id	sid	tid	token	lemma	pos
eurjchem-782	1	1	untitled	untitle	VERB
eurjchem-782	1	2	european	european	PROPN
eurjchem-782	1	3	journal	journal	PROPN
eurjchem-782	1	4	of	of	ADP
eurjchem-782	1	5	chemistry	chemistry	NOUN
eurjchem-782	1	6	4	4	NUM
eurjchem-782	1	7	(	(	PUNCT
eurjchem-782	1	8	3	3	NUM
eurjchem-782	1	9	)	)	PUNCT
eurjchem-782	1	10	(	(	PUNCT
eurjchem-782	1	11	2013	2013	NUM
eurjchem-782	1	12	)	)	PUNCT
eurjchem-782	1	13	235‐239	235‐239	NUM
eurjchem-782	1	14	european	european	PROPN
eurjchem-782	1	15	journal	journal	PROPN
eurjchem-782	1	16	of	of	ADP
eurjchem-782	1	17	chemistry	chemistry	NOUN
eurjchem-782	1	18	issn	issn	PROPN
eurjchem-782	1	19	2153‐2249	2153‐2249	PROPN
eurjchem-782	1	20	(	(	PUNCT
eurjchem-782	1	21	print	print	NOUN
eurjchem-782	1	22	)	)	PUNCT
eurjchem-782	1	23	/	/	SYM
eurjchem-782	1	24	issn	issn	PROPN
eurjchem-782	1	25	2153‐2257	2153‐2257	NUM
eurjchem-782	1	26	(	(	PUNCT
eurjchem-782	1	27	online	online	ADJ
eurjchem-782	1	28	)	)	PUNCT
eurjchem-782	1	29			NOUN
eurjchem-782	1	30	2013	2013	NUM
eurjchem-782	1	31	eurjchem	eurjchem	PROPN
eurjchem-782	1	32	doi:10.5155	doi:10.5155	PROPN
eurjchem-782	1	33	/	/	SYM
eurjchem-782	1	34	eurjchem.4.3.235‐239.782	eurjchem.4.3.235‐239.782	PROPN
eurjchem-782	1	35	european	european	PROPN
eurjchem-782	1	36	journal	journal	PROPN
eurjchem-782	1	37	of	of	ADP
eurjchem-782	1	38	chemistry	chemistry	PROPN
eurjchem-782	1	39	journal	journal	PROPN
eurjchem-782	1	40	homepage	homepage	NOUN
eurjchem-782	1	41	:	:	PUNCT
eurjchem-782	1	42	www.eurjchem.com	www.eurjchem.com	X
eurjchem-782	1	43	synthesis	synthesis	NOUN
eurjchem-782	1	44	and	and	CCONJ
eurjchem-782	1	45	characterization	characterization	NOUN
eurjchem-782	1	46	of	of	ADP
eurjchem-782	1	47	diaza	diaza	NOUN
eurjchem-782	1	48	analogues	analogue	NOUN
eurjchem-782	1	49	of	of	ADP
eurjchem-782	1	50	podophyllotoxin	podophyllotoxin	PROPN
eurjchem-782	1	51	basavaiah	basavaiah	PROPN
eurjchem-782	1	52	umesha	umesha	PROPN
eurjchem-782	1	53	and	and	CCONJ
eurjchem-782	1	54	yeriyur	yeriyur	PROPN
eurjchem-782	1	55	basavaiah	basavaiah	PROPN
eurjchem-782	1	56	basavaraju	basavaraju	PROPN
eurjchem-782	1	57	*	*	PUNCT
eurjchem-782	1	58	department	department	PROPN
eurjchem-782	1	59	of	of	ADP
eurjchem-782	1	60	studies	study	NOUN
eurjchem-782	1	61	in	in	ADP
eurjchem-782	1	62	chemistry	chemistry	NOUN
eurjchem-782	1	63	,	,	PUNCT
eurjchem-782	1	64	university	university	NOUN
eurjchem-782	1	65	of	of	ADP
eurjchem-782	1	66	mysore	mysore	PROPN
eurjchem-782	1	67	,	,	PUNCT
eurjchem-782	1	68	manasagangotri	manasagangotri	NOUN
eurjchem-782	1	69	,	,	PUNCT
eurjchem-782	1	70	mysore‐570006	mysore‐570006	PROPN
eurjchem-782	1	71	,	,	PUNCT
eurjchem-782	1	72	karnataka	karnataka	PROPN
eurjchem-782	1	73	,	,	PUNCT
eurjchem-782	1	74	india	india	PROPN
eurjchem-782	1	75	*	*	PUNCT
eurjchem-782	1	76	corresponding	correspond	VERB
eurjchem-782	1	77	author	author	NOUN
eurjchem-782	1	78	at	at	ADP
eurjchem-782	1	79	:	:	PUNCT
eurjchem-782	1	80	department	department	NOUN
eurjchem-782	1	81	of	of	ADP
eurjchem-782	1	82	studies	study	NOUN
eurjchem-782	1	83	in	in	ADP
eurjchem-782	1	84	chemistry	chemistry	NOUN
eurjchem-782	1	85	,	,	PUNCT
eurjchem-782	1	86	university	university	NOUN
eurjchem-782	1	87	of	of	ADP
eurjchem-782	1	88	mysore	mysore	PROPN
eurjchem-782	1	89	,	,	PUNCT
eurjchem-782	1	90	manasagangotri	manasagangotri	NOUN
eurjchem-782	1	91	,	,	PUNCT
eurjchem-782	1	92	mysore‐570006	mysore‐570006	PROPN
eurjchem-782	1	93	,	,	PUNCT
eurjchem-782	1	94	karnataka	karnataka	PROPN
eurjchem-782	1	95	,	,	PUNCT
eurjchem-782	1	96	india	india	PROPN
eurjchem-782	1	97	.	.	PUNCT
eurjchem-782	2	1	tel	tel	PROPN
eurjchem-782	2	2	.	.	PUNCT
eurjchem-782	2	3	:	:	PUNCT
eurjchem-782	3	1	+91.948.0441804	+91.948.0441804	NUM
eurjchem-782	3	2	;	;	PUNCT
eurjchem-782	3	3	fax	fax	NOUN
eurjchem-782	3	4	:	:	PUNCT
eurjchem-782	3	5	+91.821.2421263	+91.821.2421263	PROPN
eurjchem-782	3	6	.	.	PUNCT
eurjchem-782	3	7	e‐mail	e‐mail	PUNCT
eurjchem-782	3	8	address	address	NOUN
eurjchem-782	3	9	:	:	PUNCT
eurjchem-782	3	10	basavaraju_yb@yahoo.co.in	basavaraju_yb@yahoo.co.in	PROPN
eurjchem-782	3	11	(	(	PUNCT
eurjchem-782	3	12	y.b	y.b	PROPN
eurjchem-782	3	13	.	.	PROPN
eurjchem-782	3	14	basavaraju	basavaraju	PROPN
eurjchem-782	3	15	)	)	PUNCT
eurjchem-782	3	16	.	.	PUNCT
eurjchem-782	4	1	article	article	NOUN
eurjchem-782	4	2	information	information	PROPN
eurjchem-782	4	3	abstract	abstract	ADV
eurjchem-782	4	4	received	receive	VERB
eurjchem-782	4	5	:	:	PUNCT
eurjchem-782	4	6	23	23	NUM
eurjchem-782	4	7	march	march	NOUN
eurjchem-782	4	8	2013	2013	NUM
eurjchem-782	4	9	received	receive	VERB
eurjchem-782	4	10	in	in	ADP
eurjchem-782	4	11	revised	revise	VERB
eurjchem-782	4	12	form	form	NOUN
eurjchem-782	4	13	:	:	PUNCT
eurjchem-782	4	14	07	07	NUM
eurjchem-782	4	15	may	may	AUX
eurjchem-782	4	16	2013	2013	NUM
eurjchem-782	4	17	accepted	accept	VERB
eurjchem-782	4	18	:	:	PUNCT
