id	sid	tid	token	lemma	pos
eurjchem-681	1	1	untitled	untitle	VERB
eurjchem-681	1	2	european	european	PROPN
eurjchem-681	1	3	journal	journal	PROPN
eurjchem-681	1	4	of	of	ADP
eurjchem-681	1	5	chemistry	chemistry	NOUN
eurjchem-681	1	6	3	3	NUM
eurjchem-681	1	7	(	(	PUNCT
eurjchem-681	1	8	4	4	NUM
eurjchem-681	1	9	)	)	PUNCT
eurjchem-681	1	10	(	(	PUNCT
eurjchem-681	1	11	2012	2012	NUM
eurjchem-681	1	12	)	)	PUNCT
eurjchem-681	1	13	447‐454	447‐454	PROPN
eurjchem-681	1	14	european	european	PROPN
eurjchem-681	1	15	journal	journal	PROPN
eurjchem-681	1	16	of	of	ADP
eurjchem-681	1	17	chemistry	chemistry	NOUN
eurjchem-681	1	18	issn	issn	PROPN
eurjchem-681	1	19	2153‐2249	2153‐2249	PROPN
eurjchem-681	1	20	(	(	PUNCT
eurjchem-681	1	21	print	print	NOUN
eurjchem-681	1	22	)	)	PUNCT
eurjchem-681	1	23	/	/	SYM
eurjchem-681	1	24	issn	issn	PROPN
eurjchem-681	1	25	2153‐2257	2153‐2257	NUM
eurjchem-681	1	26	(	(	PUNCT
eurjchem-681	1	27	online	online	ADJ
eurjchem-681	1	28	)	)	PUNCT
eurjchem-681	1	29			NOUN
eurjchem-681	1	30	2012	2012	NUM
eurjchem-681	1	31	eurjchem	eurjchem	PROPN
eurjchem-681	1	32	doi:10.5155	doi:10.5155	PROPN
eurjchem-681	1	33	/	/	SYM
eurjchem-681	1	34	eurjchem.3.4.447‐454.681	eurjchem.3.4.447‐454.681	VERB
eurjchem-681	1	35	european	european	ADJ
eurjchem-681	1	36	journal	journal	PROPN
eurjchem-681	1	37	of	of	ADP
eurjchem-681	1	38	chemistry	chemistry	PROPN
eurjchem-681	1	39	journal	journal	PROPN
eurjchem-681	1	40	homepage	homepage	NOUN
eurjchem-681	1	41	:	:	PUNCT
eurjchem-681	1	42	www.eurjchem.com	www.eurjchem.com	X
eurjchem-681	1	43	development	development	NOUN
eurjchem-681	1	44	and	and	CCONJ
eurjchem-681	1	45	validation	validation	NOUN
eurjchem-681	1	46	of	of	ADP
eurjchem-681	1	47	spectrophotometric	spectrophotometric	ADJ
eurjchem-681	1	48	methods	method	NOUN
eurjchem-681	1	49	for	for	ADP
eurjchem-681	1	50	simultaneous	simultaneous	ADJ
eurjchem-681	1	51	determination	determination	NOUN
eurjchem-681	1	52	of	of	ADP
eurjchem-681	1	53	sitagliptin	sitagliptin	NOUN
eurjchem-681	1	54	and	and	CCONJ
eurjchem-681	1	55	simvastatin	simvastatin	NOUN
eurjchem-681	1	56	in	in	ADP
eurjchem-681	1	57	binary	binary	ADJ
eurjchem-681	1	58	mixture	mixture	NOUN
eurjchem-681	1	59	sherif	sherif	PROPN
eurjchem-681	1	60	abdel‐naby	abdel‐naby	PROPN
eurjchem-681	1	61	abdel‐gawad	abdel‐gawad	VERB
eurjchem-681	2	1	a	a	PRON
eurjchem-681	2	2	and	and	CCONJ
eurjchem-681	2	3	zeinab	zeinab	PROPN
eurjchem-681	2	4	abdelaziz	abdelaziz	PROPN
eurjchem-681	2	5	elsherif	elsherif	PROPN
eurjchem-681	2	6	b	b	PROPN
eurjchem-681	2	7	,	,	PUNCT
eurjchem-681	2	8	*	*	PUNCT
eurjchem-681	2	9	a	a	DET
eurjchem-681	2	10	analytical	analytical	ADJ
eurjchem-681	2	11	chemistry	chemistry	NOUN
eurjchem-681	2	12	department	department	NOUN
eurjchem-681	2	13	,	,	PUNCT
eurjchem-681	2	14	faculty	faculty	NOUN
eurjchem-681	2	15	of	of	ADP
eurjchem-681	2	16	pharmacy	pharmacy	NOUN
eurjchem-681	2	17	,	,	PUNCT
eurjchem-681	2	18	cairo	cairo	PROPN
eurjchem-681	2	19	university	university	PROPN
eurjchem-681	2	20	,	,	PUNCT
eurjchem-681	2	21	cairo	cairo	PROPN
eurjchem-681	2	22	,	,	PUNCT
eurjchem-681	2	23	11562	11562	NUM
eurjchem-681	2	24	,	,	PUNCT
eurjchem-681	2	25	egypt	egypt	PROPN
eurjchem-681	2	26	b	b	PROPN
eurjchem-681	2	27	national	national	ADJ
eurjchem-681	2	28	organization	organization	NOUN
eurjchem-681	2	29	for	for	ADP
eurjchem-681	2	30	drug	drug	NOUN
eurjchem-681	2	31	control	control	NOUN
eurjchem-681	2	32	and	and	CCONJ
eurjchem-681	2	33	research	research	NOUN
eurjchem-681	2	34	,	,	PUNCT
eurjchem-681	2	35	giza	giza	PROPN
eurjchem-681	2	36	,	,	PUNCT
eurjchem-681	2	37	11126	11126	NUM
eurjchem-681	2	38	,	,	PUNCT
eurjchem-681	2	39	egypt	egypt	PROPN
eurjchem-681	2	40	*	*	PUNCT
eurjchem-681	2	41	corresponding	correspond	VERB
eurjchem-681	2	42	author	author	NOUN
eurjchem-681	2	43	at	at	ADP
eurjchem-681	2	44	:	:	PUNCT
eurjchem-681	2	45	national	national	ADJ
eurjchem-681	2	46	organization	organization	NOUN
eurjchem-681	2	47	for	for	ADP
eurjchem-681	2	48	drug	drug	NOUN
eurjchem-681	2	49	control	control	NOUN
eurjchem-681	2	50	and	and	CCONJ
eurjchem-681	2	51	research	research	NOUN
eurjchem-681	2	52	,	,	PUNCT
eurjchem-681	2	53	giza	giza	PROPN
eurjchem-681	2	54	,	,	PUNCT
eurjchem-681	2	55	11126	11126	NUM
eurjchem-681	2	56	,	,	PUNCT
eurjchem-681	2	57	egypt	egypt	PROPN
eurjchem-681	2	58	.	.	PUNCT
eurjchem-681	3	1	tel	tel	PROPN
eurjchem-681	3	2	.	.	PUNCT
eurjchem-681	3	3	:	:	PUNCT
eurjchem-681	4	1	+20.3.5857481	+20.3.5857481	PROPN
eurjchem-681	4	2	;	;	PUNCT
eurjchem-681	4	3	fax	fax	NOUN
eurjchem-681	4	4	:	:	PUNCT
eurjchem-681	4	5	+20.3.5855587	+20.3.5855587	PROPN
eurjchem-681	4	6	.	.	PUNCT
eurjchem-681	4	7	e‐mail	e‐mail	PUNCT
eurjchem-681	5	1	address	address	NOUN
eurjchem-681	5	2	:	:	PUNCT
eurjchem-681	5	3	zelsherif@gmail.com	zelsherif@gmail.com	X
eurjchem-681	5	4	(	(	PUNCT
eurjchem-681	5	5	z.a	z.a	PROPN
eurjchem-681	5	6	.	.	PROPN
eurjchem-681	5	7	elsherif	elsherif	PROPN
eurjchem-681	5	8	)	)	PUNCT
eurjchem-681	5	9	.	.	PUNCT
eurjchem-681	6	1	article	article	NOUN
eurjchem-681	6	2	information	information	PROPN
eurjchem-681	6	3	abstract	abstract	ADV
eurjchem-681	6	4	received	receive	VERB
eurjchem-681	6	5	:	:	PUNCT
eurjchem-681	6	6	20	20	NUM
eurjchem-681	6	7	september	september	PROPN
eurjchem-681	6	8	2012	2012	NUM
eurjchem-681	6	9	received	receive	VERB
eurjchem-681	6	10	in	in	ADP
eurjchem-681	6	11	revised	revise	VERB
eurjchem-681	6	12	form	form	NOUN
eurjchem-681	6	13	:	:	PUNCT
eurjchem-681	6	14	24	24	NUM
eurjchem-681	6	15	october	october	PROPN
eurjchem-681	6	16	2012	2012	NUM
eurjchem-681	6	17	accepted	accept	VERB
eurjchem-681	6	18	:	:	PUNCT
eurjchem-681	6	19	24	24	NUM
eurjchem-681	6	20	october	october	PROPN
eurjchem-681	6	21	2012	2012	NUM
eurjchem-681	6	22	online	online	NOUN
eurjchem-681	6	23	:	:	PUNCT
eurjchem-681	6	24	31	31	NUM
eurjchem-681	6	25	december	december	PROPN
eurjchem-681	6	26	2012	2012	NUM
eurjchem-681	6	27	keywords	keyword	NOUN
eurjchem-681	6	28	simple	simple	ADJ
eurjchem-681	6	29	,	,	PUNCT
eurjchem-681	6	30	selective	selective	ADJ
eurjchem-681	6	31	and	and	CCONJ
eurjchem-681	6	32	precise	precise	ADJ
eurjchem-681	6	33	spectrophotometric	spectrophotometric	ADJ
eurjchem-681	6	34	methods	method	NOUN
eurjchem-681	6	35	were	be	AUX
eurjchem-681	6	36	adopted	adopt	VERB
eurjchem-681	6	37	for	for	ADP
eurjchem-681	6	38	simultaneous	simultaneous	ADJ
eurjchem-681	6	39	determination	determination	NOUN
eurjchem-681	6	40	of	of	ADP
eurjchem-681	6	41	sitagliptin	sitagliptin	NOUN
eurjchem-681	6	42	(	(	PUNCT
eurjchem-681	6	43	sit	sit	NOUN
eurjchem-681	6	44	)	)	PUNCT
eurjchem-681	6	45	and	and	CCONJ
eurjchem-681	6	46	simvastatin	simvastatin	NOUN
eurjchem-681	6	47	(	(	PUNCT
eurjchem-681	6	48	sim	sim	NOUN
eurjchem-681	6	49	)	)	PUNCT
eurjchem-681	6	50	in	in	ADP
eurjchem-681	6	51	new	new	ADJ
eurjchem-681	6	52	co‐formulated	co‐formulate	VERB
eurjchem-681	6	53	pharmaceutical	pharmaceutical	NOUN
eurjchem-681	6	54	dosage	dosage	NOUN
eurjchem-681	6	55	form	form	NOUN
eurjchem-681	6	56	.	.	PUNCT
eurjchem-681	7	1	in	in	ADP
eurjchem-681	7	2	the	the	DET
eurjchem-681	7	3	first	first	ADJ
eurjchem-681	7	4	method	method	NOUN
eurjchem-681	7	5	,	,	PUNCT
eurjchem-681	7	6	sit	sit	VERB
eurjchem-681	7	7	was	be	AUX
eurjchem-681	7	8	determined	determine	VERB
eurjchem-681	7	9	by	by	ADP
eurjchem-681	7	10	measuring	measure	VERB
eurjchem-681	7	11	its	its	PRON
eurjchem-681	7	12	zero	zero	NUM
eurjchem-681	7	13	order	order	NOUN
eurjchem-681	7	14	absorbance	absorbance	NOUN
eurjchem-681	7	15	at	at	ADP
eurjchem-681	7	16	266.4	266.4	NUM
eurjchem-681	7	17	nm	nm	NOUN
eurjchem-681	7	18	in	in	ADP
eurjchem-681	7	19	the	the	DET
eurjchem-681	7	20	range	range	NOUN
eurjchem-681	7	21	of	of	ADP
eurjchem-681	7	22	40‐360	40‐360	NUM
eurjchem-681	7	23	µg	µg	NOUN
eurjchem-681	7	24	/	/	SYM
eurjchem-681	7	25	ml	ml	NOUN
eurjchem-681	7	26	in	in	ADP
eurjchem-681	7	27	the	the	DET
eurjchem-681	7	28	presence	presence	NOUN
eurjchem-681	7	29	of	of	ADP
eurjchem-681	7	30	up	up	ADP
eurjchem-681	7	31	to	to	PART
eurjchem-681	7	32	70	70	NUM
eurjchem-681	7	33	%	%	NOUN
eurjchem-681	7	34	of	of	ADP
eurjchem-681	7	35	sim	sim	NOUN
eurjchem-681	7	36	.	.	PUNCT
eurjchem-681	8	1	while	while	SCONJ
eurjchem-681	8	2	,	,	PUNCT
eurjchem-681	8	3	the	the	DET
eurjchem-681	8	4	two	two	NUM
eurjchem-681	8	5	cited	cite	VERB
eurjchem-681	8	6	drugs	drug	NOUN
eurjchem-681	8	7	were	be	AUX
eurjchem-681	8	8	determined	determine	VERB
eurjchem-681	8	9	simultaneously	simultaneously	ADV
eurjchem-681	8	10	using	use	VERB
eurjchem-681	8	11	third	third	ADJ
eurjchem-681	8	12	derivative	derivative	ADJ
eurjchem-681	8	13	method	method	NOUN
eurjchem-681	8	14	by	by	ADP
eurjchem-681	8	15	measuring	measure	VERB
eurjchem-681	8	16	the	the	DET
eurjchem-681	8	17	sum	sum	NOUN
eurjchem-681	8	18	of	of	ADP
eurjchem-681	8	19	peak	peak	NOUN
eurjchem-681	8	20	amplitudes	amplitude	NOUN
eurjchem-681	8	21	(	(	PUNCT
eurjchem-681	8	22	peak	peak	NOUN
eurjchem-681	8	23	&	&	CCONJ
eurjchem-681	8	24	valley	valley	PROPN
eurjchem-681	8	25	)	)	PUNCT
eurjchem-681	8	26	at	at	ADP
eurjchem-681	8	27	275.3‐280.3	275.3‐280.3	NUM
eurjchem-681	8	28	nm	nm	ADJ
eurjchem-681	8	29	and	and	CCONJ
eurjchem-681	8	30	240.5‐244.7	240.5‐244.7	NUM
eurjchem-681	8	31	nm	nm	NOUN
eurjchem-681	8	32	in	in	ADP
eurjchem-681	8	33	the	the	DET
eurjchem-681	8	34	ranges	range	NOUN
eurjchem-681	8	35	of	of	ADP
eurjchem-681	8	36	40‐360	40‐360	NUM
eurjchem-681	8	37	µg	µg	NOUN
eurjchem-681	8	38	/	/	SYM
eurjchem-681	8	39	ml	ml	NOUN
eurjchem-681	8	40	and	and	CCONJ
eurjchem-681	8	41	2‐18	2‐18	NUM
eurjchem-681	8	42	µg	µg	ADV
eurjchem-681	8	43	/	/	SYM
eurjchem-681	8	44	ml	ml	NOUN
eurjchem-681	8	45	for	for	ADP
eurjchem-681	8	46	sit	sit	NOUN
eurjchem-681	8	47	and	and	CCONJ
eurjchem-681	8	48	sim	sim	ADJ
eurjchem-681	8	49	,	,	PUNCT
eurjchem-681	8	50	respectively	respectively	ADV
eurjchem-681	8	51	.	.	PUNCT
eurjchem-681	9	1	in	in	ADP
eurjchem-681	9	2	the	the	DET
eurjchem-681	9	3	second	second	ADJ
eurjchem-681	9	4	method	method	NOUN
eurjchem-681	9	5	,	,	PUNCT
eurjchem-681	9	6	the	the	DET
eurjchem-681	9	7	first	first	ADJ
eurjchem-681	9	8	derivative	derivative	NOUN
eurjchem-681	9	9	of	of	ADP
eurjchem-681	9	10	ratio	ratio	NOUN
eurjchem-681	9	11	spectra	spectra	PROPN
eurjchem-681	9	12	method	method	NOUN
eurjchem-681	9	13	was	be	AUX
eurjchem-681	9	14	applied	apply	VERB
eurjchem-681	9	15	by	by	ADP
eurjchem-681	9	16	measuring	measure	VERB
eurjchem-681	9	17	the	the	DET
eurjchem-681	9	18	peak	peak	NOUN
eurjchem-681	9	19	height	height	NOUN
eurjchem-681	9	20	at	at	ADP
eurjchem-681	9	21	255.9	255.9	NUM
eurjchem-681	9	22	and	and	CCONJ
eurjchem-681	9	23	275.2	275.2	NUM
eurjchem-681	9	24	nm	nm	NOUN
eurjchem-681	9	25	using	use	VERB
eurjchem-681	9	26	18	18	NUM
eurjchem-681	9	27	µg	µg	NOUN
eurjchem-681	9	28	/	/	SYM
eurjchem-681	9	29	ml	ml	NOUN
eurjchem-681	9	30	sim	sim	NOUN
eurjchem-681	9	31	as	as	ADP
eurjchem-681	9	32	devisor	devisor	NOUN
eurjchem-681	9	33	over	over	ADP
eurjchem-681	9	34	a	a	DET
eurjchem-681	9	35	concentration	concentration	NOUN
eurjchem-681	9	36	range	range	NOUN
eurjchem-681	9	37	of	of	ADP
eurjchem-681	9	38	40‐360	40‐360	NUM
eurjchem-681	9	39	µg	µg	NOUN
eurjchem-681	9	40	/	/	SYM
eurjchem-681	9	41	ml	ml	NOUN
eurjchem-681	9	42	of	of	ADP
eurjchem-681	9	43	sit	sit	VERB
eurjchem-681	9	44	and	and	CCONJ
eurjchem-681	9	45	at	at	ADP
eurjchem-681	9	46	228.3	228.3	NUM
eurjchem-681	9	47	,	,	PUNCT
eurjchem-681	9	48	240.5	240.5	NUM
eurjchem-681	9	49	and	and	CCONJ
eurjchem-681	9	50	248	248	NUM
eurjchem-681	9	51	nm	nm	NOUN
eurjchem-681	9	52	using	use	VERB
eurjchem-681	9	53	100	100	NUM
eurjchem-681	9	54	µg	µg	NOUN
eurjchem-681	9	55	/	/	SYM
eurjchem-681	9	56	ml	ml	NOUN
eurjchem-681	9	57	of	of	ADP
eurjchem-681	9	58	sit	sit	VERB
eurjchem-681	9	59	as	as	ADP
eurjchem-681	9	60	divisor	divisor	NOUN
eurjchem-681	9	61	over	over	ADP
eurjchem-681	9	62	a	a	DET
eurjchem-681	9	63	concentration	concentration	NOUN
eurjchem-681	9	64	range	range	NOUN
eurjchem-681	9	65	2‐18	2‐18	NUM
eurjchem-681	9	66	µg	µg	NOUN
eurjchem-681	9	67	/	/	SYM
eurjchem-681	9	68	ml	ml	NOUN
eurjchem-681	9	69	sim	sim	NOUN
eurjchem-681	9	70	.	.	PUNCT
eurjchem-681	10	1	in	in	ADP
eurjchem-681	10	2	the	the	DET
eurjchem-681	10	3	third	third	ADJ
eurjchem-681	10	4	method	method	NOUN
eurjchem-681	10	5	the	the	DET
eurjchem-681	10	6	ratio	ratio	NOUN
eurjchem-681	10	7	subtraction	subtraction	NOUN
eurjchem-681	10	8	spectrophotometric	spectrophotometric	ADJ
eurjchem-681	10	9	method	method	NOUN
eurjchem-681	10	10	was	be	AUX
eurjchem-681	10	11	used	use	VERB
eurjchem-681	10	12	,	,	PUNCT
eurjchem-681	10	13	where	where	SCONJ
eurjchem-681	10	14	sim	sim	NOUN
eurjchem-681	10	15	can	can	AUX
eurjchem-681	10	16	be	be	AUX
eurjchem-681	10	17	determined	determine	VERB
eurjchem-681	10	18	by	by	ADP
eurjchem-681	10	19	dividing	divide	VERB
eurjchem-681	10	20	the	the	DET
eurjchem-681	10	21	spectra	spectra	NOUN
eurjchem-681	10	22	of	of	ADP
eurjchem-681	10	23	the	the	DET
eurjchem-681	10	24	mixtures	mixture	NOUN
eurjchem-681	10	25	by	by	ADP
eurjchem-681	10	26	the	the	DET
eurjchem-681	10	27	spectrum	spectrum	NOUN
eurjchem-681	10	28	of	of	ADP
eurjchem-681	10	29	sit	sit	NOUN
eurjchem-681	10	30	(	(	PUNCT
eurjchem-681	10	31	40	40	NUM
eurjchem-681	10	32	µg	µg	NOUN
eurjchem-681	10	33	/	/	SYM
eurjchem-681	10	34	ml	ml	NOUN
eurjchem-681	10	35	)	)	PUNCT
eurjchem-681	10	36	followed	follow	VERB
eurjchem-681	10	37	by	by	ADP
eurjchem-681	10	38	subtracting	subtract	VERB
eurjchem-681	10	39	the	the	DET
eurjchem-681	10	40	constant	constant	ADJ
eurjchem-681	10	41	absorbance	absorbance	NOUN
eurjchem-681	10	42	value	value	NOUN
eurjchem-681	10	43	of	of	ADP
eurjchem-681	10	44	the	the	DET
eurjchem-681	10	45	plateau	plateau	NOUN
eurjchem-681	10	46	,	,	PUNCT
eurjchem-681	10	47	then	then	ADV
eurjchem-681	10	48	finally	finally	ADV
eurjchem-681	10	49	multiply	multiply	VERB
eurjchem-681	10	50	the	the	DET
eurjchem-681	10	51	produced	produce	VERB
eurjchem-681	10	52	spectrum	spectrum	NOUN
eurjchem-681	10	53	by	by	ADP
eurjchem-681	10	54	the	the	DET
eurjchem-681	10	55	spectrum	spectrum	NOUN
eurjchem-681	10	56	of	of	ADP
eurjchem-681	10	57	the	the	DET
eurjchem-681	10	58	devisor	devisor	NOUN
eurjchem-681	10	59	.	.	PUNCT
eurjchem-681	11	1	laboratory	laboratory	NOUN
eurjchem-681	11	2	prepared	prepare	VERB
eurjchem-681	11	3	mixtures	mixture	NOUN
eurjchem-681	11	4	were	be	AUX
eurjchem-681	11	5	successfully	successfully	ADV
eurjchem-681	11	6	tried	try	VERB
eurjchem-681	11	7	for	for	ADP
eurjchem-681	11	8	the	the	DET
eurjchem-681	11	9	three	three	NUM
eurjchem-681	11	10	compositions	composition	NOUN
eurjchem-681	11	11	of	of	ADP
eurjchem-681	11	12	tablets	tablet	NOUN
eurjchem-681	11	13	(	(	PUNCT
eurjchem-681	11	14	10	10	NUM
eurjchem-681	11	15	,	,	PUNCT
eurjchem-681	11	16	20	20	NUM
eurjchem-681	11	17	and	and	CCONJ
eurjchem-681	11	18	40	40	NUM
eurjchem-681	11	19	mg	mg	NOUN
eurjchem-681	11	20	of	of	ADP
eurjchem-681	11	21	sim	sim	NOUN
eurjchem-681	11	22	)	)	PUNCT
eurjchem-681	11	23	with	with	ADP
eurjchem-681	11	24	100	100	NUM
eurjchem-681	11	25	mg	mg	ADP
eurjchem-681	11	26	of	of	ADP
eurjchem-681	11	27	sit	sit	NOUN
eurjchem-681	11	28	.	.	PUNCT
eurjchem-681	12	1	the	the	DET
eurjchem-681	12	2	developed	develop	VERB
eurjchem-681	12	3	methods	method	NOUN
eurjchem-681	12	4	were	be	AUX
eurjchem-681	12	5	validated	validate	VERB
eurjchem-681	12	6	as	as	ADP
eurjchem-681	12	7	per	per	ADP
eurjchem-681	12	8	international	international	ADJ
eurjchem-681	12	9	conference	conference	NOUN
eurjchem-681	12	10	of	of	ADP
eurjchem-681	12	11	harmonization	harmonization	NOUN
eurjchem-681	12	12	guidelines	guideline	NOUN
eurjchem-681	12	13	.	.	PUNCT
eurjchem-681	13	1	sitagliptin	sitagliptin	NOUN
eurjchem-681	13	2	validation	validation	NOUN
eurjchem-681	13	3	simvastatin	simvastatin	PROPN
eurjchem-681	13	4	ratio	ratio	NOUN
eurjchem-681	13	5	subtraction	subtraction	NOUN
eurjchem-681	13	6	spectrophotometric	spectrophotometric	ADJ
eurjchem-681	13	7	analysis	analysis	NOUN
eurjchem-681	13	8	derivative	derivative	ADJ
eurjchem-681	13	9	spectrophotometry	spectrophotometry	NOUN
eurjchem-681	13	10	1	1	NUM
eurjchem-681	13	11	.	.	PUNCT
eurjchem-681	14	1	introduction	introduction	NOUN
eurjchem-681	14	2	sitagliptin	sitagliptin	NOUN
eurjchem-681	14	3	(	(	PUNCT
eurjchem-681	14	4	sit	sit	NOUN
eurjchem-681	14	5	)	)	PUNCT
eurjchem-681	14	6	,	,	PUNCT
eurjchem-681	14	7	(	(	PUNCT
eurjchem-681	14	8	r)‐4‐oxo‐4‐[3‐(trifluoromethyl)‐5	r)‐4‐oxo‐4‐[3‐(trifluoromethyl)‐5	NOUN
eurjchem-681	14	9	,	,	PUNCT
eurjchem-681	14	10	dihydro[1,2,4]triazolo[4,3‐a]pyrazin‐7(8h)‐yl]‐1‐(2,4,5‐	dihydro[1,2,4]triazolo[4,3‐a]pyrazin‐7(8h)‐yl]‐1‐(2,4,5‐	PROPN
eurjchem-681	14	11	trifluorophenyl	trifluorophenyl	NOUN
eurjchem-681	14	12	)	)	PUNCT
eurjchem-681	14	13	butan‐2‐amine	butan‐2‐amine	PROPN
eurjchem-681	14	14	,	,	PUNCT
eurjchem-681	14	15	is	be	AUX
eurjchem-681	14	16	an	an	DET
eurjchem-681	14	17	oral	oral	ADJ
eurjchem-681	14	18	dipeptidyl	dipeptidyl	NOUN
eurjchem-681	14	19	peptidase‐	peptidase‐	NOUN
eurjchem-681	14	20	4	4	NUM
eurjchem-681	14	21	(	(	PUNCT
eurjchem-681	14	22	dpp‐4	dpp‐4	NOUN
eurjchem-681	14	23	)	)	PUNCT
eurjchem-681	14	24	inhibitor	inhibitor	NOUN
eurjchem-681	14	25	,	,	PUNCT
eurjchem-681	14	26	which	which	PRON
eurjchem-681	14	27	improves	improve	VERB
eurjchem-681	14	28	glycaemic	glycaemic	ADJ
eurjchem-681	14	29	control	control	NOUN
eurjchem-681	14	30	by	by	ADP
eurjchem-681	14	31	inhibiting	inhibit	VERB
eurjchem-681	14	32	dpp‐4	dpp‐4	NOUN
eurjchem-681	14	33	inactivation	inactivation	NOUN
eurjchem-681	14	34	of	of	ADP
eurjchem-681	14	35	the	the	DET
eurjchem-681	14	36	incretin	incretin	ADJ
eurjchem-681	14	37	hormones	hormone	NOUN
eurjchem-681	14	38	glucagon‐like	glucagon‐like	INTJ
eurjchem-681	14	39	peptide‐1	peptide‐1	PROPN
eurjchem-681	14	40	(	(	PUNCT
eurjchem-681	14	41	glp‐1	glp‐1	NOUN
eurjchem-681	14	42	)	)	PUNCT
eurjchem-681	14	43	and	and	CCONJ
eurjchem-681	14	44	glucose‐dependent	glucose‐dependent	VERB
eurjchem-681	14	45	insulinotropic	insulinotropic	NOUN
eurjchem-681	14	46	polypeptide	polypeptide	ADJ
eurjchem-681	14	47	(	(	PUNCT
eurjchem-681	14	48	gip	gip	NOUN
eurjchem-681	14	49	)	)	PUNCT
eurjchem-681	14	50	(	(	PUNCT
eurjchem-681	14	51	figure	figure	NOUN
eurjchem-681	14	52	1	1	NUM
eurjchem-681	14	53	)	)	PUNCT
eurjchem-681	14	54	.	.	PUNCT
eurjchem-681	15	1	this	this	PRON
eurjchem-681	15	2	increases	increase	VERB
eurjchem-681	15	3	active	active	ADJ
eurjchem-681	15	4	incretin	incretin	NOUN
eurjchem-681	15	5	and	and	CCONJ
eurjchem-681	15	6	insulin	insulin	NOUN
eurjchem-681	15	7	levels	level	NOUN
eurjchem-681	15	8	and	and	CCONJ
eurjchem-681	15	9	decreases	decrease	VERB
eurjchem-681	15	10	glucagon	glucagon	NOUN
eurjchem-681	15	11	levels	level	NOUN
eurjchem-681	15	12	and	and	CCONJ
eurjchem-681	15	13	post‐glucose‐load	post‐glucose‐load	ADV
eurjchem-681	15	14	glucose	glucose	NOUN
eurjchem-681	15	15	excursion	excursion	NOUN
eurjchem-681	16	1	[	[	X
eurjchem-681	16	2	1,2	1,2	NUM
eurjchem-681	16	3	]	]	PUNCT
eurjchem-681	16	4	.	.	PUNCT
eurjchem-681	17	1	simvastatin	simvastatin	NOUN
eurjchem-681	17	2	(	(	PUNCT
eurjchem-681	17	3	sim	sim	NOUN
eurjchem-681	17	4	)	)	PUNCT
eurjchem-681	17	5	,	,	PUNCT
eurjchem-681	17	6	butanoic	butanoic	NOUN
eurjchem-681	17	7	acid	acid	NOUN
eurjchem-681	17	8	,	,	PUNCT
eurjchem-681	17	9	2,2‐dimethyl‐,1,2,3,7,8,8a‐	2,2‐dimethyl‐,1,2,3,7,8,8a‐	NUM
eurjchem-681	17	10	hexahydro‐3,7‐dimethyl‐8‐[2(tetrahydro‐4‐hydroxy‐6‐oxo‐2h‐	hexahydro‐3,7‐dimethyl‐8‐[2(tetrahydro‐4‐hydroxy‐6‐oxo‐2h‐	NOUN
eurjchem-681	17	11	pyran‐2‐yl)‐ethyl]1‐naphthalenyl	pyran‐2‐yl)‐ethyl]1‐naphthalenyl	PROPN
eurjchem-681	17	12	ester	ester	NOUN
eurjchem-681	17	13	,	,	PUNCT
eurjchem-681	17	14	is	be	AUX
eurjchem-681	17	15	a	a	DET
eurjchem-681	17	16	lipid‐lowering	lipid‐lowering	ADJ
eurjchem-681	17	17	agent	agent	NOUN
eurjchem-681	17	18	that	that	PRON
eurjchem-681	17	19	is	be	AUX
eurjchem-681	17	20	derived	derive	VERB
eurjchem-681	17	21	synthetically	synthetically	ADV
eurjchem-681	17	22	from	from	ADP
eurjchem-681	17	23	fermentation	fermentation	NOUN
eurjchem-681	17	24	products	product	NOUN
eurjchem-681	17	25	of	of	ADP
eurjchem-681	17	26	aspergillus	aspergillus	NOUN
eurjchem-681	17	27	terreus	terreus	NOUN
eurjchem-681	17	28	(	(	PUNCT
eurjchem-681	17	29	figure	figure	NOUN
eurjchem-681	17	30	1	1	NUM
eurjchem-681	17	31	)	)	PUNCT
eurjchem-681	17	32	.	.	PUNCT
eurjchem-681	18	1	after	after	SCONJ
eurjchem-681	18	2	oral	oral	ADJ
eurjchem-681	18	3	ingestion	ingestion	NOUN
eurjchem-681	18	4	simvastatin	simvastatin	NOUN
eurjchem-681	18	5	,	,	PUNCT
eurjchem-681	18	6	an	an	DET
eurjchem-681	18	7	inactive	inactive	ADJ
eurjchem-681	18	8	lactone	lactone	NOUN
eurjchem-681	18	9	,	,	PUNCT
eurjchem-681	18	10	is	be	AUX
eurjchem-681	18	11	hydrolyzed	hydrolyze	VERB
eurjchem-681	18	12	to	to	ADP
eurjchem-681	18	13	corresponding	corresponding	ADJ
eurjchem-681	18	14	ortho‐hydroxy	ortho‐hydroxy	INTJ
eurjchem-681	18	15	acid	acid	NOUN
eurjchem-681	18	16	leading	lead	VERB
eurjchem-681	18	17	to	to	ADP
eurjchem-681	18	18	the	the	DET
eurjchem-681	18	19	inhibition	inhibition	NOUN
eurjchem-681	18	20	of	of	ADP
eurjchem-681	18	21	3‐hydroxy	3‐hydroxy	NUM
eurjchem-681	18	22	3‐	3‐	NUM
eurjchem-681	18	23	methyl	methyl	NOUN
eurjchem-681	18	24	glutaryl‐coenzyme	glutaryl‐coenzyme	X
eurjchem-681	18	25	a	a	PRON
eurjchem-681	18	26	(	(	PUNCT
eurjchem-681	18	27	hmg‐co	hmg‐co	NOUN
eurjchem-681	18	28	a	a	DET
eurjchem-681	18	29	)	)	PUNCT
eurjchem-681	18	30	reductase	reductase	NOUN
eurjchem-681	18	31	,	,	PUNCT
eurjchem-681	18	32	respon‐	respon‐	NOUN
eurjchem-681	18	33	sible	sible	ADJ
eurjchem-681	18	34	for	for	ADP
eurjchem-681	18	35	catalysing	catalyse	VERB
eurjchem-681	18	36	the	the	DET
eurjchem-681	18	37	conversion	conversion	NOUN
eurjchem-681	18	38	of	of	ADP
eurjchem-681	18	39	hmg‐co	hmg‐co	PROPN
eurjchem-681	18	40	a	a	PRON
eurjchem-681	18	41	to	to	PART
eurjchem-681	18	42	mevalonate	mevalonate	VERB
eurjchem-681	18	43	,	,	PUNCT
eurjchem-681	18	44	which	which	PRON
eurjchem-681	18	45	is	be	AUX
eurjchem-681	18	46	an	an	DET
eurjchem-681	18	47	early	early	ADJ
eurjchem-681	18	48	and	and	CCONJ
eurjchem-681	18	49	rate	rate	NOUN
eurjchem-681	18	50	limiting	limit	VERB
eurjchem-681	18	51	step	step	NOUN
eurjchem-681	18	52	in	in	ADP
eurjchem-681	18	53	cholesterol	cholesterol	NOUN
eurjchem-681	18	54	biosynthesis	biosynthesis	NOUN
eurjchem-681	18	55	[	[	X
eurjchem-681	18	56	3,4	3,4	NUM
eurjchem-681	18	57	]	]	PUNCT
eurjchem-681	18	58	.	.	PUNCT
eurjchem-681	19	1	recently	recently	ADV
eurjchem-681	19	2	,	,	PUNCT
eurjchem-681	19	3	u.s	u.s	PROPN
eurjchem-681	19	4	.	.	PROPN
eurjchem-681	19	5	food	food	PROPN
eurjchem-681	19	6	and	and	CCONJ
eurjchem-681	19	7	drug	drug	PROPN
eurjchem-681	19	8	administration	administration	PROPN
eurjchem-681	19	9	(	(	PUNCT
eurjchem-681	19	10	fda	fda	PROPN
eurjchem-681	19	11	)	)	PUNCT
eurjchem-681	20	1	[	[	X
eurjchem-681	20	2	5	5	NUM
eurjchem-681	20	3	]	]	PUNCT
eurjchem-681	20	4	has	have	AUX
eurjchem-681	20	5	approved	approve	VERB
eurjchem-681	20	6	a	a	DET
eurjchem-681	20	7	fixed‐dose	fixed‐dose	NOUN
eurjchem-681	20	8	combination	combination	NOUN
eurjchem-681	20	9	tablet	tablet	NOUN
eurjchem-681	20	10	consisting	consist	VERB
eurjchem-681	20	11	of	of	ADP
eurjchem-681	20	12	sitagliptin	sitagliptin	NOUN
eurjchem-681	20	13	and	and	CCONJ
eurjchem-681	20	14	simvastatin	simvastatin	NOUN
eurjchem-681	20	15	.	.	PUNCT
eurjchem-681	21	1	this	this	PRON
eurjchem-681	21	2	is	be	AUX
eurjchem-681	21	3	the	the	DET
eurjchem-681	21	4	first	first	ADJ
eurjchem-681	21	5	product	product	NOUN
eurjchem-681	21	6	to	to	PART
eurjchem-681	21	7	combine	combine	VERB
eurjchem-681	21	8	a	a	DET
eurjchem-681	21	9	type	type	NOUN
eurjchem-681	21	10	2	2	NUM
eurjchem-681	21	11	diabetes	diabetes	NOUN
eurjchem-681	21	12	drug	drug	NOUN
eurjchem-681	21	13	with	with	ADP
eurjchem-681	21	14	a	a	DET
eurjchem-681	21	15	cholesterol	cholesterol	NOUN
eurjchem-681	21	16	lowering	lower	VERB
eurjchem-681	21	17	drug	drug	NOUN
eurjchem-681	21	18	in	in	ADP
eurjchem-681	21	19	one	one	NUM
eurjchem-681	21	20	tablet	tablet	NOUN
eurjchem-681	21	21	.	.	PUNCT
eurjchem-681	22	1	many	many	ADJ
eurjchem-681	22	2	techniques	technique	NOUN
eurjchem-681	22	3	like	like	ADP
eurjchem-681	22	4	uv‐visible	uv‐visible	ADJ
eurjchem-681	22	5	spectrophotometry	spectrophotometry	NOUN
eurjchem-681	22	6	[	[	X
eurjchem-681	22	7	6,7	6,7	NUM
eurjchem-681	22	8	]	]	PUNCT
eurjchem-681	22	9	,	,	PUNCT
eurjchem-681	22	10	hplc	hplc	NOUN
eurjchem-681	22	11	[	[	X
eurjchem-681	22	12	8‐13	8‐13	NUM
eurjchem-681	22	13	]	]	PUNCT
eurjchem-681	22	14	and	and	CCONJ
eurjchem-681	22	15	flourimetry	flourimetry	NOUN
eurjchem-681	22	16	[	[	X
eurjchem-681	22	17	14	14	NUM
eurjchem-681	22	18	]	]	PUNCT
eurjchem-681	22	19	have	have	AUX
eurjchem-681	22	20	been	be	AUX
eurjchem-681	22	21	reported	report	VERB
eurjchem-681	22	22	for	for	ADP
eurjchem-681	22	23	the	the	DET
eurjchem-681	22	24	determination	determination	NOUN
eurjchem-681	22	25	of	of	ADP
eurjchem-681	22	26	sit	sit	VERB
eurjchem-681	22	27	alone	alone	ADV
eurjchem-681	22	28	or	or	CCONJ
eurjchem-681	22	29	in	in	ADP
eurjchem-681	22	30	presence	presence	NOUN
eurjchem-681	22	31	of	of	ADP
eurjchem-681	22	32	the	the	DET
eurjchem-681	22	33	combination	combination	NOUN
eurjchem-681	22	34	with	with	ADP
eurjchem-681	22	35	other	other	ADJ
eurjchem-681	22	36	drugs	drug	NOUN
eurjchem-681	22	37	.	.	PUNCT
eurjchem-681	23	1	on	on	ADP
eurjchem-681	23	2	the	the	DET
eurjchem-681	23	3	other	other	ADJ
eurjchem-681	23	4	hand	hand	NOUN
eurjchem-681	23	5	,	,	PUNCT
eurjchem-681	23	6	sim	sim	NOUN
eurjchem-681	23	7	could	could	AUX
eurjchem-681	23	8	be	be	AUX
eurjchem-681	23	9	determined	determine	VERB
eurjchem-681	23	10	either	either	CCONJ
eurjchem-681	23	11	alone	alone	ADJ
eurjchem-681	23	12	or	or	CCONJ
eurjchem-681	23	13	in	in	ADP
eurjchem-681	23	14	presence	presence	NOUN
eurjchem-681	23	15	of	of	ADP
eurjchem-681	23	16	its	its	PRON
eurjchem-681	23	17	metabolites	metabolite	NOUN
eurjchem-681	23	18	or	or	CCONJ
eurjchem-681	23	19	in	in	ADP
eurjchem-681	23	20	combination	combination	NOUN
eurjchem-681	23	21	with	with	ADP
eurjchem-681	23	22	other	other	ADJ
eurjchem-681	23	23	drugs	drug	NOUN
eurjchem-681	23	24	using	use	VERB
eurjchem-681	23	25	different	different	ADJ
eurjchem-681	23	26	techniques	technique	NOUN
eurjchem-681	23	27	like	like	ADP
eurjchem-681	23	28	uv‐visible	uv‐visible	ADJ
eurjchem-681	23	29	spectrophotometry	spectrophotometry	NOUN
eurjchem-681	23	30	[	[	X
eurjchem-681	23	31	15‐17	15‐17	NUM
eurjchem-681	23	32	]	]	PUNCT
eurjchem-681	23	33	,	,	PUNCT
eurjchem-681	23	34	hplc	hplc	NOUN
eurjchem-681	23	35	[	[	X
eurjchem-681	23	36	18‐24	18‐24	X
eurjchem-681	23	37	]	]	PUNCT
eurjchem-681	23	38	and	and	CCONJ
eurjchem-681	23	39	lc	lc	PROPN
eurjchem-681	23	40	/	/	SYM
eurjchem-681	23	41	ms	ms	PROPN
eurjchem-681	23	42	/	/	SYM
eurjchem-681	23	43	ms	ms	NOUN
eurjchem-681	24	1	[	[	X
eurjchem-681	24	2	25‐	25‐	NUM
eurjchem-681	24	3	28	28	NUM
eurjchem-681	24	4	]	]	PUNCT
eurjchem-681	24	5	.	.	PUNCT
eurjchem-681	25	1	(	(	PUNCT
eurjchem-681	25	2	a	a	X
eurjchem-681	25	3	)	)	PUNCT
eurjchem-681	25	4	(	(	PUNCT
eurjchem-681	25	5	b	b	X
eurjchem-681	25	6	)	)	PUNCT
eurjchem-681	25	7	figure	figure	NOUN
eurjchem-681	25	8	1	1	NUM
eurjchem-681	25	9	.	.	PUNCT
eurjchem-681	26	1	chemical	chemical	ADJ
eurjchem-681	26	2	structure	structure	NOUN
eurjchem-681	26	3	of	of	ADP
eurjchem-681	26	4	(	(	PUNCT
eurjchem-681	26	5	a	a	PRON
eurjchem-681	26	6	)	)	PUNCT
eurjchem-681	26	7	sitagliptin	sitagliptin	NOUN
eurjchem-681	26	8	(	(	PUNCT
eurjchem-681	26	9	c16h15f6n5o	c16h15f6n5o	NOUN
eurjchem-681	26	10	)	)	PUNCT
eurjchem-681	26	11	and	and	CCONJ
eurjchem-681	26	12	(	(	PUNCT
eurjchem-681	26	13	b	b	NOUN
eurjchem-681	26	14	)	)	PUNCT
eurjchem-681	26	15	simvastatin	simvastatin	NOUN
eurjchem-681	26	16	(	(	PUNCT
eurjchem-681	26	17	c25h38o5	c25h38o5	PROPN
eurjchem-681	26	18	)	)	PUNCT
eurjchem-681	26	19	.	.	PUNCT
eurjchem-681	27	1	448	448	NUM
eurjchem-681	27	2	abdel‐gawad	abdel‐gawad	NOUN
eurjchem-681	27	3	and	and	CCONJ
eurjchem-681	27	4	elsherif	elsherif	VERB
eurjchem-681	27	5	/	/	SYM
eurjchem-681	27	6	european	european	PROPN
eurjchem-681	27	7	journal	journal	PROPN
eurjchem-681	27	8	of	of	ADP
eurjchem-681	27	9	chemistry	chemistry	NOUN
eurjchem-681	27	10	3	3	NUM
eurjchem-681	27	11	(	(	PUNCT
eurjchem-681	27	12	4	4	NUM
eurjchem-681	27	13	)	)	PUNCT
eurjchem-681	27	14	(	(	PUNCT
eurjchem-681	27	15	2012	2012	NUM
eurjchem-681	27	16	)	)	PUNCT
eurjchem-681	27	17	447‐454	447‐454	PROPN
eurjchem-681	27	18	for	for	ADP
eurjchem-681	27	19	the	the	DET
eurjchem-681	27	20	new	new	ADJ
eurjchem-681	27	21	co‐formulated	co‐formulate	VERB
eurjchem-681	27	22	dosage	dosage	NOUN
eurjchem-681	27	23	form	form	NOUN
eurjchem-681	27	24	,	,	PUNCT
eurjchem-681	27	25	a	a	DET
eurjchem-681	27	26	few	few	ADJ
eurjchem-681	27	27	methods	method	NOUN
eurjchem-681	27	28	were	be	AUX
eurjchem-681	27	29	published	publish	VERB
eurjchem-681	27	30	for	for	ADP
eurjchem-681	27	31	the	the	DET
eurjchem-681	27	32	determination	determination	NOUN
eurjchem-681	27	33	of	of	ADP
eurjchem-681	27	34	both	both	DET
eurjchem-681	27	35	drugs	drug	NOUN
eurjchem-681	27	36	when	when	SCONJ
eurjchem-681	27	37	present	present	ADJ
eurjchem-681	27	38	in	in	ADP
eurjchem-681	27	39	combination	combination	NOUN
eurjchem-681	27	40	.	.	PUNCT
eurjchem-681	28	1	these	these	DET
eurjchem-681	28	2	methods	method	NOUN
eurjchem-681	28	3	comprise	comprise	VERB
eurjchem-681	28	4	the	the	DET
eurjchem-681	28	5	use	use	NOUN
eurjchem-681	28	6	of	of	ADP
eurjchem-681	28	7	simultaneous	simultaneous	ADJ
eurjchem-681	28	8	equation	equation	NOUN
eurjchem-681	28	9	spectrophotometric	spectrophotometric	VERB
eurjchem-681	28	10	method	method	NOUN
eurjchem-681	28	11	[	[	X
