id sid tid token lemma pos eurjchem-65 1 1 microsoft microsoft PROPN eurjchem-65 1 2 word word NOUN eurjchem-65 1 3 european_journal_of_chemistry_1_4_2010_322_324_65 european_journal_of_chemistry_1_4_2010_322_324_65 PROPN eurjchem-65 1 4 european european ADJ eurjchem-65 1 5     SPACE eurjchem-65 1 6 journal journal NOUN eurjchem-65 1 7     SPACE eurjchem-65 1 8 of of ADP eurjchem-65 1 9     SPACE eurjchem-65 1 10 chemistry chemistry NOUN eurjchem-65 1 11     SPACE eurjchem-65 1 12 1 1 NUM eurjchem-65 1 13     SPACE eurjchem-65 1 14 ( ( PUNCT eurjchem-65 1 15 4 4 NUM eurjchem-65 1 16 ) ) PUNCT eurjchem-65 1 17     SPACE eurjchem-65 1 18 ( ( PUNCT eurjchem-65 1 19 2010 2010 NUM eurjchem-65 1 20 ) ) PUNCT eurjchem-65 1 21     SPACE eurjchem-65 1 22 322‐324 322‐324 NUM eurjchem-65 1 23         SPACE eurjchem-65 1 24 european european ADJ eurjchem-65 1 25     SPACE eurjchem-65 1 26 journal journal NOUN eurjchem-65 1 27     SPACE eurjchem-65 1 28 of of ADP eurjchem-65 1 29     SPACE eurjchem-65 1 30 chemistry chemistry NOUN eurjchem-65 1 31     SPACE eurjchem-65 1 32 issn issn VERB eurjchem-65 1 33     SPACE eurjchem-65 1 34 2153‐2249 2153‐2249 NUM eurjchem-65 1 35     SPACE eurjchem-65 1 36 ( ( PUNCT eurjchem-65 1 37 print print NOUN eurjchem-65 1 38 ) ) PUNCT eurjchem-65 1 39     SPACE eurjchem-65 1 40 / / SYM eurjchem-65 1 41     SPACE eurjchem-65 1 42 issn issn VERB eurjchem-65 1 43     SPACE eurjchem-65 1 44 2153‐2257 2153‐2257 NUM eurjchem-65 1 45     SPACE eurjchem-65 1 46 ( ( PUNCT eurjchem-65 1 47 online online ADJ eurjchem-65 1 48 ) ) PUNCT eurjchem-65 1 49     SPACE eurjchem-65 1 50   NOUN eurjchem-65 1 51     SPACE eurjchem-65 1 52 2010 2010 NUM eurjchem-65 1 53     SPACE eurjchem-65 1 54 eurjchem eurjchem NOUN eurjchem-65 1 55     SPACE eurjchem-65 1 56 doi:10.5155 doi:10.5155 NOUN eurjchem-65 1 57 / / SYM eurjchem-65 1 58 eurjchem.1.4.322‐324.65 eurjchem.1.4.322‐324.65 NOUN eurjchem-65 1 59                 SPACE eurjchem-65 1 60 european european ADJ eurjchem-65 1 61     SPACE eurjchem-65 1 62 journal journal NOUN eurjchem-65 1 63     SPACE eurjchem-65 1 64 of of ADP eurjchem-65 1 65     SPACE eurjchem-65 1 66 chemistry chemistry NOUN eurjchem-65 1 67     SPACE eurjchem-65 1 68 journal journal NOUN eurjchem-65 1 69     SPACE eurjchem-65 1 70 homepage homepage NOUN eurjchem-65 1 71 : : PUNCT eurjchem-65 1 72     SPACE eurjchem-65 1 73 www.eurjchem.com www.eurjchem.com NOUN eurjchem-65 1 74                     SPACE eurjchem-65 1 75 synthesis synthesis NOUN eurjchem-65 1 76     SPACE eurjchem-65 1 77 of of ADP eurjchem-65 1 78     SPACE eurjchem-65 1 79 some some DET eurjchem-65 1 80     SPACE eurjchem-65 1 81 pyridyl pyridyl NOUN eurjchem-65 1 82     SPACE eurjchem-65 1 83 and and CCONJ eurjchem-65 1 84     SPACE eurjchem-65 1 85 cyclohexyl cyclohexyl NOUN eurjchem-65 1 86     SPACE eurjchem-65 1 87 substituted substitute VERB eurjchem-65 1 88     SPACE eurjchem-65 1 89 1,2,4 1,2,4 NUM eurjchem-65 1 90     SPACE eurjchem-65 1 91 triazole triazole NOUN eurjchem-65 1 92 , , PUNCT eurjchem-65 1 93       SPACE eurjchem-65 1 94 1,3,4‐thiadiazole 1,3,4‐thiadiazole NUM eurjchem-65 1 95     SPACE eurjchem-65 1 96 and and CCONJ eurjchem-65 1 97     SPACE eurjchem-65 1 98 1,3,4‐oxadiazole 1,3,4‐oxadiazole ADJ eurjchem-65 1 99     SPACE eurjchem-65 1 100 derivatives derivative NOUN eurjchem-65 1 101     SPACE eurjchem-65 1 102 sattar sattar PROPN eurjchem-65 1 103     SPACE eurjchem-65 1 104 ebrahimi ebrahimi PROPN eurjchem-65 1 105     SPACE eurjchem-65 1 106 department department NOUN eurjchem-65 1 107     SPACE eurjchem-65 1 108 of of ADP eurjchem-65 1 109     SPACE eurjchem-65 1 110 chemistry chemistry NOUN eurjchem-65 1 111 , , PUNCT eurjchem-65 1 112     SPACE eurjchem-65 1 113 islamic islamic ADJ eurjchem-65 1 114     SPACE eurjchem-65 1 115 azad azad PROPN eurjchem-65 1 116     SPACE eurjchem-65 1 117 university university NOUN eurjchem-65 1 118 , , PUNCT eurjchem-65 1 119     SPACE eurjchem-65 1 120 malayer malayer NOUN eurjchem-65 1 121     SPACE eurjchem-65 1 122 branch branch NOUN eurjchem-65 1 123 , , PUNCT eurjchem-65 1 124     SPACE eurjchem-65 1 125 ir­65718­117 ir­65718­117 PROPN eurjchem-65 1 126 , , PUNCT eurjchem-65 1 127     SPACE eurjchem-65 1 128 iran iran PROPN eurjchem-65 1 129     SPACE eurjchem-65 1 130 corresponding corresponding ADJ eurjchem-65 1 131     SPACE eurjchem-65 1 132 author author NOUN eurjchem-65 1 133     SPACE eurjchem-65 1 134 at at ADP eurjchem-65 1 135 : : PUNCT eurjchem-65 1 136     SPACE eurjchem-65 1 137 department department NOUN eurjchem-65 1 138     SPACE eurjchem-65 1 139 of of ADP eurjchem-65 1 140     SPACE eurjchem-65 1 141 chemistry chemistry NOUN eurjchem-65 1 142 , , PUNCT eurjchem-65 1 143     SPACE eurjchem-65 1 144 islamic islamic ADJ eurjchem-65 1 145     SPACE eurjchem-65 1 146 azad azad PROPN eurjchem-65 1 147     SPACE eurjchem-65 1 148 university university NOUN eurjchem-65 1 149 , , PUNCT eurjchem-65 1 150     SPACE eurjchem-65 1 151 malayer malayer NOUN eurjchem-65 1 152     SPACE eurjchem-65 1 153 branch branch NOUN eurjchem-65 1 154 , , PUNCT eurjchem-65 1 155     SPACE eurjchem-65 1 156 ir­65718­117 ir­65718­117 PROPN eurjchem-65 1 157 , , PUNCT eurjchem-65 1 158     SPACE eurjchem-65 1 159 iran iran PROPN eurjchem-65 1 160 . . PUNCT eurjchem-65 1 161     SPACE eurjchem-65 2 1 tel tel PROPN eurjchem-65 2 2 . . PUNCT eurjchem-65 2 3 : : PUNCT eurjchem-65 2 4     SPACE eurjchem-65 2 5 +98.851.22230195 +98.851.22230195 PROPN eurjchem-65 2 6 ; ; PUNCT eurjchem-65 2 7     SPACE eurjchem-65 2 8 fax fax NOUN eurjchem-65 2 9 : : PUNCT eurjchem-65 2 10     SPACE eurjchem-65 2 11 +98.851.2230154 +98.851.2230154 PROPN eurjchem-65 2 12 . . PUNCT eurjchem-65 2 13       SPACE eurjchem-65 2 14 e­mail e­mail NOUN eurjchem-65 2 15     SPACE eurjchem-65 2 16 address address NOUN eurjchem-65 2 17 : : PUNCT eurjchem-65 2 18     SPACE eurjchem-65 2 19 seyonesi@gmail.com seyonesi@gmail.com X eurjchem-65 2 20     SPACE eurjchem-65 2 21 ( ( PUNCT eurjchem-65 2 22 s. s. PROPN eurjchem-65 2 23     SPACE eurjchem-65 2 24 ebrahimi ebrahimi PROPN eurjchem-65 2 25 ) ) PUNCT eurjchem-65 2 26 . . PUNCT eurjchem-65 2 27                                 SPACE eurjchem-65 2 28 article article NOUN eurjchem-65 2 29     SPACE eurjchem-65 2 30 information information NOUN eurjchem-65 2 31         SPACE eurjchem-65 2 32 abstract abstract ADJ eurjchem-65 2 33 received receive VERB eurjchem-65 2 34 : : PUNCT eurjchem-65 2 35     SPACE eurjchem-65 2 36 16 16 NUM eurjchem-65 2 37     SPACE eurjchem-65 2 38 april april PROPN eurjchem-65 2 39     SPACE eurjchem-65 2 40 2010 2010 NUM eurjchem-65 2 41     SPACE eurjchem-65 2 42 received receive VERB eurjchem-65 2 43     SPACE eurjchem-65 2 44 in in ADP eurjchem-65 2 45     SPACE eurjchem-65 2 46 revised revise VERB eurjchem-65 2 47     SPACE eurjchem-65 2 48 form form NOUN eurjchem-65 2 49 : : PUNCT eurjchem-65 2 50     SPACE eurjchem-65 2 51 01 01 NUM eurjchem-65 2 52     SPACE eurjchem-65 2 53 september september PROPN eurjchem-65 2 54     SPACE eurjchem-65 2 55 2010 2010 NUM eurjchem-65 2 56     SPACE eurjchem-65 2 57 accepted accept VERB eurjchem-65 2 58 : : PUNCT eurjchem-65 2 59     SPACE eurjchem-65 2 60 26 26 NUM eurjchem-65 2 61     SPACE eurjchem-65 2 62 september september PROPN eurjchem-65 2 63     SPACE eurjchem-65 2 64 2010 2010 NUM eurjchem-65 2 65     SPACE eurjchem-65 2 66 online online NOUN eurjchem-65 2 67 : : PUNCT eurjchem-65 2 68     SPACE eurjchem-65 2 69 31 31 NUM eurjchem-65 2 70     SPACE eurjchem-65 2 71 december december PROPN eurjchem-65 2 72     SPACE eurjchem-65 2 73 2010 2010 NUM eurjchem-65 2 74     SPACE eurjchem-65 2 75 keywords keyword VERB eurjchem-65 2 76         SPACE eurjchem-65 2 77 new new ADJ eurjchem-65 2 78     SPACE eurjchem-65 2 79 1,2,4‐triazoles 1,2,4‐triazole NOUN eurjchem-65 2 80     SPACE eurjchem-65 2 81 ( ( PUNCT eurjchem-65 2 82 4a‐c 4a‐c NOUN eurjchem-65 2 83 ) ) PUNCT eurjchem-65 2 84 , , PUNCT eurjchem-65 2 85     SPACE eurjchem-65 2 86 1,3,4‐thiadiazoles 1,3,4‐thiadiazoles PROPN eurjchem-65 2 87     SPACE eurjchem-65 2 88 ( ( PUNCT eurjchem-65 2 89 5a‐c 5a‐c NOUN eurjchem-65 2 90 ) ) PUNCT eurjchem-65 2 91     SPACE eurjchem-65 2 92 and and CCONJ eurjchem-65 2 93     SPACE eurjchem-65 2 94 1,3,4‐oxadiazoles 1,3,4‐oxadiazole NOUN eurjchem-65 2 95     SPACE eurjchem-65 2 96 ( ( PUNCT eurjchem-65 2 97 6a‐c 6a‐c NOUN eurjchem-65 2 98 ) ) PUNCT eurjchem-65 2 99     SPACE eurjchem-65 2 100 containing contain VERB eurjchem-65 2 101     SPACE eurjchem-65 2 102 isomeric isomeric ADJ eurjchem-65 2 103     SPACE eurjchem-65 2 104 pyridyl pyridyl NOUN eurjchem-65 2 105     SPACE eurjchem-65 2 106 and and CCONJ eurjchem-65 2 107     SPACE eurjchem-65 2 108 cyclohexyl cyclohexyl NOUN eurjchem-65 2 109     SPACE eurjchem-65 2 110 were be AUX eurjchem-65 2 111     SPACE eurjchem-65 2 112 synthesized synthesize VERB eurjchem-65 2 113     SPACE eurjchem-65 2 114 by by ADP eurjchem-65 2 115     SPACE eurjchem-65 2 116 intramolecular intramolecular ADJ eurjchem-65 2 117     SPACE eurjchem-65 2 118 cyclization cyclization NOUN eurjchem-65 2 119     SPACE eurjchem-65 2 120 of of ADP eurjchem-65 2 121     SPACE eurjchem-65 2 122 1,4‐ 1,4‐ NUM eurjchem-65 2 123 disubstituted disubstitute VERB eurjchem-65 2 124     SPACE eurjchem-65 2 125 thiosemicarbazides thiosemicarbazide NOUN eurjchem-65 2 126     SPACE eurjchem-65 2 127 ( ( PUNCT eurjchem-65 2 128 3a‐c 3a‐c PROPN eurjchem-65 2 129 ) ) PUNCT eurjchem-65 2 130     SPACE eurjchem-65 2 131 in in ADP eurjchem-65 2 132     SPACE eurjchem-65 2 133 alkaline alkaline NOUN eurjchem-65 2 134     SPACE eurjchem-65 2 135 media medium NOUN eurjchem-65 2 136 , , PUNCT eurjchem-65 2 137     SPACE eurjchem-65 2 138 acid acid NOUN eurjchem-65 2 139     SPACE eurjchem-65 2 140 and and CCONJ eurjchem-65 2 141     SPACE eurjchem-65 2 142 neutral neutral ADJ eurjchem-65 2 143     SPACE eurjchem-65 2 144 condition condition NOUN eurjchem-65 2 145     SPACE eurjchem-65 2 146 respectively respectively ADV eurjchem-65 2 147 . . PUNCT eurjchem-65 2 148     SPACE eurjchem-65 2 149 the the DET eurjchem-65 2 150     SPACE eurjchem-65 2 151 chemical chemical NOUN eurjchem-65 2 152     SPACE eurjchem-65 2 153 structures structure NOUN eurjchem-65 2 154     SPACE eurjchem-65 2 155 of of ADP eurjchem-65 2 156     SPACE eurjchem-65 2 157 newly newly ADV eurjchem-65 2 158     SPACE eurjchem-65 2 159 synthesized synthesize VERB eurjchem-65 2 160     SPACE eurjchem-65 2 161 compounds compound NOUN eurjchem-65 2 162     SPACE eurjchem-65 2 163 were be AUX eurjchem-65 2 164     SPACE eurjchem-65 2 165 established establish VERB eurjchem-65 2 166     SPACE eurjchem-65 2 167 with with ADP eurjchem-65 2 168     SPACE eurjchem-65 2 169 help help NOUN eurjchem-65 2 170     SPACE eurjchem-65 2 171 of of ADP eurjchem-65 2 172     SPACE eurjchem-65 2 173 ft‐ir ft‐ir NOUN eurjchem-65 2 174 , , PUNCT eurjchem-65 2 175     SPACE eurjchem-65 2 176 1h‐nmr 1h‐nmr NUM eurjchem-65 2 177     SPACE eurjchem-65 2 178 and and CCONJ eurjchem-65 2 179     SPACE eurjchem-65 2 180 mass mass PROPN eurjchem-65 2 181     SPACE eurjchem-65 2 182 spectral spectral ADJ eurjchem-65 2 183     SPACE eurjchem-65 2 184 data datum NOUN eurjchem-65 2 185 . . PUNCT eurjchem-65 2 186     SPACE eurjchem-65 3 1 1,2,4‐triazole 1,2,4‐triazole NOUN eurjchem-65 3 2     SPACE eurjchem-65 3 3 1,3,4‐thiadiazole 1,3,4‐thiadiazole NUM eurjchem-65 3 4     SPACE eurjchem-65 3 5 1,3,4‐oxadiazole 1,3,4‐oxadiazole NUM eurjchem-65 3 6     SPACE eurjchem-65 3 7 thiosemicarbazide thiosemicarbazide NOUN eurjchem-65 3 8         SPACE eurjchem-65 3 9 1 1 NUM eurjchem-65 3 10 . . PUNCT eurjchem-65 3 11     SPACE eurjchem-65 3 12 introduction introduction NOUN eurjchem-65 3 13         SPACE eurjchem-65 3 14 in in ADP eurjchem-65 3 15     SPACE eurjchem-65 3 16 the the DET eurjchem-65 3 17     SPACE eurjchem-65 3 18 last last ADJ eurjchem-65 3 19     SPACE eurjchem-65 3 20 few few ADJ eurjchem-65 3 21     SPACE eurjchem-65 3 22 decades decade NOUN eurjchem-65 3 23 , , PUNCT eurjchem-65 3 24     SPACE eurjchem-65 3 25 the the DET eurjchem-65 3 26     SPACE eurjchem-65 3 27 chemistry chemistry NOUN eurjchem-65 3 28     SPACE eurjchem-65 3 29 of of ADP eurjchem-65 3 30     SPACE eurjchem-65 3 31 five‐membered five‐membered ADJ eurjchem-65 3 32     SPACE eurjchem-65 3 33 heterocyclic heterocyclic NOUN eurjchem-65 3 34     SPACE eurjchem-65 3 35 rings ring NOUN eurjchem-65 3 36     SPACE eurjchem-65 3 37 has have AUX eurjchem-65 3 38     SPACE eurjchem-65 3 39 received receive VERB eurjchem-65 3 40     SPACE eurjchem-65 3 41 considerable considerable ADJ eurjchem-65 3 42     SPACE eurjchem-65 3 43 attention attention NOUN eurjchem-65 3 44     SPACE eurjchem-65 3 45 owing owe VERB eurjchem-65 3 46     SPACE eurjchem-65 3 47 to to ADP eurjchem-65 3 48     SPACE eurjchem-65 3 49 their their PRON eurjchem-65 3 50     SPACE eurjchem-65 3 51 synthetic synthetic NOUN eurjchem-65 3 52     SPACE eurjchem-65 3 53 and and CCONJ eurjchem-65 3 54     SPACE eurjchem-65 3 55 effective effective ADJ eurjchem-65 3 56     SPACE eurjchem-65 3 57 biological biological ADJ eurjchem-65 3 58     SPACE eurjchem-65 3 59 importance importance NOUN eurjchem-65 3 60 . . PUNCT eurjchem-65 3 61     SPACE eurjchem-65 4 1 derivatives derivative NOUN eurjchem-65 4 2     SPACE eurjchem-65 4 3 of of ADP eurjchem-65 4 4     SPACE eurjchem-65 4 5 1,3,4 1,3,4 NUM eurjchem-65 4 6 – – PUNCT eurjchem-65 4 7 oxadiazole oxadiazole NOUN eurjchem-65 4 8 , , PUNCT eurjchem-65 4 9     SPACE eurjchem-65 4 10 1,3,4 1,3,4 NUM eurjchem-65 4 11 – – PUNCT eurjchem-65 4 12 thiadiazole thiadiazole NOUN eurjchem-65 4 13     SPACE eurjchem-65 4 14 and and CCONJ eurjchem-65 4 15     SPACE eurjchem-65 4 16 1,2,4‐triazole 1,2,4‐triazole NOUN eurjchem-65 4 17     SPACE eurjchem-65 4 18 have have AUX eurjchem-65 4 19     SPACE eurjchem-65 4 20 been be AUX eurjchem-65 4 21     SPACE eurjchem-65 4 22 found find VERB eurjchem-65 4 23     SPACE eurjchem-65 4 24 to to PART eurjchem-65 4 25     SPACE eurjchem-65 4 26 possess possess VERB eurjchem-65 4 27     SPACE eurjchem-65 4 28 a a DET eurjchem-65 4 29     SPACE eurjchem-65 4 30 wide wide ADJ eurjchem-65 4 31     SPACE eurjchem-65 4 32 spectrum spectrum NOUN eurjchem-65 4 33     SPACE eurjchem-65 4 34 of of ADP eurjchem-65 4 35     SPACE eurjchem-65 4 36 biological biological ADJ eurjchem-65 4 37     SPACE eurjchem-65 4 38 activity activity NOUN eurjchem-65 4 39     SPACE eurjchem-65 5 1 [ [ X eurjchem-65 5 2 1‐ 1‐ NUM eurjchem-65 5 3 8 8 NUM eurjchem-65 5 4 ] ] PUNCT eurjchem-65 5 5 . . PUNCT eurjchem-65 5 6     SPACE eurjchem-65 6 1 moreover moreover ADV eurjchem-65 6 2 , , PUNCT eurjchem-65 6 3     SPACE eurjchem-65 6 4 the the DET eurjchem-65 6 5     SPACE eurjchem-65 6 6 mercapto‐ mercapto‐ NOUN eurjchem-65 6 7     SPACE eurjchem-65 6 8 and and CCONJ eurjchem-65 6 9     SPACE eurjchem-65 6 10 thione‐substituted thione‐substitute VERB eurjchem-65 6 11     SPACE eurjchem-65 6 12 1,2,4‐ 1,2,4‐ NUM eurjchem-65 6 13 triazole triazole NOUN eurjchem-65 6 14     SPACE eurjchem-65 6 15 ring ring NOUN eurjchem-65 6 16     SPACE eurjchem-65 6 17 systems system NOUN eurjchem-65 6 18     SPACE eurjchem-65 6 19 have have AUX eurjchem-65 6 20     SPACE eurjchem-65 6 21 been be AUX eurjchem-65 6 22     SPACE eurjchem-65 6 23 well well ADV eurjchem-65 6 24     SPACE eurjchem-65 6 25 studied study VERB eurjchem-65 6 26     SPACE eurjchem-65 6 27 and and CCONJ eurjchem-65 6 28     SPACE eurjchem-65 6 29 a a DET eurjchem-65 6 30     SPACE eurjchem-65 6 31 variety variety NOUN eurjchem-65 6 32     SPACE eurjchem-65 6 33 of of ADP eurjchem-65 6 34     SPACE eurjchem-65 6 35 biological biological ADJ eurjchem-65 6 36     SPACE eurjchem-65 6 37 activities activity NOUN eurjchem-65 6 38     SPACE eurjchem-65 6 39 have have AUX eurjchem-65 6 40     SPACE eurjchem-65 6 41 been be AUX eurjchem-65 6 42     SPACE eurjchem-65 6 43 reported report VERB eurjchem-65 6 44     SPACE eurjchem-65 6 45 for for ADP eurjchem-65 6 46     SPACE eurjchem-65 6 47 a a DET eurjchem-65 6 48     SPACE eurjchem-65 6 49 large large ADJ eurjchem-65 6 50     SPACE eurjchem-65 6 51 number number NOUN eurjchem-65 6 52     SPACE eurjchem-65 6 53 of of ADP eurjchem-65 6 54     SPACE eurjchem-65 6 55 their their PRON eurjchem-65 6 56     SPACE eurjchem-65 6 57 derivatives derivative NOUN eurjchem-65 6 58 , , PUNCT eurjchem-65 6 59     SPACE eurjchem-65 6 60 such such ADJ eurjchem-65 6 61     SPACE eurjchem-65 6 62 as as ADP eurjchem-65 6 63     SPACE eurjchem-65 6 64 antiproliferative antiproliferative NOUN eurjchem-65 6 65     SPACE eurjchem-65 7 1 [ [ X eurjchem-65 7 2 9 9 NUM eurjchem-65 7 3 ] ] PUNCT eurjchem-65 7 4 , , PUNCT eurjchem-65 7 5     SPACE eurjchem-65 7 6 antimicrobial antimicrobial ADJ eurjchem-65 7 7     SPACE eurjchem-65 8 1 [ [ X eurjchem-65 8 2 10 10 NUM eurjchem-65 8 3 ] ] PUNCT eurjchem-65 8 4 , , PUNCT eurjchem-65 8 5     SPACE eurjchem-65 8 6 antifungal antifungal PROPN eurjchem-65 8 7     SPACE eurjchem-65 9 1 [ [ X eurjchem-65 9 2 11 11 NUM eurjchem-65 9 3 ] ] PUNCT eurjchem-65 9 4 , , PUNCT eurjchem-65 9 5     SPACE eurjchem-65 9 6 anticancer anticancer NOUN eurjchem-65 9 7     SPACE eurjchem-65 10 1 [ [ X eurjchem-65 10 2 12,13 12,13 NUM eurjchem-65 10 3 ] ] NOUN eurjchem-65 10 4     SPACE eurjchem-65 10 5 properties property NOUN eurjchem-65 10 6 . . PUNCT eurjchem-65 10 7     SPACE eurjchem-65 10 8 in in ADP eurjchem-65 10 9     SPACE eurjchem-65 10 10 addition addition NOUN eurjchem-65 10 11 , , PUNCT eurjchem-65 10 12     SPACE eurjchem-65 10 13 mercapto‐1,2,4‐triazoles mercapto‐1,2,4‐triazole NOUN eurjchem-65 10 14     SPACE eurjchem-65 10 15 are be AUX eurjchem-65 10 16     SPACE eurjchem-65 10 17 also also ADV eurjchem-65 10 18     SPACE eurjchem-65 10 19 of of ADP eurjchem-65 10 20     SPACE eurjchem-65 10 21 great great ADJ eurjchem-65 10 22     SPACE eurjchem-65 10 23 utility utility NOUN eurjchem-65 10 24     SPACE eurjchem-65 10 25 to to PART eurjchem-65 10 26     SPACE eurjchem-65 10 27 prepare prepare VERB eurjchem-65 10 28     SPACE eurjchem-65 10 29 other other ADJ eurjchem-65 10 30     SPACE eurjchem-65 10 31 heterocyclic heterocyclic NOUN eurjchem-65 10 32     SPACE eurjchem-65 10 33 compounds compound VERB eurjchem-65 10 34     SPACE eurjchem-65 11 1 [ [ X eurjchem-65 11 2 14‐16 14‐16 NUM eurjchem-65 11 3 ] ] X eurjchem-65 11 4 . . PUNCT eurjchem-65 11 5       SPACE eurjchem-65 11 6 prompted prompt VERB eurjchem-65 11 7     SPACE eurjchem-65 11 8 by by ADP eurjchem-65 11 9     SPACE eurjchem-65 11 10 these these DET eurjchem-65 11 11     SPACE eurjchem-65 11 12 observations observation NOUN eurjchem-65 11 13     SPACE eurjchem-65 11 14 and and CCONJ eurjchem-65 11 15     SPACE eurjchem-65 11 16 as as ADP eurjchem-65 11 17     SPACE eurjchem-65 11 18 a a DET eurjchem-65 11 19     SPACE eurjchem-65 11 20 continuation continuation NOUN eurjchem-65 11 21     SPACE eurjchem-65 11 22 of of ADP eurjchem-65 11 23     SPACE eurjchem-65 11 24 our our PRON eurjchem-65 11 25     SPACE eurjchem-65 11 26 research research NOUN eurjchem-65 11 27     SPACE eurjchem-65 11 28 program program NOUN eurjchem-65 11 29     SPACE eurjchem-65 11 30 on on ADP eurjchem-65 11 31     SPACE eurjchem-65 11 32 the the DET eurjchem-65 11 33     SPACE eurjchem-65 11 34 synthesis synthesis NOUN eurjchem-65 11 35     SPACE eurjchem-65 11 36 of of ADP eurjchem-65 11 37     SPACE eurjchem-65 11 38 1,2,4‐triazole 1,2,4‐triazole NOUN eurjchem-65 11 39     SPACE eurjchem-65 11 40 derivatives derivative NOUN eurjchem-65 11 41     SPACE eurjchem-65 11 42 [ [ X eurjchem-65 11 43 17‐21 17‐21 X eurjchem-65 11 44 ] ] X eurjchem-65 11 45 , , PUNCT eurjchem-65 11 46     SPACE eurjchem-65 11 47 herein herein NOUN eurjchem-65 11 48     SPACE eurjchem-65 11 49 we we PRON eurjchem-65 11 50     SPACE eurjchem-65 11 51 wish wish VERB eurjchem-65 11 52     SPACE eurjchem-65 11 53 to to PART eurjchem-65 11 54     SPACE eurjchem-65 11 55 disclose disclose VERB eurjchem-65 11 56     SPACE eurjchem-65 11 57 synthesis synthesis NOUN eurjchem-65 11 58     SPACE eurjchem-65 11 59 of of ADP eurjchem-65 11 60     SPACE eurjchem-65 11 61 some some DET eurjchem-65 11 62     SPACE eurjchem-65 11 63 novel novel NOUN eurjchem-65 11 64     SPACE eurjchem-65 11 65 five five NUM eurjchem-65 11 66     SPACE eurjchem-65 11 67 memberd memberd NOUN eurjchem-65 11 68     SPACE eurjchem-65 11 69 heterocycle heterocycle NOUN eurjchem-65 11 70     SPACE eurjchem-65 11 71 derivatives derivative NOUN eurjchem-65 11 72     SPACE eurjchem-65 11 73 via via ADP eurjchem-65 11 74     SPACE eurjchem-65 11 75 intramolecular intramolecular ADJ eurjchem-65 11 76     SPACE eurjchem-65 11 77 cyclization cyclization NOUN eurjchem-65 11 78     SPACE eurjchem-65 11 79 reactions reaction NOUN eurjchem-65 11 80     SPACE eurjchem-65 11 81 in in ADP eurjchem-65 11 82     SPACE eurjchem-65 11 83 good good ADJ eurjchem-65 11 84     SPACE eurjchem-65 11 85 yield yield NOUN eurjchem-65 11 86 . . PUNCT eurjchem-65 11 87         SPACE eurjchem-65 12 1 2 2 NUM eurjchem-65 12 2 . . PUNCT eurjchem-65 12 3     SPACE eurjchem-65 12 4 experimental experimental ADJ eurjchem-65 12 5         SPACE eurjchem-65 12 6 2.1 2.1 NUM eurjchem-65 12 7 . . PUNCT eurjchem-65 12 8     SPACE eurjchem-65 12 9 instrumentation instrumentation NOUN eurjchem-65 12 10         SPACE eurjchem-65 12 11 all all DET eurjchem-65 12 12     SPACE eurjchem-65 12 13 melting melting NOUN eurjchem-65 12 14     SPACE eurjchem-65 12 15 points point NOUN eurjchem-65 12 16     SPACE eurjchem-65 12 17 are be AUX eurjchem-65 12 18     SPACE eurjchem-65 12 19 uncorrected uncorrecte VERB eurjchem-65 12 20 . . PUNCT eurjchem-65 12 21     SPACE eurjchem-65 12 22 ir ir AUX eurjchem-65 12 23     SPACE eurjchem-65 12 24 spectra spectra NOUN eurjchem-65 12 25     SPACE eurjchem-65 12 26 ( ( PUNCT eurjchem-65 12 27 kbr kbr PROPN eurjchem-65 12 28 ) ) PUNCT eurjchem-65 12 29     SPACE eurjchem-65 12 30 were be AUX eurjchem-65 12 31     SPACE eurjchem-65 12 32 recorded record VERB eurjchem-65 12 33     SPACE eurjchem-65 12 34 on on ADP eurjchem-65 12 35     SPACE eurjchem-65 12 36 a a DET eurjchem-65 12 37     SPACE eurjchem-65 12 38 galaxy galaxy NOUN eurjchem-65 12 39     SPACE eurjchem-65 12 40 series series NOUN eurjchem-65 12 41     SPACE eurjchem-65 12 42 ft‐ir ft‐ir NOUN eurjchem-65 12 43     SPACE eurjchem-65 12 44 5000 5000 NUM eurjchem-65 12 45     SPACE eurjchem-65 12 46 spectrophotometer spectrophotometer NOUN eurjchem-65 12 47 . . PUNCT eurjchem-65 12 48     SPACE eurjchem-65 13 1 1h‐ 1h‐ NUM eurjchem-65 13 2 nmr nmr NOUN eurjchem-65 13 3     SPACE eurjchem-65 13 4 spectra spectra NOUN eurjchem-65 13 5     SPACE eurjchem-65 13 6 ( ( PUNCT eurjchem-65 13 7 500 500 NUM eurjchem-65 13 8     SPACE eurjchem-65 13 9 mhz mhz NOUN eurjchem-65 13 10 ) ) PUNCT