eurjchem-782	4	19	07	07	NUM
eurjchem-782	4	20	may	may	PROPN
eurjchem-782	4	21	2013	2013	NUM
eurjchem-782	4	22	online	online	NOUN
eurjchem-782	4	23	:	:	PUNCT
eurjchem-782	4	24	30	30	NUM
eurjchem-782	4	25	september	september	PROPN
eurjchem-782	4	26	2013	2013	NUM
eurjchem-782	4	27	keywords	keyword	NOUN
eurjchem-782	4	28	in	in	ADP
eurjchem-782	4	29	an	an	DET
eurjchem-782	4	30	attempt	attempt	NOUN
eurjchem-782	4	31	to	to	PART
eurjchem-782	4	32	synthesize	synthesize	VERB
eurjchem-782	4	33	the	the	DET
eurjchem-782	4	34	novel	novel	ADJ
eurjchem-782	4	35	diaza	diaza	NOUN
eurjchem-782	4	36	analogues	analogue	NOUN
eurjchem-782	4	37	of	of	ADP
eurjchem-782	4	38	podophyllotoxin	podophyllotoxin	PROPN
eurjchem-782	4	39	(	(	PUNCT
eurjchem-782	4	40	7a‐d	7a‐d	NOUN
eurjchem-782	4	41	)	)	PUNCT
eurjchem-782	4	42	in	in	ADP
eurjchem-782	4	43	five	five	NUM
eurjchem-782	4	44	step	step	NOUN
eurjchem-782	4	45	reactions	reaction	NOUN
eurjchem-782	4	46	.	.	PUNCT
eurjchem-782	5	1	the	the	DET
eurjchem-782	5	2	synthesis	synthesis	NOUN
eurjchem-782	5	3	of	of	ADP
eurjchem-782	5	4	title	title	NOUN
eurjchem-782	5	5	compounds	compound	NOUN
eurjchem-782	5	6	has	have	AUX
eurjchem-782	5	7	been	be	AUX
eurjchem-782	5	8	achieved	achieve	VERB
eurjchem-782	5	9	from	from	ADP
eurjchem-782	5	10	tetralones	tetralone	NOUN
eurjchem-782	5	11	,	,	PUNCT
eurjchem-782	5	12	which	which	PRON
eurjchem-782	5	13	were	be	AUX
eurjchem-782	5	14	formylated	formylate	VERB
eurjchem-782	5	15	with	with	ADP
eurjchem-782	5	16	ethylformate	ethylformate	NOUN
eurjchem-782	5	17	;	;	PUNCT
eurjchem-782	5	18	prepared	prepare	VERB
eurjchem-782	5	19	via	via	ADP
eurjchem-782	5	20	cyclization	cyclization	NOUN
eurjchem-782	5	21	with	with	ADP
eurjchem-782	5	22	hydrazine	hydrazine	NOUN
eurjchem-782	5	23	hydrate	hydrate	NOUN
eurjchem-782	5	24	.	.	PUNCT
eurjchem-782	6	1	furthermore	furthermore	ADV
eurjchem-782	6	2	,	,	PUNCT
eurjchem-782	6	3	these	these	DET
eurjchem-782	6	4	newly	newly	ADV
eurjchem-782	6	5	synthesized	synthesize	VERB
eurjchem-782	6	6	compounds	compound	NOUN
eurjchem-782	6	7	were	be	AUX
eurjchem-782	6	8	characterized	characterize	VERB
eurjchem-782	6	9	by	by	ADP
eurjchem-782	6	10	spectral	spectral	ADJ
eurjchem-782	6	11	and	and	CCONJ
eurjchem-782	6	12	elemental	elemental	ADJ
eurjchem-782	6	13	analysis	analysis	NOUN
eurjchem-782	6	14	data	datum	NOUN
eurjchem-782	6	15	.	.	PUNCT
eurjchem-782	7	1	chalcones	chalcone	VERB
eurjchem-782	7	2	tetralones	tetralone	NOUN
eurjchem-782	7	3	ethylformate	ethylformate	PROPN
eurjchem-782	7	4	sodium	sodium	NOUN
eurjchem-782	7	5	hydride	hydride	NOUN
eurjchem-782	7	6	hydrazine	hydrazine	NOUN
eurjchem-782	7	7	hydrate	hydrate	NOUN
eurjchem-782	7	8	cyclopropyl	cyclopropyl	NOUN
eurjchem-782	7	9	ketones	ketone	NOUN
eurjchem-782	7	10	1	1	NUM
eurjchem-782	7	11	.	.	PUNCT
eurjchem-782	8	1	introduction	introduction	NOUN
eurjchem-782	8	2	in	in	ADP
eurjchem-782	8	3	the	the	DET
eurjchem-782	8	4	recent	recent	ADJ
eurjchem-782	8	5	years	year	NOUN
eurjchem-782	8	6	,	,	PUNCT
eurjchem-782	8	7	efforts	effort	NOUN
eurjchem-782	8	8	have	have	AUX
eurjchem-782	8	9	been	be	AUX
eurjchem-782	8	10	made	make	VERB
eurjchem-782	8	11	to	to	PART
eurjchem-782	8	12	synthesize	synthesize	VERB
eurjchem-782	8	13	novel	novel	ADJ
eurjchem-782	8	14	analogues	analogue	NOUN
eurjchem-782	8	15	of	of	ADP
eurjchem-782	8	16	podophyllotoxin	podophyllotoxin	NOUN
eurjchem-782	8	17	that	that	PRON
eurjchem-782	8	18	may	may	AUX
eurjchem-782	8	19	bear	bear	VERB
eurjchem-782	8	20	antibacterial	antibacterial	ADJ
eurjchem-782	8	21	,	,	PUNCT
eurjchem-782	8	22	antiviral	antiviral	NOUN
eurjchem-782	8	23	,	,	PUNCT
eurjchem-782	8	24	anticancer	anticancer	NOUN
eurjchem-782	8	25	and	and	CCONJ
eurjchem-782	8	26	antimitotic	antimitotic	ADJ
eurjchem-782	8	27	activity	activity	NOUN
eurjchem-782	8	28	[	[	X
eurjchem-782	8	29	1	1	NUM
eurjchem-782	8	30	]	]	PUNCT
eurjchem-782	8	31	.	.	PUNCT
eurjchem-782	9	1	aryltetra‐	aryltetra‐	PROPN
eurjchem-782	9	2	hydronaphthalene‐type	hydronaphthalene‐type	PROPN
eurjchem-782	9	3	lignans	lignan	NOUN
eurjchem-782	9	4	as	as	ADP
eurjchem-782	9	5	podophyl	podophyl	PROPN
eurjchem-782	9	6	lotoxin	lotoxin	PROPN
eurjchem-782	9	7	and	and	CCONJ
eurjchem-782	9	8	its	its	PRON
eurjchem-782	9	9	derivatives	derivative	NOUN
eurjchem-782	9	10	are	be	AUX
eurjchem-782	9	11	important	important	ADJ
eurjchem-782	9	12	natural	natural	ADJ
eurjchem-782	9	13	products	product	NOUN
eurjchem-782	9	14	in	in	ADP
eurjchem-782	9	15	the	the	DET
eurjchem-782	9	16	armamentarium	armamentarium	NOUN
eurjchem-782	9	17	of	of	ADP
eurjchem-782	9	18	antineoplastic	antineoplastic	ADJ
eurjchem-782	9	19	agents	agent	NOUN
eurjchem-782	9	20	.	.	PUNCT
eurjchem-782	10	1	the	the	DET
eurjchem-782	10	2	biological	biological	ADJ
eurjchem-782	10	3	assessment	assessment	NOUN
eurjchem-782	10	4	of	of	ADP
eurjchem-782	10	5	podophyllotoxin	podophyllotoxin	PROPN