eurjchem-681	28	12	29	29	NUM
eurjchem-681	28	13	]	]	PUNCT
eurjchem-681	28	14	,	,	PUNCT
eurjchem-681	28	15	rp‐	rp‐	ADP
eurjchem-681	28	16	hplc	hplc	NOUN
eurjchem-681	29	1	[	[	X
eurjchem-681	29	2	30,31	30,31	NUM
eurjchem-681	29	3	]	]	PUNCT
eurjchem-681	29	4	and	and	CCONJ
eurjchem-681	29	5	in	in	ADP
eurjchem-681	29	6	human	human	ADJ
eurjchem-681	29	7	plasma	plasma	NOUN
eurjchem-681	29	8	by	by	ADP
eurjchem-681	29	9	lc‐ms	lc‐ms	AUX
eurjchem-681	29	10	/	/	SYM
eurjchem-681	29	11	ms	ms	PROPN
eurjchem-681	29	12	and	and	CCONJ
eurjchem-681	29	13	its	its	PRON
eurjchem-681	29	14	application	application	NOUN
eurjchem-681	29	15	to	to	ADP
eurjchem-681	29	16	a	a	DET
eurjchem-681	29	17	human	human	ADJ
eurjchem-681	29	18	pharmacokinetic	pharmacokinetic	NOUN
eurjchem-681	29	19	[	[	X
eurjchem-681	29	20	32	32	NUM
eurjchem-681	29	21	]	]	PUNCT
eurjchem-681	29	22	.	.	PUNCT
eurjchem-681	30	1	the	the	DET
eurjchem-681	30	2	goal	goal	NOUN
eurjchem-681	30	3	of	of	ADP
eurjchem-681	30	4	the	the	DET
eurjchem-681	30	5	present	present	ADJ
eurjchem-681	30	6	work	work	NOUN
eurjchem-681	30	7	is	be	AUX
eurjchem-681	30	8	to	to	PART
eurjchem-681	30	9	develop	develop	VERB
eurjchem-681	30	10	validated	validate	VERB
eurjchem-681	30	11	,	,	PUNCT
eurjchem-681	30	12	simple	simple	ADJ
eurjchem-681	30	13	,	,	PUNCT
eurjchem-681	30	14	accurate	accurate	ADJ
eurjchem-681	30	15	,	,	PUNCT
eurjchem-681	30	16	precise	precise	ADJ
eurjchem-681	30	17	,	,	PUNCT
eurjchem-681	30	18	economic	economic	ADJ
eurjchem-681	30	19	spectrophotometric	spectrophotometric	ADJ
eurjchem-681	30	20	methods	method	NOUN
eurjchem-681	30	21	due	due	ADP
eurjchem-681	30	22	to	to	ADP
eurjchem-681	30	23	its	its	PRON
eurjchem-681	30	24	wide	wide	ADJ
eurjchem-681	30	25	availability	availability	NOUN
eurjchem-681	30	26	in	in	ADP
eurjchem-681	30	27	most	most	ADJ
eurjchem-681	30	28	quality	quality	NOUN
eurjchem-681	30	29	control	control	NOUN
eurjchem-681	30	30	laboratories	laboratory	NOUN
eurjchem-681	30	31	for	for	ADP
eurjchem-681	30	32	the	the	DET
eurjchem-681	30	33	simultaneous	simultaneous	ADJ
eurjchem-681	30	34	quantification	quantification	NOUN
eurjchem-681	30	35	of	of	ADP
eurjchem-681	30	36	the	the	DET
eurjchem-681	30	37	combined	combine	VERB
eurjchem-681	30	38	diabetes	diabetes	NOUN
eurjchem-681	30	39	with	with	ADP
eurjchem-681	30	40	cholesterol	cholesterol	NOUN
eurjchem-681	30	41	lowering	lower	VERB
eurjchem-681	30	42	drug	drug	NOUN
eurjchem-681	30	43	tablet	tablet	NOUN
eurjchem-681	30	44	.	.	PUNCT
eurjchem-681	31	1	2	2	X
eurjchem-681	31	2	.	.	X
eurjchem-681	31	3	experimental	experimental	ADJ
eurjchem-681	31	4	2.1	2.1	NUM
eurjchem-681	31	5	.	.	PUNCT
eurjchem-681	31	6	instrumentation	instrumentation	NOUN
eurjchem-681	31	7	a	a	DET
eurjchem-681	31	8	double	double	ADJ
eurjchem-681	31	9	beam	beam	NOUN
eurjchem-681	31	10	uv‐vis	uv‐vis	PROPN
eurjchem-681	31	11	spectrophotometer	spectrophotometer	X
eurjchem-681	31	12	(	(	PUNCT
eurjchem-681	31	13	shimadzu	shimadzu	PROPN
eurjchem-681	31	14	,	,	PUNCT
eurjchem-681	31	15	japan	japan	PROPN
eurjchem-681	31	16	)	)	PUNCT
eurjchem-681	31	17	model	model	NOUN
eurjchem-681	31	18	uv‐1601	uv‐1601	PROPN
eurjchem-681	31	19	pc	pc	NOUN
eurjchem-681	31	20	with	with	ADP
eurjchem-681	31	21	matched	match	VERB
eurjchem-681	31	22	quartz	quartz	NOUN
eurjchem-681	31	23	cell	cell	NOUN
eurjchem-681	31	24	(	(	PUNCT
eurjchem-681	31	25	1	1	NUM
eurjchem-681	31	26	cm	cm	NOUN
eurjchem-681	31	27	path	path	NOUN
eurjchem-681	31	28	length	length	NOUN
eurjchem-681	31	29	)	)	PUNCT
eurjchem-681	31	30	connected	connect	VERB
eurjchem-681	31	31	to	to	ADP
eurjchem-681	31	32	ibm	ibm	PROPN
eurjchem-681	31	33	compatible	compatible	ADJ
eurjchem-681	31	34	computer	computer	NOUN
eurjchem-681	31	35	and	and	CCONJ
eurjchem-681	31	36	hp	hp	VERB
eurjchem-681	31	37	680	680	NUM
eurjchem-681	31	38	inkjet	inkjet	NOUN
eurjchem-681	31	39	printer	printer	NOUN
eurjchem-681	31	40	(	(	PUNCT
eurjchem-681	31	41	hewlett	hewlett	PROPN
eurjchem-681	31	42	packard	packard	PROPN
eurjchem-681	31	43	,	,	PUNCT
eurjchem-681	31	44	usa	usa	PROPN
eurjchem-681	31	45	)	)	PUNCT
eurjchem-681	31	46	.	.	PUNCT
eurjchem-681	32	1	the	the	DET
eurjchem-681	32	2	bundled	bundle	VERB
eurjchem-681	32	3	uvpc	uvpc	ADJ
eurjchem-681	32	4	personal	personal	ADJ
eurjchem-681	32	5	spectroscopy	spectroscopy	NOUN
eurjchem-681	32	6	software	software	NOUN
eurjchem-681	32	7	version	version	NOUN
eurjchem-681	32	8	3.7	3.7	NUM
eurjchem-681	32	9	was	be	AUX
eurjchem-681	32	10	used	use	VERB
eurjchem-681	32	11	;	;	PUNCT
eurjchem-681	32	12	at	at	ADP
eurjchem-681	32	13	a	a	DET
eurjchem-681	32	14	spectral	spectral	ADJ
eurjchem-681	32	15	bandwidth	bandwidth	NOUN
eurjchem-681	32	16	2	2	NUM
eurjchem-681	32	17	nm	nm	NOUN
eurjchem-681	32	18	and	and	CCONJ
eurjchem-681	32	19	scanning	scan	VERB
eurjchem-681	32	20	speed	speed	NOUN
eurjchem-681	32	21	of	of	ADP
eurjchem-681	32	22	2800	2800	NUM
eurjchem-681	32	23	nm	nm	NOUN
eurjchem-681	32	24	/	/	SYM
eurjchem-681	32	25	min	min	NOUN
eurjchem-681	32	26	.	.	PROPN
eurjchem-681	32	27	2.2	2.2	NUM
eurjchem-681	32	28	.	.	PUNCT
eurjchem-681	33	1	chemicals	chemical	NOUN
eurjchem-681	33	2	and	and	CCONJ
eurjchem-681	33	3	materials	material	NOUN
eurjchem-681	33	4	pure	pure	ADJ
eurjchem-681	33	5	simvastatin	simvastatin	NOUN
eurjchem-681	33	6	and	and	CCONJ
eurjchem-681	33	7	sitagliptin	sitagliptin	PROPN
eurjchem-681	33	8	phosphate	phosphate	NOUN
eurjchem-681	33	9	monohydrate	monohydrate	NOUN
eurjchem-681	33	10	were	be	AUX
eurjchem-681	33	11	kindly	kindly	ADV
eurjchem-681	33	12	supplied	supply	VERB
eurjchem-681	33	13	by	by	ADP
eurjchem-681	33	14	merck	merck	PROPN
eurjchem-681	33	15	sharp	sharp	PROPN
eurjchem-681	33	16	&	&	CCONJ
eurjchem-681	33	17	dohme	dohme	PROPN
eurjchem-681	33	18	international	international	PROPN
eurjchem-681	33	19	,	,	PUNCT
eurjchem-681	33	20	usa	usa	PROPN
eurjchem-681	33	21	.	.	PUNCT
eurjchem-681	34	1	the	the	DET
eurjchem-681	34	2	marketed	market	VERB
eurjchem-681	34	3	formulation	formulation	NOUN
eurjchem-681	34	4	studied	study	VERB
eurjchem-681	34	5	was	be	AUX
eurjchem-681	34	6	juvisync	juvisync	NOUN
eurjchem-681	34	7	™	™	ADJ
eurjchem-681	34	8	tablets	tablet	NOUN
eurjchem-681	34	9	manufactured	manufacture	VERB
eurjchem-681	34	10	by	by	ADP
eurjchem-681	34	11	merck	merck	PROPN
eurjchem-681	34	12	sharp	sharp	PROPN
eurjchem-681	34	13	dohme	dohme	PROPN
eurjchem-681	34	14	international	international	PROPN
eurjchem-681	34	15	,	,	PUNCT
eurjchem-681	34	16	usa	usa	PROPN
eurjchem-681	34	17	bno	bno	PROPN
eurjchem-681	34	18	g011008	g011008	PROPN
eurjchem-681	34	19	each	each	DET
eurjchem-681	34	20	tablet	tablet	NOUN
eurjchem-681	34	21	contains	contain	VERB
eurjchem-681	34	22	:	:	PUNCT
eurjchem-681	34	23	128.5	128.5	NUM
eurjchem-681	34	24	mg	mg	PROPN
eurjchem-681	34	25	sitagliptin	sitagliptin	PROPN
eurjchem-681	34	26	phosphate	phosphate	PROPN
eurjchem-681	34	27	monohydrate	monohydrate	NOUN
eurjchem-681	34	28	equivalent	equivalent	ADJ
eurjchem-681	34	29	to	to	ADP
eurjchem-681	34	30	100	100	NUM
eurjchem-681	34	31	mg	mg	PROPN
eurjchem-681	34	32	sitagliptin	sitagliptin	NOUN
eurjchem-681	34	33	free	free	ADJ
eurjchem-681	34	34	base	base	NOUN
eurjchem-681	34	35	and	and	CCONJ
eurjchem-681	34	36	20	20	NUM
eurjchem-681	34	37	mg	mg	PROPN
eurjchem-681	34	38	simvastatin	simvastatin	PROPN
eurjchem-681	34	39	.	.	PUNCT
eurjchem-681	35	1	distilled	distil	VERB
eurjchem-681	35	2	water	water	NOUN
eurjchem-681	35	3	from	from	ADP
eurjchem-681	35	4	"	"	PUNCT
eurjchem-681	35	5	aquatron	aquatron	NOUN
eurjchem-681	35	6	"	"	PUNCT
eurjchem-681	35	7	automotive	automotive	ADJ
eurjchem-681	35	8	water	water	NOUN
eurjchem-681	35	9	still	still	ADV
eurjchem-681	35	10	a	a	DET
eurjchem-681	35	11	4000	4000	NUM
eurjchem-681	35	12	(	(	PUNCT
eurjchem-681	35	13	bibby	bibby	PROPN
eurjchem-681	35	14	sterillin	sterillin	PROPN
eurjchem-681	35	15	ltd	ltd	PROPN
eurjchem-681	35	16	.	.	PROPN
eurjchem-681	35	17	,	,	PUNCT
eurjchem-681	35	18	staffordshire	staffordshire	NOUN
eurjchem-681	35	19	,	,	PUNCT
eurjchem-681	35	20	uk	uk	PROPN
eurjchem-681	35	21	)	)	PUNCT
eurjchem-681	35	22	.	.	PUNCT
eurjchem-681	36	1	methanol	methanol	NOUN
eurjchem-681	36	2	from	from	ADP
eurjchem-681	36	3	e.	e.	PROPN
eurjchem-681	36	4	merck	merck	PROPN
eurjchem-681	36	5	,	,	PUNCT
eurjchem-681	36	6	darmstadt	darmstadt	PROPN
eurjchem-681	36	7	,	,	PUNCT
eurjchem-681	36	8	germany	germany	PROPN
eurjchem-681	36	9	.	.	PUNCT
eurjchem-681	37	1	methanol	methanol	NOUN
eurjchem-681	37	2	spectroscopy	spectroscopy	NOUN
eurjchem-681	37	3	grade	grade	NOUN
eurjchem-681	37	4	is	be	AUX
eurjchem-681	37	5	purchased	purchase	VERB
eurjchem-681	37	6	from	from	ADP
eurjchem-681	37	7	el‐nasr	el‐nasr	PROPN
eurjchem-681	37	8	pharmaceutical	pharmaceutical	PROPN
eurjchem-681	37	9	chemicals	chemicals	PROPN
eurjchem-681	37	10	co.	co.	PROPN
eurjchem-681	37	11	,	,	PUNCT
eurjchem-681	37	12	abu‐zaabal	abu‐zaabal	PROPN
eurjchem-681	37	13	,	,	PUNCT
eurjchem-681	37	14	cairo	cairo	PROPN
eurjchem-681	37	15	,	,	PUNCT
eurjchem-681	37	16	egypt	egypt	PROPN
eurjchem-681	37	17	.	.	PUNCT
eurjchem-681	38	1	2.3	2.3	NUM
eurjchem-681	38	2	.	.	PUNCT
eurjchem-681	39	1	standard	standard	ADJ
eurjchem-681	39	2	solutions	solution	NOUN
eurjchem-681	39	3	sitagliptin	sitagliptin	NOUN
eurjchem-681	39	4	phosphate	phosphate	NOUN
eurjchem-681	39	5	monohydrate	monohydrate	PROPN
eurjchem-681	39	6	standard	standard	PROPN
eurjchem-681	39	7	solution	solution	NOUN
eurjchem-681	39	8	(	(	PUNCT
eurjchem-681	39	9	1	1	NUM
eurjchem-681	39	10	mg	mg	NUM
eurjchem-681	39	11	/	/	SYM
eurjchem-681	39	12	ml	ml	NOUN
eurjchem-681	39	13	)	)	PUNCT
eurjchem-681	39	14	was	be	AUX
eurjchem-681	39	15	prepared	prepare	VERB
eurjchem-681	39	16	by	by	ADP
eurjchem-681	39	17	dissolving	dissolve	VERB
eurjchem-681	39	18	100	100	NUM
eurjchem-681	39	19	mg	mg	ADP
eurjchem-681	39	20	of	of	ADP
eurjchem-681	39	21	the	the	DET
eurjchem-681	39	22	pure	pure	ADJ
eurjchem-681	39	23	drug	drug	NOUN
eurjchem-681	39	24	in	in	ADP
eurjchem-681	39	25	30	30	NUM
eurjchem-681	39	26	ml	ml	NOUN
eurjchem-681	39	27	of	of	ADP
eurjchem-681	39	28	70	70	NUM
eurjchem-681	39	29	%	%	NOUN
eurjchem-681	39	30	methanol	methanol	NOUN
eurjchem-681	39	31	into	into	ADP
eurjchem-681	39	32	100	100	NUM
eurjchem-681	39	33	ml	ml	NOUN
eurjchem-681	39	34	measuring	measure	VERB
eurjchem-681	39	35	flask	flask	NOUN
eurjchem-681	39	36	with	with	ADP
eurjchem-681	39	37	continuous	continuous	ADJ
eurjchem-681	39	38	shaking	shaking	NOUN
eurjchem-681	39	39	for	for	ADP
eurjchem-681	39	40	about	about	ADV
eurjchem-681	39	41	10	10	NUM
eurjchem-681	39	42	minutes	minute	NOUN
eurjchem-681	39	43	.	.	PUNCT
eurjchem-681	40	1	the	the	DET
eurjchem-681	40	2	volume	volume	NOUN
eurjchem-681	40	3	was	be	AUX
eurjchem-681	40	4	completed	complete	VERB
eurjchem-681	40	5	to	to	ADP
eurjchem-681	40	6	the	the	DET
eurjchem-681	40	7	mark	mark	NOUN
eurjchem-681	40	8	with	with	ADP
eurjchem-681	40	9	the	the	DET
eurjchem-681	40	10	corresponding	correspond	VERB
eurjchem-681	40	11	solvent	solvent	NOUN
eurjchem-681	40	12	.	.	PUNCT
eurjchem-681	41	1	simvastatin	simvastatin	PROPN
eurjchem-681	41	2	standard	standard	ADJ
eurjchem-681	41	3	solution	solution	NOUN
eurjchem-681	41	4	(	(	PUNCT
eurjchem-681	41	5	0.1	0.1	NUM
eurjchem-681	41	6	mg	mg	NUM
eurjchem-681	41	7	/	/	SYM
eurjchem-681	41	8	ml	ml	NOUN
eurjchem-681	41	9	)	)	PUNCT
eurjchem-681	41	10	was	be	AUX
eurjchem-681	41	11	prepared	prepare	VERB
eurjchem-681	41	12	by	by	ADP
eurjchem-681	41	13	dissolving	dissolve	VERB
eurjchem-681	41	14	10	10	NUM
eurjchem-681	41	15	mg	mg	NOUN
eurjchem-681	41	16	of	of	ADP
eurjchem-681	41	17	the	the	DET
eurjchem-681	41	18	pure	pure	ADJ
eurjchem-681	41	19	base	base	NOUN
eurjchem-681	41	20	in	in	ADP
eurjchem-681	41	21	the	the	DET
eurjchem-681	41	22	same	same	ADJ
eurjchem-681	41	23	solvent	solvent	NOUN
eurjchem-681	41	24	by	by	ADP
eurjchem-681	41	25	the	the	DET
eurjchem-681	41	26	same	same	ADJ
eurjchem-681	41	27	manner	manner	NOUN
eurjchem-681	41	28	to	to	PART
eurjchem-681	41	29	get	get	VERB
eurjchem-681	41	30	the	the	DET
eurjchem-681	41	31	desired	desire	VERB
eurjchem-681	41	32	final	final	ADJ
eurjchem-681	41	33	concentration	concentration	NOUN
eurjchem-681	41	34	.	.	PUNCT
eurjchem-681	42	1	2.4	2.4	NUM
eurjchem-681	42	2	.	.	PUNCT
eurjchem-681	42	3	procedures	procedure	NOUN
eurjchem-681	42	4	2.4.1	2.4.1	NUM
eurjchem-681	42	5	.	.	PUNCT
eurjchem-681	43	1	linearity	linearity	NOUN
eurjchem-681	43	2	aliquots	aliquot	NOUN
eurjchem-681	43	3	of	of	ADP
eurjchem-681	43	4	standard	standard	ADJ
eurjchem-681	43	5	solutions	solution	NOUN
eurjchem-681	43	6	of	of	ADP
eurjchem-681	43	7	sim	sim	NOUN
eurjchem-681	43	8	(	(	PUNCT
eurjchem-681	43	9	0.1	0.1	NUM
eurjchem-681	43	10	mg	mg	PROPN
eurjchem-681	43	11	/	/	SYM
eurjchem-681	43	12	ml	ml	NOUN
eurjchem-681	43	13	)	)	PUNCT
eurjchem-681	43	14	and	and	CCONJ
eurjchem-681	43	15	sit	sit	VERB
eurjchem-681	43	16	(	(	PUNCT
eurjchem-681	43	17	1	1	NUM
eurjchem-681	43	18	mg	mg	NUM
eurjchem-681	43	19	/	/	SYM
eurjchem-681	43	20	ml	ml	NOUN
eurjchem-681	43	21	)	)	PUNCT
eurjchem-681	43	22	equivalent	equivalent	ADJ
eurjchem-681	43	23	to	to	ADP
eurjchem-681	43	24	20‐180	20‐180	NUM
eurjchem-681	43	25	µg	µg	ADV
eurjchem-681	44	1	and	and	CCONJ
eurjchem-681	44	2	0.4‐3.6	0.4‐3.6	PRON
eurjchem-681	44	3	mg	mg	INTJ
eurjchem-681	44	4	in	in	ADP
eurjchem-681	44	5	70	70	NUM
eurjchem-681	44	6	%	%	NOUN
eurjchem-681	44	7	methanol	methanol	NOUN
eurjchem-681	44	8	were	be	AUX
eurjchem-681	44	9	accurately	accurately	ADV
eurjchem-681	44	10	and	and	CCONJ
eurjchem-681	44	11	separately	separately	ADV
eurjchem-681	44	12	transferred	transfer	VERB
eurjchem-681	44	13	into	into	ADP
eurjchem-681	44	14	a	a	DET
eurjchem-681	44	15	series	series	NOUN
eurjchem-681	44	16	of	of	ADP
eurjchem-681	44	17	10	10	NUM
eurjchem-681	44	18	ml	ml	NOUN
eurjchem-681	44	19	volumetric	volumetric	ADJ
eurjchem-681	44	20	flasks	flask	NOUN
eurjchem-681	44	21	and	and	CCONJ
eurjchem-681	44	22	the	the	DET
eurjchem-681	44	23	volume	volume	NOUN
eurjchem-681	44	24	of	of	ADP
eurjchem-681	44	25	each	each	PRON
eurjchem-681	44	26	was	be	AUX
eurjchem-681	44	27	completed	complete	VERB
eurjchem-681	44	28	to	to	ADP
eurjchem-681	44	29	the	the	DET
eurjchem-681	44	30	mark	mark	NOUN
eurjchem-681	44	31	with	with	ADP
eurjchem-681	44	32	the	the	DET
eurjchem-681	44	33	same	same	ADJ
eurjchem-681	44	34	solvent	solvent	NOUN
eurjchem-681	44	35	.	.	PUNCT
eurjchem-681	45	1	for	for	ADP
eurjchem-681	45	2	determination	determination	NOUN
eurjchem-681	45	3	of	of	ADP
eurjchem-681	45	4	sit	sit	NOUN
eurjchem-681	45	5	by	by	ADP
eurjchem-681	45	6	the	the	DET
eurjchem-681	45	7	zero	zero	NUM
eurjchem-681	45	8	order	order	NOUN
eurjchem-681	45	9	method	method	NOUN
eurjchem-681	45	10	,	,	PUNCT
eurjchem-681	45	11	the	the	DET
eurjchem-681	45	12	absorbencies	absorbency	NOUN
eurjchem-681	45	13	of	of	ADP
eurjchem-681	45	14	sit	sit	NOUN
eurjchem-681	45	15	were	be	AUX
eurjchem-681	45	16	measured	measure	VERB
eurjchem-681	45	17	at	at	ADP
eurjchem-681	45	18	266.4	266.4	NUM
eurjchem-681	45	19	nm	nm	NOUN
eurjchem-681	45	20	.	.	PUNCT
eurjchem-681	46	1	for	for	ADP
eurjchem-681	46	2	simultaneous	simultaneous	ADJ
eurjchem-681	46	3	determination	determination	NOUN
eurjchem-681	46	4	of	of	ADP
eurjchem-681	46	5	both	both	DET
eurjchem-681	46	6	drugs	drug	NOUN
eurjchem-681	46	7	by	by	ADP
eurjchem-681	46	8	the	the	DET
eurjchem-681	46	9	third	third	ADJ
eurjchem-681	46	10	derivative	derivative	ADJ
eurjchem-681	46	11	method	method	NOUN
eurjchem-681	46	12	,	,	PUNCT
eurjchem-681	46	13	the	the	DET
eurjchem-681	46	14	peak	peak	NOUN
eurjchem-681	46	15	amplitudes	amplitude	NOUN
eurjchem-681	46	16	(	(	PUNCT
eurjchem-681	46	17	peak	peak	NOUN
eurjchem-681	46	18	&	&	CCONJ
eurjchem-681	46	19	valley	valley	PROPN
eurjchem-681	46	20	)	)	PUNCT
eurjchem-681	46	21	were	be	AUX
eurjchem-681	46	22	measured	measure	VERB
eurjchem-681	46	23	at	at	ADP
eurjchem-681	46	24	275.3‐280.3	275.3‐280.3	NUM
eurjchem-681	46	25	nm	nm	ADJ
eurjchem-681	46	26	and	and	CCONJ
eurjchem-681	46	27	240.5‐244.7	240.5‐244.7	NUM
eurjchem-681	46	28	nm	nm	NOUN
eurjchem-681	46	29	for	for	ADP
eurjchem-681	46	30	sit	sit	NOUN
eurjchem-681	46	31	and	and	CCONJ
eurjchem-681	46	32	sim	sim	ADJ
eurjchem-681	46	33	,	,	PUNCT
eurjchem-681	46	34	respectively	respectively	ADV
eurjchem-681	46	35	.	.	PUNCT
eurjchem-681	47	1	for	for	ADP
eurjchem-681	47	2	simultaneous	simultaneous	ADJ
eurjchem-681	47	3	determination	determination	NOUN
eurjchem-681	47	4	of	of	ADP
eurjchem-681	47	5	both	both	DET
eurjchem-681	47	6	drugs	drug	NOUN
eurjchem-681	47	7	by	by	ADP
eurjchem-681	47	8	the	the	DET
eurjchem-681	47	9	first	first	ADJ
eurjchem-681	47	10	derivative	derivative	NOUN
eurjchem-681	47	11	of	of	ADP
eurjchem-681	47	12	ratio	ratio	NOUN
eurjchem-681	47	13	spectra	spectra	PROPN
eurjchem-681	47	14	method	method	NOUN
eurjchem-681	47	15	,	,	PUNCT
eurjchem-681	47	16	the	the	DET
eurjchem-681	47	17	peak	peak	NOUN
eurjchem-681	47	18	heights	height	NOUN
eurjchem-681	47	19	were	be	AUX
eurjchem-681	47	20	measured	measure	VERB
eurjchem-681	47	21	at	at	ADP
eurjchem-681	47	22	255.9	255.9	NUM
eurjchem-681	47	23	and	and	CCONJ
eurjchem-681	47	24	275.2	275.2	NUM
eurjchem-681	47	25	nm	nm	NOUN
eurjchem-681	47	26	using	use	VERB
eurjchem-681	47	27	18	18	NUM
eurjchem-681	47	28	µg	µg	NOUN
eurjchem-681	47	29	/	/	SYM
eurjchem-681	47	30	ml	ml	NOUN
eurjchem-681	47	31	sim	sim	NOUN
eurjchem-681	47	32	as	as	ADP
eurjchem-681	47	33	devisor	devisor	NOUN
eurjchem-681	47	34	to	to	PART
eurjchem-681	47	35	determine	determine	VERB
eurjchem-681	47	36	sit	sit	VERB
eurjchem-681	47	37	in	in	ADP
eurjchem-681	47	38	a	a	DET
eurjchem-681	47	39	concentration	concentration	NOUN
eurjchem-681	47	40	range	range	NOUN
eurjchem-681	47	41	of	of	ADP
eurjchem-681	47	42	40‐360	40‐360	NUM
eurjchem-681	47	43	µg	µg	NOUN
eurjchem-681	47	44	/	/	SYM
eurjchem-681	47	45	ml	ml	NOUN
eurjchem-681	47	46	and	and	CCONJ
eurjchem-681	47	47	at	at	ADP
eurjchem-681	47	48	228.3	228.3	NUM
eurjchem-681	47	49	,	,	PUNCT
eurjchem-681	47	50	240.5	240.5	NUM
eurjchem-681	47	51	and	and	CCONJ
eurjchem-681	47	52	248.0	248.0	NUM
eurjchem-681	47	53	nm	nm	NOUN
eurjchem-681	47	54	(	(	PUNCT
eurjchem-681	47	55	peak	peak	NOUN
eurjchem-681	47	56	amplitude	amplitude	NOUN
eurjchem-681	47	57	)	)	PUNCT
eurjchem-681	47	58	using	use	VERB
eurjchem-681	47	59	100	100	NUM
eurjchem-681	47	60	µg	µg	NOUN
eurjchem-681	47	61	/	/	SYM
eurjchem-681	47	62	ml	ml	VERB
eurjchem-681	47	63	sit	sit	VERB
eurjchem-681	47	64	as	as	ADP
eurjchem-681	47	65	divisor	divisor	NOUN
eurjchem-681	47	66	to	to	PART
eurjchem-681	47	67	determine	determine	VERB
eurjchem-681	47	68	sim	sim	NOUN
eurjchem-681	47	69	in	in	ADP
eurjchem-681	47	70	a	a	DET
eurjchem-681	47	71	concentration	concentration	NOUN
eurjchem-681	47	72	range	range	NOUN
eurjchem-681	47	73	2‐18	2‐18	NUM
eurjchem-681	47	74	µg	µg	NOUN
eurjchem-681	47	75	/	/	SYM
eurjchem-681	47	76	ml	ml	NOUN
eurjchem-681	47	77	sim	sim	NOUN
eurjchem-681	47	78	.	.	PUNCT
eurjchem-681	48	1	for	for	ADP
eurjchem-681	48	2	determination	determination	NOUN
eurjchem-681	48	3	of	of	ADP
eurjchem-681	48	4	sim	sim	NOUN
eurjchem-681	48	5	by	by	ADP
eurjchem-681	48	6	the	the	DET
eurjchem-681	48	7	ratio	ratio	NOUN
eurjchem-681	48	8	subtraction	subtraction	NOUN
eurjchem-681	48	9	method	method	NOUN
eurjchem-681	48	10	,	,	PUNCT
eurjchem-681	48	11	sim	sim	NOUN
eurjchem-681	48	12	can	can	AUX
eurjchem-681	48	13	be	be	AUX
eurjchem-681	48	14	determined	determine	VERB
eurjchem-681	48	15	by	by	ADP
eurjchem-681	48	16	dividing	divide	VERB
eurjchem-681	48	17	the	the	DET
eurjchem-681	48	18	spectra	spectra	NOUN
eurjchem-681	48	19	of	of	ADP
eurjchem-681	48	20	the	the	DET
eurjchem-681	48	21	mixtures	mixture	NOUN
eurjchem-681	48	22	of	of	ADP
eurjchem-681	48	23	both	both	DET
eurjchem-681	48	24	drugs	drug	NOUN
eurjchem-681	48	25	by	by	ADP
eurjchem-681	48	26	the	the	DET
eurjchem-681	48	27	spectrum	spectrum	NOUN
eurjchem-681	48	28	of	of	ADP
eurjchem-681	48	29	sit	sit	NOUN
eurjchem-681	48	30	(	(	PUNCT
eurjchem-681	48	31	40	40	NUM
eurjchem-681	48	32	µg	µg	NOUN
eurjchem-681	48	33	/	/	SYM
eurjchem-681	48	34	ml	ml	NOUN
eurjchem-681	48	35	)	)	PUNCT
eurjchem-681	48	36	followed	follow	VERB
eurjchem-681	48	37	by	by	ADP
eurjchem-681	48	38	subtracting	subtract	VERB
eurjchem-681	48	39	the	the	DET
eurjchem-681	48	40	constant	constant	ADJ
eurjchem-681	48	41	absorbance	absorbance	NOUN
eurjchem-681	48	42	value	value	NOUN
eurjchem-681	48	43	of	of	ADP
eurjchem-681	48	44	the	the	DET
eurjchem-681	48	45	plateau	plateau	NOUN
eurjchem-681	48	46	and	and	CCONJ
eurjchem-681	48	47	finally	finally	ADV
eurjchem-681	48	48	multiply	multiply	VERB
eurjchem-681	48	49	the	the	DET
eurjchem-681	48	50	produced	produce	VERB
eurjchem-681	48	51	spectrum	spectrum	NOUN
eurjchem-681	48	52	by	by	ADP
eurjchem-681	48	53	the	the	DET
eurjchem-681	48	54	spectrum	spectrum	NOUN
eurjchem-681	48	55	of	of	ADP
eurjchem-681	48	56	the	the	DET
eurjchem-681	48	57	devisor	devisor	NOUN
eurjchem-681	48	58	.	.	PUNCT
eurjchem-681	49	1	2.4.2	2.4.2	NUM
eurjchem-681	49	2	.	.	PUNCT
eurjchem-681	49	3	accuracy	accuracy	NOUN
eurjchem-681	49	4	accuracy	accuracy	NOUN
eurjchem-681	49	5	was	be	AUX
eurjchem-681	49	6	assured	assure	VERB
eurjchem-681	49	7	by	by	ADP
eurjchem-681	49	8	carrying	carry	VERB
eurjchem-681	49	9	out	out	ADP
eurjchem-681	49	10	the	the	DET
eurjchem-681	49	11	previously	previously	ADV
eurjchem-681	49	12	mentioned	mention	VERB
eurjchem-681	49	13	procedures	procedure	NOUN
eurjchem-681	49	14	under	under	ADP
eurjchem-681	49	15	linearity	linearity	NOUN
eurjchem-681	49	16	for	for	ADP
eurjchem-681	49	17	the	the	DET
eurjchem-681	49	18	determination	determination	NOUN
eurjchem-681	49	19	of	of	ADP
eurjchem-681	49	20	different	different	ADJ
eurjchem-681	49	21	concentrations	concentration	NOUN
eurjchem-681	49	22	of	of	ADP
eurjchem-681	49	23	pure	pure	ADJ
eurjchem-681	49	24	sit	sit	NOUN
eurjchem-681	49	25	and	and	CCONJ
eurjchem-681	49	26	sim	sim	NOUN
eurjchem-681	49	27	.	.	PUNCT
eurjchem-681	50	1	the	the	DET
eurjchem-681	50	2	concentrations	concentration	NOUN
eurjchem-681	50	3	were	be	AUX
eurjchem-681	50	4	calculated	calculate	VERB
eurjchem-681	50	5	from	from	ADP
eurjchem-681	50	6	the	the	DET
eurjchem-681	50	7	corresponding	corresponding	ADJ
eurjchem-681	50	8	regression	regression	NOUN
eurjchem-681	50	9	equations	equation	NOUN
eurjchem-681	50	10	.	.	PUNCT
eurjchem-681	51	1	2.4.3	2.4.3	X
eurjchem-681	51	2	.	.	PUNCT
eurjchem-681	51	3	precision	precision	PROPN
eurjchem-681	51	4	2.4.3.1	2.4.3.1	NUM
eurjchem-681	51	5	.	.	PUNCT
eurjchem-681	51	6	intraday	intraday	PROPN
eurjchem-681	51	7	precision	precision	NOUN
eurjchem-681	51	8	(	(	PUNCT
eurjchem-681	51	9	repeatability	repeatability	NOUN
eurjchem-681	51	10	)	)	PUNCT
eurjchem-681	51	11	three	three	NUM
eurjchem-681	51	12	concentrations	concentration	NOUN
eurjchem-681	51	13	of	of	ADP
eurjchem-681	51	14	each	each	DET
eurjchem-681	51	15	drug	drug	NOUN
eurjchem-681	51	16	were	be	AUX
eurjchem-681	51	17	analyzed	analyze	VERB
eurjchem-681	51	18	three	three	NUM
eurjchem-681	51	19	times	time	NOUN
eurjchem-681	51	20	intraday	intraday	NOUN
eurjchem-681	51	21	using	use	VERB
eurjchem-681	51	22	the	the	DET
eurjchem-681	51	23	previously	previously	ADV
eurjchem-681	51	24	mentioned	mention	VERB
eurjchem-681	51	25	procedures	procedure	NOUN
eurjchem-681	51	26	.	.	PUNCT
eurjchem-681	52	1	the	the	DET
eurjchem-681	52	2	percentage	percentage	NOUN
eurjchem-681	52	3	recoveries	recovery	NOUN
eurjchem-681	52	4	of	of	ADP
eurjchem-681	52	5	each	each	DET
eurjchem-681	52	6	drug	drug	NOUN
eurjchem-681	52	7	and	and	CCONJ
eurjchem-681	52	8	its	its	PRON
eurjchem-681	52	9	relative	relative	ADJ
eurjchem-681	52	10	standard	standard	ADJ
eurjchem-681	52	11	deviation	deviation	NOUN
eurjchem-681	52	12	were	be	AUX
eurjchem-681	52	13	calculated	calculate	VERB
eurjchem-681	52	14	using	use	VERB
eurjchem-681	52	15	the	the	DET
eurjchem-681	52	16	suggested	suggest	VERB
eurjchem-681	52	17	methods	method	NOUN
eurjchem-681	52	18	.	.	PUNCT
eurjchem-681	53	1	2.4.3.2	2.4.3.2	NUM
eurjchem-681	53	2	.	.	PUNCT
eurjchem-681	53	3	intermediate	intermediate	ADJ
eurjchem-681	53	4	precision	precision	NOUN
eurjchem-681	53	5	three	three	NUM
eurjchem-681	53	6	concentrations	concentration	NOUN
eurjchem-681	53	7	of	of	ADP
eurjchem-681	53	8	each	each	DET
eurjchem-681	53	9	drug	drug	NOUN
eurjchem-681	53	10	were	be	AUX
eurjchem-681	53	11	analyzed	analyze	VERB
eurjchem-681	53	12	on	on	ADP
eurjchem-681	53	13	three	three	NUM
eurjchem-681	53	14	successive	successive	ADJ
eurjchem-681	53	15	days	day	NOUN
eurjchem-681	53	16	using	use	VERB
eurjchem-681	53	17	the	the	DET
eurjchem-681	53	18	procedure	procedure	NOUN
eurjchem-681	53	19	stated	state	VERB
eurjchem-681	53	20	under	under	ADP
eurjchem-681	53	21	linearity	linearity	NOUN
eurjchem-681	53	22	.	.	PUNCT
eurjchem-681	54	1	the	the	DET
eurjchem-681	54	2	percentage	percentage	NOUN
eurjchem-681	54	3	recoveries	recovery	NOUN
eurjchem-681	54	4	of	of	ADP
eurjchem-681	54	5	each	each	DET
eurjchem-681	54	6	drug	drug	NOUN
eurjchem-681	54	7	and	and	CCONJ
eurjchem-681	54	8	its	its	PRON
eurjchem-681	54	9	relative	relative	ADJ
eurjchem-681	54	10	standard	standard	ADJ
eurjchem-681	54	11	deviation	deviation	NOUN
eurjchem-681	54	12	were	be	AUX
eurjchem-681	54	13	calculated	calculate	VERB
eurjchem-681	54	14	using	use	VERB
eurjchem-681	54	15	the	the	DET
eurjchem-681	54	16	suggested	suggest	VERB
eurjchem-681	54	17	method	method	NOUN
eurjchem-681	54	18	.	.	PUNCT
eurjchem-681	55	1	2.4.4	2.4.4	NUM
eurjchem-681	55	2	.	.	PUNCT
eurjchem-681	56	1	analysis	analysis	NOUN
eurjchem-681	56	2	of	of	ADP
eurjchem-681	56	3	marketed	market	VERB
eurjchem-681	56	4	formulation	formulation	NOUN
eurjchem-681	56	5	ten	ten	NUM
eurjchem-681	56	6	tablets	tablet	NOUN
eurjchem-681	56	7	(	(	PUNCT
eurjchem-681	56	8	juvisync	juvisync	VERB
eurjchem-681	56	9	™	™	ADJ
eurjchem-681	56	10	tablets	tablet	NOUN
eurjchem-681	56	11	)	)	PUNCT
eurjchem-681	56	12	were	be	AUX
eurjchem-681	56	13	weighed	weigh	VERB
eurjchem-681	56	14	and	and	CCONJ
eurjchem-681	56	15	finely	finely	ADV
eurjchem-681	56	16	powdered	powder	VERB
eurjchem-681	56	17	.	.	PUNCT
eurjchem-681	57	1	an	an	DET
eurjchem-681	57	2	amount	amount	NOUN
eurjchem-681	57	3	of	of	ADP
eurjchem-681	57	4	powdered	powdered	ADJ
eurjchem-681	57	5	equivalent	equivalent	NOUN
eurjchem-681	57	6	to	to	ADP
eurjchem-681	57	7	64.25	64.25	NUM
eurjchem-681	57	8	mg	mg	NOUN
eurjchem-681	57	9	sit	sit	VERB
eurjchem-681	57	10	phosphate	phosphate	ADJ
eurjchem-681	57	11	monohydrate	monohydrate	NOUN
eurjchem-681	57	12	and	and	CCONJ
eurjchem-681	57	13	10	10	NUM
eurjchem-681	57	14	mg	mg	NOUN
eurjchem-681	57	15	sim	sim	NOUN
eurjchem-681	57	16	was	be	AUX
eurjchem-681	57	17	transferred	transfer	VERB
eurjchem-681	57	18	into	into	ADP
eurjchem-681	57	19	a	a	DET
eurjchem-681	57	20	100	100	NUM
eurjchem-681	57	21	ml	ml	NOUN
eurjchem-681	57	22	round	round	ADJ
eurjchem-681	57	23	bottom	bottom	ADJ
eurjchem-681	57	24	flask	flask	NOUN
eurjchem-681	57	25	;	;	PUNCT
eurjchem-681	57	26	30	30	NUM
eurjchem-681	57	27	ml	ml	NUM
eurjchem-681	57	28	70	70	NUM
eurjchem-681	57	29	%	%	NOUN
eurjchem-681	57	30	methanol	methanol	NOUN
eurjchem-681	57	31	were	be	AUX
eurjchem-681	57	32	added	add	VERB
eurjchem-681	57	33	and	and	CCONJ
eurjchem-681	57	34	stirred	stir	VERB
eurjchem-681	57	35	for	for	ADP
eurjchem-681	57	36	30	30	NUM
eurjchem-681	57	37	minutes	minute	NOUN
eurjchem-681	57	38	then	then	ADV
eurjchem-681	57	39	filtered	filter	VERB
eurjchem-681	57	40	through	through	ADP
eurjchem-681	57	41	0.5	0.5	NUM
eurjchem-681	57	42	μm	μm	NOUN
eurjchem-681	57	43	whatman	whatman	NOUN
eurjchem-681	57	44	paper	paper	NOUN
eurjchem-681	57	45	into	into	ADP
eurjchem-681	57	46	100	100	NUM
eurjchem-681	57	47	ml	ml	NOUN
eurjchem-681	57	48	measuring	measure	VERB
eurjchem-681	57	49	flask	flask	NOUN
eurjchem-681	57	50	.	.	PUNCT
eurjchem-681	58	1	the	the	DET
eurjchem-681	58	2	residue	residue	NOUN
eurjchem-681	58	3	was	be	AUX
eurjchem-681	58	4	washed	wash	VERB
eurjchem-681	58	5	with	with	ADP
eurjchem-681	58	6	2	2	NUM
eurjchem-681	58	7	x	x	SYM
eurjchem-681	58	8	20	20	NUM
eurjchem-681	58	9	ml	ml	NUM
eurjchem-681	58	10	70	70	NUM
eurjchem-681	58	11	%	%	NOUN
eurjchem-681	58	12	methanol	methanol	NOUN
eurjchem-681	58	13	,	,	PUNCT
eurjchem-681	58	14	and	and	CCONJ
eurjchem-681	58	15	then	then	ADV
eurjchem-681	58	16	the	the	DET
eurjchem-681	58	17	volume	volume	NOUN
eurjchem-681	58	18	was	be	AUX
eurjchem-681	58	19	completed	complete	VERB
eurjchem-681	58	20	to	to	ADP
eurjchem-681	58	21	the	the	DET
eurjchem-681	58	22	mark	mark	NOUN
eurjchem-681	58	23	with	with	ADP
eurjchem-681	58	24	the	the	DET
eurjchem-681	58	25	same	same	ADJ
eurjchem-681	58	26	solvent	solvent	NOUN
eurjchem-681	58	27	and	and	CCONJ
eurjchem-681	58	28	mixed	mixed	ADJ
eurjchem-681	58	29	well	well	ADV
eurjchem-681	58	30	.	.	PUNCT
eurjchem-681	59	1	one	one	NUM
eurjchem-681	59	2	ml	ml	NOUN
eurjchem-681	59	3	of	of	ADP
eurjchem-681	59	4	the	the	DET
eurjchem-681	59	5	resulted	resulted	ADJ
eurjchem-681	59	6	solution	solution	NOUN
eurjchem-681	59	7	was	be	AUX
eurjchem-681	59	8	transferred	transfer	VERB
eurjchem-681	59	9	to	to	ADP
eurjchem-681	59	10	10	10	NUM
eurjchem-681	59	11	ml	ml	NOUN
eurjchem-681	59	12	measuring	measure	VERB
eurjchem-681	59	13	flask	flask	NOUN
eurjchem-681	59	14	then	then	ADV
eurjchem-681	59	15	the	the	DET
eurjchem-681	59	16	volume	volume	NOUN
eurjchem-681	59	17	was	be	AUX
eurjchem-681	59	18	completed	complete	VERB
eurjchem-681	59	19	to	to	ADP
eurjchem-681	59	20	the	the	DET
eurjchem-681	59	21	mark	mark	NOUN
eurjchem-681	59	22	using	use	VERB
eurjchem-681	59	23	the	the	DET
eurjchem-681	59	24	same	same	ADJ
eurjchem-681	59	25	solvent	solvent	NOUN
eurjchem-681	59	26	and	and	CCONJ
