id sid tid token lemma pos eurjchem-71 1 1 microsoft microsoft PROPN eurjchem-71 1 2 word word NOUN eurjchem-71 1 3 european_journal_of_chemistry_1_2_2010_134_139_71 european_journal_of_chemistry_1_2_2010_134_139_71 PROPN eurjchem-71 1 4 european european PROPN eurjchem-71 1 5     SPACE eurjchem-71 1 6 journal journal NOUN eurjchem-71 1 7     SPACE eurjchem-71 1 8 of of ADP eurjchem-71 1 9     SPACE eurjchem-71 1 10 chemistry chemistry NOUN eurjchem-71 1 11     SPACE eurjchem-71 1 12 1 1 NUM eurjchem-71 1 13     SPACE eurjchem-71 1 14 ( ( PUNCT eurjchem-71 1 15 2 2 NUM eurjchem-71 1 16 ) ) PUNCT eurjchem-71 1 17     SPACE eurjchem-71 1 18 ( ( PUNCT eurjchem-71 1 19 2010 2010 NUM eurjchem-71 1 20 ) ) PUNCT eurjchem-71 1 21     SPACE eurjchem-71 1 22 134‐139 134‐139 NUM eurjchem-71 1 23         SPACE eurjchem-71 1 24 european european ADJ eurjchem-71 1 25     SPACE eurjchem-71 1 26 journal journal NOUN eurjchem-71 1 27     SPACE eurjchem-71 1 28 of of ADP eurjchem-71 1 29     SPACE eurjchem-71 1 30 chemistry chemistry NOUN eurjchem-71 1 31     SPACE eurjchem-71 1 32 issn issn VERB eurjchem-71 1 33     SPACE eurjchem-71 1 34 2153‐2249 2153‐2249 NUM eurjchem-71 1 35     SPACE eurjchem-71 1 36 ( ( PUNCT eurjchem-71 1 37 print print NOUN eurjchem-71 1 38 ) ) PUNCT eurjchem-71 1 39     SPACE eurjchem-71 1 40 / / SYM eurjchem-71 1 41     SPACE eurjchem-71 1 42 issn issn VERB eurjchem-71 1 43     SPACE eurjchem-71 1 44 2153‐2257 2153‐2257 NUM eurjchem-71 1 45     SPACE eurjchem-71 1 46 ( ( PUNCT eurjchem-71 1 47 online online ADJ eurjchem-71 1 48 ) ) PUNCT eurjchem-71 1 49     SPACE eurjchem-71 1 50   NOUN eurjchem-71 1 51     SPACE eurjchem-71 1 52 2010 2010 NUM eurjchem-71 1 53     SPACE eurjchem-71 1 54 eurjchem eurjchem NOUN eurjchem-71 1 55     SPACE eurjchem-71 1 56 doi:10.5155 doi:10.5155 NOUN eurjchem-71 1 57 / / SYM eurjchem-71 1 58 eurjchem.1.2.134‐139.71 eurjchem.1.2.134‐139.71 NOUN eurjchem-71 1 59                 SPACE eurjchem-71 1 60 european european ADJ eurjchem-71 1 61     SPACE eurjchem-71 1 62 journal journal NOUN eurjchem-71 1 63     SPACE eurjchem-71 1 64 of of ADP eurjchem-71 1 65     SPACE eurjchem-71 1 66 chemistry chemistry NOUN eurjchem-71 1 67     SPACE eurjchem-71 1 68 journal journal NOUN eurjchem-71 1 69     SPACE eurjchem-71 1 70 homepage homepage NOUN eurjchem-71 1 71 : : PUNCT eurjchem-71 1 72     SPACE eurjchem-71 1 73 www.eurjchem.com www.eurjchem.com NOUN eurjchem-71 1 74                     SPACE eurjchem-71 1 75 novel novel NOUN eurjchem-71 1 76     SPACE eurjchem-71 1 77 isoquinoline isoquinoline ADJ eurjchem-71 1 78     SPACE eurjchem-71 1 79 derivatives derivative NOUN eurjchem-71 1 80     SPACE eurjchem-71 1 81 from from ADP eurjchem-71 1 82     SPACE eurjchem-71 1 83 isochromen‐1,3‐dione isochromen‐1,3‐dione NUM eurjchem-71 1 84     SPACE eurjchem-71 1 85 mahmoud mahmoud PROPN eurjchem-71 1 86     SPACE eurjchem-71 1 87 refaee refaee PROPN eurjchem-71 1 88     SPACE eurjchem-71 1 89 mahmoud mahmoud PROPN eurjchem-71 1 90 , , PUNCT eurjchem-71 1 91     SPACE eurjchem-71 1 92 manal manal PROPN eurjchem-71 1 93     SPACE eurjchem-71 1 94 mohamed mohamed PROPN eurjchem-71 1 95     SPACE eurjchem-71 1 96 el‐shahawi el‐shahawi PROPN eurjchem-71 1 97 , , PUNCT eurjchem-71 1 98       SPACE eurjchem-71 1 99 eman eman NOUN eurjchem-71 1 100     SPACE eurjchem-71 1 101 abd abd PROPN eurjchem-71 1 102     SPACE eurjchem-71 1 103 el‐fattah el‐fattah PROPN eurjchem-71 1 104     SPACE eurjchem-71 1 105 el‐bordany el‐bordany PROPN eurjchem-71 1 106     SPACE eurjchem-71 1 107 and and CCONJ eurjchem-71 1 108     SPACE eurjchem-71 1 109 fatma fatma PROPN eurjchem-71 1 110     SPACE eurjchem-71 1 111 saber saber PROPN eurjchem-71 1 112     SPACE eurjchem-71 1 113 mohamed mohamed PROPN eurjchem-71 1 114     SPACE eurjchem-71 1 115 abu abu PROPN eurjchem-71 1 116     SPACE eurjchem-71 1 117 el‐azm el‐azm PROPN eurjchem-71 1 118 * * PUNCT eurjchem-71 1 119     SPACE eurjchem-71 1 120 chemistry chemistry NOUN eurjchem-71 1 121     SPACE eurjchem-71 1 122 department department NOUN eurjchem-71 1 123 , , PUNCT eurjchem-71 1 124     SPACE eurjchem-71 1 125 faculty faculty NOUN eurjchem-71 1 126     SPACE eurjchem-71 1 127 of of ADP eurjchem-71 1 128     SPACE eurjchem-71 1 129 science science NOUN eurjchem-71 1 130 , , PUNCT eurjchem-71 1 131     SPACE eurjchem-71 1 132 ain ain PROPN eurjchem-71 1 133     SPACE eurjchem-71 1 134 shams sham NOUN eurjchem-71 1 135     SPACE eurjchem-71 1 136 university university NOUN eurjchem-71 1 137 , , PUNCT eurjchem-71 1 138     SPACE eurjchem-71 1 139 abbassia abbassia NOUN eurjchem-71 1 140     SPACE eurjchem-71 1 141 11566 11566 NUM eurjchem-71 1 142 , , PUNCT eurjchem-71 1 143     SPACE eurjchem-71 1 144 cairo cairo PROPN eurjchem-71 1 145 , , PUNCT eurjchem-71 1 146     SPACE eurjchem-71 1 147 egypt egypt PROPN eurjchem-71 1 148     SPACE eurjchem-71 1 149 * * PROPN eurjchem-71 1 150 corresponding corresponding ADJ eurjchem-71 1 151     SPACE eurjchem-71 1 152 author author NOUN eurjchem-71 1 153     SPACE eurjchem-71 1 154 at at ADP eurjchem-71 1 155 : : PUNCT eurjchem-71 1 156     SPACE eurjchem-71 1 157 chemistry chemistry NOUN eurjchem-71 1 158     SPACE eurjchem-71 1 159 department department NOUN eurjchem-71 1 160 , , PUNCT eurjchem-71 1 161     SPACE eurjchem-71 1 162 faculty faculty NOUN eurjchem-71 1 163     SPACE eurjchem-71 1 164 of of ADP eurjchem-71 1 165     SPACE eurjchem-71 1 166 science science NOUN eurjchem-71 1 167 , , PUNCT eurjchem-71 1 168     SPACE eurjchem-71 1 169 ain ain PROPN eurjchem-71 1 170     SPACE eurjchem-71 1 171 shams sham NOUN eurjchem-71 1 172     SPACE eurjchem-71 1 173 university university NOUN eurjchem-71 1 174 , , PUNCT eurjchem-71 1 175     SPACE eurjchem-71 1 176 abbassia abbassia NOUN eurjchem-71 1 177     SPACE eurjchem-71 1 178 11566 11566 NUM eurjchem-71 1 179 , , PUNCT eurjchem-71 1 180     SPACE eurjchem-71 1 181 cairo cairo PROPN eurjchem-71 1 182 , , PUNCT eurjchem-71 1 183     SPACE eurjchem-71 1 184 egypt egypt PROPN eurjchem-71 1 185 . . PUNCT eurjchem-71 1 186     SPACE eurjchem-71 2 1 tel tel PROPN eurjchem-71 2 2 . . PUNCT eurjchem-71 2 3 : : PUNCT eurjchem-71 2 4     SPACE eurjchem-71 3 1 +2.202.4821096 +2.202.4821096 ADJ eurjchem-71 3 2 ; ; PUNCT eurjchem-71 3 3     SPACE eurjchem-71 3 4 fax fax NOUN eurjchem-71 3 5 : : PUNCT eurjchem-71 3 6     SPACE eurjchem-71 3 7 +2.202.831836 +2.202.831836 PROPN eurjchem-71 3 8 . . PUNCT eurjchem-71 3 9     SPACE eurjchem-71 3 10 e­mail e­mail NOUN eurjchem-71 3 11     SPACE eurjchem-71 3 12 address address NOUN eurjchem-71 3 13 : : PUNCT eurjchem-71 3 14     SPACE eurjchem-71 3 15 ftmsaber@yahoo.com ftmsaber@yahoo.com X eurjchem-71 3 16       SPACE eurjchem-71 3 17 ( ( PUNCT eurjchem-71 3 18 f. f. PROPN eurjchem-71 3 19     SPACE eurjchem-71 3 20 saber saber NOUN eurjchem-71 3 21 ) ) PUNCT eurjchem-71 3 22 . . PUNCT eurjchem-71 3 23                                 SPACE eurjchem-71 4 1 article article NOUN eurjchem-71 4 2     SPACE eurjchem-71 4 3 information information NOUN eurjchem-71 4 4         SPACE eurjchem-71 4 5 abstract abstract ADJ eurjchem-71 4 6 received receive VERB eurjchem-71 4 7 : : PUNCT eurjchem-71 4 8     SPACE eurjchem-71 4 9 21 21 NUM eurjchem-71 4 10     SPACE eurjchem-71 4 11 april april PROPN eurjchem-71 4 12     SPACE eurjchem-71 4 13 2010 2010 NUM eurjchem-71 4 14     SPACE eurjchem-71 4 15 received receive VERB eurjchem-71 4 16     SPACE eurjchem-71 4 17 in in ADP eurjchem-71 4 18     SPACE eurjchem-71 4 19 revised revise VERB eurjchem-71 4 20     SPACE eurjchem-71 4 21 form form NOUN eurjchem-71 4 22 : : PUNCT eurjchem-71 4 23     SPACE eurjchem-71 4 24 12 12 NUM eurjchem-71 4 25     SPACE eurjchem-71 4 26 may may AUX eurjchem-71 4 27     SPACE eurjchem-71 4 28 2010 2010 NUM eurjchem-71 4 29     SPACE eurjchem-71 4 30 accepted accept VERB eurjchem-71 4 31 : : PUNCT eurjchem-71 4 32     SPACE eurjchem-71 4 33 12 12 NUM eurjchem-71 4 34     SPACE eurjchem-71 4 35 may may AUX eurjchem-71 4 36     SPACE eurjchem-71 4 37 2010 2010 NUM eurjchem-71 4 38     SPACE eurjchem-71 4 39 online online NOUN eurjchem-71 4 40 : : PUNCT eurjchem-71 4 41     SPACE eurjchem-71 4 42 30 30 NUM eurjchem-71 4 43     SPACE eurjchem-71 4 44 june june PROPN eurjchem-71 4 45     SPACE eurjchem-71 4 46 2010 2010 NUM eurjchem-71 4 47     SPACE eurjchem-71 4 48 keywords keyword VERB eurjchem-71 4 49         SPACE eurjchem-71 4 50 a a DET eurjchem-71 4 51     SPACE eurjchem-71 4 52 number number NOUN eurjchem-71 4 53     SPACE eurjchem-71 4 54 of of ADP eurjchem-71 4 55     SPACE eurjchem-71 4 56 novel novel NOUN eurjchem-71 4 57     SPACE eurjchem-71 4 58 isoquinoline isoquinoline ADJ eurjchem-71 4 59     SPACE eurjchem-71 4 60 derivatives derivative NOUN eurjchem-71 4 61     SPACE eurjchem-71 4 62 have have AUX eurjchem-71 4 63     SPACE eurjchem-71 4 64 been be AUX eurjchem-71 4 65     SPACE eurjchem-71 4 66 synthesized synthesize VERB eurjchem-71 4 67     SPACE eurjchem-71 4 68 using use VERB eurjchem-71 4 69     SPACE eurjchem-71 4 70 the the DET eurjchem-71 4 71     SPACE eurjchem-71 4 72 readily readily ADV eurjchem-71 4 73 obtainable obtainable ADJ eurjchem-71 4 74     SPACE eurjchem-71 4 75 ( ( PUNCT eurjchem-71 4 76 e)‐4‐(3,4‐dimethoxybenzylidene)‐4h‐isochromene‐1,3‐dione e)‐4‐(3,4‐dimethoxybenzylidene)‐4h‐isochromene‐1,3‐dione NOUN eurjchem-71 4 77 , , PUNCT eurjchem-71 4 78     SPACE eurjchem-71 4 79 2 2 NUM eurjchem-71 4 80 , , PUNCT eurjchem-71 4 81     SPACE eurjchem-71 4 82 via via ADP eurjchem-71 4 83     SPACE eurjchem-71 4 84 the the DET eurjchem-71 4 85     SPACE eurjchem-71 4 86 reaction reaction NOUN eurjchem-71 4 87 with with ADP eurjchem-71 4 88     SPACE eurjchem-71 4 89 different different ADJ eurjchem-71 4 90     SPACE eurjchem-71 4 91 nitrogen nitrogen NOUN eurjchem-71 4 92     SPACE eurjchem-71 4 93 nucleophiles nucleophile NOUN eurjchem-71 4 94     SPACE eurjchem-71 4 95 such such ADJ eurjchem-71 4 96     SPACE eurjchem-71 4 97 as as ADP eurjchem-71 4 98     SPACE eurjchem-71 4 99 cyanoethanoic cyanoethanoic ADJ eurjchem-71 4 100     SPACE eurjchem-71 4 101 hydrazide hydrazide ADJ eurjchem-71 4 102 , , PUNCT eurjchem-71 4 103     SPACE eurjchem-71 4 104 cyclohexylamine cyclohexylamine NOUN eurjchem-71 4 105 , , PUNCT eurjchem-71 4 106 2‐aminothiophenol 2‐aminothiophenol NOUN eurjchem-71 4 107     SPACE eurjchem-71 4 108 and and CCONJ eurjchem-71 4 109     SPACE eurjchem-71 4 110 p‐toluenesulfonohydrazide p‐toluenesulfonohydrazide NOUN eurjchem-71 4 111 . . PUNCT eurjchem-71 4 112     SPACE eurjchem-71 5 1 furthermore furthermore ADV eurjchem-71 5 2 , , PUNCT eurjchem-71 5 3     SPACE eurjchem-71 5 4 the the DET eurjchem-71 5 5     SPACE eurjchem-71 5 6 reactivity reactivity NOUN eurjchem-71 5 7     SPACE eurjchem-71 5 8 of of ADP eurjchem-71 5 9     SPACE eurjchem-71 5 10 2 2 NUM eurjchem-71 5 11     SPACE eurjchem-71 5 12 towards towards ADP eurjchem-71 5 13 thiophenol thiophenol NOUN eurjchem-71 5 14 , , PUNCT eurjchem-71 5 15     SPACE eurjchem-71 5 16 and and CCONJ eurjchem-71 5 17     SPACE eurjchem-71 5 18 ethylcyanoacetate ethylcyanoacetate NOUN eurjchem-71 5 19     SPACE eurjchem-71 5 20 has have AUX eurjchem-71 5 21     SPACE eurjchem-71 5 22 been be AUX eurjchem-71 5 23     SPACE eurjchem-71 5 24 investigated investigate VERB eurjchem-71 5 25 . . PUNCT eurjchem-71 5 26     SPACE eurjchem-71 6 1 isochromene‐1,3‐dione isochromene‐1,3‐dione NOUN eurjchem-71 6 2     SPACE eurjchem-71 6 3 isoquinolines isoquinoline VERB eurjchem-71 6 4     SPACE eurjchem-71 6 5 2‐cyanoethanoic 2‐cyanoethanoic NUM eurjchem-71 6 6     SPACE eurjchem-71 6 7 hydrazide hydrazide ADJ eurjchem-71 6 8     SPACE eurjchem-71 6 9 nitrogen nitrogen NOUN eurjchem-71 6 10     SPACE eurjchem-71 6 11 nucleophiles nucleophile NOUN eurjchem-71 6 12         SPACE eurjchem-71 6 13 1 1 NUM eurjchem-71 6 14 . . PUNCT eurjchem-71 6 15     SPACE eurjchem-71 6 16 introduction introduction NOUN eurjchem-71 6 17         SPACE eurjchem-71 6 18 in in ADP eurjchem-71 6 19     SPACE eurjchem-71 6 20 recent recent ADJ eurjchem-71 6 21     SPACE eurjchem-71 6 22 years year NOUN eurjchem-71 6 23 , , PUNCT eurjchem-71 6 24     SPACE eurjchem-71 6 25 there there PRON eurjchem-71 6 26     SPACE eurjchem-71 6 27 has have AUX eurjchem-71 6 28     SPACE eurjchem-71 6 29 been be AUX eurjchem-71 6 30     SPACE eurjchem-71 6 31 increasing increase VERB eurjchem-71 6 32     SPACE eurjchem-71 6 33 interest interest NOUN eurjchem-71 6 34     SPACE eurjchem-71 6 35 in in ADP eurjchem-71 6 36     SPACE eurjchem-71 6 37 the the DET eurjchem-71 6 38     SPACE eurjchem-71 6 39 synthesis synthesis NOUN eurjchem-71 6 40     SPACE eurjchem-71 6 41 of of ADP eurjchem-71 6 42     SPACE eurjchem-71 6 43 natural natural ADJ eurjchem-71 6 44     SPACE eurjchem-71 6 45 products product NOUN eurjchem-71 6 46 , , PUNCT eurjchem-71 6 47     SPACE eurjchem-71 6 48 since since ADV eurjchem-71 6 49 ; ; PUNCT eurjchem-71 6 50     SPACE eurjchem-71 6 51 they they PRON eurjchem-71 6 52     SPACE eurjchem-71 6 53 are be AUX eurjchem-71 6 54     SPACE eurjchem-71 6 55 an an DET eurjchem-71 6 56     SPACE eurjchem-71 6 57 excellent excellent NOUN eurjchem-71 6 58     SPACE eurjchem-71 6 59 and and CCONJ eurjchem-71 6 60     SPACE eurjchem-71 6 61 reliable reliable ADJ eurjchem-71 6 62     SPACE eurjchem-71 6 63 source source NOUN eurjchem-71 6 64     SPACE eurjchem-71 6 65 for for ADP eurjchem-71 6 66     SPACE eurjchem-71 6 67 the the DET eurjchem-71 6 68     SPACE eurjchem-71 6 69 development development NOUN eurjchem-71 6 70     SPACE eurjchem-71 6 71 of of ADP eurjchem-71 6 72     SPACE eurjchem-71 6 73 new new ADJ eurjchem-71 6 74     SPACE eurjchem-71 6 75 drugs drug NOUN eurjchem-71 6 76 . . PUNCT eurjchem-71 6 77     SPACE eurjchem-71 6 78 in in ADP eurjchem-71 6 79     SPACE eurjchem-71 6 80 this this DET eurjchem-71 6 81     SPACE eurjchem-71 6 82 context context NOUN eurjchem-71 6 83 , , PUNCT eurjchem-71 6 84     SPACE eurjchem-71 6 85 chromene chromene NOUN eurjchem-71 6 86     SPACE eurjchem-71 6 87 derivatives derivative NOUN eurjchem-71 6 88     SPACE eurjchem-71 6 89 are be AUX eurjchem-71 6 90     SPACE eurjchem-71 6 91 a a DET eurjchem-71 6 92     SPACE eurjchem-71 6 93 class class NOUN eurjchem-71 6 94     SPACE eurjchem-71 6 95 of of ADP eurjchem-71 6 96     SPACE eurjchem-71 6 97 natural natural ADJ eurjchem-71 6 98     SPACE eurjchem-71 6 99 products product NOUN eurjchem-71 6 100     SPACE eurjchem-71 6 101 that that PRON eurjchem-71 6 102     SPACE eurjchem-71 6 103 often often ADV eurjchem-71 6 104     SPACE eurjchem-71 6 105 occurs occur VERB eurjchem-71 6 106     SPACE eurjchem-71 6 107 as as ADP eurjchem-71 6 108     SPACE eurjchem-71 6 109 microbial microbial ADJ eurjchem-71 6 110     SPACE eurjchem-71 6 111 metabolites metabolite NOUN eurjchem-71 6 112     SPACE eurjchem-71 6 113 and and CCONJ eurjchem-71 6 114     SPACE eurjchem-71 6 115 that that PRON eurjchem-71 6 116     SPACE eurjchem-71 6 117 have have AUX eurjchem-71 6 118     SPACE eurjchem-71 6 119 been be AUX eurjchem-71 6 120     SPACE eurjchem-71 6 121 found find VERB eurjchem-71 6 122     SPACE eurjchem-71 6 123 to to PART eurjchem-71 6 124     SPACE eurjchem-71 6 125 exhibit exhibit VERB eurjchem-71 6 126     SPACE eurjchem-71 6 127 interesting interesting ADJ eurjchem-71 6 128     SPACE eurjchem-71 6 129 biological biological ADJ eurjchem-71 6 130     SPACE eurjchem-71 6 131 properties property NOUN eurjchem-71 6 132 , , PUNCT eurjchem-71 6 133     SPACE eurjchem-71 6 134 [ [ X eurjchem-71 6 135 1‐7 1‐7 NOUN eurjchem-71 6 136 ] ] PUNCT eurjchem-71 6 137     SPACE eurjchem-71 6 138 including include VERB eurjchem-71 6 139     SPACE eurjchem-71 6 140 antifungal antifungal ADJ eurjchem-71 6 141 , , PUNCT eurjchem-71 6 142     SPACE eurjchem-71 6 143 anti‐inflammatory anti‐inflammatory ADJ eurjchem-71 6 144 , , PUNCT eurjchem-71 6 145     SPACE eurjchem-71 6 146 anti‐allergic anti‐allergic ADJ eurjchem-71 6 147 , , PUNCT eurjchem-71 6 148     SPACE eurjchem-71 6 149 narcotic narcotic ADJ eurjchem-71 6 150 , , PUNCT eurjchem-71 6 151     SPACE eurjchem-71 6 152 anti‐angiogenic anti‐angiogenic ADJ eurjchem-71 6 153 , , PUNCT eurjchem-71 6 154     SPACE eurjchem-71 6 155 anti‐malarial anti‐malarial ADJ eurjchem-71 6 156 , , PUNCT eurjchem-71 6 157     SPACE eurjchem-71 7 1 [ [ X eurjchem-71 7 2 8 8 NUM eurjchem-71 7 3 ] ] SYM eurjchem-71 7 4     SPACE eurjchem-71 7 5 anti‐bacterial anti‐bacterial ADJ eurjchem-71 7 6 , , PUNCT eurjchem-71 7 7     SPACE eurjchem-71 7 8 [ [ X eurjchem-71 7 9 9 9 NUM eurjchem-71 7 10 ] ] SYM eurjchem-71 7 11     SPACE eurjchem-71 7 12 anti‐cancer anti‐cancer NOUN eurjchem-71 7 13 , , PUNCT eurjchem-71 7 14     SPACE eurjchem-71 7 15 anti‐virus anti‐virus NOUN eurjchem-71 7 16     SPACE eurjchem-71 8 1 [ [ X eurjchem-71 8 2 10 10 NUM eurjchem-71 8 3 ] ] SYM eurjchem-71 8 4     SPACE eurjchem-71 8 5 and and CCONJ eurjchem-71 8 6     SPACE eurjchem-71 8 7 anti‐microbial anti‐microbial ADJ eurjchem-71 8 8     SPACE eurjchem-71 8 9 activities activity NOUN eurjchem-71 8 10     SPACE eurjchem-71 9 1 [ [ X eurjchem-71 9 2 11,12 11,12 NUM eurjchem-71 9 3 ] ] PUNCT eurjchem-71 9 4 . . PUNCT eurjchem-71 9 5     SPACE eurjchem-71 10 1 in in ADP eurjchem-71 10 2     SPACE eurjchem-71 10 3 view view NOUN eurjchem-71 10 4     SPACE eurjchem-71 10 5 of of ADP eurjchem-71 10 6     SPACE eurjchem-71 10 7 their their PRON eurjchem-71 10 8     SPACE eurjchem-71 10 9 natural natural ADJ eurjchem-71 10 10     SPACE eurjchem-71 10 11 occurrence occurrence NOUN eurjchem-71 10 12 , , PUNCT eurjchem-71 10 13     SPACE eurjchem-71 10 14 biological biological ADJ eurjchem-71 10 15     SPACE eurjchem-71 10 16 activities activity NOUN eurjchem-71 10 17     SPACE eurjchem-71 10 18 and and CCONJ eurjchem-71 10 19     SPACE eurjchem-71 10 20 utility utility NOUN eurjchem-71 10 21     SPACE eurjchem-71 10 22 as as ADP eurjchem-71 10 23     SPACE eurjchem-71 10 24 synthetic synthetic ADJ eurjchem-71 10 25     SPACE eurjchem-71 10 26 intermediates intermediate NOUN eurjchem-71 10 27 , , PUNCT eurjchem-71 10 28     SPACE eurjchem-71 10 29 [ [ X eurjchem-71 10 30 13‐27 13‐27 NUM eurjchem-71 10 31 ] ] X eurjchem-71 10 32     SPACE eurjchem-71 10 33 we we PRON eurjchem-71 10 34     SPACE eurjchem-71 10 35 report report VERB eurjchem-71 10 36     SPACE eurjchem-71 10 37 here here ADV eurjchem-71 10 38     SPACE eurjchem-71 10 39 the the DET eurjchem-71 10 40     SPACE eurjchem-71 10 41 synthesis synthesis NOUN eurjchem-71 10 42       SPACE eurjchem-71 10 43 of of ADP eurjchem-71 10 44     SPACE eurjchem-71 10 45 novel novel NOUN eurjchem-71 10 46     SPACE eurjchem-71 10 47 isochromene isochromene NOUN eurjchem-71 10 48     SPACE eurjchem-71 10 49 and and CCONJ eurjchem-71 10 50     SPACE eurjchem-71 10 51 isoquinoline isoquinoline ADJ eurjchem-71 10 52     SPACE eurjchem-71 10 53 derivatives derivative NOUN eurjchem-71 10 54     SPACE eurjchem-71 10 55 starting start VERB eurjchem-71 10 56     SPACE eurjchem-71 10 57 from from ADP eurjchem-71 10 58     SPACE eurjchem-71 10 59 the the DET eurjchem-71 10 60     SPACE eurjchem-71 10 61 readily readily ADV eurjchem-71 10 62     SPACE eurjchem-71 10 63 obtainable obtainable ADJ eurjchem-71 10 64     SPACE eurjchem-71 10 65 z‐2‐[1‐carboxy‐2‐(3,4‐dimethoxy z‐2‐[1‐carboxy‐2‐(3,4‐dimethoxy PROPN eurjchem-71 10 66     SPACE eurjchem-71 10 67 phenyl)vinyl]‐benzoic phenyl)vinyl]‐benzoic PROPN eurjchem-71 10 68     SPACE eurjchem-71 10 69 acid acid NOUN eurjchem-71 10 70 , , PUNCT eurjchem-71 10 71     SPACE eurjchem-71 10 72 1 1 NUM eurjchem-71 10 73     SPACE eurjchem-71 10 74 [ [ X eurjchem-71 10 75 28 28 NUM eurjchem-71 10 76 ] ] PUNCT eurjchem-71 10 77 . . PUNCT eurjchem-71 10 78         SPACE eurjchem-71 11 1 2 2 NUM eurjchem-71 11 2 . . PUNCT eurjchem-71 11 3     SPACE eurjchem-71 11 4 experimental experimental ADJ eurjchem-71 11 5           SPACE eurjchem-71 11 6 all all DET eurjchem-71 11 7     SPACE eurjchem-71 11 8 melting melting NOUN eurjchem-71 11 9     SPACE eurjchem-71 11 10 points point NOUN eurjchem-71 11 11     SPACE eurjchem-71 11 12 were be AUX eurjchem-71 11 13     SPACE eurjchem-71 11 14 taken take VERB eurjchem-71 11 15     SPACE eurjchem-71 11 16 on on ADP eurjchem-71 11 17     SPACE eurjchem-71 11 18 griffin griffin NOUN eurjchem-71 11 19     SPACE eurjchem-71 11 20 and and CCONJ eurjchem-71 11 21     SPACE eurjchem-71 11 22 geory geory NOUN eurjchem-71 11 23     SPACE eurjchem-71 11 24 melting melting NOUN eurjchem-71 11 25     SPACE eurjchem-71 11 26 point point NOUN eurjchem-71 11 27     SPACE eurjchem-71 11 28 apparatus apparatus NOUN eurjchem-71 11 29     SPACE eurjchem-71 11 30 and and CCONJ eurjchem-71 11 31     SPACE eurjchem-71 11 32 are be AUX eurjchem-71 11 33     SPACE eurjchem-71 11 34 uncorrected uncorrecte VERB eurjchem-71 11 35 . . PUNCT eurjchem-71 11 36     SPACE eurjchem-71 11 37 ir ir PROPN eurjchem-71 11 38     SPACE eurjchem-71 11 39 spectra spectra NOUN eurjchem-71 11 40     SPACE eurjchem-71 11 41 were be AUX eurjchem-71 11 42     SPACE eurjchem-71 11 43 recorded record VERB eurjchem-71 11 44     SPACE eurjchem-71 11 45 on on ADP eurjchem-71 11 46     SPACE eurjchem-71 11 47 pye pye NOUN eurjchem-71 11 48     SPACE eurjchem-71 11 49 unicam unicam NOUN eurjchem-71 11 50     SPACE eurjchem-71 11 51 sp sp AUX eurjchem-71 11 52     SPACE eurjchem-71 11 53 1200 1200 NUM eurjchem-71 11 54     SPACE eurjchem-71 11 55 spectrophotometer spectrophotometer NOUN eurjchem-71 11 56     SPACE eurjchem-71 11 57 using use VERB eurjchem-71 11 58     SPACE eurjchem-71 11 59 kbr kbr PROPN eurjchem-71 11 60     SPACE eurjchem-71 11 61 wafer wafer NOUN eurjchem-71 11 62     SPACE eurjchem-71 11 63 technique technique NOUN eurjchem-71 11 64 . . PUNCT eurjchem-71 11 65     SPACE eurjchem-71 12 1 1h‐nmr 1h‐nmr NUM eurjchem-71 12 2     SPACE eurjchem-71 12 3 spectra spectra NOUN eurjchem-71 12 4     SPACE eurjchem-71 12 5 were be AUX eurjchem-71 12 6     SPACE eurjchem-71 12 7 determined determine VERB eurjchem-71 12 8     SPACE eurjchem-71 12 9 on on ADP eurjchem-71 12 10     SPACE eurjchem-71 12 11 a a DET eurjchem-71 12 12     SPACE eurjchem-71 12 13 varian varian PROPN eurjchem-71 12 14     SPACE eurjchem-71 12 15 gemini gemini PROPN eurjchem-71 12 16     SPACE eurjchem-71 12 17 300 300 NUM eurjchem-71 12 18     SPACE eurjchem-71 12 19 mhz mhz NOUN eurjchem-71 12 20     SPACE eurjchem-71 12 21 using use VERB eurjchem-71 12 22     SPACE eurjchem-71 12 23 tms tms NOUN eurjchem-71 12 24     SPACE eurjchem-71 12 25 as as ADP eurjchem-71 12 26     SPACE eurjchem-71 12 27 internal internal ADJ eurjchem-71 12 28     SPACE eurjchem-71 12 29 standard standard NOUN eurjchem-71 12 30     SPACE eurjchem-71 12 31 ( ( PUNCT eurjchem-71 12 32 chemical chemical NOUN eurjchem-71 12 33     SPACE eurjchem-71 12 34 shifts shift NOUN eurjchem-71 12 35     SPACE eurjchem-71 12 36 in in ADP eurjchem-71 12 37     SPACE eurjchem-71 12 38 δ‐scale δ‐scale PUNCT eurjchem-71 12 39 ) ) PUNCT eurjchem-71 12 40 . . PUNCT eurjchem-71 12 41     SPACE eurjchem-71 13 1 ei‐ms ei‐ms ADV eurjchem-71 13 2     SPACE eurjchem-71 13 3 were be AUX eurjchem-71 13 4     SPACE eurjchem-71 13 5 measured measure VERB eurjchem-71 13 6     SPACE eurjchem-71 13 7 on on ADP eurjchem-71 13 8     SPACE eurjchem-71 13 9 a a DET eurjchem-71 13 10     SPACE eurjchem-71 13 11 schimadzu‐gc‐ms schimadzu‐gc‐ms NOUN eurjchem-71 13 12 , , PUNCT eurjchem-71 13 13     SPACE eurjchem-71 13 14 qp qp ADP eurjchem-71 13 15     SPACE eurjchem-71 13 16 1000 1000 NUM eurjchem-71 13 17     SPACE eurjchem-71 13 18 ex ex NOUN eurjchem-71 13 19     SPACE eurjchem-71 13 20 instrument instrument NOUN eurjchem-71 13 21     SPACE eurjchem-71 13 22 operating operate VERB eurjchem-71 13 23     SPACE eurjchem-71 13 24 at at ADP eurjchem-71 13 25     SPACE eurjchem-71 13 26 70 70 NUM eurjchem-71 13 27     SPACE eurjchem-71 13 28 ev ev PROPN eurjchem-71 13 29 . . PROPN eurjchem-71 13 30     SPACE eurjchem-71 13 31 elemental elemental NOUN eurjchem-71 13 32     SPACE eurjchem-71 13 33 analyses analysis NOUN eurjchem-71 13 34     SPACE eurjchem-71 13 35 were be AUX eurjchem-71 13 36     SPACE eurjchem-71 13 37 carried carry VERB eurjchem-71 13 38     SPACE eurjchem-71 13 39 out out ADP eurjchem-71 13 40     SPACE eurjchem-71 13 41 at at ADP eurjchem-71 13 42     SPACE eurjchem-71 13 43 the the DET eurjchem-71 13 44     SPACE eurjchem-71 13 45 microanalytical microanalytical ADJ eurjchem-71 13 46     SPACE eurjchem-71 13 47 unit unit NOUN eurjchem-71 13 48 , , PUNCT eurjchem-71 13 49     SPACE eurjchem-71 13 50 faculty faculty NOUN eurjchem-71 13 51     SPACE eurjchem-71 13 52 of of ADP eurjchem-71 13 53     SPACE eurjchem-71 13 54 science science NOUN eurjchem-71 13 55 , , PUNCT eurjchem-71 13 56     SPACE eurjchem-71 13 57 ain ain NOUN eurjchem-71 13 58     SPACE eurjchem-71 13 59 shams sham NOUN eurjchem-71 13 60     SPACE eurjchem-71 13 61 university university NOUN eurjchem-71 13 62     SPACE eurjchem-71 13 63 by by ADP eurjchem-71 13 64     SPACE eurjchem-71 13 65 using use VERB eurjchem-71 13 66     SPACE eurjchem-71 13 67 perkin‐elmer perkin‐elmer NOUN eurjchem-71 13 68     SPACE eurjchem-71 13 69 2400 2400 NUM eurjchem-71 13 70     SPACE eurjchem-71 13 71 chn chn PROPN eurjchem-71 13 72     SPACE eurjchem-71 13 73 elemental elemental ADJ eurjchem-71 13 74     SPACE eurjchem-71 13 75 analyzer analyzer NOUN eurjchem-71 13 76     SPACE eurjchem-71 13 77 and and CCONJ eurjchem-71 13 78     SPACE eurjchem-71 13 79 satisfactory satisfactory ADJ eurjchem-71 13 80     SPACE eurjchem-71 13 81 analytical analytical ADJ eurjchem-71 13 82     SPACE eurjchem-71 13 83 data datum NOUN eurjchem-71 13 84     SPACE eurjchem-71 13 85 ( ( PUNCT eurjchem-71 13 86 ± ± NOUN eurjchem-71 13 87     SPACE eurjchem-71 13 88 0.4 0.4 NUM eurjchem-71 13 89 ) ) PUNCT eurjchem-71 13 90     SPACE eurjchem-71 13 91 were be AUX eurjchem-71 13 92     SPACE eurjchem-71 13 93 obtained obtain VERB eurjchem-71 13 94     SPACE eurjchem-71 13 95 for for ADP eurjchem-71 13 96     SPACE eurjchem-71 13 97 all all DET eurjchem-71 13 98     SPACE eurjchem-71 13 99 compounds compound NOUN eurjchem-71 13 100 . . PUNCT eurjchem-71 13 101           SPACE eurjchem-71 13 102 2.1 2.1 NUM eurjchem-71 13 103 . . PUNCT eurjchem-71 13 104     SPACE eurjchem-71 13 105 ( ( PUNCT eurjchem-71 13 106 e)­4­(3,4­dimethoxybenzylidene)­4h­isochromene­1,3­ e)­4­(3,4­dimethoxybenzylidene)­4h­isochromene­1,3­ NOUN eurjchem-71 13 107 dione dione NOUN eurjchem-71 13 108     SPACE eurjchem-71 13 109 ( ( PUNCT eurjchem-71 13 110 2 2 NUM eurjchem-71 13 111 ) ) PUNCT eurjchem-71 13 112         SPACE eurjchem-71 13 113 a a DET eurjchem-71 13 114     SPACE eurjchem-71 13 115 mixture mixture NOUN eurjchem-71 13 116     SPACE eurjchem-71 13 117 of of ADP eurjchem-71 13 118     SPACE eurjchem-71 13 119 the the DET eurjchem-71 13 120     SPACE eurjchem-71 13 121 diacid diacid NOUN eurjchem-71 13 122     SPACE eurjchem-71 13 123 1 1 NUM eurjchem-71 13 124     SPACE eurjchem-71 13 125 ( ( PUNCT eurjchem-71 13 126 3.28 3.28 NUM eurjchem-71 13 127     SPACE eurjchem-71 13 128 g g NOUN eurjchem-71 13 129 , , PUNCT eurjchem-71 13 130     SPACE eurjchem-71 13 131 0.01 0.01 NUM eurjchem-71 13 132     SPACE eurjchem-71 13 133 mole mole NOUN eurjchem-71 13 134 ) ) PUNCT eurjchem-71 13 135     SPACE eurjchem-71 13 136 and and CCONJ eurjchem-71 13 137     SPACE eurjchem-71 13 138 acetyl acetyl NOUN eurjchem-71 13 139     SPACE eurjchem-71 13 140 chloride chloride NOUN eurjchem-71 13 141     SPACE eurjchem-71 13 142 ( ( PUNCT eurjchem-71 13 143 30 30 NUM eurjchem-71 13 144     SPACE eurjchem-71 13 145 ml ml NOUN eurjchem-71 13 146 ) ) PUNCT eurjchem-71 13 147     SPACE eurjchem-71 13 148 was be AUX eurjchem-71 13 149     SPACE eurjchem-71 13 150 refluxed refluxe VERB eurjchem-71 13 151     SPACE eurjchem-71 13 152 for for ADP eurjchem-71 13 153     SPACE eurjchem-71 13 154 10 10 NUM eurjchem-71 13 155     SPACE eurjchem-71 13 156 minutes minute NOUN eurjchem-71 13 157     SPACE eurjchem-71 13 158 on on ADP eurjchem-71 13 159     SPACE eurjchem-71 13 160 water water NOUN eurjchem-71 13 161     SPACE eurjchem-71 13 162 bath bath NOUN eurjchem-71 13 163 . . PUNCT eurjchem-71 13 164     SPACE eurjchem-71 14 1 the the DET eurjchem-71 14 2     SPACE eurjchem-71 14 3 reaction reaction NOUN eurjchem-71 14 4     SPACE eurjchem-71 14 5 mixture mixture NOUN eurjchem-71 14 6     SPACE eurjchem-71 14 7 was be AUX eurjchem-71 14 8     SPACE eurjchem-71 14 9 allowed allow VERB eurjchem-71 14 10     SPACE eurjchem-71 14 11 to to PART eurjchem-71 14 12     SPACE eurjchem-71 14 13 cool cool VERB eurjchem-71 14 14     SPACE eurjchem-71 14 15 then then ADV eurjchem-71 14 16     SPACE eurjchem-71 14 17 the the DET eurjchem-71 14 18     SPACE eurjchem-71 14 19 separated separate VERB eurjchem-71 14 20     SPACE eurjchem-71 14 21 solid solid NOUN eurjchem-71 14 22     SPACE eurjchem-71 14 23 was be AUX eurjchem-71 14 24     SPACE eurjchem-71 14 25 filtered filter VERB eurjchem-71 14 26     SPACE eurjchem-71 14 27 off off ADP eurjchem-71 14 28 , , PUNCT eurjchem-71 14 29     SPACE eurjchem-71 14 30 dried dry VERB eurjchem-71 14 31     SPACE eurjchem-71 14 32 and and CCONJ eurjchem-71 14 33     SPACE eurjchem-71 14 34 then then ADV eurjchem-71 14 35     SPACE eurjchem-71 14 36 recrystallized recrystallize VERB eurjchem-71 14 37     SPACE eurjchem-71 14 38 from from ADP eurjchem-71 14 39     SPACE eurjchem-71 14 40 ethanol ethanol NOUN eurjchem-71 14 41     SPACE eurjchem-71 14 42 to to PART eurjchem-71 14 43     SPACE eurjchem-71 14 44 give give VERB eurjchem-71 14 45     SPACE eurjchem-71 14 46 2 2 NUM eurjchem-71 14 47     SPACE eurjchem-71 14 48 as as ADP eurjchem-71 14 49     SPACE eurjchem-71 14 50 orange orange ADJ eurjchem-71 14 51     SPACE eurjchem-71 14 52 crystals crystal NOUN eurjchem-71 14 53 . . PUNCT eurjchem-71 14 54     SPACE eurjchem-71 15 1 m.p m.p AUX eurjchem-71 15 2 . . PROPN eurjchem-71 15 3 : : PUNCT eurjchem-71 15 4     SPACE eurjchem-71 15 5 138‐140 138‐140 NUM eurjchem-71 15 6     SPACE eurjchem-71 15 7 oc oc NOUN eurjchem-71 15 8 , , PUNCT eurjchem-71 15 9     SPACE eurjchem-71 15 10 yield yield NOUN eurjchem-71 15 11     SPACE eurjchem-71 15 12 ( ( PUNCT eurjchem-71 15 13 2.89 2.89 NUM eurjchem-71 15 14     SPACE eurjchem-71 15 15 g g NOUN eurjchem-71 15 16 ) ) PUNCT eurjchem-71 15 17     SPACE eurjchem-71 15 18 90 90 NUM eurjchem-71 15 19 % % NOUN eurjchem-71 15 20 . . PUNCT eurjchem-71 15 21     SPACE eurjchem-71 16 1 ir ir VERB eurjchem-71 16 2     SPACE eurjchem-71 16 3 ( ( PUNCT eurjchem-71 16 4 ν ν NOUN eurjchem-71 16 5 ): ): NOUN eurjchem-71 16 6     SPACE eurjchem-71 16 7 1773 1773 NUM eurjchem-71 16 8 , , PUNCT eurjchem-71 16 9     SPACE eurjchem-71 16 10 1725 1725 NUM eurjchem-71 16 11     SPACE eurjchem-71 16 12 cm‐1 cm‐1 NOUN eurjchem-71 16 13     SPACE eurjchem-71 16 14 ( ( PUNCT eurjchem-71 16 15 c c NOUN eurjchem-71 16 16 = = SYM eurjchem-71 16 17 ocoupling ocouple VERB eurjchem-71 16 18     SPACE eurjchem-71 16 19 bands band NOUN eurjchem-71 16 20 ) ) PUNCT eurjchem-71 16 21 . . PUNCT eurjchem-71 16 22     SPACE eurjchem-71 17 1 1h‐nmr 1h‐nmr NUM eurjchem-71 17 2     SPACE eurjchem-71 17 3 ( ( PUNCT eurjchem-71 17 4 cdcl3 cdcl3 PROPN eurjchem-71 17 5 ) ) PUNCT eurjchem-71 17 6     SPACE eurjchem-71 17 7 δ δ PROPN eurjchem-71 17 8     SPACE eurjchem-71 17 9 8.1‐7 8.1‐7 NOUN eurjchem-71 17 10     SPACE eurjchem-71 17 11 ( ( PUNCT eurjchem-71 17 12 m m PROPN eurjchem-71 17 13 , , PUNCT eurjchem-71 17 14     SPACE eurjchem-71 17 15 7harom 7harom NUM eurjchem-71 17 16 . . PUNCT eurjchem-71 17 17 ) ) PUNCT eurjchem-71 17 18 , , PUNCT eurjchem-71 17 19     SPACE eurjchem-71 17 20 6.9 6.9 NUM eurjchem-71 17 21     SPACE eurjchem-71 17 22 ( ( PUNCT eurjchem-71 17 23 s s PROPN eurjchem-71 17 24 , , PUNCT eurjchem-71 17 25     SPACE eurjchem-71 17 26 1h 1h NUM eurjchem-71 17 27 , , PUNCT eurjchem-71 17 28     SPACE eurjchem-71 17 29 olefinic olefinic ADJ eurjchem-71 17 30     SPACE eurjchem-71 17 31 h h NOUN eurjchem-71 17 32 ) ) PUNCT eurjchem-71 17 33 , , PUNCT eurjchem-71 17 34     SPACE eurjchem-71 17 35 3.93 3.93 NUM eurjchem-71 17 36     SPACE eurjchem-71 17 37 ( ( PUNCT eurjchem-71 17 38 s s PROPN eurjchem-71 17 39 , , PUNCT eurjchem-71 17 40     SPACE eurjchem-71 17 41 3h 3h NUM eurjchem-71 17 42 , , PUNCT eurjchem-71 17 43     SPACE eurjchem-71 17 44 ome ome NOUN eurjchem-71 17 45 ) ) PUNCT eurjchem-71 17 46     SPACE eurjchem-71 17 47 and and CCONJ eurjchem-71 17 48     SPACE eurjchem-71 17 49 3.69 3.69 NUM eurjchem-71 17 50     SPACE eurjchem-71 17 51 ( ( PUNCT eurjchem-71 17 52 s s PROPN eurjchem-71 17 53 , , PUNCT eurjchem-71 17 54     SPACE eurjchem-71 17 55 3h 3h NUM eurjchem-71 17 56 , , PUNCT eurjchem-71 17 57     SPACE eurjchem-71 17 58 ome ome NOUN eurjchem-71 17 59 ) ) PUNCT eurjchem-71 17 60 . . PUNCT eurjchem-71 17 61     SPACE eurjchem-71 18 1 ms ms NOUN eurjchem-71 18 2 : : PUNCT eurjchem-71 18 3     SPACE eurjchem-71 18 4 310 310 NUM eurjchem-71 18 5     SPACE eurjchem-71 18 6 ( ( PUNCT eurjchem-71 18 7 100 100 NUM eurjchem-71 18 8 ) ) PUNCT eurjchem-71 18 9 , , PUNCT eurjchem-71 18 10     SPACE eurjchem-71 18 11 295 295 NUM eurjchem-71 18 12     SPACE eurjchem-71 18 13 ( ( PUNCT eurjchem-71 18 14 12.6 12.6 NUM eurjchem-71 18 15 ) ) PUNCT eurjchem-71 18 16 , , PUNCT eurjchem-71 18 17     SPACE eurjchem-71 18 18 222 222 NUM eurjchem-71 18 19     SPACE eurjchem-71 18 20 ( ( PUNCT eurjchem-71 18 21 11.2 11.2 NUM eurjchem-71 18 22 ) ) PUNCT eurjchem-71 18 23 , , PUNCT eurjchem-71 18 24     SPACE eurjchem-71 18 25 165 165 NUM eurjchem-71 18 26     SPACE eurjchem-71 18 27 ( ( PUNCT eurjchem-71 18 28 14.0 14.0 NUM eurjchem-71 18 29 ) ) PUNCT eurjchem-71 18 30 , , PUNCT eurjchem-71 18 31     SPACE eurjchem-71 18 32 151 151 NUM eurjchem-71 18 33     SPACE eurjchem-71 18 34 ( ( PUNCT eurjchem-71 18 35 12.9 12.9 NUM eurjchem-71 18 36 ) ) PUNCT eurjchem-71 18 37 , , PUNCT eurjchem-71 18 38     SPACE eurjchem-71 18 39 89 89 NUM eurjchem-71 18 40     SPACE eurjchem-71 18 41 ( ( PUNCT eurjchem-71 18 42 3.8 3.8 NUM eurjchem-71 18 43 ) ) PUNCT eurjchem-71 18 44 . . PUNCT eurjchem-71 18 45     SPACE eurjchem-71 19 1 anal anal ADJ eurjchem-71 19 2 . . PUNCT eurjchem-71 19 3     SPACE eurjchem-71 19 4 calcd calcd NOUN eurjchem-71 19 5 . . PUNCT eurjchem-71 19 6     SPACE eurjchem-71 19 7 for for ADP eurjchem-71 19 8     SPACE eurjchem-71 19 9 c18h14o5 c18h14o5 PROPN eurjchem-71 19 10     SPACE eurjchem-71 19 11 ( ( PUNCT eurjchem-71 19 12 310.3 310.3 NUM eurjchem-71 19 13 ): ): SYM eurjchem-71 19 14     SPACE eurjchem-71 19 15 c c NOUN eurjchem-71 19 16 , , PUNCT eurjchem-71 19 17     SPACE eurjchem-71 19 18 69.76 69.76 NUM eurjchem-71 19 19 ; ; PUNCT eurjchem-71 19 20     SPACE eurjchem-71 19 21 h h NOUN eurjchem-71 19 22 , , PUNCT eurjchem-71 19 23     SPACE eurjchem-71 19 24 4.55 4.55 NUM eurjchem-71 19 25 . . PUNCT eurjchem-71 19 26     SPACE eurjchem-71 19 27 found find VERB eurjchem-71 19 28 : : PUNCT eurjchem-71 19 29     SPACE eurjchem-71 19 30 c c X eurjchem-71 19 31 , , PUNCT eurjchem-71 19 32     SPACE eurjchem-71 19 33 69.63 69.63 NUM eurjchem-71 19 34 ; ; PUNCT eurjchem-71 19 35     SPACE eurjchem-71 19 36 h h NOUN eurjchem-71 19 37 , , PUNCT eurjchem-71 19 38     SPACE eurjchem-71 19 39 4.61 4.61 NUM eurjchem-71 19 40 . . PUNCT eurjchem-71 19 41         SPACE eurjchem-71 19 42 2.2 2.2 NUM eurjchem-71 19 43 . . PUNCT eurjchem-71 19 44     SPACE eurjchem-71 20 1 ( ( PUNCT eurjchem-71 20 2 z)­4­(3,4­dimethoxybenzylidene)­4h­isochromene­1,3­ z)­4­(3,4­dimethoxybenzylidene)­4h­isochromene­1,3­ PROPN eurjchem-71 20 3 dione dione PROPN eurjchem-71 20 4     SPACE eurjchem-71 20 5 ( ( PUNCT eurjchem-71 20 6 3 3 NUM eurjchem-71 20 7 ) ) PUNCT eurjchem-71 20 8         SPACE eurjchem-71 20 9 a a DET eurjchem-71 20 10     SPACE eurjchem-71 20 11 mixture mixture NOUN eurjchem-71 20 12     SPACE eurjchem-71 20 13 of of ADP eurjchem-71 