id	sid	tid	token	lemma	pos
eurjchem-610	1	1	untitled	untitle	VERB
eurjchem-610	1	2	european	european	PROPN
eurjchem-610	1	3	journal	journal	PROPN
eurjchem-610	1	4	of	of	ADP
eurjchem-610	1	5	chemistry	chemistry	NOUN
eurjchem-610	1	6	3	3	NUM
eurjchem-610	1	7	(	(	PUNCT
eurjchem-610	1	8	3	3	NUM
eurjchem-610	1	9	)	)	PUNCT
eurjchem-610	1	10	(	(	PUNCT
eurjchem-610	1	11	2012	2012	NUM
eurjchem-610	1	12	)	)	PUNCT
eurjchem-610	1	13	305‐309	305‐309	PROPN
eurjchem-610	1	14	european	european	PROPN
eurjchem-610	1	15	journal	journal	PROPN
eurjchem-610	1	16	of	of	ADP
eurjchem-610	1	17	chemistry	chemistry	NOUN
eurjchem-610	1	18	issn	issn	PROPN
eurjchem-610	1	19	2153‐2249	2153‐2249	PROPN
eurjchem-610	1	20	(	(	PUNCT
eurjchem-610	1	21	print	print	NOUN
eurjchem-610	1	22	)	)	PUNCT
eurjchem-610	1	23	/	/	SYM
eurjchem-610	1	24	issn	issn	PROPN
eurjchem-610	1	25	2153‐2257	2153‐2257	NUM
eurjchem-610	1	26	(	(	PUNCT
eurjchem-610	1	27	online	online	ADJ
eurjchem-610	1	28	)	)	PUNCT
eurjchem-610	1	29			NOUN
eurjchem-610	1	30	2012	2012	NUM
eurjchem-610	1	31	eurjchem	eurjchem	PROPN
eurjchem-610	1	32	doi:10.5155	doi:10.5155	ADJ
eurjchem-610	1	33	/	/	SYM
eurjchem-610	1	34	eurjchem.3.3.305‐309.610	eurjchem.3.3.305‐309.610	ADJ
eurjchem-610	1	35	european	european	ADJ
eurjchem-610	1	36	journal	journal	NOUN
eurjchem-610	1	37	of	of	ADP
eurjchem-610	1	38	chemistry	chemistry	PROPN
eurjchem-610	1	39	journal	journal	PROPN
eurjchem-610	1	40	homepage	homepage	NOUN
eurjchem-610	1	41	:	:	PUNCT
eurjchem-610	1	42	www.eurjchem.com	www.eurjchem.com	X
eurjchem-610	1	43	efficient	efficient	ADJ
eurjchem-610	1	44	deprotection	deprotection	NOUN
eurjchem-610	1	45	of	of	ADP
eurjchem-610	1	46	boc	boc	NOUN
eurjchem-610	1	47	group	group	NOUN
eurjchem-610	1	48	in	in	ADP
eurjchem-610	1	49	amines	amine	NOUN
eurjchem-610	1	50	and	and	CCONJ
eurjchem-610	1	51	sulfamides	sulfamide	NOUN
eurjchem-610	1	52	using	use	VERB
eurjchem-610	1	53	dawson	dawson	PROPN
eurjchem-610	1	54	heteropolyacid	heteropolyacid	PROPN
eurjchem-610	1	55	catalyst	catalyst	NOUN
eurjchem-610	1	56	roubila	roubila	PROPN
eurjchem-610	1	57	belghiche	belghiche	PROPN
eurjchem-610	1	58	,	,	PUNCT
eurjchem-610	1	59	zinelaabidine	zinelaabidine	PROPN
eurjchem-610	1	60	cheraiet	cheraiet	PROPN
eurjchem-610	1	61	,	,	PUNCT
eurjchem-610	1	62	malika	malika	PROPN
eurjchem-610	1	63	berredjem	berredjem	PROPN
eurjchem-610	1	64	,	,	PUNCT
eurjchem-610	1	65	mostefa	mostefa	NOUN
eurjchem-610	1	66	abbessi	abbessi	NOUN
eurjchem-610	1	67	and	and	CCONJ
eurjchem-610	1	68	nour‐eddine	nour‐eddine	ADJ
eurjchem-610	1	69	aouf	aouf	PROPN
eurjchem-610	1	70	*	*	PUNCT
eurjchem-610	1	71	laboratory	laboratory	NOUN
eurjchem-610	1	72	of	of	ADP
eurjchem-610	1	73	applied	apply	VERB
eurjchem-610	1	74	organic	organic	ADJ
eurjchem-610	1	75	chemistry	chemistry	NOUN
eurjchem-610	1	76	,	,	PUNCT
eurjchem-610	1	77	bioorganic	bioorganic	ADJ
eurjchem-610	1	78	chemistry	chemistry	NOUN
eurjchem-610	1	79	group	group	NOUN
eurjchem-610	1	80	,	,	PUNCT
eurjchem-610	1	81	sciences	sciences	PROPN
eurjchem-610	1	82	faculty	faculty	NOUN
eurjchem-610	1	83	,	,	PUNCT
eurjchem-610	1	84	chemistry	chemistry	NOUN
eurjchem-610	1	85	department	department	NOUN
eurjchem-610	1	86	,	,	PUNCT
eurjchem-610	1	87	badji	badji	PROPN
eurjchem-610	1	88	mokhtar	mokhtar	PROPN
eurjchem-610	1	89	annaba	annaba	PROPN
eurjchem-610	1	90	university	university	PROPN
eurjchem-610	1	91	,	,	PUNCT
eurjchem-610	1	92	23000	23000	NUM
eurjchem-610	1	93	,	,	PUNCT
eurjchem-610	1	94	algeria	algeria	PROPN
eurjchem-610	1	95	*	*	PUNCT
eurjchem-610	1	96	corresponding	correspond	VERB
eurjchem-610	1	97	author	author	NOUN
eurjchem-610	1	98	at	at	ADP
eurjchem-610	1	99	:	:	PUNCT
eurjchem-610	1	100	laboratory	laboratory	NOUN
eurjchem-610	1	101	of	of	ADP
eurjchem-610	1	102	applied	apply	VERB
eurjchem-610	1	103	organic	organic	ADJ
eurjchem-610	1	104	chemistry	chemistry	NOUN
eurjchem-610	1	105	,	,	PUNCT
eurjchem-610	1	106	bioorganic	bioorganic	ADJ
eurjchem-610	1	107	chemistry	chemistry	NOUN
eurjchem-610	1	108	group	group	NOUN
eurjchem-610	1	109	,	,	PUNCT
eurjchem-610	1	110	sciences	sciences	PROPN
eurjchem-610	1	111	faculty	faculty	NOUN
eurjchem-610	1	112	,	,	PUNCT
eurjchem-610	1	113	chemistry	chemistry	NOUN
eurjchem-610	1	114	department	department	NOUN
eurjchem-610	1	115	,	,	PUNCT
eurjchem-610	1	116	badji	badji	PROPN
eurjchem-610	1	117	mokhtar	mokhtar	PROPN
eurjchem-610	1	118	annaba	annaba	PROPN
eurjchem-610	1	119	university	university	PROPN
eurjchem-610	1	120	,	,	PUNCT
eurjchem-610	1	121	23000	23000	NUM
eurjchem-610	1	122	,	,	PUNCT
eurjchem-610	1	123	algeria	algeria	PROPN
eurjchem-610	1	124	.	.	PUNCT
eurjchem-610	2	1	tel	tel	PROPN
eurjchem-610	2	2	.	.	PUNCT
eurjchem-610	2	3	:	:	PUNCT
eurjchem-610	3	1	+213.38872789	+213.38872789	ADV
eurjchem-610	3	2	;	;	PUNCT
eurjchem-610	3	3	fax	fax	NOUN
eurjchem-610	3	4	:	:	PUNCT
eurjchem-610	3	5	+213.38872789	+213.38872789	PROPN
eurjchem-610	3	6	.	.	PUNCT
eurjchem-610	3	7	e‐mail	e‐mail	PUNCT
eurjchem-610	3	8	address	address	NOUN
eurjchem-610	3	9	:	:	PUNCT
eurjchem-610	3	10	noureddineaouf@yahoo.fr	noureddineaouf@yahoo.fr	PROPN
eurjchem-610	3	11	(	(	PUNCT
eurjchem-610	3	12	n‐e	n‐e	PROPN
eurjchem-610	3	13	.	.	PUNCT
eurjchem-610	3	14	aouf	aouf	PROPN
eurjchem-610	3	15	)	)	PUNCT
eurjchem-610	3	16	.	.	PUNCT
eurjchem-610	4	1	article	article	NOUN
eurjchem-610	4	2	information	information	PROPN
eurjchem-610	4	3	abstract	abstract	ADV
eurjchem-610	4	4	received	receive	VERB
eurjchem-610	4	5	:	:	PUNCT
eurjchem-610	4	6	07	07	NUM
eurjchem-610	4	7	april	april	PROPN
eurjchem-610	4	8	2012	2012	NUM
eurjchem-610	4	9	received	receive	VERB
eurjchem-610	4	10	in	in	ADP
eurjchem-610	4	11	revised	revise	VERB
eurjchem-610	4	12	form	form	NOUN
eurjchem-610	4	13	:	:	PUNCT
eurjchem-610	4	14	19	19	NUM
eurjchem-610	4	15	may	may	AUX
eurjchem-610	4	16	2012	2012	NUM
eurjchem-610	4	17	accepted	accept	VERB
eurjchem-610	4	18	:	:	PUNCT
eurjchem-610	4	19	19	19	NUM
eurjchem-610	4	20	may	may	PROPN
eurjchem-610	4	21	2012	2012	NUM
eurjchem-610	4	22	online	online	NOUN
eurjchem-610	4	23	:	:	PUNCT
eurjchem-610	4	24	30	30	NUM
eurjchem-610	4	25	september	september	PROPN
eurjchem-610	4	26	2012	2012	NUM
eurjchem-610	4	27	keywords	keyword	VERB
eurjchem-610	4	28	a	a	DET
eurjchem-610	4	29	series	series	NOUN
eurjchem-610	4	30	of	of	ADP
eurjchem-610	4	31	sulfamides	sulfamide	NOUN
eurjchem-610	4	32	containing	contain	VERB
eurjchem-610	4	33	two	two	NUM
eurjchem-610	4	34	protecting	protect	VERB
eurjchem-610	4	35	groups	group	NOUN
eurjchem-610	4	36	have	have	AUX
eurjchem-610	4	37	been	be	AUX
eurjchem-610	4	38	synthesized	synthesize	VERB
eurjchem-610	4	39	starting	start	VERB
eurjchem-610	4	40	from	from	ADP
eurjchem-610	4	41	n‐benzoylaminoacids	n‐benzoylaminoacid	NOUN
eurjchem-610	4	42	derivatives	derivative	NOUN
eurjchem-610	4	43	of	of	ADP
eurjchem-610	4	44	(	(	PUNCT
eurjchem-610	4	45	glycine	glycine	NOUN
eurjchem-610	4	46	,	,	PUNCT
eurjchem-610	4	47	alanine	alanine	NOUN
eurjchem-610	4	48	,	,	PUNCT
eurjchem-610	4	49	valine	valine	NOUN
eurjchem-610	4	50	,	,	PUNCT
eurjchem-610	4	51	leucine	leucine	NOUN
eurjchem-610	4	52	,	,	PUNCT
eurjchem-610	4	53	phenylalanine	phenylalanine	NOUN
eurjchem-610	4	54	)	)	PUNCT
eurjchem-610	4	55	,	,	PUNCT
eurjchem-610	4	56	chlorosulfonylisocyanate	chlorosulfonylisocyanate	ADJ
eurjchem-610	4	57	and	and	CCONJ
eurjchem-610	4	58	primary	primary	ADJ
eurjchem-610	4	59	amines	amine	NOUN
eurjchem-610	4	60	.	.	PUNCT
eurjchem-610	5	1	selective	selective	ADJ
eurjchem-610	5	2	deprotection	deprotection	NOUN
eurjchem-610	5	3	of	of	ADP
eurjchem-610	5	4	the	the	DET
eurjchem-610	5	5	cyclic	cyclic	ADJ
eurjchem-610	5	6	or	or	CCONJ
eurjchem-610	5	7	linear	linear	ADJ
eurjchem-610	5	8	sulfamides	sulfamide	NOUN
eurjchem-610	5	9	and	and	CCONJ
eurjchem-610	5	10	amines	amine	NOUN
eurjchem-610	5	11	has	have	AUX
eurjchem-610	5	12	been	be	AUX
eurjchem-610	5	13	achieved	achieve	VERB
eurjchem-610	5	14	by	by	ADP
eurjchem-610	5	15	treatment	treatment	NOUN
eurjchem-610	5	16	with	with	ADP
eurjchem-610	5	17	heteropolyacid	heteropolyacid	NOUN
eurjchem-610	5	18	,	,	PUNCT
eurjchem-610	5	19	which	which	PRON
eurjchem-610	5	20	is	be	AUX
eurjchem-610	5	21	easily	easily	ADV
eurjchem-610	5	22	recoverable	recoverable	ADJ
eurjchem-610	5	23	and	and	CCONJ
eurjchem-610	5	24	reusable	reusable	ADJ
eurjchem-610	5	25	.	.	PUNCT
eurjchem-610	6	1	this	this	DET
eurjchem-610	6	2	method	method	NOUN
eurjchem-610	6	3	represents	represent	VERB
eurjchem-610	6	4	a	a	DET
eurjchem-610	6	5	reasonable	reasonable	ADJ
eurjchem-610	6	6	alternative	alternative	NOUN
eurjchem-610	6	7	to	to	ADP
eurjchem-610	6	8	the	the	DET
eurjchem-610	6	9	previous	previous	ADJ
eurjchem-610	6	10	reported	report	VERB
eurjchem-610	6	11	deprotection	deprotection	NOUN
eurjchem-610	6	12	procedures	procedure	NOUN
eurjchem-610	6	13	.	.	PUNCT
eurjchem-610	7	1	heteroplyacid	heteroplyacid	PROPN
eurjchem-610	7	2	cyclosulfamides	cyclosulfamide	VERB
eurjchem-610	7	3	protective	protective	ADJ
eurjchem-610	7	4	group	group	NOUN
eurjchem-610	7	5	n‐boc	n‐boc	DET
eurjchem-610	7	6	deprotection	deprotection	NOUN
eurjchem-610	7	7	dawson	dawson	PROPN
eurjchem-610	7	8	heteropolyacid	heteropolyacid	X
eurjchem-610	7	9	heterogeneous	heterogeneous	ADJ
eurjchem-610	7	10	catalysis	catalysis	NOUN
eurjchem-610	7	11	1	1	NUM
eurjchem-610	7	12	.	.	PUNCT
eurjchem-610	8	1	introduction	introduction	NOUN
eurjchem-610	8	2	the	the	DET
eurjchem-610	8	3	development	development	NOUN
eurjchem-610	8	4	of	of	ADP
eurjchem-610	8	5	mild	mild	ADJ
eurjchem-610	8	6	and	and	CCONJ
eurjchem-610	8	7	chemoselective	chemoselective	ADJ
eurjchem-610	8	8	methods	method	NOUN
eurjchem-610	8	9	for	for	ADP
eurjchem-610	8	10	the	the	DET
eurjchem-610	8	11	protection	protection	NOUN
eurjchem-610	8	12	and	and	CCONJ
eurjchem-610	8	13	deprotection	deprotection	NOUN
eurjchem-610	8	14	of	of	ADP
eurjchem-610	8	15	functional	functional	ADJ
eurjchem-610	8	16	groups	group	NOUN
eurjchem-610	8	17	continues	continue	VERB
eurjchem-610	8	18	to	to	PART
eurjchem-610	8	19	be	be	AUX
eurjchem-610	8	20	significant	significant	ADJ
eurjchem-610	8	21	tool	tool	NOUN
eurjchem-610	8	22	in	in	ADP
eurjchem-610	8	23	organic	organic	ADJ
eurjchem-610	8	24	synthesis	synthesis	NOUN
eurjchem-610	8	25	.	.	PUNCT
eurjchem-610	9	1	the	the	DET
eurjchem-610	9	2	tert‐	tert‐	PROPN
eurjchem-610	9	3	butyloxycarbonyl	butyloxycarbonyl	NOUN
eurjchem-610	9	4	(	(	PUNCT
eurjchem-610	9	5	boc	boc	NOUN
eurjchem-610	9	6	)	)	PUNCT
eurjchem-610	9	7	group	group	NOUN
eurjchem-610	9	8	is	be	AUX
eurjchem-610	9	9	extensively	extensively	ADV
eurjchem-610	9	10	used	use	VERB
eurjchem-610	9	11	in	in	ADP
eurjchem-610	9	12	peptide	peptide	NOUN
eurjchem-610	9	13	and	and	CCONJ
eurjchem-610	9	14	heterocyclic	heterocyclic	ADJ
eurjchem-610	9	15	synthesis	synthesis	NOUN
eurjchem-610	9	16	for	for	ADP
eurjchem-610	9	17	amine	amine	ADJ
eurjchem-610	9	18	protection	protection	NOUN
eurjchem-610	9	19	.	.	PUNCT
eurjchem-610	10	1	it	it	PRON
eurjchem-610	10	2	is	be	AUX
eurjchem-610	10	3	stable	stable	ADJ
eurjchem-610	10	4	against	against	ADP
eurjchem-610	10	5	hydrolysis	hydrolysis	NOUN
eurjchem-610	10	6	under	under	ADP
eurjchem-610	10	7	basic	basic	ADJ
eurjchem-610	10	8	conditions	condition	NOUN
eurjchem-610	10	9	and	and	CCONJ
eurjchem-610	10	10	to	to	ADP
eurjchem-610	10	11	many	many	ADJ
eurjchem-610	10	12	other	other	ADJ
eurjchem-610	10	13	nucleophic	nucleophic	ADJ
eurjchem-610	10	14	reagents	reagent	NOUN
eurjchem-610	10	15	.	.	PUNCT
eurjchem-610	11	1	it	it	PRON
eurjchem-610	11	2	is	be	AUX
eurjchem-610	11	3	easily	easily	ADV
eurjchem-610	11	4	introduced	introduce	VERB
eurjchem-610	11	5	using	use	VERB
eurjchem-610	11	6	commercially	commercially	ADV
eurjchem-610	11	7	available	available	ADJ
eurjchem-610	11	8	di‐tert‐butyldicarbonate	di‐tert‐butyldicarbonate	PROPN
eurjchem-610	11	9	(	(	PUNCT
eurjchem-610	11	10	tert‐	tert‐	VERB
eurjchem-610	12	1	buoco)2o	buoco)2o	ADP
eurjchem-610	12	2	under	under	ADP
eurjchem-610	12	3	standard	standard	ADJ
eurjchem-610	12	4	basic	basic	ADJ
eurjchem-610	12	5	conditions	condition	NOUN
eurjchem-610	12	6	.	.	PUNCT
eurjchem-610	13	1	deprotection	deprotection	NOUN
eurjchem-610	13	2	is	be	AUX
eurjchem-610	13	3	generally	generally	ADV
eurjchem-610	13	4	achieved	achieve	VERB
eurjchem-610	13	5	under	under	ADP
eurjchem-610	13	6	acid	acid	NOUN
eurjchem-610	13	7	conditions	condition	NOUN
eurjchem-610	13	8	,	,	PUNCT
eurjchem-610	13	9	as	as	SCONJ
eurjchem-610	13	10	extensively	extensively	ADV
eurjchem-610	13	11	described	describe	VERB
eurjchem-610	13	12	in	in	ADP
eurjchem-610	13	13	greene	greene	PROPN
eurjchem-610	13	14	’s	’s	PART
eurjchem-610	13	15	protective	protective	ADJ
eurjchem-610	13	16	group	group	NOUN
eurjchem-610	13	17	in	in	ADP
eurjchem-610	13	18	organic	organic	ADJ
eurjchem-610	13	19	synthesis	synthesis	NOUN
eurjchem-610	14	1	[	[	X
eurjchem-610	14	2	1,2	1,2	NUM
eurjchem-610	14	3	]	]	PUNCT
eurjchem-610	14	4	.	.	PUNCT
eurjchem-610	15	1	a	a	DET
eurjchem-610	15	2	variety	variety	NOUN
eurjchem-610	15	3	of	of	ADP
eurjchem-610	15	4	reagents	reagent	NOUN
eurjchem-610	15	5	have	have	AUX
eurjchem-610	15	6	been	be	AUX
eurjchem-610	15	7	employed	employ	VERB
eurjchem-610	15	8	to	to	PART
eurjchem-610	15	9	affect	affect	VERB
eurjchem-610	15	10	this	this	DET
eurjchem-610	15	11	transformation	transformation	NOUN
eurjchem-610	15	12	including	include	VERB
eurjchem-610	15	13	strong	strong	ADJ
eurjchem-610	15	14	acids	acid	NOUN
eurjchem-610	15	15	(	(	PUNCT
eurjchem-610	15	16	trifluoacetic	trifluoacetic	NOUN
eurjchem-610	15	17	acid“tfa	acid“tfa	NOUN
eurjchem-610	15	18	”	"	PUNCT
eurjchem-610	15	19	,	,	PUNCT
eurjchem-610	15	20	hcl	hcl	PROPN
eurjchem-610	15	21	,	,	PUNCT
eurjchem-610	15	22	hbr	hbr	PROPN
eurjchem-610	15	23	,	,	PUNCT
eurjchem-610	15	24	h2so4	h2so4	PROPN
eurjchem-610	15	25	,	,	PUNCT
eurjchem-610	15	26	hno3and	hno3and	PROPN
eurjchem-610	15	27	lewis	lewis	PROPN
eurjchem-610	15	28	acids	acids	PROPN
eurjchem-610	15	29	(	(	PUNCT
eurjchem-610	15	30	bf3.et2o	bf3.et2o	NOUN
eurjchem-610	15	31	and	and	CCONJ
eurjchem-610	15	32	znbr	znbr	NOUN
eurjchem-610	15	33	)	)	PUNCT
eurjchem-610	15	34	)	)	PUNCT
eurjchem-610	15	35	.	.	PUNCT
eurjchem-610	16	1	cleavage	cleavage	NOUN
eurjchem-610	16	2	of	of	ADP
eurjchem-610	16	3	the	the	DET
eurjchem-610	16	4	boc	boc	NOUN
eurjchem-610	16	5	moiety	moiety	NOUN
eurjchem-610	16	6	can	can	AUX
eurjchem-610	16	7	be	be	AUX
eurjchem-610	16	8	obtained	obtain	VERB
eurjchem-610	16	9	under	under	ADP
eurjchem-610	16	10	basic	basic	ADJ
eurjchem-610	16	11	conditions	condition	NOUN
eurjchem-610	16	12	only	only	ADV
eurjchem-610	16	13	in	in	ADP
eurjchem-610	16	14	special	special	ADJ
eurjchem-610	16	15	cases	case	NOUN
eurjchem-610	16	16	,	,	PUNCT
eurjchem-610	16	17	where	where	SCONJ
eurjchem-610	16	18	the	the	DET
eurjchem-610	16	19	amine	amine	NOUN
eurjchem-610	16	20	is	be	AUX
eurjchem-610	16	21	highly	highly	ADV
eurjchem-610	16	22	activated	activate	VERB
eurjchem-610	16	23	,	,	PUNCT
eurjchem-610	16	24	such	such	ADJ
eurjchem-610	16	25	as	as	ADP
eurjchem-610	16	26	a	a	DET
eurjchem-610	16	27	pyrrole	pyrrole	NOUN
eurjchem-610	16	28	[	[	X
eurjchem-610	16	29	3	3	NUM
eurjchem-610	16	30	]	]	PUNCT
eurjchem-610	16	31	.	.	PUNCT
eurjchem-610	17	1	thermal	thermal	ADJ
eurjchem-610	17	2	deprotection	deprotection	NOUN
eurjchem-610	17	3	have	have	AUX
eurjchem-610	17	4	also	also	ADV
eurjchem-610	17	5	been	be	AUX
eurjchem-610	17	6	reported	report	VERB
eurjchem-610	17	7	[	[	X
eurjchem-610	17	8	4,5	4,5	NUM
eurjchem-610	17	9	]	]	PUNCT
eurjchem-610	17	10	.	.	PUNCT
eurjchem-610	18	1	the	the	DET
eurjchem-610	18	2	deprotection	deprotection	NOUN
eurjchem-610	18	3	can	can	AUX
eurjchem-610	18	4	also	also	ADV
eurjchem-610	18	5	be	be	AUX
eurjchem-610	18	6	effected	effect	VERB
eurjchem-610	18	7	with	with	ADP
eurjchem-610	18	8	mildly	mildly	ADV
eurjchem-610	18	9	acidic	acidic	ADJ
eurjchem-610	18	10	conditions	condition	NOUN
eurjchem-610	18	11	such	such	ADJ
eurjchem-610	18	12	as	as	ADP
eurjchem-610	18	13	montmorillonite	montmorillonite	ADJ
eurjchem-610	18	14	k10	k10	PROPN
eurjchem-610	18	15	clay	clay	NOUN
eurjchem-610	18	16	catalyst	catalyst	NOUN
eurjchem-610	19	1	[	[	X
eurjchem-610	19	2	6	6	NUM
eurjchem-610	19	3	]	]	PUNCT
eurjchem-610	19	4	and	and	CCONJ
eurjchem-610	19	5	silica	silica	NOUN
eurjchem-610	19	6	gel	gel	NOUN
eurjchem-610	19	7	(	(	PUNCT
eurjchem-610	19	8	in	in	ADP
eurjchem-610	19	9	low	low	ADJ
eurjchem-610	19	10	pressure	pressure	NOUN
eurjchem-610	19	11	)	)	PUNCT
eurjchem-610	20	1	[	[	X
eurjchem-610	20	2	7	7	NUM
eurjchem-610	20	3	]	]	PUNCT
eurjchem-610	20	4	.	.	PUNCT
eurjchem-610	21	1	many	many	ADJ
eurjchem-610	21	2	of	of	ADP
eurjchem-610	21	3	these	these	DET
eurjchem-610	21	4	methods	method	NOUN
eurjchem-610	21	5	suffer	suffer	VERB
eurjchem-610	21	6	from	from	ADP
eurjchem-610	21	7	disadvantages	disadvantage	NOUN
eurjchem-610	21	8	such	such	ADJ
eurjchem-610	21	9	high	high	ADJ
eurjchem-610	21	10	acidity	acidity	NOUN
eurjchem-610	21	11	,	,	PUNCT
eurjchem-610	21	12	expensive	expensive	ADJ
eurjchem-610	21	13	reagents	reagent	NOUN
eurjchem-610	21	14	and	and	CCONJ
eurjchem-610	21	15	using	use	VERB
eurjchem-610	21	16	more	more	ADV
eurjchem-610	21	17	excessive	excessive	ADJ
eurjchem-610	21	18	amounts	amount	NOUN
eurjchem-610	21	19	of	of	ADP
eurjchem-610	21	20	catalysts	catalyst	NOUN
eurjchem-610	21	21	,	,	PUNCT
eurjchem-610	21	22	high	high	ADJ
eurjchem-610	21	23	temperature	temperature	NOUN
eurjchem-610	21	24	and	and	CCONJ
eurjchem-610	21	25	slow	slow	ADJ
eurjchem-610	21	26	rate	rate	NOUN
eurjchem-610	21	27	reaction	reaction	NOUN
eurjchem-610	21	28	.	.	PUNCT
eurjchem-610	22	1	in	in	ADP
eurjchem-610	22	2	our	our	PRON
eurjchem-610	22	3	previous	previous	ADJ
eurjchem-610	22	4	work	work	NOUN
eurjchem-610	22	5	,	,	PUNCT
eurjchem-610	22	6	we	we	PRON
eurjchem-610	22	7	have	have	AUX
eurjchem-610	22	8	reported	report	VERB
eurjchem-610	22	9	the	the	DET
eurjchem-610	22	10	fusion	fusion	NOUN
eurjchem-610	22	11	method	method	NOUN
eurjchem-610	22	12	for	for	ADP
eurjchem-610	22	13	the	the	DET
eurjchem-610	22	14	n‐boc	n‐boc	DET
eurjchem-610	22	15	deprotection	deprotection	NOUN
eurjchem-610	22	16	[	[	X
eurjchem-610	22	17	8	8	NUM
eurjchem-610	22	18	]	]	PUNCT
eurjchem-610	22	19	.	.	PUNCT
eurjchem-610	23	1	more	more	ADV
eurjchem-610	23	2	recently	recently	ADV
eurjchem-610	23	3	,	,	PUNCT
eurjchem-610	23	4	we	we	PRON
eurjchem-610	23	5	have	have	AUX
eurjchem-610	23	6	developed	develop	VERB
eurjchem-610	23	7	the	the	DET
eurjchem-610	23	8	catalyst‐free	catalyst‐free	ADJ
eurjchem-610	23	9	water‐related	water‐relate	VERB
eurjchem-610	23	10	system	system	NOUN
eurjchem-610	23	11	for	for	ADP
eurjchem-610	23	12	the	the	DET
eurjchem-610	23	13	n‐boc	n‐boc	DET
eurjchem-610	23	14	protection	protection	NOUN
eurjchem-610	23	15	/	/	SYM
eurjchem-610	23	16	deprotection	deprotection	NOUN
eurjchem-610	23	17	[	[	X
eurjchem-610	23	18	9,10	9,10	NUM
eurjchem-610	23	19	]	]	X
eurjchem-610	23	20	.	.	PUNCT
eurjchem-610	24	1	in	in	ADP
eurjchem-610	24	2	the	the	DET
eurjchem-610	24	3	continuity	continuity	NOUN
eurjchem-610	24	4	of	of	ADP
eurjchem-610	24	5	our	our	PRON
eurjchem-610	24	6	research	research	NOUN
eurjchem-610	24	7	,	,	PUNCT
eurjchem-610	24	8	we	we	PRON
eurjchem-610	24	9	have	have	AUX
eurjchem-610	24	10	focussed	focusse	VERB
eurjchem-610	24	11	to	to	ADP
eurjchem-610	24	12	the	the	DET
eurjchem-610	24	13	development	development	NOUN
eurjchem-610	24	14	of	of	ADP
eurjchem-610	24	15	new	new	ADJ
eurjchem-610	24	16	reagents	reagent	NOUN
eurjchem-610	24	17	and	and	CCONJ
eurjchem-610	24	18	methods	method	NOUN
eurjchem-610	24	19	for	for	ADP
eurjchem-610	24	20	the	the	DET
eurjchem-610	24	21	n‐boc	n‐boc	DET
eurjchem-610	24	22	deprotection	deprotection	NOUN
eurjchem-610	24	23	,	,	PUNCT
eurjchem-610	24	24	we	we	PRON
eurjchem-610	24	25	attempt	attempt	VERB
eurjchem-610	24	26	to	to	PART
eurjchem-610	24	27	use	use	VERB
eurjchem-610	24	28	the	the	DET
eurjchem-610	24	29	dawson	dawson	NOUN
eurjchem-610	24	30	heteropolyacid	heteropolyacid	PROPN
eurjchem-610	24	31	(	(	PUNCT
eurjchem-610	24	32	hpa	hpa	NOUN
eurjchem-610	24	33	)	)	PUNCT
eurjchem-610	24	34	as	as	ADP
eurjchem-610	24	35	catalyst	catalyst	NOUN
eurjchem-610	24	36	.	.	PUNCT
eurjchem-610	25	1	heteropolyacids	heteropolyacid	NOUN
eurjchem-610	25	2	have	have	AUX
eurjchem-610	25	3	been	be	AUX
eurjchem-610	25	4	reported	report	VERB
eurjchem-610	25	5	as	as	ADP
eurjchem-610	25	6	versatile	versatile	ADJ
eurjchem-610	25	7	green	green	ADJ
eurjchem-610	25	8	catalysts	catalyst	NOUN
eurjchem-610	25	9	for	for	ADP
eurjchem-610	25	10	a	a	DET
eurjchem-610	25	11	variety	variety	NOUN
eurjchem-610	25	12	of	of	ADP
eurjchem-610	25	13	reactions	reaction	NOUN
eurjchem-610	25	14	[	[	X
eurjchem-610	25	15	11	11	NUM
eurjchem-610	25	16	]	]	PUNCT
eurjchem-610	25	17	.	.	PUNCT
eurjchem-610	26	1	the	the	DET
eurjchem-610	26	2	large	large	ADJ
eurjchem-610	26	3	field	field	NOUN
eurjchem-610	26	4	of	of	ADP
eurjchem-610	26	5	research	research	NOUN
eurjchem-610	26	6	in	in	ADP
eurjchem-610	26	7	heteropolyanion	heteropolyanion	NOUN
eurjchem-610	26	8	(	(	PUNCT
eurjchem-610	26	9	hpan	hpan	NOUN
eurjchem-610	26	10	)	)	PUNCT
eurjchem-610	26	11	chemistry	chemistry	NOUN
eurjchem-610	26	12	has	have	AUX
eurjchem-610	26	13	been	be	AUX
eurjchem-610	26	14	devoted	devote	VERB
eurjchem-610	26	15	to	to	ADP
eurjchem-610	26	16	the	the	DET
eurjchem-610	26	17	preparation	preparation	NOUN
eurjchem-610	26	18	,	,	PUNCT
eurjchem-610	26	19	structure	structure	NOUN
eurjchem-610	26	20	characterization	characterization	NOUN
eurjchem-610	26	21	,	,	PUNCT
eurjchem-610	26	22	and	and	CCONJ
eurjchem-610	26	23	analytical	analytical	ADJ
eurjchem-610	26	24	applications	application	NOUN
eurjchem-610	26	25	of	of	ADP
eurjchem-610	26	26	these	these	DET
eurjchem-610	26	27	compounds	compound	NOUN
eurjchem-610	26	28	[	[	X
eurjchem-610	26	29	12,13	12,13	NUM
eurjchem-610	26	30	]	]	PUNCT
eurjchem-610	26	31	.	.	PUNCT
eurjchem-610	27	1	surprisingly	surprisingly	ADV
eurjchem-610	27	2	,	,	PUNCT
eurjchem-610	27	3	in	in	ADP
eurjchem-610	27	4	spite	spite	NOUN
eurjchem-610	27	5	of	of	ADP
eurjchem-610	27	6	their	their	PRON
eurjchem-610	27	7	importance	importance	NOUN
eurjchem-610	27	8	,	,	PUNCT
eurjchem-610	27	9	dawson	dawson	PROPN
eurjchem-610	27	10	hpa	hpa	PROPN
eurjchem-610	27	11	is	be	AUX
eurjchem-610	27	12	not	not	PART
eurjchem-610	27	13	extensively	extensively	ADV
eurjchem-610	27	14	used	use	VERB
eurjchem-610	27	15	in	in	ADP
eurjchem-610	27	16	organic	organic	ADJ
eurjchem-610	27	17	synthesis	synthesis	NOUN
eurjchem-610	27	18	,	,	PUNCT
eurjchem-610	27	19	except	except	SCONJ
eurjchem-610	27	20	in	in	ADP
eurjchem-610	27	21	few	few	ADJ
eurjchem-610	27	22	examples	example	NOUN
eurjchem-610	27	23	described	describe	VERB
eurjchem-610	27	24	in	in	ADP
eurjchem-610	27	25	literature	literature	NOUN
eurjchem-610	27	26	[	[	X
eurjchem-610	27	27	14‐19	14‐19	NUM
eurjchem-610	27	28	]	]	PUNCT
eurjchem-610	27	29	.	.	PUNCT
eurjchem-610	28	1	heydari	heydari	PROPN
eurjchem-610	28	2	et	et	PROPN
eurjchem-610	28	3	al	al	PROPN
eurjchem-610	28	4	.	.	PUNCT
eurjchem-610	29	1	[	[	X
eurjchem-610	29	2	20	20	NUM
eurjchem-610	29	3	]	]	PUNCT
eurjchem-610	29	4	reported	report	VERB
eurjchem-610	29	5	the	the	DET
eurjchem-610	29	6	n‐tert‐butoxycarbonylation	n‐tert‐butoxycarbonylation	NOUN
eurjchem-610	29	7	of	of	ADP
eurjchem-610	29	8	amines	amine	NOUN
eurjchem-610	29	9	using	use	VERB
eurjchem-610	29	10	commercially	commercially	ADV
eurjchem-610	29	11	available	available	ADJ
eurjchem-610	29	12	keggin	keggin	NOUN
eurjchem-610	29	13	heteropolyacids	heteropolyacid	NOUN
eurjchem-610	29	14	(	(	PUNCT
eurjchem-610	29	15	h3pw12o40	h3pw12o40	NOUN
eurjchem-610	29	16	)	)	PUNCT
eurjchem-610	29	17	.	.	PUNCT
eurjchem-610	30	1	except	except	SCONJ
eurjchem-610	30	2	very	very	ADV
eurjchem-610	30	3	few	few	ADJ
eurjchem-610	30	4	examples	example	NOUN
eurjchem-610	30	5	,	,	PUNCT
eurjchem-610	30	6	no	no	DET
eurjchem-610	30	7	reference	reference	NOUN
eurjchem-610	30	8	reported	report	VERB
eurjchem-610	30	9	the	the	DET
eurjchem-610	30	10	use	use	NOUN
eurjchem-610	30	11	the	the	DET
eurjchem-610	30	12	hpa	hpa	NOUN
eurjchem-610	30	13	in	in	ADP
eurjchem-610	30	14	protecting	protect	VERB
eurjchem-610	30	15	group	group	NOUN
eurjchem-610	30	16	chemistry	chemistry	NOUN
eurjchem-610	30	17	.	.	PUNCT
eurjchem-610	31	1	in	in	ADP
eurjchem-610	31	2	this	this	DET
eurjchem-610	31	3	paper	paper	NOUN
eurjchem-610	31	4	,	,	PUNCT
eurjchem-610	31	5	we	we	PRON
eurjchem-610	31	6	report	report	VERB
eurjchem-610	31	7	a	a	DET
eurjchem-610	31	8	deprotection	deprotection	NOUN
eurjchem-610	31	9	study	study	NOUN
eurjchem-610	31	10	of	of	ADP
eurjchem-610	31	11	the	the	DET
eurjchem-610	31	12	boc	boc	NOUN
eurjchem-610	31	13	group	group	NOUN
eurjchem-610	31	14	in	in	ADP
eurjchem-610	31	15	cyclosulfamides	cyclosulfamide	NOUN
eurjchem-610	31	16	,	,	PUNCT
eurjchem-610	31	17	linear	linear	ADJ
eurjchem-610	31	18	sulfamides	sulfamide	NOUN
eurjchem-610	31	19	and	and	CCONJ
eurjchem-610	31	20	amines	amine	NOUN
eurjchem-610	31	21	carried	carry	VERB
eurjchem-610	31	22	out	out	ADP
eurjchem-610	31	23	using	use	VERB
eurjchem-610	31	24	a	a	DET
eurjchem-610	31	25	heteropolyacid	heteropolyacid	NOUN
eurjchem-610	31	26	with	with	ADP
eurjchem-610	31	27	wells‐dawson	wells‐dawson	NOUN
eurjchem-610	31	28	structure	structure	NOUN
eurjchem-610	31	29	in	in	ADP
eurjchem-610	31	30	dichloromethane	dichloromethane	NOUN
eurjchem-610	31	31	.	.	PUNCT
eurjchem-610	32	1	2	2	X
eurjchem-610	32	2	.	.	X
eurjchem-610	32	3	experimental	experimental	ADJ
eurjchem-610	32	4	all	all	DET
eurjchem-610	32	5	commercial	commercial	ADJ
eurjchem-610	32	6	chemicals	chemical	NOUN
eurjchem-610	32	7	and	and	CCONJ
eurjchem-610	32	8	solvents	solvent	NOUN
eurjchem-610	32	9	were	be	AUX
eurjchem-610	32	10	without	without	ADP
eurjchem-610	32	11	further	further	ADJ
eurjchem-610	32	12	purification	purification	NOUN
eurjchem-610	32	13	.	.	PUNCT
eurjchem-610	33	1	all	all	DET
eurjchem-610	33	2	reactions	reaction	NOUN
eurjchem-610	33	3	were	be	AUX
eurjchem-610	33	4	carried	carry	VERB
eurjchem-610	33	5	out	out	ADP
eurjchem-610	33	6	under	under	ADP
eurjchem-610	33	7	inert	inert	ADJ
eurjchem-610	33	8	argon	argon	NOUN
eurjchem-610	33	9	atmosphere	atmosphere	NOUN
eurjchem-610	33	10	.	.	PUNCT
eurjchem-610	34	1	melting	melt	VERB
eurjchem-610	34	2	points	point	NOUN
eurjchem-610	34	3	were	be	AUX