eurjchem-65 13 11     SPACE eurjchem-65 13 12 were be AUX eurjchem-65 13 13     SPACE eurjchem-65 13 14 recorded record VERB eurjchem-65 13 15     SPACE eurjchem-65 13 16 on on ADP eurjchem-65 13 17     SPACE eurjchem-65 13 18 a a DET eurjchem-65 13 19     SPACE eurjchem-65 13 20 bruker bruker NOUN eurjchem-65 13 21     SPACE eurjchem-65 13 22 instrument instrument NOUN eurjchem-65 13 23     SPACE eurjchem-65 13 24 using use VERB eurjchem-65 13 25     SPACE eurjchem-65 13 26 tms tms NOUN eurjchem-65 13 27     SPACE eurjchem-65 13 28 as as ADP eurjchem-65 13 29     SPACE eurjchem-65 13 30 internal internal ADJ eurjchem-65 13 31     SPACE eurjchem-65 13 32 standard standard NOUN eurjchem-65 13 33     SPACE eurjchem-65 13 34 and and CCONJ eurjchem-65 13 35     SPACE eurjchem-65 13 36 dmso‐d6 dmso‐d6 NOUN eurjchem-65 13 37     SPACE eurjchem-65 13 38 as as ADP eurjchem-65 13 39     SPACE eurjchem-65 13 40 solvent solvent NOUN eurjchem-65 13 41 . . PUNCT eurjchem-65 13 42     SPACE eurjchem-65 13 43 mass mass PROPN eurjchem-65 13 44     SPACE eurjchem-65 13 45 spectra spectra NOUN eurjchem-65 13 46     SPACE eurjchem-65 13 47 were be AUX eurjchem-65 13 48     SPACE eurjchem-65 13 49 recorded record VERB eurjchem-65 13 50     SPACE eurjchem-65 13 51 on on ADP eurjchem-65 13 52     SPACE eurjchem-65 13 53 a a DET eurjchem-65 13 54     SPACE eurjchem-65 13 55 mat‐112‐s mat‐112‐ NOUN eurjchem-65 13 56     SPACE eurjchem-65 13 57 machine machine NOUN eurjchem-65 13 58     SPACE eurjchem-65 13 59 ( ( PUNCT eurjchem-65 13 60 ei ei PROPN eurjchem-65 13 61 , , PUNCT eurjchem-65 13 62     SPACE eurjchem-65 13 63 70 70 NUM eurjchem-65 13 64     SPACE eurjchem-65 13 65 ev ev NOUN eurjchem-65 13 66 ) ) PUNCT eurjchem-65 13 67 . . PUNCT eurjchem-65 13 68                     SPACE eurjchem-65 14 1 2.2 2.2 NUM eurjchem-65 14 2 . . PUNCT eurjchem-65 14 3     SPACE eurjchem-65 14 4 general general ADJ eurjchem-65 14 5     SPACE eurjchem-65 14 6 procedure procedure NOUN eurjchem-65 14 7     SPACE eurjchem-65 14 8 for for ADP eurjchem-65 14 9     SPACE eurjchem-65 14 10 the the DET eurjchem-65 14 11     SPACE eurjchem-65 14 12 synthesis synthesis NOUN eurjchem-65 14 13     SPACE eurjchem-65 14 14 of of ADP eurjchem-65 14 15     SPACE eurjchem-65 14 16 1,2,4­triazoles 1,2,4­triazoles NUM eurjchem-65 14 17     SPACE eurjchem-65 14 18 4a­c 4a­c NOUN eurjchem-65 14 19         SPACE eurjchem-65 14 20 a a DET eurjchem-65 14 21     SPACE eurjchem-65 14 22 solution solution NOUN eurjchem-65 14 23     SPACE eurjchem-65 14 24 of of ADP eurjchem-65 14 25     SPACE eurjchem-65 14 26 thiosemicarbazide thiosemicarbazide NOUN eurjchem-65 14 27     SPACE eurjchem-65 14 28 3a­c 3a­c NOUN eurjchem-65 14 29     SPACE eurjchem-65 14 30 ( ( PUNCT eurjchem-65 14 31 10 10 NUM eurjchem-65 14 32     SPACE eurjchem-65 14 33 mmol mmol NOUN eurjchem-65 14 34 ) ) PUNCT eurjchem-65 14 35     SPACE eurjchem-65 14 36 in in ADP eurjchem-65 14 37     SPACE eurjchem-65 14 38 2n 2n NUM eurjchem-65 14 39     SPACE eurjchem-65 14 40 naoh naoh NOUN eurjchem-65 14 41     SPACE eurjchem-65 14 42 ( ( PUNCT eurjchem-65 14 43 10 10 NUM eurjchem-65 14 44     SPACE eurjchem-65 14 45 ml ml NOUN eurjchem-65 14 46 ) ) PUNCT eurjchem-65 14 47     SPACE eurjchem-65 14 48 was be AUX eurjchem-65 14 49     SPACE eurjchem-65 14 50 refluxed refluxe VERB eurjchem-65 14 51     SPACE eurjchem-65 14 52 for for ADP eurjchem-65 14 53     SPACE eurjchem-65 14 54 3 3 NUM eurjchem-65 14 55     SPACE eurjchem-65 14 56 h. h. NOUN eurjchem-65 14 57     SPACE eurjchem-65 14 58 the the DET eurjchem-65 14 59     SPACE eurjchem-65 14 60 resulting result VERB eurjchem-65 14 61     SPACE eurjchem-65 14 62 solution solution NOUN eurjchem-65 14 63     SPACE eurjchem-65 14 64 was be AUX eurjchem-65 14 65     SPACE eurjchem-65 14 66 cooled cool VERB eurjchem-65 14 67     SPACE eurjchem-65 14 68 to to PART eurjchem-65 14 69     SPACE eurjchem-65 14 70 room room NOUN eurjchem-65 14 71     SPACE eurjchem-65 14 72 temperature temperature NOUN eurjchem-65 14 73     SPACE eurjchem-65 14 74 and and CCONJ eurjchem-65 14 75     SPACE eurjchem-65 14 76 acidified acidify VERB eurjchem-65 14 77     SPACE eurjchem-65 14 78 ( ( PUNCT eurjchem-65 14 79 ph ph VERB eurjchem-65 14 80     SPACE eurjchem-65 14 81 = = NOUN eurjchem-65 14 82     SPACE eurjchem-65 14 83 3 3 NUM eurjchem-65 14 84 ) ) PUNCT eurjchem-65 14 85     SPACE eurjchem-65 14 86 with with ADP eurjchem-65 14 87     SPACE eurjchem-65 14 88 2n 2n NUM eurjchem-65 14 89     SPACE eurjchem-65 14 90 hcl hcl PROPN eurjchem-65 14 91 . . PUNCT eurjchem-65 14 92       SPACE eurjchem-65 14 93 the the DET eurjchem-65 14 94     SPACE eurjchem-65 14 95 solid solid NOUN eurjchem-65 14 96     SPACE eurjchem-65 14 97 was be AUX eurjchem-65 14 98     SPACE eurjchem-65 14 99 filtered filter VERB eurjchem-65 14 100 , , PUNCT eurjchem-65 14 101     SPACE eurjchem-65 14 102 washed wash VERB eurjchem-65 14 103     SPACE eurjchem-65 14 104 with with ADP eurjchem-65 14 105     SPACE eurjchem-65 14 106 water water NOUN eurjchem-65 14 107 . . PUNCT eurjchem-65 14 108     SPACE eurjchem-65 15 1 the the DET eurjchem-65 15 2     SPACE eurjchem-65 15 3 compound compound NOUN eurjchem-65 15 4     SPACE eurjchem-65 15 5 so so ADV eurjchem-65 15 6     SPACE eurjchem-65 15 7 obtained obtain VERB eurjchem-65 15 8     SPACE eurjchem-65 15 9 was be AUX eurjchem-65 15 10     SPACE eurjchem-65 15 11 dried dry VERB eurjchem-65 15 12     SPACE eurjchem-65 15 13 and and CCONJ eurjchem-65 15 14     SPACE eurjchem-65 15 15 crystallized crystallize VERB eurjchem-65 15 16     SPACE eurjchem-65 15 17 from from ADP eurjchem-65 15 18     SPACE eurjchem-65 15 19 dmf dmf PROPN eurjchem-65 15 20 : : PUNCT eurjchem-65 15 21 etoh etoh PROPN eurjchem-65 15 22     SPACE eurjchem-65 15 23 ( ( PUNCT eurjchem-65 15 24 1:2 1:2 NUM eurjchem-65 15 25 ) ) PUNCT eurjchem-65 15 26     SPACE eurjchem-65 15 27 to to PART eurjchem-65 15 28     SPACE eurjchem-65 15 29 give give VERB eurjchem-65 15 30     SPACE eurjchem-65 15 31 compound compound NOUN eurjchem-65 15 32     SPACE eurjchem-65 15 33 4a­c 4a­c PROPN eurjchem-65 15 34     SPACE eurjchem-65 15 35 ( ( PUNCT eurjchem-65 15 36 scheme scheme NOUN eurjchem-65 15 37     SPACE eurjchem-65 15 38 1 1 NUM eurjchem-65 15 39 ) ) PUNCT eurjchem-65 15 40 . . PUNCT eurjchem-65 15 41     SPACE eurjchem-65 16 1 4­cyclohexyl­5­(pyridin­2­yl)­4h­1,2,4­triazole­3­thiol 4­cyclohexyl­5­(pyridin­2­yl)­4h­1,2,4­triazole­3­thiol NUM eurjchem-65 16 2     SPACE eurjchem-65 16 3 ( ( PUNCT eurjchem-65 16 4 4a 4a NUM eurjchem-65 16 5 ): ): PUNCT eurjchem-65 16 6     SPACE eurjchem-65 16 7 yield yield NOUN eurjchem-65 16 8 : : PUNCT eurjchem-65 16 9     SPACE eurjchem-65 16 10 87 87 NUM eurjchem-65 16 11 % % NOUN eurjchem-65 16 12 . . PUNCT eurjchem-65 16 13     SPACE eurjchem-65 17 1 m.p m.p PROPN eurjchem-65 17 2 . . PROPN eurjchem-65 17 3 : : PUNCT eurjchem-65 17 4     SPACE eurjchem-65 17 5 238‐240 238‐240 NUM eurjchem-65 17 6     SPACE eurjchem-65 17 7 oc oc PROPN eurjchem-65 17 8 . . PUNCT eurjchem-65 17 9     SPACE eurjchem-65 17 10 ir ir VERB eurjchem-65 17 11     SPACE eurjchem-65 17 12 ( ( PUNCT eurjchem-65 17 13 kbr kbr PROPN eurjchem-65 17 14 , , PUNCT eurjchem-65 17 15     SPACE eurjchem-65 17 16 cm‐1 cm‐1 NOUN eurjchem-65 17 17 ): ): PUNCT eurjchem-65 17 18     SPACE eurjchem-65 17 19 3098 3098 NUM eurjchem-65 17 20     SPACE eurjchem-65 17 21 (arom (arom PROPN eurjchem-65 17 22 . . PROPN eurjchem-65 17 23     SPACE eurjchem-65 17 24 ch ch NOUN eurjchem-65 17 25 ) ) PUNCT eurjchem-65 17 26 , , PUNCT eurjchem-65 17 27     SPACE eurjchem-65 17 28 2858 2858 NUM eurjchem-65 17 29     SPACE eurjchem-65 17 30 (aliph (aliph NOUN eurjchem-65 17 31 . . PUNCT eurjchem-65 17 32     SPACE eurjchem-65 17 33 ch ch NOUN eurjchem-65 17 34 ) ) PUNCT eurjchem-65 17 35 , , PUNCT eurjchem-65 17 36     SPACE eurjchem-65 17 37 2777 2777 NUM eurjchem-65 17 38     SPACE eurjchem-65 17 39 (sh (sh NOUN eurjchem-65 17 40 ) ) PUNCT eurjchem-65 17 41 , , PUNCT eurjchem-65 17 42     SPACE eurjchem-65 17 43 1556 1556 NUM eurjchem-65 17 44     SPACE eurjchem-65 17 45 (c (c PROPN eurjchem-65 17 46 = = SYM eurjchem-65 17 47 n n CCONJ eurjchem-65 17 48     SPACE eurjchem-65 17 49 and and CCONJ eurjchem-65 17 50     SPACE eurjchem-65 17 51 c c NOUN eurjchem-65 17 52 = = NOUN eurjchem-65 17 53 c c NOUN eurjchem-65 17 54 ) ) PUNCT eurjchem-65 17 55 . . PUNCT eurjchem-65 17 56     SPACE eurjchem-65 18 1 1h 1h NUM eurjchem-65 18 2     SPACE eurjchem-65 18 3 nmr nmr NOUN eurjchem-65 18 4     SPACE eurjchem-65 18 5 ( ( PUNCT eurjchem-65 18 6 dmso‐d6 dmso‐d6 PROPN eurjchem-65 18 7 , , PUNCT eurjchem-65 18 8     SPACE eurjchem-65 18 9 δ δ PROPN eurjchem-65 18 10 , , PUNCT eurjchem-65 18 11     SPACE eurjchem-65 18 12 ppm ppm NOUN eurjchem-65 18 13 ): ): PUNCT eurjchem-65 18 14     SPACE eurjchem-65 18 15 1.03 1.03 NUM eurjchem-65 18 16     SPACE eurjchem-65 18 17 ( ( PUNCT eurjchem-65 18 18 d d PROPN eurjchem-65 18 19 , , PUNCT eurjchem-65 18 20     SPACE eurjchem-65 18 21 j j PROPN eurjchem-65 18 22     SPACE eurjchem-65 18 23 = = NOUN eurjchem-65 18 24     SPACE eurjchem-65 18 25 11.6 11.6 NUM eurjchem-65 18 26     SPACE eurjchem-65 18 27 hz hz VERB eurjchem-65 18 28 , , PUNCT eurjchem-65 18 29     SPACE eurjchem-65 18 30 1h 1h NUM eurjchem-65 18 31 , , PUNCT eurjchem-65 18 32     SPACE eurjchem-65 18 33 haliph haliph NOUN eurjchem-65 18 34 . . PUNCT eurjchem-65 18 35 ) ) PUNCT eurjchem-65 18 36 , , PUNCT eurjchem-65 18 37     SPACE eurjchem-65 18 38 1.23 1.23 NUM eurjchem-65 18 39     SPACE eurjchem-65 18 40 ( ( PUNCT eurjchem-65 18 41 d d NOUN eurjchem-65 18 42 , , PUNCT eurjchem-65 18 43     SPACE eurjchem-65 18 44 2h 2h NUM eurjchem-65 18 45 , , PUNCT eurjchem-65 18 46     SPACE eurjchem-65 18 47 j j PROPN eurjchem-65 18 48     SPACE eurjchem-65 18 49 = = VERB eurjchem-65 18 50     SPACE eurjchem-65 18 51 11.7 11.7 NUM eurjchem-65 18 52     SPACE eurjchem-65 18 53 hz hz VERB eurjchem-65 18 54 , , PUNCT eurjchem-65 18 55     SPACE eurjchem-65 18 56 haliph haliph NOUN eurjchem-65 18 57 . . PUNCT eurjchem-65 18 58 ) ) PUNCT eurjchem-65 18 59 , , PUNCT eurjchem-65 18 60     SPACE eurjchem-65 18 61 1.57 1.57 NUM eurjchem-65 18 62     SPACE eurjchem-65 18 63 ( ( PUNCT eurjchem-65 18 64 d d PROPN eurjchem-65 18 65 , , PUNCT eurjchem-65 18 66     SPACE eurjchem-65 18 67 j j NOUN eurjchem-65 18 68     SPACE eurjchem-65 18 69 = = NOUN eurjchem-65 18 70     SPACE eurjchem-65 18 71 10.9 10.9 NUM eurjchem-65 18 72     SPACE eurjchem-65 18 73 hz hz VERB eurjchem-65 18 74 , , PUNCT eurjchem-65 18 75     SPACE eurjchem-65 18 76 1h 1h NUM eurjchem-65 18 77 , , PUNCT eurjchem-65 18 78     SPACE eurjchem-65 18 79 haliph haliph NOUN eurjchem-65 18 80 .. .. PUNCT eurjchem-65 18 81 ) ) PUNCT eurjchem-65 18 82 , , PUNCT eurjchem-65 18 83     SPACE eurjchem-65 18 84 1.67 1.67 NUM eurjchem-65 18 85     SPACE eurjchem-65 18 86 ( ( PUNCT eurjchem-65 18 87 d d PROPN eurjchem-65 18 88 , , PUNCT eurjchem-65 18 89     SPACE eurjchem-65 18 90 j j PROPN eurjchem-65 18 91     SPACE eurjchem-65 18 92 = = NOUN eurjchem-65 18 93     SPACE eurjchem-65 18 94 8.6 8.6 NUM eurjchem-65 18 95     SPACE eurjchem-65 18 96 hz hz VERB eurjchem-65 18 97 , , PUNCT eurjchem-65 18 98     SPACE eurjchem-65 18 99 2h 2h NUM eurjchem-65 18 100 , , PUNCT eurjchem-65 18 101     SPACE eurjchem-65 18 102 haliph haliph NOUN eurjchem-65 18 103 . . PUNCT eurjchem-65 18 104 ) ) PUNCT eurjchem-65 19 1 , , PUNCT eurjchem-65 19 2     SPACE eurjchem-65 19 3 1.73 1.73 NUM eurjchem-65 19 4     SPACE eurjchem-65 19 5 ( ( PUNCT eurjchem-65 19 6 d d PROPN eurjchem-65 19 7 , , PUNCT eurjchem-65 19 8     SPACE eurjchem-65 19 9 j j PROPN eurjchem-65 19 10     SPACE eurjchem-65 19 11 = = NOUN eurjchem-65 19 12     SPACE eurjchem-65 19 13 11.0 11.0 NUM eurjchem-65 19 14     SPACE eurjchem-65 19 15 hz hz VERB eurjchem-65 19 16 , , PUNCT eurjchem-65 19 17     SPACE eurjchem-65 19 18 2h 2h NUM eurjchem-65 19 19 , , PUNCT eurjchem-65 19 20     SPACE eurjchem-65 19 21 haliph haliph NOUN eurjchem-65 19 22 . . PUNCT eurjchem-65 19 23 ) ) PUNCT eurjchem-65 20 1 , , PUNCT eurjchem-65 20 2     SPACE eurjchem-65 20 3 2.30 2.30 NUM eurjchem-65 20 4     SPACE eurjchem-65 20 5 ( ( PUNCT eurjchem-65 20 6 br br PROPN eurjchem-65 20 7 , , PUNCT eurjchem-65 20 8     SPACE eurjchem-65 20 9 2h 2h NUM eurjchem-65 20 10 , , PUNCT eurjchem-65 20 11     SPACE eurjchem-65 20 12 haliph haliph NOUN eurjchem-65 20 13 .. .. PUNCT eurjchem-65 20 14 ) ) PUNCT eurjchem-65 20 15 , , PUNCT eurjchem-65 20 16     SPACE eurjchem-65 20 17 4.81 4.81 NUM eurjchem-65 20 18     SPACE eurjchem-65 20 19 ( ( PUNCT eurjchem-65 20 20 br br PROPN eurjchem-65 20 21 , , PUNCT eurjchem-65 20 22     SPACE eurjchem-65 20 23 1h 1h NUM eurjchem-65 20 24 , , PUNCT eurjchem-65 20 25     SPACE eurjchem-65 20 26 ch‐n ch‐n PROPN eurjchem-65 20 27 ) ) PUNCT eurjchem-65 20 28 , , PUNCT eurjchem-65 20 29     SPACE eurjchem-65 20 30 7.61 7.61 NUM eurjchem-65 20 31     SPACE eurjchem-65 20 32 ( ( PUNCT eurjchem-65 20 33 s s PROPN eurjchem-65 20 34 , , PUNCT eurjchem-65 20 35     SPACE eurjchem-65 20 36 1h 1h NUM eurjchem-65 20 37 , , PUNCT eurjchem-65 20 38     SPACE eurjchem-65 20 39 ar‐h ar‐h NOUN eurjchem-65 20 40 ) ) PUNCT eurjchem-65 20 41 , , PUNCT eurjchem-65 20 42     SPACE eurjchem-65 20 43 7.84 7.84 NUM eurjchem-65 20 44     SPACE eurjchem-65 20 45 ( ( PUNCT eurjchem-65 20 46 d d PROPN eurjchem-65 20 47 , , PUNCT eurjchem-65 20 48     SPACE eurjchem-65 20 49 j j NOUN eurjchem-65 20 50     SPACE eurjchem-65 20 51 = = NOUN eurjchem-65 20 52     SPACE eurjchem-65 20 53 6.4 6.4 NUM eurjchem-65 20 54     SPACE eurjchem-65 20 55 hz hz VERB eurjchem-65 20 56 , , PUNCT eurjchem-65 20 57     SPACE eurjchem-65 20 58 1h 1h NUM eurjchem-65 20 59 , , PUNCT eurjchem-65 20 60     SPACE eurjchem-65 20 61 ar‐h ar‐h NOUN eurjchem-65 20 62 ) ) PUNCT eurjchem-65 20 63 , , PUNCT eurjchem-65 20 64     SPACE eurjchem-65 20 65 8.01 8.01 NUM eurjchem-65 20 66     SPACE eurjchem-65 20 67 ( ( PUNCT eurjchem-65 20 68 s s PROPN eurjchem-65 20 69 , , PUNCT eurjchem-65 20 70     SPACE eurjchem-65 20 71 1h 1h NUM eurjchem-65 20 72 , , PUNCT eurjchem-65 20 73     SPACE eurjchem-65 20 74 ar‐h ar‐h NOUN eurjchem-65 20 75 ) ) PUNCT eurjchem-65 20 76 , , PUNCT eurjchem-65 20 77     SPACE eurjchem-65 20 78 8.77 8.77 NUM eurjchem-65 20 79     SPACE eurjchem-65 20 80 ( ( PUNCT eurjchem-65 20 81 s s PROPN eurjchem-65 20 82 , , PUNCT eurjchem-65 20 83     SPACE eurjchem-65 20 84 1h 1h NUM eurjchem-65 20 85 , , PUNCT eurjchem-65 20 86     SPACE eurjchem-65 20 87 ar‐h ar‐h NOUN eurjchem-65 20 88 ) ) PUNCT eurjchem-65 20 89 , , PUNCT eurjchem-65 20 90     SPACE eurjchem-65 20 91 14.05 14.05 NUM eurjchem-65 20 92     SPACE eurjchem-65 20 93 ( ( PUNCT eurjchem-65 20 94 s s PROPN eurjchem-65 20 95 , , PUNCT eurjchem-65 20 96     SPACE eurjchem-65 20 97 1h 1h NUM eurjchem-65 20 98 , , PUNCT eurjchem-65 20 99     SPACE eurjchem-65 20 100 sh sh PROPN eurjchem-65 20 101 ) ) PUNCT eurjchem-65 20 102 . . PUNCT eurjchem-65 20 103     SPACE eurjchem-65 21 1 ms ms PROPN eurjchem-65 21 2     SPACE eurjchem-65 21 3 ( ( PUNCT eurjchem-65 21 4 ei ei PROPN eurjchem-65 21 5 , , PUNCT eurjchem-65 21 6     SPACE eurjchem-65 21 7 m m NOUN eurjchem-65 21 8 / / SYM eurjchem-65 21 9 z(% z(% NOUN eurjchem-65 21 10 ) ) PUNCT eurjchem-65 21 11 ): ): PUNCT eurjchem-65 21 12     SPACE eurjchem-65 21 13 260 260 NUM eurjchem-65 21 14     SPACE eurjchem-65 21 15 ( ( PUNCT eurjchem-65 21 16 m+ m+ NOUN eurjchem-65 21 17 ) ) PUNCT eurjchem-65 21 18 , , PUNCT eurjchem-65 21 19     SPACE eurjchem-65 21 20 179 179 NUM eurjchem-65 21 21 , , PUNCT eurjchem-65 21 22     SPACE eurjchem-65 21 23 119 119 NUM eurjchem-65 21 24 , , PUNCT eurjchem-65 21 25     SPACE eurjchem-65 21 26 105 105 NUM eurjchem-65 21 27     SPACE eurjchem-65 21 28 ( ( PUNCT eurjchem-65 21 29 base base NOUN eurjchem-65 21 30     SPACE eurjchem-65 21 31 peak peak NOUN eurjchem-65 21 32 ) ) PUNCT eurjchem-65 21 33 , , PUNCT eurjchem-65 21 34     SPACE eurjchem-65 21 35 77 77 NUM eurjchem-65 21 36 . . PUNCT eurjchem-65 21 37     SPACE eurjchem-65 22 1 4­cyclohexyl­5­(pyridin­3­yl)­4h­1,2,4­triazole­3­thiol 4­cyclohexyl­5­(pyridin­3­yl)­4h­1,2,4­triazole­3­thiol NUM eurjchem-65 22 2     SPACE eurjchem-65 22 3 ( ( PUNCT eurjchem-65 22 4 4b 4b X eurjchem-65 22 5 ): ): PUNCT eurjchem-65 22 6     SPACE eurjchem-65 22 7 yield yield NOUN eurjchem-65 22 8 : : PUNCT eurjchem-65 22 9     SPACE eurjchem-65 22 10 85 85 NUM eurjchem-65 22 11 % % NOUN eurjchem-65 22 12 . . PUNCT eurjchem-65 22 13     SPACE eurjchem-65 23 1 m.p m.p PROPN eurjchem-65 23 2 . . PROPN eurjchem-65 23 3 : : PUNCT eurjchem-65 23 4     SPACE eurjchem-65 23 5 230‐232 230‐232 NUM eurjchem-65 23 6     SPACE eurjchem-65 23 7 oc oc PROPN eurjchem-65 23 8 . . PUNCT eurjchem-65 23 9     SPACE eurjchem-65 23 10 ir ir VERB eurjchem-65 23 11     SPACE eurjchem-65 23 12 ( ( PUNCT eurjchem-65 23 13 kbr kbr PROPN eurjchem-65 23 14 , , PUNCT eurjchem-65 23 15     SPACE eurjchem-65 23 16 cm‐1 cm‐1 PROPN eurjchem-65 23 17 ): ): PUNCT eurjchem-65 23 18     SPACE eurjchem-65 23 19 3055 3055 NUM eurjchem-65 23 20     SPACE eurjchem-65 23 21 (arom (arom PROPN eurjchem-65 23 22 . . PROPN eurjchem-65 23 23     SPACE eurjchem-65 23 24 ch ch NOUN eurjchem-65 23 25 ) ) PUNCT eurjchem-65 23 26 , , PUNCT eurjchem-65 23 27     SPACE eurjchem-65 23 28 2931 2931 NUM eurjchem-65 23 29 , , PUNCT eurjchem-65 23 30     SPACE eurjchem-65 23 31 2854 2854 NUM eurjchem-65 23 32     SPACE eurjchem-65 23 33 (aliph (aliph PROPN eurjchem-65 23 34 . . PUNCT eurjchem-65 23 35     SPACE eurjchem-65 23 36 ch ch NOUN eurjchem-65 23 37 ) ) PUNCT eurjchem-65 23 38 , , PUNCT eurjchem-65 23 39     SPACE eurjchem-65 23 40 2742 2742 NUM eurjchem-65 23 41     SPACE eurjchem-65 23 42 (sh (sh PROPN eurjchem-65 23 43 ) ) PUNCT eurjchem-65 23 44 , , PUNCT eurjchem-65 23 45     SPACE eurjchem-65 23 46 1523 1523 NUM eurjchem-65 23 47     SPACE eurjchem-65 23 48 (c (c PROPN eurjchem-65 23 49 = = SYM eurjchem-65 23 50 n n CCONJ eurjchem-65 23 51     SPACE eurjchem-65 23 52 and and CCONJ eurjchem-65 23 53     SPACE eurjchem-65 23 54 c c NOUN eurjchem-65 23 55 = = NOUN eurjchem-65 23 56 c c NOUN eurjchem-65 23 57 ) ) PUNCT eurjchem-65 23 58 . . PUNCT eurjchem-65 23 59     SPACE eurjchem-65 24 1 1h 1h NUM eurjchem-65 24 2     SPACE eurjchem-65 24 3 nmr nmr NOUN eurjchem-65 24 4     SPACE eurjchem-65 24 5 ( ( PUNCT eurjchem-65 24 6 dmso‐d6 dmso‐d6 PROPN eurjchem-65 24 7 , , PUNCT eurjchem-65 24 8     SPACE eurjchem-65 24 9 δ δ PROPN eurjchem-65 24 10 , , PUNCT eurjchem-65 24 11     SPACE eurjchem-65 24 12 ppm ppm NOUN eurjchem-65 24 13 ): ): PUNCT eurjchem-65 24 14     SPACE eurjchem-65 24 15 0.91 0.91 NUM eurjchem-65 24 16     SPACE eurjchem-65 24 17 ( ( PUNCT eurjchem-65 24 18 d d PROPN eurjchem-65 24 19 , , PUNCT eurjchem-65 24 20     SPACE eurjchem-65 24 21 j j PROPN eurjchem-65 24 22     SPACE eurjchem-65 24 23 = = NOUN eurjchem-65 24 24     SPACE eurjchem-65 24 25 7.7 7.7 NUM eurjchem-65 24 26     SPACE eurjchem-65 24 27 hz hz VERB eurjchem-65 24 28 , , PUNCT eurjchem-65 24 29     SPACE eurjchem-65 24 30 1h 1h NUM eurjchem-65 24 31 , , PUNCT eurjchem-65 24 32     SPACE eurjchem-65 24 33 haliph haliph NOUN eurjchem-65 24 34 . . PUNCT eurjchem-65 24 35 ) ) PUNCT eurjchem-65 25 1 , , PUNCT eurjchem-65 25 2     SPACE eurjchem-65 25 3 1.19 1.19 NUM eurjchem-65 25 4     SPACE eurjchem-65 25 5 ( ( PUNCT eurjchem-65 25 6 q q NOUN eurjchem-65 25 7 , , PUNCT eurjchem-65 25 8     SPACE eurjchem-65 25 9 j j PROPN eurjchem-65 25 10     SPACE eurjchem-65 25 11 = = NOUN eurjchem-65 25 12     SPACE eurjchem-65 25 13 12.9 12.9 NUM eurjchem-65 25 14     SPACE eurjchem-65 25 15 hz hz VERB eurjchem-65 25 16 , , PUNCT eurjchem-65 25 17     SPACE eurjchem-65 25 18 2h 2h NUM eurjchem-65 25 19 , , PUNCT eurjchem-65 25 20     SPACE eurjchem-65 25 21 haliph haliph NOUN eurjchem-65 25 22 . . PUNCT eurjchem-65 25 23 ) ) PUNCT eurjchem-65 26 1 , , PUNCT eurjchem-65 26 2     SPACE eurjchem-65 26 3 1.53 1.53 NUM eurjchem-65 26 4     SPACE eurjchem-65 26 5 ( ( PUNCT eurjchem-65 26 6 d d PROPN eurjchem-65 26 7 , , PUNCT eurjchem-65 26 8     SPACE eurjchem-65 26 9 j j PROPN eurjchem-65 26 10     SPACE eurjchem-65 26 11 = = NOUN eurjchem-65 26 12     SPACE eurjchem-65 26 13 12.6 12.6 NUM eurjchem-65 26 14     SPACE eurjchem-65 26 15 hz hz VERB eurjchem-65 26 16 , , PUNCT eurjchem-65 26 17     SPACE eurjchem-65 26 18 1h 1h NUM eurjchem-65 26 19 , , PUNCT eurjchem-65 26 20     SPACE eurjchem-65 26 21 haliph haliph NOUN eurjchem-65 26 22 . . PUNCT eurjchem-65 26 23 ) ) PUNCT eurjchem-65 27 1 , , PUNCT eurjchem-65 27 2     SPACE eurjchem-65 27 3 1.70 1.70 NUM eurjchem-65 27 4     SPACE eurjchem-65 27 5 ( ( PUNCT eurjchem-65 27 6 d d PROPN eurjchem-65 27 7 , , PUNCT eurjchem-65 27 8     SPACE eurjchem-65 27 9 j j NOUN eurjchem-65 27 10     SPACE eurjchem-65 27 11 = = NOUN eurjchem-65 27 12     SPACE eurjchem-65 27 13 12.8 12.8 NUM eurjchem-65 27 14     SPACE eurjchem-65 27 15 hz hz VERB eurjchem-65 27 16 , , PUNCT eurjchem-65 27 17     SPACE eurjchem-65 27 18 2h 2h NUM eurjchem-65 27 19 , , PUNCT eurjchem-65 27 20     SPACE eurjchem-65 27 21 haliph haliph NOUN eurjchem-65 27 22 . . PUNCT eurjchem-65 27 23 ) ) PUNCT eurjchem-65 27 24 , , PUNCT eurjchem-65 27 25     SPACE eurjchem-65 27 26 1.77 1.77 NUM eurjchem-65 27 27     SPACE eurjchem-65 27 28 ( ( PUNCT eurjchem-65 27 29 d d PROPN eurjchem-65 27 30 , , PUNCT eurjchem-65 27 31     SPACE eurjchem-65 27 32 j j NOUN eurjchem-65 27 33     SPACE eurjchem-65 27 34 = = VERB eurjchem-65 27 35     SPACE eurjchem-65 27 36 11.0 11.0 NUM eurjchem-65 27 37     SPACE eurjchem-65 27 38 hz hz VERB eurjchem-65 27 39 , , PUNCT eurjchem-65 27 40     SPACE eurjchem-65 27 41 2h 2h NUM eurjchem-65 27 42 , , PUNCT eurjchem-65 27 43     SPACE eurjchem-65 27 44 haliph haliph NOUN eurjchem-65 27 45 . . PUNCT eurjchem-65 27 46 ) ) PUNCT eurjchem-65 28 1 , , PUNCT eurjchem-65 28 2     SPACE eurjchem-65 28 3 2.00 2.00 NUM eurjchem-65 28 4     SPACE eurjchem-65 28 5 ( ( PUNCT eurjchem-65 28 6 br br PROPN eurjchem-65 28 7 , , PUNCT eurjchem-65 28 8     SPACE eurjchem-65 28 9 2h 2h NUM eurjchem-65 28 10 , , PUNCT eurjchem-65 28 11     SPACE eurjchem-65 28 12 haliph haliph NOUN eurjchem-65 28 13 . . PUNCT eurjchem-65 28 14 ) ) PUNCT eurjchem-65 28 15 , , PUNCT eurjchem-65 28 16     SPACE eurjchem-65 28 17 4.26 4.26 NUM eurjchem-65 28 18     SPACE eurjchem-65 28 19 ( ( PUNCT eurjchem-65 28 20 br br PROPN eurjchem-65 28 21 , , PUNCT eurjchem-65 28 22     SPACE eurjchem-65 28 23 1h 1h NUM eurjchem-65 28 24 , , PUNCT eurjchem-65 28 25     SPACE eurjchem-65 28 26 ch‐n ch‐n PROPN eurjchem-65 28 27 ) ) PUNCT eurjchem-65 28 28 , , PUNCT eurjchem-65 28 29     SPACE eurjchem-65 28 30 7.61 7.61 NUM eurjchem-65 28 31     SPACE eurjchem-65 28 32 ( ( PUNCT eurjchem-65 28 33 d d PROPN eurjchem-65 28 34 , , PUNCT eurjchem-65 28 35     