20 14     SPACE eurjchem-71 20 15 the the DET eurjchem-71 20 16     SPACE eurjchem-71 20 17 diacid diacid NOUN eurjchem-71 20 18     SPACE eurjchem-71 20 19 1 1 NUM eurjchem-71 20 20     SPACE eurjchem-71 20 21 ( ( PUNCT eurjchem-71 20 22 3.28 3.28 NUM eurjchem-71 20 23     SPACE eurjchem-71 20 24 g g NOUN eurjchem-71 20 25 , , PUNCT eurjchem-71 20 26     SPACE eurjchem-71 20 27 0.01 0.01 NUM eurjchem-71 20 28     SPACE eurjchem-71 20 29 mole mole NOUN eurjchem-71 20 30 ) ) PUNCT eurjchem-71 20 31     SPACE eurjchem-71 20 32 and and CCONJ eurjchem-71 20 33     SPACE eurjchem-71 20 34 n n CCONJ eurjchem-71 20 35 , , PUNCT eurjchem-71 20 36 n‐ n‐ PROPN eurjchem-71 20 37 dicyclohexyl dicyclohexyl PROPN eurjchem-71 20 38     SPACE eurjchem-71 20 39 carbodiimide carbodiimide NOUN eurjchem-71 20 40     SPACE eurjchem-71 20 41 dcc dcc PROPN eurjchem-71 20 42     SPACE eurjchem-71 20 43 ( ( PUNCT eurjchem-71 20 44 2 2 NUM eurjchem-71 20 45     SPACE eurjchem-71 20 46 g g NOUN eurjchem-71 20 47 ) ) PUNCT eurjchem-71 20 48     SPACE eurjchem-71 20 49 in in ADP eurjchem-71 20 50     SPACE eurjchem-71 20 51 dry dry ADJ eurjchem-71 20 52     SPACE eurjchem-71 20 53 benzene benzene NOUN eurjchem-71 20 54     SPACE eurjchem-71 20 55 ( ( PUNCT eurjchem-71 20 56 30 30 NUM eurjchem-71 20 57     SPACE eurjchem-71 20 58 ml ml NOUN eurjchem-71 20 59 ) ) PUNCT eurjchem-71 20 60     SPACE eurjchem-71 20 61 was be AUX eurjchem-71 20 62     SPACE eurjchem-71 20 63 stirred stir VERB eurjchem-71 20 64     SPACE eurjchem-71 20 65 overnight overnight ADV eurjchem-71 20 66     SPACE eurjchem-71 20 67 at at ADP eurjchem-71 20 68     SPACE eurjchem-71 20 69 room room NOUN eurjchem-71 20 70     SPACE eurjchem-71 20 71 temperature temperature NOUN eurjchem-71 20 72 . . PUNCT eurjchem-71 20 73     SPACE eurjchem-71 21 1 the the DET eurjchem-71 21 2     SPACE eurjchem-71 21 3 deposited deposit VERB eurjchem-71 21 4     SPACE eurjchem-71 21 5 dicyclohexylurea dicyclohexylurea PROPN eurjchem-71 21 6     SPACE eurjchem-71 21 7 was be AUX eurjchem-71 21 8     SPACE eurjchem-71 21 9 separated separate VERB eurjchem-71 21 10 . . PUNCT eurjchem-71 21 11     SPACE eurjchem-71 22 1 evaporation evaporation NOUN eurjchem-71 22 2     SPACE eurjchem-71 22 3 of of ADP eurjchem-71 22 4     SPACE eurjchem-71 22 5 benzene benzene NOUN eurjchem-71 22 6     SPACE eurjchem-71 22 7 left leave VERB eurjchem-71 22 8     SPACE eurjchem-71 22 9 a a DET eurjchem-71 22 10     SPACE eurjchem-71 22 11 yellow yellow ADJ eurjchem-71 22 12     SPACE eurjchem-71 22 13 solid solid NOUN eurjchem-71 22 14     SPACE eurjchem-71 22 15 which which PRON eurjchem-71 22 16     SPACE eurjchem-71 22 17 filtered filter VERB eurjchem-71 22 18     SPACE eurjchem-71 22 19 off off ADP eurjchem-71 22 20 , , PUNCT eurjchem-71 22 21     SPACE eurjchem-71 22 22 dried dry VERB eurjchem-71 22 23     SPACE eurjchem-71 22 24 and and CCONJ eurjchem-71 22 25     SPACE eurjchem-71 22 26 then then ADV eurjchem-71 22 27     SPACE eurjchem-71 22 28 recrystallized recrystallize VERB eurjchem-71 22 29     SPACE eurjchem-71 22 30 from from ADP eurjchem-71 22 31     SPACE eurjchem-71 22 32 ethanol ethanol NOUN eurjchem-71 22 33     SPACE eurjchem-71 22 34 to to PART eurjchem-71 22 35     SPACE eurjchem-71 22 36 give give VERB eurjchem-71 22 37     SPACE eurjchem-71 22 38 3 3 NUM eurjchem-71 22 39     SPACE eurjchem-71 22 40 as as ADP eurjchem-71 22 41     SPACE eurjchem-71 22 42 yellow yellow ADJ eurjchem-71 22 43     SPACE eurjchem-71 22 44 crystals crystal NOUN eurjchem-71 22 45 ; ; PUNCT eurjchem-71 22 46     SPACE eurjchem-71 22 47 m.p m.p PROPN eurjchem-71 22 48 . . PROPN eurjchem-71 22 49 : : PUNCT eurjchem-71 22 50     SPACE eurjchem-71 22 51 163‐165 163‐165 NUM eurjchem-71 22 52     SPACE eurjchem-71 22 53 oc oc NOUN eurjchem-71 22 54 , , PUNCT eurjchem-71 22 55     SPACE eurjchem-71 22 56 yield yield NOUN eurjchem-71 22 57     SPACE eurjchem-71 22 58 ( ( PUNCT eurjchem-71 22 59 2.64 2.64 NUM eurjchem-71 22 60     SPACE eurjchem-71 22 61 g g NOUN eurjchem-71 22 62 ) ) PUNCT eurjchem-71 22 63     SPACE eurjchem-71 22 64 85 85 NUM eurjchem-71 22 65 % % NOUN eurjchem-71 22 66 . . PUNCT eurjchem-71 22 67     SPACE eurjchem-71 23 1 ir ir VERB eurjchem-71 23 2     SPACE eurjchem-71 23 3 ( ( PUNCT eurjchem-71 23 4 ν ν NOUN eurjchem-71 23 5 ): ): NOUN eurjchem-71 23 6     SPACE eurjchem-71 23 7 1768 1768 NUM eurjchem-71 23 8 , , PUNCT eurjchem-71 23 9     SPACE eurjchem-71 23 10 1720 1720 NUM eurjchem-71 23 11     SPACE eurjchem-71 23 12 cm‐1 cm‐1 NOUN eurjchem-71 23 13     SPACE eurjchem-71 23 14 ( ( PUNCT eurjchem-71 23 15 c c NOUN eurjchem-71 23 16 = = SYM eurjchem-71 23 17 ocoupling ocouple VERB eurjchem-71 23 18     SPACE eurjchem-71 23 19 bands band NOUN eurjchem-71 23 20 ) ) PUNCT eurjchem-71 23 21 . . PUNCT eurjchem-71 23 22     SPACE eurjchem-71 24 1 1h‐ 1h‐ NUM eurjchem-71 24 2 nmr nmr PROPN eurjchem-71 24 3     SPACE eurjchem-71 24 4 ( ( PUNCT eurjchem-71 24 5 cdcl3 cdcl3 PROPN eurjchem-71 24 6 ) ) PUNCT eurjchem-71 24 7     SPACE eurjchem-71 24 8 δ δ PROPN eurjchem-71 24 9     SPACE eurjchem-71 24 10 8.3‐7 8.3‐7 PROPN eurjchem-71 24 11     SPACE eurjchem-71 24 12 ( ( PUNCT eurjchem-71 24 13 m m PROPN eurjchem-71 24 14 , , PUNCT eurjchem-71 24 15     SPACE eurjchem-71 24 16 7harom 7harom NUM eurjchem-71 24 17 . . PUNCT eurjchem-71 24 18 ) ) PUNCT eurjchem-71 24 19 , , PUNCT eurjchem-71 24 20     SPACE eurjchem-71 24 21 6.4 6.4 NUM eurjchem-71 24 22     SPACE eurjchem-71 24 23 ( ( PUNCT eurjchem-71 24 24 s s PROPN eurjchem-71 24 25 , , PUNCT eurjchem-71 24 26     SPACE eurjchem-71 24 27 1h 1h NUM eurjchem-71 24 28 , , PUNCT eurjchem-71 24 29     SPACE eurjchem-71 24 30 ch= ch= NOUN eurjchem-71 24 31 ) ) PUNCT eurjchem-71 24 32 , , PUNCT eurjchem-71 24 33     SPACE eurjchem-71 24 34 3.8 3.8 NUM eurjchem-71 24 35     SPACE eurjchem-71 24 36 ( ( PUNCT eurjchem-71 24 37 s s PROPN eurjchem-71 24 38 , , PUNCT eurjchem-71 24 39     SPACE eurjchem-71 24 40 3h 3h NUM eurjchem-71 24 41 , , PUNCT eurjchem-71 24 42     SPACE eurjchem-71 24 43 ome ome NOUN eurjchem-71 24 44 ) ) PUNCT eurjchem-71 24 45 , , PUNCT eurjchem-71 24 46     SPACE eurjchem-71 24 47 3.74 3.74 NUM eurjchem-71 24 48     SPACE eurjchem-71 24 49 ( ( PUNCT eurjchem-71 24 50 s s PROPN eurjchem-71 24 51 , , PUNCT eurjchem-71 24 52     SPACE eurjchem-71 24 53 3h 3h NUM eurjchem-71 24 54 , , PUNCT eurjchem-71 24 55     SPACE eurjchem-71 24 56 ome ome NOUN eurjchem-71 24 57 ) ) PUNCT eurjchem-71 24 58 . . PUNCT eurjchem-71 24 59     SPACE eurjchem-71 25 1 ms ms NOUN eurjchem-71 25 2 : : PUNCT eurjchem-71 25 3     SPACE eurjchem-71 25 4 310 310 NUM eurjchem-71 25 5     SPACE eurjchem-71 25 6 ( ( PUNCT eurjchem-71 25 7 100 100 NUM eurjchem-71 25 8 ) ) PUNCT eurjchem-71 25 9 . . PUNCT eurjchem-71 25 10     SPACE eurjchem-71 26 1 anal anal ADJ eurjchem-71 26 2 . . PUNCT eurjchem-71 26 3     SPACE eurjchem-71 26 4 calcd calcd NOUN eurjchem-71 26 5 . . PUNCT eurjchem-71 26 6     SPACE eurjchem-71 26 7 for for ADP eurjchem-71 26 8     SPACE eurjchem-71 26 9 c18h14o5 c18h14o5 PROPN eurjchem-71 26 10     SPACE eurjchem-71 26 11 ( ( PUNCT eurjchem-71 26 12 310.3 310.3 NUM eurjchem-71 26 13 ): ): SYM eurjchem-71 26 14     SPACE eurjchem-71 26 15 c c NOUN eurjchem-71 26 16 , , PUNCT eurjchem-71 26 17     SPACE eurjchem-71 26 18 69.76 69.76 NUM eurjchem-71 26 19 ; ; PUNCT eurjchem-71 26 20     SPACE eurjchem-71 26 21 h h NOUN eurjchem-71 26 22 , , PUNCT eurjchem-71 26 23     SPACE eurjchem-71 26 24 4.55 4.55 NUM eurjchem-71 26 25 . . PUNCT eurjchem-71 26 26     SPACE eurjchem-71 26 27 found find VERB eurjchem-71 26 28 : : PUNCT eurjchem-71 26 29     SPACE eurjchem-71 26 30 c c X eurjchem-71 26 31 , , PUNCT eurjchem-71 26 32     SPACE eurjchem-71 26 33 69.69 69.69 NUM eurjchem-71 26 34 ; ; PUNCT eurjchem-71 26 35     SPACE eurjchem-71 26 36 h h NOUN eurjchem-71 26 37 , , PUNCT eurjchem-71 26 38     SPACE eurjchem-71 26 39 4.63 4.63 NUM eurjchem-71 26 40 . . PUNCT eurjchem-71 26 41         SPACE eurjchem-71 26 42 2.3 2.3 NUM eurjchem-71 26 43 . . PUNCT eurjchem-71 26 44     SPACE eurjchem-71 27 1 ( ( PUNCT eurjchem-71 27 2 e)­n­(4­(3,4­dimethoxybenzylidene)­1,3­dioxo­3,4­ e)­n­(4­(3,4­dimethoxybenzylidene)­1,3­dioxo­3,4­ X eurjchem-71 27 3 dihydroisoquinolin­2(1h)­yl)­2­cyano­acetamide dihydroisoquinolin­2(1h)­yl)­2­cyano­acetamide NOUN eurjchem-71 27 4     SPACE eurjchem-71 27 5 ( ( PUNCT eurjchem-71 27 6 4 4 NUM eurjchem-71 27 7 ) ) PUNCT eurjchem-71 27 8       SPACE eurjchem-71 27 9 and and CCONJ eurjchem-71 27 10     SPACE eurjchem-71 27 11 ( ( PUNCT eurjchem-71 27 12 e)­n'­(3,4­dimethoxybenzylidene)­2­cyanoacetohydrazide e)­n'­(3,4­dimethoxybenzylidene)­2­cyanoacetohydrazide PROPN eurjchem-71 27 13     SPACE eurjchem-71 27 14 ( ( PUNCT eurjchem-71 27 15 5 5 NUM eurjchem-71 27 16 ) ) PUNCT eurjchem-71 27 17         SPACE eurjchem-71 27 18 a a DET eurjchem-71 27 19     SPACE eurjchem-71 27 20 mixture mixture NOUN eurjchem-71 27 21     SPACE eurjchem-71 27 22 of of ADP eurjchem-71 27 23     SPACE eurjchem-71 27 24 compound compound NOUN eurjchem-71 27 25     SPACE eurjchem-71 27 26 2 2 NUM eurjchem-71 27 27     SPACE eurjchem-71 27 28 ( ( PUNCT eurjchem-71 27 29 3.1 3.1 NUM eurjchem-71 27 30     SPACE eurjchem-71 27 31 g g NOUN eurjchem-71 27 32 , , PUNCT eurjchem-71 27 33     SPACE eurjchem-71 27 34 0.01 0.01 NUM eurjchem-71 27 35     SPACE eurjchem-71 27 36 mole mole NOUN eurjchem-71 27 37 ) ) PUNCT eurjchem-71 27 38     SPACE eurjchem-71 27 39 and and CCONJ eurjchem-71 27 40     SPACE eurjchem-71 27 41 cyanoethanoic cyanoethanoic ADJ eurjchem-71 27 42     SPACE eurjchem-71 27 43 hydrazide hydrazide ADV eurjchem-71 27 44     SPACE eurjchem-71 27 45 ( ( PUNCT eurjchem-71 27 46 0.99 0.99 NUM eurjchem-71 27 47     SPACE eurjchem-71 27 48 g g NOUN eurjchem-71 27 49 , , PUNCT eurjchem-71 27 50     SPACE eurjchem-71 27 51 0.01 0.01 NUM eurjchem-71 27 52     SPACE eurjchem-71 27 53 mole mole NOUN eurjchem-71 27 54 ) ) PUNCT eurjchem-71 27 55     SPACE eurjchem-71 27 56 in in ADP eurjchem-71 27 57     SPACE eurjchem-71 27 58 dioxane dioxane NOUN eurjchem-71 27 59     SPACE eurjchem-71 27 60 ( ( PUNCT eurjchem-71 27 61 30 30 NUM eurjchem-71 27 62     SPACE eurjchem-71 27 63 ml ml NOUN eurjchem-71 27 64 ) ) PUNCT eurjchem-71 27 65     SPACE eurjchem-71 27 66 was be AUX eurjchem-71 27 67     SPACE eurjchem-71 27 68 refluxed refluxe VERB eurjchem-71 27 69     SPACE eurjchem-71 27 70 for for ADP eurjchem-71 27 71     SPACE eurjchem-71 27 72 6 6 NUM eurjchem-71 27 73     SPACE eurjchem-71 27 74 h. h. NOUN eurjchem-71 27 75     SPACE eurjchem-71 27 76 after after ADP eurjchem-71 27 77     SPACE eurjchem-71 27 78 concentration concentration NOUN eurjchem-71 27 79     SPACE eurjchem-71 27 80 of of ADP eurjchem-71 27 81     SPACE eurjchem-71 27 82 the the DET eurjchem-71 27 83     SPACE eurjchem-71 27 84 solvent solvent NOUN eurjchem-71 27 85 , , PUNCT eurjchem-71 27 86     SPACE eurjchem-71 27 87 a a DET eurjchem-71 27 88     SPACE eurjchem-71 27 89 yellow yellow ADJ eurjchem-71 27 90     SPACE eurjchem-71 27 91 solid solid NOUN eurjchem-71 27 92     SPACE eurjchem-71 27 93 was be AUX eurjchem-71 27 94     SPACE eurjchem-71 27 95 deposited deposit VERB eurjchem-71 27 96     SPACE eurjchem-71 27 97 which which PRON eurjchem-71 27 98     SPACE eurjchem-71 27 99 filtered filter VERB eurjchem-71 27 100     SPACE eurjchem-71 27 101 off off ADP eurjchem-71 27 102 , , PUNCT eurjchem-71 27 103     SPACE eurjchem-71 27 104 dried dry VERB eurjchem-71 27 105     SPACE eurjchem-71 27 106 and and CCONJ eurjchem-71 27 107     SPACE eurjchem-71 27 108 then then ADV eurjchem-71 27 109     SPACE eurjchem-71 27 110 recrystallized recrystallize VERB eurjchem-71 27 111     SPACE eurjchem-71 27 112 from from ADP eurjchem-71 27 113     SPACE eurjchem-71 27 114 ethanol ethanol NOUN eurjchem-71 27 115     SPACE eurjchem-71 27 116 to to PART eurjchem-71 27 117     SPACE eurjchem-71 27 118 give give VERB eurjchem-71 27 119     SPACE eurjchem-71 27 120 4 4 NUM eurjchem-71 27 121 . . PUNCT eurjchem-71 27 122     SPACE eurjchem-71 27 123 slow slow ADJ eurjchem-71 27 124     SPACE eurjchem-71 27 125 evaporation evaporation NOUN eurjchem-71 27 126     SPACE eurjchem-71 27 127 of of ADP eurjchem-71 27 128     SPACE eurjchem-71 27 129 the the DET eurjchem-71 27 130     SPACE eurjchem-71 27 131 filtrate filtrate NOUN eurjchem-71 27 132     SPACE eurjchem-71 27 133 leave leave VERB eurjchem-71 27 134     SPACE eurjchem-71 27 135 oil oil NOUN eurjchem-71 27 136     SPACE eurjchem-71 27 137 which which PRON eurjchem-71 27 138     SPACE eurjchem-71 27 139 solidify solidify VERB eurjchem-71 27 140     SPACE eurjchem-71 27 141 after after ADP eurjchem-71 27 142     SPACE eurjchem-71 27 143 trituration trituration NOUN eurjchem-71 27 144     SPACE eurjchem-71 27 145 with with ADP eurjchem-71 27 146     SPACE eurjchem-71 27 147 small small ADJ eurjchem-71 27 148     SPACE eurjchem-71 27 149 amount amount NOUN eurjchem-71 27 150     SPACE eurjchem-71 27 151 of of ADP eurjchem-71 27 152     SPACE eurjchem-71 27 153 ethanol ethanol NOUN eurjchem-71 27 154 . . PUNCT eurjchem-71 27 155     SPACE eurjchem-71 28 1 the the DET eurjchem-71 28 2     SPACE eurjchem-71 28 3 separated separate VERB eurjchem-71 28 4     SPACE eurjchem-71 28 5 solid solid NOUN eurjchem-71 28 6     SPACE eurjchem-71 28 7 was be AUX eurjchem-71 28 8     SPACE eurjchem-71 28 9 filtered filter VERB eurjchem-71 28 10     SPACE eurjchem-71 28 11 off off ADP eurjchem-71 28 12 , , PUNCT eurjchem-71 28 13     SPACE eurjchem-71 28 14 dried dry VERB eurjchem-71 28 15     SPACE eurjchem-71 28 16 mahmoud mahmoud PROPN eurjchem-71 28 17     SPACE eurjchem-71 28 18 et et PROPN eurjchem-71 28 19     SPACE eurjchem-71 28 20 al al PROPN eurjchem-71 28 21 . . PROPN eurjchem-71 28 22     SPACE eurjchem-71 28 23 / / SYM eurjchem-71 28 24     SPACE eurjchem-71 28 25 european european ADJ eurjchem-71 28 26     SPACE eurjchem-71 28 27 journal journal NOUN eurjchem-71 28 28     SPACE eurjchem-71 28 29 of of ADP eurjchem-71 28 30     SPACE eurjchem-71 28 31 chemistry chemistry NOUN eurjchem-71 28 32     SPACE eurjchem-71 28 33 1 1 NUM eurjchem-71 28 34     SPACE eurjchem-71 28 35 ( ( PUNCT eurjchem-71 28 36 2 2 NUM eurjchem-71 28 37 ) ) PUNCT eurjchem-71 28 38     SPACE eurjchem-71 28 39 ( ( PUNCT eurjchem-71 28 40 2010 2010 NUM eurjchem-71 28 41 ) ) PUNCT eurjchem-71 28 42     SPACE eurjchem-71 28 43 134­139 134­139 NUM eurjchem-71 28 44     SPACE eurjchem-71 28 45 135 135 NUM eurjchem-71 28 46     SPACE eurjchem-71 28 47 and and CCONJ eurjchem-71 28 48     SPACE eurjchem-71 28 49 then then ADV eurjchem-71 28 50     SPACE eurjchem-71 28 51 recrystallized recrystallize VERB eurjchem-71 28 52     SPACE eurjchem-71 28 53 from from ADP eurjchem-71 28 54     SPACE eurjchem-71 28 55 ethanol ethanol NOUN eurjchem-71 28 56     SPACE eurjchem-71 28 57 to to PART eurjchem-71 28 58     SPACE eurjchem-71 28 59 give give VERB eurjchem-71 28 60     SPACE eurjchem-71 28 61 5 5 NUM eurjchem-71 28 62     SPACE eurjchem-71 28 63 as as ADP eurjchem-71 28 64     SPACE eurjchem-71 28 65 pale pale ADJ eurjchem-71 28 66     SPACE eurjchem-71 28 67 yellow yellow ADJ eurjchem-71 28 68     SPACE eurjchem-71 28 69 crystals crystal NOUN eurjchem-71 28 70 . . PUNCT eurjchem-71 28 71     SPACE eurjchem-71 29 1 4 4 NUM eurjchem-71 29 2 : : PUNCT eurjchem-71 29 3     SPACE eurjchem-71 29 4 m.p m.p PROPN eurjchem-71 29 5 . . PROPN eurjchem-71 29 6 : : PUNCT eurjchem-71 29 7     SPACE eurjchem-71 29 8 210‐213 210‐213 PROPN eurjchem-71 29 9     SPACE eurjchem-71 29 10 oc oc NOUN eurjchem-71 29 11 , , PUNCT eurjchem-71 29 12     SPACE eurjchem-71 29 13 yield yield NOUN eurjchem-71 29 14     SPACE eurjchem-71 29 15 45 45 NUM eurjchem-71 29 16 % % NOUN eurjchem-71 29 17 . . PUNCT eurjchem-71 29 18     SPACE eurjchem-71 30 1 ir ir VERB eurjchem-71 30 2     SPACE eurjchem-71 30 3 ( ( PUNCT eurjchem-71 30 4 ν ν NOUN eurjchem-71 30 5 ): ): NOUN eurjchem-71 30 6     SPACE eurjchem-71 30 7 3210 3210 NUM eurjchem-71 30 8     SPACE eurjchem-71 30 9 cm‐1 cm‐1 NOUN eurjchem-71 30 10     SPACE eurjchem-71 30 11 ( ( PUNCT eurjchem-71 30 12 nh nh NOUN eurjchem-71 30 13 ) ) PUNCT eurjchem-71 30 14 , , PUNCT eurjchem-71 30 15     SPACE eurjchem-71 30 16 2257 2257 NUM eurjchem-71 30 17     SPACE eurjchem-71 30 18 cm‐1 cm‐1 NOUN eurjchem-71 30 19     SPACE eurjchem-71 30 20 ( ( PUNCT eurjchem-71 30 21 c≡n c≡n PROPN eurjchem-71 30 22 ) ) PUNCT eurjchem-71 30 23 , , PUNCT eurjchem-71 30 24     SPACE eurjchem-71 30 25 1748 1748 NUM eurjchem-71 30 26 , , PUNCT eurjchem-71 30 27     SPACE eurjchem-71 30 28 1682 1682 NUM eurjchem-71 30 29     SPACE eurjchem-71 30 30 cm‐1 cm‐1 NOUN eurjchem-71 30 31     SPACE eurjchem-71 30 32 ( ( PUNCT eurjchem-71 30 33 c c NOUN eurjchem-71 30 34 = = NOUN eurjchem-71 30 35 o o NOUN eurjchem-71 30 36 ) ) PUNCT eurjchem-71 30 37 . . PUNCT eurjchem-71 30 38     SPACE eurjchem-71 31 1 1h‐nmr 1h‐nmr NUM eurjchem-71 31 2     SPACE eurjchem-71 31 3 ( ( PUNCT eurjchem-71 31 4 dmso‐d6 dmso‐d6 NOUN eurjchem-71 31 5 ) ) PUNCT eurjchem-71 31 6     SPACE eurjchem-71 31 7 δ δ PROPN eurjchem-71 31 8     SPACE eurjchem-71 31 9 11.07 11.07 NUM eurjchem-71 31 10     SPACE eurjchem-71 31 11 ( ( PUNCT eurjchem-71 31 12 s s PROPN eurjchem-71 31 13 , , PUNCT eurjchem-71 31 14     SPACE eurjchem-71 31 15 1h 1h NUM eurjchem-71 31 16 , , PUNCT eurjchem-71 31 17     SPACE eurjchem-71 31 18 nh nh PROPN eurjchem-71 31 19 , , PUNCT eurjchem-71 31 20     SPACE eurjchem-71 31 21 exchangeable exchangeable ADJ eurjchem-71 31 22     SPACE eurjchem-71 31 23 with with ADP eurjchem-71 31 24     SPACE eurjchem-71 31 25 d2o d2o NOUN eurjchem-71 31 26 ) ) PUNCT eurjchem-71 31 27 , , PUNCT eurjchem-71 31 28     SPACE eurjchem-71 31 29 8.09‐7.08 8.09‐7.08 NUM eurjchem-71 31 30     SPACE eurjchem-71 31 31 ( ( PUNCT eurjchem-71 31 32 m m PROPN eurjchem-71 31 33 , , PUNCT eurjchem-71 31 34     SPACE eurjchem-71 31 35 8harom 8harom NUM eurjchem-71 31 36 . . PUNCT eurjchem-71 31 37     SPACE eurjchem-71 32 1 + + ADV eurjchem-71 32 2     SPACE eurjchem-71 32 3 olefinic olefinic ADJ eurjchem-71 32 4     SPACE eurjchem-71 32 5 h h NOUN eurjchem-71 32 6 ) ) PUNCT eurjchem-71 32 7 , , PUNCT eurjchem-71 32 8     SPACE eurjchem-71 32 9 4.05 4.05 NUM eurjchem-71 32 10     SPACE eurjchem-71 32 11 ( ( PUNCT eurjchem-71 32 12 s s PROPN eurjchem-71 32 13 , , PUNCT eurjchem-71 32 14     SPACE eurjchem-71 32 15 2h 2h NUM eurjchem-71 32 16 , , PUNCT eurjchem-71 32 17     SPACE eurjchem-71 32 18 coch2cn coch2cn VERB eurjchem-71 32 19 ) ) PUNCT eurjchem-71 32 20 , , PUNCT eurjchem-71 32 21     SPACE eurjchem-71 32 22 3.85 3.85 NUM eurjchem-71 32 23     SPACE eurjchem-71 32 24 ( ( PUNCT eurjchem-71 32 25 s s PROPN eurjchem-71 32 26 , , PUNCT eurjchem-71 32 27     SPACE eurjchem-71 32 28 6h 6h NOUN eurjchem-71 32 29 , , PUNCT eurjchem-71 32 30     SPACE eurjchem-71 32 31 2ome 2ome NUM eurjchem-71 32 32 ) ) PUNCT eurjchem-71 32 33 . . PUNCT eurjchem-71 32 34     SPACE eurjchem-71 33 1 ms ms NOUN eurjchem-71 33 2 : : PUNCT eurjchem-71 33 3     SPACE eurjchem-71 33 4 391 391 NUM eurjchem-71 33 5     SPACE eurjchem-71 33 6 ( ( PUNCT eurjchem-71 33 7 71.3 71.3 NUM eurjchem-71 33 8 ) ) PUNCT eurjchem-71 33 9 , , PUNCT eurjchem-71 33 10     SPACE eurjchem-71 33 11 323 323 NUM eurjchem-71 33 12     SPACE eurjchem-71 33 13 ( ( PUNCT eurjchem-71 33 14 21.4 21.4 NUM eurjchem-71 33 15 ) ) PUNCT eurjchem-71 33 16 , , PUNCT eurjchem-71 33 17     SPACE eurjchem-71 33 18 309 309 NUM eurjchem-71 33 19     SPACE eurjchem-71 33 20 ( ( PUNCT eurjchem-71 33 21 17.1 17.1 NUM eurjchem-71 33 22 ) ) PUNCT eurjchem-71 33 23 , , PUNCT eurjchem-71 33 24     SPACE eurjchem-71 33 25 216 216 NUM eurjchem-71 33 26     SPACE eurjchem-71 33 27 ( ( PUNCT eurjchem-71 33 28 100 100 NUM eurjchem-71 33 29 ) ) PUNCT eurjchem-71 33 30 , , PUNCT eurjchem-71 33 31     SPACE eurjchem-71 33 32 176 176 NUM eurjchem-71 33 33     SPACE eurjchem-71 33 34 ( ( PUNCT eurjchem-71 33 35 43.5 43.5 NUM eurjchem-71 33 36 ) ) PUNCT eurjchem-71 33 37 , , PUNCT eurjchem-71 33 38     SPACE eurjchem-71 33 39 151 151 NUM eurjchem-71 33 40     SPACE eurjchem-71 33 41 ( ( PUNCT eurjchem-71 33 42 50.8 50.8 NUM eurjchem-71 33 43 ) ) PUNCT eurjchem-71 33 44 , , PUNCT eurjchem-71 33 45     SPACE eurjchem-71 33 46 145 145 NUM eurjchem-71 33 47     SPACE eurjchem-71 33 48 ( ( PUNCT eurjchem-71 33 49 32.2 32.2 NUM eurjchem-71 33 50 ) ) PUNCT eurjchem-71 33 51 , , PUNCT eurjchem-71 33 52     SPACE eurjchem-71 33 53 90 90 NUM eurjchem-71 33 54     SPACE eurjchem-71 33 55 ( ( PUNCT eurjchem-71 33 56 49.5 49.5 NUM eurjchem-71 33 57 ) ) PUNCT eurjchem-71 33 58 , , PUNCT eurjchem-71 33 59     SPACE eurjchem-71 33 60 64 64 NUM eurjchem-71 33 61     SPACE eurjchem-71 33 62 ( ( PUNCT eurjchem-71 33 63 13.8 13.8 NUM eurjchem-71 33 64 ) ) PUNCT eurjchem-71 33 65 . . PUNCT eurjchem-71 33 66     SPACE eurjchem-71 34 1 anal anal ADJ eurjchem-71 34 2 . . PUNCT eurjchem-71 34 3     SPACE eurjchem-71 34 4 calcd calcd NOUN eurjchem-71 34 5 . . PUNCT eurjchem-71 34 6     SPACE eurjchem-71 34 7 for for ADP eurjchem-71 34 8     SPACE eurjchem-71 34 9 c21h17n3o5 c21h17n3o5 NOUN eurjchem-71 34 10     SPACE eurjchem-71 34 11 ( ( PUNCT eurjchem-71 34 12 391.38 391.38 NUM eurjchem-71 34 13 ): ): PUNCT eurjchem-71 34 14     SPACE eurjchem-71 34 15 c c NOUN eurjchem-71 34 16 , , PUNCT eurjchem-71 34 17     SPACE eurjchem-71 34 18 64.45; 64.45; NOUN eurjchem-71 34 19     SPACE eurjchem-71 34 20 h h NOUN eurjchem-71 34 21 , , PUNCT eurjchem-71 34 22     SPACE eurjchem-71 34 23 4.38 4.38 NUM eurjchem-71 34 24 ; ; PUNCT eurjchem-71 34 25     SPACE eurjchem-71 34 26 n n CCONJ eurjchem-71 34 27 , , PUNCT eurjchem-71 34 28     SPACE eurjchem-71 34 29 10.74 10.74 NUM eurjchem-71 34 30 . . PUNCT eurjchem-71 34 31     SPACE eurjchem-71 34 32 found find VERB eurjchem-71 34 33 : : PUNCT eurjchem-71 34 34     SPACE eurjchem-71 34 35 c c X eurjchem-71 34 36 , , PUNCT eurjchem-71 34 37     SPACE eurjchem-71 34 38 64.24 64.24 NUM eurjchem-71 34 39 ; ; PUNCT eurjchem-71 34 40     SPACE eurjchem-71 34 41 h h NOUN eurjchem-71 34 42 , , PUNCT eurjchem-71 34 43     SPACE eurjchem-71 34 44 4.18 4.18 NUM eurjchem-71 34 45 ; ; PUNCT eurjchem-71 34 46     SPACE eurjchem-71 34 47 n n CCONJ eurjchem-71 34 48 , , PUNCT eurjchem-71 34 49     SPACE eurjchem-71 34 50 10.44 10.44 NUM eurjchem-71 34 51 . . PUNCT eurjchem-71 34 52     SPACE eurjchem-71 35 1 13c‐nmr 13c‐nmr NUM eurjchem-71 35 2     SPACE eurjchem-71 35 3 ( ( PUNCT eurjchem-71 35 4 dmso‐d6 dmso‐d6 NOUN eurjchem-71 35 5 ) ) PUNCT eurjchem-71 35 6     SPACE eurjchem-71 35 7 for for ADP eurjchem-71 35 8     SPACE eurjchem-71 35 9 compound compound NOUN eurjchem-71 35 10     SPACE eurjchem-71 35 11 4 4 NUM eurjchem-71 35 12     SPACE eurjchem-71 35 13 is be AUX eurjchem-71 35 14     SPACE eurjchem-71 35 15 given give VERB eurjchem-71 35 16     SPACE eurjchem-71 35 17 in in ADP eurjchem-71 35 18     SPACE eurjchem-71 35 19 scheme scheme NOUN eurjchem-71 35 20     SPACE eurjchem-71 35 21 1 1 NUM eurjchem-71 35 22 . . PUNCT eurjchem-71 35 23         SPACE eurjchem-71 35 24 scheme scheme NOUN eurjchem-71 35 25     SPACE eurjchem-71 35 26 1 1 NUM eurjchem-71 35 27         SPACE eurjchem-71 35 28 5 5 NUM eurjchem-71 35 29 : : PUNCT eurjchem-71 35 30     SPACE eurjchem-71 35 31 m.p m.p PROPN eurjchem-71 35 32 . . PROPN eurjchem-71 35 33 : : PUNCT eurjchem-71 35 34     SPACE eurjchem-71 35 35 150‐152oc 150‐152oc NUM eurjchem-71 35 36 , , PUNCT eurjchem-71 35 37     SPACE eurjchem-71 35 38 yield yield NOUN eurjchem-71 35 39     SPACE eurjchem-71 35 40 13 13 NUM eurjchem-71 35 41 % % NOUN eurjchem-71 35 42 . . PUNCT eurjchem-71 35 43     SPACE eurjchem-71 36 1 ir ir VERB eurjchem-71 36 2     SPACE eurjchem-71 36 3 ( ( PUNCT eurjchem-71 36 4 ν ν NOUN eurjchem-71 36 5 ): ): NOUN eurjchem-71 36 6     SPACE eurjchem-71 36 7 3194 3194 NUM eurjchem-71 36 8     SPACE eurjchem-71 36 9 cm‐1 cm‐1 NOUN eurjchem-71 36 10     SPACE eurjchem-71 36 11 ( ( PUNCT eurjchem-71 36 12 nh nh NOUN eurjchem-71 36 13 ) ) PUNCT eurjchem-71 36 14 , , PUNCT eurjchem-71 36 15     SPACE eurjchem-71 36 16 2261 2261 NUM eurjchem-71 36 17     SPACE eurjchem-71 36 18 cm‐ cm‐ NOUN eurjchem-71 36 19 1 1 NUM eurjchem-71 36 20     SPACE eurjchem-71 36 21 ( ( PUNCT eurjchem-71 36 22 c≡n c≡n PROPN eurjchem-71 36 23 ) ) PUNCT eurjchem-71 36 24 , , PUNCT eurjchem-71 36 25     SPACE eurjchem-71 36 26 1680 1680 NUM eurjchem-71 36 27     SPACE eurjchem-71 36 28 cm‐1 cm‐1 NOUN eurjchem-71 36 29     SPACE eurjchem-71 36 30 ( ( PUNCT eurjchem-71 36 31 c c NOUN eurjchem-71 36 32 = = NOUN eurjchem-71 36 33 o o NOUN eurjchem-71 36 34 ) ) PUNCT eurjchem-71 36 35 . . PUNCT eurjchem-71 36 36     SPACE eurjchem-71 37 1 1h‐nmr 1h‐nmr NUM eurjchem-71 37 2     SPACE eurjchem-71 37 3 ( ( PUNCT eurjchem-71 37 4 cdcl3 cdcl3 PROPN eurjchem-71 37 5 ) ) PUNCT eurjchem-71 37 6     SPACE eurjchem-71 37 7 δ δ PROPN eurjchem-71 37 8     SPACE eurjchem-71 37 9 10.1 10.1 NUM eurjchem-71 37 10     SPACE eurjchem-71 37 11 ( ( PUNCT eurjchem-71 37 12 br.s br.s PROPN eurjchem-71 37 13 , , PUNCT eurjchem-71 37 14     SPACE eurjchem-71 37 15 1h 1h NUM eurjchem-71 37 16 , , PUNCT eurjchem-71 37 17     SPACE eurjchem-71 37 18 nh nh PROPN eurjchem-71 37 19 ) ) PUNCT eurjchem-71 37 20 , , PUNCT eurjchem-71 37 21     SPACE eurjchem-71 37 22 8.6 8.6 NUM eurjchem-71 37 23     SPACE eurjchem-71 37 24 ( ( PUNCT eurjchem-71 37 25 s s PROPN eurjchem-71 37 26 , , PUNCT eurjchem-71 37 27     SPACE eurjchem-71 37 28 1h 1h NUM eurjchem-71 37 29 , , PUNCT eurjchem-71 37 30     SPACE eurjchem-71 37 31 ch ch NOUN eurjchem-71 37 32 = = NOUN eurjchem-71 37 33 n n CCONJ eurjchem-71 37 34 ) ) PUNCT eurjchem-71 37 35 , , PUNCT eurjchem-71 37 36     SPACE eurjchem-71 37 37 7.7‐7.1 7.7‐7.1 NUM eurjchem-71 37 38     SPACE eurjchem-71 37 39 ( ( PUNCT eurjchem-71 37 40 m m PROPN eurjchem-71 37 41 , , PUNCT eurjchem-71 37 42     SPACE eurjchem-71 37 43 3harom 3harom NUM eurjchem-71 37 44 . . PROPN eurjchem-71 37 45 ) ) PUNCT eurjchem-71 37 46 , , PUNCT eurjchem-71 37 47     SPACE eurjchem-71 37 48 4.0 4.0 NUM eurjchem-71 37 49     SPACE eurjchem-71 37 50 ( ( PUNCT eurjchem-71 37 51 s s PROPN eurjchem-71 37 52 , , PUNCT eurjchem-71 37 53     SPACE eurjchem-71 37 54 2h 2h NUM eurjchem-71 37 55 , , PUNCT eurjchem-71 37 56     SPACE eurjchem-71 37 57 coch2cn coch2cn VERB eurjchem-71 37 58 ) ) PUNCT eurjchem-71 37 59 , , PUNCT eurjchem-71 37 60     SPACE eurjchem-71 37 61 3.88 3.88 NUM eurjchem-71 37 62     SPACE eurjchem-71 37 63 ( ( PUNCT eurjchem-71 37 64 s s PROPN eurjchem-71 37 65 , , PUNCT eurjchem-71 37 66     SPACE eurjchem-71 37 67 3h 3h NUM eurjchem-71 37 68 , , PUNCT eurjchem-71 37 69     SPACE eurjchem-71 37 70 ome ome NOUN eurjchem-71 37 71 ) ) PUNCT eurjchem-71 37 72 , , PUNCT eurjchem-71 37 73     SPACE eurjchem-71 37 74 3.8 3.8 NUM eurjchem-71 37 75     SPACE eurjchem-71 37 76 ( ( PUNCT eurjchem-71 37 77 s s PROPN eurjchem-71 37 78 , , PUNCT eurjchem-71 37 79     SPACE eurjchem-71 37 80 3h 3h NUM eurjchem-71 37 81 , , PUNCT eurjchem-71 37 82     SPACE eurjchem-71 37 83 ome ome NOUN eurjchem-71 37 84 ) ) PUNCT eurjchem-71 37 85 . . PUNCT eurjchem-71 37 86     SPACE eurjchem-71 38 1 ms ms NOUN eurjchem-71 38 2 : : PUNCT eurjchem-71 38 3     SPACE eurjchem-71 38 4 247 247 NUM eurjchem-71 38 5     SPACE eurjchem-71 38 6 ( ( PUNCT eurjchem-71 38 7 61.6 61.6 NUM eurjchem-71 38 8 ) ) PUNCT eurjchem-71 38 9 , , PUNCT eurjchem-71 38 10     SPACE eurjchem-71 38 11 163 163 NUM eurjchem-71 38 12     SPACE eurjchem-71 38 13 ( ( PUNCT eurjchem-71 38 14 100 100 NUM eurjchem-71 38 15 ) ) PUNCT eurjchem-71 38 16 , , PUNCT eurjchem-71 38 17     SPACE eurjchem-71 38 18 148 148 NUM eurjchem-71 38 19     SPACE eurjchem-71 38 20 ( ( PUNCT eurjchem-71 38 21 35.6 35.6 NUM eurjchem-71 38 22 ) ) PUNCT eurjchem-71 38 23 , , PUNCT eurjchem-71 38 24     SPACE eurjchem-71 38 25 120 120 NUM eurjchem-71 38 26     SPACE eurjchem-71 38 27 ( ( PUNCT eurjchem-71 38 28 11.8 11.8 NUM eurjchem-71 38 29 ) ) PUNCT eurjchem-71 38 30 , , PUNCT eurjchem-71 38 31     SPACE eurjchem-71 38 32 92 92 NUM eurjchem-71 38 33     SPACE eurjchem-71 38 34 ( ( PUNCT eurjchem-71 38 35 25.4 25.4 NUM eurjchem-71 38 36 ) ) PUNCT eurjchem-71 38 37 . . PUNCT eurjchem-71 38 38     SPACE eurjchem-71 39 1 anal anal ADJ eurjchem-71 39 2 . . PUNCT eurjchem-71 39 3     SPACE eurjchem-71 39 4 calcd calcd NOUN eurjchem-71 39 5 . . PUNCT eurjchem-71 39 6     SPACE eurjchem-71 39 7 for for ADP eurjchem-71 39 8     SPACE eurjchem-71 39 9 c12h13n3o3 c12h13n3o3 NOUN eurjchem-71 39 10     SPACE eurjchem-71 39 11 ( ( PUNCT eurjchem-71 39 12 247.25 247.25 NUM eurjchem-71 39 13 ): ): PUNCT eurjchem-71 39 14     SPACE eurjchem-71 39 15 c c NOUN eurjchem-71 39 16 , , PUNCT eurjchem-71 39 17     SPACE eurjchem-71 39 18 58.29; 58.29; NOUN eurjchem-71 39 19     SPACE eurjchem-71 39 20 h h NOUN eurjchem-71 39 21 , , PUNCT eurjchem-71 39 22     SPACE eurjchem-71 39 23 5.30 5.30 NUM eurjchem-71 39 24 ; ; PUNCT eurjchem-71 39 25     SPACE eurjchem-71 39 26 n n CCONJ eurjchem-71 39 27 , , PUNCT eurjchem-71 39 28     SPACE eurjchem-71 39 29 16.99 16.99 NUM eurjchem-71 39 30 . . PUNCT eurjchem-71 39 31     SPACE eurjchem-71 39 32 found find VERB eurjchem-71 39 33 : : PUNCT eurjchem-71 39 34     SPACE eurjchem-71 39 35 c c X eurjchem-71 39 36 , , PUNCT eurjchem-71 39 37     SPACE eurjchem-71 39 38 58.4 58.4 NUM eurjchem-71 39 39 ; ; PUNCT eurjchem-71 39 40     SPACE eurjchem-71 39 41 h h NOUN eurjchem-71 39 42 , , PUNCT eurjchem-71 39 43     SPACE eurjchem-71 39 44 5.12 5.12 NUM eurjchem-71 39 45 ; ; PUNCT eurjchem-71 39 46     SPACE eurjchem-71 39 47 n n CCONJ eurjchem-71 39 48 , , PUNCT eurjchem-71 39 49     SPACE eurjchem-71 39 50 17.09 17.09 NUM eurjchem-71 39 51 . . PUNCT eurjchem-71 39 52         SPACE eurjchem-71 39 53 2.4 2.4 NUM eurjchem-71 39 54 . . PUNCT eurjchem-71 39 55     SPACE eurjchem-71 39 56 pyrido[1,2­b]­1,2,4­triazolo[5,1­a]isoquinolinone pyrido[1,2­b]­1,2,4­triazolo[5,1­a]isoquinolinone NOUN eurjchem-71 39 57     SPACE eurjchem-71 39 58 derivative derivative NOUN eurjchem-71 39 59     SPACE eurjchem-71 39 60 ( ( PUNCT eurjchem-71 39 61 6 6 NUM eurjchem-71 39 62 ) ) PUNCT eurjchem-71 39 63         SPACE eurjchem-71 39 64 a a DET eurjchem-71 39 65     SPACE eurjchem-71 39 66 mixture mixture NOUN eurjchem-71 39 67     SPACE eurjchem-71 39 68 of of ADP eurjchem-71 39 69     SPACE eurjchem-71 39 70 the the DET eurjchem-71 39 71     SPACE eurjchem-71 39 72 isoquinolin‐1,3‐dione isoquinolin‐1,3‐dione NOUN eurjchem-71 39 73     SPACE eurjchem-71 39 74 4 4 NUM eurjchem-71 39 75     SPACE eurjchem-71 39 76 ( ( PUNCT eurjchem-71 39 77 3.91 3.91 NUM eurjchem-71 39 78     SPACE eurjchem-71 39 79 g g NOUN eurjchem-71 39 80 , , PUNCT eurjchem-71 39 81     SPACE eurjchem-71 39 82 0.01 0.01 NUM eurjchem-71 39 83     SPACE eurjchem-71 39 84 mole mole NOUN eurjchem-71 39 85 ) ) PUNCT eurjchem-71 39 86     SPACE eurjchem-71 39 87 and and CCONJ eurjchem-71 39 88     SPACE eurjchem-71 39 89 p‐chlorobenzylidene‐malononitrile p‐chlorobenzylidene‐malononitrile VERB eurjchem-71 39 90     SPACE eurjchem-71 39 91 ( ( PUNCT eurjchem-71 39 92 1.88 1.88 NUM eurjchem-71 39 93     SPACE eurjchem-71 39 94 g g NOUN eurjchem-71 39 95 , , PUNCT eurjchem-71 39 96     SPACE eurjchem-71 39 97 0.01 0.01 NUM eurjchem-71 39 98     SPACE eurjchem-71 39 99 mole mole NOUN eurjchem-71 39 100 ) ) PUNCT eurjchem-71 39 101     SPACE eurjchem-71 39 102 in in ADP eurjchem-71 39 103     SPACE eurjchem-71 39 104 50 50 NUM eurjchem-71 39 105     SPACE eurjchem-71 39 106 ml ml NOUN eurjchem-71 39 107     SPACE eurjchem-71 39 108 ethanol ethanol NOUN eurjchem-71 39 109     SPACE eurjchem-71 39 110 and and CCONJ eurjchem-71 39 111     SPACE eurjchem-71 39 112 drops drop VERB eurjchem-71 39 113     SPACE eurjchem-71 39 114 of of ADP eurjchem-71 39 115     SPACE eurjchem-71 39 116 piperidine piperidine NOUN eurjchem-71 39 117     SPACE eurjchem-71 39 118 was be AUX eurjchem-71 39 119     SPACE eurjchem-71 39 120 refluxed refluxe VERB eurjchem-71 39 121     SPACE eurjchem-71 39 122 for for ADP eurjchem-71 39 123     SPACE eurjchem-71 39 124 6 6 NUM eurjchem-71 39 125     SPACE eurjchem-71 39 126 h. h. NOUN eurjchem-71 39 127     SPACE eurjchem-71 39 128 after after ADP eurjchem-71 39 129     SPACE eurjchem-71 39 130 cooling cooling NOUN eurjchem-71 39 131 , , PUNCT eurjchem-71 39 132     SPACE eurjchem-71 39 133 the the DET eurjchem-71 39 134     SPACE eurjchem-71 39 135 reaction reaction NOUN eurjchem-71 39 136     SPACE eurjchem-71 39 137 mixture mixture NOUN eurjchem-71 39 138     SPACE eurjchem-71 39 139 was be AUX eurjchem-71 39 140     SPACE eurjchem-71 39 141 acidified acidify VERB eurjchem-71 39 142     SPACE eurjchem-71 39 143 with with ADP eurjchem-71 39 144     SPACE eurjchem-71 39 145 cold cold ADJ eurjchem-71 39 146     SPACE eurjchem-71 39 147 dilute dilute NOUN eurjchem-71 39 148     SPACE eurjchem-71 39 149 hydrochloric hydrochloric ADJ eurjchem-71 39 150     SPACE eurjchem-71 39 151 acid acid NOUN eurjchem-71 39 152 . . PUNCT eurjchem-71 39 153     SPACE eurjchem-71 40 1 the the DET eurjchem-71 40 2     SPACE eurjchem-71 40 3 precipitated precipitate VERB eurjchem-71 40 4     SPACE eurjchem-71 40 5 solid solid NOUN eurjchem-71 40 6     SPACE eurjchem-71 40 7 was be AUX eurjchem-71 40 8     SPACE eurjchem-71 40 9 collected collect VERB eurjchem-71 40 10     SPACE eurjchem-71 40 11 by by ADP eurjchem-71 40 12     SPACE eurjchem-71 40 13 filtration filtration NOUN eurjchem-71 40 14 , , PUNCT eurjchem-71 40 15     SPACE eurjchem-71 40 16 washed wash VERB eurjchem-71 40 17     SPACE eurjchem-71 40 18 with with ADP eurjchem-71 40 19     SPACE eurjchem-71 40 20 water water NOUN eurjchem-71 40 21 , , PUNCT eurjchem-71 40 22     SPACE eurjchem-71 40 23 dried dry VERB eurjchem-71 40 24     SPACE eurjchem-71 40 25 and and CCONJ eurjchem-71 40 26     SPACE eurjchem-71 40 27 then then ADV eurjchem-71 40 28     SPACE eurjchem-71 40 29 recrystallized recrystallize VERB eurjchem-71 40 30     SPACE eurjchem-71 40 31 from from ADP eurjchem-71 40 32     SPACE eurjchem-71 40 33 benzene benzene NOUN eurjchem-71 40 34 / / SYM eurjchem-71 40 35 ethanol ethanol NOUN eurjchem-71 40 36     SPACE eurjchem-71 40 37 to to PART eurjchem-71 40 38     SPACE eurjchem-71 40 39 give give VERB eurjchem-71 40 40     SPACE eurjchem-71 40 41 6 6 NUM eurjchem-71 40 42     SPACE eurjchem-71 40 43 as as ADP eurjchem-71 40 44     SPACE eurjchem-71 40 45 buff buff PROPN eurjchem-71 40 46     SPACE eurjchem-71 40 47 crystals crystal NOUN eurjchem-71 40 48 . . PUNCT eurjchem-71 40 49     SPACE eurjchem-71 41 1 m.p m.p PROPN eurjchem-71 41 2 . . PROPN eurjchem-71 41 3 : : PUNCT eurjchem-71 41 4     SPACE eurjchem-71 41 5 310‐ 310‐ NUM eurjchem-71 41 6 312oc 312oc PROPN eurjchem-71 41 7 , , PUNCT eurjchem-71 41 8     SPACE eurjchem-71 41 9 yield yield NOUN eurjchem-71 41 10     SPACE eurjchem-71 41 11 55 55 NUM eurjchem-71 41 12 % % NOUN eurjchem-71 41 13 . . PUNCT eurjchem-71 41 14     SPACE eurjchem-71 42 1 ir ir VERB eurjchem-71 42 2     SPACE eurjchem-71 42 3 ( ( PUNCT eurjchem-71 42 4 ν ν NOUN eurjchem-71 42 5 ): ): NOUN eurjchem-71 42 6     SPACE eurjchem-71 42 7 2220 2220 NUM eurjchem-71 42 8     SPACE eurjchem-71 42 9 cm‐1 cm‐1 NOUN eurjchem-71 42 10     SPACE eurjchem-71 42 11 ( ( PUNCT eurjchem-71 42 12 c≡n c≡n PROPN eurjchem-71 42 13 ) ) PUNCT eurjchem-71 42 14 , , PUNCT eurjchem-71 42 15     SPACE eurjchem-71 42 16 1672 1672 NUM eurjchem-71 42 17     SPACE eurjchem-71 42 18 cm‐1 cm‐1 NOUN eurjchem-71 42 19     SPACE eurjchem-71 42 20 ( ( PUNCT eurjchem-71 42 21 c c NOUN eurjchem-71 42 22 = = ADJ eurjchem-71 42 23 ocyclic ocyclic ADJ eurjchem-71 42 24     SPACE eurjchem-71 42 25 amide amide NOUN eurjchem-71 42 26 ) ) PUNCT eurjchem-71 42 27 . . PUNCT eurjchem-71 42 28     SPACE eurjchem-71 43 1 1h‐nmr 1h‐nmr NUM eurjchem-71 43 2     SPACE eurjchem-71 43 3 ( ( PUNCT eurjchem-71 43 4 dmso‐d6 dmso‐d6 NOUN eurjchem-71 43 5 ) ) PUNCT eurjchem-71 43 6     SPACE eurjchem-71 43 7 δ δ PROPN