eurjchem-610	34	4	determined	determine	VERB
eurjchem-610	34	5	in	in	ADP
eurjchem-610	34	6	open	open	ADJ
eurjchem-610	34	7	capillary	capillary	ADJ
eurjchem-610	34	8	tubes	tube	NOUN
eurjchem-610	34	9	on	on	ADP
eurjchem-610	34	10	a	a	DET
eurjchem-610	34	11	büchi	büchi	ADJ
eurjchem-610	34	12	apparatus	apparatus	NOUN
eurjchem-610	34	13	and	and	CCONJ
eurjchem-610	34	14	are	be	AUX
eurjchem-610	34	15	uncorrected	uncorrecte	VERB
eurjchem-610	34	16	.	.	PUNCT
eurjchem-610	35	1	1h	1h	NUM
eurjchem-610	35	2	and	and	CCONJ
eurjchem-610	35	3	13c	13c	NOUN
eurjchem-610	35	4	nmr	nmr	NOUN
eurjchem-610	35	5	spectra	spectra	NOUN
eurjchem-610	35	6	were	be	AUX
eurjchem-610	35	7	recorded	record	VERB
eurjchem-610	35	8	in	in	ADP
eurjchem-610	35	9	a	a	DET
eurjchem-610	35	10	250	250	NUM
eurjchem-610	35	11	mhz	mhz	NOUN
eurjchem-610	35	12	bruker	bruker	NOUN
eurjchem-610	35	13	spectrometer	spectrometer	NOUN
eurjchem-610	35	14	.	.	PUNCT
eurjchem-610	36	1	microanalyses	microanalysis	NOUN
eurjchem-610	36	2	were	be	AUX
eurjchem-610	36	3	performed	perform	VERB
eurjchem-610	36	4	in	in	ADP
eurjchem-610	36	5	the	the	DET
eurjchem-610	36	6	microanalysis	microanalysis	ADJ
eurjchem-610	36	7	laboratory	laboratory	NOUN
eurjchem-610	36	8	of	of	ADP
eurjchem-610	36	9	enscm	enscm	PROPN
eurjchem-610	36	10	(	(	PUNCT
eurjchem-610	36	11	montpellier	montpellier	NOUN
eurjchem-610	36	12	)	)	PUNCT
eurjchem-610	36	13	.	.	PUNCT
eurjchem-610	37	1	spectral	spectral	ADJ
eurjchem-610	37	2	data	datum	NOUN
eurjchem-610	37	3	are	be	AUX
eurjchem-610	37	4	reported	report	VERB
eurjchem-610	37	5	in	in	ADP
eurjchem-610	37	6	δ	δ	PROPN
eurjchem-610	37	7	unit	unit	NOUN
eurjchem-610	37	8	(	(	PUNCT
eurjchem-610	37	9	ppm	ppm	NOUN
eurjchem-610	37	10	)	)	PUNCT
eurjchem-610	37	11	relative	relative	ADJ
eurjchem-610	37	12	to	to	ADP
eurjchem-610	37	13	tetramethyl	tetramethyl	NOUN
eurjchem-610	37	14	silane	silane	NOUN
eurjchem-610	37	15	(	(	PUNCT
eurjchem-610	37	16	tms	tms	PROPN
eurjchem-610	37	17	)	)	PUNCT
eurjchem-610	37	18	as	as	ADP
eurjchem-610	37	19	reference	reference	NOUN
eurjchem-610	37	20	.	.	PUNCT
eurjchem-610	38	1	all	all	PRON
eurjchem-610	38	2	coupling	couple	VERB
eurjchem-610	38	3	constants	constant	NOUN
eurjchem-610	38	4	j	j	PROPN
eurjchem-610	38	5	are	be	AUX
eurjchem-610	38	6	reported	report	VERB
eurjchem-610	38	7	in	in	ADP
eurjchem-610	38	8	hertz	hertz	NOUN
eurjchem-610	38	9	.	.	PUNCT
eurjchem-610	39	1	multiplicity	multiplicity	NOUN
eurjchem-610	39	2	is	be	AUX
eurjchem-610	39	3	indicated	indicate	VERB
eurjchem-610	39	4	as	as	ADP
eurjchem-610	39	5	s	s	NOUN
eurjchem-610	39	6	(	(	PUNCT
eurjchem-610	39	7	singlet	singlet	NOUN
eurjchem-610	39	8	)	)	PUNCT
eurjchem-610	39	9	,	,	PUNCT
eurjchem-610	39	10	d	d	X
eurjchem-610	39	11	(	(	PUNCT
eurjchem-610	39	12	doublet	doublet	PROPN
eurjchem-610	39	13	)	)	PUNCT
eurjchem-610	39	14	,	,	PUNCT
eurjchem-610	39	15	t	t	PROPN
eurjchem-610	39	16	(	(	PUNCT
eurjchem-610	39	17	triplet	triplet	NOUN
eurjchem-610	39	18	)	)	PUNCT
eurjchem-610	39	19	,	,	PUNCT
eurjchem-610	39	20	q	q	PROPN
eurjchem-610	39	21	(	(	PUNCT
eurjchem-610	39	22	quartet	quartet	NOUN
eurjchem-610	39	23	)	)	PUNCT
eurjchem-610	39	24	,	,	PUNCT
eurjchem-610	39	25	m	m	PROPN
eurjchem-610	39	26	(	(	PUNCT
eurjchem-610	39	27	multiplet	multiplet	NOUN
eurjchem-610	39	28	)	)	PUNCT
eurjchem-610	39	29	and	and	CCONJ
eurjchem-610	39	30	combination	combination	NOUN
eurjchem-610	39	31	of	of	ADP
eurjchem-610	39	32	these	these	DET
eurjchem-610	39	33	signals	signal	NOUN
eurjchem-610	39	34	.	.	PUNCT
eurjchem-610	40	1	electron	electron	NOUN
eurjchem-610	40	2	ionisation	ionisation	NOUN
eurjchem-610	40	3	mass	mass	NOUN
eurjchem-610	40	4	spectra	spectra	NOUN
eurjchem-610	40	5	(	(	PUNCT
eurjchem-610	40	6	30	30	NUM
eurjchem-610	40	7	ev	ev	NOUN
eurjchem-610	40	8	)	)	PUNCT
eurjchem-610	40	9	were	be	AUX
eurjchem-610	40	10	recorded	record	VERB
eurjchem-610	40	11	in	in	ADP
eurjchem-610	40	12	positive	positive	ADJ
eurjchem-610	40	13	or	or	CCONJ
eurjchem-610	40	14	negative	negative	ADJ
eurjchem-610	40	15	mode	mode	NOUN
eurjchem-610	40	16	on	on	ADP
eurjchem-610	40	17	a	a	DET
eurjchem-610	40	18	water	water	NOUN
eurjchem-610	40	19	micromass	micromass	NOUN
eurjchem-610	40	20	zq	zq	PROPN
eurjchem-610	40	21	.	.	PROPN
eurjchem-610	40	22	306	306	NUM
eurjchem-610	40	23	belghiche	belghiche	PROPN
eurjchem-610	40	24	et	et	PROPN
eurjchem-610	40	25	al	al	PROPN
eurjchem-610	40	26	.	.	PUNCT
eurjchem-610	40	27	/	/	SYM
eurjchem-610	40	28	european	european	PROPN
eurjchem-610	40	29	journal	journal	PROPN
eurjchem-610	40	30	of	of	ADP
eurjchem-610	40	31	chemistry	chemistry	NOUN
eurjchem-610	40	32	3	3	NUM
eurjchem-610	40	33	(	(	PUNCT
eurjchem-610	40	34	3	3	NUM
eurjchem-610	40	35	)	)	PUNCT
eurjchem-610	40	36	(	(	PUNCT
eurjchem-610	40	37	2012	2012	NUM
eurjchem-610	40	38	)	)	PUNCT
eurjchem-610	40	39	305‐309	305‐309	PROPN
eurjchem-610	40	40	n	n	CCONJ
eurjchem-610	40	41	s	s	NOUN
eurjchem-610	40	42	n	n	CCONJ
eurjchem-610	40	43	-	-	PUNCT
eurjchem-610	40	44	boc	boc	NOUN
eurjchem-610	40	45	r	r	NOUN
eurjchem-610	40	46	rt	rt	PROPN
eurjchem-610	40	47	,	,	PUNCT
eurjchem-610	40	48	ch2cl2	ch2cl2	PUNCT
eurjchem-610	40	49	n	n	PROPN
eurjchem-610	40	50	s	s	NOUN
eurjchem-610	40	51	n	n	CCONJ
eurjchem-610	40	52	-	-	PUNCT
eurjchem-610	40	53	h	h	NOUN
eurjchem-610	41	1	o	o	NOUN
eurjchem-610	41	2	o	o	NOUN
eurjchem-610	41	3	r	r	NOUN
eurjchem-610	41	4	oo	oo	NOUN
eurjchem-610	41	5	1a	1a	NOUN
eurjchem-610	41	6	:	:	PUNCT
eurjchem-610	42	1	r	r	X
eurjchem-610	42	2	=	=	NOUN
eurjchem-610	42	3	h	h	NOUN
eurjchem-610	42	4	2a	2a	NUM
eurjchem-610	42	5	.	.	PUNCT
eurjchem-610	43	1	r	r	X
eurjchem-610	43	2	=	=	SYM
eurjchem-610	43	3	ch3	ch3	PROPN
eurjchem-610	43	4	3a	3a	NUM
eurjchem-610	43	5	:	:	PUNCT
eurjchem-610	43	6	r	r	X
eurjchem-610	43	7	=	=	NOUN
eurjchem-610	43	8	ch(ch3)2	ch(ch3)2	NOUN
eurjchem-610	43	9	4a	4a	NUM
eurjchem-610	43	10	.	.	PUNCT
eurjchem-610	44	1	r	r	X
eurjchem-610	44	2	=	=	NOUN
eurjchem-610	44	3	ch2	ch2	NOUN
eurjchem-610	44	4	ch	ch	NOUN
eurjchem-610	44	5	(	(	PUNCT
eurjchem-610	44	6	ch3)2	ch3)2	PROPN
eurjchem-610	44	7	5a	5a	NUM
eurjchem-610	44	8	:	:	PUNCT
eurjchem-610	44	9	r	r	X
eurjchem-610	44	10	=	=	NOUN
eurjchem-610	44	11	ch2ph	ch2ph	PRON
eurjchem-610	44	12	1	1	NUM
eurjchem-610	44	13	-	-	SYM
eurjchem-610	44	14	5	5	NUM
eurjchem-610	44	15	1a-5a	1a-5a	NOUN
eurjchem-610	44	16	h6p2w12mo6o62	h6p2w12mo6o62	ADP
eurjchem-610	44	17	scheme	scheme	NOUN
eurjchem-610	44	18	1	1	NUM
eurjchem-610	44	19	high‐resolution	high‐resolution	NOUN
eurjchem-610	44	20	massspectra	massspectra	NOUN
eurjchem-610	44	21	were	be	AUX
eurjchem-610	44	22	measured	measure	VERB
eurjchem-610	44	23	on	on	ADP
eurjchem-610	44	24	a	a	DET
eurjchem-610	44	25	jeol	jeol	ADJ
eurjchem-610	44	26	sx102	sx102	PROPN
eurjchem-610	44	27	mass	mass	NOUN
eurjchem-610	44	28	spectrometer	spectrometer	NOUN
eurjchem-610	44	29	and	and	CCONJ
eurjchem-610	44	30	recorded	record	VERB
eurjchem-610	44	31	in	in	ADP
eurjchem-610	44	32	fab	fab	PROPN
eurjchem-610	44	33	(	(	PUNCT
eurjchem-610	44	34	fast	fast	ADJ
eurjchem-610	44	35	atom	atom	NOUN
eurjchem-610	44	36	bombardement	bombardement	NOUN
eurjchem-610	44	37	)	)	PUNCT
eurjchem-610	44	38	positive	positive	ADJ
eurjchem-610	44	39	mode	mode	NOUN
eurjchem-610	44	40	.	.	PUNCT
eurjchem-610	45	1	all	all	DET
eurjchem-610	45	2	reactions	reaction	NOUN
eurjchem-610	45	3	were	be	AUX
eurjchem-610	45	4	monitored	monitor	VERB
eurjchem-610	45	5	by	by	ADP
eurjchem-610	45	6	thin	thin	ADJ
eurjchem-610	45	7	layer	layer	NOUN
eurjchem-610	45	8	chromatography	chromatography	NOUN
eurjchem-610	45	9	(	(	PUNCT
eurjchem-610	45	10	tlc	tlc	NOUN
eurjchem-610	45	11	)	)	PUNCT
eurjchem-610	45	12	on	on	ADP
eurjchem-610	45	13	silica	silica	NOUN
eurjchem-610	45	14	merck	merck	NOUN
eurjchem-610	45	15	60	60	NUM
eurjchem-610	45	16	f254precoated	f254precoate	VERB
eurjchem-610	45	17	aluminium	aluminium	NOUN
eurjchem-610	45	18	plates	plate	NOUN
eurjchem-610	45	19	and	and	CCONJ
eurjchem-610	45	20	were	be	AUX
eurjchem-610	45	21	developed	develop	VERB
eurjchem-610	45	22	by	by	ADP
eurjchem-610	45	23	spraying	spray	VERB
eurjchem-610	45	24	with	with	ADP
eurjchem-610	45	25	ninhydrin	ninhydrin	NOUN
eurjchem-610	45	26	solution	solution	NOUN
eurjchem-610	45	27	.	.	PUNCT
eurjchem-610	46	1	optical	optical	ADJ
eurjchem-610	46	2	rotations	rotation	NOUN
eurjchem-610	46	3	were	be	AUX
eurjchem-610	46	4	measured	measure	VERB
eurjchem-610	46	5	on	on	ADP
eurjchem-610	46	6	a	a	DET
eurjchem-610	46	7	jasco	jasco	ADJ
eurjchem-610	46	8	dip‐370	dip‐370	PROPN
eurjchem-610	46	9	digital	digital	ADJ
eurjchem-610	46	10	polarimeter	polarimeter	NOUN
eurjchem-610	46	11	.	.	PUNCT
eurjchem-610	47	1	columns	column	NOUN
eurjchem-610	47	2	chroma‐tographies	chroma‐tographie	NOUN
eurjchem-610	47	3	were	be	AUX
eurjchem-610	47	4	performed	perform	VERB
eurjchem-610	47	5	on	on	ADP
eurjchem-610	47	6	merck	merck	PROPN
eurjchem-610	47	7	silica	silica	NOUN
eurjchem-610	47	8	gel	gel	NOUN
eurjchem-610	47	9	(	(	PUNCT
eurjchem-610	47	10	230‐	230‐	NUM
eurjchem-610	47	11	400	400	NUM
eurjchem-610	47	12	mesh	mesh	NOUN
eurjchem-610	47	13	)	)	PUNCT
eurjchem-610	47	14	.	.	PUNCT
eurjchem-610	48	1	2.1	2.1	NUM
eurjchem-610	48	2	.	.	PUNCT
eurjchem-610	48	3	synthesis	synthesis	VERB
eurjchem-610	48	4	the	the	DET
eurjchem-610	48	5	heteropolyanions	heteropolyanion	NOUN
eurjchem-610	48	6	precursor	precursor	NOUN
eurjchem-610	48	7	’s	’s	PART
eurjchem-610	48	8	k6p2w18o62.14h2o	k6p2w18o62.14h2o	NOUN
eurjchem-610	48	9	and	and	CCONJ
eurjchem-610	48	10	k6p2w12mo6o62.14h2o	k6p2w12mo6o62.14h2o	NOUN
eurjchem-610	48	11	as	as	ADV
eurjchem-610	48	12	well	well	ADV
eurjchem-610	48	13	as	as	ADP
eurjchem-610	48	14	their	their	PRON
eurjchem-610	48	15	acids	acid	NOUN
eurjchem-610	48	16	forms	form	NOUN
eurjchem-610	48	17	were	be	AUX
eurjchem-610	48	18	synthesized	synthesize	VERB
eurjchem-610	48	19	according	accord	VERB
eurjchem-610	48	20	to	to	ADP
eurjchem-610	48	21	published	publish	VERB
eurjchem-610	48	22	procedures	procedure	NOUN
eurjchem-610	48	23	[	[	X
eurjchem-610	48	24	21,22	21,22	X
eurjchem-610	48	25	]	]	X
eurjchem-610	48	26	and	and	CCONJ
eurjchem-610	48	27	purity	purity	NOUN
eurjchem-610	48	28	was	be	AUX
eurjchem-610	48	29	confirmed	confirm	VERB
eurjchem-610	48	30	by	by	ADP
eurjchem-610	48	31	infrared	infrared	PROPN
eurjchem-610	48	32	and	and	CCONJ
eurjchem-610	48	33	31p	31p	NUM
eurjchem-610	48	34	nmr	nmr	NOUN
eurjchem-610	48	35	spectroscopy	spectroscopy	NOUN
eurjchem-610	48	36	.	.	PUNCT
eurjchem-610	49	1	heteropolyanion	heteropolyanion	NOUN
eurjchem-610	49	2	potassium	potassium	NOUN
eurjchem-610	49	3	salt	salt	NOUN
eurjchem-610	49	4	(	(	PUNCT
eurjchem-610	49	5	10	10	NUM
eurjchem-610	49	6	g	g	NOUN
eurjchem-610	49	7	)	)	PUNCT
eurjchem-610	49	8	was	be	AUX
eurjchem-610	49	9	dissolved	dissolve	VERB
eurjchem-610	49	10	in	in	ADP
eurjchem-610	49	11	50	50	NUM
eurjchem-610	49	12	ml	ml	NOUN
eurjchem-610	49	13	of	of	ADP
eurjchem-610	49	14	hcl	hcl	PROPN
eurjchem-610	49	15	0.5	0.5	NUM
eurjchem-610	49	16	n.	n.	NOUN
eurjchem-610	49	17	to	to	ADP
eurjchem-610	49	18	the	the	DET
eurjchem-610	49	19	obtained	obtain	VERB
eurjchem-610	49	20	solution	solution	NOUN
eurjchem-610	49	21	,	,	PUNCT
eurjchem-610	49	22	we	we	PRON
eurjchem-610	49	23	added	add	VERB
eurjchem-610	49	24	30	30	NUM
eurjchem-610	49	25	ml	ml	NOUN
eurjchem-610	49	26	of	of	ADP
eurjchem-610	49	27	concentrated	concentrate	VERB
eurjchem-610	49	28	hcl	hcl	PROPN
eurjchem-610	49	29	(	(	PUNCT
eurjchem-610	49	30	d	d	NOUN
eurjchem-610	49	31	=	=	SYM
eurjchem-610	49	32	1.184	1.184	NUM
eurjchem-610	49	33	g	g	NOUN
eurjchem-610	49	34	/	/	SYM
eurjchem-610	49	35	cm3	cm3	NOUN
eurjchem-610	49	36	)	)	PUNCT
eurjchem-610	49	37	and	and	CCONJ
eurjchem-610	49	38	100	100	NUM
eurjchem-610	49	39	ml	ml	NOUN
eurjchem-610	49	40	of	of	ADP
eurjchem-610	49	41	ether	ether	NOUN
eurjchem-610	49	42	.	.	PUNCT
eurjchem-610	50	1	after	after	ADP
eurjchem-610	50	2	stirring	stirring	NOUN
eurjchem-610	50	3	,	,	PUNCT
eurjchem-610	50	4	the	the	DET
eurjchem-610	50	5	heavy	heavy	ADJ
eurjchem-610	50	6	phase	phase	NOUN
eurjchem-610	50	7	was	be	AUX
eurjchem-610	50	8	deposed	depose	VERB
eurjchem-610	50	9	in	in	ADP
eurjchem-610	50	10	decanted	decant	VERB
eurjchem-610	50	11	bulb	bulb	NOUN
eurjchem-610	50	12	.	.	PUNCT
eurjchem-610	51	1	the	the	DET
eurjchem-610	51	2	heteropolyacid	heteropolyacid	PROPN
eurjchem-610	51	3	was	be	AUX
eurjchem-610	51	4	extracted	extract	VERB
eurjchem-610	51	5	.	.	PUNCT
eurjchem-610	52	1	5ml	5ml	NOUN
eurjchem-610	52	2	of	of	ADP
eurjchem-610	52	3	water	water	NOUN
eurjchem-610	52	4	was	be	AUX
eurjchem-610	52	5	added	add	VERB
eurjchem-610	52	6	to	to	ADP
eurjchem-610	52	7	the	the	DET
eurjchem-610	52	8	heteropolyacid	heteropolyacid	ADJ
eurjchem-610	52	9	and	and	CCONJ
eurjchem-610	52	10	stirred	stir	VERB
eurjchem-610	52	11	.	.	PUNCT
eurjchem-610	53	1	the	the	DET
eurjchem-610	53	2	heteropolyacid	heteropolyacid	PROPN
eurjchem-610	53	3	was	be	AUX
eurjchem-610	53	4	obtained	obtain	VERB
eurjchem-610	53	5	by	by	ADP
eurjchem-610	53	6	vapour	vapour	NOUN
eurjchem-610	53	7	diffusion	diffusion	NOUN
eurjchem-610	53	8	over	over	ADP
eurjchem-610	53	9	a	a	DET
eurjchem-610	53	10	period	period	NOUN
eurjchem-610	53	11	of	of	ADP
eurjchem-610	53	12	3	3	NUM
eurjchem-610	53	13	days	day	NOUN
eurjchem-610	53	14	.	.	PUNCT
eurjchem-610	54	1	2.1.1	2.1.1	X
eurjchem-610	54	2	.	.	X
eurjchem-610	54	3	n2‐boc‐4‐alkyle‐n5‐benzyl‐1,2,5‐thiadiazolidine	n2‐boc‐4‐alkyle‐n5‐benzyl‐1,2,5‐thiadiazolidine	PROPN
eurjchem-610	54	4	1,1‐	1,1‐	NUM
eurjchem-610	54	5	dioxide	dioxide	NOUN
eurjchem-610	54	6	(	(	PUNCT
eurjchem-610	54	7	1‐5	1‐5	NUM
eurjchem-610	54	8	)	)	PUNCT
eurjchem-610	54	9	the	the	DET
eurjchem-610	54	10	synthesis	synthesis	NOUN
eurjchem-610	54	11	of	of	ADP
eurjchem-610	54	12	the	the	DET
eurjchem-610	54	13	compounds	compound	NOUN
eurjchem-610	54	14	,	,	PUNCT
eurjchem-610	54	15	starting	start	VERB
eurjchem-610	54	16	from	from	ADP
eurjchem-610	54	17	chlorosulfonyl	chlorosulfonyl	ADJ
eurjchem-610	54	18	isocyanate	isocyanate	NOUN
eurjchem-610	54	19	(	(	PUNCT
eurjchem-610	54	20	csi	csi	PROPN
eurjchem-610	54	21	)	)	PUNCT
eurjchem-610	54	22	,	,	PUNCT
eurjchem-610	54	23	tert‐butyl	tert‐butyl	ADP
eurjchem-610	54	24	alcohol	alcohol	NOUN
eurjchem-610	54	25	and	and	CCONJ
eurjchem-610	54	26	methyl	methyl	NOUN
eurjchem-610	54	27	esters	ester	NOUN
eurjchem-610	54	28	of	of	ADP
eurjchem-610	54	29	amino	amino	ADJ
eurjchem-610	54	30	acids	acid	NOUN
eurjchem-610	54	31	(	(	PUNCT
eurjchem-610	54	32	gylcine	gylcine	NOUN
eurjchem-610	54	33	,	,	PUNCT
eurjchem-610	54	34	l‐alanine	l‐alanine	X
eurjchem-610	54	35	,	,	PUNCT
eurjchem-610	54	36	l‐leucine	l‐leucine	PUNCT
eurjchem-610	54	37	and	and	CCONJ
eurjchem-610	54	38	l‐	l‐	PROPN
eurjchem-610	54	39	phenyalanine	phenyalanine	NOUN
eurjchem-610	54	40	)	)	PUNCT
eurjchem-610	54	41	has	have	AUX
eurjchem-610	54	42	been	be	AUX
eurjchem-610	54	43	previously	previously	ADV
eurjchem-610	54	44	reported	report	VERB
eurjchem-610	54	45	[	[	X
eurjchem-610	54	46	21	21	NUM
eurjchem-610	54	47	]	]	PUNCT
eurjchem-610	54	48	.	.	PUNCT
eurjchem-610	55	1	2.1.2	2.1.2	X
eurjchem-610	55	2	.	.	X
eurjchem-610	55	3	synthesis	synthesis	NOUN
eurjchem-610	55	4	of	of	ADP
eurjchem-610	55	5	compounds	compound	NOUN
eurjchem-610	55	6	1a‐5a	1a‐5a	NUM
eurjchem-610	55	7	n2‐boc‐4‐alkyle‐n5‐benzyl‐1,2,5‐thiadiazolidine	n2‐boc‐4‐alkyle‐n5‐benzyl‐1,2,5‐thiadiazolidine	NOUN
eurjchem-610	55	8	1,1‐	1,1‐	NUM
eurjchem-610	55	9	dioxide	dioxide	NOUN
eurjchem-610	55	10	(	(	PUNCT
eurjchem-610	55	11	1	1	NUM
eurjchem-610	55	12	mmol	mmol	NOUN
eurjchem-610	55	13	)	)	PUNCT
eurjchem-610	55	14	was	be	AUX
eurjchem-610	55	15	dissolved	dissolve	VERB
eurjchem-610	55	16	in	in	ADP
eurjchem-610	55	17	ch2cl2	ch2cl2	PROPN
eurjchem-610	55	18	,	,	PUNCT
eurjchem-610	55	19	10	10	NUM
eurjchem-610	55	20	%	%	NOUN
eurjchem-610	55	21	of	of	ADP
eurjchem-610	55	22	heteropolyacid	heteropolyacid	ADJ
eurjchem-610	55	23	catalyst	catalyst	NOUN
eurjchem-610	55	24	was	be	AUX
eurjchem-610	55	25	added	add	VERB
eurjchem-610	55	26	and	and	CCONJ
eurjchem-610	55	27	the	the	DET
eurjchem-610	55	28	mixture	mixture	NOUN
eurjchem-610	55	29	was	be	AUX
eurjchem-610	55	30	stirred	stir	VERB
eurjchem-610	55	31	at	at	ADP
eurjchem-610	55	32	room	room	NOUN
eurjchem-610	55	33	temperature	temperature	NOUN
eurjchem-610	55	34	for	for	ADP
eurjchem-610	55	35	a	a	DET
eurjchem-610	55	36	few	few	ADJ
eurjchem-610	55	37	minutes	minute	NOUN
eurjchem-610	55	38	.	.	PUNCT
eurjchem-610	56	1	the	the	DET
eurjchem-610	56	2	suspension	suspension	NOUN
eurjchem-610	56	3	was	be	AUX
eurjchem-610	56	4	filtered	filter	VERB
eurjchem-610	56	5	,	,	PUNCT
eurjchem-610	56	6	the	the	DET
eurjchem-610	56	7	solution	solution	NOUN
eurjchem-610	56	8	was	be	AUX
eurjchem-610	56	9	dried	dry	VERB
eurjchem-610	56	10	over	over	ADP
eurjchem-610	56	11	anhydrous	anhydrous	ADJ
eurjchem-610	56	12	na2so4	na2so4	NOUN
eurjchem-610	56	13	,	,	PUNCT
eurjchem-610	56	14	filtered	filter	VERB
eurjchem-610	56	15	and	and	CCONJ
eurjchem-610	56	16	concentrated	concentrate	VERB
eurjchem-610	56	17	under	under	ADP
eurjchem-610	56	18	vacuum	vacuum	NOUN
eurjchem-610	56	19	,	,	PUNCT
eurjchem-610	56	20	and	and	CCONJ
eurjchem-610	56	21	the	the	DET
eurjchem-610	56	22	crude	crude	ADJ
eurjchem-610	56	23	product	product	NOUN
eurjchem-610	56	24	was	be	AUX
eurjchem-610	56	25	subjected	subject	VERB
eurjchem-610	56	26	to	to	ADP
eurjchem-610	56	27	column	column	NOUN
eurjchem-610	56	28	chromatography	chromatography	NOUN
eurjchem-610	56	29	(	(	PUNCT
eurjchem-610	56	30	dcm	dcm	PROPN
eurjchem-610	56	31	:	:	PUNCT
eurjchem-610	56	32	meoh	meoh	PROPN
eurjchem-610	56	33	,	,	PUNCT
eurjchem-610	56	34	9:1	9:1	NUM
eurjchem-610	56	35	)	)	PUNCT
eurjchem-610	56	36	.	.	PUNCT
eurjchem-610	57	1	deprotected	deprotecte	VERB
eurjchem-610	57	2	compounds	compound	NOUN
eurjchem-610	57	3	(	(	PUNCT
eurjchem-610	57	4	1a‐5a	1a‐5a	NUM
eurjchem-610	57	5	)	)	PUNCT
eurjchem-610	57	6	were	be	AUX
eurjchem-610	57	7	obtained	obtain	VERB
eurjchem-610	57	8	in	in	ADP
eurjchem-610	57	9	90‐95	90‐95	NUM
eurjchem-610	57	10	%	%	NOUN
eurjchem-610	57	11	yield	yield	NOUN
eurjchem-610	57	12	.	.	PUNCT
eurjchem-610	58	1	the	the	DET
eurjchem-610	58	2	heteropolyacid	heteropolyacid	PROPN
eurjchem-610	58	3	was	be	AUX
eurjchem-610	58	4	recuperated	recuperate	VERB
eurjchem-610	58	5	by	by	ADP
eurjchem-610	58	6	filtration	filtration	NOUN
eurjchem-610	58	7	and	and	CCONJ
eurjchem-610	58	8	used	use	VERB
eurjchem-610	58	9	again	again	ADV
eurjchem-610	58	10	(	(	PUNCT
eurjchem-610	58	11	scheme	scheme	NOUN
eurjchem-610	58	12	1	1	NUM
eurjchem-610	58	13	)	)	PUNCT
eurjchem-610	58	14	.	.	PUNCT
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eurjchem-610	59	4	1a	1a	NUM
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eurjchem-610	60	4	(	(	PUNCT
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eurjchem-610	60	8	,	,	PUNCT
eurjchem-610	60	9	95:5	95:5	NUM
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eurjchem-610	60	11	.	.	PUNCT
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eurjchem-610	61	2	.	.	PROPN
eurjchem-610	61	3	:	:	PUNCT
eurjchem-610	62	1	98‐100	98‐100	NUM
eurjchem-610	62	2	°	°	SYM
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eurjchem-610	62	4	.	.	PUNCT
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eurjchem-610	63	3	kbr	kbr	PROPN
eurjchem-610	63	4	,	,	PUNCT
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eurjchem-610	63	6	):	):	PUNCT
eurjchem-610	63	7	3267	3267	NUM
eurjchem-610	63	8	,	,	PUNCT
eurjchem-610	63	9	3335	3335	NUM
eurjchem-610	63	10	,	,	PUNCT
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eurjchem-610	63	12	(nh	(nh	PROPN
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eurjchem-610	63	14	,	,	PUNCT
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eurjchem-610	63	16	,	,	PUNCT
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eurjchem-610	63	18	(so2	(so2	NOUN
eurjchem-610	63	19	)	)	PUNCT
eurjchem-610	63	20	.	.	PUNCT
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eurjchem-610	64	3	(	(	PUNCT
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eurjchem-610	64	6	,	,	PUNCT
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eurjchem-610	64	8	,	,	PUNCT
eurjchem-610	64	9	δ	δ	PROPN
eurjchem-610	64	10	,	,	PUNCT
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eurjchem-610	64	12	):	):	PUNCT
eurjchem-610	64	13	7.40	7.40	NUM
eurjchem-610	64	14	(	(	PUNCT
eurjchem-610	64	15	m	m	PROPN
eurjchem-610	64	16	,	,	PUNCT
eurjchem-610	64	17	5h	5h	NUM
eurjchem-610	64	18	,	,	PUNCT
eurjchem-610	64	19	arh	arh	PROPN
eurjchem-610	64	20	)	)	PUNCT
eurjchem-610	64	21	,	,	PUNCT
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eurjchem-610	64	23	(	(	PUNCT
eurjchem-610	64	24	t	t	PROPN
eurjchem-610	64	25	,	,	PUNCT
eurjchem-610	64	26	j	j	PROPN
eurjchem-610	64	27	=	=	SYM
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eurjchem-610	64	29	hz	hz	NOUN
eurjchem-610	64	30	,	,	PUNCT
eurjchem-610	64	31	1h	1h	NUM
eurjchem-610	64	32	,	,	PUNCT
eurjchem-610	64	33	nh	nh	PROPN
eurjchem-610	64	34	)	)	PUNCT
eurjchem-610	64	35	,	,	PUNCT
eurjchem-610	64	36	4.30	4.30	NUM
eurjchem-610	64	37	(	(	PUNCT
eurjchem-610	64	38	s	s	PROPN
eurjchem-610	64	39	,	,	PUNCT
eurjchem-610	64	40	2h	2h	NUM
eurjchem-610	64	41	,	,	PUNCT
eurjchem-610	64	42	phch2	phch2	PROPN
eurjchem-610	64	43	)	)	PUNCT
eurjchem-610	64	44	,	,	PUNCT
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eurjchem-610	64	47	t	t	PROPN
eurjchem-610	64	48	,	,	PUNCT
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eurjchem-610	64	50	=	=	PROPN
eurjchem-610	64	51	6.4	6.4	NUM
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eurjchem-610	64	53	,	,	PUNCT
eurjchem-610	64	54	2h	2h	NUM
eurjchem-610	64	55	,	,	PUNCT
eurjchem-610	64	56	ch2	ch2	PROPN
eurjchem-610	64	57	)	)	PUNCT
eurjchem-610	64	58	,	,	PUNCT
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eurjchem-610	65	3	(	(	PUNCT
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eurjchem-610	65	6	,	,	PUNCT
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eurjchem-610	65	9	δ	δ	PROPN
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eurjchem-610	65	14	,	,	PUNCT
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eurjchem-610	65	24	,	,	PUNCT
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eurjchem-610	65	26	.	.	PUNCT
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eurjchem-610	66	2	(	(	PUNCT
eurjchem-610	66	3	esi+	esi+	PROPN
eurjchem-610	66	4	,	,	PUNCT
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eurjchem-610	66	7	,	,	PUNCT
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eurjchem-610	66	11	,	,	PUNCT
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eurjchem-610	66	13	i	i	PRON
eurjchem-610	66	14	rel	rel	VERB
eurjchem-610	66	15	,	,	PUNCT
eurjchem-610	66	16	%	%	INTJ
eurjchem-610	66	17	)	)	PUNCT
eurjchem-610	66	18	):	):	PUNCT
eurjchem-610	66	19	213	213	NUM
eurjchem-610	67	1	[	[	X
eurjchem-610	67	2	m+h]+	m+h]+	X
eurjchem-610	67	3	(	(	PUNCT
eurjchem-610	67	4	100	100	NUM
eurjchem-610	67	5	)	)	PUNCT
eurjchem-610	67	6	,	,	PUNCT
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eurjchem-610	67	9	bn]+	bn]+	X
eurjchem-610	67	10	(	(	PUNCT
eurjchem-610	67	11	77	77	NUM
eurjchem-610	67	12	)	)	PUNCT
eurjchem-610	67	13	.	.	PUNCT
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eurjchem-610	68	2	.	.	PUNCT
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eurjchem-610	68	4	.	.	PUNCT
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eurjchem-610	69	3	:	:	PUNCT
eurjchem-610	69	4	c	c	X
eurjchem-610	69	5	,	,	PUNCT
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eurjchem-610	69	9	,	,	PUNCT
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eurjchem-610	69	13	,	,	PUNCT
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eurjchem-610	70	2	,	,	PUNCT
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eurjchem-610	70	5	h	h	NOUN
eurjchem-610	70	6	,	,	PUNCT
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eurjchem-610	70	10	,	,	PUNCT
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eurjchem-610	70	13	.	.	PUNCT
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eurjchem-610	71	5	,	,	PUNCT
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eurjchem-610	71	8	2a	2a	NUM
eurjchem-610	71	9	):	):	PUNCT
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eurjchem-610	72	2	=	=	NOUN
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eurjchem-610	72	4	(	(	PUNCT
eurjchem-610	72	5	ch2cl2	ch2cl2	NOUN
eurjchem-610	72	6	:	:	PUNCT
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eurjchem-610	72	8	,	,	PUNCT
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eurjchem-610	73	2	.	.	PROPN
eurjchem-610	73	3	:	:	PUNCT
eurjchem-610	74	1	100‐102	100‐102	NUM
eurjchem-610	74	2	°	°	SYM
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eurjchem-610	74	4	.	.	PUNCT
eurjchem-610	75	1	[	[	X
eurjchem-610	75	2	α]d	α]d	X
eurjchem-610	75	3	=	=	SYM
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eurjchem-610	75	6	(	(	PUNCT
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eurjchem-610	75	8	=	=	SYM
eurjchem-610	75	9	1	1	NUM
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eurjchem-610	75	11	chcl3	chcl3	PROPN
eurjchem-610	75	12	)	)	PUNCT
eurjchem-610	75	13	.	.	PUNCT
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eurjchem-610	76	2	(	(	PUNCT
eurjchem-610	76	3	kbr	kbr	PROPN
eurjchem-610	76	4	,	,	PUNCT
eurjchem-610	76	5	cm‐1	cm‐1	PROPN
eurjchem-610	76	6	):	):	PUNCT
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eurjchem-610	76	8	,	,	PUNCT
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eurjchem-610	76	10	,	,	PUNCT
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eurjchem-610	76	20	.	.	PUNCT
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eurjchem-610	77	3	(	(	PUNCT
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eurjchem-610	77	8	,	,	PUNCT
eurjchem-610	77	9	δ	δ	PROPN
eurjchem-610	77	10	,	,	PUNCT
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eurjchem-610	77	12	):	):	PUNCT
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eurjchem-610	77	20	)	)	PUNCT
eurjchem-610	77	21	,	,	PUNCT
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eurjchem-610	77	25	,	,	PUNCT
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eurjchem-610	77	27	=	=	SYM
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eurjchem-610	77	30	,	,	PUNCT
eurjchem-610	77	31	1h	1h	NUM