SPACE eurjchem-65 28 36 d d PROPN eurjchem-65 28 37 , , PUNCT eurjchem-65 28 38     SPACE eurjchem-65 28 39 j j PROPN eurjchem-65 28 40     SPACE eurjchem-65 28 41 = = NOUN eurjchem-65 28 42     SPACE eurjchem-65 28 43 7.2 7.2 NUM eurjchem-65 28 44 , , PUNCT eurjchem-65 28 45     SPACE eurjchem-65 28 46 5.3 5.3 NUM eurjchem-65 28 47     SPACE eurjchem-65 28 48 hz hz VERB eurjchem-65 28 49 , , PUNCT eurjchem-65 28 50     SPACE eurjchem-65 28 51 1h 1h NUM eurjchem-65 28 52 , , PUNCT eurjchem-65 28 53     SPACE eurjchem-65 28 54 ar‐h ar‐h NOUN eurjchem-65 28 55 ) ) PUNCT eurjchem-65 28 56 , , PUNCT eurjchem-65 28 57     SPACE eurjchem-65 28 58 8.05 8.05 NUM eurjchem-65 28 59     SPACE eurjchem-65 28 60 ( ( PUNCT eurjchem-65 28 61 d d PROPN eurjchem-65 28 62 , , PUNCT eurjchem-65 28 63     SPACE eurjchem-65 28 64 j j PROPN eurjchem-65 28 65     SPACE eurjchem-65 29 1 = = NOUN eurjchem-65 29 2     SPACE eurjchem-65 29 3 7.6 7.6 NUM eurjchem-65 29 4     SPACE eurjchem-65 29 5 hz hz VERB eurjchem-65 29 6 , , PUNCT eurjchem-65 29 7     SPACE eurjchem-65 29 8 1h 1h NUM eurjchem-65 29 9 , , PUNCT eurjchem-65 29 10     SPACE eurjchem-65 29 11 ar‐h ar‐h NOUN eurjchem-65 29 12 ) ) PUNCT eurjchem-65 29 13 , , PUNCT eurjchem-65 29 14     SPACE eurjchem-65 29 15 8.77 8.77 NUM eurjchem-65 29 16     SPACE eurjchem-65 29 17 ( ( PUNCT eurjchem-65 29 18 s s PROPN eurjchem-65 29 19 , , PUNCT eurjchem-65 29 20     SPACE eurjchem-65 29 21 1h 1h NUM eurjchem-65 29 22 , , PUNCT eurjchem-65 29 23     SPACE eurjchem-65 29 24 ar‐h ar‐h NOUN eurjchem-65 29 25 . . PUNCT eurjchem-65 29 26 ) ) PUNCT eurjchem-65 30 1 , , PUNCT eurjchem-65 30 2     SPACE eurjchem-65 30 3 8.80 8.80 NUM eurjchem-65 30 4     SPACE eurjchem-65 30 5 ( ( PUNCT eurjchem-65 30 6 d d PROPN eurjchem-65 30 7 , , PUNCT eurjchem-65 30 8     SPACE eurjchem-65 30 9 j j PROPN eurjchem-65 30 10     SPACE eurjchem-65 30 11 = = NOUN eurjchem-65 30 12     SPACE eurjchem-65 30 13 4.5 4.5 NUM eurjchem-65 30 14     SPACE eurjchem-65 30 15 hz hz VERB eurjchem-65 30 16 , , PUNCT eurjchem-65 30 17     SPACE eurjchem-65 30 18 1h 1h NUM eurjchem-65 30 19 , , PUNCT eurjchem-65 30 20     SPACE eurjchem-65 30 21 ar‐h ar‐h NOUN eurjchem-65 30 22 ) ) PUNCT eurjchem-65 30 23 , , PUNCT eurjchem-65 30 24     SPACE eurjchem-65 30 25 14.04 14.04 NUM eurjchem-65 30 26     SPACE eurjchem-65 30 27 ( ( PUNCT eurjchem-65 30 28 s s PROPN eurjchem-65 30 29 , , PUNCT eurjchem-65 30 30     SPACE eurjchem-65 30 31 1h 1h NUM eurjchem-65 30 32 , , PUNCT eurjchem-65 30 33     SPACE eurjchem-65 30 34 sh sh PROPN eurjchem-65 30 35 ) ) PUNCT eurjchem-65 30 36 . . PUNCT eurjchem-65 30 37     SPACE eurjchem-65 31 1 ms ms PROPN eurjchem-65 31 2     SPACE eurjchem-65 31 3 ( ( PUNCT eurjchem-65 31 4 ei ei PROPN eurjchem-65 31 5 , , PUNCT eurjchem-65 31 6     SPACE eurjchem-65 31 7 m m NOUN eurjchem-65 31 8 / / SYM eurjchem-65 31 9 z(% z(% NOUN eurjchem-65 31 10 ) ) PUNCT eurjchem-65 31 11 ): ): PUNCT eurjchem-65 31 12     SPACE eurjchem-65 31 13 260 260 NUM eurjchem-65 31 14     SPACE eurjchem-65 31 15 ( ( PUNCT eurjchem-65 31 16 m+ m+ NOUN eurjchem-65 31 17 ) ) PUNCT eurjchem-65 31 18 , , PUNCT eurjchem-65 31 19     SPACE eurjchem-65 31 20 179 179 NUM eurjchem-65 31 21     SPACE eurjchem-65 31 22 ( ( PUNCT eurjchem-65 31 23 base base NOUN eurjchem-65 31 24     SPACE eurjchem-65 31 25 peak peak NOUN eurjchem-65 31 26 ) ) PUNCT eurjchem-65 31 27 , , PUNCT eurjchem-65 31 28     SPACE eurjchem-65 31 29 105 105 NUM eurjchem-65 31 30 , , PUNCT eurjchem-65 31 31     SPACE eurjchem-65 31 32 77 77 NUM eurjchem-65 31 33 . . PUNCT eurjchem-65 31 34     SPACE eurjchem-65 32 1 4­cyclohexyl­5­(pyridin­4­yl)­4h­1,2,4­triazole­3­thiol 4­cyclohexyl­5­(pyridin­4­yl)­4h­1,2,4­triazole­3­thiol NUM eurjchem-65 32 2     SPACE eurjchem-65 32 3 ( ( PUNCT eurjchem-65 32 4 4c 4c NOUN eurjchem-65 32 5 ): ): PUNCT eurjchem-65 32 6       SPACE eurjchem-65 32 7 yield yield NOUN eurjchem-65 32 8 : : PUNCT eurjchem-65 32 9       SPACE eurjchem-65 32 10 86 86 NUM eurjchem-65 32 11 % % NOUN eurjchem-65 32 12 . . PUNCT eurjchem-65 32 13     SPACE eurjchem-65 33 1 m.p m.p PROPN eurjchem-65 33 2 . . PROPN eurjchem-65 33 3 : : PUNCT eurjchem-65 33 4     SPACE eurjchem-65 33 5 314‐316 314‐316 NUM eurjchem-65 33 6     SPACE eurjchem-65 33 7 oc oc PROPN eurjchem-65 33 8 . . PUNCT eurjchem-65 33 9     SPACE eurjchem-65 33 10 ir ir VERB eurjchem-65 33 11     SPACE eurjchem-65 33 12 ( ( PUNCT eurjchem-65 33 13 kbr kbr PROPN eurjchem-65 33 14 , , PUNCT eurjchem-65 33 15     SPACE eurjchem-65 33 16 cm‐1 cm‐1 NOUN eurjchem-65 33 17 ): ): PUNCT eurjchem-65 33 18     SPACE eurjchem-65 33 19 3098 3098 NUM eurjchem-65 33 20     SPACE eurjchem-65 33 21 (arom (arom PROPN eurjchem-65 33 22 . . PROPN eurjchem-65 33 23     SPACE eurjchem-65 33 24 ch ch NOUN eurjchem-65 33 25 ) ) PUNCT eurjchem-65 33 26 , , PUNCT eurjchem-65 33 27     SPACE eurjchem-65 33 28 2941 2941 NUM eurjchem-65 33 29 , , PUNCT eurjchem-65 33 30     SPACE eurjchem-65 33 31 2854 2854 NUM eurjchem-65 33 32     SPACE eurjchem-65 33 33 (aliph (aliph PROPN eurjchem-65 33 34 . . PUNCT eurjchem-65 33 35     SPACE eurjchem-65 33 36 c‐h c‐h PROPN eurjchem-65 33 37 ) ) PUNCT eurjchem-65 33 38 , , PUNCT eurjchem-65 33 39     SPACE eurjchem-65 33 40 2729 2729 NUM eurjchem-65 33 41     SPACE eurjchem-65 33 42 (sh (sh PROPN eurjchem-65 33 43 ) ) PUNCT eurjchem-65 33 44 , , PUNCT eurjchem-65 33 45     SPACE eurjchem-65 33 46 1558 1558 NUM eurjchem-65 33 47     SPACE eurjchem-65 33 48 (c (c PROPN eurjchem-65 33 49 = = SYM eurjchem-65 33 50 n n CCONJ eurjchem-65 33 51     SPACE eurjchem-65 33 52 and and CCONJ eurjchem-65 33 53     SPACE eurjchem-65 33 54 c c NOUN eurjchem-65 33 55 = = NOUN eurjchem-65 33 56 c c NOUN eurjchem-65 33 57 ) ) PUNCT eurjchem-65 33 58 . . PUNCT eurjchem-65 33 59     SPACE eurjchem-65 34 1 1h 1h NUM eurjchem-65 34 2     SPACE eurjchem-65 34 3 nmr nmr NOUN eurjchem-65 34 4     SPACE eurjchem-65 34 5 ( ( PUNCT eurjchem-65 34 6 dmso‐d6 dmso‐d6 PROPN eurjchem-65 34 7 , , PUNCT eurjchem-65 34 8     SPACE eurjchem-65 34 9 δ δ PROPN eurjchem-65 34 10 , , PUNCT eurjchem-65 34 11     SPACE eurjchem-65 34 12 ppm ppm NOUN eurjchem-65 34 13 ): ): PUNCT eurjchem-65 34 14     SPACE eurjchem-65 34 15 0.96 0.96 NUM eurjchem-65 34 16     SPACE eurjchem-65 34 17 ( ( PUNCT eurjchem-65 34 18 d d PROPN eurjchem-65 34 19 , , PUNCT eurjchem-65 34 20     SPACE eurjchem-65 34 21 j=12.9 j=12.9 PROPN eurjchem-65 34 22     SPACE eurjchem-65 34 23 hz hz VERB eurjchem-65 34 24 , , PUNCT eurjchem-65 34 25     SPACE eurjchem-65 34 26 1h 1h NUM eurjchem-65 34 27 , , PUNCT eurjchem-65 34 28     SPACE eurjchem-65 34 29 haliph haliph NOUN eurjchem-65 34 30 . . PUNCT eurjchem-65 34 31 ) ) PUNCT eurjchem-65 35 1 , , PUNCT eurjchem-65 35 2     SPACE eurjchem-65 35 3 1.19 1.19 NUM eurjchem-65 35 4     SPACE eurjchem-65 35 5 ( ( PUNCT eurjchem-65 35 6 q q NOUN eurjchem-65 35 7 , , PUNCT eurjchem-65 35 8     SPACE eurjchem-65 35 9 j j PROPN eurjchem-65 35 10     SPACE eurjchem-65 35 11 = = VERB eurjchem-65 35 12     SPACE eurjchem-65 35 13 12.0 12.0 NUM eurjchem-65 35 14     SPACE eurjchem-65 35 15 hz hz VERB eurjchem-65 35 16 , , PUNCT eurjchem-65 35 17     SPACE eurjchem-65 35 18 2h 2h NUM eurjchem-65 35 19 , , PUNCT eurjchem-65 35 20     SPACE eurjchem-65 35 21 haliph haliph NOUN eurjchem-65 35 22 . . PUNCT eurjchem-65 35 23 ) ) PUNCT eurjchem-65 36 1 , , PUNCT eurjchem-65 36 2     SPACE eurjchem-65 36 3 1.54 1.54 NUM eurjchem-65 36 4     SPACE eurjchem-65 36 5 ( ( PUNCT eurjchem-65 36 6 d d PROPN eurjchem-65 36 7 , , PUNCT eurjchem-65 36 8     SPACE eurjchem-65 36 9 j j PROPN eurjchem-65 36 10     SPACE eurjchem-65 36 11 = = NOUN eurjchem-65 36 12     SPACE eurjchem-65 36 13 12.5 12.5 NUM eurjchem-65 36 14     SPACE eurjchem-65 36 15 hz hz VERB eurjchem-65 36 16 , , PUNCT eurjchem-65 36 17     SPACE eurjchem-65 36 18 1h 1h NUM eurjchem-65 36 19 , , PUNCT eurjchem-65 36 20     SPACE eurjchem-65 36 21 haliph haliph NOUN eurjchem-65 36 22 . . PUNCT eurjchem-65 36 23 ) ) PUNCT eurjchem-65 36 24 , , PUNCT eurjchem-65 36 25     SPACE eurjchem-65 36 26 1.72 1.72 NUM eurjchem-65 36 27     SPACE eurjchem-65 36 28 ( ( PUNCT eurjchem-65 36 29 d d PROPN eurjchem-65 36 30 , , PUNCT eurjchem-65 36 31     SPACE eurjchem-65 36 32 j j NOUN eurjchem-65 36 33     SPACE eurjchem-65 36 34 = = VERB eurjchem-65 36 35     SPACE eurjchem-65 36 36 12.9 12.9 NUM eurjchem-65 36 37     SPACE eurjchem-65 36 38 hz hz VERB eurjchem-65 36 39 , , PUNCT eurjchem-65 36 40     SPACE eurjchem-65 36 41 2h 2h NUM eurjchem-65 36 42 , , PUNCT eurjchem-65 36 43     SPACE eurjchem-65 36 44 haliph haliph NOUN eurjchem-65 36 45 . . PUNCT eurjchem-65 36 46 ) ) PUNCT eurjchem-65 37 1 , , PUNCT eurjchem-65 37 2     SPACE eurjchem-65 37 3 1.76 1.76 NUM eurjchem-65 37 4     SPACE eurjchem-65 37 5 ( ( PUNCT eurjchem-65 37 6 d d PROPN eurjchem-65 37 7 , , PUNCT eurjchem-65 37 8     SPACE eurjchem-65 37 9 j j PROPN eurjchem-65 37 10     SPACE eurjchem-65 37 11 = = VERB eurjchem-65 37 12     SPACE eurjchem-65 37 13 11.7 11.7 NUM eurjchem-65 37 14     SPACE eurjchem-65 37 15 hz hz VERB eurjchem-65 37 16 , , PUNCT eurjchem-65 37 17     SPACE eurjchem-65 37 18 2h 2h NUM eurjchem-65 37 19 , , PUNCT eurjchem-65 37 20     SPACE eurjchem-65 37 21 haliph haliph NOUN eurjchem-65 37 22 . . PUNCT eurjchem-65 37 23 ) ) PUNCT eurjchem-65 38 1 , , PUNCT eurjchem-65 38 2     SPACE eurjchem-65 38 3 2.13 2.13 NUM eurjchem-65 38 4     SPACE eurjchem-65 38 5 ( ( PUNCT eurjchem-65 38 6 br br PROPN eurjchem-65 38 7 , , PUNCT eurjchem-65 38 8     SPACE eurjchem-65 38 9 2h 2h NUM eurjchem-65 38 10 , , PUNCT eurjchem-65 38 11           SPACE eurjchem-65 38 12 ebrahimi ebrahimi NOUN eurjchem-65 38 13     SPACE eurjchem-65 38 14 / / SYM eurjchem-65 38 15     SPACE eurjchem-65 38 16 european european ADJ eurjchem-65 38 17     SPACE eurjchem-65 38 18 journal journal NOUN eurjchem-65 38 19     SPACE eurjchem-65 38 20 of of ADP eurjchem-65 38 21     SPACE eurjchem-65 38 22 chemistry chemistry NOUN eurjchem-65 38 23     SPACE eurjchem-65 38 24 1 1 NUM eurjchem-65 38 25     SPACE eurjchem-65 38 26 ( ( PUNCT eurjchem-65 38 27 4 4 NUM eurjchem-65 38 28 ) ) PUNCT eurjchem-65 38 29     SPACE eurjchem-65 38 30 ( ( PUNCT eurjchem-65 38 31 2010 2010 NUM eurjchem-65 38 32 ) ) PUNCT eurjchem-65 38 33     SPACE eurjchem-65 38 34 322­324 322­324 NUM eurjchem-65 38 35     SPACE eurjchem-65 38 36 323 323 NUM eurjchem-65 38 37             SPACE eurjchem-65 38 38 scheme scheme NOUN eurjchem-65 38 39     SPACE eurjchem-65 38 40 1 1 NUM eurjchem-65 38 41         SPACE eurjchem-65 38 42 haliph haliph NOUN eurjchem-65 38 43 . . PUNCT eurjchem-65 38 44 ) ) PUNCT eurjchem-65 38 45 , , PUNCT eurjchem-65 38 46     SPACE eurjchem-65 38 47 4.25 4.25 NUM eurjchem-65 38 48     SPACE eurjchem-65 38 49 ( ( PUNCT eurjchem-65 38 50 br br PROPN eurjchem-65 38 51 , , PUNCT eurjchem-65 38 52     SPACE eurjchem-65 38 53 1h 1h NUM eurjchem-65 38 54 , , PUNCT eurjchem-65 38 55     SPACE eurjchem-65 38 56 ch‐n ch‐n PROPN eurjchem-65 38 57 ) ) PUNCT eurjchem-65 38 58 , , PUNCT eurjchem-65 38 59     SPACE eurjchem-65 38 60 7.62 7.62 NUM eurjchem-65 38 61     SPACE eurjchem-65 38 62 ( ( PUNCT eurjchem-65 38 63 d d NOUN eurjchem-65 38 64 , , PUNCT eurjchem-65 38 65     SPACE eurjchem-65 38 66 2h 2h NUM eurjchem-65 38 67 , , PUNCT eurjchem-65 38 68     SPACE eurjchem-65 38 69 j j PROPN eurjchem-65 38 70     SPACE eurjchem-65 38 71 = = NOUN eurjchem-65 38 72     SPACE eurjchem-65 38 73 4.6 4.6 NUM eurjchem-65 38 74     SPACE eurjchem-65 38 75 hz hz VERB eurjchem-65 38 76 , , PUNCT eurjchem-65 38 77     SPACE eurjchem-65 38 78 ar‐h ar‐h NOUN eurjchem-65 38 79 ) ) PUNCT eurjchem-65 38 80 , , PUNCT eurjchem-65 38 81     SPACE eurjchem-65 38 82 8.80 8.80 NUM eurjchem-65 38 83     SPACE eurjchem-65 38 84 ( ( PUNCT eurjchem-65 38 85 d d PROPN eurjchem-65 38 86 , , PUNCT eurjchem-65 38 87     SPACE eurjchem-65 38 88 j j NOUN eurjchem-65 38 89     SPACE eurjchem-65 39 1 = = NOUN eurjchem-65 39 2     SPACE eurjchem-65 39 3 4.5 4.5 NUM eurjchem-65 39 4     SPACE eurjchem-65 39 5 hz hz VERB eurjchem-65 39 6 , , PUNCT eurjchem-65 39 7     SPACE eurjchem-65 39 8 2h 2h NUM eurjchem-65 39 9 , , PUNCT eurjchem-65 39 10     SPACE eurjchem-65 39 11 ar‐h ar‐h NOUN eurjchem-65 39 12 . . PUNCT eurjchem-65 39 13 ) ) PUNCT eurjchem-65 40 1 , , PUNCT eurjchem-65 40 2     SPACE eurjchem-65 40 3 14.08 14.08 NUM eurjchem-65 40 4     SPACE eurjchem-65 40 5 ( ( PUNCT eurjchem-65 40 6 s s PROPN eurjchem-65 40 7 , , PUNCT eurjchem-65 40 8     SPACE eurjchem-65 40 9 1h 1h NUM eurjchem-65 40 10 , , PUNCT eurjchem-65 40 11     SPACE eurjchem-65 40 12 sh sh PROPN eurjchem-65 40 13 ) ) PUNCT eurjchem-65 40 14 . . PUNCT eurjchem-65 40 15     SPACE eurjchem-65 41 1 ms ms PROPN eurjchem-65 41 2     SPACE eurjchem-65 41 3 ( ( PUNCT eurjchem-65 41 4 ei ei PROPN eurjchem-65 41 5 , , PUNCT eurjchem-65 41 6     SPACE eurjchem-65 41 7 m m NOUN eurjchem-65 41 8 / / SYM eurjchem-65 41 9 z(% z(% NOUN eurjchem-65 41 10 ) ) PUNCT eurjchem-65 41 11 ): ): PUNCT eurjchem-65 41 12     SPACE eurjchem-65 41 13 260 260 NUM eurjchem-65 41 14     SPACE eurjchem-65 41 15 ( ( PUNCT eurjchem-65 41 16 m+ m+ NOUN eurjchem-65 41 17 ) ) PUNCT eurjchem-65 41 18 , , PUNCT eurjchem-65 41 19     SPACE eurjchem-65 41 20 179 179 NUM eurjchem-65 41 21     SPACE eurjchem-65 41 22 ( ( PUNCT eurjchem-65 41 23 base base NOUN eurjchem-65 41 24     SPACE eurjchem-65 41 25 peak peak NOUN eurjchem-65 41 26 ) ) PUNCT eurjchem-65 41 27 , , PUNCT eurjchem-65 41 28     SPACE eurjchem-65 41 29 119 119 NUM eurjchem-65 41 30 , , PUNCT eurjchem-65 41 31     SPACE eurjchem-65 41 32 105 105 NUM eurjchem-65 41 33 , , PUNCT eurjchem-65 41 34     SPACE eurjchem-65 41 35 77 77 NUM eurjchem-65 41 36 . . PUNCT eurjchem-65 41 37         SPACE eurjchem-65 41 38 2.3 2.3 NUM eurjchem-65 41 39 . . PUNCT eurjchem-65 41 40     SPACE eurjchem-65 41 41 general general ADJ eurjchem-65 41 42     SPACE eurjchem-65 41 43 procedure procedure NOUN eurjchem-65 41 44     SPACE eurjchem-65 41 45 for for ADP eurjchem-65 41 46     SPACE eurjchem-65 41 47 the the DET eurjchem-65 41 48     SPACE eurjchem-65 41 49 synthesis synthesis NOUN eurjchem-65 41 50     SPACE eurjchem-65 41 51 of of ADP eurjchem-65 41 52     SPACE eurjchem-65 41 53 1,3,4­thiadizoles 1,3,4­thiadizoles NUM eurjchem-65 41 54     SPACE eurjchem-65 41 55 5a­c 5a­c NUM eurjchem-65 41 56         SPACE eurjchem-65 41 57 each each DET eurjchem-65 41 58     SPACE eurjchem-65 41 59 thiosemicarbazide thiosemicarbazide NOUN eurjchem-65 41 60     SPACE eurjchem-65 41 61 3a­c 3a­c NOUN eurjchem-65 41 62     SPACE eurjchem-65 41 63 ( ( PUNCT eurjchem-65 41 64 5 5 NUM eurjchem-65 41 65     SPACE eurjchem-65 41 66 mmol mmol NOUN eurjchem-65 41 67 , , PUNCT eurjchem-65 41 68 ) ) PUNCT eurjchem-65 41 69     SPACE eurjchem-65 41 70 was be AUX eurjchem-65 41 71     SPACE eurjchem-65 41 72 added add VERB eurjchem-65 41 73     SPACE eurjchem-65 41 74 portion portion NOUN eurjchem-65 41 75     SPACE eurjchem-65 41 76 wise wise ADJ eurjchem-65 41 77     SPACE eurjchem-65 41 78 to to ADP eurjchem-65 41 79     SPACE eurjchem-65 41 80 10 10 NUM eurjchem-65 41 81     SPACE eurjchem-65 41 82 ml ml NOUN eurjchem-65 41 83     SPACE eurjchem-65 41 84 of of ADP eurjchem-65 41 85     SPACE eurjchem-65 41 86 conc conc NOUN eurjchem-65 41 87 . . PUNCT eurjchem-65 41 88     SPACE eurjchem-65 41 89 sulfuric sulfuric ADJ eurjchem-65 41 90     SPACE eurjchem-65 41 91 acid acid NOUN eurjchem-65 41 92     SPACE eurjchem-65 41 93 with with ADP eurjchem-65 41 94     SPACE eurjchem-65 41 95 continuous continuous ADJ eurjchem-65 41 96     SPACE eurjchem-65 41 97 stirring stirring NOUN eurjchem-65 41 98 . . PUNCT eurjchem-65 41 99     SPACE eurjchem-65 42 1 the the DET eurjchem-65 42 2     SPACE eurjchem-65 42 3 reaction reaction NOUN eurjchem-65 42 4     SPACE eurjchem-65 42 5 mixture mixture NOUN eurjchem-65 42 6     SPACE eurjchem-65 42 7 was be AUX eurjchem-65 42 8     SPACE eurjchem-65 42 9 stirred stir VERB eurjchem-65 42 10     SPACE eurjchem-65 42 11 further far ADV eurjchem-65 42 12     SPACE eurjchem-65 42 13 for for ADP eurjchem-65 42 14     SPACE eurjchem-65 42 15 3 3 NUM eurjchem-65 42 16     SPACE eurjchem-65 42 17 h h NOUN eurjchem-65 42 18     SPACE eurjchem-65 42 19 at at ADP eurjchem-65 42 20     SPACE eurjchem-65 42 21 room room NOUN eurjchem-65 42 22     SPACE eurjchem-65 42 23 temperature temperature NOUN eurjchem-65 42 24 . . PUNCT eurjchem-65 42 25     SPACE eurjchem-65 43 1 the the DET eurjchem-65 43 2     SPACE eurjchem-65 43 3 reaction reaction NOUN eurjchem-65 43 4     SPACE eurjchem-65 43 5 mixture mixture NOUN eurjchem-65 43 6     SPACE eurjchem-65 43 7 was be AUX eurjchem-65 43 8     SPACE eurjchem-65 43 9 slowly slowly ADV eurjchem-65 43 10     SPACE eurjchem-65 43 11 poured pour VERB eurjchem-65 43 12     SPACE eurjchem-65 43 13 into into ADP eurjchem-65 43 14     SPACE eurjchem-65 43 15 crashed crash VERB eurjchem-65 43 16     SPACE eurjchem-65 43 17 ice ice NOUN eurjchem-65 43 18     SPACE eurjchem-65 43 19 with with ADP eurjchem-65 43 20     SPACE eurjchem-65 43 21 stirring stirring NOUN eurjchem-65 43 22     SPACE eurjchem-65 43 23 and and CCONJ eurjchem-65 43 24     SPACE eurjchem-65 43 25 neutralized neutralize VERB eurjchem-65 43 26     SPACE eurjchem-65 43 27 with with ADP eurjchem-65 43 28     SPACE eurjchem-65 43 29 ammonia ammonia NOUN eurjchem-65 43 30 . . PUNCT eurjchem-65 43 31     SPACE eurjchem-65 44 1 the the DET eurjchem-65 44 2     SPACE eurjchem-65 44 3 mixture mixture NOUN eurjchem-65 44 4     SPACE eurjchem-65 44 5 was be AUX eurjchem-65 44 6     SPACE eurjchem-65 44 7 allowed allow VERB eurjchem-65 44 8     SPACE eurjchem-65 44 9 to to PART eurjchem-65 44 10     SPACE eurjchem-65 44 11 stand stand VERB eurjchem-65 44 12     SPACE eurjchem-65 44 13 overnight overnight ADV eurjchem-65 44 14     SPACE eurjchem-65 44 15 and and CCONJ eurjchem-65 44 16     SPACE eurjchem-65 44 17 the the DET eurjchem-65 44 18     SPACE eurjchem-65 44 19 solid solid NOUN eurjchem-65 44 20     SPACE eurjchem-65 44 21 separated separate VERB eurjchem-65 44 22     SPACE eurjchem-65 44 23 out out ADP eurjchem-65 44 24     SPACE eurjchem-65 44 25 was be AUX eurjchem-65 44 26     SPACE eurjchem-65 44 27 filtered filter VERB eurjchem-65 44 28     SPACE eurjchem-65 44 29 and and CCONJ eurjchem-65 44 30     SPACE eurjchem-65 44 31 washed wash VERB eurjchem-65 44 32     SPACE eurjchem-65 44 33 with with ADP eurjchem-65 44 34     SPACE eurjchem-65 44 35 cold cold ADJ eurjchem-65 44 36     SPACE eurjchem-65 44 37 water water NOUN eurjchem-65 44 38 . . PUNCT eurjchem-65 44 39     SPACE eurjchem-65 45 1 the the DET eurjchem-65 45 2     SPACE eurjchem-65 45 3 solid solid NOUN eurjchem-65 45 4     SPACE eurjchem-65 45 5 was be AUX eurjchem-65 45 6     SPACE eurjchem-65 45 7 dried dry VERB eurjchem-65 45 8     SPACE eurjchem-65 45 9 and and CCONJ eurjchem-65 45 10     SPACE eurjchem-65 45 11 crystallized crystallize VERB eurjchem-65 45 12     SPACE eurjchem-65 45 13 from from ADP eurjchem-65 45 14     SPACE eurjchem-65 45 15 a a DET eurjchem-65 45 16     SPACE eurjchem-65 45 17 mixture mixture NOUN eurjchem-65 45 18     SPACE eurjchem-65 45 19 of of ADP eurjchem-65 45 20     SPACE eurjchem-65 45 21 acetic acetic ADJ eurjchem-65 45 22     SPACE eurjchem-65 45 23 acid acid NOUN eurjchem-65 45 24     SPACE eurjchem-65 45 25 and and CCONJ eurjchem-65 45 26     SPACE eurjchem-65 45 27 water water NOUN eurjchem-65 45 28     SPACE eurjchem-65 45 29 ( ( PUNCT eurjchem-65 45 30 1:2 1:2 NUM eurjchem-65 45 31 ) ) PUNCT eurjchem-65 45 32     SPACE eurjchem-65 45 33 to to PART eurjchem-65 45 34     SPACE eurjchem-65 45 35 furnish furnish VERB eurjchem-65 45 36     SPACE eurjchem-65 45 37 di‐substituted di‐substitute VERB eurjchem-65 45 38     SPACE eurjchem-65 45 39 1,3,4‐thiadiazole 1,3,4‐thiadiazole NUM eurjchem-65 45 40     SPACE eurjchem-65 45 41 5a­c 5a­c NUM eurjchem-65 45 42     SPACE eurjchem-65 45 43 ( ( PUNCT eurjchem-65 45 44 scheme scheme NOUN eurjchem-65 45 45     SPACE eurjchem-65 45 46 1 1 NUM eurjchem-65 45 47 ) ) PUNCT eurjchem-65 45 48 . . PUNCT eurjchem-65 45 49     SPACE eurjchem-65 46 1 n­cyclohexyl­5­(pyridin­2­yl)­1,3,4­thiadiazol­2­amine n­cyclohexyl­5­(pyridin­2­yl)­1,3,4­thiadiazol­2­amine NOUN eurjchem-65 46 2     SPACE eurjchem-65 46 3 ( ( PUNCT eurjchem-65 46 4 5a 5a NUM eurjchem-65 46 5 ): ): PUNCT eurjchem-65 46 6       SPACE eurjchem-65 46 7 yield yield NOUN eurjchem-65 46 8 : : PUNCT eurjchem-65 46 9     SPACE eurjchem-65 46 10 70 70 NUM eurjchem-65 46 11 % % NOUN eurjchem-65 46 12 . . PUNCT eurjchem-65 46 13     SPACE eurjchem-65 47 1 m.p m.p PROPN eurjchem-65 47 2 . . PROPN eurjchem-65 47 3 : : PUNCT eurjchem-65 47 4     SPACE eurjchem-65 47 5 168‐169 168‐169 NUM eurjchem-65 47 6     SPACE eurjchem-65 47 7 oc oc PROPN eurjchem-65 47 8 . . PUNCT eurjchem-65 47 9     SPACE eurjchem-65 47 10 ir ir VERB eurjchem-65 47 11     SPACE eurjchem-65 47 12 ( ( PUNCT eurjchem-65 47 13 kbr kbr PROPN eurjchem-65 47 14 , , PUNCT eurjchem-65 47 15     SPACE eurjchem-65 47 16 cm‐1 cm‐1 NOUN eurjchem-65 47 17 ): ): PUNCT eurjchem-65 47 18     SPACE eurjchem-65 47 19 3277 3277 NUM eurjchem-65 47 20     SPACE eurjchem-65 47 21 (nh (nh PROPN eurjchem-65 47 22 ) ) PUNCT eurjchem-65 47 23 , , PUNCT eurjchem-65 47 24     SPACE eurjchem-65 47 25 3013 3013 NUM eurjchem-65 47 26     SPACE eurjchem-65 47 27 (arom (arom PROPN eurjchem-65 47 28 . . PROPN eurjchem-65 47 29     SPACE eurjchem-65 47 30 ch ch NOUN eurjchem-65 47 31 ) ) PUNCT eurjchem-65 47 32 , , PUNCT eurjchem-65 47 33     SPACE eurjchem-65 47 34 2930 2930 NUM eurjchem-65 47 35 , , PUNCT eurjchem-65 47 36     SPACE eurjchem-65 47 37 2858 2858 NUM eurjchem-65 47 38     SPACE eurjchem-65 47 39 (aliph (aliph NOUN eurjchem-65 47 40 . . PUNCT eurjchem-65 47 41     SPACE eurjchem-65 47 42 c‐h c‐h PROPN eurjchem-65 47 43 ) ) PUNCT eurjchem-65 47 44 , , PUNCT eurjchem-65 47 45     SPACE eurjchem-65 47 46 1548 1548 NUM eurjchem-65 47 47     SPACE eurjchem-65 47 48 (c (c PROPN eurjchem-65 47 49 = = SYM eurjchem-65 47 50 n n CCONJ eurjchem-65 47 51     SPACE eurjchem-65 47 52 and and CCONJ eurjchem-65 47 53     SPACE eurjchem-65 47 54 c c NOUN eurjchem-65 47 55 = = NOUN eurjchem-65 47 56 c c NOUN eurjchem-65 47 57 ) ) PUNCT eurjchem-65 47 58 . . PUNCT eurjchem-65 47 59     SPACE eurjchem-65 47 60 1h 1h NUM eurjchem-65 47 61     SPACE eurjchem-65 47 62 nmr nmr NOUN eurjchem-65 47 63     SPACE eurjchem-65 47 64 ( ( PUNCT eurjchem-65 47 65 dmso‐d6 dmso‐d6 PROPN eurjchem-65 47 66 , , PUNCT eurjchem-65 47 67     SPACE eurjchem-65 47 68 δ δ PROPN eurjchem-65 47 69 , , PUNCT eurjchem-65 47 70     SPACE eurjchem-65 47 71 ppm ppm ADJ eurjchem-65 47 72 ): ): PUNCT eurjchem-65 47 73     SPACE eurjchem-65 47 74 1.17‐1.36 1.17‐1.36 NUM eurjchem-65 47 75     SPACE eurjchem-65 47 76 ( ( PUNCT eurjchem-65 47 77 m m PROPN eurjchem-65 47 78 , , PUNCT eurjchem-65 47 79     SPACE eurjchem-65 47 80 5h 5h NUM eurjchem-65 47 81 , , PUNCT eurjchem-65 47 82     SPACE eurjchem-65 47 83 haliph haliph NOUN eurjchem-65 47 84 . . PUNCT eurjchem-65 47 85 ) ) PUNCT eurjchem-65 47 86 , , PUNCT eurjchem-65 47 87     SPACE eurjchem-65 47 88 1.57 1.57 NUM eurjchem-65 47 89     SPACE eurjchem-65 47 90 ( ( PUNCT eurjchem-65 47 91 d d PROPN eurjchem-65 47 92 , , PUNCT eurjchem-65 47 93     SPACE eurjchem-65 47 94 1h 1h NUM eurjchem-65 47 95 , , PUNCT eurjchem-65 47 96     SPACE eurjchem-65 47 97 j j PROPN eurjchem-65 47 98     SPACE eurjchem-65 47 99 = = VERB eurjchem-65 47 100     SPACE eurjchem-65 47 101 12.2 12.2 NUM eurjchem-65 47 102     SPACE eurjchem-65 47 103 hz hz VERB eurjchem-65 47 104 , , PUNCT eurjchem-65 47 105     SPACE eurjchem-65 47 106 haliph haliph NOUN eurjchem-65 47 107 . . PUNCT eurjchem-65 47 108 ) ) PUNCT eurjchem-65 48 1 , , PUNCT eurjchem-65 48 2     SPACE eurjchem-65 48 3 1.71 1.71 NUM eurjchem-65 48 4     SPACE eurjchem-65 48 5 ( ( PUNCT eurjchem-65 48 6 d d NOUN eurjchem-65 48 7 , , PUNCT eurjchem-65 48 8     SPACE eurjchem-65 48 9 2h 2h NUM eurjchem-65 48 10 , , PUNCT eurjchem-65 48 11     SPACE eurjchem-65 48 12 j j PROPN eurjchem-65 48 13     SPACE eurjchem-65 48 14 = = NOUN eurjchem-65 48 15     SPACE eurjchem-65 48 16 10.1 10.1 NUM eurjchem-65 48 17     SPACE eurjchem-65 48 18 hz hz VERB eurjchem-65 48 19 , , PUNCT eurjchem-65 48 20     SPACE eurjchem-65 48 21 haliph haliph NOUN eurjchem-65 48 22 . . PUNCT eurjchem-65 48 23 ) ) PUNCT eurjchem-65 48 24 , , PUNCT eurjchem-65 48 25     SPACE eurjchem-65 48 26 2.00 2.00 NUM eurjchem-65 48 27     SPACE eurjchem-65 48 28 ( ( PUNCT eurjchem-65 48 29 d d NOUN eurjchem-65 48 30 , , PUNCT eurjchem-65 48 31     SPACE eurjchem-65 48 32 2h 2h NUM eurjchem-65 48 33 , , PUNCT eurjchem-65 48 34     SPACE eurjchem-65 48 35 j j PROPN eurjchem-65 48 36     SPACE eurjchem-65 48 37 = = NOUN eurjchem-65 48 38     SPACE eurjchem-65 48 39 10.8 10.8 NUM eurjchem-65 48 40     SPACE eurjchem-65 48 41 hz hz VERB eurjchem-65 48 42 , , PUNCT eurjchem-65 48 43       SPACE eurjchem-65 48 44 haliph haliph NOUN eurjchem-65 48 45 . . PUNCT eurjchem-65 48 46 ) ) PUNCT eurjchem-65 48 47 , , PUNCT eurjchem-65 48 48     SPACE eurjchem-65 48 49 3.57 3.57 NUM eurjchem-65 48 50     SPACE eurjchem-65 48 51 ( ( PUNCT eurjchem-65 48 52 br br PROPN eurjchem-65 48 53 , , PUNCT eurjchem-65 48 54     SPACE eurjchem-65 48 55 1h 1h NUM eurjchem-65 48 56 , , PUNCT eurjchem-65 48 57     SPACE eurjchem-65 48 58 ch‐n ch‐n PROPN eurjchem-65 48 59 ) ) PUNCT eurjchem-65 48 60 , , PUNCT eurjchem-65 48 61     SPACE eurjchem-65 48 62 7.41 7.41 NUM eurjchem-65 48 63     SPACE eurjchem-65 48 64 ( ( PUNCT eurjchem-65 48 65 t t PROPN eurjchem-65 48 66 , , PUNCT eurjchem-65 48 67     SPACE eurjchem-65 48 68 1h 1h NUM eurjchem-65 48 69 , , PUNCT eurjchem-65 48 70     SPACE eurjchem-65 48 71 j j PROPN eurjchem-65 48 72     SPACE eurjchem-65 48 73 = = NOUN eurjchem-65 48 74     SPACE eurjchem-65 48 75 5.6 5.6 NUM eurjchem-65 48 76     SPACE eurjchem-65 48 77 hz hz VERB eurjchem-65 48 78 , , PUNCT eurjchem-65 48 79     SPACE eurjchem-65 48 80 ar‐h ar‐h NOUN eurjchem-65 48 81 ) ) PUNCT eurjchem-65 48 82 , , PUNCT eurjchem-65 48 83       SPACE eurjchem-65 48 84 7.91 7.91 NUM eurjchem-65 48 85     SPACE eurjchem-65 48 86 ( ( PUNCT eurjchem-65 48 87 t t PROPN eurjchem-65 48 88 , , PUNCT eurjchem-65 48 89     SPACE eurjchem-65 48 90 1h 1h NUM eurjchem-65 48 91 , , PUNCT eurjchem-65 48 92     SPACE eurjchem-65 48 93 j j PROPN eurjchem-65 48 94     SPACE eurjchem-65 49 1 = = NOUN eurjchem-65 49 2     SPACE eurjchem-65 49 3 7.6 7.6 NUM eurjchem-65 49 4     SPACE eurjchem-65 49 5 hz hz VERB eurjchem-65 49 6 , , PUNCT eurjchem-65 49 7     SPACE eurjchem-65 49 8 ar‐h ar‐h NOUN eurjchem-65 49 9 ) ) PUNCT eurjchem-65 49 10 , , PUNCT eurjchem-65 49 11     SPACE eurjchem-65 49 12 8.03 8.03 NUM eurjchem-65 49 13     SPACE eurjchem-65 49 14 ( ( PUNCT eurjchem-65 49 15 d d PROPN eurjchem-65 49 16 , , PUNCT eurjchem-65 49 17     SPACE eurjchem-65 49 18 1h 1h NUM eurjchem-65 49 19 , , PUNCT eurjchem-65 49 20     SPACE eurjchem-65 49 21 j j PROPN eurjchem-65 49 22     SPACE eurjchem-65 49 23 = = NOUN eurjchem-65 49 24     SPACE eurjchem-65 49 25 5.2 5.2 NUM eurjchem-65 49 26     SPACE eurjchem-65 49 27 hz hz VERB eurjchem-65 49 28 , , PUNCT eurjchem-65 49 29     SPACE eurjchem-65 49 30 ar‐h ar‐h NOUN eurjchem-65 49 31 ) ) PUNCT eurjchem-65 49 32 , , PUNCT eurjchem-65 49 33     SPACE eurjchem-65 49 34 8.05 8.05 NUM eurjchem-65 49 35     SPACE eurjchem-65 49 36 ( ( PUNCT eurjchem-65 49 37 s s PROPN eurjchem-65 49 38 , , PUNCT eurjchem-65 49 39     SPACE eurjchem-65 49 40 1h 1h NUM eurjchem-65 49 41 , , PUNCT eurjchem-65 49 42     SPACE eurjchem-65 49 43 nh nh PROPN eurjchem-65 49 44 , , PUNCT eurjchem-65 49 45     SPACE eurjchem-65 49 46 d2o d2o NOUN eurjchem-65 49 47     SPACE eurjchem-65 49 48 exchange exchange NOUN eurjchem-65 49 49 ) ) PUNCT eurjchem-65 49 50 , , PUNCT eurjchem-65 49 51     SPACE eurjchem-65 49 52 8.57 8.57 NUM eurjchem-65 49 53     SPACE eurjchem-65 49 54 ( ( PUNCT eurjchem-65 49 55 d d PROPN eurjchem-65 49 56 , , PUNCT eurjchem-65 49 57     SPACE eurjchem-65 49 58 j j PROPN eurjchem-65 49 59     SPACE eurjchem-65 50 1 = = NOUN eurjchem-65 50 2     SPACE eurjchem-65 50 3 4.1 4.1 NUM eurjchem-65 50 4     SPACE eurjchem-65 50 5 hz hz VERB eurjchem-65 50 6 , , PUNCT eurjchem-65 50 7     SPACE eurjchem-65 50 8 1h 1h NUM eurjchem-65 50 9 , , PUNCT eurjchem-65 50 10     SPACE eurjchem-65 50 11 ar‐ ar‐ NOUN eurjchem-65 50 12 h h NOUN eurjchem-65 50 13 ) ) PUNCT eurjchem-65 50 14 . . PUNCT eurjchem-65 50 15     SPACE eurjchem-65 51 1 ms ms PROPN eurjchem-65 51 2     SPACE eurjchem-65 51 3 ( ( PUNCT eurjchem-65 51 4 ei ei PROPN eurjchem-65 51 5 , , PUNCT eurjchem-65 51 6     SPACE eurjchem-65 51 7 m m NOUN eurjchem-65 51 8 / / SYM eurjchem-65 51 9 z(% z(% NOUN eurjchem-65 51 10 ) ) PUNCT eurjchem-65 51 11 ): ): PUNCT eurjchem-65 51 12     SPACE eurjchem-65 51 13 260 260 NUM eurjchem-65 51 14     SPACE eurjchem-65 51 15 ( ( PUNCT eurjchem-65 51 16 m+ m+ NOUN eurjchem-65 51 17 ) ) PUNCT eurjchem-65 51 18 , , PUNCT eurjchem-65 51 19     SPACE eurjchem-65 51 20 178 178 NUM eurjchem-65 51 21     SPACE eurjchem-65 51 22 ( ( PUNCT eurjchem-65 51 23 base base NOUN eurjchem-65 51 24     SPACE eurjchem-65 51 25 peak peak NOUN eurjchem-65 51 26 ) ) PUNCT eurjchem-65 51 27 , , PUNCT eurjchem-65 51 28     SPACE eurjchem-65 51 29 119 119 NUM eurjchem-65 51 30 , , PUNCT eurjchem-65 51 31     SPACE eurjchem-65 51 32 105 105 NUM eurjchem-65 51 33 , , PUNCT eurjchem-65 51 34     SPACE eurjchem-65 51 35 78 78 NUM eurjchem-65 51 36 , , PUNCT eurjchem-65 51 37     SPACE eurjchem-65 51 38 55 55 NUM eurjchem-65 51 39 , , PUNCT eurjchem-65 51 40     SPACE eurjchem-65 51 41 41 41 NUM eurjchem-65 51 42 . . PUNCT eurjchem-65 51 43     SPACE eurjchem-65 51 44 n­cyclohexyl­5­(pyridin­3­yl)­1,3,4­thiadiazol­2­amine n­cyclohexyl­5­(pyridin­3­yl)­1,3,4­thiadiazol­2­amine NOUN eurjchem-65 51 45     SPACE eurjchem-65 51 46 ( ( PUNCT eurjchem-65 51 47 5b 5b NUM eurjchem-65 51 48 ): ): PUNCT eurjchem-65 51 49     SPACE eurjchem-65 51 50 yield yield NOUN eurjchem-65 51 51 : : PUNCT eurjchem-65 51 52     SPACE eurjchem-65 51 53 60 60 NUM eurjchem-65 51 54 % % NOUN eurjchem-65 51 55 . . PUNCT eurjchem-65 51 56     SPACE eurjchem-65 52 1 m.p m.p AUX eurjchem-65 52 2 . . PROPN eurjchem-65 52 3 : : PUNCT eurjchem-65 52 4     SPACE eurjchem-65 52 5 144‐145 144‐145 NUM eurjchem-65 52 6     SPACE eurjchem-65 52 7 oc oc PROPN eurjchem-65 52 8 . . PUNCT eurjchem-65 52 9     SPACE eurjchem-65 52 10 ir ir VERB eurjchem-65 52 11     SPACE eurjchem-65 52 12 ( ( PUNCT eurjchem-65 52 13 kbr kbr PROPN eurjchem-65 52 14 , , PUNCT eurjchem-65 52 15     SPACE eurjchem-65 52 16 cm‐1 cm‐1 NOUN eurjchem-65 52 17 ): ): PUNCT eurjchem-65 52 18     SPACE eurjchem-65 52 19 3205 3205 NUM eurjchem-65 52 20     SPACE eurjchem-65 52 21 (nh (nh PROPN eurjchem-65 52 22 ) ) PUNCT eurjchem-65 52 23 , , PUNCT eurjchem-65 52 24     SPACE eurjchem-65 52 25 3011 3011 NUM eurjchem-65 52 26     SPACE eurjchem-65 52 27 (arom (arom PROPN eurjchem-65 52 28 . . PROPN eurjchem-65 52 29     SPACE eurjchem-65 52 30 ch ch NOUN eurjchem-65 52 31 ) ) PUNCT eurjchem-65 52 32 , , PUNCT eurjchem-65 52 33     SPACE eurjchem-65 52 34 2937 2937 NUM eurjchem-65 52 35 , , PUNCT eurjchem-65 52 36     SPACE eurjchem-65 52 37 2852 2852 NUM eurjchem-65 52 38     SPACE eurjchem-65 52 39 (aliph (aliph NOUN eurjchem-65 52 40 . . PUNCT eurjchem-65 52 41     SPACE eurjchem-65 52 42 c‐h c‐h PROPN eurjchem-65 52 43 ) ) PUNCT eurjchem-65 52 44 , , PUNCT eurjchem-65 52 45     SPACE eurjchem-65 52 46 1550 1550 NUM eurjchem-65 52 47     SPACE eurjchem-65 52 48 (c (c PROPN eurjchem-65 52 49 = = SYM eurjchem-65 52 50 n n CCONJ eurjchem-65 52 51     SPACE eurjchem-65 52 52 and and CCONJ eurjchem-65 52 53     SPACE eurjchem-65 52 54 c c NOUN eurjchem-65 52 55 = = NOUN eurjchem-65 52 56 c c NOUN eurjchem-65 52 57 ) ) PUNCT eurjchem-65 52 58 . . PUNCT eurjchem-65 52 59     SPACE eurjchem-65 52 60 1h 1h NUM eurjchem-65 52 61     SPACE eurjchem-65 52 62 nmr nmr NOUN eurjchem-65 52 63     SPACE eurjchem-65 52 64 ( ( PUNCT eurjchem-65 52 65 dmso‐d6 dmso‐d6 PROPN eurjchem-65 52 66 , , PUNCT eurjchem-65 52 67     SPACE eurjchem-65 52 68 δ δ PROPN eurjchem-65 52 69 , , PUNCT eurjchem-65 52 70     SPACE eurjchem-65 52 71 ppm ppm ADJ eurjchem-65 52 72 ): ): PUNCT eurjchem-65 52 73     SPACE eurjchem-65 52 74 1.19‐1.35 1.19‐1.35 NUM eurjchem-65 52 75     SPACE eurjchem-65 52 76 ( ( PUNCT eurjchem-65 52 77 m m PROPN eurjchem-65 52 78 , , PUNCT eurjchem-65 52 79     SPACE eurjchem-65 52 80 5h 5h NUM eurjchem-65 52 81 , , PUNCT eurjchem-65 52 82     SPACE eurjchem-65 52 83 haliph haliph NOUN eurjchem-65 52 84 . . PUNCT eurjchem-65 52 85 ) ) PUNCT eurjchem-65 52 86 , , PUNCT eurjchem-65 52 87     SPACE eurjchem-65 52 88 1.58 1.58 NUM eurjchem-65 52 89     SPACE eurjchem-65 52 90 ( ( PUNCT eurjchem-65 52 91 d d PROPN eurjchem-65 52 92 , , PUNCT eurjchem-65 52 93     SPACE eurjchem-65 52 94 j j NOUN eurjchem-65 52 95     SPACE eurjchem-65 52 96 = = NOUN eurjchem-65 52 97     SPACE eurjchem-65 52 98 10.8 10.8 NUM eurjchem-65 52 99     SPACE eurjchem-65 52 100 hz hz VERB eurjchem-65 52 101 , , PUNCT eurjchem-65 52 102     SPACE eurjchem-65 52 103 1h 1h NUM eurjchem-65 52 104 , , PUNCT eurjchem-65 52 105     SPACE eurjchem-65 52 106 haliph haliph NOUN eurjchem-65 52 107 . . PUNCT eurjchem-65 52 108 ) ) PUNCT eurjchem-65 53 1 , , PUNCT eurjchem-65 53 2     SPACE eurjchem-65 53 3 1.70 1.70 NUM eurjchem-65 53 4     SPACE eurjchem-65 53 5 ( ( PUNCT eurjchem-65 53 6 d d PROPN eurjchem-65 53 7 , , PUNCT eurjchem-65 53 8     SPACE eurjchem-65 53 9 j j NOUN eurjchem-65 53 10     SPACE eurjchem-65 53 11 = = VERB eurjchem-65 53 12     SPACE eurjchem-65 53 13 10.0 10.0 NUM eurjchem-65 53 14     SPACE eurjchem-65 53 15 hz hz VERB eurjchem-65 53 16 , , PUNCT eurjchem-65 53 17     SPACE eurjchem-65 53 18 2h 2h NUM eurjchem-65 53 19 , , PUNCT eurjchem-65 53 20     SPACE eurjchem-65 53 21 haliph haliph NOUN eurjchem-65 53 22 . . PUNCT eurjchem-65 53 23 ) ) PUNCT eurjchem-65 54 1 , , PUNCT eurjchem-65 54 2     SPACE eurjchem-65 54 3 2.01 2.01 NUM eurjchem-65 54 4     SPACE eurjchem-65 54 5 ( ( PUNCT eurjchem-65 54 6 d d PROPN eurjchem-65 54 7 , , PUNCT eurjchem-65 54 8     SPACE eurjchem-65 54 9 j j NOUN eurjchem-65 54 10     SPACE eurjchem-65 54 11 = = VERB eurjchem-65 54 12     SPACE eurjchem-65 54 13 9.2 9.2 NUM eurjchem-65 54 14     SPACE eurjchem-65 54 15 hz hz VERB eurjchem-65 54 16 , , PUNCT eurjchem-65 54 17       SPACE eurjchem-65 54 18 2h 2h NUM eurjchem-65 54 19 , , PUNCT eurjchem-65 54 20     SPACE eurjchem-65 54 21 haliph haliph NOUN eurjchem-65 54 22 . . PUNCT eurjchem-65 54 23 ) ) PUNCT eurjchem-65 55 1 , , PUNCT eurjchem-65 55 2     SPACE eurjchem-65 55 3 3.57 3.57 NUM eurjchem-65 55 4     SPACE eurjchem-65 55 5 ( ( PUNCT eurjchem-65 55 6 br br PROPN eurjchem-65 55 7 , , PUNCT eurjchem-65 55 8     SPACE eurjchem-65 55 9 1h 1h NUM eurjchem-65 55 10 , , PUNCT eurjchem-65 55 11     SPACE eurjchem-65 55 12 ch‐n ch‐n PROPN eurjchem-65 55 13 ) ) PUNCT eurjchem-65 55 14 , , PUNCT eurjchem-65 55 15     SPACE eurjchem-65 55 16 7.50 7.50 NUM eurjchem-65 55 17     SPACE eurjchem-65 55 18 ( ( PUNCT eurjchem-65 55 19 br br PROPN eurjchem-65 55 20 , , PUNCT eurjchem-65 55 21     SPACE eurjchem-65 55 22 1h 1h NUM eurjchem-65 55 23 , , PUNCT eurjchem-65 55 24     SPACE eurjchem-65 55 25 ar‐h ar‐h NOUN eurjchem-65 55 26 ) ) PUNCT eurjchem-65 55 27 , , PUNCT eurjchem-65 55 28     SPACE eurjchem-65 55 29 8.05 8.05 NUM eurjchem-65 55 30     SPACE eurjchem-65 55 31 ( ( PUNCT eurjchem-65 55 32 s s PROPN eurjchem-65 55 33 , , PUNCT eurjchem-65 55 34     SPACE eurjchem-65 55 35 1h 1h NUM eurjchem-65 55 36 , , PUNCT eurjchem-65 55 37     SPACE eurjchem-65 55 38 nh nh PROPN eurjchem-65 55 39 , , PUNCT eurjchem-65 55 40     SPACE eurjchem-65 55 41 d2o d2o NOUN eurjchem-65 55 42     SPACE eurjchem-65 55 43 exchange exchange NOUN eurjchem-65 55 44 ) ) PUNCT eurjchem-65 55 45 , , PUNCT eurjchem-65 55 46     SPACE eurjchem-65 55 47 8.13 8.13 NUM eurjchem-65 55 48     SPACE eurjchem-65 55 49 ( ( PUNCT eurjchem-65 55 50 d d PROPN eurjchem-65 55 51 , , PUNCT eurjchem-65 55 52     SPACE eurjchem-65 55 53 j j PROPN eurjchem-65 55 54     SPACE eurjchem-65 56 1 = = NOUN eurjchem-65 56 2     SPACE eurjchem-65 56 3 7.5 7.5 NUM eurjchem-65 56 4       SPACE eurjchem-65 56 5 hz hz VERB eurjchem-65 56 6 , , PUNCT eurjchem-65 56 7     SPACE eurjchem-65 56 8 1h 1h NUM eurjchem-65 56 9 , , PUNCT eurjchem-65 56 10     SPACE eurjchem-65 56 11 ar‐h ar‐h NOUN eurjchem-65 56 12 ) ) PUNCT eurjchem-65 56 13 , , PUNCT eurjchem-65 56 14     SPACE eurjchem-65 56 15 8.61 8.61 NUM eurjchem-65 56 16     SPACE eurjchem-65 56 17 ( ( PUNCT eurjchem-65 56 18 s s PROPN eurjchem-65 56 19 , , PUNCT eurjchem-65 56 20     SPACE eurjchem-65 56 21 1h 1h NUM eurjchem-65 56 22 , , PUNCT eurjchem-65 56 23     SPACE eurjchem-65 56 24 ar‐h ar‐h NOUN eurjchem-65 56 25 ) ) PUNCT eurjchem-65 56 26 , , PUNCT eurjchem-65 56 27     SPACE eurjchem-65 56 28 8.94 8.94 NUM eurjchem-65 56 29     SPACE eurjchem-65 56 30 ( ( PUNCT eurjchem-65 56 31 s s PROPN eurjchem-65 56 32 , , PUNCT eurjchem-65 56 33     SPACE eurjchem-65 56 34 1h 1h NUM eurjchem-65 56 35 , , PUNCT eurjchem-65 56 36     SPACE eurjchem-65 56 37 ar‐h ar‐h NOUN eurjchem-65 56 38 ) ) PUNCT eurjchem-65 56 39 . . PUNCT eurjchem-65 56 40     SPACE eurjchem-65 57 1 ms ms PROPN eurjchem-65 57 2     SPACE eurjchem-65 57 3 ( ( PUNCT eurjchem-65 57 4 ei ei PROPN eurjchem-65 57 5 , , PUNCT eurjchem-65 57 6     SPACE eurjchem-65 57 7 m m NOUN eurjchem-65 57 8 / / SYM eurjchem-65 57 9 z(% z(% NOUN eurjchem-65 57 10 ) ) PUNCT eurjchem-65 57 11 ): ): PUNCT eurjchem-65 57 12     SPACE eurjchem-65 57 13 260 260 NUM eurjchem-65 57 14     SPACE eurjchem-65 57 15 ( ( PUNCT eurjchem-65 57 16 m+ m+ NOUN eurjchem-65 57 17 ) ) PUNCT eurjchem-65 57 18 , , PUNCT eurjchem-65 57 19     SPACE eurjchem-65 57 20 203 203 NUM eurjchem-65 57 21 , , PUNCT eurjchem-65 57 22     SPACE eurjchem-65 57 23 178 178 NUM eurjchem-65 57 24     SPACE eurjchem-65 57 25 ( ( PUNCT eurjchem-65 57 26 base base NOUN eurjchem-65 57 27     SPACE eurjchem-65 57 28 peak peak NOUN eurjchem-65 57 29 ) ) PUNCT eurjchem-65 57 30 , , PUNCT eurjchem-65 57 31     SPACE eurjchem-65 57 32 156 156 NUM eurjchem-65 57 33 , , PUNCT eurjchem-65 57 34     SPACE eurjchem-65 57 35 119 119 NUM eurjchem-65 57 36 , , PUNCT eurjchem-65 57 37     SPACE eurjchem-65 57 38 105 105 NUM eurjchem-65 57 39 , , PUNCT eurjchem-65 57 40     SPACE eurjchem-65 57 41 77 77 NUM eurjchem-65 57 42 . . PUNCT eurjchem-65 57 43     SPACE eurjchem-65 58 1 n­cyclohexyl­5­(pyridin­4­yl)­1,3,4­thiadiazol­2­amine n­cyclohexyl­5­(pyridin­4­yl)­1,3,4­thiadiazol­2­amine NUM eurjchem-65 58 2     SPACE eurjchem-65 58 3 ( ( PUNCT eurjchem-65 58 4 5c 5c NUM eurjchem-65 58 5 ): ): PUNCT eurjchem-65 58 6     SPACE eurjchem-65 58 7 yield yield NOUN eurjchem-65 58 8 : : PUNCT eurjchem-65 58 9     SPACE eurjchem-65 58 10 66 66 NUM eurjchem-65 58 11 % % NOUN eurjchem-65 58 12 . . PUNCT eurjchem-65 58 13     SPACE eurjchem-65 59 1 m.p m.p PROPN eurjchem-65 59 2 . . PROPN eurjchem-65 59 3 : : PUNCT eurjchem-65 59 4     SPACE eurjchem-65 59 5 230‐231 230‐231 NUM eurjchem-65 59 6     SPACE eurjchem-65 59 7 oc oc PROPN eurjchem-65 59 8 . . PUNCT eurjchem-65 59 9     SPACE eurjchem-65 59 10 ir ir VERB eurjchem-65 59 11     SPACE eurjchem-65 59 12 ( ( PUNCT eurjchem-65 59 13 kbr kbr PROPN eurjchem-65 59 14 , , PUNCT eurjchem-65 59 15     SPACE eurjchem-65 59 16 cm‐1 cm‐1 NOUN eurjchem-65 59 17 ): ): PUNCT eurjchem-65 59 18     SPACE eurjchem-65 59 19 3190 3190 NUM eurjchem-65 59 20     SPACE eurjchem-65 59 21 (nh (nh NOUN eurjchem-65 59 22 ) ) PUNCT eurjchem-65 59 23 , , PUNCT eurjchem-65 59 24     SPACE eurjchem-65 59 25 3010 3010 NUM eurjchem-65 59 26     SPACE eurjchem-65 59 27 (arom (arom PROPN eurjchem-65 59 28 . . PROPN eurjchem-65 59 29     SPACE eurjchem-65 59 30 ch ch NOUN eurjchem-65 59 31 ) ) PUNCT eurjchem-65 59 32 , , PUNCT eurjchem-65 59 33     SPACE eurjchem-65 59 34 2930 2930 NUM eurjchem-65 59 35 , , PUNCT eurjchem-65 59 36     SPACE eurjchem-65 59 37 2850 2850 NUM eurjchem-65 59 38     SPACE eurjchem-65 59 39 (aliph (aliph PROPN eurjchem-65 59 40 . . PUNCT eurjchem-65 59 41     SPACE eurjchem-65 59 42 c‐h c‐h PROPN eurjchem-65 59 43 ) ) PUNCT eurjchem-65 59 44 , , PUNCT eurjchem-65 59 45     SPACE eurjchem-65 59 46 1580 1580 NUM eurjchem-65 59 47     SPACE eurjchem-65 59 48 (c (c PROPN eurjchem-65 59 49 = = SYM eurjchem-65 59 50 n n CCONJ eurjchem-65 59 51     SPACE eurjchem-65 59 52 and and CCONJ eurjchem-65 59 53     SPACE eurjchem-65 59 54 c c NOUN eurjchem-65 59 55 = = NOUN eurjchem-65 59 56 c c NOUN eurjchem-65 59 57 ) ) PUNCT eurjchem-65 59 58 . . PUNCT eurjchem-65 59 59     SPACE eurjchem-65 59 60 1h 1h NUM eurjchem-65 59 61     SPACE eurjchem-65 59 62 nmr nmr NOUN eurjchem-65 59 63     SPACE eurjchem-65 59 64 ( ( PUNCT eurjchem-65 59 65 dmso‐d6 dmso‐d6 PROPN eurjchem-65 59 66 , , PUNCT eurjchem-65 59 67     SPACE eurjchem-65 59 68 δ δ PROPN eurjchem-65 59 69 , , PUNCT eurjchem-65 59 70     SPACE eurjchem-65 59 71 ppm ppm ADJ eurjchem-65 59 72 ): ): PUNCT eurjchem-65 59 73     SPACE eurjchem-65 59 74 1.19‐1.35 1.19‐1.35 NUM eurjchem-65 59 75     SPACE eurjchem-65 59 76 ( ( PUNCT eurjchem-65 59 77 m m PROPN eurjchem-65 59 78 , , PUNCT eurjchem-65 59 79     SPACE eurjchem-65 59 80 5h 5h NUM eurjchem-65 59 81 , , PUNCT eurjchem-65 59 82     SPACE eurjchem-65 59 83 haliph haliph NOUN eurjchem-65 59 84 . . PUNCT eurjchem-65 59 85 ) ) PUNCT eurjchem-65 59 86 , , PUNCT eurjchem-65 59 87     SPACE eurjchem-65 59 88 1.57 1.57 NUM eurjchem-65 59 89     SPACE eurjchem-65 59 90 ( ( PUNCT eurjchem-65 59 91 d d PROPN eurjchem-65 59 92 , , PUNCT eurjchem-65 59 93     SPACE eurjchem-65 59 94 j j NOUN eurjchem-65 59 95     SPACE eurjchem-65 59 96 = = NOUN eurjchem-65 59 97     SPACE eurjchem-65 59 98 11.9 11.9 NUM eurjchem-65 59 99     SPACE eurjchem-65 59 100 hz hz VERB eurjchem-65 59 101 , , PUNCT eurjchem-65 59 102     SPACE eurjchem-65 59 103 1h 1h NUM eurjchem-65 59 104 , , PUNCT eurjchem-65 59 105     SPACE eurjchem-65 59 106 haliph haliph NOUN eurjchem-65 59 107 . . PUNCT eurjchem-65 59 108 ) ) PUNCT eurjchem-65 60 1 , , PUNCT eurjchem-65 60 2     SPACE eurjchem-65 60 3 1.71 1.71 NUM eurjchem-65 60 4     SPACE eurjchem-65 60 5 ( ( PUNCT eurjchem-65 60 6 d d PROPN eurjchem-65 60 7 , , PUNCT eurjchem-65 60 8     SPACE eurjchem-65 60 9 j j PROPN eurjchem-65 60 10     SPACE eurjchem-65 60 11 = = NOUN eurjchem-65 60 12     SPACE eurjchem-65 60 13 8.8 8.8 NUM eurjchem-65 60 14     SPACE eurjchem-65 60 15 hz hz VERB eurjchem-65 60 16 , , PUNCT eurjchem-65 60 17     SPACE eurjchem-65 60 18 2h 2h NUM eurjchem-65 60 19 , , PUNCT eurjchem-65 60 20     SPACE eurjchem-65 60 21 haliph haliph NOUN eurjchem-65 60 22 . . PUNCT eurjchem-65 60 23 ) ) PUNCT eurjchem-65 61 1 , , PUNCT eurjchem-65 61 2     SPACE eurjchem-65 61 3 2.01 2.01 NUM eurjchem-65 61 4     SPACE eurjchem-65 61 5 ( ( PUNCT eurjchem-65 61 6 d d PROPN eurjchem-65 61 7 , , PUNCT eurjchem-65 61 8     SPACE eurjchem-65 61 9 j j PROPN eurjchem-65 61 10     SPACE eurjchem-65 61 11 = = NOUN eurjchem-65 61 12     SPACE eurjchem-65 61 13 9.8 9.8 NUM eurjchem-65 61 14     SPACE eurjchem-65 61 15 hz hz VERB eurjchem-65 61 16 , , PUNCT eurjchem-65 61 17         SPACE eurjchem-65 61 18 2h 2h NUM eurjchem-65 61 19 , , PUNCT eurjchem-65 61 20     SPACE eurjchem-65 61 21 haliph haliph NOUN eurjchem-65 61 22 .. .. PUNCT eurjchem-65 61 23 ) ) PUNCT eurjchem-65 61 24 , , PUNCT eurjchem-65 61 25     SPACE eurjchem-65 61 26 3.58 3.58 NUM eurjchem-65 61 27     SPACE eurjchem-65 61 28 ( ( PUNCT eurjchem-65 61 29 br br PROPN eurjchem-65 61 30 , , PUNCT eurjchem-65 61 31     SPACE eurjchem-65 61 32 1h 1h NUM eurjchem-65 61 33 , , PUNCT eurjchem-65 61 34     SPACE eurjchem-65 61 35 ch‐n ch‐n PROPN eurjchem-65 61 36 ) ) PUNCT eurjchem-65 61 37 , , PUNCT eurjchem-65 61 38     SPACE eurjchem-65 61 39 7.70 7.70 NUM eurjchem-65 61 40     SPACE eurjchem-65 61 41 ( ( PUNCT eurjchem-65 61 42 d d PROPN eurjchem-65 61 43 , , PUNCT eurjchem-65 61 44     SPACE eurjchem-65 61 45 j j PROPN eurjchem-65 61 46     SPACE eurjchem-65 61 47 = = NOUN eurjchem-65 61 48     SPACE eurjchem-65 61 49 4.6 4.6 NUM eurjchem-65 61 50     SPACE eurjchem-65 61 51 hz hz VERB eurjchem-65 61 52 , , PUNCT eurjchem-65 61 53     SPACE eurjchem-65 61 54 2h 2h NUM eurjchem-65 61 55 , , PUNCT eurjchem-65 61 56     SPACE eurjchem-65 61 57 ar‐ ar‐ NOUN eurjchem-65 61 58 h h NOUN eurjchem-65 61 59 ) ) PUNCT eurjchem-65 61 60 , , PUNCT eurjchem-65 61 61     SPACE eurjchem-65 61 62 8.20 8.20 NUM eurjchem-65 61 63     SPACE eurjchem-65 61 64 ( ( PUNCT eurjchem-65 61 65 s s PROPN eurjchem-65 61 66 , , PUNCT eurjchem-65 61 67     SPACE eurjchem-65 61 68 1h 1h NUM eurjchem-65 61 69 , , PUNCT eurjchem-65 61 70     SPACE eurjchem-65 61 71 nh nh PROPN eurjchem-65 61 72 , , PUNCT eurjchem-65 61 73     SPACE eurjchem-65 61 74 d2o d2o NOUN eurjchem-65 61 75     SPACE eurjchem-65 61 76 exchange exchange NOUN eurjchem-65 61 77 ) ) PUNCT eurjchem-65 61 78 , , PUNCT eurjchem-65 61 79     SPACE eurjchem-65 61 80 8.64 8.64 NUM eurjchem-65 61 81     SPACE eurjchem-65 61 82 ( ( PUNCT eurjchem-65 61 83 d d PROPN eurjchem-65 61 84 , , PUNCT eurjchem-65 61 85     SPACE eurjchem-65 61 86 j j NOUN eurjchem-65 61 87     SPACE eurjchem-65 62 1 = = NOUN eurjchem-65 62 2     SPACE eurjchem-65 62 3 4.4 4.4 NUM eurjchem-65 62 4     SPACE eurjchem-65 62 5 hz hz VERB eurjchem-65 62 6 , , PUNCT eurjchem-65 62 7     SPACE eurjchem-65 62 8 2h 2h NUM eurjchem-65 62 9 , , PUNCT eurjchem-65 62 10     SPACE eurjchem-65 62 11 ar‐h ar‐h NOUN eurjchem-65 62 12 ) ) PUNCT eurjchem-65 62 13 . . PUNCT eurjchem-65 