eurjchem-681	59	27	mixed	mixed	ADJ
eurjchem-681	59	28	well	well	ADV
eurjchem-681	59	29	.	.	PUNCT
eurjchem-681	60	1	the	the	DET
eurjchem-681	60	2	general	general	ADJ
eurjchem-681	60	3	procedure	procedure	NOUN
eurjchem-681	60	4	was	be	AUX
eurjchem-681	60	5	followed	follow	VERB
eurjchem-681	60	6	as	as	SCONJ
eurjchem-681	60	7	mentioned	mention	VERB
eurjchem-681	60	8	before	before	ADV
eurjchem-681	60	9	and	and	CCONJ
eurjchem-681	60	10	the	the	DET
eurjchem-681	60	11	concentration	concentration	NOUN
eurjchem-681	60	12	of	of	ADP
eurjchem-681	60	13	drug	drug	NOUN
eurjchem-681	60	14	was	be	AUX
eurjchem-681	60	15	calculated	calculate	VERB
eurjchem-681	60	16	from	from	ADP
eurjchem-681	60	17	the	the	DET
eurjchem-681	60	18	corresponding	corresponding	ADJ
eurjchem-681	60	19	regression	regression	NOUN
eurjchem-681	60	20	equation	equation	NOUN
eurjchem-681	60	21	.	.	PUNCT
eurjchem-681	61	1	3	3	X
eurjchem-681	61	2	.	.	NOUN
eurjchem-681	61	3	results	result	NOUN
eurjchem-681	61	4	and	and	CCONJ
eurjchem-681	61	5	discussion	discussion	VERB
eurjchem-681	61	6	a	a	DET
eurjchem-681	61	7	fixed‐dose	fixed‐dose	NOUN
eurjchem-681	61	8	of	of	ADP
eurjchem-681	61	9	sitagliptin	sitagliptin	NOUN
eurjchem-681	61	10	and	and	CCONJ
eurjchem-681	61	11	simvastatin	simvastatin	NOUN
eurjchem-681	61	12	in	in	ADP
eurjchem-681	61	13	their	their	PRON
eurjchem-681	61	14	new	new	ADJ
eurjchem-681	61	15	co‐	co‐	NOUN
eurjchem-681	61	16	formulated	formulate	VERB
eurjchem-681	61	17	pharmaceutical	pharmaceutical	NOUN
eurjchem-681	61	18	dosage	dosage	NOUN
eurjchem-681	61	19	form	form	NOUN
eurjchem-681	61	20	[	[	X
eurjchem-681	61	21	5	5	NUM
eurjchem-681	61	22	]	]	PUNCT
eurjchem-681	61	23	is	be	AUX
eurjchem-681	61	24	the	the	DET
eurjchem-681	61	25	first	first	ADJ
eurjchem-681	61	26	product	product	NOUN
eurjchem-681	61	27	to	to	PART
eurjchem-681	61	28	combine	combine	VERB
eurjchem-681	61	29	a	a	DET
eurjchem-681	61	30	type	type	NOUN
eurjchem-681	61	31	2	2	NUM
eurjchem-681	61	32	diabetes	diabetes	NOUN
eurjchem-681	61	33	drug	drug	NOUN
eurjchem-681	61	34	with	with	ADP
eurjchem-681	61	35	a	a	DET
eurjchem-681	61	36	cholesterol	cholesterol	NOUN
eurjchem-681	61	37	lowering	lower	VERB
eurjchem-681	61	38	drug	drug	NOUN
eurjchem-681	61	39	in	in	ADP
eurjchem-681	61	40	one	one	NUM
eurjchem-681	61	41	tablet	tablet	NOUN
eurjchem-681	61	42	.	.	PUNCT
eurjchem-681	62	1	the	the	DET
eurjchem-681	62	2	aim	aim	NOUN
eurjchem-681	62	3	of	of	ADP
eurjchem-681	62	4	this	this	DET
eurjchem-681	62	5	work	work	NOUN
eurjchem-681	62	6	is	be	AUX
eurjchem-681	62	7	to	to	PART
eurjchem-681	62	8	develop	develop	VERB
eurjchem-681	62	9	simple	simple	ADJ
eurjchem-681	62	10	and	and	CCONJ
eurjchem-681	62	11	accurate	accurate	ADJ
eurjchem-681	62	12	methods	method	NOUN
eurjchem-681	62	13	for	for	ADP
eurjchem-681	62	14	the	the	DET
eurjchem-681	62	15	simultaneous	simultaneous	ADJ
eurjchem-681	62	16	determination	determination	NOUN
eurjchem-681	62	17	of	of	ADP
eurjchem-681	62	18	the	the	DET
eurjchem-681	62	19	new	new	ADJ
eurjchem-681	62	20	combination	combination	NOUN
eurjchem-681	62	21	of	of	ADP
eurjchem-681	62	22	sit	sit	NOUN
eurjchem-681	62	23	and	and	CCONJ
eurjchem-681	62	24	sim	sim	VERB
eurjchem-681	62	25	in	in	ADP
eurjchem-681	62	26	tablets	tablet	NOUN
eurjchem-681	62	27	.	.	PUNCT
eurjchem-681	63	1	molecular	molecular	ADJ
eurjchem-681	63	2	absorption	absorption	NOUN
eurjchem-681	63	3	spectroscopy	spectroscopy	NOUN
eurjchem-681	63	4	has	have	AUX
eurjchem-681	63	5	been	be	AUX
eurjchem-681	63	6	extensively	extensively	ADV
eurjchem-681	63	7	used	use	VERB
eurjchem-681	63	8	for	for	ADP
eurjchem-681	63	9	the	the	DET
eurjchem-681	63	10	determination	determination	NOUN
eurjchem-681	63	11	of	of	ADP
eurjchem-681	63	12	drugs	drug	NOUN
eurjchem-681	63	13	in	in	ADP
eurjchem-681	63	14	pharmaceutical	pharmaceutical	ADJ
eurjchem-681	63	15	preparation	preparation	NOUN
eurjchem-681	63	16	with	with	ADP
eurjchem-681	63	17	a	a	DET
eurjchem-681	63	18	view	view	NOUN
eurjchem-681	63	19	to	to	ADP
eurjchem-681	63	20	the	the	DET
eurjchem-681	63	21	development	development	NOUN
eurjchem-681	63	22	of	of	ADP
eurjchem-681	63	23	analytical	analytical	ADJ
eurjchem-681	63	24	methods	method	NOUN
eurjchem-681	63	25	.	.	PUNCT
eurjchem-681	64	1	the	the	DET
eurjchem-681	64	2	use	use	NOUN
eurjchem-681	64	3	of	of	ADP
eurjchem-681	64	4	this	this	DET
eurjchem-681	64	5	technique	technique	NOUN
eurjchem-681	64	6	for	for	ADP
eurjchem-681	64	7	pharmaceutical	pharmaceutical	NOUN
eurjchem-681	64	8	analyses	analysis	NOUN
eurjchem-681	64	9	has	have	VERB
eurjchem-681	64	10	the	the	DET
eurjchem-681	64	11	inherent	inherent	ADJ
eurjchem-681	64	12	constraint	constraint	NOUN
eurjchem-681	64	13	that	that	SCONJ
eurjchem-681	64	14	most	most	ADV
eurjchem-681	64	15	active	active	ADJ
eurjchem-681	64	16	drugs	drug	NOUN
eurjchem-681	64	17	absorb	absorb	VERB
eurjchem-681	64	18	in	in	ADP
eurjchem-681	64	19	the	the	DET
eurjchem-681	64	20	uv	uv	NOUN
eurjchem-681	64	21	region	region	NOUN
eurjchem-681	64	22	and	and	CCONJ
eurjchem-681	64	23	exhibit	exhibit	VERB
eurjchem-681	64	24	strongly	strongly	ADV
eurjchem-681	64	25	overlapped	overlap	VERB
eurjchem-681	64	26	spectra	spectra	NOUN
eurjchem-681	64	27	that	that	PRON
eurjchem-681	64	28	impede	impede	VERB
eurjchem-681	64	29	their	their	PRON
eurjchem-681	64	30	simultaneous	simultaneous	ADJ
eurjchem-681	64	31	determination	determination	NOUN
eurjchem-681	64	32	.	.	PUNCT
eurjchem-681	65	1	the	the	DET
eurjchem-681	65	2	zero‐order	zero‐order	NOUN
eurjchem-681	65	3	absorption	absorption	NOUN
eurjchem-681	65	4	spectra	spectra	NOUN
eurjchem-681	65	5	(	(	PUNCT
eurjchem-681	65	6	d0	d0	NOUN
eurjchem-681	65	7	)	)	PUNCT
eurjchem-681	65	8	of	of	ADP
eurjchem-681	65	9	a	a	DET
eurjchem-681	65	10	mixture	mixture	NOUN
eurjchem-681	65	11	of	of	ADP
eurjchem-681	65	12	sit	sit	NOUN
eurjchem-681	65	13	and	and	CCONJ
eurjchem-681	65	14	sim	sim	VERB
eurjchem-681	65	15	at	at	ADP
eurjchem-681	65	16	the	the	DET
eurjchem-681	65	17	ratio	ratio	NOUN
eurjchem-681	65	18	of	of	ADP
eurjchem-681	65	19	their	their	PRON
eurjchem-681	65	20	presence	presence	NOUN
eurjchem-681	65	21	in	in	ADP
eurjchem-681	65	22	tablets	tablet	NOUN
eurjchem-681	65	23	showed	show	VERB
eurjchem-681	65	24	overlapping	overlap	VERB
eurjchem-681	65	25	(	(	PUNCT
eurjchem-681	65	26	figure	figure	NOUN
eurjchem-681	65	27	2	2	NUM
eurjchem-681	65	28	)	)	PUNCT
eurjchem-681	65	29	which	which	PRON
eurjchem-681	65	30	allows	allow	VERB
eurjchem-681	65	31	the	the	DET
eurjchem-681	65	32	analysis	analysis	NOUN
eurjchem-681	65	33	of	of	ADP
eurjchem-681	65	34	sit	sit	NOUN
eurjchem-681	65	35	in	in	ADP
eurjchem-681	65	36	presence	presence	NOUN
eurjchem-681	65	37	of	of	ADP
eurjchem-681	65	38	sim	sim	NOUN
eurjchem-681	65	39	at	at	ADP
eurjchem-681	65	40	266.4	266.4	NUM
eurjchem-681	65	41	nm	nm	NOUN
eurjchem-681	65	42	,	,	PUNCT
eurjchem-681	65	43	but	but	CCONJ
eurjchem-681	65	44	prevents	prevent	VERB
eurjchem-681	65	45	the	the	DET
eurjchem-681	65	46	analysis	analysis	NOUN
eurjchem-681	65	47	of	of	ADP
eurjchem-681	65	48	sim	sim	NOUN
eurjchem-681	65	49	.	.	PUNCT
eurjchem-681	66	1	as	as	SCONJ
eurjchem-681	66	2	sit	sit	NOUN
eurjchem-681	66	3	is	be	AUX
eurjchem-681	66	4	soluble	soluble	ADJ
eurjchem-681	66	5	in	in	ADP
eurjchem-681	66	6	water	water	NOUN
eurjchem-681	66	7	and	and	CCONJ
eurjchem-681	66	8	slightly	slightly	ADV
eurjchem-681	66	9	soluble	soluble	ADJ
eurjchem-681	66	10	in	in	ADP
eurjchem-681	66	11	methanol	methanol	NOUN
eurjchem-681	66	12	while	while	NOUN
eurjchem-681	66	13	,	,	PUNCT
eurjchem-681	66	14	sim	sim	NOUN
eurjchem-681	66	15	is	be	AUX
eurjchem-681	66	16	insoluble	insoluble	ADJ
eurjchem-681	66	17	in	in	ADP
eurjchem-681	66	18	water	water	NOUN
eurjchem-681	66	19	and	and	CCONJ
eurjchem-681	66	20	freely	freely	ADV
eurjchem-681	66	21	soluble	soluble	ADJ
eurjchem-681	66	22	in	in	ADP
eurjchem-681	66	23	methanol	methanol	NOUN
eurjchem-681	66	24	trails	trail	NOUN
eurjchem-681	66	25	were	be	AUX
eurjchem-681	66	26	made	make	VERB
eurjchem-681	66	27	to	to	PART
eurjchem-681	66	28	dissolve	dissolve	VERB
eurjchem-681	66	29	the	the	DET
eurjchem-681	66	30	mixture	mixture	NOUN
eurjchem-681	66	31	of	of	ADP
eurjchem-681	66	32	the	the	DET
eurjchem-681	66	33	two	two	NUM
eurjchem-681	66	34	drugs	drug	NOUN
eurjchem-681	66	35	in	in	ADP
eurjchem-681	66	36	methanol	methanol	NOUN
eurjchem-681	66	37	:	:	PUNCT
eurjchem-681	66	38	water	water	NOUN
eurjchem-681	66	39	mixture	mixture	NOUN
eurjchem-681	66	40	.	.	PUNCT
eurjchem-681	67	1	different	different	ADJ
eurjchem-681	67	2	ratios	ratio	NOUN
eurjchem-681	67	3	of	of	ADP
eurjchem-681	67	4	methanol	methanol	NOUN
eurjchem-681	67	5	and	and	CCONJ
eurjchem-681	67	6	abdel‐gawad	abdel‐gawad	NOUN
eurjchem-681	67	7	and	and	CCONJ
eurjchem-681	67	8	elsherif	elsherif	VERB
eurjchem-681	67	9	/	/	SYM
eurjchem-681	67	10	european	european	PROPN
eurjchem-681	67	11	journal	journal	PROPN
eurjchem-681	67	12	of	of	ADP
eurjchem-681	67	13	chemistry	chemistry	NOUN
eurjchem-681	67	14	3	3	NUM
eurjchem-681	67	15	(	(	PUNCT
eurjchem-681	67	16	4	4	NUM
eurjchem-681	67	17	)	)	PUNCT
eurjchem-681	67	18	(	(	PUNCT
eurjchem-681	67	19	2012	2012	NUM
eurjchem-681	67	20	)	)	PUNCT
eurjchem-681	67	21	447‐454	447‐454	PROPN
eurjchem-681	67	22	449	449	NUM
eurjchem-681	67	23	water	water	NOUN
eurjchem-681	67	24	were	be	AUX
eurjchem-681	67	25	tried	try	VERB
eurjchem-681	67	26	and	and	CCONJ
eurjchem-681	67	27	70	70	NUM
eurjchem-681	67	28	%	%	NOUN
eurjchem-681	67	29	were	be	AUX
eurjchem-681	67	30	chosen	choose	VERB
eurjchem-681	67	31	;	;	PUNCT
eurjchem-681	67	32	which	which	PRON
eurjchem-681	67	33	fulfills	fulfill	VERB
eurjchem-681	67	34	complete	complete	ADJ
eurjchem-681	67	35	solubility	solubility	NOUN
eurjchem-681	67	36	.	.	PUNCT
eurjchem-681	68	1	a	a	DET
eurjchem-681	68	2	calibration	calibration	NOUN
eurjchem-681	68	3	curve	curve	NOUN
eurjchem-681	68	4	is	be	AUX
eurjchem-681	68	5	constructed	construct	VERB
eurjchem-681	68	6	relating	relate	VERB
eurjchem-681	68	7	the	the	DET
eurjchem-681	68	8	absorbance	absorbance	NOUN
eurjchem-681	68	9	of	of	ADP
eurjchem-681	68	10	zero	zero	NUM
eurjchem-681	68	11	order	order	NOUN
eurjchem-681	68	12	spectra	spectra	NOUN
eurjchem-681	68	13	of	of	ADP
eurjchem-681	68	14	sit	sit	VERB
eurjchem-681	68	15	at	at	ADP
eurjchem-681	68	16	266.4	266.4	NUM
eurjchem-681	68	17	nm	nm	NOUN
eurjchem-681	68	18	to	to	ADP
eurjchem-681	68	19	the	the	DET
eurjchem-681	68	20	corresponding	corresponding	ADJ
eurjchem-681	68	21	concentrations	concentration	NOUN
eurjchem-681	68	22	where	where	SCONJ
eurjchem-681	68	23	sim	sim	NOUN
eurjchem-681	68	24	shows	show	VERB
eurjchem-681	68	25	no	no	DET
eurjchem-681	68	26	absorbance	absorbance	NOUN
eurjchem-681	68	27	,	,	PUNCT
eurjchem-681	68	28	the	the	DET
eurjchem-681	68	29	regression	regression	NOUN
eurjchem-681	68	30	equation	equation	NOUN
eurjchem-681	68	31	is	be	AUX
eurjchem-681	68	32	computed	compute	VERB
eurjchem-681	68	33	.	.	PUNCT
eurjchem-681	69	1	asit	asit	NOUN
eurjchem-681	69	2	=	=	PROPN
eurjchem-681	69	3	0.0033c	0.0033c	PROPN
eurjchem-681	70	1	+	+	CCONJ
eurjchem-681	70	2	0.0237	0.0237	NUM
eurjchem-681	70	3	r2	r2	NOUN
eurjchem-681	70	4	=	=	PUNCT
eurjchem-681	70	5	0.9997	0.9997	NUM
eurjchem-681	70	6	(	(	PUNCT
eurjchem-681	70	7	1	1	NUM
eurjchem-681	70	8	)	)	PUNCT
eurjchem-681	70	9	where	where	SCONJ
eurjchem-681	70	10	c	c	NOUN
eurjchem-681	70	11	is	be	AUX
eurjchem-681	70	12	the	the	DET
eurjchem-681	70	13	concentration	concentration	NOUN
eurjchem-681	70	14	of	of	ADP
eurjchem-681	70	15	sit	sit	VERB
eurjchem-681	70	16	in	in	ADP
eurjchem-681	70	17	µg	µg	ADV
eurjchem-681	70	18	/	/	SYM
eurjchem-681	70	19	ml	ml	PROPN
eurjchem-681	70	20	,	,	PUNCT
eurjchem-681	70	21	asit	asit	PROPN
eurjchem-681	70	22	is	be	AUX
eurjchem-681	70	23	the	the	DET
eurjchem-681	70	24	peak	peak	NOUN
eurjchem-681	70	25	amplitude	amplitude	NOUN
eurjchem-681	70	26	of	of	ADP
eurjchem-681	70	27	the	the	DET
eurjchem-681	70	28	zero	zero	NUM
eurjchem-681	70	29	order	order	NOUN
eurjchem-681	70	30	spectrum	spectrum	NOUN
eurjchem-681	70	31	of	of	ADP
eurjchem-681	70	32	sit	sit	NOUN
eurjchem-681	70	33	at	at	ADP
eurjchem-681	70	34	266.4	266.4	NUM
eurjchem-681	70	35	nm	nm	NOUN
eurjchem-681	70	36	,	,	PUNCT
eurjchem-681	70	37	and	and	CCONJ
eurjchem-681	70	38	r	r	NOUN
eurjchem-681	70	39	is	be	AUX
eurjchem-681	70	40	the	the	DET
eurjchem-681	70	41	correlation	correlation	NOUN
eurjchem-681	70	42	coefficient	coefficient	NOUN
eurjchem-681	70	43	.	.	PUNCT
eurjchem-681	71	1	figure	figure	NOUN
eurjchem-681	71	2	2	2	NUM
eurjchem-681	72	1	.	.	NOUN
eurjchem-681	72	2	zero	zero	NUM
eurjchem-681	72	3	order	order	NOUN
eurjchem-681	72	4	absorption	absorption	NOUN
eurjchem-681	72	5	spectra	spectra	NOUN
eurjchem-681	72	6	of	of	ADP
eurjchem-681	72	7	10	10	NUM
eurjchem-681	72	8	µg	µg	NOUN
eurjchem-681	72	9	/	/	SYM
eurjchem-681	72	10	ml	ml	NOUN
eurjchem-681	72	11	simvastatin	simvastatin	NOUN
eurjchem-681	72	12	(	(	PUNCT
eurjchem-681	72	13	—	—	PUNCT
eurjchem-681	72	14	)	)	PUNCT
eurjchem-681	72	15	and	and	CCONJ
eurjchem-681	72	16	100	100	NUM
eurjchem-681	72	17	µg	µg	ADJ
eurjchem-681	72	18	/	/	SYM
eurjchem-681	72	19	ml	ml	NOUN
eurjchem-681	72	20	sitagliptin	sitagliptin	NOUN
eurjchem-681	72	21	(	(	PUNCT
eurjchem-681	72	22	…	…	PUNCT
eurjchem-681	72	23	…	…	PUNCT
eurjchem-681	72	24	)	)	PUNCT
eurjchem-681	72	25	.	.	PUNCT
eurjchem-681	73	1	3.1	3.1	NUM
eurjchem-681	73	2	.	.	PUNCT
eurjchem-681	74	1	derivative	derivative	ADJ
eurjchem-681	74	2	spectrophotometric	spectrophotometric	ADJ
eurjchem-681	74	3	method	method	NOUN
eurjchem-681	74	4	(	(	PUNCT
eurjchem-681	74	5	3d	3d	NOUN
eurjchem-681	74	6	)	)	PUNCT
eurjchem-681	74	7	for	for	ADP
eurjchem-681	74	8	further	further	ADJ
eurjchem-681	74	9	improvement	improvement	NOUN
eurjchem-681	74	10	of	of	ADP
eurjchem-681	74	11	the	the	DET
eurjchem-681	74	12	selectivity	selectivity	NOUN
eurjchem-681	74	13	to	to	PART
eurjchem-681	74	14	resolve	resolve	VERB
eurjchem-681	74	15	the	the	DET
eurjchem-681	74	16	overlap	overlap	NOUN
eurjchem-681	74	17	present	present	ADJ
eurjchem-681	74	18	between	between	ADP
eurjchem-681	74	19	sit	sit	VERB
eurjchem-681	74	20	and	and	CCONJ
eurjchem-681	74	21	sim	sim	VERB
eurjchem-681	74	22	in	in	ADP
eurjchem-681	74	23	the	the	DET
eurjchem-681	74	24	mixture	mixture	NOUN
eurjchem-681	74	25	,	,	PUNCT
eurjchem-681	74	26	a	a	DET
eurjchem-681	74	27	simple	simple	ADJ
eurjchem-681	74	28	third	third	ADJ
eurjchem-681	74	29	derivative	derivative	ADJ
eurjchem-681	74	30	method	method	NOUN
eurjchem-681	74	31	(	(	PUNCT
eurjchem-681	74	32	3d	3d	NOUN
eurjchem-681	74	33	)	)	PUNCT
eurjchem-681	75	1	[	[	X
eurjchem-681	75	2	33‐38	33‐38	X
eurjchem-681	75	3	]	]	X
eurjchem-681	75	4	is	be	AUX
eurjchem-681	75	5	applied	apply	VERB
eurjchem-681	75	6	.	.	PUNCT
eurjchem-681	76	1	the	the	DET
eurjchem-681	76	2	method	method	NOUN
eurjchem-681	76	3	is	be	AUX
eurjchem-681	76	4	based	base	VERB
eurjchem-681	76	5	on	on	ADP
eurjchem-681	76	6	measuring	measure	VERB
eurjchem-681	76	7	the	the	DET
eurjchem-681	76	8	sum	sum	NOUN
eurjchem-681	76	9	of	of	ADP
eurjchem-681	76	10	peak	peak	NOUN
eurjchem-681	76	11	amplitudes	amplitude	NOUN
eurjchem-681	76	12	(	(	PUNCT
eurjchem-681	76	13	peak	peak	NOUN
eurjchem-681	76	14	&	&	CCONJ
eurjchem-681	76	15	valley	valley	PROPN
eurjchem-681	76	16	)	)	PUNCT
eurjchem-681	76	17	at	at	ADP
eurjchem-681	76	18	275.3‐280.3	275.3‐280.3	NUM
eurjchem-681	76	19	nm	nm	ADJ
eurjchem-681	76	20	and	and	CCONJ
eurjchem-681	76	21	240.5‐244.7	240.5‐244.7	ADJ
eurjchem-681	76	22	nm	nm	ADJ
eurjchem-681	76	23	(	(	PUNCT
eurjchem-681	76	24	figure	figure	NOUN
eurjchem-681	76	25	3	3	NUM
eurjchem-681	76	26	)	)	PUNCT
eurjchem-681	76	27	for	for	ADP
eurjchem-681	76	28	sit	sit	VERB
eurjchem-681	76	29	and	and	CCONJ
eurjchem-681	76	30	sim	sim	ADJ
eurjchem-681	76	31	,	,	PUNCT
eurjchem-681	76	32	respectively	respectively	ADV
eurjchem-681	76	33	.	.	PUNCT
eurjchem-681	77	1	figure	figure	VERB
eurjchem-681	77	2	3	3	NUM
eurjchem-681	77	3	.	.	PUNCT
eurjchem-681	77	4	third	third	ADJ
eurjchem-681	77	5	derivative	derivative	ADJ
eurjchem-681	77	6	spectra	spectra	NOUN
eurjchem-681	77	7	of	of	ADP
eurjchem-681	77	8	10	10	NUM
eurjchem-681	77	9	µg	µg	NOUN
eurjchem-681	77	10	/	/	SYM
eurjchem-681	77	11	ml	ml	NOUN
eurjchem-681	77	12	simvastatin	simvastatin	NOUN
eurjchem-681	77	13	(	(	PUNCT
eurjchem-681	77	14	—	—	PUNCT
eurjchem-681	77	15	)	)	PUNCT
eurjchem-681	77	16	and	and	CCONJ
eurjchem-681	77	17	100	100	NUM
eurjchem-681	77	18	µg	µg	ADJ
eurjchem-681	77	19	/	/	SYM
eurjchem-681	77	20	ml	ml	NOUN
eurjchem-681	77	21	sitagliptin	sitagliptin	NOUN
eurjchem-681	77	22	(	(	PUNCT
eurjchem-681	77	23	—	—	PUNCT
eurjchem-681	77	24	—	—	PUNCT
eurjchem-681	77	25	)	)	PUNCT
eurjchem-681	77	26	.	.	PUNCT
eurjchem-681	78	1	the	the	DET
eurjchem-681	78	2	main	main	ADJ
eurjchem-681	78	3	instrumental	instrumental	ADJ
eurjchem-681	78	4	parameters	parameter	NOUN
eurjchem-681	78	5	that	that	PRON
eurjchem-681	78	6	affect	affect	VERB
eurjchem-681	78	7	the	the	DET
eurjchem-681	78	8	shape	shape	NOUN
eurjchem-681	78	9	of	of	ADP
eurjchem-681	78	10	the	the	DET
eurjchem-681	78	11	derivative	derivative	ADJ
eurjchem-681	78	12	spectra	spectra	NOUN
eurjchem-681	78	13	such	such	ADJ
eurjchem-681	78	14	as	as	ADP
eurjchem-681	78	15	the	the	DET
eurjchem-681	78	16	speed	speed	NOUN
eurjchem-681	78	17	,	,	PUNCT
eurjchem-681	78	18	the	the	DET
eurjchem-681	78	19	wavelength	wavelength	NOUN
eurjchem-681	78	20	increment	increment	NOUN
eurjchem-681	78	21	over	over	ADP
eurjchem-681	78	22	which	which	PRON
eurjchem-681	78	23	the	the	DET
eurjchem-681	78	24	derivative	derivative	NOUN
eurjchem-681	78	25	is	be	AUX
eurjchem-681	78	26	obtained	obtain	VERB
eurjchem-681	78	27	(	(	PUNCT
eurjchem-681	78	28	δλ	δλ	NOUN
eurjchem-681	78	29	)	)	PUNCT
eurjchem-681	78	30	and	and	CCONJ
eurjchem-681	78	31	degree	degree	NOUN
eurjchem-681	78	32	of	of	ADP
eurjchem-681	78	33	smoothing	smoothing	NOUN
eurjchem-681	78	34	were	be	AUX
eurjchem-681	78	35	optimized	optimize	VERB
eurjchem-681	78	36	to	to	PART
eurjchem-681	78	37	give	give	VERB
eurjchem-681	78	38	a	a	DET
eurjchem-681	78	39	well	well	ADV
eurjchem-681	78	40	resolved	resolve	VERB
eurjchem-681	78	41	peak	peak	NOUN
eurjchem-681	78	42	.	.	PUNCT
eurjchem-681	79	1	linearity	linearity	NOUN
eurjchem-681	79	2	relationship	relationship	NOUN
eurjchem-681	79	3	was	be	AUX
eurjchem-681	79	4	obtained	obtain	VERB
eurjchem-681	79	5	between	between	ADP
eurjchem-681	79	6	the	the	DET
eurjchem-681	79	7	peak	peak	NOUN
eurjchem-681	79	8	amplitudes	amplitude	NOUN
eurjchem-681	79	9	and	and	CCONJ
eurjchem-681	79	10	the	the	DET
eurjchem-681	79	11	concentration	concentration	NOUN
eurjchem-681	79	12	over	over	ADP
eurjchem-681	79	13	the	the	DET
eurjchem-681	79	14	range	range	NOUN
eurjchem-681	79	15	of	of	ADP
eurjchem-681	79	16	40‐360	40‐360	NUM
eurjchem-681	79	17	µg	µg	NOUN
eurjchem-681	79	18	/	/	SYM
eurjchem-681	79	19	ml	ml	NOUN
eurjchem-681	79	20	and	and	CCONJ
eurjchem-681	79	21	2‐18	2‐18	NUM
eurjchem-681	79	22	µg	µg	ADV
eurjchem-681	79	23	/	/	SYM
eurjchem-681	79	24	ml	ml	NOUN
eurjchem-681	79	25	for	for	ADP
eurjchem-681	79	26	sit	sit	NOUN
eurjchem-681	79	27	and	and	CCONJ
eurjchem-681	79	28	sim	sim	ADJ
eurjchem-681	79	29	,	,	PUNCT
eurjchem-681	79	30	respectively	respectively	ADV
eurjchem-681	79	31	(	(	PUNCT
eurjchem-681	79	32	figure	figure	NOUN
eurjchem-681	79	33	4	4	NUM
eurjchem-681	79	34	and	and	CCONJ
eurjchem-681	79	35	5	5	NUM
eurjchem-681	79	36	)	)	PUNCT
eurjchem-681	79	37	,	,	PUNCT
eurjchem-681	79	38	from	from	ADP
eurjchem-681	79	39	which	which	PRON
eurjchem-681	79	40	the	the	DET
eurjchem-681	79	41	linear	linear	ADJ
eurjchem-681	79	42	regression	regression	NOUN
eurjchem-681	79	43	equation	equation	NOUN
eurjchem-681	79	44	were	be	AUX
eurjchem-681	79	45	computed	compute	VERB
eurjchem-681	79	46	and	and	CCONJ
eurjchem-681	79	47	found	find	VERB
eurjchem-681	79	48	to	to	PART
eurjchem-681	79	49	be	be	AUX
eurjchem-681	79	50	:	:	PUNCT
eurjchem-681	79	51	3dsim	3dsim	NUM
eurjchem-681	79	52	=	=	SYM
eurjchem-681	79	53	0.1156	0.1156	NUM
eurjchem-681	79	54	‐	‐	VERB
eurjchem-681	79	55	0.0217	0.0217	NUM
eurjchem-681	79	56	r2	r2	NOUN
eurjchem-681	79	57	=	=	SYM
eurjchem-681	79	58	0.9994	0.9994	NUM
eurjchem-681	79	59	for	for	ADP
eurjchem-681	79	60	sim	sim	ADJ
eurjchem-681	79	61	(	(	PUNCT
eurjchem-681	79	62	2	2	NUM
eurjchem-681	79	63	)	)	PUNCT
eurjchem-681	79	64	3dsit	3dsit	NUM
eurjchem-681	79	65	=	=	SYM
eurjchem-681	79	66	0.0039	0.0039	NUM
eurjchem-681	79	67	+	+	CCONJ
eurjchem-681	79	68	0.0279	0.0279	NUM
eurjchem-681	79	69	r2	r2	NOUN
eurjchem-681	79	70	=	=	PUNCT
eurjchem-681	79	71	0.9995	0.9995	NUM
eurjchem-681	79	72	for	for	ADP
eurjchem-681	79	73	sit	sit	NOUN
eurjchem-681	79	74	(	(	PUNCT
eurjchem-681	79	75	3	3	NUM
eurjchem-681	79	76	)	)	PUNCT
eurjchem-681	79	77	where	where	SCONJ
eurjchem-681	79	78	3d	3d	NOUN
eurjchem-681	79	79	is	be	AUX
eurjchem-681	79	80	the	the	DET
eurjchem-681	79	81	sum	sum	NOUN
eurjchem-681	79	82	of	of	ADP
eurjchem-681	79	83	peak	peak	NOUN
eurjchem-681	79	84	amplitudes	amplitude	NOUN
eurjchem-681	79	85	(	(	PUNCT
eurjchem-681	79	86	peak	peak	NOUN
eurjchem-681	79	87	&	&	CCONJ
eurjchem-681	79	88	valley	valley	NOUN
eurjchem-681	79	89	)	)	PUNCT
eurjchem-681	79	90	of	of	ADP
eurjchem-681	79	91	the	the	DET
eurjchem-681	79	92	spectra	spectra	NOUN
eurjchem-681	79	93	,	,	PUNCT
eurjchem-681	79	94	c	c	PROPN
eurjchem-681	79	95	is	be	AUX
eurjchem-681	79	96	the	the	DET
eurjchem-681	79	97	corresponding	corresponding	ADJ
eurjchem-681	79	98	concentration	concentration	NOUN
eurjchem-681	79	99	and	and	CCONJ
eurjchem-681	79	100	r	r	NOUN
eurjchem-681	79	101	is	be	AUX
eurjchem-681	79	102	the	the	DET
eurjchem-681	79	103	correlation	correlation	NOUN
eurjchem-681	79	104	coefficient	coefficient	NOUN
eurjchem-681	79	105	.	.	PUNCT
eurjchem-681	80	1	figure	figure	VERB
eurjchem-681	80	2	4	4	NUM
eurjchem-681	80	3	.	.	PUNCT
eurjchem-681	80	4	third	third	ADJ
eurjchem-681	80	5	derivative	derivative	ADJ
eurjchem-681	80	6	spectra	spectra	NOUN
eurjchem-681	80	7	of	of	ADP
eurjchem-681	80	8	simvastatin	simvastatin	NOUN
eurjchem-681	80	9	in	in	ADP
eurjchem-681	80	10	the	the	DET
eurjchem-681	80	11	range	range	NOUN
eurjchem-681	80	12	of	of	ADP
eurjchem-681	80	13	2‐18	2‐18	NUM
eurjchem-681	80	14	µg	µg	NOUN
eurjchem-681	80	15	/	/	SYM
eurjchem-681	80	16	ml	ml	NOUN
eurjchem-681	80	17	.	.	PUNCT
eurjchem-681	80	18	figure	figure	NOUN
eurjchem-681	80	19	5	5	NUM
eurjchem-681	80	20	.	.	PUNCT
eurjchem-681	80	21	third	third	ADJ
eurjchem-681	80	22	derivative	derivative	ADJ
eurjchem-681	80	23	spectra	spectra	NOUN
eurjchem-681	80	24	of	of	ADP
eurjchem-681	80	25	sitagliptin	sitagliptin	NOUN
eurjchem-681	80	26	in	in	ADP
eurjchem-681	80	27	the	the	DET
eurjchem-681	80	28	range	range	NOUN
eurjchem-681	80	29	of	of	ADP
eurjchem-681	80	30	40‐360	40‐360	NUM
eurjchem-681	80	31	µg	µg	NOUN
eurjchem-681	80	32	/	/	SYM
eurjchem-681	80	33	ml	ml	NOUN
eurjchem-681	80	34	.	.	NOUN
eurjchem-681	80	35	3.2	3.2	NUM
eurjchem-681	80	36	.	.	PUNCT
eurjchem-681	81	1	ratio‐spectra	ratio‐spectra	ADJ
eurjchem-681	81	2	derivative	derivative	ADJ
eurjchem-681	81	3	spectrophotometric	spectrophotometric	ADJ
eurjchem-681	81	4	method	method	NOUN
eurjchem-681	81	5	(	(	PUNCT
eurjchem-681	81	6	dd1	dd1	NOUN
eurjchem-681	81	7	)	)	PUNCT
eurjchem-681	81	8	as	as	SCONJ
eurjchem-681	81	9	can	can	AUX
eurjchem-681	81	10	be	be	AUX
eurjchem-681	81	11	seen	see	VERB
eurjchem-681	81	12	in	in	ADP
eurjchem-681	81	13	figure	figure	NOUN
eurjchem-681	81	14	2	2	NUM
eurjchem-681	81	15	,	,	PUNCT
eurjchem-681	81	16	the	the	DET
eurjchem-681	81	17	absorption	absorption	NOUN
eurjchem-681	81	18	spectra	spectra	NOUN
eurjchem-681	81	19	of	of	ADP
eurjchem-681	81	20	sit	sit	NOUN
eurjchem-681	81	21	and	and	CCONJ
eurjchem-681	81	22	sim	sim	NOUN
eurjchem-681	81	23	;	;	PUNCT
eurjchem-681	81	24	the	the	DET
eurjchem-681	81	25	maximum	maximum	ADJ
eurjchem-681	81	26	wavelengths	wavelength	NOUN
eurjchem-681	81	27	of	of	ADP
eurjchem-681	81	28	the	the	DET
eurjchem-681	81	29	two	two	NUM
eurjchem-681	81	30	compounds	compound	NOUN
eurjchem-681	81	31	are	be	AUX
eurjchem-681	81	32	close	close	ADJ
eurjchem-681	81	33	to	to	ADP
eurjchem-681	81	34	each	each	DET
eurjchem-681	81	35	other	other	ADJ
eurjchem-681	81	36	and	and	CCONJ
eurjchem-681	81	37	their	their	PRON
eurjchem-681	81	38	spectra	spectra	ADJ
eurjchem-681	81	39	overlap	overlap	NOUN
eurjchem-681	81	40	at	at	ADP
eurjchem-681	81	41	200‐260	200‐260	NUM
eurjchem-681	81	42	nm	nm	NOUN
eurjchem-681	81	43	;	;	PUNCT
eurjchem-681	81	44	which	which	PRON
eurjchem-681	81	45	ca	can	AUX
eurjchem-681	81	46	n’t	not	PART
eurjchem-681	81	47	permits	permit	VERB
eurjchem-681	81	48	the	the	DET
eurjchem-681	81	49	determination	determination	NOUN
eurjchem-681	81	50	of	of	ADP
eurjchem-681	81	51	the	the	DET
eurjchem-681	81	52	cited	cite	VERB
eurjchem-681	81	53	drugs	drug	NOUN
eurjchem-681	81	54	.	.	PUNCT
eurjchem-681	82	1	therefore	therefore	ADV
eurjchem-681	82	2	,	,	PUNCT
eurjchem-681	82	3	the	the	DET
eurjchem-681	82	4	simultaneous	simultaneous	ADJ
eurjchem-681	82	5	determination	determination	NOUN
eurjchem-681	82	6	of	of	ADP
eurjchem-681	82	7	sit	sit	NOUN
eurjchem-681	82	8	and	and	CCONJ
eurjchem-681	82	9	sim	sim	NOUN
eurjchem-681	82	10	is	be	AUX
eurjchem-681	82	11	impossible	impossible	ADJ
eurjchem-681	82	12	by	by	ADP
eurjchem-681	82	13	classical	classical	ADJ
eurjchem-681	82	14	spectrophotometry	spectrophotometry	NOUN
eurjchem-681	82	15	and	and	CCONJ
eurjchem-681	82	16	it	it	PRON
eurjchem-681	82	17	is	be	AUX
eurjchem-681	82	18	necessary	necessary	ADJ
eurjchem-681	82	19	to	to	PART
eurjchem-681	82	20	use	use	VERB
eurjchem-681	82	21	another	another	DET
eurjchem-681	82	22	method	method	NOUN
eurjchem-681	82	23	to	to	PART
eurjchem-681	82	24	solve	solve	VERB
eurjchem-681	82	25	this	this	DET
eurjchem-681	82	26	problem	problem	NOUN
eurjchem-681	82	27	.	.	PUNCT
eurjchem-681	83	1	salinas	salinas	PROPN
eurjchem-681	83	2	et	et	PROPN
eurjchem-681	83	3	al	al	PROPN
eurjchem-681	83	4	.	.	PUNCT
eurjchem-681	84	1	[	[	X
eurjchem-681	84	2	39	39	NUM
eurjchem-681	84	3	]	]	PUNCT
eurjchem-681	84	4	designed	design	VERB
eurjchem-681	84	5	a	a	DET
eurjchem-681	84	6	spectrophotometric	spectrophotometric	ADJ
eurjchem-681	84	7	method	method	NOUN
eurjchem-681	84	8	,	,	PUNCT
eurjchem-681	84	9	which	which	PRON
eurjchem-681	84	10	is	be	AUX
eurjchem-681	84	11	based	base	VERB
eurjchem-681	84	12	on	on	ADP
eurjchem-681	84	13	the	the	DET
eurjchem-681	84	14	derivation	derivation	NOUN
eurjchem-681	84	15	of	of	ADP
eurjchem-681	84	16	the	the	DET
eurjchem-681	84	17	ratio‐spectra	ratio‐spectra	PROPN
eurjchem-681	84	18	for	for	ADP
eurjchem-681	84	19	resolving	resolve	VERB
eurjchem-681	84	20	binary	binary	ADJ
eurjchem-681	84	21	mixtures	mixture	NOUN
eurjchem-681	84	22	.	.	PUNCT
eurjchem-681	85	1	the	the	DET
eurjchem-681	85	2	main	main	ADJ
eurjchem-681	85	3	advantage	advantage	NOUN
eurjchem-681	85	4	of	of	ADP
eurjchem-681	85	5	the	the	DET
eurjchem-681	85	6	ratio‐	ratio‐	NOUN
eurjchem-681	85	7	spectra	spectra	ADJ
eurjchem-681	85	8	derivative	derivative	ADJ
eurjchem-681	85	9	spectrophotometry	spectrophotometry	NOUN
eurjchem-681	85	10	is	be	AUX
eurjchem-681	85	11	the	the	DET
eurjchem-681	85	12	chance	chance	NOUN
eurjchem-681	85	13	of	of	ADP
eurjchem-681	85	14	doing	do	VERB
eurjchem-681	85	15	easy	easy	ADJ
eurjchem-681	85	16	measurements	measurement	NOUN
eurjchem-681	85	17	in	in	ADP
eurjchem-681	85	18	correspondence	correspondence	NOUN
eurjchem-681	85	19	of	of	ADP
eurjchem-681	85	20	peaks	peak	NOUN
eurjchem-681	85	21	so	so	SCONJ
eurjchem-681	85	22	it	it	PRON
eurjchem-681	85	23	permits	permit	VERB
eurjchem-681	85	24	the	the	DET
eurjchem-681	85	25	use	use	NOUN
eurjchem-681	85	26	of	of	ADP
eurjchem-681	85	27	the	the	DET
eurjchem-681	85	28	wavelength	wavelength	NOUN
eurjchem-681	85	29	of	of	ADP
eurjchem-681	85	30	highest	high	ADJ
eurjchem-681	85	31	value	value	NOUN
eurjchem-681	85	32	of	of	ADP
eurjchem-681	85	33	analytical	analytical	ADJ
eurjchem-681	85	34	signals	signal	NOUN
eurjchem-681	85	35	.	.	PUNCT
eurjchem-681	86	1	moreover	moreover	ADV
eurjchem-681	86	2	,	,	PUNCT
eurjchem-681	86	3	the	the	DET
eurjchem-681	86	4	presence	presence	NOUN
eurjchem-681	86	5	of	of	ADP
eurjchem-681	86	6	a	a	DET
eurjchem-681	86	7	lot	lot	NOUN
eurjchem-681	86	8	of	of	ADP
eurjchem-681	86	9	maxima	maxima	NOUN
eurjchem-681	86	10	and	and	CCONJ
eurjchem-681	86	11	minima	minima	NOUN
eurjchem-681	86	12	is	be	AUX
eurjchem-681	86	13	another	another	DET
eurjchem-681	86	14	advantage	advantage	NOUN
eurjchem-681	86	15	by	by	ADP
eurjchem-681	86	16	the	the	DET
eurjchem-681	86	17	fact	fact	NOUN
eurjchem-681	86	18	that	that	SCONJ
eurjchem-681	86	19	these	these	DET
eurjchem-681	86	20	wavelengths	wavelength	NOUN
eurjchem-681	86	21	give	give	VERB
eurjchem-681	86	22	an	an	DET
eurjchem-681	86	23	opportunity	opportunity	NOUN
eurjchem-681	86	24	for	for	ADP
eurjchem-681	86	25	the	the	DET
eurjchem-681	86	26	determination	determination	NOUN
eurjchem-681	86	27	of	of	ADP
eurjchem-681	86	28	active	active	ADJ
eurjchem-681	86	29	compounds	compound	NOUN
eurjchem-681	86	30	in	in	ADP
eurjchem-681	86	31	the	the	DET
eurjchem-681	86	32	presence	presence	NOUN
eurjchem-681	86	33	of	of	ADP
eurjchem-681	86	34	other	other	ADJ
eurjchem-681	86	35	compounds	compound	NOUN
eurjchem-681	86	36	and	and	CCONJ
eurjchem-681	86	37	excipients	excipient	NOUN
eurjchem-681	86	38	which	which	PRON
eurjchem-681	86	39	possibly	possibly	ADV
eurjchem-681	86	40	interfere	interfere	VERB
eurjchem-681	86	41	the	the	DET
eurjchem-681	86	42	assay	assay	NOUN
eurjchem-681	86	43	.	.	PUNCT
eurjchem-681	87	1	in	in	ADP
eurjchem-681	87	2	this	this	DET
eurjchem-681	87	3	method	method	NOUN
eurjchem-681	87	4	the	the	DET