eurjchem-610	77	32	,	,	PUNCT
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eurjchem-610	77	34	)	)	PUNCT
eurjchem-610	77	35	,	,	PUNCT
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eurjchem-610	77	38	d	d	PROPN
eurjchem-610	77	39	,	,	PUNCT
eurjchem-610	77	40	1h	1h	NUM
eurjchem-610	77	41	,	,	PUNCT
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eurjchem-610	77	43	=	=	SYM
eurjchem-610	77	44	15.2	15.2	NUM
eurjchem-610	77	45	hz	hz	NOUN
eurjchem-610	77	46	,	,	PUNCT
eurjchem-610	77	47	phch2	phch2	PROPN
eurjchem-610	77	48	)	)	PUNCT
eurjchem-610	77	49	,	,	PUNCT
eurjchem-610	77	50	4.10	4.10	NUM
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eurjchem-610	77	52	d	d	PROPN
eurjchem-610	77	53	,	,	PUNCT
eurjchem-610	77	54	1h	1h	NUM
eurjchem-610	77	55	,	,	PUNCT
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eurjchem-610	77	57	=	=	PROPN
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eurjchem-610	77	60	,	,	PUNCT
eurjchem-610	77	61	phch2	phch2	PROPN
eurjchem-610	77	62	)	)	PUNCT
eurjchem-610	77	63	,	,	PUNCT
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eurjchem-610	77	71	)	)	PUNCT
eurjchem-610	77	72	,	,	PUNCT
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eurjchem-610	77	77	1h	1h	NUM
eurjchem-610	77	78	,	,	PUNCT
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eurjchem-610	77	81	,	,	PUNCT
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eurjchem-610	77	84	d	d	PROPN
eurjchem-610	77	85	,	,	PUNCT
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eurjchem-610	77	87	=	=	SYM
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eurjchem-610	77	90	,	,	PUNCT
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eurjchem-610	77	92	,	,	PUNCT
eurjchem-610	77	93	ch3	ch3	PROPN
eurjchem-610	77	94	)	)	PUNCT
eurjchem-610	77	95	.	.	PUNCT
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eurjchem-610	78	3	(	(	PUNCT
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eurjchem-610	78	6	,	,	PUNCT
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eurjchem-610	78	8	,	,	PUNCT
eurjchem-610	78	9	δ	δ	PROPN
eurjchem-610	78	10	,	,	PUNCT
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eurjchem-610	78	12	):	):	PUNCT
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eurjchem-610	78	14	,	,	PUNCT
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eurjchem-610	78	16	,	,	PUNCT
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eurjchem-610	78	18	,	,	PUNCT
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eurjchem-610	78	20	,	,	PUNCT
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eurjchem-610	78	22	,	,	PUNCT
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eurjchem-610	78	24	,	,	PUNCT
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eurjchem-610	78	26	,	,	PUNCT
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eurjchem-610	79	2	(	(	PUNCT
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eurjchem-610	79	4	,	,	PUNCT
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eurjchem-610	79	7	,	,	PUNCT
eurjchem-610	79	8	m	m	PROPN
eurjchem-610	79	9	/	/	SYM
eurjchem-610	79	10	z	z	NOUN
eurjchem-610	79	11	,	,	PUNCT
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eurjchem-610	79	13	i	i	PRON
eurjchem-610	79	14	rel	rel	VERB
eurjchem-610	79	15	,	,	PUNCT
eurjchem-610	79	16	%	%	NOUN
eurjchem-610	79	17	)	)	PUNCT
eurjchem-610	79	18	):	):	PUNCT
eurjchem-610	79	19	227	227	NUM
eurjchem-610	79	20	[	[	X
eurjchem-610	79	21	m+h]+	m+h]+	X
eurjchem-610	79	22	(	(	PUNCT
eurjchem-610	79	23	100	100	NUM
eurjchem-610	79	24	)	)	PUNCT
eurjchem-610	79	25	.	.	PUNCT
eurjchem-610	80	1	anal	anal	PROPN
eurjchem-610	80	2	.	.	PUNCT
eurjchem-610	80	3	calcd	calcd	NOUN
eurjchem-610	80	4	.	.	PUNCT
eurjchem-610	81	1	for	for	SCONJ
eurjchem-610	81	2	c10h14n2o2s	c10h14n2o2s	PROPN
eurjchem-610	81	3	:	:	PUNCT
eurjchem-610	81	4	c	c	X
eurjchem-610	81	5	,	,	PUNCT
eurjchem-610	81	6	53.09	53.09	NUM
eurjchem-610	81	7	;	;	PUNCT
eurjchem-610	81	8	h	h	NOUN
eurjchem-610	81	9	,	,	PUNCT
eurjchem-610	81	10	6.19	6.19	NUM
eurjchem-610	81	11	;	;	PUNCT
eurjchem-610	81	12	n	n	CCONJ
eurjchem-610	81	13	,	,	PUNCT
eurjchem-610	81	14	12.39	12.39	NUM
eurjchem-610	81	15	.	.	PUNCT
eurjchem-610	81	16	found	find	VERB
eurjchem-610	81	17	:	:	PUNCT
eurjchem-610	82	1	c	c	X
eurjchem-610	82	2	,	,	PUNCT
eurjchem-610	82	3	53.00	53.00	NUM
eurjchem-610	82	4	;	;	PUNCT
eurjchem-610	82	5	h	h	NOUN
eurjchem-610	82	6	,	,	PUNCT
eurjchem-610	82	7	6.23	6.23	NUM
eurjchem-610	82	8	;	;	PUNCT
eurjchem-610	82	9	n	n	CCONJ
eurjchem-610	82	10	,	,	PUNCT
eurjchem-610	82	11	12.31	12.31	NUM
eurjchem-610	82	12	%	%	NOUN
eurjchem-610	82	13	.	.	PUNCT
eurjchem-610	83	1	n5‐benzyl‐4‐isopropyl	n5‐benzyl‐4‐isopropyl	PROPN
eurjchem-610	84	1	1	1	NUM
eurjchem-610	84	2	,	,	PUNCT
eurjchem-610	84	3	2	2	NUM
eurjchem-610	84	4	,	,	PUNCT
eurjchem-610	84	5	5‐thiadiazolidine	5‐thiadiazolidine	NUM
eurjchem-610	84	6	1,1‐dioxide	1,1‐dioxide	NUM
eurjchem-610	84	7	(	(	PUNCT
eurjchem-610	84	8	3a	3a	NUM
eurjchem-610	84	9	):	):	PUNCT
eurjchem-610	84	10	yield	yield	NOUN
eurjchem-610	84	11	:	:	PUNCT
eurjchem-610	84	12	96	96	NUM
eurjchem-610	84	13	%	%	NOUN
eurjchem-610	84	14	.	.	PUNCT
eurjchem-610	85	1	rf	rf	NOUN
eurjchem-610	85	2	=	=	NOUN
eurjchem-610	85	3	0.62	0.62	NUM
eurjchem-610	85	4	(	(	PUNCT
eurjchem-610	85	5	ch2cl2	ch2cl2	NOUN
eurjchem-610	85	6	:	:	PUNCT
eurjchem-610	85	7	meoh	meoh	NOUN
eurjchem-610	85	8	,	,	PUNCT
eurjchem-610	85	9	95:5	95:5	NUM
eurjchem-610	85	10	)	)	PUNCT
eurjchem-610	85	11	.	.	PUNCT
eurjchem-610	86	1	m.p	m.p	PROPN
eurjchem-610	86	2	.	.	PROPN
eurjchem-610	86	3	:	:	PUNCT
eurjchem-610	87	1	104‐106	104‐106	NUM
eurjchem-610	87	2	°	°	SYM
eurjchem-610	87	3	c	c	NOUN
eurjchem-610	87	4	.	.	PUNCT
eurjchem-610	88	1	[	[	X
eurjchem-610	88	2	α]d	α]d	NOUN
eurjchem-610	88	3	=	=	SYM
eurjchem-610	88	4	+23	+23	X
eurjchem-610	88	5	°	°	NOUN
eurjchem-610	88	6	(	(	PUNCT
eurjchem-610	88	7	c	c	NOUN
eurjchem-610	88	8	=	=	SYM
eurjchem-610	88	9	1	1	NUM
eurjchem-610	88	10	,	,	PUNCT
eurjchem-610	88	11	etoh	etoh	NOUN
eurjchem-610	88	12	)	)	PUNCT
eurjchem-610	88	13	.	.	PUNCT
eurjchem-610	89	1	ft‐ir	ft‐ir	NOUN
eurjchem-610	89	2	(	(	PUNCT
eurjchem-610	89	3	kbr	kbr	PROPN
eurjchem-610	89	4	,	,	PUNCT
eurjchem-610	89	5	cm‐1	cm‐1	PROPN
eurjchem-610	89	6	):	):	PUNCT
eurjchem-610	89	7	3331	3331	NUM
eurjchem-610	89	8	,	,	PUNCT
eurjchem-610	89	9	3314	3314	NUM
eurjchem-610	89	10	,	,	PUNCT
eurjchem-610	89	11	3252	3252	NUM
eurjchem-610	89	12	(nh	(nh	NOUN
eurjchem-610	89	13	)	)	PUNCT
eurjchem-610	89	14	,	,	PUNCT
eurjchem-610	89	15	1345	1345	NUM
eurjchem-610	89	16	and	and	CCONJ
eurjchem-610	89	17	1165	1165	NUM
eurjchem-610	89	18	(so2	(so2	NUM
eurjchem-610	89	19	)	)	PUNCT
eurjchem-610	89	20	.	.	PUNCT
eurjchem-610	90	1	1h	1h	NUM
eurjchem-610	90	2	nmr	nmr	NOUN
eurjchem-610	90	3	(	(	PUNCT
eurjchem-610	90	4	250	250	NUM
eurjchem-610	90	5	mhz	mhz	NOUN
eurjchem-610	90	6	,	,	PUNCT
eurjchem-610	90	7	cdcl3	cdcl3	PROPN
eurjchem-610	90	8	,	,	PUNCT
eurjchem-610	90	9	δ	δ	PROPN
eurjchem-610	90	10	,	,	PUNCT
eurjchem-610	90	11	ppm	ppm	NUM
eurjchem-610	90	12	):	):	PUNCT
eurjchem-610	90	13	7.40	7.40	NUM
eurjchem-610	90	14	(	(	PUNCT
eurjchem-610	90	15	m	m	PROPN
eurjchem-610	90	16	,	,	PUNCT
eurjchem-610	90	17	5h	5h	NUM
eurjchem-610	90	18	,	,	PUNCT
eurjchem-610	90	19	arh	arh	PROPN
eurjchem-610	90	20	)	)	PUNCT
eurjchem-610	90	21	,	,	PUNCT
eurjchem-610	90	22	4.88	4.88	NUM
eurjchem-610	90	23	(	(	PUNCT
eurjchem-610	90	24	s	s	PROPN
eurjchem-610	90	25	,	,	PUNCT
eurjchem-610	90	26	1h	1h	NUM
eurjchem-610	90	27	,	,	PUNCT
eurjchem-610	90	28	nh	nh	PROPN
eurjchem-610	90	29	)	)	PUNCT
eurjchem-610	90	30	,	,	PUNCT
eurjchem-610	90	31	4.35	4.35	NUM
eurjchem-610	90	32	(	(	PUNCT
eurjchem-610	90	33	d	d	PROPN
eurjchem-610	90	34	,	,	PUNCT
eurjchem-610	90	35	j	j	PROPN
eurjchem-610	90	36	=	=	SYM
eurjchem-610	90	37	13.8	13.8	NUM
eurjchem-610	90	38	hz	hz	NOUN
eurjchem-610	90	39	,	,	PUNCT
eurjchem-610	90	40	1h	1h	NUM
eurjchem-610	90	41	,	,	PUNCT
eurjchem-610	90	42	ch2‐ph	ch2‐ph	PROPN
eurjchem-610	90	43	)	)	PUNCT
eurjchem-610	90	44	,	,	PUNCT
eurjchem-610	90	45	3.95	3.95	NUM
eurjchem-610	90	46	(	(	PUNCT
eurjchem-610	90	47	d	d	PROPN
eurjchem-610	90	48	,	,	PUNCT
eurjchem-610	90	49	j	j	PROPN
eurjchem-610	90	50	=	=	SYM
eurjchem-610	90	51	13.8	13.8	NUM
eurjchem-610	90	52	hz	hz	NOUN
eurjchem-610	90	53	,	,	PUNCT
eurjchem-610	90	54	1h	1h	NUM
eurjchem-610	90	55	,	,	PUNCT
eurjchem-610	90	56	ch2‐ph	ch2‐ph	PROPN
eurjchem-610	90	57	)	)	PUNCT
eurjchem-610	90	58	,	,	PUNCT
eurjchem-610	90	59	3.40	3.40	NUM
eurjchem-610	90	60	(	(	PUNCT
eurjchem-610	90	61	m	m	PROPN
eurjchem-610	90	62	,	,	PUNCT
eurjchem-610	90	63	3h	3h	NUM
eurjchem-610	90	64	,	,	PUNCT
eurjchem-610	90	65	*	*	PUNCT
eurjchem-610	90	66	ch	ch	NOUN
eurjchem-610	90	67	and	and	CCONJ
eurjchem-610	90	68	ch2	ch2	PROPN
eurjchem-610	90	69	)	)	PUNCT
eurjchem-610	90	70	,	,	PUNCT
eurjchem-610	90	71	2.8	2.8	NUM
eurjchem-610	90	72	(	(	PUNCT
eurjchem-610	90	73	m	m	PROPN
eurjchem-610	90	74	,	,	PUNCT
eurjchem-610	90	75	1h	1h	NUM
eurjchem-610	90	76	,	,	PUNCT
eurjchem-610	90	77	ch	ch	NOUN
eurjchem-610	90	78	ipr	ipr	PROPN
eurjchem-610	90	79	)	)	PUNCT
eurjchem-610	90	80	,	,	PUNCT
eurjchem-610	90	81	0.90	0.90	NUM
eurjchem-610	90	82	and	and	CCONJ
eurjchem-610	90	83	1.00	1.00	NUM
eurjchem-610	90	84	(	(	PUNCT
eurjchem-610	90	85	2d	2d	NUM
eurjchem-610	90	86	,	,	PUNCT
eurjchem-610	90	87	j	j	PROPN
eurjchem-610	91	1	=	=	PROPN
eurjchem-610	91	2	6.7	6.7	NUM
eurjchem-610	91	3	hz	hz	NOUN
eurjchem-610	91	4	,	,	PUNCT
eurjchem-610	91	5	6h	6h	NUM
eurjchem-610	91	6	,	,	PUNCT
eurjchem-610	91	7	2ch3	2ch3	NUM
eurjchem-610	91	8	)	)	PUNCT
eurjchem-610	91	9	.	.	PUNCT
eurjchem-610	92	1	13c	13c	NOUN
eurjchem-610	92	2	nmr	nmr	NOUN
eurjchem-610	92	3	(	(	PUNCT
eurjchem-610	92	4	62.89	62.89	NUM
eurjchem-610	92	5	mhz	mhz	NOUN
eurjchem-610	92	6	,	,	PUNCT
eurjchem-610	92	7	cdcl3	cdcl3	PROPN
eurjchem-610	92	8	,	,	PUNCT
eurjchem-610	92	9	δ	δ	PROPN
eurjchem-610	92	10	,	,	PUNCT
eurjchem-610	92	11	ppm	ppm	NOUN
eurjchem-610	92	12	):	):	PUNCT
eurjchem-610	92	13	139.2	139.2	NUM
eurjchem-610	92	14	,	,	PUNCT
eurjchem-610	92	15	128.3	128.3	NUM
eurjchem-610	92	16	,	,	PUNCT
eurjchem-610	92	17	129.4	129.4	NUM
eurjchem-610	92	18	,	,	PUNCT
eurjchem-610	92	19	12.5	12.5	NUM
eurjchem-610	92	20	,	,	PUNCT
eurjchem-610	92	21	51.2	51.2	NUM
eurjchem-610	92	22	,	,	PUNCT
eurjchem-610	92	23	50.6	50.6	NUM
eurjchem-610	92	24	,	,	PUNCT
eurjchem-610	92	25	32.3	32.3	NUM
eurjchem-610	92	26	,	,	PUNCT
eurjchem-610	92	27	23.5	23.5	NUM
eurjchem-610	92	28	,	,	PUNCT
eurjchem-610	92	29	19.4	19.4	NUM
eurjchem-610	92	30	,	,	PUNCT
eurjchem-610	92	31	18.2	18.2	NUM
eurjchem-610	92	32	.	.	PUNCT
eurjchem-610	93	1	ms	ms	NOUN
eurjchem-610	93	2	(	(	PUNCT
eurjchem-610	93	3	esi+	esi+	PROPN
eurjchem-610	93	4	,	,	PUNCT
eurjchem-610	93	5	30	30	NUM
eurjchem-610	93	6	ev	ev	NOUN
eurjchem-610	93	7	,	,	PUNCT
eurjchem-610	93	8	m	m	PROPN
eurjchem-610	93	9	/	/	SYM
eurjchem-610	93	10	z	z	NOUN
eurjchem-610	93	11	,	,	PUNCT
eurjchem-610	93	12	(	(	PUNCT
eurjchem-610	93	13	i	i	PRON
eurjchem-610	93	14	rel	rel	VERB
eurjchem-610	93	15	,	,	PUNCT
eurjchem-610	93	16	%	%	INTJ
eurjchem-610	93	17	)	)	PUNCT
eurjchem-610	93	18	):	):	PUNCT
eurjchem-610	93	19	255	255	NUM
eurjchem-610	94	1	[	[	X
eurjchem-610	94	2	m+h]+	m+h]+	X
eurjchem-610	94	3	(	(	PUNCT
eurjchem-610	94	4	72	72	NUM
eurjchem-610	94	5	)	)	PUNCT
eurjchem-610	94	6	,	,	PUNCT
eurjchem-610	94	7	91	91	NUM
eurjchem-610	94	8	[	[	X
eurjchem-610	94	9	bn]+	bn]+	X
eurjchem-610	94	10	(	(	PUNCT
eurjchem-610	94	11	80	80	NUM
eurjchem-610	94	12	)	)	PUNCT
eurjchem-610	94	13	.	.	PUNCT
eurjchem-610	95	1	anal	anal	PROPN
eurjchem-610	95	2	.	.	PUNCT
eurjchem-610	95	3	calcd	calcd	NOUN
eurjchem-610	95	4	.	.	PUNCT
eurjchem-610	96	1	for	for	ADP
eurjchem-610	96	2	c12h18n2o2s	c12h18n2o2s	NUM
eurjchem-610	96	3	:	:	PUNCT
eurjchem-610	96	4	c	c	X
eurjchem-610	96	5	,	,	PUNCT
eurjchem-610	96	6	56.69	56.69	NUM
eurjchem-610	96	7	;	;	PUNCT
eurjchem-610	96	8	h	h	NOUN
eurjchem-610	96	9	,	,	PUNCT
eurjchem-610	96	10	7.08	7.08	NUM
eurjchem-610	96	11	;	;	PUNCT
eurjchem-610	96	12	n	n	CCONJ
eurjchem-610	96	13	,	,	PUNCT
eurjchem-610	96	14	11.02	11.02	NUM
eurjchem-610	96	15	.	.	PUNCT
eurjchem-610	96	16	found	find	VERB
eurjchem-610	96	17	:	:	PUNCT
eurjchem-610	97	1	c	c	X
eurjchem-610	97	2	,	,	PUNCT
eurjchem-610	97	3	56.67	56.67	NUM
eurjchem-610	97	4	;	;	PUNCT
eurjchem-610	97	5	h	h	NOUN
eurjchem-610	97	6	,	,	PUNCT
eurjchem-610	97	7	7.14	7.14	NUM
eurjchem-610	97	8	;	;	PUNCT
eurjchem-610	97	9	n	n	CCONJ
eurjchem-610	97	10	,	,	PUNCT
eurjchem-610	97	11	10.95	10.95	NUM
eurjchem-610	97	12	%	%	NOUN
eurjchem-610	97	13	.	.	PUNCT
eurjchem-610	98	1	n5‐benzyl‐4‐isobutyl	n5‐benzyl‐4‐isobutyl	PRON
eurjchem-610	98	2	1	1	NUM
eurjchem-610	98	3	,	,	PUNCT
eurjchem-610	98	4	2	2	NUM
eurjchem-610	98	5	,	,	PUNCT
eurjchem-610	98	6	5‐thiadiazolidine	5‐thiadiazolidine	NUM
eurjchem-610	98	7	1,1‐dioxide	1,1‐dioxide	NOUN
eurjchem-610	98	8	(	(	PUNCT
eurjchem-610	98	9	4a	4a	NOUN
eurjchem-610	98	10	):	):	PUNCT
eurjchem-610	98	11	yield	yield	NOUN
eurjchem-610	98	12	:	:	PUNCT
eurjchem-610	98	13	92	92	NUM
eurjchem-610	98	14	%	%	NOUN
eurjchem-610	98	15	.	.	PUNCT
eurjchem-610	99	1	rf	rf	NOUN
eurjchem-610	99	2	=	=	NOUN
eurjchem-610	99	3	0.60	0.60	NUM
eurjchem-610	99	4	(	(	PUNCT
eurjchem-610	99	5	ch2cl2	ch2cl2	NOUN
eurjchem-610	99	6	:	:	PUNCT
eurjchem-610	99	7	meoh	meoh	NOUN
eurjchem-610	99	8	,	,	PUNCT
eurjchem-610	99	9	95:5	95:5	NUM
eurjchem-610	99	10	)	)	PUNCT
eurjchem-610	99	11	.	.	PUNCT
eurjchem-610	100	1	m.p	m.p	PROPN
eurjchem-610	100	2	.	.	PROPN
eurjchem-610	100	3	:	:	PUNCT
eurjchem-610	100	4	117‐119	117‐119	NUM
eurjchem-610	100	5	°	°	NUM
eurjchem-610	100	6	c	c	NOUN
eurjchem-610	100	7	.	.	PUNCT
eurjchem-610	101	1	[	[	X
eurjchem-610	101	2	α]d	α]d	X
eurjchem-610	101	3	=	=	SYM
eurjchem-610	101	4	+3	+3	PROPN
eurjchem-610	101	5	°	°	INTJ
eurjchem-610	101	6	(	(	PUNCT
eurjchem-610	101	7	c	c	NOUN
eurjchem-610	101	8	=	=	SYM
eurjchem-610	101	9	1	1	NUM
eurjchem-610	101	10	,	,	PUNCT
eurjchem-610	101	11	etoh	etoh	NOUN
eurjchem-610	101	12	)	)	PUNCT
eurjchem-610	101	13	.	.	PUNCT
eurjchem-610	102	1	ft‐ir	ft‐ir	NOUN
eurjchem-610	102	2	(	(	PUNCT
eurjchem-610	102	3	kbr	kbr	PROPN
eurjchem-610	102	4	,	,	PUNCT
eurjchem-610	102	5	cm‐1	cm‐1	PROPN
eurjchem-610	102	6	):	):	PUNCT
eurjchem-610	102	7	3327	3327	NUM
eurjchem-610	102	8	,	,	PUNCT
eurjchem-610	102	9	3242	3242	NUM
eurjchem-610	102	10	,	,	PUNCT
eurjchem-610	102	11	3273	3273	NUM
eurjchem-610	102	12	(nh	(nh	PROPN
eurjchem-610	102	13	)	)	PUNCT
eurjchem-610	102	14	,	,	PUNCT
eurjchem-610	102	15	1332	1332	NUM
eurjchem-610	102	16	,	,	PUNCT
eurjchem-610	102	17	1161	1161	NUM
eurjchem-610	102	18	(so2	(so2	NOUN
eurjchem-610	102	19	)	)	PUNCT
eurjchem-610	102	20	.	.	PUNCT
eurjchem-610	103	1	1h	1h	NUM
eurjchem-610	103	2	nmr	nmr	NOUN
eurjchem-610	103	3	(	(	PUNCT
eurjchem-610	103	4	250	250	NUM
eurjchem-610	103	5	mhz	mhz	NOUN
eurjchem-610	103	6	,	,	PUNCT
eurjchem-610	103	7	cdcl3	cdcl3	PROPN
eurjchem-610	103	8	,	,	PUNCT
eurjchem-610	103	9	δ	δ	PROPN
eurjchem-610	103	10	,	,	PUNCT
eurjchem-610	103	11	ppm	ppm	NUM
eurjchem-610	103	12	):	):	PUNCT
eurjchem-610	103	13	7.35	7.35	NUM
eurjchem-610	103	14	(	(	PUNCT
eurjchem-610	103	15	m	m	PROPN
eurjchem-610	103	16	,	,	PUNCT
eurjchem-610	103	17	5h	5h	NUM
eurjchem-610	103	18	,	,	PUNCT
eurjchem-610	103	19	arh	arh	PROPN
eurjchem-610	103	20	)	)	PUNCT
eurjchem-610	103	21	,	,	PUNCT
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eurjchem-610	103	23	(	(	PUNCT
eurjchem-610	103	24	d	d	PROPN
eurjchem-610	103	25	,	,	PUNCT
eurjchem-610	103	26	1h	1h	NUM
eurjchem-610	103	27	,	,	PUNCT
eurjchem-610	103	28	j	j	PROPN
eurjchem-610	103	29	=	=	SYM
eurjchem-610	103	30	7.4	7.4	NUM
eurjchem-610	103	31	hz	hz	NOUN
eurjchem-610	103	32	,	,	PUNCT
eurjchem-610	103	33	nh	nh	PROPN
eurjchem-610	103	34	)	)	PUNCT
eurjchem-610	103	35	,	,	PUNCT
eurjchem-610	103	36	4.35	4.35	NUM
eurjchem-610	103	37	(	(	PUNCT
eurjchem-610	103	38	d	d	PROPN
eurjchem-610	103	39	,	,	PUNCT
eurjchem-610	103	40	j	j	PROPN
eurjchem-610	104	1	=	=	SYM
eurjchem-610	104	2	13.8	13.8	NUM
eurjchem-610	104	3	hz	hz	NOUN
eurjchem-610	104	4	,	,	PUNCT
eurjchem-610	104	5	1h	1h	NUM
eurjchem-610	104	6	,	,	PUNCT
eurjchem-610	104	7	ch2‐ph	ch2‐ph	PROPN
eurjchem-610	104	8	)	)	PUNCT
eurjchem-610	104	9	,	,	PUNCT
eurjchem-610	104	10	4.10	4.10	NUM
eurjchem-610	104	11	(	(	PUNCT
eurjchem-610	104	12	d	d	PROPN
eurjchem-610	104	13	,	,	PUNCT
eurjchem-610	104	14	j	j	PROPN
eurjchem-610	105	1	=	=	SYM
eurjchem-610	105	2	13.8	13.8	NUM
eurjchem-610	105	3	hz	hz	NOUN
eurjchem-610	105	4	,	,	PUNCT
eurjchem-610	105	5	1h	1h	NUM
eurjchem-610	105	6	,	,	PUNCT
eurjchem-610	105	7	ch2‐ph	ch2‐ph	PROPN
eurjchem-610	105	8	)	)	PUNCT
eurjchem-610	105	9	,	,	PUNCT
eurjchem-610	105	10	3.80	3.80	NUM
eurjchem-610	105	11	(	(	PUNCT
eurjchem-610	105	12	m	m	PROPN
eurjchem-610	105	13	,	,	PUNCT
eurjchem-610	105	14	1h	1h	NUM
eurjchem-610	105	15	,	,	PUNCT
eurjchem-610	105	16	chasy	chasy	NOUN
eurjchem-610	105	17	)	)	PUNCT
eurjchem-610	105	18	,	,	PUNCT
eurjchem-610	105	19	2.90	2.90	NUM
eurjchem-610	105	20	(	(	PUNCT
eurjchem-610	105	21	dd	dd	PROPN
eurjchem-610	105	22	,	,	PUNCT
eurjchem-610	105	23	j	j	PROPN
eurjchem-610	105	24	=	=	PUNCT
eurjchem-610	105	25	j	j	PROPN
eurjchem-610	105	26	’	'	PUNCT
eurjchem-610	105	27	=	=	SYM
eurjchem-610	105	28	6.9	6.9	NUM
eurjchem-610	105	29	hz	hz	NOUN
eurjchem-610	105	30	,	,	PUNCT
eurjchem-610	105	31	1h	1h	NUM
eurjchem-610	105	32	,	,	PUNCT
eurjchem-610	105	33	ch2	ch2	PROPN
eurjchem-610	105	34	)	)	PUNCT
eurjchem-610	105	35	,	,	PUNCT
eurjchem-610	105	36	2.35	2.35	NUM
eurjchem-610	105	37	(	(	PUNCT
eurjchem-610	105	38	dd	dd	PROPN
eurjchem-610	105	39	,	,	PUNCT
eurjchem-610	105	40	j	j	PROPN
eurjchem-610	105	41	=	=	PUNCT
eurjchem-610	105	42	j	j	PROPN
eurjchem-610	105	43	’	'	PUNCT
eurjchem-610	105	44	=	=	SYM
eurjchem-610	105	45	6.9	6.9	NUM
eurjchem-610	105	46	hz	hz	NOUN
eurjchem-610	105	47	,	,	PUNCT
eurjchem-610	105	48	1h	1h	NUM
eurjchem-610	105	49	,	,	PUNCT
eurjchem-610	105	50	ch2	ch2	PROPN
eurjchem-610	105	51	)	)	PUNCT
eurjchem-610	105	52	,	,	PUNCT
eurjchem-610	105	53	1.60	1.60	NUM
eurjchem-610	105	54	(	(	PUNCT
eurjchem-610	105	55	m	m	PROPN
eurjchem-610	105	56	,	,	PUNCT
eurjchem-610	105	57	1h	1h	NUM
eurjchem-610	105	58	,	,	PUNCT
eurjchem-610	105	59	ch‐ibu	ch‐ibu	NOUN
eurjchem-610	105	60	)	)	PUNCT
eurjchem-610	105	61	,	,	PUNCT
eurjchem-610	105	62	1.45	1.45	NUM
eurjchem-610	105	63	(	(	PUNCT
eurjchem-610	105	64	m	m	PROPN
eurjchem-610	105	65	,	,	PUNCT
eurjchem-610	105	66	2h	2h	NUM
eurjchem-610	105	67	,	,	PUNCT
eurjchem-610	105	68	ch2	ch2	PROPN
eurjchem-610	105	69	)	)	PUNCT
eurjchem-610	105	70	,	,	PUNCT
eurjchem-610	105	71	0.90	0.90	NUM
eurjchem-610	105	72	and	and	CCONJ
eurjchem-610	105	73	0.95	0.95	NUM
eurjchem-610	105	74	(	(	PUNCT
eurjchem-610	105	75	2d	2d	NOUN
eurjchem-610	105	76	,	,	PUNCT
eurjchem-610	105	77	j	j	PROPN
eurjchem-610	106	1	=	=	SYM
eurjchem-610	106	2	6.2	6.2	NUM
eurjchem-610	106	3	hz	hz	NOUN
eurjchem-610	106	4	,	,	PUNCT
eurjchem-610	106	5	6h	6h	NUM
eurjchem-610	106	6	,	,	PUNCT
eurjchem-610	106	7	2ch3	2ch3	NUM
eurjchem-610	106	8	)	)	PUNCT
eurjchem-610	106	9	.	.	PUNCT
eurjchem-610	107	1	13c	13c	NOUN
eurjchem-610	107	2	nmr	nmr	NOUN
eurjchem-610	107	3	(	(	PUNCT
eurjchem-610	107	4	62.89	62.89	NUM
eurjchem-610	107	5	mhz	mhz	NOUN
eurjchem-610	107	6	,	,	PUNCT
eurjchem-610	107	7	cdcl3	cdcl3	PROPN
eurjchem-610	107	8	,	,	PUNCT
eurjchem-610	107	9	δ	δ	PROPN
eurjchem-610	107	10	,	,	PUNCT
eurjchem-610	107	11	ppm	ppm	NOUN
eurjchem-610	107	12	):	):	PUNCT
eurjchem-610	107	13	138.7	138.7	NUM
eurjchem-610	107	14	,	,	PUNCT
eurjchem-610	107	15	127.5	127.5	NUM
eurjchem-610	107	16	,	,	PUNCT
eurjchem-610	107	17	127.4	127.4	NUM
eurjchem-610	107	18	,	,	PUNCT
eurjchem-610	107	19	125.5	125.5	NUM
eurjchem-610	107	20	,	,	PUNCT
eurjchem-610	107	21	54.3	54.3	NUM
eurjchem-610	107	22	,	,	PUNCT
eurjchem-610	107	23	52.3	52.3	NUM
eurjchem-610	107	24	,	,	PUNCT
eurjchem-610	107	25	42.2	42.2	NUM
eurjchem-610	107	26	,	,	PUNCT
eurjchem-610	107	27	23.5	23.5	NUM
eurjchem-610	107	28	,	,	PUNCT
eurjchem-610	107	29	19.2	19.2	NUM
eurjchem-610	107	30	,	,	PUNCT
eurjchem-610	107	31	17.4	17.4	NUM
eurjchem-610	107	32	.	.	PUNCT
eurjchem-610	108	1	ms	ms	NOUN
eurjchem-610	108	2	(	(	PUNCT
eurjchem-610	108	3	esi+	esi+	PROPN
eurjchem-610	108	4	,	,	PUNCT
eurjchem-610	108	5	30	30	NUM
eurjchem-610	108	6	ev	ev	NOUN
eurjchem-610	108	7	,	,	PUNCT
eurjchem-610	108	8	m	m	PROPN
eurjchem-610	108	9	/	/	SYM
eurjchem-610	108	10	z	z	NOUN
eurjchem-610	108	11	,	,	PUNCT
eurjchem-610	108	12	(	(	PUNCT
eurjchem-610	108	13	i	i	PRON
eurjchem-610	108	14	rel	rel	VERB
eurjchem-610	108	15	,	,	PUNCT
eurjchem-610	108	16	%	%	NOUN
eurjchem-610	108	17	)	)	PUNCT
eurjchem-610	108	18	):	):	PUNCT
eurjchem-610	108	19	269	269	NUM
eurjchem-610	109	1	[	[	X
eurjchem-610	109	2	m+h]+	m+h]+	X
eurjchem-610	109	3	(	(	PUNCT
eurjchem-610	109	4	76	76	NUM
eurjchem-610	109	5	)	)	PUNCT
eurjchem-610	109	6	,	,	PUNCT
eurjchem-610	109	7	91[bn]+	91[bn]+	NUM
eurjchem-610	109	8	(	(	PUNCT
eurjchem-610	109	9	56	56	NUM
eurjchem-610	109	10	)	)	PUNCT
eurjchem-610	109	11	.	.	PUNCT
eurjchem-610	110	1	anal	anal	PROPN
eurjchem-610	110	2	.	.	PUNCT
eurjchem-610	110	3	calcd	calcd	NOUN
eurjchem-610	110	4	.	.	PUNCT
eurjchem-610	111	1	for	for	ADP
eurjchem-610	111	2	c13h20n2o2s	c13h20n2o2s	PROPN
eurjchem-610	111	3	:	:	PUNCT
eurjchem-610	111	4	c,58.21	c,58.21	NOUN
eurjchem-610	111	5	;	;	PUNCT
eurjchem-610	111	6	h	h	NOUN
eurjchem-610	111	7	,	,	PUNCT
eurjchem-610	111	8	7.46	7.46	NUM
eurjchem-610	111	9	;	;	PUNCT
eurjchem-610	111	10	n	n	CCONJ
eurjchem-610	111	11	,	,	PUNCT
eurjchem-610	111	12	10.45	10.45	NUM
eurjchem-610	111	13	.	.	PUNCT
eurjchem-610	111	14	found	find	VERB
eurjchem-610	111	15	:	:	PUNCT
eurjchem-610	112	1	c	c	X
eurjchem-610	112	2	,	,	PUNCT
eurjchem-610	112	3	58.31	58.31	NUM
eurjchem-610	112	4	;	;	PUNCT
eurjchem-610	112	5	h	h	NOUN
eurjchem-610	112	6	,	,	PUNCT
eurjchem-610	112	7	7.53	7.53	NUM
eurjchem-610	112	8	;	;	PUNCT
eurjchem-610	112	9	n	n	CCONJ
eurjchem-610	112	10	,	,	PUNCT
eurjchem-610	112	11	10.41	10.41	NUM
eurjchem-610	112	12	%	%	NOUN
eurjchem-610	112	13	.	.	PUNCT
eurjchem-610	113	1	n5‐3‐dibenzyl‐1,2,5‐thiadiazolidine	n5‐3‐dibenzyl‐1,2,5‐thiadiazolidine	ADJ
eurjchem-610	113	2	1,1‐dioxide	1,1‐dioxide	NUM
eurjchem-610	113	3	(	(	PUNCT
eurjchem-610	113	4	5a	5a	NUM
eurjchem-610	113	5	):	):	PUNCT
eurjchem-610	113	6	yield	yield	NOUN
eurjchem-610	113	7	:	:	PUNCT
eurjchem-610	113	8	93.2	93.2	NUM
eurjchem-610	113	9	%	%	NOUN
eurjchem-610	113	10	.	.	PUNCT
eurjchem-610	114	1	rf	rf	PRON
eurjchem-610	114	2	=	=	NOUN
eurjchem-610	114	3	0.52	0.52	NUM
eurjchem-610	114	4	(	(	PUNCT
eurjchem-610	114	5	ch2cl2	ch2cl2	NOUN
eurjchem-610	114	6	)	)	PUNCT
eurjchem-610	114	7	.	.	PUNCT
eurjchem-610	115	1	m.p	m.p	PROPN
eurjchem-610	115	2	.	.	PROPN
eurjchem-610	115	3	:	:	PUNCT
eurjchem-610	115	4	97‐98	97‐98	NUM
eurjchem-610	115	5	°	°	SYM
eurjchem-610	115	6	c	c	NOUN
eurjchem-610	115	7	.	.	PUNCT
eurjchem-610	116	1	[	[	X
eurjchem-610	116	2	α]d	α]d	NOUN
eurjchem-610	116	3	=	=	PUNCT
eurjchem-610	116	4	‐23	‐23	X
eurjchem-610	116	5	°	°	NOUN
eurjchem-610	116	6	(	(	PUNCT
eurjchem-610	116	7	c	c	NOUN
eurjchem-610	116	8	=	=	SYM
eurjchem-610	116	9	1	1	NUM
eurjchem-610	116	10	,	,	PUNCT
eurjchem-610	116	11	etoh	etoh	NOUN
eurjchem-610	116	12	)	)	PUNCT
eurjchem-610	116	13	.	.	PUNCT
eurjchem-610	117	1	ft‐ir	ft‐ir	NOUN
eurjchem-610	117	2	(	(	PUNCT
eurjchem-610	117	3	kbr	kbr	PROPN
eurjchem-610	117	4	,	,	PUNCT
eurjchem-610	117	5	cm‐1	cm‐1	PROPN
eurjchem-610	117	6	):	):	PUNCT
eurjchem-610	117	7	3269	3269	NUM
eurjchem-610	117	8	(nh	(nh	PROPN
eurjchem-610	117	9	)	)	PUNCT
eurjchem-610	117	10	,	,	PUNCT
eurjchem-610	117	11	1338	1338	NUM
eurjchem-610	117	12	,	,	PUNCT
eurjchem-610	117	13	1172	1172	NUM
eurjchem-610	117	14	(so2	(so2	NOUN
eurjchem-610	117	15	)	)	PUNCT
eurjchem-610	117	16	.	.	PUNCT
eurjchem-610	118	1	1h	1h	NUM
eurjchem-610	118	2	nmr	nmr	NOUN
eurjchem-610	118	3	(	(	PUNCT
eurjchem-610	118	4	250	250	NUM
eurjchem-610	118	5	mhz	mhz	NOUN
eurjchem-610	118	6	,	,	PUNCT
eurjchem-610	118	7	cdcl3	cdcl3	PROPN
eurjchem-610	118	8	,	,	PUNCT
eurjchem-610	118	9	δ	δ	PROPN
eurjchem-610	118	10	,	,	PUNCT
eurjchem-610	118	11	ppm	ppm	NOUN
eurjchem-610	118	12	):	):	PUNCT
eurjchem-610	118	13	7.52	7.52	NUM
eurjchem-610	118	14	(	(	PUNCT
eurjchem-610	118	15	m	m	PROPN
eurjchem-610	118	16	,	,	PUNCT
eurjchem-610	118	17	10h	10h	NUM
eurjchem-610	118	18	,	,	PUNCT
eurjchem-610	118	19	arh	arh	PROPN
eurjchem-610	118	20	)	)	PUNCT
eurjchem-610	118	21	,	,	PUNCT
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eurjchem-610	118	23	(	(	PUNCT
eurjchem-610	118	24	t	t	PROPN
eurjchem-610	118	25	,	,	PUNCT
eurjchem-610	118	26	j	j	PROPN
eurjchem-610	118	27	=	=	SYM
eurjchem-610	118	28	9.6	9.6	NUM
eurjchem-610	118	29	hz	hz	NOUN
eurjchem-610	118	30	,	,	PUNCT
eurjchem-610	118	31	1h	1h	NUM
eurjchem-610	118	32	,	,	PUNCT
eurjchem-610	118	33	nh	nh	PROPN
eurjchem-610	118	34	)	)	PUNCT
eurjchem-610	118	35	,	,	PUNCT
eurjchem-610	118	36	4.40	4.40	NUM
eurjchem-610	118	37	(	(	PUNCT
eurjchem-610	118	38	m	m	PROPN
eurjchem-610	118	39	,	,	PUNCT
eurjchem-610	118	40	1h	1h	NUM
eurjchem-610	118	41	,	,	PUNCT
eurjchem-610	118	42	chasy	chasy	NOUN
eurjchem-610	118	43	)	)	PUNCT
eurjchem-610	118	44	,	,	PUNCT
eurjchem-610	118	45	4.10	4.10	NUM
eurjchem-610	118	46	(	(	PUNCT
eurjchem-610	118	47	d	d	PROPN
eurjchem-610	118	48	,	,	PUNCT
eurjchem-610	118	49	j	j	PROPN
eurjchem-610	118	50	=	=	SYM
eurjchem-610	118	51	13.6	13.6	NUM
eurjchem-610	118	52	hz	hz	NOUN
eurjchem-610	118	53	,	,	PUNCT
eurjchem-610	118	54	1h	1h	NUM
eurjchem-610	118	55	,	,	PUNCT
eurjchem-610	118	56	ch2‐ph	ch2‐ph	PROPN
eurjchem-610	118	57	)	)	PUNCT
eurjchem-610	118	58	,	,	PUNCT
eurjchem-610	118	59	4.35	4.35	NUM
eurjchem-610	118	60	(	(	PUNCT
eurjchem-610	118	61	d	d	PROPN
eurjchem-610	118	62	,	,	PUNCT
eurjchem-610	118	63	j	j	PROPN
eurjchem-610	118	64	=	=	SYM
eurjchem-610	118	65	13.6	13.6	NUM
eurjchem-610	118	66	hz	hz	NOUN
eurjchem-610	118	67	,	,	PUNCT
eurjchem-610	118	68	1h	1h	NUM
eurjchem-610	118	69	,	,	PUNCT
eurjchem-610	118	70	ch2‐ph	ch2‐ph	PROPN
eurjchem-610	118	71	)	)	PUNCT
eurjchem-610	118	72	,	,	PUNCT
eurjchem-610	118	73	2.90	2.90	NUM
eurjchem-610	118	74	(	(	PUNCT
eurjchem-610	118	75	m	m	PROPN
eurjchem-610	118	76	,	,	PUNCT
eurjchem-610	118	77	2h	2h	NUM
eurjchem-610	118	78	,	,	PUNCT
eurjchem-610	118	79	ch2	ch2	PROPN
eurjchem-610	118	80	)	)	PUNCT