62 14     SPACE eurjchem-65 63 1 ms ms PROPN eurjchem-65 63 2     SPACE eurjchem-65 63 3 ( ( PUNCT eurjchem-65 63 4 ei ei PROPN eurjchem-65 63 5 , , PUNCT eurjchem-65 63 6     SPACE eurjchem-65 63 7 m m NOUN eurjchem-65 63 8 / / SYM eurjchem-65 63 9 z(% z(% NOUN eurjchem-65 63 10 ) ) PUNCT eurjchem-65 63 11 ): ): PUNCT eurjchem-65 63 12     SPACE eurjchem-65 63 13 260 260 NUM eurjchem-65 63 14     SPACE eurjchem-65 63 15 ( ( PUNCT eurjchem-65 63 16 m+ m+ NOUN eurjchem-65 63 17 ) ) PUNCT eurjchem-65 63 18 , , PUNCT eurjchem-65 63 19     SPACE eurjchem-65 63 20 203 203 NUM eurjchem-65 63 21 , , PUNCT eurjchem-65 63 22     SPACE eurjchem-65 63 23 178 178 NUM eurjchem-65 63 24     SPACE eurjchem-65 63 25 ( ( PUNCT eurjchem-65 63 26 base base NOUN eurjchem-65 63 27     SPACE eurjchem-65 63 28 peak peak NOUN eurjchem-65 63 29 ) ) PUNCT eurjchem-65 63 30 , , PUNCT eurjchem-65 63 31     SPACE eurjchem-65 63 32 119 119 NUM eurjchem-65 63 33 , , PUNCT eurjchem-65 63 34     SPACE eurjchem-65 63 35 105 105 NUM eurjchem-65 63 36 , , PUNCT eurjchem-65 63 37     SPACE eurjchem-65 63 38 55 55 NUM eurjchem-65 63 39 , , PUNCT eurjchem-65 63 40     SPACE eurjchem-65 63 41 41 41 NUM eurjchem-65 63 42 . . PUNCT eurjchem-65 63 43         SPACE eurjchem-65 63 44 2.4 2.4 NUM eurjchem-65 63 45 . . PUNCT eurjchem-65 63 46     SPACE eurjchem-65 63 47 general general ADJ eurjchem-65 63 48     SPACE eurjchem-65 63 49 procedure procedure NOUN eurjchem-65 63 50     SPACE eurjchem-65 63 51 for for ADP eurjchem-65 63 52     SPACE eurjchem-65 63 53 the the DET eurjchem-65 63 54     SPACE eurjchem-65 63 55 synthesis synthesis NOUN eurjchem-65 63 56     SPACE eurjchem-65 63 57 of of ADP eurjchem-65 63 58     SPACE eurjchem-65 63 59 1,3,4­oxadizoles 1,3,4­oxadizole NOUN eurjchem-65 63 60       SPACE eurjchem-65 63 61 6a­c 6a­c NOUN eurjchem-65 63 62         SPACE eurjchem-65 63 63 a a DET eurjchem-65 63 64     SPACE eurjchem-65 63 65 mixture mixture NOUN eurjchem-65 63 66     SPACE eurjchem-65 63 67 of of ADP eurjchem-65 63 68     SPACE eurjchem-65 63 69 thiosemicarbazide thiosemicarbazide NOUN eurjchem-65 63 70     SPACE eurjchem-65 63 71 3a­c 3a­c NOUN eurjchem-65 63 72     SPACE eurjchem-65 63 73 ( ( PUNCT eurjchem-65 63 74 10 10 NUM eurjchem-65 63 75     SPACE eurjchem-65 63 76 mmol mmol NOUN eurjchem-65 63 77 ) ) PUNCT eurjchem-65 63 78     SPACE eurjchem-65 63 79 and and CCONJ eurjchem-65 63 80     SPACE eurjchem-65 63 81 mercuric mercuric NOUN eurjchem-65 63 82     SPACE eurjchem-65 63 83 acetate acetate NOUN eurjchem-65 63 84     SPACE eurjchem-65 63 85 ( ( PUNCT eurjchem-65 63 86 10 10 NUM eurjchem-65 63 87     SPACE eurjchem-65 63 88 mmol mmol NOUN eurjchem-65 63 89 ) ) PUNCT eurjchem-65 63 90     SPACE eurjchem-65 63 91 in in ADP eurjchem-65 63 92     SPACE eurjchem-65 63 93 ethanol ethanol NOUN eurjchem-65 63 94     SPACE eurjchem-65 63 95 ( ( PUNCT eurjchem-65 63 96 30 30 NUM eurjchem-65 63 97     SPACE eurjchem-65 63 98 ml ml NOUN eurjchem-65 63 99 ) ) PUNCT eurjchem-65 63 100     SPACE eurjchem-65 63 101 was be AUX eurjchem-65 63 102     SPACE eurjchem-65 63 103 refluxed refluxe VERB eurjchem-65 63 104     SPACE eurjchem-65 63 105 for for ADP eurjchem-65 63 106     SPACE eurjchem-65 63 107 3 3 NUM eurjchem-65 63 108     SPACE eurjchem-65 63 109 h. h. NOUN eurjchem-65 63 110     SPACE eurjchem-65 63 111 the the DET eurjchem-65 63 112     SPACE eurjchem-65 63 113 mixture mixture NOUN eurjchem-65 63 114     SPACE eurjchem-65 63 115 was be AUX eurjchem-65 63 116     SPACE eurjchem-65 63 117 cooled cool VERB eurjchem-65 63 118     SPACE eurjchem-65 63 119 at at ADP eurjchem-65 63 120     SPACE eurjchem-65 63 121 room room NOUN eurjchem-65 63 122     SPACE eurjchem-65 63 123 temperature temperature NOUN eurjchem-65 63 124 , , PUNCT eurjchem-65 63 125     SPACE eurjchem-65 63 126 the the DET eurjchem-65 63 127     SPACE eurjchem-65 63 128 solid solid NOUN eurjchem-65 63 129     SPACE eurjchem-65 63 130 was be AUX eurjchem-65 63 131     SPACE eurjchem-65 63 132 filtered filter VERB eurjchem-65 63 133     SPACE eurjchem-65 63 134 and and CCONJ eurjchem-65 63 135     SPACE eurjchem-65 63 136 solvent solvent NOUN eurjchem-65 63 137     SPACE eurjchem-65 63 138 was be AUX eurjchem-65 63 139     SPACE eurjchem-65 63 140 evaporated evaporate VERB eurjchem-65 63 141 . . PUNCT eurjchem-65 63 142     SPACE eurjchem-65 64 1 the the DET eurjchem-65 64 2     SPACE eurjchem-65 64 3 crude crude NOUN eurjchem-65 64 4     SPACE eurjchem-65 64 5 product product NOUN eurjchem-65 64 6     SPACE eurjchem-65 64 7 was be AUX eurjchem-65 64 8     SPACE eurjchem-65 64 9 crystallized crystallize VERB eurjchem-65 64 10     SPACE eurjchem-65 64 11 from from ADP eurjchem-65 64 12     SPACE eurjchem-65 64 13 a a DET eurjchem-65 64 14     SPACE eurjchem-65 64 15 mixture mixture NOUN eurjchem-65 64 16     SPACE eurjchem-65 64 17 of of ADP eurjchem-65 64 18     SPACE eurjchem-65 64 19 tetrahydrofuran tetrahydrofuran NOUN eurjchem-65 64 20     SPACE eurjchem-65 64 21 and and CCONJ eurjchem-65 64 22     SPACE eurjchem-65 64 23 petroleum petroleum NOUN eurjchem-65 64 24     SPACE eurjchem-65 64 25 ether ether NOUN eurjchem-65 64 26     SPACE eurjchem-65 64 27 ( ( PUNCT eurjchem-65 64 28 1:2 1:2 NUM eurjchem-65 64 29 ) ) PUNCT eurjchem-65 64 30     SPACE eurjchem-65 64 31 to to PART eurjchem-65 64 32     SPACE eurjchem-65 64 33 furnish furnish VERB eurjchem-65 64 34     SPACE eurjchem-65 64 35 di‐substituted di‐substitute VERB eurjchem-65 64 36     SPACE eurjchem-65 64 37 1,3,4‐oxadiazole 1,3,4‐oxadiazole NUM eurjchem-65 64 38     SPACE eurjchem-65 64 39 6a­c 6a­c NOUN eurjchem-65 64 40     SPACE eurjchem-65 64 41 ( ( PUNCT eurjchem-65 64 42 scheme scheme NOUN eurjchem-65 64 43     SPACE eurjchem-65 64 44 1 1 NUM eurjchem-65 64 45 ) ) PUNCT eurjchem-65 64 46 . . PUNCT eurjchem-65 64 47     SPACE eurjchem-65 65 1 n­cyclohexyl­5­(pyridin­2­yl)­1,3,4­oxadiazol­2­amine n­cyclohexyl­5­(pyridin­2­yl)­1,3,4­oxadiazol­2­amine PRON eurjchem-65 65 2     SPACE eurjchem-65 65 3 ( ( PUNCT eurjchem-65 65 4 6a 6a NOUN eurjchem-65 65 5 ): ): PUNCT eurjchem-65 65 6     SPACE eurjchem-65 65 7 yield yield NOUN eurjchem-65 65 8 : : PUNCT eurjchem-65 65 9     SPACE eurjchem-65 65 10 85 85 NUM eurjchem-65 65 11 % % NOUN eurjchem-65 65 12 . . PUNCT eurjchem-65 65 13     SPACE eurjchem-65 66 1 m.p m.p PROPN eurjchem-65 66 2 . . PROPN eurjchem-65 66 3 : : PUNCT eurjchem-65 66 4     SPACE eurjchem-65 66 5 210‐211 210‐211 NUM eurjchem-65 66 6     SPACE eurjchem-65 66 7 oc oc PROPN eurjchem-65 66 8 . . PUNCT eurjchem-65 66 9     SPACE eurjchem-65 66 10 ir ir VERB eurjchem-65 66 11     SPACE eurjchem-65 66 12 ( ( PUNCT eurjchem-65 66 13 kbr kbr PROPN eurjchem-65 66 14 , , PUNCT eurjchem-65 66 15     SPACE eurjchem-65 66 16 cm‐1 cm‐1 NOUN eurjchem-65 66 17 ): ): PUNCT eurjchem-65 66 18     SPACE eurjchem-65 66 19 3244 3244 NUM eurjchem-65 66 20     SPACE eurjchem-65 66 21 (nh (nh PROPN eurjchem-65 66 22 ) ) PUNCT eurjchem-65 66 23 , , PUNCT eurjchem-65 66 24     SPACE eurjchem-65 66 25 3010 3010 NUM eurjchem-65 66 26     SPACE eurjchem-65 66 27 (arom (arom PROPN eurjchem-65 66 28 . . PROPN eurjchem-65 66 29     SPACE eurjchem-65 66 30 ch ch NOUN eurjchem-65 66 31 ) ) PUNCT eurjchem-65 66 32 , , PUNCT eurjchem-65 66 33     SPACE eurjchem-65 66 34 2931 2931 NUM eurjchem-65 66 35 , , PUNCT eurjchem-65 66 36     SPACE eurjchem-65 66 37 2851 2851 NUM eurjchem-65 66 38     SPACE eurjchem-65 66 39 (aliph (aliph NOUN eurjchem-65 66 40 . . PUNCT eurjchem-65 66 41     SPACE eurjchem-65 66 42 c‐h c‐h PROPN eurjchem-65 66 43 ) ) PUNCT eurjchem-65 66 44 , , PUNCT eurjchem-65 66 45     SPACE eurjchem-65 66 46 1562 1562 NUM eurjchem-65 66 47     SPACE eurjchem-65 66 48 (c (c PROPN eurjchem-65 66 49 = = SYM eurjchem-65 66 50 n n CCONJ eurjchem-65 66 51     SPACE eurjchem-65 66 52 and and CCONJ eurjchem-65 66 53     SPACE eurjchem-65 66 54 c c NOUN eurjchem-65 66 55 = = NOUN eurjchem-65 66 56 c c NOUN eurjchem-65 66 57 ) ) PUNCT eurjchem-65 66 58 . . PUNCT eurjchem-65 66 59     SPACE eurjchem-65 66 60 1h 1h NUM eurjchem-65 66 61     SPACE eurjchem-65 66 62 nmr nmr NOUN eurjchem-65 66 63     SPACE eurjchem-65 66 64 ( ( PUNCT eurjchem-65 66 65 dmso‐d6 dmso‐d6 PROPN eurjchem-65 66 66 , , PUNCT eurjchem-65 66 67     SPACE eurjchem-65 66 68 δ δ PROPN eurjchem-65 66 69 , , PUNCT eurjchem-65 66 70     SPACE eurjchem-65 66 71 ppm ppm NOUN eurjchem-65 66 72 ): ): PUNCT eurjchem-65 66 73     SPACE eurjchem-65 66 74 1.18 1.18 NUM eurjchem-65 66 75     SPACE eurjchem-65 66 76 ( ( PUNCT eurjchem-65 66 77 d d PROPN eurjchem-65 66 78 , , PUNCT eurjchem-65 66 79     SPACE eurjchem-65 66 80 j j PROPN eurjchem-65 66 81     SPACE eurjchem-65 67 1 = = NOUN eurjchem-65 67 2     SPACE eurjchem-65 67 3 4.9 4.9 NUM eurjchem-65 67 4     SPACE eurjchem-65 67 5 hz hz VERB eurjchem-65 67 6 , , PUNCT eurjchem-65 67 7     SPACE eurjchem-65 67 8 1h 1h NUM eurjchem-65 67 9 , , PUNCT eurjchem-65 67 10     SPACE eurjchem-65 67 11 haliph haliph NOUN eurjchem-65 67 12 ) ) PUNCT eurjchem-65 67 13 , , PUNCT eurjchem-65 67 14     SPACE eurjchem-65 67 15 1.32 1.32 NUM eurjchem-65 67 16     SPACE eurjchem-65 67 17 ( ( PUNCT eurjchem-65 67 18 q q NOUN eurjchem-65 67 19 , , PUNCT eurjchem-65 67 20     SPACE eurjchem-65 67 21 j j PROPN eurjchem-65 67 22     SPACE eurjchem-65 67 23 = = VERB eurjchem-65 67 24     SPACE eurjchem-65 67 25 5.4 5.4 NUM eurjchem-65 67 26     SPACE eurjchem-65 67 27 hz hz VERB eurjchem-65 67 28 , , PUNCT eurjchem-65 67 29     SPACE eurjchem-65 67 30 4h 4h NOUN eurjchem-65 67 31 , , PUNCT eurjchem-65 67 32     SPACE eurjchem-65 67 33 haliph haliph NOUN eurjchem-65 67 34 ) ) PUNCT eurjchem-65 67 35 , , PUNCT eurjchem-65 67 36     SPACE eurjchem-65 67 37 1.57 1.57 NUM eurjchem-65 67 38     SPACE eurjchem-65 67 39 ( ( PUNCT eurjchem-65 67 40 d d PROPN eurjchem-65 67 41 , , PUNCT eurjchem-65 67 42     SPACE eurjchem-65 67 43 j j PROPN eurjchem-65 67 44     SPACE eurjchem-65 68 1 = = NOUN eurjchem-65 68 2     SPACE eurjchem-65 68 3 11.8 11.8 NUM eurjchem-65 68 4     SPACE eurjchem-65 68 5 hz hz VERB eurjchem-65 68 6 , , PUNCT eurjchem-65 68 7     SPACE eurjchem-65 68 8 1h 1h NUM eurjchem-65 68 9 , , PUNCT eurjchem-65 68 10     SPACE eurjchem-65 68 11 haliph haliph NOUN eurjchem-65 68 12 . . PUNCT eurjchem-65 68 13 ) ) PUNCT eurjchem-65 69 1 , , PUNCT eurjchem-65 69 2     SPACE eurjchem-65 69 3 1.73 1.73 NUM eurjchem-65 69 4     SPACE eurjchem-65 69 5 ( ( PUNCT eurjchem-65 69 6 q q ADJ eurjchem-65 69 7 , , PUNCT eurjchem-65 69 8     SPACE eurjchem-65 69 9 j= j= NOUN eurjchem-65 69 10     SPACE eurjchem-65 69 11 4.9 4.9 NUM eurjchem-65 69 12     SPACE eurjchem-65 69 13 hz hz VERB eurjchem-65 69 14 , , PUNCT eurjchem-65 69 15     SPACE eurjchem-65 69 16 2h 2h NUM eurjchem-65 69 17 , , PUNCT eurjchem-65 69 18     SPACE eurjchem-65 69 19 haliph haliph NOUN eurjchem-65 69 20 . . PUNCT eurjchem-65 69 21 ) ) PUNCT eurjchem-65 70 1 , , PUNCT eurjchem-65 70 2     SPACE eurjchem-65 70 3 1.96 1.96 NUM eurjchem-65 70 4     SPACE eurjchem-65 70 5 ( ( PUNCT eurjchem-65 70 6 d d PROPN eurjchem-65 70 7 , , PUNCT eurjchem-65 70 8     SPACE eurjchem-65 70 9 j j NOUN eurjchem-65 70 10     SPACE eurjchem-65 70 11 = = NOUN eurjchem-65 70 12     SPACE eurjchem-65 70 13 1.9 1.9 NUM eurjchem-65 70 14     SPACE eurjchem-65 70 15 hz hz VERB eurjchem-65 70 16 , , PUNCT eurjchem-65 70 17       SPACE eurjchem-65 70 18 2h 2h NUM eurjchem-65 70 19 , , PUNCT eurjchem-65 70 20     SPACE eurjchem-65 70 21 haliph haliph NOUN eurjchem-65 70 22 . . PUNCT eurjchem-65 70 23 ) ) PUNCT eurjchem-65 71 1 , , PUNCT eurjchem-65 71 2     SPACE eurjchem-65 71 3 3.45 3.45 NUM eurjchem-65 71 4     SPACE eurjchem-65 71 5 ( ( PUNCT eurjchem-65 71 6 br br PROPN eurjchem-65 71 7 , , PUNCT eurjchem-65 71 8     SPACE eurjchem-65 71 9 1h 1h NUM eurjchem-65 71 10 , , PUNCT eurjchem-65 71 11     SPACE eurjchem-65 71 12 ch‐n ch‐n PROPN eurjchem-65 71 13 ) ) PUNCT eurjchem-65 71 14 , , PUNCT eurjchem-65 71 15     SPACE eurjchem-65 71 16 7.76 7.76 NUM eurjchem-65 71 17     SPACE eurjchem-65 71 18 ( ( PUNCT eurjchem-65 71 19 d d PROPN eurjchem-65 71 20 , , PUNCT eurjchem-65 71 21     SPACE eurjchem-65 71 22 d d PROPN eurjchem-65 71 23 , , PUNCT eurjchem-65 71 24     SPACE eurjchem-65 71 25 j j PROPN eurjchem-65 71 26     SPACE eurjchem-65 71 27 = = NOUN eurjchem-65 71 28     SPACE eurjchem-65 71 29 4.2 4.2 NUM eurjchem-65 71 30 , , PUNCT eurjchem-65 71 31     SPACE eurjchem-65 71 32 7.8 7.8 NUM eurjchem-65 71 33     SPACE eurjchem-65 71 34 hz hz VERB eurjchem-65 71 35 , , PUNCT eurjchem-65 71 36     SPACE eurjchem-65 71 37 1h 1h NUM eurjchem-65 71 38 , , PUNCT eurjchem-65 71 39     SPACE eurjchem-65 71 40 ar‐h ar‐h NOUN eurjchem-65 71 41 ) ) PUNCT eurjchem-65 71 42 , , PUNCT eurjchem-65 71 43     SPACE eurjchem-65 71 44 8.08 8.08 NUM eurjchem-65 71 45     SPACE eurjchem-65 71 46 ( ( PUNCT eurjchem-65 71 47 s s PROPN eurjchem-65 71 48 , , PUNCT eurjchem-65 71 49     SPACE eurjchem-65 71 50 1h 1h NUM eurjchem-65 71 51 , , PUNCT eurjchem-65 71 52     SPACE eurjchem-65 71 53 nh nh PROPN eurjchem-65 71 54 , , PUNCT eurjchem-65 71 55     SPACE eurjchem-65 71 56 d2o d2o NOUN eurjchem-65 71 57     SPACE eurjchem-65 71 58 exchange exchange NOUN eurjchem-65 71 59 ) ) PUNCT eurjchem-65 71 60 , , PUNCT eurjchem-65 71 61     SPACE eurjchem-65 71 62 8.36 8.36 NUM eurjchem-65 71 63     SPACE eurjchem-65 71 64 ( ( PUNCT eurjchem-65 71 65 d d PROPN eurjchem-65 71 66 , , PUNCT eurjchem-65 71 67     SPACE eurjchem-65 71 68 d d PROPN eurjchem-65 71 69 , , PUNCT eurjchem-65 71 70     SPACE eurjchem-65 71 71 j j PROPN eurjchem-65 71 72     SPACE eurjchem-65 71 73 = = NOUN eurjchem-65 71 74     SPACE eurjchem-65 71 75 6.1 6.1 NUM eurjchem-65 71 76 , , PUNCT eurjchem-65 71 77     SPACE eurjchem-65 71 78 1.4 1.4 NUM eurjchem-65 71 79     SPACE eurjchem-65 71 80 hz hz VERB eurjchem-65 71 81 , , PUNCT eurjchem-65 71 82     SPACE eurjchem-65 71 83 1h 1h NUM eurjchem-65 71 84 , , PUNCT eurjchem-65 71 85     SPACE eurjchem-65 71 86 ar‐h ar‐h NOUN eurjchem-65 71 87 ) ) PUNCT eurjchem-65 71 88 , , PUNCT eurjchem-65 71 89     SPACE eurjchem-65 71 90 8.89 8.89 NUM eurjchem-65 71 91     SPACE eurjchem-65 71 92 ( ( PUNCT eurjchem-65 71 93 d d PROPN eurjchem-65 71 94 , , PUNCT eurjchem-65 71 95     SPACE eurjchem-65 71 96 d d PROPN eurjchem-65 71 97 , , PUNCT eurjchem-65 71 98     SPACE eurjchem-65 71 99 j j PROPN eurjchem-65 71 100     SPACE eurjchem-65 72 1 = = NOUN eurjchem-65 72 2     SPACE eurjchem-65 72 3 4.9 4.9 NUM eurjchem-65 72 4 , , PUNCT eurjchem-65 72 5     SPACE eurjchem-65 72 6 1.5 1.5 NUM eurjchem-65 72 7     SPACE eurjchem-65 72 8 hz hz VERB eurjchem-65 72 9 , , PUNCT eurjchem-65 72 10     SPACE eurjchem-65 72 11 1h 1h NUM eurjchem-65 72 12 , , PUNCT eurjchem-65 72 13     SPACE eurjchem-65 72 14 ar‐h ar‐h NOUN eurjchem-65 72 15 ) ) PUNCT eurjchem-65 72 16 , , PUNCT eurjchem-65 72 17     SPACE eurjchem-65 72 18 9.18 9.18 NUM eurjchem-65 72 19     SPACE eurjchem-65 72 20 ( ( PUNCT eurjchem-65 72 21 d d PROPN eurjchem-65 72 22 , , PUNCT eurjchem-65 72 23     SPACE eurjchem-65 72 24 d d PROPN eurjchem-65 72 25 , , PUNCT eurjchem-65 72 26     SPACE eurjchem-65 72 27 j j NOUN eurjchem-65 72 28     SPACE eurjchem-65 73 1 = = NOUN eurjchem-65 73 2     SPACE eurjchem-65 73 3 4.8 4.8 NUM eurjchem-65 73 4 , , PUNCT eurjchem-65 73 5     SPACE eurjchem-65 73 6 0.9 0.9 NUM eurjchem-65 73 7     SPACE eurjchem-65 73 8 hz hz VERB eurjchem-65 73 9 , , PUNCT eurjchem-65 73 10     SPACE eurjchem-65 73 11 1h 1h NUM eurjchem-65 73 12 , , PUNCT eurjchem-65 73 13     SPACE eurjchem-65 73 14 ar‐h ar‐h NOUN eurjchem-65 73 15 ) ) PUNCT eurjchem-65 73 16 . . PUNCT eurjchem-65 73 17     SPACE eurjchem-65 74 1 ms ms PROPN eurjchem-65 74 2     SPACE eurjchem-65 74 3 ( ( PUNCT eurjchem-65 74 4 ei ei PROPN eurjchem-65 74 5 , , PUNCT eurjchem-65 74 6     SPACE eurjchem-65 74 7 m m NOUN eurjchem-65 74 8 / / SYM eurjchem-65 74 9 z(% z(% NOUN eurjchem-65 74 10 ) ) PUNCT eurjchem-65 74 11 ): ): PUNCT eurjchem-65 74 12     SPACE eurjchem-65 74 13 244 244 NUM eurjchem-65 74 14     SPACE eurjchem-65 74 15 ( ( PUNCT eurjchem-65 74 16 m+ m+ NOUN eurjchem-65 74 17 ) ) PUNCT eurjchem-65 74 18 , , PUNCT eurjchem-65 74 19     SPACE eurjchem-65 74 20 227 227 NUM eurjchem-65 74 21 , , PUNCT eurjchem-65 74 22       SPACE eurjchem-65 74 23 162 162 NUM eurjchem-65 74 24     SPACE eurjchem-65 74 25 ( ( PUNCT eurjchem-65 74 26 base base NOUN eurjchem-65 74 27     SPACE eurjchem-65 74 28 peak peak NOUN eurjchem-65 74 29 ) ) PUNCT eurjchem-65 74 30 , , PUNCT eurjchem-65 74 31     SPACE eurjchem-65 74 32 119 119 NUM eurjchem-65 74 33 , , PUNCT eurjchem-65 74 34     SPACE eurjchem-65 74 35 78 78 NUM eurjchem-65 74 36 . . PUNCT eurjchem-65 74 37     SPACE eurjchem-65 74 38 n­cyclohexyl­5­(pyridin­3­yl)­1,3,4­oxadiazol­2­amine n­cyclohexyl­5­(pyridin­3­yl)­1,3,4­oxadiazol­2­amine PRON eurjchem-65 74 39     SPACE eurjchem-65 74 40 ( ( PUNCT eurjchem-65 74 41 6b 6b NOUN eurjchem-65 74 42 ): ): PUNCT eurjchem-65 74 43     SPACE eurjchem-65 74 44 yield yield NOUN eurjchem-65 74 45 : : PUNCT eurjchem-65 74 46     SPACE eurjchem-65 74 47 65 65 NUM eurjchem-65 74 48 % % NOUN eurjchem-65 74 49 . . PUNCT eurjchem-65 74 50     SPACE eurjchem-65 75 1 m.p m.p AUX eurjchem-65 75 2 . . PROPN eurjchem-65 75 3 : : PUNCT eurjchem-65 75 4     SPACE eurjchem-65 75 5 160‐161 160‐161 NUM eurjchem-65 75 6     SPACE eurjchem-65 75 7 oc oc PROPN eurjchem-65 75 8 . . PUNCT eurjchem-65 75 9     SPACE eurjchem-65 75 10 ir ir VERB eurjchem-65 75 11     SPACE eurjchem-65 75 12 ( ( PUNCT eurjchem-65 75 13 kbr kbr PROPN eurjchem-65 75 14 , , PUNCT eurjchem-65 75 15     SPACE eurjchem-65 75 16 cm‐1 cm‐1 PROPN eurjchem-65 75 17 ): ): PUNCT eurjchem-65 75 18     SPACE eurjchem-65 75 19 3200 3200 NUM eurjchem-65 75 20     SPACE eurjchem-65 75 21 (nh (nh PROPN eurjchem-65 75 22 ) ) PUNCT eurjchem-65 75 23 , , PUNCT eurjchem-65 75 24     SPACE eurjchem-65 75 25 3010 3010 NUM eurjchem-65 75 26     SPACE eurjchem-65 75 27 (arom (arom PROPN eurjchem-65 75 28 . . PROPN eurjchem-65 75 29     SPACE eurjchem-65 75 30 ch ch NOUN eurjchem-65 75 31 ) ) PUNCT eurjchem-65 75 32 , , PUNCT eurjchem-65 75 33     SPACE eurjchem-65 75 34 2930 2930 NUM eurjchem-65 75 35 , , PUNCT eurjchem-65 75 36     SPACE eurjchem-65 75 37 2858 2858 NUM eurjchem-65 75 38     SPACE eurjchem-65 75 39 (aliph (aliph NOUN eurjchem-65 75 40 . . PUNCT eurjchem-65 75 41     SPACE eurjchem-65 75 42 c‐h c‐h PROPN eurjchem-65 75 43 ) ) PUNCT eurjchem-65 75 44 , , PUNCT eurjchem-65 75 45     SPACE eurjchem-65 75 46 1565 1565 NUM eurjchem-65 75 47     SPACE eurjchem-65 75 48 (c (c PROPN eurjchem-65 75 49 = = SYM eurjchem-65 75 50 n n CCONJ eurjchem-65 75 51     SPACE eurjchem-65 75 52 and and CCONJ eurjchem-65 75 53     SPACE eurjchem-65 75 54 c c NOUN eurjchem-65 75 55 = = NOUN eurjchem-65 75 56 c c NOUN eurjchem-65 75 57 ) ) PUNCT eurjchem-65 75 58 . . PUNCT eurjchem-65 75 59     SPACE eurjchem-65 75 60 1h 1h NUM eurjchem-65 75 61     SPACE eurjchem-65 75 62 nmr nmr NOUN eurjchem-65 75 63     SPACE eurjchem-65 75 64 ( ( PUNCT eurjchem-65 75 65 dmso‐d6 dmso‐d6 PROPN eurjchem-65 75 66 , , PUNCT eurjchem-65 75 67     SPACE eurjchem-65 75 68 δ δ PROPN eurjchem-65 75 69 , , PUNCT eurjchem-65 75 70     SPACE eurjchem-65 75 71 ppm ppm NOUN eurjchem-65 75 72 ): ): PUNCT eurjchem-65 75 73     SPACE eurjchem-65 75 74 1.12 1.12 NUM eurjchem-65 75 75     SPACE eurjchem-65 75 76 ( ( PUNCT eurjchem-65 75 77 d d PROPN eurjchem-65 75 78 , , PUNCT eurjchem-65 75 79     SPACE eurjchem-65 75 80 j j PROPN eurjchem-65 75 81     SPACE eurjchem-65 75 82 = = VERB eurjchem-65 75 83     SPACE eurjchem-65 75 84 12.2 12.2 NUM eurjchem-65 75 85     SPACE eurjchem-65 75 86 hz hz VERB eurjchem-65 75 87 , , PUNCT eurjchem-65 75 88     SPACE eurjchem-65 75 89 1h 1h NUM eurjchem-65 75 90 , , PUNCT eurjchem-65 75 91     SPACE eurjchem-65 75 92 haliph haliph NOUN eurjchem-65 75 93 ) ) PUNCT eurjchem-65 75 94 , , PUNCT eurjchem-65 75 95     SPACE eurjchem-65 75 96 1.31 1.31 NUM eurjchem-65 75 97     SPACE eurjchem-65 75 98 ( ( PUNCT eurjchem-65 75 99 q q NOUN eurjchem-65 75 100 , , PUNCT eurjchem-65 75 101     SPACE eurjchem-65 75 102 j j PROPN eurjchem-65 75 103     SPACE eurjchem-65 75 104 = = NOUN eurjchem-65 75 105     SPACE eurjchem-65 75 106 9.4 9.4 NUM eurjchem-65 75 107     SPACE eurjchem-65 75 108 hz hz VERB eurjchem-65 75 109 , , PUNCT eurjchem-65 75 110     SPACE eurjchem-65 75 111 4h 4h NOUN eurjchem-65 75 112 , , PUNCT eurjchem-65 75 113     SPACE eurjchem-65 75 114 haliph haliph NOUN eurjchem-65 75 115 ) ) PUNCT eurjchem-65 75 116 , , PUNCT eurjchem-65 75 117     SPACE eurjchem-65 75 118 1.58 1.58 NUM eurjchem-65 75 119     SPACE eurjchem-65 75 120 ( ( PUNCT eurjchem-65 75 121 d d PROPN eurjchem-65 75 122 , , PUNCT eurjchem-65 75 123     SPACE eurjchem-65 75 124 j j PROPN eurjchem-65 75 125     SPACE eurjchem-65 75 126 = = NOUN eurjchem-65 75 127     SPACE eurjchem-65 75 128 12.3 12.3 NUM eurjchem-65 75 129     SPACE eurjchem-65 75 130 hz hz VERB eurjchem-65 75 131 , , PUNCT eurjchem-65 75 132     SPACE eurjchem-65 75 133 1h 1h NUM eurjchem-65 75 134 , , PUNCT eurjchem-65 75 135     SPACE eurjchem-65 75 136 haliph haliph NOUN eurjchem-65 75 137 . . PUNCT eurjchem-65 75 138 ) ) PUNCT eurjchem-65 75 139 , , PUNCT eurjchem-65 75 140     SPACE eurjchem-65 75 141 1.74 1.74 NUM eurjchem-65 75 142     SPACE eurjchem-65 75 143 ( ( PUNCT eurjchem-65 75 144 q q NOUN eurjchem-65 75 145 , , PUNCT eurjchem-65 75 146     SPACE eurjchem-65 75 147 j j PROPN eurjchem-65 75 148     SPACE eurjchem-65 75 149 = = NOUN eurjchem-65 75 150     SPACE eurjchem-65 75 151 4.8 4.8 NUM eurjchem-65 75 152     SPACE eurjchem-65 75 153 hz hz VERB eurjchem-65 75 154 , , PUNCT eurjchem-65 75 155     SPACE eurjchem-65 75 156 2h 2h NUM eurjchem-65 75 157 , , PUNCT eurjchem-65 75 158     SPACE eurjchem-65 75 159 haliph haliph NOUN eurjchem-65 75 160 . . PUNCT eurjchem-65 75 161 ) ) PUNCT eurjchem-65 76 1 , , PUNCT eurjchem-65 76 2     SPACE eurjchem-65 76 3 1.97 1.97 NUM eurjchem-65 76 4     SPACE eurjchem-65 76 5 ( ( PUNCT eurjchem-65 76 6 d d PROPN eurjchem-65 76 7 , , PUNCT eurjchem-65 76 8     SPACE eurjchem-65 76 9 j j PROPN eurjchem-65 76 10     SPACE eurjchem-65 76 11 = = NOUN eurjchem-65 76 12     SPACE eurjchem-65 76 13 8.3 8.3 NUM eurjchem-65 76 14     SPACE eurjchem-65 76 15 hz hz VERB eurjchem-65 76 16 , , PUNCT eurjchem-65 76 17       SPACE eurjchem-65 76 18 2h 2h NUM eurjchem-65 76 19 , , PUNCT eurjchem-65 76 20     SPACE eurjchem-65 76 21 haliph haliph NOUN eurjchem-65 76 22 . . PUNCT eurjchem-65 76 23 ) ) PUNCT eurjchem-65 76 24 , , PUNCT eurjchem-65 76 25     SPACE eurjchem-65 76 26 3.43 3.43 NUM eurjchem-65 76 27     SPACE eurjchem-65 76 28 ( ( PUNCT eurjchem-65 76 29 br br PROPN eurjchem-65 76 30 , , PUNCT eurjchem-65 76 31     SPACE eurjchem-65 76 32 1h 1h NUM eurjchem-65 76 33 , , PUNCT eurjchem-65 76 34     SPACE eurjchem-65 76 35 