eurjchem-782	10	6	was	be	AUX
eurjchem-782	10	7	followed	follow	VERB
eurjchem-782	10	8	by	by	ADP
eurjchem-782	10	9	discovery	discovery	NOUN
eurjchem-782	10	10	of	of	ADP
eurjchem-782	10	11	its	its	PRON
eurjchem-782	10	12	mode	mode	NOUN
eurjchem-782	10	13	of	of	ADP
eurjchem-782	10	14	action	action	NOUN
eurjchem-782	10	15	and	and	CCONJ
eurjchem-782	10	16	culminated	culminate	VERB
eurjchem-782	10	17	in	in	ADP
eurjchem-782	10	18	the	the	DET
eurjchem-782	10	19	synthesis	synthesis	NOUN
eurjchem-782	10	20	of	of	ADP
eurjchem-782	10	21	the	the	DET
eurjchem-782	10	22	anticancer	anticancer	NOUN
eurjchem-782	10	23	drugs	drug	NOUN
eurjchem-782	10	24	etoposide	etoposide	NOUN
eurjchem-782	10	25	and	and	CCONJ
eurjchem-782	10	26	teniposide	teniposide	VERB
eurjchem-782	10	27	[	[	X
eurjchem-782	10	28	2	2	NUM
eurjchem-782	10	29	]	]	PUNCT
eurjchem-782	10	30	.	.	PUNCT
eurjchem-782	11	1	hence	hence	ADV
eurjchem-782	11	2	,	,	PUNCT
eurjchem-782	11	3	current	current	ADJ
eurjchem-782	11	4	research	research	NOUN
eurjchem-782	11	5	is	be	AUX
eurjchem-782	11	6	focused	focus	VERB
eurjchem-782	11	7	on	on	ADP
eurjchem-782	11	8	synthesizing	synthesize	VERB
eurjchem-782	11	9	novel	novel	ADJ
eurjchem-782	11	10	compounds	compound	NOUN
eurjchem-782	11	11	and	and	CCONJ
eurjchem-782	11	12	to	to	PART
eurjchem-782	11	13	study	study	VERB
eurjchem-782	11	14	their	their	PRON
eurjchem-782	11	15	structure	structure	NOUN
eurjchem-782	11	16	activity	activity	NOUN
eurjchem-782	11	17	relationship	relationship	NOUN
eurjchem-782	12	1	[	[	X
eurjchem-782	12	2	3	3	NUM
eurjchem-782	12	3	]	]	PUNCT
eurjchem-782	12	4	.	.	PUNCT
eurjchem-782	13	1	there	there	PRON
eurjchem-782	13	2	exist	exist	VERB
eurjchem-782	13	3	a	a	DET
eurjchem-782	13	4	class	class	NOUN
eurjchem-782	13	5	of	of	ADP
eurjchem-782	13	6	natural	natural	ADJ
eurjchem-782	13	7	products	product	NOUN
eurjchem-782	13	8	called	call	VERB
eurjchem-782	13	9	lignans	lignan	NOUN
eurjchem-782	13	10	,	,	PUNCT
eurjchem-782	13	11	derived	derive	VERB
eurjchem-782	13	12	from	from	ADP
eurjchem-782	13	13	the	the	DET
eurjchem-782	13	14	plants	plant	NOUN
eurjchem-782	13	15	of	of	ADP
eurjchem-782	13	16	the	the	DET
eurjchem-782	13	17	podophyllum	podophyllum	NOUN
eurjchem-782	13	18	species	specie	NOUN
eurjchem-782	13	19	[	[	X
eurjchem-782	13	20	4,5	4,5	NUM
eurjchem-782	13	21	]	]	PUNCT
eurjchem-782	13	22	.	.	PUNCT
eurjchem-782	14	1	podophyllotoxin	podophyllotoxin	PROPN
eurjchem-782	14	2	is	be	AUX
eurjchem-782	14	3	an	an	DET
eurjchem-782	14	4	important	important	ADJ
eurjchem-782	14	5	member	member	NOUN
eurjchem-782	14	6	of	of	ADP
eurjchem-782	14	7	this	this	DET
eurjchem-782	14	8	class	class	NOUN
eurjchem-782	14	9	and	and	CCONJ
eurjchem-782	14	10	it	it	PRON
eurjchem-782	14	11	has	have	AUX
eurjchem-782	14	12	received	receive	VERB
eurjchem-782	14	13	considerable	considerable	ADJ
eurjchem-782	14	14	attention	attention	NOUN
eurjchem-782	14	15	for	for	ADP
eurjchem-782	14	16	its	its	PRON
eurjchem-782	14	17	remarkable	remarkable	ADJ
eurjchem-782	14	18	biological	biological	ADJ
eurjchem-782	14	19	applications	application	NOUN
eurjchem-782	14	20	(	(	PUNCT
eurjchem-782	14	21	figure	figure	NOUN
eurjchem-782	14	22	1	1	NUM
eurjchem-782	14	23	)	)	PUNCT
eurjchem-782	14	24	.	.	PUNCT
eurjchem-782	15	1	since	since	SCONJ
eurjchem-782	15	2	it	it	PRON
eurjchem-782	15	3	is	be	AUX
eurjchem-782	15	4	having	have	VERB
eurjchem-782	15	5	toxic	toxic	ADJ
eurjchem-782	15	6	properties	property	NOUN
eurjchem-782	15	7	and	and	CCONJ
eurjchem-782	15	8	solubility	solubility	NOUN
eurjchem-782	15	9	problem	problem	NOUN
eurjchem-782	15	10	in	in	ADP
eurjchem-782	15	11	water	water	NOUN
eurjchem-782	15	12	,	,	PUNCT
eurjchem-782	15	13	it	it	PRON
eurjchem-782	15	14	can	can	AUX
eurjchem-782	15	15	not	not	PART
eurjchem-782	15	16	be	be	AUX
eurjchem-782	15	17	directly	directly	ADV
eurjchem-782	15	18	applied	apply	VERB
eurjchem-782	15	19	for	for	ADP
eurjchem-782	15	20	the	the	DET
eurjchem-782	15	21	clinical	clinical	ADJ
eurjchem-782	15	22	use	use	NOUN
eurjchem-782	15	23	,	,	PUNCT
eurjchem-782	15	24	instead	instead	ADV
eurjchem-782	15	25	certain	certain	ADJ
eurjchem-782	15	26	extensive	extensive	ADJ
eurjchem-782	15	27	structural	structural	ADJ
eurjchem-782	15	28	modifications	modification	NOUN
eurjchem-782	15	29	have	have	VERB
eurjchem-782	15	30	to	to	PART
eurjchem-782	15	31	be	be	AUX
eurjchem-782	15	32	done	do	VERB
eurjchem-782	15	33	[	[	PUNCT
eurjchem-782	15	34	6	6	NUM
eurjchem-782	15	35	]	]	PUNCT
eurjchem-782	15	36	.	.	PUNCT
eurjchem-782	16	1	as	as	ADP
eurjchem-782	16	2	a	a	DET
eurjchem-782	16	3	result	result	NOUN
eurjchem-782	16	4	of	of	ADP
eurjchem-782	16	5	these	these	DET
eurjchem-782	16	6	modifications	modification	NOUN
eurjchem-782	16	7	,	,	PUNCT
eurjchem-782	16	8	some	some	PRON
eurjchem-782	16	9	of	of	ADP
eurjchem-782	16	10	the	the	DET
eurjchem-782	16	11	semisynthetic	semisynthetic	ADJ