eurjchem-681	87	5	absorption	absorption	NOUN
eurjchem-681	87	6	spectrum	spectrum	NOUN
eurjchem-681	87	7	of	of	ADP
eurjchem-681	87	8	the	the	DET
eurjchem-681	87	9	mixture	mixture	NOUN
eurjchem-681	87	10	(	(	PUNCT
eurjchem-681	87	11	absorbance	absorbance	NOUN
eurjchem-681	87	12	at	at	ADP
eurjchem-681	87	13	each	each	DET
eurjchem-681	87	14	wavelength	wavelength	NOUN
eurjchem-681	87	15	)	)	PUNCT
eurjchem-681	87	16	is	be	AUX
eurjchem-681	87	17	divided	divide	VERB
eurjchem-681	87	18	by	by	ADP
eurjchem-681	87	19	the	the	DET
eurjchem-681	87	20	absorption	absorption	NOUN
eurjchem-681	87	21	spectrum	spectrum	NOUN
eurjchem-681	87	22	of	of	ADP
eurjchem-681	87	23	a	a	DET
eurjchem-681	87	24	standard	standard	ADJ
eurjchem-681	87	25	solution	solution	NOUN
eurjchem-681	87	26	of	of	ADP
eurjchem-681	87	27	one	one	NUM
eurjchem-681	87	28	of	of	ADP
eurjchem-681	87	29	the	the	DET
eurjchem-681	87	30	components	component	NOUN
eurjchem-681	87	31	,	,	PUNCT
eurjchem-681	87	32	and	and	CCONJ
eurjchem-681	87	33	the	the	DET
eurjchem-681	87	34	first	first	ADJ
eurjchem-681	87	35	derivative	derivative	NOUN
eurjchem-681	87	36	of	of	ADP
eurjchem-681	87	37	the	the	DET
eurjchem-681	87	38	ratio	ratio	NOUN
eurjchem-681	87	39	spectrum	spectrum	NOUN
eurjchem-681	87	40	is	be	AUX
eurjchem-681	87	41	450	450	NUM
eurjchem-681	87	42	abdel‐gawad	abdel‐gawad	NOUN
eurjchem-681	87	43	and	and	CCONJ
eurjchem-681	87	44	elsherif	elsherif	VERB
eurjchem-681	87	45	/	/	SYM
eurjchem-681	87	46	european	european	PROPN
eurjchem-681	87	47	journal	journal	PROPN
eurjchem-681	87	48	of	of	ADP
eurjchem-681	87	49	chemistry	chemistry	NOUN
eurjchem-681	87	50	3	3	NUM
eurjchem-681	87	51	(	(	PUNCT
eurjchem-681	87	52	4	4	NUM
eurjchem-681	87	53	)	)	PUNCT
eurjchem-681	87	54	(	(	PUNCT
eurjchem-681	87	55	2012	2012	NUM
eurjchem-681	87	56	)	)	PUNCT
eurjchem-681	88	1	447‐454	447‐454	PROPN
eurjchem-681	88	2	obtained	obtain	VERB
eurjchem-681	88	3	.	.	PUNCT
eurjchem-681	89	1	the	the	DET
eurjchem-681	89	2	concentration	concentration	NOUN
eurjchem-681	89	3	of	of	ADP
eurjchem-681	89	4	the	the	DET
eurjchem-681	89	5	other	other	ADJ
eurjchem-681	89	6	component	component	NOUN
eurjchem-681	89	7	is	be	AUX
eurjchem-681	89	8	then	then	ADV
eurjchem-681	89	9	determined	determine	VERB
eurjchem-681	89	10	from	from	ADP
eurjchem-681	89	11	a	a	DET
eurjchem-681	89	12	calibration	calibration	NOUN
eurjchem-681	89	13	graph	graph	NOUN
eurjchem-681	89	14	.	.	PUNCT
eurjchem-681	90	1	the	the	DET
eurjchem-681	90	2	main	main	ADJ
eurjchem-681	90	3	parameters	parameter	NOUN
eurjchem-681	90	4	that	that	PRON
eurjchem-681	90	5	affect	affect	VERB
eurjchem-681	90	6	the	the	DET
eurjchem-681	90	7	shape	shape	NOUN
eurjchem-681	90	8	of	of	ADP
eurjchem-681	90	9	the	the	DET
eurjchem-681	90	10	ratio	ratio	NOUN
eurjchem-681	90	11	spectra	spectra	NOUN
eurjchem-681	90	12	which	which	PRON
eurjchem-681	90	13	are	be	AUX
eurjchem-681	90	14	wavelength	wavelength	NOUN
eurjchem-681	90	15	,	,	PUNCT
eurjchem-681	90	16	scanning	scan	VERB
eurjchem-681	90	17	speed	speed	NOUN
eurjchem-681	90	18	,	,	PUNCT
eurjchem-681	90	19	the	the	DET
eurjchem-681	90	20	concentration	concentration	NOUN
eurjchem-681	90	21	of	of	ADP
eurjchem-681	90	22	the	the	DET
eurjchem-681	90	23	standard	standard	ADJ
eurjchem-681	90	24	solution	solution	NOUN
eurjchem-681	90	25	used	use	VERB
eurjchem-681	90	26	as	as	ADP
eurjchem-681	90	27	a	a	DET
eurjchem-681	90	28	divisor	divisor	NOUN
eurjchem-681	90	29	,	,	PUNCT
eurjchem-681	90	30	the	the	DET
eurjchem-681	90	31	wavelength	wavelength	NOUN
eurjchem-681	90	32	increment	increment	NOUN
eurjchem-681	90	33	over	over	ADP
eurjchem-681	90	34	which	which	PRON
eurjchem-681	90	35	the	the	DET
eurjchem-681	90	36	derivative	derivative	NOUN
eurjchem-681	90	37	is	be	AUX
eurjchem-681	90	38	obtained	obtain	VERB
eurjchem-681	90	39	and	and	CCONJ
eurjchem-681	90	40	the	the	DET
eurjchem-681	90	41	smoothing	smooth	VERB
eurjchem-681	90	42	function	function	NOUN
eurjchem-681	90	43	are	be	AUX
eurjchem-681	90	44	carefully	carefully	ADV
eurjchem-681	90	45	tested	test	VERB
eurjchem-681	90	46	.	.	PUNCT
eurjchem-681	91	1	accordingly	accordingly	ADV
eurjchem-681	91	2	,	,	PUNCT
eurjchem-681	91	3	the	the	DET
eurjchem-681	91	4	first	first	ADJ
eurjchem-681	91	5	derivative	derivative	NOUN
eurjchem-681	91	6	of	of	ADP
eurjchem-681	91	7	the	the	DET
eurjchem-681	91	8	ratio	ratio	NOUN
eurjchem-681	91	9	spectra	spectra	PROPN
eurjchem-681	91	10	presented	present	VERB
eurjchem-681	91	11	in	in	ADP
eurjchem-681	91	12	figure	figure	NOUN
eurjchem-681	91	13	6	6	NUM
eurjchem-681	91	14	and	and	CCONJ
eurjchem-681	91	15	7	7	NUM
eurjchem-681	91	16	for	for	ADP
eurjchem-681	91	17	sitagliptin	sitagliptin	NOUN
eurjchem-681	91	18	and	and	CCONJ
eurjchem-681	91	19	simvastatin	simvastatin	NOUN
eurjchem-681	91	20	in	in	ADP
eurjchem-681	91	21	the	the	DET
eurjchem-681	91	22	different	different	ADJ
eurjchem-681	91	23	concentration	concentration	NOUN
eurjchem-681	91	24	may	may	AUX
eurjchem-681	91	25	provide	provide	VERB
eurjchem-681	91	26	a	a	DET
eurjchem-681	91	27	good	good	ADJ
eurjchem-681	91	28	proof	proof	NOUN
eurjchem-681	91	29	for	for	ADP
eurjchem-681	91	30	this	this	DET
eurjchem-681	91	31	understanding	understanding	NOUN
eurjchem-681	91	32	.	.	PUNCT
eurjchem-681	92	1	different	different	ADJ
eurjchem-681	92	2	concentrations	concentration	NOUN
eurjchem-681	92	3	of	of	ADP
eurjchem-681	92	4	divisor	divisor	NOUN
eurjchem-681	92	5	were	be	AUX
eurjchem-681	92	6	also	also	ADV
eurjchem-681	92	7	tried	try	VERB
eurjchem-681	92	8	for	for	ADP
eurjchem-681	92	9	sit	sit	VERB
eurjchem-681	92	10	and	and	CCONJ
eurjchem-681	92	11	sim	sim	ADJ
eurjchem-681	92	12	which	which	PRON
eurjchem-681	92	13	give	give	VERB
eurjchem-681	92	14	the	the	DET
eurjchem-681	92	15	best	good	ADJ
eurjchem-681	92	16	regarding	regard	VERB
eurjchem-681	92	17	average	average	ADJ
eurjchem-681	92	18	recovery	recovery	NOUN
eurjchem-681	92	19	percent	percent	NOUN
eurjchem-681	92	20	when	when	SCONJ
eurjchem-681	92	21	they	they	PRON
eurjchem-681	92	22	were	be	AUX
eurjchem-681	92	23	used	use	VERB
eurjchem-681	92	24	for	for	ADP
eurjchem-681	92	25	the	the	DET
eurjchem-681	92	26	prediction	prediction	NOUN
eurjchem-681	92	27	of	of	ADP
eurjchem-681	92	28	sit	sit	VERB
eurjchem-681	92	29	and	and	CCONJ
eurjchem-681	92	30	sim	sim	ADJ
eurjchem-681	92	31	concentrations	concentration	NOUN
eurjchem-681	92	32	in	in	ADP
eurjchem-681	92	33	bulk	bulk	ADJ
eurjchem-681	92	34	powder	powder	NOUN
eurjchem-681	92	35	as	as	ADV
eurjchem-681	92	36	well	well	ADV
eurjchem-681	92	37	as	as	ADP
eurjchem-681	92	38	in	in	ADP
eurjchem-681	92	39	laboratory	laboratory	NOUN
eurjchem-681	92	40	prepared	prepare	VERB
eurjchem-681	92	41	mixtures	mixture	NOUN
eurjchem-681	92	42	.	.	PUNCT
eurjchem-681	93	1	figure	figure	VERB
eurjchem-681	93	2	6	6	NUM
eurjchem-681	93	3	.	.	PUNCT
eurjchem-681	94	1	dd1‐spectra	dd1‐spectra	PROPN
eurjchem-681	94	2	of	of	ADP
eurjchem-681	94	3	sitagliptin	sitagliptin	NOUN
eurjchem-681	94	4	in	in	ADP
eurjchem-681	94	5	the	the	DET
eurjchem-681	94	6	range	range	NOUN
eurjchem-681	94	7	of	of	ADP
eurjchem-681	94	8	40‐360	40‐360	NUM
eurjchem-681	94	9	µg	µg	NOUN
eurjchem-681	94	10	/	/	SYM
eurjchem-681	94	11	ml	ml	NOUN
eurjchem-681	94	12	using	use	VERB
eurjchem-681	94	13	18	18	NUM
eurjchem-681	94	14	µg	µg	NOUN
eurjchem-681	94	15	/	/	SYM
eurjchem-681	94	16	ml	ml	NOUN
eurjchem-681	94	17	simvastatin	simvastatin	NOUN
eurjchem-681	94	18	as	as	ADP
eurjchem-681	94	19	divisor	divisor	NOUN
eurjchem-681	94	20	.	.	PUNCT
eurjchem-681	95	1	figure	figure	NOUN
eurjchem-681	95	2	7	7	NUM
eurjchem-681	95	3	.	.	PUNCT
eurjchem-681	96	1	dd1‐spectra	dd1‐spectra	PROPN
eurjchem-681	96	2	of	of	ADP
eurjchem-681	96	3	simvastatin	simvastatin	NOUN
eurjchem-681	96	4	in	in	ADP
eurjchem-681	96	5	the	the	DET
eurjchem-681	96	6	range	range	NOUN
eurjchem-681	96	7	of	of	ADP
eurjchem-681	96	8	2‐18	2‐18	NUM
eurjchem-681	96	9	µg	µg	NOUN
eurjchem-681	96	10	/	/	SYM
eurjchem-681	96	11	ml	ml	VERB
eurjchem-681	96	12	using	use	VERB
eurjchem-681	96	13	100	100	NUM
eurjchem-681	96	14	µg	µg	ADJ
eurjchem-681	96	15	/	/	SYM
eurjchem-681	96	16	ml	ml	NOUN
eurjchem-681	96	17	sitagliptin	sitagliptin	NOUN
eurjchem-681	96	18	as	as	ADP
eurjchem-681	96	19	divisor	divisor	NOUN
eurjchem-681	96	20	.	.	PUNCT
eurjchem-681	97	1	the	the	DET
eurjchem-681	97	2	method	method	NOUN
eurjchem-681	97	3	was	be	AUX
eurjchem-681	97	4	applied	apply	VERB
eurjchem-681	97	5	by	by	ADP
eurjchem-681	97	6	measuring	measure	VERB
eurjchem-681	97	7	the	the	DET
eurjchem-681	97	8	peak	peak	NOUN
eurjchem-681	97	9	height	height	NOUN
eurjchem-681	97	10	at	at	ADP
eurjchem-681	97	11	255.9	255.9	NUM
eurjchem-681	97	12	and	and	CCONJ
eurjchem-681	97	13	275.2	275.2	NUM
eurjchem-681	97	14	nm	nm	NOUN
eurjchem-681	97	15	using	use	VERB
eurjchem-681	97	16	18	18	NUM
eurjchem-681	97	17	µg	µg	NOUN
eurjchem-681	97	18	/	/	SYM
eurjchem-681	97	19	ml	ml	NOUN
eurjchem-681	97	20	sim	sim	NOUN
eurjchem-681	97	21	as	as	ADP
eurjchem-681	97	22	devisor	devisor	NOUN
eurjchem-681	97	23	over	over	ADP
eurjchem-681	97	24	a	a	DET
eurjchem-681	97	25	concentration	concentration	NOUN
eurjchem-681	97	26	range	range	NOUN
eurjchem-681	97	27	of	of	ADP
eurjchem-681	97	28	40‐360	40‐360	NUM
eurjchem-681	97	29	µg	µg	NOUN
eurjchem-681	97	30	/	/	SYM
eurjchem-681	97	31	ml	ml	NOUN
eurjchem-681	97	32	of	of	ADP
eurjchem-681	97	33	sit	sit	NOUN
eurjchem-681	97	34	(	(	PUNCT
eurjchem-681	97	35	figure	figure	NOUN
eurjchem-681	97	36	6	6	NUM
eurjchem-681	97	37	)	)	PUNCT
eurjchem-681	97	38	and	and	CCONJ
eurjchem-681	97	39	at	at	ADP
eurjchem-681	97	40	228.3	228.3	NUM
eurjchem-681	97	41	,	,	PUNCT
eurjchem-681	97	42	240.5	240.5	NUM
eurjchem-681	97	43	and	and	CCONJ
eurjchem-681	97	44	248.0	248.0	NUM
eurjchem-681	97	45	nm	nm	NOUN
eurjchem-681	97	46	using	use	VERB
eurjchem-681	97	47	100	100	NUM
eurjchem-681	97	48	µg	µg	NOUN
eurjchem-681	97	49	/	/	SYM
eurjchem-681	97	50	ml	ml	NOUN
eurjchem-681	97	51	of	of	ADP
eurjchem-681	97	52	sit	sit	VERB
eurjchem-681	97	53	as	as	ADP
eurjchem-681	97	54	divisor	divisor	NOUN
eurjchem-681	97	55	over	over	ADP
eurjchem-681	97	56	a	a	DET
eurjchem-681	97	57	concentration	concentration	NOUN
eurjchem-681	97	58	range	range	NOUN
eurjchem-681	97	59	of	of	ADP
eurjchem-681	97	60	2‐18	2‐18	NUM
eurjchem-681	97	61	µg	µg	NOUN
eurjchem-681	97	62	/	/	SYM
eurjchem-681	97	63	ml	ml	NOUN
eurjchem-681	97	64	sim	sim	ADJ
eurjchem-681	97	65	(	(	PUNCT
eurjchem-681	97	66	figure	figure	NOUN
eurjchem-681	97	67	7	7	NUM
eurjchem-681	97	68	)	)	PUNCT
eurjchem-681	97	69	.	.	PUNCT
eurjchem-681	98	1	the	the	DET
eurjchem-681	98	2	linear	linear	PROPN
eurjchem-681	98	3	regression	regression	NOUN
eurjchem-681	98	4	equations	equation	NOUN
eurjchem-681	98	5	are	be	AUX
eurjchem-681	98	6	found	find	VERB
eurjchem-681	98	7	to	to	PART
eurjchem-681	98	8	be	be	AUX
eurjchem-681	98	9	:	:	PUNCT
eurjchem-681	98	10	psit	psit	VERB
eurjchem-681	98	11	=	=	PUNCT
eurjchem-681	98	12	0.0086c	0.0086c	PROPN
eurjchem-681	98	13	+	+	CCONJ
eurjchem-681	98	14	0.053	0.053	NUM
eurjchem-681	98	15	r2	r2	NOUN
eurjchem-681	98	16	=	=	SYM
eurjchem-681	98	17	0.9995	0.9995	NUM
eurjchem-681	98	18	(	(	PUNCT
eurjchem-681	98	19	4	4	NUM
eurjchem-681	98	20	)	)	PUNCT
eurjchem-681	98	21	psim=	psim=	NOUN
eurjchem-681	98	22	0.0120c	0.0120c	NOUN
eurjchem-681	98	23	‐	‐	NOUN
eurjchem-681	98	24	0.0841	0.0841	NUM
eurjchem-681	98	25	r2	r2	NOUN
eurjchem-681	98	26	=	=	SYM
eurjchem-681	98	27	0.9994	0.9994	NUM
eurjchem-681	98	28	(	(	PUNCT
eurjchem-681	98	29	5	5	NUM
eurjchem-681	98	30	)	)	PUNCT
eurjchem-681	98	31	where	where	SCONJ
eurjchem-681	98	32	,	,	PUNCT
eurjchem-681	98	33	c	c	PROPN
eurjchem-681	98	34	is	be	AUX
eurjchem-681	98	35	the	the	DET
eurjchem-681	98	36	concentration	concentration	NOUN
eurjchem-681	98	37	in	in	ADP
eurjchem-681	98	38	µg	µg	ADV
eurjchem-681	98	39	/	/	SYM
eurjchem-681	98	40	ml	ml	NOUN
eurjchem-681	98	41	,	,	PUNCT
eurjchem-681	98	42	p	p	NOUN
eurjchem-681	98	43	is	be	AUX
eurjchem-681	98	44	the	the	DET
eurjchem-681	98	45	peak	peak	NOUN
eurjchem-681	98	46	amplitude	amplitude	NOUN
eurjchem-681	98	47	of	of	ADP
eurjchem-681	98	48	the	the	DET
eurjchem-681	98	49	first	first	ADJ
eurjchem-681	98	50	derivative	derivative	NOUN
eurjchem-681	98	51	of	of	ADP
eurjchem-681	98	52	the	the	DET
eurjchem-681	98	53	ratio	ratio	NOUN
eurjchem-681	98	54	spectrum	spectrum	NOUN
eurjchem-681	98	55	curve	curve	NOUN
eurjchem-681	98	56	and	and	CCONJ
eurjchem-681	98	57	r	r	NOUN
eurjchem-681	98	58	is	be	AUX
eurjchem-681	98	59	the	the	DET
eurjchem-681	98	60	correlation	correlation	NOUN
eurjchem-681	98	61	coefficient	coefficient	NOUN
eurjchem-681	98	62	.	.	PUNCT
eurjchem-681	99	1	3.3	3.3	NUM
eurjchem-681	99	2	.	.	PUNCT
eurjchem-681	100	1	ratio	ratio	NOUN
eurjchem-681	100	2	subtraction	subtraction	NOUN
eurjchem-681	100	3	method	method	NOUN
eurjchem-681	100	4	the	the	DET
eurjchem-681	100	5	ratio	ratio	NOUN
eurjchem-681	100	6	subtraction	subtraction	NOUN
eurjchem-681	100	7	technique	technique	NOUN
eurjchem-681	101	1	[	[	X
eurjchem-681	101	2	40	40	NUM
eurjchem-681	101	3	]	]	PUNCT
eurjchem-681	101	4	depends	depend	VERB
eurjchem-681	101	5	on	on	ADP
eurjchem-681	101	6	that	that	PRON
eurjchem-681	101	7	,	,	PUNCT
eurjchem-681	101	8	if	if	SCONJ
eurjchem-681	101	9	you	you	PRON
eurjchem-681	101	10	have	have	VERB
eurjchem-681	101	11	a	a	DET
eurjchem-681	101	12	mixture	mixture	NOUN
eurjchem-681	101	13	of	of	ADP
eurjchem-681	101	14	two	two	NUM
eurjchem-681	101	15	drugs	drug	NOUN
eurjchem-681	101	16	x	x	PUNCT
eurjchem-681	101	17	and	and	CCONJ
eurjchem-681	101	18	y	y	PROPN
eurjchem-681	101	19	of	of	ADP
eurjchem-681	101	20	overlapping	overlap	VERB
eurjchem-681	101	21	spectra	spectra	NOUN
eurjchem-681	101	22	,	,	PUNCT
eurjchem-681	101	23	you	you	PRON
eurjchem-681	101	24	can	can	AUX
eurjchem-681	101	25	determine	determine	VERB
eurjchem-681	101	26	x	x	PUNCT
eurjchem-681	101	27	by	by	ADP
eurjchem-681	101	28	dividing	divide	VERB
eurjchem-681	101	29	the	the	DET
eurjchem-681	101	30	spectrum	spectrum	NOUN
eurjchem-681	101	31	of	of	ADP
eurjchem-681	101	32	the	the	DET
eurjchem-681	101	33	mixture	mixture	NOUN
eurjchem-681	101	34	by	by	ADP
eurjchem-681	101	35	known	know	VERB
eurjchem-681	101	36	concentration	concentration	NOUN
eurjchem-681	101	37	of	of	ADP
eurjchem-681	101	38	y	y	PROPN
eurjchem-681	101	39	as	as	ADP
eurjchem-681	101	40	a	a	DET
eurjchem-681	101	41	divisor	divisor	NOUN
eurjchem-681	101	42	(	(	PUNCT
eurjchem-681	101	43	yʹ	yʹ	PROPN
eurjchem-681	101	44	)	)	PUNCT
eurjchem-681	101	45	.	.	PUNCT
eurjchem-681	102	1	the	the	DET
eurjchem-681	102	2	division	division	NOUN
eurjchem-681	102	3	will	will	AUX
eurjchem-681	102	4	give	give	VERB
eurjchem-681	102	5	a	a	DET
eurjchem-681	102	6	new	new	ADJ
eurjchem-681	102	7	curve	curve	NOUN
eurjchem-681	102	8	that	that	PRON
eurjchem-681	102	9	represents	represent	VERB
eurjchem-681	102	10	(	(	PUNCT
eurjchem-681	102	11	x	x	SYM
eurjchem-681	102	12	/	/	SYM
eurjchem-681	102	13	y	y	NOUN
eurjchem-681	102	14	)	)	PUNCT
eurjchem-681	103	1	+	+	CCONJ
eurjchem-681	103	2	constant	constant	ADJ
eurjchem-681	103	3	.	.	PUNCT
eurjchem-681	104	1	if	if	SCONJ
eurjchem-681	104	2	we	we	PRON
eurjchem-681	104	3	subtract	subtract	VERB
eurjchem-681	104	4	this	this	DET
eurjchem-681	104	5	constant	constant	ADJ
eurjchem-681	104	6	,	,	PUNCT
eurjchem-681	104	7	then	then	ADV
eurjchem-681	104	8	multiply	multiply	VERB
eurjchem-681	104	9	the	the	DET
eurjchem-681	104	10	new	new	ADJ
eurjchem-681	104	11	curve	curve	NOUN
eurjchem-681	104	12	obtained	obtain	VERB
eurjchem-681	104	13	after	after	ADP
eurjchem-681	104	14	subtraction	subtraction	NOUN
eurjchem-681	104	15	by	by	ADP
eurjchem-681	104	16	yʹ	yʹ	PROPN
eurjchem-681	104	17	(	(	PUNCT
eurjchem-681	104	18	the	the	DET
eurjchem-681	104	19	divisor	divisor	NOUN
eurjchem-681	104	20	)	)	PUNCT
eurjchem-681	104	21	,	,	PUNCT
eurjchem-681	104	22	therefore	therefore	ADV
eurjchem-681	104	23	we	we	PRON
eurjchem-681	104	24	can	can	AUX
eurjchem-681	104	25	obtain	obtain	VERB
eurjchem-681	104	26	the	the	DET
eurjchem-681	104	27	curve	curve	NOUN
eurjchem-681	104	28	of	of	ADP
eurjchem-681	104	29	x	x	X
eurjchem-681	104	30	again	again	ADV
eurjchem-681	104	31	.	.	PUNCT
eurjchem-681	105	1	this	this	PRON
eurjchem-681	105	2	can	can	AUX
eurjchem-681	105	3	be	be	AUX
eurjchem-681	105	4	summarized	summarize	VERB
eurjchem-681	105	5	as	as	ADP
eurjchem-681	105	6	the	the	DET
eurjchem-681	105	7	following	following	NOUN
eurjchem-681	105	8	:	:	PUNCT
eurjchem-681	106	1	=	=	SYM
eurjchem-681	106	2	=	=	PUNCT
eurjchem-681	107	1	+	+	CCONJ
eurjchem-681	107	2	constant	constant	ADJ
eurjchem-681	107	3	(	(	PUNCT
eurjchem-681	107	4	6	6	NUM
eurjchem-681	107	5	)	)	PUNCT
eurjchem-681	107	6	constant	constant	ADJ
eurjchem-681	107	7	–	–	PUNCT
eurjchem-681	107	8	constant	constant	ADJ
eurjchem-681	107	9	=	=	SYM
eurjchem-681	107	10	(	(	PUNCT
eurjchem-681	107	11	7	7	NUM
eurjchem-681	107	12	)	)	PUNCT
eurjchem-681	107	13	.	.	PUNCT
eurjchem-681	108	1	(	(	PUNCT
eurjchem-681	108	2	8)	8)	NUM
eurjchem-681	108	3	this	this	DET
eurjchem-681	108	4	constant	constant	ADJ
eurjchem-681	108	5	can	can	AUX
eurjchem-681	108	6	be	be	AUX
eurjchem-681	108	7	determined	determine	VERB
eurjchem-681	108	8	directly	directly	ADV
eurjchem-681	108	9	from	from	ADP
eurjchem-681	108	10	the	the	DET
eurjchem-681	108	11	curve	curve	NOUN
eurjchem-681	108	12	by	by	ADP
eurjchem-681	108	13	the	the	DET
eurjchem-681	108	14	straight	straight	ADJ
eurjchem-681	108	15	line	line	NOUN
eurjchem-681	108	16	which	which	PRON
eurjchem-681	108	17	is	be	AUX
eurjchem-681	108	18	parallel	parallel	ADJ
eurjchem-681	108	19	to	to	ADP
eurjchem-681	108	20	λ	λ	PROPN
eurjchem-681	108	21	axis	axis	NOUN
eurjchem-681	108	22	in	in	ADP
eurjchem-681	108	23	this	this	DET
eurjchem-681	108	24	region	region	NOUN
eurjchem-681	108	25	.	.	PUNCT
eurjchem-681	109	1	practically	practically	ADV
eurjchem-681	109	2	,	,	PUNCT
eurjchem-681	109	3	the	the	DET
eurjchem-681	109	4	ratio	ratio	NOUN
eurjchem-681	109	5	subtraction	subtraction	NOUN
eurjchem-681	109	6	method	method	NOUN
eurjchem-681	109	7	starts	start	VERB
eurjchem-681	109	8	by	by	ADP
eurjchem-681	109	9	scanning	scan	VERB
eurjchem-681	109	10	zero‐	zero‐	NUM
eurjchem-681	109	11	order	order	NOUN
eurjchem-681	109	12	spectra	spectra	NOUN
eurjchem-681	109	13	of	of	ADP
eurjchem-681	109	14	the	the	DET
eurjchem-681	109	15	prepared	prepare	VERB
eurjchem-681	109	16	standard	standard	ADJ
eurjchem-681	109	17	solutions	solution	NOUN
eurjchem-681	109	18	of	of	ADP
eurjchem-681	109	19	sim	sim	NOUN
eurjchem-681	109	20	in	in	ADP
eurjchem-681	109	21	70	70	NUM
eurjchem-681	109	22	%	%	NOUN
eurjchem-681	109	23	methanol	methanol	NOUN
eurjchem-681	109	24	(	(	PUNCT
eurjchem-681	109	25	figure	figure	NOUN
eurjchem-681	109	26	2	2	NUM
eurjchem-681	109	27	)	)	PUNCT
eurjchem-681	109	28	,	,	PUNCT
eurjchem-681	109	29	then	then	ADV
eurjchem-681	109	30	the	the	DET
eurjchem-681	109	31	linearity	linearity	NOUN
eurjchem-681	109	32	is	be	AUX
eurjchem-681	109	33	checked	check	VERB
eurjchem-681	109	34	between	between	ADP
eurjchem-681	109	35	absorbance	absorbance	NOUN
eurjchem-681	109	36	at	at	ADP
eurjchem-681	109	37	the	the	DET
eurjchem-681	109	38	selected	select	VERB
eurjchem-681	109	39	wavelength	wavelength	NOUN
eurjchem-681	109	40	at	at	ADP
eurjchem-681	109	41	237.5	237.5	NUM
eurjchem-681	109	42	nm	nm	NOUN
eurjchem-681	109	43	and	and	CCONJ
eurjchem-681	109	44	the	the	DET
eurjchem-681	109	45	corresponding	corresponding	ADJ
eurjchem-681	109	46	concentration	concentration	NOUN
eurjchem-681	109	47	of	of	ADP
eurjchem-681	109	48	sim	sim	NOUN
eurjchem-681	109	49	.	.	PUNCT
eurjchem-681	110	1	the	the	DET
eurjchem-681	110	2	method	method	NOUN
eurjchem-681	110	3	depends	depend	VERB
eurjchem-681	110	4	on	on	ADP
eurjchem-681	110	5	that	that	PRON
eurjchem-681	110	6	,	,	PUNCT
eurjchem-681	110	7	when	when	SCONJ
eurjchem-681	110	8	a	a	DET
eurjchem-681	110	9	mixture	mixture	NOUN
eurjchem-681	110	10	of	of	ADP
eurjchem-681	110	11	sim	sim	ADJ
eurjchem-681	110	12	(	(	PUNCT
eurjchem-681	110	13	x	x	NOUN
eurjchem-681	110	14	)	)	PUNCT
eurjchem-681	110	15	and	and	CCONJ
eurjchem-681	110	16	sit	sit	VERB
eurjchem-681	110	17	(	(	PUNCT
eurjchem-681	110	18	y	y	NOUN
eurjchem-681	110	19	)	)	PUNCT
eurjchem-681	110	20	;	;	PUNCT
eurjchem-681	110	21	where	where	SCONJ
eurjchem-681	110	22	the	the	DET
eurjchem-681	110	23	spectrum	spectrum	NOUN
eurjchem-681	110	24	of	of	ADP
eurjchem-681	110	25	(	(	PUNCT
eurjchem-681	110	26	y	y	NOUN
eurjchem-681	110	27	)	)	PUNCT
eurjchem-681	110	28	is	be	AUX
eurjchem-681	110	29	more	more	ADV
eurjchem-681	110	30	extended	extended	ADJ
eurjchem-681	110	31	(	(	PUNCT
eurjchem-681	110	32	figure	figure	NOUN
eurjchem-681	110	33	2	2	NUM
eurjchem-681	110	34	)	)	PUNCT
eurjchem-681	110	35	,	,	PUNCT
eurjchem-681	110	36	the	the	DET
eurjchem-681	110	37	determination	determination	NOUN
eurjchem-681	110	38	of	of	ADP
eurjchem-681	110	39	(	(	PUNCT
eurjchem-681	110	40	x	x	X
eurjchem-681	110	41	)	)	PUNCT
eurjchem-681	110	42	could	could	AUX
eurjchem-681	110	43	be	be	AUX
eurjchem-681	110	44	done	do	VERB
eurjchem-681	110	45	by	by	ADP
eurjchem-681	110	46	scanning	scan	VERB
eurjchem-681	110	47	the	the	DET
eurjchem-681	110	48	zero	zero	NUM
eurjchem-681	110	49	order	order	NOUN
eurjchem-681	110	50	absorption	absorption	NOUN
eurjchem-681	110	51	spectra	spectra	NOUN
eurjchem-681	110	52	of	of	ADP
eurjchem-681	110	53	the	the	DET
eurjchem-681	110	54	laboratory‐prepared	laboratory‐prepare	VERB
eurjchem-681	110	55	mixtures	mixture	NOUN
eurjchem-681	110	56	(	(	PUNCT
eurjchem-681	110	57	sim	sim	ADJ
eurjchem-681	110	58	and	and	CCONJ
eurjchem-681	110	59	sit	sit	VERB
eurjchem-681	110	60	)	)	PUNCT
eurjchem-681	110	61	,	,	PUNCT
eurjchem-681	110	62	dividing	divide	VERB
eurjchem-681	110	63	them	they	PRON
eurjchem-681	110	64	by	by	ADP
eurjchem-681	110	65	carefully	carefully	ADV
eurjchem-681	110	66	chosen	choose	VERB
eurjchem-681	110	67	concentration	concentration	NOUN
eurjchem-681	110	68	(	(	PUNCT
eurjchem-681	110	69	40	40	NUM
eurjchem-681	110	70	µg	µg	NOUN
eurjchem-681	110	71	/	/	SYM
eurjchem-681	110	72	ml	ml	NOUN
eurjchem-681	110	73	)	)	PUNCT
eurjchem-681	110	74	of	of	ADP
eurjchem-681	110	75	standard	standard	ADJ
eurjchem-681	110	76	sit	sit	NOUN
eurjchem-681	110	77	(	(	PUNCT
eurjchem-681	110	78	y	y	NOUN
eurjchem-681	110	79	=	=	PUNCT
eurjchem-681	110	80	divisor	divisor	NOUN
eurjchem-681	110	81	)	)	PUNCT
eurjchem-681	110	82	producing	produce	VERB
eurjchem-681	110	83	a	a	DET
eurjchem-681	110	84	new	new	ADJ
eurjchem-681	110	85	ratio	ratio	NOUN
eurjchem-681	110	86	spectra	spectra	NOUN
eurjchem-681	110	87	that	that	PRON
eurjchem-681	110	88	represent	represent	VERB
eurjchem-681	110	89	(	(	PUNCT
eurjchem-681	110	90	x	x	SYM
eurjchem-681	110	91	/	/	SYM
eurjchem-681	110	92	y	y	NOUN
eurjchem-681	110	93	)	)	PUNCT
eurjchem-681	110	94	+	+	CCONJ
eurjchem-681	110	95	constant	constant	ADJ
eurjchem-681	110	96	as	as	SCONJ
eurjchem-681	110	97	shown	show	VERB
eurjchem-681	110	98	in	in	ADP
eurjchem-681	110	99	figure	figure	NOUN
eurjchem-681	110	100	8	8	NUM
eurjchem-681	110	101	then	then	ADV
eurjchem-681	110	102	subtraction	subtraction	NOUN
eurjchem-681	110	103	of	of	ADP
eurjchem-681	110	104	the	the	DET
eurjchem-681	110	105	absorbance	absorbance	NOUN
eurjchem-681	110	106	values	value	NOUN
eurjchem-681	110	107	of	of	ADP
eurjchem-681	110	108	these	these	DET
eurjchem-681	110	109	constants	constant	NOUN
eurjchem-681	110	110	(	(	PUNCT
eurjchem-681	110	111	y/	y/	NOUN
eurjchem-681	110	112	yʹ	yʹ	PROPN
eurjchem-681	110	113	)	)	PUNCT
eurjchem-681	110	114	in	in	ADP
eurjchem-681	110	115	plateau	plateau	NOUN
eurjchem-681	110	116	as	as	SCONJ
eurjchem-681	110	117	shown	show	VERB
eurjchem-681	110	118	in	in	ADP
eurjchem-681	110	119	figure	figure	NOUN
eurjchem-681	110	120	9	9	NUM
eurjchem-681	110	121	,	,	PUNCT
eurjchem-681	110	122	followed	follow	VERB
eurjchem-681	110	123	by	by	ADP
eurjchem-681	110	124	multiplication	multiplication	NOUN
eurjchem-681	110	125	of	of	ADP
eurjchem-681	110	126	the	the	DET
eurjchem-681	110	127	obtained	obtain	VERB
eurjchem-681	110	128	spectra	spectra	NOUN
eurjchem-681	110	129	by	by	ADP
eurjchem-681	110	130	(	(	PUNCT
eurjchem-681	110	131	yʹ	yʹ	PROPN
eurjchem-681	110	132	)	)	PUNCT
eurjchem-681	110	133	the	the	DET
eurjchem-681	110	134	divisor	divisor	NOUN
eurjchem-681	110	135	as	as	SCONJ
eurjchem-681	110	136	shown	show	VERB
eurjchem-681	110	137	in	in	ADP
eurjchem-681	110	138	figure	figure	NOUN
eurjchem-681	110	139	10	10	NUM
eurjchem-681	110	140	.	.	PUNCT
eurjchem-681	111	1	figure	figure	VERB
eurjchem-681	111	2	8	8	NUM
eurjchem-681	111	3	.	.	PUNCT
eurjchem-681	112	1	absorption	absorption	NOUN
eurjchem-681	112	2	spectra	spectra	NOUN
eurjchem-681	112	3	of	of	ADP
eurjchem-681	112	4	laboratory	laboratory	NOUN
eurjchem-681	112	5	prepared	prepare	VERB
eurjchem-681	112	6	mixtures	mixture	NOUN
eurjchem-681	112	7	of	of	ADP
eurjchem-681	112	8	sitagliptin	sitagliptin	NOUN
eurjchem-681	112	9	and	and	CCONJ
eurjchem-681	112	10	simvastatin	simvastatin	NOUN
eurjchem-681	112	11	in	in	ADP
eurjchem-681	112	12	the	the	DET
eurjchem-681	112	13	ratio	ratio	NOUN
eurjchem-681	112	14	of	of	ADP
eurjchem-681	112	15	100:10	100:10	PROPN
eurjchem-681	112	16	(	(	PUNCT
eurjchem-681	112	17	—	—	PUNCT
eurjchem-681	112	18	)	)	PUNCT
eurjchem-681	112	19	,	,	PUNCT
eurjchem-681	112	20	60:12	60:12	NUM
eurjchem-681	112	21	(	(	PUNCT
eurjchem-681	112	22	.	.	PUNCT
eurjchem-681	112	23	…	…	PUNCT
eurjchem-681	112	24	)	)	PUNCT
eurjchem-681	112	25	and	and	CCONJ
eurjchem-681	112	26	40:16	40:16	NUM
eurjchem-681	112	27	(	(	PUNCT
eurjchem-681	112	28	—	—	PUNCT
eurjchem-681	112	29	—	—	PUNCT
eurjchem-681	112	30	)	)	PUNCT
eurjchem-681	112	31	.	.	PUNCT
eurjchem-681	113	1	finally	finally	ADV
eurjchem-681	113	2	,	,	PUNCT
eurjchem-681	113	3	the	the	DET
eurjchem-681	113	4	original	original	ADJ
eurjchem-681	113	5	spectra	spectra	NOUN
eurjchem-681	113	6	of	of	ADP
eurjchem-681	113	7	sim	sim	ADJ
eurjchem-681	113	8	(	(	PUNCT
eurjchem-681	113	9	x	x	X
eurjchem-681	113	10	)	)	PUNCT
eurjchem-681	113	11	could	could	AUX
eurjchem-681	113	12	be	be	AUX
eurjchem-681	113	13	obtained	obtain	VERB
eurjchem-681	113	14	which	which	PRON
eurjchem-681	113	15	are	be	AUX
eurjchem-681	113	16	used	use	VERB
eurjchem-681	113	17	for	for	ADP
eurjchem-681	113	18	direct	direct	ADJ
eurjchem-681	113	19	determination	determination	NOUN
eurjchem-681	113	20	of	of	ADP
eurjchem-681	113	21	sim	sim	NOUN
eurjchem-681	113	22	at	at	ADP
eurjchem-681	113	23	237.5	237.5	NUM
eurjchem-681	113	24	nm	nm	NOUN
eurjchem-681	113	25	and	and	CCONJ
eurjchem-681	113	26	calculation	calculation	NOUN
eurjchem-681	113	27	of	of	ADP
eurjchem-681	113	28	the	the	DET
eurjchem-681	113	29	concentration	concentration	NOUN
eurjchem-681	113	30	from	from	ADP
eurjchem-681	113	31	the	the	DET
eurjchem-681	113	32	corresponding	corresponding	ADJ
eurjchem-681	113	33	regression	regression	NOUN
eurjchem-681	113	34	equation	equation	NOUN
eurjchem-681	113	35	.	.	PUNCT
eurjchem-681	114	1	a	a	DET
eurjchem-681	114	2	linear	linear	ADJ
eurjchem-681	114	3	correlation	correlation	NOUN
eurjchem-681	114	4	is	be	AUX
eurjchem-681	114	5	obtained	obtain	VERB
eurjchem-681	114	6	between	between	ADP
eurjchem-681	114	7	the	the	DET
eurjchem-681	114	8	absorbance	absorbance	NOUN
eurjchem-681	114	9	and	and	CCONJ
eurjchem-681	114	10	the	the	DET
eurjchem-681	114	11	corresponding	corresponding	ADJ
eurjchem-681	114	12	concentration	concentration	NOUN
eurjchem-681	114	13	of	of	ADP
eurjchem-681	114	14	sim	sim	NOUN
eurjchem-681	114	15	at	at	ADP
eurjchem-681	114	16	237.5	237.5	NUM
eurjchem-681	114	17	nm	nm	NOUN
eurjchem-681	114	18	.	.	PUNCT
eurjchem-681	115	1	the	the	DET
eurjchem-681	115	2	regression	regression	NOUN
eurjchem-681	115	3	equation	equation	NOUN
eurjchem-681	115	4	is	be	AUX
eurjchem-681	115	5	:	:	PUNCT
eurjchem-681	115	6	psim=	psim=	PUNCT
eurjchem-681	115	7	0.059c+0.0217	0.059c+0.0217	NUM
eurjchem-681	115	8	r2	r2	NOUN
eurjchem-681	115	9	=	=	NOUN
eurjchem-681	115	10	0.9999	0.9999	NUM
eurjchem-681	115	11	(	(	PUNCT
eurjchem-681	115	12	9	9	NUM
eurjchem-681	115	13	)	)	PUNCT
eurjchem-681	115	14	where	where	SCONJ
eurjchem-681	115	15	c	c	NOUN
eurjchem-681	115	16	is	be	AUX
eurjchem-681	115	17	the	the	DET
eurjchem-681	115	18	concentration	concentration	NOUN
eurjchem-681	115	19	of	of	ADP
eurjchem-681	115	20	sim	sim	NOUN
eurjchem-681	115	21	in	in	ADP
eurjchem-681	115	22	µg	µg	ADV
eurjchem-681	115	23	/	/	SYM
eurjchem-681	115	24	ml	ml	NOUN
eurjchem-681	115	25	,	,	PUNCT
eurjchem-681	115	26	psim	psim	NOUN
eurjchem-681	115	27	is	be	AUX
eurjchem-681	115	28	the	the	DET
eurjchem-681	115	29	peak	peak	NOUN
eurjchem-681	115	30	amplitude	amplitude	NOUN
eurjchem-681	115	31	of	of	ADP
eurjchem-681	115	32	the	the	DET
eurjchem-681	115	33	zero	zero	NUM
eurjchem-681	115	34	order	order	NOUN
eurjchem-681	115	35	spectrum	spectrum	NOUN
eurjchem-681	115	36	of	of	ADP
eurjchem-681	115	37	sim	sim	NOUN
eurjchem-681	115	38	at	at	ADP
eurjchem-681	115	39	237.5	237.5	NUM
eurjchem-681	115	40	nm	nm	NOUN
eurjchem-681	115	41	,	,	PUNCT
eurjchem-681	115	42	and	and	CCONJ
eurjchem-681	115	43	r	r	NOUN
eurjchem-681	115	44	is	be	AUX
eurjchem-681	115	45	the	the	DET
eurjchem-681	115	46	correlation	correlation	NOUN
eurjchem-681	115	47	coefficient	coefficient	NOUN
eurjchem-681	115	48	.	.	PUNCT
eurjchem-681	116	1	on	on	ADP
eurjchem-681	116	2	the	the	DET
eurjchem-681	116	3	other	other	ADJ
eurjchem-681	116	4	hand	hand	NOUN
eurjchem-681	116	5	for	for	ADP
eurjchem-681	116	6	determination	determination	NOUN
eurjchem-681	116	7	of	of	ADP
eurjchem-681	116	8	sit	sit	VERB
eurjchem-681	116	9	alone	alone	ADV
eurjchem-681	116	10	a	a	DET
eurjchem-681	116	11	calibration	calibration	NOUN
eurjchem-681	116	12	curve	curve	NOUN
eurjchem-681	116	13	is	be	AUX