ch‐n ch‐n PROPN eurjchem-65 76 36 ) ) PUNCT eurjchem-65 76 37 , , PUNCT eurjchem-65 76 38     SPACE eurjchem-65 76 39 7.57 7.57 NUM eurjchem-65 76 40     SPACE eurjchem-65 76 41 ( ( PUNCT eurjchem-65 76 42 d d PROPN eurjchem-65 76 43 , , PUNCT eurjchem-65 76 44     SPACE eurjchem-65 76 45 d d PROPN eurjchem-65 76 46 , , PUNCT eurjchem-65 76 47     SPACE eurjchem-65 76 48 j j PROPN eurjchem-65 76 49     SPACE eurjchem-65 76 50 = = NOUN eurjchem-65 76 51     SPACE eurjchem-65 76 52 4.8 4.8 NUM eurjchem-65 76 53 , , PUNCT eurjchem-65 76 54     SPACE eurjchem-65 76 55 7.9 7.9 NUM eurjchem-65 76 56     SPACE eurjchem-65 76 57 hz hz VERB eurjchem-65 76 58 , , PUNCT eurjchem-65 76 59     SPACE eurjchem-65 76 60 1h 1h NUM eurjchem-65 76 61 , , PUNCT eurjchem-65 76 62     SPACE eurjchem-65 76 63 ar‐h ar‐h NOUN eurjchem-65 76 64 ) ) PUNCT eurjchem-65 76 65 , , PUNCT eurjchem-65 76 66     SPACE eurjchem-65 76 67 7.88 7.88 NUM eurjchem-65 76 68     SPACE eurjchem-65 76 69 ( ( PUNCT eurjchem-65 76 70 d d PROPN eurjchem-65 76 71 , , PUNCT eurjchem-65 76 72     SPACE eurjchem-65 76 73 j j PROPN eurjchem-65 76 74     SPACE eurjchem-65 76 75 = = NOUN eurjchem-65 76 76     SPACE eurjchem-65 76 77 7.5 7.5 NUM eurjchem-65 76 78     SPACE eurjchem-65 76 79 hz,1h hz,1h NOUN eurjchem-65 76 80 , , PUNCT eurjchem-65 76 81     SPACE eurjchem-65 76 82 ar‐h ar‐h NOUN eurjchem-65 76 83 ) ) PUNCT eurjchem-65 76 84 , , PUNCT eurjchem-65 76 85     SPACE eurjchem-65 76 86 8.15 8.15 NUM eurjchem-65 76 87     SPACE eurjchem-65 76 88 ( ( PUNCT eurjchem-65 76 89 s s PROPN eurjchem-65 76 90 , , PUNCT eurjchem-65 76 91     SPACE eurjchem-65 76 92 1h 1h NUM eurjchem-65 76 93 , , PUNCT eurjchem-65 76 94     SPACE eurjchem-65 76 95 nh nh PROPN eurjchem-65 76 96 , , PUNCT eurjchem-65 76 97     SPACE eurjchem-65 76 98 d2o d2o NOUN eurjchem-65 76 99     SPACE eurjchem-65 76 100 exchange exchange NOUN eurjchem-65 76 101 ) ) PUNCT eurjchem-65 76 102 , , PUNCT eurjchem-65 76 103     SPACE eurjchem-65 76 104 8.69 8.69 NUM eurjchem-65 76 105     SPACE eurjchem-65 76 106 ( ( PUNCT eurjchem-65 76 107 d d PROPN eurjchem-65 76 108 , , PUNCT eurjchem-65 76 109     SPACE eurjchem-65 76 110 d d PROPN eurjchem-65 76 111 , , PUNCT eurjchem-65 76 112     SPACE eurjchem-65 76 113 j j PROPN eurjchem-65 76 114     SPACE eurjchem-65 77 1 = = NOUN eurjchem-65 77 2     SPACE eurjchem-65 77 3 4.9 4.9 NUM eurjchem-65 77 4 , , PUNCT eurjchem-65 77 5     SPACE eurjchem-65 77 6 1.1 1.1 NUM eurjchem-65 77 7     SPACE eurjchem-65 77 8 hz hz VERB eurjchem-65 77 9 , , PUNCT eurjchem-65 77 10     SPACE eurjchem-65 77 11 1h 1h NUM eurjchem-65 77 12 , , PUNCT eurjchem-65 77 13     SPACE eurjchem-65 77 14 ar‐h ar‐h NOUN eurjchem-65 77 15 ) ) PUNCT eurjchem-65 77 16 , , PUNCT eurjchem-65 77 17     SPACE eurjchem-65 77 18 8.98 8.98 NUM eurjchem-65 77 19     SPACE eurjchem-65 77 20 ( ( PUNCT eurjchem-65 77 21 d d PROPN eurjchem-65 77 22 , , PUNCT eurjchem-65 77 23     SPACE eurjchem-65 77 24 j j PROPN eurjchem-65 77 25     SPACE eurjchem-65 78 1 = = NOUN eurjchem-65 78 2     SPACE eurjchem-65 78 3 1.5 1.5 NUM eurjchem-65 78 4     SPACE eurjchem-65 78 5 hz hz VERB eurjchem-65 78 6 , , PUNCT eurjchem-65 78 7     SPACE eurjchem-65 78 8 1h 1h NUM eurjchem-65 78 9 , , PUNCT eurjchem-65 78 10     SPACE eurjchem-65 78 11 ar‐h ar‐h NOUN eurjchem-65 78 12 ) ) PUNCT eurjchem-65 78 13 . . PUNCT eurjchem-65 78 14     SPACE eurjchem-65 79 1 ms ms PROPN eurjchem-65 79 2     SPACE eurjchem-65 79 3 ( ( PUNCT eurjchem-65 79 4 ei ei PROPN eurjchem-65 79 5 , , PUNCT eurjchem-65 79 6     SPACE eurjchem-65 79 7 m m NOUN eurjchem-65 79 8 / / SYM eurjchem-65 79 9 z(% z(% NOUN eurjchem-65 79 10 ) ) PUNCT eurjchem-65 79 11 ): ): PUNCT eurjchem-65 79 12     SPACE eurjchem-65 79 13 244 244 NUM eurjchem-65 79 14     SPACE eurjchem-65 79 15 ( ( PUNCT eurjchem-65 79 16 m+ m+ NOUN eurjchem-65 79 17 ) ) PUNCT eurjchem-65 79 18 , , PUNCT eurjchem-65 79 19     SPACE eurjchem-65 79 20 162 162 NUM eurjchem-65 79 21     SPACE eurjchem-65 79 22 ( ( PUNCT eurjchem-65 79 23 base base NOUN eurjchem-65 79 24     SPACE eurjchem-65 79 25 peak peak NOUN eurjchem-65 79 26 ) ) PUNCT eurjchem-65 79 27 , , PUNCT eurjchem-65 79 28     SPACE eurjchem-65 79 29 119 119 NUM eurjchem-65 79 30 , , PUNCT eurjchem-65 79 31     SPACE eurjchem-65 79 32 78 78 NUM eurjchem-65 79 33 , , PUNCT eurjchem-65 79 34     SPACE eurjchem-65 79 35 55 55 NUM eurjchem-65 79 36 . . PUNCT eurjchem-65 79 37     SPACE eurjchem-65 79 38 n­cyclohexyl­5­(pyridin­4­yl)­1,3,4­oxadiazol­2­amine n­cyclohexyl­5­(pyridin­4­yl)­1,3,4­oxadiazol­2­amine PRON eurjchem-65 79 39     SPACE eurjchem-65 79 40 ( ( PUNCT eurjchem-65 79 41 6c 6c NOUN eurjchem-65 79 42 ): ): PUNCT eurjchem-65 79 43     SPACE eurjchem-65 79 44 yield yield NOUN eurjchem-65 79 45 : : PUNCT eurjchem-65 79 46     SPACE eurjchem-65 79 47 70 70 NUM eurjchem-65 79 48 % % NOUN eurjchem-65 79 49 . . PUNCT eurjchem-65 79 50     SPACE eurjchem-65 80 1 m.p m.p PROPN eurjchem-65 80 2 . . PROPN eurjchem-65 80 3 : : PUNCT eurjchem-65 80 4     SPACE eurjchem-65 80 5 231‐232 231‐232 NUM eurjchem-65 80 6     SPACE eurjchem-65 80 7 oc oc PROPN eurjchem-65 80 8 . . PUNCT eurjchem-65 80 9     SPACE eurjchem-65 80 10 ir ir VERB eurjchem-65 80 11     SPACE eurjchem-65 80 12 ( ( PUNCT eurjchem-65 80 13 kbr kbr PROPN eurjchem-65 80 14 , , PUNCT eurjchem-65 80 15     SPACE eurjchem-65 80 16 cm‐1 cm‐1 PROPN eurjchem-65 80 17 ): ): PUNCT eurjchem-65 80 18     SPACE eurjchem-65 80 19 3150 3150 NUM eurjchem-65 80 20     SPACE eurjchem-65 80 21 (nh (nh PROPN eurjchem-65 80 22 ) ) PUNCT eurjchem-65 80 23 , , PUNCT eurjchem-65 80 24     SPACE eurjchem-65 80 25 3040 3040 NUM eurjchem-65 80 26     SPACE eurjchem-65 80 27 (arom (arom PROPN eurjchem-65 80 28 . . PROPN eurjchem-65 80 29     SPACE eurjchem-65 80 30 ch ch NOUN eurjchem-65 80 31 ) ) PUNCT eurjchem-65 80 32 , , PUNCT eurjchem-65 80 33     SPACE eurjchem-65 80 34 2930 2930 NUM eurjchem-65 80 35 , , PUNCT eurjchem-65 80 36     SPACE eurjchem-65 80 37 2855 2855 NUM eurjchem-65 80 38     SPACE eurjchem-65 80 39 (aliph (aliph PROPN eurjchem-65 80 40 . . PUNCT eurjchem-65 80 41     SPACE eurjchem-65 80 42 c‐h c‐h PROPN eurjchem-65 80 43 ) ) PUNCT eurjchem-65 80 44 , , PUNCT eurjchem-65 80 45     SPACE eurjchem-65 80 46 1600 1600 NUM eurjchem-65 80 47     SPACE eurjchem-65 80 48 (c (c PROPN eurjchem-65 80 49 = = SYM eurjchem-65 80 50 n n CCONJ eurjchem-65 80 51     SPACE eurjchem-65 80 52 and and CCONJ eurjchem-65 80 53     SPACE eurjchem-65 80 54 c c NOUN eurjchem-65 80 55 = = NOUN eurjchem-65 80 56 c c NOUN eurjchem-65 80 57 ) ) PUNCT eurjchem-65 80 58 . . PUNCT eurjchem-65 80 59     SPACE eurjchem-65 80 60 1h 1h NUM eurjchem-65 80 61     SPACE eurjchem-65 80 62 nmr nmr NOUN eurjchem-65 80 63     SPACE eurjchem-65 80 64 ( ( PUNCT eurjchem-65 80 65 dmso‐d6 dmso‐d6 PROPN eurjchem-65 80 66 , , PUNCT eurjchem-65 80 67     SPACE eurjchem-65 80 68 δ δ PROPN eurjchem-65 80 69 , , PUNCT eurjchem-65 80 70     SPACE eurjchem-65 80 71 ppm ppm NOUN eurjchem-65 80 72 ): ): PUNCT eurjchem-65 80 73     SPACE eurjchem-65 80 74 1.18 1.18 NUM eurjchem-65 80 75     SPACE eurjchem-65 80 76 ( ( PUNCT eurjchem-65 80 77 d d PROPN eurjchem-65 80 78 , , PUNCT eurjchem-65 80 79     SPACE eurjchem-65 80 80 j j NOUN eurjchem-65 80 81     SPACE eurjchem-65 80 82 = = VERB eurjchem-65 80 83     SPACE eurjchem-65 80 84 12.1 12.1 NUM eurjchem-65 80 85     SPACE eurjchem-65 80 86 hz hz VERB eurjchem-65 80 87 , , PUNCT eurjchem-65 80 88     SPACE eurjchem-65 80 89 1h 1h NUM eurjchem-65 80 90 , , PUNCT eurjchem-65 80 91     SPACE eurjchem-65 80 92 haliph haliph NOUN eurjchem-65 80 93 ) ) PUNCT eurjchem-65 80 94 , , PUNCT eurjchem-65 80 95     SPACE eurjchem-65 80 96 1.32 1.32 NUM eurjchem-65 80 97     SPACE eurjchem-65 80 98 324 324 NUM eurjchem-65 80 99     SPACE eurjchem-65 80 100 ebrahimi ebrahimi NOUN eurjchem-65 80 101     SPACE eurjchem-65 80 102 / / SYM eurjchem-65 80 103     SPACE eurjchem-65 80 104 european european ADJ eurjchem-65 80 105     SPACE eurjchem-65 80 106 journal journal NOUN eurjchem-65 80 107     SPACE eurjchem-65 80 108 of of ADP eurjchem-65 80 109     SPACE eurjchem-65 80 110 chemistry chemistry NOUN eurjchem-65 80 111     SPACE eurjchem-65 80 112 1 1 NUM eurjchem-65 80 113     SPACE eurjchem-65 80 114 ( ( PUNCT eurjchem-65 80 115 4 4 NUM eurjchem-65 80 116 ) ) PUNCT eurjchem-65 80 117     SPACE eurjchem-65 80 118 ( ( PUNCT eurjchem-65 80 119 2010 2010 NUM eurjchem-65 80 120 ) ) PUNCT eurjchem-65 80 121     SPACE eurjchem-65 81 1 322­324 322­324 NUM eurjchem-65 81 2         SPACE eurjchem-65 81 3 ( ( PUNCT eurjchem-65 81 4 q q NOUN eurjchem-65 81 5 , , PUNCT eurjchem-65 81 6     SPACE eurjchem-65 81 7 j j PROPN eurjchem-65 81 8     SPACE eurjchem-65 81 9 = = NOUN eurjchem-65 81 10     SPACE eurjchem-65 81 11 8.7 8.7 NUM eurjchem-65 81 12     SPACE eurjchem-65 81 13 hz hz VERB eurjchem-65 81 14 , , PUNCT eurjchem-65 81 15     SPACE eurjchem-65 81 16 4h 4h NOUN eurjchem-65 81 17 , , PUNCT eurjchem-65 81 18     SPACE eurjchem-65 81 19 haliph haliph NOUN eurjchem-65 81 20 ) ) PUNCT eurjchem-65 81 21 , , PUNCT eurjchem-65 81 22     SPACE eurjchem-65 81 23 1.58 1.58 NUM eurjchem-65 81 24     SPACE eurjchem-65 81 25 ( ( PUNCT eurjchem-65 81 26 d d PROPN eurjchem-65 81 27 , , PUNCT eurjchem-65 81 28     SPACE eurjchem-65 81 29 j j PROPN eurjchem-65 81 30     SPACE eurjchem-65 81 31 = = VERB eurjchem-65 81 32     SPACE eurjchem-65 81 33 12.2 12.2 NUM eurjchem-65 81 34     SPACE eurjchem-65 81 35 hz hz VERB eurjchem-65 81 36 , , PUNCT eurjchem-65 81 37     SPACE eurjchem-65 81 38 1h 1h NUM eurjchem-65 81 39 , , PUNCT eurjchem-65 81 40     SPACE eurjchem-65 81 41 haliph haliph NOUN eurjchem-65 81 42 . . PUNCT eurjchem-65 81 43 ) ) PUNCT eurjchem-65 82 1 , , PUNCT eurjchem-65 82 2     SPACE eurjchem-65 82 3 1.73 1.73 NUM eurjchem-65 82 4     SPACE eurjchem-65 82 5 ( ( PUNCT eurjchem-65 82 6 q q ADJ eurjchem-65 82 7 , , PUNCT eurjchem-65 82 8     SPACE eurjchem-65 82 9 j= j= NOUN eurjchem-65 82 10     SPACE eurjchem-65 82 11 4.7 4.7 NUM eurjchem-65 82 12     SPACE eurjchem-65 82 13 hz hz VERB eurjchem-65 82 14 , , PUNCT eurjchem-65 82 15     SPACE eurjchem-65 82 16 2h 2h NUM eurjchem-65 82 17 , , PUNCT eurjchem-65 82 18     SPACE eurjchem-65 82 19 ar‐h ar‐h NOUN eurjchem-65 82 20 ) ) PUNCT eurjchem-65 82 21 , , PUNCT eurjchem-65 82 22     SPACE eurjchem-65 82 23 1.96 1.96 NUM eurjchem-65 82 24     SPACE eurjchem-65 82 25 ( ( PUNCT eurjchem-65 82 26 d d PROPN eurjchem-65 82 27 , , PUNCT eurjchem-65 82 28     SPACE eurjchem-65 82 29 j j PROPN eurjchem-65 82 30     SPACE eurjchem-65 82 31 = = NOUN eurjchem-65 82 32     SPACE eurjchem-65 82 33 8.0 8.0 NUM eurjchem-65 82 34     SPACE eurjchem-65 82 35 hz hz VERB eurjchem-65 82 36 , , PUNCT eurjchem-65 82 37       SPACE eurjchem-65 82 38 2h 2h NUM eurjchem-65 82 39 , , PUNCT eurjchem-65 82 40     SPACE eurjchem-65 82 41 ar‐h ar‐h NOUN eurjchem-65 82 42 ) ) PUNCT eurjchem-65 82 43 , , PUNCT eurjchem-65 82 44     SPACE eurjchem-65 82 45 3.46 3.46 NUM eurjchem-65 82 46     SPACE eurjchem-65 82 47 ( ( PUNCT eurjchem-65 82 48 br br PROPN eurjchem-65 82 49 , , PUNCT eurjchem-65 82 50     SPACE eurjchem-65 82 51 1h 1h NUM eurjchem-65 82 52 , , PUNCT eurjchem-65 82 53     SPACE eurjchem-65 82 54 ch‐n ch‐n PROPN eurjchem-65 82 55 ) ) PUNCT eurjchem-65 82 56 , , PUNCT eurjchem-65 82 57     SPACE eurjchem-65 82 58 7.72 7.72 NUM eurjchem-65 82 59     SPACE eurjchem-65 82 60 ( ( PUNCT eurjchem-65 82 61 d d PROPN eurjchem-65 82 62 , , PUNCT eurjchem-65 82 63     SPACE eurjchem-65 82 64 j j PROPN eurjchem-65 82 65     SPACE eurjchem-65 83 1 = = NOUN eurjchem-65 83 2     SPACE eurjchem-65 83 3 5.4 5.4 NUM eurjchem-65 83 4     SPACE eurjchem-65 83 5 hz hz VERB eurjchem-65 83 6 , , PUNCT eurjchem-65 83 7     SPACE eurjchem-65 83 8 2h 2h NUM eurjchem-65 83 9 , , PUNCT eurjchem-65 83 10     SPACE eurjchem-65 83 11 ar‐h ar‐h NOUN eurjchem-65 83 12 ) ) PUNCT eurjchem-65 83 13 , , PUNCT eurjchem-65 83 14     SPACE eurjchem-65 83 15 8.01 8.01 NUM eurjchem-65 83 16     SPACE eurjchem-65 83 17 ( ( PUNCT eurjchem-65 83 18 s s PROPN eurjchem-65 83 19 , , PUNCT eurjchem-65 83 20     SPACE eurjchem-65 83 21 1h 1h NUM eurjchem-65 83 22 , , PUNCT eurjchem-65 83 23     SPACE eurjchem-65 83 24 nh nh PROPN eurjchem-65 83 25 , , PUNCT eurjchem-65 83 26     SPACE eurjchem-65 83 27 d2o d2o NOUN eurjchem-65 83 28     SPACE eurjchem-65 83 29 exchange exchange NOUN eurjchem-65 83 30 ) ) PUNCT eurjchem-65 83 31 , , PUNCT eurjchem-65 83 32     SPACE eurjchem-65 83 33 8.73 8.73 NUM eurjchem-65 83 34     SPACE eurjchem-65 83 35 ( ( PUNCT eurjchem-65 83 36 d d PROPN eurjchem-65 83 37 , , PUNCT eurjchem-65 83 38     SPACE eurjchem-65 83 39 j j PROPN eurjchem-65 83 40     SPACE eurjchem-65 84 1 = = VERB eurjchem-65 84 2     SPACE eurjchem-65 84 3 5.4 5.4 NUM eurjchem-65 84 4     SPACE eurjchem-65 84 5 hz hz VERB eurjchem-65 84 6 , , PUNCT eurjchem-65 84 7     SPACE eurjchem-65 84 8 2h 2h NUM eurjchem-65 84 9 , , PUNCT eurjchem-65 84 10     SPACE eurjchem-65 84 11 ar‐h ar‐h NOUN eurjchem-65 84 12 ) ) PUNCT eurjchem-65 84 13 . . PUNCT eurjchem-65 84 14     SPACE eurjchem-65 85 1 ms ms PROPN eurjchem-65 85 2     SPACE eurjchem-65 85 3 ( ( PUNCT eurjchem-65 85 4 ei ei PROPN eurjchem-65 85 5 , , PUNCT eurjchem-65 85 6     SPACE eurjchem-65 85 7 m m NOUN eurjchem-65 85 8 / / SYM eurjchem-65 85 9 z(% z(% NOUN eurjchem-65 85 10 ) ) PUNCT eurjchem-65 85 11 ): ): PUNCT eurjchem-65 85 12     SPACE eurjchem-65 85 13 244 244 NUM eurjchem-65 85 14     SPACE eurjchem-65 85 15 ( ( PUNCT eurjchem-65 85 16 m+ m+ NOUN eurjchem-65 85 17 ) ) PUNCT eurjchem-65 85 18 , , PUNCT eurjchem-65 85 19     SPACE eurjchem-65 85 20 277 277 NUM eurjchem-65 85 21 , , PUNCT eurjchem-65 85 22     SPACE eurjchem-65 85 23 162 162 NUM eurjchem-65 85 24     SPACE eurjchem-65 85 25 ( ( PUNCT eurjchem-65 85 26 base base NOUN eurjchem-65 85 27     SPACE eurjchem-65 85 28 peak peak NOUN eurjchem-65 85 29 ) ) PUNCT eurjchem-65 85 30 , , PUNCT eurjchem-65 85 31     SPACE eurjchem-65 85 32 119 119 NUM eurjchem-65 85 33 , , PUNCT eurjchem-65 85 34     SPACE eurjchem-65 85 35 78 78 NUM eurjchem-65 85 36 , , PUNCT eurjchem-65 85 37     SPACE eurjchem-65 85 38 55 55 NUM eurjchem-65 85 39 , , PUNCT eurjchem-65 85 40     SPACE eurjchem-65 85 41 41 41 NUM eurjchem-65 85 42 . . PUNCT eurjchem-65 85 43         SPACE eurjchem-65 86 1 3 3 NUM eurjchem-65 86 2 . . PUNCT eurjchem-65 86 3     SPACE eurjchem-65 86 4 results result VERB eurjchem-65 86 5     SPACE eurjchem-65 86 6 and and CCONJ eurjchem-65 86 7     SPACE eurjchem-65 86 8 discussion discussion NOUN eurjchem-65 86 9           SPACE eurjchem-65 86 10 the the DET eurjchem-65 86 11     SPACE eurjchem-65 86 12 synthesis synthesis NOUN eurjchem-65 86 13     SPACE eurjchem-65 86 14 of of ADP eurjchem-65 86 15     SPACE eurjchem-65 86 16 all all DET eurjchem-65 86 17     SPACE eurjchem-65 86 18 the the DET eurjchem-65 86 19     SPACE eurjchem-65 86 20 intermediate intermediate ADJ eurjchem-65 86 21     SPACE eurjchem-65 86 22 and and CCONJ eurjchem-65 86 23     SPACE eurjchem-65 86 24 target target NOUN eurjchem-65 86 25     SPACE eurjchem-65 86 26 compounds compound NOUN eurjchem-65 86 27     SPACE eurjchem-65 86 28 were be AUX eurjchem-65 86 29     SPACE eurjchem-65 86 30 accomplished accomplish VERB eurjchem-65 86 31     SPACE eurjchem-65 86 32 by by ADP eurjchem-65 86 33     SPACE eurjchem-65 86 34 the the DET eurjchem-65 86 35     SPACE eurjchem-65 86 36 reaction reaction NOUN eurjchem-65 86 37     SPACE eurjchem-65 86 38 sequence sequence NOUN eurjchem-65 86 39     SPACE eurjchem-65 86 40 illustrated illustrate VERB eurjchem-65 86 41     SPACE eurjchem-65 86 42 in in ADP eurjchem-65 86 43     SPACE eurjchem-65 86 44 scheme scheme NOUN eurjchem-65 86 45     SPACE eurjchem-65 86 46 1 1 NUM eurjchem-65 86 47 . . PUNCT eurjchem-65 86 48     SPACE eurjchem-65 86 49 the the DET eurjchem-65 86 50     SPACE eurjchem-65 86 51 synthesis synthesis NOUN eurjchem-65 86 52     SPACE eurjchem-65 86 53 of of ADP eurjchem-65 86 54     SPACE eurjchem-65 86 55 new new ADJ eurjchem-65 86 56     SPACE eurjchem-65 86 57 1,3,4‐thiadiazole 1,3,4‐thiadiazole NUM eurjchem-65 86 58 , , PUNCT eurjchem-65 86 59     SPACE eurjchem-65 86 60 1,3,4‐ 1,3,4‐ NUM eurjchem-65 86 61 oxadiazole oxadiazole NOUN eurjchem-65 86 62     SPACE eurjchem-65 86 63 and and CCONJ eurjchem-65 86 64     SPACE eurjchem-65 86 65 1,2,4‐triazole 1,2,4‐triazole NOUN eurjchem-65 86 66     SPACE eurjchem-65 86 67 compounds compound NOUN eurjchem-65 86 68     SPACE eurjchem-65 86 69 was be AUX eurjchem-65 86 70     SPACE eurjchem-65 86 71 performed perform VERB eurjchem-65 86 72     SPACE eurjchem-65 86 73 in in ADP eurjchem-65 86 74     SPACE eurjchem-65 86 75 several several ADJ eurjchem-65 86 76     SPACE eurjchem-65 86 77 steps step NOUN eurjchem-65 86 78 . . PUNCT eurjchem-65 86 79     SPACE eurjchem-65 87 1 the the DET eurjchem-65 87 2     SPACE eurjchem-65 87 3 required require VERB eurjchem-65 87 4     SPACE eurjchem-65 87 5 isomeric isomeric ADJ eurjchem-65 87 6     SPACE eurjchem-65 87 7 pyridine pyridine NOUN eurjchem-65 87 8     SPACE eurjchem-65 87 9 carboxylic carboxylic NOUN eurjchem-65 87 10     SPACE eurjchem-65 87 11 acid acid NOUN eurjchem-65 87 12     SPACE eurjchem-65 87 13 hydrazides hydrazide NOUN eurjchem-65 87 14     SPACE eurjchem-65 87 15 1a­c 1a­c PROPN eurjchem-65 87 16     SPACE eurjchem-65 87 17 were be AUX eurjchem-65 87 18     SPACE eurjchem-65 87 19 prepared prepare VERB eurjchem-65 87 20     SPACE eurjchem-65 87 21 by by ADP eurjchem-65 87 22     SPACE eurjchem-65 87 23 treatment treatment NOUN eurjchem-65 87 24     SPACE eurjchem-65 87 25 of of ADP eurjchem-65 87 26     SPACE eurjchem-65 87 27 the the DET eurjchem-65 87 28     SPACE eurjchem-65 87 29 corresponding corresponding ADJ eurjchem-65 87 30     SPACE eurjchem-65 87 31 pyridine pyridine NOUN eurjchem-65 87 32     SPACE eurjchem-65 87 33 carboxylic carboxylic NOUN eurjchem-65 87 34     SPACE eurjchem-65 87 35 acid acid NOUN eurjchem-65 87 36     SPACE eurjchem-65 87 37 with with ADP eurjchem-65 87 38     SPACE eurjchem-65 87 39 hydrazine hydrazine NOUN eurjchem-65 87 40     SPACE eurjchem-65 87 41 hydrate hydrate NOUN eurjchem-65 87 42     SPACE eurjchem-65 87 43 according accord VERB eurjchem-65 87 44     SPACE eurjchem-65 87 45 the the DET eurjchem-65 87 46     SPACE eurjchem-65 87 47 reported report VERB eurjchem-65 87 48     SPACE eurjchem-65 87 49 procedure procedure NOUN eurjchem-65 87 50     SPACE eurjchem-65 88 1 [ [ X eurjchem-65 88 2 22 22 NUM eurjchem-65 88 3 ] ] PUNCT eurjchem-65 88 4 . . PUNCT eurjchem-65 88 5     SPACE eurjchem-65 89 1 the the DET eurjchem-65 89 2     SPACE eurjchem-65 89 3 thiosemicarbazides thiosemicarbazide NOUN eurjchem-65 89 4     SPACE eurjchem-65 89 5 3a­c 3a­c NOUN eurjchem-65 89 6     SPACE eurjchem-65 89 7 were be AUX eurjchem-65 89 8     SPACE eurjchem-65 89 9 prepared prepare VERB eurjchem-65 89 10     SPACE eurjchem-65 89 11 by by ADP eurjchem-65 89 12     SPACE eurjchem-65 89 13 the the DET eurjchem-65 89 14     SPACE eurjchem-65 89 15 reaction reaction NOUN eurjchem-65 89 16     SPACE eurjchem-65 89 17 of of ADP eurjchem-65 89 18     SPACE eurjchem-65 89 19 pyridine pyridine NOUN eurjchem-65 89 20     SPACE eurjchem-65 89 21 carboxylic carboxylic NOUN eurjchem-65 89 22     SPACE eurjchem-65 89 23 acid acid NOUN eurjchem-65 89 24     SPACE eurjchem-65 89 25 hydrazides hydrazide NOUN eurjchem-65 89 26     SPACE eurjchem-65 89 27 1a­c 1a­c PROPN eurjchem-65 89 28     SPACE eurjchem-65 89 29 and and CCONJ eurjchem-65 89 30     SPACE eurjchem-65 89 31 cyclohexyl cyclohexyl NOUN eurjchem-65 89 32     SPACE eurjchem-65 89 33 isothiocyanate isothiocyanate NOUN eurjchem-65 89 34     SPACE eurjchem-65 89 35 2 2 NUM eurjchem-65 89 36 . . PUNCT eurjchem-65 89 37     SPACE eurjchem-65 89 38 then then ADV eurjchem-65 89 39                                 SPACE eurjchem-65 89 40 4‐cyclohexyl‐5‐(pyridyl)‐4h‐1,2,4‐triazole‐3‐thiol 4‐cyclohexyl‐5‐(pyridyl)‐4h‐1,2,4‐triazole‐3‐thiol NUM eurjchem-65 89 41     SPACE eurjchem-65 89 42 4a­c 4a­c NOUN eurjchem-65 89 43     SPACE eurjchem-65 89 44 were be AUX eurjchem-65 89 45     SPACE eurjchem-65 89 46 prepared prepare VERB eurjchem-65 89 47     SPACE eurjchem-65 89 48 by by ADP eurjchem-65 89 49     SPACE eurjchem-65 89 50 the the DET eurjchem-65 89 51     SPACE eurjchem-65 89 52 reaction reaction NOUN eurjchem-65 89 53     SPACE eurjchem-65 89 54 of of ADP eurjchem-65 89 55     SPACE eurjchem-65 89 56 the the DET eurjchem-65 89 57     SPACE eurjchem-65 89 58 appropriate appropriate ADJ eurjchem-65 89 59     SPACE eurjchem-65 89 60 thiosemicarbazides thiosemicarbazide NOUN eurjchem-65 89 61     SPACE eurjchem-65 89 62 3a­c 3a­c NOUN eurjchem-65 89 63     SPACE eurjchem-65 89 64 and and CCONJ eurjchem-65 89 65     SPACE eurjchem-65 89 66 sodium sodium NOUN eurjchem-65 89 67     SPACE eurjchem-65 89 68 hydroxide hydroxide NOUN eurjchem-65 89 69     SPACE eurjchem-65 89 70 in in ADP eurjchem-65 89 71     SPACE eurjchem-65 89 72 ethanol ethanol NOUN eurjchem-65 89 73     SPACE eurjchem-65 89 74 for for ADP eurjchem-65 89 75     SPACE eurjchem-65 89 76 3 3 NUM eurjchem-65 89 77     SPACE eurjchem-65 89 78 hours hour NOUN eurjchem-65 89 79     SPACE eurjchem-65 89 80 under under ADP eurjchem-65 89 81     SPACE eurjchem-65 89 82 reflux reflux NOUN eurjchem-65 89 83 , , PUNCT eurjchem-65 89 84     SPACE eurjchem-65 89 85 followed follow VERB eurjchem-65 89 86     SPACE eurjchem-65 89 87 by by ADP eurjchem-65 89 88     SPACE eurjchem-65 89 89 acidification acidification NOUN eurjchem-65 89 90     SPACE eurjchem-65 89 91 with with ADP eurjchem-65 89 92     SPACE eurjchem-65 89 93 hydrochloric hydrochloric ADJ eurjchem-65 89 94     SPACE eurjchem-65 89 95 acid acid NOUN eurjchem-65 89 96 . . PUNCT eurjchem-65 89 97     SPACE eurjchem-65 90 1 the the DET eurjchem-65 90 2     SPACE eurjchem-65 90 3 substituted substitute VERB eurjchem-65 90 4     SPACE eurjchem-65 90 5 thiosemicarbazides thiosemicarbazide NOUN eurjchem-65 90 6     SPACE eurjchem-65 90 7 3a­c 3a­c NOUN eurjchem-65 90 8     SPACE eurjchem-65 90 9 in in ADP eurjchem-65 90 10     SPACE eurjchem-65 90 11 conc conc NOUN eurjchem-65 90 12 . . PUNCT eurjchem-65 90 13     SPACE eurjchem-65 90 14 sulfuric sulfuric ADJ eurjchem-65 90 15     SPACE eurjchem-65 90 16 acid acid NOUN eurjchem-65 90 17     SPACE eurjchem-65 90 18 underwent underwent NOUN eurjchem-65 90 19     SPACE eurjchem-65 90 20 intramolecular intramolecular ADJ eurjchem-65 90 21     SPACE eurjchem-65 90 22 dehydration dehydration NOUN eurjchem-65 90 23     SPACE eurjchem-65 90 24 to to PART eurjchem-65 90 25     SPACE eurjchem-65 90 26 form form VERB eurjchem-65 90 27     SPACE eurjchem-65 90 28 substituted substitute VERB eurjchem-65 90 29     SPACE eurjchem-65 90 30 1,3,4‐thiadiazoles 1,3,4‐thiadiazoles PROPN eurjchem-65 90 