eurjchem-71 43 8     SPACE eurjchem-71 43 9 8.7‐7.2 8.7‐7.2 NUM eurjchem-71 43 10     SPACE eurjchem-71 43 11 ( ( PUNCT eurjchem-71 43 12 m m PROPN eurjchem-71 43 13 , , PUNCT eurjchem-71 43 14     SPACE eurjchem-71 43 15 11 11 NUM eurjchem-71 43 16     SPACE eurjchem-71 43 17 harom harom NOUN eurjchem-71 43 18 . . PUNCT eurjchem-71 43 19 ) ) PUNCT eurjchem-71 43 20 , , PUNCT eurjchem-71 43 21     SPACE eurjchem-71 43 22 6.9 6.9 NUM eurjchem-71 43 23     SPACE eurjchem-71 43 24 ( ( PUNCT eurjchem-71 43 25 s s PROPN eurjchem-71 43 26 , , PUNCT eurjchem-71 43 27     SPACE eurjchem-71 43 28 1h 1h NUM eurjchem-71 43 29 , , PUNCT eurjchem-71 43 30     SPACE eurjchem-71 43 31 ch= ch= NOUN eurjchem-71 43 32 ) ) PUNCT eurjchem-71 43 33 , , PUNCT eurjchem-71 43 34     SPACE eurjchem-71 43 35 4.08 4.08 NUM eurjchem-71 43 36     SPACE eurjchem-71 43 37 ( ( PUNCT eurjchem-71 43 38 d d PROPN eurjchem-71 43 39 , , PUNCT eurjchem-71 43 40     SPACE eurjchem-71 43 41 1h 1h NUM eurjchem-71 43 42 , , PUNCT eurjchem-71 43 43     SPACE eurjchem-71 43 44 cochcn cochcn NOUN eurjchem-71 43 45 ) ) PUNCT eurjchem-71 43 46 , , PUNCT eurjchem-71 43 47     SPACE eurjchem-71 43 48 3.9 3.9 NUM eurjchem-71 43 49     SPACE eurjchem-71 43 50 ( ( PUNCT eurjchem-71 43 51 s s PROPN eurjchem-71 43 52 , , PUNCT eurjchem-71 43 53     SPACE eurjchem-71 43 54 3h 3h NUM eurjchem-71 43 55 , , PUNCT eurjchem-71 43 56     SPACE eurjchem-71 43 57 ome ome NOUN eurjchem-71 43 58 ) ) PUNCT eurjchem-71 43 59 , , PUNCT eurjchem-71 43 60     SPACE eurjchem-71 43 61 3.82 3.82 NUM eurjchem-71 43 62     SPACE eurjchem-71 43 63 ( ( PUNCT eurjchem-71 43 64 s s PROPN eurjchem-71 43 65 , , PUNCT eurjchem-71 43 66     SPACE eurjchem-71 43 67 3h 3h NUM eurjchem-71 43 68 , , PUNCT eurjchem-71 43 69     SPACE eurjchem-71 43 70 ome ome NOUN eurjchem-71 43 71 ) ) PUNCT eurjchem-71 43 72 , , PUNCT eurjchem-71 43 73     SPACE eurjchem-71 43 74 3.66 3.66 NUM eurjchem-71 43 75     SPACE eurjchem-71 43 76 ( ( PUNCT eurjchem-71 43 77 d d PROPN eurjchem-71 43 78 , , PUNCT eurjchem-71 43 79     SPACE eurjchem-71 43 80 1h 1h NUM eurjchem-71 43 81 , , PUNCT eurjchem-71 43 82     SPACE eurjchem-71 43 83 ch ch NOUN eurjchem-71 43 84 ) ) PUNCT eurjchem-71 43 85 . . PUNCT eurjchem-71 43 86       SPACE eurjchem-71 44 1 ms ms NOUN eurjchem-71 44 2 : : PUNCT eurjchem-71 44 3     SPACE eurjchem-71 44 4 298 298 NUM eurjchem-71 44 5     SPACE eurjchem-71 44 6 ( ( PUNCT eurjchem-71 44 7 [ [ X eurjchem-71 44 8 m‐c17h12o3 m‐c17h12o3 X eurjchem-71 44 9 ] ] X eurjchem-71 44 10 , , PUNCT eurjchem-71 44 11     SPACE eurjchem-71 44 12 65.0 65.0 NUM eurjchem-71 44 13 ) ) PUNCT eurjchem-71 44 14 , , PUNCT eurjchem-71 44 15     SPACE eurjchem-71 44 16 265 265 NUM eurjchem-71 44 17     SPACE eurjchem-71 44 18 ( ( PUNCT eurjchem-71 44 19 83.3 83.3 NUM eurjchem-71 44 20 ) ) PUNCT eurjchem-71 44 21 , , PUNCT eurjchem-71 44 22     SPACE eurjchem-71 44 23 185 185 NUM eurjchem-71 44 24     SPACE eurjchem-71 44 25 ( ( PUNCT eurjchem-71 44 26 100 100 NUM eurjchem-71 44 27 ) ) PUNCT eurjchem-71 44 28 , , PUNCT eurjchem-71 44 29     SPACE eurjchem-71 44 30 129 129 NUM eurjchem-71 44 31     SPACE eurjchem-71 44 32 ( ( PUNCT eurjchem-71 44 33 40.8 40.8 NUM eurjchem-71 44 34 ) ) PUNCT eurjchem-71 44 35 , , PUNCT eurjchem-71 44 36     SPACE eurjchem-71 44 37 105 105 NUM eurjchem-71 44 38     SPACE eurjchem-71 44 39 ( ( PUNCT eurjchem-71 44 40 54.2 54.2 NUM eurjchem-71 44 41 ) ) PUNCT eurjchem-71 44 42 , , PUNCT eurjchem-71 44 43     SPACE eurjchem-71 44 44 78 78 NUM eurjchem-71 44 45     SPACE eurjchem-71 44 46 ( ( PUNCT eurjchem-71 44 47 25.0 25.0 NUM eurjchem-71 44 48 ) ) PUNCT eurjchem-71 44 49 , , PUNCT eurjchem-71 44 50     SPACE eurjchem-71 44 51 77 77 NUM eurjchem-71 44 52     SPACE eurjchem-71 44 53 ( ( PUNCT eurjchem-71 44 54 23.3 23.3 NUM eurjchem-71 44 55 ) ) PUNCT eurjchem-71 44 56 . . PUNCT eurjchem-71 44 57     SPACE eurjchem-71 45 1 anal anal ADJ eurjchem-71 45 2 . . PUNCT eurjchem-71 45 3     SPACE eurjchem-71 45 4 calcd calcd NOUN eurjchem-71 45 5 . . PUNCT eurjchem-71 45 6     SPACE eurjchem-71 46 1 for for ADP eurjchem-71 46 2     SPACE eurjchem-71 46 3 c31h20cln5o4 c31h20cln5o4 NOUN eurjchem-71 46 4     SPACE eurjchem-71 46 5 ( ( PUNCT eurjchem-71 46 6 561.97 561.97 NUM eurjchem-71 46 7 ): ): PUNCT eurjchem-71 46 8     SPACE eurjchem-71 46 9 c c NOUN eurjchem-71 46 10 , , PUNCT eurjchem-71 46 11     SPACE eurjchem-71 46 12 66.25; 66.25; VERB eurjchem-71 46 13     SPACE eurjchem-71 46 14 h h NOUN eurjchem-71 46 15 , , PUNCT eurjchem-71 46 16     SPACE eurjchem-71 46 17 3.59 3.59 NUM eurjchem-71 46 18 ; ; PUNCT eurjchem-71 46 19     SPACE eurjchem-71 46 20 cl cl NOUN eurjchem-71 46 21 , , PUNCT eurjchem-71 46 22     SPACE eurjchem-71 46 23 6.31 6.31 NUM eurjchem-71 46 24 ; ; PUNCT eurjchem-71 46 25     SPACE eurjchem-71 46 26 n n CCONJ eurjchem-71 46 27 , , PUNCT eurjchem-71 46 28     SPACE eurjchem-71 46 29 12.46 12.46 NUM eurjchem-71 46 30 . . PUNCT eurjchem-71 46 31     SPACE eurjchem-71 46 32 found find VERB eurjchem-71 46 33 : : PUNCT eurjchem-71 46 34     SPACE eurjchem-71 46 35 c c X eurjchem-71 46 36 , , PUNCT eurjchem-71 46 37     SPACE eurjchem-71 46 38 66.4; 66.4; NUM eurjchem-71 46 39     SPACE eurjchem-71 46 40 h h NOUN eurjchem-71 46 41 , , PUNCT eurjchem-71 46 42     SPACE eurjchem-71 46 43 3.36 3.36 NUM eurjchem-71 46 44 ; ; PUNCT eurjchem-71 46 45     SPACE eurjchem-71 46 46 cl cl NOUN eurjchem-71 46 47 , , PUNCT eurjchem-71 46 48     SPACE eurjchem-71 46 49 6.09 6.09 NUM eurjchem-71 46 50 ; ; PUNCT eurjchem-71 46 51     SPACE eurjchem-71 46 52 n n CCONJ eurjchem-71 46 53 , , PUNCT eurjchem-71 46 54     SPACE eurjchem-71 46 55 12.11 12.11 NUM eurjchem-71 46 56 . . PUNCT eurjchem-71 46 57         SPACE eurjchem-71 46 58 2.5 2.5 NUM eurjchem-71 46 59 . . PUNCT eurjchem-71 46 60     SPACE eurjchem-71 46 61 ( ( PUNCT eurjchem-71 46 62 e)­1­[4­(3,4­dimethoxybenzylidene)1,3­dioxo­3,4­ e)­1­[4­(3,4­dimethoxybenzylidene)1,3­dioxo­3,4­ VERB eurjchem-71 46 63 dihydroisoquinolin­2­(1h)­yl]­6­amino­2­oxo­1,2­ dihydroisoquinolin­2­(1h)­yl]­6­amino­2­oxo­1,2­ PROPN eurjchem-71 46 64 dihydropyridin­3,5­dicarbonitrile dihydropyridin­3,5­dicarbonitrile PROPN eurjchem-71 46 65     SPACE eurjchem-71 46 66 ( ( PUNCT eurjchem-71 46 67 7 7 NUM eurjchem-71 46 68 ) ) PUNCT eurjchem-71 46 69         SPACE eurjchem-71 46 70 a a DET eurjchem-71 46 71     SPACE eurjchem-71 46 72 mixture mixture NOUN eurjchem-71 46 73     SPACE eurjchem-71 46 74 of of ADP eurjchem-71 46 75     SPACE eurjchem-71 46 76 the the DET eurjchem-71 46 77     SPACE eurjchem-71 46 78 isoquinolin‐1,3‐dione isoquinolin‐1,3‐dione NOUN eurjchem-71 46 79     SPACE eurjchem-71 46 80 4 4 NUM eurjchem-71 46 81     SPACE eurjchem-71 46 82 ( ( PUNCT eurjchem-71 46 83 3.91 3.91 NUM eurjchem-71 46 84     SPACE eurjchem-71 46 85 g g NOUN eurjchem-71 46 86 , , PUNCT eurjchem-71 46 87     SPACE eurjchem-71 46 88 0.01 0.01 NUM eurjchem-71 46 89     SPACE eurjchem-71 46 90 mole mole NOUN eurjchem-71 46 91 ) ) PUNCT eurjchem-71 46 92     SPACE eurjchem-71 46 93 and and CCONJ eurjchem-71 46 94     SPACE eurjchem-71 46 95 ethoxymethylene‐malononitrile ethoxymethylene‐malononitrile PROPN eurjchem-71 46 96     SPACE eurjchem-71 46 97 ( ( PUNCT eurjchem-71 46 98 1.22 1.22 NUM eurjchem-71 46 99     SPACE eurjchem-71 46 100 g g NOUN eurjchem-71 46 101 , , PUNCT eurjchem-71 46 102     SPACE eurjchem-71 46 103 0.01 0.01 NUM eurjchem-71 46 104     SPACE eurjchem-71 46 105 mole mole NOUN eurjchem-71 46 106 ) ) PUNCT eurjchem-71 46 107     SPACE eurjchem-71 46 108 in in ADP eurjchem-71 46 109     SPACE eurjchem-71 46 110 50 50 NUM eurjchem-71 46 111     SPACE eurjchem-71 46 112 ml ml NOUN eurjchem-71 46 113     SPACE eurjchem-71 46 114 ethanol ethanol NOUN eurjchem-71 46 115     SPACE eurjchem-71 46 116 and and CCONJ eurjchem-71 46 117     SPACE eurjchem-71 46 118 drops drop NOUN eurjchem-71 46 119     SPACE eurjchem-71 46 120 of of ADP eurjchem-71 46 121     SPACE eurjchem-71 46 122 piperidine piperidine NOUN eurjchem-71 46 123     SPACE eurjchem-71 46 124 was be AUX eurjchem-71 46 125     SPACE eurjchem-71 46 126 refluxed refluxe VERB eurjchem-71 46 127     SPACE eurjchem-71 46 128 for for ADP eurjchem-71 46 129     SPACE eurjchem-71 46 130 6 6 NUM eurjchem-71 46 131     SPACE eurjchem-71 46 132 h. h. NOUN eurjchem-71 46 133     SPACE eurjchem-71 46 134 after after ADP eurjchem-71 46 135     SPACE eurjchem-71 46 136 cooling cooling NOUN eurjchem-71 46 137 , , PUNCT eurjchem-71 46 138     SPACE eurjchem-71 46 139 the the DET eurjchem-71 46 140     SPACE eurjchem-71 46 141 reaction reaction NOUN eurjchem-71 46 142     SPACE eurjchem-71 46 143 mixture mixture NOUN eurjchem-71 46 144     SPACE eurjchem-71 46 145 was be AUX eurjchem-71 46 146     SPACE eurjchem-71 46 147 acidified acidify VERB eurjchem-71 46 148     SPACE eurjchem-71 46 149 with with ADP eurjchem-71 46 150     SPACE eurjchem-71 46 151 cold cold ADJ eurjchem-71 46 152     SPACE eurjchem-71 46 153 dilute dilute NOUN eurjchem-71 46 154     SPACE eurjchem-71 46 155 hydrochloric hydrochloric ADJ eurjchem-71 46 156     SPACE eurjchem-71 46 157 acid acid NOUN eurjchem-71 46 158 . . PUNCT eurjchem-71 46 159     SPACE eurjchem-71 46 160 the the DET eurjchem-71 46 161     SPACE eurjchem-71 46 162 precipitate precipitate NOUN eurjchem-71 46 163     SPACE eurjchem-71 46 164 was be AUX eurjchem-71 46 165     SPACE eurjchem-71 46 166 collected collect VERB eurjchem-71 46 167     SPACE eurjchem-71 46 168 by by ADP eurjchem-71 46 169     SPACE eurjchem-71 46 170 filtration filtration NOUN eurjchem-71 46 171 , , PUNCT eurjchem-71 46 172     SPACE eurjchem-71 46 173 washed wash VERB eurjchem-71 46 174     SPACE eurjchem-71 46 175 with with ADP eurjchem-71 46 176     SPACE eurjchem-71 46 177 water water NOUN eurjchem-71 46 178 , , PUNCT eurjchem-71 46 179     SPACE eurjchem-71 46 180 dried dry VERB eurjchem-71 46 181     SPACE eurjchem-71 46 182 and and CCONJ eurjchem-71 46 183     SPACE eurjchem-71 46 184 then then ADV eurjchem-71 46 185     SPACE eurjchem-71 46 186 recrystallized recrystallize VERB eurjchem-71 46 187     SPACE eurjchem-71 46 188 from from ADP eurjchem-71 46 189     SPACE eurjchem-71 46 190 ethanol ethanol NOUN eurjchem-71 46 191     SPACE eurjchem-71 46 192 to to PART eurjchem-71 46 193     SPACE eurjchem-71 46 194 give give VERB eurjchem-71 46 195     SPACE eurjchem-71 46 196 7 7 NUM eurjchem-71 46 197     SPACE eurjchem-71 46 198 as as ADP eurjchem-71 46 199     SPACE eurjchem-71 46 200 brown brown ADJ eurjchem-71 46 201     SPACE eurjchem-71 46 202 crystals crystal NOUN eurjchem-71 46 203 . . PUNCT eurjchem-71 46 204     SPACE eurjchem-71 47 1 m.p m.p PROPN eurjchem-71 47 2 . . PROPN eurjchem-71 47 3 : : PUNCT eurjchem-71 47 4     SPACE eurjchem-71 47 5 200‐203oc 200‐203oc NUM eurjchem-71 47 6 , , PUNCT eurjchem-71 47 7     SPACE eurjchem-71 47 8 yield yield NOUN eurjchem-71 47 9     SPACE eurjchem-71 47 10 35 35 NUM eurjchem-71 47 11 % % NOUN eurjchem-71 47 12 . . PUNCT eurjchem-71 47 13     SPACE eurjchem-71 48 1 ir ir VERB eurjchem-71 48 2     SPACE eurjchem-71 48 3 ( ( PUNCT eurjchem-71 48 4 ν ν NOUN eurjchem-71 48 5 ): ): NOUN eurjchem-71 48 6     SPACE eurjchem-71 48 7 br br NOUN eurjchem-71 48 8 . . PUNCT eurjchem-71 48 9     SPACE eurjchem-71 48 10 3332 3332 NUM eurjchem-71 48 11     SPACE eurjchem-71 48 12 cm‐1 cm‐1 NOUN eurjchem-71 48 13     SPACE eurjchem-71 48 14 ( ( PUNCT eurjchem-71 48 15 nh nh NOUN eurjchem-71 48 16 ) ) PUNCT eurjchem-71 48 17 , , PUNCT eurjchem-71 48 18     SPACE eurjchem-71 48 19 2210 2210 NUM eurjchem-71 48 20     SPACE eurjchem-71 48 21 cm‐1 cm‐1 PROPN eurjchem-71 48 22     SPACE eurjchem-71 48 23 ( ( PUNCT eurjchem-71 48 24 c≡n c≡n PROPN eurjchem-71 48 25 ) ) PUNCT eurjchem-71 48 26 , , PUNCT eurjchem-71 48 27     SPACE eurjchem-71 48 28 1682 1682 NUM eurjchem-71 48 29     SPACE eurjchem-71 48 30 cm‐1 cm‐1 NOUN eurjchem-71 48 31     SPACE eurjchem-71 48 32 ( ( PUNCT eurjchem-71 48 33 c c NOUN eurjchem-71 48 34 = = NOUN eurjchem-71 48 35 o o NOUN eurjchem-71 48 36 ) ) PUNCT eurjchem-71 48 37 . . PUNCT eurjchem-71 48 38     SPACE eurjchem-71 49 1 1h‐nmr 1h‐nmr NUM eurjchem-71 49 2     SPACE eurjchem-71 49 3 ( ( PUNCT eurjchem-71 49 4 dmso‐d6 dmso‐d6 NOUN eurjchem-71 49 5 ) ) PUNCT eurjchem-71 49 6     SPACE eurjchem-71 49 7 δ δ PROPN eurjchem-71 49 8     SPACE eurjchem-71 49 9 8.8‐7.3 8.8‐7.3 PRON eurjchem-71 49 10     SPACE eurjchem-71 49 11 ( ( PUNCT eurjchem-71 49 12 m m PROPN eurjchem-71 49 13 , , PUNCT eurjchem-71 49 14     SPACE eurjchem-71 49 15 8harom 8harom NUM eurjchem-71 49 16 . . PUNCT eurjchem-71 49 17 ) ) PUNCT eurjchem-71 49 18 , , PUNCT eurjchem-71 49 19     SPACE eurjchem-71 49 20 7.0 7.0 NUM eurjchem-71 49 21     SPACE eurjchem-71 49 22 ( ( PUNCT eurjchem-71 49 23 s s PROPN eurjchem-71 49 24 , , PUNCT eurjchem-71 49 25     SPACE eurjchem-71 49 26 1h 1h NUM eurjchem-71 49 27 , , PUNCT eurjchem-71 49 28     SPACE eurjchem-71 49 29 olefinic olefinic ADJ eurjchem-71 49 30     SPACE eurjchem-71 49 31 h h NOUN eurjchem-71 49 32 ) ) PUNCT eurjchem-71 49 33 , , PUNCT eurjchem-71 49 34     SPACE eurjchem-71 49 35 3.9 3.9 NUM eurjchem-71 49 36     SPACE eurjchem-71 49 37 ( ( PUNCT eurjchem-71 49 38 s s PROPN eurjchem-71 49 39 , , PUNCT eurjchem-71 49 40     SPACE eurjchem-71 49 41 3h 3h NUM eurjchem-71 49 42 , , PUNCT eurjchem-71 49 43     SPACE eurjchem-71 49 44 ome ome NOUN eurjchem-71 49 45 ) ) PUNCT eurjchem-71 49 46 , , PUNCT eurjchem-71 49 47     SPACE eurjchem-71 49 48 3.76 3.76 NUM eurjchem-71 49 49     SPACE eurjchem-71 49 50 ( ( PUNCT eurjchem-71 49 51 s s PROPN eurjchem-71 49 52 , , PUNCT eurjchem-71 49 53     SPACE eurjchem-71 49 54 3h 3h NUM eurjchem-71 49 55 , , PUNCT eurjchem-71 49 56     SPACE eurjchem-71 49 57 ome ome NOUN eurjchem-71 49 58 ) ) PUNCT eurjchem-71 49 59 , , PUNCT eurjchem-71 49 60     SPACE eurjchem-71 49 61 3.0 3.0 NUM eurjchem-71 49 62     SPACE eurjchem-71 49 63 ( ( PUNCT eurjchem-71 49 64 br.s br.s PROPN eurjchem-71 49 65 , , PUNCT eurjchem-71 49 66     SPACE eurjchem-71 49 67 2h 2h NUM eurjchem-71 49 68 , , PUNCT eurjchem-71 49 69     SPACE eurjchem-71 49 70 nh2 nh2 PROPN eurjchem-71 49 71 , , PUNCT eurjchem-71 49 72     SPACE eurjchem-71 49 73 exchangeable exchangeable ADJ eurjchem-71 49 74     SPACE eurjchem-71 49 75 with with ADP eurjchem-71 49 76     SPACE eurjchem-71 49 77 d2o d2o NOUN eurjchem-71 49 78 ) ) PUNCT eurjchem-71 49 79 . . PUNCT eurjchem-71 49 80     SPACE eurjchem-71 50 1 ms ms NOUN eurjchem-71 50 2 : : PUNCT eurjchem-71 50 3     SPACE eurjchem-71 50 4 329 329 NUM eurjchem-71 50 5     SPACE eurjchem-71 50 6 ( ( PUNCT eurjchem-71 50 7 [ [ X eurjchem-71 50 8 m‐ar m‐ar ADJ eurjchem-71 50 9 . . PROPN eurjchem-71 50 10 , , PUNCT eurjchem-71 50 11     SPACE eurjchem-71 50 12 ‐h ‐h PROPN eurjchem-71 50 13 . . PROPN eurjchem-71 50 14 ] ] X eurjchem-71 50 15 , , PUNCT eurjchem-71 50 16     SPACE eurjchem-71 50 17 67.9 67.9 NUM eurjchem-71 50 18 ) ) PUNCT eurjchem-71 50 19 , , PUNCT eurjchem-71 50 20     SPACE eurjchem-71 50 21 328 328 NUM eurjchem-71 50 22     SPACE eurjchem-71 50 23 ( ( PUNCT eurjchem-71 50 24 100 100 NUM eurjchem-71 50 25 ) ) PUNCT eurjchem-71 50 26 , , PUNCT eurjchem-71 50 27     SPACE eurjchem-71 50 28 302 302 NUM eurjchem-71 50 29     SPACE eurjchem-71 50 30 ( ( PUNCT eurjchem-71 50 31 29.9 29.9 NUM eurjchem-71 50 32 ) ) PUNCT eurjchem-71 50 33 , , PUNCT eurjchem-71 50 34     SPACE eurjchem-71 50 35 301 301 NUM eurjchem-71 50 36     SPACE eurjchem-71 50 37 ( ( PUNCT eurjchem-71 50 38 77.4 77.4 NUM eurjchem-71 50 39 ) ) PUNCT eurjchem-71 50 40 , , PUNCT eurjchem-71 50 41     SPACE eurjchem-71 50 42 247 247 NUM eurjchem-71 50 43     SPACE eurjchem-71 50 44 ( ( PUNCT eurjchem-71 50 45 67.9 67.9 NUM eurjchem-71 50 46 ) ) PUNCT eurjchem-71 50 47 , , PUNCT eurjchem-71 50 48     SPACE eurjchem-71 50 49 151 151 NUM eurjchem-71 50 50     SPACE eurjchem-71 50 51 ( ( PUNCT eurjchem-71 50 52 59.9 59.9 NUM eurjchem-71 50 53 ) ) PUNCT eurjchem-71 50 54 , , PUNCT eurjchem-71 50 55     SPACE eurjchem-71 50 56 91 91 NUM eurjchem-71 50 57     SPACE eurjchem-71 50 58 ( ( PUNCT eurjchem-71 50 59 17.7 17.7 NUM eurjchem-71 50 60 ) ) PUNCT eurjchem-71 50 61 , , PUNCT eurjchem-71 50 62     SPACE eurjchem-71 50 63 65 65 NUM eurjchem-71 50 64     SPACE eurjchem-71 50 65 ( ( PUNCT eurjchem-71 50 66 13.4 13.4 NUM eurjchem-71 50 67 ) ) PUNCT eurjchem-71 50 68 . . PUNCT eurjchem-71 50 69     SPACE eurjchem-71 51 1 anal anal ADJ eurjchem-71 51 2 . . PUNCT eurjchem-71 51 3     SPACE eurjchem-71 51 4 calcd calcd NOUN eurjchem-71 51 5 . . PUNCT eurjchem-71 51 6     SPACE eurjchem-71 51 7 for for ADP eurjchem-71 51 8     SPACE eurjchem-71 51 9 c25h17n5o5 c25h17n5o5 NOUN eurjchem-71 51 10     SPACE eurjchem-71 51 11 ( ( PUNCT eurjchem-71 51 12 467.43 467.43 NUM eurjchem-71 51 13 ): ): PUNCT eurjchem-71 51 14     SPACE eurjchem-71 51 15 c c NOUN eurjchem-71 51 16 , , PUNCT eurjchem-71 51 17     SPACE eurjchem-71 51 18 64.24; 64.24; NOUN eurjchem-71 51 19     SPACE eurjchem-71 51 20 h h NOUN eurjchem-71 51 21 , , PUNCT eurjchem-71 51 22     SPACE eurjchem-71 51 23 3.67 3.67 NUM eurjchem-71 51 24 ; ; PUNCT eurjchem-71 51 25     SPACE eurjchem-71 51 26 n n CCONJ eurjchem-71 51 27 , , PUNCT eurjchem-71 51 28     SPACE eurjchem-71 51 29 14.98 14.98 NUM eurjchem-71 51 30 . . PUNCT eurjchem-71 51 31     SPACE eurjchem-71 51 32 found find VERB eurjchem-71 51 33 : : PUNCT eurjchem-71 51 34     SPACE eurjchem-71 51 35 c c X eurjchem-71 51 36 , , PUNCT eurjchem-71 51 37     SPACE eurjchem-71 51 38 64.2; 64.2; NOUN eurjchem-71 51 39     SPACE eurjchem-71 51 40 h h NOUN eurjchem-71 51 41 , , PUNCT eurjchem-71 51 42     SPACE eurjchem-71 51 43 3.53 3.53 NUM eurjchem-71 51 44 ; ; PUNCT eurjchem-71 51 45     SPACE eurjchem-71 51 46 n n CCONJ eurjchem-71 51 47 , , PUNCT eurjchem-71 51 48     SPACE eurjchem-71 51 49 14.66 14.66 NUM eurjchem-71 51 50 . . PUNCT eurjchem-71 51 51         SPACE eurjchem-71 51 52 2.6 2.6 NUM eurjchem-71 51 53 . . PUNCT eurjchem-71 51 54     SPACE eurjchem-71 51 55 ( ( PUNCT eurjchem-71 51 56 e)­2­(2­(cyclohexylcarbamoyl)phenyl)­3­(3,4­ e)­2­(2­(cyclohexylcarbamoyl)phenyl)­3­(3,4­ PROPN eurjchem-71 51 57 dimethoxyphenyl)acrylic dimethoxyphenyl)acrylic NOUN eurjchem-71 51 58     SPACE eurjchem-71 51 59 acid acid NOUN eurjchem-71 51 60     SPACE eurjchem-71 51 61 ( ( PUNCT eurjchem-71 51 62 8) 8) NUM eurjchem-71 51 63         SPACE eurjchem-71 51 64 a a DET eurjchem-71 51 65     SPACE eurjchem-71 51 66 mixture mixture NOUN eurjchem-71 51 67     SPACE eurjchem-71 51 68 of of ADP eurjchem-71 51 69     SPACE eurjchem-71 51 70 compound compound NOUN eurjchem-71 51 71     SPACE eurjchem-71 51 72 2 2 NUM eurjchem-71 51 73     SPACE eurjchem-71 51 74 ( ( PUNCT eurjchem-71 51 75 3.1 3.1 NUM eurjchem-71 51 76     SPACE eurjchem-71 51 77 g g NOUN eurjchem-71 51 78 , , PUNCT eurjchem-71 51 79     SPACE eurjchem-71 51 80 0.01 0.01 NUM eurjchem-71 51 81     SPACE eurjchem-71 51 82 mole mole NOUN eurjchem-71 51 83 ) ) PUNCT eurjchem-71 51 84     SPACE eurjchem-71 51 85 and and CCONJ eurjchem-71 51 86     SPACE eurjchem-71 51 87 cyclohexyl cyclohexyl NOUN eurjchem-71 51 88     SPACE eurjchem-71 51 89 amine amine NOUN eurjchem-71 51 90     SPACE eurjchem-71 51 91 ( ( PUNCT eurjchem-71 51 92 0.99 0.99 NUM eurjchem-71 51 93     SPACE eurjchem-71 51 94 ml ml NOUN eurjchem-71 51 95 , , PUNCT eurjchem-71 51 96     SPACE eurjchem-71 51 97 0.01 0.01 NUM eurjchem-71 51 98     SPACE eurjchem-71 51 99 mole mole NOUN eurjchem-71 51 100 ) ) PUNCT eurjchem-71 51 101     SPACE eurjchem-71 51 102 in in ADP eurjchem-71 51 103     SPACE eurjchem-71 51 104 30 30 NUM eurjchem-71 51 105     SPACE eurjchem-71 51 106 ml ml NOUN eurjchem-71 51 107     SPACE eurjchem-71 51 108 dioxane dioxane NOUN eurjchem-71 51 109     SPACE eurjchem-71 51 110 was be AUX eurjchem-71 51 111     SPACE eurjchem-71 51 112 refluxed refluxe VERB eurjchem-71 51 113     SPACE eurjchem-71 51 114 for for ADP eurjchem-71 51 115     SPACE eurjchem-71 51 116 3 3 NUM eurjchem-71 51 117     SPACE eurjchem-71 51 118 h. h. NOUN eurjchem-71 51 119     SPACE eurjchem-71 51 120 after after ADP eurjchem-71 51 121     SPACE eurjchem-71 51 122 concentration concentration NOUN eurjchem-71 51 123     SPACE eurjchem-71 51 124 of of ADP eurjchem-71 51 125     SPACE eurjchem-71 51 126 the the DET eurjchem-71 51 127     SPACE eurjchem-71 51 128 solvent solvent NOUN eurjchem-71 51 129 , , PUNCT eurjchem-71 51 130     SPACE eurjchem-71 51 131 a a DET eurjchem-71 51 132     SPACE eurjchem-71 51 133 yellowish yellowish NOUN eurjchem-71 51 134     SPACE eurjchem-71 51 135 white white ADJ eurjchem-71 51 136     SPACE eurjchem-71 51 137 solid solid NOUN eurjchem-71 51 138     SPACE eurjchem-71 51 139 was be AUX eurjchem-71 51 140     SPACE eurjchem-71 51 141 deposited deposit VERB eurjchem-71 51 142     SPACE eurjchem-71 51 143 then then ADV eurjchem-71 51 144     SPACE eurjchem-71 51 145 filtered filter VERB eurjchem-71 51 146     SPACE eurjchem-71 51 147 off off ADP eurjchem-71 51 148 , , PUNCT eurjchem-71 51 149     SPACE eurjchem-71 51 150 washed wash VERB eurjchem-71 51 151     SPACE eurjchem-71 51 152 with with ADP eurjchem-71 51 153     SPACE eurjchem-71 51 154 ethanol ethanol NOUN eurjchem-71 51 155 , , PUNCT eurjchem-71 51 156     SPACE eurjchem-71 51 157 dried dry VERB eurjchem-71 51 158     SPACE eurjchem-71 51 159 and and CCONJ eurjchem-71 51 160     SPACE eurjchem-71 51 161 recrystallized recrystallize VERB eurjchem-71 51 162     SPACE eurjchem-71 51 163 from from ADP eurjchem-71 51 164     SPACE eurjchem-71 51 165 ethanol ethanol NOUN eurjchem-71 51 166     SPACE eurjchem-71 51 167 to to PART eurjchem-71 51 168     SPACE eurjchem-71 51 169 give give VERB eurjchem-71 51 170     SPACE eurjchem-71 51 171 8 8 NUM eurjchem-71 51 172     SPACE eurjchem-71 51 173 as as ADP eurjchem-71 51 174     SPACE eurjchem-71 51 175 yellowish yellowish VERB eurjchem-71 51 176     SPACE eurjchem-71 51 177 white white ADJ eurjchem-71 51 178     SPACE eurjchem-71 51 179 crystals crystal NOUN eurjchem-71 51 180 . . PUNCT eurjchem-71 51 181     SPACE eurjchem-71 52 1 m.p m.p PROPN eurjchem-71 52 2 . . PROPN eurjchem-71 52 3 : : PUNCT eurjchem-71 52 4     SPACE eurjchem-71 52 5 162‐164oc 162‐164oc NUM eurjchem-71 52 6 , , PUNCT eurjchem-71 52 7     SPACE eurjchem-71 52 8 yield yield NOUN eurjchem-71 52 9     SPACE eurjchem-71 52 10 70 70 NUM eurjchem-71 52 11 % % NOUN eurjchem-71 52 12 . . PUNCT eurjchem-71 52 13     SPACE eurjchem-71 53 1 ir ir VERB eurjchem-71 53 2     SPACE eurjchem-71 53 3 ( ( PUNCT eurjchem-71 53 4 ν ν NOUN eurjchem-71 53 5 ): ): NOUN eurjchem-71 53 6     SPACE eurjchem-71 53 7 br br PROPN eurjchem-71 53 8 . . PUNCT eurjchem-71 53 9     SPACE eurjchem-71 53 10 nh nh PROPN eurjchem-71 53 11 , , PUNCT eurjchem-71 53 12     SPACE eurjchem-71 53 13 oh oh VERB eurjchem-71 53 14     SPACE eurjchem-71 53 15 centered center VERB eurjchem-71 53 16     SPACE eurjchem-71 53 17 at at ADP eurjchem-71 53 18     SPACE eurjchem-71 53 19 3309 3309 NUM eurjchem-71 53 20     SPACE eurjchem-71 53 21 cm‐1 cm‐1 NOUN eurjchem-71 53 22 , , PUNCT eurjchem-71 53 23     SPACE eurjchem-71 53 24 1707 1707 NUM eurjchem-71 53 25     SPACE eurjchem-71 53 26 cm‐1 cm‐1 NOUN eurjchem-71 53 27     SPACE eurjchem-71 53 28 ( ( PUNCT eurjchem-71 53 29 c c NOUN eurjchem-71 53 30 = = NOUN eurjchem-71 53 31 oacid oacid NOUN eurjchem-71 53 32 ) ) PUNCT eurjchem-71 53 33 , , PUNCT eurjchem-71 53 34     SPACE eurjchem-71 53 35 1640 1640 NUM eurjchem-71 53 36     SPACE eurjchem-71 53 37 cm‐1 cm‐1 NOUN eurjchem-71 53 38     SPACE eurjchem-71 53 39 ( ( PUNCT eurjchem-71 53 40 c c NOUN eurjchem-71 53 41 = = NOUN eurjchem-71 53 42 oamide oamide ADV eurjchem-71 53 43 ) ) PUNCT eurjchem-71 53 44 . . PUNCT eurjchem-71 53 45     SPACE eurjchem-71 54 1 1h‐nmr 1h‐nmr NUM eurjchem-71 54 2     SPACE eurjchem-71 54 3 ( ( PUNCT eurjchem-71 54 4 cdcl3 cdcl3 PROPN eurjchem-71 54 5 ) ) PUNCT eurjchem-71 54 6     SPACE eurjchem-71 54 7 δ δ PROPN eurjchem-71 54 8     SPACE eurjchem-71 54 9 11.6 11.6 NUM eurjchem-71 54 10     SPACE eurjchem-71 54 11 ( ( PUNCT eurjchem-71 54 12 br.s br.s PROPN eurjchem-71 54 13 , , PUNCT eurjchem-71 54 14     SPACE eurjchem-71 54 15 1h 1h NUM eurjchem-71 54 16 , , PUNCT eurjchem-71 54 17     SPACE eurjchem-71 54 18 cooh cooh NOUN eurjchem-71 54 19 ) ) PUNCT eurjchem-71 54 20 , , PUNCT eurjchem-71 54 21     SPACE eurjchem-71 54 22 9.2‐9.4 9.2‐9.4 NUM eurjchem-71 54 23     SPACE eurjchem-71 54 24 ( ( PUNCT eurjchem-71 54 25 br.s br.s PROPN eurjchem-71 54 26 , , PUNCT eurjchem-71 54 27     SPACE eurjchem-71 54 28 2h 2h NUM eurjchem-71 54 29 , , PUNCT eurjchem-71 54 30     SPACE eurjchem-71 54 31 exchangeable exchangeable ADJ eurjchem-71 54 32     SPACE eurjchem-71 54 33 with with ADP eurjchem-71 54 34     SPACE eurjchem-71 54 35 d2o d2o NOUN eurjchem-71 54 36 ) ) PUNCT eurjchem-71 54 37 , , PUNCT eurjchem-71 54 38     SPACE eurjchem-71 54 39 8.3‐6.4 8.3‐6.4 NUM eurjchem-71 54 40     SPACE eurjchem-71 54 41 ( ( PUNCT eurjchem-71 54 42 m m PROPN eurjchem-71 54 43 , , PUNCT eurjchem-71 54 44     SPACE eurjchem-71 54 45 7harom 7harom NUM eurjchem-71 54 46 . . PUNCT eurjchem-71 54 47 ) ) PUNCT eurjchem-71 54 48 , , PUNCT eurjchem-71 54 49     SPACE eurjchem-71 54 50 5.8 5.8 NUM eurjchem-71 54 51     SPACE eurjchem-71 54 52 ( ( PUNCT eurjchem-71 54 53 s s PROPN eurjchem-71 54 54 , , PUNCT eurjchem-71 54 55     SPACE eurjchem-71 54 56 1h 1h NUM eurjchem-71 54 57 , , PUNCT eurjchem-71 54 58     SPACE eurjchem-71 54 59 olefinic olefinic ADJ eurjchem-71 54 60     SPACE eurjchem-71 54 61 h h NOUN eurjchem-71 54 62 ) ) PUNCT eurjchem-71 54 63 , , PUNCT eurjchem-71 54 64     SPACE eurjchem-71 54 65 3.7 3.7 NUM eurjchem-71 54 66     SPACE eurjchem-71 54 67 ( ( PUNCT eurjchem-71 54 68 s s PROPN eurjchem-71 54 69 , , PUNCT eurjchem-71 54 70     SPACE eurjchem-71 54 71 6h 6h NOUN eurjchem-71 54 72 , , PUNCT eurjchem-71 54 73     SPACE eurjchem-71 54 74 2ome 2ome NUM eurjchem-71 54 75 ) ) PUNCT eurjchem-71 54 76     SPACE eurjchem-71 54 77 and and CCONJ eurjchem-71 54 78     SPACE eurjchem-71 54 79 1.8‐0.96 1.8‐0.96 NUM eurjchem-71 54 80     SPACE eurjchem-71 54 81 ( ( PUNCT eurjchem-71 54 82 m m PROPN eurjchem-71 54 83 , , PUNCT eurjchem-71 54 84     SPACE eurjchem-71 54 85 11h 11h NOUN eurjchem-71 54 86 , , PUNCT eurjchem-71 54 87     SPACE eurjchem-71 54 88 c6h11‐ c6h11‐ PROPN eurjchem-71 54 89 ) ) PUNCT eurjchem-71 54 90 . . PUNCT eurjchem-71 54 91     SPACE eurjchem-71 55 1 ms ms NOUN eurjchem-71 55 2 : : PUNCT eurjchem-71 55 3     SPACE eurjchem-71 55 4 409 409 NUM eurjchem-71 55 5     SPACE eurjchem-71 55 6 ( ( PUNCT eurjchem-71 55 7 4.5 4.5 NUM eurjchem-71 55 8 ) ) PUNCT eurjchem-71 55 9 , , PUNCT eurjchem-71 55 10     SPACE eurjchem-71 55 11 311 311 NUM eurjchem-71 55 12     SPACE eurjchem-71 55 13 ( ( PUNCT eurjchem-71 55 14 5.6 5.6 NUM eurjchem-71 55 15 ) ) PUNCT eurjchem-71 55 16 , , PUNCT eurjchem-71 55 17     SPACE eurjchem-71 55 18 310 310 NUM eurjchem-71 55 19     SPACE eurjchem-71 55 20 ( ( PUNCT eurjchem-71 55 21 20.5 20.5 NUM eurjchem-71 55 22 ) ) PUNCT eurjchem-71 55 23 , , PUNCT eurjchem-71 55 24     SPACE eurjchem-71 55 25 295 295 NUM eurjchem-71 55 26     SPACE eurjchem-71 55 27 ( ( PUNCT eurjchem-71 55 28 3.4 3.4 NUM eurjchem-71 55 29 ) ) PUNCT eurjchem-71 55 30 , , PUNCT eurjchem-71 55 31     SPACE eurjchem-71 55 32 222 222 NUM eurjchem-71 55 33     SPACE eurjchem-71 55 34 ( ( PUNCT eurjchem-71 55 35 4.7 4.7 NUM eurjchem-71 55 36 ) ) PUNCT eurjchem-71 55 37 , , PUNCT eurjchem-71 55 38     SPACE eurjchem-71 55 39 165 165 NUM eurjchem-71 55 40     SPACE eurjchem-71 55 41 ( ( PUNCT eurjchem-71 55 42 10.8 10.8 NUM eurjchem-71 55 43 ) ) PUNCT eurjchem-71 55 44 , , PUNCT eurjchem-71 55 45     SPACE eurjchem-71 55 46 151 151 NUM eurjchem-71 55 47     SPACE eurjchem-71 55 48 ( ( PUNCT eurjchem-71 55 49 33.0 33.0 NUM eurjchem-71 55 50 ) ) PUNCT eurjchem-71 55 51 , , PUNCT eurjchem-71 55 52     SPACE eurjchem-71 55 53 98 98 NUM eurjchem-71 55 54     SPACE eurjchem-71 55 55 ( ( PUNCT eurjchem-71 55 56 9.2 9.2 NUM eurjchem-71 55 57 ) ) PUNCT eurjchem-71 55 58 , , PUNCT eurjchem-71 55 59     SPACE eurjchem-71 55 60 89 89 NUM eurjchem-71 55 61     SPACE eurjchem-71 55 62 ( ( PUNCT eurjchem-71 55 63 8.5 8.5 NUM eurjchem-71 55 64 ) ) PUNCT eurjchem-71 55 65 , , PUNCT eurjchem-71 55 66     SPACE eurjchem-71 55 67 56 56 NUM eurjchem-71 55 68     SPACE eurjchem-71 55 69 ( ( PUNCT eurjchem-71 55 70 100 100 NUM eurjchem-71 55 71 ) ) PUNCT eurjchem-71 55 72 . . PUNCT eurjchem-71 55 73     SPACE eurjchem-71 56 1 anal anal ADJ eurjchem-71 56 2 . . PUNCT eurjchem-71 56 3     SPACE eurjchem-71 56 4 calcd calcd NOUN eurjchem-71 56 5 . . PUNCT eurjchem-71 56 6     SPACE eurjchem-71 56 7 for for ADP eurjchem-71 56 8     SPACE eurjchem-71 56 9 c24h27no5 c24h27no5 NOUN eurjchem-71 56 10     SPACE eurjchem-71 56 11 ( ( PUNCT eurjchem-71 56 12 409.47 409.47 NUM eurjchem-71 56 13 ): ): PUNCT eurjchem-71 56 14     SPACE eurjchem-71 56 15 c c NOUN eurjchem-71 56 16 , , PUNCT eurjchem-71 56 17     SPACE eurjchem-71 56 18 70.40; 70.40; NUM eurjchem-71 56 19     SPACE eurjchem-71 56 20 h h NOUN eurjchem-71 56 21 , , PUNCT eurjchem-71 56 22     SPACE eurjchem-71 56 23 6.65 6.65 NUM eurjchem-71 56 24 ; ; PUNCT eurjchem-71 56 25     SPACE eurjchem-71 56 26 n n CCONJ eurjchem-71 56 27 , , PUNCT eurjchem-71 56 28     SPACE eurjchem-71 56 29 3.42 3.42 NUM eurjchem-71 56 30 . . PUNCT eurjchem-71 56 31     SPACE eurjchem-71 56 32 found find VERB eurjchem-71 56 33 : : PUNCT eurjchem-71 56 34     SPACE eurjchem-71 56 35 c c X eurjchem-71 56 36 , , PUNCT eurjchem-71 56 37     SPACE eurjchem-71 56 38 70.36 70.36 NUM eurjchem-71 56 39 ; ; PUNCT eurjchem-71 56 40     SPACE eurjchem-71 56 41 h h NOUN eurjchem-71 56 42 , , PUNCT eurjchem-71 56 43     SPACE eurjchem-71 56 44 6.41 6.41 NUM eurjchem-71 56 45 ; ; PUNCT eurjchem-71 56 46     SPACE eurjchem-71 56 47 n n CCONJ eurjchem-71 56 48 , , PUNCT eurjchem-71 56 49     SPACE eurjchem-71 56 50 3.5 3.5 NUM eurjchem-71 56 51 . . PUNCT eurjchem-71 56 52         SPACE eurjchem-71 56 53 2.7 2.7 NUM eurjchem-71 56 54 . . PUNCT eurjchem-71 56 55     SPACE eurjchem-71 57 1 ( ( PUNCT eurjchem-71 57 2 e)­4­(3,4­dimethoxybenzylidene)­2­cyclohexyl e)­4­(3,4­dimethoxybenzylidene)­2­cyclohexyl X eurjchem-71 57 3     SPACE eurjchem-71 57 4 isoquinoline­1,3(2h,4h)­dione isoquinoline­1,3(2h,4h)­dione PROPN eurjchem-71 57 5     SPACE eurjchem-71 57 6 ( ( PUNCT eurjchem-71 57 7 9 9 NUM eurjchem-71 57 8 ) ) PUNCT eurjchem-71 57 9         SPACE eurjchem-71 57 10 a a DET eurjchem-71 57 11     SPACE eurjchem-71 57 12 mixture mixture NOUN eurjchem-71 57 13     SPACE eurjchem-71 57 14 of of ADP eurjchem-71 57 15     SPACE eurjchem-71 57 16 8 8 NUM eurjchem-71 57 17     SPACE eurjchem-71 57 18 ( ( PUNCT eurjchem-71 57 19 4.1 4.1 NUM eurjchem-71 57 20     SPACE eurjchem-71 57 21 g g NOUN eurjchem-71 57 22 , , PUNCT eurjchem-71 57 23     SPACE eurjchem-71 57 24 0.01 0.01 NUM eurjchem-71 57 25     SPACE eurjchem-71 57 26 mole mole NOUN eurjchem-71 57 27 ) ) PUNCT eurjchem-71 57 28     SPACE eurjchem-71 57 29 and and CCONJ eurjchem-71 57 30     SPACE eurjchem-71 57 31 freshly freshly ADV eurjchem-71 57 32     SPACE eurjchem-71 57 33 distilled distil VERB eurjchem-71 57 34     SPACE eurjchem-71 57 35 acetic acetic ADJ eurjchem-71 57 36     SPACE eurjchem-71 57 37 anhydride anhydride NOUN eurjchem-71 57 38     SPACE eurjchem-71 57 39 ( ( PUNCT eurjchem-71 57 40 20 20 NUM eurjchem-71 57 41     SPACE eurjchem-71 57 42 ml ml NOUN eurjchem-71 57 43 ) ) PUNCT eurjchem-71 57 44     SPACE eurjchem-71 57 45 was be AUX eurjchem-71 57 46     SPACE eurjchem-71 57 47 refluxed refluxe VERB eurjchem-71 57 48     SPACE eurjchem-71 57 49 for for ADP eurjchem-71 57 50     SPACE eurjchem-71 57 51 2 2 NUM eurjchem-71 57 52     SPACE eurjchem-71 57 53 h. h. NOUN eurjchem-71 57 54     SPACE eurjchem-71 57 55 the the DET eurjchem-71 57 56     SPACE eurjchem-71 57 57 reaction reaction NOUN eurjchem-71 57 58     SPACE eurjchem-71 57 59 mixture mixture NOUN eurjchem-71 57 60     SPACE eurjchem-71 57 61 was be AUX eurjchem-71 57 62     SPACE eurjchem-71 57 63 allowed allow VERB eurjchem-71 57 64     SPACE eurjchem-71 57 65 to to PART eurjchem-71 57 66     SPACE eurjchem-71 57 67 cool cool VERB eurjchem-71 57 68     SPACE eurjchem-71 57 69 then then ADV eurjchem-71 57 70     SPACE eurjchem-71 57 71 poured pour VERB eurjchem-71 57 72     SPACE eurjchem-71 57 73 on on ADP eurjchem-71 57 74     SPACE eurjchem-71 57 75 ice‐cold ice‐cold VERB eurjchem-71 57 76     SPACE eurjchem-71 57 77 water water NOUN eurjchem-71 57 78 . . PUNCT eurjchem-71 57 79     SPACE eurjchem-71 58 1 the the DET eurjchem-71 58 2     SPACE eurjchem-71 58 3 deposited deposit VERB eurjchem-71 58 4     SPACE eurjchem-71 58 5 solid solid NOUN eurjchem-71 58 6     SPACE eurjchem-71 58 7 was be AUX eurjchem-71 58 8     SPACE eurjchem-71 58 9 filtered filter VERB eurjchem-71 58 10     SPACE eurjchem-71 58 11 off off ADP eurjchem-71 58 12 , , PUNCT eurjchem-71 58 13     SPACE eurjchem-71 58 14 washed wash VERB eurjchem-71 58 15     SPACE eurjchem-71 58 16 several several ADJ eurjchem-71 58 17     SPACE eurjchem-71 58 18 times time NOUN eurjchem-71 58 19     SPACE eurjchem-71 58 20 with with ADP eurjchem-71 58 21     SPACE eurjchem-71 58 22 water water NOUN eurjchem-71 58 23 , , PUNCT eurjchem-71 58 24     SPACE eurjchem-71 58 25 dried dry VERB eurjchem-71 58 26     SPACE eurjchem-71 58 27 and and CCONJ eurjchem-71 58 28     SPACE eurjchem-71 58 29 then then ADV eurjchem-71 58 30     SPACE eurjchem-71 58 31 recrystallized recrystallize VERB eurjchem-71 58 32     SPACE eurjchem-71 58 33 from from ADP eurjchem-71 58 34     SPACE eurjchem-71 58 35 benzene benzene NOUN eurjchem-71 58 36     SPACE eurjchem-71 58 37 to to PART eurjchem-71 58 38     SPACE eurjchem-71 58 39 give give VERB eurjchem-71 58 40     SPACE eurjchem-71 58 41 9 9 NUM eurjchem-71 58 42     SPACE eurjchem-71 58 43 as as ADV eurjchem-71 58 44     SPACE eurjchem-71 58 45 orange orange ADJ eurjchem-71 58 46     SPACE eurjchem-71 58 47 crystals crystal NOUN eurjchem-71 58 48 . . PUNCT eurjchem-71 58 49     SPACE eurjchem-71 59 1 m.p m.p PROPN eurjchem-71 59 2 . . PROPN eurjchem-71 59 3 : : PUNCT eurjchem-71 59 4     SPACE eurjchem-71 59 5 162‐4oc 162‐4oc NUM eurjchem-71 59 6 , , PUNCT eurjchem-71 59 7     SPACE eurjchem-71 59 8 yield yield NOUN eurjchem-71 59 9     SPACE eurjchem-71 59 10 80 80 NUM eurjchem-71 59 11 % % NOUN eurjchem-71 59 12 . . PUNCT eurjchem-71 59 13     SPACE eurjchem-71 60 1 ir ir VERB eurjchem-71 60 2     SPACE eurjchem-71 60 3 ( ( PUNCT eurjchem-71 60 4 ν ν NOUN eurjchem-71 60 5 ): ): NOUN eurjchem-71 60 6     SPACE eurjchem-71 60 7 1759 1759 NUM eurjchem-71 60 8 , , PUNCT eurjchem-71 60 9     SPACE eurjchem-71 60 10 1723 1723 NUM eurjchem-71 60 11     SPACE eurjchem-71 60 12 cm‐1 cm‐1 NOUN eurjchem-71 60 13     SPACE eurjchem-71 60 14 ( ( PUNCT eurjchem-71 60 15 c c NOUN eurjchem-71 60 16 = = SYM eurjchem-71 60 17 ocoupling ocouple VERB eurjchem-71 60 18     SPACE eurjchem-71 60 19 bands band NOUN eurjchem-71 60 20 ) ) PUNCT eurjchem-71 60 21 . . PUNCT eurjchem-71 60 22     SPACE eurjchem-71 61 1 1h‐nmr 1h‐nmr NUM eurjchem-71 61 2     SPACE eurjchem-71 61 3 ( ( PUNCT eurjchem-71 61 4 cdcl3 cdcl3 PROPN eurjchem-71 61 5 ) ) PUNCT eurjchem-71 61 6     SPACE eurjchem-71 61 7 δ δ PROPN eurjchem-71 61 8     SPACE eurjchem-71 61 9 7.9‐6.8 7.9‐6.8 NOUN eurjchem-71 61 10     SPACE eurjchem-71 61 11 ( ( PUNCT eurjchem-71 61 12 m m PROPN eurjchem-71 61 13 , , PUNCT eurjchem-71 61 14     SPACE eurjchem-71 61 15 8harom 8harom NUM eurjchem-71 61 16 . . PUNCT eurjchem-71 61 17     SPACE eurjchem-71 62 1 + + ADV eurjchem-71 62 2     SPACE eurjchem-71 62 3 olefinic olefinic ADJ eurjchem-71 62 4     SPACE eurjchem-71 62 5 h h NOUN eurjchem-71 62 6 ) ) PUNCT eurjchem-71 62 7 , , PUNCT eurjchem-71 62 8     SPACE eurjchem-71 62 9 3.8 3.8 NUM eurjchem-71 62 10     SPACE eurjchem-71 62 11 ( ( PUNCT eurjchem-71 62 12 s s PROPN eurjchem-71 62 13 , , PUNCT eurjchem-71 62 