eurjchem-681	116	14	constructed	construct	VERB
eurjchem-681	116	15	relating	relate	VERB
eurjchem-681	116	16	the	the	DET
eurjchem-681	116	17	absorbance	absorbance	NOUN
eurjchem-681	116	18	of	of	ADP
eurjchem-681	116	19	zero	zero	NUM
eurjchem-681	116	20	order	order	NOUN
eurjchem-681	116	21	spectra	spectra	NOUN
eurjchem-681	116	22	of	of	ADP
eurjchem-681	116	23	sit	sit	VERB
eurjchem-681	116	24	at	at	ADP
eurjchem-681	116	25	266.4	266.4	NUM
eurjchem-681	116	26	nm	nm	NOUN
eurjchem-681	116	27	to	to	ADP
eurjchem-681	116	28	the	the	DET
eurjchem-681	116	29	corresponding	corresponding	ADJ
eurjchem-681	116	30	concentrations	concentration	NOUN
eurjchem-681	116	31	where	where	SCONJ
eurjchem-681	116	32	sim	sim	NOUN
eurjchem-681	116	33	shows	show	VERB
eurjchem-681	116	34	no	no	DET
eurjchem-681	116	35	absorbance	absorbance	NOUN
eurjchem-681	116	36	.	.	PUNCT
eurjchem-681	117	1	abdel‐gawad	abdel‐gawad	PROPN
eurjchem-681	117	2	and	and	CCONJ
eurjchem-681	117	3	elsherif	elsherif	VERB
eurjchem-681	117	4	/	/	SYM
eurjchem-681	117	5	european	european	PROPN
eurjchem-681	117	6	journal	journal	PROPN
eurjchem-681	117	7	of	of	ADP
eurjchem-681	117	8	chemistry	chemistry	NOUN
eurjchem-681	117	9	3	3	NUM
eurjchem-681	117	10	(	(	PUNCT
eurjchem-681	117	11	4	4	NUM
eurjchem-681	117	12	)	)	PUNCT
eurjchem-681	117	13	(	(	PUNCT
eurjchem-681	117	14	2012	2012	NUM
eurjchem-681	117	15	)	)	PUNCT
eurjchem-681	117	16	447‐454	447‐454	PROPN
eurjchem-681	117	17	451	451	NUM
eurjchem-681	117	18	table	table	NOUN
eurjchem-681	117	19	1	1	NUM
eurjchem-681	117	20	.	.	PUNCT
eurjchem-681	118	1	determination	determination	NOUN
eurjchem-681	118	2	of	of	ADP
eurjchem-681	118	3	simvastatin	simvastatin	NOUN
eurjchem-681	118	4	and	and	CCONJ
eurjchem-681	118	5	sitagliptin	sitagliptin	PROPN
eurjchem-681	118	6	phosphate	phosphate	NOUN
eurjchem-681	118	7	monohydrate	monohydrate	NOUN
eurjchem-681	118	8	in	in	ADP
eurjchem-681	118	9	laboratory	laboratory	NOUN
eurjchem-681	118	10	prepared	prepare	VERB
eurjchem-681	118	11	mixtures	mixture	NOUN
eurjchem-681	118	12	by	by	ADP
eurjchem-681	118	13	the	the	DET
eurjchem-681	118	14	proposed	propose	VERB
eurjchem-681	118	15	methods	method	NOUN
eurjchem-681	118	16	.	.	PUNCT
eurjchem-681	119	1	claimed	claim	VERB
eurjchem-681	119	2	ratio	ratio	NOUN
eurjchem-681	119	3	(	(	PUNCT
eurjchem-681	119	4	µg	µg	NOUN
eurjchem-681	119	5	/	/	SYM
eurjchem-681	119	6	ml	ml	NOUN
eurjchem-681	119	7	)	)	PUNCT
eurjchem-681	119	8	simvastatin	simvastatin	NOUN
eurjchem-681	119	9	ratio	ratio	NOUN
eurjchem-681	119	10	subtraction	subtraction	NOUN
eurjchem-681	119	11	d3‐method	d3‐method	PROPN
eurjchem-681	119	12	dd1‐method	dd1‐method	PROPN
eurjchem-681	119	13	237.5	237.5	NUM
eurjchem-681	119	14	nm	nm	PROPN
eurjchem-681	119	15	240.5‐244.7	240.5‐244.7	NUM
eurjchem-681	119	16	nm	nm	ADP
eurjchem-681	119	17	228.3	228.3	NUM
eurjchem-681	119	18	nm	nm	NOUN
eurjchem-681	119	19	240.5	240.5	NUM
eurjchem-681	119	20	nm	nm	PRON
eurjchem-681	119	21	248	248	NUM
eurjchem-681	119	22	nm	nm	ADV
eurjchem-681	119	23	found	find	VERB
eurjchem-681	119	24	*	*	PUNCT
eurjchem-681	119	25	recovery	recovery	NOUN
eurjchem-681	119	26	found	find	VERB
eurjchem-681	119	27	*	*	PUNCT
eurjchem-681	119	28	recovery	recovery	NOUN
eurjchem-681	119	29	found	find	VERB
eurjchem-681	119	30	*	*	PUNCT
eurjchem-681	119	31	recovery	recovery	NOUN
eurjchem-681	119	32	found	find	VERB
eurjchem-681	119	33	*	*	PUNCT
eurjchem-681	119	34	recovery	recovery	NOUN
eurjchem-681	119	35	found	find	VERB
eurjchem-681	119	36	*	*	PUNCT
eurjchem-681	119	37	recovery	recovery	NOUN
eurjchem-681	119	38	10:128.5	10:128.5	NUM
eurjchem-681	119	39	9.96	9.96	NUM
eurjchem-681	119	40	99.60	99.60	NUM
eurjchem-681	119	41	10.02	10.02	NUM
eurjchem-681	119	42	100.20	100.20	NUM
eurjchem-681	119	43	10.08	10.08	NUM
eurjchem-681	119	44	100.80	100.80	NUM
eurjchem-681	119	45	9.95	9.95	NUM
eurjchem-681	119	46	99.50	99.50	NUM
eurjchem-681	119	47	10.04	10.04	NUM
eurjchem-681	119	48	100.40	100.40	NUM
eurjchem-681	119	49	12:77.1	12:77.1	NUM
eurjchem-681	119	50	12.04	12.04	NUM
eurjchem-681	119	51	100.33	100.33	NUM
eurjchem-681	119	52	11.98	11.98	NUM
eurjchem-681	119	53	99.83	99.83	NUM
eurjchem-681	119	54	12.01	12.01	NUM
eurjchem-681	119	55	100.08	100.08	NUM
eurjchem-681	119	56	11.94	11.94	NUM
eurjchem-681	119	57	99.50	99.50	NUM
eurjchem-681	119	58	12.07	12.07	NUM
eurjchem-681	119	59	100.58	100.58	NUM
eurjchem-681	119	60	16:51.4	16:51.4	NUM
eurjchem-681	119	61	15.98	15.98	NUM
eurjchem-681	119	62	99.88	99.88	NUM
eurjchem-681	119	63	15.86	15.86	NUM
eurjchem-681	119	64	99.13	99.13	NUM
eurjchem-681	119	65	16.05	16.05	NUM
eurjchem-681	119	66	100.31	100.31	NUM
eurjchem-681	119	67	15.97	15.97	NUM
eurjchem-681	119	68	99.81	99.81	NUM
eurjchem-681	119	69	15.99	15.99	NUM
eurjchem-681	119	70	99.94	99.94	NUM
eurjchem-681	119	71	mean	mean	NOUN
eurjchem-681	119	72	±	±	NUM
eurjchem-681	119	73	s.d	s.d	PROPN
eurjchem-681	119	74	.	.	PUNCT
eurjchem-681	120	1	99.94±0.368	99.94±0.368	PROPN
eurjchem-681	121	1	99.72±0.543	99.72±0.543	NUM
eurjchem-681	121	2	100.40±0.368	100.40±0.368	NOUN
eurjchem-681	121	3	99.60±0.120	99.60±0.120	NUM
eurjchem-681	121	4	100.31±0.330	100.31±0.330	NUM
eurjchem-681	121	5	*	*	PUNCT
eurjchem-681	121	6	average	average	NOUN
eurjchem-681	121	7	of	of	ADP
eurjchem-681	121	8	three	three	NUM
eurjchem-681	121	9	determinations	determination	NOUN
eurjchem-681	121	10	.	.	PUNCT
eurjchem-681	122	1	table	table	NOUN
eurjchem-681	122	2	2	2	NUM
eurjchem-681	122	3	.	.	PUNCT
eurjchem-681	123	1	determination	determination	NOUN
eurjchem-681	123	2	of	of	ADP
eurjchem-681	123	3	simvastatin	simvastatin	NOUN
eurjchem-681	123	4	and	and	CCONJ
eurjchem-681	123	5	sitagliptin	sitagliptin	PROPN
eurjchem-681	123	6	phosphate	phosphate	NOUN
eurjchem-681	123	7	monohydrate	monohydrate	NOUN
eurjchem-681	123	8	in	in	ADP
eurjchem-681	123	9	laboratory	laboratory	NOUN
eurjchem-681	123	10	prepared	prepare	VERB
eurjchem-681	123	11	mixtures	mixture	NOUN
eurjchem-681	123	12	by	by	ADP
eurjchem-681	123	13	the	the	DET
eurjchem-681	123	14	proposed	propose	VERB
eurjchem-681	123	15	methods	method	NOUN
eurjchem-681	123	16	.	.	PUNCT
eurjchem-681	124	1	claimed	claim	VERB
eurjchem-681	124	2	ratio	ratio	NOUN
eurjchem-681	124	3	(	(	PUNCT
eurjchem-681	124	4	µg	µg	NOUN
eurjchem-681	124	5	/	/	SYM
eurjchem-681	124	6	ml	ml	NOUN
eurjchem-681	124	7	)	)	PUNCT
eurjchem-681	124	8	sitagliptin	sitagliptin	NOUN
eurjchem-681	124	9	d3‐method	d3‐method	PROPN
eurjchem-681	124	10	dd1‐method	dd1‐method	PROPN
eurjchem-681	124	11	d0‐method	d0‐method	X
eurjchem-681	124	12	275.3‐280.3	275.3‐280.3	NUM
eurjchem-681	124	13	nm	nm	VERB
eurjchem-681	124	14	255.9	255.9	NUM
eurjchem-681	124	15	nm	nm	NOUN
eurjchem-681	124	16	275.2	275.2	NUM
eurjchem-681	124	17	nm	nm	NUM
eurjchem-681	124	18	266.4	266.4	NUM
eurjchem-681	124	19	nm	nm	NOUN
eurjchem-681	124	20	found	find	VERB
eurjchem-681	124	21	*	*	PUNCT
eurjchem-681	124	22	recovery	recovery	NOUN
eurjchem-681	124	23	found	find	VERB
eurjchem-681	124	24	*	*	PUNCT
eurjchem-681	124	25	recovery	recovery	NOUN
eurjchem-681	124	26	found	find	VERB
eurjchem-681	124	27	*	*	PUNCT
eurjchem-681	124	28	recovery	recovery	NOUN
eurjchem-681	124	29	found	find	VERB
eurjchem-681	124	30	*	*	PUNCT
eurjchem-681	124	31	recovery	recovery	NOUN
eurjchem-681	124	32	10:128.5	10:128.5	NUM
eurjchem-681	124	33	128.40	128.40	NUM
eurjchem-681	124	34	99.92	99.92	NUM
eurjchem-681	124	35	128.60	128.60	NUM
eurjchem-681	124	36	100.08	100.08	NUM
eurjchem-681	124	37	128.60	128.60	NUM
eurjchem-681	124	38	100.08	100.08	NUM
eurjchem-681	124	39	128.29	128.29	NUM
eurjchem-681	124	40	99.84	99.84	NUM
eurjchem-681	124	41	12:77.1	12:77.1	NUM
eurjchem-681	124	42	77.05	77.05	NUM
eurjchem-681	124	43	99.94	99.94	NUM
eurjchem-681	124	44	77.15	77.15	NUM
eurjchem-681	124	45	100.06	100.06	NUM
eurjchem-681	124	46	77.04	77.04	NUM
eurjchem-681	124	47	99.92	99.92	NUM
eurjchem-681	124	48	77.12	77.12	NUM
eurjchem-681	124	49	100.03	100.03	NUM
eurjchem-681	124	50	16:51.4	16:51.4	NUM
eurjchem-681	124	51	51.51	51.51	NUM
eurjchem-681	125	1	100.21	100.21	NUM
eurjchem-681	125	2	51.35	51.35	NUM
eurjchem-681	125	3	99.90	99.90	NUM
eurjchem-681	125	4	51.26	51.26	NUM
eurjchem-681	125	5	99.79	99.79	NUM
eurjchem-681	125	6	51.50	51.50	NUM
eurjchem-681	125	7	100.19	100.19	NUM
eurjchem-681	125	8	mean	mean	NOUN
eurjchem-681	125	9	±	±	NUM
eurjchem-681	125	10	s.d	s.d	PROPN
eurjchem-681	125	11	.	.	PROPN
eurjchem-681	125	12	100.02±0.162	100.02±0.162	PROPN
eurjchem-681	125	13	100.01±0.099	100.01±0.099	NUM
eurjchem-681	126	1	99.93±0.145	99.93±0.145	NUM
eurjchem-681	126	2	100.02±0.175	100.02±0.175	NOUN
eurjchem-681	126	3	*	*	PUNCT
eurjchem-681	126	4	average	average	NOUN
eurjchem-681	126	5	of	of	ADP
eurjchem-681	126	6	three	three	NUM
eurjchem-681	126	7	determinations	determination	NOUN
eurjchem-681	126	8	.	.	PUNCT
eurjchem-681	127	1	table	table	NOUN
eurjchem-681	127	2	3	3	NUM
eurjchem-681	127	3	.	.	PUNCT
eurjchem-681	128	1	determination	determination	NOUN
eurjchem-681	128	2	of	of	ADP
eurjchem-681	128	3	simvastatin	simvastatin	NOUN
eurjchem-681	128	4	in	in	ADP
eurjchem-681	128	5	pharmaceutical	pharmaceutical	ADJ
eurjchem-681	128	6	formulation	formulation	NOUN
eurjchem-681	128	7	and	and	CCONJ
eurjchem-681	128	8	application	application	NOUN
eurjchem-681	128	9	of	of	ADP
eurjchem-681	128	10	standard	standard	ADJ
eurjchem-681	128	11	addition	addition	NOUN
eurjchem-681	128	12	technique	technique	NOUN
eurjchem-681	128	13	.	.	PUNCT
eurjchem-681	129	1	pharmaceutical	pharmaceutical	ADJ
eurjchem-681	129	2	formulation	formulation	NOUN
eurjchem-681	129	3	simvastatin	simvastatin	NOUN
eurjchem-681	129	4	taken	take	VERB
eurjchem-681	129	5	(	(	PUNCT
eurjchem-681	129	6	µg	µg	NOUN
eurjchem-681	129	7	/	/	SYM
eurjchem-681	129	8	ml	ml	NOUN
eurjchem-681	129	9	)	)	PUNCT
eurjchem-681	129	10	found	find	VERB
eurjchem-681	129	11	*	*	PUNCT
eurjchem-681	129	12	%	%	X
eurjchem-681	130	1	±s.d	±s.d	PROPN
eurjchem-681	130	2	.	.	PUNCT
eurjchem-681	131	1	standard	standard	ADJ
eurjchem-681	131	2	addition	addition	NOUN
eurjchem-681	131	3	technique	technique	NOUN
eurjchem-681	131	4	juvisync	juvisync	NOUN
eurjchem-681	131	5	™	™	ADJ
eurjchem-681	131	6	tablets	tablet	NOUN
eurjchem-681	131	7	containing	contain	VERB
eurjchem-681	131	8	20	20	NUM
eurjchem-681	131	9	mg	mg	PROPN
eurjchem-681	131	10	simvastatin	simvastatin	NOUN
eurjchem-681	131	11	and	and	CCONJ
eurjchem-681	131	12	128.5	128.5	NUM
eurjchem-681	131	13	mg	mg	PROPN
eurjchem-681	131	14	sitagliptin	sitagliptin	PROPN
eurjchem-681	131	15	phosphate	phosphate	PROPN
eurjchem-681	131	16	monohydrate	monohydrate	NOUN
eurjchem-681	131	17	equivalent	equivalent	ADJ
eurjchem-681	131	18	to	to	ADP
eurjchem-681	131	19	100	100	NUM
eurjchem-681	131	20	mg	mg	PROPN
eurjchem-681	131	21	sitagliptin	sitagliptin	PROPN
eurjchem-681	131	22	base	base	PROPN
eurjchem-681	131	23	bnog011008	bnog011008	PROPN
eurjchem-681	131	24	.	.	PUNCT
eurjchem-681	132	1	10.00	10.00	NUM
eurjchem-681	132	2	101.32±0.924	101.32±0.924	NOUN
eurjchem-681	132	3	pure	pure	ADJ
eurjchem-681	132	4	added	add	VERB
eurjchem-681	132	5	(	(	PUNCT
eurjchem-681	132	6	µg	µg	ADJ
eurjchem-681	132	7	/	/	SYM
eurjchem-681	132	8	ml	ml	NOUN
eurjchem-681	132	9	)	)	PUNCT
eurjchem-681	132	10	pure	pure	ADJ
eurjchem-681	132	11	found	find	VERB
eurjchem-681	132	12	*	*	PUNCT
eurjchem-681	132	13	(	(	PUNCT
eurjchem-681	132	14	µg	µg	ADJ
eurjchem-681	132	15	/	/	SYM
eurjchem-681	132	16	ml	ml	NOUN
eurjchem-681	132	17	)	)	PUNCT
eurjchem-681	132	18	recovery	recovery	NOUN
eurjchem-681	132	19	(	(	PUNCT
eurjchem-681	132	20	%	%	INTJ
eurjchem-681	132	21	)	)	PUNCT
eurjchem-681	132	22	ratio	ratio	NOUN
eurjchem-681	132	23	subtr	subtr	VERB
eurjchem-681	132	24	.	.	PUNCT
eurjchem-681	133	1	d3	d3	PROPN
eurjchem-681	133	2	dd1	dd1	PROPN
eurjchem-681	133	3	ratio	ratio	NOUN
eurjchem-681	133	4	subtr	subtr	VERB
eurjchem-681	133	5	.	.	PUNCT
eurjchem-681	134	1	d3	d3	PROPN
eurjchem-681	134	2	dd1	dd1	VERB
eurjchem-681	134	3	228.3	228.3	NUM
eurjchem-681	134	4	nm	nm	NOUN
eurjchem-681	134	5	240.5	240.5	NUM
eurjchem-681	134	6	nm	nm	NOUN
eurjchem-681	134	7	248	248	NUM
eurjchem-681	134	8	nm	nm	ADV
eurjchem-681	134	9	228.3	228.3	NUM
eurjchem-681	134	10	nm	nm	NOUN
eurjchem-681	134	11	240.5	240.5	NUM
eurjchem-681	134	12	nm	nm	NOUN
eurjchem-681	134	13	248	248	NUM
eurjchem-681	134	14	nm	nm	ADV
eurjchem-681	134	15	2	2	NUM
eurjchem-681	134	16	1.99	1.99	NUM
eurjchem-681	134	17	2.01	2.01	NUM
eurjchem-681	134	18	2.02	2.02	NUM
eurjchem-681	134	19	1.99	1.99	NUM
eurjchem-681	134	20	1.98	1.98	NUM
eurjchem-681	134	21	99.50	99.50	NUM
eurjchem-681	134	22	100.50	100.50	NUM
eurjchem-681	134	23	101.00	101.00	NUM
eurjchem-681	134	24	99.50	99.50	NUM
eurjchem-681	134	25	99.00	99.00	NUM
eurjchem-681	134	26	4	4	NUM
eurjchem-681	134	27	4.03	4.03	NUM
eurjchem-681	134	28	3.99	3.99	NUM
eurjchem-681	134	29	3.96	3.96	NUM
eurjchem-681	134	30	3.99	3.99	NUM
eurjchem-681	134	31	3.98	3.98	NUM
eurjchem-681	134	32	100.75	100.75	NUM
eurjchem-681	134	33	99.75	99.75	NUM
eurjchem-681	134	34	99.00	99.00	NUM
eurjchem-681	134	35	99.75	99.75	NUM
eurjchem-681	134	36	99.50	99.50	NUM
eurjchem-681	134	37	6	6	NUM
eurjchem-681	134	38	6.02	6.02	NUM
eurjchem-681	134	39	5.98	5.98	NUM
eurjchem-681	134	40	5.97	5.97	NUM
eurjchem-681	134	41	5.97	5.97	NUM
eurjchem-681	134	42	5.97	5.97	NUM
eurjchem-681	134	43	100.33	100.33	NUM
eurjchem-681	134	44	99.50	99.50	NUM
eurjchem-681	134	45	99.67	99.67	NUM
eurjchem-681	134	46	99.50	99.50	NUM
eurjchem-681	134	47	99.50	99.50	NUM
eurjchem-681	134	48	mean	mean	NOUN
eurjchem-681	134	49	100.19	100.19	NUM
eurjchem-681	134	50	99.92	99.92	NUM
eurjchem-681	134	51	99.89	99.89	NUM
eurjchem-681	134	52	99.58	99.58	NUM
eurjchem-681	134	53	99.33	99.33	NUM
eurjchem-681	134	54	s.d	s.d	PROPN
eurjchem-681	134	55	.	.	PROPN
eurjchem-681	134	56	0.636	0.636	NUM
eurjchem-681	134	57	0.520	0.520	NUM
eurjchem-681	134	58	1.018	1.018	NUM
eurjchem-681	134	59	0.144	0.144	NUM
eurjchem-681	134	60	0.289	0.289	NUM
eurjchem-681	134	61	r.s.d	r.s.d	NOUN
eurjchem-681	134	62	.	.	PUNCT
eurjchem-681	135	1	0.635	0.635	NUM
eurjchem-681	135	2	0.520	0.520	NUM
eurjchem-681	135	3	1.019	1.019	NUM
eurjchem-681	135	4	0.145	0.145	NUM
eurjchem-681	135	5	0.291	0.291	NUM
eurjchem-681	135	6	*	*	PUNCT
eurjchem-681	135	7	average	average	NOUN
eurjchem-681	135	8	of	of	ADP
eurjchem-681	135	9	three	three	NUM
eurjchem-681	135	10	determinations	determination	NOUN
eurjchem-681	135	11	.	.	PUNCT
eurjchem-681	136	1	figure	figure	NOUN
eurjchem-681	136	2	9	9	NUM
eurjchem-681	136	3	.	.	PUNCT
eurjchem-681	137	1	absorption	absorption	NOUN
eurjchem-681	137	2	spectra	spectra	NOUN
eurjchem-681	137	3	of	of	ADP
eurjchem-681	137	4	laboratory	laboratory	NOUN
eurjchem-681	137	5	prepared	prepare	VERB
eurjchem-681	137	6	mixtures	mixture	NOUN
eurjchem-681	137	7	of	of	ADP
eurjchem-681	137	8	sitagliptin	sitagliptin	NOUN
eurjchem-681	137	9	and	and	CCONJ
eurjchem-681	137	10	simvastatin	simvastatin	NOUN
eurjchem-681	137	11	in	in	ADP
eurjchem-681	137	12	the	the	DET
eurjchem-681	137	13	ratio	ratio	NOUN
eurjchem-681	137	14	of	of	ADP
eurjchem-681	137	15	100:10	100:10	PROPN
eurjchem-681	137	16	(	(	PUNCT
eurjchem-681	137	17	—	—	PUNCT
eurjchem-681	137	18	)	)	PUNCT
eurjchem-681	137	19	,	,	PUNCT
eurjchem-681	137	20	60:12	60:12	NUM
eurjchem-681	137	21	(	(	PUNCT
eurjchem-681	137	22	…	…	PUNCT
eurjchem-681	137	23	.	.	PUNCT
eurjchem-681	137	24	)	)	PUNCT
eurjchem-681	137	25	and	and	CCONJ
eurjchem-681	137	26	40:16	40:16	NUM
eurjchem-681	137	27	(	(	PUNCT
eurjchem-681	137	28	—	—	PUNCT
eurjchem-681	137	29	—	—	PUNCT
eurjchem-681	137	30	)	)	PUNCT
eurjchem-681	137	31	after	after	ADP
eurjchem-681	137	32	division	division	NOUN
eurjchem-681	137	33	on	on	ADP
eurjchem-681	137	34	the	the	DET
eurjchem-681	137	35	spectrum	spectrum	NOUN
eurjchem-681	137	36	of	of	ADP
eurjchem-681	137	37	40	40	NUM
eurjchem-681	137	38	µg	µg	NOUN
eurjchem-681	137	39	/	/	SYM
eurjchem-681	137	40	ml	ml	NOUN
eurjchem-681	137	41	sitagliptin	sitagliptin	NOUN
eurjchem-681	137	42	and	and	CCONJ
eurjchem-681	137	43	subtraction	subtraction	NOUN
eurjchem-681	137	44	of	of	ADP
eurjchem-681	137	45	the	the	DET
eurjchem-681	137	46	constant	constant	ADJ
eurjchem-681	137	47	value	value	NOUN
eurjchem-681	137	48	.	.	PUNCT
eurjchem-681	138	1	the	the	DET
eurjchem-681	138	2	selectivity	selectivity	NOUN
eurjchem-681	138	3	of	of	ADP
eurjchem-681	138	4	the	the	DET
eurjchem-681	138	5	proposed	propose	VERB
eurjchem-681	138	6	procedures	procedure	NOUN
eurjchem-681	138	7	is	be	AUX
eurjchem-681	138	8	assessed	assess	VERB
eurjchem-681	138	9	by	by	ADP
eurjchem-681	138	10	the	the	DET
eurjchem-681	138	11	analysis	analysis	NOUN
eurjchem-681	138	12	of	of	ADP
eurjchem-681	138	13	laboratory	laboratory	NOUN
eurjchem-681	138	14	prepared	prepare	VERB
eurjchem-681	138	15	mixtures	mixture	NOUN
eurjchem-681	138	16	containing	contain	VERB
eurjchem-681	138	17	different	different	ADJ
eurjchem-681	138	18	ratios	ratio	NOUN
eurjchem-681	138	19	of	of	ADP
eurjchem-681	138	20	the	the	DET
eurjchem-681	138	21	two	two	NUM
eurjchem-681	138	22	drugs	drug	NOUN
eurjchem-681	138	23	,	,	PUNCT
eurjchem-681	138	24	where	where	SCONJ
eurjchem-681	138	25	satisfactory	satisfactory	ADJ
eurjchem-681	138	26	results	result	NOUN
eurjchem-681	138	27	are	be	AUX
eurjchem-681	138	28	obtained	obtain	VERB
eurjchem-681	138	29	over	over	ADP
eurjchem-681	138	30	the	the	DET
eurjchem-681	138	31	calibration	calibration	NOUN
eurjchem-681	138	32	ranges	range	VERB
eurjchem-681	138	33	as	as	SCONJ
eurjchem-681	138	34	shown	show	VERB
eurjchem-681	138	35	in	in	ADP
eurjchem-681	138	36	tables	table	NOUN
eurjchem-681	138	37	1	1	NUM
eurjchem-681	138	38	and	and	CCONJ
eurjchem-681	138	39	2	2	NUM
eurjchem-681	138	40	.	.	PUNCT
eurjchem-681	139	1	the	the	DET
eurjchem-681	139	2	proposed	propose	VERB
eurjchem-681	139	3	procedures	procedure	NOUN
eurjchem-681	139	4	are	be	AUX
eurjchem-681	139	5	also	also	ADV
eurjchem-681	139	6	applied	apply	VERB
eurjchem-681	139	7	for	for	ADP
eurjchem-681	139	8	the	the	DET
eurjchem-681	139	9	determination	determination	NOUN
eurjchem-681	139	10	of	of	ADP
eurjchem-681	139	11	sit	sit	NOUN
eurjchem-681	139	12	and	and	CCONJ
eurjchem-681	139	13	sim	sim	VERB
eurjchem-681	139	14	in	in	ADP
eurjchem-681	139	15	juvisync	juvisync	NOUN
eurjchem-681	139	16	™	™	ADJ
eurjchem-681	139	17	tablets	tablet	NOUN
eurjchem-681	139	18	.	.	PUNCT
eurjchem-681	140	1	the	the	DET
eurjchem-681	140	2	validity	validity	NOUN
eurjchem-681	140	3	of	of	ADP
eurjchem-681	140	4	the	the	DET
eurjchem-681	140	5	proposed	propose	VERB
eurjchem-681	140	6	procedures	procedure	NOUN
eurjchem-681	140	7	is	be	AUX
eurjchem-681	140	8	further	far	ADV
eurjchem-681	140	9	assessed	assess	VERB
eurjchem-681	140	10	by	by	ADP
eurjchem-681	140	11	applying	apply	VERB
eurjchem-681	140	12	the	the	DET
eurjchem-681	140	13	standard	standard	ADJ
eurjchem-681	140	14	addition	addition	NOUN
eurjchem-681	140	15	technique	technique	NOUN
eurjchem-681	140	16	(	(	PUNCT
eurjchem-681	140	17	table	table	NOUN
eurjchem-681	140	18	3	3	NUM
eurjchem-681	140	19	and	and	CCONJ
eurjchem-681	140	20	4	4	NUM
eurjchem-681	140	21	)	)	PUNCT
eurjchem-681	140	22	.	.	PUNCT
eurjchem-681	141	1	results	result	NOUN
eurjchem-681	141	2	obtained	obtain	VERB
eurjchem-681	141	3	by	by	ADP
eurjchem-681	141	4	the	the	DET
eurjchem-681	141	5	proposed	propose	VERB
eurjchem-681	141	6	procedures	procedure	NOUN
eurjchem-681	141	7	for	for	ADP
eurjchem-681	141	8	the	the	DET
eurjchem-681	141	9	determination	determination	NOUN
eurjchem-681	141	10	of	of	ADP
eurjchem-681	141	11	pure	pure	ADJ
eurjchem-681	141	12	samples	sample	NOUN
eurjchem-681	141	13	of	of	ADP
eurjchem-681	141	14	sit	sit	VERB
eurjchem-681	141	15	and	and	CCONJ
eurjchem-681	141	16	sim	sim	NOUN
eurjchem-681	141	17	are	be	AUX
eurjchem-681	141	18	statistically	statistically	ADV
eurjchem-681	141	19	compared	compare	VERB
eurjchem-681	141	20	to	to	ADP
eurjchem-681	141	21	those	those	PRON
eurjchem-681	141	22	obtained	obtain	VERB
eurjchem-681	141	23	by	by	ADP
eurjchem-681	141	24	the	the	DET
eurjchem-681	141	25	reference	reference	NOUN
eurjchem-681	141	26	method	method	NOUN
eurjchem-681	141	27	[	[	X
eurjchem-681	141	28	16	16	NUM
eurjchem-681	141	29	]	]	PUNCT
eurjchem-681	141	30	(	(	PUNCT
eurjchem-681	141	31	d2‐method	d2‐method	NOUN
eurjchem-681	141	32	for	for	ADP
eurjchem-681	141	33	determination	determination	NOUN
eurjchem-681	141	34	of	of	ADP
eurjchem-681	141	35	simvastatin	simvastatin	NOUN
eurjchem-681	141	36	at	at	ADP
eurjchem-681	141	37	243.5	243.5	NUM
eurjchem-681	141	38	nm	nm	NOUN
eurjchem-681	141	39	)	)	PUNCT
eurjchem-681	141	40	.	.	PUNCT
eurjchem-681	142	1	the	the	DET
eurjchem-681	142	2	results	result	NOUN
eurjchem-681	142	3	showed	show	VERB
eurjchem-681	142	4	no	no	DET
eurjchem-681	142	5	significant	significant	ADJ
eurjchem-681	142	6	differences	difference	NOUN
eurjchem-681	142	7	between	between	ADP
eurjchem-681	142	8	the	the	DET
eurjchem-681	142	9	proposed	propose	VERB
eurjchem-681	142	10	methods	method	NOUN
eurjchem-681	142	11	and	and	CCONJ
eurjchem-681	142	12	the	the	DET
eurjchem-681	142	13	reported	report	VERB
eurjchem-681	142	14	one	one	NUM
eurjchem-681	142	15	as	as	SCONJ
eurjchem-681	142	16	presented	present	VERB
eurjchem-681	142	17	in	in	ADP
eurjchem-681	142	18	table	table	NOUN
eurjchem-681	142	19	5	5	NUM
eurjchem-681	142	20	and	and	CCONJ
eurjchem-681	142	21	6	6	NUM
eurjchem-681	142	22	;	;	PUNCT
eurjchem-681	142	23	the	the	DET
eurjchem-681	142	24	observed	observe	VERB
eurjchem-681	142	25	good	good	ADJ
eurjchem-681	142	26	agreement	agreement	NOUN
eurjchem-681	142	27	between	between	ADP
eurjchem-681	142	28	proposed	propose	VERB
eurjchem-681	142	29	method	method	NOUN
eurjchem-681	142	30	and	and	CCONJ
eurjchem-681	142	31	the	the	DET
eurjchem-681	142	32	reference	reference	NOUN
eurjchem-681	142	33	method	method	NOUN
eurjchem-681	142	34	,	,	PUNCT
eurjchem-681	142	35	the	the	DET
eurjchem-681	142	36	high	high	ADJ
eurjchem-681	142	37	percentage	percentage	NOUN
eurjchem-681	142	38	recoveries	recovery	NOUN
eurjchem-681	142	39	(	(	PUNCT
eurjchem-681	142	40	99.33‐100.96	99.33‐100.96	NUM
eurjchem-681	142	41	)	)	PUNCT
eurjchem-681	142	42	and	and	CCONJ
eurjchem-681	142	43	low	low	ADJ
eurjchem-681	142	44	%	%	NOUN
eurjchem-681	142	45	r.s.d	r.s.d	NOUN
eurjchem-681	142	46	.	.	PUNCT
eurjchem-681	143	1	(	(	PUNCT
eurjchem-681	143	2	0.291‐1.337	0.291‐1.337	NOUN
eurjchem-681	143	3	)	)	PUNCT
eurjchem-681	143	4	values	value	NOUN
eurjchem-681	143	5	confirm	confirm	VERB
eurjchem-681	143	6	the	the	DET
eurjchem-681	143	7	suitability	suitability	NOUN
eurjchem-681	143	8	of	of	ADP
eurjchem-681	143	9	the	the	DET
eurjchem-681	143	10	proposed	propose	VERB
eurjchem-681	143	11	method	method	NOUN
eurjchem-681	143	12	for	for	ADP
eurjchem-681	143	13	the	the	DET
eurjchem-681	143	14	routine	routine	ADJ
eurjchem-681	143	15	determination	determination	NOUN
eurjchem-681	143	16	of	of	ADP
eurjchem-681	143	17	these	these	DET
eurjchem-681	143	18	components	component	NOUN
eurjchem-681	143	19	in	in	ADP
eurjchem-681	143	20	the	the	DET
eurjchem-681	143	21	new	new	ADJ
eurjchem-681	143	22	combined	combined	ADJ
eurjchem-681	143	23	formulation	formulation	NOUN
eurjchem-681	143	24	.	.	PUNCT
eurjchem-681	144	1	figure	figure	NOUN
eurjchem-681	144	2	10	10	NUM
eurjchem-681	144	3	.	.	PUNCT
eurjchem-681	145	1	absorption	absorption	NOUN
eurjchem-681	145	2	spectra	spectra	NOUN
eurjchem-681	145	3	of	of	ADP
eurjchem-681	145	4	laboratory	laboratory	NOUN
eurjchem-681	145	5	prepared	prepare	VERB
eurjchem-681	145	6	mixtures	mixture	NOUN
eurjchem-681	145	7	of	of	ADP
eurjchem-681	145	8	sitagliptin	sitagliptin	NOUN
eurjchem-681	145	9	and	and	CCONJ
eurjchem-681	145	10	simvastatin	simvastatin	NOUN
eurjchem-681	145	11	in	in	ADP
eurjchem-681	145	12	the	the	DET
eurjchem-681	145	13	ratio	ratio	NOUN
eurjchem-681	145	14	of	of	ADP
eurjchem-681	145	15	100:10	100:10	PROPN
eurjchem-681	145	16	(	(	PUNCT
eurjchem-681	145	17	—	—	PUNCT
eurjchem-681	145	18	)	)	PUNCT
eurjchem-681	145	19	,	,	PUNCT
eurjchem-681	145	20	60:12	60:12	NUM
eurjchem-681	145	21	(	(	PUNCT
eurjchem-681	145	22	…	…	PUNCT
eurjchem-681	145	23	..	..	PUNCT
eurjchem-681	145	24	)	)	PUNCT
eurjchem-681	145	25	and	and	CCONJ
eurjchem-681	145	26	40:16	40:16	NUM
eurjchem-681	145	27	(	(	PUNCT
eurjchem-681	145	28	—	—	PUNCT
eurjchem-681	145	29	—	—	PUNCT
eurjchem-681	145	30	)	)	PUNCT
eurjchem-681	145	31	after	after	ADP
eurjchem-681	145	32	division	division	NOUN
eurjchem-681	145	33	on	on	ADP
eurjchem-681	145	34	the	the	DET
eurjchem-681	145	35	spectrum	spectrum	NOUN
eurjchem-681	145	36	of	of	ADP
eurjchem-681	145	37	40	40	NUM
eurjchem-681	145	38	µg	µg	NOUN
eurjchem-681	145	39	/	/	SYM
eurjchem-681	145	40	ml	ml	NOUN
eurjchem-681	145	41	sitagliptin	sitagliptin	NOUN
eurjchem-681	145	42	and	and	CCONJ
eurjchem-681	145	43	subtraction	subtraction	NOUN
eurjchem-681	145	44	of	of	ADP
eurjchem-681	145	45	the	the	DET
eurjchem-681	145	46	constant	constant	ADJ
eurjchem-681	145	47	value	value	NOUN
eurjchem-681	145	48	then	then	ADV
eurjchem-681	145	49	multiplication	multiplication	NOUN
eurjchem-681	145	50	in	in	ADP
eurjchem-681	145	51	the	the	DET
eurjchem-681	145	52	spectrum	spectrum	NOUN
eurjchem-681	145	53	of	of	ADP
eurjchem-681	145	54	40	40	NUM
eurjchem-681	145	55	µg	µg	NOUN
eurjchem-681	145	56	/	/	SYM
eurjchem-681	145	57	ml	ml	NOUN
eurjchem-681	145	58	sitagliptin	sitagliptin	NOUN
eurjchem-681	145	59	.	.	PUNCT
eurjchem-681	146	1	3.4	3.4	NUM
eurjchem-681	146	2	.	.	PUNCT
eurjchem-681	146	3	method	method	NOUN
eurjchem-681	146	4	validation	validation	NOUN
eurjchem-681	146	5	validation	validation	NOUN
eurjchem-681	146	6	was	be	AUX
eurjchem-681	146	7	done	do	VERB
eurjchem-681	146	8	according	accord	VERB
eurjchem-681	146	9	to	to	ADP
eurjchem-681	146	10	ich	ich	NOUN
eurjchem-681	146	11	recommendations	recommendation	NOUN
eurjchem-681	146	12	[	[	X
eurjchem-681	146	13	41	41	NUM
eurjchem-681	146	14	]	]	PUNCT
eurjchem-681	146	15	.	.	PUNCT
eurjchem-681	147	1	linearity	linearity	NOUN
eurjchem-681	147	2	of	of	ADP
eurjchem-681	147	3	the	the	DET
eurjchem-681	147	4	methods	method	NOUN
eurjchem-681	147	5	was	be	AUX
eurjchem-681	147	6	evaluated	evaluate	VERB
eurjchem-681	147	7	by	by	ADP
eurjchem-681	147	8	analyzing	analyze	VERB
eurjchem-681	147	9	different	different	ADJ
eurjchem-681	147	10	concentrations	concentration	NOUN
eurjchem-681	147	11	of	of	ADP
eurjchem-681	147	12	sit	sit	VERB
eurjchem-681	147	13	and	and	CCONJ
eurjchem-681	147	14	sim	sim	ADJ
eurjchem-681	147	15	ranging	ranging	NOUN
eurjchem-681	147	16	between	between	ADP
eurjchem-681	147	17	40‐	40‐	NUM
eurjchem-681	147	18	360	360	NUM
eurjchem-681	147	19	µg	µg	NOUN
eurjchem-681	147	20	/	/	SYM
eurjchem-681	147	21	ml	ml	NOUN
eurjchem-681	147	22	and	and	CCONJ
eurjchem-681	147	23	2‐18	2‐18	NUM
eurjchem-681	147	24	µg	µg	ADV
eurjchem-681	147	25	/	/	SYM
eurjchem-681	147	26	ml	ml	NOUN
eurjchem-681	147	27	,	,	PUNCT
eurjchem-681	147	28	respectively	respectively	ADV
eurjchem-681	147	29	(	(	PUNCT
eurjchem-681	147	30	table	table	NOUN
eurjchem-681	147	31	7	7	NUM
eurjchem-681	147	32	and	and	CCONJ
eurjchem-681	147	33	8)	8)	NUM
eurjchem-681	147	34	.	.	PUNCT
eurjchem-681	148	1	each	each	DET
eurjchem-681	148	2	concentration	concentration	NOUN
eurjchem-681	148	3	was	be	AUX
eurjchem-681	148	4	made	make	VERB
eurjchem-681	148	5	in	in	ADP
eurjchem-681	148	6	triplicate	triplicate	NOUN
eurjchem-681	148	7	.	.	PUNCT
eurjchem-681	149	1	the	the	DET
eurjchem-681	149	2	assay	assay	NOUN
eurjchem-681	149	3	was	be	AUX
eurjchem-681	149	4	performed	perform	VERB
eurjchem-681	149	5	according	accord	VERB
eurjchem-681	149	6	to	to	ADP
eurjchem-681	149	7	the	the	DET
eurjchem-681	149	8	experimental	experimental	ADJ
eurjchem-681	149	9	conditions	condition	NOUN
eurjchem-681	149	10	.	.	PUNCT
eurjchem-681	150	1	the	the	DET
eurjchem-681	150	2	percentage	percentage	NOUN
eurjchem-681	150	3	recovery	recovery	NOUN
eurjchem-681	150	4	was	be	AUX
eurjchem-681	150	5	calculated	calculate	VERB
eurjchem-681	150	6	for	for	ADP
eurjchem-681	150	7	marketed	market	VERB
eurjchem-681	150	8	formulation	formulation	NOUN
eurjchem-681	150	9	by	by	ADP
eurjchem-681	150	10	standard	standard	ADJ
eurjchem-681	150	11	addition	addition	NOUN
eurjchem-681	150	12	of	of	ADP
eurjchem-681	150	13	pure	pure	ADJ
eurjchem-681	150	14	drugs	drug	NOUN
eurjchem-681	150	15	at	at	ADP
eurjchem-681	150	16	four	four	NUM
eurjchem-681	150	17	known	know	VERB
eurjchem-681	150	18	concentrations	concentration	NOUN
eurjchem-681	150	19	an	an	DET
eurjchem-681	150	20	excellent	excellent	ADJ
eurjchem-681	150	21	recovery	recovery	NOUN
eurjchem-681	150	22	were	be	AUX
eurjchem-681	150	23	obtained	obtain	VERB
eurjchem-681	150	24	at	at	ADP
eurjchem-681	150	25	each	each	DET
eurjchem-681	150	26	level	level	NOUN
eurjchem-681	150	27	.	.	PUNCT
eurjchem-681	151	1	452	452	NUM
eurjchem-681	151	2	abdel‐gawad	abdel‐gawad	NOUN
eurjchem-681	151	3	and	and	CCONJ
eurjchem-681	151	4	elsherif	elsherif	VERB
eurjchem-681	151	5	/	/	SYM
eurjchem-681	151	6	european	european	PROPN
eurjchem-681	151	7	journal	journal	PROPN
eurjchem-681	151	8	of	of	ADP
eurjchem-681	151	9	chemistry	chemistry	NOUN
eurjchem-681	151	10	3	3	NUM
eurjchem-681	151	11	(	(	PUNCT
eurjchem-681	151	12	4	4	NUM
eurjchem-681	151	13	)	)	PUNCT
eurjchem-681	151	14	(	(	PUNCT
eurjchem-681	151	15	2012	2012	NUM
eurjchem-681	151	16	)	)	PUNCT
eurjchem-681	151	17	447‐454	447‐454	PROPN
eurjchem-681	151	18	table	table	NOUN
eurjchem-681	151	19	4	4	NUM
eurjchem-681	151	20	.	.	PUNCT
eurjchem-681	152	1	determination	determination	NOUN
eurjchem-681	152	2	of	of	ADP
eurjchem-681	152	3	sitagliptin	sitagliptin	NOUN
eurjchem-681	152	4	in	in	ADP
eurjchem-681	152	5	pharmaceutical	pharmaceutical	ADJ
eurjchem-681	152	6	formulation	formulation	NOUN