eurjchem-610	118	81	,	,	PUNCT
eurjchem-610	118	82	3.50	3.50	NUM
eurjchem-610	118	83	and	and	CCONJ
eurjchem-610	118	84	3.20	3.20	NUM
eurjchem-610	118	85	(	(	PUNCT
eurjchem-610	118	86	2dd	2dd	NOUN
eurjchem-610	118	87	,	,	PUNCT
eurjchem-610	118	88	,	,	PUNCT
eurjchem-610	118	89	j	j	PROPN
eurjchem-610	118	90	=	=	NOUN
eurjchem-610	118	91	18.3	18.3	NUM
eurjchem-610	118	92	,	,	PUNCT
eurjchem-610	118	93	j	j	NOUN
eurjchem-610	118	94	’	'	PUNCT
eurjchem-610	119	1	=	=	SYM
eurjchem-610	119	2	4.7	4.7	NUM
eurjchem-610	119	3	and	and	CCONJ
eurjchem-610	119	4	j’’=	j’’=	PROPN
eurjchem-610	119	5	7.3	7.3	NUM
eurjchem-610	119	6	hz	hz	NOUN
eurjchem-610	119	7	,	,	PUNCT
eurjchem-610	119	8	2h	2h	NUM
eurjchem-610	119	9	,	,	PUNCT
eurjchem-610	119	10	ch2‐	ch2‐	NOUN
eurjchem-610	119	11	ph	ph	NOUN
eurjchem-610	119	12	)	)	PUNCT
eurjchem-610	119	13	.	.	PUNCT
eurjchem-610	120	1	13c	13c	NOUN
eurjchem-610	120	2	nmr	nmr	NOUN
eurjchem-610	120	3	(	(	PUNCT
eurjchem-610	120	4	62.89	62.89	NUM
eurjchem-610	120	5	mhz	mhz	NOUN
eurjchem-610	120	6	,	,	PUNCT
eurjchem-610	120	7	cdcl3	cdcl3	PROPN
eurjchem-610	120	8	,	,	PUNCT
eurjchem-610	120	9	δ	δ	PROPN
eurjchem-610	120	10	,	,	PUNCT
eurjchem-610	120	11	ppm	ppm	NOUN
eurjchem-610	120	12	):	):	PUNCT
eurjchem-610	120	13	138.7	138.7	NUM
eurjchem-610	120	14	,	,	PUNCT
eurjchem-610	120	15	137.3	137.3	NUM
eurjchem-610	120	16	,	,	PUNCT
eurjchem-610	120	17	129.2	129.2	NUM
eurjchem-610	120	18	,	,	PUNCT
eurjchem-610	120	19	128.3	128.3	NUM
eurjchem-610	120	20	,	,	PUNCT
eurjchem-610	120	21	127.5	127.5	NUM
eurjchem-610	120	22	,	,	PUNCT
eurjchem-610	120	23	127.1	127.1	NUM
eurjchem-610	120	24	,	,	PUNCT
eurjchem-610	120	25	125.5	125.5	NUM
eurjchem-610	120	26	,	,	PUNCT
eurjchem-610	120	27	124.5	124.5	NUM
eurjchem-610	120	28	,	,	PUNCT
eurjchem-610	120	29	57.3	57.3	NUM
eurjchem-610	120	30	,	,	PUNCT
eurjchem-610	120	31	54.2	54.2	NUM
eurjchem-610	120	32	,	,	PUNCT
eurjchem-610	120	33	52.1	52.1	NUM
eurjchem-610	120	34	,	,	PUNCT
eurjchem-610	120	35	42.7	42.7	NUM
eurjchem-610	120	36	.	.	PUNCT
eurjchem-610	121	1	ms	ms	NOUN
eurjchem-610	121	2	(	(	PUNCT
eurjchem-610	121	3	esi+	esi+	PROPN
eurjchem-610	121	4	,	,	PUNCT
eurjchem-610	121	5	30	30	NUM
eurjchem-610	121	6	ev	ev	NOUN
eurjchem-610	121	7	,	,	PUNCT
eurjchem-610	121	8	m	m	PROPN
eurjchem-610	121	9	/	/	SYM
eurjchem-610	121	10	z	z	NOUN
eurjchem-610	121	11	,	,	PUNCT
eurjchem-610	121	12	(	(	PUNCT
eurjchem-610	121	13	i	i	PRON
eurjchem-610	121	14	rel	rel	VERB
eurjchem-610	121	15	,	,	PUNCT
eurjchem-610	121	16	%	%	NOUN
eurjchem-610	121	17	)	)	PUNCT
eurjchem-610	121	18	):	):	PUNCT
eurjchem-610	122	1	303	303	NUM
eurjchem-610	122	2	[	[	X
eurjchem-610	122	3	m+h]+	m+h]+	X
eurjchem-610	122	4	(	(	PUNCT
eurjchem-610	122	5	100	100	NUM
eurjchem-610	122	6	)	)	PUNCT
eurjchem-610	122	7	,	,	PUNCT
eurjchem-610	122	8	91	91	NUM
eurjchem-610	122	9	[	[	X
eurjchem-610	122	10	bn]+	bn]+	X
eurjchem-610	122	11	(	(	PUNCT
eurjchem-610	122	12	67	67	NUM
eurjchem-610	122	13	)	)	PUNCT
eurjchem-610	122	14	.	.	PUNCT
eurjchem-610	123	1	anal	anal	PROPN
eurjchem-610	123	2	.	.	PUNCT
eurjchem-610	123	3	calcd	calcd	NOUN
eurjchem-610	123	4	.	.	PUNCT
eurjchem-610	124	1	for	for	ADP
eurjchem-610	124	2	c16h18n2o2s	c16h18n2o2s	PROPN
eurjchem-610	124	3	:	:	PUNCT
eurjchem-610	124	4	c	c	X
eurjchem-610	124	5	,	,	PUNCT
eurjchem-610	124	6	63.57	63.57	NUM
eurjchem-610	124	7	;	;	PUNCT
eurjchem-610	124	8	h	h	X
eurjchem-610	124	9	,	,	PUNCT
eurjchem-610	124	10	5.96	5.96	NUM
eurjchem-610	124	11	;	;	PUNCT
eurjchem-610	124	12	n	n	CCONJ
eurjchem-610	124	13	,	,	PUNCT
eurjchem-610	124	14	9.27	9.27	NUM
eurjchem-610	124	15	.	.	PUNCT
eurjchem-610	124	16	found	find	VERB
eurjchem-610	124	17	:	:	PUNCT
eurjchem-610	125	1	c	c	X
eurjchem-610	125	2	,	,	PUNCT
eurjchem-610	125	3	63.51	63.51	NUM
eurjchem-610	125	4	;	;	PUNCT
eurjchem-610	125	5	h	h	NOUN
eurjchem-610	125	6	,	,	PUNCT
eurjchem-610	125	7	5.92	5.92	NUM
eurjchem-610	125	8	;	;	PUNCT
eurjchem-610	125	9	n	n	CCONJ
eurjchem-610	125	10	,	,	PUNCT
eurjchem-610	125	11	9.29	9.29	NUM
eurjchem-610	125	12	%	%	NOUN
eurjchem-610	125	13	.	.	PUNCT
eurjchem-610	126	1	2.1.3	2.1.3	NUM
eurjchem-610	126	2	.	.	PUNCT
eurjchem-610	126	3	n‐tert	n‐tert	X
eurjchem-610	126	4	‐butyloxycarbonyl	‐butyloxycarbonyl	PROPN
eurjchem-610	126	5	,	,	PUNCT
eurjchem-610	126	6	n’‐benzylsulfamide	n’‐benzylsulfamide	X
eurjchem-610	126	7	(	(	PUNCT
eurjchem-610	126	8	6	6	NUM
eurjchem-610	126	9	)	)	PUNCT
eurjchem-610	126	10	the	the	DET
eurjchem-610	126	11	synthesis	synthesis	NOUN
eurjchem-610	126	12	of	of	ADP
eurjchem-610	126	13	the	the	DET
eurjchem-610	126	14	compound	compound	NOUN
eurjchem-610	126	15	6	6	NUM
eurjchem-610	126	16	,	,	PUNCT
eurjchem-610	126	17	starting	start	VERB
eurjchem-610	126	18	from	from	ADP
eurjchem-610	126	19	csi	csi	PROPN
eurjchem-610	126	20	,	,	PUNCT
eurjchem-610	126	21	tert‐	tert‐	PROPN
eurjchem-610	126	22	butyl	butyl	NOUN
eurjchem-610	126	23	alcohol	alcohol	NOUN
eurjchem-610	126	24	and	and	CCONJ
eurjchem-610	126	25	benzylamine	benzylamine	NOUN
eurjchem-610	126	26	with	with	ADP
eurjchem-610	126	27	a	a	DET
eurjchem-610	126	28	reaction	reaction	NOUN
eurjchem-610	126	29	of	of	ADP
eurjchem-610	126	30	carbamoylation‐sulfamoylation	carbamoylation‐sulfamoylation	NOUN
eurjchem-610	126	31	affording	afford	VERB
eurjchem-610	126	32	n‐boc‐benzyl	n‐boc‐benzyl	NOUN
eurjchem-610	126	33	sulfamide	sulfamide	NOUN
eurjchem-610	126	34	,	,	PUNCT
eurjchem-610	126	35	that	that	PRON
eurjchem-610	126	36	has	have	AUX
eurjchem-610	126	37	been	be	AUX
eurjchem-610	126	38	previously	previously	ADV
eurjchem-610	126	39	reported	report	VERB
eurjchem-610	126	40	[	[	X
eurjchem-610	126	41	21	21	NUM
eurjchem-610	126	42	]	]	PUNCT
eurjchem-610	126	43	.	.	PUNCT
eurjchem-610	127	1	2.1.4	2.1.4	NUM
eurjchem-610	127	2	.	.	PUNCT
eurjchem-610	127	3	synthesis	synthesis	NOUN
eurjchem-610	127	4	of	of	ADP
eurjchem-610	127	5	n’‐benzylsulfamide	n’‐benzylsulfamide	NOUN
eurjchem-610	127	6	(	(	PUNCT
eurjchem-610	127	7	6a	6a	NOUN
eurjchem-610	127	8	)	)	PUNCT
eurjchem-610	127	9	n‐boc	n‐boc	ADJ
eurjchem-610	127	10	,	,	PUNCT
eurjchem-610	127	11	n’‐benzylsulfamide	n’‐benzylsulfamide	ADJ
eurjchem-610	127	12	(	(	PUNCT
eurjchem-610	127	13	1	1	NUM
eurjchem-610	127	14	mmol	mmol	NOUN
eurjchem-610	127	15	)	)	PUNCT
eurjchem-610	127	16	was	be	AUX
eurjchem-610	127	17	dissolved	dissolve	VERB
eurjchem-610	127	18	in	in	ADP
eurjchem-610	127	19	was	be	AUX
eurjchem-610	127	20	ch2cl2	ch2cl2	ADJ
eurjchem-610	127	21	,	,	PUNCT
eurjchem-610	127	22	10	10	NUM
eurjchem-610	127	23	%	%	NOUN
eurjchem-610	127	24	of	of	ADP
eurjchem-610	127	25	heteropolyacid	heteropolyacid	ADJ
eurjchem-610	127	26	catalyst	catalyst	NOUN
eurjchem-610	127	27	was	be	AUX
eurjchem-610	127	28	added	add	VERB
eurjchem-610	127	29	and	and	CCONJ
eurjchem-610	127	30	the	the	DET
eurjchem-610	127	31	mixture	mixture	NOUN
eurjchem-610	127	32	was	be	AUX
eurjchem-610	127	33	stirred	stir	VERB
eurjchem-610	127	34	at	at	ADP
eurjchem-610	127	35	room	room	NOUN
eurjchem-610	127	36	temperature	temperature	NOUN
eurjchem-610	127	37	for	for	ADP
eurjchem-610	127	38	a	a	DET
eurjchem-610	127	39	few	few	ADJ
eurjchem-610	127	40	minutes	minute	NOUN
eurjchem-610	127	41	.	.	PUNCT
eurjchem-610	128	1	the	the	DET
eurjchem-610	128	2	suspension	suspension	NOUN
eurjchem-610	128	3	was	be	AUX
eurjchem-610	128	4	filtered	filter	VERB
eurjchem-610	128	5	,	,	PUNCT
eurjchem-610	128	6	the	the	DET
eurjchem-610	128	7	solution	solution	NOUN
eurjchem-610	128	8	was	be	AUX
eurjchem-610	128	9	dried	dry	VERB
eurjchem-610	128	10	over	over	ADP
eurjchem-610	128	11	anhydrous	anhydrous	ADJ
eurjchem-610	128	12	na2so4	na2so4	NOUN
eurjchem-610	128	13	,	,	PUNCT
eurjchem-610	128	14	filtered	filter	VERB
eurjchem-610	128	15	and	and	CCONJ
eurjchem-610	128	16	concentrated	concentrate	VERB
eurjchem-610	128	17	under	under	ADP
eurjchem-610	128	18	vacuum	vacuum	NOUN
eurjchem-610	128	19	,	,	PUNCT
eurjchem-610	128	20	belghiche	belghiche	PROPN
eurjchem-610	128	21	et	et	PROPN
eurjchem-610	128	22	al	al	PROPN
eurjchem-610	128	23	.	.	PUNCT
eurjchem-610	128	24	/	/	SYM
eurjchem-610	128	25	european	european	PROPN
eurjchem-610	128	26	journal	journal	PROPN
eurjchem-610	128	27	of	of	ADP
eurjchem-610	128	28	chemistry	chemistry	NOUN
eurjchem-610	128	29	3	3	NUM
eurjchem-610	128	30	(	(	PUNCT
eurjchem-610	128	31	3	3	NUM
eurjchem-610	128	32	)	)	PUNCT
eurjchem-610	128	33	(	(	PUNCT
eurjchem-610	128	34	2012	2012	NUM
eurjchem-610	128	35	)	)	PUNCT
eurjchem-610	128	36	305‐309	305‐309	NOUN
eurjchem-610	128	37	307	307	NUM
eurjchem-610	128	38	scheme	scheme	NOUN
eurjchem-610	128	39	2	2	NUM
eurjchem-610	128	40	and	and	CCONJ
eurjchem-610	128	41	the	the	DET
eurjchem-610	128	42	crude	crude	ADJ
eurjchem-610	128	43	product	product	NOUN
eurjchem-610	128	44	was	be	AUX
eurjchem-610	128	45	subjected	subject	VERB
eurjchem-610	128	46	to	to	ADP
eurjchem-610	128	47	column	column	NOUN
eurjchem-610	128	48	chromatography	chromatography	NOUN
eurjchem-610	128	49	(	(	PUNCT
eurjchem-610	128	50	dcm	dcm	PROPN
eurjchem-610	128	51	:	:	PUNCT
eurjchem-610	128	52	meoh	meoh	PROPN
eurjchem-610	128	53	,	,	PUNCT
eurjchem-610	128	54	9:1	9:1	NUM
eurjchem-610	128	55	)	)	PUNCT
eurjchem-610	128	56	.	.	PUNCT
eurjchem-610	129	1	n’‐benzylsulfamide	n’‐benzylsulfamide	ADJ
eurjchem-610	129	2	6a	6a	NOUN
eurjchem-610	129	3	was	be	AUX
eurjchem-610	129	4	obtained	obtain	VERB
eurjchem-610	129	5	in	in	ADP
eurjchem-610	129	6	92	92	NUM
eurjchem-610	129	7	%	%	NOUN
eurjchem-610	129	8	yield	yield	NOUN
eurjchem-610	129	9	.	.	PUNCT
eurjchem-610	130	1	the	the	DET
eurjchem-610	130	2	heteropolyacid	heteropolyacid	PROPN
eurjchem-610	130	3	was	be	AUX
eurjchem-610	130	4	recuperated	recuperate	VERB
eurjchem-610	130	5	by	by	ADP
eurjchem-610	130	6	filtration	filtration	NOUN
eurjchem-610	130	7	and	and	CCONJ
eurjchem-610	130	8	used	use	VERB
eurjchem-610	130	9	again	again	ADV
eurjchem-610	130	10	(	(	PUNCT
eurjchem-610	130	11	scheme	scheme	NOUN
eurjchem-610	130	12	2	2	NUM
eurjchem-610	130	13	)	)	PUNCT
eurjchem-610	130	14	.	.	PUNCT
eurjchem-610	131	1	n’‐benzylsulfamide	n’‐benzylsulfamide	NOUN
eurjchem-610	131	2	(	(	PUNCT
eurjchem-610	131	3	6a	6a	NOUN
eurjchem-610	131	4	):	):	PUNCT
eurjchem-610	131	5	yield	yield	NOUN
eurjchem-610	131	6	:	:	PUNCT
eurjchem-610	131	7	92	92	NUM
eurjchem-610	131	8	%	%	NOUN
eurjchem-610	131	9	.	.	PUNCT
eurjchem-610	132	1	rf	rf	PRON
eurjchem-610	132	2	=	=	NOUN
eurjchem-610	132	3	0.43	0.43	NUM
eurjchem-610	132	4	(	(	PUNCT
eurjchem-610	132	5	chcl2	chcl2	PROPN
eurjchem-610	132	6	:	:	PUNCT
eurjchem-610	132	7	meoh	meoh	PROPN
eurjchem-610	132	8	,	,	PUNCT
eurjchem-610	132	9	9:1	9:1	NUM
eurjchem-610	132	10	)	)	PUNCT
eurjchem-610	132	11	.	.	PUNCT
eurjchem-610	133	1	m.p	m.p	PROPN
eurjchem-610	133	2	.	.	PROPN
eurjchem-610	133	3	:	:	PUNCT
eurjchem-610	134	1	86‐88	86‐88	NUM
eurjchem-610	134	2	°	°	SYM
eurjchem-610	134	3	c	c	X
eurjchem-610	134	4	.	.	PUNCT
eurjchem-610	135	1	ft‐ir	ft‐ir	NOUN
eurjchem-610	135	2	(	(	PUNCT
eurjchem-610	135	3	kbr	kbr	PROPN
eurjchem-610	135	4	,	,	PUNCT
eurjchem-610	135	5	cm‐1	cm‐1	PROPN
eurjchem-610	135	6	):	):	PUNCT
eurjchem-610	135	7	3335	3335	NUM
eurjchem-610	135	8	,	,	PUNCT
eurjchem-610	135	9	3298	3298	NUM
eurjchem-610	135	10	,	,	PUNCT
eurjchem-610	135	11	3265	3265	NUM
eurjchem-610	135	12	(nh	(nh	NOUN
eurjchem-610	135	13	)	)	PUNCT
eurjchem-610	135	14	,	,	PUNCT
eurjchem-610	135	15	1354	1354	NUM
eurjchem-610	135	16	,	,	PUNCT
eurjchem-610	135	17	1142	1142	NUM
eurjchem-610	135	18	(so2	(so2	NOUN
eurjchem-610	135	19	)	)	PUNCT
eurjchem-610	135	20	.	.	PUNCT
eurjchem-610	136	1	1h	1h	NUM
eurjchem-610	136	2	nmr	nmr	NOUN
eurjchem-610	136	3	(	(	PUNCT
eurjchem-610	136	4	250	250	NUM
eurjchem-610	136	5	mhz	mhz	NOUN
eurjchem-610	136	6	,	,	PUNCT
eurjchem-610	136	7	cdcl3	cdcl3	PROPN
eurjchem-610	136	8	,	,	PUNCT
eurjchem-610	136	9	δ	δ	PROPN
eurjchem-610	136	10	,	,	PUNCT
eurjchem-610	136	11	ppm	ppm	NUM
eurjchem-610	136	12	):	):	PUNCT
eurjchem-610	136	13	7.32	7.32	NUM
eurjchem-610	136	14	(	(	PUNCT
eurjchem-610	136	15	m	m	PROPN
eurjchem-610	136	16	,	,	PUNCT
eurjchem-610	136	17	5h	5h	NUM
eurjchem-610	136	18	,	,	PUNCT
eurjchem-610	136	19	ar‐h	ar‐h	NOUN
eurjchem-610	136	20	)	)	PUNCT
eurjchem-610	136	21	,	,	PUNCT
eurjchem-610	136	22	6.05	6.05	NUM
eurjchem-610	136	23	(	(	PUNCT
eurjchem-610	136	24	t	t	PROPN
eurjchem-610	136	25	,	,	PUNCT
eurjchem-610	136	26	j	j	PROPN
eurjchem-610	136	27	=	=	PROPN
eurjchem-610	136	28	6.7	6.7	NUM
eurjchem-610	136	29	hz	hz	NOUN
eurjchem-610	136	30	,	,	PUNCT
eurjchem-610	136	31	1h	1h	NUM
eurjchem-610	136	32	,	,	PUNCT
eurjchem-610	136	33	nh	nh	PROPN
eurjchem-610	136	34	)	)	PUNCT
eurjchem-610	136	35	,	,	PUNCT
eurjchem-610	136	36	5.80	5.80	NUM
eurjchem-610	136	37	(	(	PUNCT
eurjchem-610	136	38	s	s	PROPN
eurjchem-610	136	39	,	,	PUNCT
eurjchem-610	136	40	2h	2h	NUM
eurjchem-610	136	41	,	,	PUNCT
eurjchem-610	136	42	nh2	nh2	PROPN
eurjchem-610	136	43	)	)	PUNCT
eurjchem-610	136	44	,	,	PUNCT
eurjchem-610	136	45	4.28	4.28	NUM
eurjchem-610	136	46	(	(	PUNCT
eurjchem-610	136	47	d	d	PROPN
eurjchem-610	136	48	,	,	PUNCT
eurjchem-610	136	49	j	j	PROPN
eurjchem-610	136	50	=	=	SYM
eurjchem-610	136	51	6.7	6.7	NUM
eurjchem-610	136	52	hz	hz	NOUN
eurjchem-610	136	53	,	,	PUNCT
eurjchem-610	136	54	2h	2h	NUM
eurjchem-610	136	55	,	,	PUNCT
eurjchem-610	136	56	ch2‐ph	ch2‐ph	PROPN
eurjchem-610	136	57	)	)	PUNCT
eurjchem-610	136	58	.	.	PUNCT
eurjchem-610	137	1	13c	13c	NOUN
eurjchem-610	137	2	nmr	nmr	NOUN
eurjchem-610	137	3	(	(	PUNCT
eurjchem-610	137	4	62.89	62.89	NUM
eurjchem-610	137	5	mhz	mhz	NOUN
eurjchem-610	137	6	,	,	PUNCT
eurjchem-610	137	7	cdcl3	cdcl3	PROPN
eurjchem-610	137	8	,	,	PUNCT
eurjchem-610	137	9	δ	δ	PROPN
eurjchem-610	137	10	,	,	PUNCT
eurjchem-610	137	11	ppm	ppm	NOUN
eurjchem-610	137	12	):	):	PUNCT
eurjchem-610	137	13	52.5	52.5	NUM
eurjchem-610	137	14	,	,	PUNCT
eurjchem-610	137	15	127.7	127.7	NUM
eurjchem-610	137	16	,	,	PUNCT
eurjchem-610	137	17	129.8	129.8	NUM
eurjchem-610	137	18	,	,	PUNCT
eurjchem-610	137	19	129.9	129.9	NUM
eurjchem-610	137	20	,	,	PUNCT
eurjchem-610	137	21	138.2	138.2	NUM
eurjchem-610	137	22	.	.	PUNCT
eurjchem-610	138	1	ms	ms	NOUN
eurjchem-610	138	2	(	(	PUNCT
eurjchem-610	138	3	esi+	esi+	PROPN
eurjchem-610	138	4	,	,	PUNCT
eurjchem-610	138	5	30	30	NUM
eurjchem-610	138	6	ev	ev	NOUN
eurjchem-610	138	7	,	,	PUNCT
eurjchem-610	138	8	m	m	PROPN
eurjchem-610	138	9	/	/	SYM
eurjchem-610	138	10	z	z	NOUN
eurjchem-610	138	11	,	,	PUNCT
eurjchem-610	138	12	(	(	PUNCT
eurjchem-610	138	13	i	i	PRON
eurjchem-610	138	14	rel	rel	VERB
eurjchem-610	138	15	,	,	PUNCT
eurjchem-610	138	16	%	%	NOUN
eurjchem-610	138	17	)	)	PUNCT
eurjchem-610	138	18	):	):	PUNCT
eurjchem-610	138	19	187	187	NUM
eurjchem-610	139	1	[	[	X
eurjchem-610	139	2	m+h]+	m+h]+	X
eurjchem-610	139	3	(	(	PUNCT
eurjchem-610	139	4	100	100	NUM
eurjchem-610	139	5	)	)	PUNCT
eurjchem-610	139	6	.	.	PUNCT
eurjchem-610	140	1	anal	anal	PROPN
eurjchem-610	140	2	.	.	PUNCT
eurjchem-610	140	3	calcd	calcd	NOUN
eurjchem-610	140	4	.	.	PUNCT
eurjchem-610	141	1	for	for	ADP
eurjchem-610	141	2	c7h10n2o2s	c7h10n2o2s	NOUN
eurjchem-610	141	3	:	:	PUNCT
eurjchem-610	141	4	c	c	X
eurjchem-610	141	5	,	,	PUNCT
eurjchem-610	141	6	45.16	45.16	NUM
eurjchem-610	141	7	;	;	PUNCT
eurjchem-610	141	8	h	h	NOUN
eurjchem-610	141	9	,	,	PUNCT
eurjchem-610	141	10	5.37	5.37	NUM
eurjchem-610	141	11	;	;	PUNCT
eurjchem-610	141	12	n	n	CCONJ
eurjchem-610	141	13	,	,	PUNCT
eurjchem-610	141	14	15.05	15.05	NUM
eurjchem-610	141	15	.	.	PUNCT
eurjchem-610	141	16	found	find	VERB
eurjchem-610	141	17	:	:	PUNCT
eurjchem-610	142	1	c	c	X
eurjchem-610	142	2	,	,	PUNCT
eurjchem-610	142	3	45.12	45.12	NUM
eurjchem-610	142	4	;	;	PUNCT
eurjchem-610	142	5	h	h	NOUN
eurjchem-610	142	6	,	,	PUNCT
eurjchem-610	142	7	5.40	5.40	NUM
eurjchem-610	142	8	;	;	PUNCT
eurjchem-610	142	9	n	n	CCONJ
eurjchem-610	142	10	,	,	PUNCT
eurjchem-610	142	11	15.12	15.12	NUM
eurjchem-610	142	12	%	%	NOUN
eurjchem-610	142	13	.	.	PUNCT
eurjchem-610	143	1	2.1.5	2.1.5	NUM
eurjchem-610	143	2	.	.	PUNCT
eurjchem-610	143	3	methyl	methyl	NOUN
eurjchem-610	143	4	esters	ester	NOUN
eurjchem-610	143	5	of	of	ADP
eurjchem-610	143	6	[	[	X
eurjchem-610	143	7	(	(	PUNCT
eurjchem-610	143	8	n‐(n‐boc)‐sulfamoyl	n‐(n‐boc)‐sulfamoyl	NOUN
eurjchem-610	143	9	]	]	X
eurjchem-610	143	10	amino	amino	ADJ
eurjchem-610	143	11	acids	acid	NOUN
eurjchem-610	143	12	(	(	PUNCT
eurjchem-610	143	13	7‐11	7‐11	X
eurjchem-610	143	14	)	)	PUNCT
eurjchem-610	143	15	the	the	DET
eurjchem-610	143	16	synthesis	synthesis	NOUN
eurjchem-610	143	17	of	of	ADP
eurjchem-610	143	18	the	the	DET
eurjchem-610	143	19	compounds	compound	NOUN
eurjchem-610	143	20	,	,	PUNCT
eurjchem-610	143	21	starting	start	VERB
eurjchem-610	143	22	from	from	ADP
eurjchem-610	143	23	csi	csi	PROPN
eurjchem-610	143	24	tert‐	tert‐	PROPN
eurjchem-610	143	25	butyl	butyl	NOUN
eurjchem-610	143	26	alcohol	alcohol	NOUN
eurjchem-610	143	27	and	and	CCONJ
eurjchem-610	143	28	methyl	methyl	NOUN
eurjchem-610	143	29	esters	ester	NOUN
eurjchem-610	143	30	of	of	ADP
eurjchem-610	143	31	amino	amino	ADJ
eurjchem-610	143	32	acids	acid	NOUN
eurjchem-610	143	33	(	(	PUNCT
eurjchem-610	143	34	gylcine	gylcine	NOUN
eurjchem-610	143	35	,	,	PUNCT
eurjchem-610	143	36	l‐	l‐	PROPN
eurjchem-610	143	37	alanine	alanine	NOUN
eurjchem-610	143	38	,	,	PUNCT
eurjchem-610	143	39	l‐leucine	l‐leucine	NOUN
eurjchem-610	143	40	,	,	PUNCT
eurjchem-610	143	41	and	and	CCONJ
eurjchem-610	143	42	l‐phenyalanine	l‐phenyalanine	PUNCT
eurjchem-610	143	43	)	)	PUNCT
eurjchem-610	143	44	has	have	AUX
eurjchem-610	143	45	been	be	AUX
eurjchem-610	143	46	previously	previously	ADV
eurjchem-610	143	47	reported	report	VERB
eurjchem-610	143	48	[	[	PUNCT
eurjchem-610	143	49	22,23	22,23	NOUN
eurjchem-610	143	50	]	]	X
eurjchem-610	143	51	.	.	PUNCT
eurjchem-610	144	1	2.1.6	2.1.6	X
eurjchem-610	144	2	.	.	PUNCT
eurjchem-610	144	3	synthesis	synthesis	NOUN
eurjchem-610	144	4	of	of	ADP
eurjchem-610	144	5	compounds	compound	NOUN
eurjchem-610	144	6	(	(	PUNCT
eurjchem-610	144	7	7a‐11a	7a‐11a	NUM
eurjchem-610	144	8	)	)	PUNCT
eurjchem-610	144	9	n‐boc	n‐boc	DET
eurjchem-610	144	10	linear	linear	NOUN
eurjchem-610	144	11	sulfamides	sulfamide	NOUN
eurjchem-610	144	12	(	(	PUNCT
eurjchem-610	144	13	7‐11	7‐11	NUM
eurjchem-610	144	14	)	)	PUNCT
eurjchem-610	144	15	(	(	PUNCT
eurjchem-610	144	16	1	1	NUM
eurjchem-610	144	17	mmol	mmol	NOUN
eurjchem-610	144	18	)	)	PUNCT
eurjchem-610	144	19	was	be	AUX
eurjchem-610	144	20	dissolved	dissolve	VERB
eurjchem-610	144	21	in	in	ADP
eurjchem-610	144	22	ch2cl2	ch2cl2	PROPN
eurjchem-610	144	23	,	,	PUNCT
eurjchem-610	144	24	10	10	NUM
eurjchem-610	144	25	%	%	NOUN
eurjchem-610	144	26	of	of	ADP
eurjchem-610	144	27	heteropolyacid	heteropolyacid	ADJ
eurjchem-610	144	28	catalyst	catalyst	NOUN
eurjchem-610	144	29	was	be	AUX
eurjchem-610	144	30	added	add	VERB
eurjchem-610	144	31	and	and	CCONJ
eurjchem-610	144	32	the	the	DET
eurjchem-610	144	33	mixture	mixture	NOUN
eurjchem-610	144	34	was	be	AUX
eurjchem-610	144	35	stirred	stir	VERB
eurjchem-610	144	36	at	at	ADP
eurjchem-610	144	37	room	room	NOUN
eurjchem-610	144	38	temperature	temperature	NOUN
eurjchem-610	144	39	for	for	ADP
eurjchem-610	144	40	a	a	DET
eurjchem-610	144	41	few	few	ADJ
eurjchem-610	144	42	minutes	minute	NOUN
eurjchem-610	144	43	.	.	PUNCT
eurjchem-610	145	1	the	the	DET
eurjchem-610	145	2	suspension	suspension	NOUN
eurjchem-610	145	3	was	be	AUX
eurjchem-610	145	4	filtered	filter	VERB
eurjchem-610	145	5	,	,	PUNCT
eurjchem-610	145	6	the	the	DET
eurjchem-610	145	7	solution	solution	NOUN
eurjchem-610	145	8	was	be	AUX
eurjchem-610	145	9	dried	dry	VERB
eurjchem-610	145	10	over	over	ADP
eurjchem-610	145	11	anhydrous	anhydrous	ADJ
eurjchem-610	145	12	na2so4	na2so4	NOUN
eurjchem-610	145	13	,	,	PUNCT
eurjchem-610	145	14	filtered	filter	VERB
eurjchem-610	145	15	and	and	CCONJ
eurjchem-610	145	16	concentrated	concentrate	VERB
eurjchem-610	145	17	under	under	ADP
eurjchem-610	145	18	vacuum	vacuum	NOUN
eurjchem-610	145	19	,	,	PUNCT
eurjchem-610	145	20	and	and	CCONJ
eurjchem-610	145	21	the	the	DET
eurjchem-610	145	22	crude	crude	ADJ
eurjchem-610	145	23	product	product	NOUN
eurjchem-610	145	24	was	be	AUX
eurjchem-610	145	25	subjected	subject	VERB
eurjchem-610	145	26	to	to	ADP
eurjchem-610	145	27	column	column	NOUN
eurjchem-610	145	28	chromatography	chromatography	NOUN
eurjchem-610	145	29	(	(	PUNCT
eurjchem-610	145	30	dcm	dcm	PROPN
eurjchem-610	145	31	:	:	PUNCT
eurjchem-610	145	32	meoh	meoh	PROPN
eurjchem-610	145	33	,	,	PUNCT
eurjchem-610	145	34	9:1	9:1	NUM
eurjchem-610	145	35	)	)	PUNCT
eurjchem-610	145	36	.	.	PUNCT
eurjchem-610	146	1	deprotected	deprotecte	VERB
eurjchem-610	146	2	compounds	compound	NOUN
eurjchem-610	146	3	(	(	PUNCT
eurjchem-610	146	4	7a‐11a	7a‐11a	NOUN
eurjchem-610	146	5	)	)	PUNCT
eurjchem-610	146	6	were	be	AUX
eurjchem-610	146	7	obtained	obtain	VERB
eurjchem-610	146	8	in	in	ADP
eurjchem-610	146	9	92‐95	92‐95	NOUN
eurjchem-610	146	10	%	%	NOUN
eurjchem-610	146	11	yield	yield	NOUN
eurjchem-610	146	12	.	.	PUNCT
eurjchem-610	147	1	the	the	DET
eurjchem-610	147	2	heteropolyacid	heteropolyacid	PROPN
eurjchem-610	147	3	was	be	AUX
eurjchem-610	147	4	recuperated	recuperate	VERB
eurjchem-610	147	5	by	by	ADP
eurjchem-610	147	6	filtration	filtration	NOUN
eurjchem-610	147	7	and	and	CCONJ
eurjchem-610	147	8	used	use	VERB
eurjchem-610	147	9	again	again	ADV
eurjchem-610	147	10	(	(	PUNCT
eurjchem-610	147	11	scheme	scheme	NOUN
eurjchem-610	147	12	3	3	NUM
eurjchem-610	147	13	)	)	PUNCT
eurjchem-610	147	14	.	.	PUNCT
eurjchem-610	148	1	methyl	methyl	NOUN
eurjchem-610	149	1	[	[	X
eurjchem-610	149	2	n‐sulfamoyl]‐glycinate	n‐sulfamoyl]‐glycinate	NOUN
eurjchem-610	149	3	(	(	PUNCT
eurjchem-610	149	4	7a	7a	NUM
eurjchem-610	149	5	):	):	PUNCT
eurjchem-610	149	6	yield	yield	NOUN
eurjchem-610	149	7	:	:	PUNCT
eurjchem-610	149	8	95	95	NUM
eurjchem-610	149	9	%	%	NOUN
eurjchem-610	149	10	.	.	PUNCT
eurjchem-610	150	1	rf	rf	PRON
eurjchem-610	150	2	=	=	NOUN
eurjchem-610	150	3	0.56	0.56	NUM
eurjchem-610	150	4	(	(	PUNCT
eurjchem-610	150	5	ch2cl2	ch2cl2	NOUN
eurjchem-610	150	6	:	:	PUNCT
eurjchem-610	150	7	meoh	meoh	NOUN
eurjchem-610	150	8	,	,	PUNCT
eurjchem-610	150	9	9:1	9:1	NUM
eurjchem-610	150	10	)	)	PUNCT
eurjchem-610	150	11	.	.	PUNCT
eurjchem-610	151	1	m.p	m.p	PROPN
eurjchem-610	151	2	.	.	PROPN
eurjchem-610	151	3	:	:	PUNCT
eurjchem-610	152	1	61‐62	61‐62	NUM
eurjchem-610	152	2	°	°	ADP
eurjchem-610	152	3	c	c	NOUN
eurjchem-610	152	4	.	.	PUNCT
eurjchem-610	152	5	ft‐ir	ft‐ir	NOUN
eurjchem-610	152	6	(	(	PUNCT
eurjchem-610	152	7	kbr	kbr	PROPN
eurjchem-610	152	8	,	,	PUNCT
eurjchem-610	152	9	cm‐1	cm‐1	PROPN
eurjchem-610	152	10	):	):	PUNCT
eurjchem-610	152	11	1738	1738	NUM
eurjchem-610	152	12	(c	(c	PROPN
eurjchem-610	152	13	=	=	SYM
eurjchem-610	152	14	o	o	NOUN
eurjchem-610	152	15	)	)	PUNCT
eurjchem-610	152	16	,	,	PUNCT
eurjchem-610	152	17	1351	1351	NUM
eurjchem-610	152	18	,	,	PUNCT
eurjchem-610	152	19	1139	1139	NUM
eurjchem-610	152	20	(so2	(so2	NOUN
eurjchem-610	152	21	)	)	PUNCT
eurjchem-610	152	22	,	,	PUNCT
eurjchem-610	152	23	3320	3320	NUM
eurjchem-610	152	24	,	,	PUNCT
eurjchem-610	152	25	3265	3265	NUM
eurjchem-610	152	26	(nh	(nh	NOUN
eurjchem-610	152	27	)	)	PUNCT
eurjchem-610	152	28	.	.	PUNCT
eurjchem-610	153	1	1h	1h	NUM
eurjchem-610	153	2	nmr	nmr	NOUN
eurjchem-610	153	3	(	(	PUNCT
eurjchem-610	153	4	250	250	NUM
eurjchem-610	153	5	mhz	mhz	NOUN
eurjchem-610	153	6	,	,	PUNCT
eurjchem-610	153	7	cdcl3	cdcl3	PROPN
eurjchem-610	153	8	,	,	PUNCT
eurjchem-610	153	9	δ	δ	PROPN
eurjchem-610	153	10	,	,	PUNCT
eurjchem-610	153	11	ppm	ppm	NUM
eurjchem-610	153	12	):	):	PUNCT
eurjchem-610	153	13	6.62	6.62	NUM
eurjchem-610	153	14	(	(	PUNCT
eurjchem-610	153	15	s	s	PROPN
eurjchem-610	153	16	,	,	PUNCT
eurjchem-610	153	17	2h	2h	NUM
eurjchem-610	153	18	,	,	PUNCT
eurjchem-610	153	19	nh2	nh2	PROPN
eurjchem-610	153	20	)	)	PUNCT
eurjchem-610	153	21	,	,	PUNCT
eurjchem-610	153	22	6.05	6.05	NUM
eurjchem-610	153	23	(	(	PUNCT
eurjchem-610	153	24	t	t	PROPN
eurjchem-610	153	25	,	,	PUNCT
eurjchem-610	153	26	j	j	PROPN
eurjchem-610	153	27	=	=	SYM
eurjchem-610	153	28	6.8	6.8	NUM
eurjchem-610	153	29	hz	hz	NOUN
eurjchem-610	153	30	,	,	PUNCT
eurjchem-610	153	31	1h	1h	NUM
eurjchem-610	153	32	,	,	PUNCT
eurjchem-610	153	33	nh	nh	PROPN
eurjchem-610	153	34	)	)	PUNCT
eurjchem-610	153	35	,	,	PUNCT
eurjchem-610	153	36	4.35	4.35	NUM
eurjchem-610	153	37	(	(	PUNCT
eurjchem-610	153	38	d	d	PROPN
eurjchem-610	153	39	,	,	PUNCT
eurjchem-610	153	40	j	j	PROPN
eurjchem-610	153	41	=	=	SYM
eurjchem-610	153	42	6.8	6.8	NUM
eurjchem-610	153	43	hz	hz	NOUN
eurjchem-610	153	44	,	,	PUNCT
eurjchem-610	153	45	2h	2h	NUM
eurjchem-610	153	46	,	,	PUNCT
eurjchem-610	153	47	ch2	ch2	PROPN
eurjchem-610	153	48	)	)	PUNCT
eurjchem-610	153	49	,	,	PUNCT
eurjchem-610	153	50	3.65	3.65	NUM
eurjchem-610	153	51	(	(	PUNCT
eurjchem-610	153	52	s	s	PROPN
eurjchem-610	153	53	,	,	PUNCT
eurjchem-610	153	54	3h	3h	NUM
eurjchem-610	153	55	,	,	PUNCT
eurjchem-610	153	56	och3	och3	ADJ
eurjchem-610	153	57	)	)	PUNCT
eurjchem-610	153	58	.	.	PUNCT
eurjchem-610	154	1	13c	13c	NOUN
eurjchem-610	154	2	nmr	nmr	NOUN
eurjchem-610	154	3	(	(	PUNCT
eurjchem-610	154	4	62.89	62.89	NUM
eurjchem-610	154	5	mhz	mhz	NOUN
eurjchem-610	154	6	,	,	PUNCT
eurjchem-610	154	7	cdcl3	cdcl3	PROPN
eurjchem-610	154	8	,	,	PUNCT
eurjchem-610	154	9	δ	δ	PROPN
eurjchem-610	154	10	,	,	PUNCT
eurjchem-610	154	11	ppm	ppm	NOUN
eurjchem-610	154	12	):	):	PUNCT
eurjchem-610	154	13	52.8	52.8	NUM
eurjchem-610	154	14	,	,	PUNCT
eurjchem-610	154	15	58.0	58.0	NUM
eurjchem-610	154	16	,	,	PUNCT
eurjchem-610	154	17	160.2	160.2	NUM
eurjchem-610	154	18	.	.	PUNCT
eurjchem-610	155	1	ms	ms	NOUN
eurjchem-610	155	2	(	(	PUNCT
eurjchem-610	155	3	esi+	esi+	PROPN
eurjchem-610	155	4	,	,	PUNCT
eurjchem-610	155	5	30	30	NUM
eurjchem-610	155	6	ev	ev	NOUN
eurjchem-610	155	7	,	,	PUNCT
eurjchem-610	155	8	m	m	PROPN
eurjchem-610	155	9	/	/	SYM
eurjchem-610	155	10	z	z	NOUN
eurjchem-610	155	11	,	,	PUNCT
eurjchem-610	155	12	(	(	PUNCT
eurjchem-610	155	13	i	i	PRON
eurjchem-610	155	14	rel	rel	VERB
eurjchem-610	155	15	,	,	PUNCT
eurjchem-610	155	16	%	%	INTJ
eurjchem-610	155	17	)	)	PUNCT
eurjchem-610	155	18	):	):	PUNCT
eurjchem-610	155	19	191	191	NUM
eurjchem-610	155	20	[	[	X
eurjchem-610	155	21	m+na]+	m+na]+	NOUN
eurjchem-610	155	22	(	(	PUNCT
eurjchem-610	155	23	100	100	NUM
eurjchem-610	155	24	%	%	NOUN
eurjchem-610	155	25	)	)	PUNCT
eurjchem-610	155	26	.	.	PUNCT
eurjchem-610	156	1	anal	anal	PROPN
eurjchem-610	156	2	.	.	PUNCT