14     SPACE eurjchem-71 62 15 3h 3h NUM eurjchem-71 62 16 , , PUNCT eurjchem-71 62 17     SPACE eurjchem-71 62 18 ome ome NOUN eurjchem-71 62 19 ) ) PUNCT eurjchem-71 62 20 , , PUNCT eurjchem-71 62 21     SPACE eurjchem-71 62 22 3.77 3.77 NUM eurjchem-71 62 23     SPACE eurjchem-71 62 24 ( ( PUNCT eurjchem-71 62 25 s s PROPN eurjchem-71 62 26 , , PUNCT eurjchem-71 62 27     SPACE eurjchem-71 62 28 3h 3h NUM eurjchem-71 62 29 , , PUNCT eurjchem-71 62 30     SPACE eurjchem-71 62 31 ome ome NOUN eurjchem-71 62 32 ) ) PUNCT eurjchem-71 62 33 , , PUNCT eurjchem-71 62 34     SPACE eurjchem-71 62 35 2.6‐1.14 2.6‐1.14 NUM eurjchem-71 62 36     SPACE eurjchem-71 62 37 ( ( PUNCT eurjchem-71 62 38 m m PROPN eurjchem-71 62 39 , , PUNCT eurjchem-71 62 40     SPACE eurjchem-71 62 41 11h 11h NOUN eurjchem-71 62 42 , , PUNCT eurjchem-71 62 43     SPACE eurjchem-71 62 44 c6h11‐ c6h11‐ PROPN eurjchem-71 62 45 ) ) PUNCT eurjchem-71 62 46 . . PUNCT eurjchem-71 62 47     SPACE eurjchem-71 63 1 ms ms NOUN eurjchem-71 63 2 : : PUNCT eurjchem-71 63 3     SPACE eurjchem-71 63 4 391 391 NUM eurjchem-71 63 5     SPACE eurjchem-71 63 6 ( ( PUNCT eurjchem-71 63 7 3.0 3.0 NUM eurjchem-71 63 8 ) ) PUNCT eurjchem-71 63 9 , , PUNCT eurjchem-71 63 10     SPACE eurjchem-71 63 11 310 310 NUM eurjchem-71 63 12     SPACE eurjchem-71 63 13 ( ( PUNCT eurjchem-71 63 14 [ [ X eurjchem-71 63 15 m‐c6h11 m‐c6h11 X eurjchem-71 63 16 ] ] PUNCT eurjchem-71 63 17 , , PUNCT eurjchem-71 63 18     SPACE eurjchem-71 63 19 100 100 NUM eurjchem-71 63 20 ) ) PUNCT eurjchem-71 63 21 . . PUNCT eurjchem-71 63 22     SPACE eurjchem-71 64 1 anal anal ADJ eurjchem-71 64 2 . . PUNCT eurjchem-71 64 3     SPACE eurjchem-71 64 4 calcd calcd NOUN eurjchem-71 64 5 . . PUNCT eurjchem-71 64 6     SPACE eurjchem-71 64 7 for for ADP eurjchem-71 64 8     SPACE eurjchem-71 64 9 c24h25no4 c24h25no4 PROPN eurjchem-71 64 10     SPACE eurjchem-71 64 11 ( ( PUNCT eurjchem-71 64 12 391.46 391.46 NUM eurjchem-71 64 13 ): ): PUNCT eurjchem-71 64 14     SPACE eurjchem-71 64 15 c c NOUN eurjchem-71 64 16 , , PUNCT eurjchem-71 64 17     SPACE eurjchem-71 64 18 73.64; 73.64; NOUN eurjchem-71 64 19     SPACE eurjchem-71 64 20 h h NOUN eurjchem-71 64 21 , , PUNCT eurjchem-71 64 22     SPACE eurjchem-71 64 23 6.44 6.44 NUM eurjchem-71 64 24 ; ; PUNCT eurjchem-71 64 25     SPACE eurjchem-71 64 26 n n CCONJ eurjchem-71 64 27 , , PUNCT eurjchem-71 64 28     SPACE eurjchem-71 64 29 3.58 3.58 NUM eurjchem-71 64 30 . . PUNCT eurjchem-71 64 31     SPACE eurjchem-71 64 32 found find VERB eurjchem-71 64 33 : : PUNCT eurjchem-71 64 34     SPACE eurjchem-71 64 35 c c X eurjchem-71 64 36 , , PUNCT eurjchem-71 64 37     SPACE eurjchem-71 64 38 73.7 73.7 NUM eurjchem-71 64 39 ; ; PUNCT eurjchem-71 64 40     SPACE eurjchem-71 64 41 h h NOUN eurjchem-71 64 42 , , PUNCT eurjchem-71 64 43     SPACE eurjchem-71 64 44 6.32 6.32 NUM eurjchem-71 64 45 ; ; PUNCT eurjchem-71 64 46     SPACE eurjchem-71 64 47 n n CCONJ eurjchem-71 64 48 , , PUNCT eurjchem-71 64 49     SPACE eurjchem-71 64 50 3.29 3.29 NUM eurjchem-71 64 51 . . PUNCT eurjchem-71 64 52     SPACE eurjchem-71 65 1 13c‐nmr 13c‐nmr NOUN eurjchem-71 65 2     SPACE eurjchem-71 65 3 ( ( PUNCT eurjchem-71 65 4 cdcl3 cdcl3 PROPN eurjchem-71 65 5 ) ) PUNCT eurjchem-71 65 6     SPACE eurjchem-71 65 7 for for ADP eurjchem-71 65 8     SPACE eurjchem-71 65 9 compound compound NOUN eurjchem-71 65 10     SPACE eurjchem-71 65 11 9 9 NUM eurjchem-71 65 12     SPACE eurjchem-71 65 13 is be AUX eurjchem-71 65 14     SPACE eurjchem-71 65 15 given give VERB eurjchem-71 65 16     SPACE eurjchem-71 65 17 in in ADP eurjchem-71 65 18     SPACE eurjchem-71 65 19 scheme scheme NOUN eurjchem-71 65 20     SPACE eurjchem-71 65 21 2 2 NUM eurjchem-71 65 22 . . PUNCT eurjchem-71 65 23         SPACE eurjchem-71 65 24 scheme scheme NOUN eurjchem-71 65 25     SPACE eurjchem-71 65 26 2 2 NUM eurjchem-71 65 27         SPACE eurjchem-71 65 28 2.8 2.8 NUM eurjchem-71 65 29 . . PUNCT eurjchem-71 65 30     SPACE eurjchem-71 65 31 ( ( PUNCT eurjchem-71 65 32 e)­n­((e)­4­(3,4­dimethoxybenzylidene)­3­oxo­3,4­ e)­n­((e)­4­(3,4­dimethoxybenzylidene)­3­oxo­3,4­ ADJ eurjchem-71 65 33 dihydroisochromen­1­ylidene)­cyclo­hexanaminium dihydroisochromen­1­ylidene)­cyclo­hexanaminium NOUN eurjchem-71 65 34     SPACE eurjchem-71 65 35 perchlorate perchlorate NOUN eurjchem-71 65 36     SPACE eurjchem-71 65 37 ( ( PUNCT eurjchem-71 65 38 10 10 NUM eurjchem-71 65 39 ) ) PUNCT eurjchem-71 65 40         SPACE eurjchem-71 65 41 a a DET eurjchem-71 65 42     SPACE eurjchem-71 65 43 suspension suspension NOUN eurjchem-71 65 44     SPACE eurjchem-71 65 45 of of ADP eurjchem-71 65 46     SPACE eurjchem-71 65 47 compound compound NOUN eurjchem-71 65 48     SPACE eurjchem-71 65 49 8 8 NUM eurjchem-71 65 50     SPACE eurjchem-71 65 51 ( ( PUNCT eurjchem-71 65 52 4.1 4.1 NUM eurjchem-71 65 53     SPACE eurjchem-71 65 54 g g NOUN eurjchem-71 65 55 , , PUNCT eurjchem-71 65 56     SPACE eurjchem-71 65 57 0.01 0.01 NUM eurjchem-71 65 58     SPACE eurjchem-71 65 59 mole mole NOUN eurjchem-71 65 60 ) ) PUNCT eurjchem-71 65 61     SPACE eurjchem-71 65 62 in in ADP eurjchem-71 65 63     SPACE eurjchem-71 65 64 acetic acetic ADJ eurjchem-71 65 65     SPACE eurjchem-71 65 66 anhydride anhydride NOUN eurjchem-71 65 67     SPACE eurjchem-71 65 68 ( ( PUNCT eurjchem-71 65 69 20 20 NUM eurjchem-71 65 70     SPACE eurjchem-71 65 71 ml ml NOUN eurjchem-71 65 72 ) ) PUNCT eurjchem-71 65 73     SPACE eurjchem-71 65 74 and and CCONJ eurjchem-71 65 75     SPACE eurjchem-71 65 76 ( ( PUNCT eurjchem-71 65 77 1 1 NUM eurjchem-71 65 78     SPACE eurjchem-71 65 79 ml ml NOUN eurjchem-71 65 80 , , PUNCT eurjchem-71 65 81     SPACE eurjchem-71 65 82 0.01 0.01 NUM eurjchem-71 65 83     SPACE eurjchem-71 65 84 mole mole NOUN eurjchem-71 65 85 ) ) PUNCT eurjchem-71 65 86     SPACE eurjchem-71 65 87 perchloric perchloric ADJ eurjchem-71 65 88     SPACE eurjchem-71 65 89 acid acid NOUN eurjchem-71 65 90     SPACE eurjchem-71 65 91 was be AUX eurjchem-71 65 92     SPACE eurjchem-71 65 93 stirred stir VERB eurjchem-71 65 94     SPACE eurjchem-71 65 95 at at ADP eurjchem-71 65 96     SPACE eurjchem-71 65 97 room room NOUN eurjchem-71 65 98     SPACE eurjchem-71 65 99 temperature temperature NOUN eurjchem-71 65 100     SPACE eurjchem-71 65 101 in in ADP eurjchem-71 65 102     SPACE eurjchem-71 65 103 an an DET eurjchem-71 65 104     SPACE eurjchem-71 65 105 ice ice NOUN eurjchem-71 65 106     SPACE eurjchem-71 65 107 bath bath NOUN eurjchem-71 65 108     SPACE eurjchem-71 65 109 for for ADP eurjchem-71 65 110     SPACE eurjchem-71 65 111 a a DET eurjchem-71 65 112     SPACE eurjchem-71 65 113 few few ADJ eurjchem-71 65 114     SPACE eurjchem-71 65 115 minutes minute NOUN eurjchem-71 65 116     SPACE eurjchem-71 65 117 until until SCONJ eurjchem-71 65 118     SPACE eurjchem-71 65 119 an an DET eurjchem-71 65 120     SPACE eurjchem-71 65 121 orange orange NOUN eurjchem-71 65 122     SPACE eurjchem-71 65 123 crystals crystal NOUN eurjchem-71 65 124     SPACE eurjchem-71 65 125 were be AUX eurjchem-71 65 126     SPACE eurjchem-71 65 127 formed form VERB eurjchem-71 65 128 . . PUNCT eurjchem-71 65 129     SPACE eurjchem-71 66 1 the the DET eurjchem-71 66 2     SPACE eurjchem-71 66 3 deposited deposit VERB eurjchem-71 66 4     SPACE eurjchem-71 66 5 crystals crystal NOUN eurjchem-71 66 6     SPACE eurjchem-71 66 7 were be AUX eurjchem-71 66 8     SPACE eurjchem-71 66 9 filtered filter VERB eurjchem-71 66 10     SPACE eurjchem-71 66 11 off off ADP eurjchem-71 66 12 , , PUNCT eurjchem-71 66 13     SPACE eurjchem-71 66 14 washed wash VERB eurjchem-71 66 15     SPACE eurjchem-71 66 16 with with ADP eurjchem-71 66 17     SPACE eurjchem-71 66 18 dry dry ADJ eurjchem-71 66 19     SPACE eurjchem-71 66 20 diethyl diethyl NOUN eurjchem-71 66 21     SPACE eurjchem-71 66 22 ether ether NOUN eurjchem-71 66 23     SPACE eurjchem-71 66 24 to to PART eurjchem-71 66 25     SPACE eurjchem-71 66 26 give give VERB eurjchem-71 66 27     SPACE eurjchem-71 66 28 10 10 NUM eurjchem-71 66 29 ; ; PUNCT eurjchem-71 66 30     SPACE eurjchem-71 66 31 yield yield NOUN eurjchem-71 66 32     SPACE eurjchem-71 66 33 85 85 NUM eurjchem-71 66 34 % % NOUN eurjchem-71 66 35 . . PUNCT eurjchem-71 66 36     SPACE eurjchem-71 67 1 ir ir VERB eurjchem-71 67 2     SPACE eurjchem-71 67 3 ( ( PUNCT eurjchem-71 67 4 ν ν NOUN eurjchem-71 67 5 ): ): NOUN eurjchem-71 67 6     SPACE eurjchem-71 67 7 3345 3345 NUM eurjchem-71 67 8     SPACE eurjchem-71 67 9 cm‐1 cm‐1 NOUN eurjchem-71 67 10     SPACE eurjchem-71 67 11 ( ( PUNCT eurjchem-71 67 12 nh+ nh+ NOUN eurjchem-71 67 13 ) ) PUNCT eurjchem-71 67 14 , , PUNCT eurjchem-71 67 15     SPACE eurjchem-71 67 16 1809 1809 NUM eurjchem-71 67 17     SPACE eurjchem-71 67 18 cm‐1 cm‐1 NOUN eurjchem-71 67 19     SPACE eurjchem-71 67 20 ( ( PUNCT eurjchem-71 67 21 c c NOUN eurjchem-71 67 22 = = NOUN eurjchem-71 67 23 o o NOUN eurjchem-71 67 24 ) ) PUNCT eurjchem-71 67 25 , , PUNCT eurjchem-71 67 26     SPACE eurjchem-71 67 27 1643 1643 NUM eurjchem-71 67 28     SPACE eurjchem-71 67 29 cm‐1 cm‐1 NOUN eurjchem-71 67 30     SPACE eurjchem-71 67 31 ( ( PUNCT eurjchem-71 67 32 c c NOUN eurjchem-71 67 33 = = NOUN eurjchem-71 67 34 n+ n+ X eurjchem-71 67 35 ) ) PUNCT eurjchem-71 67 36 . . PUNCT eurjchem-71 67 37     SPACE eurjchem-71 68 1 ms ms NOUN eurjchem-71 68 2 : : PUNCT eurjchem-71 68 3     SPACE eurjchem-71 68 4 391 391 NUM eurjchem-71 68 5     SPACE eurjchem-71 68 6 ( ( PUNCT eurjchem-71 68 7 [ [ X eurjchem-71 68 8 m‐hclo4 m‐hclo4 X eurjchem-71 68 9 ] ] X eurjchem-71 68 10 , , PUNCT eurjchem-71 68 11     SPACE eurjchem-71 68 12 17.9 17.9 NUM eurjchem-71 68 13 ) ) PUNCT eurjchem-71 68 14 , , PUNCT eurjchem-71 68 15     SPACE eurjchem-71 68 16 308 308 NUM eurjchem-71 68 17     SPACE eurjchem-71 68 18 ( ( PUNCT eurjchem-71 68 19 22.5 22.5 NUM eurjchem-71 68 20 ) ) PUNCT eurjchem-71 68 21 , , PUNCT eurjchem-71 68 22     SPACE eurjchem-71 68 23 294 294 NUM eurjchem-71 68 24     SPACE eurjchem-71 68 25 ( ( PUNCT eurjchem-71 68 26 12.1 12.1 NUM eurjchem-71 68 27 ) ) PUNCT eurjchem-71 68 28 , , PUNCT eurjchem-71 68 29     SPACE eurjchem-71 68 30 278 278 NUM eurjchem-71 68 31     SPACE eurjchem-71 68 32 ( ( PUNCT eurjchem-71 68 33 13.9 13.9 NUM eurjchem-71 68 34 ) ) PUNCT eurjchem-71 68 35 , , PUNCT eurjchem-71 68 36     SPACE eurjchem-71 68 37 151 151 NUM eurjchem-71 68 38     SPACE eurjchem-71 68 39 ( ( PUNCT eurjchem-71 68 40 36.4 36.4 NUM eurjchem-71 68 41 ) ) PUNCT eurjchem-71 68 42 , , PUNCT eurjchem-71 68 43     SPACE eurjchem-71 68 44 89 89 NUM eurjchem-71 68 45     SPACE eurjchem-71 68 46 ( ( PUNCT eurjchem-71 68 47 15.6 15.6 NUM eurjchem-71 68 48 ) ) PUNCT eurjchem-71 68 49 , , PUNCT eurjchem-71 68 50     SPACE eurjchem-71 68 51 55 55 NUM eurjchem-71 68 52     SPACE eurjchem-71 68 53 ( ( PUNCT eurjchem-71 68 54 100 100 NUM eurjchem-71 68 55 ) ) PUNCT eurjchem-71 68 56 . . PUNCT eurjchem-71 68 57     SPACE eurjchem-71 69 1 anal anal ADJ eurjchem-71 69 2 . . PUNCT eurjchem-71 69 3     SPACE eurjchem-71 69 4 calcd calcd NOUN eurjchem-71 69 5 . . PUNCT eurjchem-71 69 6     SPACE eurjchem-71 69 7 for for ADP eurjchem-71 69 8     SPACE eurjchem-71 69 9 c24h26clno8 c24h26clno8 NOUN eurjchem-71 69 10     SPACE eurjchem-71 69 11 ( ( PUNCT eurjchem-71 69 12 491.92 491.92 NUM eurjchem-71 69 13 ): ): PUNCT eurjchem-71 69 14     SPACE eurjchem-71 69 15 c c NOUN eurjchem-71 69 16 , , PUNCT eurjchem-71 69 17     SPACE eurjchem-71 69 18 58.60; 58.60; NUM eurjchem-71 69 19     SPACE eurjchem-71 69 20 h h NOUN eurjchem-71 69 21 , , PUNCT eurjchem-71 69 22     SPACE eurjchem-71 69 23 5.33 5.33 NUM eurjchem-71 69 24 ; ; PUNCT eurjchem-71 69 25     SPACE eurjchem-71 69 26 cl cl NOUN eurjchem-71 69 27 , , PUNCT eurjchem-71 69 28     SPACE eurjchem-71 69 29 7.21 7.21 NUM eurjchem-71 69 30 ; ; PUNCT eurjchem-71 69 31     SPACE eurjchem-71 69 32 n n CCONJ eurjchem-71 69 33 , , PUNCT eurjchem-71 69 34     SPACE eurjchem-71 69 35 2.85 2.85 NUM eurjchem-71 69 36 . . PUNCT eurjchem-71 69 37     SPACE eurjchem-71 69 38 found find VERB eurjchem-71 69 39 : : PUNCT eurjchem-71 69 40     SPACE eurjchem-71 69 41 c c X eurjchem-71 69 42 , , PUNCT eurjchem-71 69 43     SPACE eurjchem-71 69 44 58.3; 58.3; NUM eurjchem-71 69 45     SPACE eurjchem-71 69 46 h h NOUN eurjchem-71 69 47 , , PUNCT eurjchem-71 69 48     SPACE eurjchem-71 69 49 5.1 5.1 NUM eurjchem-71 69 50 ; ; PUNCT eurjchem-71 69 51     SPACE eurjchem-71 69 52 cl cl NOUN eurjchem-71 69 53 , , PUNCT eurjchem-71 69 54     SPACE eurjchem-71 69 55 7.4 7.4 NUM eurjchem-71 69 56 ; ; PUNCT eurjchem-71 69 57     SPACE eurjchem-71 69 58 n n CCONJ eurjchem-71 69 59 , , PUNCT eurjchem-71 69 60     SPACE eurjchem-71 69 61 3.0 3.0 NUM eurjchem-71 69 62 . . PUNCT eurjchem-71 69 63         SPACE eurjchem-71 69 64 136 136 NUM eurjchem-71 69 65     SPACE eurjchem-71 69 66 mahmoud mahmoud PROPN eurjchem-71 69 67     SPACE eurjchem-71 69 68 et et PROPN eurjchem-71 69 69     SPACE eurjchem-71 69 70 al al PROPN eurjchem-71 69 71 . . PROPN eurjchem-71 69 72     SPACE eurjchem-71 69 73 / / SYM eurjchem-71 69 74     SPACE eurjchem-71 69 75 european european ADJ eurjchem-71 69 76     SPACE eurjchem-71 69 77 journal journal NOUN eurjchem-71 69 78     SPACE eurjchem-71 69 79 of of ADP eurjchem-71 69 80     SPACE eurjchem-71 69 81 chemistry chemistry NOUN eurjchem-71 69 82     SPACE eurjchem-71 69 83 1 1 NUM eurjchem-71 69 84     SPACE eurjchem-71 69 85 ( ( PUNCT eurjchem-71 69 86 2 2 NUM eurjchem-71 69 87 ) ) PUNCT eurjchem-71 69 88     SPACE eurjchem-71 69 89 ( ( PUNCT eurjchem-71 69 90 2010 2010 NUM eurjchem-71 69 91 ) ) PUNCT eurjchem-71 69 92     SPACE eurjchem-71 69 93 134­139 134­139 NUM eurjchem-71 69 94         SPACE eurjchem-71 69 95 2.9 2.9 NUM eurjchem-71 69 96 . . PUNCT eurjchem-71 69 97     SPACE eurjchem-71 70 1 2­((2e,4e)­2­(3,4­dimethoxyphenyl)benzo[b][1,4 2­((2e,4e)­2­(3,4­dimethoxyphenyl)benzo[b][1,4 ADV eurjchem-71 70 2 ] ] PUNCT eurjchem-71 70 3     SPACE eurjchem-71 70 4 thiazepin­3­yl)benzoic thiazepin­3­yl)benzoic NOUN eurjchem-71 70 5     SPACE eurjchem-71 70 6 acid acid NOUN eurjchem-71 70 7     SPACE eurjchem-71 70 8 ( ( PUNCT eurjchem-71 70 9 11 11 NUM eurjchem-71 70 10 ) ) PUNCT eurjchem-71 70 11         SPACE eurjchem-71 70 12 a a DET eurjchem-71 70 13     SPACE eurjchem-71 70 14 mixture mixture NOUN eurjchem-71 70 15     SPACE eurjchem-71 70 16 of of ADP eurjchem-71 70 17     SPACE eurjchem-71 70 18 compound compound NOUN eurjchem-71 70 19     SPACE eurjchem-71 70 20 2 2 NUM eurjchem-71 70 21     SPACE eurjchem-71 70 22 ( ( PUNCT eurjchem-71 70 23 3.1 3.1 NUM eurjchem-71 70 24     SPACE eurjchem-71 70 25 g g NOUN eurjchem-71 70 26 , , PUNCT eurjchem-71 70 27     SPACE eurjchem-71 70 28 0.01 0.01 NUM eurjchem-71 70 29     SPACE eurjchem-71 70 30 mole mole NOUN eurjchem-71 70 31 ) ) PUNCT eurjchem-71 70 32     SPACE eurjchem-71 70 33 and and CCONJ eurjchem-71 70 34     SPACE eurjchem-71 70 35 2‐ 2‐ NUM eurjchem-71 70 36 aminothiophenol aminothiophenol NOUN eurjchem-71 70 37     SPACE eurjchem-71 70 38 ( ( PUNCT eurjchem-71 70 39 1.25 1.25 NUM eurjchem-71 70 40     SPACE eurjchem-71 70 41 g g NOUN eurjchem-71 70 42 , , PUNCT eurjchem-71 70 43     SPACE eurjchem-71 70 44 0.01 0.01 NUM eurjchem-71 70 45     SPACE eurjchem-71 70 46 mole mole NOUN eurjchem-71 70 47 ) ) PUNCT eurjchem-71 70 48     SPACE eurjchem-71 70 49 in in ADP eurjchem-71 70 50     SPACE eurjchem-71 70 51 30 30 NUM eurjchem-71 70 52     SPACE eurjchem-71 70 53 ml ml NOUN eurjchem-71 70 54     SPACE eurjchem-71 70 55 dioxane dioxane NOUN eurjchem-71 70 56     SPACE eurjchem-71 70 57 was be AUX eurjchem-71 70 58     SPACE eurjchem-71 70 59 refluxed refluxe VERB eurjchem-71 70 60     SPACE eurjchem-71 70 61 for for ADP eurjchem-71 70 62     SPACE eurjchem-71 70 63 8 8 NUM eurjchem-71 70 64     SPACE eurjchem-71 70 65 h. h. NOUN eurjchem-71 70 66     SPACE eurjchem-71 70 67 after after ADP eurjchem-71 70 68     SPACE eurjchem-71 70 69 concentration concentration NOUN eurjchem-71 70 70     SPACE eurjchem-71 70 71 of of ADP eurjchem-71 70 72     SPACE eurjchem-71 70 73 the the DET eurjchem-71 70 74     SPACE eurjchem-71 70 75 solvent solvent NOUN eurjchem-71 70 76 , , PUNCT eurjchem-71 70 77     SPACE eurjchem-71 70 78 a a DET eurjchem-71 70 79     SPACE eurjchem-71 70 80 yellowish yellowish NOUN eurjchem-71 70 81     SPACE eurjchem-71 70 82 white white ADJ eurjchem-71 70 83     SPACE eurjchem-71 70 84 solid solid NOUN eurjchem-71 70 85     SPACE eurjchem-71 70 86 was be AUX eurjchem-71 70 87     SPACE eurjchem-71 70 88 deposited deposit VERB eurjchem-71 70 89     SPACE eurjchem-71 70 90 which which PRON eurjchem-71 70 91     SPACE eurjchem-71 70 92 filtered filter VERB eurjchem-71 70 93     SPACE eurjchem-71 70 94 off off ADP eurjchem-71 70 95 , , PUNCT eurjchem-71 70 96     SPACE eurjchem-71 70 97 dried dry VERB eurjchem-71 70 98     SPACE eurjchem-71 70 99 and and CCONJ eurjchem-71 70 100     SPACE eurjchem-71 70 101 recrystallized recrystallize VERB eurjchem-71 70 102     SPACE eurjchem-71 70 103 from from ADP eurjchem-71 70 104     SPACE eurjchem-71 70 105 benzene benzene NOUN eurjchem-71 70 106 / / SYM eurjchem-71 70 107 ethanol ethanol NOUN eurjchem-71 70 108     SPACE eurjchem-71 70 109 to to PART eurjchem-71 70 110     SPACE eurjchem-71 70 111 give give VERB eurjchem-71 70 112     SPACE eurjchem-71 70 113 11 11 NUM eurjchem-71 70 114     SPACE eurjchem-71 70 115 as as ADP eurjchem-71 70 116     SPACE eurjchem-71 70 117 yellowish yellowish VERB eurjchem-71 70 118     SPACE eurjchem-71 70 119 white white ADJ eurjchem-71 70 120     SPACE eurjchem-71 70 121 crystals crystal NOUN eurjchem-71 70 122 . . PUNCT eurjchem-71 70 123     SPACE eurjchem-71 71 1 m.p m.p AUX eurjchem-71 71 2 . . PROPN eurjchem-71 71 3 : : PUNCT eurjchem-71 71 4     SPACE eurjchem-71 71 5 176‐178oc 176‐178oc NUM eurjchem-71 71 6 , , PUNCT eurjchem-71 71 7     SPACE eurjchem-71 71 8 yield yield NOUN eurjchem-71 71 9     SPACE eurjchem-71 71 10 73 73 NUM eurjchem-71 71 11 % % NOUN eurjchem-71 71 12 . . PUNCT eurjchem-71 71 13     SPACE eurjchem-71 72 1 ir ir VERB eurjchem-71 72 2     SPACE eurjchem-71 72 3 ( ( PUNCT eurjchem-71 72 4 ν ν NOUN eurjchem-71 72 5 ): ): NOUN eurjchem-71 72 6     SPACE eurjchem-71 72 7 br br NOUN eurjchem-71 72 8 . . PUNCT eurjchem-71 72 9     SPACE eurjchem-71 72 10 3422‐ 3422‐ NUM eurjchem-71 72 11 2836 2836 NUM eurjchem-71 72 12     SPACE eurjchem-71 72 13 cm‐1 cm‐1 NOUN eurjchem-71 72 14     SPACE eurjchem-71 72 15 ( ( PUNCT eurjchem-71 72 16 ohacid ohacid ADJ eurjchem-71 72 17 ) ) PUNCT eurjchem-71 72 18 , , PUNCT eurjchem-71 72 19     SPACE eurjchem-71 72 20 1684 1684 NUM eurjchem-71 72 21     SPACE eurjchem-71 72 22 cm‐1 cm‐1 NOUN eurjchem-71 72 23     SPACE eurjchem-71 72 24 ( ( PUNCT eurjchem-71 72 25 c c NOUN eurjchem-71 72 26 = = NOUN eurjchem-71 72 27 o o NOUN eurjchem-71 72 28 ) ) PUNCT eurjchem-71 72 29 . . PUNCT eurjchem-71 72 30     SPACE eurjchem-71 73 1 1h‐nmr 1h‐nmr NUM eurjchem-71 73 2     SPACE eurjchem-71 73 3 ( ( PUNCT eurjchem-71 73 4 cdcl3 cdcl3 PROPN eurjchem-71 73 5 ) ) PUNCT eurjchem-71 73 6     SPACE eurjchem-71 73 7 δ δ PROPN eurjchem-71 73 8     SPACE eurjchem-71 73 9 10.5 10.5 NUM eurjchem-71 73 10     SPACE eurjchem-71 73 11 ( ( PUNCT eurjchem-71 73 12 s s PROPN eurjchem-71 73 13 , , PUNCT eurjchem-71 73 14     SPACE eurjchem-71 73 15 1h 1h NUM eurjchem-71 73 16 , , PUNCT eurjchem-71 73 17     SPACE eurjchem-71 73 18 cooh cooh NOUN eurjchem-71 73 19 , , PUNCT eurjchem-71 73 20     SPACE eurjchem-71 73 21 exchangeable exchangeable ADJ eurjchem-71 73 22     SPACE eurjchem-71 73 23 with with ADP eurjchem-71 73 24     SPACE eurjchem-71 73 25 d2o d2o NOUN eurjchem-71 73 26 ) ) PUNCT eurjchem-71 73 27 , , PUNCT eurjchem-71 73 28     SPACE eurjchem-71 73 29 7.8‐6.5 7.8‐6.5 NUM eurjchem-71 73 30     SPACE eurjchem-71 73 31 ( ( PUNCT eurjchem-71 73 32 m m PROPN eurjchem-71 73 33 , , PUNCT eurjchem-71 73 34     SPACE eurjchem-71 73 35 12harom 12harom NUM eurjchem-71 73 36 . . PUNCT eurjchem-71 73 37     SPACE eurjchem-71 74 1 + + NOUN eurjchem-71 74 2     SPACE eurjchem-71 74 3 1h 1h NUM eurjchem-71 74 4 , , PUNCT eurjchem-71 74 5     SPACE eurjchem-71 74 6 n n CCONJ eurjchem-71 74 7 = = NOUN eurjchem-71 74 8 ch ch NOUN eurjchem-71 74 9 ) ) PUNCT eurjchem-71 74 10 , , PUNCT eurjchem-71 74 11     SPACE eurjchem-71 74 12 3.85 3.85 NUM eurjchem-71 74 13     SPACE eurjchem-71 74 14 ( ( PUNCT eurjchem-71 74 15 s s PROPN eurjchem-71 74 16 , , PUNCT eurjchem-71 74 17     SPACE eurjchem-71 74 18 3h 3h NUM eurjchem-71 74 19 , , PUNCT eurjchem-71 74 20     SPACE eurjchem-71 74 21 ome ome NOUN eurjchem-71 74 22 ) ) PUNCT eurjchem-71 74 23 , , PUNCT eurjchem-71 74 24     SPACE eurjchem-71 74 25 3.7 3.7 NUM eurjchem-71 74 26     SPACE eurjchem-71 74 27 ( ( PUNCT eurjchem-71 74 28 s s PROPN eurjchem-71 74 29 , , PUNCT eurjchem-71 74 30     SPACE eurjchem-71 74 31 3h 3h NUM eurjchem-71 74 32 , , PUNCT eurjchem-71 74 33     SPACE eurjchem-71 74 34 ome ome NOUN eurjchem-71 74 35 ) ) PUNCT eurjchem-71 74 36 . . PUNCT eurjchem-71 74 37     SPACE eurjchem-71 75 1 ms ms NOUN eurjchem-71 75 2 : : PUNCT eurjchem-71 75 3     SPACE eurjchem-71 75 4 417 417 NUM eurjchem-71 75 5     SPACE eurjchem-71 75 6 ( ( PUNCT eurjchem-71 75 7 12.5 12.5 NUM eurjchem-71 75 8 ) ) PUNCT eurjchem-71 75 9 , , PUNCT eurjchem-71 75 10     SPACE eurjchem-71 75 11 310 310 NUM eurjchem-71 75 12     SPACE eurjchem-71 75 13 ( ( PUNCT eurjchem-71 75 14 49.6 49.6 NUM eurjchem-71 75 15 ) ) PUNCT eurjchem-71 75 16 , , PUNCT eurjchem-71 75 17     SPACE eurjchem-71 75 18 240 240 NUM eurjchem-71 75 19     SPACE eurjchem-71 75 20 ( ( PUNCT eurjchem-71 75 21 6.3 6.3 NUM eurjchem-71 75 22 ) ) PUNCT eurjchem-71 75 23 , , PUNCT eurjchem-71 75 24     SPACE eurjchem-71 75 25 151 151 NUM eurjchem-71 75 26     SPACE eurjchem-71 75 27 ( ( PUNCT eurjchem-71 75 28 69.7 69.7 NUM eurjchem-71 75 29 ) ) PUNCT eurjchem-71 75 30 , , PUNCT eurjchem-71 75 31     SPACE eurjchem-71 75 32 134 134 NUM eurjchem-71 75 33     SPACE eurjchem-71 75 34 ( ( PUNCT eurjchem-71 75 35 9.4 9.4 NUM eurjchem-71 75 36 ) ) PUNCT eurjchem-71 75 37 , , PUNCT eurjchem-71 75 38     SPACE eurjchem-71 75 39 108 108 NUM eurjchem-71 75 40     SPACE eurjchem-71 75 41 ( ( PUNCT eurjchem-71 75 42 13.8 13.8 NUM eurjchem-71 75 43 ) ) PUNCT eurjchem-71 75 44 , , PUNCT eurjchem-71 75 45     SPACE eurjchem-71 75 46 91 91 NUM eurjchem-71 75 47     SPACE eurjchem-71 75 48 ( ( PUNCT eurjchem-71 75 49 15.6 15.6 NUM eurjchem-71 75 50 ) ) PUNCT eurjchem-71 75 51 , , PUNCT eurjchem-71 75 52     SPACE eurjchem-71 75 53 76 76 NUM eurjchem-71 75 54     SPACE eurjchem-71 75 55 ( ( PUNCT eurjchem-71 75 56 57.5 57.5 NUM eurjchem-71 75 57 ) ) PUNCT eurjchem-71 75 58 , , PUNCT eurjchem-71 75 59     SPACE eurjchem-71 75 60 65 65 NUM eurjchem-71 75 61     SPACE eurjchem-71 75 62 ( ( PUNCT eurjchem-71 75 63 43.1 43.1 NUM eurjchem-71 75 64 ) ) PUNCT eurjchem-71 75 65 . . PUNCT eurjchem-71 75 66     SPACE eurjchem-71 76 1 anal anal ADJ eurjchem-71 76 2 . . PUNCT eurjchem-71 76 3     SPACE eurjchem-71 76 4 calcd calcd NOUN eurjchem-71 76 5 . . PUNCT eurjchem-71 76 6     SPACE eurjchem-71 76 7 for for ADP eurjchem-71 76 8     SPACE eurjchem-71 76 9 c24h19no4s c24h19no4s NOUN eurjchem-71 76 10     SPACE eurjchem-71 76 11 ( ( PUNCT eurjchem-71 76 12 417.48 417.48 NUM eurjchem-71 76 13 ): ): PUNCT eurjchem-71 76 14     SPACE eurjchem-71 76 15 c c NOUN eurjchem-71 76 16 , , PUNCT eurjchem-71 76 17     SPACE eurjchem-71 76 18 69.05; 69.05; NOUN eurjchem-71 76 19     SPACE eurjchem-71 76 20 h h NOUN eurjchem-71 76 21 , , PUNCT eurjchem-71 76 22     SPACE eurjchem-71 76 23 4.59 4.59 NUM eurjchem-71 76 24 ; ; PUNCT eurjchem-71 76 25     SPACE eurjchem-71 76 26 n n CCONJ eurjchem-71 76 27 , , PUNCT eurjchem-71 76 28     SPACE eurjchem-71 76 29 3.36 3.36 NUM eurjchem-71 76 30 ; ; PUNCT eurjchem-71 76 31     SPACE eurjchem-71 76 32 s s PROPN eurjchem-71 76 33 , , PUNCT eurjchem-71 76 34     SPACE eurjchem-71 76 35 7.68 7.68 NUM eurjchem-71 76 36 . . PUNCT eurjchem-71 76 37     SPACE eurjchem-71 77 1 found find VERB eurjchem-71 77 2 : : PUNCT eurjchem-71 77 3     SPACE eurjchem-71 77 4 c c X eurjchem-71 77 5 , , PUNCT eurjchem-71 77 6     SPACE eurjchem-71 77 7 68.8 68.8 NUM eurjchem-71 77 8 ; ; PUNCT eurjchem-71 77 9     SPACE eurjchem-71 77 10 h h NOUN eurjchem-71 77 11 , , PUNCT eurjchem-71 77 12     SPACE eurjchem-71 77 13 4.32 4.32 NUM eurjchem-71 77 14 ; ; PUNCT eurjchem-71 77 15     SPACE eurjchem-71 77 16 n n CCONJ eurjchem-71 77 17 , , PUNCT eurjchem-71 77 18     SPACE eurjchem-71 77 19 3.09 3.09 NUM eurjchem-71 77 20 ; ; PUNCT eurjchem-71 77 21     SPACE eurjchem-71 77 22 s s X eurjchem-71 77 23 , , PUNCT eurjchem-71 77 24     SPACE eurjchem-71 77 25 7.41 7.41 NUM eurjchem-71 77 26 . . PUNCT eurjchem-71 77 27     SPACE eurjchem-71 78 1 13c‐nmr 13c‐nmr NUM eurjchem-71 78 2     SPACE eurjchem-71 78 3 ( ( PUNCT eurjchem-71 78 4 cdcl3 cdcl3 PROPN eurjchem-71 78 5 ) ) PUNCT eurjchem-71 78 6     SPACE eurjchem-71 78 7 for for ADP eurjchem-71 78 8     SPACE eurjchem-71 78 9 compound compound NOUN eurjchem-71 78 10     SPACE eurjchem-71 78 11 11 11 NUM eurjchem-71 78 12     SPACE eurjchem-71 78 13 is be AUX eurjchem-71 78 14     SPACE eurjchem-71 78 15 given give VERB eurjchem-71 78 16     SPACE eurjchem-71 78 17 in in ADP eurjchem-71 78 18     SPACE eurjchem-71 78 19 scheme scheme NOUN eurjchem-71 78 20     SPACE eurjchem-71 78 21 3 3 NUM eurjchem-71 78 22 . . PUNCT eurjchem-71 78 23         SPACE eurjchem-71 78 24 scheme scheme NOUN eurjchem-71 78 25     SPACE eurjchem-71 78 26 3 3 NUM eurjchem-71 78 27         SPACE eurjchem-71 78 28 2.10 2.10 NUM eurjchem-71 78 29 . . PUNCT eurjchem-71 78 30     SPACE eurjchem-71 79 1 2­[1­carboxy­2­(3,4­dimethoxyphenyl)­2­(phenylthio 2­[1­carboxy­2­(3,4­dimethoxyphenyl)­2­(phenylthio NUM eurjchem-71 79 2 ) ) PUNCT eurjchem-71 79 3     SPACE eurjchem-71 80 1 ethyl]benzoic ethyl]benzoic PROPN eurjchem-71 80 2     SPACE eurjchem-71 80 3 acid acid NOUN eurjchem-71 80 4     SPACE eurjchem-71 80 5 ( ( PUNCT eurjchem-71 80 6 12 12 NUM eurjchem-71 80 7 ) ) PUNCT eurjchem-71 80 8         SPACE eurjchem-71 80 9 a a DET eurjchem-71 80 10     SPACE eurjchem-71 80 11 mixture mixture NOUN eurjchem-71 80 12     SPACE eurjchem-71 80 13 of of ADP eurjchem-71 80 14     SPACE eurjchem-71 80 15 compound compound NOUN eurjchem-71 80 16     SPACE eurjchem-71 80 17 2 2 NUM eurjchem-71 80 18     SPACE eurjchem-71 80 19 ( ( PUNCT eurjchem-71 80 20 3.1 3.1 NUM eurjchem-71 80 21     SPACE eurjchem-71 80 22 g g NOUN eurjchem-71 80 23 , , PUNCT eurjchem-71 80 24     SPACE eurjchem-71 80 25 0.01 0.01 NUM eurjchem-71 80 26     SPACE eurjchem-71 80 27 mole mole NOUN eurjchem-71 80 28 ) ) PUNCT eurjchem-71 80 29     SPACE eurjchem-71 80 30 and and CCONJ eurjchem-71 80 31     SPACE eurjchem-71 80 32 thiophenol thiophenol NOUN eurjchem-71 80 33     SPACE eurjchem-71 80 34 ( ( PUNCT eurjchem-71 80 35 1.1 1.1 NUM eurjchem-71 80 36     SPACE eurjchem-71 80 37 ml ml NOUN eurjchem-71 80 38 , , PUNCT eurjchem-71 80 39     SPACE eurjchem-71 80 40 0.01 0.01 NUM eurjchem-71 80 41     SPACE eurjchem-71 80 42 mole mole NOUN eurjchem-71 80 43 ) ) PUNCT eurjchem-71 80 44     SPACE eurjchem-71 80 45 in in ADP eurjchem-71 80 46     SPACE eurjchem-71 80 47 40 40 NUM eurjchem-71 80 48     SPACE eurjchem-71 80 49 ml ml NOUN eurjchem-71 80 50     SPACE eurjchem-71 80 51 dry dry ADJ eurjchem-71 80 52     SPACE eurjchem-71 80 53 benzene benzene NOUN eurjchem-71 80 54     SPACE eurjchem-71 80 55 was be AUX eurjchem-71 80 56     SPACE eurjchem-71 80 57 refluxed refluxe VERB eurjchem-71 80 58     SPACE eurjchem-71 80 59 for for ADP eurjchem-71 80 60     SPACE eurjchem-71 80 61 10 10 NUM eurjchem-71 80 62     SPACE eurjchem-71 80 63 hrs hrs NOUN eurjchem-71 80 64 . . PUNCT eurjchem-71 80 65     SPACE eurjchem-71 80 66 after after ADP eurjchem-71 80 67     SPACE eurjchem-71 80 68 concentration concentration NOUN eurjchem-71 80 69     SPACE eurjchem-71 80 70 of of ADP eurjchem-71 80 71     SPACE eurjchem-71 80 72 the the DET eurjchem-71 80 73     SPACE eurjchem-71 80 74 solvent solvent NOUN eurjchem-71 80 75 , , PUNCT eurjchem-71 80 76     SPACE eurjchem-71 80 77 a a DET eurjchem-71 80 78     SPACE eurjchem-71 80 79 yellow yellow ADJ eurjchem-71 80 80     SPACE eurjchem-71 80 81 oil oil NOUN eurjchem-71 80 82     SPACE eurjchem-71 80 83 was be AUX eurjchem-71 80 84     SPACE eurjchem-71 80 85 obtained obtain VERB eurjchem-71 80 86     SPACE eurjchem-71 80 87 which which PRON eurjchem-71 80 88     SPACE eurjchem-71 80 89 was be AUX eurjchem-71 80 90     SPACE eurjchem-71 80 91 solidified solidify VERB eurjchem-71 80 92     SPACE eurjchem-71 80 93 after after ADP eurjchem-71 80 94     SPACE eurjchem-71 80 95 trituration trituration NOUN eurjchem-71 80 96     SPACE eurjchem-71 80 97 with with ADP eurjchem-71 80 98     SPACE eurjchem-71 80 99 diethyl diethyl NOUN eurjchem-71 80 100     SPACE eurjchem-71 80 101 ether ether NOUN eurjchem-71 80 102 . . PUNCT eurjchem-71 80 103     SPACE eurjchem-71 81 1 the the DET eurjchem-71 81 2     SPACE eurjchem-71 81 3 separated separate VERB eurjchem-71 81 4     SPACE eurjchem-71 81 5 solid solid NOUN eurjchem-71 81 6     SPACE eurjchem-71 81 7 was be AUX eurjchem-71 81 8     SPACE eurjchem-71 81 9 filtered filter VERB eurjchem-71 81 10     SPACE eurjchem-71 81 11 off off ADP eurjchem-71 81 12 , , PUNCT eurjchem-71 81 13     SPACE eurjchem-71 81 14 dried dry VERB eurjchem-71 81 15     SPACE eurjchem-71 81 16 and and CCONJ eurjchem-71 81 17     SPACE eurjchem-71 81 18 recrystallized recrystallize VERB eurjchem-71 81 19     SPACE eurjchem-71 81 20 from from ADP eurjchem-71 81 21     SPACE eurjchem-71 81 22 benzene benzene NOUN eurjchem-71 81 23 / / SYM eurjchem-71 81 24 ethanol ethanol NOUN eurjchem-71 81 25     SPACE eurjchem-71 81 26 to to PART eurjchem-71 81 27     SPACE eurjchem-71 81 28 give give VERB eurjchem-71 81 29     SPACE eurjchem-71 81 30 12 12 NUM eurjchem-71 81 31     SPACE eurjchem-71 81 32 as as ADP eurjchem-71 81 33     SPACE eurjchem-71 81 34 colorless colorless ADJ eurjchem-71 81 35     SPACE eurjchem-71 81 36 crystals crystal NOUN eurjchem-71 81 37 . . PUNCT eurjchem-71 81 38     SPACE eurjchem-71 82 1 m.p m.p PROPN eurjchem-71 82 2 . . PROPN eurjchem-71 82 3 : : PUNCT eurjchem-71 82 4     SPACE eurjchem-71 82 5 170‐173oc 170‐173oc NUM eurjchem-71 82 6 , , PUNCT eurjchem-71 82 7     SPACE eurjchem-71 82 8 yield yield NOUN eurjchem-71 82 9     SPACE eurjchem-71 82 10 81 81 NUM eurjchem-71 82 11 % % NOUN eurjchem-71 82 12 . . PUNCT eurjchem-71 82 13     SPACE eurjchem-71 83 1 ir ir VERB eurjchem-71 83 2     SPACE eurjchem-71 83 3 ( ( PUNCT eurjchem-71 83 4 ν ν NOUN eurjchem-71 83 5 ): ): NOUN eurjchem-71 83 6     SPACE eurjchem-71 83 7 br br PROPN eurjchem-71 83 8 . . PUNCT eurjchem-71 83 9     SPACE eurjchem-71 83 10 3480‐2500 3480‐2500 NUM eurjchem-71 83 11     SPACE eurjchem-71 83 12 cm‐1 cm‐1 NOUN eurjchem-71 83 13     SPACE eurjchem-71 83 14 ( ( PUNCT eurjchem-71 83 15 ohacid ohacid ADJ eurjchem-71 83 16 ) ) PUNCT eurjchem-71 83 17 , , PUNCT eurjchem-71 83 18     SPACE eurjchem-71 83 19 1717 1717 NUM eurjchem-71 83 20 , , PUNCT eurjchem-71 83 21     SPACE eurjchem-71 83 22 1700 1700 NUM eurjchem-71 83 23     SPACE eurjchem-71 83 24 cm‐1 cm‐1 NOUN eurjchem-71 83 25     SPACE eurjchem-71 83 26 ( ( PUNCT eurjchem-71 83 27 c c NOUN eurjchem-71 83 28 = = NOUN eurjchem-71 83 29 o o NOUN eurjchem-71 83 30 ) ) PUNCT eurjchem-71 83 31 . . PUNCT eurjchem-71 83 32     SPACE eurjchem-71 84 1 1h‐nmr 1h‐nmr NUM eurjchem-71 84 2     SPACE eurjchem-71 84 3 ( ( PUNCT eurjchem-71 84 4 dmso‐d6 dmso‐d6 NOUN eurjchem-71 84 5 ) ) PUNCT eurjchem-71 84 6     SPACE eurjchem-71 84 7 δ δ PROPN eurjchem-71 84 8     SPACE eurjchem-71 84 9 7.6‐6.5 7.6‐6.5 NUM eurjchem-71 84 10     SPACE eurjchem-71 84 11 ( ( PUNCT eurjchem-71 84 12 m m PROPN eurjchem-71 84 13 , , PUNCT eurjchem-71 84 14     SPACE eurjchem-71 84 15 12 12 NUM eurjchem-71 84 16     SPACE eurjchem-71 84 17 harom harom NOUN eurjchem-71 84 18 . . PUNCT eurjchem-71 84 19 ) ) PUNCT eurjchem-71 84 20 , , PUNCT eurjchem-71 84 21     SPACE eurjchem-71 84 22 5.67‐5.63 5.67‐5.63 NOUN eurjchem-71 84 23     SPACE eurjchem-71 84 24 ( ( PUNCT eurjchem-71 84 25 d d NOUN eurjchem-71 84 26 , , PUNCT eurjchem-71 84 27     SPACE eurjchem-71 84 28 ih ih X eurjchem-71 84 29 , , PUNCT eurjchem-71 84 30     SPACE eurjchem-71 84 31 j j PROPN eurjchem-71 84 32     SPACE eurjchem-71 84 33 = = NOUN eurjchem-71 84 34     SPACE eurjchem-71 84 35 12 12 NUM eurjchem-71 84 36     SPACE eurjchem-71 84 37 hz hz NOUN eurjchem-71 84 38 ) ) PUNCT eurjchem-71 84 39 , , PUNCT eurjchem-71 84 40     SPACE eurjchem-71 84 41 5.0‐4.97 5.0‐4.97 NOUN eurjchem-71 84 42     SPACE eurjchem-71 84 43 ( ( PUNCT eurjchem-71 84 44 d d NOUN eurjchem-71 84 45 , , PUNCT eurjchem-71 84 46     SPACE eurjchem-71 84 47 ih ih X eurjchem-71 84 48 , , PUNCT eurjchem-71 84 49     SPACE eurjchem-71 84 50 j j PROPN eurjchem-71 84 51     SPACE eurjchem-71 85 1 = = NOUN eurjchem-71 85 2     SPACE eurjchem-71 85 3 9 9 NUM eurjchem-71 85 4     SPACE eurjchem-71 85 5 hz hz NOUN eurjchem-71 85 6 ) ) PUNCT eurjchem-71 85 7 , , PUNCT eurjchem-71 85 8     SPACE eurjchem-71 85 9 3.69 3.69 NUM eurjchem-71 85 10     SPACE eurjchem-71 85 11 ( ( PUNCT eurjchem-71 85 12 s s PROPN eurjchem-71 85 13 , , PUNCT eurjchem-71 85 14     SPACE eurjchem-71 85 15 6h 6h NOUN eurjchem-71 85 16 , , PUNCT eurjchem-71 85 17     SPACE eurjchem-71 85 18 2ome 2ome NUM eurjchem-71 85 19 ) ) PUNCT eurjchem-71 85 20 . . PUNCT eurjchem-71 85 21     SPACE eurjchem-71 86 1 ms ms NOUN eurjchem-71 86 2 : : PUNCT eurjchem-71 86 3     SPACE eurjchem-71 86 4 328 328 NUM eurjchem-71 86 5     SPACE eurjchem-71 86 6 ( ( PUNCT eurjchem-71 86 7 [ [ X eurjchem-71 86 8 m‐phsh m‐phsh X eurjchem-71 86 9 ] ] X eurjchem-71 86 10 , , PUNCT eurjchem-71 86 11     SPACE eurjchem-71 86 12 5.5 5.5 NUM eurjchem-71 86 13 ) ) PUNCT eurjchem-71 86 14 , , PUNCT eurjchem-71 86 15     SPACE eurjchem-71 86 16 310 310 NUM eurjchem-71 86 17     SPACE eurjchem-71 86 18 ( ( PUNCT eurjchem-71 86 19 13 13 NUM eurjchem-71 86 20 ) ) PUNCT eurjchem-71 86 21 , , PUNCT eurjchem-71 86 22     SPACE eurjchem-71 86 23 151 151 NUM eurjchem-71 86 24     SPACE eurjchem-71 86 25 ( ( PUNCT eurjchem-71 86 26 19.9 19.9 NUM eurjchem-71 86 27 ) ) PUNCT eurjchem-71 86 28 , , PUNCT eurjchem-71 86 29     SPACE eurjchem-71 86 30 110 110 NUM eurjchem-71 86 31     SPACE eurjchem-71 86 32 ( ( PUNCT eurjchem-71 87 1 [ [ X eurjchem-71 87 2 phsh+ phsh+ X eurjchem-71 87 3 . . PUNCT eurjchem-71 87 4 ] ] X eurjchem-71 87 5 , , PUNCT eurjchem-71 87 6     SPACE eurjchem-71 87 7 61.6 61.6 NUM eurjchem-71 87 8 ) ) PUNCT eurjchem-71 87 9 , , PUNCT eurjchem-71 87 10     SPACE eurjchem-71 87 11 91 91 NUM eurjchem-71 87 12     SPACE eurjchem-71 87 13 ( ( PUNCT eurjchem-71 87 14 19.9 19.9 NUM eurjchem-71 87 15 ) ) PUNCT eurjchem-71 87 16 , , PUNCT eurjchem-71 87 17     SPACE eurjchem-71 87 18 65 65 NUM eurjchem-71 87 19     SPACE eurjchem-71 87 20 ( ( PUNCT eurjchem-71 87 21 26 26 NUM eurjchem-71 87 22 ) ) PUNCT eurjchem-71 87 23 . . PUNCT eurjchem-71 87 24     SPACE eurjchem-71 88 1 anal anal ADJ eurjchem-71 88 2 . . PUNCT eurjchem-71 88 3     SPACE eurjchem-71 88 4 calcd calcd NOUN eurjchem-71 88 5 . . PUNCT eurjchem-71 88 6     SPACE eurjchem-71 88 7 for for ADP eurjchem-71 88 8     SPACE eurjchem-71 88 9 c24h22o6s c24h22o6s NOUN eurjchem-71 88 10     SPACE eurjchem-71 88 11 ( ( PUNCT eurjchem-71 88 12 438.49 438.49 NUM eurjchem-71 88 13 ): ): PUNCT eurjchem-71 88 14     SPACE eurjchem-71 88 15 c c NOUN eurjchem-71 88 16 , , PUNCT eurjchem-71 88 17     SPACE eurjchem-71 88 18 65.74; 65.74; NUM eurjchem-71 88 19     SPACE eurjchem-71 88 20 h h NOUN eurjchem-71 88 21 , , PUNCT eurjchem-71 88 22     SPACE eurjchem-71 88 23 5.06 5.06 NUM eurjchem-71 88 24 ; ; PUNCT eurjchem-71 88 25     SPACE eurjchem-71 88 26 s s PROPN eurjchem-71 88 27 , , PUNCT eurjchem-71 88 28     SPACE eurjchem-71 88 29 7.31 7.31 NUM eurjchem-71 88 