eurjchem-782	16	12	analogues	analogue	NOUN
eurjchem-782	16	13	of	of	ADP
eurjchem-782	16	14	podophyllotoxin	podophyllotoxin	NOUN
eurjchem-782	16	15	have	have	AUX
eurjchem-782	16	16	been	be	AUX
eurjchem-782	16	17	synthesized	synthesize	VERB
eurjchem-782	16	18	,	,	PUNCT
eurjchem-782	16	19	namely	namely	ADV
eurjchem-782	16	20	etoposide	etoposide	NOUN
eurjchem-782	16	21	and	and	CCONJ
eurjchem-782	16	22	teniposide	teniposide	NOUN
eurjchem-782	16	23	are	be	AUX
eurjchem-782	16	24	now	now	ADV
eurjchem-782	16	25	in	in	ADP
eurjchem-782	16	26	clinical	clinical	ADJ
eurjchem-782	16	27	use	use	NOUN
eurjchem-782	16	28	[	[	X
eurjchem-782	16	29	7‐11	7‐11	NUM
eurjchem-782	16	30	]	]	PUNCT
eurjchem-782	16	31	.	.	PUNCT
eurjchem-782	17	1	so	so	ADV
eurjchem-782	17	2	it	it	PRON
eurjchem-782	17	3	is	be	AUX
eurjchem-782	17	4	necessary	necessary	ADJ
eurjchem-782	17	5	to	to	PART
eurjchem-782	17	6	study	study	VERB
eurjchem-782	17	7	their	their	PRON
eurjchem-782	17	8	structural	structural	ADJ
eurjchem-782	17	9	activity	activity	NOUN
eurjchem-782	17	10	relationship	relationship	NOUN
eurjchem-782	17	11	,	,	PUNCT
eurjchem-782	17	12	hence	hence	ADV
eurjchem-782	17	13	several	several	ADJ
eurjchem-782	17	14	podophyllotoxin	podophyllotoxin	NOUN
eurjchem-782	17	15	analogues	analogue	NOUN
eurjchem-782	17	16	have	have	AUX
eurjchem-782	17	17	been	be	AUX
eurjchem-782	17	18	synthesized	synthesize	VERB
eurjchem-782	17	19	[	[	PUNCT
eurjchem-782	17	20	12	12	NUM
eurjchem-782	17	21	]	]	PUNCT
eurjchem-782	17	22	.	.	PUNCT
eurjchem-782	18	1	in	in	ADP
eurjchem-782	18	2	view	view	NOUN
eurjchem-782	18	3	of	of	ADP
eurjchem-782	18	4	the	the	DET
eurjchem-782	18	5	above	above	ADJ
eurjchem-782	18	6	facts	fact	NOUN
eurjchem-782	18	7	,	,	PUNCT
eurjchem-782	18	8	it	it	PRON
eurjchem-782	18	9	was	be	AUX
eurjchem-782	18	10	decided	decide	VERB
eurjchem-782	18	11	to	to	PART
eurjchem-782	18	12	modify	modify	VERB
eurjchem-782	18	13	the	the	DET
eurjchem-782	18	14	structure	structure	NOUN
eurjchem-782	18	15	of	of	ADP
eurjchem-782	18	16	podophyllotoxin	podophyllotoxin	NOUN
eurjchem-782	18	17	to	to	PART
eurjchem-782	18	18	synthesize	synthesize	VERB
eurjchem-782	18	19	novel	novel	ADJ
eurjchem-782	18	20	diaza	diaza	NOUN
eurjchem-782	18	21	analogues	analogue	NOUN
eurjchem-782	18	22	of	of	ADP
eurjchem-782	18	23	podophyllotoxin	podophyllotoxin	NOUN
eurjchem-782	18	24	.	.	PUNCT
eurjchem-782	19	1	2	2	X
eurjchem-782	19	2	.	.	X
eurjchem-782	19	3	experimental	experimental	ADJ
eurjchem-782	19	4	2.1	2.1	NUM
eurjchem-782	19	5	.	.	PUNCT
eurjchem-782	19	6	materials	material	NOUN
eurjchem-782	19	7	and	and	CCONJ
eurjchem-782	19	8	methods	method	NOUN
eurjchem-782	19	9	all	all	DET
eurjchem-782	19	10	reagents	reagent	NOUN
eurjchem-782	19	11	and	and	CCONJ
eurjchem-782	19	12	chemicals	chemical	NOUN
eurjchem-782	19	13	were	be	AUX
eurjchem-782	19	14	purchased	purchase	VERB
eurjchem-782	19	15	from	from	ADP
eurjchem-782	19	16	merck	merck	NOUN
eurjchem-782	19	17	chemicals	chemical	NOUN
eurjchem-782	19	18	used	use	VERB
eurjchem-782	19	19	without	without	ADP
eurjchem-782	19	20	further	further	ADJ
eurjchem-782	19	21	purification	purification	NOUN
eurjchem-782	19	22	.	.	PUNCT
eurjchem-782	20	1	melting	melting	NOUN
eurjchem-782	20	2	points	point	NOUN
eurjchem-782	20	3	were	be	AUX
eurjchem-782	20	4	taken	take	VERB
eurjchem-782	20	5	in	in	ADP
eurjchem-782	20	6	open	open	ADJ
eurjchem-782	20	7	capillary	capillary	ADJ
eurjchem-782	20	8	tubes	tube	NOUN
eurjchem-782	20	9	and	and	CCONJ
eurjchem-782	20	10	are	be	AUX
eurjchem-782	20	11	uncorrected	uncorrecte	VERB
eurjchem-782	20	12	.	.	PUNCT
eurjchem-782	21	1	tlc	tlc	NOUN
eurjchem-782	21	2	is	be	AUX
eurjchem-782	21	3	performed	perform	VERB
eurjchem-782	21	4	with	with	ADP
eurjchem-782	21	5	e.	e.	PROPN
eurjchem-782	21	6	merck	merck	PROPN
eurjchem-782	21	7	precoated	precoated	PROPN
eurjchem-782	21	8	silica	silica	NOUN
eurjchem-782	21	9	gel	gel	NOUN
eurjchem-782	21	10	plates	plate	NOUN
eurjchem-782	21	11	(	(	PUNCT
eurjchem-782	21	12	60f254	60f254	PROPN
eurjchem-782	21	13	)	)	PUNCT
eurjchem-782	21	14	with	with	ADP
eurjchem-782	21	15	iodine	iodine	NOUN
eurjchem-782	21	16	as	as	ADP
eurjchem-782	21	17	a	a	DET
eurjchem-782	21	18	developing	develop	VERB
eurjchem-782	21	19	agent	agent	NOUN
eurjchem-782	21	20	.	.	PUNCT
eurjchem-782	22	1	acme	acme	PROPN
eurjchem-782	22	2	,	,	PUNCT
eurjchem-782	22	3	india	india	PROPN
eurjchem-782	22	4	silica	silica	PROPN
eurjchem-782	22	5	gel	gel	NOUN
eurjchem-782	22	6	,	,	PUNCT
eurjchem-782	22	7	60‐120	60‐120	ADJ
eurjchem-782	22	8	mesh	mesh	NOUN
eurjchem-782	22	9	for	for	ADP
eurjchem-782	22	10	column	column	NOUN
eurjchem-782	22	11	chromatography	chromatography	NOUN
eurjchem-782	22	12	is	be	AUX
eurjchem-782	22	13	used	use	VERB
eurjchem-782	22	14	.	.	PUNCT
eurjchem-782	23	1	ir	ir	PROPN
eurjchem-782	23	2	spectra	spectra	PROPN
eurjchem-782	23	3	in	in	ADP
eurjchem-782	23	4	kbr	kbr	PROPN
