,	,	PUNCT
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eurjchem-591	138	6	.	.	PUNCT
eurjchem-591	139	1	[	[	X
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eurjchem-591	139	4	.	.	PUNCT
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eurjchem-591	141	2	.	.	PUNCT
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eurjchem-591	142	2	,	,	PUNCT
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eurjchem-591	142	4	,	,	PUNCT
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eurjchem-591	143	3	]	]	PUNCT
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eurjchem-591	143	6	,	,	PUNCT
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eurjchem-591	144	2	.	.	PUNCT
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eurjchem-591	145	2	,	,	PUNCT
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eurjchem-591	146	3	]	]	SYM
eurjchem-591	146	4	.	.	PUNCT
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eurjchem-591	147	4	;	;	PUNCT
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eurjchem-591	147	6	,	,	PUNCT
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eurjchem-591	149	2	.	.	PUNCT
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eurjchem-591	150	2	,	,	PUNCT
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eurjchem-591	150	4	,	,	PUNCT
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eurjchem-591	151	3	]	]	PUNCT
eurjchem-591	151	4	.	.	PUNCT
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eurjchem-591	152	2	,	,	PUNCT
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eurjchem-591	152	6	,	,	PUNCT
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eurjchem-591	153	3	.	.	PUNCT
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eurjchem-591	154	2	,	,	PUNCT
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eurjchem-591	154	4	,	,	PUNCT
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eurjchem-591	155	3	]	]	PUNCT
eurjchem-591	155	4	.	.	PUNCT
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eurjchem-591	156	2	,	,	PUNCT
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eurjchem-591	156	6	,	,	PUNCT
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eurjchem-591	157	2	.	.	PUNCT
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eurjchem-591	158	2	,	,	PUNCT
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eurjchem-591	158	4	,	,	PUNCT
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eurjchem-591	159	3	]	]	PUNCT
eurjchem-591	159	4	.	.	PUNCT
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eurjchem-591	160	2	,	,	PUNCT
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eurjchem-591	160	6	,	,	PUNCT
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eurjchem-591	160	13	.	.	PUNCT
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eurjchem-591	162	2	,	,	PUNCT
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eurjchem-591	162	4	,	,	PUNCT
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eurjchem-591	163	6	,	,	PUNCT
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eurjchem-591	163	10	,	,	PUNCT
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eurjchem-591	164	2	.	.	PUNCT
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eurjchem-591	165	2	,	,	PUNCT
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eurjchem-591	165	4	,	,	PUNCT
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eurjchem-591	166	6	,	,	PUNCT
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eurjchem-591	166	10	,	,	PUNCT
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eurjchem-591	166	14	,	,	PUNCT
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eurjchem-591	168	6	,	,	PUNCT
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eurjchem-591	177	2	,	,	PUNCT
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eurjchem-591	180	3	,	,	PUNCT
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eurjchem-591	190	24	)	)	PUNCT
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eurjchem-591	192	3	,	,	PUNCT
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eurjchem-591	196	4	)	)	PUNCT
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eurjchem-591	200	2	,	,	PUNCT
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