30 . . PUNCT eurjchem-71 88 31     SPACE eurjchem-71 88 32 found find VERB eurjchem-71 88 33 : : PUNCT eurjchem-71 88 34     SPACE eurjchem-71 88 35 c c X eurjchem-71 88 36 , , PUNCT eurjchem-71 88 37     SPACE eurjchem-71 88 38 65.46 65.46 NUM eurjchem-71 88 39 ; ; PUNCT eurjchem-71 88 40     SPACE eurjchem-71 88 41 h h NOUN eurjchem-71 88 42 , , PUNCT eurjchem-71 88 43     SPACE eurjchem-71 88 44 5.0 5.0 NUM eurjchem-71 88 45 ; ; PUNCT eurjchem-71 88 46     SPACE eurjchem-71 88 47 s s PROPN eurjchem-71 88 48 , , PUNCT eurjchem-71 88 49     SPACE eurjchem-71 88 50 7.62 7.62 NUM eurjchem-71 88 51 . . PUNCT eurjchem-71 88 52         SPACE eurjchem-71 88 53 2.11 2.11 NUM eurjchem-71 88 54 . . PUNCT eurjchem-71 88 55     SPACE eurjchem-71 88 56 ( ( PUNCT eurjchem-71 88 57 e)­2­(2­(4­methylbenzenesulfonamidocarbamoyl e)­2­(2­(4­methylbenzenesulfonamidocarbamoyl PROPN eurjchem-71 88 58 ) ) PUNCT eurjchem-71 88 59     SPACE eurjchem-71 88 60 phenyl)­3­(3,4­dimethoxyphenyl)­acrylic phenyl)­3­(3,4­dimethoxyphenyl)­acrylic ADJ eurjchem-71 88 61     SPACE eurjchem-71 88 62 acid acid NOUN eurjchem-71 88 63     SPACE eurjchem-71 88 64 ( ( PUNCT eurjchem-71 88 65 13 13 NUM eurjchem-71 88 66 ) ) PUNCT eurjchem-71 88 67         SPACE eurjchem-71 88 68 a a DET eurjchem-71 88 69     SPACE eurjchem-71 88 70 mixture mixture NOUN eurjchem-71 88 71     SPACE eurjchem-71 88 72 of of ADP eurjchem-71 88 73     SPACE eurjchem-71 88 74 compound compound NOUN eurjchem-71 88 75     SPACE eurjchem-71 88 76 2 2 NUM eurjchem-71 88 77     SPACE eurjchem-71 88 78 ( ( PUNCT eurjchem-71 88 79 3.1 3.1 NUM eurjchem-71 88 80     SPACE eurjchem-71 88 81 g g NOUN eurjchem-71 88 82 , , PUNCT eurjchem-71 88 83     SPACE eurjchem-71 88 84 0.01 0.01 NUM eurjchem-71 88 85     SPACE eurjchem-71 88 86 mole mole NOUN eurjchem-71 88 87 ) ) PUNCT eurjchem-71 88 88     SPACE eurjchem-71 88 89 and and CCONJ eurjchem-71 88 90     SPACE eurjchem-71 88 91 p‐ p‐ NOUN eurjchem-71 88 92 toluenesulfonohydrazide toluenesulfonohydrazide PROPN eurjchem-71 88 93     SPACE eurjchem-71 88 94 ( ( PUNCT eurjchem-71 88 95 1.86 1.86 NUM eurjchem-71 88 96     SPACE eurjchem-71 88 97 g g NOUN eurjchem-71 88 98 , , PUNCT eurjchem-71 88 99     SPACE eurjchem-71 88 100 0.01 0.01 NUM eurjchem-71 88 101     SPACE eurjchem-71 88 102 mole mole NOUN eurjchem-71 88 103 ) ) PUNCT eurjchem-71 88 104     SPACE eurjchem-71 88 105 in in ADP eurjchem-71 88 106     SPACE eurjchem-71 88 107 30 30 NUM eurjchem-71 88 108     SPACE eurjchem-71 88 109 ml ml NOUN eurjchem-71 88 110     SPACE eurjchem-71 88 111 dioxane dioxane NOUN eurjchem-71 88 112     SPACE eurjchem-71 88 113 was be AUX eurjchem-71 88 114     SPACE eurjchem-71 88 115 refluxed refluxe VERB eurjchem-71 88 116     SPACE eurjchem-71 88 117 for for ADP eurjchem-71 88 118     SPACE eurjchem-71 88 119 6 6 NUM eurjchem-71 88 120     SPACE eurjchem-71 88 121 h. h. NOUN eurjchem-71 88 122     SPACE eurjchem-71 88 123 after after ADP eurjchem-71 88 124     SPACE eurjchem-71 88 125 concentration concentration NOUN eurjchem-71 88 126     SPACE eurjchem-71 88 127 of of ADP eurjchem-71 88 128     SPACE eurjchem-71 88 129 the the DET eurjchem-71 88 130     SPACE eurjchem-71 88 131 solvent solvent NOUN eurjchem-71 88 132 , , PUNCT eurjchem-71 88 133     SPACE eurjchem-71 88 134 a a DET eurjchem-71 88 135     SPACE eurjchem-71 88 136 yellow yellow ADJ eurjchem-71 88 137     SPACE eurjchem-71 88 138 solid solid NOUN eurjchem-71 88 139     SPACE eurjchem-71 88 140 was be AUX eurjchem-71 88 141     SPACE eurjchem-71 88 142 deposited deposit VERB eurjchem-71 88 143     SPACE eurjchem-71 88 144 then then ADV eurjchem-71 88 145     SPACE eurjchem-71 88 146 filtered filter VERB eurjchem-71 88 147     SPACE eurjchem-71 88 148 off off ADP eurjchem-71 88 149 , , PUNCT eurjchem-71 88 150     SPACE eurjchem-71 88 151 dried dry VERB eurjchem-71 88 152     SPACE eurjchem-71 88 153 and and CCONJ eurjchem-71 88 154     SPACE eurjchem-71 88 155 recrystallized recrystallize VERB eurjchem-71 88 156     SPACE eurjchem-71 88 157 from from ADP eurjchem-71 88 158     SPACE eurjchem-71 88 159 benzene benzene NOUN eurjchem-71 88 160 / / SYM eurjchem-71 88 161 ethanol ethanol NOUN eurjchem-71 88 162     SPACE eurjchem-71 88 163 to to PART eurjchem-71 88 164     SPACE eurjchem-71 88 165 give give VERB eurjchem-71 88 166     SPACE eurjchem-71 88 167 13 13 NUM eurjchem-71 88 168     SPACE eurjchem-71 88 169 as as ADP eurjchem-71 88 170     SPACE eurjchem-71 88 171 yellow yellow ADJ eurjchem-71 88 172     SPACE eurjchem-71 88 173 crystals crystal NOUN eurjchem-71 88 174 . . PUNCT eurjchem-71 88 175     SPACE eurjchem-71 89 1 m.p m.p PROPN eurjchem-71 89 2 . . PROPN eurjchem-71 89 3 : : PUNCT eurjchem-71 89 4     SPACE eurjchem-71 89 5 168‐170oc 168‐170oc NUM eurjchem-71 89 6 , , PUNCT eurjchem-71 89 7     SPACE eurjchem-71 89 8 yield yield NOUN eurjchem-71 89 9     SPACE eurjchem-71 89 10 68 68 NUM eurjchem-71 89 11 % % NOUN eurjchem-71 89 12 . . PUNCT eurjchem-71 89 13     SPACE eurjchem-71 90 1 ir ir VERB eurjchem-71 90 2     SPACE eurjchem-71 90 3 ( ( PUNCT eurjchem-71 90 4 ν ν X eurjchem-71 90 5 ): ): NOUN eurjchem-71 90 6     SPACE eurjchem-71 90 7 3350‐2530 3350‐2530 NUM eurjchem-71 90 8     SPACE eurjchem-71 90 9 cm‐1 cm‐1 NOUN eurjchem-71 90 10     SPACE eurjchem-71 90 11 ( ( PUNCT eurjchem-71 90 12 oh oh INTJ eurjchem-71 90 13 ) ) PUNCT eurjchem-71 90 14 , , PUNCT eurjchem-71 90 15     SPACE eurjchem-71 90 16 3315 3315 NUM eurjchem-71 90 17     SPACE eurjchem-71 90 18 cm‐1 cm‐1 NOUN eurjchem-71 90 19     SPACE eurjchem-71 90 20 ( ( PUNCT eurjchem-71 90 21 nh nh NOUN eurjchem-71 90 22 ) ) PUNCT eurjchem-71 90 23 , , PUNCT eurjchem-71 90 24     SPACE eurjchem-71 90 25 1699 1699 NUM eurjchem-71 90 26     SPACE eurjchem-71 90 27 cm‐1 cm‐1 NOUN eurjchem-71 90 28     SPACE eurjchem-71 90 29 ( ( PUNCT eurjchem-71 90 30 c c NOUN eurjchem-71 90 31 = = NOUN eurjchem-71 90 32 oacid oacid NOUN eurjchem-71 90 33 ) ) PUNCT eurjchem-71 90 34 , , PUNCT eurjchem-71 90 35     SPACE eurjchem-71 90 36 1676 1676 NUM eurjchem-71 90 37     SPACE eurjchem-71 90 38 cm‐1 cm‐1 NOUN eurjchem-71 90 39     SPACE eurjchem-71 90 40 ( ( PUNCT eurjchem-71 90 41 c c NOUN eurjchem-71 90 42 = = NOUN eurjchem-71 90 43 oacid oacid NOUN eurjchem-71 90 44     SPACE eurjchem-71 90 45 hydrazide hydrazide ADV eurjchem-71 90 46 ) ) PUNCT eurjchem-71 90 47 . . PUNCT eurjchem-71 90 48     SPACE eurjchem-71 91 1 ms ms NOUN eurjchem-71 91 2 : : PUNCT eurjchem-71 91 3     SPACE eurjchem-71 91 4 330 330 NUM eurjchem-71 91 5     SPACE eurjchem-71 91 6 ( ( PUNCT eurjchem-71 91 7 11.3 11.3 NUM eurjchem-71 91 8 ) ) PUNCT eurjchem-71 91 9 , , PUNCT eurjchem-71 91 10     SPACE eurjchem-71 91 11 186 186 NUM eurjchem-71 91 12     SPACE eurjchem-71 91 13 ( ( PUNCT eurjchem-71 91 14 28.0 28.0 NUM eurjchem-71 91 15 ) ) PUNCT eurjchem-71 91 16 , , PUNCT eurjchem-71 91 17     SPACE eurjchem-71 91 18 163 163 NUM eurjchem-71 91 19     SPACE eurjchem-71 91 20 ( ( PUNCT eurjchem-71 91 21 47.5 47.5 NUM eurjchem-71 91 22 ) ) PUNCT eurjchem-71 91 23 , , PUNCT eurjchem-71 91 24     SPACE eurjchem-71 91 25 135 135 NUM eurjchem-71 91 26     SPACE eurjchem-71 91 27 ( ( PUNCT eurjchem-71 91 28 94.7 94.7 NUM eurjchem-71 91 29 ) ) PUNCT eurjchem-71 91 30 , , PUNCT eurjchem-71 91 31     SPACE eurjchem-71 91 32 91 91 NUM eurjchem-71 91 33     SPACE eurjchem-71 91 34 ( ( PUNCT eurjchem-71 91 35 100 100 NUM eurjchem-71 91 36 ) ) PUNCT eurjchem-71 91 37 , , PUNCT eurjchem-71 91 38     SPACE eurjchem-71 91 39 65 65 NUM eurjchem-71 91 40     SPACE eurjchem-71 91 41 ( ( PUNCT eurjchem-71 91 42 65.5 65.5 NUM eurjchem-71 91 43 ) ) PUNCT eurjchem-71 91 44 . . PUNCT eurjchem-71 91 45     SPACE eurjchem-71 92 1 anal anal ADJ eurjchem-71 92 2 . . PUNCT eurjchem-71 92 3     SPACE eurjchem-71 92 4 calcd calcd NOUN eurjchem-71 92 5 . . PUNCT eurjchem-71 92 6     SPACE eurjchem-71 92 7 for for ADP eurjchem-71 92 8     SPACE eurjchem-71 92 9 c25h24n2o7s c25h24n2o7s NOUN eurjchem-71 92 10     SPACE eurjchem-71 92 11 ( ( PUNCT eurjchem-71 92 12 496.53 496.53 NUM eurjchem-71 92 13 ): ): PUNCT eurjchem-71 92 14     SPACE eurjchem-71 92 15 c c NOUN eurjchem-71 92 16 , , PUNCT eurjchem-71 92 17     SPACE eurjchem-71 92 18 60.47; 60.47; NOUN eurjchem-71 92 19     SPACE eurjchem-71 92 20 h h NOUN eurjchem-71 92 21 , , PUNCT eurjchem-71 92 22     SPACE eurjchem-71 92 23 4.87 4.87 NUM eurjchem-71 92 24 ; ; PUNCT eurjchem-71 92 25     SPACE eurjchem-71 92 26 n n CCONJ eurjchem-71 92 27 , , PUNCT eurjchem-71 92 28     SPACE eurjchem-71 92 29 5.64 5.64 NUM eurjchem-71 92 30 ; ; PUNCT eurjchem-71 92 31     SPACE eurjchem-71 92 32 s s PROPN eurjchem-71 92 33 , , PUNCT eurjchem-71 92 34     SPACE eurjchem-71 92 35 6.46 6.46 NUM eurjchem-71 92 36 . . PUNCT eurjchem-71 92 37     SPACE eurjchem-71 92 38 found find VERB eurjchem-71 92 39 : : PUNCT eurjchem-71 92 40     SPACE eurjchem-71 92 41 c c X eurjchem-71 92 42 , , PUNCT eurjchem-71 92 43     SPACE eurjchem-71 92 44 60.73 60.73 NUM eurjchem-71 92 45 ; ; PUNCT eurjchem-71 92 46     SPACE eurjchem-71 92 47 h h NOUN eurjchem-71 92 48 , , PUNCT eurjchem-71 92 49     SPACE eurjchem-71 92 50 4.77 4.77 NUM eurjchem-71 92 51 ; ; PUNCT eurjchem-71 92 52     SPACE eurjchem-71 92 53 n n CCONJ eurjchem-71 92 54 , , PUNCT eurjchem-71 92 55     SPACE eurjchem-71 92 56 5.45 5.45 NUM eurjchem-71 92 57 ; ; PUNCT eurjchem-71 92 58     SPACE eurjchem-71 92 59 s s PROPN eurjchem-71 92 60 , , PUNCT eurjchem-71 92 61     SPACE eurjchem-71 92 62 6.24 6.24 NUM eurjchem-71 92 63 . . PUNCT eurjchem-71 92 64         SPACE eurjchem-71 93 1 2.12 2.12 NUM eurjchem-71 93 2 . . PUNCT eurjchem-71 93 3     SPACE eurjchem-71 93 4 ethyl­α­cyano­3,4­dimethoxy ethyl­α­cyano­3,4­dimethoxy ADJ eurjchem-71 93 5     SPACE eurjchem-71 93 6 cinnamate cinnamate NOUN eurjchem-71 93 7     SPACE eurjchem-71 93 8 ( ( PUNCT eurjchem-71 93 9 14 14 NUM eurjchem-71 93 10 ) ) PUNCT eurjchem-71 93 11         SPACE eurjchem-71 93 12 a a DET eurjchem-71 93 13     SPACE eurjchem-71 93 14 mixture mixture NOUN eurjchem-71 93 15     SPACE eurjchem-71 93 16 of of ADP eurjchem-71 93 17     SPACE eurjchem-71 93 18 compound compound NOUN eurjchem-71 93 19     SPACE eurjchem-71 93 20 2 2 NUM eurjchem-71 93 21     SPACE eurjchem-71 93 22 ( ( PUNCT eurjchem-71 93 23 3.1 3.1 NUM eurjchem-71 93 24     SPACE eurjchem-71 93 25 g g NOUN eurjchem-71 93 26 , , PUNCT eurjchem-71 93 27     SPACE eurjchem-71 93 28 0.01 0.01 NUM eurjchem-71 93 29     SPACE eurjchem-71 93 30 mole mole NOUN eurjchem-71 93 31 ) ) PUNCT eurjchem-71 93 32     SPACE eurjchem-71 93 33 and and CCONJ eurjchem-71 93 34     SPACE eurjchem-71 93 35 ethyl ethyl NOUN eurjchem-71 93 36     SPACE eurjchem-71 93 37 cyanoacetate cyanoacetate NOUN eurjchem-71 93 38     SPACE eurjchem-71 93 39 ( ( PUNCT eurjchem-71 93 40 1.13 1.13 NUM eurjchem-71 93 41     SPACE eurjchem-71 93 42 ml ml NOUN eurjchem-71 93 43 , , PUNCT eurjchem-71 93 44     SPACE eurjchem-71 93 45 0.01 0.01 NUM eurjchem-71 93 46     SPACE eurjchem-71 93 47 mole mole NOUN eurjchem-71 93 48 ) ) PUNCT eurjchem-71 93 49     SPACE eurjchem-71 93 50 in in ADP eurjchem-71 93 51     SPACE eurjchem-71 93 52 30 30 NUM eurjchem-71 93 53     SPACE eurjchem-71 93 54 ml ml NOUN eurjchem-71 93 55     SPACE eurjchem-71 93 56 dioxane dioxane NOUN eurjchem-71 93 57     SPACE eurjchem-71 93 58 in in ADP eurjchem-71 93 59     SPACE eurjchem-71 93 60 the the DET eurjchem-71 93 61     SPACE eurjchem-71 93 62 presence presence NOUN eurjchem-71 93 63     SPACE eurjchem-71 93 64 of of ADP eurjchem-71 93 65     SPACE eurjchem-71 93 66 drops drop NOUN eurjchem-71 93 67     SPACE eurjchem-71 93 68 of of ADP eurjchem-71 93 69     SPACE eurjchem-71 93 70 triethylamine triethylamine NOUN eurjchem-71 93 71     SPACE eurjchem-71 93 72 was be AUX eurjchem-71 93 73     SPACE eurjchem-71 93 74 refluxed refluxe VERB eurjchem-71 93 75     SPACE eurjchem-71 93 76 for for ADP eurjchem-71 93 77     SPACE eurjchem-71 93 78 3 3 NUM eurjchem-71 93 79     SPACE eurjchem-71 93 80 h. h. NOUN eurjchem-71 93 81     SPACE eurjchem-71 93 82 after after ADP eurjchem-71 93 83     SPACE eurjchem-71 93 84 concentration concentration NOUN eurjchem-71 93 85     SPACE eurjchem-71 93 86 of of ADP eurjchem-71 93 87     SPACE eurjchem-71 93 88 the the DET eurjchem-71 93 89     SPACE eurjchem-71 93 90 solvent solvent NOUN eurjchem-71 93 91 , , PUNCT eurjchem-71 93 92     SPACE eurjchem-71 93 93 a a DET eurjchem-71 93 94     SPACE eurjchem-71 93 95 pale pale ADJ eurjchem-71 93 96     SPACE eurjchem-71 93 97 yellow yellow ADJ eurjchem-71 93 98     SPACE eurjchem-71 93 99 solid solid NOUN eurjchem-71 93 100     SPACE eurjchem-71 93 101 was be AUX eurjchem-71 93 102     SPACE eurjchem-71 93 103 deposited deposit VERB eurjchem-71 93 104     SPACE eurjchem-71 93 105 then then ADV eurjchem-71 93 106     SPACE eurjchem-71 93 107 filtered filter VERB eurjchem-71 93 108     SPACE eurjchem-71 93 109 off off ADP eurjchem-71 93 110 , , PUNCT eurjchem-71 93 111     SPACE eurjchem-71 93 112 dried dry VERB eurjchem-71 93 113     SPACE eurjchem-71 93 114 and and CCONJ eurjchem-71 93 115     SPACE eurjchem-71 93 116 recrystallized recrystallize VERB eurjchem-71 93 117     SPACE eurjchem-71 93 118 from from ADP eurjchem-71 93 119     SPACE eurjchem-71 93 120 ethanol ethanol NOUN eurjchem-71 93 121     SPACE eurjchem-71 93 122 to to PART eurjchem-71 93 123     SPACE eurjchem-71 93 124 give give VERB eurjchem-71 93 125     SPACE eurjchem-71 93 126 14 14 NUM eurjchem-71 93 127     SPACE eurjchem-71 93 128 as as ADP eurjchem-71 93 129     SPACE eurjchem-71 93 130 pale pale ADJ eurjchem-71 93 131     SPACE eurjchem-71 93 132 yellow yellow ADJ eurjchem-71 93 133     SPACE eurjchem-71 93 134 crystals crystal NOUN eurjchem-71 93 135 . . PUNCT eurjchem-71 93 136     SPACE eurjchem-71 94 1 m.p m.p PROPN eurjchem-71 94 2 . . PROPN eurjchem-71 94 3 : : PUNCT eurjchem-71 94 4     SPACE eurjchem-71 94 5 138‐140oc 138‐140oc NUM eurjchem-71 94 6 , , PUNCT eurjchem-71 94 7     SPACE eurjchem-71 94 8 yield yield NOUN eurjchem-71 94 9     SPACE eurjchem-71 94 10 77 77 NUM eurjchem-71 94 11 % % NOUN eurjchem-71 94 12 . . PUNCT eurjchem-71 94 13     SPACE eurjchem-71 95 1 ir ir VERB eurjchem-71 95 2     SPACE eurjchem-71 95 3 ( ( PUNCT eurjchem-71 95 4 ν ν NOUN eurjchem-71 95 5 ): ): NOUN eurjchem-71 95 6     SPACE eurjchem-71 95 7 2221 2221 NUM eurjchem-71 95 8     SPACE eurjchem-71 95 9 cm‐1 cm‐1 NOUN eurjchem-71 95 10     SPACE eurjchem-71 95 11 ( ( PUNCT eurjchem-71 95 12 c≡n c≡n PROPN eurjchem-71 95 13 ) ) PUNCT eurjchem-71 95 14 , , PUNCT eurjchem-71 95 15     SPACE eurjchem-71 95 16 1713 1713 NUM eurjchem-71 95 17     SPACE eurjchem-71 95 18 cm‐1 cm‐1 NOUN eurjchem-71 95 19     SPACE eurjchem-71 95 20 ( ( PUNCT eurjchem-71 95 21 c c NOUN eurjchem-71 95 22 = = NOUN eurjchem-71 95 23 oester oester NOUN eurjchem-71 95 24 ) ) PUNCT eurjchem-71 95 25 . . PUNCT eurjchem-71 95 26     SPACE eurjchem-71 96 1 ms ms NOUN eurjchem-71 96 2 : : PUNCT eurjchem-71 96 3     SPACE eurjchem-71 96 4 261 261 NUM eurjchem-71 96 5     SPACE eurjchem-71 96 6 ( ( PUNCT eurjchem-71 96 7 100 100 NUM eurjchem-71 96 8 ) ) PUNCT eurjchem-71 96 9 . . PUNCT eurjchem-71 96 10     SPACE eurjchem-71 97 1 anal anal ADJ eurjchem-71 97 2 . . PUNCT eurjchem-71 97 3     SPACE eurjchem-71 97 4 calcd calcd NOUN eurjchem-71 97 5 . . PUNCT eurjchem-71 97 6     SPACE eurjchem-71 97 7 for for ADP eurjchem-71 97 8     SPACE eurjchem-71 97 9 c14h15no4 c14h15no4 NOUN eurjchem-71 97 10     SPACE eurjchem-71 97 11 ( ( PUNCT eurjchem-71 97 12 261.27 261.27 NUM eurjchem-71 97 13 ): ): PUNCT eurjchem-71 97 14     SPACE eurjchem-71 97 15 c c NOUN eurjchem-71 97 16 , , PUNCT eurjchem-71 97 17     SPACE eurjchem-71 97 18 64.36; 64.36; NOUN eurjchem-71 97 19     SPACE eurjchem-71 97 20 h h NOUN eurjchem-71 97 21 , , PUNCT eurjchem-71 97 22     SPACE eurjchem-71 97 23 5.79 5.79 NUM eurjchem-71 97 24 ; ; PUNCT eurjchem-71 97 25     SPACE eurjchem-71 97 26 n n CCONJ eurjchem-71 97 27 , , PUNCT eurjchem-71 97 28     SPACE eurjchem-71 97 29 5.36 5.36 NUM eurjchem-71 97 30 . . PUNCT eurjchem-71 97 31     SPACE eurjchem-71 97 32 found find VERB eurjchem-71 97 33 : : PUNCT eurjchem-71 97 34     SPACE eurjchem-71 97 35 c c X eurjchem-71 97 36 , , PUNCT eurjchem-71 97 37     SPACE eurjchem-71 97 38 64.6 64.6 NUM eurjchem-71 97 39 ; ; PUNCT eurjchem-71 97 40     SPACE eurjchem-71 97 41 h h NOUN eurjchem-71 97 42 , , PUNCT eurjchem-71 97 43     SPACE eurjchem-71 97 44 5.71 5.71 NUM eurjchem-71 97 45 ; ; PUNCT eurjchem-71 97 46     SPACE eurjchem-71 97 47 n n CCONJ eurjchem-71 97 48 , , PUNCT eurjchem-71 97 49     SPACE eurjchem-71 97 50 5.34 5.34 NUM eurjchem-71 97 51 . . PUNCT eurjchem-71 97 52         SPACE eurjchem-71 98 1 3 3 NUM eurjchem-71 98 2 . . PUNCT eurjchem-71 98 3     SPACE eurjchem-71 98 4 results result VERB eurjchem-71 98 5     SPACE eurjchem-71 98 6 and and CCONJ eurjchem-71 98 7     SPACE eurjchem-71 98 8 discussion discussion NOUN eurjchem-71 98 9         SPACE eurjchem-71 98 10 3.1 3.1 NUM eurjchem-71 98 11 . . PUNCT eurjchem-71 98 12     SPACE eurjchem-71 98 13 chemistry chemistry NOUN eurjchem-71 98 14         SPACE eurjchem-71 98 15 attempted attempt VERB eurjchem-71 98 16     SPACE eurjchem-71 98 17 cyclization cyclization NOUN eurjchem-71 98 18     SPACE eurjchem-71 98 19 of of ADP eurjchem-71 98 20     SPACE eurjchem-71 98 21 1 1 NUM eurjchem-71 98 22     SPACE eurjchem-71 98 23 using use VERB eurjchem-71 98 24     SPACE eurjchem-71 98 25 acetyl acetyl NOUN eurjchem-71 98 26     SPACE eurjchem-71 98 27 chloride chloride NOUN eurjchem-71 98 28     SPACE eurjchem-71 98 29 for for ADP eurjchem-71 98 30     SPACE eurjchem-71 98 31 15 15 NUM eurjchem-71 98 32     SPACE eurjchem-71 98 33 min min NOUN eurjchem-71 98 34 . . PROPN eurjchem-71 98 35     SPACE eurjchem-71 98 36 produced produce VERB eurjchem-71 98 37     SPACE eurjchem-71 98 38 ( ( PUNCT eurjchem-71 98 39 e)‐4‐(3,4‐dimethoxybenzylidene)‐4h‐isochromene‐ e)‐4‐(3,4‐dimethoxybenzylidene)‐4h‐isochromene‐ PROPN eurjchem-71 98 40 1,3‐dione 1,3‐dione NUM eurjchem-71 98 41     SPACE eurjchem-71 98 42 2 2 NUM eurjchem-71 98 43     SPACE eurjchem-71 98 44 as as ADP eurjchem-71 98 45     SPACE eurjchem-71 98 46 the the DET eurjchem-71 98 47     SPACE eurjchem-71 98 48 sole sole ADJ eurjchem-71 98 49     SPACE eurjchem-71 98 50 product product NOUN eurjchem-71 98 51     SPACE eurjchem-71 98 52 ( ( PUNCT eurjchem-71 98 53 yield yield VERB eurjchem-71 98 54     SPACE eurjchem-71 98 55 90 90 NUM eurjchem-71 98 56 % % NOUN eurjchem-71 98 57 ) ) PUNCT eurjchem-71 98 58 . . PUNCT eurjchem-71 98 59     SPACE eurjchem-71 99 1 the the DET eurjchem-71 99 2     SPACE eurjchem-71 99 3 formation formation NOUN eurjchem-71 99 4     SPACE eurjchem-71 99 5 of of ADP eurjchem-71 99 6     SPACE eurjchem-71 99 7 the the DET eurjchem-71 99 8     SPACE eurjchem-71 99 9 e‐isomer e‐isomer NOUN eurjchem-71 99 10     SPACE eurjchem-71 99 11 2 2 NUM eurjchem-71 99 12     SPACE eurjchem-71 99 13 may may AUX eurjchem-71 99 14     SPACE eurjchem-71 99 15 be be AUX eurjchem-71 99 16     SPACE eurjchem-71 99 17 attributed attribute VERB eurjchem-71 99 18     SPACE eurjchem-71 99 19 to to ADP eurjchem-71 99 20     SPACE eurjchem-71 99 21 the the DET eurjchem-71 99 22     SPACE eurjchem-71 99 23 cis‐trans cis‐tran NOUN eurjchem-71 99 24     SPACE eurjchem-71 99 25 isomerization isomerization NOUN eurjchem-71 99 26     SPACE eurjchem-71 99 27 which which PRON eurjchem-71 99 28     SPACE eurjchem-71 99 29 understandable understandable ADJ eurjchem-71 99 30     SPACE eurjchem-71 99 31 in in ADP eurjchem-71 99 32     SPACE eurjchem-71 99 33 view view NOUN eurjchem-71 99 34     SPACE eurjchem-71 99 35 of of ADP eurjchem-71 99 36     SPACE eurjchem-71 99 37 the the DET eurjchem-71 99 38     SPACE eurjchem-71 99 39 drastic drastic ADJ eurjchem-71 99 40     SPACE eurjchem-71 99 41 acidic acidic ADJ eurjchem-71 99 42     SPACE eurjchem-71 99 43 reaction reaction NOUN eurjchem-71 99 44     SPACE eurjchem-71 99 45 conditions condition NOUN eurjchem-71 99 46 , , PUNCT eurjchem-71 99 47     SPACE eurjchem-71 99 48 being be AUX eurjchem-71 99 49     SPACE eurjchem-71 99 50 hcl hcl PROPN eurjchem-71 99 51     SPACE eurjchem-71 99 52 liberated liberate VERB eurjchem-71 99 53     SPACE eurjchem-71 99 54 during during ADP eurjchem-71 99 55     SPACE eurjchem-71 99 56 anhydride anhydride NOUN eurjchem-71 99 57     SPACE eurjchem-71 99 58 formation formation NOUN eurjchem-71 99 59 . . PUNCT eurjchem-71 99 60     SPACE eurjchem-71 100 1 complications complication NOUN eurjchem-71 100 2     SPACE eurjchem-71 100 3 due due ADJ eurjchem-71 100 4     SPACE eurjchem-71 100 5 to to PART eurjchem-71 100 6     SPACE eurjchem-71 100 7 isomerization isomerization NOUN eurjchem-71 100 8     SPACE eurjchem-71 100 9 were be AUX eurjchem-71 100 10     SPACE eurjchem-71 100 11 overcome overcome VERB eurjchem-71 100 12     SPACE eurjchem-71 100 13 by by ADP eurjchem-71 100 14     SPACE eurjchem-71 100 15 the the DET eurjchem-71 100 16     SPACE eurjchem-71 100 17 use use NOUN eurjchem-71 100 18     SPACE eurjchem-71 100 19 of of ADP eurjchem-71 100 20     SPACE eurjchem-71 100 21 dcc dcc NOUN eurjchem-71 100 22     SPACE eurjchem-71 100 23 as as ADP eurjchem-71 100 24     SPACE eurjchem-71 100 25 dehydrating dehydrate VERB eurjchem-71 100 26     SPACE eurjchem-71 100 27 agent agent NOUN eurjchem-71 100 28     SPACE eurjchem-71 100 29 which which PRON eurjchem-71 100 30     SPACE eurjchem-71 100 31 gave give VERB eurjchem-71 100 32     SPACE eurjchem-71 100 33 3 3 NUM eurjchem-71 100 34     SPACE eurjchem-71 100 35 as as ADP eurjchem-71 100 36     SPACE eurjchem-71 100 37 the the DET eurjchem-71 100 38     SPACE eurjchem-71 100 39 sole sole ADJ eurjchem-71 100 40     SPACE eurjchem-71 100 41 product product NOUN eurjchem-71 100 42     SPACE eurjchem-71 100 43 ( ( PUNCT eurjchem-71 100 44 scheme scheme NOUN eurjchem-71 100 45     SPACE eurjchem-71 100 46 4 4 NUM eurjchem-71 100 47 ) ) PUNCT eurjchem-71 100 48 . . PUNCT eurjchem-71 100 49     SPACE eurjchem-71 101 1 cyclization cyclization NOUN eurjchem-71 101 2     SPACE eurjchem-71 101 3 to to PART eurjchem-71 101 4     SPACE eurjchem-71 101 5 compounds compound VERB eurjchem-71 101 6     SPACE eurjchem-71 101 7 2 2 NUM eurjchem-71 101 8     SPACE eurjchem-71 101 9 and and CCONJ eurjchem-71 101 10     SPACE eurjchem-71 101 11 3 3 NUM eurjchem-71 101 12     SPACE eurjchem-71 101 13 was be AUX eurjchem-71 101 14     SPACE eurjchem-71 101 15 inferred infer VERB eurjchem-71 101 16     SPACE eurjchem-71 101 17 from from ADP eurjchem-71 101 18     SPACE eurjchem-71 101 19 the the DET eurjchem-71 101 20     SPACE eurjchem-71 101 21 ir ir PROPN eurjchem-71 101 22     SPACE eurjchem-71 101 23 spectra spectra NOUN eurjchem-71 101 24     SPACE eurjchem-71 101 25 which which PRON eurjchem-71 101 26     SPACE eurjchem-71 101 27 displayed display VERB eurjchem-71 101 28     SPACE eurjchem-71 101 29 the the DET eurjchem-71 101 30     SPACE eurjchem-71 101 31 carbonyl carbonyl NOUN eurjchem-71 101 32     SPACE eurjchem-71 101 33 coupling coupling NOUN eurjchem-71 101 34     SPACE eurjchem-71 101 35 bands band NOUN eurjchem-71 101 36     SPACE eurjchem-71 101 37 expected expect VERB eurjchem-71 101 38     SPACE eurjchem-71 101 39 for for ADP eurjchem-71 101 40     SPACE eurjchem-71 101 41 the the DET eurjchem-71 101 42     SPACE eurjchem-71 101 43 six‐membered six‐membere VERB eurjchem-71 101 44     SPACE eurjchem-71 101 45 anhydride anhydride NOUN eurjchem-71 101 46     SPACE eurjchem-71 101 47 with with ADP eurjchem-71 101 48     SPACE eurjchem-71 101 49 α α NOUN eurjchem-71 101 50 , , PUNCT eurjchem-71 101 51 β‐conjugation β‐conjugation PUNCT eurjchem-71 101 52 . . PUNCT eurjchem-71 101 53     SPACE eurjchem-71 101 54 analysis analysis NOUN eurjchem-71 101 55     SPACE eurjchem-71 101 56 of of ADP eurjchem-71 101 57     SPACE eurjchem-71 101 58 the the DET eurjchem-71 101 59     SPACE eurjchem-71 101 60 observed observe VERB eurjchem-71 101 61     SPACE eurjchem-71 101 62 signals signal NOUN eurjchem-71 101 63     SPACE eurjchem-71 101 64 in in ADP eurjchem-71 101 65     SPACE eurjchem-71 101 66 the the DET eurjchem-71 101 67     SPACE eurjchem-71 101 68 1h‐nmr 1h‐nmr NUM eurjchem-71 101 69     SPACE eurjchem-71 101 70 spectra spectra NOUN eurjchem-71 101 71     SPACE eurjchem-71 101 72 of of ADP eurjchem-71 101 73     SPACE eurjchem-71 101 74 2 2 NUM eurjchem-71 101 75     SPACE eurjchem-71 101 76 and and CCONJ eurjchem-71 101 77     SPACE eurjchem-71 101 78 3 3 NUM eurjchem-71 101 79     SPACE eurjchem-71 101 80 revealed reveal VERB eurjchem-71 101 81     SPACE eurjchem-71 101 82 a a DET eurjchem-71 101 83     SPACE eurjchem-71 101 84 singlet singlet NOUN eurjchem-71 101 85     SPACE eurjchem-71 101 86 for for ADP eurjchem-71 101 87     SPACE eurjchem-71 101 88 ethylenic ethylenic NOUN eurjchem-71 101 89     SPACE eurjchem-71 101 90 proton proton NOUN eurjchem-71 101 91     SPACE eurjchem-71 101 92 with with ADP eurjchem-71 101 93     SPACE eurjchem-71 101 94 down down ADP eurjchem-71 101 95     SPACE eurjchem-71 101 96 field field NOUN eurjchem-71 101 97     SPACE eurjchem-71 101 98 chemical chemical NOUN eurjchem-71 101 99     SPACE eurjchem-71 101 100 shift shift NOUN eurjchem-71 101 101     SPACE eurjchem-71 101 102 at at ADP eurjchem-71 101 103     SPACE eurjchem-71 101 104 δ δ PROPN eurjchem-71 101 105     SPACE eurjchem-71 101 106 = = NOUN eurjchem-71 101 107     SPACE eurjchem-71 101 108 6.9 6.9 NUM eurjchem-71 101 109     SPACE eurjchem-71 101 110 ppm ppm NOUN eurjchem-71 101 111     SPACE eurjchem-71 101 112 which which PRON eurjchem-71 101 113     SPACE eurjchem-71 101 114 may may AUX eurjchem-71 101 115     SPACE eurjchem-71 101 116 suffer suffer VERB eurjchem-71 101 117     SPACE eurjchem-71 101 118 from from ADP eurjchem-71 101 119     SPACE eurjchem-71 101 120 the the DET eurjchem-71 101 121     SPACE eurjchem-71 101 122 shield shield NOUN eurjchem-71 101 123     SPACE eurjchem-71 101 124 effect effect NOUN eurjchem-71 101 125     SPACE eurjchem-71 101 126 of of ADP eurjchem-71 101 127     SPACE eurjchem-71 101 128 the the DET eurjchem-71 101 129     SPACE eurjchem-71 101 130 carbonyl carbonyl NOUN eurjchem-71 101 131     SPACE eurjchem-71 101 132 group group NOUN eurjchem-71 101 133 , , PUNCT eurjchem-71 101 134     SPACE eurjchem-71 101 135 and and CCONJ eurjchem-71 101 136     SPACE eurjchem-71 101 137 that that PRON eurjchem-71 101 138     SPACE eurjchem-71 101 139 of of ADP eurjchem-71 101 140     SPACE eurjchem-71 101 141 the the DET eurjchem-71 101 142     SPACE eurjchem-71 101 143 z‐isomer z‐isomer NOUN eurjchem-71 101 144     SPACE eurjchem-71 101 145 3 3 NUM eurjchem-71 101 146     SPACE eurjchem-71 101 147 at at ADP eurjchem-71 101 148     SPACE eurjchem-71 101 149 lower low ADJ eurjchem-71 101 150     SPACE eurjchem-71 101 151 value value NOUN eurjchem-71 101 152     SPACE eurjchem-71 101 153 ( ( PUNCT eurjchem-71 101 154 δ δ NOUN eurjchem-71 101 155     SPACE eurjchem-71 101 156 = = NOUN eurjchem-71 101 157     SPACE eurjchem-71 101 158 6.4 6.4 NUM eurjchem-71 101 159     SPACE eurjchem-71 101 160 ppm ppm NOUN eurjchem-71 101 161 ) ) PUNCT eurjchem-71 101 162 . . PUNCT eurjchem-71 101 163     SPACE eurjchem-71 102 1 [ [ X eurjchem-71 102 2 29,30 29,30 NUM eurjchem-71 102 3 ] ] PUNCT eurjchem-71 102 4     SPACE eurjchem-71 102 5 furthermore furthermore ADV eurjchem-71 102 6 , , PUNCT eurjchem-71 102 7     SPACE eurjchem-71 102 8 the the DET eurjchem-71 102 9     SPACE eurjchem-71 102 10 mass mass PROPN eurjchem-71 102 11     SPACE eurjchem-71 102 12 spectra spectra NOUN eurjchem-71 102 13     SPACE eurjchem-71 102 14 of of ADP eurjchem-71 102 15     SPACE eurjchem-71 102 16 2 2 NUM eurjchem-71 102 17     SPACE eurjchem-71 102 18 and and CCONJ eurjchem-71 102 19     SPACE eurjchem-71 102 20 3 3 NUM eurjchem-71 102 21     SPACE eurjchem-71 102 22 show show NOUN eurjchem-71 102 23     SPACE eurjchem-71 102 24 the the DET eurjchem-71 102 25     SPACE eurjchem-71 102 26 correct correct ADJ eurjchem-71 102 27     SPACE eurjchem-71 102 28 molecular molecular ADJ eurjchem-71 102 29     SPACE eurjchem-71 102 30 ion ion NOUN eurjchem-71 102 31     SPACE eurjchem-71 102 32 peak peak NOUN eurjchem-71 102 33     SPACE eurjchem-71 102 34 at at ADP eurjchem-71 102 35     SPACE eurjchem-71 102 36 m m PROPN eurjchem-71 102 37 / / PROPN eurjchem-71 102 38 z z NOUN eurjchem-71 102 39     SPACE eurjchem-71 102 40 = = NOUN eurjchem-71 102 41     SPACE eurjchem-71 102 42 310 310 NUM eurjchem-71 102 43     SPACE eurjchem-71 102 44 which which PRON eurjchem-71 102 45     SPACE eurjchem-71 102 46 is be AUX eurjchem-71 102 47     SPACE eurjchem-71 102 48 the the DET eurjchem-71 102 49     SPACE eurjchem-71 102 50 base base NOUN eurjchem-71 102 51     SPACE eurjchem-71 102 52 peak peak NOUN eurjchem-71 102 53 . . PUNCT eurjchem-71 102 54                       SPACE eurjchem-71 102 55 scheme scheme NOUN eurjchem-71 102 56     SPACE eurjchem-71 102 57 4 4 NUM eurjchem-71 102 58         SPACE eurjchem-71 102 59 a a DET eurjchem-71 102 60     SPACE eurjchem-71 102 61 number number NOUN eurjchem-71 102 62     SPACE eurjchem-71 102 63 of of ADP eurjchem-71 102 64     SPACE eurjchem-71 102 65 novel novel NOUN eurjchem-71 102 66     SPACE eurjchem-71 102 67 isoquinoline‐1,3‐diones isoquinoline‐1,3‐dione NOUN eurjchem-71 102 68     SPACE eurjchem-71 102 69 have have AUX eurjchem-71 102 70     SPACE eurjchem-71 102 71 been be AUX eurjchem-71 102 72     SPACE eurjchem-71 102 73 synthesized synthesize VERB eurjchem-71 102 74     SPACE eurjchem-71 102 75 using use VERB eurjchem-71 102 76     SPACE eurjchem-71 102 77 isochromen‐1,3‐dione isochromen‐1,3‐dione NUM eurjchem-71 102 78     SPACE eurjchem-71 102 79 2 2 NUM eurjchem-71 102 80     SPACE eurjchem-71 102 81 upon upon SCONJ eurjchem-71 102 82     SPACE eurjchem-71 102 83 treatment treatment NOUN eurjchem-71 102 84     SPACE eurjchem-71 102 85 with with ADP eurjchem-71 102 86     SPACE eurjchem-71 102 87 cyanoethanoic cyanoethanoic ADJ eurjchem-71 102 88     SPACE eurjchem-71 102 89 hydrazide hydrazide NOUN eurjchem-71 102 90     SPACE eurjchem-71 102 91 or or CCONJ eurjchem-71 102 92     SPACE eurjchem-71 102 93 cyclohexylamine cyclohexylamine NOUN eurjchem-71 102 94 . . PUNCT eurjchem-71 102 95     SPACE eurjchem-71 102 96 thus thus ADV eurjchem-71 102 97 , , PUNCT eurjchem-71 102 98     SPACE eurjchem-71 102 99 refluxing refluxing NOUN eurjchem-71 102 100     SPACE eurjchem-71 102 101 2 2 NUM eurjchem-71 102 102     SPACE eurjchem-71 102 103 with with ADP eurjchem-71 102 104     SPACE eurjchem-71 102 105 cyanoethanoic cyanoethanoic ADJ eurjchem-71 102 106     SPACE eurjchem-71 102 107 hydrazide hydrazide ADV eurjchem-71 102 108     SPACE eurjchem-71 102 109 in in ADP eurjchem-71 102 110     SPACE eurjchem-71 102 111 dioxane dioxane NOUN eurjchem-71 102 112     SPACE eurjchem-71 102 113 gave give VERB eurjchem-71 102 114     SPACE eurjchem-71 102 115 isoquinoline isoquinoline ADJ eurjchem-71 102 116     SPACE eurjchem-71 102 117 derivative derivative NOUN eurjchem-71 102 118     SPACE eurjchem-71 102 119 4 4 NUM eurjchem-71 102 120     SPACE eurjchem-71 102 121 together together ADV eurjchem-71 102 122     SPACE eurjchem-71 102 123 with with ADP eurjchem-71 102 124     SPACE eurjchem-71 102 125 a a DET eurjchem-71 102 126     SPACE eurjchem-71 102 127 minor minor ADJ eurjchem-71 102 128     SPACE eurjchem-71 102 129 amount amount NOUN eurjchem-71 102 130     SPACE eurjchem-71 102 131 of of ADP eurjchem-71 102 132     SPACE eurjchem-71 102 133 the the DET eurjchem-71 102 134     SPACE eurjchem-71 102 135 elimination elimination NOUN eurjchem-71 102 136     SPACE eurjchem-71 102 137 product product NOUN eurjchem-71 102 138     SPACE eurjchem-71 102 139 5 5 NUM eurjchem-71 102 140     SPACE eurjchem-71 102 141 ( ( PUNCT eurjchem-71 102 142 scheme scheme NOUN eurjchem-71 102 143     SPACE eurjchem-71 102 144 5 5 NUM eurjchem-71 102 145 ) ) PUNCT eurjchem-71 102 146 . . PUNCT eurjchem-71 102 147         SPACE eurjchem-71 103 1 the the DET eurjchem-71 103 2     SPACE eurjchem-71 103 3 ir ir NOUN eurjchem-71 103 4     SPACE eurjchem-71 103 5 spectrum spectrum NOUN eurjchem-71 103 6     SPACE eurjchem-71 103 7 of of ADP eurjchem-71 103 8     SPACE eurjchem-71 103 9 4 4 NUM eurjchem-71 103 10     SPACE eurjchem-71 103 11 displayed display VERB eurjchem-71 103 12     SPACE eurjchem-71 103 13 υnh υnh NOUN eurjchem-71 103 14     SPACE eurjchem-71 103 15 at at ADP eurjchem-71 103 16     SPACE eurjchem-71 103 17 3210 3210 NUM eurjchem-71 103 18     SPACE eurjchem-71 103 19 cm‐1 cm‐1 NOUN eurjchem-71 103 20 , , PUNCT eurjchem-71 103 21     SPACE eurjchem-71 103 22 υc≡n υc≡n NOUN eurjchem-71 103 23     SPACE eurjchem-71 103 24 at at ADP eurjchem-71 103 25     SPACE eurjchem-71 103 26 2257 2257 NUM eurjchem-71 103 27     SPACE eurjchem-71 103 28 cm‐1 cm‐1 NOUN eurjchem-71 103 29 , , PUNCT eurjchem-71 103 30     SPACE eurjchem-71 103 31 υc υc NOUN eurjchem-71 103 32 = = NOUN eurjchem-71 103 33 o o NOUN eurjchem-71 103 34     SPACE eurjchem-71 103 35 at at ADP eurjchem-71 103 36     SPACE eurjchem-71 103 37 1748 1748 NUM eurjchem-71 103 38     SPACE eurjchem-71 103 39 and and CCONJ eurjchem-71 103 40     SPACE eurjchem-71 103 41 1682 1682 NUM eurjchem-71 103 42     SPACE eurjchem-71 103 43 cm‐1 cm‐1 NOUN eurjchem-71 103 44     SPACE eurjchem-71 103 45 due due ADJ eurjchem-71 103 46     SPACE eurjchem-71 103 47 to to ADP eurjchem-71 103 48     SPACE eurjchem-71 103 49 the the DET eurjchem-71 103 50     SPACE eurjchem-71 103 51 carbonyl carbonyl NOUN eurjchem-71 103 52     SPACE eurjchem-71 103 53 absorption absorption NOUN eurjchem-71 103 54     SPACE eurjchem-71 103 55 bands band NOUN eurjchem-71 103 56     SPACE eurjchem-71 103 57 of of ADP eurjchem-71 103 58     SPACE eurjchem-71 103 59 the the DET eurjchem-71 103 60     SPACE eurjchem-71 103 61 vibrational vibrational NOUN eurjchem-71 103 62     SPACE eurjchem-71 103 63 coupling coupling NOUN eurjchem-71 103 64     SPACE eurjchem-71 103 65 and and CCONJ eurjchem-71 103 66     SPACE eurjchem-71 103 67 saturated saturate VERB eurjchem-71 103 68     SPACE eurjchem-71 103 69 carbonyl carbonyl NOUN eurjchem-71 103 70     SPACE eurjchem-71 103 71 group group NOUN eurjchem-71 103 72     SPACE eurjchem-71 103 73 in in ADP eurjchem-71 103 74     SPACE eurjchem-71 103 75 the the DET eurjchem-71 103 76     SPACE eurjchem-71 103 77 side side NOUN eurjchem-71 103 78     SPACE eurjchem-71 103 79 chain chain NOUN eurjchem-71 103 80 . . PUNCT eurjchem-71 103 81     SPACE eurjchem-71 104 1 1h‐nmr 1h‐nmr NUM eurjchem-71 104 2     SPACE eurjchem-71 104 3 spectrum spectrum NOUN eurjchem-71 104 4     SPACE eurjchem-71 104 5 of of ADP eurjchem-71 104 6     SPACE eurjchem-71 104 7 4 4 NUM eurjchem-71 104 8     SPACE eurjchem-71 104 9 ( ( PUNCT eurjchem-71 104 10 dmso‐d6 dmso‐d6 NOUN eurjchem-71 104 11 ) ) PUNCT eurjchem-71 104 12     SPACE eurjchem-71 104 13 revealed reveal VERB eurjchem-71 104 14     SPACE eurjchem-71 104 15 signals signal NOUN eurjchem-71 104 16     SPACE eurjchem-71 104 17 at at ADP eurjchem-71 104 18     SPACE eurjchem-71 104 19 δ δ PROPN eurjchem-71 104 20     SPACE eurjchem-71 104 21 ( ( PUNCT eurjchem-71 104 22 ppm ppm PROPN eurjchem-71 104 23 ): ): PUNCT eurjchem-71 104 24     SPACE eurjchem-71 104 25 11.07 11.07 NUM eurjchem-71 104 26     SPACE eurjchem-71 104 27 ( ( PUNCT eurjchem-71 104 28 s s PROPN eurjchem-71 104 29 , , PUNCT eurjchem-71 104 30     SPACE eurjchem-71 104 31 1h 1h NUM eurjchem-71 104 32 , , PUNCT eurjchem-71 104 33     SPACE eurjchem-71 104 34 nh nh PROPN eurjchem-71 104 35 , , PUNCT eurjchem-71 104 36     SPACE eurjchem-71 104 37 exchangeable exchangeable ADJ eurjchem-71 104 38     SPACE eurjchem-71 104 39 with with ADP eurjchem-71 104 40     SPACE eurjchem-71 104 41 d2o d2o NOUN eurjchem-71 104 42 ) ) PUNCT eurjchem-71 104 43 , , PUNCT eurjchem-71 104 44     SPACE eurjchem-71 104 45 8.09‐7.08 8.09‐7.08 