eurjchem-681	152	7	and	and	CCONJ
eurjchem-681	152	8	application	application	NOUN
eurjchem-681	152	9	of	of	ADP
eurjchem-681	152	10	standard	standard	ADJ
eurjchem-681	152	11	addition	addition	NOUN
eurjchem-681	152	12	technique	technique	NOUN
eurjchem-681	152	13	.	.	PUNCT
eurjchem-681	153	1	pharmaceutical	pharmaceutical	ADJ
eurjchem-681	153	2	formulation	formulation	NOUN
eurjchem-681	153	3	sitagliptin	sitagliptin	NOUN
eurjchem-681	153	4	taken	take	VERB
eurjchem-681	153	5	(	(	PUNCT
eurjchem-681	153	6	µg	µg	NOUN
eurjchem-681	153	7	/	/	SYM
eurjchem-681	153	8	ml	ml	NOUN
eurjchem-681	153	9	)	)	PUNCT
eurjchem-681	153	10	found	find	VERB
eurjchem-681	153	11	*	*	PUNCT
eurjchem-681	153	12	%	%	PROPN
eurjchem-681	153	13	±s.d	±s.d	PROPN
eurjchem-681	153	14	.	.	PUNCT
eurjchem-681	154	1	standard	standard	ADJ
eurjchem-681	154	2	addition	addition	NOUN
eurjchem-681	154	3	technique	technique	NOUN
eurjchem-681	154	4	juvisync	juvisync	NOUN
eurjchem-681	154	5	™	™	ADJ
eurjchem-681	154	6	tablets	tablet	NOUN
eurjchem-681	154	7	containing	contain	VERB
eurjchem-681	154	8	20	20	NUM
eurjchem-681	154	9	mg	mg	PROPN
eurjchem-681	154	10	simvastatin	simvastatin	NOUN
eurjchem-681	154	11	and	and	CCONJ
eurjchem-681	154	12	128.5	128.5	NUM
eurjchem-681	154	13	mg	mg	PROPN
eurjchem-681	154	14	sitagliptin	sitagliptin	PROPN
eurjchem-681	154	15	phosphate	phosphate	PROPN
eurjchem-681	154	16	monohydrate	monohydrate	NOUN
eurjchem-681	154	17	equivalent	equivalent	ADJ
eurjchem-681	154	18	to	to	ADP
eurjchem-681	154	19	100	100	NUM
eurjchem-681	154	20	mg	mg	PROPN
eurjchem-681	154	21	sitagliptin	sitagliptin	PROPN
eurjchem-681	154	22	base	base	PROPN
eurjchem-681	154	23	bnog011008	bnog011008	PROPN
eurjchem-681	154	24	.	.	PUNCT
eurjchem-681	155	1	64.25	64.25	NUM
eurjchem-681	155	2	99.18±0.896	99.18±0.896	NUM
eurjchem-681	155	3	pure	pure	ADJ
eurjchem-681	155	4	added	add	VERB
eurjchem-681	155	5	(	(	PUNCT
eurjchem-681	155	6	µg	µg	ADJ
eurjchem-681	155	7	/	/	SYM
eurjchem-681	155	8	ml	ml	NOUN
eurjchem-681	155	9	)	)	PUNCT
eurjchem-681	155	10	pure	pure	ADJ
eurjchem-681	155	11	found	find	VERB
eurjchem-681	155	12	*	*	PUNCT
eurjchem-681	155	13	(	(	PUNCT
eurjchem-681	155	14	µg	µg	ADJ
eurjchem-681	155	15	/	/	SYM
eurjchem-681	155	16	ml	ml	NOUN
eurjchem-681	155	17	)	)	PUNCT
eurjchem-681	155	18	recovery	recovery	NOUN
eurjchem-681	155	19	(	(	PUNCT
eurjchem-681	155	20	%	%	INTJ
eurjchem-681	155	21	)	)	PUNCT
eurjchem-681	155	22	d0	d0	PROPN
eurjchem-681	155	23	d3	d3	PROPN
eurjchem-681	155	24	dd1	dd1	NOUN
eurjchem-681	155	25	d0	d0	PROPN
eurjchem-681	155	26	d3	d3	PROPN
eurjchem-681	155	27	dd1	dd1	NOUN
eurjchem-681	155	28	255.9	255.9	NUM
eurjchem-681	155	29	nm	nm	NOUN
eurjchem-681	155	30	275.2	275.2	NUM
eurjchem-681	155	31	nm	nm	NOUN
eurjchem-681	155	32	255.9	255.9	NUM
eurjchem-681	155	33	nm	nm	ADV
eurjchem-681	155	34	275.2	275.2	NUM
eurjchem-681	155	35	nm	nm	ADV
eurjchem-681	155	36	40	40	NUM
eurjchem-681	155	37	40.65	40.65	NUM
eurjchem-681	155	38	40.73	40.73	NUM
eurjchem-681	155	39	39.75	39.75	NUM
eurjchem-681	155	40	40.51	40.51	NUM
eurjchem-681	156	1	101.63	101.63	NUM
eurjchem-681	156	2	101.83	101.83	NUM
eurjchem-681	156	3	99.38	99.38	NUM
eurjchem-681	156	4	101.28	101.28	NUM
eurjchem-681	156	5	80	80	NUM
eurjchem-681	156	6	79.21	79.21	NUM
eurjchem-681	156	7	81.24	81.24	NUM
eurjchem-681	156	8	78.98	78.98	NUM
eurjchem-681	156	9	79.96	79.96	NUM
eurjchem-681	156	10	99.01	99.01	NUM
eurjchem-681	157	1	101.55	101.55	NUM
eurjchem-681	157	2	98.73	98.73	NUM
eurjchem-681	157	3	99.95	99.95	NUM
eurjchem-681	157	4	120	120	NUM
eurjchem-681	157	5	121.01	121.01	NUM
eurjchem-681	157	6	119.40	119.40	NUM
eurjchem-681	157	7	121.11	121.11	NUM
eurjchem-681	157	8	119.84	119.84	NUM
eurjchem-681	157	9	100.84	100.84	NUM
eurjchem-681	157	10	99.50	99.50	NUM
eurjchem-681	157	11	100.93	100.93	NUM
eurjchem-681	157	12	99.87	99.87	NUM
eurjchem-681	157	13	mean	mean	NOUN
eurjchem-681	157	14	100.49	100.49	NUM
eurjchem-681	157	15	100.96	100.96	NUM
eurjchem-681	157	16	99.68	99.68	NUM
eurjchem-681	157	17	100.37	100.37	NUM
eurjchem-681	157	18	s.d	s.d	PROPN
eurjchem-681	157	19	.	.	PROPN
eurjchem-681	157	20	1.344	1.344	NUM
eurjchem-681	157	21	1.272	1.272	NUM
eurjchem-681	157	22	1.130	1.130	NUM
eurjchem-681	157	23	0.792	0.792	NUM
eurjchem-681	157	24	r.s.d	r.s.d	NOUN
eurjchem-681	157	25	.	.	PUNCT
eurjchem-681	158	1	1.337	1.337	NUM
eurjchem-681	158	2	1.260	1.260	NUM
eurjchem-681	158	3	1.134	1.134	NUM
eurjchem-681	158	4	0.789	0.789	NUM
eurjchem-681	158	5	*	*	PUNCT
eurjchem-681	158	6	average	average	NOUN
eurjchem-681	158	7	of	of	ADP
eurjchem-681	158	8	three	three	NUM
eurjchem-681	158	9	determinations	determination	NOUN
eurjchem-681	158	10	.	.	PUNCT
eurjchem-681	159	1	table	table	NOUN
eurjchem-681	159	2	5	5	NUM
eurjchem-681	159	3	.	.	PUNCT
eurjchem-681	160	1	statistical	statistical	ADJ
eurjchem-681	160	2	comparison	comparison	NOUN
eurjchem-681	160	3	between	between	ADP
eurjchem-681	160	4	the	the	DET
eurjchem-681	160	5	proposed	propose	VERB
eurjchem-681	160	6	methods	method	NOUN
eurjchem-681	160	7	for	for	ADP
eurjchem-681	160	8	the	the	DET
eurjchem-681	160	9	determination	determination	NOUN
eurjchem-681	160	10	of	of	ADP
eurjchem-681	160	11	sitagliptin	sitagliptin	NOUN
eurjchem-681	160	12	and	and	CCONJ
eurjchem-681	160	13	a	a	DET
eurjchem-681	160	14	reference	reference	NOUN
eurjchem-681	160	15	method	method	NOUN
eurjchem-681	160	16	.	.	PUNCT
eurjchem-681	161	1	parameter	parameter	PROPN
eurjchem-681	161	2	sitagliptin	sitagliptin	PROPN
eurjchem-681	161	3	reference	reference	NOUN
eurjchem-681	161	4	method	method	NOUN
eurjchem-681	161	5	*	*	PUNCT
eurjchem-681	161	6	d3	d3	PROPN
eurjchem-681	161	7	dd1	dd1	NOUN
eurjchem-681	161	8	d0	d0	PROPN
eurjchem-681	161	9	275.3‐280.3	275.3‐280.3	PROPN
eurjchem-681	161	10	nm	nm	VERB
eurjchem-681	161	11	255.9	255.9	NUM
eurjchem-681	161	12	nm	nm	NOUN
eurjchem-681	161	13	275.2	275.2	NUM
eurjchem-681	161	14	nm	nm	NOUN
eurjchem-681	161	15	266.4	266.4	NUM
eurjchem-681	161	16	nm	nm	ADV
eurjchem-681	161	17	mean±s.d	mean±s.d	PROPN
eurjchem-681	161	18	.	.	PUNCT
eurjchem-681	162	1	100.25±0.526	100.25±0.526	PROPN
eurjchem-681	162	2	100.39±0.650	100.39±0.650	NUM
eurjchem-681	162	3	100.42±0.547	100.42±0.547	NUM
eurjchem-681	162	4	99.96±0.381	99.96±0.381	NUM
eurjchem-681	162	5	100.12±0.489	100.12±0.489	NUM
eurjchem-681	162	6	r.s.d	r.s.d	NOUN
eurjchem-681	162	7	.	.	PUNCT
eurjchem-681	163	1	0.525	0.525	NUM
eurjchem-681	163	2	0.647	0.647	NUM
eurjchem-681	163	3	0.546	0.546	NUM
eurjchem-681	163	4	0.381	0.381	NUM
eurjchem-681	163	5	0.488	0.488	NUM
eurjchem-681	163	6	n	n	DET
eurjchem-681	163	7	4	4	NUM
eurjchem-681	163	8	4	4	NUM
eurjchem-681	163	9	4	4	NUM
eurjchem-681	163	10	4	4	NUM
eurjchem-681	163	11	4	4	NUM
eurjchem-681	163	12	variance	variance	NOUN
eurjchem-681	163	13	0.277	0.277	NUM
eurjchem-681	163	14	0.423	0.423	NUM
eurjchem-681	163	15	0.299	0.299	NUM
eurjchem-681	163	16	0.145	0.145	NUM
eurjchem-681	163	17	0.239	0.239	NUM
eurjchem-681	163	18	f‐value	f‐value	PUNCT
eurjchem-681	164	1	*	*	PUNCT
eurjchem-681	164	2	*	*	PUNCT
eurjchem-681	164	3	(	(	PUNCT
eurjchem-681	164	4	9.55	9.55	NUM
eurjchem-681	164	5	)	)	PUNCT
eurjchem-681	164	6	1.159	1.159	NUM
eurjchem-681	164	7	1.770	1.770	NUM
eurjchem-681	164	8	1.251	1.251	NUM
eurjchem-681	164	9	1.648	1.648	NUM
eurjchem-681	164	10	‐	‐	NOUN
eurjchem-681	164	11	student	student	NOUN
eurjchem-681	164	12	's	's	PART
eurjchem-681	164	13	t‐test	t‐test	PUNCT
eurjchem-681	164	14	*	*	PUNCT
eurjchem-681	164	15	*	*	PUNCT
eurjchem-681	164	16	(	(	PUNCT
eurjchem-681	164	17	1.943	1.943	NUM
eurjchem-681	164	18	)	)	PUNCT
eurjchem-681	164	19	0.362	0.362	NUM
eurjchem-681	164	20	0.663	0.663	NUM
eurjchem-681	164	21	0.813	0.813	NUM
eurjchem-681	164	22	0.516	0.516	NUM
eurjchem-681	164	23	‐	‐	NOUN
eurjchem-681	164	24	*	*	PUNCT
eurjchem-681	164	25	reference	reference	NOUN
eurjchem-681	164	26	colorimetric	colorimetric	ADJ
eurjchem-681	164	27	method	method	NOUN
eurjchem-681	164	28	for	for	ADP
eurjchem-681	164	29	the	the	DET
eurjchem-681	164	30	determination	determination	NOUN
eurjchem-681	164	31	of	of	ADP
eurjchem-681	164	32	sitagliptin	sitagliptin	NOUN
eurjchem-681	164	33	by	by	ADP
eurjchem-681	164	34	condensation	condensation	NOUN
eurjchem-681	164	35	of	of	ADP
eurjchem-681	164	36	its	its	PRON
eurjchem-681	164	37	primary	primary	ADJ
eurjchem-681	164	38	amino	amino	NOUN
eurjchem-681	164	39	group	group	NOUN
eurjchem-681	164	40	with	with	ADP
eurjchem-681	164	41	acetyl	acetyl	NOUN
eurjchem-681	164	42	acetone	acetone	NOUN
eurjchem-681	164	43	and	and	CCONJ
eurjchem-681	164	44	formaldehyde	formaldehyde	NOUN
eurjchem-681	164	45	then	then	ADV
eurjchem-681	164	46	measuring	measure	VERB
eurjchem-681	164	47	the	the	DET
eurjchem-681	164	48	produced	produce	VERB
eurjchem-681	164	49	color	color	NOUN
eurjchem-681	164	50	at	at	ADP
eurjchem-681	164	51	430	430	NUM
eurjchem-681	164	52	nm	nm	NOUN
eurjchem-681	164	53	.	.	PUNCT
eurjchem-681	165	1	*	*	PUNCT
eurjchem-681	165	2	*	*	NOUN
eurjchem-681	165	3	values	value	NOUN
eurjchem-681	165	4	in	in	ADP
eurjchem-681	165	5	parenthesis	parenthesis	NOUN
eurjchem-681	165	6	are	be	AUX
eurjchem-681	165	7	the	the	DET
eurjchem-681	165	8	theoretical	theoretical	ADJ
eurjchem-681	165	9	values	value	NOUN
eurjchem-681	165	10	of	of	ADP
eurjchem-681	165	11	t	t	PROPN
eurjchem-681	165	12	and	and	CCONJ
eurjchem-681	165	13	f	f	PROPN
eurjchem-681	165	14	at	at	ADP
eurjchem-681	165	15	p	p	NOUN
eurjchem-681	165	16	=	=	NOUN
eurjchem-681	165	17	0.05	0.05	NUM
eurjchem-681	165	18	.	.	PUNCT
eurjchem-681	165	19	table	table	NOUN
eurjchem-681	165	20	6	6	NUM
eurjchem-681	165	21	.	.	PUNCT
eurjchem-681	166	1	statistical	statistical	ADJ
eurjchem-681	166	2	comparison	comparison	NOUN
eurjchem-681	166	3	between	between	ADP
eurjchem-681	166	4	the	the	DET
eurjchem-681	166	5	proposed	propose	VERB
eurjchem-681	166	6	methods	method	NOUN
eurjchem-681	166	7	for	for	ADP
eurjchem-681	166	8	the	the	DET
eurjchem-681	166	9	determination	determination	NOUN
eurjchem-681	166	10	of	of	ADP
eurjchem-681	166	11	simvastatin	simvastatin	NOUN
eurjchem-681	166	12	and	and	CCONJ
eurjchem-681	166	13	a	a	DET
eurjchem-681	166	14	reference	reference	NOUN
eurjchem-681	166	15	method	method	NOUN
eurjchem-681	166	16	.	.	PUNCT
eurjchem-681	167	1	parameter	parameter	PROPN
eurjchem-681	167	2	simvastatin	simvastatin	PROPN
eurjchem-681	167	3	reference	reference	NOUN
eurjchem-681	167	4	method	method	NOUN
eurjchem-681	167	5	*	*	PUNCT
eurjchem-681	167	6	d3‐method	d3‐method	PUNCT
eurjchem-681	167	7	dd1‐method	dd1‐method	PROPN
eurjchem-681	167	8	240.5‐244.7	240.5‐244.7	NUM
eurjchem-681	167	9	nm	nm	NOUN
eurjchem-681	167	10	228.3	228.3	NUM
eurjchem-681	167	11	nm	nm	NOUN
eurjchem-681	167	12	240.5	240.5	NUM
eurjchem-681	167	13	nm	nm	PRON
eurjchem-681	167	14	248	248	NUM
eurjchem-681	167	15	nm	nm	ADV
eurjchem-681	167	16	mean±s.d	mean±s.d	PROPN
eurjchem-681	167	17	.	.	PUNCT
eurjchem-681	168	1	100.00±0.797	100.00±0.797	NOUN
eurjchem-681	168	2	100.24±0.723	100.24±0.723	NUM
eurjchem-681	168	3	100.17±0.466	100.17±0.466	NUM
eurjchem-681	168	4	100.39±0.366	100.39±0.366	NUM
eurjchem-681	168	5	100.27±0.808	100.27±0.808	NUM
eurjchem-681	168	6	r.s.d	r.s.d	NOUN
eurjchem-681	168	7	.	.	PUNCT
eurjchem-681	169	1	0.797	0.797	NUM
eurjchem-681	169	2	0.721	0.721	NUM
eurjchem-681	169	3	0.465	0.465	NUM
eurjchem-681	169	4	0.365	0.365	NUM
eurjchem-681	169	5	0.806	0.806	NUM
eurjchem-681	169	6	n	n	PRON
eurjchem-681	169	7	4	4	NUM
eurjchem-681	169	8	4	4	NUM
eurjchem-681	169	9	4	4	NUM
eurjchem-681	169	10	4	4	NUM
eurjchem-681	169	11	3	3	NUM
eurjchem-681	169	12	variance	variance	NOUN
eurjchem-681	169	13	0.635	0.635	NUM
eurjchem-681	169	14	0.523	0.523	NUM
eurjchem-681	169	15	0.217	0.217	NUM
eurjchem-681	169	16	0.134	0.134	NUM
eurjchem-681	169	17	0.653	0.653	NUM
eurjchem-681	169	18	f‐value	f‐value	PUNCT
eurjchem-681	170	1	*	*	PUNCT
eurjchem-681	170	2	*	*	PUNCT
eurjchem-681	170	3	(	(	PUNCT
eurjchem-681	170	4	9.55	9.55	NUM
eurjchem-681	170	5	)	)	PUNCT
eurjchem-681	170	6	1.028	1.028	NUM
eurjchem-681	170	7	1.249	1.249	NUM
eurjchem-681	170	8	3.009	3.009	NUM
eurjchem-681	170	9	4.873	4.873	NUM
eurjchem-681	170	10	‐	‐	NOUN
eurjchem-681	170	11	student	student	NOUN
eurjchem-681	170	12	's	's	PART
eurjchem-681	170	13	t‐test	t‐test	PUNCT
eurjchem-681	171	1	*	*	PUNCT
eurjchem-681	171	2	*	*	PUNCT
eurjchem-681	171	3	(	(	PUNCT
eurjchem-681	171	4	1.943	1.943	NUM
eurjchem-681	171	5	)	)	PUNCT
eurjchem-681	171	6	0.443	0.443	NUM
eurjchem-681	171	7	0.052	0.052	NUM
eurjchem-681	171	8	0.210	0.210	NUM
eurjchem-681	171	9	0.270	0.270	NUM
eurjchem-681	171	10	‐	‐	NOUN
eurjchem-681	171	11	*	*	PUNCT
eurjchem-681	171	12	d2‐method	d2‐method	NOUN
eurjchem-681	171	13	for	for	ADP
eurjchem-681	171	14	determination	determination	NOUN
eurjchem-681	171	15	of	of	ADP
eurjchem-681	171	16	simvastatin	simvastatin	NOUN
eurjchem-681	171	17	at	at	ADP
eurjchem-681	171	18	243.5	243.5	NUM
eurjchem-681	171	19	nm	nm	NOUN
eurjchem-681	171	20	.	.	PUNCT
eurjchem-681	172	1	*	*	PUNCT
eurjchem-681	172	2	*	*	NOUN
eurjchem-681	172	3	values	value	NOUN
eurjchem-681	172	4	in	in	ADP
eurjchem-681	172	5	parenthesis	parenthesis	NOUN
eurjchem-681	172	6	are	be	AUX
eurjchem-681	172	7	the	the	DET
eurjchem-681	172	8	theoretical	theoretical	ADJ
eurjchem-681	172	9	values	value	NOUN
eurjchem-681	172	10	of	of	ADP
eurjchem-681	172	11	t	t	PROPN
eurjchem-681	172	12	and	and	CCONJ
eurjchem-681	172	13	f	f	PROPN
eurjchem-681	172	14	at	at	ADP
eurjchem-681	172	15	p	p	NOUN
eurjchem-681	172	16	=	=	NOUN
eurjchem-681	172	17	0.05	0.05	NUM
eurjchem-681	172	18	.	.	PUNCT
eurjchem-681	172	19	table	table	NOUN
eurjchem-681	172	20	7	7	NUM
eurjchem-681	172	21	.	.	PUNCT
eurjchem-681	172	22	assay	assay	NOUN
eurjchem-681	172	23	validation	validation	NOUN
eurjchem-681	172	24	results	result	NOUN
eurjchem-681	172	25	of	of	ADP
eurjchem-681	172	26	the	the	DET
eurjchem-681	172	27	proposed	propose	VERB
eurjchem-681	172	28	methods	method	NOUN
eurjchem-681	172	29	.	.	PUNCT
eurjchem-681	173	1	parameter	parameter	PROPN
eurjchem-681	173	2	simvastatin	simvastatin	PROPN
eurjchem-681	173	3	d3‐method	d3‐method	PROPN
eurjchem-681	173	4	dd1‐method	dd1‐method	PROPN
eurjchem-681	173	5	240.5‐244.7	240.5‐244.7	NUM
eurjchem-681	173	6	nm	nm	NOUN
eurjchem-681	173	7	228.3	228.3	NUM
eurjchem-681	173	8	nm	nm	NOUN
eurjchem-681	173	9	240.5	240.5	NUM
eurjchem-681	173	10	nm	nm	PRON
eurjchem-681	173	11	248	248	NUM
eurjchem-681	173	12	nm	nm	ADJ
eurjchem-681	173	13	accuracy	accuracy	NOUN
eurjchem-681	173	14	100.00±0.797	100.00±0.797	NOUN
eurjchem-681	173	15	100.24±0.723	100.24±0.723	NUM
eurjchem-681	173	16	100.17±0.466	100.17±0.466	NUM
eurjchem-681	173	17	100.39±0.366	100.39±0.366	ADJ
eurjchem-681	173	18	specificity	specificity	NOUN
eurjchem-681	173	19	and	and	CCONJ
eurjchem-681	173	20	selectivity	selectivity	NOUN
eurjchem-681	173	21	99.72±0.543	99.72±0.543	NUM
eurjchem-681	173	22	100.40±0.368	100.40±0.368	NUM
eurjchem-681	173	23	99.60±0.120	99.60±0.120	NUM
eurjchem-681	173	24	100.31±0.330	100.31±0.330	NUM
eurjchem-681	173	25	precision	precision	NOUN
eurjchem-681	173	26	repeatability	repeatability	NOUN
eurjchem-681	173	27	*	*	PUNCT
eurjchem-681	174	1	98.95±0.0.981	98.95±0.0.981	NUM
eurjchem-681	174	2	100.96±0.961	100.96±0.961	NUM
eurjchem-681	174	3	101.34±0.694	101.34±0.694	ADP
eurjchem-681	174	4	99.32±0.0.812	99.32±0.0.812	PROPN
eurjchem-681	174	5	intermediate	intermediate	ADJ
eurjchem-681	174	6	precision	precision	NOUN
eurjchem-681	174	7	*	*	PUNCT
eurjchem-681	174	8	101.35±0.894	101.35±0.894	NUM
eurjchem-681	174	9	99.17±1.013	99.17±1.013	NUM
eurjchem-681	174	10	101.54±0.0.789	101.54±0.0.789	NUM
eurjchem-681	174	11	100.84±0.0.741	100.84±0.0.741	NUM
eurjchem-681	174	12	robustness	robustness	NOUN
eurjchem-681	174	13	99.68±0.541	99.68±0.541	NUM
eurjchem-681	174	14	100.95±0.514	100.95±0.514	NUM
eurjchem-681	174	15	101.07±0.941	101.07±0.941	NUM
eurjchem-681	174	16	101.24±0.514	101.24±0.514	NUM
eurjchem-681	174	17	linearity	linearity	NOUN
eurjchem-681	174	18	,	,	PUNCT
eurjchem-681	174	19	slope	slope	VERB
eurjchem-681	174	20	0.1156	0.1156	NUM
eurjchem-681	174	21	0.0946	0.0946	NUM
eurjchem-681	174	22	0.1404	0.1404	NUM
eurjchem-681	174	23	0.0866	0.0866	NUM
eurjchem-681	174	24	linearity	linearity	NOUN
eurjchem-681	174	25	,	,	PUNCT
eurjchem-681	174	26	intercept	intercept	NOUN
eurjchem-681	174	27	‐0.0217	‐0.0217	NOUN
eurjchem-681	174	28	0.0412	0.0412	NUM
eurjchem-681	174	29	0.0447	0.0447	NUM
eurjchem-681	174	30	0.0357	0.0357	NUM
eurjchem-681	174	31	linearity	linearity	NOUN
eurjchem-681	174	32	,	,	PUNCT
eurjchem-681	174	33	correlation	correlation	NOUN
eurjchem-681	174	34	coefficient	coefficient	NOUN
eurjchem-681	174	35	(	(	PUNCT
eurjchem-681	174	36	r	r	NOUN
eurjchem-681	174	37	)	)	PUNCT
eurjchem-681	174	38	0.9997	0.9997	NUM
eurjchem-681	174	39	0.9997	0.9997	NUM
eurjchem-681	174	40	0.9998	0.9998	NUM
eurjchem-681	174	41	0.9997	0.9997	NUM
eurjchem-681	174	42	range	range	NOUN
eurjchem-681	174	43	(	(	PUNCT
eurjchem-681	174	44	µg	µg	NOUN
eurjchem-681	174	45	/	/	SYM
eurjchem-681	174	46	ml	ml	NOUN
eurjchem-681	174	47	)	)	PUNCT
eurjchem-681	174	48	2‐18	2‐18	NUM
eurjchem-681	174	49	2‐18	2‐18	NUM
eurjchem-681	174	50	2‐18	2‐18	NUM
eurjchem-681	174	51	2‐18	2‐18	NUM
eurjchem-681	175	1	lod	lod	NOUN
eurjchem-681	175	2	*	*	PUNCT
eurjchem-681	175	3	*	*	PUNCT
eurjchem-681	175	4	(	(	PUNCT
eurjchem-681	175	5	µg	µg	NOUN
eurjchem-681	175	6	/	/	SYM
eurjchem-681	175	7	ml	ml	NOUN
eurjchem-681	175	8	)	)	PUNCT
eurjchem-681	175	9	1	1	NUM
eurjchem-681	175	10	1	1	NUM
eurjchem-681	175	11	1	1	NUM
eurjchem-681	175	12	1	1	NUM
eurjchem-681	175	13	loq	loq	PROPN
eurjchem-681	175	14	*	*	PUNCT
eurjchem-681	175	15	*	*	PUNCT
eurjchem-681	175	16	(	(	PUNCT
eurjchem-681	175	17	µg	µg	NOUN
eurjchem-681	175	18	/	/	SYM
eurjchem-681	175	19	ml	ml	NOUN
eurjchem-681	175	20	)	)	PUNCT
eurjchem-681	175	21	2	2	NUM
eurjchem-681	175	22	2	2	NUM
eurjchem-681	175	23	2	2	NUM
eurjchem-681	175	24	2	2	NUM
eurjchem-681	175	25	*	*	NOUN
eurjchem-681	175	26	intra‐day	intra‐day	NOUN
eurjchem-681	175	27	and	and	CCONJ
eurjchem-681	175	28	inter‐day	inter‐day	PROPN
eurjchem-681	175	29	relative	relative	ADJ
eurjchem-681	175	30	standard	standard	ADJ
eurjchem-681	175	31	deviation	deviation	NOUN
eurjchem-681	175	32	of	of	ADP
eurjchem-681	175	33	the	the	DET
eurjchem-681	175	34	average	average	NOUN
eurjchem-681	175	35	of	of	ADP
eurjchem-681	175	36	three	three	NUM
eurjchem-681	175	37	concentrations	concentration	NOUN
eurjchem-681	175	38	of	of	ADP
eurjchem-681	175	39	the	the	DET
eurjchem-681	175	40	studied	study	VERB
eurjchem-681	175	41	drug	drug	NOUN
eurjchem-681	175	42	.	.	PUNCT
eurjchem-681	176	1	*	*	PUNCT
eurjchem-681	176	2	*	*	PUNCT
eurjchem-681	176	3	lod	lod	PROPN
eurjchem-681	176	4	and	and	CCONJ
eurjchem-681	176	5	loq	loq	PROPN
eurjchem-681	176	6	are	be	AUX
eurjchem-681	176	7	obtained	obtain	VERB
eurjchem-681	176	8	experimentally	experimentally	ADV
eurjchem-681	176	9	.	.	PUNCT
eurjchem-681	177	1	table	table	NOUN
eurjchem-681	177	2	8	8	NUM
eurjchem-681	177	3	.	.	PUNCT
eurjchem-681	178	1	assay	assay	NOUN
eurjchem-681	178	2	validation	validation	NOUN
eurjchem-681	178	3	results	result	NOUN
eurjchem-681	178	4	of	of	ADP
eurjchem-681	178	5	the	the	DET
eurjchem-681	178	6	proposed	propose	VERB
eurjchem-681	178	7	methods	method	NOUN
eurjchem-681	178	8	.	.	PUNCT
eurjchem-681	179	1	parameter	parameter	PROPN
eurjchem-681	179	2	sitagliptin	sitagliptin	PROPN
eurjchem-681	179	3	d3‐method	d3‐method	PROPN
eurjchem-681	179	4	dd1‐method	dd1‐method	PROPN
eurjchem-681	180	1	d0‐method	d0‐method	X
eurjchem-681	180	2	275.3‐280.3	275.3‐280.3	NUM
eurjchem-681	180	3	nm	nm	VERB
eurjchem-681	180	4	255.9	255.9	NUM
eurjchem-681	180	5	nm	nm	NOUN
eurjchem-681	180	6	275.2	275.2	NUM
eurjchem-681	180	7	nm	nm	NOUN
eurjchem-681	180	8	275.3‐280.3	275.3‐280.3	NUM
eurjchem-681	180	9	nm	nm	DET
eurjchem-681	180	10	accuracy	accuracy	NOUN
eurjchem-681	180	11	100.25±0.526	100.25±0.526	NOUN
eurjchem-681	180	12	100.39±0.650	100.39±0.650	NUM
eurjchem-681	180	13	100.42±0.547	100.42±0.547	NOUN
eurjchem-681	180	14	99.96±0.381	99.96±0.381	NUM
eurjchem-681	180	15	specificity	specificity	NOUN
eurjchem-681	180	16	and	and	CCONJ
eurjchem-681	180	17	selectivity	selectivity	NOUN
eurjchem-681	180	18	100.02±0.162	100.02±0.162	NOUN
eurjchem-681	180	19	100.01±0.099	100.01±0.099	NUM
eurjchem-681	180	20	99.93±0.145	99.93±0.145	NUM
eurjchem-681	180	21	100.02±0.175	100.02±0.175	PROPN
eurjchem-681	180	22	precision	precision	NOUN
eurjchem-681	180	23	,	,	PUNCT
eurjchem-681	180	24	repeatability	repeatability	NOUN
eurjchem-681	180	25	*	*	PUNCT
eurjchem-681	180	26	99.51±0.1.123	99.51±0.1.123	NUM
eurjchem-681	180	27	99.42±0	99.42±0	NOUN
eurjchem-681	180	28	.	.	PUNCT
eurjchem-681	181	1	594	594	NUM
eurjchem-681	181	2	101.91±0.426	101.91±0.426	NOUN
eurjchem-681	181	3	102.01±1.094	102.01±1.094	CCONJ
eurjchem-681	181	4	intermediate	intermediate	ADJ
eurjchem-681	181	5	precision	precision	NOUN
eurjchem-681	181	6	*	*	PUNCT
eurjchem-681	181	7	100.94±1.184	100.94±1.184	NUM
eurjchem-681	181	8	99.91±0.0.694	99.91±0.0.694	NUM
eurjchem-681	181	9	99.12±0.0.912	99.12±0.0.912	PROPN
eurjchem-681	181	10	10159±1.278	10159±1.278	NUM
eurjchem-681	181	11	robustness	robustness	NOUN
eurjchem-681	181	12	98.99±0.621	98.99±0.621	NUM
eurjchem-681	182	1	99.34±0.895	99.34±0.895	NUM
eurjchem-681	182	2	102.37±1.024	102.37±1.024	NOUN
eurjchem-681	182	3	99.63±0.845	99.63±0.845	ADJ
eurjchem-681	182	4	linearity	linearity	NOUN
eurjchem-681	182	5	,	,	PUNCT
eurjchem-681	182	6	slope	slope	NOUN
eurjchem-681	182	7	0.0039	0.0039	NUM
eurjchem-681	182	8	0.0086	0.0086	NUM
eurjchem-681	182	9	0.012	0.012	NUM
eurjchem-681	182	10	0.0033	0.0033	NUM
eurjchem-681	182	11	linearity	linearity	NOUN
eurjchem-681	182	12	,	,	PUNCT
eurjchem-681	182	13	intercept	intercept	VERB
eurjchem-681	182	14	0.0279	0.0279	NUM
eurjchem-681	182	15	0.053	0.053	NUM
eurjchem-681	182	16	0.0841	0.0841	NUM
eurjchem-681	182	17	0.0237	0.0237	NUM
eurjchem-681	182	18	linearity	linearity	NOUN
eurjchem-681	182	19	,	,	PUNCT
eurjchem-681	182	20	correlation	correlation	NOUN
eurjchem-681	182	21	coefficient	coefficient	NOUN
eurjchem-681	182	22	(	(	PUNCT
eurjchem-681	182	23	r	r	NOUN
eurjchem-681	182	24	)	)	PUNCT
eurjchem-681	182	25	0.9997	0.9997	NUM
eurjchem-681	182	26	0.9997	0.9997	NUM
eurjchem-681	183	1	0.9998	0.9998	NUM
eurjchem-681	183	2	0.9997	0.9997	NUM
eurjchem-681	183	3	range	range	NOUN
eurjchem-681	183	4	(	(	PUNCT
eurjchem-681	183	5	µg	µg	NOUN
eurjchem-681	183	6	/	/	SYM
eurjchem-681	183	7	ml	ml	NOUN
eurjchem-681	183	8	)	)	PUNCT
eurjchem-681	183	9	40‐360	40‐360	NUM
eurjchem-681	183	10	40‐360	40‐360	NUM
eurjchem-681	183	11	40‐360	40‐360	NUM
eurjchem-681	183	12	40‐360	40‐360	NUM
eurjchem-681	184	1	lod	lod	NOUN
eurjchem-681	184	2	*	*	PUNCT
eurjchem-681	184	3	*	*	PUNCT
eurjchem-681	184	4	(	(	PUNCT
eurjchem-681	184	5	µg	µg	NOUN
eurjchem-681	184	6	/	/	SYM
eurjchem-681	184	7	ml	ml	NOUN
eurjchem-681	184	8	)	)	PUNCT
eurjchem-681	184	9	20	20	NUM
eurjchem-681	184	10	20	20	NUM
eurjchem-681	184	11	20	20	NUM
eurjchem-681	184	12	20	20	NUM
eurjchem-681	184	13	loq	loq	NOUN
eurjchem-681	184	14	*	*	PUNCT
eurjchem-681	184	15	*	*	PUNCT
eurjchem-681	184	16	(	(	PUNCT
eurjchem-681	184	17	µg	µg	NOUN
eurjchem-681	184	18	/	/	SYM
eurjchem-681	184	19	ml	ml	NOUN
eurjchem-681	184	20	)	)	PUNCT
eurjchem-681	184	21	40	40	NUM
eurjchem-681	184	22	40	40	NUM
eurjchem-681	184	23	40	40	NUM
eurjchem-681	184	24	40	40	NUM
eurjchem-681	184	25	*	*	PUNCT
eurjchem-681	184	26	intra‐day	intra‐day	NOUN
eurjchem-681	184	27	and	and	CCONJ
eurjchem-681	184	28	inter‐day	inter‐day	PROPN
eurjchem-681	184	29	relative	relative	ADJ
eurjchem-681	184	30	standard	standard	ADJ
eurjchem-681	184	31	deviation	deviation	NOUN
eurjchem-681	184	32	of	of	ADP
eurjchem-681	184	33	the	the	DET
eurjchem-681	184	34	average	average	NOUN
eurjchem-681	184	35	of	of	ADP
eurjchem-681	184	36	three	three	NUM
eurjchem-681	184	37	concentrations	concentration	NOUN
eurjchem-681	184	38	of	of	ADP
eurjchem-681	184	39	the	the	DET
eurjchem-681	184	40	studied	study	VERB
eurjchem-681	184	41	drug	drug	NOUN
eurjchem-681	184	42	.	.	PUNCT
eurjchem-681	185	1	*	*	PUNCT
eurjchem-681	185	2	*	*	PUNCT
eurjchem-681	185	3	lod	lod	PROPN
eurjchem-681	185	4	and	and	CCONJ
eurjchem-681	185	5	loq	loq	PROPN
eurjchem-681	185	6	are	be	AUX
eurjchem-681	185	7	obtained	obtain	VERB
eurjchem-681	185	8	experimentally	experimentally	ADV
eurjchem-681	185	9	.	.	PUNCT
eurjchem-681	186	1	abdel‐gawad	abdel‐gawad	PROPN
eurjchem-681	186	2	and	and	CCONJ
eurjchem-681	186	3	elsherif	elsherif	VERB
eurjchem-681	186	4	/	/	SYM
eurjchem-681	186	5	european	european	PROPN
eurjchem-681	186	6	journal	journal	PROPN
eurjchem-681	186	7	of	of	ADP
eurjchem-681	186	8	chemistry	chemistry	NOUN
eurjchem-681	186	9	3	3	NUM
eurjchem-681	186	10	(	(	PUNCT
eurjchem-681	186	11	4	4	NUM
eurjchem-681	186	12	)	)	PUNCT
eurjchem-681	186	13	(	(	PUNCT
eurjchem-681	186	14	2012	2012	NUM
eurjchem-681	186	15	)	)	PUNCT
eurjchem-681	186	16	447‐454	447‐454	PROPN
eurjchem-681	186	17	453	453	NUM
eurjchem-681	186	18	table	table	NOUN
eurjchem-681	186	19	9	9	NUM
eurjchem-681	186	20	.	.	PUNCT
eurjchem-681	186	21	results	result	NOUN
eurjchem-681	186	22	of	of	ADP
eurjchem-681	186	23	accuracy	accuracy	NOUN
eurjchem-681	186	24	for	for	ADP
eurjchem-681	186	25	the	the	DET
eurjchem-681	186	26	simultaneous	simultaneous	ADJ
eurjchem-681	186	27	determination	determination	NOUN
eurjchem-681	186	28	of	of	ADP
eurjchem-681	186	29	simvastatin	simvastatin	NOUN
eurjchem-681	186	30	and	and	CCONJ
eurjchem-681	186	31	sitagliptin	sitagliptin	NOUN
eurjchem-681	186	32	by	by	ADP
eurjchem-681	186	33	the	the	DET
eurjchem-681	186	34	proposed	propose	VERB
eurjchem-681	186	35	methods	method	NOUN
eurjchem-681	186	36	.	.	PUNCT
eurjchem-681	187	1	claimed	claim	VERB
eurjchem-681	187	2	simvastatin	simvastatin	NOUN
eurjchem-681	187	3	(	(	PUNCT
eurjchem-681	187	4	µg	µg	ADJ
eurjchem-681	187	5	/	/	SYM
eurjchem-681	187	6	ml	ml	NOUN
eurjchem-681	187	7	)	)	PUNCT
eurjchem-681	187	8	d3‐method	d3‐method	PROPN
eurjchem-681	187	9	dd1‐method	dd1‐method	PROPN
eurjchem-681	187	10	240.5‐244.7	240.5‐244.7	NUM
eurjchem-681	187	11	nm	nm	NOUN
eurjchem-681	187	12	228.3	228.3	NUM
eurjchem-681	187	13	nm	nm	NOUN
eurjchem-681	187	14	240.5	240.5	NUM
eurjchem-681	187	15	nm	nm	PRON
eurjchem-681	187	16	248	248	NUM
eurjchem-681	187	17	nm	nm	ADV
eurjchem-681	187	18	found	find	VERB
eurjchem-681	187	19	*	*	PUNCT
eurjchem-681	187	20	recovery	recovery	NOUN
eurjchem-681	187	21	found	find	VERB
eurjchem-681	187	22	*	*	PUNCT
eurjchem-681	187	23	recovery	recovery	NOUN
eurjchem-681	187	24	found	find	VERB
eurjchem-681	187	25	*	*	PUNCT
eurjchem-681	187	26	recovery	recovery	NOUN
eurjchem-681	187	27	found	find	VERB
eurjchem-681	187	28	*	*	PUNCT
eurjchem-681	187	29	recovery	recovery	NOUN
eurjchem-681	187	30	4	4	NUM
eurjchem-681	187	31	4.03	4.03	NUM
eurjchem-681	187	32	100.75	100.75	NUM
eurjchem-681	187	33	4.04	4.04	NUM
eurjchem-681	187	34	101.00	101.00	NUM
eurjchem-681	187	35	3.98	3.98	NUM
eurjchem-681	187	36	99.50	99.50	NUM
eurjchem-681	187	37	4.03	4.03	NUM
eurjchem-681	187	38	100.75	100.75	NUM
eurjchem-681	187	39	8	8	NUM
eurjchem-681	187	40	8.05	8.05	NUM
eurjchem-681	187	41	100.63	100.63	NUM
eurjchem-681	187	42	7.96	7.96	NUM
eurjchem-681	187	43	99.50	99.50	NUM
eurjchem-681	187	44	8.03	8.03	NUM
eurjchem-681	187	45	100.38	100.38	NUM
eurjchem-681	187	46	7.99	7.99	NUM
eurjchem-681	187	47	99.88	99.88	NUM
eurjchem-681	187	48	12	12	NUM
eurjchem-681	187	49	11.91	11.91	NUM
eurjchem-681	187	50	99.25	99.25	NUM
eurjchem-681	187	51	11.97	11.97	NUM
eurjchem-681	187	52	99.75	99.75	NUM
eurjchem-681	187	53	12.03	12.03	NUM
eurjchem-681	187	54	100.25	100.25	NUM
eurjchem-681	187	55	12.05	12.05	NUM
eurjchem-681	187	56	100.42	100.42	NUM
eurjchem-681	187	57	16	16	NUM
eurjchem-681	187	58	15.90	15.90	NUM
eurjchem-681	187	59	99.38	99.38	NUM
eurjchem-681	187	60	16.11	16.11	NUM
eurjchem-681	187	61	100.69	100.69	NUM
eurjchem-681	187	62	16.09	16.09	NUM
eurjchem-681	187	63	100.56	100.56	NUM
eurjchem-681	187	64	16.08	16.08	NUM
eurjchem-681	187	65	100.50	100.50	NUM
eurjchem-681	187	66	mean	mean	NOUN
eurjchem-681	187	67	±	±	NUM
eurjchem-681	187	68	s.d	s.d	PROPN
eurjchem-681	187	69	.	.	PROPN
eurjchem-681	187	70	100.00±0.797	100.00±0.797	PROPN
eurjchem-681	187	71	100.24±0.723	100.24±0.723	NUM
eurjchem-681	187	72	100.17±0.466	100.17±0.466	NUM
eurjchem-681	187	73	100.39±0.366	100.39±0.366	NUM
eurjchem-681	187	74	*	*	PUNCT
eurjchem-681	187	75	average	average	NOUN
eurjchem-681	187	76	of	of	ADP
eurjchem-681	187	77	three	three	NUM
eurjchem-681	187	78	determinations	determination	NOUN
eurjchem-681	187	79	.	.	PUNCT
eurjchem-681	188	1	table	table	NOUN
eurjchem-681	188	2	10	10	NUM
eurjchem-681	188	3	.	.	PUNCT
eurjchem-681	189	1	results	result	NOUN
eurjchem-681	189	2	of	of	ADP
eurjchem-681	189	3	accuracy	accuracy	NOUN
eurjchem-681	189	4	for	for	ADP
eurjchem-681	189	5	the	the	DET
eurjchem-681	189	6	simultaneous	simultaneous	ADJ
eurjchem-681	189	7	determination	determination	NOUN
eurjchem-681	189	8	of	of	ADP
eurjchem-681	189	9	simvastatin	simvastatin	NOUN
eurjchem-681	189	10	and	and	CCONJ
eurjchem-681	189	11	sitagliptin	sitagliptin	NOUN
eurjchem-681	189	12	by	by	ADP
eurjchem-681	189	13	the	the	DET
eurjchem-681	189	14	proposed	propose	VERB
eurjchem-681	189	15	methods	method	NOUN
eurjchem-681	189	16	.	.	PUNCT
eurjchem-681	190	1	claimed	claim	VERB
eurjchem-681	190	2	sitagliptin	sitagliptin	NOUN
eurjchem-681	190	3	(	(	PUNCT
eurjchem-681	190	4	µg	µg	NOUN
eurjchem-681	190	5	/	/	SYM
eurjchem-681	190	6	ml	ml	NOUN
eurjchem-681	190	7	)	)	PUNCT
eurjchem-681	190	8	d3‐method	d3‐method	NOUN
eurjchem-681	190	9	dd1‐method	dd1‐method	NOUN
eurjchem-681	190	10	d0‐method	d0‐method	X