eurjchem-782	23	5	were	be	AUX
eurjchem-782	23	6	recorded	record	VERB
eurjchem-782	23	7	on	on	ADP
eurjchem-782	23	8	perkin‐elmer	perkin‐elmer	PROPN
eurjchem-782	23	9	model	model	NOUN
eurjchem-782	23	10	683	683	NUM
eurjchem-782	23	11	or	or	CCONJ
eurjchem-782	23	12	1310	1310	NUM
eurjchem-782	23	13	spectrometers	spectrometer	NOUN
eurjchem-782	23	14	.	.	PUNCT
eurjchem-782	24	1	1h	1h	NUM
eurjchem-782	24	2	nmr	nmr	NOUN
eurjchem-782	24	3	(	(	PUNCT
eurjchem-782	24	4	400	400	NUM
eurjchem-782	24	5	mhz	mhz	NOUN
eurjchem-782	24	6	)	)	PUNCT
eurjchem-782	24	7	and	and	CCONJ
eurjchem-782	24	8	13c	13c	NOUN
eurjchem-782	24	9	nmr	nmr	NOUN
eurjchem-782	24	10	(	(	PUNCT
eurjchem-782	24	11	100	100	NUM
eurjchem-782	24	12	mhz	mhz	NOUN
eurjchem-782	24	13	)	)	PUNCT
eurjchem-782	24	14	spectra	spectra	NOUN
eurjchem-782	24	15	using	use	VERB
eurjchem-782	24	16	trimethyl	trimethyl	PROPN
eurjchem-782	24	17	silane	silane	NOUN
eurjchem-782	24	18	(	(	PUNCT
eurjchem-782	24	19	tms	tms	PROPN
eurjchem-782	24	20	)	)	PUNCT
eurjchem-782	24	21	as	as	ADP
eurjchem-782	24	22	an	an	DET
eurjchem-782	24	23	internal	internal	ADJ
eurjchem-782	24	24	reference	reference	NOUN
eurjchem-782	24	25	were	be	AUX
eurjchem-782	24	26	recorded	record	VERB
eurjchem-782	24	27	on	on	ADP
eurjchem-782	24	28	bruker	bruker	PROPN
eurjchem-782	24	29	spectrometer	spectrometer	NOUN
eurjchem-782	24	30	,	,	PUNCT
eurjchem-782	24	31	elemental	elemental	ADJ
eurjchem-782	24	32	analyses	analysis	NOUN
eurjchem-782	24	33	were	be	AUX
eurjchem-782	24	34	performed	perform	VERB
eurjchem-782	24	35	on	on	ADP
eurjchem-782	24	36	a	a	DET
eurjchem-782	24	37	perkin‐elmer	perkin‐elmer	NOUN
eurjchem-782	24	38	2400	2400	NUM
eurjchem-782	24	39	,	,	PUNCT
eurjchem-782	24	40	elemental	elemental	ADJ
eurjchem-782	24	41	analyzer	analyzer	NOUN
eurjchem-782	24	42	and	and	CCONJ
eurjchem-782	24	43	the	the	DET
eurjchem-782	24	44	mass	mass	ADJ
eurjchem-782	24	45	spectra	spectra	NOUN
eurjchem-782	24	46	were	be	AUX
eurjchem-782	24	47	obtained	obtain	VERB
eurjchem-782	24	48	on	on	ADP
eurjchem-782	24	49	cec‐21‐100b	cec‐21‐100b	PROPN
eurjchem-782	24	50	,	,	PUNCT
eurjchem-782	24	51	finnigan	finnigan	NOUN
eurjchem-782	24	52	mat	mat	NOUN
eurjchem-782	24	53	1210	1210	NUM
eurjchem-782	24	54	or	or	CCONJ
eurjchem-782	24	55	micro	micro	ADJ
eurjchem-782	24	56	mass	mass	NOUN
eurjchem-782	24	57	7070	7070	NUM
eurjchem-782	24	58	spectrometers	spectrometer	NOUN
eurjchem-782	24	59	operating	operate	VERB
eurjchem-782	24	60	at	at	ADP
eurjchem-782	24	61	70ev	70ev	NOUN
eurjchem-782	24	62	using	use	VERB
eurjchem-782	24	63	a	a	DET
eurjchem-782	24	64	direct	direct	ADJ
eurjchem-782	24	65	inlet	inlet	NOUN
eurjchem-782	24	66	system	system	NOUN
eurjchem-782	24	67	.	.	PUNCT
eurjchem-782	25	1	o	o	X
eurjchem-782	26	1	o	o	X
eurjchem-782	27	1	o	o	NOUN
eurjchem-782	28	1	oh	oh	INTJ
eurjchem-782	28	2	h	h	NOUN
eurjchem-782	29	1	h	h	NOUN
eurjchem-782	30	1	o	o	NOUN
eurjchem-782	31	1	o	o	X
eurjchem-782	31	2	o	o	X
eurjchem-782	31	3	o	o	NOUN
eurjchem-782	31	4	figure	figure	NOUN
eurjchem-782	31	5	1	1	NUM
eurjchem-782	31	6	.	.	PUNCT
eurjchem-782	32	1	the	the	DET
eurjchem-782	32	2	structure	structure	NOUN
eurjchem-782	32	3	of	of	ADP
eurjchem-782	32	4	podophyllotoxin	podophyllotoxin	PROPN
eurjchem-782	32	5	.	.	PUNCT
eurjchem-782	33	1	2.2	2.2	NUM
eurjchem-782	33	2	.	.	PUNCT
eurjchem-782	33	3	synthesis	synthesis	NOUN
eurjchem-782	33	4	2.2.1	2.2.1	NUM
eurjchem-782	33	5	.	.	PUNCT
eurjchem-782	33	6	general	general	ADJ
eurjchem-782	33	7	procedure	procedure	NOUN
eurjchem-782	33	8	for	for	ADP
eurjchem-782	33	9	the	the	DET
eurjchem-782	33	10	synthesis	synthesis	NOUN
eurjchem-782	33	11	of	of	ADP
eurjchem-782	33	12	chalcones	chalcone	NOUN
eurjchem-782	33	13	(	(	PUNCT
eurjchem-782	33	14	3a‐	3a‐	NUM
eurjchem-782	33	15	d	d	NOUN
eurjchem-782	33	16	)	)	PUNCT
eurjchem-782	33	17	substituted	substitute	VERB
eurjchem-782	33	18	acetophenones	acetophenone	NOUN
eurjchem-782	33	19	(	(	PUNCT
eurjchem-782	33	20	0.0487	0.0487	NUM
eurjchem-782	33	21	mol	mol	NOUN
eurjchem-782	33	22	)	)	PUNCT
eurjchem-782	33	23	and	and	CCONJ
eurjchem-782	33	24	benzaldehyde	benzaldehyde	NOUN
eurjchem-782	33	25	(	(	PUNCT
eurjchem-782	33	26	5.2	5.2	NUM
eurjchem-782	33	27	g	g	NOUN
eurjchem-782	33	28	,	,	PUNCT
eurjchem-782	33	29	0.0487	0.0487	NUM
eurjchem-782	33	30	mol	mol	NOUN
eurjchem-782	33	31	)	)	PUNCT
eurjchem-782	33	32	were	be	AUX
eurjchem-782	33	33	stirred	stir	VERB
eurjchem-782	33	34	in	in	ADP
eurjchem-782	33	35	water	water	NOUN
eurjchem-782	33	36	(	(	PUNCT
eurjchem-782	33	37	40	40	NUM
eurjchem-782	33	38	ml	ml	NOUN
eurjchem-782	33	39	)	)	PUNCT
eurjchem-782	33	40	and	and	CCONJ
eurjchem-782	33	41	ethanol	ethanol	NOUN
eurjchem-782	33	42	(	(	PUNCT
eurjchem-782	33	43	25	25	NUM
eurjchem-782	33	44	ml	ml	NOUN
eurjchem-782	33	45	)	)	PUNCT
eurjchem-782	33	46	mixture	mixture	NOUN
eurjchem-782	33	47	in	in	ADP
eurjchem-782	33	48	the	the	DET