31     SPACE eurjchem-65 90 32 5a­c 5a­c NUM eurjchem-65 90 33 . . PUNCT eurjchem-65 90 34     SPACE eurjchem-65 90 35 1,3,4‐oxadiazole 1,3,4‐oxadiazole NUM eurjchem-65 90 36     SPACE eurjchem-65 90 37 6a­c 6a­c NOUN eurjchem-65 90 38     SPACE eurjchem-65 90 39 was be AUX eurjchem-65 90 40     SPACE eurjchem-65 90 41 synthesized synthesize VERB eurjchem-65 90 42     SPACE eurjchem-65 90 43 from from ADP eurjchem-65 90 44     SPACE eurjchem-65 90 45 corresponding corresponding ADJ eurjchem-65 90 46     SPACE eurjchem-65 90 47 thiosemacarbazide thiosemacarbazide NOUN eurjchem-65 90 48     SPACE eurjchem-65 90 49 in in ADP eurjchem-65 90 50     SPACE eurjchem-65 90 51 presence presence NOUN eurjchem-65 90 52     SPACE eurjchem-65 90 53 of of ADP eurjchem-65 90 54     SPACE eurjchem-65 90 55 mercuric mercuric NOUN eurjchem-65 90 56     SPACE eurjchem-65 90 57 acetate acetate NOUN eurjchem-65 90 58     SPACE eurjchem-65 90 59 as as ADP eurjchem-65 90 60     SPACE eurjchem-65 90 61 an an DET eurjchem-65 90 62     SPACE eurjchem-65 90 63 oxidizing oxidizing NOUN eurjchem-65 90 64     SPACE eurjchem-65 90 65 agent agent NOUN eurjchem-65 90 66 . . PUNCT eurjchem-65 90 67     SPACE eurjchem-65 91 1 the the DET eurjchem-65 91 2     SPACE eurjchem-65 91 3 ir ir PROPN eurjchem-65 91 4 , , PUNCT eurjchem-65 91 5     SPACE eurjchem-65 91 6 nmr nmr NOUN eurjchem-65 91 7     SPACE eurjchem-65 91 8 and and CCONJ eurjchem-65 91 9     SPACE eurjchem-65 91 10 mass mass PROPN eurjchem-65 91 11     SPACE eurjchem-65 91 12 spectra spectra PROPN eurjchem-65 91 13     SPACE eurjchem-65 91 14 data datum NOUN eurjchem-65 91 15     SPACE eurjchem-65 91 16 were be AUX eurjchem-65 91 17     SPACE eurjchem-65 91 18 used use VERB eurjchem-65 91 19     SPACE eurjchem-65 91 20 to to PART eurjchem-65 91 21     SPACE eurjchem-65 91 22 establish establish VERB eurjchem-65 91 23     SPACE eurjchem-65 91 24 the the DET eurjchem-65 91 25     SPACE eurjchem-65 91 26 structures structure NOUN eurjchem-65 91 27     SPACE eurjchem-65 91 28 of of ADP eurjchem-65 91 29     SPACE eurjchem-65 91 30 synthesized synthesize VERB eurjchem-65 91 31     SPACE eurjchem-65 91 32 compounds compound NOUN eurjchem-65 91 33 . . PUNCT eurjchem-65 91 34     SPACE eurjchem-65 91 35 1h 1h NUM eurjchem-65 91 36     SPACE eurjchem-65 91 37 nmr nmr NOUN eurjchem-65 91 38     SPACE eurjchem-65 91 39 spectra spectra NOUN eurjchem-65 91 40     SPACE eurjchem-65 91 41 of of ADP eurjchem-65 91 42     SPACE eurjchem-65 91 43 compounds compound NOUN eurjchem-65 91 44     SPACE eurjchem-65 91 45 4a­c 4a­c NOUN eurjchem-65 91 46     SPACE eurjchem-65 91 47 have have AUX eurjchem-65 91 48     SPACE eurjchem-65 91 49 shown show VERB eurjchem-65 91 50     SPACE eurjchem-65 91 51 a a DET eurjchem-65 91 52     SPACE eurjchem-65 91 53 singlet singlet NOUN eurjchem-65 91 54     SPACE eurjchem-65 91 55 signal signal NOUN eurjchem-65 91 56     SPACE eurjchem-65 91 57 at at ADP eurjchem-65 91 58     SPACE eurjchem-65 91 59 14 14 NUM eurjchem-65 91 60     SPACE eurjchem-65 91 61 ppm ppm NOUN eurjchem-65 91 62     SPACE eurjchem-65 91 63 due due ADJ eurjchem-65 91 64     SPACE eurjchem-65 91 65 to to ADP eurjchem-65 91 66     SPACE eurjchem-65 91 67 the the DET eurjchem-65 91 68     SPACE eurjchem-65 91 69 resonance resonance NOUN eurjchem-65 91 70     SPACE eurjchem-65 91 71 of of ADP eurjchem-65 91 72     SPACE eurjchem-65 91 73 sh sh PROPN eurjchem-65 91 74     SPACE eurjchem-65 91 75 proton proton NOUN eurjchem-65 91 76 . . PUNCT eurjchem-65 91 77         SPACE eurjchem-65 91 78 in in ADP eurjchem-65 91 79     SPACE eurjchem-65 91 80 the the DET eurjchem-65 91 81     SPACE eurjchem-65 91 82 ir ir PROPN eurjchem-65 91 83     SPACE eurjchem-65 91 84 spectra spectra NOUN eurjchem-65 91 85     SPACE eurjchem-65 91 86 of of ADP eurjchem-65 91 87     SPACE eurjchem-65 91 88 compounds compound NOUN eurjchem-65 91 89     SPACE eurjchem-65 91 90 4a­c 4a­c NUM eurjchem-65 91 91     SPACE eurjchem-65 91 92 the the DET eurjchem-65 91 93     SPACE eurjchem-65 91 94 absence absence NOUN eurjchem-65 91 95     SPACE eurjchem-65 91 96 of of ADP eurjchem-65 91 97     SPACE eurjchem-65 91 98 absorptions absorption NOUN eurjchem-65 91 99     SPACE eurjchem-65 91 100 due due ADJ eurjchem-65 91 101     SPACE eurjchem-65 91 102 to to ADP eurjchem-65 91 103     SPACE eurjchem-65 91 104 nh nh PROPN eurjchem-65 91 105     SPACE eurjchem-65 91 106 and and CCONJ eurjchem-65 91 107     SPACE eurjchem-65 91 108 carbonyl carbonyl NOUN eurjchem-65 91 109     SPACE eurjchem-65 91 110 groups group NOUN eurjchem-65 91 111     SPACE eurjchem-65 91 112 and and CCONJ eurjchem-65 91 113     SPACE eurjchem-65 91 114 the the DET eurjchem-65 91 115     SPACE eurjchem-65 91 116 appearance appearance NOUN eurjchem-65 91 117     SPACE eurjchem-65 91 118 of of ADP eurjchem-65 91 119     SPACE eurjchem-65 91 120 the the DET eurjchem-65 91 121     SPACE eurjchem-65 91 122 absorption absorption NOUN eurjchem-65 91 123     SPACE eurjchem-65 91 124 at at ADP eurjchem-65 91 125     SPACE eurjchem-65 91 126 2750 2750 NUM eurjchem-65 91 127     SPACE eurjchem-65 91 128 cm‐1 cm‐1 NOUN eurjchem-65 91 129     SPACE eurjchem-65 91 130 ( ( PUNCT eurjchem-65 91 131 sh sh PROPN eurjchem-65 91 132 ) ) PUNCT eurjchem-65 91 133 , , PUNCT eurjchem-65 91 134     SPACE eurjchem-65 91 135 established establish VERB eurjchem-65 91 136     SPACE eurjchem-65 91 137 their their PRON eurjchem-65 91 138     SPACE eurjchem-65 91 139 structures structure NOUN eurjchem-65 91 140 . . PUNCT eurjchem-65 91 141     SPACE eurjchem-65 91 142 similarly similarly ADV eurjchem-65 91 143     SPACE eurjchem-65 91 144 the the DET eurjchem-65 91 145     SPACE eurjchem-65 91 146 1h 1h NUM eurjchem-65 91 147     SPACE eurjchem-65 91 148 nmr nmr NOUN eurjchem-65 91 149     SPACE eurjchem-65 91 150 spectra spectra NOUN eurjchem-65 91 151     SPACE eurjchem-65 91 152 of of ADP eurjchem-65 91 153     SPACE eurjchem-65 91 154 the the DET eurjchem-65 91 155     SPACE eurjchem-65 91 156 compounds compound NOUN eurjchem-65 91 157     SPACE eurjchem-65 91 158 5a­c 5a­c NUM eurjchem-65 91 159     SPACE eurjchem-65 91 160 and and CCONJ eurjchem-65 91 161     SPACE eurjchem-65 91 162 6a­c 6a­c NOUN eurjchem-65 91 163     SPACE eurjchem-65 91 164 showed show VERB eurjchem-65 91 165     SPACE eurjchem-65 91 166 characteristic characteristic NOUN eurjchem-65 91 167     SPACE eurjchem-65 91 168 absorp‐ absorp‐ NOUN eurjchem-65 91 169 tion tion NOUN eurjchem-65 91 170     SPACE eurjchem-65 91 171 ( ( PUNCT eurjchem-65 91 172 singlet singlet NOUN eurjchem-65 91 173     SPACE eurjchem-65 91 174 at at ADP eurjchem-65 91 175     SPACE eurjchem-65 91 176 δ=8.0 δ=8.0 NOUN eurjchem-65 91 177 , , PUNCT eurjchem-65 91 178     SPACE eurjchem-65 91 179 d2o d2o NOUN eurjchem-65 91 180     SPACE eurjchem-65 91 181 exchange exchange NOUN eurjchem-65 91 182 ) ) PUNCT eurjchem-65 91 183     SPACE eurjchem-65 91 184 that that PRON eurjchem-65 91 185     SPACE eurjchem-65 91 186 was be AUX eurjchem-65 91 187     SPACE eurjchem-65 91 188 attributed attribute VERB eurjchem-65 91 189     SPACE eurjchem-65 91 190 to to ADP eurjchem-65 91 191     SPACE eurjchem-65 91 192 the the DET eurjchem-65 91 193     SPACE eurjchem-65 91 194 nh nh PROPN eurjchem-65 91 195     SPACE eurjchem-65 91 196 group group NOUN eurjchem-65 91 197 , , PUNCT eurjchem-65 91 198     SPACE eurjchem-65 91 199 is be AUX eurjchem-65 91 200     SPACE eurjchem-65 91 201 a a DET eurjchem-65 91 202     SPACE eurjchem-65 91 203 good good ADJ eurjchem-65 91 204     SPACE eurjchem-65 91 205 evidence evidence NOUN eurjchem-65 91 206     SPACE eurjchem-65 91 207 of of ADP eurjchem-65 91 208     SPACE eurjchem-65 91 209 the the DET eurjchem-65 91 210     SPACE eurjchem-65 91 211 expected expect VERB eurjchem-65 91 212     SPACE eurjchem-65 91 213 reactions reaction NOUN eurjchem-65 91 214 . . PUNCT eurjchem-65 91 215         SPACE eurjchem-65 92 1 4 4 NUM eurjchem-65 92 2 . . PUNCT eurjchem-65 92 3     SPACE eurjchem-65 92 4 conclusion conclusion NOUN eurjchem-65 92 5         SPACE eurjchem-65 92 6 a a DET eurjchem-65 92 7     SPACE eurjchem-65 92 8 series series NOUN eurjchem-65 92 9     SPACE eurjchem-65 92 10 of of ADP eurjchem-65 92 11     SPACE eurjchem-65 92 12 new new ADJ eurjchem-65 92 13     SPACE eurjchem-65 92 14 1,2,4‐triazoles 1,2,4‐triazoles NUM eurjchem-65 92 15     SPACE eurjchem-65 92 16 4a­c 4a­c NUM eurjchem-65 92 17 , , PUNCT eurjchem-65 92 18     SPACE eurjchem-65 92 19 1,3,4‐thiadiazoles 1,3,4‐thiadiazole NOUN eurjchem-65 92 20     SPACE eurjchem-65 92 21 5a­c 5a­c NUM eurjchem-65 92 22 , , PUNCT eurjchem-65 92 23       SPACE eurjchem-65 92 24 and and CCONJ eurjchem-65 92 25     SPACE eurjchem-65 92 26 1,3,4‐oxadiazoles 1,3,4‐oxadiazole NOUN eurjchem-65 92 27     SPACE eurjchem-65 92 28 6a­c 6a­c NOUN eurjchem-65 92 29 , , PUNCT eurjchem-65 92 30     SPACE eurjchem-65 92 31 were be AUX eurjchem-65 92 32     SPACE eurjchem-65 92 33 synthesized synthesize VERB eurjchem-65 92 34     SPACE eurjchem-65 92 35 by by ADP eurjchem-65 92 36     SPACE eurjchem-65 92 37 intramolecular intramolecular ADJ eurjchem-65 92 38     SPACE eurjchem-65 92 39 cyclization cyclization NOUN eurjchem-65 92 40     SPACE eurjchem-65 92 41 of of ADP eurjchem-65 92 42     SPACE eurjchem-65 92 43 1,4‐disubstituted 1,4‐disubstituted NUM eurjchem-65 92 44     SPACE eurjchem-65 92 45 thiosemicarbazides thiosemicarbazide NOUN eurjchem-65 92 46     SPACE eurjchem-65 92 47 in in ADP eurjchem-65 92 48     SPACE eurjchem-65 92 49 alkaline alkaline NOUN eurjchem-65 92 50 , , PUNCT eurjchem-65 92 51     SPACE eurjchem-65 92 52 acid acid NOUN eurjchem-65 92 53     SPACE eurjchem-65 92 54 and and CCONJ eurjchem-65 92 55     SPACE eurjchem-65 92 56 neutral neutral ADJ eurjchem-65 92 57     SPACE eurjchem-65 92 58 condition condition NOUN eurjchem-65 92 59 , , PUNCT eurjchem-65 92 60     SPACE eurjchem-65 92 61 respectively respectively ADV eurjchem-65 92 62 . . PUNCT eurjchem-65 92 63     SPACE eurjchem-65 92 64 in in ADP eurjchem-65 92 65     SPACE eurjchem-65 92 66 addition addition NOUN eurjchem-65 92 67     SPACE eurjchem-65 92 68 to to ADP eurjchem-65 92 69     SPACE eurjchem-65 92 70 the the DET eurjchem-65 92 71     SPACE eurjchem-65 92 72 efficiency efficiency NOUN eurjchem-65 92 73     SPACE eurjchem-65 92 74 and and CCONJ eurjchem-65 92 75     SPACE eurjchem-65 92 76 simplicity simplicity NOUN eurjchem-65 92 77     SPACE eurjchem-65 92 78 provided provide VERB eurjchem-65 92 79 , , PUNCT eurjchem-65 92 80     SPACE eurjchem-65 92 81 this this DET eurjchem-65 92 82     SPACE eurjchem-65 92 83 protocol protocol NOUN eurjchem-65 92 84     SPACE eurjchem-65 92 85 describes describe VERB eurjchem-65 92 86     SPACE eurjchem-65 92 87 good good ADJ eurjchem-65 92 88     SPACE eurjchem-65 92 89 yields yield NOUN eurjchem-65 92 90     SPACE eurjchem-65 92 91 of of ADP eurjchem-65 92 92     SPACE eurjchem-65 92 93 cyclization cyclization NOUN eurjchem-65 92 94     SPACE eurjchem-65 92 95 and and CCONJ eurjchem-65 92 96     SPACE eurjchem-65 92 97 simple simple ADJ eurjchem-65 92 98     SPACE eurjchem-65 92 99 purification purification NOUN eurjchem-65 92 100     SPACE eurjchem-65 92 101 for for ADP eurjchem-65 92 102     SPACE eurjchem-65 92 103 these these DET eurjchem-65 92 104     SPACE eurjchem-65 92 105 products product NOUN eurjchem-65 92 106 . . PUNCT eurjchem-65 92 107         SPACE eurjchem-65 93 1 acknowledgement acknowledgement NOUN eurjchem-65 93 2         SPACE eurjchem-65 93 3 we we PRON eurjchem-65 93 4     SPACE eurjchem-65 93 5 are be AUX eurjchem-65 93 6     SPACE eurjchem-65 93 7 thankful thankful ADJ eurjchem-65 93 8     SPACE eurjchem-65 93 9 to to ADP eurjchem-65 93 10     SPACE eurjchem-65 93 11 arak arak PROPN eurjchem-65 93 12     SPACE eurjchem-65 93 13 university university NOUN eurjchem-65 93 14     SPACE eurjchem-65 93 15 research research NOUN eurjchem-65 93 16     SPACE eurjchem-65 93 17 council council NOUN eurjchem-65 93 18     SPACE eurjchem-65 93 19 and and CCONJ eurjchem-65 93 20     SPACE eurjchem-65 93 21 islamic islamic ADJ eurjchem-65 93 22     SPACE eurjchem-65 93 23 azad azad PROPN eurjchem-65 93 24     SPACE eurjchem-65 93 25 university university NOUN eurjchem-65 93 26     SPACE eurjchem-65 93 27 branch branch NOUN eurjchem-65 93 28     SPACE eurjchem-65 93 29 malayer malayer NOUN eurjchem-65 93 30     SPACE eurjchem-65 93 31 for for ADP eurjchem-65 93 32     SPACE eurjchem-65 93 33 their their PRON eurjchem-65 93 34     SPACE eurjchem-65 93 35 financial financial ADJ eurjchem-65 93 36     SPACE eurjchem-65 93 37 support support NOUN eurjchem-65 93 38 . . PUNCT eurjchem-65 93 39         SPACE eurjchem-65 94 1 references reference NOUN eurjchem-65 94 2         SPACE eurjchem-65 94 3 [ [ X eurjchem-65 94 4 1 1 NUM eurjchem-65 94 5 ] ] PUNCT eurjchem-65 94 6 . . PUNCT eurjchem-65 95 1 suresh suresh PROPN eurjchem-65 95 2     SPACE eurjchem-65 95 3 kumar kumar PROPN eurjchem-65 95 4 , , PUNCT eurjchem-65 95 5     SPACE eurjchem-65 95 6 g. g. PROPN eurjchem-65 95 7     SPACE eurjchem-65 95 8 v. v. PROPN eurjchem-65 95 9 ; ; PUNCT eurjchem-65 95 10     SPACE eurjchem-65 95 11 rajendraprasad rajendraprasad ADJ eurjchem-65 95 12 , , PUNCT eurjchem-65 95 13     SPACE eurjchem-65 95 14 y. y. NOUN eurjchem-65 95 15 ; ; PUNCT eurjchem-65 95 16     SPACE eurjchem-65 95 17 mallikarjuna mallikarjuna PROPN eurjchem-65 95 18 , , PUNCT eurjchem-65 95 19     SPACE eurjchem-65 95 20 b. b. PROPN eurjchem-65 95 21     SPACE eurjchem-65 95 22 p. p. NOUN eurjchem-65 95 23 ; ; PUNCT eurjchem-65 95 24     SPACE eurjchem-65 95 25 chandrashekar chandrashekar NOUN eurjchem-65 95 26 , , PUNCT eurjchem-65 95 27     SPACE eurjchem-65 95 28 s. s. PROPN eurjchem-65 95 29     SPACE eurjchem-65 95 30 m. m. NOUN eurjchem-65 95 31 ; ; PUNCT eurjchem-65 95 32     SPACE eurjchem-65 95 33 kistayya kistayya PROPN eurjchem-65 95 34 , , PUNCT eurjchem-65 95 35     SPACE eurjchem-65 95 36 c. c. PROPN eurjchem-65 95 37     SPACE eurjchem-65 95 38 eur eur PROPN eurjchem-65 95 39 . . PUNCT eurjchem-65 95 40     SPACE eurjchem-65 95 41 j. j. PROPN eurjchem-65 95 42     SPACE eurjchem-65 95 43 med med PROPN eurjchem-65 95 44 . . PUNCT eurjchem-65 95 45     SPACE eurjchem-65 95 46 chem chem NOUN eurjchem-65 95 47 . . PUNCT eurjchem-65 95 48     SPACE eurjchem-65 96 1 2010 2010 NUM eurjchem-65 96 2 , , PUNCT eurjchem-65 96 3     SPACE eurjchem-65 96 4 45 45 NUM eurjchem-65 96 5 , , PUNCT eurjchem-65 96 6     SPACE eurjchem-65 96 7 2063‐ 2063‐ NUM eurjchem-65 96 8 2074 2074 NUM eurjchem-65 96 9 . . PUNCT eurjchem-65 96 10     SPACE eurjchem-65 97 1 [ [ X eurjchem-65 97 2 2 2 NUM eurjchem-65 97 3 ] ] PUNCT eurjchem-65 97 4 . . PUNCT eurjchem-65 98 1 mallikarjuna mallikarjuna PROPN eurjchem-65 98 2 , , PUNCT eurjchem-65 98 3     SPACE eurjchem-65 98 4 b. b. PROPN eurjchem-65 98 5     SPACE eurjchem-65 98 6 p. p. NOUN eurjchem-65 98 7 ; ; PUNCT eurjchem-65 98 8     SPACE eurjchem-65 98 9 sastry sastry NOUN eurjchem-65 98 10 , , PUNCT eurjchem-65 98 11     SPACE eurjchem-65 98 12 b. b. PROPN eurjchem-65 98 13     SPACE eurjchem-65 98 14 s. s. PROPN eurjchem-65 98 15 ; ; PUNCT eurjchem-65 98 16     SPACE eurjchem-65 98 17 suresh suresh PROPN eurjchem-65 98 18     SPACE eurjchem-65 98 19 kumar kumar PROPN eurjchem-65 98 20 , , PUNCT eurjchem-65 98 21     SPACE eurjchem-65 98 22 g. g. PROPN eurjchem-65 98 23     SPACE eurjchem-65 98 24 v. v. PROPN eurjchem-65 98 25 ; ; PUNCT eurjchem-65 98 26     SPACE eurjchem-65 98 27 rajendraprasad rajendraprasad ADJ eurjchem-65 98 28 , , PUNCT eurjchem-65 98 29     SPACE eurjchem-65 98 30 y. y. NOUN eurjchem-65 98 31 ; ; PUNCT eurjchem-65 98 32     SPACE eurjchem-65 98 33 chandrashekar chandrashekar NOUN eurjchem-65 98 34 , , PUNCT eurjchem-65 98 35     SPACE eurjchem-65 98 36 s. s. PROPN eurjchem-65 98 37     SPACE eurjchem-65 98 38 m. m. NOUN eurjchem-65 98 39 ; ; PUNCT eurjchem-65 98 40     SPACE eurjchem-65 98 41 sathisha sathisha NOUN eurjchem-65 98 42 , , PUNCT eurjchem-65 98 43     SPACE eurjchem-65 98 44 k. k. PROPN eurjchem-65 98 45     SPACE eurjchem-65 98 46 eur eur PROPN eurjchem-65 98 47 . . PUNCT eurjchem-65 98 48     SPACE eurjchem-65 98 49 j. j. PROPN eurjchem-65 98 50     SPACE eurjchem-65 98 51 med med PROPN eurjchem-65 98 52 . . PUNCT eurjchem-65 98 53     SPACE eurjchem-65 98 54 chem chem NOUN eurjchem-65 98 55 . . PUNCT eurjchem-65 98 56     SPACE eurjchem-65 98 57 2009 2009 NUM eurjchem-65 98 58 , , PUNCT eurjchem-65 98 59     SPACE eurjchem-65 98 60 44 44 NUM eurjchem-65 98 61 , , PUNCT eurjchem-65 98 62     SPACE eurjchem-65 98 63 4739‐4746 4739‐4746 NUM eurjchem-65 98 64 . . PUNCT eurjchem-65 98 65     SPACE eurjchem-65 99 1 [ [ X eurjchem-65 99 2 3 3 NUM eurjchem-65 99 3 ] ] PUNCT eurjchem-65 99 4 . . PUNCT eurjchem-65 100 1 onkol onkol PROPN eurjchem-65 100 2 , , PUNCT eurjchem-65 100 3     SPACE eurjchem-65 100 4 t. t. PROPN eurjchem-65 100 5 ; ; PUNCT eurjchem-65 100 6     SPACE eurjchem-65 100 7 cakir cakir NOUN eurjchem-65 100 8 , , PUNCT eurjchem-65 100 9     SPACE eurjchem-65 100 10 b. b. PROPN eurjchem-65 100 11 ; ; PUNCT eurjchem-65 100 12     SPACE eurjchem-65 100 13 sahin sahin PROPN eurjchem-65 100 14 , , PUNCT eurjchem-65 100 15     SPACE eurjchem-65 100 16 m. m. NOUN eurjchem-65 100 17     SPACE eurjchem-65 100 18 f. f. PROPN eurjchem-65 100 19     SPACE eurjchem-65 100 20 turk turk PROPN eurjchem-65 100 21 . . PUNCT eurjchem-65 100 22     SPACE eurjchem-65 101 1 j. j. PROPN eurjchem-65 101 2     SPACE eurjchem-65 101 3 chem chem NOUN eurjchem-65 101 4 . . PUNCT eurjchem-65 101 5     SPACE eurjchem-65 101 6 2004 2004 NUM eurjchem-65 101 7 , , PUNCT eurjchem-65 101 8     SPACE eurjchem-65 101 9 28 28 NUM eurjchem-65 101 10 , , PUNCT eurjchem-65 101 11     SPACE eurjchem-65 101 12 461‐466 461‐466 PROPN eurjchem-65 101 13 . . PUNCT eurjchem-65 101 14     SPACE eurjchem-65 102 1 [ [ X eurjchem-65 102 2 4 4 NUM eurjchem-65 102 3 ] ] PUNCT eurjchem-65 102 4 . . PUNCT eurjchem-65 103 1 schenone schenone PROPN eurjchem-65 103 2 , , PUNCT eurjchem-65 103 3     SPACE eurjchem-65 103 4 s. s. PROPN eurjchem-65 103 5 ; ; PUNCT eurjchem-65 103 6     SPACE eurjchem-65 103 7 bruno bruno PROPN eurjchem-65 103 8 , , PUNCT eurjchem-65 103 9     SPACE eurjchem-65 103 10 o. o. PROPN eurjchem-65 103 11 ; ; PUNCT eurjchem-65 103 12     SPACE eurjchem-65 103 13 ranise ranise NOUN eurjchem-65 103 14 , , PUNCT eurjchem-65 103 15     SPACE eurjchem-65 103 16 a. a. NOUN eurjchem-65 103 17 ; ; PUNCT eurjchem-65 103 18     SPACE eurjchem-65 103 19 bondavalli bondavalli PROPN eurjchem-65 103 20 , , PUNCT eurjchem-65 103 21     SPACE eurjchem-65 103 22 f. f. PROPN eurjchem-65 103 23 ; ; PUNCT eurjchem-65 103 24     SPACE eurjchem-65 103 25 filippeli filippeli ADV eurjchem-65 103 26 , , PUNCT eurjchem-65 103 27     SPACE eurjchem-65 103 28 w. w. PROPN eurjchem-65 103 29 ; ; PUNCT eurjchem-65 103 30     SPACE eurjchem-65 103 31 falcone falcone NOUN eurjchem-65 103 32 , , PUNCT eurjchem-65 103 33     SPACE eurjchem-65 103 34 g. g. NOUN eurjchem-65 103 35 ; ; PUNCT eurjchem-65 103 36     SPACE eurjchem-65 103 37 giordano giordano PROPN eurjchem-65 103 38 , , PUNCT eurjchem-65 103 39     SPACE eurjchem-65 103 40 l. l. PROPN eurjchem-65 103 41 ; ; PUNCT eurjchem-65 103 42     SPACE eurjchem-65 103 43 vitelli vitelli PROPN eurjchem-65 103 44 , , PUNCT eurjchem-65 103 45     SPACE eurjchem-65 103 46 m. m. NOUN eurjchem-65 103 47     SPACE eurjchem-65 103 48 r. r. PROPN eurjchem-65 103 49     SPACE eurjchem-65 103 50 bioorg bioorg PROPN eurjchem-65 103 51 . . PUNCT eurjchem-65 103 52     SPACE eurjchem-65 104 1 med med PROPN eurjchem-65 104 2 . . PUNCT eurjchem-65 104 3     SPACE eurjchem-65 104 4 chem chem NOUN eurjchem-65 104 5 . . PUNCT eurjchem-65 104 6     SPACE eurjchem-65 104 7 2001 2001 NUM eurjchem-65 104 8 , , PUNCT eurjchem-65 104 9     SPACE eurjchem-65 104 10 9 9 NUM eurjchem-65 104 11 , , PUNCT eurjchem-65 104 12     SPACE eurjchem-65 104 13 2149‐2153 2149‐2153 NUM eurjchem-65 104 14 . . PUNCT eurjchem-65 104 15     SPACE eurjchem-65 105 1 [ [ X eurjchem-65 105 2 5 5 NUM eurjchem-65 105 3 ] ] PUNCT eurjchem-65 105 4 . . PUNCT eurjchem-65 105 5 holla holla PROPN eurjchem-65 105 6 , , PUNCT eurjchem-65 105 7     SPACE eurjchem-65 105 8 b. b. PROPN eurjchem-65 105 9     SPACE eurjchem-65 105 10 s. s. PROPN eurjchem-65 105 11 ; ; PUNCT eurjchem-65 105 12     SPACE eurjchem-65 105 13 gonsalves gonsalve NOUN eurjchem-65 105 14 , , PUNCT eurjchem-65 105 15     SPACE eurjchem-65 105 16 r. r. PROPN eurjchem-65 105 17 ; ; PUNCT eurjchem-65 105 18     SPACE eurjchem-65 105 19 shenoy shenoy NOUN eurjchem-65 105 20 , , PUNCT eurjchem-65 105 21     SPACE eurjchem-65 105 22 s. s. PROPN eurjchem-65 105 23     SPACE eurjchem-65 105 24 eur eur PROPN eurjchem-65 105 25 . . PUNCT eurjchem-65 105 26     SPACE eurjchem-65 105 27 j. j. PROPN eurjchem-65 105 28     SPACE eurjchem-65 105 29 med med PROPN eurjchem-65 105 30 . . PUNCT eurjchem-65 105 31     SPACE eurjchem-65 105 32 chem chem NOUN eurjchem-65 105 33 . . PUNCT eurjchem-65 105 34     SPACE eurjchem-65 105 35 2000 2000 NUM eurjchem-65 105 36 , , PUNCT eurjchem-65 105 37     SPACE eurjchem-65 105 38 35 35 NUM eurjchem-65 105 39 , , PUNCT eurjchem-65 105 40     SPACE eurjchem-65 105 41 267 267 NUM eurjchem-65 105 42 – – PUNCT eurjchem-65 105 43     SPACE eurjchem-65 105 44 271 271 NUM eurjchem-65 105 45 . . PUNCT eurjchem-65 105 46     SPACE eurjchem-65 106 1 [ [ X eurjchem-65 106 2 6 6 NUM eurjchem-65 106 3 ] ] PUNCT eurjchem-65 106 4 . . PUNCT eurjchem-65 106 5 gokce gokce PROPN eurjchem-65 106 6 . . PUNCT eurjchem-65 106 7     SPACE eurjchem-65 106 8 m. m. NOUN eurjchem-65 106 9 ; ; PUNCT eurjchem-65 106 10     SPACE eurjchem-65 106 11 cakir cakir NOUN eurjchem-65 106 12 , , PUNCT eurjchem-65 106 13     SPACE eurjchem-65 106 14 b. b. PROPN eurjchem-65 106 15 ; ; PUNCT eurjchem-65 106 16     SPACE eurjchem-65 106 17 erol erol NOUN eurjchem-65 106 18 , , PUNCT eurjchem-65 106 19     SPACE eurjchem-65 106 20 k. k. PROPN eurjchem-65 106 21 ; ; PUNCT eurjchem-65 106 22     SPACE eurjchem-65 106 23 sahin sahin PROPN eurjchem-65 106 24 , , PUNCT eurjchem-65 106 25     SPACE eurjchem-65 106 26 m. m. NOUN eurjchem-65 106 27     SPACE eurjchem-65 106 28 f. f. PROPN eurjchem-65 106 29     SPACE eurjchem-65 106 30 arch arch NOUN eurjchem-65 106 31 . . PUNCT eurjchem-65 106 32     SPACE eurjchem-65 107 1 pharm pharm PROPN eurjchem-65 107 2 . . PUNCT eurjchem-65 107 3     SPACE eurjchem-65 108 1 2001 2001 NUM eurjchem-65 108 2 , , PUNCT eurjchem-65 108 3     SPACE eurjchem-65 108 4 334 334 NUM eurjchem-65 108 5 , , PUNCT eurjchem-65 108 6     SPACE eurjchem-65 108 7 279‐ 279‐ NUM eurjchem-65 108 8 283 283 NUM eurjchem-65 108 9 . . PUNCT eurjchem-65 108 10     SPACE eurjchem-65 109 1 [ [ X eurjchem-65 109 2 7 7 NUM eurjchem-65 109 3 ] ] PUNCT eurjchem-65 