eurjchem-610	156	3	calcd	calcd	NOUN
eurjchem-610	156	4	.	.	PUNCT
eurjchem-610	157	1	for	for	ADP
eurjchem-610	157	2	c3h8n2o4s	c3h8n2o4s	NOUN
eurjchem-610	157	3	:	:	PUNCT
eurjchem-610	157	4	c	c	X
eurjchem-610	157	5	,	,	PUNCT
eurjchem-610	157	6	21.43	21.43	NUM
eurjchem-610	157	7	;	;	PUNCT
eurjchem-610	157	8	h	h	NOUN
eurjchem-610	157	9	,	,	PUNCT
eurjchem-610	157	10	4.76	4.76	NUM
eurjchem-610	157	11	;	;	PUNCT
eurjchem-610	157	12	n	n	CCONJ
eurjchem-610	157	13	,	,	PUNCT
eurjchem-610	157	14	16.66	16.66	NUM
eurjchem-610	157	15	.	.	PUNCT
eurjchem-610	157	16	found	find	VERB
eurjchem-610	157	17	:	:	PUNCT
eurjchem-610	158	1	c	c	X
eurjchem-610	158	2	,	,	PUNCT
eurjchem-610	158	3	21.38	21.38	NUM
eurjchem-610	158	4	;	;	PUNCT
eurjchem-610	158	5	h	h	NOUN
eurjchem-610	158	6	,	,	PUNCT
eurjchem-610	158	7	4.79	4.79	NUM
eurjchem-610	158	8	;	;	PUNCT
eurjchem-610	158	9	n	n	CCONJ
eurjchem-610	158	10	,	,	PUNCT
eurjchem-610	158	11	16.64	16.64	NUM
eurjchem-610	158	12	%	%	NOUN
eurjchem-610	158	13	.	.	PUNCT
eurjchem-610	159	1	[	[	X
eurjchem-610	159	2	(	(	PUNCT
eurjchem-610	159	3	s)(‐	s)(‐	PROPN
eurjchem-610	159	4	)	)	PUNCT
eurjchem-610	159	5	methyl	methyl	NOUN
eurjchem-610	160	1	[	[	X
eurjchem-610	160	2	n‐sulfamoyl]‐alaninate	n‐sulfamoyl]‐alaninate	NOUN
eurjchem-610	160	3	(	(	PUNCT
eurjchem-610	160	4	8a	8a	NUM
eurjchem-610	160	5	):	):	PUNCT
eurjchem-610	160	6	yield	yield	NOUN
eurjchem-610	160	7	:	:	PUNCT
eurjchem-610	160	8	92	92	NUM
eurjchem-610	160	9	%	%	NOUN
eurjchem-610	160	10	.	.	PUNCT
eurjchem-610	161	1	rf	rf	PRON
eurjchem-610	161	2	=	=	NOUN
eurjchem-610	161	3	0.46	0.46	NUM
eurjchem-610	161	4	(	(	PUNCT
eurjchem-610	161	5	ch2cl2	ch2cl2	NOUN
eurjchem-610	161	6	:	:	PUNCT
eurjchem-610	161	7	meoh	meoh	NOUN
eurjchem-610	161	8	,	,	PUNCT
eurjchem-610	161	9	9:1	9:1	NUM
eurjchem-610	161	10	)	)	PUNCT
eurjchem-610	161	11	.	.	PUNCT
eurjchem-610	162	1	m.p	m.p	PROPN
eurjchem-610	162	2	.	.	PROPN
eurjchem-610	162	3	:	:	PUNCT
eurjchem-610	162	4	67‐68	67‐68	NUM
eurjchem-610	163	1	°	°	NOUN
eurjchem-610	163	2	c	c	NOUN
eurjchem-610	163	3	.	.	PUNCT
eurjchem-610	164	1	[	[	X
eurjchem-610	164	2	α]d=	α]d=	NUM
eurjchem-610	164	3	‐18	‐18	NOUN
eurjchem-610	164	4	°	°	NOUN
eurjchem-610	164	5	(	(	PUNCT
eurjchem-610	164	6	c	c	NOUN
eurjchem-610	164	7	=	=	SYM
eurjchem-610	164	8	1	1	NUM
eurjchem-610	164	9	,	,	PUNCT
eurjchem-610	164	10	etoh	etoh	NOUN
eurjchem-610	164	11	)	)	PUNCT
eurjchem-610	164	12	.	.	PUNCT
eurjchem-610	165	1	ft‐ir	ft‐ir	NOUN
eurjchem-610	165	2	(	(	PUNCT
eurjchem-610	165	3	kbr	kbr	PROPN
eurjchem-610	165	4	,	,	PUNCT
eurjchem-610	165	5	cm‐1	cm‐1	PROPN
eurjchem-610	165	6	):	):	PUNCT
eurjchem-610	165	7	3290	3290	NUM
eurjchem-610	165	8	,	,	PUNCT
eurjchem-610	165	9	3372	3372	NUM
eurjchem-610	165	10	(nh	(nh	PROPN
eurjchem-610	165	11	)	)	PUNCT
eurjchem-610	165	12	,	,	PUNCT
eurjchem-610	165	13	1746	1746	NUM
eurjchem-610	165	14	(c	(c	PROPN
eurjchem-610	165	15	=	=	SYM
eurjchem-610	165	16	o	o	NOUN
eurjchem-610	165	17	)	)	PUNCT
eurjchem-610	165	18	,	,	PUNCT
eurjchem-610	165	19	1341	1341	NUM
eurjchem-610	165	20	,	,	PUNCT
eurjchem-610	165	21	1149	1149	NUM
eurjchem-610	165	22	(so2	(so2	NOUN
eurjchem-610	165	23	)	)	PUNCT
eurjchem-610	165	24	,	,	PUNCT
eurjchem-610	165	25	3330	3330	NUM
eurjchem-610	165	26	,	,	PUNCT
eurjchem-610	165	27	3270	3270	NUM
eurjchem-610	165	28	,	,	PUNCT
eurjchem-610	165	29	3250	3250	NUM
eurjchem-610	165	30	(nh	(nh	NOUN
eurjchem-610	165	31	)	)	PUNCT
eurjchem-610	165	32	.	.	PUNCT
eurjchem-610	166	1	1h	1h	NUM
eurjchem-610	166	2	nmr	nmr	NOUN
eurjchem-610	166	3	(	(	PUNCT
eurjchem-610	166	4	250	250	NUM
eurjchem-610	166	5	mhz	mhz	NOUN
eurjchem-610	166	6	,	,	PUNCT
eurjchem-610	166	7	cdcl3	cdcl3	PROPN
eurjchem-610	166	8	,	,	PUNCT
eurjchem-610	166	9	δ	δ	PROPN
eurjchem-610	166	10	,	,	PUNCT
eurjchem-610	166	11	ppm	ppm	NOUN
eurjchem-610	166	12	):	):	PUNCT
eurjchem-610	166	13	6.95	6.95	NUM
eurjchem-610	166	14	(	(	PUNCT
eurjchem-610	166	15	d	d	NOUN
eurjchem-610	166	16	,	,	PUNCT
eurjchem-610	166	17	j	j	PROPN
eurjchem-610	166	18	=	=	SYM
eurjchem-610	166	19	8.6	8.6	NUM
eurjchem-610	166	20	hz	hz	NOUN
eurjchem-610	166	21	,	,	PUNCT
eurjchem-610	166	22	1h	1h	NUM
eurjchem-610	166	23	,	,	PUNCT
eurjchem-610	166	24	nh	nh	PROPN
eurjchem-610	166	25	)	)	PUNCT
eurjchem-610	166	26	,	,	PUNCT
eurjchem-610	166	27	5.40	5.40	NUM
eurjchem-610	166	28	(	(	PUNCT
eurjchem-610	166	29	s	s	PROPN
eurjchem-610	166	30	,	,	PUNCT
eurjchem-610	166	31	2h	2h	NUM
eurjchem-610	166	32	,	,	PUNCT
eurjchem-610	166	33	nh2	nh2	PROPN
eurjchem-610	166	34	)	)	PUNCT
eurjchem-610	166	35	,	,	PUNCT
eurjchem-610	166	36	4.20	4.20	NUM
eurjchem-610	166	37	(	(	PUNCT
eurjchem-610	166	38	m	m	PROPN
eurjchem-610	166	39	,	,	PUNCT
eurjchem-610	166	40	1h	1h	NUM
eurjchem-610	166	41	,	,	PUNCT
eurjchem-610	166	42	c*h	c*h	PROPN
eurjchem-610	166	43	)	)	PUNCT
eurjchem-610	166	44	,	,	PUNCT
eurjchem-610	166	45	3.65	3.65	NUM
eurjchem-610	166	46	(	(	PUNCT
eurjchem-610	166	47	s	s	PROPN
eurjchem-610	166	48	,	,	PUNCT
eurjchem-610	166	49	3h	3h	NUM
eurjchem-610	166	50	,	,	PUNCT
eurjchem-610	166	51	och3	och3	ADJ
eurjchem-610	166	52	)	)	PUNCT
eurjchem-610	166	53	,	,	PUNCT
eurjchem-610	166	54	1.45	1.45	NUM
eurjchem-610	166	55	(	(	PUNCT
eurjchem-610	166	56	d	d	PROPN
eurjchem-610	166	57	,	,	PUNCT
eurjchem-610	166	58	j	j	PROPN
eurjchem-610	166	59	=	=	SYM
eurjchem-610	166	60	7.2	7.2	NUM
eurjchem-610	166	61	hz	hz	NOUN
eurjchem-610	166	62	,	,	PUNCT
eurjchem-610	166	63	3h	3h	NUM
eurjchem-610	166	64	,	,	PUNCT
eurjchem-610	166	65	ch3	ch3	PROPN
eurjchem-610	166	66	)	)	PUNCT
eurjchem-610	166	67	.	.	PUNCT
eurjchem-610	167	1	13c	13c	NOUN
eurjchem-610	167	2	nmr	nmr	NOUN
eurjchem-610	167	3	(	(	PUNCT
eurjchem-610	167	4	62.89	62.89	NUM
eurjchem-610	167	5	mhz	mhz	NOUN
eurjchem-610	167	6	,	,	PUNCT
eurjchem-610	167	7	cdcl3	cdcl3	PROPN
eurjchem-610	167	8	,	,	PUNCT
eurjchem-610	167	9	δ	δ	PROPN
eurjchem-610	167	10	,	,	PUNCT
eurjchem-610	167	11	ppm	ppm	NOUN
eurjchem-610	167	12	):	):	PUNCT
eurjchem-610	167	13	19.3	19.3	NUM
eurjchem-610	167	14	,	,	PUNCT
eurjchem-610	167	15	51.3	51.3	NUM
eurjchem-610	167	16	,	,	PUNCT
eurjchem-610	167	17	53.2	53.2	NUM
eurjchem-610	167	18	,	,	PUNCT
eurjchem-610	167	19	171.2	171.2	NUM
eurjchem-610	167	20	.	.	PUNCT
eurjchem-610	168	1	ms	ms	NOUN
eurjchem-610	168	2	(	(	PUNCT
eurjchem-610	168	3	esi+	esi+	PROPN
eurjchem-610	168	4	,	,	PUNCT
eurjchem-610	168	5	30	30	NUM
eurjchem-610	168	6	ev	ev	NOUN
eurjchem-610	168	7	,	,	PUNCT
eurjchem-610	168	8	m	m	PROPN
eurjchem-610	168	9	/	/	SYM
eurjchem-610	168	10	z	z	NOUN
eurjchem-610	168	11	,	,	PUNCT
eurjchem-610	168	12	(	(	PUNCT
eurjchem-610	168	13	i	i	PRON
eurjchem-610	168	14	rel	rel	VERB
eurjchem-610	168	15	,	,	PUNCT
eurjchem-610	168	16	%	%	NOUN
eurjchem-610	168	17	)	)	PUNCT
eurjchem-610	168	18	):	):	PUNCT
eurjchem-610	168	19	183	183	NUM
eurjchem-610	169	1	[	[	X
eurjchem-610	169	2	m+h]+	m+h]+	X
eurjchem-610	169	3	(	(	PUNCT
eurjchem-610	169	4	80	80	NUM
eurjchem-610	169	5	)	)	PUNCT
eurjchem-610	169	6	,	,	PUNCT
eurjchem-610	169	7	365	365	NUM
eurjchem-610	169	8	[	[	SYM
eurjchem-610	169	9	2m+h]+(20	2m+h]+(20	NOUN
eurjchem-610	169	10	)	)	PUNCT
eurjchem-610	169	11	.	.	PUNCT
eurjchem-610	170	1	anal	anal	PROPN
eurjchem-610	170	2	.	.	PUNCT
eurjchem-610	170	3	calcd	calcd	NOUN
eurjchem-610	170	4	.	.	PUNCT
eurjchem-610	171	1	for	for	ADP
eurjchem-610	171	2	c4h10n2o4s	c4h10n2o4	NOUN
eurjchem-610	171	3	:	:	PUNCT
eurjchem-610	172	1	c	c	X
eurjchem-610	172	2	,	,	PUNCT
eurjchem-610	172	3	26.37	26.37	NUM
eurjchem-610	172	4	;	;	PUNCT
eurjchem-610	172	5	h	h	NOUN
eurjchem-610	172	6	,	,	PUNCT
eurjchem-610	172	7	5.49	5.49	NUM
eurjchem-610	172	8	;	;	PUNCT
eurjchem-610	172	9	n	n	CCONJ
eurjchem-610	172	10	,	,	PUNCT
eurjchem-610	172	11	15.38	15.38	NUM
eurjchem-610	172	12	.	.	PUNCT
eurjchem-610	173	1	found	find	VERB
eurjchem-610	173	2	:	:	PUNCT
eurjchem-610	174	1	c	c	X
eurjchem-610	174	2	,	,	PUNCT
eurjchem-610	174	3	26.42	26.42	NUM
eurjchem-610	174	4	;	;	PUNCT
eurjchem-610	174	5	h	h	NOUN
eurjchem-610	174	6	,	,	PUNCT
eurjchem-610	174	7	5.44	5.44	NUM
eurjchem-610	174	8	;	;	PUNCT
eurjchem-610	174	9	n	n	CCONJ
eurjchem-610	174	10	,	,	PUNCT
eurjchem-610	174	11	15.43	15.43	NUM
eurjchem-610	174	12	%	%	NOUN
eurjchem-610	174	13	.	.	PUNCT
eurjchem-610	175	1	[	[	X
eurjchem-610	175	2	(	(	PUNCT
eurjchem-610	175	3	s)(+	s)(+	PROPN
eurjchem-610	175	4	)	)	PUNCT
eurjchem-610	175	5	methyl	methyl	NOUN
eurjchem-610	176	1	[	[	X
eurjchem-610	176	2	n‐sulfamoyl]‐valinate	n‐sulfamoyl]‐valinate	NOUN
eurjchem-610	176	3	(	(	PUNCT
eurjchem-610	176	4	9a	9a	NOUN
eurjchem-610	176	5	):	):	PUNCT
eurjchem-610	176	6	yield	yield	NOUN
eurjchem-610	176	7	:	:	PUNCT
eurjchem-610	176	8	92	92	NUM
eurjchem-610	176	9	%	%	NOUN
eurjchem-610	176	10	.	.	PUNCT
eurjchem-610	177	1	rf	rf	PRON
eurjchem-610	177	2	=	=	NOUN
eurjchem-610	177	3	0.49	0.49	NUM
eurjchem-610	177	4	(	(	PUNCT
eurjchem-610	177	5	ch2cl2	ch2cl2	NOUN
eurjchem-610	177	6	:	:	PUNCT
eurjchem-610	177	7	meoh	meoh	NOUN
eurjchem-610	177	8	,	,	PUNCT
eurjchem-610	177	9	9:1	9:1	NUM
eurjchem-610	177	10	)	)	PUNCT
eurjchem-610	177	11	.	.	PUNCT
eurjchem-610	178	1	m.p	m.p	PROPN
eurjchem-610	178	2	.	.	PROPN
eurjchem-610	178	3	:	:	PUNCT
eurjchem-610	179	1	52‐54	52‐54	NUM
eurjchem-610	179	2	°	°	SYM
eurjchem-610	179	3	c	c	NOUN
eurjchem-610	179	4	.	.	PUNCT
eurjchem-610	180	1	[	[	X
eurjchem-610	180	2	α]d	α]d	NOUN
eurjchem-610	180	3	=	=	PUNCT
eurjchem-610	180	4	+9.5	+9.5	PROPN
eurjchem-610	180	5	°	°	INTJ
eurjchem-610	180	6	(	(	PUNCT
eurjchem-610	180	7	c	c	NOUN
eurjchem-610	180	8	=	=	SYM
eurjchem-610	180	9	1	1	NUM
eurjchem-610	180	10	,	,	PUNCT
eurjchem-610	180	11	etoh	etoh	NOUN
eurjchem-610	180	12	)	)	PUNCT
eurjchem-610	180	13	.	.	PUNCT
eurjchem-610	181	1	ft‐ir	ft‐ir	NOUN
eurjchem-610	181	2	(	(	PUNCT
eurjchem-610	181	3	kbr	kbr	PROPN
eurjchem-610	181	4	,	,	PUNCT
eurjchem-610	181	5	cm‐1	cm‐1	PROPN
eurjchem-610	181	6	):	):	PUNCT
eurjchem-610	181	7	1748	1748	NUM
eurjchem-610	181	8	(c	(c	NOUN
eurjchem-610	181	9	=	=	SYM
eurjchem-610	181	10	o	o	NOUN
eurjchem-610	181	11	)	)	PUNCT
eurjchem-610	181	12	,	,	PUNCT
eurjchem-610	181	13	1352	1352	NUM
eurjchem-610	181	14	,	,	PUNCT
eurjchem-610	181	15	1158	1158	NUM
eurjchem-610	181	16	(so2	(so2	NOUN
eurjchem-610	181	17	)	)	PUNCT
eurjchem-610	181	18	,	,	PUNCT
eurjchem-610	181	19	3332	3332	NUM
eurjchem-610	181	20	,	,	PUNCT
eurjchem-610	181	21	3258	3258	NUM
eurjchem-610	181	22	,	,	PUNCT
eurjchem-610	181	23	3274	3274	NUM
eurjchem-610	181	24	(nh	(nh	NOUN
eurjchem-610	181	25	)	)	PUNCT
eurjchem-610	181	26	.	.	PUNCT
eurjchem-610	182	1	1h	1h	NUM
eurjchem-610	182	2	nmr	nmr	NOUN
eurjchem-610	182	3	(	(	PUNCT
eurjchem-610	182	4	250	250	NUM
eurjchem-610	182	5	mhz	mhz	NOUN
eurjchem-610	182	6	,	,	PUNCT
eurjchem-610	182	7	cdcl3	cdcl3	PROPN
eurjchem-610	182	8	,	,	PUNCT
eurjchem-610	182	9	δ	δ	PROPN
eurjchem-610	182	10	,	,	PUNCT
eurjchem-610	182	11	ppm	ppm	NUM
eurjchem-610	182	12	):	):	PUNCT
eurjchem-610	182	13	5.73	5.73	NUM
eurjchem-610	182	14	(	(	PUNCT
eurjchem-610	182	15	d	d	NOUN
eurjchem-610	182	16	,	,	PUNCT
eurjchem-610	182	17	j	j	PROPN
eurjchem-610	182	18	=	=	SYM
eurjchem-610	182	19	8.3	8.3	NUM
eurjchem-610	182	20	hz	hz	NOUN
eurjchem-610	182	21	,	,	PUNCT
eurjchem-610	182	22	1h	1h	NUM
eurjchem-610	182	23	,	,	PUNCT
eurjchem-610	182	24	nh	nh	PROPN
eurjchem-610	182	25	)	)	PUNCT
eurjchem-610	182	26	,	,	PUNCT
eurjchem-610	182	27	5.04	5.04	NUM
eurjchem-610	182	28	(	(	PUNCT
eurjchem-610	182	29	s	s	PROPN
eurjchem-610	182	30	,	,	PUNCT
eurjchem-610	182	31	2h	2h	NUM
eurjchem-610	182	32	,	,	PUNCT
eurjchem-610	182	33	nh2	nh2	PROPN
eurjchem-610	182	34	)	)	PUNCT
eurjchem-610	182	35	,	,	PUNCT
eurjchem-610	182	36	3.90	3.90	NUM
eurjchem-610	182	37	and	and	CCONJ
eurjchem-610	182	38	3.95	3.95	NUM
eurjchem-610	182	39	(	(	PUNCT
eurjchem-610	182	40	dd	dd	NOUN
eurjchem-610	182	41	,	,	PUNCT
eurjchem-610	182	42	j=	j=	NOUN
eurjchem-610	182	43	4.8	4.8	NUM
eurjchem-610	182	44	and	and	CCONJ
eurjchem-610	182	45	j’=	j’=	PROPN
eurjchem-610	182	46	4.8	4.8	NUM
eurjchem-610	182	47	hz	hz	VERB
eurjchem-610	182	48	,	,	PUNCT
eurjchem-610	182	49	1h	1h	NUM
eurjchem-610	182	50	,	,	PUNCT
eurjchem-610	182	51	c*h	c*h	PROPN
eurjchem-610	182	52	)	)	PUNCT
eurjchem-610	182	53	,	,	PUNCT
eurjchem-610	182	54	3.80	3.80	NUM
eurjchem-610	182	55	(	(	PUNCT
eurjchem-610	182	56	s	s	PROPN
eurjchem-610	182	57	,	,	PUNCT
eurjchem-610	182	58	3h	3h	NUM
eurjchem-610	182	59	,	,	PUNCT
eurjchem-610	182	60	och3	och3	ADJ
eurjchem-610	182	61	)	)	PUNCT
eurjchem-610	182	62	,	,	PUNCT
eurjchem-610	182	63	2.20	2.20	NUM
eurjchem-610	182	64	(	(	PUNCT
eurjchem-610	182	65	m	m	PROPN
eurjchem-610	182	66	,	,	PUNCT
eurjchem-610	182	67	1h	1h	NUM
eurjchem-610	182	68	,	,	PUNCT
eurjchem-610	182	69	chβ	chβ	ADJ
eurjchem-610	182	70	)	)	PUNCT
eurjchem-610	182	71	,	,	PUNCT
eurjchem-610	182	72	0.9	0.9	NUM
eurjchem-610	182	73	and	and	CCONJ
eurjchem-610	182	74	1.1	1.1	NUM
eurjchem-610	182	75	(	(	PUNCT
eurjchem-610	182	76	2d	2d	NOUN
eurjchem-610	182	77	,	,	PUNCT
eurjchem-610	182	78	j	j	PROPN
eurjchem-610	182	79	=	=	SYM
eurjchem-610	182	80	6.8	6.8	NUM
eurjchem-610	182	81	hz	hz	NOUN
eurjchem-610	182	82	,	,	PUNCT
eurjchem-610	182	83	6h	6h	NUM
eurjchem-610	182	84	,	,	PUNCT
eurjchem-610	182	85	2ch3	2ch3	NUM
eurjchem-610	182	86	)	)	PUNCT
eurjchem-610	182	87	.	.	PUNCT
eurjchem-610	183	1	13c	13c	NOUN
eurjchem-610	183	2	nmr	nmr	NOUN
eurjchem-610	183	3	(	(	PUNCT
eurjchem-610	183	4	62.89	62.89	NUM
eurjchem-610	183	5	mhz	mhz	NOUN
eurjchem-610	183	6	,	,	PUNCT
eurjchem-610	183	7	cdcl3	cdcl3	PROPN
eurjchem-610	183	8	,	,	PUNCT
eurjchem-610	183	9	δ	δ	PROPN
eurjchem-610	183	10	,	,	PUNCT
eurjchem-610	183	11	ppm	ppm	NUM
eurjchem-610	183	12	):	):	PUNCT
eurjchem-610	183	13	19.7	19.7	NUM
eurjchem-610	183	14	,	,	PUNCT
eurjchem-610	183	15	20.0	20.0	NUM
eurjchem-610	183	16	,	,	PUNCT
eurjchem-610	183	17	30.3	30.3	NUM
eurjchem-610	183	18	,	,	PUNCT
eurjchem-610	183	19	56.7	56.7	NUM
eurjchem-610	183	20	,	,	PUNCT
eurjchem-610	183	21	62.2	62.2	NUM
eurjchem-610	183	22	,	,	PUNCT
eurjchem-610	183	23	175.6	175.6	NUM
eurjchem-610	183	24	.	.	PUNCT
eurjchem-610	184	1	ms	ms	NOUN
eurjchem-610	184	2	(	(	PUNCT
eurjchem-610	184	3	esi+	esi+	PROPN
eurjchem-610	184	4	,	,	PUNCT
eurjchem-610	184	5	30	30	NUM
eurjchem-610	184	6	ev	ev	NOUN
eurjchem-610	184	7	,	,	PUNCT
eurjchem-610	184	8	m	m	PROPN
eurjchem-610	184	9	/	/	SYM
eurjchem-610	184	10	z	z	NOUN
eurjchem-610	184	11	,	,	PUNCT
eurjchem-610	184	12	(	(	PUNCT
eurjchem-610	184	13	i	i	PRON
eurjchem-610	184	14	rel	rel	VERB
eurjchem-610	184	15	,	,	PUNCT
eurjchem-610	184	16	%	%	INTJ
eurjchem-610	184	17	)	)	PUNCT
eurjchem-610	184	18	):	):	PUNCT
eurjchem-610	184	19	211	211	NUM
eurjchem-610	185	1	[	[	X
eurjchem-610	185	2	m+h]+	m+h]+	X
eurjchem-610	185	3	(	(	PUNCT
eurjchem-610	185	4	100	100	NUM
eurjchem-610	185	5	)	)	PUNCT
eurjchem-610	185	6	.	.	PUNCT
eurjchem-610	186	1	anal	anal	PROPN
eurjchem-610	186	2	.	.	PUNCT
eurjchem-610	186	3	calcd	calcd	NOUN
eurjchem-610	186	4	.	.	PUNCT
eurjchem-610	187	1	for	for	SCONJ
eurjchem-610	187	2	c6h14n2o2s	c6h14n2o2s	NOUN
eurjchem-610	187	3	:	:	PUNCT
eurjchem-610	187	4	c	c	X
eurjchem-610	187	5	,	,	PUNCT
eurjchem-610	187	6	34.28	34.28	NUM
eurjchem-610	187	7	;	;	PUNCT
eurjchem-610	187	8	h	h	NOUN
eurjchem-610	187	9	,	,	PUNCT
eurjchem-610	187	10	6.66	6.66	NUM
eurjchem-610	187	11	;	;	PUNCT
eurjchem-610	187	12	n	n	CCONJ
eurjchem-610	187	13	,	,	PUNCT
eurjchem-610	187	14	13.33	13.33	NUM
eurjchem-610	187	15	.	.	PUNCT
eurjchem-610	187	16	found	find	VERB
eurjchem-610	187	17	:	:	PUNCT
eurjchem-610	188	1	c	c	X
eurjchem-610	188	2	,	,	PUNCT
eurjchem-610	188	3	34.42	34.42	NUM
eurjchem-610	188	4	;	;	PUNCT
eurjchem-610	188	5	h	h	NOUN
eurjchem-610	188	6	,	,	PUNCT
eurjchem-610	188	7	6.71	6.71	NUM
eurjchem-610	188	8	;	;	PUNCT
eurjchem-610	188	9	n	n	CCONJ
eurjchem-610	188	10	,	,	PUNCT
eurjchem-610	188	11	13.12	13.12	NUM
eurjchem-610	188	12	%	%	NOUN
eurjchem-610	188	13	.	.	PUNCT
eurjchem-610	189	1	[	[	X
eurjchem-610	189	2	(	(	PUNCT
eurjchem-610	189	3	s)(‐	s)(‐	PROPN
eurjchem-610	189	4	)	)	PUNCT
eurjchem-610	189	5	]	]	PUNCT
eurjchem-610	189	6	methyl	methyl	NOUN
eurjchem-610	190	1	[	[	X
eurjchem-610	190	2	n‐sulfamoyl]‐leucinate	n‐sulfamoyl]‐leucinate	X
eurjchem-610	190	3	(	(	PUNCT
eurjchem-610	190	4	10a	10a	NUM
eurjchem-610	190	5	):	):	PUNCT
eurjchem-610	190	6	yield	yield	NOUN
eurjchem-610	190	7	:	:	PUNCT
eurjchem-610	190	8	95	95	NUM
eurjchem-610	190	9	%	%	NOUN
eurjchem-610	190	10	.	.	PUNCT
eurjchem-610	191	1	rf	rf	NOUN
eurjchem-610	191	2	=	=	NOUN
eurjchem-610	191	3	0.47	0.47	NUM
eurjchem-610	191	4	(	(	PUNCT
eurjchem-610	191	5	ch2cl2	ch2cl2	NOUN
eurjchem-610	191	6	:	:	PUNCT
eurjchem-610	191	7	meoh	meoh	NOUN
eurjchem-610	191	8	,	,	PUNCT
eurjchem-610	191	9	9:1	9:1	NUM
eurjchem-610	191	10	)	)	PUNCT
eurjchem-610	191	11	.	.	PUNCT
eurjchem-610	192	1	m.p	m.p	PROPN
eurjchem-610	192	2	.	.	PROPN
eurjchem-610	192	3	:	:	PUNCT
eurjchem-610	193	1	58‐60	58‐60	NUM
eurjchem-610	193	2	°	°	ADP
eurjchem-610	193	3	c	c	X
eurjchem-610	193	4	.	.	PUNCT
eurjchem-610	194	1	[	[	X
eurjchem-610	194	2	α]d	α]d	NOUN
eurjchem-610	194	3	=	=	PUNCT
eurjchem-610	194	4	‐21.5	‐21.5	NOUN
eurjchem-610	194	5	°	°	NOUN
eurjchem-610	194	6	(	(	PUNCT
eurjchem-610	194	7	c	c	NOUN
eurjchem-610	194	8	=	=	SYM
eurjchem-610	194	9	1	1	NUM
eurjchem-610	194	10	,	,	PUNCT
eurjchem-610	194	11	meoh	meoh	PROPN
eurjchem-610	194	12	)	)	PUNCT
eurjchem-610	194	13	.	.	PUNCT
eurjchem-610	195	1	ft‐ir	ft‐ir	NOUN
eurjchem-610	195	2	(	(	PUNCT
eurjchem-610	195	3	kbr	kbr	PROPN
eurjchem-610	195	4	,	,	PUNCT
eurjchem-610	195	5	cm‐1	cm‐1	PROPN
eurjchem-610	195	6	):	):	PUNCT
eurjchem-610	195	7	1751	1751	NUM
eurjchem-610	195	8	(c	(c	PROPN
eurjchem-610	195	9	=	=	SYM
eurjchem-610	195	10	o	o	NOUN
eurjchem-610	195	11	)	)	PUNCT
eurjchem-610	195	12	,	,	PUNCT
eurjchem-610	195	13	1348	1348	NUM
eurjchem-610	195	14	,	,	PUNCT
eurjchem-610	195	15	1154	1154	NUM
eurjchem-610	195	16	(so2	(so2	NOUN
eurjchem-610	195	17	)	)	PUNCT
eurjchem-610	195	18	,	,	PUNCT
eurjchem-610	195	19	3310	3310	NUM
eurjchem-610	195	20	,	,	PUNCT
eurjchem-610	195	21	3251	3251	NUM
eurjchem-610	195	22	,	,	PUNCT
eurjchem-610	195	23	3282	3282	NUM
eurjchem-610	195	24	(nh	(nh	NOUN
eurjchem-610	195	25	)	)	PUNCT
eurjchem-610	195	26	.	.	PUNCT
eurjchem-610	196	1	1h	1h	NUM
eurjchem-610	196	2	nmr	nmr	NOUN
eurjchem-610	196	3	(	(	PUNCT
eurjchem-610	196	4	250	250	NUM
eurjchem-610	196	5	mhz	mhz	NOUN
eurjchem-610	196	6	,	,	PUNCT
eurjchem-610	196	7	cdcl3	cdcl3	PROPN
eurjchem-610	196	8	,	,	PUNCT
eurjchem-610	196	9	δ	δ	PROPN
eurjchem-610	196	10	,	,	PUNCT
eurjchem-610	196	11	ppm	ppm	NUM
eurjchem-610	196	12	):	):	PUNCT
eurjchem-610	196	13	5.20	5.20	NUM
eurjchem-610	196	14	(	(	PUNCT
eurjchem-610	196	15	s	s	PROPN
eurjchem-610	196	16	,	,	PUNCT
eurjchem-610	196	17	1h	1h	NUM
eurjchem-610	196	18	,	,	PUNCT
eurjchem-610	196	19	nh	nh	PROPN
eurjchem-610	196	20	exch	exch	PROPN
eurjchem-610	196	21	)	)	PUNCT
eurjchem-610	196	22	,	,	PUNCT
eurjchem-610	196	23	5.20	5.20	NUM
eurjchem-610	196	24	(	(	PUNCT
eurjchem-610	196	25	s	s	PROPN
eurjchem-610	196	26	,	,	PUNCT
eurjchem-610	196	27	2h	2h	NUM
eurjchem-610	196	28	,	,	PUNCT
eurjchem-610	196	29	nh2	nh2	PROPN
eurjchem-610	196	30	)	)	PUNCT
eurjchem-610	196	31	,	,	PUNCT
eurjchem-610	196	32	4.25	4.25	NUM
eurjchem-610	196	33	(	(	PUNCT
eurjchem-610	196	34	t	t	PROPN
eurjchem-610	196	35	,	,	PUNCT
eurjchem-610	196	36	j	j	PROPN
eurjchem-610	196	37	=	=	SYM
eurjchem-610	196	38	7.4	7.4	NUM
eurjchem-610	196	39	hz	hz	NOUN
eurjchem-610	196	40	,	,	PUNCT
eurjchem-610	196	41	1h	1h	NUM
eurjchem-610	196	42	,	,	PUNCT
eurjchem-610	196	43	c*h	c*h	PROPN
eurjchem-610	196	44	)	)	PUNCT
eurjchem-610	196	45	,	,	PUNCT
eurjchem-610	196	46	3.66	3.66	NUM
eurjchem-610	196	47	(	(	PUNCT
eurjchem-610	196	48	s	s	PROPN
eurjchem-610	196	49	,	,	PUNCT
eurjchem-610	196	50	3h	3h	NUM
eurjchem-610	196	51	,	,	PUNCT
eurjchem-610	196	52	och3	och3	ADJ
eurjchem-610	196	53	)	)	PUNCT
eurjchem-610	196	54	,	,	PUNCT
eurjchem-610	196	55	1.85	1.85	NUM
eurjchem-610	196	56	(	(	PUNCT
eurjchem-610	196	57	m	m	PROPN
eurjchem-610	196	58	,	,	PUNCT
eurjchem-610	196	59	1h	1h	NUM
eurjchem-610	196	60	,	,	PUNCT
eurjchem-610	196	61	ipr	ipr	PROPN
eurjchem-610	196	62	)	)	PUNCT
eurjchem-610	196	63	,	,	PUNCT
eurjchem-610	196	64	1.55	1.55	NUM
eurjchem-610	196	65	(	(	PUNCT
eurjchem-610	196	66	m	m	PROPN
eurjchem-610	196	67	,	,	PUNCT
eurjchem-610	196	68	2h	2h	NUM
eurjchem-610	196	69	,	,	PUNCT
eurjchem-610	196	70	ch2β	ch2β	NOUN
eurjchem-610	196	71	)	)	PUNCT
eurjchem-610	196	72	,	,	PUNCT
eurjchem-610	196	73	0.93	0.93	NUM
eurjchem-610	196	74	and	and	CCONJ
eurjchem-610	196	75	0.75	0.75	NUM
eurjchem-610	196	76	(	(	PUNCT
eurjchem-610	196	77	2d	2d	NUM
eurjchem-610	196	78	,	,	PUNCT
eurjchem-610	196	79	j	j	PROPN
eurjchem-610	196	80	=	=	SYM
eurjchem-610	196	81	2.9	2.9	NUM
eurjchem-610	196	82	hz	hz	NOUN
eurjchem-610	196	83	,	,	PUNCT
eurjchem-610	196	84	6h	6h	NUM
eurjchem-610	196	85	,	,	PUNCT
eurjchem-610	196	86	2ch3	2ch3	NUM
eurjchem-610	196	87	)	)	PUNCT
eurjchem-610	196	88	.	.	PUNCT
eurjchem-610	197	1	13c	13c	NOUN
eurjchem-610	197	2	nmr	nmr	NOUN
eurjchem-610	197	3	(	(	PUNCT
eurjchem-610	197	4	62.89	62.89	NUM
eurjchem-610	197	5	mhz	mhz	NOUN
eurjchem-610	197	6	,	,	PUNCT
eurjchem-610	197	7	cdcl3	cdcl3	PROPN
eurjchem-610	197	8	,	,	PUNCT
eurjchem-610	197	9	δ	δ	PROPN
eurjchem-610	197	10	,	,	PUNCT
eurjchem-610	197	11	ppm	ppm	NOUN
eurjchem-610	197	12	):	):	PUNCT
eurjchem-610	197	13	21.05	21.05	NUM
eurjchem-610	197	14	,	,	PUNCT
eurjchem-610	197	15	22.50	22.50	NUM
eurjchem-610	197	16	,	,	PUNCT
eurjchem-610	197	17	23.50	23.50	NUM
eurjchem-610	197	18	,	,	PUNCT
eurjchem-610	197	19	41.90	41.90	NUM
eurjchem-610	197	20	,	,	PUNCT
eurjchem-610	197	21	52.20	52.20	NUM
eurjchem-610	197	22	,	,	PUNCT
eurjchem-610	197	23	57.4	57.4	NUM
eurjchem-610	197	24	,	,	PUNCT
eurjchem-610	197	25	172.28	172.28	NUM
eurjchem-610	197	26	.	.	PUNCT
eurjchem-610	198	1	ms	ms	NOUN
eurjchem-610	198	2	(	(	PUNCT
eurjchem-610	198	3	esi+	esi+	PROPN
eurjchem-610	198	4	,	,	PUNCT
eurjchem-610	198	5	30	30	NUM
eurjchem-610	198	6	ev	ev	NOUN
eurjchem-610	198	7	,	,	PUNCT
eurjchem-610	198	8	m	m	PROPN
eurjchem-610	198	9	/	/	SYM
eurjchem-610	198	10	z	z	NOUN
eurjchem-610	198	11	,	,	PUNCT
eurjchem-610	198	12	(	(	PUNCT
eurjchem-610	198	13	i	i	PRON
eurjchem-610	198	14	rel	rel	VERB
eurjchem-610	198	15	,	,	PUNCT
eurjchem-610	198	16	%	%	INTJ
eurjchem-610	198	17	)	)	PUNCT
eurjchem-610	198	18	):	):	PUNCT
eurjchem-610	198	19	225	225	NUM
eurjchem-610	198	20	[	[	X
eurjchem-610	198	21	m+h]+	m+h]+	X
eurjchem-610	198	22	(	(	PUNCT
eurjchem-610	198	23	100	100	NUM
eurjchem-610	198	24	)	)	PUNCT
eurjchem-610	198	25	.	.	PUNCT
eurjchem-610	199	1	anal	anal	PROPN
eurjchem-610	199	2	.	.	PUNCT
eurjchem-610	199	3	calcd	calcd	NOUN
eurjchem-610	199	4	.	.	PUNCT
eurjchem-610	200	1	for	for	SCONJ
eurjchem-610	200	2	c7h16n2o2s	c7h16n2o2s	NOUN
eurjchem-610	200	3	:	:	PUNCT
eurjchem-610	200	4	c	c	X
eurjchem-610	200	5	,	,	PUNCT
eurjchem-610	200	6	37.50	37.50	NUM
eurjchem-610	200	7	;	;	PUNCT
eurjchem-610	200	8	h	h	NOUN
eurjchem-610	200	9	,	,	PUNCT
eurjchem-610	200	10	7.14	7.14	NUM
eurjchem-610	200	11	;	;	PUNCT
eurjchem-610	200	12	n	n	CCONJ
eurjchem-610	200	13	,	,	PUNCT
eurjchem-610	200	14	12.50	12.50	NUM
eurjchem-610	200	15	.	.	PUNCT
eurjchem-610	200	16	found	find	VERB
eurjchem-610	200	17	:	:	PUNCT
eurjchem-610	201	1	c	c	X
eurjchem-610	201	2	,	,	PUNCT
eurjchem-610	201	3	37.46	37.46	NUM
eurjchem-610	201	4	;	;	PUNCT
eurjchem-610	201	5	h	h	NOUN
eurjchem-610	201	6	,	,	PUNCT
eurjchem-610	201	7	7.13	7.13	NUM
eurjchem-610	201	8	;	;	PUNCT
eurjchem-610	201	9	n	n	CCONJ
eurjchem-610	201	10	,	,	PUNCT
eurjchem-610	201	11	12.54	12.54	NUM
eurjchem-610	201	12	%	%	NOUN
eurjchem-610	201	13	.	.	PUNCT
eurjchem-610	202	1	[	[	X
eurjchem-610	202	2	(	(	PUNCT
eurjchem-610	202	3	s)(+	s)(+	PROPN
eurjchem-610	202	4	)	)	PUNCT
eurjchem-610	202	5	]	]	PUNCT
eurjchem-610	203	1	methyl	methyl	NOUN
eurjchem-610	204	1	[	[	X
eurjchem-610	204	2	n‐sulfamoyl]‐phenylalaninate	n‐sulfamoyl]‐phenylalaninate	PROPN
eurjchem-610	204	3	(	(	PUNCT
eurjchem-610	204	4	11a	11a	NUM
eurjchem-610	204	5	):	):	PUNCT
eurjchem-610	204	6	yield	yield	NOUN
eurjchem-610	204	7	:	:	PUNCT
eurjchem-610	204	8	92	92	NUM
eurjchem-610	204	9	%	%	NOUN
eurjchem-610	204	10	.	.	PUNCT
eurjchem-610	205	1	rf	rf	NOUN
eurjchem-610	205	2	=	=	NOUN
eurjchem-610	205	3	0.53	0.53	NUM
eurjchem-610	205	4	(	(	PUNCT
eurjchem-610	205	5	ch2cl2	ch2cl2	NOUN
eurjchem-610	205	6	:	:	PUNCT
eurjchem-610	205	7	meoh	meoh	NOUN
eurjchem-610	205	8	,	,	PUNCT
eurjchem-610	205	9	9:1	9:1	NUM
eurjchem-610	205	10	)	)	PUNCT
eurjchem-610	205	11	.	.	PUNCT
eurjchem-610	206	1	m.p	m.p	PROPN
eurjchem-610	206	2	.	.	PROPN
eurjchem-610	206	3	:	:	PUNCT
eurjchem-610	206	4	64‐65	64‐65	NUM
eurjchem-610	206	5	°	°	ADP
eurjchem-610	206	6	c	c	NOUN
eurjchem-610	206	7	.	.	PUNCT
eurjchem-610	207	1	[	[	X
eurjchem-610	207	2	α]d	α]d	NOUN
eurjchem-610	207	3	=	=	PUNCT
eurjchem-610	207	4	+45	+45	NOUN
eurjchem-610	207	5	°	°	PRON
eurjchem-610	207	6	(	(	PUNCT
eurjchem-610	207	7	c	c	NOUN
eurjchem-610	207	8	=	=	SYM
eurjchem-610	207	9	1	1	NUM
eurjchem-610	207	10	,	,	PUNCT
eurjchem-610	207	11	meoh	meoh	PROPN
eurjchem-610	207	12	)	)	PUNCT
eurjchem-610	207	13	.	.	PUNCT
eurjchem-610	208	1	ft‐ir	ft‐ir	NOUN
eurjchem-610	208	2	(	(	PUNCT
eurjchem-610	208	3	kbr	kbr	PROPN
eurjchem-610	208	4	,	,	PUNCT
eurjchem-610	208	5	cm‐1	cm‐1	PROPN
eurjchem-610	208	6	):	):	PUNCT
eurjchem-610	208	7	1745	1745	NUM
eurjchem-610	208	8	(c	(c	PROPN
eurjchem-610	208	9	=	=	SYM
eurjchem-610	208	10	o	o	NOUN
eurjchem-610	208	11	)	)	PUNCT
eurjchem-610	208	12	,	,	PUNCT
eurjchem-610	208	13	1338	1338	NUM
eurjchem-610	208	14	and	and	CCONJ
eurjchem-610	208	15	1152	1152	NUM
eurjchem-610	208	16	(so2	(so2	NOUN
eurjchem-610	208	17	)	)	PUNCT
eurjchem-610	208	18	,	,	PUNCT
eurjchem-610	208	19	3312	3312	NUM
eurjchem-610	208	20	,	,	PUNCT
eurjchem-610	208	21	3245	3245	NUM
eurjchem-610	208	22	,	,	PUNCT
eurjchem-610	208	23	3482	3482	NUM
eurjchem-610	208	24	(nh	(nh	NOUN
eurjchem-610	208	25	)	)	PUNCT
eurjchem-610	208	26	.	.	PUNCT
eurjchem-610	209	1	1h	1h	NUM
eurjchem-610	209	2	nmr	nmr	NOUN
eurjchem-610	209	3	(	(	PUNCT
eurjchem-610	209	4	250	250	NUM
eurjchem-610	209	5	mhz	mhz	NOUN
eurjchem-610	209	6	,	,	PUNCT
eurjchem-610	209	7	cdcl3	cdcl3	PROPN
eurjchem-610	209	8	,	,	PUNCT
eurjchem-610	209	9	δ	δ	PROPN
eurjchem-610	209	10	,	,	PUNCT
eurjchem-610	209	11	ppm	ppm	NUM
eurjchem-610	209	12	):	):	PUNCT
eurjchem-610	209	13	7.25	7.25	NUM
eurjchem-610	209	14	(	(	PUNCT
eurjchem-610	209	15	m	m	PROPN