eurjchem-782	33	49	presence	presence	NOUN
eurjchem-782	33	50	of	of	ADP
eurjchem-782	33	51	sodium	sodium	NOUN
eurjchem-782	33	52	hydroxide	hydroxide	NOUN
eurjchem-782	33	53	(	(	PUNCT
eurjchem-782	33	54	1.9	1.9	NUM
eurjchem-782	33	55	g	g	NOUN
eurjchem-782	33	56	,	,	PUNCT
eurjchem-782	33	57	0.0487	0.0487	NUM
eurjchem-782	33	58	mol	mol	NOUN
eurjchem-782	33	59	)	)	PUNCT
eurjchem-782	33	60	at	at	ADP
eurjchem-782	33	61	15‐30	15‐30	NUM
eurjchem-782	33	62	oc	oc	NOUN
eurjchem-782	33	63	for	for	ADP
eurjchem-782	33	64	4h	4h	NUM
eurjchem-782	33	65	.	.	PUNCT
eurjchem-782	34	1	the	the	DET
eurjchem-782	34	2	reaction	reaction	NOUN
eurjchem-782	34	3	mixture	mixture	NOUN
eurjchem-782	34	4	was	be	AUX
eurjchem-782	34	5	kept	keep	VERB
eurjchem-782	34	6	overnight	overnight	ADV
eurjchem-782	34	7	in	in	ADP
eurjchem-782	34	8	an	an	DET
eurjchem-782	34	9	ice	ice	NOUN
eurjchem-782	34	10	bath	bath	NOUN
eurjchem-782	34	11	.	.	PUNCT
eurjchem-782	35	1	the	the	DET
eurjchem-782	35	2	precipitated	precipitate	VERB
eurjchem-782	35	3	products	product	NOUN
eurjchem-782	35	4	were	be	AUX
eurjchem-782	35	5	filtered	filter	VERB
eurjchem-782	35	6	and	and	CCONJ
eurjchem-782	35	7	recrystallized	recrystallize	VERB
eurjchem-782	35	8	from	from	ADP
eurjchem-782	35	9	ethanol	ethanol	NOUN
eurjchem-782	35	10	(	(	PUNCT
eurjchem-782	35	11	scheme	scheme	NOUN
eurjchem-782	35	12	1	1	NUM
eurjchem-782	35	13	)	)	PUNCT
eurjchem-782	35	14	.	.	PUNCT
eurjchem-782	36	1	236	236	NUM
eurjchem-782	36	2	umesha	umesha	ADJ
eurjchem-782	36	3	and	and	CCONJ
eurjchem-782	36	4	basavaraju	basavaraju	NOUN
eurjchem-782	36	5	/	/	SYM
eurjchem-782	36	6	european	european	ADJ
eurjchem-782	36	7	journal	journal	PROPN
eurjchem-782	36	8	of	of	ADP
eurjchem-782	36	9	chemistry	chemistry	NOUN
eurjchem-782	36	10	4	4	NUM
eurjchem-782	36	11	(	(	PUNCT
eurjchem-782	36	12	3	3	NUM
eurjchem-782	36	13	)	)	PUNCT
eurjchem-782	36	14	(	(	PUNCT
eurjchem-782	36	15	2013	2013	NUM
eurjchem-782	36	16	)	)	PUNCT
eurjchem-782	36	17	235‐239	235‐239	NUM
eurjchem-782	36	18	o	o	NOUN
eurjchem-782	36	19	r1	r1	PROPN
eurjchem-782	36	20	o	o	PROPN
eurjchem-782	36	21	r1	r1	PROPN
eurjchem-782	36	22	o	o	PROPN
eurjchem-782	36	23	r1	r1	PROPN
eurjchem-782	36	24	o	o	PROPN
eurjchem-782	36	25	r1	r1	PROPN
eurjchem-782	36	26	r1	r1	PROPN
eurjchem-782	36	27	naoh	naoh	PROPN
eurjchem-782	36	28	etoh	etoh	PROPN
eurjchem-782	36	29	-	-	PUNCT
eurjchem-782	36	30	h2o	h2o	PROPN
eurjchem-782	36	31	ch3i	ch3i	PROPN
eurjchem-782	36	32	/	/	SYM
eurjchem-782	36	33	nah	nah	NOUN
eurjchem-782	36	34	ac2o	ac2o	PROPN
eurjchem-782	36	35	,	,	PUNCT
eurjchem-782	36	36	anhyd.sncl4	anhyd.sncl4	ADJ
eurjchem-782	36	37	dry	dry	ADJ
eurjchem-782	36	38	ch2cl2	ch2cl2	PUNCT
eurjchem-782	36	39	nhn	nhn	PROPN
eurjchem-782	36	40	nah	nah	PROPN
eurjchem-782	36	41	,	,	PUNCT
eurjchem-782	36	42	dry	dry	PROPN
eurjchem-782	36	43	c6h6	c6h6	VERB
eurjchem-782	36	44	r1	r1	PROPN
eurjchem-782	36	45	o	o	PROPN
eurjchem-782	37	1	oh	oh	INTJ
eurjchem-782	37	2	nh2nh2	nh2nh2	NOUN
eurjchem-782	37	3	/	/	SYM
eurjchem-782	37	4	etoh	etoh	NOUN
eurjchem-782	37	5	r2	r2	PROPN
eurjchem-782	37	6	r2	r2	PROPN
eurjchem-782	37	7	r2	r2	PROPN
eurjchem-782	37	8	r2	r2	PROPN
eurjchem-782	37	9	r2	r2	PROPN
eurjchem-782	37	10	hcooc2h5	hcooc2h5	PROPN
eurjchem-782	37	11	(	(	PUNCT
eurjchem-782	37	12	1a	1a	X
eurjchem-782	37	13	-	-	PUNCT
eurjchem-782	37	14	d	d	NOUN
eurjchem-782	37	15	)	)	PUNCT
eurjchem-782	37	16	2	2	NUM
eurjchem-782	37	17	(	(	PUNCT
eurjchem-782	37	18	3a	3a	NUM
eurjchem-782	37	19	-	-	SYM
eurjchem-782	37	20	d	d	NOUN
eurjchem-782	37	21	)	)	PUNCT
eurjchem-782	37	22	(	(	PUNCT
eurjchem-782	37	23	4a	4a	NUM
eurjchem-782	37	24	-	-	SYM
eurjchem-782	37	25	d	d	NOUN
eurjchem-782	37	26	)	)	PUNCT
eurjchem-782	37	27	(	(	PUNCT
eurjchem-782	37	28	5a	5a	NUM
eurjchem-782	37	29	-	-	SYM
eurjchem-782	37	30	d	d	NOUN
eurjchem-782	37	31	)	)	PUNCT
eurjchem-782	37	32	(	(	PUNCT
eurjchem-782	37	33	6a	6a	NOUN
eurjchem-782	37	34	-	-	SYM
eurjchem-782	37	35	d	d	NOUN
eurjchem-782	37	36	)	)	PUNCT
eurjchem-782	37	37	(	(	PUNCT
eurjchem-782	37	38	7a	7a	NUM
eurjchem-782	37	39	-	-	SYM
eurjchem-782	37	40	d	d	NOUN
eurjchem-782	37	41	)	)	PUNCT
eurjchem-782	37	42	9	9	NUM
eurjchem-782	37	43	o	o	NOUN
eurjchem-782	37	44	h	h	NOUN
eurjchem-782	37	45	dmso	dmso	NOUN
eurjchem-782	37	46	r2	r2	PROPN
eurjchem-782	37	47	1	1	NUM
eurjchem-782	37	48	'	'	PART
eurjchem-782	37	49	2	2	NUM
eurjchem-782	37	50	'	'	NUM
eurjchem-782	37	51	3	3	NUM
eurjchem-782	37	52	'	'	NUM
eurjchem-782	37	53	4	4	NUM
eurjchem-782	37	54	'	'	NUM
eurjchem-782	37	55	5	5	NUM
eurjchem-782	37	56	'	'	NUM
eurjchem-782	37	57	6	6	NUM
eurjchem-782	37	58	'	'	NUM
eurjchem-782	37	59	1	1	NUM
eurjchem-782	37	60	''	''	SYM
eurjchem-782	37	61	2	2	NUM
eurjchem-782	37	62	''	''	SYM
eurjchem-782	37	63	3	3	NUM
eurjchem-782	37	64	''	''	PUNCT
eurjchem-782	37	65	4	4	NUM
eurjchem-782	37	66	''	''	SYM
eurjchem-782	37	67	5	5	NUM
eurjchem-782	37	68	''	''	PUNCT