NUM eurjchem-71 104 46     SPACE eurjchem-71 104 47 ( ( PUNCT eurjchem-71 104 48 m m PROPN eurjchem-71 104 49 , , PUNCT eurjchem-71 104 50     SPACE eurjchem-71 104 51 8harom 8harom NUM eurjchem-71 104 52 . . PUNCT eurjchem-71 104 53     SPACE eurjchem-71 105 1 + + ADJ eurjchem-71 105 2     SPACE eurjchem-71 105 3 olefinic olefinic ADJ eurjchem-71 105 4     SPACE eurjchem-71 105 5 h h NOUN eurjchem-71 105 6 ) ) PUNCT eurjchem-71 105 7 , , PUNCT eurjchem-71 105 8     SPACE eurjchem-71 105 9 4.05 4.05 NUM eurjchem-71 105 10     SPACE eurjchem-71 105 11 ( ( PUNCT eurjchem-71 105 12 s s PROPN eurjchem-71 105 13 , , PUNCT eurjchem-71 105 14     SPACE eurjchem-71 105 15 2h 2h NUM eurjchem-71 105 16 , , PUNCT eurjchem-71 105 17     SPACE eurjchem-71 105 18 coch2cn coch2cn ADJ eurjchem-71 105 19 ) ) PUNCT eurjchem-71 105 20     SPACE eurjchem-71 105 21 and and CCONJ eurjchem-71 105 22     SPACE eurjchem-71 105 23 3.85 3.85 NUM eurjchem-71 105 24     SPACE eurjchem-71 105 25 ( ( PUNCT eurjchem-71 105 26 s s PROPN eurjchem-71 105 27 , , PUNCT eurjchem-71 105 28     SPACE eurjchem-71 105 29 6h 6h NOUN eurjchem-71 105 30 , , PUNCT eurjchem-71 105 31     SPACE eurjchem-71 105 32 2ome 2ome NUM eurjchem-71 105 33 ) ) PUNCT eurjchem-71 105 34 . . PUNCT eurjchem-71 105 35     SPACE eurjchem-71 106 1 furthermore furthermore ADV eurjchem-71 106 2 , , PUNCT eurjchem-71 106 3     SPACE eurjchem-71 106 4 full full ADJ eurjchem-71 106 5     SPACE eurjchem-71 106 6 analysis analysis NOUN eurjchem-71 106 7     SPACE eurjchem-71 106 8 of of ADP eurjchem-71 106 9     SPACE eurjchem-71 106 10 the the DET eurjchem-71 106 11     SPACE eurjchem-71 106 12 mass mass NOUN eurjchem-71 106 13     SPACE eurjchem-71 106 14 spectrum spectrum NOUN eurjchem-71 106 15     SPACE eurjchem-71 106 16 of of ADP eurjchem-71 106 17     SPACE eurjchem-71 106 18 compound compound NOUN eurjchem-71 106 19     SPACE eurjchem-71 106 20 4 4 NUM eurjchem-71 106 21     SPACE eurjchem-71 106 22 agrees agree VERB eurjchem-71 106 23     SPACE eurjchem-71 106 24 well well ADV eurjchem-71 106 25     SPACE eurjchem-71 106 26 with with ADP eurjchem-71 106 27     SPACE eurjchem-71 106 28 the the DET eurjchem-71 106 29     SPACE eurjchem-71 106 30 assigned assign VERB eurjchem-71 106 31     SPACE eurjchem-71 106 32 structure structure NOUN eurjchem-71 106 33 . . PUNCT eurjchem-71 106 34     SPACE eurjchem-71 107 1 thus thus ADV eurjchem-71 107 2 , , PUNCT eurjchem-71 107 3     SPACE eurjchem-71 107 4 the the DET eurjchem-71 107 5     SPACE eurjchem-71 107 6 ei ei NOUN eurjchem-71 107 7     SPACE eurjchem-71 107 8 fragmentation fragmentation NOUN eurjchem-71 107 9     SPACE eurjchem-71 107 10 shows show VERB eurjchem-71 107 11     SPACE eurjchem-71 107 12 the the DET eurjchem-71 107 13     SPACE eurjchem-71 107 14 correct correct ADJ eurjchem-71 107 15     SPACE eurjchem-71 107 16 molecular molecular ADJ eurjchem-71 107 17     SPACE eurjchem-71 107 18 ion ion NOUN eurjchem-71 107 19     SPACE eurjchem-71 107 20 peak peak NOUN eurjchem-71 107 21     SPACE eurjchem-71 107 22 at at ADP eurjchem-71 107 23     SPACE eurjchem-71 107 24 m m PROPN eurjchem-71 107 25 / / PROPN eurjchem-71 107 26 z z NOUN eurjchem-71 107 27     SPACE eurjchem-71 107 28 = = NOUN eurjchem-71 107 29     SPACE eurjchem-71 107 30 391 391 NUM eurjchem-71 107 31     SPACE eurjchem-71 107 32 ( ( PUNCT eurjchem-71 107 33 71.3 71.3 NUM eurjchem-71 107 34 % % NOUN eurjchem-71 107 35 ) ) PUNCT eurjchem-71 107 36     SPACE eurjchem-71 107 37 together together ADV eurjchem-71 107 38     SPACE eurjchem-71 107 39 with with ADP eurjchem-71 107 40     SPACE eurjchem-71 107 41 the the DET eurjchem-71 107 42     SPACE eurjchem-71 107 43 base base NOUN eurjchem-71 107 44     SPACE eurjchem-71 107 45 peak peak NOUN eurjchem-71 107 46     SPACE eurjchem-71 107 47 at at ADP eurjchem-71 107 48     SPACE eurjchem-71 107 49 m m PROPN eurjchem-71 107 50 / / PROPN eurjchem-71 107 51 z z NOUN eurjchem-71 107 52     SPACE eurjchem-71 107 53 = = NOUN eurjchem-71 107 54     SPACE eurjchem-71 107 55 216 216 NUM eurjchem-71 107 56 . . PUNCT eurjchem-71 107 57         SPACE eurjchem-71 107 58 mahmoud mahmoud PROPN eurjchem-71 107 59     SPACE eurjchem-71 107 60 et et PROPN eurjchem-71 107 61     SPACE eurjchem-71 107 62 al al PROPN eurjchem-71 107 63 . . PROPN eurjchem-71 107 64     SPACE eurjchem-71 107 65 / / SYM eurjchem-71 107 66     SPACE eurjchem-71 107 67 european european ADJ eurjchem-71 107 68     SPACE eurjchem-71 107 69 journal journal NOUN eurjchem-71 107 70     SPACE eurjchem-71 107 71 of of ADP eurjchem-71 107 72     SPACE eurjchem-71 107 73 chemistry chemistry NOUN eurjchem-71 107 74     SPACE eurjchem-71 107 75 1 1 NUM eurjchem-71 107 76     SPACE eurjchem-71 107 77 ( ( PUNCT eurjchem-71 107 78 2 2 NUM eurjchem-71 107 79 ) ) PUNCT eurjchem-71 107 80     SPACE eurjchem-71 107 81 ( ( PUNCT eurjchem-71 107 82 2010 2010 NUM eurjchem-71 107 83 ) ) PUNCT eurjchem-71 107 84     SPACE eurjchem-71 107 85 134­139 134­139 NUM eurjchem-71 107 86     SPACE eurjchem-71 107 87 137 137 NUM eurjchem-71 107 88     SPACE eurjchem-71 107 89 scheme scheme NOUN eurjchem-71 107 90     SPACE eurjchem-71 107 91 5 5 NUM eurjchem-71 107 92       SPACE eurjchem-71 107 93 the the DET eurjchem-71 107 94     SPACE eurjchem-71 107 95 structure structure NOUN eurjchem-71 107 96     SPACE eurjchem-71 107 97 of of ADP eurjchem-71 107 98     SPACE eurjchem-71 107 99 the the DET eurjchem-71 107 100     SPACE eurjchem-71 107 101 minor minor ADJ eurjchem-71 107 102     SPACE eurjchem-71 107 103 product product NOUN eurjchem-71 107 104     SPACE eurjchem-71 107 105 ( ( PUNCT eurjchem-71 107 106 13 13 NUM eurjchem-71 107 107 % % NOUN eurjchem-71 107 108 ) ) PUNCT eurjchem-71 107 109     SPACE eurjchem-71 107 110 5 5 NUM eurjchem-71 107 111     SPACE eurjchem-71 107 112 was be AUX eurjchem-71 107 113     SPACE eurjchem-71 107 114 confirmed confirm VERB eurjchem-71 107 115     SPACE eurjchem-71 107 116 from from ADP eurjchem-71 107 117     SPACE eurjchem-71 107 118 the the DET eurjchem-71 107 119     SPACE eurjchem-71 107 120 analytical analytical NOUN eurjchem-71 107 121     SPACE eurjchem-71 107 122 and and CCONJ eurjchem-71 107 123     SPACE eurjchem-71 107 124 spectroscopic spectroscopic NOUN eurjchem-71 107 125     SPACE eurjchem-71 107 126 data datum NOUN eurjchem-71 107 127 . . PUNCT eurjchem-71 107 128     SPACE eurjchem-71 107 129 the the DET eurjchem-71 107 130     SPACE eurjchem-71 107 131 highest high ADJ eurjchem-71 107 132     SPACE eurjchem-71 107 133 recorded record VERB eurjchem-71 107 134     SPACE eurjchem-71 107 135 peak peak NOUN eurjchem-71 107 136     SPACE eurjchem-71 107 137 in in ADP eurjchem-71 107 138     SPACE eurjchem-71 107 139 the the DET eurjchem-71 107 140     SPACE eurjchem-71 107 141 mass mass ADJ eurjchem-71 107 142     SPACE eurjchem-71 107 143 spectrum spectrum NOUN eurjchem-71 107 144     SPACE eurjchem-71 107 145 at at ADP eurjchem-71 107 146     SPACE eurjchem-71 107 147 m m PROPN eurjchem-71 107 148 / / PROPN eurjchem-71 107 149 z z NOUN eurjchem-71 107 150     SPACE eurjchem-71 107 151 = = NOUN eurjchem-71 107 152     SPACE eurjchem-71 107 153 247 247 NUM eurjchem-71 107 154     SPACE eurjchem-71 107 155 ( ( PUNCT eurjchem-71 107 156 61.6 61.6 NUM eurjchem-71 107 157 % % NOUN eurjchem-71 107 158 ) ) PUNCT eurjchem-71 107 159     SPACE eurjchem-71 107 160 represent represent VERB eurjchem-71 107 161     SPACE eurjchem-71 107 162 the the DET eurjchem-71 107 163     SPACE eurjchem-71 107 164 molecular molecular ADJ eurjchem-71 107 165     SPACE eurjchem-71 107 166 ion ion NOUN eurjchem-71 107 167     SPACE eurjchem-71 107 168 which which PRON eurjchem-71 107 169     SPACE eurjchem-71 107 170 upon upon SCONJ eurjchem-71 107 171     SPACE eurjchem-71 107 172 loss loss NOUN eurjchem-71 107 173     SPACE eurjchem-71 107 174 of of ADP eurjchem-71 107 175     SPACE eurjchem-71 107 176 cyanoacetamide cyanoacetamide ADJ eurjchem-71 107 177     SPACE eurjchem-71 107 178 molecule molecule NOUN eurjchem-71 107 179     SPACE eurjchem-71 107 180 afforded afford VERB eurjchem-71 107 181     SPACE eurjchem-71 107 182 the the DET eurjchem-71 107 183     SPACE eurjchem-71 107 184 base base NOUN eurjchem-71 107 185     SPACE eurjchem-71 107 186 peak peak NOUN eurjchem-71 107 187     SPACE eurjchem-71 107 188 at at ADP eurjchem-71 107 189     SPACE eurjchem-71 107 190 m m PROPN eurjchem-71 107 191 / / PROPN eurjchem-71 107 192 z z NOUN eurjchem-71 107 193     SPACE eurjchem-71 107 194 = = NOUN eurjchem-71 107 195     SPACE eurjchem-71 107 196 163 163 NUM eurjchem-71 107 197     SPACE eurjchem-71 107 198 ( ( PUNCT eurjchem-71 107 199 scheme scheme NOUN eurjchem-71 107 200     SPACE eurjchem-71 107 201 6 6 NUM eurjchem-71 107 202 ) ) PUNCT eurjchem-71 107 203 . . PUNCT eurjchem-71 107 204         SPACE eurjchem-71 108 1 scheme scheme NOUN eurjchem-71 108 2     SPACE eurjchem-71 108 3 6 6 NUM eurjchem-71 108 4         SPACE eurjchem-71 108 5 adequate adequate ADJ eurjchem-71 108 6     SPACE eurjchem-71 108 7 evidence evidence NOUN eurjchem-71 108 8     SPACE eurjchem-71 108 9 for for ADP eurjchem-71 108 10     SPACE eurjchem-71 108 11 the the DET eurjchem-71 108 12     SPACE eurjchem-71 108 13 structure structure NOUN eurjchem-71 108 14     SPACE eurjchem-71 108 15 5 5 NUM eurjchem-71 108 16     SPACE eurjchem-71 108 17 was be AUX eurjchem-71 108 18     SPACE eurjchem-71 108 19 performed perform VERB eurjchem-71 108 20     SPACE eurjchem-71 108 21 by by ADP eurjchem-71 108 22     SPACE eurjchem-71 108 23 comparison comparison NOUN eurjchem-71 108 24     SPACE eurjchem-71 108 25 ( ( PUNCT eurjchem-71 108 26 m.p m.p PROPN eurjchem-71 108 27 . . PROPN eurjchem-71 108 28 , , PUNCT eurjchem-71 108 29     SPACE eurjchem-71 108 30 tlc tlc NOUN eurjchem-71 108 31     SPACE eurjchem-71 108 32 and and CCONJ eurjchem-71 108 33     SPACE eurjchem-71 108 34 ir ir PROPN eurjchem-71 108 35     SPACE eurjchem-71 108 36 spectrum spectrum NOUN eurjchem-71 108 37 ) ) PUNCT eurjchem-71 108 38     SPACE eurjchem-71 108 39 with with SCONJ eurjchem-71 108 40     SPACE eurjchem-71 108 41 authentic authentic ADJ eurjchem-71 108 42     SPACE eurjchem-71 108 43 sample sample NOUN eurjchem-71 108 44     SPACE eurjchem-71 108 45 prepared prepare VERB eurjchem-71 108 46     SPACE eurjchem-71 108 47 from from ADP eurjchem-71 108 48     SPACE eurjchem-71 108 49 the the DET eurjchem-71 108 50     SPACE eurjchem-71 108 51 condensation condensation NOUN eurjchem-71 108 52     SPACE eurjchem-71 108 53 of of ADP eurjchem-71 108 54     SPACE eurjchem-71 108 55 3,4‐dimethoxy‐ 3,4‐dimethoxy‐ PROPN eurjchem-71 108 56 benzaldehyde benzaldehyde NOUN eurjchem-71 108 57     SPACE eurjchem-71 108 58 with with ADP eurjchem-71 108 59     SPACE eurjchem-71 108 60 cyanoethanoic cyanoethanoic ADJ eurjchem-71 108 61     SPACE eurjchem-71 108 62 hydrazide hydrazide ADV eurjchem-71 108 63     SPACE eurjchem-71 108 64 in in ADP eurjchem-71 108 65     SPACE eurjchem-71 108 66 refluxing refluxing NOUN eurjchem-71 108 67     SPACE eurjchem-71 108 68 ethanol ethanol NOUN eurjchem-71 108 69 . . PUNCT eurjchem-71 108 70     SPACE eurjchem-71 109 1 the the DET eurjchem-71 109 2     SPACE eurjchem-71 109 3 formation formation NOUN eurjchem-71 109 4     SPACE eurjchem-71 109 5 of of ADP eurjchem-71 109 6     SPACE eurjchem-71 109 7 compounds compound NOUN eurjchem-71 109 8     SPACE eurjchem-71 109 9 4 4 NUM eurjchem-71 109 10     SPACE eurjchem-71 109 11 and and CCONJ eurjchem-71 109 12     SPACE eurjchem-71 109 13 5 5 NUM eurjchem-71 109 14     SPACE eurjchem-71 109 15 could could AUX eurjchem-71 109 16     SPACE eurjchem-71 109 17 be be AUX eurjchem-71 109 18     SPACE eurjchem-71 109 19 explained explain VERB eurjchem-71 109 20     SPACE eurjchem-71 109 21 according accord VERB eurjchem-71 109 22     SPACE eurjchem-71 109 23 to to PART eurjchem-71 109 24     SPACE eurjchem-71 109 25 scheme scheme VERB eurjchem-71 109 26     SPACE eurjchem-71 109 27 7 7 NUM eurjchem-71 109 28 . . PUNCT eurjchem-71 109 29           SPACE eurjchem-71 109 30 compelling compelling ADJ eurjchem-71 109 31     SPACE eurjchem-71 109 32 evidence evidence NOUN eurjchem-71 109 33     SPACE eurjchem-71 109 34 for for ADP eurjchem-71 109 35     SPACE eurjchem-71 109 36 the the DET eurjchem-71 109 37     SPACE eurjchem-71 109 38 isoquinolin‐1,3‐dione isoquinolin‐1,3‐dione NOUN eurjchem-71 109 39     SPACE eurjchem-71 109 40 4 4 NUM eurjchem-71 109 41     SPACE eurjchem-71 109 42 is be AUX eurjchem-71 109 43     SPACE eurjchem-71 109 44 forthcoming forthcoming ADJ eurjchem-71 109 45     SPACE eurjchem-71 109 46 by by ADP eurjchem-71 109 47     SPACE eurjchem-71 109 48 study study NOUN eurjchem-71 109 49     SPACE eurjchem-71 109 50 of of ADP eurjchem-71 109 51     SPACE eurjchem-71 109 52 its its PRON eurjchem-71 109 53     SPACE eurjchem-71 109 54 reactivity reactivity NOUN eurjchem-71 109 55     SPACE eurjchem-71 109 56 towards towards ADP eurjchem-71 109 57     SPACE eurjchem-71 109 58 some some DET eurjchem-71 109 59     SPACE eurjchem-71 109 60 activated activate VERB eurjchem-71 109 61     SPACE eurjchem-71 109 62 nitriles nitrile NOUN eurjchem-71 109 63     SPACE eurjchem-71 109 64 such such ADJ eurjchem-71 109 65     SPACE eurjchem-71 109 66 as as ADV eurjchem-71 109 67     SPACE eurjchem-71 109 68 arylidenemalononitrile arylidenemalononitrile ADJ eurjchem-71 109 69     SPACE eurjchem-71 109 70 and and CCONJ eurjchem-71 109 71     SPACE eurjchem-71 109 72 ethoxy‐ ethoxy‐ NOUN eurjchem-71 109 73     SPACE eurjchem-71 109 74 methylenemalononitrile methylenemalononitrile NOUN eurjchem-71 109 75 . . PUNCT eurjchem-71 109 76     SPACE eurjchem-71 109 77 thus thus ADV eurjchem-71 109 78 , , PUNCT eurjchem-71 109 79     SPACE eurjchem-71 109 80 reaction reaction NOUN eurjchem-71 109 81     SPACE eurjchem-71 109 82 of of ADP eurjchem-71 109 83     SPACE eurjchem-71 109 84 4 4 NUM eurjchem-71 109 85     SPACE eurjchem-71 109 86 with with ADP eurjchem-71 109 87     SPACE eurjchem-71 109 88 p‐ p‐ NOUN eurjchem-71 109 89 chlorobenzylidenemalononitrile chlorobenzylidenemalononitrile NOUN eurjchem-71 109 90     SPACE eurjchem-71 109 91 in in ADP eurjchem-71 109 92     SPACE eurjchem-71 109 93 refluxing refluxing NOUN eurjchem-71 109 94     SPACE eurjchem-71 109 95 ethanol ethanol NOUN eurjchem-71 109 96     SPACE eurjchem-71 109 97 in in ADP eurjchem-71 109 98     SPACE eurjchem-71 109 99 the the DET eurjchem-71 109 100     SPACE eurjchem-71 109 101 presence presence NOUN eurjchem-71 109 102     SPACE eurjchem-71 109 103 of of ADP eurjchem-71 109 104     SPACE eurjchem-71 109 105 piperidine piperidine NOUN eurjchem-71 109 106     SPACE eurjchem-71 109 107 afforded afford VERB eurjchem-71 109 108     SPACE eurjchem-71 109 109 pyrido[1,2‐b]‐1,2,4‐ pyrido[1,2‐b]‐1,2,4‐ NOUN eurjchem-71 109 110 triazolo[5,1‐a]isoquinolinone triazolo[5,1‐a]isoquinolinone NOUN eurjchem-71 109 111     SPACE eurjchem-71 109 112 derivative derivative NOUN eurjchem-71 109 113     SPACE eurjchem-71 109 114 6 6 NUM eurjchem-71 109 115 , , PUNCT eurjchem-71 109 116     SPACE eurjchem-71 109 117 whereas whereas ADV eurjchem-71 109 118     SPACE eurjchem-71 109 119 under under ADP eurjchem-71 109 120     SPACE eurjchem-71 109 121 the the DET eurjchem-71 109 122     SPACE eurjchem-71 109 123 same same ADJ eurjchem-71 109 124     SPACE eurjchem-71 109 125 conditions condition NOUN eurjchem-71 109 126 , , PUNCT eurjchem-71 109 127     SPACE eurjchem-71 109 128 treatment treatment NOUN eurjchem-71 109 129     SPACE eurjchem-71 109 130 of of ADP eurjchem-71 109 131     SPACE eurjchem-71 109 132 4 4 NUM eurjchem-71 109 133     SPACE eurjchem-71 109 134 with with ADP eurjchem-71 109 135     SPACE eurjchem-71 109 136 ethoxymethylenemalono‐ ethoxymethylenemalono‐ NOUN eurjchem-71 109 137 nitrile nitrile PROPN eurjchem-71 109 138     SPACE eurjchem-71 109 139 yielded yield VERB eurjchem-71 109 140     SPACE eurjchem-71 109 141 ( ( PUNCT eurjchem-71 109 142 e)‐1‐[4‐(3,4‐dimethoxybenzylidene)1,3‐dioxo‐ e)‐1‐[4‐(3,4‐dimethoxybenzylidene)1,3‐dioxo‐ NOUN eurjchem-71 109 143 3,4‐dihydroisoquinolin‐2‐(1h)‐yl]‐6‐amino‐2‐oxo‐1,2‐dihydro 3,4‐dihydroisoquinolin‐2‐(1h)‐yl]‐6‐amino‐2‐oxo‐1,2‐dihydro PRON eurjchem-71 109 144     SPACE eurjchem-71 109 145 pyridin‐3,5‐dicarbonitrile pyridin‐3,5‐dicarbonitrile ADV eurjchem-71 109 146     SPACE eurjchem-71 109 147 7 7 NUM eurjchem-71 109 148     SPACE eurjchem-71 109 149 ( ( PUNCT eurjchem-71 109 150 scheme scheme NOUN eurjchem-71 109 151     SPACE eurjchem-71 109 152 5 5 NUM eurjchem-71 109 153 ) ) PUNCT eurjchem-71 109 154 . . PUNCT eurjchem-71 109 155         SPACE eurjchem-71 110 1 scheme scheme NOUN eurjchem-71 110 2     SPACE eurjchem-71 110 3 7 7 NUM eurjchem-71 110 4         SPACE eurjchem-71 110 5 138 138 NUM eurjchem-71 110 6     SPACE eurjchem-71 110 7 mahmoud mahmoud PROPN eurjchem-71 110 8     SPACE eurjchem-71 110 9 et et PROPN eurjchem-71 110 10     SPACE eurjchem-71 110 11 al al PROPN eurjchem-71 110 12 . . PROPN eurjchem-71 110 13     SPACE eurjchem-71 110 14 / / SYM eurjchem-71 110 15     SPACE eurjchem-71 110 16 european european ADJ eurjchem-71 110 17     SPACE eurjchem-71 110 18 journal journal NOUN eurjchem-71 110 19     SPACE eurjchem-71 110 20 of of ADP eurjchem-71 110 21     SPACE eurjchem-71 110 22 chemistry chemistry NOUN eurjchem-71 110 23     SPACE eurjchem-71 110 24 1 1 NUM eurjchem-71 110 25     SPACE eurjchem-71 110 26 ( ( PUNCT eurjchem-71 110 27 2 2 NUM eurjchem-71 110 28 ) ) PUNCT eurjchem-71 110 29     SPACE eurjchem-71 110 30 ( ( PUNCT eurjchem-71 110 31 2010 2010 NUM eurjchem-71 110 32 ) ) PUNCT eurjchem-71 110 33     SPACE eurjchem-71 110 34 134­139 134­139 NUM eurjchem-71 110 35         SPACE eurjchem-71 110 36 the the DET eurjchem-71 110 37     SPACE eurjchem-71 110 38 reaction reaction NOUN eurjchem-71 110 39     SPACE eurjchem-71 110 40 of of ADP eurjchem-71 110 41     SPACE eurjchem-71 110 42 isochromene isochromene NOUN eurjchem-71 110 43     SPACE eurjchem-71 110 44 2 2 NUM eurjchem-71 110 45     SPACE eurjchem-71 110 46 with with ADP eurjchem-71 110 47     SPACE eurjchem-71 110 48 cyclohexylamine cyclohexylamine NOUN eurjchem-71 110 49     SPACE eurjchem-71 110 50 in in ADP eurjchem-71 110 51     SPACE eurjchem-71 110 52 refluxing refluxing NOUN eurjchem-71 110 53     SPACE eurjchem-71 110 54 dioxane dioxane NOUN eurjchem-71 110 55     SPACE eurjchem-71 110 56 afforded afford VERB eurjchem-71 110 57     SPACE eurjchem-71 110 58 ( ( PUNCT eurjchem-71 110 59 e)‐2‐[2‐(n‐cyclohexyl‐ e)‐2‐[2‐(n‐cyclohexyl‐ NOUN eurjchem-71 110 60 carbamoyl)phenyl]‐3‐(3,4‐dimethoxyphenyl carbamoyl)phenyl]‐3‐(3,4‐dimethoxyphenyl PROPN eurjchem-71 110 61 ) ) PUNCT eurjchem-71 110 62     SPACE eurjchem-71 110 63 acrylic acrylic NOUN eurjchem-71 110 64     SPACE eurjchem-71 110 65 acid acid NOUN eurjchem-71 110 66     SPACE eurjchem-71 110 67 8 8 NUM eurjchem-71 110 68     SPACE eurjchem-71 110 69 which which PRON eurjchem-71 110 70     SPACE eurjchem-71 110 71 readily readily ADV eurjchem-71 110 72     SPACE eurjchem-71 110 73 cyclized cyclize VERB eurjchem-71 110 74     SPACE eurjchem-71 110 75 using use VERB eurjchem-71 110 76     SPACE eurjchem-71 110 77 freshly freshly ADV eurjchem-71 110 78     SPACE eurjchem-71 110 79 distilled distil VERB eurjchem-71 110 80     SPACE eurjchem-71 110 81 acetic acetic ADJ eurjchem-71 110 82     SPACE eurjchem-71 110 83 anhydride anhydride NOUN eurjchem-71 110 84     SPACE eurjchem-71 110 85 to to PART eurjchem-71 110 86     SPACE eurjchem-71 110 87 give give VERB eurjchem-71 110 88     SPACE eurjchem-71 110 89 ( ( PUNCT eurjchem-71 110 90 e)‐4‐(3,4‐dimethoxy e)‐4‐(3,4‐dimethoxy PROPN eurjchem-71 110 91     SPACE eurjchem-71 110 92 benzylidene)‐2‐cyclohexyliso benzylidene)‐2‐cyclohexyliso NOUN eurjchem-71 110 93     SPACE eurjchem-71 110 94 quinoline‐1,3‐(2h,4h)‐dione quinoline‐1,3‐(2h,4h)‐dione VERB eurjchem-71 110 95     SPACE eurjchem-71 110 96 9 9 NUM eurjchem-71 110 97 . . PUNCT eurjchem-71 110 98     SPACE eurjchem-71 111 1 furthermore furthermore ADV eurjchem-71 111 2 , , PUNCT eurjchem-71 111 3     SPACE eurjchem-71 111 4 the the DET eurjchem-71 111 5     SPACE eurjchem-71 111 6 amido amido NOUN eurjchem-71 111 7     SPACE eurjchem-71 111 8 acid acid NOUN eurjchem-71 111 9     SPACE eurjchem-71 111 10 8 8 NUM eurjchem-71 111 11     SPACE eurjchem-71 111 12 in in ADP eurjchem-71 111 13     SPACE eurjchem-71 111 14 the the DET eurjchem-71 111 15     SPACE eurjchem-71 111 16 presence presence NOUN eurjchem-71 111 17     SPACE eurjchem-71 111 18 of of ADP eurjchem-71 111 19     SPACE eurjchem-71 111 20 a a DET eurjchem-71 111 21     SPACE eurjchem-71 111 22 mixture mixture NOUN eurjchem-71 111 23     SPACE eurjchem-71 111 24 of of ADP eurjchem-71 111 25     SPACE eurjchem-71 111 26 acetic acetic ADJ eurjchem-71 111 27     SPACE eurjchem-71 111 28 anhydride anhydride NOUN eurjchem-71 111 29     SPACE eurjchem-71 111 30 and and CCONJ eurjchem-71 111 31     SPACE eurjchem-71 111 32 perchloric perchloric ADJ eurjchem-71 111 33     SPACE eurjchem-71 111 34 acid acid NOUN eurjchem-71 111 35     SPACE eurjchem-71 111 36 at at ADP eurjchem-71 111 37     SPACE eurjchem-71 111 38 0oc 0oc NOUN eurjchem-71 111 39     SPACE eurjchem-71 111 40 under under ADP eurjchem-71 111 41     SPACE eurjchem-71 111 42 the the DET eurjchem-71 111 43     SPACE eurjchem-71 111 44 condition condition NOUN eurjchem-71 111 45     SPACE eurjchem-71 111 46 described describe VERB eurjchem-71 111 47     SPACE eurjchem-71 111 48 by by ADP eurjchem-71 111 49     SPACE eurjchem-71 111 50 boyed boyed ADJ eurjchem-71 111 51     SPACE eurjchem-71 111 52 et et PROPN eurjchem-71 111 53     SPACE eurjchem-71 111 54 al al PROPN eurjchem-71 111 55 . . PROPN eurjchem-71 111 56     SPACE eurjchem-71 112 1 [ [ X eurjchem-71 112 2 31 31 NUM eurjchem-71 112 3 ] ] PUNCT eurjchem-71 112 4     SPACE eurjchem-71 112 5 yielded yield VERB eurjchem-71 112 6     SPACE eurjchem-71 112 7 the the DET eurjchem-71 112 8     SPACE eurjchem-71 112 9 homophthalisoimidium homophthalisoimidium NOUN eurjchem-71 112 10     SPACE eurjchem-71 112 11 perchlorate perchlorate NOUN eurjchem-71 112 12     SPACE eurjchem-71 112 13 10 10 NUM eurjchem-71 112 14 . . PUNCT eurjchem-71 112 15     SPACE eurjchem-71 112 16 the the DET eurjchem-71 112 17     SPACE eurjchem-71 112 18 ir ir NOUN eurjchem-71 112 19     SPACE eurjchem-71 112 20 spectrum spectrum NOUN eurjchem-71 112 21     SPACE eurjchem-71 112 22 of of ADP eurjchem-71 112 23     SPACE eurjchem-71 112 24 10 10 NUM eurjchem-71 112 25     SPACE eurjchem-71 112 26 exhibited exhibit VERB eurjchem-71 112 27     SPACE eurjchem-71 112 28 typical typical ADJ eurjchem-71 112 29     SPACE eurjchem-71 112 30 carbonyl carbonyl NOUN eurjchem-71 112 31     SPACE eurjchem-71 112 32 and and CCONJ eurjchem-71 112 33     SPACE eurjchem-71 112 34 iminium iminium NOUN eurjchem-71 112 35     SPACE eurjchem-71 112 36 c c NOUN eurjchem-71 112 37 = = SYM eurjchem-71 112 38 n+ n+ NOUN eurjchem-71 112 39     SPACE eurjchem-71 112 40 absorption absorption NOUN eurjchem-71 112 41     SPACE eurjchem-71 112 42 frequencies frequency NOUN eurjchem-71 112 43     SPACE eurjchem-71 112 44 at at ADP eurjchem-71 112 45     SPACE eurjchem-71 112 46 1809 1809 NUM eurjchem-71 112 47     SPACE eurjchem-71 112 48 cm‐1 cm‐1 NOUN eurjchem-71 112 49     SPACE eurjchem-71 112 50 and and CCONJ eurjchem-71 112 51     SPACE eurjchem-71 112 52 1643 1643 NUM eurjchem-71 112 53     SPACE eurjchem-71 112 54 cm‐1 cm‐1 NOUN eurjchem-71 112 55 , , PUNCT eurjchem-71 112 56     SPACE eurjchem-71 112 57 respectively respectively ADV eurjchem-71 112 58 . . PUNCT eurjchem-71 112 59     SPACE eurjchem-71 113 1 the the DET eurjchem-71 113 2     SPACE eurjchem-71 113 3 highest high ADJ eurjchem-71 113 4     SPACE eurjchem-71 113 5 recorded record VERB eurjchem-71 113 6     SPACE eurjchem-71 113 7 peak peak NOUN eurjchem-71 113 8     SPACE eurjchem-71 113 9 in in ADP eurjchem-71 113 10     SPACE eurjchem-71 113 11 the the DET eurjchem-71 113 12     SPACE eurjchem-71 113 13 mass mass NOUN eurjchem-71 113 14     SPACE eurjchem-71 113 15 spectrum spectrum NOUN eurjchem-71 113 16     SPACE eurjchem-71 113 17 of of ADP eurjchem-71 113 18     SPACE eurjchem-71 113 19 10 10 NUM eurjchem-71 113 20     SPACE eurjchem-71 113 21 represents represent VERB eurjchem-71 113 22     SPACE eurjchem-71 113 23 the the DET eurjchem-71 113 24     SPACE eurjchem-71 113 25 radical radical ADJ eurjchem-71 113 26     SPACE eurjchem-71 113 27 cation cation NOUN eurjchem-71 113 28     SPACE eurjchem-71 114 1 [ [ X eurjchem-71 114 2 m+ m+ NUM eurjchem-71 114 3 . . PUNCT eurjchem-71 114 4     SPACE eurjchem-71 114 5 – – PUNCT eurjchem-71 114 6     SPACE eurjchem-71 114 7 hclo4 hclo4 NOUN eurjchem-71 114 8 ] ] X eurjchem-71 114 9     SPACE eurjchem-71 114 10 ( ( PUNCT eurjchem-71 114 11 scheme scheme NOUN eurjchem-71 114 12     SPACE eurjchem-71 114 13 5 5 NUM eurjchem-71 114 14 ) ) PUNCT eurjchem-71 114 15 . . PUNCT eurjchem-71 114 16     SPACE eurjchem-71 115 1 a a DET eurjchem-71 115 2     SPACE eurjchem-71 115 3 tentative tentative ADJ eurjchem-71 115 4     SPACE eurjchem-71 115 5 explanation explanation NOUN eurjchem-71 115 6     SPACE eurjchem-71 115 7 for for ADP eurjchem-71 115 8     SPACE eurjchem-71 115 9 the the DET eurjchem-71 115 10     SPACE eurjchem-71 115 11 formation formation NOUN eurjchem-71 115 12     SPACE eurjchem-71 115 13 of of ADP eurjchem-71 115 14     SPACE eurjchem-71 115 15 10 10 NUM eurjchem-71 115 16     SPACE eurjchem-71 115 17 is be AUX eurjchem-71 115 18     SPACE eurjchem-71 115 19 represented represent VERB eurjchem-71 115 20     SPACE eurjchem-71 115 21 in in ADP eurjchem-71 115 22     SPACE eurjchem-71 115 23 scheme scheme NOUN eurjchem-71 115 24     SPACE eurjchem-71 115 25 5 5 NUM eurjchem-71 115 26 . . PUNCT eurjchem-71 115 27         SPACE eurjchem-71 115 28 scheme scheme NOUN eurjchem-71 115 29     SPACE eurjchem-71 115 30 8 8 NUM eurjchem-71 115 31         SPACE eurjchem-71 115 32 isochromen‐1,3‐dione isochromen‐1,3‐dione NUM eurjchem-71 115 33     SPACE eurjchem-71 115 34 2 2 NUM eurjchem-71 115 35     SPACE eurjchem-71 115 36 behave behave VERB eurjchem-71 115 37     SPACE eurjchem-71 115 38 differently differently ADV eurjchem-71 115 39     SPACE eurjchem-71 115 40 when when SCONJ eurjchem-71 115 41     SPACE eurjchem-71 115 42 reacted react VERB eurjchem-71 115 43     SPACE eurjchem-71 115 44 with with ADP eurjchem-71 115 45     SPACE eurjchem-71 115 46 2‐aminothiophenol 2‐aminothiophenol NOUN eurjchem-71 115 47 . . PUNCT eurjchem-71 115 48     SPACE eurjchem-71 115 49 reaction reaction NOUN eurjchem-71 115 50     SPACE eurjchem-71 115 51 using use VERB eurjchem-71 115 52     SPACE eurjchem-71 115 53 a a DET eurjchem-71 115 54     SPACE eurjchem-71 115 55 1:1 1:1 NUM eurjchem-71 115 56     SPACE eurjchem-71 115 57 molar molar ADJ eurjchem-71 115 58     SPACE eurjchem-71 115 59 ratio ratio NOUN eurjchem-71 115 60     SPACE eurjchem-71 115 61 in in ADP eurjchem-71 115 62     SPACE eurjchem-71 115 63 refluxing refluxing NOUN eurjchem-71 115 64     SPACE eurjchem-71 115 65 dioxane dioxane NOUN eurjchem-71 115 66     SPACE eurjchem-71 115 67 afforded afford VERB eurjchem-71 115 68     SPACE eurjchem-71 115 69 the the DET eurjchem-71 115 70     SPACE eurjchem-71 115 71 adduct adduct NOUN eurjchem-71 115 72     SPACE eurjchem-71 115 73 with with ADP eurjchem-71 115 74     SPACE eurjchem-71 115 75 molecular molecular ADJ eurjchem-71 115 76     SPACE eurjchem-71 115 77 formula formula NOUN eurjchem-71 115 78     SPACE eurjchem-71 115 79 c24h19no4s c24h19no4s NOUN eurjchem-71 115 80     SPACE eurjchem-71 116 1 [ [ X eurjchem-71 116 2 m+ m+ NUM eurjchem-71 116 3 . . PUNCT eurjchem-71 116 4     SPACE eurjchem-71 117 1 = = NOUN eurjchem-71 117 2     SPACE eurjchem-71 117 3 417 417 NUM eurjchem-71 117 4 ] ] PUNCT eurjchem-71 117 5 . . PUNCT eurjchem-71 117 6     SPACE eurjchem-71 118 1 many many ADJ eurjchem-71 118 2     SPACE eurjchem-71 118 3 structures structure NOUN eurjchem-71 118 4     SPACE eurjchem-71 118 5 seemed seem VERB eurjchem-71 118 6     SPACE eurjchem-71 118 7 possible possible ADJ eurjchem-71 118 8     SPACE eurjchem-71 118 9 for for ADP eurjchem-71 118 10     SPACE eurjchem-71 118 11 this this DET eurjchem-71 118 12     SPACE eurjchem-71 118 13 product product NOUN eurjchem-71 118 14 . . PUNCT eurjchem-71 118 15     SPACE eurjchem-71 119 1 the the DET eurjchem-71 119 2     SPACE eurjchem-71 119 3 assigned assign VERB eurjchem-71 119 4     SPACE eurjchem-71 119 5 benzo[1,4]‐thiazepine benzo[1,4]‐thiazepine NOUN eurjchem-71 119 6     SPACE eurjchem-71 119 7 structure structure NOUN eurjchem-71 119 8     SPACE eurjchem-71 119 9 11 11 NUM eurjchem-71 119 10     SPACE eurjchem-71 119 11 was be AUX eurjchem-71 119 12     SPACE eurjchem-71 119 13 validated validate VERB eurjchem-71 119 14     SPACE eurjchem-71 119 15 on on ADP eurjchem-71 119 16     SPACE eurjchem-71 119 17 the the DET eurjchem-71 119 18     SPACE eurjchem-71 119 19 basis basis NOUN eurjchem-71 119 20     SPACE eurjchem-71 119 21 of of ADP eurjchem-71 119 22     SPACE eurjchem-71 119 23 the the DET eurjchem-71 119 24     SPACE eurjchem-71 119 25 following follow VERB eurjchem-71 119 26     SPACE eurjchem-71 119 27 arguments argument NOUN eurjchem-71 119 28 : : PUNCT eurjchem-71 119 29     SPACE eurjchem-71 119 30 i‐ i‐ VERB eurjchem-71 119 31         SPACE eurjchem-71 119 32 the the DET eurjchem-71 119 33     SPACE eurjchem-71 119 34 compound compound NOUN eurjchem-71 119 35     SPACE eurjchem-71 119 36 is be AUX eurjchem-71 119 37     SPACE eurjchem-71 119 38 soluble soluble ADJ eurjchem-71 119 39     SPACE eurjchem-71 119 40 in in ADP eurjchem-71 119 41     SPACE eurjchem-71 119 42 aqueous aqueous ADJ eurjchem-71 119 43     SPACE eurjchem-71 119 44 sodium sodium NOUN eurjchem-71 119 45     SPACE eurjchem-71 119 46 bicarbonate bicarbonate NOUN eurjchem-71 119 47     SPACE eurjchem-71 119 48 solution solution NOUN eurjchem-71 119 49 , , PUNCT eurjchem-71 119 50     SPACE eurjchem-71 119 51 ii‐ ii‐ ADV eurjchem-71 119 52     SPACE eurjchem-71 119 53 the the DET eurjchem-71 119 54     SPACE eurjchem-71 119 55 ir ir NOUN eurjchem-71 119 56     SPACE eurjchem-71 119 57 spectrum spectrum NOUN eurjchem-71 119 58     SPACE eurjchem-71 119 59 revealed reveal VERB eurjchem-71 119 60     SPACE eurjchem-71 119 61 the the DET eurjchem-71 119 62     SPACE eurjchem-71 119 63 presence presence NOUN eurjchem-71 119 64     SPACE eurjchem-71 119 65 of of ADP eurjchem-71 119 66     SPACE eurjchem-71 119 67 carbonyl carbonyl NOUN eurjchem-71 119 68     SPACE eurjchem-71 119 69 stretching stretch VERB eurjchem-71 119 70     SPACE eurjchem-71 119 71 absorption absorption NOUN eurjchem-71 119 72     SPACE eurjchem-71 119 73 band band NOUN eurjchem-71 119 74     SPACE eurjchem-71 119 75 at at ADP eurjchem-71 119 76     SPACE eurjchem-71 119 77 1684 1684 NUM eurjchem-71 119 78     SPACE eurjchem-71 119 79 cm‐1 cm‐1 NOUN eurjchem-71 119 80     SPACE eurjchem-71 119 81 together together ADV eurjchem-71 119 82     SPACE eurjchem-71 119 83 with with ADP eurjchem-71 119 84     SPACE eurjchem-71 119 85 the the DET eurjchem-71 119 86     SPACE eurjchem-71 119 87 broad broad ADJ eurjchem-71 119 88     SPACE eurjchem-71 119 89 band band NOUN eurjchem-71 119 90     SPACE eurjchem-71 119 91 for for ADP eurjchem-71 119 92     SPACE eurjchem-71 119 93 carboxylic‐oh carboxylic‐oh NOUN eurjchem-71 119 94     SPACE eurjchem-71 119 95 at at ADP eurjchem-71 119 96     SPACE eurjchem-71 119 97 3480‐2850 3480‐2850 NUM eurjchem-71 119 98     SPACE eurjchem-71 119 99 cm‐1 cm‐1 NOUN eurjchem-71 119 100 , , PUNCT eurjchem-71 119 101     SPACE eurjchem-71 119 102 iii‐ iii‐ PRON eurjchem-71 119 103     SPACE eurjchem-71 119 104 the the DET eurjchem-71 119 105     SPACE eurjchem-71 119 106 spot spot NOUN eurjchem-71 119 107     SPACE eurjchem-71 119 108 test test NOUN eurjchem-71 119 109     SPACE eurjchem-71 119 110 for for ADP eurjchem-71 119 111     SPACE eurjchem-71 119 112 sh sh PROPN eurjchem-71 119 113     SPACE eurjchem-71 119 114 group group NOUN eurjchem-71 119 115     SPACE eurjchem-71 119 116 is be AUX eurjchem-71 119 117     SPACE eurjchem-71 119 118 negative negative ADJ eurjchem-71 119 119       SPACE eurjchem-71 119 120 ( ( PUNCT eurjchem-71 119 121 scheme scheme NOUN eurjchem-71 119 122     SPACE eurjchem-71 119 123 9 9 NUM eurjchem-71 119 124 ) ) PUNCT eurjchem-71 119 125 . . PUNCT eurjchem-71 119 126       SPACE eurjchem-71 120 1 when when SCONJ eurjchem-71 120 2     SPACE eurjchem-71 120 3 equimolar equimolar NOUN eurjchem-71 120 4     SPACE eurjchem-71 120 5 amounts amount NOUN eurjchem-71 120 6     SPACE eurjchem-71 120 7 of of ADP eurjchem-71 120 8     SPACE eurjchem-71 120 9 compound compound NOUN eurjchem-71 120 10     SPACE eurjchem-71 120 11 2 2 NUM eurjchem-71 120 12     SPACE eurjchem-71 120 13 and and CCONJ eurjchem-71 120 14     SPACE eurjchem-71 120 15 thiophenol thiophenol NOUN eurjchem-71 120 16     SPACE eurjchem-71 120 17 were be AUX eurjchem-71 120 18     SPACE eurjchem-71 120 19 refluxed refluxe VERB eurjchem-71 120 20     SPACE eurjchem-71 120 21 in in ADP eurjchem-71 120 22     SPACE eurjchem-71 120 23 boiling boil VERB eurjchem-71 120 24     SPACE eurjchem-71 120 25 dioxane dioxane NOUN eurjchem-71 120 26     SPACE eurjchem-71 120 27 evaporation evaporation NOUN eurjchem-71 120 28     SPACE eurjchem-71 120 29 of of ADP eurjchem-71 120 30     SPACE eurjchem-71 120 31 the the DET eurjchem-71 120 32     SPACE eurjchem-71 120 33 solvent solvent NOUN eurjchem-71 120 34     SPACE eurjchem-71 120 35 left leave VERB eurjchem-71 120 36     SPACE eurjchem-71 120 37 a a DET eurjchem-71 120 38     SPACE eurjchem-71 120 39 crude crude NOUN eurjchem-71 120 40     SPACE eurjchem-71 120 41 solid solid ADJ eurjchem-71 120 42     SPACE eurjchem-71 120 43 product product NOUN eurjchem-71 120 44     SPACE eurjchem-71 120 45 which which PRON eurjchem-71 120 46     SPACE eurjchem-71 120 47 completely completely ADV eurjchem-71 120 48     SPACE eurjchem-71 120 49 dissolved dissolve VERB eurjchem-71 120 50     SPACE eurjchem-71 120 51 in in ADP eurjchem-71 120 52     SPACE eurjchem-71 120 53 an an DET eurjchem-71 120 54     SPACE eurjchem-71 120 55 aqueous aqueous ADJ eurjchem-71 120 56     SPACE eurjchem-71 120 57 sodium sodium NOUN eurjchem-71 120 58     SPACE eurjchem-71 120 59 bicarbonate bicarbonate NOUN eurjchem-71 120 60     SPACE eurjchem-71 120 61 solution solution NOUN eurjchem-71 120 62     SPACE eurjchem-71 120 63 and and CCONJ eurjchem-71 120 64     SPACE eurjchem-71 120 65 precipitated precipitate VERB eurjchem-71 120 66     SPACE eurjchem-71 120 67 when when SCONJ eurjchem-71 120 68     SPACE eurjchem-71 120 69 treated treat VERB eurjchem-71 120 70     SPACE eurjchem-71 120 71 with with ADP eurjchem-71 120 72     SPACE eurjchem-71 120 73 ice ice NOUN eurjchem-71 120 74     SPACE eurjchem-71 120 75 cold cold ADJ eurjchem-71 120 76     SPACE eurjchem-71 120 77 hydrochloric hydrochloric ADJ eurjchem-71 120 78     SPACE eurjchem-71 120 79 acid acid NOUN eurjchem-71 120 80 . . PUNCT eurjchem-71 120 81     SPACE eurjchem-71 120 82 this this DET eurjchem-71 120 83     SPACE eurjchem-71 120 84 product product NOUN eurjchem-71 120 85     SPACE eurjchem-71 120 86 was be AUX eurjchem-71 120 87     SPACE eurjchem-71 120 88 identified identify VERB eurjchem-71 120 89     SPACE eurjchem-71 120 90 as as ADP eurjchem-71 120 91     SPACE eurjchem-71 120 92 2‐[1‐carboxy‐2‐(3,4‐dimethoxyphenyl)‐2‐(phenyl 2‐[1‐carboxy‐2‐(3,4‐dimethoxyphenyl)‐2‐(phenyl NUM eurjchem-71 120 93     SPACE eurjchem-71 120 94 thio)ethyl]benzoic thio)ethyl]benzoic ADJ eurjchem-71 120 95     SPACE eurjchem-71 120 96 acid acid NOUN eurjchem-71 120 97     SPACE eurjchem-71 120 98 12 12 NUM eurjchem-71 120 99     SPACE eurjchem-71 120 100 as as ADP eurjchem-71 120 101     SPACE eurjchem-71 120 102 by by ADP eurjchem-71 120 103     SPACE eurjchem-71 120 104 