eurjchem-610	209	16	,	,	PUNCT
eurjchem-610	209	17	5h	5h	NUM
eurjchem-610	209	18	,	,	PUNCT
eurjchem-610	209	19	ar‐h	ar‐h	NOUN
eurjchem-610	209	20	)	)	PUNCT
eurjchem-610	209	21	,	,	PUNCT
eurjchem-610	209	22	5.60	5.60	NUM
eurjchem-610	209	23	(	(	PUNCT
eurjchem-610	209	24	d	d	PROPN
eurjchem-610	209	25	,	,	PUNCT
eurjchem-610	209	26	1h	1h	NUM
eurjchem-610	209	27	,	,	PUNCT
eurjchem-610	209	28	j	j	PROPN
eurjchem-610	209	29	=	=	SYM
eurjchem-610	209	30	8.8	8.8	NUM
eurjchem-610	209	31	hz	hz	NOUN
eurjchem-610	209	32	,	,	PUNCT
eurjchem-610	209	33	nh	nh	PROPN
eurjchem-610	209	34	)	)	PUNCT
eurjchem-610	209	35	,	,	PUNCT
eurjchem-610	209	36	4.90	4.90	NUM
eurjchem-610	209	37	(	(	PUNCT
eurjchem-610	209	38	s	s	PROPN
eurjchem-610	209	39	,	,	PUNCT
eurjchem-610	209	40	2h	2h	NUM
eurjchem-610	209	41	,	,	PUNCT
eurjchem-610	209	42	nh2	nh2	PROPN
eurjchem-610	209	43	)	)	PUNCT
eurjchem-610	209	44	,	,	PUNCT
eurjchem-610	209	45	4.40	4.40	NUM
eurjchem-610	209	46	(	(	PUNCT
eurjchem-610	209	47	dt	dt	PROPN
eurjchem-610	209	48	,	,	PUNCT
eurjchem-610	209	49	j	j	PROPN
eurjchem-610	209	50	=	=	SYM
eurjchem-610	209	51	5.5	5.5	NUM
eurjchem-610	209	52	hz	hz	NOUN
eurjchem-610	209	53	and	and	CCONJ
eurjchem-610	209	54	j	j	NOUN
eurjchem-610	209	55	’	'	PUNCT
eurjchem-610	209	56	=	=	SYM
eurjchem-610	209	57	8.8	8.8	NUM
eurjchem-610	209	58	hz	hz	NOUN
eurjchem-610	209	59	,	,	PUNCT
eurjchem-610	209	60	1h	1h	NUM
eurjchem-610	209	61	,	,	PUNCT
eurjchem-610	209	62	c*h	c*h	PROPN
eurjchem-610	209	63	)	)	PUNCT
eurjchem-610	209	64	,	,	PUNCT
eurjchem-610	209	65	3.65	3.65	NUM
eurjchem-610	209	66	(	(	PUNCT
eurjchem-610	209	67	s	s	PROPN
eurjchem-610	209	68	,	,	PUNCT
eurjchem-610	209	69	3h	3h	NUM
eurjchem-610	209	70	,	,	PUNCT
eurjchem-610	209	71	och3	och3	ADJ
eurjchem-610	209	72	)	)	PUNCT
eurjchem-610	209	73	,	,	PUNCT
eurjchem-610	209	74	3.00‐3.20	3.00‐3.20	NUM
eurjchem-610	209	75	(	(	PUNCT
eurjchem-610	209	76	2dd	2dd	NOUN
eurjchem-610	209	77	,	,	PUNCT
eurjchem-610	209	78	(	(	PUNCT
eurjchem-610	209	79	abx	abx	NOUN
eurjchem-610	209	80	system	system	NOUN
eurjchem-610	209	81	)	)	PUNCT
eurjchem-610	209	82	,	,	PUNCT
eurjchem-610	209	83	j1	j1	PROPN
eurjchem-610	209	84	=	=	SYM
eurjchem-610	209	85	5.7	5.7	NUM
eurjchem-610	209	86	,	,	PUNCT
eurjchem-610	209	87	j2	j2	PROPN
eurjchem-610	209	88	=	=	SYM
eurjchem-610	209	89	7.00	7.00	NUM
eurjchem-610	209	90	and	and	CCONJ
eurjchem-610	209	91	jgem	jgem	NOUN
eurjchem-610	210	1	=	=	SYM
eurjchem-610	210	2	13.8	13.8	NUM
eurjchem-610	210	3	hz	hz	NOUN
eurjchem-610	210	4	,	,	PUNCT
eurjchem-610	210	5	2h	2h	NUM
eurjchem-610	210	6	,	,	PUNCT
eurjchem-610	210	7	ch2	ch2	PROPN
eurjchem-610	210	8	)	)	PUNCT
eurjchem-610	210	9	.	.	PUNCT
eurjchem-610	211	1	13c	13c	NOUN
eurjchem-610	211	2	nmr	nmr	NOUN
eurjchem-610	211	3	(	(	PUNCT
eurjchem-610	211	4	62.89	62.89	NUM
eurjchem-610	211	5	mhz	mhz	NOUN
eurjchem-610	211	6	,	,	PUNCT
eurjchem-610	211	7	cdcl3	cdcl3	PROPN
eurjchem-610	211	8	,	,	PUNCT
eurjchem-610	211	9	δ	δ	PROPN
eurjchem-610	211	10	,	,	PUNCT
eurjchem-610	211	11	ppm	ppm	NOUN
eurjchem-610	211	12	):	):	PUNCT
eurjchem-610	211	13	39.5	39.5	NUM
eurjchem-610	211	14	,	,	PUNCT
eurjchem-610	211	15	52.5	52.5	NUM
eurjchem-610	211	16	,	,	PUNCT
eurjchem-610	211	17	58.6	58.6	NUM
eurjchem-610	211	18	,	,	PUNCT
eurjchem-610	211	19	127.7	127.7	NUM
eurjchem-610	211	20	,	,	PUNCT
eurjchem-610	211	21	129.8	129.8	NUM
eurjchem-610	211	22	,	,	PUNCT
eurjchem-610	211	23	129.9	129.9	NUM
eurjchem-610	211	24	,	,	PUNCT
eurjchem-610	211	25	137.3	137.3	NUM
eurjchem-610	211	26	,	,	PUNCT
eurjchem-610	211	27	173.5	173.5	NUM
eurjchem-610	211	28	.	.	PUNCT
eurjchem-610	212	1	ms	ms	NOUN
eurjchem-610	212	2	(	(	PUNCT
eurjchem-610	212	3	esi+	esi+	PROPN
eurjchem-610	212	4	,	,	PUNCT
eurjchem-610	212	5	30	30	NUM
eurjchem-610	212	6	ev	ev	NOUN
eurjchem-610	212	7	,	,	PUNCT
eurjchem-610	212	8	m	m	PROPN
eurjchem-610	212	9	/	/	SYM
eurjchem-610	212	10	z	z	NOUN
eurjchem-610	212	11	,	,	PUNCT
eurjchem-610	212	12	(	(	PUNCT
eurjchem-610	212	13	i	i	PRON
eurjchem-610	212	14	rel	rel	VERB
eurjchem-610	212	15	,	,	PUNCT
eurjchem-610	212	16	%	%	INTJ
eurjchem-610	212	17	)	)	PUNCT
eurjchem-610	212	18	):	):	PUNCT
eurjchem-610	212	19	259	259	NUM
eurjchem-610	213	1	[	[	X
eurjchem-610	213	2	m+h]+	m+h]+	X
eurjchem-610	213	3	(	(	PUNCT
eurjchem-610	213	4	100	100	NUM
eurjchem-610	213	5	)	)	PUNCT
eurjchem-610	213	6	.	.	PUNCT
eurjchem-610	214	1	anal	anal	PROPN
eurjchem-610	214	2	.	.	PUNCT
eurjchem-610	214	3	calcd	calcd	NOUN
eurjchem-610	214	4	.	.	PUNCT
eurjchem-610	215	1	for	for	SCONJ
eurjchem-610	215	2	c10h14n2o2s	c10h14n2o2s	PROPN
eurjchem-610	215	3	:	:	PUNCT
eurjchem-610	215	4	c,46.51	c,46.51	NOUN
eurjchem-610	215	5	;	;	PUNCT
eurjchem-610	215	6	h	h	NOUN
eurjchem-610	215	7	,	,	PUNCT
eurjchem-610	215	8	5.42	5.42	NUM
eurjchem-610	215	9	;	;	PUNCT
eurjchem-610	215	10	n	n	CCONJ
eurjchem-610	215	11	,	,	PUNCT
eurjchem-610	215	12	10.85	10.85	NUM
eurjchem-610	215	13	.	.	PUNCT
eurjchem-610	215	14	found	find	VERB
eurjchem-610	215	15	:	:	PUNCT
eurjchem-610	216	1	c	c	X
eurjchem-610	216	2	,	,	PUNCT
eurjchem-610	216	3	46.49	46.49	NUM
eurjchem-610	216	4	;	;	PUNCT
eurjchem-610	216	5	h	h	NOUN
eurjchem-610	216	6	,	,	PUNCT
eurjchem-610	216	7	5.39	5.39	NUM
eurjchem-610	216	8	;	;	PUNCT
eurjchem-610	216	9	n	n	CCONJ
eurjchem-610	216	10	,	,	PUNCT
eurjchem-610	216	11	10.80	10.80	NUM
eurjchem-610	216	12	%	%	NOUN
eurjchem-610	216	13	.	.	PUNCT
eurjchem-610	217	1	2.1.7	2.1.7	X
eurjchem-610	217	2	.	.	PUNCT
eurjchem-610	217	3	general	general	ADJ
eurjchem-610	217	4	procedure	procedure	NOUN
eurjchem-610	217	5	of	of	ADP
eurjchem-610	217	6	the	the	DET
eurjchem-610	217	7	deprotection	deprotection	NOUN
eurjchem-610	217	8	of	of	ADP
eurjchem-610	217	9	n‐boc	n‐boc	DET
eurjchem-610	217	10	amines	amine	NOUN
eurjchem-610	217	11	(	(	PUNCT
eurjchem-610	217	12	12‐16	12‐16	NOUN
eurjchem-610	217	13	)	)	PUNCT
eurjchem-610	217	14	to	to	ADP
eurjchem-610	217	15	a	a	DET
eurjchem-610	217	16	mixture	mixture	NOUN
eurjchem-610	217	17	of	of	ADP
eurjchem-610	217	18	n‐boc	n‐boc	DET
eurjchem-610	217	19	amine	amine	ADJ
eurjchem-610	217	20	(	(	PUNCT
eurjchem-610	217	21	12‐16	12‐16	NUM
eurjchem-610	217	22	)	)	PUNCT
eurjchem-610	217	23	(	(	PUNCT
eurjchem-610	217	24	1	1	NUM
eurjchem-610	217	25	mmol	mmol	NOUN
eurjchem-610	217	26	)	)	PUNCT
eurjchem-610	217	27	and	and	CCONJ
eurjchem-610	217	28	h6p2w18o62.14h2o	h6p2w18o62.14h2o	NOUN
eurjchem-610	217	29	(	(	PUNCT
eurjchem-610	217	30	10	10	NUM
eurjchem-610	217	31	%	%	NOUN
eurjchem-610	217	32	mmol	mmol	NOUN
eurjchem-610	217	33	)	)	PUNCT
eurjchem-610	217	34	in	in	ADP
eurjchem-610	217	35	5	5	NUM
eurjchem-610	217	36	ml	ml	NOUN
eurjchem-610	217	37	of	of	ADP
eurjchem-610	217	38	ch2cl2	ch2cl2	NOUN
eurjchem-610	217	39	was	be	AUX
eurjchem-610	217	40	stirred	stir	VERB
eurjchem-610	217	41	at	at	ADP
eurjchem-610	217	42	room	room	NOUN
eurjchem-610	217	43	temperature	temperature	NOUN
eurjchem-610	217	44	for	for	ADP
eurjchem-610	217	45	20	20	NUM
eurjchem-610	217	46	min	min	NOUN
eurjchem-610	217	47	.	.	PUNCT
eurjchem-610	218	1	the	the	DET
eurjchem-610	218	2	catalyst	catalyst	NOUN
eurjchem-610	218	3	was	be	AUX
eurjchem-610	218	4	removed	remove	VERB
eurjchem-610	218	5	by	by	ADP
eurjchem-610	218	6	filtration	filtration	NOUN
eurjchem-610	218	7	and	and	CCONJ
eurjchem-610	218	8	was	be	AUX
eurjchem-610	218	9	washed	wash	VERB
eurjchem-610	218	10	with	with	ADP
eurjchem-610	218	11	toluene	toluene	NOUN
eurjchem-610	218	12	(	(	PUNCT
eurjchem-610	218	13	1	1	NUM
eurjchem-610	218	14	ml	ml	NOUN
eurjchem-610	218	15	)	)	PUNCT
eurjchem-610	218	16	.	.	PUNCT
eurjchem-610	219	1	the	the	DET
eurjchem-610	219	2	solution	solution	NOUN
eurjchem-610	219	3	was	be	AUX
eurjchem-610	219	4	concentrated	concentrate	VERB
eurjchem-610	219	5	and	and	CCONJ
eurjchem-610	219	6	the	the	DET
eurjchem-610	219	7	residue	residue	NOUN
eurjchem-610	219	8	was	be	AUX
eurjchem-610	219	9	generally	generally	ADV
eurjchem-610	219	10	subjected	subject	VERB
eurjchem-610	219	11	to	to	ADP
eurjchem-610	219	12	column	column	NOUN
eurjchem-610	219	13	chromatography	chromatography	NOUN
eurjchem-610	219	14	on	on	ADP
eurjchem-610	219	15	silica	silica	NOUN
eurjchem-610	219	16	to	to	PART
eurjchem-610	219	17	give	give	VERB
eurjchem-610	219	18	the	the	DET
eurjchem-610	219	19	corresponding	correspond	VERB
eurjchem-610	219	20	amine	amine	NOUN
eurjchem-610	219	21	.	.	PUNCT
eurjchem-610	220	1	the	the	DET
eurjchem-610	220	2	products	product	NOUN
eurjchem-610	220	3	12a	12a	NOUN
eurjchem-610	220	4	triethylamine	triethylamine	NOUN
eurjchem-610	220	5	,	,	PUNCT
eurjchem-610	220	6	13a	13a	PROPN
eurjchem-610	220	7	aniline	aniline	PROPN
eurjchem-610	220	8	,	,	PUNCT
eurjchem-610	220	9	14a	14a	NOUN
eurjchem-610	220	10	benylamine	benylamine	NOUN
eurjchem-610	220	11	,	,	PUNCT
eurjchem-610	220	12	15a	15a	NOUN
eurjchem-610	220	13	morpholine	morpholine	PROPN
eurjchem-610	220	14	are	be	AUX
eurjchem-610	220	15	commercially	commercially	ADV
eurjchem-610	220	16	available	available	ADJ
eurjchem-610	220	17	and	and	CCONJ
eurjchem-610	220	18	were	be	AUX
eurjchem-610	220	19	identified	identify	VERB
eurjchem-610	220	20	by	by	ADP
eurjchem-610	220	21	comparison	comparison	NOUN
eurjchem-610	220	22	of	of	ADP
eurjchem-610	220	23	analytical	analytical	ADJ
eurjchem-610	220	24	data	datum	NOUN
eurjchem-610	220	25	(	(	PUNCT
eurjchem-610	220	26	tlc	tlc	NOUN
eurjchem-610	220	27	and	and	CCONJ
eurjchem-610	220	28	ir	ir	NOUN
eurjchem-610	220	29	)	)	PUNCT
eurjchem-610	220	30	with	with	ADP
eurjchem-610	220	31	those	those	PRON
eurjchem-610	220	32	reported	report	VERB
eurjchem-610	220	33	or	or	CCONJ
eurjchem-610	220	34	with	with	ADP
eurjchem-610	220	35	authentic	authentic	ADJ
eurjchem-610	220	36	samples	sample	NOUN
eurjchem-610	220	37	prepared	prepare	VERB
eurjchem-610	220	38	by	by	ADP
eurjchem-610	220	39	the	the	DET
eurjchem-610	220	40	conventional	conventional	ADJ
eurjchem-610	220	41	method	method	NOUN
eurjchem-610	220	42	(	(	PUNCT
eurjchem-610	220	43	scheme	scheme	NOUN
eurjchem-610	220	44	4	4	NUM
eurjchem-610	220	45	)	)	PUNCT
eurjchem-610	220	46	.	.	PUNCT
eurjchem-610	221	1	[	[	X
eurjchem-610	221	2	(	(	PUNCT
eurjchem-610	221	3	2s)(3s)(+)]2‐amino‐3‐(benzyloxy)butanoic	2s)(3s)(+)]2‐amino‐3‐(benzyloxy)butanoic	ADJ
eurjchem-610	221	4	acid	acid	NOUN
eurjchem-610	221	5	(	(	PUNCT
eurjchem-610	221	6	16a	16a	NOUN
eurjchem-610	221	7	):	):	PUNCT
eurjchem-610	221	8	yield	yield	NOUN
eurjchem-610	221	9	:	:	PUNCT
eurjchem-610	221	10	90	90	NUM
eurjchem-610	221	11	%	%	NOUN
eurjchem-610	221	12	.	.	PUNCT
eurjchem-610	222	1	rf	rf	NOUN
eurjchem-610	222	2	=	=	SYM
eurjchem-610	222	3	0.58	0.58	NUM
eurjchem-610	222	4	(	(	PUNCT
eurjchem-610	222	5	ch2cl2	ch2cl2	NOUN
eurjchem-610	222	6	:	:	PUNCT
eurjchem-610	222	7	meoh	meoh	NOUN
eurjchem-610	222	8	,	,	PUNCT
eurjchem-610	222	9	9:1	9:1	NUM
eurjchem-610	222	10	)	)	PUNCT
eurjchem-610	222	11	.	.	PUNCT
eurjchem-610	223	1	m.p	m.p	PROPN
eurjchem-610	223	2	.	.	PROPN
eurjchem-610	223	3	:	:	PUNCT
eurjchem-610	224	1	94‐95	94‐95	NUM
eurjchem-610	225	1	°	°	ADP
eurjchem-610	225	2	c	c	NOUN
eurjchem-610	225	3	.	.	PUNCT
eurjchem-610	226	1	[	[	X
eurjchem-610	226	2	α]d	α]d	NOUN
eurjchem-610	226	3	=	=	SYM
eurjchem-610	226	4	+32	+32	NOUN
eurjchem-610	226	5	°	°	NOUN
eurjchem-610	226	6	(	(	PUNCT
eurjchem-610	226	7	c	c	NOUN
eurjchem-610	226	8	=	=	SYM
eurjchem-610	226	9	1	1	NUM
eurjchem-610	226	10	,	,	PUNCT
eurjchem-610	226	11	meoh	meoh	PROPN
eurjchem-610	226	12	)	)	PUNCT
eurjchem-610	226	13	.	.	PUNCT
eurjchem-610	227	1	ft‐ir	ft‐ir	NOUN
eurjchem-610	227	2	(	(	PUNCT
eurjchem-610	227	3	kbr	kbr	PROPN
eurjchem-610	227	4	,	,	PUNCT
eurjchem-610	227	5	cm‐1	cm‐1	PROPN
eurjchem-610	227	6	):	):	PUNCT
eurjchem-610	227	7	1708	1708	NUM
eurjchem-610	227	8	(c	(c	PROPN
eurjchem-610	227	9	=	=	SYM
eurjchem-610	227	10	o	o	NOUN
eurjchem-610	227	11	)	)	PUNCT
eurjchem-610	227	12	,	,	PUNCT
eurjchem-610	227	13	3308	3308	NUM
eurjchem-610	227	14	,	,	PUNCT
eurjchem-610	227	15	3241	3241	NUM
eurjchem-610	227	16	,	,	PUNCT
eurjchem-610	227	17	3479	3479	NUM
eurjchem-610	227	18	(nh	(nh	NOUN
eurjchem-610	227	19	)	)	PUNCT
eurjchem-610	227	20	.	.	PUNCT
eurjchem-610	228	1	1h	1h	NUM
eurjchem-610	228	2	nmr	nmr	NOUN
eurjchem-610	228	3	(	(	PUNCT
eurjchem-610	228	4	250	250	NUM
eurjchem-610	228	5	mhz	mhz	NOUN
eurjchem-610	228	6	,	,	PUNCT
eurjchem-610	228	7	cdcl3	cdcl3	PROPN
eurjchem-610	228	8	,	,	PUNCT
eurjchem-610	228	9	δ	δ	PROPN
eurjchem-610	228	10	,	,	PUNCT
eurjchem-610	228	11	ppm	ppm	NOUN
eurjchem-610	228	12	):	):	PUNCT
eurjchem-610	228	13	11.10	11.10	NUM
eurjchem-610	228	14	(	(	PUNCT
eurjchem-610	228	15	s	s	PROPN
eurjchem-610	228	16	,	,	PUNCT
eurjchem-610	228	17	1h	1h	NUM
eurjchem-610	228	18	,	,	PUNCT
eurjchem-610	228	19	oh	oh	INTJ
eurjchem-610	228	20	)	)	PUNCT
eurjchem-610	228	21	,	,	PUNCT
eurjchem-610	228	22	7.25‐7.40	7.25‐7.40	NUM
eurjchem-610	228	23	(	(	PUNCT
eurjchem-610	228	24	m	m	PROPN
eurjchem-610	228	25	,	,	PUNCT
eurjchem-610	228	26	5h	5h	NUM
eurjchem-610	228	27	,	,	PUNCT
eurjchem-610	228	28	ar‐h	ar‐h	NOUN
eurjchem-610	228	29	)	)	PUNCT
eurjchem-610	228	30	,	,	PUNCT
eurjchem-610	228	31	5.10	5.10	NUM
eurjchem-610	228	32	(	(	PUNCT
eurjchem-610	228	33	s	s	PROPN
eurjchem-610	228	34	,	,	PUNCT
eurjchem-610	228	35	2h	2h	NUM
eurjchem-610	228	36	,	,	PUNCT
eurjchem-610	228	37	nh2	nh2	PROPN
eurjchem-610	228	38	)	)	PUNCT
eurjchem-610	228	39	,	,	PUNCT
eurjchem-610	228	40	4.60	4.60	NUM
eurjchem-610	228	41	(	(	PUNCT
eurjchem-610	228	42	s	s	PROPN
eurjchem-610	228	43	,	,	PUNCT
eurjchem-610	228	44	2h	2h	NUM
eurjchem-610	228	45	,	,	PUNCT
eurjchem-610	228	46	och2	och2	PROPN
eurjchem-610	228	47	)	)	PUNCT
eurjchem-610	228	48	,	,	PUNCT
eurjchem-610	228	49	3.85	3.85	NUM
eurjchem-610	228	50	(	(	PUNCT
eurjchem-610	228	51	d	d	NOUN
eurjchem-610	228	52	,	,	PUNCT
eurjchem-610	228	53	j	j	PROPN
eurjchem-610	228	54	=	=	SYM
eurjchem-610	228	55	6.2	6.2	NUM
eurjchem-610	228	56	hz	hz	NOUN
eurjchem-610	228	57	,	,	PUNCT
eurjchem-610	228	58	1h	1h	NUM
eurjchem-610	228	59	,	,	PUNCT
eurjchem-610	228	60	ch	ch	NOUN
eurjchem-610	228	61	)	)	PUNCT
eurjchem-610	228	62	,	,	PUNCT
eurjchem-610	228	63	3.57	3.57	NUM
eurjchem-610	228	64	(	(	PUNCT
eurjchem-610	228	65	m	m	PROPN
eurjchem-610	228	66	,	,	PUNCT
eurjchem-610	228	67	1h	1h	NUM
eurjchem-610	228	68	,	,	PUNCT
eurjchem-610	228	69	ch	ch	NOUN
eurjchem-610	228	70	)	)	PUNCT
eurjchem-610	228	71	,	,	PUNCT
eurjchem-610	228	72	1.20	1.20	NUM
eurjchem-610	228	73	(	(	PUNCT
eurjchem-610	228	74	d	d	PROPN
eurjchem-610	228	75	,	,	PUNCT
eurjchem-610	228	76	j	j	PROPN
eurjchem-610	228	77	=	=	SYM
eurjchem-610	228	78	6.8	6.8	NUM
eurjchem-610	228	79	hz	hz	NOUN
eurjchem-610	228	80	,	,	PUNCT
eurjchem-610	228	81	3h	3h	NUM
eurjchem-610	228	82	,	,	PUNCT
eurjchem-610	228	83	ch3	ch3	PROPN
eurjchem-610	228	84	)	)	PUNCT
eurjchem-610	228	85	.	.	PUNCT
eurjchem-610	229	1	13c	13c	NOUN
eurjchem-610	229	2	nmr	nmr	NOUN
eurjchem-610	229	3	(	(	PUNCT
eurjchem-610	229	4	62.89	62.89	NUM
eurjchem-610	229	5	mhz	mhz	NOUN
eurjchem-610	229	6	,	,	PUNCT
eurjchem-610	229	7	cdcl3	cdcl3	PROPN
eurjchem-610	229	8	,	,	PUNCT
eurjchem-610	229	9	δ	δ	PROPN
eurjchem-610	229	10	,	,	PUNCT
eurjchem-610	229	11	ppm	ppm	NOUN
eurjchem-610	229	12	):	):	PUNCT
eurjchem-610	229	13	17.8	17.8	NUM
eurjchem-610	229	14	,	,	PUNCT
eurjchem-610	229	15	60.9	60.9	NUM
eurjchem-610	229	16	,	,	PUNCT
eurjchem-610	229	17	72.6	72.6	NUM
eurjchem-610	229	18	,	,	PUNCT
eurjchem-610	229	19	85.3	85.3	NUM
eurjchem-610	229	20	,	,	PUNCT
eurjchem-610	229	21	127.7	127.7	NUM
eurjchem-610	229	22	,	,	PUNCT
eurjchem-610	229	23	128.2	128.2	NUM
eurjchem-610	229	24	,	,	PUNCT
eurjchem-610	229	25	128.9	128.9	NUM
eurjchem-610	229	26	,	,	PUNCT
eurjchem-610	229	27	137.3	137.3	NUM
eurjchem-610	229	28	,	,	PUNCT
eurjchem-610	229	29	174.5	174.5	NUM
eurjchem-610	229	30	.	.	PUNCT
eurjchem-610	230	1	ms	ms	NOUN
eurjchem-610	230	2	(	(	PUNCT
eurjchem-610	230	3	esi+	esi+	PROPN
eurjchem-610	230	4	,	,	PUNCT
eurjchem-610	230	5	30	30	NUM
eurjchem-610	230	6	ev	ev	NOUN
eurjchem-610	230	7	,	,	PUNCT
eurjchem-610	230	8	m	m	PROPN
eurjchem-610	230	9	/	/	SYM
eurjchem-610	230	10	z	z	NOUN
eurjchem-610	230	11	,	,	PUNCT
eurjchem-610	230	12	(	(	PUNCT
eurjchem-610	230	13	i	i	PRON
eurjchem-610	230	14	rel	rel	VERB
eurjchem-610	230	15	,	,	PUNCT
eurjchem-610	230	16	%	%	NOUN
eurjchem-610	230	17	)	)	PUNCT
eurjchem-610	230	18	):	):	PUNCT
eurjchem-610	230	19	210	210	NUM
eurjchem-610	231	1	[	[	X
eurjchem-610	231	2	m+h]+	m+h]+	X
eurjchem-610	231	3	(	(	PUNCT
eurjchem-610	231	4	100	100	NUM
eurjchem-610	231	5	)	)	PUNCT
eurjchem-610	231	6	.	.	PUNCT
eurjchem-610	232	1	anal	anal	PROPN
eurjchem-610	232	2	.	.	PUNCT
eurjchem-610	232	3	calcd	calcd	NOUN
eurjchem-610	232	4	.	.	PUNCT
eurjchem-610	233	1	for	for	ADP
eurjchem-610	233	2	c11h15no3	c11h15no3	PROPN
eurjchem-610	233	3	:	:	PUNCT
eurjchem-610	233	4	c,63.15	c,63.15	NOUN
eurjchem-610	233	5	;	;	PUNCT
eurjchem-610	233	6	h	h	NOUN
eurjchem-610	233	7	,	,	PUNCT
eurjchem-610	233	8	7.18	7.18	NUM
eurjchem-610	233	9	;	;	PUNCT
eurjchem-610	233	10	n	n	CCONJ
eurjchem-610	233	11	,	,	PUNCT
eurjchem-610	233	12	6.70	6.70	NUM
eurjchem-610	233	13	.	.	PUNCT
eurjchem-610	233	14	found	find	VERB
eurjchem-610	233	15	:	:	PUNCT
eurjchem-610	234	1	c	c	X
eurjchem-610	234	2	,	,	PUNCT
eurjchem-610	234	3	63.09	63.09	NUM
eurjchem-610	234	4	;	;	PUNCT
eurjchem-610	234	5	h	h	X
eurjchem-610	234	6	,	,	PUNCT
eurjchem-610	234	7	7.18	7.18	NUM
eurjchem-610	234	8	;	;	PUNCT
eurjchem-610	234	9	n	n	CCONJ
eurjchem-610	234	10	,	,	PUNCT
eurjchem-610	234	11	6.80	6.80	NUM
eurjchem-610	234	12	%	%	NOUN
eurjchem-610	234	13	.	.	PUNCT
eurjchem-610	235	1	3	3	X
eurjchem-610	235	2	.	.	NOUN
eurjchem-610	235	3	results	result	NOUN
eurjchem-610	235	4	and	and	CCONJ
eurjchem-610	235	5	discussion	discussion	NOUN
eurjchem-610	235	6	in	in	ADP
eurjchem-610	235	7	recent	recent	ADJ
eurjchem-610	235	8	years	year	NOUN
eurjchem-610	235	9	,	,	PUNCT
eurjchem-610	235	10	there	there	PRON
eurjchem-610	235	11	has	have	AUX
eurjchem-610	235	12	been	be	AUX
eurjchem-610	235	13	great	great	ADJ
eurjchem-610	235	14	interest	interest	NOUN
eurjchem-610	235	15	in	in	ADP
eurjchem-610	235	16	the	the	DET
eurjchem-610	235	17	reactions	reaction	NOUN
eurjchem-610	235	18	performed	perform	VERB
eurjchem-610	235	19	under	under	ADP
eurjchem-610	235	20	heterogeneous	heterogeneous	ADJ
eurjchem-610	235	21	catalysis	catalysis	NOUN
eurjchem-610	235	22	,	,	PUNCT
eurjchem-610	235	23	because	because	SCONJ
eurjchem-610	235	24	of	of	ADP
eurjchem-610	235	25	the	the	DET
eurjchem-610	235	26	possibility	possibility	NOUN
eurjchem-610	235	27	of	of	ADP
eurjchem-610	235	28	recovering	recover	VERB
eurjchem-610	235	29	and	and	CCONJ
eurjchem-610	235	30	recycling	recycle	VERB
eurjchem-610	235	31	the	the	DET
eurjchem-610	235	32	acid	acid	NOUN
eurjchem-610	235	33	catalyst	catalyst	NOUN
eurjchem-610	235	34	,	,	PUNCT
eurjchem-610	235	35	largely	largely	ADV
eurjchem-610	235	36	reducing	reduce	VERB
eurjchem-610	235	37	the	the	DET
eurjchem-610	235	38	environmental	environmental	ADJ
eurjchem-610	235	39	impact	impact	NOUN
eurjchem-610	235	40	.	.	PUNCT
eurjchem-610	236	1	308	308	NUM
eurjchem-610	236	2	belghiche	belghiche	NOUN
eurjchem-610	236	3	et	et	PROPN
eurjchem-610	236	4	al	al	PROPN
eurjchem-610	236	5	.	.	PUNCT
eurjchem-610	236	6	/	/	SYM
eurjchem-610	236	7	european	european	PROPN
eurjchem-610	236	8	journal	journal	PROPN
eurjchem-610	236	9	of	of	ADP
eurjchem-610	236	10	chemistry	chemistry	NOUN
eurjchem-610	236	11	3	3	NUM
eurjchem-610	236	12	(	(	PUNCT
eurjchem-610	236	13	3	3	NUM
eurjchem-610	236	14	)	)	PUNCT
eurjchem-610	236	15	(	(	PUNCT
eurjchem-610	236	16	2012	2012	NUM
eurjchem-610	236	17	)	)	PUNCT
eurjchem-610	236	18	305‐309	305‐309	PROPN
eurjchem-610	236	19	scheme	scheme	NOUN
eurjchem-610	236	20	3	3	NUM
eurjchem-610	236	21	r	r	NOUN
eurjchem-610	236	22	=	=	NOUN
eurjchem-610	236	23	see	see	VERB
eurjchem-610	236	24	table	table	NOUN
eurjchem-610	236	25	1	1	NUM
eurjchem-610	236	26	scheme	scheme	NOUN
eurjchem-610	236	27	4	4	NUM
eurjchem-610	236	28	table	table	NOUN
eurjchem-610	236	29	1	1	NUM
eurjchem-610	236	30	.	.	PUNCT
eurjchem-610	236	31	dawsonheteropolyacid	dawsonheteropolyacid	ADJ
eurjchem-610	236	32	catalysed	catalyse	VERB
eurjchem-610	236	33	cleavage	cleavage	NOUN
eurjchem-610	236	34	of	of	ADP
eurjchem-610	236	35	n‐boc	n‐boc	DET
eurjchem-610	236	36	amines	amine	NOUN
eurjchem-610	236	37	.	.	PUNCT
eurjchem-610	237	1	entry	entry	NOUN
eurjchem-610	237	2	substrat	substrat	NOUN
eurjchem-610	237	3	product	product	NOUN
eurjchem-610	237	4	this	this	DET
eurjchem-610	237	5	study	study	NOUN
eurjchem-610	237	6	literature	literature	NOUN
eurjchem-610	237	7	[	[	X
eurjchem-610	237	8	27	27	NUM
eurjchem-610	237	9	]	]	SYM
eurjchem-610	237	10	time	time	NOUN
eurjchem-610	237	11	(	(	PUNCT
eurjchem-610	237	12	min	min	NOUN
eurjchem-610	237	13	)	)	PUNCT
eurjchem-610	237	14	yield	yield	NOUN
eurjchem-610	237	15	(	(	PUNCT
eurjchem-610	237	16	%	%	NOUN
eurjchem-610	237	17	)	)	PUNCT
eurjchem-610	237	18	time	time	NOUN
eurjchem-610	237	19	(	(	PUNCT
eurjchem-610	237	20	h	h	NOUN
eurjchem-610	237	21	)	)	PUNCT
eurjchem-610	237	22	yield	yield	NOUN
eurjchem-610	237	23	(	(	PUNCT
eurjchem-610	237	24	%	%	NOUN
eurjchem-610	237	25	)	)	PUNCT
eurjchem-610	238	1	12	12	NUM
eurjchem-610	238	2	8	8	NUM
eurjchem-610	238	3	88	88	NUM
eurjchem-610	238	4	‐	‐	NOUN
eurjchem-610	238	5	‐	‐	ADV
eurjchem-610	238	6	13	13	NUM
eurjchem-610	238	7	10	10	NUM
eurjchem-610	238	8	92	92	NUM
eurjchem-610	238	9	4	4	NUM
eurjchem-610	238	10	86	86	NUM
eurjchem-610	238	11	14	14	NUM
eurjchem-610	238	12	nhboc	nhboc	NOUN
eurjchem-610	238	13	12	12	NUM
eurjchem-610	238	14	92	92	NUM
eurjchem-610	238	15	4	4	NUM
eurjchem-610	238	16	86	86	NUM
eurjchem-610	238	17	15	15	NUM
eurjchem-610	238	18	nho	nho	NOUN
eurjchem-610	238	19	4	4	NUM
eurjchem-610	238	20	85	85	NUM
eurjchem-610	238	21	‐	‐	NOUN
eurjchem-610	238	22	‐	‐	ADV
eurjchem-610	238	23	16	16	NUM
eurjchem-610	238	24	10	10	NUM
eurjchem-610	238	25	94	94	NUM
eurjchem-610	238	26	‐	‐	NOUN
eurjchem-610	238	27	‐	‐	VERB
eurjchem-610	238	28	the	the	DET
eurjchem-610	238	29	structure	structure	NOUN
eurjchem-610	238	30	of	of	ADP
eurjchem-610	238	31	wells‐dawson	wells‐dawson	PROPN
eurjchem-610	238	32	(	(	PUNCT
eurjchem-610	238	33	w.d	w.d	PROPN
eurjchem-610	238	34	.	.	PUNCT
eurjchem-610	238	35	)	)	PUNCT
eurjchem-610	239	1	heteropolyacid	heteropolyacid	VERB
eurjchem-610	239	2	h6p2w18o62.14h2o	h6p2w18o62.14h2o	PROPN
eurjchem-610	239	3	consists	consist	VERB
eurjchem-610	239	4	of	of	ADP
eurjchem-610	239	5	a	a	DET
eurjchem-610	239	6	close‐packed	close‐packe	VERB
eurjchem-610	239	7	framework	framework	NOUN
eurjchem-610	239	8	of	of	ADP
eurjchem-610	239	9	octahedral	octahedral	ADJ
eurjchem-610	239	10	wo6	wo6	NOUN
eurjchem-610	239	11	surrounding	surround	VERB
eurjchem-610	239	12	a	a	DET
eurjchem-610	239	13	central	central	ADJ
eurjchem-610	239	14	p	p	NOUN
eurjchem-610	239	15	atom	atom	NOUN
eurjchem-610	239	16	,	,	PUNCT
eurjchem-610	239	17	two	two	NUM
eurjchem-610	239	18	identical	identical	ADJ
eurjchem-610	239	19	‘	'	PUNCT
eurjchem-610	239	20	half	half	ADJ
eurjchem-610	239	21	unit	unit	NOUN
eurjchem-610	239	22	’	'	PUNCT
eurjchem-610	239	23	pw9	pw9	NOUN
eurjchem-610	239	24	are	be	AUX
eurjchem-610	239	25	linked	link	VERB
eurjchem-610	239	26	through	through	ADP
eurjchem-610	239	27	the	the	DET
eurjchem-610	239	28	oxygen	oxygen	NOUN
eurjchem-610	239	29	atom	atom	NOUN
eurjchem-610	239	30	.	.	PUNCT
eurjchem-610	240	1	these	these	DET
eurjchem-610	240	2	proprieties	propriety	NOUN
eurjchem-610	240	3	make	make	VERB
eurjchem-610	240	4	them	they	PRON
eurjchem-610	240	5	suitable	suitable	ADJ
eurjchem-610	240	6	catalytic	catalytic	ADJ
eurjchem-610	240	7	materials	material	NOUN
eurjchem-610	240	8	in	in	ADP
eurjchem-610	240	9	homogeneous	homogeneous	ADJ
eurjchem-610	240	10	and	and	CCONJ
eurjchem-610	240	11	heterogeneous	heterogeneous	ADJ
eurjchem-610	240	12	liquid‐phase	liquid‐phase	ADJ
eurjchem-610	240	13	reaction	reaction	NOUN
eurjchem-610	240	14	replacing	replace	VERB
eurjchem-610	240	15	the	the	DET
eurjchem-610	240	16	conventional	conventional	ADJ
eurjchem-610	240	17	liquid‐acid	liquid‐acid	PROPN
eurjchem-610	240	18	.	.	PUNCT
eurjchem-610	241	1	for	for	ADP
eurjchem-610	241	2	reasons	reason	NOUN
eurjchem-610	241	3	of	of	ADP
eurjchem-610	241	4	the	the	DET
eurjchem-610	241	5	relative	relative	ADJ
eurjchem-610	241	6	solubility	solubility	NOUN
eurjchem-610	241	7	in	in	ADP
eurjchem-610	241	8	organic	organic	ADJ
eurjchem-610	241	9	solvents	solvent	NOUN
eurjchem-610	241	10	,	,	PUNCT
eurjchem-610	241	11	we	we	PRON
eurjchem-610	241	12	are	be	AUX
eurjchem-610	241	13	especially	especially	ADV
eurjchem-610	241	14	interested	interested	ADJ
eurjchem-610	241	15	to	to	ADP
eurjchem-610	241	16	the	the	DET
eurjchem-610	241	17	acid	acid	NOUN
eurjchem-610	241	18	form	form	NOUN
eurjchem-610	241	19	of	of	ADP
eurjchem-610	241	20	heteropolyanion	heteropolyanion	NOUN
eurjchem-610	241	21	(	(	PUNCT
eurjchem-610	241	22	h6p2w12mo6o62	h6p2w12mo6o62	INTJ
eurjchem-610	241	23	)	)	PUNCT
eurjchem-610	241	24	(	(	PUNCT
eurjchem-610	241	25	hpa	hpa	NOUN
eurjchem-610	241	26	)	)	PUNCT
eurjchem-610	241	27	was	be	AUX
eurjchem-610	241	28	prepared	prepare	VERB
eurjchem-610	241	29	starting	start	VERB
eurjchem-610	241	30	from	from	ADP
eurjchem-610	241	31	an	an	DET
eurjchem-610	241	32	aqueous	aqueous	ADJ
eurjchem-610	241	33	solution	solution	NOUN
eurjchem-610	241	34	of	of	ADP
eurjchem-610	241	35	α‐k6p2w12mo6o62	α‐k6p2w12mo6o62	PROPN
eurjchem-610	241	36	salt	salt	NOUN
eurjchem-610	241	37	,	,	PUNCT
eurjchem-610	241	38	which	which	PRON
eurjchem-610	241	39	was	be	AUX
eurjchem-610	241	40	treated	treat	VERB
eurjchem-610	241	41	with	with	ADP
eurjchem-610	241	42	diethyl	diethyl	NOUN
eurjchem-610	241	43	ether	ether	NOUN
eurjchem-610	241	44	and	and	CCONJ
eurjchem-610	241	45	a	a	DET
eurjchem-610	241	46	concentrated	concentrate	VERB
eurjchem-610	241	47	hcl	hcl	NOUN
eurjchem-610	241	48	solution	solution	NOUN
eurjchem-610	241	49	(	(	PUNCT
eurjchem-610	241	50	37	37	NUM
eurjchem-610	241	51	%	%	NOUN
eurjchem-610	241	52	)	)	PUNCT
eurjchem-610	242	1	[	[	X
eurjchem-610	242	2	24	24	NUM
eurjchem-610	242	3	]	]	PUNCT
eurjchem-610	242	4	.	.	PUNCT
eurjchem-610	243	1	the	the	DET
eurjchem-610	243	2	preparation	preparation	NOUN
eurjchem-610	243	3	of	of	ADP
eurjchem-610	243	4	cyclosulfamides	cyclosulfamides	PROPN
eurjchem-610	243	5	(	(	PUNCT
eurjchem-610	243	6	1‐5	1‐5	NUM
eurjchem-610	243	7	)	)	PUNCT
eurjchem-610	243	8	with	with	ADP