eurjchem-681	190	11	275.3‐280.3	275.3‐280.3	NUM
eurjchem-681	190	12	nm	nm	VERB
eurjchem-681	190	13	255.9	255.9	NUM
eurjchem-681	190	14	nm	nm	NOUN
eurjchem-681	190	15	275.2	275.2	NUM
eurjchem-681	190	16	nm	nm	NUM
eurjchem-681	190	17	266.4	266.4	NUM
eurjchem-681	190	18	nm	nm	NOUN
eurjchem-681	190	19	found	find	VERB
eurjchem-681	190	20	*	*	PUNCT
eurjchem-681	190	21	recovery	recovery	NOUN
eurjchem-681	190	22	found	find	VERB
eurjchem-681	190	23	*	*	PUNCT
eurjchem-681	190	24	recovery	recovery	NOUN
eurjchem-681	190	25	found	find	VERB
eurjchem-681	190	26	*	*	PUNCT
eurjchem-681	190	27	recovery	recovery	NOUN
eurjchem-681	190	28	found	find	VERB
eurjchem-681	190	29	*	*	PUNCT
eurjchem-681	190	30	recovery	recovery	NOUN
eurjchem-681	190	31	80	80	NUM
eurjchem-681	190	32	79.85	79.85	NUM
eurjchem-681	190	33	99.81	99.81	NUM
eurjchem-681	190	34	80.96	80.96	NUM
eurjchem-681	190	35	101.20	101.20	NUM
eurjchem-681	190	36	80.79	80.79	NUM
eurjchem-681	190	37	80.79	80.79	NUM
eurjchem-681	190	38	79.69	79.69	NUM
eurjchem-681	190	39	99.61	99.61	NUM
eurjchem-681	190	40	160	160	NUM
eurjchem-681	190	41	161.51	161.51	NUM
eurjchem-681	190	42	100.94	100.94	NUM
eurjchem-681	190	43	160.84	160.84	NUM
eurjchem-681	190	44	100.53	100.53	NUM
eurjchem-681	190	45	161.12	161.12	NUM
eurjchem-681	190	46	161.12	161.12	NUM
eurjchem-681	190	47	159.64	159.64	NUM
eurjchem-681	190	48	99.78	99.78	NUM
eurjchem-681	190	49	240	240	NUM
eurjchem-681	190	50	240.91	240.91	NUM
eurjchem-681	190	51	100.38	100.38	NUM
eurjchem-681	190	52	239.15	239.15	NUM
eurjchem-681	190	53	99.65	99.65	NUM
eurjchem-681	190	54	240.68	240.68	NUM
eurjchem-681	190	55	240.68	240.68	NUM
eurjchem-681	190	56	239.87	239.87	NUM
eurjchem-681	190	57	99.95	99.95	NUM
eurjchem-681	190	58	320	320	NUM
eurjchem-681	190	59	319.58	319.58	NUM
eurjchem-681	190	60	99.87	99.87	NUM
eurjchem-681	190	61	320.58	320.58	NUM
eurjchem-681	190	62	100.18	100.18	NUM
eurjchem-681	190	63	319.15	319.15	NUM
eurjchem-681	190	64	319.15	319.15	NUM
eurjchem-681	190	65	321.56	321.56	NUM
eurjchem-681	190	66	100.49	100.49	NUM
eurjchem-681	190	67	mean	mean	NOUN
eurjchem-681	190	68	±	±	NUM
eurjchem-681	190	69	s.d	s.d	PROPN
eurjchem-681	190	70	.	.	PROPN
eurjchem-681	190	71	100.25±0.526	100.25±0.526	PROPN
eurjchem-681	190	72	100.39±0.650	100.39±0.650	X
eurjchem-681	191	1	100.42±.547	100.42±.547	NUM
eurjchem-681	192	1	99.96±0.381	99.96±0.381	NUM
eurjchem-681	193	1	*	*	PUNCT
eurjchem-681	193	2	average	average	NOUN
eurjchem-681	193	3	of	of	ADP
eurjchem-681	193	4	three	three	NUM
eurjchem-681	193	5	determinations	determination	NOUN
eurjchem-681	193	6	.	.	PUNCT
eurjchem-681	194	1	the	the	DET
eurjchem-681	194	2	respective	respective	ADJ
eurjchem-681	194	3	%	%	NOUN
eurjchem-681	194	4	recovery	recovery	NOUN
eurjchem-681	195	1	and	and	CCONJ
eurjchem-681	195	2	%	%	INTJ
eurjchem-681	195	3	r.s.d.s	r.s.d.s	INTJ
eurjchem-681	195	4	for	for	ADP
eurjchem-681	195	5	the	the	DET
eurjchem-681	195	6	two	two	NUM
eurjchem-681	195	7	drugs	drug	NOUN
eurjchem-681	195	8	are	be	AUX
eurjchem-681	195	9	shown	show	VERB
eurjchem-681	195	10	in	in	ADP
eurjchem-681	195	11	table	table	NOUN
eurjchem-681	195	12	3	3	NUM
eurjchem-681	195	13	and	and	CCONJ
eurjchem-681	195	14	4	4	NUM
eurjchem-681	195	15	where	where	SCONJ
eurjchem-681	195	16	,	,	PUNCT
eurjchem-681	195	17	the	the	DET
eurjchem-681	195	18	relative	relative	ADJ
eurjchem-681	195	19	standard	standard	ADJ
eurjchem-681	195	20	deviation	deviation	NOUN
eurjchem-681	195	21	is	be	AUX
eurjchem-681	195	22	<	<	X
eurjchem-681	195	23	1.5	1.5	NUM
eurjchem-681	195	24	in	in	ADP
eurjchem-681	195	25	the	the	DET
eurjchem-681	195	26	assay	assay	NOUN
eurjchem-681	195	27	of	of	ADP
eurjchem-681	195	28	raw	raw	ADJ
eurjchem-681	195	29	materials	material	NOUN
eurjchem-681	195	30	and	and	CCONJ
eurjchem-681	195	31	tablets	tablet	NOUN
eurjchem-681	195	32	by	by	ADP
eurjchem-681	195	33	the	the	DET
eurjchem-681	195	34	three	three	NUM
eurjchem-681	195	35	proposed	propose	VERB
eurjchem-681	195	36	method	method	NOUN
eurjchem-681	195	37	.	.	PUNCT
eurjchem-681	196	1	accuracy	accuracy	NOUN
eurjchem-681	196	2	:	:	PUNCT
eurjchem-681	196	3	the	the	DET
eurjchem-681	196	4	accuracy	accuracy	NOUN
eurjchem-681	196	5	of	of	ADP
eurjchem-681	196	6	the	the	DET
eurjchem-681	196	7	results	result	NOUN
eurjchem-681	196	8	was	be	AUX
eurjchem-681	196	9	checked	check	VERB
eurjchem-681	196	10	by	by	ADP
eurjchem-681	196	11	applying	apply	VERB
eurjchem-681	196	12	the	the	DET
eurjchem-681	196	13	proposed	propose	VERB
eurjchem-681	196	14	methods	method	NOUN
eurjchem-681	196	15	for	for	ADP
eurjchem-681	196	16	determination	determination	NOUN
eurjchem-681	196	17	of	of	ADP
eurjchem-681	196	18	different	different	ADJ
eurjchem-681	196	19	samples	sample	NOUN
eurjchem-681	196	20	of	of	ADP
eurjchem-681	196	21	sit	sit	NOUN
eurjchem-681	196	22	and	and	CCONJ
eurjchem-681	196	23	sim	sim	NOUN
eurjchem-681	196	24	.	.	PUNCT
eurjchem-681	197	1	the	the	DET
eurjchem-681	197	2	concentrations	concentration	NOUN
eurjchem-681	197	3	were	be	AUX
eurjchem-681	197	4	obtained	obtain	VERB
eurjchem-681	197	5	from	from	ADP
eurjchem-681	197	6	the	the	DET
eurjchem-681	197	7	corresponding	corresponding	ADJ
eurjchem-681	197	8	regression	regression	NOUN
eurjchem-681	197	9	equations	equation	NOUN
eurjchem-681	197	10	.	.	PUNCT
eurjchem-681	198	1	from	from	ADP
eurjchem-681	198	2	which	which	PRON
eurjchem-681	198	3	the	the	DET
eurjchem-681	198	4	percentage	percentage	NOUN
eurjchem-681	198	5	recoveries	recovery	NOUN
eurjchem-681	198	6	were	be	AUX
eurjchem-681	198	7	calculated	calculate	VERB
eurjchem-681	198	8	with	with	ADP
eurjchem-681	198	9	mean	mean	ADJ
eurjchem-681	198	10	percentage	percentage	NOUN
eurjchem-681	198	11	recovery	recovery	NOUN
eurjchem-681	198	12	shown	show	VERB
eurjchem-681	198	13	in	in	ADP
eurjchem-681	198	14	table	table	NOUN
eurjchem-681	198	15	9	9	NUM
eurjchem-681	198	16	and	and	CCONJ
eurjchem-681	198	17	10	10	NUM
eurjchem-681	198	18	.	.	PUNCT
eurjchem-681	199	1	accuracy	accuracy	NOUN
eurjchem-681	199	2	of	of	ADP
eurjchem-681	199	3	the	the	DET
eurjchem-681	199	4	methods	method	NOUN
eurjchem-681	199	5	was	be	AUX
eurjchem-681	199	6	further	far	ADV
eurjchem-681	199	7	assured	assure	VERB
eurjchem-681	199	8	by	by	ADP
eurjchem-681	199	9	the	the	DET
eurjchem-681	199	10	use	use	NOUN
eurjchem-681	199	11	of	of	ADP
eurjchem-681	199	12	the	the	DET
eurjchem-681	199	13	standard	standard	ADJ
eurjchem-681	199	14	addition	addition	NOUN
eurjchem-681	199	15	technique	technique	NOUN
eurjchem-681	199	16	,	,	PUNCT
eurjchem-681	199	17	it	it	PRON
eurjchem-681	199	18	was	be	AUX
eurjchem-681	199	19	performed	perform	VERB
eurjchem-681	199	20	by	by	ADP
eurjchem-681	199	21	addition	addition	NOUN
eurjchem-681	199	22	of	of	ADP
eurjchem-681	199	23	known	known	ADJ
eurjchem-681	199	24	amounts	amount	NOUN
eurjchem-681	199	25	of	of	ADP
eurjchem-681	199	26	pure	pure	ADJ
eurjchem-681	199	27	sit	sit	NOUN
eurjchem-681	199	28	(	(	PUNCT
eurjchem-681	199	29	40	40	NUM
eurjchem-681	199	30	,	,	PUNCT
eurjchem-681	199	31	80	80	NUM
eurjchem-681	199	32	and	and	CCONJ
eurjchem-681	199	33	120	120	NUM
eurjchem-681	199	34	µg	µg	ADJ
eurjchem-681	199	35	/	/	SYM
eurjchem-681	199	36	ml	ml	NOUN
eurjchem-681	199	37	)	)	PUNCT
eurjchem-681	199	38	and	and	CCONJ
eurjchem-681	199	39	sim	sim	ADJ
eurjchem-681	199	40	(	(	PUNCT
eurjchem-681	199	41	2	2	NUM
eurjchem-681	199	42	,	,	PUNCT
eurjchem-681	199	43	4	4	NUM
eurjchem-681	199	44	and	and	CCONJ
eurjchem-681	199	45	6	6	NUM
eurjchem-681	199	46	µg	µg	NOUN
eurjchem-681	199	47	/	/	SYM
eurjchem-681	199	48	ml	ml	NOUN
eurjchem-681	199	49	)	)	PUNCT
eurjchem-681	199	50	to	to	ADP
eurjchem-681	199	51	known	know	VERB
eurjchem-681	199	52	concentrations	concentration	NOUN
eurjchem-681	199	53	of	of	ADP
eurjchem-681	199	54	the	the	DET
eurjchem-681	199	55	pharmaceutical	pharmaceutical	ADJ
eurjchem-681	199	56	preparation	preparation	NOUN
eurjchem-681	199	57	(	(	PUNCT
eurjchem-681	199	58	64.25	64.25	NUM
eurjchem-681	199	59	for	for	ADP
eurjchem-681	199	60	sit	sit	NOUN
eurjchem-681	199	61	and	and	CCONJ
eurjchem-681	199	62	10	10	NUM
eurjchem-681	199	63	µg	µg	NOUN
eurjchem-681	199	64	/	/	SYM
eurjchem-681	199	65	ml	ml	NOUN
eurjchem-681	199	66	for	for	ADP
eurjchem-681	199	67	sim	sim	NOUN
eurjchem-681	199	68	)	)	PUNCT
eurjchem-681	199	69	the	the	DET
eurjchem-681	199	70	resulting	result	VERB
eurjchem-681	199	71	mixtures	mixture	NOUN
eurjchem-681	199	72	were	be	AUX
eurjchem-681	199	73	assayed	assayed	ADJ
eurjchem-681	199	74	,	,	PUNCT
eurjchem-681	199	75	and	and	CCONJ
eurjchem-681	199	76	the	the	DET
eurjchem-681	199	77	results	result	NOUN
eurjchem-681	199	78	obtained	obtain	VERB
eurjchem-681	199	79	were	be	AUX
eurjchem-681	199	80	compared	compare	VERB
eurjchem-681	199	81	with	with	ADP
eurjchem-681	199	82	the	the	DET
eurjchem-681	199	83	expected	expect	VERB
eurjchem-681	199	84	results	result	NOUN
eurjchem-681	199	85	(	(	PUNCT
eurjchem-681	199	86	table	table	NOUN
eurjchem-681	199	87	3	3	NUM
eurjchem-681	199	88	and	and	CCONJ
eurjchem-681	199	89	4	4	NUM
eurjchem-681	199	90	)	)	PUNCT
eurjchem-681	199	91	.	.	PUNCT
eurjchem-681	200	1	the	the	DET
eurjchem-681	200	2	good	good	ADJ
eurjchem-681	200	3	recoveries	recovery	NOUN
eurjchem-681	200	4	of	of	ADP
eurjchem-681	200	5	standard	standard	ADJ
eurjchem-681	200	6	addition	addition	NOUN
eurjchem-681	200	7	technique	technique	NOUN
eurjchem-681	200	8	suggested	suggest	VERB
eurjchem-681	200	9	good	good	ADJ
eurjchem-681	200	10	accuracy	accuracy	NOUN
eurjchem-681	200	11	of	of	ADP
eurjchem-681	200	12	the	the	DET
eurjchem-681	200	13	proposed	propose	VERB
eurjchem-681	200	14	methods	method	NOUN
eurjchem-681	200	15	.	.	PUNCT
eurjchem-681	201	1	selectivity	selectivity	NOUN
eurjchem-681	201	2	:	:	PUNCT
eurjchem-681	201	3	the	the	DET
eurjchem-681	201	4	selectivity	selectivity	NOUN
eurjchem-681	201	5	of	of	ADP
eurjchem-681	201	6	the	the	DET
eurjchem-681	201	7	methods	method	NOUN
eurjchem-681	201	8	was	be	AUX
eurjchem-681	201	9	achieved	achieve	VERB
eurjchem-681	201	10	by	by	ADP
eurjchem-681	201	11	the	the	DET
eurjchem-681	201	12	analysis	analysis	NOUN
eurjchem-681	201	13	of	of	ADP
eurjchem-681	201	14	different	different	ADJ
eurjchem-681	201	15	laboratory	laboratory	NOUN
eurjchem-681	201	16	prepared	prepare	VERB
eurjchem-681	201	17	mixtures	mixture	NOUN
eurjchem-681	201	18	of	of	ADP
eurjchem-681	201	19	sit	sit	NOUN
eurjchem-681	201	20	and	and	CCONJ
eurjchem-681	201	21	sim	sim	VERB
eurjchem-681	201	22	within	within	ADP
eurjchem-681	201	23	the	the	DET
eurjchem-681	201	24	linearity	linearity	NOUN
eurjchem-681	201	25	range	range	NOUN
eurjchem-681	201	26	.	.	PUNCT
eurjchem-681	202	1	satisfactory	satisfactory	ADJ
eurjchem-681	202	2	results	result	NOUN
eurjchem-681	202	3	(	(	PUNCT
eurjchem-681	202	4	table	table	NOUN
eurjchem-681	202	5	3	3	NUM
eurjchem-681	202	6	and	and	CCONJ
eurjchem-681	202	7	4	4	NUM
eurjchem-681	202	8	)	)	PUNCT
eurjchem-681	202	9	;	;	PUNCT
eurjchem-681	202	10	which	which	PRON
eurjchem-681	202	11	prove	prove	VERB
eurjchem-681	202	12	that	that	SCONJ
eurjchem-681	202	13	the	the	DET
eurjchem-681	202	14	proposed	propose	VERB
eurjchem-681	202	15	methods	method	NOUN
eurjchem-681	202	16	,	,	PUNCT
eurjchem-681	202	17	in	in	ADP
eurjchem-681	202	18	addition	addition	NOUN
eurjchem-681	202	19	to	to	ADP
eurjchem-681	202	20	its	its	PRON
eurjchem-681	202	21	selectivity	selectivity	NOUN
eurjchem-681	202	22	to	to	ADP
eurjchem-681	202	23	the	the	DET
eurjchem-681	202	24	cited	cite	VERB
eurjchem-681	202	25	drug	drug	NOUN
eurjchem-681	202	26	no	no	DET
eurjchem-681	202	27	interference	interference	NOUN
eurjchem-681	202	28	from	from	ADP
eurjchem-681	202	29	the	the	DET
eurjchem-681	202	30	presence	presence	NOUN
eurjchem-681	202	31	of	of	ADP
eurjchem-681	202	32	formulation	formulation	NOUN
eurjchem-681	202	33	matrix	matrix	NOUN
eurjchem-681	202	34	.	.	PUNCT
eurjchem-681	203	1	robustness	robustness	NOUN
eurjchem-681	203	2	:	:	PUNCT
eurjchem-681	203	3	robustness	robustness	NOUN
eurjchem-681	203	4	which	which	PRON
eurjchem-681	203	5	is	be	AUX
eurjchem-681	203	6	the	the	DET
eurjchem-681	203	7	prove	prove	NOUN
eurjchem-681	203	8	that	that	SCONJ
eurjchem-681	203	9	the	the	DET
eurjchem-681	203	10	method	method	NOUN
eurjchem-681	203	11	is	be	AUX
eurjchem-681	203	12	not	not	PART
eurjchem-681	203	13	affected	affect	VERB
eurjchem-681	203	14	by	by	ADP
eurjchem-681	203	15	small	small	ADJ
eurjchem-681	203	16	deliberated	deliberate	VERB
eurjchem-681	203	17	change	change	NOUN
eurjchem-681	203	18	was	be	AUX
eurjchem-681	203	19	tested	test	VERB
eurjchem-681	203	20	i.e.	i.e.	X
eurjchem-681	203	21	by	by	ADP
eurjchem-681	203	22	trying	try	VERB
eurjchem-681	203	23	to	to	PART
eurjchem-681	203	24	apply	apply	VERB
eurjchem-681	203	25	the	the	DET
eurjchem-681	203	26	proposed	propose	VERB
eurjchem-681	203	27	methods	method	NOUN
eurjchem-681	203	28	using	use	VERB
eurjchem-681	203	29	small	small	ADJ
eurjchem-681	203	30	variation	variation	NOUN
eurjchem-681	203	31	of	of	ADP
eurjchem-681	203	32	ratio	ratio	NOUN
eurjchem-681	203	33	of	of	ADP
eurjchem-681	203	34	the	the	DET
eurjchem-681	203	35	solvent	solvent	NOUN
eurjchem-681	203	36	mixture	mixture	NOUN
eurjchem-681	203	37	used	use	VERB
eurjchem-681	203	38	and	and	CCONJ
eurjchem-681	203	39	the	the	DET
eurjchem-681	203	40	degree	degree	NOUN
eurjchem-681	203	41	of	of	ADP
eurjchem-681	203	42	the	the	DET
eurjchem-681	203	43	smoothing	smoothing	NOUN
eurjchem-681	203	44	of	of	ADP
eurjchem-681	203	45	the	the	DET
eurjchem-681	203	46	derivative	derivative	ADJ
eurjchem-681	203	47	curves	curve	NOUN
eurjchem-681	203	48	and	and	CCONJ
eurjchem-681	203	49	no	no	DET
eurjchem-681	203	50	effects	effect	NOUN
eurjchem-681	203	51	was	be	AUX
eurjchem-681	203	52	observed	observe	VERB
eurjchem-681	203	53	.	.	PUNCT
eurjchem-681	204	1	repeatability	repeatability	NOUN
eurjchem-681	204	2	:	:	PUNCT
eurjchem-681	204	3	three	three	NUM
eurjchem-681	204	4	concentrations	concentration	NOUN
eurjchem-681	204	5	of	of	ADP
eurjchem-681	204	6	sit	sit	VERB
eurjchem-681	204	7	and	and	CCONJ
eurjchem-681	204	8	sim	sim	NOUN
eurjchem-681	204	9	were	be	AUX
eurjchem-681	204	10	analyzed	analyze	VERB
eurjchem-681	204	11	three	three	NUM
eurjchem-681	204	12	times	time	NOUN
eurjchem-681	204	13	intra‐daily	intra‐daily	ADV
eurjchem-681	204	14	using	use	VERB
eurjchem-681	204	15	the	the	DET
eurjchem-681	204	16	proposed	propose	VERB
eurjchem-681	204	17	methods	method	NOUN
eurjchem-681	204	18	.	.	PUNCT
eurjchem-681	205	1	the	the	DET
eurjchem-681	205	2	percentage	percentage	NOUN
eurjchem-681	205	3	recoveries	recovery	NOUN
eurjchem-681	205	4	and	and	CCONJ
eurjchem-681	205	5	relative	relative	ADJ
eurjchem-681	205	6	standard	standard	ADJ
eurjchem-681	205	7	deviation	deviation	NOUN
eurjchem-681	205	8	were	be	AUX
eurjchem-681	205	9	calculated	calculate	VERB
eurjchem-681	205	10	(	(	PUNCT
eurjchem-681	205	11	table	table	NOUN
eurjchem-681	205	12	7	7	NUM
eurjchem-681	205	13	and	and	CCONJ
eurjchem-681	205	14	8)	8)	NUM
eurjchem-681	205	15	.	.	PUNCT
eurjchem-681	206	1	intermediate	intermediate	ADJ
eurjchem-681	206	2	precision	precision	NOUN
eurjchem-681	206	3	:	:	PUNCT
eurjchem-681	206	4	the	the	DET
eurjchem-681	206	5	previous	previous	ADJ
eurjchem-681	206	6	procedures	procedure	NOUN
eurjchem-681	206	7	were	be	AUX
eurjchem-681	206	8	repeated	repeat	VERB
eurjchem-681	206	9	inter‐daily	inter‐daily	ADV
eurjchem-681	206	10	on	on	ADP
eurjchem-681	206	11	three	three	NUM
eurjchem-681	206	12	different	different	ADJ
eurjchem-681	206	13	days	day	NOUN
eurjchem-681	206	14	for	for	ADP
eurjchem-681	206	15	the	the	DET
eurjchem-681	206	16	analysis	analysis	NOUN
eurjchem-681	206	17	of	of	ADP
eurjchem-681	206	18	the	the	DET
eurjchem-681	206	19	chosen	choose	VERB
eurjchem-681	206	20	concentrations	concentration	NOUN
eurjchem-681	206	21	.	.	PUNCT
eurjchem-681	207	1	the	the	DET
eurjchem-681	207	2	percentage	percentage	NOUN
eurjchem-681	207	3	recoveries	recovery	NOUN
eurjchem-681	207	4	and	and	CCONJ
eurjchem-681	207	5	relative	relative	ADJ
eurjchem-681	207	6	standard	standard	ADJ
eurjchem-681	207	7	deviation	deviation	NOUN
eurjchem-681	207	8	were	be	AUX
eurjchem-681	207	9	calculated	calculate	VERB
eurjchem-681	207	10	(	(	PUNCT
eurjchem-681	207	11	table	table	NOUN
eurjchem-681	207	12	7	7	NUM
eurjchem-681	207	13	and	and	CCONJ
eurjchem-681	207	14	8)	8)	NUM
eurjchem-681	207	15	.	.	NOUN
eurjchem-681	208	1	3.5	3.5	NUM
eurjchem-681	208	2	.	.	PUNCT
eurjchem-681	208	3	application	application	NOUN
eurjchem-681	208	4	of	of	ADP
eurjchem-681	208	5	the	the	DET
eurjchem-681	208	6	method	method	NOUN
eurjchem-681	208	7	in	in	ADP
eurjchem-681	208	8	tablets	tablet	NOUN
eurjchem-681	208	9	the	the	DET
eurjchem-681	208	10	proposed	propose	VERB
eurjchem-681	208	11	methods	method	NOUN
eurjchem-681	208	12	were	be	AUX
eurjchem-681	208	13	applied	apply	VERB
eurjchem-681	208	14	for	for	ADP
eurjchem-681	208	15	the	the	DET
eurjchem-681	208	16	determination	determination	NOUN
eurjchem-681	208	17	of	of	ADP
eurjchem-681	208	18	sit	sit	NOUN
eurjchem-681	208	19	and	and	CCONJ
eurjchem-681	208	20	sim	sim	VERB
eurjchem-681	208	21	in	in	ADP
eurjchem-681	208	22	their	their	PRON
eurjchem-681	208	23	combined	combine	VERB
eurjchem-681	208	24	pharmaceutical	pharmaceutical	ADJ
eurjchem-681	208	25	formulation	formulation	NOUN
eurjchem-681	208	26	.	.	PUNCT
eurjchem-681	209	1	laboratory	laboratory	NOUN
eurjchem-681	209	2	prepared	prepare	VERB
eurjchem-681	209	3	mixtures	mixture	NOUN
eurjchem-681	209	4	were	be	AUX
eurjchem-681	209	5	successfully	successfully	ADV
eurjchem-681	209	6	tried	try	VERB
eurjchem-681	209	7	for	for	ADP
eurjchem-681	209	8	the	the	DET
eurjchem-681	209	9	three	three	NUM
eurjchem-681	209	10	compositions	composition	NOUN
eurjchem-681	209	11	of	of	ADP
eurjchem-681	209	12	tablets	tablet	NOUN
eurjchem-681	209	13	(	(	PUNCT
eurjchem-681	209	14	10	10	NUM
eurjchem-681	209	15	,	,	PUNCT
eurjchem-681	209	16	20	20	NUM
eurjchem-681	209	17	and	and	CCONJ
eurjchem-681	209	18	40	40	NUM
eurjchem-681	209	19	mg	mg	NOUN
eurjchem-681	209	20	of	of	ADP
eurjchem-681	209	21	sim	sim	NOUN
eurjchem-681	209	22	)	)	PUNCT
eurjchem-681	209	23	with	with	ADP
eurjchem-681	209	24	100	100	NUM
eurjchem-681	209	25	mg	mg	ADP
eurjchem-681	209	26	of	of	ADP
eurjchem-681	209	27	sit	sit	NOUN
eurjchem-681	209	28	,	,	PUNCT
eurjchem-681	209	29	the	the	DET
eurjchem-681	209	30	results	result	NOUN
eurjchem-681	209	31	are	be	AUX
eurjchem-681	209	32	shown	show	VERB
eurjchem-681	209	33	in	in	ADP
eurjchem-681	209	34	table	table	NOUN
eurjchem-681	209	35	1	1	NUM
eurjchem-681	209	36	.	.	PUNCT
eurjchem-681	210	1	the	the	DET
eurjchem-681	210	2	high	high	ADJ
eurjchem-681	210	3	percentage	percentage	NOUN
eurjchem-681	210	4	recoveries	recovery	NOUN
eurjchem-681	210	5	(	(	PUNCT
eurjchem-681	210	6	99.60‐100.31	99.60‐100.31	NUM
eurjchem-681	210	7	%	%	NOUN
eurjchem-681	210	8	)	)	PUNCT
eurjchem-681	210	9	and	and	CCONJ
eurjchem-681	210	10	low	low	ADJ
eurjchem-681	210	11	%	%	NOUN
eurjchem-681	210	12	cv	cv	PROPN
eurjchem-681	210	13	(	(	PUNCT
eurjchem-681	210	14	0.099‐	0.099‐	NOUN
eurjchem-681	210	15	0.543	0.543	NUM
eurjchem-681	210	16	)	)	PUNCT
eurjchem-681	210	17	values	value	NOUN
eurjchem-681	210	18	confirm	confirm	VERB
eurjchem-681	210	19	the	the	DET
eurjchem-681	210	20	suitability	suitability	NOUN
eurjchem-681	210	21	of	of	ADP
eurjchem-681	210	22	the	the	DET
eurjchem-681	210	23	proposed	propose	VERB
eurjchem-681	210	24	methods	method	NOUN
eurjchem-681	210	25	for	for	ADP
eurjchem-681	210	26	the	the	DET
eurjchem-681	210	27	routine	routine	ADJ
eurjchem-681	210	28	determination	determination	NOUN
eurjchem-681	210	29	of	of	ADP
eurjchem-681	210	30	these	these	DET
eurjchem-681	210	31	components	component	NOUN
eurjchem-681	210	32	in	in	ADP
eurjchem-681	210	33	new	new	ADJ
eurjchem-681	210	34	combined	combined	ADJ
eurjchem-681	210	35	formulation	formulation	NOUN
eurjchem-681	210	36	.	.	PUNCT
eurjchem-681	211	1	moreover	moreover	ADV
eurjchem-681	211	2	,	,	PUNCT
eurjchem-681	211	3	the	the	DET
eurjchem-681	211	4	proposed	propose	VERB
eurjchem-681	211	5	methods	method	NOUN
eurjchem-681	211	6	is	be	AUX
eurjchem-681	211	7	proved	prove	VERB
eurjchem-681	211	8	to	to	PART
eurjchem-681	211	9	be	be	AUX
eurjchem-681	211	10	much	much	ADV
eurjchem-681	211	11	more	more	ADV
eurjchem-681	211	12	sensitive	sensitive	ADJ
eurjchem-681	211	13	than	than	ADP
eurjchem-681	211	14	the	the	DET
eurjchem-681	211	15	published	publish	VERB
eurjchem-681	211	16	hplc	hplc	NOUN
eurjchem-681	211	17	method	method	NOUN
eurjchem-681	211	18	[	[	X
eurjchem-681	211	19	30	30	NUM
eurjchem-681	211	20	]	]	PUNCT
eurjchem-681	211	21	especially	especially	ADV
eurjchem-681	211	22	for	for	ADP
eurjchem-681	211	23	sim	sim	NOUN
eurjchem-681	211	24	which	which	PRON
eurjchem-681	211	25	is	be	AUX
eurjchem-681	211	26	the	the	DET
eurjchem-681	211	27	lower	low	ADJ
eurjchem-681	211	28	concentration	concentration	NOUN
eurjchem-681	211	29	(	(	PUNCT
eurjchem-681	211	30	linearity	linearity	NOUN
eurjchem-681	211	31	rang	ring	VERB
eurjchem-681	211	32	2‐18	2‐18	NUM
eurjchem-681	211	33	µg	µg	NOUN
eurjchem-681	211	34	/	/	SYM
eurjchem-681	211	35	ml	ml	ADP
eurjchem-681	211	36	;	;	PUNCT
eurjchem-681	211	37	while	while	SCONJ
eurjchem-681	211	38	the	the	DET
eurjchem-681	211	39	reported	report	VERB
eurjchem-681	211	40	method	method	NOUN
eurjchem-681	211	41	is	be	AUX
eurjchem-681	211	42	20‐200	20‐200	NUM
eurjchem-681	211	43	µg	µg	NOUN
eurjchem-681	211	44	/	/	SYM
eurjchem-681	211	45	ml	ml	NOUN
eurjchem-681	211	46	)	)	PUNCT
eurjchem-681	211	47	.	.	PUNCT
eurjchem-681	212	1	4	4	X
eurjchem-681	212	2	.	.	X
eurjchem-681	212	3	conclusion	conclusion	NOUN
eurjchem-681	212	4	the	the	DET
eurjchem-681	212	5	proposed	propose	VERB
eurjchem-681	212	6	methods	method	NOUN
eurjchem-681	212	7	are	be	AUX
eurjchem-681	212	8	simple	simple	ADJ
eurjchem-681	212	9	and	and	CCONJ
eurjchem-681	212	10	do	do	AUX
eurjchem-681	212	11	not	not	PART
eurjchem-681	212	12	require	require	VERB
eurjchem-681	212	13	sophisticated	sophisticated	ADJ
eurjchem-681	212	14	technique	technique	NOUN
eurjchem-681	212	15	or	or	CCONJ
eurjchem-681	212	16	instrument	instrument	NOUN
eurjchem-681	212	17	.	.	PUNCT
eurjchem-681	213	1	the	the	DET
eurjchem-681	213	2	methods	method	NOUN
eurjchem-681	213	3	also	also	ADV
eurjchem-681	213	4	,	,	PUNCT
eurjchem-681	213	5	offer	offer	VERB
eurjchem-681	213	6	a	a	DET
eurjchem-681	213	7	practical	practical	ADJ
eurjchem-681	213	8	potential	potential	NOUN
eurjchem-681	213	9	for	for	ADP
eurjchem-681	213	10	the	the	DET
eurjchem-681	213	11	simultaneous	simultaneous	ADJ
eurjchem-681	213	12	determination	determination	NOUN
eurjchem-681	213	13	of	of	ADP
eurjchem-681	213	14	the	the	DET
eurjchem-681	213	15	cited	cite	VERB
eurjchem-681	213	16	drugs	drug	NOUN
eurjchem-681	213	17	,	,	PUNCT
eurjchem-681	213	18	without	without	ADP
eurjchem-681	213	19	prior	prior	ADJ
eurjchem-681	213	20	separation	separation	NOUN
eurjchem-681	213	21	,	,	PUNCT
eurjchem-681	213	22	especially	especially	ADV
eurjchem-681	213	23	with	with	ADP
eurjchem-681	213	24	its	its	PRON
eurjchem-681	213	25	advantages	advantage	NOUN
eurjchem-681	213	26	of	of	ADP
eurjchem-681	213	27	acceptable	acceptable	ADJ
eurjchem-681	213	28	sensitivity	sensitivity	NOUN
eurjchem-681	213	29	and	and	CCONJ
eurjchem-681	213	30	high	high	ADJ
eurjchem-681	213	31	selectivity	selectivity	NOUN
eurjchem-681	213	32	.	.	PUNCT
eurjchem-681	214	1	method	method	NOUN
eurjchem-681	214	2	validation	validation	NOUN
eurjchem-681	214	3	has	have	AUX
eurjchem-681	214	4	been	be	AUX
eurjchem-681	214	5	demonstrated	demonstrate	VERB
eurjchem-681	214	6	by	by	ADP
eurjchem-681	214	7	variety	variety	NOUN
eurjchem-681	214	8	of	of	ADP
eurjchem-681	214	9	tests	test	NOUN
eurjchem-681	214	10	for	for	ADP
eurjchem-681	214	11	linearity	linearity	NOUN
eurjchem-681	214	12	,	,	PUNCT
eurjchem-681	214	13	accuracy	accuracy	NOUN
eurjchem-681	214	14	,	,	PUNCT
eurjchem-681	214	15	precision	precision	NOUN
eurjchem-681	214	16	lod	lod	PROPN
eurjchem-681	214	17	and	and	CCONJ
eurjchem-681	214	18	loq	loq	PROPN
eurjchem-681	214	19	.	.	PUNCT
eurjchem-681	215	1	the	the	DET
eurjchem-681	215	2	developed	develop	VERB
eurjchem-681	215	3	methods	method	NOUN
eurjchem-681	215	4	have	have	VERB
eurjchem-681	215	5	several	several	ADJ
eurjchem-681	215	6	advantages	advantage	NOUN
eurjchem-681	215	7	,	,	PUNCT
eurjchem-681	215	8	as	as	SCONJ
eurjchem-681	215	9	it	it	PRON
eurjchem-681	215	10	is	be	AUX
eurjchem-681	215	11	robust	robust	ADJ
eurjchem-681	215	12	,	,	PUNCT
eurjchem-681	215	13	economical	economical	ADJ
eurjchem-681	215	14	and	and	CCONJ
eurjchem-681	215	15	much	much	ADV
eurjchem-681	215	16	more	more	ADV
eurjchem-681	215	17	sensitive	sensitive	ADJ
eurjchem-681	215	18	than	than	ADP
eurjchem-681	215	19	the	the	DET
eurjchem-681	215	20	recently	recently	ADV
eurjchem-681	215	21	published	publish	VERB
eurjchem-681	215	22	hplc	hplc	NOUN
eurjchem-681	215	23	;	;	PUNCT
eurjchem-681	215	24	in	in	ADP
eurjchem-681	215	25	addition	addition	NOUN
eurjchem-681	215	26	to	to	ADP
eurjchem-681	215	27	its	its	PRON
eurjchem-681	215	28	importance	importance	NOUN
eurjchem-681	215	29	as	as	SCONJ
eurjchem-681	215	30	very	very	ADV
eurjchem-681	215	31	few	few	ADJ
eurjchem-681	215	32	methods	method	NOUN
eurjchem-681	215	33	were	be	AUX
eurjchem-681	215	34	reported	report	VERB
eurjchem-681	215	35	in	in	ADP
eurjchem-681	215	36	the	the	DET
eurjchem-681	215	37	last	last	ADJ
eurjchem-681	215	38	few	few	ADJ
eurjchem-681	215	39	months	month	NOUN
eurjchem-681	215	40	for	for	ADP
eurjchem-681	215	41	the	the	DET
eurjchem-681	215	42	first	first	ADJ
eurjchem-681	215	43	combination	combination	NOUN
eurjchem-681	215	44	drug	drug	NOUN
eurjchem-681	215	45	to	to	PART
eurjchem-681	215	46	treat	treat	VERB
eurjchem-681	215	47	type	type	NOUN
eurjchem-681	215	48	2	2	NUM
eurjchem-681	215	49	diabetes	diabetes	NOUN
eurjchem-681	215	50	and	and	CCONJ
eurjchem-681	215	51	high	high	ADJ
eurjchem-681	215	52	cholesterol	cholesterol	NOUN
eurjchem-681	215	53	in	in	ADP
eurjchem-681	215	54	one	one	NUM
eurjchem-681	215	55	tablet	tablet	NOUN
eurjchem-681	215	56	.	.	PUNCT
eurjchem-681	216	1	references	reference	NOUN
eurjchem-681	216	2	[	[	X
eurjchem-681	216	3	1	1	NUM
eurjchem-681	216	4	]	]	PUNCT
eurjchem-681	216	5	.	.	PUNCT
eurjchem-681	217	1	url	url	X
eurjchem-681	217	2	(	(	PUNCT
eurjchem-681	217	3	10.24.2012	10.24.2012	NOUN
eurjchem-681	217	4	):	):	PUNCT
eurjchem-681	217	5	http://en.wikipedia.org/wiki/sitagliptin.svs	http://en.wikipedia.org/wiki/sitagliptin.svs	PROPN
eurjchem-681	218	1	[	[	X
eurjchem-681	218	2	2	2	NUM
eurjchem-681	218	3	]	]	PUNCT
eurjchem-681	218	4	.	.	PUNCT
eurjchem-681	218	5	url	url	X
eurjchem-681	218	6	(	(	PUNCT
eurjchem-681	218	7	10.24.2012	10.24.2012	NOUN
eurjchem-681	218	8	):	):	PUNCT
eurjchem-681	218	9	http://www.drugbank.ca/drugs/db01261	http://www.drugbank.ca/drugs/db01261	NOUN
eurjchem-681	218	10	[	[	X
eurjchem-681	218	11	3	3	NUM
eurjchem-681	218	12	]	]	PUNCT
eurjchem-681	218	13	.	.	PUNCT
eurjchem-681	219	1	the	the	DET
eurjchem-681	219	2	united	united	PROPN
eurjchem-681	219	3	states	states	PROPN
eurjchem-681	219	4	pharmacopeia	pharmacopeia	PROPN
eurjchem-681	219	5	usp	usp	PROPN
eurjchem-681	219	6	28	28	NUM
eurjchem-681	219	7	,	,	PUNCT
eurjchem-681	219	8	national	national	ADJ
eurjchem-681	219	9	formulary	formulary	NOUN
eurjchem-681	219	10	,	,	PUNCT
eurjchem-681	219	11	press	press	NOUN
eurjchem-681	219	12	:	:	PUNCT
eurjchem-681	219	13	the	the	DET
eurjchem-681	219	14	united	united	PROPN
eurjchem-681	219	15	states	states	PROPN
eurjchem-681	219	16	pharmacopeial	pharmacopeial	ADJ
eurjchem-681	219	17	convention	convention	PROPN
eurjchem-681	219	18	,	,	PUNCT
eurjchem-681	219	19	inc	inc	PROPN
eurjchem-681	219	20	.	.	PROPN
eurjchem-681	219	21	,	,	PUNCT
eurjchem-681	219	22	rockville	rockville	PROPN
eurjchem-681	219	23	,	,	PUNCT
eurjchem-681	219	24	pp	pp	ADJ
eurjchem-681	219	25	.	.	PUNCT
eurjchem-681	220	1	1770‐1772	1770‐1772	NUM
eurjchem-681	220	2	,	,	PUNCT
eurjchem-681	220	3	2006	2006	NUM
eurjchem-681	220	4	.	.	PUNCT
eurjchem-681	221	1	[	[	X
eurjchem-681	221	2	4	4	NUM
eurjchem-681	221	3	]	]	PUNCT
eurjchem-681	221	4	.	.	PUNCT
eurjchem-681	221	5	url	url	X
eurjchem-681	221	6	(	(	PUNCT
eurjchem-681	221	7	10.24.2012	10.24.2012	NOUN
eurjchem-681	221	8	):	):	PUNCT
eurjchem-681	221	9	http://www.drugbank.ca/drugs/db00641	http://www.drugbank.ca/drugs/db00641	PROPN
eurjchem-681	222	1	[	[	X
eurjchem-681	222	2	5	5	NUM
eurjchem-681	222	3	]	]	PUNCT
eurjchem-681	222	4	.	.	PUNCT
eurjchem-681	223	1	url	url	X
eurjchem-681	223	2	(	(	PUNCT
eurjchem-681	223	3	10.24.2012	10.24.2012	NOUN
eurjchem-681	223	4	):	):	PUNCT
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eurjchem-681	224	1	[	[	X
eurjchem-681	224	2	6	6	NUM
eurjchem-681	224	3	]	]	PUNCT
eurjchem-681	224	4	.	.	PUNCT
eurjchem-681	225	1	bala	bala	PROPN
eurjchem-681	225	2	,	,	PUNCT
eurjchem-681	225	3	s.	s.	PROPN
eurjchem-681	225	4	c.	c.	PROPN
eurjchem-681	225	5	;	;	PUNCT
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eurjchem-681	225	7	,	,	PUNCT
eurjchem-681	225	8	r.	r.	PROPN
eurjchem-681	225	9	a.	a.	PROPN
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eurjchem-681	225	11	.	.	PROPN
eurjchem-681	225	12	quim	quim	PROPN
eurjchem-681	225	13	.	.	PUNCT
eurjchem-681	226	1	sao	sao	PROPN
eurjchem-681	226	2	paulo	paulo	PROPN
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eurjchem-681	226	4	,	,	PUNCT
eurjchem-681	226	5	35	35	NUM
eurjchem-681	226	6	,	,	PUNCT
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eurjchem-681	226	8	.	.	PUNCT
eurjchem-681	227	1	[	[	X
eurjchem-681	227	2	7	7	NUM
eurjchem-681	227	3	]	]	PUNCT
eurjchem-681	227	4	.	.	PUNCT
eurjchem-681	228	1	el‐bagary	el‐bagary	PROPN