spectroscopic spectroscopic NOUN eurjchem-71 120 105     SPACE eurjchem-71 120 106 data datum NOUN eurjchem-71 120 107 . . PUNCT eurjchem-71 120 108     SPACE eurjchem-71 121 1 thus thus ADV eurjchem-71 121 2 , , PUNCT eurjchem-71 121 3     SPACE eurjchem-71 121 4 the the DET eurjchem-71 121 5     SPACE eurjchem-71 121 6 ir ir NOUN eurjchem-71 121 7     SPACE eurjchem-71 121 8 spectrum spectrum NOUN eurjchem-71 121 9     SPACE eurjchem-71 121 10 of of ADP eurjchem-71 121 11     SPACE eurjchem-71 121 12 12 12 NUM eurjchem-71 121 13     SPACE eurjchem-71 121 14 showed show VERB eurjchem-71 121 15     SPACE eurjchem-71 121 16 the the DET eurjchem-71 121 17     SPACE eurjchem-71 121 18 typical typical ADJ eurjchem-71 121 19     SPACE eurjchem-71 121 20 stretching stretch VERB eurjchem-71 121 21     SPACE eurjchem-71 121 22 absorption absorption NOUN eurjchem-71 121 23     SPACE eurjchem-71 121 24 bands band NOUN eurjchem-71 121 25     SPACE eurjchem-71 121 26 at at ADP eurjchem-71 121 27     SPACE eurjchem-71 121 28 3480‐2500 3480‐2500 NUM eurjchem-71 121 29     SPACE eurjchem-71 121 30 ( ( PUNCT eurjchem-71 121 31 br br NOUN eurjchem-71 121 32 ) ) PUNCT eurjchem-71 121 33     SPACE eurjchem-71 121 34 and and CCONJ eurjchem-71 121 35     SPACE eurjchem-71 121 36 1717 1717 NUM eurjchem-71 121 37 , , PUNCT eurjchem-71 121 38     SPACE eurjchem-71 121 39 1700 1700 NUM eurjchem-71 121 40     SPACE eurjchem-71 121 41 cm‐1 cm‐1 NOUN eurjchem-71 121 42     SPACE eurjchem-71 121 43 of of ADP eurjchem-71 121 44     SPACE eurjchem-71 121 45 the the DET eurjchem-71 121 46     SPACE eurjchem-71 121 47 carboxylic carboxylic NOUN eurjchem-71 121 48     SPACE eurjchem-71 121 49 acid acid NOUN eurjchem-71 121 50     SPACE eurjchem-71 121 51 group group NOUN eurjchem-71 121 52     SPACE eurjchem-71 121 53 ( ( PUNCT eurjchem-71 121 54 νoh νoh NOUN eurjchem-71 121 55 , , PUNCT eurjchem-71 121 56     SPACE eurjchem-71 121 57 νco νco NOUN eurjchem-71 121 58 ) ) PUNCT eurjchem-71 121 59 . . PUNCT eurjchem-71 121 60     SPACE eurjchem-71 122 1 1h‐nmr 1h‐nmr NUM eurjchem-71 122 2     SPACE eurjchem-71 122 3 spectrum spectrum NOUN eurjchem-71 122 4     SPACE eurjchem-71 122 5 ( ( PUNCT eurjchem-71 122 6 dmso‐d6 dmso‐d6 NOUN eurjchem-71 122 7 ) ) PUNCT eurjchem-71 122 8     SPACE eurjchem-71 122 9 of of ADP eurjchem-71 122 10     SPACE eurjchem-71 122 11 12 12 NUM eurjchem-71 122 12     SPACE eurjchem-71 122 13 revealed reveal VERB eurjchem-71 122 14     SPACE eurjchem-71 122 15 the the DET eurjchem-71 122 16     SPACE eurjchem-71 122 17 signals signal NOUN eurjchem-71 122 18     SPACE eurjchem-71 122 19 at at ADP eurjchem-71 122 20     SPACE eurjchem-71 122 21 δ δ PROPN eurjchem-71 122 22     SPACE eurjchem-71 122 23 7.6‐6.5 7.6‐6.5 NUM eurjchem-71 122 24     SPACE eurjchem-71 122 25 ( ( PUNCT eurjchem-71 122 26 m m PROPN eurjchem-71 122 27 , , PUNCT eurjchem-71 122 28     SPACE eurjchem-71 122 29 12 12 NUM eurjchem-71 122 30     SPACE eurjchem-71 122 31 harom harom NOUN eurjchem-71 122 32 . . PUNCT eurjchem-71 122 33 ) ) PUNCT eurjchem-71 122 34 , , PUNCT eurjchem-71 122 35     SPACE eurjchem-71 122 36 5.7‐5.6 5.7‐5.6 NUM eurjchem-71 122 37     SPACE eurjchem-71 122 38 ( ( PUNCT eurjchem-71 122 39 d d PROPN eurjchem-71 122 40 , , PUNCT eurjchem-71 122 41     SPACE eurjchem-71 122 42 ih ih X eurjchem-71 122 43 , , PUNCT eurjchem-71 122 44     SPACE eurjchem-71 122 45 j j PROPN eurjchem-71 122 46     SPACE eurjchem-71 122 47 = = NOUN eurjchem-71 122 48     SPACE eurjchem-71 122 49 12 12 NUM eurjchem-71 122 50     SPACE eurjchem-71 122 51 hz hz NOUN eurjchem-71 122 52 ) ) PUNCT eurjchem-71 122 53 , , PUNCT eurjchem-71 122 54     SPACE eurjchem-71 122 55 5.0‐4.97 5.0‐4.97 NOUN eurjchem-71 122 56     SPACE eurjchem-71 122 57 ( ( PUNCT eurjchem-71 122 58 d d NOUN eurjchem-71 122 59 , , PUNCT eurjchem-71 122 60     SPACE eurjchem-71 122 61 ih ih X eurjchem-71 122 62 , , PUNCT eurjchem-71 122 63     SPACE eurjchem-71 122 64 j j PROPN eurjchem-71 122 65     SPACE eurjchem-71 122 66 = = NOUN eurjchem-71 122 67     SPACE eurjchem-71 122 68 9 9 NUM eurjchem-71 122 69     SPACE eurjchem-71 122 70 hz hz NOUN eurjchem-71 122 71 ) ) PUNCT eurjchem-71 122 72     SPACE eurjchem-71 122 73 and and CCONJ eurjchem-71 122 74     SPACE eurjchem-71 122 75 3.69 3.69 NUM eurjchem-71 122 76     SPACE eurjchem-71 122 77 ( ( PUNCT eurjchem-71 122 78 s s PROPN eurjchem-71 122 79 , , PUNCT eurjchem-71 122 80     SPACE eurjchem-71 122 81 6h 6h NOUN eurjchem-71 122 82 , , PUNCT eurjchem-71 122 83     SPACE eurjchem-71 122 84 2ome 2ome NUM eurjchem-71 122 85 ) ) PUNCT eurjchem-71 122 86 . . PUNCT eurjchem-71 122 87     SPACE eurjchem-71 123 1 treatment treatment NOUN eurjchem-71 123 2     SPACE eurjchem-71 123 3 of of ADP eurjchem-71 123 4     SPACE eurjchem-71 123 5 the the DET eurjchem-71 123 6     SPACE eurjchem-71 123 7 isochromene isochromene NOUN eurjchem-71 123 8     SPACE eurjchem-71 123 9 dione dione NOUN eurjchem-71 123 10     SPACE eurjchem-71 123 11 2 2 NUM eurjchem-71 123 12     SPACE eurjchem-71 123 13 with with ADP eurjchem-71 123 14     SPACE eurjchem-71 123 15 p‐ p‐ NOUN eurjchem-71 123 16 toluenesulfonohydrazide toluenesulfonohydrazide NOUN eurjchem-71 123 17     SPACE eurjchem-71 123 18 in in ADP eurjchem-71 123 19     SPACE eurjchem-71 123 20 refluxing refluxing NOUN eurjchem-71 123 21     SPACE eurjchem-71 123 22 dioxane dioxane NOUN eurjchem-71 123 23     SPACE eurjchem-71 123 24 yielded yield VERB eurjchem-71 123 25     SPACE eurjchem-71 123 26 the the DET eurjchem-71 123 27     SPACE eurjchem-71 123 28 hydrazide hydrazide ADJ eurjchem-71 123 29     SPACE eurjchem-71 123 30 derivative derivative NOUN eurjchem-71 123 31     SPACE eurjchem-71 123 32 13 13 NUM eurjchem-71 123 33     SPACE eurjchem-71 123 34 ( ( PUNCT eurjchem-71 123 35 scheme scheme NOUN eurjchem-71 123 36     SPACE eurjchem-71 123 37 9 9 NUM eurjchem-71 123 38 ) ) PUNCT eurjchem-71 123 39 . . PUNCT eurjchem-71 123 40     SPACE eurjchem-71 124 1 the the DET eurjchem-71 124 2     SPACE eurjchem-71 124 3 reactivity reactivity NOUN eurjchem-71 124 4     SPACE eurjchem-71 124 5 of of ADP eurjchem-71 124 6     SPACE eurjchem-71 124 7 compound compound NOUN eurjchem-71 124 8     SPACE eurjchem-71 124 9 2 2 NUM eurjchem-71 124 10     SPACE eurjchem-71 124 11 towards towards ADP eurjchem-71 124 12     SPACE eurjchem-71 124 13 the the DET eurjchem-71 124 14     SPACE eurjchem-71 124 15 carbon carbon NOUN eurjchem-71 124 16     SPACE eurjchem-71 124 17 nucleophiles nucleophile NOUN eurjchem-71 124 18     SPACE eurjchem-71 124 19 has have AUX eurjchem-71 124 20     SPACE eurjchem-71 124 21 been be AUX eurjchem-71 124 22     SPACE eurjchem-71 124 23 investigated investigate VERB eurjchem-71 124 24     SPACE eurjchem-71 124 25 too too ADV eurjchem-71 124 26 . . PUNCT eurjchem-71 124 27     SPACE eurjchem-71 125 1 thus thus ADV eurjchem-71 125 2 , , PUNCT eurjchem-71 125 3     SPACE eurjchem-71 125 4 isochromene‐1,3‐ isochromene‐1,3‐ PROPN eurjchem-71 125 5 dione dione NOUN eurjchem-71 125 6     SPACE eurjchem-71 125 7 2 2 NUM eurjchem-71 125 8     SPACE eurjchem-71 125 9 when when SCONJ eurjchem-71 125 10     SPACE eurjchem-71 125 11 reacted react VERB eurjchem-71 125 12     SPACE eurjchem-71 125 13 with with ADP eurjchem-71 125 14     SPACE eurjchem-71 125 15 ethyl ethyl PROPN eurjchem-71 125 16     SPACE eurjchem-71 125 17 cyanoacetate cyanoacetate NOUN eurjchem-71 125 18     SPACE eurjchem-71 125 19 in in ADP eurjchem-71 125 20     SPACE eurjchem-71 125 21 the the DET eurjchem-71 125 22     SPACE eurjchem-71 125 23 presence presence NOUN eurjchem-71 125 24     SPACE eurjchem-71 125 25 of of ADP eurjchem-71 125 26     SPACE eurjchem-71 125 27 triethylamine triethylamine NOUN eurjchem-71 125 28     SPACE eurjchem-71 125 29 in in ADP eurjchem-71 125 30     SPACE eurjchem-71 125 31 boiling boil VERB eurjchem-71 125 32     SPACE eurjchem-71 125 33 dioxane dioxane NOUN eurjchem-71 125 34     SPACE eurjchem-71 125 35 afforded afford VERB eurjchem-71 125 36     SPACE eurjchem-71 125 37 the the DET eurjchem-71 125 38     SPACE eurjchem-71 125 39 unexpected unexpected ADJ eurjchem-71 125 40     SPACE eurjchem-71 125 41 ethyl‐α‐cyano‐3,4‐dimethoxy ethyl‐α‐cyano‐3,4‐dimethoxy PROPN eurjchem-71 125 42     SPACE eurjchem-71 125 43 cinnamate cinnamate NOUN eurjchem-71 125 44     SPACE eurjchem-71 126 1 [ [ X eurjchem-71 126 2 32 32 NUM eurjchem-71 126 3 ] ] SYM eurjchem-71 126 4     SPACE eurjchem-71 126 5 14 14 NUM eurjchem-71 126 6 . . PUNCT eurjchem-71 126 7       SPACE eurjchem-71 127 1 the the DET eurjchem-71 127 2     SPACE eurjchem-71 127 3 structure structure NOUN eurjchem-71 127 4     SPACE eurjchem-71 127 5 of of ADP eurjchem-71 127 6     SPACE eurjchem-71 127 7 14 14 NUM eurjchem-71 127 8     SPACE eurjchem-71 127 9 was be AUX eurjchem-71 127 10     SPACE eurjchem-71 127 11 confirmed confirm VERB eurjchem-71 127 12     SPACE eurjchem-71 127 13 besides besides SCONJ eurjchem-71 127 14     SPACE eurjchem-71 127 15 the the DET eurjchem-71 127 16     SPACE eurjchem-71 127 17 spectroscopic spectroscopic NOUN eurjchem-71 127 18     SPACE eurjchem-71 127 19 data datum NOUN eurjchem-71 127 20     SPACE eurjchem-71 127 21 by by ADP eurjchem-71 127 22     SPACE eurjchem-71 127 23 identity identity NOUN eurjchem-71 127 24     SPACE eurjchem-71 127 25 with with ADP eurjchem-71 127 26     SPACE eurjchem-71 127 27 an an DET eurjchem-71 127 28     SPACE eurjchem-71 127 29 authentic authentic ADJ eurjchem-71 127 30     SPACE eurjchem-71 127 31 sample sample NOUN eurjchem-71 127 32     SPACE eurjchem-71 127 33 obtained obtain VERB eurjchem-71 127 34     SPACE eurjchem-71 127 35 from from ADP eurjchem-71 127 36     SPACE eurjchem-71 127 37 the the DET eurjchem-71 127 38     SPACE eurjchem-71 127 39 condensation condensation NOUN eurjchem-71 127 40     SPACE eurjchem-71 127 41 of of ADP eurjchem-71 127 42     SPACE eurjchem-71 127 43 3,4‐dimethoxybenzaldehyde 3,4‐dimethoxybenzaldehyde NOUN eurjchem-71 127 44     SPACE eurjchem-71 127 45 with with ADP eurjchem-71 127 46     SPACE eurjchem-71 127 47 ethyl ethyl PROPN eurjchem-71 127 48     SPACE eurjchem-71 127 49 cyanoacetate cyanoacetate NOUN eurjchem-71 127 50     SPACE eurjchem-71 127 51 in in ADP eurjchem-71 127 52     SPACE eurjchem-71 127 53 refluxing refluxing NOUN eurjchem-71 127 54     SPACE eurjchem-71 127 55 ethanol ethanol NOUN eurjchem-71 127 56     SPACE eurjchem-71 127 57 in in ADP eurjchem-71 127 58     SPACE eurjchem-71 127 59 the the DET eurjchem-71 127 60     SPACE eurjchem-71 127 61 presence presence NOUN eurjchem-71 127 62     SPACE eurjchem-71 127 63 of of ADP eurjchem-71 127 64     SPACE eurjchem-71 127 65 drops drop VERB eurjchem-71 127 66     SPACE eurjchem-71 127 67 piperidine piperidine NOUN eurjchem-71 127 68 . . PUNCT eurjchem-71 127 69     SPACE eurjchem-71 128 1 the the DET eurjchem-71 128 2     SPACE eurjchem-71 128 3 formation formation NOUN eurjchem-71 128 4     SPACE eurjchem-71 128 5 of of ADP eurjchem-71 128 6     SPACE eurjchem-71 128 7 14 14 NUM eurjchem-71 128 8     SPACE eurjchem-71 128 9 could could AUX eurjchem-71 128 10     SPACE eurjchem-71 128 11 be be AUX eurjchem-71 128 12     SPACE eurjchem-71 128 13 explained explain VERB eurjchem-71 128 14     SPACE eurjchem-71 128 15 as as ADP eurjchem-71 128 16     SPACE eurjchem-71 128 17 outlined outline VERB eurjchem-71 128 18     SPACE eurjchem-71 128 19 in in ADP eurjchem-71 128 20     SPACE eurjchem-71 128 21 scheme scheme NOUN eurjchem-71 128 22     SPACE eurjchem-71 128 23 10 10 NUM eurjchem-71 128 24 . . PUNCT eurjchem-71 128 25           SPACE eurjchem-71 128 26 2 2 NUM eurjchem-71 128 27 dioxane dioxane NOUN eurjchem-71 128 28 / / SYM eurjchem-71 128 29 14 14 NUM eurjchem-71 128 30 11 11 NUM eurjchem-71 128 31 12 12 NUM eurjchem-71 128 32 ar ar NOUN eurjchem-71 128 33 = = SYM eurjchem-71 128 34 -c6h3(ome)2 -c6h3(ome)2 PROPN eurjchem-71 128 35 3:4 3:4 NUM eurjchem-71 128 36 13 13 NUM eurjchem-71 128 37 hs hs PROPN eurjchem-71 128 38 h2n h2n PROPN eurjchem-71 128 39 co2h co2h PROPN eurjchem-71 128 40 n n CCONJ eurjchem-71 128 41 sar sar AUX eurjchem-71 128 42 har har VERB eurjchem-71 128 43 co2h co2h PROPN eurjchem-71 128 44 o o PROPN eurjchem-71 128 45 nh nh PROPN eurjchem-71 128 46 - - PUNCT eurjchem-71 128 47 nh nh PROPN eurjchem-71 128 48 - - PUNCT eurjchem-71 128 49 so2 so2 NOUN eurjchem-71 128 50 me me PROPN eurjchem-71 128 51 nh2 nh2 PROPN eurjchem-71 128 52 - - PUNCT eurjchem-71 128 53 nh nh PROPN eurjchem-71 128 54 - - PUNCT eurjchem-71 128 55 so2 so2 NOUN eurjchem-71 128 56 me me PROPN eurjchem-71 128 57 dioxane dioxane NOUN eurjchem-71 128 58 co2h co2h PROPN eurjchem-71 128 59 co2h co2h PROPN eurjchem-71 128 60 h h PROPN eurjchem-71 128 61 ar ar PROPN eurjchem-71 128 62 sph sph PROPN eurjchem-71 128 63 h h PROPN eurjchem-71 128 64 dioxane dioxane PROPN eurjchem-71 128 65 / / PUNCT eurjchem-71 128 66 sh sh INTJ eurjchem-71 128 67 cn cn PROPN eurjchem-71 128 68 co2et co2et VERB eurjchem-71 128 69 net3 net3 NOUN eurjchem-71 128 70 / / SYM eurjchem-71 128 71 dioxane dioxane NOUN eurjchem-71 128 72 cn cn PROPN eurjchem-71 128 73 co2et co2et VERB eurjchem-71 128 74 ar ar NOUN eurjchem-71 128 75 h h PROPN eurjchem-71 128 76 scheme scheme NOUN eurjchem-71 128 77     SPACE eurjchem-71 128 78 9 9 NUM eurjchem-71 128 79         SPACE eurjchem-71 128 80 scheme scheme NOUN eurjchem-71 128 81     SPACE eurjchem-71 128 82 10 10 NUM eurjchem-71 128 83         SPACE eurjchem-71 128 84 3.2 3.2 NUM eurjchem-71 128 85 . . PUNCT eurjchem-71 128 86     SPACE eurjchem-71 128 87 biological biological ADJ eurjchem-71 128 88     SPACE eurjchem-71 128 89 investigation­antimicrobial investigation­antimicrobial ADJ eurjchem-71 128 90     SPACE eurjchem-71 128 91 activity activity NOUN eurjchem-71 128 92           SPACE eurjchem-71 128 93 the the DET eurjchem-71 128 94     SPACE eurjchem-71 128 95 antimicrobial antimicrobial ADJ eurjchem-71 128 96     SPACE eurjchem-71 128 97 screening screening NOUN eurjchem-71 128 98     SPACE eurjchem-71 128 99 of of ADP eurjchem-71 128 100     SPACE eurjchem-71 128 101 some some PRON eurjchem-71 128 102     SPACE eurjchem-71 128 103 of of ADP eurjchem-71 128 104     SPACE eurjchem-71 128 105 the the DET eurjchem-71 128 106     SPACE eurjchem-71 128 107 synthesized synthesize VERB eurjchem-71 128 108     SPACE eurjchem-71 128 109 compounds compound NOUN eurjchem-71 128 110     SPACE eurjchem-71 128 111 was be AUX eurjchem-71 128 112     SPACE eurjchem-71 128 113 done do VERB eurjchem-71 128 114     SPACE eurjchem-71 128 115 using use VERB eurjchem-71 128 116     SPACE eurjchem-71 128 117 the the DET eurjchem-71 128 118     SPACE eurjchem-71 128 119 agar agar NOUN eurjchem-71 128 120     SPACE eurjchem-71 128 121 diffusion diffusion NOUN eurjchem-71 128 122     SPACE eurjchem-71 128 123 assay assay NOUN eurjchem-71 128 124 . . PUNCT eurjchem-71 128 125     SPACE eurjchem-71 129 1 this this DET eurjchem-71 129 2     SPACE eurjchem-71 129 3 screening screening NOUN eurjchem-71 129 4     SPACE eurjchem-71 129 5 was be AUX eurjchem-71 129 6     SPACE eurjchem-71 129 7 performed perform VERB eurjchem-71 129 8     SPACE eurjchem-71 129 9 against against ADP eurjchem-71 129 10     SPACE eurjchem-71 129 11 the the DET eurjchem-71 129 12     SPACE eurjchem-71 129 13 gram‐negative gram‐negative ADJ eurjchem-71 129 14     SPACE eurjchem-71 129 15 bacteria bacteria NOUN eurjchem-71 129 16 , , PUNCT eurjchem-71 129 17     SPACE eurjchem-71 129 18 escherichia escherichia NOUN eurjchem-71 129 19     SPACE eurjchem-71 129 20 coli coli NOUN eurjchem-71 129 21     SPACE eurjchem-71 129 22 atcc atcc NOUN eurjchem-71 129 23     SPACE eurjchem-71 129 24 10536 10536 NUM eurjchem-71 129 25     SPACE eurjchem-71 129 26 and and CCONJ eurjchem-71 129 27     SPACE eurjchem-71 129 28 gram‐positive gram‐positive ADJ eurjchem-71 129 29     SPACE eurjchem-71 129 30 bacteria bacteria NOUN eurjchem-71 129 31 , , PUNCT eurjchem-71 129 32     SPACE eurjchem-71 129 33 staphylococcus staphylococcus NOUN eurjchem-71 129 34     SPACE eurjchem-71 129 35 aureus aureus NOUN eurjchem-71 129 36     SPACE eurjchem-71 129 37 atcc atcc NOUN eurjchem-71 129 38     SPACE eurjchem-71 129 39 06538 06538 NUM eurjchem-71 129 40     SPACE eurjchem-71 129 41 in in ADP eurjchem-71 129 42     SPACE eurjchem-71 129 43 addition addition NOUN eurjchem-71 129 44     SPACE eurjchem-71 129 45 to to ADP eurjchem-71 129 46     SPACE eurjchem-71 129 47 the the DET eurjchem-71 129 48     SPACE eurjchem-71 129 49 pathogenic pathogenic ADJ eurjchem-71 129 50     SPACE eurjchem-71 129 51 fungi fungi PROPN eurjchem-71 129 52     SPACE eurjchem-71 129 53 candida candida NOUN eurjchem-71 129 54     SPACE eurjchem-71 129 55 albicans albican NOUN eurjchem-71 129 56     SPACE eurjchem-71 129 57 atcc atcc NOUN eurjchem-71 129 58     SPACE eurjchem-71 129 59 1023 1023 NUM eurjchem-71 129 60     SPACE eurjchem-71 129 61 and and CCONJ eurjchem-71 129 62     SPACE eurjchem-71 129 63 aspergilus aspergilus ADJ eurjchem-71 129 64     SPACE eurjchem-71 129 65 flavus flavus NOUN eurjchem-71 129 66 . . PUNCT eurjchem-71 129 67     SPACE eurjchem-71 130 1 a a DET eurjchem-71 130 2     SPACE eurjchem-71 130 3 strong strong ADJ eurjchem-71 130 4     SPACE eurjchem-71 130 5 activity activity NOUN eurjchem-71 130 6     SPACE eurjchem-71 130 7 was be AUX eurjchem-71 130 8     SPACE eurjchem-71 130 9 observed observe VERB eurjchem-71 130 10     SPACE eurjchem-71 130 11 with with ADP eurjchem-71 130 12     SPACE eurjchem-71 130 13 compounds compound NOUN eurjchem-71 130 14     SPACE eurjchem-71 130 15 4 4 NUM eurjchem-71 130 16 , , PUNCT eurjchem-71 130 17     SPACE eurjchem-71 130 18 9 9 NUM eurjchem-71 130 19 , , PUNCT eurjchem-71 130 20     SPACE eurjchem-71 130 21 11 11 NUM eurjchem-71 130 22 , , PUNCT eurjchem-71 130 23     SPACE eurjchem-71 130 24 12 12 NUM eurjchem-71 130 25     SPACE eurjchem-71 130 26 and and CCONJ eurjchem-71 130 27     SPACE eurjchem-71 130 28 13 13 NUM eurjchem-71 130 29     SPACE eurjchem-71 130 30 which which PRON eurjchem-71 130 31     SPACE eurjchem-71 130 32 proved prove VERB eurjchem-71 130 33     SPACE eurjchem-71 130 34 to to PART eurjchem-71 130 35     SPACE eurjchem-71 130 36 possess possess VERB eurjchem-71 130 37     SPACE eurjchem-71 130 38 marked mark VERB eurjchem-71 130 39     SPACE eurjchem-71 130 40 activity activity NOUN eurjchem-71 130 41     SPACE eurjchem-71 130 42 against against ADP eurjchem-71 130 43     SPACE eurjchem-71 130 44 e. e. PROPN eurjchem-71 130 45     SPACE eurjchem-71 130 46 coli coli NOUN eurjchem-71 130 47 , , PUNCT eurjchem-71 130 48     SPACE eurjchem-71 130 49 s. s. PROPN eurjchem-71 130 50     SPACE eurjchem-71 130 51 aurous aurous ADJ eurjchem-71 130 52     SPACE eurjchem-71 130 53 and and CCONJ eurjchem-71 130 54     SPACE eurjchem-71 130 55 c. c. NOUN eurjchem-71 130 56     SPACE eurjchem-71 130 57 albicans albican NOUN eurjchem-71 130 58 . . PUNCT eurjchem-71 130 59     SPACE eurjchem-71 131 1 the the DET eurjchem-71 131 2     SPACE eurjchem-71 131 3 inhibitory inhibitory ADJ eurjchem-71 131 4     SPACE eurjchem-71 131 5 concentration concentration NOUN eurjchem-71 131 6     SPACE eurjchem-71 131 7 was be AUX eurjchem-71 131 8     SPACE eurjchem-71 131 9 determined determine VERB eurjchem-71 131 10     SPACE eurjchem-71 131 11 for for ADP eurjchem-71 131 12     SPACE eurjchem-71 131 13 each each PRON eurjchem-71 131 14     SPACE eurjchem-71 131 15 of of ADP eurjchem-71 131 16     SPACE eurjchem-71 131 17 the the DET eurjchem-71 131 18     SPACE eurjchem-71 131 19 active active ADJ eurjchem-71 131 20     SPACE eurjchem-71 131 21 compounds compound NOUN eurjchem-71 131 22     SPACE eurjchem-71 131 23 along along ADP eurjchem-71 131 24     SPACE eurjchem-71 131 25 with with ADP eurjchem-71 131 26     SPACE eurjchem-71 131 27 tetracycline tetracycline NOUN eurjchem-71 131 28     SPACE eurjchem-71 131 29 antibacterial antibacterial ADJ eurjchem-71 131 30     SPACE eurjchem-71 131 31 agent agent NOUN eurjchem-71 131 32     SPACE eurjchem-71 131 33 and and CCONJ eurjchem-71 131 34     SPACE eurjchem-71 131 35 amphotericin amphotericin VERB eurjchem-71 131 36     SPACE eurjchem-71 131 37 b b X eurjchem-71 131 38     SPACE eurjchem-71 131 39 antifungal antifungal ADJ eurjchem-71 131 40     SPACE eurjchem-71 131 41 agent agent NOUN eurjchem-71 131 42 . . PUNCT eurjchem-71 131 43     SPACE eurjchem-71 132 1 no no DET eurjchem-71 132 2     SPACE eurjchem-71 132 3 activity activity NOUN eurjchem-71 132 4     SPACE eurjchem-71 132 5 was be AUX eurjchem-71 132 6     SPACE eurjchem-71 132 7 detected detect VERB eurjchem-71 132 8     SPACE eurjchem-71 132 9 for for ADP eurjchem-71 132 10     SPACE eurjchem-71 132 11 all all PRON eurjchem-71 132 12     SPACE eurjchem-71 132 13 the the DET eurjchem-71 132 14     SPACE eurjchem-71 132 15 synthesized synthesize VERB eurjchem-71 132 16     SPACE eurjchem-71 132 17 compounds compound NOUN eurjchem-71 132 18     SPACE eurjchem-71 132 19 towards towards ADP eurjchem-71 132 20     SPACE eurjchem-71 132 21 aspergilus aspergilus ADJ eurjchem-71 132 22     SPACE eurjchem-71 132 23 flavus flavus NOUN eurjchem-71 132 24 . . PUNCT eurjchem-71 132 25     SPACE eurjchem-71 133 1 results result NOUN eurjchem-71 133 2     SPACE eurjchem-71 133 3 are be AUX eurjchem-71 133 4     SPACE eurjchem-71 133 5 shown show VERB eurjchem-71 133 6     SPACE eurjchem-71 133 7 in in ADP eurjchem-71 133 8     SPACE eurjchem-71 133 9 table table NOUN eurjchem-71 133 10     SPACE eurjchem-71 133 11 1 1 NUM eurjchem-71 133 12 . . PUNCT eurjchem-71 133 13                             SPACE eurjchem-71 133 14 mahmoud mahmoud PROPN eurjchem-71 133 15     SPACE eurjchem-71 133 16 et et PROPN eurjchem-71 133 17     SPACE eurjchem-71 133 18 al al PROPN eurjchem-71 133 19 . . PROPN eurjchem-71 133 20     SPACE eurjchem-71 133 21 / / SYM eurjchem-71 133 22     SPACE eurjchem-71 133 23 european european ADJ eurjchem-71 133 24     SPACE eurjchem-71 133 25 journal journal NOUN eurjchem-71 133 26     SPACE eurjchem-71 133 27 of of ADP eurjchem-71 133 28     SPACE eurjchem-71 133 29 chemistry chemistry NOUN eurjchem-71 133 30     SPACE eurjchem-71 133 31 1 1 NUM eurjchem-71 133 32     SPACE eurjchem-71 133 33 ( ( PUNCT eurjchem-71 133 34 2 2 NUM eurjchem-71 133 35 ) ) PUNCT eurjchem-71 133 36     SPACE eurjchem-71 133 37 ( ( PUNCT eurjchem-71 133 38 2010 2010 NUM eurjchem-71 133 39 ) ) PUNCT eurjchem-71 133 40     SPACE eurjchem-71 133 41 134­139 134­139 NUM eurjchem-71 133 42     SPACE eurjchem-71 133 43 139 139 NUM eurjchem-71 133 44     SPACE eurjchem-71 133 45 table table NOUN eurjchem-71 133 46     SPACE eurjchem-71 133 47 1 1 NUM eurjchem-71 133 48 . . PUNCT eurjchem-71 133 49     SPACE eurjchem-71 133 50 antimicrobial antimicrobial ADJ eurjchem-71 133 51     SPACE eurjchem-71 133 52 screening screening NOUN eurjchem-71 133 53     SPACE eurjchem-71 133 54 results result NOUN eurjchem-71 133 55     SPACE eurjchem-71 133 56 of of ADP eurjchem-71 133 57     SPACE eurjchem-71 133 58 the the DET eurjchem-71 133 59     SPACE eurjchem-71 133 60 tested test VERB eurjchem-71 133 61     SPACE eurjchem-71 133 62 compounds compound NOUN eurjchem-71 133 63     SPACE eurjchem-71 133 64 at at ADP eurjchem-71 133 65     SPACE eurjchem-71 133 66 1000 1000 NUM eurjchem-71 133 67     SPACE eurjchem-71 133 68 g g PROPN eurjchem-71 133 69 / / SYM eurjchem-71 133 70 mla mla PROPN eurjchem-71 133 71 . . PUNCT eurjchem-71 133 72     SPACE eurjchem-71 133 73 sample sample NOUN eurjchem-71 133 74     SPACE eurjchem-71 133 75 inhibition inhibition NOUN eurjchem-71 133 76     SPACE eurjchem-71 133 77 zone zone NOUN eurjchem-71 133 78     SPACE eurjchem-71 133 79 diameter diameter NOUN eurjchem-71 133 80     SPACE eurjchem-71 133 81 ( ( PUNCT eurjchem-71 133 82 mm mm PROPN eurjchem-71 133 83 / / SYM eurjchem-71 133 84 mg mg PROPN eurjchem-71 133 85     SPACE eurjchem-71 133 86 sample sample NOUN eurjchem-71 133 87 ) ) PUNCT eurjchem-71 133 88     SPACE eurjchem-71 133 89 escherichia escherichia NOUN eurjchem-71 133 90     SPACE eurjchem-71 133 91 coli coli NOUN eurjchem-71 133 92     SPACE eurjchem-71 133 93 ( ( PUNCT eurjchem-71 133 94 g­ g­ PROPN eurjchem-71 133 95 ) ) PUNCT eurjchem-71 133 96     SPACE eurjchem-71 133 97 staphylococcus staphylococcus NOUN eurjchem-71 133 98     SPACE eurjchem-71 133 99 aureus aureus NOUN eurjchem-71 133 100     SPACE eurjchem-71 133 101 ( ( PUNCT eurjchem-71 133 102 g+ g+ NOUN eurjchem-71 133 103 ) ) PUNCT eurjchem-71 133 104     SPACE eurjchem-71 133 105 aspergilus aspergilus PROPN eurjchem-71 133 106       SPACE eurjchem-71 133 107 flavus flavus NOUN eurjchem-71 133 108     SPACE eurjchem-71 133 109 ( ( PUNCT eurjchem-71 133 110 fungus fungus NOUN eurjchem-71 133 111 ) ) PUNCT eurjchem-71 133 112     SPACE eurjchem-71 133 113 candida candida NOUN eurjchem-71 133 114     SPACE eurjchem-71 133 115 albicans albican NOUN eurjchem-71 133 116     SPACE eurjchem-71 133 117 ( ( PUNCT eurjchem-71 133 118 fungus fungus NOUN eurjchem-71 133 119 ) ) PUNCT eurjchem-71 133 120     SPACE eurjchem-71 133 121 control control NOUN eurjchem-71 133 122     SPACE eurjchem-71 133 123 : : PUNCT eurjchem-71 133 124     SPACE eurjchem-71 133 125 dmso dmso VERB eurjchem-71 133 126 0.0 0.0 NUM eurjchem-71 133 127 0.0 0.0 NUM eurjchem-71 133 128 0.0 0.0 NUM eurjchem-71 133 129     SPACE eurjchem-71 133 130 0.0 0.0 NUM eurjchem-71 133 131 tetracycline tetracycline NOUN eurjchem-71 133 132     SPACE eurjchem-71 133 133 antibacterial antibacterial ADJ eurjchem-71 133 134     SPACE eurjchem-71 133 135 agent agent NOUN eurjchem-71 133 136     SPACE eurjchem-71 133 137 ( ( PUNCT eurjchem-71 133 138 standard standard NOUN eurjchem-71 133 139 ) ) PUNCT eurjchem-71 133 140     SPACE eurjchem-71 133 141 32 32 NUM eurjchem-71 133 142 30 30 NUM eurjchem-71 133 143 ‐‐ ‐‐ NOUN eurjchem-71 133 144     SPACE eurjchem-71 133 145 ‐‐ ‐‐ NOUN eurjchem-71 133 146 amphotericin amphotericin VERB eurjchem-71 133 147     SPACE eurjchem-71 133 148 b b X eurjchem-71 133 149     SPACE eurjchem-71 133 150 antifungal antifungal ADJ eurjchem-71 133 151     SPACE eurjchem-71 133 152 agent agent NOUN eurjchem-71 133 153     SPACE eurjchem-71 133 154 ( ( PUNCT eurjchem-71 133 155 standard standard NOUN eurjchem-71 133 156 ) ) PUNCT eurjchem-71 133 157     SPACE eurjchem-71 133 158 ‐‐ ‐‐ NOUN eurjchem-71 133 159 ‐‐ ‐‐ PROPN eurjchem-71 133 160 18 18 NUM eurjchem-71 133 161     SPACE eurjchem-71 133 162 20 20 NUM eurjchem-71 133 163 4 4 NUM eurjchem-71 133 164     SPACE eurjchem-71 133 165 15 15 NUM eurjchem-71 133 166 15 15 NUM eurjchem-71 133 167 0.0 0.0 NUM eurjchem-71 133 168     SPACE eurjchem-71 133 169 0.0 0.0 NUM eurjchem-71 133 170 9 9 NUM eurjchem-71 133 171     SPACE eurjchem-71 133 172 17 17 NUM eurjchem-71 133 173 18 18 NUM eurjchem-71 133 174 0.0 0.0 NUM eurjchem-71 133 175     SPACE eurjchem-71 133 176 16 16 NUM eurjchem-71 133 177 11 11 NUM eurjchem-71 133 178     SPACE eurjchem-71 133 179 15 15 NUM eurjchem-71 133 180 14 14 NUM eurjchem-71 133 181 0.0 0.0 NUM eurjchem-71 133 182     SPACE eurjchem-71 133 183 0.0 0.0 NUM eurjchem-71 133 184 12 12 NUM eurjchem-71 133 185     SPACE eurjchem-71 133 186 16 16 NUM eurjchem-71 133 187 17 17 NUM eurjchem-71 133 188 0.0 0.0 NUM eurjchem-71 133 189     SPACE eurjchem-71 133 190 0.0 0.0 NUM eurjchem-71 133 191 13 13 NUM eurjchem-71 133 192     SPACE eurjchem-71 133 193 18 18 NUM eurjchem-71 133 194 16 16 NUM eurjchem-71 133 195 0.0 0.0 NUM eurjchem-71 133 196     SPACE eurjchem-71 133 197 15 15 NUM eurjchem-71 133 198 a a DET eurjchem-71 133 199     SPACE eurjchem-71 133 200 0.0 0.0 NUM eurjchem-71 133 201 , , PUNCT eurjchem-71 133 202     SPACE eurjchem-71 133 203 no no DET eurjchem-71 133 204     SPACE eurjchem-71 133 205 activity activity NOUN eurjchem-71 133 206 , , PUNCT eurjchem-71 133 207     SPACE eurjchem-71 133 208 ( ( PUNCT eurjchem-71 133 209 inhibition inhibition NOUN eurjchem-71 133 210     SPACE eurjchem-71 133 211 zone zone NOUN eurjchem-71 133 212     SPACE eurjchem-71 133 213 < < X eurjchem-71 133 214     SPACE eurjchem-71 133 215 7 7 NUM eurjchem-71 133 216     SPACE eurjchem-71 133 217 mm mm NOUN eurjchem-71 133 218 ) ) PUNCT eurjchem-71 133 219 , , PUNCT eurjchem-71 133 220     SPACE eurjchem-71 133 221 weak weak ADJ eurjchem-71 133 222     SPACE eurjchem-71 133 223 activity activity NOUN eurjchem-71 133 224     SPACE eurjchem-71 133 225 ( ( PUNCT eurjchem-71 133 226 7‐10 7‐10 NUM eurjchem-71 133 227     SPACE eurjchem-71 133 228 mm mm NOUN eurjchem-71 133 229 ) ) PUNCT eurjchem-71 133 230 , , PUNCT eurjchem-71 133 231     SPACE eurjchem-71 133 232 moderate moderate ADJ eurjchem-71 133 233     SPACE eurjchem-71 133 234 activity activity NOUN eurjchem-71 133 235     SPACE eurjchem-71 133 236 ( ( PUNCT eurjchem-71 133 237 11‐15 11‐15 NUM eurjchem-71 133 238     SPACE eurjchem-71 133 239 mm mm PROPN eurjchem-71 133 240 ) ) PUNCT eurjchem-71 133 241 , , PUNCT eurjchem-71 133 242     SPACE eurjchem-71 133 243 strong strong ADJ eurjchem-71 133 244     SPACE eurjchem-71 133 245 activity activity NOUN eurjchem-71 133 246     SPACE eurjchem-71 133 247 ( ( PUNCT eurjchem-71 133 248 > > X eurjchem-71 133 249     SPACE eurjchem-71 133 250 15 15 NUM eurjchem-71 133 251     SPACE eurjchem-71 133 252 mm mm NUM eurjchem-71 133 253 ) ) PUNCT eurjchem-71 133 254 . . PUNCT eurjchem-71 133 255     SPACE eurjchem-71 134 1 solvent solvent NOUN eurjchem-71 134 2     SPACE eurjchem-71 134 3 : : PUNCT eurjchem-71 134 4     SPACE eurjchem-71 134 5 dmso dmso NOUN eurjchem-71 134 6 . . PUNCT eurjchem-71 134 7         SPACE eurjchem-71 134 8 references reference NOUN eurjchem-71 134 9         SPACE eurjchem-71 134 10 [ [ X eurjchem-71 134 11 1 1 NUM eurjchem-71 134 12 ] ] PUNCT eurjchem-71 134 13 . . PUNCT eurjchem-71 135 1 alien alien PROPN eurjchem-71 135 2 , , PUNCT eurjchem-71 135 3     SPACE eurjchem-71 135 4 g. g. PROPN eurjchem-71 135 5     SPACE eurjchem-71 135 6 r. r. PROPN eurjchem-71 135 7 ; ; PUNCT eurjchem-71 135 8     SPACE eurjchem-71 135 9 littell littell NOUN eurjchem-71 135 10 , , PUNCT eurjchem-71 135 11     SPACE eurjchem-71 135 12 r. r. PROPN eurjchem-71 135 13 ; ; PUNCT eurjchem-71 135 14     SPACE eurjchem-71 135 15 mcevoy mcevoy NOUN eurjchem-71 135 16 , , PUNCT eurjchem-71 135 17     SPACE eurjchem-71 135 18 f. f. PROPN eurjchem-71 135 19     SPACE eurjchem-71 135 20 j. j. PROPN eurjchem-71 135 21 ; ; PUNCT eurjchem-71 135 22     SPACE eurjchem-71 135 23 sloboda sloboda PROPN eurjchem-71 135 24 , , PUNCT eurjchem-71 135 25     SPACE eurjchem-71 135 26 a. a. NOUN eurjchem-71 135 27     SPACE eurjchem-71 135 28 e. e. PROPN eurjchem-71 135 29     SPACE eurjchem-71 135 30 j. j. PROPN eurjchem-71 135 31     SPACE eurjchem-71 135 32 med med PROPN eurjchem-71 135 33 . . PUNCT eurjchem-71 135 34     SPACE eurjchem-71 135 35 chem chem NOUN eurjchem-71 135 36 . . PUNCT eurjchem-71 135 37     SPACE eurjchem-71 136 1 1972 1972 NUM eurjchem-71 136 2 , , PUNCT eurjchem-71 136 3     SPACE eurjchem-71 136 4 15 15 NUM eurjchem-71 136 5 , , PUNCT eurjchem-71 136 6     SPACE eurjchem-71 136 7 934‐937 934‐937 NUM eurjchem-71 136 8 . . PUNCT eurjchem-71 136 9     SPACE eurjchem-71 137 1 [ [ X eurjchem-71 137 2 2 2 NUM eurjchem-71 137 3 ] ] PUNCT eurjchem-71 137 4 . . PUNCT eurjchem-71 138 1 barry barry PROPN eurjchem-71 138 2 , , PUNCT eurjchem-71 138 3     SPACE eurjchem-71 138 4 r. r. PROPN eurjchem-71 138 5     SPACE eurjchem-71 138 6 p. p. NOUN eurjchem-71 138 7     SPACE eurjchem-71 138 8 chem chem NOUN eurjchem-71 138 9 . . PUNCT eurjchem-71 138 10     SPACE eurjchem-71 138 11 rev rev VERB eurjchem-71 138 12 . . PUNCT eurjchem-71 138 13     SPACE eurjchem-71 138 14 1964 1964 NUM eurjchem-71 138 15 , , PUNCT eurjchem-71 138 16     SPACE eurjchem-71 138 17 64 64 NUM eurjchem-71 138 18 , , PUNCT eurjchem-71 138 19     SPACE eurjchem-71 138 20 229‐260 229‐260 NOUN eurjchem-71 138 21 . . PUNCT eurjchem-71 138 22     SPACE eurjchem-71 139 1 [ [ X eurjchem-71 139 2 3 3 NUM eurjchem-71 139 3 ] ] PUNCT eurjchem-71 139 4 . . PUNCT eurjchem-71 140 1 billingam billingam PROPN eurjchem-71 140 2 , , PUNCT eurjchem-71 140 3     SPACE eurjchem-71 140 4 m. m. NOUN eurjchem-71 140 5     SPACE eurjchem-71 140 6 e. e. PROPN eurjchem-71 140 7     SPACE eurjchem-71 140 8 g. g. PROPN eurjchem-71 140 9     SPACE eurjchem-71 140 10 j. j. PROPN eurjchem-71 140 11     SPACE eurjchem-71 140 12 pharmacol pharmacol PROPN eurjchem-71 140 13 . . PUNCT eurjchem-71 140 14     SPACE eurjchem-71 140 15 1981 1981 NUM eurjchem-71 140 16 , , PUNCT eurjchem-71 140 17     SPACE eurjchem-71 140 18 72 72 NUM eurjchem-71 140 19 , , PUNCT eurjchem-71 140 20     SPACE eurjchem-71 140 21 523‐526 523‐526 NOUN eurjchem-71 140 22 . . PUNCT eurjchem-71 140 23     SPACE eurjchem-71 141 1 [ [ X eurjchem-71 141 2 4 4 NUM eurjchem-71 141 3 ] ] PUNCT eurjchem-71 141 4 . . PUNCT eurjchem-71 142 1 kovacs kovacs PROPN eurjchem-71 142 2 , , PUNCT eurjchem-71 142 3     SPACE eurjchem-71 142 4 t. t. PROPN eurjchem-71 142 5 ; ; PUNCT eurjchem-71 142 6     SPACE eurjchem-71 142 7 sonnenbichler sonnenbichler NOUN eurjchem-71 142 8 , , PUNCT eurjchem-71 142 9     SPACE eurjchem-71 142 10 j. j. PROPN eurjchem-71 142 11     SPACE eurjchem-71 142 12 liebigs liebig VERB eurjchem-71 142 13     SPACE eurjchem-71 142 14 ann ann PROPN eurjchem-71 142 15 . . PUNCT eurjchem-71 142 16     SPACE eurjchem-71 142 17 rcl rcl NOUN eurjchem-71 142 18 . . PUNCT eurjchem-71 142 19     SPACE eurjchem-71 143 1 1997 1997 NUM eurjchem-71 143 2 , , PUNCT eurjchem-71 143 3     SPACE eurjchem-71 143 4 1 1 NUM eurjchem-71 143 5 , , PUNCT eurjchem-71 143 6     SPACE eurjchem-71 143 7 211‐212 211‐212 NUM eurjchem-71 143 8 . . PUNCT eurjchem-71 143 9     SPACE eurjchem-71 144 1 [ [ X eurjchem-71 144 2 5 5 NUM eurjchem-71 144 3 ] ] PUNCT eurjchem-71 144 4 . . PUNCT eurjchem-71 144 5 mali mali PROPN eurjchem-71 144 6 , , PUNCT eurjchem-71 144 7     SPACE eurjchem-71 144 8 r. r. PROPN eurjchem-71 144 9     SPACE eurjchem-71 144 10 s. s. PROPN eurjchem-71 144 11 ; ; PUNCT eurjchem-71 144 12     SPACE eurjchem-71 144 13 babu babu PROPN eurjchem-71 144 14 , , PUNCT eurjchem-71 144 15     SPACE eurjchem-71 144 16 k.n k.n PROPN eurjchem-71 144 17     SPACE eurjchem-71 144 18 . . PUNCT eurjchem-71 144 19     SPACE eurjchem-71 144 20 j. j. PROPN eurjchem-71 144 21     SPACE eurjchem-71 144 22 org org PROPN eurjchem-71 144 23 . . PUNCT eurjchem-71 144 24     SPACE eurjchem-71 144 25 chem chem NOUN eurjchem-71 144 26 . . PUNCT eurjchem-71 144 27     SPACE eurjchem-71 144 28 1998 1998 NUM eurjchem-71 144 29 , , PUNCT eurjchem-71 144 30     SPACE eurjchem-71 144 31 63 63 NUM eurjchem-71 144 32 , , PUNCT eurjchem-71 144 33     SPACE eurjchem-71 144 34 2488 2488 NUM eurjchem-71 144 35 . . PUNCT eurjchem-71 144 36     SPACE eurjchem-71 145 1 [ [ X eurjchem-71 145 2 6 6 NUM eurjchem-71 145 3 ] ] PUNCT eurjchem-71 145 4 . . PUNCT eurjchem-71 146 1 noguchi noguchi PROPN eurjchem-71 146 2 , , PUNCT eurjchem-71 146 3     SPACE eurjchem-71 146 4 s. s. PROPN eurjchem-71 146 5 ; ; PUNCT eurjchem-71 146 6     SPACE eurjchem-71 146 7 kishimoto kishimoto NOUN eurjchem-71 146 8 , , PUNCT eurjchem-71 146 9     SPACE eurjchem-71 146 10 s. s. PROPN eurjchem-71 146 11 ; ; PUNCT eurjchem-71 146 12     SPACE eurjchem-71 146 13 minamida minamida PROPN eurjchem-71 146 14 , , PUNCT eurjchem-71 146 15     SPACE eurjchem-71 146 16 i. i. NOUN eurjchem-71 146 17 ; ; PUNCT eurjchem-71 146 18     SPACE eurjchem-71 146 19 obayashi obayashi ADJ eurjchem-71 146 20 , , PUNCT eurjchem-71 146 21     SPACE eurjchem-71 146 22 m. m. NOUN eurjchem-71 146 23     SPACE eurjchem-71 146 24 chem chem NOUN eurjchem-71 146 25 . . PUNCT eurjchem-71 146 26     SPACE eurjchem-71 146 27 pharm pharm PROPN eurjchem-71 146 28 . . PUNCT eurjchem-71 146 29     SPACE eurjchem-71 146 30 bull bull NOUN eurjchem-71 146 31 . . PUNCT eurjchem-71 146 32     SPACE eurjchem-71 146 33 1974 1974 NUM eurjchem-71 146 34 , , PUNCT eurjchem-71 146 35     SPACE