eurjchem-610	243	9	orthogonal	orthogonal	ADJ
eurjchem-610	243	10	protecting	protect	VERB
eurjchem-610	243	11	group	group	NOUN
eurjchem-610	243	12	was	be	AUX
eurjchem-610	243	13	performed	perform	VERB
eurjchem-610	243	14	in	in	ADP
eurjchem-610	243	15	four	four	NUM
eurjchem-610	243	16	steps	step	NOUN
eurjchem-610	243	17	starting	start	VERB
eurjchem-610	243	18	from	from	ADP
eurjchem-610	243	19	amino	amino	ADJ
eurjchem-610	243	20	acids	acid	NOUN
eurjchem-610	243	21	(	(	PUNCT
eurjchem-610	243	22	glycine	glycine	NOUN
eurjchem-610	243	23	,	,	PUNCT
eurjchem-610	243	24	alanine	alanine	NOUN
eurjchem-610	243	25	,	,	PUNCT
eurjchem-610	243	26	valine	valine	NOUN
eurjchem-610	243	27	,	,	PUNCT
eurjchem-610	243	28	leucine	leucine	NOUN
eurjchem-610	243	29	and	and	CCONJ
eurjchem-610	243	30	phenyl	phenyl	NOUN
eurjchem-610	243	31	alanine	alanine	NOUN
eurjchem-610	243	32	)	)	PUNCT
eurjchem-610	243	33	and	and	CCONJ
eurjchem-610	243	34	chlorosulfonylisocyanate	chlorosulfonylisocyanate	VERB
eurjchem-610	243	35	as	as	SCONJ
eurjchem-610	243	36	previously	previously	ADV
eurjchem-610	243	37	described	describe	VERB
eurjchem-610	243	38	[	[	X
eurjchem-610	243	39	25,26	25,26	NUM
eurjchem-610	243	40	]	]	X
eurjchem-610	243	41	.	.	PUNCT
eurjchem-610	244	1	the	the	DET
eurjchem-610	244	2	deprotection	deprotection	NOUN
eurjchem-610	244	3	reaction	reaction	NOUN
eurjchem-610	244	4	was	be	AUX
eurjchem-610	244	5	studied	study	VERB
eurjchem-610	244	6	using	use	VERB
eurjchem-610	244	7	compounds	compound	NOUN
eurjchem-610	244	8	1‐5	1‐5	PROPN
eurjchem-610	244	9	as	as	ADP
eurjchem-610	244	10	substrates	substrate	NOUN
eurjchem-610	244	11	.	.	PUNCT
eurjchem-610	245	1	when	when	SCONJ
eurjchem-610	245	2	n‐boc‐cyclo‐	n‐boc‐cyclo‐	PRON
eurjchem-610	245	3	sulfamides	sulfamide	VERB
eurjchem-610	245	4	(	(	PUNCT
eurjchem-610	245	5	1‐5	1‐5	NUM
eurjchem-610	245	6	)	)	PUNCT
eurjchem-610	245	7	were	be	AUX
eurjchem-610	245	8	treated	treat	VERB
eurjchem-610	245	9	with	with	ADP
eurjchem-610	245	10	heteropolyacid	heteropolyacid	ADJ
eurjchem-610	245	11	(	(	PUNCT
eurjchem-610	245	12	10	10	NUM
eurjchem-610	245	13	%	%	NOUN
eurjchem-610	245	14	,	,	PUNCT
eurjchem-610	245	15	w	w	NOUN
eurjchem-610	245	16	:	:	SYM
eurjchem-610	245	17	w	w	X
eurjchem-610	245	18	)	)	PUNCT
eurjchem-610	245	19	in	in	ADP
eurjchem-610	245	20	dcm	dcm	PROPN
eurjchem-610	245	21	at	at	ADP
eurjchem-610	245	22	room	room	NOUN
eurjchem-610	245	23	temperature	temperature	NOUN
eurjchem-610	245	24	for	for	ADP
eurjchem-610	245	25	15‐30	15‐30	NUM
eurjchem-610	245	26	minutes	minute	NOUN
eurjchem-610	245	27	,	,	PUNCT
eurjchem-610	245	28	the	the	DET
eurjchem-610	245	29	deprotected	deprotecte	VERB
eurjchem-610	245	30	cyclosulfamides	cyclosulfamide	NOUN
eurjchem-610	245	31	were	be	AUX
eurjchem-610	245	32	obtained	obtain	VERB
eurjchem-610	245	33	in	in	ADP
eurjchem-610	245	34	quantitative	quantitative	ADJ
eurjchem-610	245	35	yield	yield	NOUN
eurjchem-610	245	36	.	.	PUNCT
eurjchem-610	246	1	the	the	DET
eurjchem-610	246	2	reaction	reaction	NOUN
eurjchem-610	246	3	was	be	AUX
eurjchem-610	246	4	monitored	monitor	VERB
eurjchem-610	246	5	by	by	ADP
eurjchem-610	246	6	lc‐ms	lc‐ms	X
eurjchem-610	246	7	.	.	PUNCT
eurjchem-610	247	1	as	as	SCONJ
eurjchem-610	247	2	outlined	outline	VERB
eurjchem-610	247	3	in	in	ADP
eurjchem-610	247	4	scheme	scheme	NOUN
eurjchem-610	247	5	2	2	NUM
eurjchem-610	247	6	,	,	PUNCT
eurjchem-610	247	7	the	the	DET
eurjchem-610	247	8	deprotection	deprotection	NOUN
eurjchem-610	247	9	was	be	AUX
eurjchem-610	247	10	envisioned	envision	VERB
eurjchem-610	247	11	in	in	ADP
eurjchem-610	247	12	first	first	ADJ
eurjchem-610	247	13	reaction	reaction	NOUN
eurjchem-610	247	14	sequence	sequence	NOUN
eurjchem-610	247	15	starting	start	VERB
eurjchem-610	247	16	from	from	ADP
eurjchem-610	247	17	n‐benzyl‐tert‐	n‐benzyl‐tert‐	PROPN
eurjchem-610	247	18	butyloxycarbonylsulfamide	butyloxycarbonylsulfamide	ADJ
eurjchem-610	247	19	6	6	NUM
eurjchem-610	247	20	.	.	PUNCT
eurjchem-610	248	1	in	in	ADP
eurjchem-610	248	2	a	a	DET
eurjchem-610	248	3	typical	typical	ADJ
eurjchem-610	248	4	experimental	experimental	ADJ
eurjchem-610	248	5	procedure	procedure	NOUN
eurjchem-610	248	6	,	,	PUNCT
eurjchem-610	248	7	heteropolyacid	heteropolyacid	PROPN
eurjchem-610	248	8	was	be	AUX
eurjchem-610	248	9	added	add	VERB
eurjchem-610	248	10	to	to	ADP
eurjchem-610	248	11	a	a	DET
eurjchem-610	248	12	solution	solution	NOUN
eurjchem-610	248	13	of	of	ADP
eurjchem-610	248	14	reaction	reaction	NOUN
eurjchem-610	248	15	substrate	substrate	NOUN
eurjchem-610	248	16	in	in	ADP
eurjchem-610	248	17	an	an	DET
eurjchem-610	248	18	organic	organic	ADJ
eurjchem-610	248	19	solvent	solvent	NOUN
eurjchem-610	248	20	.	.	PUNCT
eurjchem-610	249	1	the	the	DET
eurjchem-610	249	2	mixture	mixture	NOUN
eurjchem-610	249	3	was	be	AUX
eurjchem-610	249	4	stirred	stir	VERB
eurjchem-610	249	5	at	at	ADP
eurjchem-610	249	6	room	room	NOUN
eurjchem-610	249	7	temperature	temperature	NOUN
eurjchem-610	249	8	until	until	SCONJ
eurjchem-610	249	9	reaction	reaction	NOUN
eurjchem-610	249	10	was	be	AUX
eurjchem-610	249	11	complete	complete	ADJ
eurjchem-610	249	12	(	(	PUNCT
eurjchem-610	249	13	monitored	monitor	VERB
eurjchem-610	249	14	by	by	ADP
eurjchem-610	249	15	hplc	hplc	NOUN
eurjchem-610	249	16	,	,	PUNCT
eurjchem-610	249	17	typically	typically	ADV
eurjchem-610	249	18	15	15	NUM
eurjchem-610	249	19	min	min	NOUN
eurjchem-610	249	20	)	)	PUNCT
eurjchem-610	249	21	.	.	PUNCT
eurjchem-610	250	1	this	this	DET
eurjchem-610	250	2	requisite	requisite	ADJ
eurjchem-610	250	3	substrate	substrate	NOUN
eurjchem-610	250	4	was	be	AUX
eurjchem-610	250	5	prepared	prepare	VERB
eurjchem-610	250	6	by	by	ADP
eurjchem-610	250	7	sulfamoylation	sulfamoylation	NOUN
eurjchem-610	250	8	of	of	ADP
eurjchem-610	250	9	benzyl	benzyl	NOUN
eurjchem-610	250	10	amine	amine	NOUN
eurjchem-610	250	11	as	as	SCONJ
eurjchem-610	250	12	previously	previously	ADV
eurjchem-610	250	13	described	describe	VERB
eurjchem-610	250	14	[	[	X
eurjchem-610	250	15	21	21	NUM
eurjchem-610	250	16	]	]	PUNCT
eurjchem-610	250	17	.	.	PUNCT
eurjchem-610	251	1	chemoselective	chemoselective	ADJ
eurjchem-610	251	2	deprotection	deprotection	NOUN
eurjchem-610	251	3	of	of	ADP
eurjchem-610	251	4	compound	compound	NOUN
eurjchem-610	251	5	6	6	NUM
eurjchem-610	251	6	was	be	AUX
eurjchem-610	251	7	carried	carry	VERB
eurjchem-610	251	8	out	out	ADP
eurjchem-610	251	9	in	in	ADP
eurjchem-610	251	10	heterogeneous	heterogeneous	ADJ
eurjchem-610	251	11	system	system	NOUN
eurjchem-610	251	12	using	use	VERB
eurjchem-610	251	13	heteropolyacid	heteropolyacid	X
eurjchem-610	251	14	in	in	ADP
eurjchem-610	251	15	dichloromethane	dichloromethane	NOUN
eurjchem-610	251	16	to	to	PART
eurjchem-610	251	17	afford	afford	VERB
eurjchem-610	251	18	deprotected	deprotecte	VERB
eurjchem-610	251	19	compound	compound	VERB
eurjchem-610	251	20	6a	6a	NOUN
eurjchem-610	251	21	in	in	ADP
eurjchem-610	251	22	good	good	ADJ
eurjchem-610	251	23	yield	yield	NOUN
eurjchem-610	251	24	.	.	PUNCT
eurjchem-610	252	1	in	in	ADP
eurjchem-610	252	2	our	our	PRON
eurjchem-610	252	3	previous	previous	ADJ
eurjchem-610	252	4	studies	study	NOUN
eurjchem-610	252	5	[	[	X
eurjchem-610	252	6	20	20	NUM
eurjchem-610	252	7	]	]	PUNCT
eurjchem-610	252	8	,	,	PUNCT
eurjchem-610	252	9	we	we	PRON
eurjchem-610	252	10	described	describe	VERB
eurjchem-610	252	11	a	a	DET
eurjchem-610	252	12	convenient	convenient	ADJ
eurjchem-610	252	13	access	access	NOUN
eurjchem-610	252	14	to	to	ADP
eurjchem-610	252	15	a	a	DET
eurjchem-610	252	16	series	series	NOUN
eurjchem-610	252	17	of	of	ADP
eurjchem-610	252	18	sulfamides	sulfamide	NOUN
eurjchem-610	252	19	n	n	CCONJ
eurjchem-610	252	20	,	,	PUNCT
eurjchem-610	252	21	n’‐disubstituted	n’‐disubstituted	ADJ
eurjchem-610	252	22	,	,	PUNCT
eurjchem-610	252	23	(	(	PUNCT
eurjchem-610	252	24	7‐11	7‐11	X
eurjchem-610	252	25	)	)	PUNCT
eurjchem-610	252	26	starting	start	VERB
eurjchem-610	252	27	from	from	ADP
eurjchem-610	252	28	amino	amino	ADJ
eurjchem-610	252	29	acids	acid	NOUN
eurjchem-610	252	30	and	and	CCONJ
eurjchem-610	252	31	chlorosulfonylisocyanate	chlorosulfonylisocyanate	VERB
eurjchem-610	252	32	in	in	ADP
eurjchem-610	252	33	two	two	NUM
eurjchem-610	252	34	steps	step	NOUN
eurjchem-610	252	35	(	(	PUNCT
eurjchem-610	252	36	carbamoyaltion‐sulfamoylation	carbamoyaltion‐sulfamoylation	NOUN
eurjchem-610	252	37	)	)	PUNCT
eurjchem-610	252	38	.	.	PUNCT
eurjchem-610	253	1	the	the	DET
eurjchem-610	253	2	deprotection	deprotection	NOUN
eurjchem-610	253	3	protocol	protocol	NOUN
eurjchem-610	253	4	giving	give	VERB
eurjchem-610	253	5	linear	linear	NOUN
eurjchem-610	253	6	sulfamides	sulfamide	NOUN
eurjchem-610	253	7	(	(	PUNCT
eurjchem-610	253	8	7a‐11a	7a‐11a	NOUN
eurjchem-610	253	9	)	)	PUNCT
eurjchem-610	253	10	is	be	AUX
eurjchem-610	253	11	outlined	outline	VERB
eurjchem-610	253	12	in	in	ADP
eurjchem-610	253	13	scheme	scheme	NOUN
eurjchem-610	253	14	3	3	NUM
eurjchem-610	253	15	.	.	PUNCT
eurjchem-610	253	16	deprotection	deprotection	NOUN
eurjchem-610	253	17	of	of	ADP
eurjchem-610	253	18	compounds	compound	NOUN
eurjchem-610	253	19	7‐11	7‐11	NUM
eurjchem-610	253	20	was	be	AUX
eurjchem-610	253	21	performed	perform	VERB
eurjchem-610	253	22	using	use	VERB
eurjchem-610	253	23	the	the	DET
eurjchem-610	253	24	standardized	standardized	ADJ
eurjchem-610	253	25	reaction	reaction	NOUN
eurjchem-610	253	26	conditions	condition	NOUN
eurjchem-610	253	27	,	,	PUNCT
eurjchem-610	253	28	giving	give	VERB
eurjchem-610	253	29	yields	yield	NOUN
eurjchem-610	253	30	better	well	ADJ
eurjchem-610	253	31	than	than	ADP
eurjchem-610	253	32	92	92	NUM
eurjchem-610	253	33	%	%	NOUN
eurjchem-610	253	34	.	.	PUNCT
eurjchem-610	254	1	the	the	DET
eurjchem-610	254	2	reaction	reaction	NOUN
eurjchem-610	254	3	carried	carry	VERB
eurjchem-610	254	4	out	out	ADP
eurjchem-610	254	5	with	with	ADP
eurjchem-610	254	6	n‐boc	n‐boc	DET
eurjchem-610	254	7	amines	amine	NOUN
eurjchem-610	254	8	12‐16	12‐16	NUM
eurjchem-610	254	9	shown	show	VERB
eurjchem-610	254	10	in	in	ADP
eurjchem-610	254	11	table	table	NOUN
eurjchem-610	254	12	1	1	NUM
eurjchem-610	254	13	affordsthe	affordsthe	DET
eurjchem-610	254	14	corresponding	correspond	VERB
eurjchem-610	254	15	commercially	commercially	ADV
eurjchem-610	254	16	available	available	ADJ
eurjchem-610	254	17	amines	amine	NOUN
eurjchem-610	254	18	using	use	VERB
eurjchem-610	254	19	standard	standard	ADJ
eurjchem-610	254	20	conditions	condition	NOUN
eurjchem-610	254	21	.	.	PUNCT
eurjchem-610	255	1	carbamates	carbamate	NOUN
eurjchem-610	255	2	12‐16	12‐16	NUM
eurjchem-610	255	3	were	be	AUX
eurjchem-610	255	4	deprotected	deprotecte	VERB
eurjchem-610	255	5	cleanly	cleanly	ADV
eurjchem-610	255	6	to	to	PART
eurjchem-610	255	7	provide	provide	VERB
eurjchem-610	255	8	the	the	DET
eurjchem-610	255	9	corresponding	corresponding	ADJ
eurjchem-610	255	10	amines	amine	NOUN
eurjchem-610	255	11	with	with	ADP
eurjchem-610	255	12	quantitative	quantitative	ADJ
eurjchem-610	255	13	yields	yield	NOUN
eurjchem-610	255	14	,	,	PUNCT
eurjchem-610	255	15	all	all	DET
eurjchem-610	255	16	results	result	NOUN
eurjchem-610	255	17	summarized	summarize	VERB
eurjchem-610	255	18	in	in	ADP
eurjchem-610	255	19	table	table	NOUN
eurjchem-610	255	20	1	1	NUM
eurjchem-610	255	21	.	.	PUNCT
eurjchem-610	256	1	wang	wang	PROPN
eurjchem-610	256	2	et	et	PROPN
eurjchem-610	256	3	al	al	PROPN
eurjchem-610	256	4	.	.	PUNCT
eurjchem-610	257	1	[	[	X
eurjchem-610	257	2	27	27	NUM
eurjchem-610	257	3	]	]	PUNCT
eurjchem-610	257	4	report	report	NOUN
eurjchem-610	257	5	the	the	DET
eurjchem-610	257	6	n‐boc	n‐boc	DET
eurjchem-610	257	7	deprotection	deprotection	NOUN
eurjchem-610	257	8	of	of	ADP
eurjchem-610	257	9	a	a	DET
eurjchem-610	257	10	variety	variety	NOUN
eurjchem-610	257	11	of	of	ADP
eurjchem-610	257	12	aromatic	aromatic	ADJ
eurjchem-610	257	13	amines	amine	NOUN
eurjchem-610	257	14	and	and	CCONJ
eurjchem-610	257	15	amino	amino	NOUN
eurjchem-610	257	16	ester	ester	NOUN
eurjchem-610	257	17	under	under	ADP
eurjchem-610	257	18	catalyst‐free	catalyst‐free	ADJ
eurjchem-610	257	19	conditions	condition	NOUN
eurjchem-610	257	20	in	in	ADP
eurjchem-610	257	21	subcritical	subcritical	ADJ
eurjchem-610	257	22	water	water	NOUN
eurjchem-610	257	23	with	with	ADP
eurjchem-610	257	24	height	height	NOUN
eurjchem-610	257	25	pressure	pressure	NOUN
eurjchem-610	257	26	.	.	PUNCT
eurjchem-610	258	1	the	the	DET
eurjchem-610	258	2	both	both	PRON
eurjchem-610	258	3	removed	remove	VERB
eurjchem-610	258	4	of	of	ADP
eurjchem-610	258	5	acid‐sensitive	acid‐sensitive	ADJ
eurjchem-610	258	6	groups	group	NOUN
eurjchem-610	258	7	(	(	PUNCT
eurjchem-610	258	8	methyl	methyl	NOUN
eurjchem-610	258	9	ester	ester	NOUN
eurjchem-610	258	10	and	and	CCONJ
eurjchem-610	258	11	boc	boc	NOUN
eurjchem-610	258	12	)	)	PUNCT
eurjchem-610	258	13	,	,	PUNCT
eurjchem-610	258	14	the	the	DET
eurjchem-610	258	15	prolonged	prolonged	ADJ
eurjchem-610	258	16	reaction	reaction	NOUN
eurjchem-610	258	17	time	time	NOUN
eurjchem-610	258	18	,	,	PUNCT
eurjchem-610	258	19	that	that	SCONJ
eurjchem-610	258	20	the	the	DET
eurjchem-610	258	21	disadvantage	disadvantage	NOUN
eurjchem-610	258	22	of	of	ADP
eurjchem-610	258	23	chemoselectivity	chemoselectivity	NOUN
eurjchem-610	258	24	.	.	PUNCT
eurjchem-610	259	1	the	the	DET
eurjchem-610	259	2	corresponding	corresponding	ADJ
eurjchem-610	259	3	amines	amine	NOUN
eurjchem-610	259	4	were	be	AUX
eurjchem-610	259	5	obtained	obtain	VERB
eurjchem-610	259	6	in	in	ADP
eurjchem-610	259	7	excellent	excellent	ADJ
eurjchem-610	259	8	yields	yield	NOUN
eurjchem-610	259	9	.	.	PUNCT
eurjchem-610	260	1	the	the	DET
eurjchem-610	260	2	substrate	substrate	NOUN
eurjchem-610	260	3	examined	examine	VERB
eurjchem-610	260	4	in	in	ADP
eurjchem-610	260	5	these	these	DET
eurjchem-610	260	6	studies	study	NOUN
eurjchem-610	260	7	and	and	CCONJ
eurjchem-610	260	8	the	the	DET
eurjchem-610	260	9	results	result	NOUN
eurjchem-610	260	10	obtained	obtain	VERB
eurjchem-610	260	11	are	be	AUX
eurjchem-610	260	12	summarized	summarize	VERB
eurjchem-610	260	13	in	in	ADP
eurjchem-610	260	14	table	table	NOUN
eurjchem-610	260	15	1	1	NUM
eurjchem-610	260	16	.	.	PUNCT
eurjchem-610	261	1	the	the	DET
eurjchem-610	261	2	reaction	reaction	NOUN
eurjchem-610	261	3	preserves	preserve	VERB
eurjchem-610	261	4	stereochemical	stereochemical	ADJ
eurjchem-610	261	5	integrity	integrity	NOUN
eurjchem-610	261	6	of	of	ADP
eurjchem-610	261	7	n‐boc	n‐boc	DET
eurjchem-610	261	8	amino	amino	ADJ
eurjchem-610	261	9	acids	acid	NOUN
eurjchem-610	261	10	(	(	PUNCT
eurjchem-610	261	11	16	16	NUM
eurjchem-610	261	12	)	)	PUNCT
eurjchem-610	261	13	and	and	CCONJ
eurjchem-610	261	14	regioselectivity	regioselectivity	NOUN
eurjchem-610	261	15	of	of	ADP
eurjchem-610	261	16	compounds	compound	NOUN
eurjchem-610	261	17	(	(	PUNCT
eurjchem-610	261	18	15‐16	15‐16	NUM
eurjchem-610	261	19	)	)	PUNCT
eurjchem-610	261	20	containing	contain	VERB
eurjchem-610	261	21	two	two	NUM
eurjchem-610	261	22	orthogonal	orthogonal	ADJ
eurjchem-610	261	23	protecting	protect	VERB
eurjchem-610	261	24	groups	group	NOUN
eurjchem-610	261	25	(	(	PUNCT
eurjchem-610	261	26	bn	bn	NOUN
eurjchem-610	261	27	and	and	CCONJ
eurjchem-610	261	28	boc	boc	NOUN
eurjchem-610	261	29	)	)	PUNCT
eurjchem-610	261	30	(	(	PUNCT
eurjchem-610	261	31	bn	bn	NOUN
eurjchem-610	261	32	=	=	NOUN
eurjchem-610	261	33	benzyl	benzyl	NOUN
eurjchem-610	261	34	)	)	PUNCT
eurjchem-610	261	35	.	.	PUNCT
eurjchem-610	262	1	the	the	DET
eurjchem-610	262	2	generally	generally	ADV
eurjchem-610	262	3	accepted	accept	VERB
eurjchem-610	262	4	mechanism	mechanism	NOUN
eurjchem-610	262	5	for	for	ADP
eurjchem-610	262	6	the	the	DET
eurjchem-610	262	7	boc	boc	PROPN
eurjchem-610	262	8	removal	removal	PROPN
eurjchem-610	262	9	group	group	NOUN
eurjchem-610	262	10	belghiche	belghiche	PROPN
eurjchem-610	262	11	et	et	PROPN
eurjchem-610	262	12	al	al	PROPN
eurjchem-610	262	13	.	.	PUNCT
eurjchem-610	262	14	/	/	SYM
eurjchem-610	262	15	european	european	PROPN
eurjchem-610	262	16	journal	journal	PROPN
eurjchem-610	262	17	of	of	ADP
eurjchem-610	262	18	chemistry	chemistry	NOUN
eurjchem-610	262	19	3	3	NUM
eurjchem-610	262	20	(	(	PUNCT
eurjchem-610	262	21	3	3	NUM
eurjchem-610	262	22	)	)	PUNCT
eurjchem-610	262	23	(	(	PUNCT
eurjchem-610	262	24	2012	2012	NUM
eurjchem-610	262	25	)	)	PUNCT
eurjchem-610	262	26	305‐309	305‐309	NOUN
eurjchem-610	262	27	309	309	NUM
eurjchem-610	262	28	under	under	ADP
eurjchem-610	262	29	acid	acid	NOUN
eurjchem-610	262	30	conditions	condition	NOUN
eurjchem-610	262	31	involves	involve	VERB
eurjchem-610	262	32	the	the	DET
eurjchem-610	262	33	formation	formation	NOUN
eurjchem-610	262	34	of	of	ADP
eurjchem-610	262	35	carbon	carbon	NOUN
eurjchem-610	262	36	dioxide	dioxide	NOUN
eurjchem-610	262	37	and	and	CCONJ
eurjchem-610	262	38	tert‐butyl	tert‐butyl	ADP
eurjchem-610	262	39	cation	cation	NOUN
eurjchem-610	262	40	,	,	PUNCT
eurjchem-610	262	41	which	which	PRON
eurjchem-610	262	42	after	after	ADP
eurjchem-610	262	43	losing	lose	VERB
eurjchem-610	262	44	a	a	DET
eurjchem-610	262	45	proton	proton	NOUN
eurjchem-610	262	46	gives	give	VERB
eurjchem-610	262	47	isobutene	isobutene	NOUN
eurjchem-610	262	48	.	.	PUNCT
eurjchem-610	263	1	concerning	concern	VERB
eurjchem-610	263	2	a	a	DET
eurjchem-610	263	3	possible	possible	ADJ
eurjchem-610	263	4	reaction	reaction	NOUN
eurjchem-610	263	5	mechanism	mechanism	NOUN
eurjchem-610	263	6	,	,	PUNCT
eurjchem-610	263	7	we	we	PRON
eurjchem-610	263	8	assume	assume	VERB
eurjchem-610	263	9	that	that	SCONJ
eurjchem-610	263	10	the	the	DET
eurjchem-610	263	11	heteropolyacid‐catalyzed	heteropolyacid‐catalyze	VERB
eurjchem-610	263	12	proceed	proceed	VERB
eurjchem-610	263	13	with	with	ADP
eurjchem-610	263	14	exchange	exchange	NOUN
eurjchem-610	263	15	of	of	ADP
eurjchem-610	263	16	protons	proton	NOUN
eurjchem-610	263	17	with	with	ADP
eurjchem-610	263	18	the	the	DET
eurjchem-610	263	19	product	product	NOUN
eurjchem-610	263	20	.	.	PUNCT
eurjchem-610	264	1	however	however	ADV
eurjchem-610	264	2	the	the	DET
eurjchem-610	264	3	relative	relative	ADJ
eurjchem-610	264	4	insolubility	insolubility	NOUN
eurjchem-610	264	5	of	of	ADP
eurjchem-610	264	6	the	the	DET
eurjchem-610	264	7	heteropolyacid	heteropolyacid	ADJ
eurjchem-610	264	8	catalyst	catalyst	NOUN
eurjchem-610	264	9	in	in	ADP
eurjchem-610	264	10	dichloromethane	dichloromethane	NOUN
eurjchem-610	264	11	allows	allow	VERB
eurjchem-610	264	12	for	for	ADP
eurjchem-610	264	13	easy	easy	ADJ
eurjchem-610	264	14	separation	separation	NOUN
eurjchem-610	264	15	of	of	ADP
eurjchem-610	264	16	the	the	DET
eurjchem-610	264	17	product	product	NOUN
eurjchem-610	264	18	by	by	ADP
eurjchem-610	264	19	simple	simple	ADJ
eurjchem-610	264	20	filtration	filtration	NOUN
eurjchem-610	264	21	,	,	PUNCT
eurjchem-610	264	22	heteropolyacid	heteropolyacid	PROPN
eurjchem-610	264	23	was	be	AUX
eurjchem-610	264	24	reused	reuse	VERB
eurjchem-610	264	25	with	with	ADP
eurjchem-610	264	26	only	only	ADV
eurjchem-610	264	27	a	a	DET
eurjchem-610	264	28	gradual	gradual	ADJ
eurjchem-610	264	29	decrease	decrease	NOUN
eurjchem-610	264	30	in	in	ADP
eurjchem-610	264	31	its	its	PRON
eurjchem-610	264	32	activity	activity	NOUN
eurjchem-610	264	33	observed	observe	VERB
eurjchem-610	264	34	.	.	PUNCT
eurjchem-610	265	1	the	the	DET
eurjchem-610	265	2	structures	structure	NOUN
eurjchem-610	265	3	of	of	ADP
eurjchem-610	265	4	all	all	DET
eurjchem-610	265	5	the	the	DET
eurjchem-610	265	6	compounds	compound	NOUN
eurjchem-610	265	7	were	be	AUX
eurjchem-610	265	8	unambiguously	unambiguously	ADV
eurjchem-610	265	9	confirmed	confirm	VERB
eurjchem-610	265	10	by	by	ADP
eurjchem-610	265	11	usual	usual	ADJ
eurjchem-610	265	12	spectroscopic	spectroscopic	ADJ
eurjchem-610	265	13	methods	method	NOUN
eurjchem-610	265	14	.	.	PUNCT
eurjchem-610	266	1	for	for	ADP
eurjchem-610	266	2	the	the	DET
eurjchem-610	266	3	final	final	ADJ
eurjchem-610	266	4	derivatives	derivative	NOUN
eurjchem-610	266	5	,	,	PUNCT
eurjchem-610	266	6	the	the	DET
eurjchem-610	266	7	different	different	ADJ
eurjchem-610	266	8	nmr	nmr	NOUN
eurjchem-610	266	9	spectra	spectra	NOUN
eurjchem-610	266	10	showed	show	VERB
eurjchem-610	266	11	a	a	DET
eurjchem-610	266	12	signal	signal	NOUN
eurjchem-610	266	13	of	of	ADP
eurjchem-610	266	14	nh	nh	PROPN
eurjchem-610	266	15	proton	proton	NOUN
eurjchem-610	266	16	and	and	CCONJ
eurjchem-610	266	17	disappearance	disappearance	NOUN
eurjchem-610	266	18	of	of	ADP
eurjchem-610	266	19	signal	signal	NOUN
eurjchem-610	266	20	corresponding	correspond	VERB
eurjchem-610	266	21	to	to	ADP
eurjchem-610	266	22	the	the	DET
eurjchem-610	266	23	tert‐	tert‐	ADJ
eurjchem-610	266	24	butyl	butyl	NOUN
eurjchem-610	266	25	protons	proton	NOUN
eurjchem-610	266	26	.	.	PUNCT
eurjchem-610	267	1	these	these	DET
eurjchem-610	267	2	compounds	compound	NOUN
eurjchem-610	267	3	exhibited	exhibit	VERB
eurjchem-610	267	4	characteristic	characteristic	ADJ
eurjchem-610	267	5	absorption	absorption	NOUN
eurjchem-610	267	6	in	in	ADP
eurjchem-610	267	7	the	the	DET
eurjchem-610	267	8	ir	ir	PROPN
eurjchem-610	267	9	spectrum	spectrum	NOUN
eurjchem-610	267	10	and	and	CCONJ
eurjchem-610	267	11	disappearance	disappearance	NOUN
eurjchem-610	267	12	of	of	ADP
eurjchem-610	267	13	the	the	DET
eurjchem-610	267	14	absorption	absorption	NOUN
eurjchem-610	267	15	at	at	ADP
eurjchem-610	267	16	1702‐1712	1702‐1712	NUM
eurjchem-610	267	17	cm‐1	cm‐1	NOUN
eurjchem-610	267	18	(	(	PUNCT
eurjchem-610	267	19	c	c	NOUN
eurjchem-610	267	20	=	=	NOUN
eurjchem-610	267	21	o	o	NOUN
eurjchem-610	267	22	)	)	PUNCT
eurjchem-610	267	23	.	.	PUNCT
eurjchem-610	268	1	3	3	X
eurjchem-610	268	2	.	.	X
eurjchem-610	268	3	conclusion	conclusion	NOUN
eurjchem-610	268	4	in	in	ADP
eurjchem-610	268	5	conclusion	conclusion	NOUN
eurjchem-610	268	6	,	,	PUNCT
eurjchem-610	268	7	the	the	DET
eurjchem-610	268	8	wells‐dawson	wells‐dawson	NOUN
eurjchem-610	268	9	heteropolyacid	heteropolyacid	X
eurjchem-610	268	10	can	can	AUX
eurjchem-610	268	11	be	be	AUX
eurjchem-610	268	12	used	use	VERB
eurjchem-610	268	13	as	as	ADP
eurjchem-610	268	14	an	an	DET
eurjchem-610	268	15	alternative	alternative	ADJ
eurjchem-610	268	16	reagent	reagent	NOUN
eurjchem-610	268	17	for	for	ADP
eurjchem-610	268	18	the	the	DET
eurjchem-610	268	19	deprotection	deprotection	NOUN
eurjchem-610	268	20	of	of	ADP
eurjchem-610	268	21	n‐boc	n‐boc	DET
eurjchem-610	268	22	group	group	NOUN
eurjchem-610	268	23	under	under	ADP
eurjchem-610	268	24	heterogeneous	heterogeneous	ADJ
eurjchem-610	268	25	catalysis	catalysis	NOUN
eurjchem-610	268	26	conditions	condition	NOUN
eurjchem-610	268	27	.	.	PUNCT
eurjchem-610	269	1	the	the	DET
eurjchem-610	269	2	reaction	reaction	NOUN
eurjchem-610	269	3	conditions	condition	NOUN
eurjchem-610	269	4	are	be	AUX
eurjchem-610	269	5	mild	mild	ADJ
eurjchem-610	269	6	,	,	PUNCT
eurjchem-610	269	7	and	and	CCONJ
eurjchem-610	269	8	offer	offer	VERB
eurjchem-610	269	9	good	good	ADJ
eurjchem-610	269	10	selectivity	selectivity	NOUN
eurjchem-610	269	11	among	among	ADP
eurjchem-610	269	12	other	other	ADJ
eurjchem-610	269	13	acid	acid	NOUN
eurjchem-610	269	14	/	/	SYM
eurjchem-610	269	15	base	base	NOUN
eurjchem-610	269	16	sensitive	sensitive	ADJ
eurjchem-610	269	17	groups	group	NOUN
eurjchem-610	269	18	including	include	VERB
eurjchem-610	269	19	benzyl	benzyl	NOUN
eurjchem-610	269	20	and	and	CCONJ
eurjchem-610	269	21	methyester	methyester	NOUN
eurjchem-610	269	22	.	.	PUNCT
eurjchem-610	270	1	advantages	advantage	NOUN
eurjchem-610	270	2	of	of	ADP
eurjchem-610	270	3	this	this	DET
eurjchem-610	270	4	methodology	methodology	NOUN
eurjchem-610	270	5	are	be	AUX
eurjchem-610	270	6	operational	operational	ADJ
eurjchem-610	270	7	simplicity	simplicity	NOUN
eurjchem-610	270	8	,	,	PUNCT
eurjchem-610	270	9	no	no	DET
eurjchem-610	270	10	corrosive	corrosive	ADJ
eurjchem-610	270	11	and	and	CCONJ
eurjchem-610	270	12	reusable	reusable	ADJ
eurjchem-610	270	13	.	.	PUNCT
eurjchem-610	271	1	we	we	PRON
eurjchem-610	271	2	are	be	AUX
eurjchem-610	271	3	exploring	explore	VERB
eurjchem-610	271	4	other	other	ADJ
eurjchem-610	271	5	organic	organic	ADJ
eurjchem-610	271	6	synthesis	synthesis	NOUN
eurjchem-610	271	7	applications	application	NOUN
eurjchem-610	271	8	for	for	ADP
eurjchem-610	271	9	heteropolyacid	heteropolyacid	ADJ
eurjchem-610	271	10	catalyst	catalyst	NOUN
eurjchem-610	271	11	,	,	PUNCT
eurjchem-610	271	12	and	and	CCONJ
eurjchem-610	271	13	will	will	AUX
eurjchem-610	271	14	report	report	VERB
eurjchem-610	271	15	the	the	DET
eurjchem-610	271	16	finding	finding	NOUN
eurjchem-610	271	17	in	in	ADP
eurjchem-610	271	18	due	due	ADJ
eurjchem-610	271	19	course	course	NOUN
eurjchem-610	271	20	.	.	PUNCT
eurjchem-610	272	1	acknowledgements	acknowledgement	NOUN
eurjchem-610	272	2	this	this	DET
eurjchem-610	272	3	work	work	NOUN
eurjchem-610	272	4	was	be	AUX
eurjchem-610	272	5	generously	generously	ADV
eurjchem-610	272	6	supported	support	VERB
eurjchem-610	272	7	by	by	ADP
eurjchem-610	272	8	the	the	DET
eurjchem-610	272	9	algerian	algerian	PROPN
eurjchem-610	272	10	ministry	ministry	PROPN
eurjchem-610	272	11	of	of	ADP
eurjchem-610	272	12	scientific	scientific	ADJ
eurjchem-610	272	13	research	research	NOUN
eurjchem-610	272	14	(	(	PUNCT
eurjchem-610	272	15	direction	direction	NOUN
eurjchem-610	272	16	générale	générale	X
eurjchem-610	272	17	de	de	X
eurjchem-610	272	18	la	la	X
eurjchem-610	272	19	recherche	recherche	X
eurjchem-610	272	20	scientifique	scientifique	X
eurjchem-610	272	21	et	et	PROPN
eurjchem-610	272	22	du	du	PROPN
eurjchem-610	272	23	développement	développement	PROPN
eurjchem-610	272	24	technologique	technologique	PROPN
eurjchem-610	272	25	,	,	PUNCT
eurjchem-610	272	26	dgrs‐dt	dgrs‐dt	PROPN
eurjchem-610	272	27	)	)	PUNCT
eurjchem-610	272	28	.	.	PUNCT
eurjchem-610	273	1	fruitful	fruitful	ADJ
eurjchem-610	273	2	discussions	discussion	NOUN
eurjchem-610	273	3	with	with	ADP
eurjchem-610	273	4	dr	dr	PROPN
eurjchem-610	273	5	.	.	PROPN
eurjchem-610	273	6	irwan	irwan	PROPN
eurjchem-610	273	7	guenin	guenin	PROPN
eurjchem-610	273	8	are	be	AUX
eurjchem-610	273	9	greatly	greatly	ADV
eurjchem-610	273	10	appreciated	appreciate	VERB
eurjchem-610	273	11	.	.	PUNCT
eurjchem-610	274	1	references	reference	NOUN
eurjchem-610	274	2	[	[	X
eurjchem-610	274	3	1	1	NUM
eurjchem-610	274	4	]	]	PUNCT
eurjchem-610	274	5	.	.	PUNCT
eurjchem-610	275	1	greene	greene	PROPN
eurjchem-610	275	2	,	,	PUNCT