eurjchem-782	37	69	6	6	NUM
eurjchem-782	37	70	''	''	SYM
eurjchem-782	37	71	2	2	NUM
eurjchem-782	37	72	3	3	NUM
eurjchem-782	37	73	1	1	NUM
eurjchem-782	37	74	1	1	NUM
eurjchem-782	37	75	'	'	NUM
eurjchem-782	37	76	2	2	NUM
eurjchem-782	37	77	'	'	PART
eurjchem-782	37	78	3'4	3'4	NUM
eurjchem-782	37	79	'	'	PART
eurjchem-782	37	80	5	5	NUM
eurjchem-782	37	81	'	'	NUM
eurjchem-782	37	82	6	6	NUM
eurjchem-782	37	83	'	'	NUM
eurjchem-782	37	84	1	1	NUM
eurjchem-782	37	85	''	''	SYM
eurjchem-782	37	86	2	2	NUM
eurjchem-782	37	87	''	''	SYM
eurjchem-782	37	88	3	3	NUM
eurjchem-782	37	89	''	''	PUNCT
eurjchem-782	37	90	4	4	NUM
eurjchem-782	37	91	''	''	SYM
eurjchem-782	37	92	5	5	NUM
eurjchem-782	37	93	''	''	PUNCT
eurjchem-782	37	94	6''4a	6''4a	NUM
eurjchem-782	37	95	1	1	NUM
eurjchem-782	37	96	2	2	NUM
eurjchem-782	37	97	3	3	NUM
eurjchem-782	37	98	4	4	NUM
eurjchem-782	37	99	8a	8a	NUM
eurjchem-782	37	100	5a	5a	NUM
eurjchem-782	37	101	5	5	NUM
eurjchem-782	37	102	6	6	NUM
eurjchem-782	37	103	7	7	NUM
eurjchem-782	37	104	8	8	NUM
eurjchem-782	37	105	1	1	NUM
eurjchem-782	37	106	'	'	PART
eurjchem-782	37	107	2	2	NUM
eurjchem-782	37	108	'	'	NUM
eurjchem-782	37	109	3	3	NUM
eurjchem-782	37	110	'	'	NUM
eurjchem-782	37	111	4	4	NUM
eurjchem-782	37	112	'	'	NUM
eurjchem-782	37	113	5	5	NUM
eurjchem-782	37	114	'	'	NUM
eurjchem-782	37	115	6	6	NUM
eurjchem-782	37	116	'	'	NUM
eurjchem-782	37	117	1	1	NUM
eurjchem-782	37	118	2	2	NUM
eurjchem-782	37	119	3	3	NUM
eurjchem-782	37	120	4	4	NUM
eurjchem-782	37	121	8a	8a	NUM
eurjchem-782	37	122	5a	5a	NUM
eurjchem-782	37	123	5	5	NUM
eurjchem-782	37	124	6	6	NUM
eurjchem-782	37	125	7	7	NUM
eurjchem-782	37	126	8	8	NUM
eurjchem-782	37	127	7	7	NUM
eurjchem-782	37	128	8	8	NUM
eurjchem-782	37	129	9	9	NUM
eurjchem-782	37	130	10	10	NUM
eurjchem-782	37	131	1	1	NUM
eurjchem-782	37	132	'	'	PART
eurjchem-782	37	133	2	2	NUM
eurjchem-782	37	134	'	'	NUM
eurjchem-782	37	135	3	3	NUM
eurjchem-782	37	136	'	'	NUM
eurjchem-782	37	137	4	4	NUM
eurjchem-782	37	138	'	'	NUM
eurjchem-782	37	139	5	5	NUM
eurjchem-782	37	140	'	'	NUM
eurjchem-782	37	141	6	6	NUM
eurjchem-782	37	142	'	'	NUM
eurjchem-782	37	143	8a	8a	NUM
eurjchem-782	37	144	5a	5a	NUM
eurjchem-782	37	145	5	5	NUM
eurjchem-782	37	146	6	6	NUM
eurjchem-782	37	147	7	7	NUM
eurjchem-782	37	148	8	8	NUM
eurjchem-782	37	149	1	1	NUM
eurjchem-782	37	150	2	2	NUM
eurjchem-782	37	151	3	3	NUM
eurjchem-782	37	152	4	4	NUM
eurjchem-782	37	153	9	9	NUM
eurjchem-782	37	154	1	1	NUM
eurjchem-782	37	155	'	'	PART
eurjchem-782	37	156	2	2	NUM
eurjchem-782	37	157	'	'	NUM
eurjchem-782	37	158	3	3	NUM
eurjchem-782	37	159	'	'	NUM
eurjchem-782	37	160	4	4	NUM
eurjchem-782	37	161	'	'	NUM
eurjchem-782	37	162	5	5	NUM
eurjchem-782	37	163	'	'	NUM
eurjchem-782	37	164	6	6	NUM
eurjchem-782	37	165	'	'	PUNCT
eurjchem-782	37	166	a	a	DET
eurjchem-782	37	167	b	b	NOUN
eurjchem-782	37	168	c	c	NOUN
eurjchem-782	37	169	a	a	DET
eurjchem-782	37	170	b	b	NOUN
eurjchem-782	37	171	c	c	NOUN
eurjchem-782	37	172	a	a	DET
eurjchem-782	37	173	b	b	NOUN
eurjchem-782	37	174	c	c	NOUN
eurjchem-782	37	175	a	a	PRON
eurjchem-782	37	176	b	b	NOUN
eurjchem-782	37	177	c	c	NOUN
eurjchem-782	37	178	d	d	PROPN
eurjchem-782	37	179	r1	r1	PROPN
eurjchem-782	37	180	h	h	PROPN
eurjchem-782	37	181	ch3	ch3	PROPN
eurjchem-782	37	182	och3	och3	PROPN
eurjchem-782	37	183	sch3	sch3	PROPN
eurjchem-782	37	184	r2	r2	PROPN
eurjchem-782	37	185	h	h	PROPN
eurjchem-782	37	186	h	h	NOUN
eurjchem-782	37	187	h	h	NOUN
eurjchem-782	38	1	h	h	PROPN
eurjchem-782	38	2	scheme	scheme	NOUN
eurjchem-782	38	3	1	1	NUM
eurjchem-782	38	4	(	(	PUNCT
eurjchem-782	38	5	e)‐1,3‐diphenyl‐2‐propen‐1‐one	e)‐1,3‐diphenyl‐2‐propen‐1‐one	NOUN
eurjchem-782	38	6	(	(	PUNCT
eurjchem-782	38	7	3a	3a	NUM
eurjchem-782	38	8	):	):	PUNCT
eurjchem-782	38	9	color	color	NOUN
eurjchem-782	38	10	:	:	PUNCT
eurjchem-782	38	11	light	light	ADJ
eurjchem-782	38	12	yellow	yellow	ADJ
eurjchem-782	38	13	solid	solid	ADJ
eurjchem-782	38	14	.	.	PUNCT
eurjchem-782	39	1	yield	yield	NOUN
eurjchem-782	39	2	:	:	PUNCT
eurjchem-782	39	3	89.32	89.32	NUM
eurjchem-782	39	4	%	%	NOUN
eurjchem-782	39	5	.	.	PUNCT
eurjchem-782	40	1	m.p	m.p	PROPN
eurjchem-782	40	2	.	.	PROPN
eurjchem-782	40	3	:	:	PUNCT
eurjchem-782	40	4	91‐93	91‐93	NUM
eurjchem-782	40	5	oc	oc	PROPN
eurjchem-782	40	6	.	.	PROPN
eurjchem-782	41	1	ir	ir	PROPN
eurjchem-782	41	2	(	(	PUNCT
eurjchem-782	41	3	kbr	kbr	PROPN
eurjchem-782	41	4	,	,	PUNCT
eurjchem-782	41	5	ν	ν	PROPN
eurjchem-782	41	6	,	,	PUNCT
eurjchem-782	41	7	cm‐1	cm‐1	PROPN
eurjchem-782	41	8	):	):	PUNCT
eurjchem-782	41	9	3091	3091	NUM
eurjchem-782	41	10	,	,	PUNCT
eurjchem-782	41	11	2973	2973	NUM
eurjchem-782	41	12	(	(	PUNCT
eurjchem-782	41	13	ar‐ch	ar‐ch	NUM
eurjchem-782	41	14	)	)	PUNCT
eurjchem-782	41	15	,	,	PUNCT
eurjchem-782	41	16	1663	1663	NUM
eurjchem-782	41	17	(	(	PUNCT
eurjchem-782	41	18	c	c	NOUN
eurjchem-782	41	19	=	=	NOUN