109 4 . . PUNCT eurjchem-65 110 1 laddi laddi NOUN eurjchem-65 110 2 , , PUNCT eurjchem-65 110 3     SPACE eurjchem-65 110 4 u. u. NOUN eurjchem-65 110 5     SPACE eurjchem-65 110 6 v. v. PROPN eurjchem-65 110 7 ; ; PUNCT eurjchem-65 110 8     SPACE eurjchem-65 110 9 desai desai PROPN eurjchem-65 110 10 , , PUNCT eurjchem-65 110 11     SPACE eurjchem-65 110 12 s. s. PROPN eurjchem-65 110 13     SPACE eurjchem-65 110 14 r. r. PROPN eurjchem-65 110 15 ; ; PUNCT eurjchem-65 110 16     SPACE eurjchem-65 110 17 bennur bennur NOUN eurjchem-65 110 18 , , PUNCT eurjchem-65 110 19     SPACE eurjchem-65 110 20 r. r. PROPN eurjchem-65 110 21     SPACE eurjchem-65 110 22 s. s. PROPN eurjchem-65 110 23 ; ; PUNCT eurjchem-65 110 24     SPACE eurjchem-65 110 25 bennur bennur NOUN eurjchem-65 110 26 , , PUNCT eurjchem-65 110 27     SPACE eurjchem-65 110 28 s. s. PROPN eurjchem-65 110 29     SPACE eurjchem-65 110 30 c. c. PROPN eurjchem-65 110 31     SPACE eurjchem-65 110 32 ind ind PROPN eurjchem-65 110 33 . . PUNCT eurjchem-65 110 34     SPACE eurjchem-65 110 35 j. j. PROPN eurjchem-65 110 36     SPACE eurjchem-65 110 37 heterocycl heterocycl PROPN eurjchem-65 110 38 . . PUNCT eurjchem-65 110 39     SPACE eurjchem-65 110 40 chem chem NOUN eurjchem-65 110 41 . . PUNCT eurjchem-65 110 42     SPACE eurjchem-65 110 43 2002 2002 NUM eurjchem-65 110 44 , , PUNCT eurjchem-65 110 45     SPACE eurjchem-65 110 46 11 11 NUM eurjchem-65 110 47 , , PUNCT eurjchem-65 110 48     SPACE eurjchem-65 110 49 319–322 319–322 NUM eurjchem-65 110 50 . . PUNCT eurjchem-65 110 51       SPACE eurjchem-65 111 1 [ [ X eurjchem-65 111 2 8 8 NUM eurjchem-65 111 3 ] ] PUNCT eurjchem-65 111 4 . . PUNCT eurjchem-65 112 1 sahin sahin PROPN eurjchem-65 112 2 , , PUNCT eurjchem-65 112 3     SPACE eurjchem-65 112 4 g. g. NOUN eurjchem-65 112 5 ; ; PUNCT eurjchem-65 112 6     SPACE eurjchem-65 112 7 palaska palaska NOUN eurjchem-65 112 8 , , PUNCT eurjchem-65 112 9     SPACE eurjchem-65 112 10 e. e. PROPN eurjchem-65 112 11 ; ; PUNCT eurjchem-65 112 12     SPACE eurjchem-65 112 13 melike melike NOUN eurjchem-65 112 14     SPACE eurjchem-65 112 15 ekizoglu ekizoglu PROPN eurjchem-65 112 16 , , PUNCT eurjchem-65 112 17     SPACE eurjchem-65 112 18 o. o. PROPN eurjchem-65 112 19     SPACE eurjchem-65 112 20 m. m. NOUN eurjchem-65 112 21     SPACE eurjchem-65 112 22 il il PROPN eurjchem-65 112 23     SPACE eurjchem-65 112 24 farmaco farmaco PROPN eurjchem-65 112 25     SPACE eurjchem-65 112 26 2002 2002 NUM eurjchem-65 112 27 , , PUNCT eurjchem-65 112 28     SPACE eurjchem-65 112 29 57 57 NUM eurjchem-65 112 30 , , PUNCT eurjchem-65 112 31     SPACE eurjchem-65 112 32 539 539 NUM eurjchem-65 112 33 – – PUNCT eurjchem-65 112 34 545 545 NUM eurjchem-65 112 35 . . PUNCT eurjchem-65 112 36     SPACE eurjchem-65 113 1 [ [ X eurjchem-65 113 2 9 9 NUM eurjchem-65 113 3 ] ] PUNCT eurjchem-65 113 4 . . PUNCT eurjchem-65 114 1 li li PROPN eurjchem-65 114 2 , , PUNCT eurjchem-65 114 3     SPACE eurjchem-65 114 4 z. z. PROPN eurjchem-65 114 5 ; ; PUNCT eurjchem-65 114 6     SPACE eurjchem-65 114 7 gu gu NOUN eurjchem-65 114 8 , , PUNCT eurjchem-65 114 9     SPACE eurjchem-65 114 10 z. z. PROPN eurjchem-65 114 11 ; ; PUNCT eurjchem-65 114 12     SPACE eurjchem-65 114 13 yin yin NOUN eurjchem-65 114 14 , , PUNCT eurjchem-65 114 15     SPACE eurjchem-65 114 16 k. k. PROPN eurjchem-65 114 17 ; ; PUNCT eurjchem-65 114 18     SPACE eurjchem-65 114 19 zhang zhang PROPN eurjchem-65 114 20 , , PUNCT eurjchem-65 114 21     SPACE eurjchem-65 114 22 r. r. PROPN eurjchem-65 114 23 ; ; PUNCT eurjchem-65 114 24     SPACE eurjchem-65 114 25 deng deng PROPN eurjchem-65 114 26 , , PUNCT eurjchem-65 114 27     SPACE eurjchem-65 114 28 q. q. PROPN eurjchem-65 114 29 ; ; PUNCT eurjchem-65 114 30     SPACE eurjchem-65 114 31 xiang xiang PROPN eurjchem-65 114 32 , , PUNCT eurjchem-65 114 33     SPACE eurjchem-65 114 34 j. j. PROPN eurjchem-65 114 35     SPACE eurjchem-65 114 36 eur eur PROPN eurjchem-65 114 37 . . PUNCT eurjchem-65 114 38     SPACE eurjchem-65 114 39 j. j. PROPN eurjchem-65 114 40     SPACE eurjchem-65 114 41 med med PROPN eurjchem-65 114 42 . . PUNCT eurjchem-65 114 43     SPACE eurjchem-65 114 44 chem chem NOUN eurjchem-65 114 45 . . PUNCT eurjchem-65 114 46     SPACE eurjchem-65 114 47 2009 2009 NUM eurjchem-65 114 48 , , PUNCT eurjchem-65 114 49     SPACE eurjchem-65 114 50 44 44 NUM eurjchem-65 114 51 , , PUNCT eurjchem-65 114 52     SPACE eurjchem-65 114 53 4716‐4720 4716‐4720 NOUN eurjchem-65 114 54 . . PUNCT eurjchem-65 114 55     SPACE eurjchem-65 115 1 [ [ X eurjchem-65 115 2 10 10 NUM eurjchem-65 115 3 ] ] PUNCT eurjchem-65 115 4 . . PUNCT eurjchem-65 116 1 ali ali PROPN eurjchem-65 116 2 , , PUNCT eurjchem-65 116 3     SPACE eurjchem-65 116 4 t. t. PROPN eurjchem-65 116 5     SPACE eurjchem-65 116 6 a. a. NOUN eurjchem-65 116 7 ; ; PUNCT eurjchem-65 116 8     SPACE eurjchem-65 116 9 el‐kazak el‐kazak NOUN eurjchem-65 116 10 , , PUNCT eurjchem-65 116 11     SPACE eurjchem-65 116 12 a. a. NOUN eurjchem-65 116 13     SPACE eurjchem-65 116 14 m. m. NOUN eurjchem-65 116 15     SPACE eurjchem-65 116 16 eur eur PROPN eurjchem-65 116 17 . . PUNCT eurjchem-65 116 18     SPACE eurjchem-65 116 19 j. j. PROPN eurjchem-65 116 20     SPACE eurjchem-65 116 21 chem chem NOUN eurjchem-65 116 22 . . PUNCT eurjchem-65 116 23     SPACE eurjchem-65 116 24 2010 2010 NUM eurjchem-65 116 25 , , PUNCT eurjchem-65 116 26     SPACE eurjchem-65 116 27 1(1 1(1 NUM eurjchem-65 116 28 ) ) PUNCT eurjchem-65 116 29 , , PUNCT eurjchem-65 116 30     SPACE eurjchem-65 116 31 6‐11 6‐11 NUM eurjchem-65 116 32 . . PUNCT eurjchem-65 116 33     SPACE eurjchem-65 117 1 [ [ X eurjchem-65 117 2 11 11 NUM eurjchem-65 117 3 ] ] PUNCT eurjchem-65 117 4 . . PUNCT eurjchem-65 118 1 rollas rolla NOUN eurjchem-65 118 2 , , PUNCT eurjchem-65 118 3     SPACE eurjchem-65 118 4 s. s. PROPN eurjchem-65 118 5 ; ; PUNCT eurjchem-65 118 6     SPACE eurjchem-65 118 7 kalyoncuoğlu kalyoncuoğlu NOUN eurjchem-65 118 8 , , PUNCT eurjchem-65 118 9     SPACE eurjchem-65 118 10 n. n. NOUN eurjchem-65 118 11 ; ; PUNCT eurjchem-65 118 12     SPACE eurjchem-65 118 13 sür‐altiner sür‐altiner NUM eurjchem-65 118 14 , , PUNCT eurjchem-65 118 15     SPACE eurjchem-65 118 16 d. d. PROPN eurjchem-65 118 17 ; ; PUNCT eurjchem-65 118 18     SPACE eurjchem-65 118 19 yegenoğlu yegenoğlu NOUN eurjchem-65 118 20 , , PUNCT eurjchem-65 118 21     SPACE eurjchem-65 118 22 y. y. NOUN eurjchem-65 118 23     SPACE eurjchem-65 118 24 pharmazie pharmazie PROPN eurjchem-65 118 25     SPACE eurjchem-65 118 26 1993 1993 NUM eurjchem-65 118 27 , , PUNCT eurjchem-65 118 28     SPACE eurjchem-65 118 29 48 48 NUM eurjchem-65 118 30 , , PUNCT eurjchem-65 118 31     SPACE eurjchem-65 118 32 308‐309 308‐309 NOUN eurjchem-65 118 33 . . PUNCT eurjchem-65 118 34     SPACE eurjchem-65 119 1 [ [ X eurjchem-65 119 2 12 12 NUM eurjchem-65 119 3 ] ] PUNCT eurjchem-65 119 4 . . PUNCT eurjchem-65 119 5 holla holla PROPN eurjchem-65 119 6 , , PUNCT eurjchem-65 119 7     SPACE eurjchem-65 119 8 b. b. PROPN eurjchem-65 119 9     SPACE eurjchem-65 119 10 s. s. PROPN eurjchem-65 119 11 ; ; PUNCT eurjchem-65 119 12     SPACE eurjchem-65 119 13 rao rao PROPN eurjchem-65 119 14 , , PUNCT eurjchem-65 119 15     SPACE eurjchem-65 119 16 b. b. PROPN eurjchem-65 119 17     SPACE eurjchem-65 119 18 s. s. PROPN eurjchem-65 119 19 ; ; PUNCT eurjchem-65 119 20     SPACE eurjchem-65 119 21 sarojini sarojini NOUN eurjchem-65 119 22 , , PUNCT eurjchem-65 119 23     SPACE eurjchem-65 119 24 b. b. PROPN eurjchem-65 119 25     SPACE eurjchem-65 119 26 k. k. PROPN eurjchem-65 119 27 ; ; PUNCT eurjchem-65 119 28     SPACE eurjchem-65 119 29 akberali akberali VERB eurjchem-65 119 30 , , PUNCT eurjchem-65 119 31     SPACE eurjchem-65 119 32 p. p. NOUN eurjchem-65 119 33     SPACE eurjchem-65 119 34 m. m. NOUN eurjchem-65 119 35     SPACE eurjchem-65 119 36 eur eur PROPN eurjchem-65 119 37 . . PUNCT eurjchem-65 119 38     SPACE eurjchem-65 119 39 j. j. PROPN eurjchem-65 119 40     SPACE eurjchem-65 119 41 med med PROPN eurjchem-65 119 42 . . PUNCT eurjchem-65 119 43     SPACE eurjchem-65 119 44 chem chem NOUN eurjchem-65 119 45 . . PUNCT eurjchem-65 119 46     SPACE eurjchem-65 120 1 2004 2004 NUM eurjchem-65 120 2 , , PUNCT eurjchem-65 120 3     SPACE eurjchem-65 120 4 39 39 NUM eurjchem-65 120 5 , , PUNCT eurjchem-65 120 6     SPACE eurjchem-65 120 7 777‐783 777‐783 NOUN eurjchem-65 120 8 . . PUNCT eurjchem-65 120 9     SPACE eurjchem-65 121 1 [ [ X eurjchem-65 121 2 13 13 NUM eurjchem-65 121 3 ] ] PUNCT eurjchem-65 121 4 . . PUNCT eurjchem-65 122 1 duran duran PROPN eurjchem-65 122 2 , , PUNCT eurjchem-65 122 3     SPACE eurjchem-65 122 4 a. a. NOUN eurjchem-65 122 5 ; ; PUNCT eurjchem-65 122 6     SPACE eurjchem-65 122 7 dogan dogan PROPN eurjchem-65 122 8 , , PUNCT eurjchem-65 122 9     SPACE eurjchem-65 122 10 h. h. PROPN eurjchem-65 122 11     SPACE eurjchem-65 122 12 n. n. PROPN eurjchem-65 122 13 ; ; PUNCT eurjchem-65 122 14     SPACE eurjchem-65 122 15 rollas rolla NOUN eurjchem-65 122 16     SPACE eurjchem-65 122 17 s. s. PROPN eurjchem-65 122 18 ; ; PUNCT eurjchem-65 122 19     SPACE eurjchem-65 122 20 farmaco farmaco PROPN eurjchem-65 122 21     SPACE eurjchem-65 122 22 2002 2002 NUM eurjchem-65 122 23 , , PUNCT eurjchem-65 122 24     SPACE eurjchem-65 122 25 57 57 NUM eurjchem-65 122 26 , , PUNCT eurjchem-65 122 27     SPACE eurjchem-65 122 28 559‐564 559‐564 NUM eurjchem-65 122 29 . . PUNCT eurjchem-65 122 30     SPACE eurjchem-65 123 1 [ [ X eurjchem-65 123 2 14 14 NUM eurjchem-65 123 3 ] ] PUNCT eurjchem-65 123 4 . . PUNCT eurjchem-65 124 1 sadana sadana PROPN eurjchem-65 124 2 , , PUNCT eurjchem-65 124 3     SPACE eurjchem-65 124 4 a. a. NOUN eurjchem-65 124 5     SPACE eurjchem-65 124 6 k. k. PROPN eurjchem-65 124 7 ; ; PUNCT eurjchem-65 124 8     SPACE eurjchem-65 124 9 mirza mirza PROPN eurjchem-65 124 10 , , PUNCT eurjchem-65 124 11     SPACE eurjchem-65 124 12 y. y. NOUN eurjchem-65 124 13 ; ; PUNCT eurjchem-65 124 14     SPACE eurjchem-65 124 15 aneja aneja VERB eurjchem-65 124 16 , , PUNCT eurjchem-65 124 17     SPACE eurjchem-65 124 18 k. k. PROPN eurjchem-65 124 19     SPACE eurjchem-65 124 20 r. r. PROPN eurjchem-65 124 21 ; ; PUNCT eurjchem-65 124 22     SPACE eurjchem-65 124 23 prakash prakash PROPN eurjchem-65 124 24 , , PUNCT eurjchem-65 124 25     SPACE eurjchem-65 124 26 o. o. PROPN eurjchem-65 124 27     SPACE eurjchem-65 124 28 eur eur PROPN eurjchem-65 124 29 . . PUNCT eurjchem-65 124 30     SPACE eurjchem-65 124 31 j. j. PROPN eurjchem-65 124 32     SPACE eurjchem-65 124 33 med med PROPN eurjchem-65 124 34 . . PUNCT eurjchem-65 124 35     SPACE eurjchem-65 124 36 chem chem NOUN eurjchem-65 124 37 . . PUNCT eurjchem-65 124 38     SPACE eurjchem-65 124 39 2003 2003 NUM eurjchem-65 124 40 , , PUNCT eurjchem-65 124 41     SPACE eurjchem-65 124 42 38 38 NUM eurjchem-65 124 43 , , PUNCT eurjchem-65 124 44     SPACE eurjchem-65 124 45 533‐538 533‐538 NUM eurjchem-65 124 46 . . PUNCT eurjchem-65 124 47     SPACE eurjchem-65 125 1 [ [ X eurjchem-65 125 2 15 15 NUM eurjchem-65 125 3 ] ] PUNCT eurjchem-65 125 4 . . PUNCT eurjchem-65 126 1 vu vu PROPN eurjchem-65 126 2 , , PUNCT eurjchem-65 126 3     SPACE eurjchem-65 126 4 c. c. PROPN eurjchem-65 126 5     SPACE eurjchem-65 126 6 b. b. PROPN eurjchem-65 126 7 ; ; PUNCT eurjchem-65 126 8     SPACE eurjchem-65 126 9 shields shield NOUN eurjchem-65 126 10 , , PUNCT eurjchem-65 126 11     SPACE eurjchem-65 126 12 p. p. NOUN eurjchem-65 126 13 ; ; PUNCT eurjchem-65 126 14     SPACE eurjchem-65 127 1 peng peng PROPN eurjchem-65 127 2 , , PUNCT eurjchem-65 127 3     SPACE eurjchem-65 127 4 b. b. PROPN eurjchem-65 127 5 ; ; PUNCT eurjchem-65 127 6     SPACE eurjchem-65 127 7 kumaravel kumaravel NOUN eurjchem-65 127 8 , , PUNCT eurjchem-65 127 9     SPACE eurjchem-65 127 10 g. g. NOUN eurjchem-65 127 11 ; ; PUNCT eurjchem-65 127 12     SPACE eurjchem-65 127 13 jin jin NOUN eurjchem-65 127 14 , , PUNCT eurjchem-65 127 15     SPACE eurjchem-65 127 16 x. x. NOUN eurjchem-65 127 17 ; ; PUNCT eurjchem-65 127 18     SPACE eurjchem-65 127 19 phadke phadke NOUN eurjchem-65 127 20 , , PUNCT eurjchem-65 127 21     SPACE eurjchem-65 127 22 d. d. PROPN eurjchem-65 127 23 ; ; PUNCT eurjchem-65 127 24     SPACE eurjchem-65 127 25 wang wang PROPN eurjchem-65 127 26 , , PUNCT eurjchem-65 127 27     SPACE eurjchem-65 127 28 j. j. PROPN eurjchem-65 127 29 ; ; PUNCT eurjchem-65 127 30     SPACE eurjchem-65 127 31 engber engber PROPN eurjchem-65 127 32 , , PUNCT eurjchem-65 127 33     SPACE eurjchem-65 127 34 t. t. PROPN eurjchem-65 127 35 ; ; PUNCT eurjchem-65 127 36     SPACE eurjchem-65 127 37 ayyub ayyub NOUN eurjchem-65 127 38 , , PUNCT eurjchem-65 127 39     SPACE eurjchem-65 127 40 e. e. PROPN eurjchem-65 127 41 ; ; PUNCT eurjchem-65 127 42     SPACE eurjchem-65 127 43 petter petter NOUN eurjchem-65 127 44 , , PUNCT eurjchem-65 127 45     SPACE eurjchem-65 127 46 r. r. NOUN eurjchem-65 127 47     SPACE eurjchem-65 127 48 bioorg bioorg PROPN eurjchem-65 127 49 . . PUNCT eurjchem-65 127 50     SPACE eurjchem-65 127 51 med med PROPN eurjchem-65 127 52 . . PUNCT eurjchem-65 127 53     SPACE eurjchem-65 127 54 chem chem NOUN eurjchem-65 127 55 . . PUNCT eurjchem-65 127 56     SPACE eurjchem-65 127 57 lett lett PROPN eurjchem-65 127 58 . . PUNCT eurjchem-65 127 59     SPACE eurjchem-65 127 60 2004 2004 NUM eurjchem-65 127 61 , , PUNCT eurjchem-65 127 62     SPACE eurjchem-65 127 63 14 14 NUM eurjchem-65 127 64 , , PUNCT eurjchem-65 127 65     SPACE eurjchem-65 127 66 4835‐838 4835‐838 NUM eurjchem-65 127 67 . . PUNCT eurjchem-65 127 68     SPACE eurjchem-65 128 1 [ [ X eurjchem-65 128 2 16 16 NUM eurjchem-65 128 3 ] ] PUNCT eurjchem-65 128 4 . . PUNCT eurjchem-65 129 1 ilango ilango PROPN eurjchem-65 129 2 , , PUNCT eurjchem-65 129 3     SPACE eurjchem-65 129 4 k. k. PROPN eurjchem-65 129 5 ; ; PUNCT eurjchem-65 129 6     SPACE eurjchem-65 129 7 valentina valentina PROPN eurjchem-65 129 8 , , PUNCT eurjchem-65 129 9     SPACE eurjchem-65 129 10 p. p. NOUN eurjchem-65 129 11     SPACE eurjchem-65 129 12 eur eur PROPN eurjchem-65 129 13 . . PUNCT eurjchem-65 129 14     SPACE eurjchem-65 129 15 j. j. PROPN eurjchem-65 129 16     SPACE eurjchem-65 129 17 chem chem NOUN eurjchem-65 129 18 . . PUNCT eurjchem-65 129 19     SPACE eurjchem-65 129 20 2010 2010 NUM eurjchem-65 129 21 , , PUNCT eurjchem-65 129 22     SPACE eurjchem-65 129 23 1(1 1(1 NUM eurjchem-65 129 24 ) ) PUNCT eurjchem-65 129 25 , , PUNCT eurjchem-65 129 26     SPACE eurjchem-65 129 27 50‐53 50‐53 PROPN eurjchem-65 129 28 . . PUNCT eurjchem-65 129 29     SPACE eurjchem-65 130 1 [ [ X eurjchem-65 130 2 17 17 NUM eurjchem-65 130 3 ] ] PUNCT eurjchem-65 130 4 . . PUNCT eurjchem-65 131 1 foroughifar foroughifar ADV eurjchem-65 131 2 , , PUNCT eurjchem-65 131 3     SPACE eurjchem-65 131 4 n. n. NOUN eurjchem-65 131 5 ; ; PUNCT eurjchem-65 131 6     SPACE eurjchem-65 131 7 mobinikhaledi mobinikhaledi ADJ eurjchem-65 131 8 , , PUNCT eurjchem-65 131 9     SPACE eurjchem-65 131 10 a. a. NOUN eurjchem-65 131 11 ; ; PUNCT eurjchem-65 131 12     SPACE eurjchem-65 131 13 ebrahimi ebrahimi PROPN eurjchem-65 131 14 , , PUNCT eurjchem-65 131 15     SPACE eurjchem-65 131 16 s. s. PROPN eurjchem-65 131 17     SPACE eurjchem-65 131 18 synthesis synthesis NOUN eurjchem-65 131 19     SPACE eurjchem-65 131 20 2009 2009 NUM eurjchem-65 131 21 , , PUNCT eurjchem-65 131 22     SPACE eurjchem-65 131 23 15 15 NUM eurjchem-65 131 24 , , PUNCT eurjchem-65 131 25     SPACE eurjchem-65 131 26 2557‐2560 2557‐2560 NOUN eurjchem-65 131 27 . . PUNCT eurjchem-65 131 28     SPACE eurjchem-65 132 1 [ [ X eurjchem-65 132 2 18 18 NUM eurjchem-65 132 3 ] ] PUNCT eurjchem-65 132 4 . . PUNCT eurjchem-65 132 5 mobinikhaledi mobinikhaledi PROPN eurjchem-65 132 6 , , PUNCT eurjchem-65 132 7     SPACE eurjchem-65 132 8 a. a. NOUN eurjchem-65 132 9 ; ; PUNCT eurjchem-65 132 10     SPACE eurjchem-65 132 11 foroughifar foroughifar ADV eurjchem-65 132 12 , , PUNCT eurjchem-65 132 13     SPACE eurjchem-65 132 14 n. n. NOUN eurjchem-65 132 15 ; ; PUNCT eurjchem-65 132 16     SPACE eurjchem-65 132 17 khanpour khanpour ADJ eurjchem-65 132 18 , , PUNCT eurjchem-65 132 19     SPACE eurjchem-65 132 20 m. m. NOUN eurjchem-65 132 21 ; ; PUNCT eurjchem-65 132 22     SPACE eurjchem-65 132 23 ebrahimi ebrahimi PROPN eurjchem-65 132 24 , , PUNCT eurjchem-65 132 25     SPACE eurjchem-65 132 26 s. s. PROPN eurjchem-65 132 27     SPACE eurjchem-65 132 28 eur eur PROPN eurjchem-65 132 29 . . PUNCT eurjchem-65 132 30     SPACE eurjchem-65 132 31 j. j. PROPN eurjchem-65 132 32     SPACE eurjchem-65 132 33 chem chem NOUN eurjchem-65 132 34 . . PUNCT eurjchem-65 132 35     SPACE eurjchem-65 132 36 2010 2010 NUM eurjchem-65 132 37 , , PUNCT eurjchem-65 132 38     SPACE eurjchem-65 132 39 1(1 1(1 NUM eurjchem-65 132 40 ) ) PUNCT eurjchem-65 132 41 , , PUNCT eurjchem-65 132 42     SPACE eurjchem-65 132 43 33‐36 33‐36 NUM eurjchem-65 132 44 . . PUNCT eurjchem-65 132 45     SPACE eurjchem-65 133 1 [ [ X eurjchem-65 133 2 19 19 NUM eurjchem-65 133 3 ] ] PUNCT eurjchem-65 133 4 . . PUNCT eurjchem-65 134 1 foroughifar foroughifar ADV eurjchem-65 134 2 , , PUNCT eurjchem-65 134 3     SPACE eurjchem-65 134 4 n. n. NOUN eurjchem-65 134 5 ; ; PUNCT eurjchem-65 134 6     SPACE eurjchem-65 134 7 mobinikhaledi mobinikhaledi ADJ eurjchem-65 134 8 , , PUNCT eurjchem-65 134 9     SPACE eurjchem-65 134 10 a. a. NOUN eurjchem-65 134 11 ; ; PUNCT eurjchem-65 134 12     SPACE eurjchem-65 134 13 ebrahimi ebrahimi PROPN eurjchem-65 134 14 , , PUNCT eurjchem-65 134 15     SPACE eurjchem-65 134 16 s. s. PROPN eurjchem-65 134 17 ; ; PUNCT eurjchem-65 134 18     SPACE eurjchem-65 134 19 moghanian moghanian ADJ eurjchem-65 134 20 , , PUNCT eurjchem-65 134 21     SPACE eurjchem-65 134 22 h. h. NOUN eurjchem-65 134 23 ; ; PUNCT eurjchem-65 134 24     SPACE eurjchem-65 134 25 bodaghi bodaghi NOUN eurjchem-65 134 26     SPACE eurjchem-65 134 27 fard fard NOUN eurjchem-65 134 28 , , PUNCT eurjchem-65 134 29     SPACE eurjchem-65 134 30 m. m. NOUN eurjchem-65 134 31     SPACE eurjchem-65 134 32 a. a. NOUN eurjchem-65 134 33 ; ; PUNCT eurjchem-65 134 34     SPACE eurjchem-65 134 35 kalhor kalhor NOUN eurjchem-65 134 36 , , PUNCT eurjchem-65 134 37     SPACE eurjchem-65 134 38 m. m. NOUN eurjchem-65 134 39     SPACE eurjchem-65 134 40 tetrahedron tetrahedron NOUN eurjchem-65 134 41     SPACE eurjchem-65 134 42 lett lett PROPN eurjchem-65 134 43 . . PUNCT eurjchem-65 134 44     SPACE eurjchem-65 134 45 2009 2009 NUM eurjchem-65 134 46 , , PUNCT eurjchem-65 134 47     SPACE eurjchem-65 134 48 50 50 NUM eurjchem-65 134 49 , , PUNCT eurjchem-65 134 50     SPACE eurjchem-65 134 51 836‐839 836‐839 NOUN eurjchem-65 134 52 . . PUNCT eurjchem-65 134 53     SPACE eurjchem-65 135 1 [ [ X eurjchem-65 135 2 20 20 NUM eurjchem-65 135 3 ] ] PUNCT eurjchem-65 135 4 . . PUNCT eurjchem-65 136 1 foroughifar foroughifar ADV eurjchem-65 136 2 , , PUNCT eurjchem-65 136 3     SPACE eurjchem-65 136 4 n. n. NOUN eurjchem-65 136 5 ; ; PUNCT eurjchem-65 136 6     SPACE eurjchem-65 136 7 mobinikhaledi mobinikhaledi ADJ eurjchem-65 136 8 , , PUNCT eurjchem-65 136 9     SPACE eurjchem-65 136 10 a. a. NOUN eurjchem-65 136 11 ; ; PUNCT eurjchem-65 136 12     SPACE eurjchem-65 136 13 ebrahimi ebrahimi PROPN eurjchem-65 136 14 , , PUNCT eurjchem-65 136 15     SPACE eurjchem-65 136 16 s. s. PROPN eurjchem-65 136 17 ; ; PUNCT eurjchem-65 136 18     SPACE eurjchem-65 136 19 bodaghi bodaghi NOUN eurjchem-65 136 20     SPACE eurjchem-65 136 21 fard fard NOUN eurjchem-65 136 22 , , PUNCT eurjchem-65 136 23     SPACE eurjchem-65 136 24 m. m. NOUN eurjchem-65 136 25     SPACE eurjchem-65 136 26 a. a. NOUN eurjchem-65 136 27 ; ; PUNCT eurjchem-65 136 28     SPACE eurjchem-65 136 29 moghanian moghanian ADJ eurjchem-65 136 30 , , PUNCT eurjchem-65 136 31     SPACE eurjchem-65 136 32 m. m. NOUN eurjchem-65 136 33     SPACE eurjchem-65 136 34 j. j. PROPN eurjchem-65 136 35     SPACE eurjchem-65 136 36 chin chin PROPN eurjchem-65 136 37 . . PUNCT eurjchem-65 136 38     SPACE eurjchem-65 136 39 chem chem NOUN eurjchem-65 136 40 . . PUNCT eurjchem-65 136 41     SPACE eurjchem-65 136 42 soc soc PROPN eurjchem-65 136 43 . . PUNCT eurjchem-65 136 44     SPACE eurjchem-65 136 45 2009 2009 NUM eurjchem-65 136 46 , , PUNCT eurjchem-65 136 47     SPACE eurjchem-65 136 48 56 56 NUM eurjchem-65 136 49 , , PUNCT eurjchem-65 136 50     SPACE eurjchem-65 136 51 1043‐1047 1043‐1047 NUM eurjchem-65 136 52 . . PUNCT eurjchem-65 136 53     SPACE eurjchem-65 137 1 [ [ X eurjchem-65 137 2 21 21 NUM eurjchem-65 137 3 ] ] PUNCT eurjchem-65 137 4 . . PUNCT eurjchem-65 138 1 foroughifar foroughifar ADV eurjchem-65 138 2 , , PUNCT eurjchem-65 138 3     SPACE eurjchem-65 138 4 n. n. NOUN eurjchem-65 138 5 ; ; PUNCT eurjchem-65 138 6     SPACE eurjchem-65 138 7 mobinikhaledi mobinikhaledi ADJ eurjchem-65 138 8 , , PUNCT eurjchem-65 138 9     SPACE eurjchem-65 138 10 a. a. NOUN eurjchem-65 138 11 ; ; PUNCT eurjchem-65 138 12     SPACE eurjchem-65 138 13 ebrahimi ebrahimi PROPN eurjchem-65 138 14 , , PUNCT eurjchem-65 138 15     SPACE eurjchem-65 138 16 s. s. PROPN eurjchem-65 138 17     SPACE eurjchem-65 138 18 synthetic synthetic NOUN eurjchem-65 138 19     SPACE eurjchem-65 138 20 commun commun PROPN eurjchem-65 138 21 . . PUNCT eurjchem-65 138 22     SPACE eurjchem-65 138 23 2010 2010 NUM eurjchem-65 138 24 , , PUNCT eurjchem-65 138 25     SPACE eurjchem-65 138 26 40 40 NUM eurjchem-65 138 27 , , PUNCT eurjchem-65 138 28     SPACE eurjchem-65 138 29 2421‐2428 2421‐2428 NUM eurjchem-65 138 30 . . PUNCT eurjchem-65 138 31     SPACE eurjchem-65 139 1 [ [ X eurjchem-65 139 2 22 22 NUM eurjchem-65 139 3 ] ] PUNCT eurjchem-65 139 4 . . PUNCT eurjchem-65 140 1 zamani zamani PROPN eurjchem-65 140 2 , , PUNCT eurjchem-65 140 3     SPACE eurjchem-65 140 4 kh kh PROPN eurjchem-65 140 5 . . PROPN eurjchem-65 140 6 ; ; PUNCT eurjchem-65 140 7     SPACE eurjchem-65 140 8 faghihi faghihi PROPN eurjchem-65 140 9 , , PUNCT eurjchem-65 140 10     SPACE eurjchem-65 140 11 kh kh PROPN eurjchem-65 140 12 . . PROPN eurjchem-65 140 13 ; ; PUNCT eurjchem-65 140 14     SPACE eurjchem-65 140 15 tofighi tofighi NOUN eurjchem-65 140 16 , , PUNCT eurjchem-65 140 17     SPACE eurjchem-65 140 18 t. t. PROPN eurjchem-65 140 19     SPACE eurjchem-65 140 20 turk turk PROPN eurjchem-65 140 21 . . PUNCT eurjchem-65 140 22     SPACE eurjchem-65 141 1 j. j. PROPN eurjchem-65 141 2     SPACE eurjchem-65 141 3 chem chem NOUN eurjchem-65 141 4 . . PUNCT eurjchem-65 141 5     SPACE eurjchem-65 141 6 2004 2004 NUM eurjchem-65 141 7 , , PUNCT eurjchem-65 141 8     SPACE eurjchem-65 141 9 28 28 NUM eurjchem-65 141 10 , , PUNCT eurjchem-65 141 11     SPACE eurjchem-65 141 12 95‐100 95‐100 NOUN eurjchem-65 141 13 . . PUNCT eurjchem-65 141 14     SPACE