eurjchem-610	275	3	t.	t.	PROPN
eurjchem-610	275	4	w.	w.	PROPN
eurjchem-610	275	5	;	;	PUNCT
eurjchem-610	275	6	wuts	wut	NOUN
eurjchem-610	275	7	,	,	PUNCT
eurjchem-610	276	1	p.	p.	NOUN
eurjchem-610	276	2	g.	g.	PROPN
eurjchem-610	276	3	protective	protective	ADJ
eurjchem-610	276	4	group	group	NOUN
eurjchem-610	276	5	in	in	ADP
eurjchem-610	276	6	organic	organic	ADJ
eurjchem-610	276	7	synthesis	synthesis	NOUN
eurjchem-610	276	8	,	,	PUNCT
eurjchem-610	276	9	4rd	4rd	PROPN
eurjchem-610	276	10	edition	edition	NOUN
eurjchem-610	276	11	,	,	PUNCT
eurjchem-610	276	12	john	john	PROPN
eurjchem-610	276	13	wiley	wiley	PROPN
eurjchem-610	276	14	,	,	PUNCT
eurjchem-610	276	15	new	new	PROPN
eurjchem-610	276	16	york	york	PROPN
eurjchem-610	276	17	,	,	PUNCT
eurjchem-610	276	18	2007	2007	NUM
eurjchem-610	276	19	.	.	PUNCT
eurjchem-610	277	1	[	[	X
eurjchem-610	277	2	2	2	NUM
eurjchem-610	277	3	]	]	PUNCT
eurjchem-610	277	4	.	.	PUNCT
eurjchem-610	278	1	kocienski	kocienski	PROPN
eurjchem-610	278	2	,	,	PUNCT
eurjchem-610	278	3	p.	p.	PROPN
eurjchem-610	278	4	j.	j.	PROPN
eurjchem-610	279	1	in	in	ADP
eurjchem-610	279	2	protecting	protect	VERB
eurjchem-610	279	3	group	group	NOUN
eurjchem-610	279	4	,	,	PUNCT
eurjchem-610	279	5	georges	georges	PROPN
eurjchem-610	279	6	thiemeverlag	thiemeverlag	PROPN
eurjchem-610	279	7	,	,	PUNCT
eurjchem-610	279	8	stuttgart	stuttgart	PROPN
eurjchem-610	279	9	,	,	PUNCT
eurjchem-610	279	10	2004	2004	NUM
eurjchem-610	279	11	.	.	PUNCT
eurjchem-610	280	1	[	[	X
eurjchem-610	280	2	3	3	NUM
eurjchem-610	280	3	]	]	PUNCT
eurjchem-610	280	4	.	.	PUNCT
eurjchem-610	281	1	hassa	hassa	PROPN
eurjchem-610	281	2	,	,	PUNCT
eurjchem-610	281	3	i.	i.	PROPN
eurjchem-610	281	4	;	;	PUNCT
eurjchem-610	281	5	marnelli	marnelli	PROPN
eurjchem-610	281	6	,	,	PUNCT
eurjchem-610	281	7	e.	e.	PROPN
eurjchem-610	281	8	r.	r.	PROPN
eurjchem-610	281	9	;	;	PUNCT
eurjchem-610	281	10	lin	lin	PROPN
eurjchem-610	281	11	,	,	PUNCT
eurjchem-610	281	12	l.	l.	PROPN
eurjchem-610	281	13	c.	c.	PROPN
eurjchem-610	281	14	;	;	PUNCT
eurjchem-610	281	15	fowler	fowler	PROPN
eurjchem-610	281	16	,	,	PUNCT
eurjchem-610	281	17	f.	f.	PROPN
eurjchem-610	281	18	w.	w.	PROPN
eurjchem-610	281	19	;	;	PUNCT
eurjchem-610	281	20	levy	levy	NOUN
eurjchem-610	281	21	,	,	PUNCT
eurjchem-610	281	22	a.	a.	PROPN
eurjchem-610	281	23	b.	b.	PROPN
eurjchem-610	281	24	j.	j.	PROPN
eurjchem-610	281	25	org	org	PROPN
eurjchem-610	281	26	.	.	PUNCT
eurjchem-610	281	27	chem	chem	PROPN
eurjchem-610	281	28	.	.	PUNCT
eurjchem-610	282	1	1981	1981	NUM
eurjchem-610	282	2	,	,	PUNCT
eurjchem-610	282	3	46	46	NUM
eurjchem-610	282	4	,	,	PUNCT
eurjchem-610	282	5	157‐162	157‐162	NUM
eurjchem-610	282	6	.	.	PUNCT
eurjchem-610	283	1	[	[	X
eurjchem-610	283	2	4	4	NUM
eurjchem-610	283	3	]	]	PUNCT
eurjchem-610	283	4	.	.	PUNCT
eurjchem-610	284	1	rawal	rawal	PROPN
eurjchem-610	284	2	,	,	PUNCT
eurjchem-610	284	3	r.	r.	PROPN
eurjchem-610	284	4	j.	j.	PROPN
eurjchem-610	284	5	;	;	PUNCT
eurjchem-610	284	6	jones	jones	PROPN
eurjchem-610	284	7	,	,	PUNCT
eurjchem-610	284	8	m.	m.	NOUN
eurjchem-610	284	9	p.	p.	NOUN
eurjchem-610	284	10	;	;	PUNCT
eurjchem-610	284	11	cava	cava	NOUN
eurjchem-610	284	12	,	,	PUNCT
eurjchem-610	284	13	k.	k.	PROPN
eurjchem-610	284	14	j.	j.	PROPN
eurjchem-610	284	15	org	org	PROPN
eurjchem-610	284	16	.	.	PUNCT
eurjchem-610	285	1	chem.1987	chem.1987	PROPN
eurjchem-610	285	2	,	,	PUNCT
eurjchem-610	285	3	52	52	NUM
eurjchem-610	285	4	,	,	PUNCT
eurjchem-610	285	5	19‐24	19‐24	NUM
eurjchem-610	285	6	.	.	PUNCT
eurjchem-610	286	1	[	[	X
eurjchem-610	286	2	5	5	NUM
eurjchem-610	286	3	]	]	PUNCT
eurjchem-610	286	4	.	.	PUNCT
eurjchem-610	287	1	wasserman	wasserman	PROPN
eurjchem-610	287	2	,	,	PUNCT
eurjchem-610	287	3	h.	h.	PROPN
eurjchem-610	287	4	h.	h.	PROPN
eurjchem-610	287	5	;	;	PUNCT
eurjchem-610	287	6	berger	berger	PROPN
eurjchem-610	287	7	,	,	PUNCT
eurjchem-610	287	8	g.	g.	PROPN
eurjchem-610	287	9	d.	d.	PROPN
eurjchem-610	287	10	;	;	PUNCT
eurjchem-610	287	11	cho	cho	PROPN
eurjchem-610	287	12	,	,	PUNCT
eurjchem-610	287	13	k.	k.	PROPN
eurjchem-610	287	14	r.	r.	PROPN
eurjchem-610	287	15	tetrahedron	tetrahedron	PROPN
eurjchem-610	287	16	lett	lett	PROPN
eurjchem-610	287	17	.	.	PUNCT
eurjchem-610	287	18	1982	1982	NUM
eurjchem-610	287	19	,	,	PUNCT
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eurjchem-610	287	21	,	,	PUNCT
eurjchem-610	287	22	465‐468	465‐468	NOUN
eurjchem-610	287	23	.	.	PUNCT
eurjchem-610	288	1	[	[	X
eurjchem-610	288	2	6	6	NUM
eurjchem-610	288	3	]	]	PUNCT
eurjchem-610	288	4	.	.	PUNCT
eurjchem-610	289	1	slaikh	slaikh	PROPN
eurjchem-610	289	2	,	,	PUNCT
eurjchem-610	289	3	n.	n.	PROPN
eurjchem-610	289	4	s.	s.	PROPN
eurjchem-610	289	5	;	;	PUNCT
eurjchem-610	289	6	gajare	gajare	PROPN
eurjchem-610	289	7	,	,	PUNCT
eurjchem-610	289	8	a.	a.	PROPN
eurjchem-610	289	9	s.	s.	PROPN
eurjchem-610	289	10	;	;	PUNCT
eurjchem-610	289	11	deshpande	deshpande	PROPN
eurjchem-610	289	12	,	,	PUNCT
eurjchem-610	289	13	v.	v.	PROPN
eurjchem-610	289	14	h.	h.	PROPN
eurjchem-610	289	15	;	;	PUNCT
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eurjchem-610	289	17	,	,	PUNCT
eurjchem-610	289	18	a.	a.	PROPN
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eurjchem-610	289	21	lett	lett	PROPN
eurjchem-610	289	22	.	.	PROPN
eurjchem-610	290	1	2000	2000	NUM
eurjchem-610	290	2	,	,	PUNCT
eurjchem-610	290	3	41	41	NUM
eurjchem-610	290	4	,	,	PUNCT
eurjchem-610	290	5	385‐387	385‐387	NUM
eurjchem-610	290	6	.	.	PUNCT
eurjchem-610	291	1	[	[	X
eurjchem-610	291	2	7	7	NUM
eurjchem-610	291	3	]	]	PUNCT
eurjchem-610	291	4	.	.	PUNCT
eurjchem-610	292	1	apelqvist	apelqvist	NOUN
eurjchem-610	292	2	,	,	PUNCT
eurjchem-610	292	3	t.	t.	PROPN
eurjchem-610	292	4	;	;	PUNCT
eurjchem-610	292	5	wensbo	wensbo	PROPN
eurjchem-610	292	6	,	,	PUNCT
eurjchem-610	292	7	d.	d.	PROPN
eurjchem-610	292	8	tetrahedron	tetrahedron	PROPN
eurjchem-610	292	9	lett	lett	PROPN
eurjchem-610	292	10	.	.	PUNCT
eurjchem-610	292	11	1996	1996	NUM
eurjchem-610	292	12	,	,	PUNCT
eurjchem-610	292	13	37	37	NUM
eurjchem-610	292	14	,	,	PUNCT
eurjchem-610	292	15	1471‐1472	1471‐1472	NUM
eurjchem-610	292	16	.	.	PUNCT
eurjchem-610	293	1	[	[	X
eurjchem-610	293	2	8	8	NUM
eurjchem-610	293	3	]	]	SYM
eurjchem-610	293	4	.	.	PUNCT
eurjchem-610	293	5	klai	klai	PROPN
eurjchem-610	293	6	,	,	PUNCT
eurjchem-610	293	7	n.	n.	NOUN
eurjchem-610	293	8	;	;	PUNCT
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eurjchem-610	293	10	,	,	PUNCT
eurjchem-610	293	11	m.	m.	NOUN
eurjchem-610	293	12	;	;	PUNCT
eurjchem-610	293	13	khettache	khettache	PROPN
eurjchem-610	293	14	,	,	PUNCT
eurjchem-610	293	15	n.	n.	PROPN
eurjchem-610	293	16	;	;	PUNCT
eurjchem-610	293	17	belghit	belghit	NOUN
eurjchem-610	293	18	,	,	PUNCT
eurjchem-610	293	19	m.	m.	NOUN
eurjchem-610	293	20	y.	y.	PROPN
eurjchem-610	293	21	;	;	PUNCT
eurjchem-610	293	22	regainia	regainia	PROPN
eurjchem-610	293	23	,	,	PUNCT
eurjchem-610	293	24	z.	z.	PROPN
eurjchem-610	293	25	;	;	PUNCT
eurjchem-610	293	26	aouf	aouf	PROPN
eurjchem-610	293	27	,	,	PUNCT
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eurjchem-610	293	31	.	.	PUNCT
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eurjchem-610	293	33	.	.	PUNCT
eurjchem-610	294	1	2004	2004	NUM
eurjchem-610	294	2	,	,	PUNCT
eurjchem-610	294	3	41	41	NUM
eurjchem-610	294	4	,	,	PUNCT
eurjchem-610	294	5	57‐60	57‐60	NUM
eurjchem-610	294	6	.	.	PUNCT
eurjchem-610	295	1	[	[	X
eurjchem-610	295	2	9	9	NUM
eurjchem-610	295	3	]	]	PUNCT
eurjchem-610	295	4	.	.	PUNCT
eurjchem-610	296	1	cheraiet	cheraiet	PROPN
eurjchem-610	296	2	,	,	PUNCT
eurjchem-610	296	3	z.	z.	PROPN
eurjchem-610	296	4	;	;	PUNCT
eurjchem-610	296	5	ouarna	ouarna	PROPN
eurjchem-610	296	6	,	,	PUNCT
eurjchem-610	296	7	s.	s.	PROPN
eurjchem-610	296	8	;	;	PUNCT
eurjchem-610	296	9	jamel	jamel	PROPN
eurjchem-610	296	10	,	,	PUNCT
eurjchem-610	296	11	z.	z.	PROPN
eurjchem-610	296	12	;	;	PUNCT
eurjchem-610	296	13	berredjem	berredjem	PROPN
eurjchem-610	296	14	,	,	PUNCT
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eurjchem-610	296	16	;	;	PUNCT
eurjchem-610	296	17	aouf	aouf	PROPN
eurjchem-610	296	18	,	,	PUNCT
eurjchem-610	296	19	n.	n.	PROPN
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eurjchem-610	296	21	.	.	PUNCT
eurjchem-610	297	1	j.	j.	PROPN
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eurjchem-610	297	3	.	.	PUNCT
eurjchem-610	298	1	2012	2012	NUM
eurjchem-610	298	2	,	,	PUNCT
eurjchem-610	298	3	4(3	4(3	NUM
eurjchem-610	298	4	)	)	PUNCT
eurjchem-610	298	5	,	,	PUNCT
eurjchem-610	298	6	73‐79	73‐79	NUM
eurjchem-610	298	7	.	.	PUNCT
eurjchem-610	299	1	[	[	X
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eurjchem-610	299	3	]	]	PUNCT
eurjchem-610	299	4	.	.	PUNCT
eurjchem-610	300	1	cheraiet	cheraiet	PROPN
eurjchem-610	300	2	,	,	PUNCT
eurjchem-610	300	3	z.	z.	PROPN
eurjchem-610	300	4	;	;	PUNCT
eurjchem-610	300	5	ouarna	ouarna	PROPN
eurjchem-610	300	6	,	,	PUNCT
eurjchem-610	300	7	s.	s.	PROPN
eurjchem-610	300	8	;	;	PUNCT
eurjchem-610	300	9	hessainia	hessainia	PROPN
eurjchem-610	300	10	,	,	PUNCT
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eurjchem-610	300	12	;	;	PUNCT
eurjchem-610	300	13	berredjem	berredjem	NOUN
eurjchem-610	300	14	,	,	PUNCT
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eurjchem-610	300	16	;	;	PUNCT
eurjchem-610	300	17	aouf	aouf	PROPN
eurjchem-610	300	18	,	,	PUNCT
eurjchem-610	300	19	n.	n.	PROPN
eurjchem-610	300	20	isrn	isrn	PROPN
eurjchem-610	300	21	org	org	PROPN
eurjchem-610	300	22	.	.	PUNCT
eurjchem-610	300	23	chem	chem	PROPN
eurjchem-610	300	24	.	.	PUNCT
eurjchem-610	301	1	2012	2012	NUM
eurjchem-610	301	2	,	,	PUNCT
eurjchem-610	301	3	404235	404235	NUM
eurjchem-610	301	4	,	,	PUNCT
eurjchem-610	301	5	1‐8	1‐8	NUM
eurjchem-610	301	6	.	.	PUNCT
eurjchem-610	302	1	[	[	X
eurjchem-610	302	2	11	11	NUM
eurjchem-610	302	3	]	]	PUNCT
eurjchem-610	302	4	.	.	PUNCT
eurjchem-610	303	1	kozhevnikov	kozhevnikov	PROPN
eurjchem-610	303	2	,	,	PUNCT
eurjchem-610	303	3	i.v	i.v	PROPN
eurjchem-610	303	4	.	.	PUNCT
eurjchem-610	303	5	j.	j.	PROPN
eurjchem-610	303	6	mol	mol	PROPN
eurjchem-610	303	7	.	.	PROPN
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eurjchem-610	303	9	.	.	PUNCT
eurjchem-610	304	1	a	a	DET
eurjchem-610	304	2	:	:	PUNCT
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eurjchem-610	304	4	.	.	PUNCT
eurjchem-610	305	1	2009	2009	NUM
eurjchem-610	305	2	,	,	PUNCT
eurjchem-610	305	3	305	305	NUM
eurjchem-610	305	4	,	,	PUNCT
eurjchem-610	305	5	1‐2	1‐2	NUM
eurjchem-610	305	6	,	,	PUNCT
eurjchem-610	305	7	104‐111	104‐111	NUM
eurjchem-610	305	8	.	.	PUNCT
eurjchem-610	306	1	[	[	X
eurjchem-610	306	2	12	12	NUM
eurjchem-610	306	3	]	]	PUNCT
eurjchem-610	306	4	.	.	PUNCT
eurjchem-610	307	1	day	day	PROPN
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eurjchem-610	307	3	;	;	PUNCT
eurjchem-610	307	4	klemperer	klemperer	PROPN
eurjchem-610	307	5	,	,	PUNCT
eurjchem-610	307	6	w.	w.	PROPN
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eurjchem-610	307	9	.	.	PUNCT
eurjchem-610	308	1	1985	1985	NUM
eurjchem-610	308	2	,	,	PUNCT
eurjchem-610	308	3	228	228	NUM
eurjchem-610	308	4	,	,	PUNCT
eurjchem-610	308	5	533‐538	533‐538	NUM
eurjchem-610	308	6	.	.	PUNCT
eurjchem-610	309	1	[	[	X
eurjchem-610	309	2	13	13	NUM
eurjchem-610	309	3	]	]	PUNCT
eurjchem-610	309	4	.	.	PUNCT
eurjchem-610	310	1	keita	keita	PROPN
eurjchem-610	310	2	,	,	PUNCT
eurjchem-610	310	3	b.	b.	PROPN
eurjchem-610	310	4	;	;	PUNCT
eurjchem-610	310	5	abdeldjalil	abdeldjalil	PROPN
eurjchem-610	310	6	,	,	PUNCT
eurjchem-610	310	7	e.	e.	PROPN
eurjchem-610	310	8	;	;	PUNCT
eurjchem-610	310	9	nadjo	nadjo	PROPN
eurjchem-610	310	10	,	,	PUNCT
eurjchem-610	310	11	l.	l.	PROPN
eurjchem-610	310	12	;	;	PUNCT
eurjchem-610	310	13	avisse	avisse	PROPN
eurjchem-610	310	14	,	,	PUNCT
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eurjchem-610	310	16	;	;	PUNCT
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eurjchem-610	310	18	,	,	PUNCT
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eurjchem-610	310	20	;	;	PUNCT
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eurjchem-610	310	22	,	,	PUNCT
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eurjchem-610	310	24	;	;	PUNCT
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eurjchem-610	311	2	.	.	PUNCT
eurjchem-610	312	1	2000	2000	NUM
eurjchem-610	312	2	,	,	PUNCT
eurjchem-610	312	3	2	2	NUM
eurjchem-610	312	4	,	,	PUNCT
eurjchem-610	312	5	145‐149	145‐149	NUM
eurjchem-610	312	6	.	.	PUNCT
eurjchem-610	313	1	[	[	X
eurjchem-610	313	2	14	14	NUM
eurjchem-610	313	3	]	]	PUNCT
eurjchem-610	313	4	.	.	PUNCT
eurjchem-610	314	1	romanelli	romanelli	PROPN
eurjchem-610	314	2	,	,	PUNCT
eurjchem-610	314	3	g.	g.	PROPN
eurjchem-610	314	4	t.	t.	PROPN
eurjchem-610	314	5	;	;	PUNCT
eurjchem-610	314	6	autino	autino	PROPN
eurjchem-610	314	7	,	,	PUNCT
eurjchem-610	314	8	j.	j.	PROPN
eurjchem-610	314	9	c.	c.	PROPN
eurjchem-610	314	10	;	;	PUNCT
eurjchem-610	314	11	baronetti	baronetti	PROPN
eurjchem-610	314	12	,	,	PUNCT
eurjchem-610	314	13	g.	g.	PROPN
eurjchem-610	314	14	;	;	PUNCT
eurjchem-610	314	15	thomas	thomas	PROPN
eurjchem-610	314	16	,	,	PUNCT
eurjchem-610	314	17	h.	h.	PROPN
eurjchem-610	314	18	j.	j.	PROPN
eurjchem-610	314	19	molecules	molecules	PROPN
eurjchem-610	314	20	2001	2001	NUM
eurjchem-610	314	21	,	,	PUNCT
eurjchem-610	314	22	6	6	NUM
eurjchem-610	314	23	,	,	PUNCT
eurjchem-610	314	24	1006‐1011	1006‐1011	NUM
eurjchem-610	314	25	.	.	PUNCT
eurjchem-610	315	1	[	[	X
eurjchem-610	315	2	15	15	NUM
eurjchem-610	315	3	]	]	PUNCT
eurjchem-610	315	4	.	.	PUNCT
eurjchem-610	316	1	romanelli	romanelli	PROPN
eurjchem-610	316	2	,	,	PUNCT
eurjchem-610	316	3	g.	g.	PROPN
eurjchem-610	316	4	;	;	PUNCT
eurjchem-610	316	5	autino	autino	PROPN
eurjchem-610	316	6	,	,	PUNCT
eurjchem-610	316	7	j.	j.	PROPN
eurjchem-610	316	8	c.	c.	PROPN
eurjchem-610	316	9	;	;	PUNCT
eurjchem-610	316	10	baronetti	baronetti	PROPN
eurjchem-610	316	11	,	,	PUNCT
eurjchem-610	316	12	g.	g.	PROPN
eurjchem-610	316	13	;	;	PUNCT
eurjchem-610	316	14	thomas	thomas	PROPN
eurjchem-610	316	15	,	,	PUNCT
eurjchem-610	316	16	h.	h.	PROPN
eurjchem-610	316	17	j.	j.	PROPN
eurjchem-610	316	18	tetrahedron	tetrahedron	PROPN
eurjchem-610	316	19	lett	lett	PROPN
eurjchem-610	316	20	.	.	PUNCT
eurjchem-610	317	1	2002	2002	NUM
eurjchem-610	317	2	,	,	PUNCT
eurjchem-610	317	3	43	43	NUM
eurjchem-610	317	4	,	,	PUNCT
eurjchem-610	317	5	7589‐7591	7589‐7591	NUM
eurjchem-610	317	6	.	.	PUNCT
eurjchem-610	318	1	[	[	X
eurjchem-610	318	2	16	16	NUM
eurjchem-610	318	3	]	]	PUNCT
eurjchem-610	318	4	.	.	PUNCT
eurjchem-610	319	1	romanelli	romanelli	PROPN
eurjchem-610	319	2	,	,	PUNCT
eurjchem-610	319	3	g.	g.	PROPN
eurjchem-610	319	4	;	;	PUNCT
eurjchem-610	319	5	thomas	thomas	PROPN
eurjchem-610	319	6	,	,	PUNCT
eurjchem-610	319	7	h.	h.	PROPN
eurjchem-610	319	8	j.	j.	PROPN
eurjchem-610	319	9	;	;	PUNCT
eurjchem-610	319	10	querini	querini	PROPN
eurjchem-610	319	11	,	,	PUNCT
eurjchem-610	319	12	c.	c.	PROPN
eurjchem-610	319	13	a.	a.	NOUN
eurjchem-610	319	14	appl	appl	PROPN
eurjchem-610	319	15	.	.	PUNCT
eurjchem-610	320	1	catal	catal	PROPN
eurjchem-610	320	2	.	.	PUNCT
eurjchem-610	321	1	2001	2001	NUM
eurjchem-610	321	2	,	,	PUNCT
eurjchem-610	321	3	217	217	NUM
eurjchem-610	321	4	,	,	PUNCT
eurjchem-610	321	5	131‐141	131‐141	NUM
eurjchem-610	321	6	.	.	PUNCT
eurjchem-610	322	1	[	[	X
eurjchem-610	322	2	17	17	NUM
eurjchem-610	322	3	]	]	SYM
eurjchem-610	322	4	.	.	PUNCT
eurjchem-610	322	5	heravi	heravi	PROPN
eurjchem-610	322	6	,	,	PUNCT
eurjchem-610	322	7	m.	m.	NOUN
eurjchem-610	322	8	m.	m.	NOUN
eurjchem-610	322	9	;	;	PUNCT
eurjchem-610	322	10	bakhtiari	bakhtiari	PROPN
eurjchem-610	322	11	,	,	PUNCT
eurjchem-610	322	12	k.	k.	PROPN
eurjchem-610	322	13	;	;	PUNCT
eurjchem-610	322	14	bamoharram	bamoharram	PROPN
eurjchem-610	322	15	,	,	PUNCT
eurjchem-610	322	16	f.	f.	PROPN
eurjchem-610	322	17	f.	f.	PROPN
eurjchem-610	322	18	;	;	PUNCT
eurjchem-610	322	19	tehrani	tehrani	PROPN
eurjchem-610	322	20	,	,	PUNCT
eurjchem-610	322	21	m.	m.	NOUN
eurjchem-610	322	22	h.	h.	PROPN
eurjchem-610	322	23	monatsh	monatsh	PROPN
eurjchem-610	322	24	.	.	PUNCT
eurjchem-610	323	1	chem	chem	PROPN
eurjchem-610	323	2	.	.	PUNCT
eurjchem-610	324	1	2007	2007	NUM
eurjchem-610	324	2	,	,	PUNCT
eurjchem-610	324	3	138	138	NUM
eurjchem-610	324	4	,	,	PUNCT
eurjchem-610	324	5	465‐467	465‐467	NOUN
eurjchem-610	324	6	.	.	PUNCT
eurjchem-610	325	1	[	[	X
eurjchem-610	325	2	18	18	NUM
eurjchem-610	325	3	]	]	PUNCT
eurjchem-610	325	4	.	.	PUNCT
eurjchem-610	326	1	kishore	kishore	PROPN
eurjchem-610	326	2	,	,	PUNCT
eurjchem-610	326	3	p.	p.	PROPN
eurjchem-610	326	4	s.	s.	PROPN
eurjchem-610	326	5	;	;	PUNCT
eurjchem-610	326	6	viswanathan	viswanathan	PROPN
eurjchem-610	326	7	,	,	PUNCT
eurjchem-610	326	8	b.	b.	PROPN
eurjchem-610	326	9	;	;	PUNCT
eurjchem-610	326	10	varadarajan	varadarajan	ADJ
eurjchem-610	326	11	,	,	PUNCT
eurjchem-610	326	12	t.	t.	PROPN
eurjchem-610	326	13	k.	k.	PROPN
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eurjchem-610	326	16	.	.	PUNCT
eurjchem-610	327	1	2006	2006	NUM
eurjchem-610	327	2	,	,	PUNCT
eurjchem-610	327	3	47	47	NUM
eurjchem-610	327	4	,	,	PUNCT
eurjchem-610	327	5	429‐431	429‐431	NUM
eurjchem-610	327	6	.	.	PUNCT
eurjchem-610	328	1	[	[	X
eurjchem-610	328	2	19	19	NUM
eurjchem-610	328	3	]	]	PUNCT
eurjchem-610	328	4	.	.	PUNCT
eurjchem-610	329	1	romaneli	romaneli	PROPN
eurjchem-610	329	2	,	,	PUNCT
eurjchem-610	329	3	g.	g.	PROPN
eurjchem-610	329	4	p.	p.	PROPN
eurjchem-610	329	5	;	;	PUNCT
eurjchem-610	330	1	bennardi	bennardi	PROPN
eurjchem-610	330	2	,	,	PUNCT
eurjchem-610	330	3	d.	d.	PROPN
eurjchem-610	330	4	o.	o.	PROPN
eurjchem-610	330	5	;	;	PUNCT
eurjchem-610	330	6	autino	autino	PROPN
eurjchem-610	330	7	,	,	PUNCT
eurjchem-610	330	8	j.	j.	PROPN
eurjchem-610	330	9	c.	c.	PROPN
eurjchem-610	330	10	;	;	PUNCT
eurjchem-610	330	11	baronetti	baronetti	PROPN
eurjchem-610	330	12	,	,	PUNCT
eurjchem-610	330	13	g.	g.	PROPN
eurjchem-610	330	14	;	;	PUNCT
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eurjchem-610	330	16	,	,	PUNCT
eurjchem-610	330	17	g.	g.	PROPN
eurjchem-610	330	18	t.	t.	PROPN
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eurjchem-610	330	20	of	of	ADP
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eurjchem-610	330	22	.	.	PUNCT
eurjchem-610	331	1	2008	2008	NUM
eurjchem-610	331	2	,	,	PUNCT
eurjchem-610	331	3	5	5	NUM
eurjchem-610	331	4	,	,	PUNCT
eurjchem-610	331	5	641‐647	641‐647	NUM
eurjchem-610	331	6	.	.	PUNCT
eurjchem-610	332	1	[	[	X
eurjchem-610	332	2	20	20	NUM
eurjchem-610	332	3	]	]	PUNCT
eurjchem-610	332	4	.	.	PUNCT
eurjchem-610	333	1	heydari	heydari	PROPN
eurjchem-610	333	2	,	,	PUNCT
eurjchem-610	333	3	a.	a.	NOUN
eurjchem-610	333	4	;	;	PUNCT
eurjchem-610	333	5	shiroodi	shiroodi	PROPN
eurjchem-610	333	6	,	,	PUNCT
eurjchem-610	333	7	r.	r.	PROPN
eurjchem-610	333	8	k.	k.	PROPN
eurjchem-610	333	9	;	;	PUNCT
eurjchem-610	333	10	hamadi	hamadi	PROPN
eurjchem-610	333	11	,	,	PUNCT
eurjchem-610	333	12	h.	h.	PROPN
eurjchem-610	333	13	;	;	PUNCT
eurjchem-610	333	14	esfandyari	esfandyari	NOUN
eurjchem-610	333	15	,	,	PUNCT
eurjchem-610	333	16	m.	m.	NOUN
eurjchem-610	333	17	;	;	PUNCT
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eurjchem-610	333	19	,	,	PUNCT
eurjchem-610	333	20	m.	m.	NOUN
eurjchem-610	333	21	tetrahedron	tetrahedron	PROPN
eurjchem-610	333	22	lett	lett	PROPN
eurjchem-610	333	23	.	.	PUNCT
eurjchem-610	334	1	2007	2007	NUM
eurjchem-610	334	2	,	,	PUNCT
eurjchem-610	334	3	48	48	NUM
eurjchem-610	334	4	,	,	PUNCT
eurjchem-610	334	5	5865‐5868	5865‐5868	NUM
eurjchem-610	334	6	.	.	PUNCT
eurjchem-610	335	1	[	[	X
eurjchem-610	335	2	21	21	NUM
eurjchem-610	335	3	]	]	PUNCT
eurjchem-610	335	4	.	.	PUNCT
eurjchem-610	336	1	dewynter	dewynter	PROPN
eurjchem-610	336	2	,	,	PUNCT
eurjchem-610	336	3	g.	g.	PROPN
eurjchem-610	336	4	,	,	PUNCT
eurjchem-610	336	5	aouf	aouf	PROPN
eurjchem-610	336	6	,	,	PUNCT
eurjchem-610	336	7	n.	n.	PROPN
eurjchem-610	336	8	;	;	PUNCT
eurjchem-610	336	9	criton	criton	PROPN
eurjchem-610	336	10	,	,	PUNCT
eurjchem-610	336	11	m.	m.	NOUN
eurjchem-610	336	12	;	;	PUNCT
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eurjchem-610	336	14	,	,	PUNCT
eurjchem-610	336	15	j.	j.	PROPN
eurjchem-610	336	16	l.	l.	PROPN
eurjchem-610	336	17	tetrahedron	tetrahedron	PROPN
eurjchem-610	336	18	.	.	PUNCT
eurjchem-610	337	1	1993	1993	NUM
eurjchem-610	337	2	,	,	PUNCT
eurjchem-610	337	3	49	49	NUM
eurjchem-610	337	4	,	,	PUNCT
eurjchem-610	337	5	65‐76	65‐76	NOUN
eurjchem-610	337	6	.	.	PUNCT
eurjchem-610	338	1	[	[	X
eurjchem-610	338	2	22	22	NUM
eurjchem-610	338	3	]	]	PUNCT
eurjchem-610	338	4	.	.	PUNCT
eurjchem-610	339	1	aouf	aouf	PROPN
eurjchem-610	339	2	,	,	PUNCT
eurjchem-610	339	3	n.	n.	NOUN
eurjchem-610	339	4	;	;	PUNCT
eurjchem-610	339	5	dewynter	dewynter	PROPN
eurjchem-610	339	6	,	,	PUNCT
eurjchem-610	339	7	g.	g.	PROPN
eurjchem-610	339	8	;	;	PUNCT
eurjchem-610	339	9	montero	montero	PROPN
eurjchem-610	339	10	,	,	PUNCT
eurjchem-610	339	11	j.	j.	PROPN
eurjchem-610	339	12	l.	l.	PROPN
eurjchem-610	339	13	tettrahedron	tettrahedron	PROPN
eurjchem-610	339	14	lett	lett	PROPN
eurjchem-610	339	15	.	.	PROPN
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eurjchem-610	339	17	,	,	PUNCT
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eurjchem-610	339	19	,	,	PUNCT
eurjchem-610	339	20	6545‐6546	6545‐6546	NUM
eurjchem-610	339	21	.	.	PUNCT
eurjchem-610	340	1	[	[	X
eurjchem-610	340	2	23	23	NUM
eurjchem-610	340	3	]	]	PUNCT
eurjchem-610	340	4	.	.	PUNCT
eurjchem-610	340	5	dewynter	dewynter	PROPN
eurjchem-610	340	6	,	,	PUNCT
eurjchem-610	340	7	g.	g.	PROPN
eurjchem-610	340	8	;	;	PUNCT
eurjchem-610	340	9	aouf	aouf	PROPN
eurjchem-610	340	10	,	,	PUNCT
eurjchem-610	340	11	n.	n.	PROPN
eurjchem-610	340	12	;	;	PUNCT
eurjchem-610	340	13	regainia	regainia	PROPN
eurjchem-610	340	14	,	,	PUNCT
eurjchem-610	340	15	z.	z.	PROPN
eurjchem-610	340	16	;	;	PUNCT
eurjchem-610	340	17	montero	montero	PROPN
eurjchem-610	340	18	,	,	PUNCT
eurjchem-610	340	19	j.	j.	PROPN
eurjchem-610	340	20	l.	l.	PROPN
eurjchem-610	340	21	tetrahedron	tetrahedron	PROPN
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eurjchem-610	340	23	,	,	PUNCT
eurjchem-610	340	24	52	52	NUM
eurjchem-610	340	25	,	,	PUNCT
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eurjchem-610	340	27	.	.	PUNCT
eurjchem-610	341	1	[	[	X
eurjchem-610	341	2	24	24	NUM
eurjchem-610	341	3	]	]	PUNCT
eurjchem-610	341	4	.	.	PUNCT
eurjchem-610	342	1	baronetti	baronetti	PROPN
eurjchem-610	342	2	,	,	PUNCT
eurjchem-610	342	3	g.	g.	PROPN
eurjchem-610	342	4	t.	t.	PROPN
eurjchem-610	342	5	;	;	PUNCT
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eurjchem-610	342	7	,	,	PUNCT
eurjchem-610	342	8	l.	l.	PROPN
eurjchem-610	342	9	;	;	PUNCT
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eurjchem-610	342	11	,	,	PUNCT
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eurjchem-610	342	13	;	;	PUNCT
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eurjchem-610	342	18	.	.	PUNCT
eurjchem-610	343	1	catal	catal	PROPN
eurjchem-610	343	2	.	.	PUNCT
eurjchem-610	344	1	a.	a.	PROPN
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eurjchem-610	344	3	,	,	PUNCT
eurjchem-610	344	4	172	172	NUM
eurjchem-610	344	5	,	,	PUNCT
eurjchem-610	344	6	265‐272	265‐272	NUM
eurjchem-610	344	7	.	.	PUNCT
eurjchem-610	345	1	[	[	X
eurjchem-610	345	2	25	25	NUM
eurjchem-610	345	3	]	]	PUNCT
eurjchem-610	345	4	.	.	PUNCT
eurjchem-610	346	1	regainia	regainia	PROPN
eurjchem-610	346	2	,	,	PUNCT
eurjchem-610	346	3	z.	z.	PROPN
eurjchem-610	346	4	;	;	PUNCT
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eurjchem-610	346	6	,	,	PUNCT
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eurjchem-610	346	8	;	;	PUNCT
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eurjchem-610	346	10	,	,	PUNCT
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eurjchem-610	346	12	;	;	PUNCT
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eurjchem-610	346	14	,	,	PUNCT
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eurjchem-610	346	16	;	;	PUNCT
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eurjchem-610	346	18	,	,	PUNCT
eurjchem-610	346	19	j.	j.	PROPN
eurjchem-610	346	20	l.	l.	PROPN
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eurjchem-610	346	22	.	.	PUNCT
eurjchem-610	347	1	2000	2000	NUM
eurjchem-610	347	2	,	,	PUNCT
eurjchem-610	347	3	56	56	NUM
eurjchem-610	347	4	,	,	PUNCT
eurjchem-610	347	5	381‐387	381‐387	NUM
eurjchem-610	347	6	.	.	PUNCT
eurjchem-610	348	1	[	[	X
eurjchem-610	348	2	26	26	NUM
eurjchem-610	348	3	]	]	PUNCT
eurjchem-610	348	4	.	.	PUNCT
eurjchem-610	349	1	bendjeddou	bendjeddou	PROPN
eurjchem-610	349	2	,	,	PUNCT
eurjchem-610	349	3	a.	a.	NOUN
eurjchem-610	349	4	;	;	PUNCT
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eurjchem-610	349	6	,	,	PUNCT
eurjchem-610	349	7	m.	m.	NOUN
eurjchem-610	349	8	;	;	PUNCT
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eurjchem-610	349	10	,	,	PUNCT
eurjchem-610	349	11	z.	z.	PROPN
eurjchem-610	349	12	;	;	PUNCT
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eurjchem-610	349	14	,	,	PUNCT
eurjchem-610	349	15	z.	z.	PROPN
eurjchem-610	349	16	;	;	PUNCT
eurjchem-610	349	17	aouf	aouf	PROPN
eurjchem-610	349	18	,	,	PUNCT
eurjchem-610	349	19	n.	n.	NOUN
eurjchem-610	349	20	phosphorus	phosphorus	NOUN
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eurjchem-610	349	22	.	.	PUNCT
eurjchem-610	350	1	2006	2006	NUM
eurjchem-610	350	2	,	,	PUNCT
eurjchem-610	350	3	181	181	NUM
eurjchem-610	350	4	,	,	PUNCT
eurjchem-610	350	5	1351‐1356	1351‐1356	NUM
eurjchem-610	350	6	.	.	PUNCT
eurjchem-610	351	1	[	[	X
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eurjchem-610	351	3	]	]	PUNCT
eurjchem-610	351	4	.	.	PUNCT
eurjchem-610	352	1	wang	wang	PROPN
eurjchem-610	352	2	,	,	PUNCT
eurjchem-610	352	3	g.	g.	PROPN
eurjchem-610	352	4	;	;	PUNCT
eurjchem-610	352	5	li	li	PROPN
eurjchem-610	352	6	,	,	PUNCT
eurjchem-610	352	7	c.	c.	PROPN
eurjchem-610	352	8	;	;	PUNCT
eurjchem-610	352	9	jia	jia	PROPN
eurjchem-610	352	10	,	,	PUNCT
eurjchem-610	352	11	x.	x.	PROPN
eurjchem-610	352	12	tetrahedron	tetrahedron	PROPN
eurjchem-610	352	13	lett	lett	PROPN
eurjchem-610	352	14	.	.	PUNCT
eurjchem-610	352	15	2009	2009	NUM
eurjchem-610	352	16	,	,	PUNCT
eurjchem-610	352	17	50	50	NUM
eurjchem-610	352	18	,	,	PUNCT
eurjchem-610	352	19	1438‐1440	1438‐1440	NUM
eurjchem-610	352	20	.	.	PUNCT