eurjchem-71 146 36 22 22 NUM eurjchem-71 146 37 , , PUNCT eurjchem-71 146 38     SPACE eurjchem-71 146 39 529‐536 529‐536 PROPN eurjchem-71 146 40 . . PUNCT eurjchem-71 146 41     SPACE eurjchem-71 147 1 [ [ X eurjchem-71 147 2 7 7 NUM eurjchem-71 147 3 ] ] PUNCT eurjchem-71 147 4 . . PUNCT eurjchem-71 148 1 stadler stadl ADJ eurjchem-71 148 2 , , PUNCT eurjchem-71 148 3     SPACE eurjchem-71 148 4 m. m. NOUN eurjchem-71 148 5 ; ; PUNCT eurjchem-71 148 6     SPACE eurjchem-71 148 7 anke anke ADJ eurjchem-71 148 8 , , PUNCT eurjchem-71 148 9     SPACE eurjchem-71 148 10 h. h. NOUN eurjchem-71 148 11 ; ; PUNCT eurjchem-71 148 12     SPACE eurjchem-71 148 13 sterner stern ADJ eurjchem-71 148 14 , , PUNCT eurjchem-71 148 15     SPACE eurjchem-71 148 16 o. o. PROPN eurjchem-71 148 17     SPACE eurjchem-71 148 18 j. j. PROPN eurjchem-71 148 19     SPACE eurjchem-71 148 20 antibio antibio PROPN eurjchem-71 148 21 . . PUNCT eurjchem-71 148 22     SPACE eurjchem-71 148 23 1995 1995 NUM eurjchem-71 148 24 , , PUNCT eurjchem-71 148 25     SPACE eurjchem-71 148 26 48 48 NUM eurjchem-71 148 27 , , PUNCT eurjchem-71 148 28     SPACE eurjchem-71 148 29 261‐266 261‐266 NUM eurjchem-71 148 30 . . PUNCT eurjchem-71 148 31     SPACE eurjchem-71 149 1 [ [ X eurjchem-71 149 2 8 8 NUM eurjchem-71 149 3 ] ] PUNCT eurjchem-71 149 4 . . PUNCT eurjchem-71 150 1 chinworrungs chinworrung NOUN eurjchem-71 150 2 , , PUNCT eurjchem-71 150 3     SPACE eurjchem-71 150 4 m. m. NOUN eurjchem-71 150 5 ; ; PUNCT eurjchem-71 150 6     SPACE eurjchem-71 150 7 kittakoop kittakoop NOUN eurjchem-71 150 8 , , PUNCT eurjchem-71 150 9     SPACE eurjchem-71 150 10 p. p. NOUN eurjchem-71 150 11 ; ; PUNCT eurjchem-71 150 12     SPACE eurjchem-71 150 13 isaka isaka ADV eurjchem-71 150 14 , , PUNCT eurjchem-71 150 15     SPACE eurjchem-71 150 16 m. m. NOUN eurjchem-71 150 17 ; ; PUNCT eurjchem-71 150 18     SPACE eurjchem-71 150 19 chanphen chanphen NOUN eurjchem-71 150 20 , , PUNCT eurjchem-71 150 21     SPACE eurjchem-71 150 22 r. r. PROPN eurjchem-71 150 23 ; ; PUNCT eurjchem-71 150 24     SPACE eurjchem-71 150 25 anicharoen anicharoen VERB eurjchem-71 150 26 , , PUNCT eurjchem-71 150 27     SPACE eurjchem-71 150 28 m. m. NOUN eurjchem-71 150 29 ; ; PUNCT eurjchem-71 150 30     SPACE eurjchem-71 150 31 thebtaranonth thebtaranonth ADJ eurjchem-71 150 32 , , PUNCT eurjchem-71 150 33     SPACE eurjchem-71 150 34 y. y. PROPN eurjchem-71 150 35     SPACE eurjchem-71 150 36 j. j. PROPN eurjchem-71 150 37     SPACE eurjchem-71 150 38 chem chem NOUN eurjchem-71 150 39 . . PUNCT eurjchem-71 150 40     SPACE eurjchem-71 150 41 soc soc PROPN eurjchem-71 150 42 . . PUNCT eurjchem-71 151 1 , , PUNCT eurjchem-71 151 2     SPACE eurjchem-71 151 3 perkin perkin PROPN eurjchem-71 151 4     SPACE eurjchem-71 151 5 trans tran NOUN eurjchem-71 151 6     SPACE eurjchem-71 151 7 1 1 NUM eurjchem-71 151 8     SPACE eurjchem-71 151 9 2002 2002 NUM eurjchem-71 151 10 , , PUNCT eurjchem-71 151 11     SPACE eurjchem-71 151 12 22 22 NUM eurjchem-71 151 13 , , PUNCT eurjchem-71 151 14     SPACE eurjchem-71 151 15 2473‐ 2473‐ NUM eurjchem-71 151 16 2476 2476 NUM eurjchem-71 151 17 . . PUNCT eurjchem-71 151 18     SPACE eurjchem-71 152 1 [ [ X eurjchem-71 152 2 9 9 NUM eurjchem-71 152 3 ] ] PUNCT eurjchem-71 152 4 . . PUNCT eurjchem-71 152 5 rama rama PROPN eurjchem-71 152 6 , , PUNCT eurjchem-71 152 7     SPACE eurjchem-71 152 8 n. n. PROPN eurjchem-71 152 9     SPACE eurjchem-71 152 10 h. h. PROPN eurjchem-71 152 11 ; ; PUNCT eurjchem-71 152 12     SPACE eurjchem-71 152 13 iqbal iqbal PROPN eurjchem-71 152 14 , , PUNCT eurjchem-71 152 15     SPACE eurjchem-71 152 16 r. r. PROPN eurjchem-71 152 17 ; ; PUNCT eurjchem-71 152 18     SPACE eurjchem-71 152 19 zamani zamani PROPN eurjchem-71 152 20 , , PUNCT eurjchem-71 152 21     SPACE eurjchem-71 152 22 k. k. PROPN eurjchem-71 152 23     SPACE eurjchem-71 152 24 j. j. PROPN eurjchem-71 152 25     SPACE eurjchem-71 152 26 chem chem NOUN eurjchem-71 152 27 . . PUNCT eurjchem-71 152 28     SPACE eurjchem-71 152 29 soc soc PROPN eurjchem-71 152 30 . . PUNCT eurjchem-71 152 31     SPACE eurjchem-71 152 32 pak pak PROPN eurjchem-71 152 33 . . PUNCT eurjchem-71 152 34     SPACE eurjchem-71 152 35 1998 1998 NUM eurjchem-71 152 36 , , PUNCT eurjchem-71 152 37     SPACE eurjchem-71 152 38 20 20 NUM eurjchem-71 152 39 , , PUNCT eurjchem-71 152 40     SPACE eurjchem-71 152 41 62‐65 62‐65 NUM eurjchem-71 152 42 . . PUNCT eurjchem-71 152 43     SPACE eurjchem-71 153 1 [ [ X eurjchem-71 153 2 10 10 NUM eurjchem-71 153 3 ] ] PUNCT eurjchem-71 153 4 . . PUNCT eurjchem-71 154 1 stephen stephen PROPN eurjchem-71 154 2     SPACE eurjchem-71 154 3 w. w. PROPN eurjchem-71 154 4     SPACE eurjchem-71 154 5 p. p. PROPN eurjchem-71 154 6 ; ; PUNCT eurjchem-71 154 7     SPACE eurjchem-71 154 8 koslowski koslowski NOUN eurjchem-71 154 9 , , PUNCT eurjchem-71 154 10     SPACE eurjchem-71 154 11 m. m. NOUN eurjchem-71 154 12     SPACE eurjchem-71 154 13 c. c. PROPN eurjchem-71 154 14     SPACE eurjchem-71 154 15 tetrahedron tetrahedron NOUN eurjchem-71 154 16     SPACE eurjchem-71 154 17 lett lett NOUN eurjchem-71 154 18 . . PUNCT eurjchem-71 154 19     SPACE eurjchem-71 155 1 2001 2001 NUM eurjchem-71 155 2 , , PUNCT eurjchem-71 155 3     SPACE eurjchem-71 155 4 42 42 NUM eurjchem-71 155 5 , , PUNCT eurjchem-71 155 6     SPACE eurjchem-71 155 7 3567‐ 3567‐ NUM eurjchem-71 155 8 3570 3570 NUM eurjchem-71 155 9 . . PUNCT eurjchem-71 155 10     SPACE eurjchem-71 156 1 [ [ X eurjchem-71 156 2 11 11 NUM eurjchem-71 156 3 ] ] PUNCT eurjchem-71 156 4 . . PUNCT eurjchem-71 157 1 hajipour hajipour PROPN eurjchem-71 157 2 , , PUNCT eurjchem-71 157 3     SPACE eurjchem-71 157 4 a. a. NOUN eurjchem-71 157 5     SPACE eurjchem-71 157 6 ; ; PUNCT eurjchem-71 157 7     SPACE eurjchem-71 157 8 mallakpour mallakpour NOUN eurjchem-71 157 9 , , PUNCT eurjchem-71 157 10     SPACE eurjchem-71 157 11 s. s. PROPN eurjchem-71 157 12     SPACE eurjchem-71 157 13 ; ; PUNCT eurjchem-71 157 14     SPACE eurjchem-71 157 15 imanzadeh imanzadeh PROPN eurjchem-71 157 16 , , PUNCT eurjchem-71 157 17     SPACE eurjchem-71 157 18 g. g. PROPN eurjchem-71 157 19     SPACE eurjchem-71 157 20 indian indian PROPN eurjchem-71 157 21     SPACE eurjchem-71 157 22 j. j. PROPN eurjchem-71 157 23     SPACE eurjchem-71 157 24 chem chem NOUN eurjchem-71 157 25 . . PUNCT eurjchem-71 157 26     SPACE eurjchem-71 158 1 2001 2001 NUM eurjchem-71 158 2 , , PUNCT eurjchem-71 158 3     SPACE eurjchem-71 158 4 40b 40b NOUN eurjchem-71 158 5 , , PUNCT eurjchem-71 158 6     SPACE eurjchem-71 158 7 250‐251 250‐251 NUM eurjchem-71 158 8 . . PUNCT eurjchem-71 158 9     SPACE eurjchem-71 159 1 [ [ X eurjchem-71 159 2 12 12 NUM eurjchem-71 159 3 ] ] PUNCT eurjchem-71 159 4 . . PUNCT eurjchem-71 160 1 karina karina PROPN eurjchem-71 160 2 , , PUNCT eurjchem-71 160 3     SPACE eurjchem-71 160 4 f. f. PROPN eurjchem-71 160 5 ; ; PUNCT eurjchem-71 160 6     SPACE eurjchem-71 160 7 devienna devienna NOUN eurjchem-71 160 8 , , PUNCT eurjchem-71 160 9     SPACE eurjchem-71 160 10 m. m. NOUN eurjchem-71 160 11 ; ; PUNCT eurjchem-71 160 12     SPACE eurjchem-71 160 13 sela sela PROPN eurjchem-71 160 14     SPACE eurjchem-71 160 15 raddi raddi PROPN eurjchem-71 160 16 , , PUNCT eurjchem-71 160 17     SPACE eurjchem-71 160 18 g. g. NOUN eurjchem-71 160 19 ; ; PUNCT eurjchem-71 160 20     SPACE eurjchem-71 160 21 eliana eliana PROPN eurjchem-71 160 22 , , PUNCT eurjchem-71 160 23     SPACE eurjchem-71 160 24 a. a. NOUN eurjchem-71 160 25 ; ; PUNCT eurjchem-71 160 26     SPACE eurjchem-71 160 27 varand varand NOUN eurjchem-71 160 28 , , PUNCT eurjchem-71 160 29     SPACE eurjchem-71 160 30 z. z. PROPN eurjchem-71 160 31     SPACE eurjchem-71 160 32 z. z. PROPN eurjchem-71 160 33     SPACE eurjchem-71 160 34 naturforsch naturforsch PROPN eurjchem-71 160 35     SPACE eurjchem-71 160 36 2002 2002 NUM eurjchem-71 160 37 , , PUNCT eurjchem-71 160 38     SPACE eurjchem-71 160 39 57 57 NUM eurjchem-71 160 40 , , PUNCT eurjchem-71 160 41     SPACE eurjchem-71 160 42 85‐88 85‐88 NOUN eurjchem-71 160 43 . . PUNCT eurjchem-71 160 44     SPACE eurjchem-71 161 1 [ [ X eurjchem-71 161 2 13 13 NUM eurjchem-71 161 3 ] ] PUNCT eurjchem-71 161 4 . . PUNCT eurjchem-71 162 1 gitto gitto PROPN eurjchem-71 162 2 , , PUNCT eurjchem-71 162 3     SPACE eurjchem-71 162 4 r. r. PROPN eurjchem-71 162 5 ; ; PUNCT eurjchem-71 162 6     SPACE eurjchem-71 162 7 barreca barreca NOUN eurjchem-71 162 8 , , PUNCT eurjchem-71 162 9     SPACE eurjchem-71 162 10 m. m. NOUN eurjchem-71 162 11 ; ; PUNCT eurjchem-71 162 12     SPACE eurjchem-71 162 13 francica francica NOUN eurjchem-71 162 14 , , PUNCT eurjchem-71 162 15     SPACE eurjchem-71 162 16 e. e. PROPN eurjchem-71 162 17 ; ; PUNCT eurjchem-71 162 18     SPACE eurjchem-71 162 19 caruse caruse NOUN eurjchem-71 162 20 , , PUNCT eurjchem-71 162 21     SPACE eurjchem-71 162 22 r. r. PROPN eurjchem-71 162 23 ; ; PUNCT eurjchem-71 162 24     SPACE eurjchem-71 162 25 deluea deluea NOUN eurjchem-71 162 26 , , PUNCT eurjchem-71 162 27     SPACE eurjchem-71 162 28 l. l. PROPN eurjchem-71 162 29 ; ; PUNCT eurjchem-71 162 30     SPACE eurjchem-71 162 31 russo russo NOUN eurjchem-71 162 32 , , PUNCT eurjchem-71 162 33     SPACE eurjchem-71 162 34 e. e. PROPN eurjchem-71 162 35 ; ; PUNCT eurjchem-71 162 36     SPACE eurjchem-71 162 37 desarro desarro PROPN eurjchem-71 162 38 , , PUNCT eurjchem-71 162 39     SPACE eurjchem-71 162 40 g. g. NOUN eurjchem-71 162 41 ; ; PUNCT eurjchem-71 162 42     SPACE eurjchem-71 162 43 chimirri chimirri PROPN eurjchem-71 162 44 , , PUNCT eurjchem-71 162 45     SPACE eurjchem-71 162 46 a. a. NOUN eurjchem-71 162 47     SPACE eurjchem-71 162 48 arkivoc arkivoc NOUN eurjchem-71 162 49     SPACE eurjchem-71 162 50 2004 2004 NUM eurjchem-71 162 51 , , PUNCT eurjchem-71 162 52     SPACE eurjchem-71 162 53 5 5 NUM eurjchem-71 162 54 , , PUNCT eurjchem-71 162 55     SPACE eurjchem-71 162 56 170‐180 170‐180 NUM eurjchem-71 162 57 . . PUNCT eurjchem-71 162 58     SPACE eurjchem-71 163 1 [ [ X eurjchem-71 163 2 14 14 NUM eurjchem-71 163 3 ] ] PUNCT eurjchem-71 163 4 . . PUNCT eurjchem-71 164 1 azizian azizian PROPN eurjchem-71 164 2 , , PUNCT eurjchem-71 164 3     SPACE eurjchem-71 164 4 j. j. PROPN eurjchem-71 164 5 ; ; PUNCT eurjchem-71 164 6     SPACE eurjchem-71 164 7 mohammadi mohammadi NOUN eurjchem-71 164 8 , , PUNCT eurjchem-71 164 9     SPACE eurjchem-71 164 10 a. a. NOUN eurjchem-71 164 11     SPACE eurjchem-71 164 12 a. a. NOUN eurjchem-71 164 13 ; ; PUNCT eurjchem-71 164 14     SPACE eurjchem-71 164 15 karami karami NOUN eurjchem-71 164 16 , , PUNCT eurjchem-71 164 17     SPACE eurjchem-71 164 18 a. a. NOUN eurjchem-71 164 19     SPACE eurjchem-71 164 20 r. r. PROPN eurjchem-71 164 21 ; ; PUNCT eurjchem-71 164 22     SPACE eurjchem-71 164 23 mohammadizadeh mohammadizadeh ADJ eurjchem-71 164 24 , , PUNCT eurjchem-71 164 25     SPACE eurjchem-71 164 26 m. m. NOUN eurjchem-71 164 27     SPACE eurjchem-71 164 28 r. r. PROPN eurjchem-71 164 29     SPACE eurjchem-71 164 30 a. a. PROPN eurjchem-71 164 31     SPACE eurjchem-71 164 32 j. j. PROPN eurjchem-71 164 33     SPACE eurjchem-71 164 34 org org PROPN eurjchem-71 164 35 . . PUNCT eurjchem-71 164 36     SPACE eurjchem-71 164 37 chem chem NOUN eurjchem-71 164 38 . . PUNCT eurjchem-71 164 39     SPACE eurjchem-71 164 40 2005 2005 NUM eurjchem-71 164 41 , , PUNCT eurjchem-71 164 42     SPACE eurjchem-71 164 43 70 70 NUM eurjchem-71 164 44 , , PUNCT eurjchem-71 164 45     SPACE eurjchem-71 164 46 350‐352 350‐352 NUM eurjchem-71 164 47 . . PUNCT eurjchem-71 164 48     SPACE eurjchem-71 165 1 [ [ X eurjchem-71 165 2 15 15 NUM eurjchem-71 165 3 ] ] PUNCT eurjchem-71 165 4 . . PUNCT eurjchem-71 166 1 kandinska kandinska PROPN eurjchem-71 166 2 , , PUNCT eurjchem-71 166 3     SPACE eurjchem-71 166 4 m. m. NOUN eurjchem-71 166 5     SPACE eurjchem-71 166 6 i. i. NOUN eurjchem-71 166 7 ; ; PUNCT eurjchem-71 166 8     SPACE eurjchem-71 166 9 kozekov kozekov NOUN eurjchem-71 166 10 , , PUNCT eurjchem-71 166 11     SPACE eurjchem-71 166 12 i. i. PROPN eurjchem-71 166 13     SPACE eurjchem-71 166 14 d. d. PROPN eurjchem-71 166 15 ; ; PUNCT eurjchem-71 166 16     SPACE eurjchem-71 166 17 palamareva palamareva VERB eurjchem-71 166 18 , , PUNCT eurjchem-71 166 19     SPACE eurjchem-71 166 20 m. m. NOUN eurjchem-71 166 21     SPACE eurjchem-71 166 22 d. d. PROPN eurjchem-71 166 23     SPACE eurjchem-71 166 24 molecules molecule NOUN eurjchem-71 166 25     SPACE eurjchem-71 166 26 2006 2006 NUM eurjchem-71 166 27 , , PUNCT eurjchem-71 166 28     SPACE eurjchem-71 166 29 11 11 NUM eurjchem-71 166 30 , , PUNCT eurjchem-71 166 31     SPACE eurjchem-71 166 32 403‐414 403‐414 PROPN eurjchem-71 166 33 . . PUNCT eurjchem-71 166 34     SPACE eurjchem-71 167 1 [ [ X eurjchem-71 167 2 16 16 NUM eurjchem-71 167 3 ] ] PUNCT eurjchem-71 167 4 . . PUNCT eurjchem-71 168 1 kane kane PROPN eurjchem-71 168 2 , , PUNCT eurjchem-71 168 3     SPACE eurjchem-71 168 4 t. t. PROPN eurjchem-71 168 5     SPACE eurjchem-71 168 6 r. r. PROPN eurjchem-71 168 7 ; ; PUNCT eurjchem-71 168 8     SPACE eurjchem-71 168 9 ly ly NOUN eurjchem-71 168 10 , , PUNCT eurjchem-71 168 11     SPACE eurjchem-71 168 12 c. c. PROPN eurjchem-71 168 13     SPACE eurjchem-71 168 14 q. q. PROPN eurjchem-71 168 15 ; ; PUNCT eurjchem-71 168 16     SPACE eurjchem-71 168 17 kelly kelly PROPN eurjchem-71 168 18 , , PUNCT eurjchem-71 168 19     SPACE eurjchem-71 168 20 d.e d.e PROPN eurjchem-71 168 21 . . PROPN eurjchem-71 168 22 ; ; PUNCT eurjchem-71 168 23     SPACE eurjchem-71 168 24 denner denner NOUN eurjchem-71 168 25 , , PUNCT eurjchem-71 168 26     SPACE eurjchem-71 168 27 j. j. PROPN eurjchem-71 168 28     SPACE eurjchem-71 168 29 m. m. PROPN eurjchem-71 168 30     SPACE eurjchem-71 168 31 j. j. PROPN eurjchem-71 168 32     SPACE eurjchem-71 168 33 comb comb NOUN eurjchem-71 168 34 . . PUNCT eurjchem-71 168 35     SPACE eurjchem-71 168 36 chem chem NOUN eurjchem-71 168 37 . . PUNCT eurjchem-71 168 38     SPACE eurjchem-71 168 39 2004 2004 NUM eurjchem-71 168 40 , , PUNCT eurjchem-71 168 41     SPACE eurjchem-71 168 42 6 6 NUM eurjchem-71 168 43 , , PUNCT eurjchem-71 168 44     SPACE eurjchem-71 168 45 564‐572 564‐572 PROPN eurjchem-71 168 46 . . PUNCT eurjchem-71 168 47     SPACE eurjchem-71 169 1 [ [ X eurjchem-71 169 2 17 17 NUM eurjchem-71 169 3 ] ] PUNCT eurjchem-71 169 4 . . PUNCT eurjchem-71 170 1 kim kim PROPN eurjchem-71 170 2 , , PUNCT eurjchem-71 170 3     SPACE eurjchem-71 170 4 h. h. PROPN eurjchem-71 170 5     SPACE eurjchem-71 170 6 j. j. PROPN eurjchem-71 170 7 ; ; PUNCT eurjchem-71 170 8     SPACE eurjchem-71 170 9 yoon yoon NOUN eurjchem-71 170 10 , , PUNCT eurjchem-71 170 11     SPACE eurjchem-71 170 12 u. u. PROPN eurjchem-71 170 13     SPACE eurjchem-71 170 14 c. c. PROPN eurjchem-71 170 15 ; ; PUNCT eurjchem-71 170 16     SPACE eurjchem-71 170 17 young young ADJ eurjchem-71 170 18 , , PUNCT eurjchem-71 170 19     SPACE eurjchem-71 170 20 s. s. PROPN eurjchem-71 170 21     SPACE eurjchem-71 170 22 y. y. PROPN eurjchem-71 170 23 ; ; PUNCT eurjchem-71 170 24     SPACE eurjchem-71 170 25 park park NOUN eurjchem-71 170 26 , , PUNCT eurjchem-71 170 27     SPACE eurjchem-71 170 28 n. n. PROPN eurjchem-71 170 29     SPACE eurjchem-71 170 30 s. s. PROPN eurjchem-71 170 31 ; ; PUNCT eurjchem-71 170 32     SPACE eurjchem-71 170 33 cedeistrom cedeistrom ADJ eurjchem-71 170 34 , , PUNCT eurjchem-71 170 35     SPACE eurjchem-71 170 36 e.m e.m PROPN eurjchem-71 170 37 . . PROPN eurjchem-71 170 38 ; ; PUNCT eurjchem-71 170 39     SPACE eurjchem-71 170 40 marriano marriano VERB eurjchem-71 170 41 ; ; PUNCT eurjchem-71 170 42     SPACE eurjchem-71 170 43 p. p. NOUN eurjchem-71 170 44     SPACE eurjchem-71 170 45 s. s. PROPN eurjchem-71 170 46     SPACE eurjchem-71 170 47 j. j. PROPN eurjchem-71 170 48     SPACE eurjchem-71 170 49 org org PROPN eurjchem-71 170 50 . . PUNCT eurjchem-71 170 51     SPACE eurjchem-71 170 52 chem chem NOUN eurjchem-71 170 53 . . PUNCT eurjchem-71 170 54     SPACE eurjchem-71 170 55 1998 1998 NUM eurjchem-71 170 56 , , PUNCT eurjchem-71 170 57     SPACE eurjchem-71 170 58 63 63 NUM eurjchem-71 170 59 , , PUNCT eurjchem-71 170 60     SPACE eurjchem-71 170 61 860‐863 860‐863 NUM eurjchem-71 170 62 . . PUNCT eurjchem-71 170 63     SPACE eurjchem-71 171 1 [ [ X eurjchem-71 171 2 18 18 NUM eurjchem-71 171 3 ] ] PUNCT eurjchem-71 171 4 . . PUNCT eurjchem-71 172 1 kozekov kozekov PROPN eurjchem-71 172 2 , , PUNCT eurjchem-71 172 3     SPACE eurjchem-71 172 4 i. i. PROPN eurjchem-71 172 5     SPACE eurjchem-71 172 6 d. d. PROPN eurjchem-71 172 7 ; ; PUNCT eurjchem-71 172 8     SPACE eurjchem-71 172 9 koleva koleva PROPN eurjchem-71 172 10 , , PUNCT eurjchem-71 172 11     SPACE eurjchem-71 172 12 r. r. PROPN eurjchem-71 172 13     SPACE eurjchem-71 172 14 i. i. PROPN eurjchem-71 172 15 ; ; PUNCT eurjchem-71 172 16     SPACE eurjchem-71 172 17 palamareva palamareva VERB eurjchem-71 172 18 , , PUNCT eurjchem-71 172 19     SPACE eurjchem-71 172 20 m. m. NOUN eurjchem-71 172 21     SPACE eurjchem-71 172 22 d. d. PROPN eurjchem-71 172 23     SPACE eurjchem-71 172 24 j. j. PROPN eurjchem-71 172 25     SPACE eurjchem-71 172 26 heterocyclic heterocyclic ADJ eurjchem-71 172 27     SPACE eurjchem-71 172 28 chem chem NOUN eurjchem-71 172 29 . . PUNCT eurjchem-71 172 30     SPACE eurjchem-71 172 31 2002 2002 NUM eurjchem-71 172 32 , , PUNCT eurjchem-71 172 33     SPACE eurjchem-71 172 34 39 39 NUM eurjchem-71 172 35 , , PUNCT eurjchem-71 172 36     SPACE eurjchem-71 172 37 229‐236 229‐236 NUM eurjchem-71 172 38 . . PUNCT eurjchem-71 172 39     SPACE eurjchem-71 173 1 [ [ X eurjchem-71 173 2 19 19 NUM eurjchem-71 173 3 ] ] PUNCT eurjchem-71 173 4 . . PUNCT eurjchem-71 174 1 stoyanova stoyanova PROPN eurjchem-71 174 2 , , PUNCT eurjchem-71 174 3     SPACE eurjchem-71 174 4 m. m. NOUN eurjchem-71 174 5     SPACE eurjchem-71 174 6 p. p. NOUN eurjchem-71 174 7 ; ; PUNCT eurjchem-71 174 8     SPACE eurjchem-71 174 9 kozekov kozekov NOUN eurjchem-71 174 10 , , PUNCT eurjchem-71 174 11     SPACE eurjchem-71 174 12 i. i. PROPN eurjchem-71 174 13     SPACE eurjchem-71 174 14 d. d. PROPN eurjchem-71 174 15 ; ; PUNCT eurjchem-71 174 16     SPACE eurjchem-71 174 17 palamareva palamareva VERB eurjchem-71 174 18 , , PUNCT eurjchem-71 174 19     SPACE eurjchem-71 174 20 m.d m.d PROPN eurjchem-71 174 21 . . PROPN eurjchem-71 174 22     SPACE eurjchem-71 174 23 j. j. PROPN eurjchem-71 174 24     SPACE eurjchem-71 174 25 heterocyclic heterocyclic ADJ eurjchem-71 174 26     SPACE eurjchem-71 174 27 chem chem NOUN eurjchem-71 174 28 . . PUNCT eurjchem-71 174 29     SPACE eurjchem-71 174 30 2003 2003 NUM eurjchem-71 174 31 , , PUNCT eurjchem-71 174 32     SPACE eurjchem-71 174 33 40 40 NUM eurjchem-71 174 34 , , PUNCT eurjchem-71 174 35     SPACE eurjchem-71 174 36 795‐803 795‐803 NOUN eurjchem-71 174 37 . . PUNCT eurjchem-71 174 38     SPACE eurjchem-71 175 1 [ [ X eurjchem-71 175 2 20 20 NUM eurjchem-71 175 3 ] ] PUNCT eurjchem-71 175 4 . . PUNCT eurjchem-71 176 1 yadav yadav PROPN eurjchem-71 176 2 , , PUNCT eurjchem-71 176 3     SPACE eurjchem-71 176 4 j. j. PROPN eurjchem-71 176 5     SPACE eurjchem-71 176 6 s. s. PROPN eurjchem-71 176 7 ; ; PUNCT eurjchem-71 176 8     SPACE eurjchem-71 176 9 reddy reddy NOUN eurjchem-71 176 10 , , PUNCT eurjchem-71 176 11     SPACE eurjchem-71 176 12 b. b. PROPN eurjchem-71 176 13     SPACE eurjchem-71 176 14 v. v. PROPN eurjchem-71 176 15     SPACE eurjchem-71 176 16 s. s. PROPN eurjchem-71 176 17 ; ; PUNCT eurjchem-71 176 18     SPACE eurjchem-71 176 19 saritha saritha PROPN eurjchem-71 176 20     SPACE eurjchem-71 176 21 raj raj PROPN eurjchem-71 176 22 , , PUNCT eurjchem-71 176 23     SPACE eurjchem-71 176 24 k. k. PROPN eurjchem-71 176 25 ; ; PUNCT eurjchem-71 176 26     SPACE eurjchem-71 176 27 prasad prasad NOUN eurjchem-71 176 28 , , PUNCT eurjchem-71 176 29     SPACE eurjchem-71 176 30 a. a. NOUN eurjchem-71 176 31     SPACE eurjchem-71 176 32 r. r. PROPN eurjchem-71 176 33     SPACE eurjchem-71 176 34 tetrahedron tetrahedron NOUN eurjchem-71 176 35     SPACE eurjchem-71 176 36 2003 2003 NUM eurjchem-71 176 37 , , PUNCT eurjchem-71 176 38     SPACE eurjchem-71 176 39 59 59 NUM eurjchem-71 176 40 , , PUNCT eurjchem-71 176 41     SPACE eurjchem-71 176 42 1805‐1809 1805‐1809 NUM eurjchem-71 176 43 . . PUNCT eurjchem-71 176 44     SPACE eurjchem-71 177 1 [ [ X eurjchem-71 177 2 21 21 NUM eurjchem-71 177 3 ] ] PUNCT eurjchem-71 177 4 . . PUNCT eurjchem-71 177 5 zalan zalan PROPN eurjchem-71 177 6 , , PUNCT eurjchem-71 177 7     SPACE eurjchem-71 177 8 z. z. PROPN eurjchem-71 177 9 ; ; PUNCT eurjchem-71 177 10     SPACE eurjchem-71 177 11 martinek martinek ADJ eurjchem-71 177 12 , , PUNCT eurjchem-71 177 13     SPACE eurjchem-71 177 14 t. t. NOUN eurjchem-71 177 15     SPACE eurjchem-71 177 16 a. a. NOUN eurjchem-71 177 17 ; ; PUNCT eurjchem-71 177 18     SPACE eurjchem-71 177 19 lazar lazar PROPN eurjchem-71 177 20 , , PUNCT eurjchem-71 177 21     SPACE eurjchem-71 177 22 l. l. PROPN eurjchem-71 177 23 ; ; PUNCT eurjchem-71 177 24     SPACE eurjchem-71 177 25 fulop fulop NOUN eurjchem-71 177 26 , , PUNCT eurjchem-71 177 27     SPACE eurjchem-71 177 28 f. f. PROPN eurjchem-71 177 29     SPACE eurjchem-71 177 30 tetrahedron tetrahedron NOUN eurjchem-71 177 31     SPACE eurjchem-71 177 32 2003 2003 NUM eurjchem-71 177 33 , , PUNCT eurjchem-71 177 34     SPACE eurjchem-71 177 35 59 59 NUM eurjchem-71 177 36 , , PUNCT eurjchem-71 177 37     SPACE eurjchem-71 177 38 9117‐9125 9117‐9125 NUM eurjchem-71 177 39 . . PUNCT eurjchem-71 177 40     SPACE eurjchem-71 178 1 [ [ X eurjchem-71 178 2 22 22 NUM eurjchem-71 178 3 ] ] PUNCT eurjchem-71 178 4 . . PUNCT eurjchem-71 179 1 coelho coelho PROPN eurjchem-71 179 2 , , PUNCT eurjchem-71 179 3     SPACE eurjchem-71 179 4 f. f. PROPN eurjchem-71 179 5 ; ; PUNCT eurjchem-71 179 6     SPACE eurjchem-71 179 7 veronese veronese NOUN eurjchem-71 179 8 , , PUNCT eurjchem-71 179 9     SPACE eurjchem-71 179 10 d. d. PROPN eurjchem-71 179 11 ; ; PUNCT eurjchem-71 179 12     SPACE eurjchem-71 179 13 lopes lope NOUN eurjchem-71 179 14 , , PUNCT eurjchem-71 179 15     SPACE eurjchem-71 179 16 e. e. PROPN eurjchem-71 179 17     SPACE eurjchem-71 179 18 c. c. PROPN eurjchem-71 179 19     SPACE eurjchem-71 179 20 s. s. PROPN eurjchem-71 179 21 ; ; PUNCT eurjchem-71 179 22     SPACE eurjchem-71 179 23 rossi rossi ADJ eurjchem-71 179 24 , , PUNCT eurjchem-71 179 25     SPACE eurjchem-71 179 26 r. r. PROPN eurjchem-71 179 27     SPACE eurjchem-71 179 28 c. c. PROPN eurjchem-71 179 29     SPACE eurjchem-71 179 30 tetrahedron tetrahedron NOUN eurjchem-71 179 31     SPACE eurjchem-71 179 32 lett lett PROPN eurjchem-71 179 33 . . PUNCT eurjchem-71 179 34     SPACE eurjchem-71 179 35 2003 2003 NUM eurjchem-71 179 36 , , PUNCT eurjchem-71 179 37     SPACE eurjchem-71 179 38 44 44 NUM eurjchem-71 179 39 , , PUNCT eurjchem-71 179 40     SPACE eurjchem-71 179 41 5731‐5735 5731‐5735 NUM eurjchem-71 179 42 . . PUNCT eurjchem-71 179 43     SPACE eurjchem-71 180 1 [ [ X eurjchem-71 180 2 23 23 NUM eurjchem-71 180 3 ] ] PUNCT eurjchem-71 180 4 . . PUNCT eurjchem-71 181 1 shaabani shaabani PROPN eurjchem-71 181 2 , , PUNCT eurjchem-71 181 3     SPACE eurjchem-71 181 4 a. a. NOUN eurjchem-71 181 5 ; ; PUNCT eurjchem-71 181 6     SPACE eurjchem-71 181 7 soleimani soleimani PROPN eurjchem-71 181 8 , , PUNCT eurjchem-71 181 9     SPACE eurjchem-71 181 10 e. e. PROPN eurjchem-71 181 11 ; ; PUNCT eurjchem-71 181 12     SPACE eurjchem-71 181 13 khavasi khavasi PROPN eurjchem-71 181 14 , , PUNCT eurjchem-71 181 15     SPACE eurjchem-71 181 16 h. h. PROPN eurjchem-71 181 17     SPACE eurjchem-71 181 18 r. r. PROPN eurjchem-71 181 19     SPACE eurjchem-71 181 20 tetrahedron tetrahedron PROPN eurjchem-71 181 21     SPACE eurjchem-71 181 22 lett lett PROPN eurjchem-71 181 23 . . PUNCT eurjchem-71 181 24     SPACE eurjchem-71 181 25 2007 2007 NUM eurjchem-71 181 26 , , PUNCT eurjchem-71 181 27     SPACE eurjchem-71 181 28 48 48 NUM eurjchem-71 181 29 , , PUNCT eurjchem-71 181 30     SPACE eurjchem-71 181 31 4743‐4747 4743‐4747 NUM eurjchem-71 181 32 . . PUNCT eurjchem-71 181 33     SPACE eurjchem-71 182 1 [ [ X eurjchem-71 182 2 24 24 NUM eurjchem-71 182 3 ] ] PUNCT eurjchem-71 182 4 . . PUNCT eurjchem-71 183 1 knolker knolker PROPN eurjchem-71 183 2 , , PUNCT eurjchem-71 183 3     SPACE eurjchem-71 183 4 h. h. PROPN eurjchem-71 183 5     SPACE eurjchem-71 183 6 j. j. PROPN eurjchem-71 183 7 ; ; PUNCT eurjchem-71 183 8     SPACE eurjchem-71 183 9 agarwal agarwal PROPN eurjchem-71 183 10 , , PUNCT eurjchem-71 183 11     SPACE eurjchem-71 183 12 s. s. PROPN eurjchem-71 183 13     SPACE eurjchem-71 183 14 tetrahedron tetrahedron NOUN eurjchem-71 183 15     SPACE eurjchem-71 183 16 lett lett PROPN eurjchem-71 183 17 . . PUNCT eurjchem-71 183 18     SPACE eurjchem-71 183 19 2005 2005 NUM eurjchem-71 183 20 , , PUNCT eurjchem-71 183 21     SPACE eurjchem-71 183 22 46 46 NUM eurjchem-71 183 23 , , PUNCT eurjchem-71 183 24     SPACE eurjchem-71 183 25 1173‐1175 1173‐1175 NUM eurjchem-71 183 26 . . PUNCT eurjchem-71 183 27     SPACE eurjchem-71 184 1 [ [ X eurjchem-71 184 2 25 25 NUM eurjchem-71 184 3 ] ] PUNCT eurjchem-71 184 4 . . PUNCT eurjchem-71 184 5 scott scott PROPN eurjchem-71 184 6 , , PUNCT eurjchem-71 184 7     SPACE eurjchem-71 184 8 j. j. PROPN eurjchem-71 184 9     SPACE eurjchem-71 184 10 d. d. PROPN eurjchem-71 184 11 ; ; PUNCT eurjchem-71 184 12     SPACE eurjchem-71 184 13 williams williams PROPN eurjchem-71 184 14 , , PUNCT eurjchem-71 184 15     SPACE eurjchem-71 184 16 r. r. PROPN eurjchem-71 184 17     SPACE eurjchem-71 184 18 m. m. NOUN eurjchem-71 184 19     SPACE eurjchem-71 184 20 chem chem NOUN eurjchem-71 184 21 . . PUNCT eurjchem-71 184 22     SPACE eurjchem-71 184 23 rev rev VERB eurjchem-71 184 24 . . PUNCT eurjchem-71 184 25     SPACE eurjchem-71 184 26 2002 2002 NUM eurjchem-71 184 27 , , PUNCT eurjchem-71 184 28     SPACE eurjchem-71 184 29 102 102 NUM eurjchem-71 184 30 , , PUNCT eurjchem-71 184 31     SPACE eurjchem-71 184 32 1669‐1730 1669‐1730 NUM eurjchem-71 184 33 . . PUNCT eurjchem-71 184 34     SPACE eurjchem-71 185 1 [ [ X eurjchem-71 185 2 26 26 NUM eurjchem-71 185 3 ] ] PUNCT eurjchem-71 185 4 . . PUNCT eurjchem-71 186 1 mahmoud mahmoud PROPN eurjchem-71 186 2 , , PUNCT eurjchem-71 186 3     SPACE eurjchem-71 186 4 m. m. NOUN eurjchem-71 186 5     SPACE eurjchem-71 186 6 r. r. PROPN eurjchem-71 186 7 ; ; PUNCT eurjchem-71 186 8     SPACE eurjchem-71 186 9 el‐shahawi el‐shahawi PROPN eurjchem-71 186 10 , , PUNCT eurjchem-71 186 11     SPACE eurjchem-71 186 12 m. m. NOUN eurjchem-71 186 13     SPACE eurjchem-71 186 14 m. m. NOUN eurjchem-71 186 15 ; ; PUNCT eurjchem-71 186 16     SPACE eurjchem-71 186 17 farahat farahat NOUN eurjchem-71 186 18 , , PUNCT eurjchem-71 186 19     SPACE eurjchem-71 186 20 s. s. PROPN eurjchem-71 186 21     SPACE eurjchem-71 186 22 e. e. PROPN eurjchem-71 186 23     SPACE eurjchem-71 186 24 j. j. PROPN eurjchem-71 186 25     SPACE eurjchem-71 186 26 chem chem NOUN eurjchem-71 186 27 . . PUNCT eurjchem-71 186 28     SPACE eurjchem-71 186 29 res re NOUN eurjchem-71 186 30 . . PUNCT eurjchem-71 186 31     SPACE eurjchem-71 186 32 2008 2008 NUM eurjchem-71 186 33 , , PUNCT eurjchem-71 186 34     SPACE eurjchem-71 186 35 2 2 NUM eurjchem-71 186 36 , , PUNCT eurjchem-71 186 37     SPACE eurjchem-71 186 38 86‐88 86‐88 NUM eurjchem-71 186 39 . . PUNCT eurjchem-71 186 40     SPACE eurjchem-71 187 1 [ [ X eurjchem-71 187 2 27 27 NUM eurjchem-71 187 3 ] ] PUNCT eurjchem-71 187 4 . . PUNCT eurjchem-71 188 1 mahmoud mahmoud PROPN eurjchem-71 188 2 , , PUNCT eurjchem-71 188 3     SPACE eurjchem-71 188 4 m. m. NOUN eurjchem-71 188 5     SPACE eurjchem-71 188 6 r. r. PROPN eurjchem-71 188 7 ; ; PUNCT eurjchem-71 188 8     SPACE eurjchem-71 188 9 el‐shahawi el‐shahawi PROPN eurjchem-71 188 10 , , PUNCT eurjchem-71 188 11     SPACE eurjchem-71 188 12 m. m. NOUN eurjchem-71 188 13     SPACE eurjchem-71 188 14 m. m. NOUN eurjchem-71 188 15 ; ; PUNCT eurjchem-71 188 16     SPACE eurjchem-71 188 17 farahat farahat NOUN eurjchem-71 188 18 , , PUNCT eurjchem-71 188 19     SPACE eurjchem-71 188 20 s. s. PROPN eurjchem-71 188 21     SPACE eurjchem-71 188 22 e. e. PROPN eurjchem-71 188 23     SPACE eurjchem-71 188 24 j. j. PROPN eurjchem-71 188 25     SPACE eurjchem-71 188 26 chem chem NOUN eurjchem-71 188 27 . . PUNCT eurjchem-71 188 28     SPACE eurjchem-71 188 29 res re NOUN eurjchem-71 188 30 . . PUNCT eurjchem-71 188 31     SPACE eurjchem-71 188 32 2008 2008 NUM eurjchem-71 188 33 , , PUNCT eurjchem-71 188 34     SPACE eurjchem-71 188 35 1 1 NUM eurjchem-71 188 36 , , PUNCT eurjchem-71 188 37     SPACE eurjchem-71 188 38 59‐60 59‐60 PROPN eurjchem-71 188 39 . . PUNCT eurjchem-71 188 40     SPACE eurjchem-71 189 1 [ [ X eurjchem-71 189 2 28 28 NUM eurjchem-71 189 3 ] ] PUNCT eurjchem-71 189 4 . . PUNCT eurjchem-71 190 1 mahmoud mahmoud PROPN eurjchem-71 190 2 , , PUNCT eurjchem-71 190 3     SPACE eurjchem-71 190 4 m. m. NOUN eurjchem-71 190 5     SPACE eurjchem-71 190 6 r. r. PROPN eurjchem-71 190 7 ; ; PUNCT eurjchem-71 190 8     SPACE eurjchem-71 190 9 el‐shahawi el‐shahawi PROPN eurjchem-71 190 10 , , PUNCT eurjchem-71 190 11     SPACE eurjchem-71 190 12 m. m. NOUN eurjchem-71 190 13     SPACE eurjchem-71 190 14 m. m. NOUN eurjchem-71 190 15 ; ; PUNCT eurjchem-71 190 16     SPACE eurjchem-71 190 17 el‐bordany el‐bordany PROPN eurjchem-71 190 18 , , PUNCT eurjchem-71 190 19     SPACE eurjchem-71 190 20 e. e. PROPN eurjchem-71 190 21     SPACE eurjchem-71 190 22 a. a. PROPN eurjchem-71 190 23     SPACE eurjchem-71 190 24 a. a. NOUN eurjchem-71 190 25 ; ; PUNCT eurjchem-71 190 26     SPACE eurjchem-71 190 27 abu abu NOUN eurjchem-71 190 28     SPACE eurjchem-71 190 29 el‐azm el‐azm NOUN eurjchem-71 190 30 , , PUNCT eurjchem-71 190 31     SPACE eurjchem-71 190 32 f.s f.s NOUN eurjchem-71 190 33     SPACE eurjchem-71 190 34 . . PUNCT eurjchem-71 190 35     SPACE eurjchem-71 191 1 m. m. NOUN eurjchem-71 191 2     SPACE eurjchem-71 191 3 synth synth NOUN eurjchem-71 191 4 . . PUNCT eurjchem-71 191 5     SPACE eurjchem-71 192 1 commun commun PROPN eurjchem-71 192 2 . . PUNCT eurjchem-71 192 3     SPACE eurjchem-71 192 4 2010 2010 NUM eurjchem-71 192 5 , , PUNCT eurjchem-71 192 6     SPACE eurjchem-71 192 7 40 40 NUM eurjchem-71 192 8 , , PUNCT eurjchem-71 192 9     SPACE eurjchem-71 192 10 666‐676 666‐676 NUM eurjchem-71 192 11 . . PUNCT eurjchem-71 192 12       SPACE eurjchem-71 193 1 [ [ X eurjchem-71 193 2 29 29 NUM eurjchem-71 193 3 ] ] PUNCT eurjchem-71 193 4 . . PUNCT eurjchem-71 194 1 morgenstern morgenstern ADJ eurjchem-71 194 2 , , PUNCT eurjchem-71 194 3     SPACE eurjchem-71 194 4 a. a. NOUN eurjchem-71 194 5     SPACE eurjchem-71 194 6 p. p. NOUN eurjchem-71 194 7 ; ; PUNCT eurjchem-71 194 8     SPACE eurjchem-71 194 9 schuitj schuitj VERB eurjchem-71 194 10 , , PUNCT eurjchem-71 194 11     SPACE eurjchem-71 194 12 c. c. NOUN eurjchem-71 194 13 ; ; PUNCT eurjchem-71 194 14     SPACE eurjchem-71 194 15 nauta nauta ADJ eurjchem-71 194 16 , , PUNCT eurjchem-71 194 17     SPACE eurjchem-71 194 18 w. w. PROPN eurjchem-71 194 19     SPACE eurjchem-71 194 20 t. t. PROPN eurjchem-71 194 21     SPACE eurjchem-71 194 22 j. j. PROPN eurjchem-71 194 23     SPACE eurjchem-71 194 24 chem chem NOUN eurjchem-71 194 25 . . PUNCT eurjchem-71 194 26     SPACE eurjchem-71 194 27 soc soc NOUN eurjchem-71 194 28 . . PUNCT eurjchem-71 194 29     SPACE eurjchem-71 194 30 chem chem NOUN eurjchem-71 194 31 . . PUNCT eurjchem-71 194 32     SPACE eurjchem-71 194 33 commun commun PROPN eurjchem-71 194 34 . . PUNCT eurjchem-71 194 35     SPACE eurjchem-71 194 36 1969 1969 NUM eurjchem-71 194 37 , , PUNCT eurjchem-71 194 38     SPACE eurjchem-71 194 39 7 7 NUM eurjchem-71 194 40 , , PUNCT eurjchem-71 194 41     SPACE eurjchem-71 194 42 321‐322 321‐322 PROPN eurjchem-71 194 43 . . PUNCT eurjchem-71 194 44     SPACE eurjchem-71 195 1 [ [ X eurjchem-71 195 2 30 30 NUM eurjchem-71 195 3 ] ] PUNCT eurjchem-71 195 4 . . PUNCT eurjchem-71 196 1 morgenstern morgenstern ADJ eurjchem-71 196 2 , , PUNCT eurjchem-71 196 3     SPACE eurjchem-71 196 4 a. a. NOUN eurjchem-71 196 5     SPACE eurjchem-71 196 6 p. p. NOUN eurjchem-71 196 7 ; ; PUNCT eurjchem-71 196 8     SPACE eurjchem-71 196 9 schuitj schuitj VERB eurjchem-71 196 10 , , PUNCT eurjchem-71 196 11     SPACE eurjchem-71 196 12 c. c. NOUN eurjchem-71 196 13 ; ; PUNCT eurjchem-71 196 14     SPACE eurjchem-71 196 15 nauta nauta ADJ eurjchem-71 196 16 , , PUNCT eurjchem-71 196 17     SPACE eurjchem-71 196 18 w. w. PROPN eurjchem-71 196 19     SPACE eurjchem-71 196 20 t. t. PROPN eurjchem-71 196 21     SPACE eurjchem-71 196 22 j. j. PROPN eurjchem-71 196 23     SPACE eurjchem-71 196 24 chem chem NOUN eurjchem-71 196 25 . . PUNCT eurjchem-71 196 26     SPACE eurjchem-71 196 27 soc soc PROPN eurjchem-71 196 28 . . PUNCT eurjchem-71 196 29     SPACE eurjchem-71 196 30 1971 1971 NUM eurjchem-71 196 31 , , PUNCT eurjchem-71 196 32     SPACE eurjchem-71 196 33 3706‐ 3706‐ NUM eurjchem-71 196 34 3712 3712 NUM eurjchem-71 196 35 . . PUNCT eurjchem-71 196 36     SPACE eurjchem-71 197 1 [ [ X eurjchem-71 197 2 31 31 NUM eurjchem-71 197 3 ] ] PUNCT eurjchem-71 197 4 . . PUNCT eurjchem-71 197 5 boyed boye VERB eurjchem-71 197 6 , , PUNCT eurjchem-71 197 7     SPACE eurjchem-71 197 8 g. g. NOUN eurjchem-71 197 9     SPACE eurjchem-71 197 10 v. v. PROPN eurjchem-71 197 11 ; ; PUNCT eurjchem-71 197 12     SPACE eurjchem-71 197 13 monteil monteil PROPN eurjchem-71 197 14 , , PUNCT eurjchem-71 197 15     SPACE eurjchem-71 197 16 r. r. PROPN eurjchem-71 197 17     SPACE eurjchem-71 197 18 l. l. PROPN eurjchem-71 197 19     SPACE eurjchem-71 197 20 j. j. PROPN eurjchem-71 197 21     SPACE eurjchem-71 197 22 chem chem NOUN eurjchem-71 197 23 . . PUNCT eurjchem-71 197 24     SPACE eurjchem-71 197 25 soc soc PROPN eurjchem-71 197 26 . . PUNCT eurjchem-71 197 27     SPACE eurjchem-71 197 28 perkin perkin PROPN eurjchem-71 197 29     SPACE eurjchem-71 197 30 trans tran NOUN eurjchem-71 197 31 . . PUNCT eurjchem-71 197 32     SPACE eurjchem-71 197 33 1 1 NUM eurjchem-71 197 34     SPACE eurjchem-71 197 35 1978 1978 NUM eurjchem-71 197 36 , , PUNCT eurjchem-71 197 37     SPACE eurjchem-71 197 38 11 11 NUM eurjchem-71 197 39 , , PUNCT eurjchem-71 197 40     SPACE eurjchem-71 197 41 1338‐ 1338‐ NUM eurjchem-71 197 42 1350 1350 NUM eurjchem-71 197 43 . . PUNCT eurjchem-71 197 44     SPACE eurjchem-71 198 1 [ [ X eurjchem-71 198 2 32 32 NUM eurjchem-71 198 3 ] ] PUNCT eurjchem-71 198 4 . . PUNCT eurjchem-71 199 1 sausen sausen PROPN eurjchem-71 199 2 , , PUNCT eurjchem-71 199 3     SPACE eurjchem-71 199 4 g. g. NOUN eurjchem-71 199 5     SPACE eurjchem-71 199 6 n. n. PROPN eurjchem-71 199 7 ; ; PUNCT eurjchem-71 199 8     SPACE eurjchem-71 199 9 engelhardt engelhardt PROPN eurjchem-71 199 10 , , PUNCT eurjchem-71 199 11     SPACE eurjchem-71 200 1 v. v. ADP eurjchem-71 200 2     SPACE eurjchem-71 200 3 a. a. NOUN eurjchem-71 200 4 ; ; PUNCT eurjchem-71 200 5     SPACE eurjchem-71 200 6 middleton middleton PROPN eurjchem-71 200 7 , , PUNCT eurjchem-71 200 8     SPACE eurjchem-71 200 9 w. w. PROPN eurjchem-71 200 10     SPACE eurjchem-71 200 11 j. j. PROPN eurjchem-71 200 12     SPACE eurjchem-71 200 13 j. j. PROPN eurjchem-71 200 14     SPACE eurjchem-71 200 15 am be AUX eurjchem-71 200 16 . . PUNCT eurjchem-71 200 17     SPACE eurjchem-71 200 18 chem chem NOUN eurjchem-71 200 19 . . PUNCT eurjchem-71 200 20     SPACE eurjchem-71 200 21 soc soc PROPN eurjchem-71 200 22 . . PUNCT eurjchem-71 200 23     SPACE eurjchem-71 200 24 1958 1958 NUM eurjchem-71 200 25 , , PUNCT eurjchem-71 200 26     SPACE eurjchem-71 200 27 80 80 NUM eurjchem-71 200 28 , , PUNCT eurjchem-71 200 29     SPACE eurjchem-71 200 30 2815‐2822 2815‐2822 NUM eurjchem-71 200 31 . . PUNCT eurjchem-71 200 32     SPACE