eurjchem-681	228	2	,	,	PUNCT
eurjchem-681	228	3	r.	r.	PROPN
eurjchem-681	228	4	i.	i.	PROPN
eurjchem-681	228	5	;	;	PUNCT
eurjchem-681	228	6	elkady	elkady	PROPN
eurjchem-681	228	7	,	,	PUNCT
eurjchem-681	228	8	e.	e.	PROPN
eurjchem-681	228	9	f.	f.	PROPN
eurjchem-681	228	10	;	;	PUNCT
eurjchem-681	228	11	ayoub	ayoub	PROPN
eurjchem-681	228	12	,	,	PUNCT
eurjchem-681	228	13	b.	b.	PROPN
eurjchem-681	228	14	m.	m.	PROPN
eurjchem-681	228	15	int	int	PROPN
eurjchem-681	228	16	.	.	PUNCT
eurjchem-681	229	1	j.	j.	PROPN
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eurjchem-681	229	3	.	.	PUNCT
eurjchem-681	230	1	sci	sci	PROPN
eurjchem-681	230	2	.	.	PROPN
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eurjchem-681	230	4	,	,	PUNCT
eurjchem-681	230	5	7	7	NUM
eurjchem-681	230	6	,	,	PUNCT
eurjchem-681	230	7	55‐61	55‐61	NUM
eurjchem-681	230	8	.	.	PUNCT
eurjchem-681	231	1	[	[	X
eurjchem-681	231	2	8	8	NUM
eurjchem-681	231	3	]	]	PUNCT
eurjchem-681	231	4	.	.	PUNCT
eurjchem-681	232	1	xiang‐fei	xiang‐fei	PROPN
eurjchem-681	232	2	,	,	PUNCT
eurjchem-681	232	3	j.	j.	PROPN
eurjchem-681	232	4	;	;	PUNCT
eurjchem-681	232	5	de‐wei	de‐wei	PROPN
eurjchem-681	232	6	,	,	PUNCT
eurjchem-681	232	7	s.	s.	PROPN
eurjchem-681	232	8	;	;	PUNCT
eurjchem-681	232	9	ye	ye	PROPN
eurjchem-681	232	10	,	,	PUNCT
eurjchem-681	232	11	c.	c.	PROPN
eurjchem-681	232	12	;	;	PUNCT
eurjchem-681	232	13	xin‐gang	xin‐gang	PROPN
eurjchem-681	232	14	,	,	PUNCT
eurjchem-681	232	15	l.	l.	PROPN
eurjchem-681	232	16	;	;	PUNCT
eurjchem-681	232	17	xiao‐meng	xiao‐meng	PROPN
eurjchem-681	232	18	,	,	PUNCT
eurjchem-681	232	19	w.	w.	PROPN
eurjchem-681	232	20	;	;	PUNCT
eurjchem-681	232	21	tian‐yan	tian‐yan	PROPN
eurjchem-681	232	22	,	,	PUNCT
eurjchem-681	232	23	z.	z.	PROPN
eurjchem-681	232	24	;	;	PUNCT
eurjchem-681	232	25	wei	wei	PROPN
eurjchem-681	232	26	,	,	PUNCT
eurjchem-681	232	27	l.	l.	PROPN
eurjchem-681	232	28	j.	j.	PROPN
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eurjchem-681	232	31	pharm	pharm	PROPN
eurjchem-681	232	32	.	.	PUNCT
eurjchem-681	233	1	sci	sci	PROPN
eurjchem-681	233	2	.	.	PROPN
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eurjchem-681	233	4	,	,	PUNCT
eurjchem-681	233	5	20	20	NUM
eurjchem-681	233	6	,	,	PUNCT
eurjchem-681	233	7	63‐69	63‐69	NUM
eurjchem-681	233	8	.	.	PUNCT
eurjchem-681	234	1	[	[	X
eurjchem-681	234	2	9	9	NUM
eurjchem-681	234	3	]	]	PUNCT
eurjchem-681	234	4	.	.	PUNCT
eurjchem-681	234	5	shyamala	shyamala	PROPN
eurjchem-681	234	6	,	,	PUNCT
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eurjchem-681	234	8	;	;	PUNCT
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eurjchem-681	234	10	,	,	PUNCT
eurjchem-681	234	11	s.	s.	PROPN
eurjchem-681	234	12	;	;	PUNCT
eurjchem-681	234	13	satyanarayana	satyanarayana	PROPN
eurjchem-681	234	14	,	,	PUNCT
eurjchem-681	234	15	t.	t.	PROPN
eurjchem-681	234	16	;	;	PUNCT
eurjchem-681	234	17	suresh	suresh	PROPN
eurjchem-681	234	18	,	,	PUNCT
eurjchem-681	234	19	k.	k.	PROPN
eurjchem-681	234	20	p.	p.	PROPN
eurjchem-681	234	21	n.	n.	PROPN
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eurjchem-681	234	23	;	;	PUNCT
eurjchem-681	234	24	swetha	swetha	PROPN
eurjchem-681	234	25	,	,	PUNCT
eurjchem-681	234	26	k.	k.	PROPN
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eurjchem-681	234	28	.	.	PUNCT
eurjchem-681	235	1	j.	j.	PROPN
eurjchem-681	235	2	pharm	pharm	PROPN
eurjchem-681	235	3	.	.	PUNCT
eurjchem-681	236	1	tech	tech	NOUN
eurjchem-681	236	2	.	.	PUNCT
eurjchem-681	237	1	res	re	NOUN
eurjchem-681	237	2	.	.	PROPN
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eurjchem-681	238	2	,	,	PUNCT
eurjchem-681	238	3	1	1	NUM
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eurjchem-681	238	6	.	.	PUNCT
eurjchem-681	239	1	[	[	X
eurjchem-681	239	2	10	10	NUM
eurjchem-681	239	3	]	]	PUNCT
eurjchem-681	239	4	.	.	PUNCT
eurjchem-681	240	1	el‐bagary	el‐bagary	PROPN
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eurjchem-681	240	3	r.	r.	PROPN
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eurjchem-681	240	5	;	;	PUNCT
eurjchem-681	240	6	elkady	elkady	PROPN
eurjchem-681	240	7	,	,	PUNCT
eurjchem-681	240	8	e.	e.	PROPN
eurjchem-681	240	9	f.	f.	PROPN
eurjchem-681	240	10	;	;	PUNCT
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eurjchem-681	240	12	,	,	PUNCT
eurjchem-681	240	13	b.	b.	PROPN
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eurjchem-681	240	17	,	,	PUNCT
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eurjchem-681	240	21	.	.	PUNCT
eurjchem-681	241	1	[	[	X
eurjchem-681	241	2	11	11	NUM
eurjchem-681	241	3	]	]	PUNCT
eurjchem-681	241	4	.	.	PUNCT
eurjchem-681	242	1	nirogi	nirogi	PROPN
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eurjchem-681	242	3	r.	r.	PROPN
eurjchem-681	242	4	;	;	PUNCT
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eurjchem-681	242	6	,	,	PUNCT
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eurjchem-681	242	8	;	;	PUNCT
eurjchem-681	242	9	mudigonda	mudigonda	NOUN
eurjchem-681	242	10	,	,	PUNCT
eurjchem-681	242	11	k.	k.	PROPN
eurjchem-681	242	12	;	;	PUNCT
eurjchem-681	242	13	komarneni	komarneni	PROPN
eurjchem-681	242	14	,	,	PUNCT
eurjchem-681	242	15	p.	p.	NOUN
eurjchem-681	242	16	;	;	PUNCT
eurjchem-681	242	17	aleti	aleti	PROPN
eurjchem-681	242	18	,	,	PUNCT
eurjchem-681	242	19	r.	r.	PROPN
eurjchem-681	242	20	;	;	PUNCT
eurjchem-681	242	21	boggavarapu	boggavarapu	PROPN
eurjchem-681	242	22	,	,	PUNCT
eurjchem-681	242	23	r.	r.	PROPN
eurjchem-681	242	24	biomed	biome	VERB
eurjchem-681	242	25	.	.	PUNCT
eurjchem-681	243	1	chromatogr	chromatogr	PROPN
eurjchem-681	243	2	.	.	PUNCT
eurjchem-681	244	1	2008	2008	NUM
eurjchem-681	244	2	,	,	PUNCT
eurjchem-681	244	3	22	22	NUM
eurjchem-681	244	4	,	,	PUNCT
eurjchem-681	244	5	214‐222	214‐222	NUM
eurjchem-681	244	6	.	.	PUNCT
eurjchem-681	245	1	[	[	X
eurjchem-681	245	2	12	12	NUM
eurjchem-681	245	3	]	]	PUNCT
eurjchem-681	245	4	.	.	PUNCT
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eurjchem-681	246	2	,	,	PUNCT
eurjchem-681	246	3	w.	w.	PROPN
eurjchem-681	246	4	;	;	PUNCT
eurjchem-681	246	5	musson	musson	PROPN
eurjchem-681	246	6	,	,	PUNCT
eurjchem-681	246	7	d.	d.	PROPN
eurjchem-681	246	8	g.	g.	PROPN
eurjchem-681	246	9	;	;	PUNCT
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eurjchem-681	246	11	,	,	PUNCT
eurjchem-681	246	12	a.	a.	PROPN
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eurjchem-681	246	14	;	;	PUNCT
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eurjchem-681	246	16	,	,	PUNCT
eurjchem-681	246	17	l.	l.	PROPN
eurjchem-681	246	18	;	;	PUNCT
eurjchem-681	246	19	schwartz	schwartz	PROPN
eurjchem-681	246	20	,	,	PUNCT
eurjchem-681	246	21	m.	m.	PROPN
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eurjchem-681	246	23	;	;	PUNCT
eurjchem-681	246	24	woolf	woolf	PROPN
eurjchem-681	246	25	,	,	PUNCT
eurjchem-681	246	26	e.	e.	PROPN
eurjchem-681	246	27	j.	j.	PROPN
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eurjchem-681	246	29	wang	wang	PROPN
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eurjchem-681	246	31	a.	a.	PROPN
eurjchem-681	246	32	q.	q.	PROPN
eurjchem-681	246	33	j.	j.	PROPN
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eurjchem-681	246	35	.	.	PUNCT
eurjchem-681	246	36	biomed	biome	VERB
eurjchem-681	246	37	.	.	PUNCT
eurjchem-681	247	1	anal	anal	PROPN
eurjchem-681	247	2	.	.	PUNCT
eurjchem-681	248	1	2008	2008	NUM
eurjchem-681	248	2	,	,	PUNCT
eurjchem-681	248	3	46	46	NUM
eurjchem-681	248	4	,	,	PUNCT
eurjchem-681	248	5	534‐542	534‐542	NUM
eurjchem-681	248	6	.	.	PUNCT
eurjchem-681	249	1	[	[	X
eurjchem-681	249	2	13	13	NUM
eurjchem-681	249	3	]	]	PUNCT
eurjchem-681	249	4	.	.	PUNCT
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eurjchem-681	250	2	,	,	PUNCT
eurjchem-681	250	3	r.	r.	PROPN
eurjchem-681	250	4	i.	i.	PROPN
eurjchem-681	250	5	;	;	PUNCT
eurjchem-681	250	6	elkady	elkady	PROPN
eurjchem-681	250	7	,	,	PUNCT
eurjchem-681	250	8	e.	e.	PROPN
eurjchem-681	250	9	f.	f.	PROPN
eurjchem-681	250	10	;	;	PUNCT
eurjchem-681	250	11	ayoub	ayoub	PROPN
eurjchem-681	250	12	,	,	PUNCT
eurjchem-681	250	13	b.	b.	PROPN
eurjchem-681	250	14	m.	m.	PROPN
eurjchem-681	250	15	talanta	talanta	PROPN
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eurjchem-681	250	17	,	,	PUNCT
eurjchem-681	250	18	85	85	NUM
eurjchem-681	250	19	,	,	PUNCT
eurjchem-681	250	20	673‐680	673‐680	NUM
eurjchem-681	250	21	.	.	PUNCT
eurjchem-681	251	1	[	[	X
eurjchem-681	251	2	14	14	NUM
eurjchem-681	251	3	]	]	PUNCT
eurjchem-681	251	4	.	.	PUNCT
eurjchem-681	252	1	el‐bagary	el‐bagary	PROPN
eurjchem-681	252	2	,	,	PUNCT
eurjchem-681	252	3	r.	r.	PROPN
eurjchem-681	252	4	i.	i.	PROPN
eurjchem-681	252	5	;	;	PUNCT
eurjchem-681	252	6	elkady	elkady	PROPN
eurjchem-681	252	7	,	,	PUNCT
eurjchem-681	252	8	e.	e.	PROPN
eurjchem-681	252	9	f.	f.	PROPN
eurjchem-681	252	10	;	;	PUNCT
eurjchem-681	252	11	ayoub	ayoub	PROPN
eurjchem-681	252	12	,	,	PUNCT
eurjchem-681	252	13	b.	b.	PROPN
eurjchem-681	252	14	m.	m.	PROPN
eurjchem-681	252	15	inter	inter	PROPN
eurjchem-681	252	16	.	.	PUNCT
eurjchem-681	253	1	j.	j.	PROPN
eurjchem-681	253	2	biomed	biome	VERB
eurjchem-681	253	3	.	.	PUNCT
eurjchem-681	254	1	sci	sci	PROPN
eurjchem-681	254	2	.	.	PROPN
eurjchem-681	254	3	2011	2011	NUM
eurjchem-681	254	4	,	,	PUNCT
eurjchem-681	254	5	7	7	NUM
eurjchem-681	254	6	,	,	PUNCT
eurjchem-681	254	7	62‐69	62‐69	NUM
eurjchem-681	254	8	.	.	PUNCT
eurjchem-681	255	1	[	[	X
eurjchem-681	255	2	15	15	NUM
eurjchem-681	255	3	]	]	PUNCT
eurjchem-681	255	4	.	.	PUNCT
eurjchem-681	256	1	vineet	vineet	PROPN
eurjchem-681	256	2	,	,	PUNCT
eurjchem-681	256	3	s.	s.	PROPN
eurjchem-681	256	4	;	;	PUNCT
eurjchem-681	256	5	radhika	radhika	PROPN
eurjchem-681	256	6	,	,	PUNCT
eurjchem-681	256	7	b.	b.	PROPN
eurjchem-681	256	8	;	;	PUNCT
eurjchem-681	256	9	rahul	rahul	PROPN
eurjchem-681	256	10	,	,	PUNCT
eurjchem-681	256	11	b.	b.	PROPN
eurjchem-681	256	12	rasayan	rasayan	PROPN
eurjchem-681	256	13	,	,	PUNCT
eurjchem-681	256	14	j.	j.	PROPN
eurjchem-681	256	15	j.	j.	PROPN
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eurjchem-681	256	17	.	.	PUNCT
eurjchem-681	257	1	2010	2010	NUM
eurjchem-681	257	2	,	,	PUNCT
eurjchem-681	257	3	3	3	NUM
eurjchem-681	257	4	,	,	PUNCT
eurjchem-681	257	5	507‐513	507‐513	PROPN
eurjchem-681	257	6	.	.	PUNCT
eurjchem-681	258	1	[	[	X
eurjchem-681	258	2	16	16	NUM
eurjchem-681	258	3	]	]	PUNCT
eurjchem-681	258	4	.	.	PUNCT
eurjchem-681	258	5	lei	lei	PROPN
eurjchem-681	258	6	,	,	PUNCT
eurjchem-681	258	7	w.	w.	PROPN
eurjchem-681	258	8	;	;	PUNCT
eurjchem-681	258	9	mandana	mandana	PROPN
eurjchem-681	258	10	,	,	PUNCT
eurjchem-681	258	11	a.	a.	PROPN
eurjchem-681	258	12	j.	j.	PROPN
eurjchem-681	258	13	pharm	pharm	PROPN
eurjchem-681	258	14	.	.	PUNCT
eurjchem-681	258	15	biomed	biome	VERB
eurjchem-681	258	16	.	.	PUNCT
eurjchem-681	259	1	anal	anal	PROPN
eurjchem-681	259	2	.	.	PUNCT
eurjchem-681	260	1	1999	1999	NUM
eurjchem-681	260	2	,	,	PUNCT
eurjchem-681	260	3	21	21	NUM
eurjchem-681	260	4	,	,	PUNCT
eurjchem-681	260	5	1243‐1248	1243‐1248	NUM
eurjchem-681	260	6	.	.	PUNCT
eurjchem-681	261	1	[	[	X
eurjchem-681	261	2	17	17	NUM
eurjchem-681	261	3	]	]	PUNCT
eurjchem-681	261	4	.	.	PUNCT
eurjchem-681	261	5	arayne	arayne	PROPN
eurjchem-681	261	6	,	,	PUNCT
eurjchem-681	261	7	m.	m.	NOUN
eurjchem-681	261	8	s.	s.	PROPN
eurjchem-681	261	9	;	;	PUNCT
eurjchem-681	261	10	sultana	sultana	NOUN
eurjchem-681	261	11	,	,	PUNCT
eurjchem-681	261	12	n.	n.	NOUN
eurjchem-681	261	13	;	;	PUNCT
eurjchem-681	261	14	hussain	hussain	PROPN
eurjchem-681	261	15	,	,	PUNCT
eurjchem-681	261	16	f.	f.	PROPN
eurjchem-681	261	17	;	;	PUNCT
eurjchem-681	261	18	ali	ali	PROPN
eurjchem-681	261	19	,	,	PUNCT
eurjchem-681	261	20	s.	s.	PROPN
eurjchem-681	261	21	a.	a.	PROPN
eurjchem-681	261	22	j.	j.	PROPN
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eurjchem-681	261	24	.	.	PUNCT
eurjchem-681	262	1	chem	chem	PROPN
eurjchem-681	262	2	.	.	PUNCT
eurjchem-681	263	1	2007	2007	NUM
eurjchem-681	263	2	,	,	PUNCT
eurjchem-681	263	3	62	62	NUM
eurjchem-681	263	4	,	,	PUNCT
eurjchem-681	263	5	536‐541	536‐541	NUM
eurjchem-681	263	6	.	.	PUNCT
eurjchem-681	264	1	[	[	X
eurjchem-681	264	2	18	18	NUM
eurjchem-681	264	3	]	]	PUNCT
eurjchem-681	264	4	.	.	PUNCT
eurjchem-681	265	1	anantha	anantha	PROPN
eurjchem-681	265	2	,	,	PUNCT
eurjchem-681	265	3	k.	k.	PROPN
eurjchem-681	265	4	d.	d.	PROPN
eurjchem-681	265	5	;	;	PUNCT
eurjchem-681	265	6	sujan	sujan	NOUN
eurjchem-681	265	7	,	,	PUNCT
eurjchem-681	265	8	d.	d.	PROPN
eurjchem-681	265	9	p.	p.	PROPN
eurjchem-681	265	10	;	;	PUNCT
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eurjchem-681	265	12	,	,	PUNCT
eurjchem-681	265	13	v.	v.	ADV
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eurjchem-681	265	16	,	,	PUNCT
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eurjchem-681	265	18	v.	v.	PROPN
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eurjchem-681	265	20	e‐j	e‐j	PROPN
eurjchem-681	265	21	.	.	PROPN
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eurjchem-681	265	23	.	.	PUNCT
eurjchem-681	266	1	2009	2009	NUM
eurjchem-681	266	2	,	,	PUNCT
eurjchem-681	266	3	6	6	NUM
eurjchem-681	266	4	,	,	PUNCT
eurjchem-681	266	5	541‐544	541‐544	NUM
eurjchem-681	266	6	.	.	PUNCT
eurjchem-681	267	1	[	[	X
eurjchem-681	267	2	19	19	NUM
eurjchem-681	267	3	]	]	PUNCT
eurjchem-681	267	4	.	.	PUNCT
eurjchem-681	268	1	hefnawy	hefnawy	PROPN
eurjchem-681	268	2	,	,	PUNCT
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eurjchem-681	268	4	;	;	PUNCT
eurjchem-681	268	5	al‐omar	al‐omar	PROPN
eurjchem-681	268	6	,	,	PUNCT
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eurjchem-681	268	8	;	;	PUNCT
eurjchem-681	268	9	julkhuf	julkhuf	PROPN
eurjchem-681	268	10	,	,	PUNCT
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eurjchem-681	268	16	.	.	PUNCT
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eurjchem-681	269	2	.	.	PUNCT
eurjchem-681	270	1	2009	2009	NUM
eurjchem-681	270	2	,	,	PUNCT
eurjchem-681	270	3	50	50	NUM
eurjchem-681	270	4	,	,	PUNCT
eurjchem-681	270	5	527‐534	527‐534	NUM
eurjchem-681	270	6	.	.	PUNCT
eurjchem-681	271	1	[	[	X
eurjchem-681	271	2	20	20	NUM
eurjchem-681	271	3	]	]	PUNCT
eurjchem-681	271	4	.	.	PUNCT
eurjchem-681	271	5	ali	ali	PROPN
eurjchem-681	271	6	,	,	PUNCT
eurjchem-681	271	7	h.	h.	PROPN
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eurjchem-681	271	10	,	,	PUNCT
eurjchem-681	271	11	s.	s.	PROPN
eurjchem-681	271	12	j.	j.	PROPN
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eurjchem-681	271	14	.	.	PUNCT
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eurjchem-681	271	16	.	.	PUNCT
eurjchem-681	272	1	anal	anal	ADJ
eurjchem-681	272	2	.	.	PUNCT
eurjchem-681	273	1	2009	2009	NUM
eurjchem-681	273	2	,	,	PUNCT
eurjchem-681	273	3	49	49	NUM
eurjchem-681	273	4	,	,	PUNCT
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eurjchem-681	273	6	.	.	PUNCT
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eurjchem-681	274	10	3	3	NUM
eurjchem-681	274	11	(	(	PUNCT
eurjchem-681	274	12	4	4	NUM
eurjchem-681	274	13	)	)	PUNCT
eurjchem-681	274	14	(	(	PUNCT
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eurjchem-681	274	16	)	)	PUNCT
eurjchem-681	274	17	447‐454	447‐454	PROPN
eurjchem-681	275	1	[	[	X
eurjchem-681	275	2	21	21	NUM
eurjchem-681	275	3	]	]	PUNCT
eurjchem-681	275	4	.	.	PUNCT
eurjchem-681	276	1	nilesh	nilesh	PROPN
eurjchem-681	276	2	,	,	PUNCT
eurjchem-681	276	3	j.	j.	PROPN
eurjchem-681	276	4	;	;	PUNCT
eurjchem-681	276	5	ruchi	ruchi	PROPN
eurjchem-681	276	6	,	,	PUNCT
eurjchem-681	276	7	j.	j.	PROPN
eurjchem-681	276	8	;	;	PUNCT
eurjchem-681	276	9	hemant	hemant	PROPN
eurjchem-681	276	10	,	,	PUNCT
eurjchem-681	276	11	s.	s.	PROPN
eurjchem-681	276	12	;	;	PUNCT
eurjchem-681	276	13	deepak	deepak	PROPN
eurjchem-681	276	14	,	,	PUNCT
eurjchem-681	276	15	k.	k.	PROPN
eurjchem-681	276	16	j.	j.	PROPN
eurjchem-681	276	17	asian	asian	PROPN
eurjchem-681	276	18	j.	j.	PROPN
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eurjchem-681	276	20	.	.	PROPN
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eurjchem-681	276	22	.	.	PUNCT
eurjchem-681	277	1	2008	2008	NUM
eurjchem-681	277	2	,	,	PUNCT
eurjchem-681	277	3	1	1	NUM
eurjchem-681	277	4	,	,	PUNCT
eurjchem-681	277	5	29‐31	29‐31	NUM
eurjchem-681	277	6	.	.	PUNCT
eurjchem-681	278	1	[	[	X
eurjchem-681	278	2	22	22	NUM
eurjchem-681	278	3	]	]	PUNCT
eurjchem-681	278	4	.	.	PUNCT
eurjchem-681	279	1	nagaraju	nagaraju	ADJ
eurjchem-681	279	2	,	,	PUNCT
eurjchem-681	279	3	p.	p.	NOUN
eurjchem-681	279	4	;	;	PUNCT
eurjchem-681	279	5	vishnu	vishnu	PROPN
eurjchem-681	279	6	,	,	PUNCT
eurjchem-681	279	7	v.	v.	PROPN
eurjchem-681	280	1	z.	z.	PROPN
eurjchem-681	280	2	j.	j.	PROPN
eurjchem-681	280	3	glob	glob	PROPN
eurjchem-681	280	4	.	.	PUNCT
eurjchem-681	281	1	pharm	pharm	PROPN
eurjchem-681	281	2	.	.	PUNCT
eurjchem-681	282	1	technol	technol	PROPN
eurjchem-681	282	2	.	.	PROPN
eurjchem-681	283	1	2010	2010	NUM
eurjchem-681	283	2	,	,	PUNCT
eurjchem-681	283	3	2	2	NUM
eurjchem-681	283	4	,	,	PUNCT
eurjchem-681	283	5	113‐117	113‐117	NUM
eurjchem-681	283	6	.	.	PUNCT
eurjchem-681	284	1	[	[	X
eurjchem-681	284	2	23	23	NUM
eurjchem-681	284	3	]	]	PUNCT
eurjchem-681	284	4	.	.	PUNCT
eurjchem-681	285	1	naotaka	naotaka	PROPN
eurjchem-681	285	2	,	,	PUNCT
eurjchem-681	285	3	u.	u.	PROPN
eurjchem-681	285	4	;	;	PUNCT
eurjchem-681	285	5	kazuhide	kazuhide	ADJ
eurjchem-681	285	6	,	,	PUNCT
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eurjchem-681	285	8	;	;	PUNCT
eurjchem-681	285	9	shunsuke	shunsuke	PROPN
eurjchem-681	285	10	,	,	PUNCT
eurjchem-681	285	11	h.	h.	PROPN
eurjchem-681	285	12	j.	j.	PROPN
eurjchem-681	285	13	chromatogr	chromatogr	PROPN
eurjchem-681	285	14	.	.	PUNCT
eurjchem-681	286	1	b.	b.	PROPN
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eurjchem-681	286	3	,	,	PUNCT
eurjchem-681	286	4	694	694	NUM
eurjchem-681	286	5	,	,	PUNCT
eurjchem-681	286	6	211‐217	211‐217	NUM
eurjchem-681	286	7	.	.	PUNCT
eurjchem-681	287	1	[	[	X
eurjchem-681	287	2	24	24	NUM
eurjchem-681	287	3	]	]	PUNCT
eurjchem-681	287	4	.	.	PUNCT
eurjchem-681	288	1	carlucci	carlucci	PROPN
eurjchem-681	288	2	,	,	PUNCT
eurjchem-681	288	3	g.	g.	PROPN
eurjchem-681	288	4	;	;	PUNCT
eurjchem-681	288	5	mazzeo	mazzeo	NOUN
eurjchem-681	288	6	,	,	PUNCT
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eurjchem-681	288	8	;	;	PUNCT
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eurjchem-681	288	10	,	,	PUNCT
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eurjchem-681	288	14	,	,	PUNCT
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eurjchem-681	288	18	.	.	PUNCT
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eurjchem-681	288	20	.	.	PUNCT
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eurjchem-681	289	2	.	.	PUNCT
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eurjchem-681	289	4	,	,	PUNCT
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eurjchem-681	289	6	,	,	PUNCT
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eurjchem-681	289	8	.	.	PUNCT
eurjchem-681	290	1	[	[	X
eurjchem-681	290	2	25	25	NUM
eurjchem-681	290	3	]	]	PUNCT
eurjchem-681	290	4	.	.	PUNCT
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eurjchem-681	291	2	,	,	PUNCT
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eurjchem-681	291	7	,	,	PUNCT
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eurjchem-681	291	17	,	,	PUNCT
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eurjchem-681	291	30	,	,	PUNCT
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eurjchem-681	292	3	]	]	PUNCT
eurjchem-681	292	4	.	.	PUNCT
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eurjchem-681	293	2	,	,	PUNCT
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eurjchem-681	294	2	.	.	PUNCT
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eurjchem-681	295	2	,	,	PUNCT
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eurjchem-681	295	4	,	,	PUNCT
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eurjchem-681	295	6	.	.	PUNCT
eurjchem-681	296	1	[	[	X
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eurjchem-681	296	3	]	]	PUNCT
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eurjchem-681	297	2	,	,	PUNCT
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eurjchem-681	297	6	,	,	PUNCT
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eurjchem-681	297	8	;	;	PUNCT
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eurjchem-681	297	10	,	,	PUNCT
eurjchem-681	297	11	l.	l.	PROPN
eurjchem-681	297	12	;	;	PUNCT
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eurjchem-681	297	14	,	,	PUNCT
eurjchem-681	297	15	y.	y.	PROPN
eurjchem-681	297	16	;	;	PUNCT
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eurjchem-681	297	18	,	,	PUNCT
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eurjchem-681	297	20	;	;	PUNCT
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eurjchem-681	297	22	,	,	PUNCT
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eurjchem-681	297	27	,	,	PUNCT
eurjchem-681	297	28	26(3	26(3	NUM
eurjchem-681	297	29	)	)	PUNCT
eurjchem-681	297	30	,	,	PUNCT
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eurjchem-681	297	32	.	.	PUNCT
eurjchem-681	298	1	[	[	X
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eurjchem-681	298	3	]	]	PUNCT
eurjchem-681	298	4	.	.	PUNCT
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eurjchem-681	299	2	,	,	PUNCT
eurjchem-681	299	3	j.	j.	PROPN
eurjchem-681	299	4	;	;	PUNCT
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eurjchem-681	299	6	,	,	PUNCT
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eurjchem-681	299	33	,	,	PUNCT
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eurjchem-681	300	2	.	.	PUNCT
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eurjchem-681	301	3	,	,	PUNCT
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eurjchem-681	301	5	,	,	PUNCT
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eurjchem-681	302	3	]	]	PUNCT
eurjchem-681	302	4	.	.	PUNCT
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eurjchem-681	303	6	,	,	PUNCT
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eurjchem-681	304	1	j.	j.	PROPN
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eurjchem-681	304	3	.	.	PUNCT
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eurjchem-681	305	2	,	,	PUNCT
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eurjchem-681	306	1	[	[	X
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eurjchem-681	306	3	]	]	SYM
eurjchem-681	306	4	.	.	PUNCT
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eurjchem-681	308	2	.	.	PUNCT
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eurjchem-681	309	2	.	.	PUNCT
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eurjchem-681	310	2	.	.	PUNCT
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eurjchem-681	310	4	.	.	PROPN
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eurjchem-681	311	2	,	,	PUNCT
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eurjchem-681	311	4	,	,	PUNCT
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eurjchem-681	312	3	]	]	PUNCT
eurjchem-681	312	4	.	.	PUNCT
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eurjchem-681	313	2	,	,	PUNCT
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eurjchem-681	315	2	,	,	PUNCT
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eurjchem-681	315	4	,	,	PUNCT
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eurjchem-681	316	3	]	]	PUNCT
eurjchem-681	316	4	.	.	PUNCT
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eurjchem-681	316	8	;	;	PUNCT
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eurjchem-681	317	2	,	,	PUNCT
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eurjchem-681	317	4	;	;	PUNCT
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eurjchem-681	318	2	.	.	PUNCT
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eurjchem-681	319	2	,	,	PUNCT
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eurjchem-681	319	5	,	,	PUNCT
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eurjchem-681	320	3	]	]	PUNCT
eurjchem-681	320	4	.	.	PUNCT
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eurjchem-681	320	6	,	,	PUNCT
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eurjchem-681	321	2	.	.	PROPN
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eurjchem-681	321	4	,	,	PUNCT
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eurjchem-681	321	6	,	,	PUNCT
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eurjchem-681	321	8	.	.	PUNCT
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eurjchem-681	322	6	,	,	PUNCT
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eurjchem-681	322	10	.	.	PUNCT
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eurjchem-681	323	2	.	.	PROPN
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eurjchem-681	323	4	,	,	PUNCT
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eurjchem-681	323	6	,	,	PUNCT
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eurjchem-681	323	8	.	.	PUNCT
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eurjchem-681	325	2	.	.	PROPN
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eurjchem-681	325	4	,	,	PUNCT
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eurjchem-681	325	6	,	,	PUNCT
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eurjchem-681	326	3	]	]	PUNCT
eurjchem-681	326	4	.	.	PUNCT
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eurjchem-681	326	14	,	,	PUNCT
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eurjchem-681	326	17	.	.	PUNCT
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eurjchem-681	327	2	.	.	PUNCT
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eurjchem-681	328	2	.	.	PUNCT
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eurjchem-681	329	2	.	.	PUNCT
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eurjchem-681	330	2	,	,	PUNCT
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eurjchem-681	330	4	,	,	PUNCT
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eurjchem-681	330	6	.	.	PUNCT
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eurjchem-681	331	3	]	]	SYM
eurjchem-681	331	4	.	.	PUNCT
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eurjchem-681	331	6	,	,	PUNCT
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eurjchem-681	331	10	,	,	PUNCT
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eurjchem-681	331	14	,	,	PUNCT
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eurjchem-681	331	20	,	,	PUNCT
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eurjchem-681	331	22	,	,	PUNCT
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eurjchem-681	331	24	.	.	PUNCT
eurjchem-681	332	1	[	[	X
eurjchem-681	332	2	38	38	NUM
eurjchem-681	332	3	]	]	PUNCT
eurjchem-681	332	4	.	.	PUNCT
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eurjchem-681	333	2	(	(	PUNCT
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eurjchem-681	334	4	.	.	PUNCT
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eurjchem-681	335	2	,	,	PUNCT
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eurjchem-681	335	4	;	;	PUNCT
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eurjchem-681	335	6	,	,	PUNCT
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eurjchem-681	335	10	,	,	PUNCT
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eurjchem-681	335	15	,	,	PUNCT
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eurjchem-681	335	17	,	,	PUNCT
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eurjchem-681	335	19	.	.	PUNCT
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eurjchem-681	336	2	40	40	NUM
eurjchem-681	336	3	]	]	PUNCT
eurjchem-681	336	4	.	.	PUNCT
eurjchem-681	337	1	el‐bardicy	el‐bardicy	PROPN
eurjchem-681	337	2	,	,	PUNCT
eurjchem-681	337	3	m.	m.	NOUN
eurjchem-681	337	4	g.	g.	PROPN
eurjchem-681	337	5	;	;	PUNCT
eurjchem-681	337	6	lotfy	lotfy	PROPN
eurjchem-681	337	7	,	,	PUNCT
eurjchem-681	337	8	h.	h.	PROPN
eurjchem-681	337	9	m.	m.	PROPN
eurjchem-681	337	10	;	;	PUNCT
eurjchem-681	337	11	el‐sayed	el‐saye	VERB
eurjchem-681	337	12	,	,	PUNCT
eurjchem-681	337	13	m.	m.	NOUN
eurjchem-681	337	14	a.	a.	PROPN
eurjchem-681	337	15	;	;	PUNCT
eurjchem-681	337	16	el‐tarras	el‐tarra	NOUN
eurjchem-681	337	17	,	,	PUNCT
eurjchem-681	337	18	m.	m.	PROPN
eurjchem-681	337	19	f.	f.	PROPN
eurjchem-681	337	20	j.	j.	PROPN
eurjchem-681	337	21	aoac	aoac	PROPN
eurjchem-681	337	22	int	int	PROPN
eurjchem-681	337	23	.	.	PUNCT
eurjchem-681	338	1	2008	2008	NUM
eurjchem-681	338	2	,	,	PUNCT
eurjchem-681	338	3	91	91	NUM
eurjchem-681	338	4	,	,	PUNCT
eurjchem-681	338	5	299‐310	299‐310	NUM
eurjchem-681	338	6	.	.	PUNCT
eurjchem-681	339	1	[	[	X
eurjchem-681	339	2	41	41	NUM
eurjchem-681	339	3	]	]	PUNCT
eurjchem-681	339	4	.	.	PUNCT
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eurjchem-681	340	2	conference	conference	NOUN
eurjchem-681	340	3	on	on	ADP
eurjchem-681	340	4	harmonization	harmonization	NOUN
eurjchem-681	340	5	(	(	PUNCT
eurjchem-681	340	6	ich	ich	NOUN
eurjchem-681	340	7	)	)	PUNCT
eurjchem-681	340	8	,	,	PUNCT
eurjchem-681	340	9	q2b	q2b	PROPN
eurjchem-681	340	10	:	:	PUNCT
eurjchem-681	340	11	validation	validation	NOUN
eurjchem-681	340	12	of	of	ADP
eurjchem-681	340	13	analytical	analytical	ADJ
eurjchem-681	340	14	procedures	procedure	NOUN
eurjchem-681	340	15	:	:	PUNCT
eurjchem-681	340	16	methodology	methodology	NOUN
eurjchem-681	340	17	,	,	PUNCT
eurjchem-681	340	18	62	62	NUM
eurjchem-681	340	19	,	,	PUNCT
eurjchem-681	340	20	us	us	PROPN
eurjchem-681	340	21	fda	fda	PROPN
eurjchem-681	340	22	federal	federal	PROPN
eurjchem-681	340	23	register	register	PROPN
eurjchem-681	340	24	,	,	PUNCT
eurjchem-681	340	25	1997	1997	NUM
eurjchem-681	340	26	.	.	PUNCT