eurjchem-782	41	20	o	o	NOUN
eurjchem-782	41	21	)	)	PUNCT
eurjchem-782	41	22	,	,	PUNCT
eurjchem-782	41	23	1589	1589	NUM
eurjchem-782	41	24	(	(	PUNCT
eurjchem-782	41	25	c	c	NOUN
eurjchem-782	41	26	=	=	SYM
eurjchem-782	41	27	c	c	NOUN
eurjchem-782	41	28	)	)	PUNCT
eurjchem-782	41	29	.	.	PUNCT
eurjchem-782	42	1	1h	1h	NUM
eurjchem-782	42	2	nmr	nmr	NOUN
eurjchem-782	42	3	(	(	PUNCT
eurjchem-782	42	4	400	400	NUM
eurjchem-782	42	5	mhz	mhz	NOUN
eurjchem-782	42	6	,	,	PUNCT
eurjchem-782	42	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-782	42	8	,	,	PUNCT
eurjchem-782	42	9	δ	δ	PROPN
eurjchem-782	42	10	,	,	PUNCT
eurjchem-782	42	11	ppm	ppm	NUM
eurjchem-782	42	12	):	):	PUNCT
eurjchem-782	42	13	8.06	8.06	NUM
eurjchem-782	42	14	(	(	PUNCT
eurjchem-782	42	15	d	d	PROPN
eurjchem-782	42	16	,	,	PUNCT
eurjchem-782	42	17	1h	1h	NUM
eurjchem-782	42	18	,	,	PUNCT
eurjchem-782	42	19	j	j	PROPN
eurjchem-782	42	20	=	=	PROPN
eurjchem-782	42	21	8.3	8.3	NUM
eurjchem-782	42	22	hz	hz	NOUN
eurjchem-782	42	23	,	,	PUNCT
eurjchem-782	42	24	β‐ch	β‐ch	NOUN
eurjchem-782	42	25	)	)	PUNCT
eurjchem-782	42	26	,	,	PUNCT
eurjchem-782	42	27	7.89‐7.30	7.89‐7.30	NUM
eurjchem-782	42	28	(	(	PUNCT
eurjchem-782	42	29	m	m	PROPN
eurjchem-782	42	30	,	,	PUNCT
eurjchem-782	42	31	10h	10h	NUM
eurjchem-782	42	32	,	,	PUNCT
eurjchem-782	42	33	ar‐h	ar‐h	NOUN
eurjchem-782	42	34	)	)	PUNCT
eurjchem-782	42	35	,	,	PUNCT
eurjchem-782	42	36	7.55	7.55	NUM
eurjchem-782	42	37	(	(	PUNCT
eurjchem-782	42	38	d	d	PROPN
eurjchem-782	42	39	,	,	PUNCT
eurjchem-782	42	40	1h	1h	NUM
eurjchem-782	42	41	,	,	PUNCT
eurjchem-782	42	42	j	j	PROPN
eurjchem-782	42	43	=	=	SYM
eurjchem-782	42	44	8.0	8.0	NUM
eurjchem-782	42	45	hz	hz	NOUN
eurjchem-782	42	46	,	,	PUNCT
eurjchem-782	42	47	α‐ch	α‐ch	PROPN
eurjchem-782	42	48	)	)	PUNCT
eurjchem-782	42	49	.	.	PUNCT
eurjchem-782	43	1	13c	13c	NOUN
eurjchem-782	43	2	nmr	nmr	NOUN
eurjchem-782	43	3	(	(	PUNCT
eurjchem-782	43	4	100	100	NUM
eurjchem-782	43	5	mhz	mhz	NOUN
eurjchem-782	43	6	,	,	PUNCT
eurjchem-782	43	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-782	43	8	,	,	PUNCT
eurjchem-782	43	9	δ	δ	PROPN
eurjchem-782	43	10	,	,	PUNCT
eurjchem-782	43	11	ppm	ppm	NUM
eurjchem-782	43	12	):	):	PUNCT
eurjchem-782	43	13	189.5	189.5	NUM
eurjchem-782	43	14	(	(	PUNCT
eurjchem-782	43	15	c‐1	c‐1	NOUN
eurjchem-782	43	16	)	)	PUNCT
eurjchem-782	43	17	,	,	PUNCT
eurjchem-782	43	18	145.0	145.0	NUM
eurjchem-782	43	19	(	(	PUNCT
eurjchem-782	43	20	c‐3	c‐3	NOUN
eurjchem-782	43	21	)	)	PUNCT
eurjchem-782	43	22	,	,	PUNCT
eurjchem-782	43	23	137.8	137.8	NUM
eurjchem-782	43	24	(	(	PUNCT
eurjchem-782	43	25	c‐1	c‐1	NOUN
eurjchem-782	43	26	'	'	PUNCT
eurjchem-782	43	27	)	)	PUNCT
eurjchem-782	43	28	,	,	PUNCT
eurjchem-782	43	29	135.4	135.4	NUM
eurjchem-782	43	30	(	(	PUNCT
eurjchem-782	43	31	c‐1	c‐1	NOUN
eurjchem-782	43	32	"	"	PUNCT
eurjchem-782	43	33	)	)	PUNCT
eurjchem-782	43	34	,	,	PUNCT
eurjchem-782	43	35	134.7	134.7	NUM
eurjchem-782	43	36	(	(	PUNCT
eurjchem-782	43	37	c‐4	c‐4	PROPN
eurjchem-782	43	38	'	'	PUNCT
eurjchem-782	43	39	)	)	PUNCT
eurjchem-782	43	40	,	,	PUNCT
eurjchem-782	43	41	129.2	129.2	NUM
eurjchem-782	43	42	(	(	PUNCT
eurjchem-782	43	43	c‐3	c‐3	NOUN
eurjchem-782	43	44	'	'	PUNCT
eurjchem-782	43	45	,	,	PUNCT
eurjchem-782	43	46	c‐5	c‐5	NOUN
eurjchem-782	43	47	'	'	PUNCT
eurjchem-782	43	48	)	)	PUNCT
eurjchem-782	43	49	,	,	PUNCT
eurjchem-782	43	50	128.6	128.6	NUM
eurjchem-782	43	51	(	(	PUNCT
eurjchem-782	43	52	c‐3	c‐3	NOUN
eurjchem-782	43	53	"	"	PUNCT
eurjchem-782	43	54	,	,	PUNCT
eurjchem-782	43	55	c‐5	c‐5	NOUN
eurjchem-782	43	56	"	"	PUNCT
eurjchem-782	43	57	)	)	PUNCT
eurjchem-782	43	58	,	,	PUNCT
eurjchem-782	43	59	128.1	128.1	NUM
eurjchem-782	43	60	(	(	PUNCT
eurjchem-782	43	61	c‐2	c‐2	NOUN
eurjchem-782	43	62	'	'	PUNCT
eurjchem-782	43	63	,	,	PUNCT
eurjchem-782	43	64	c‐6	c‐6	NOUN
eurjchem-782	43	65	'	'	NOUN
eurjchem-782	43	66	,	,	PUNCT
eurjchem-782	43	67	c‐2	c‐2	NOUN
eurjchem-782	43	68	"	"	PUNCT
eurjchem-782	43	69	,	,	PUNCT
eurjchem-782	43	70	c‐6	c‐6	NOUN
eurjchem-782	43	71	"	"	PUNCT
eurjchem-782	43	72	)	)	PUNCT
eurjchem-782	43	73	,	,	PUNCT
eurjchem-782	43	74	127.5	127.5	NUM
eurjchem-782	43	75	(	(	PUNCT
eurjchem-782	43	76	c‐4	c‐4	PROPN
eurjchem-782	43	77	"	"	PUNCT
eurjchem-782	43	78	)	)	PUNCT
eurjchem-782	43	79	,	,	PUNCT
eurjchem-782	43	80	121.3	121.3	NUM
eurjchem-782	43	81	(	(	PUNCT
eurjchem-782	43	82	c‐2	c‐2	NOUN
eurjchem-782	43	83	)	)	PUNCT
eurjchem-782	43	84	.	.	PUNCT
eurjchem-782	44	1	ms	ms	PROPN
eurjchem-782	44	2	(	(	PUNCT
eurjchem-782	44	3	esi	esi	PROPN
eurjchem-782	44	4	,	,	PUNCT
eurjchem-782	44	5	m	m	PROPN
eurjchem-782	44	6	/	/	SYM
eurjchem-782	44	7	z	z	NOUN
eurjchem-782	44	8	):	):	PUNCT
eurjchem-782	44	9	208.08	208.08	NUM
eurjchem-782	44	10	(	(	PUNCT
eurjchem-782	44	11	m+	m+	NUM
eurjchem-782	44	12	)	)	PUNCT
eurjchem-782	44	13	.	.	PUNCT
eurjchem-782	45	1	anal	anal	PROPN
eurjchem-782	45	2	.	.	PUNCT
eurjchem-782	45	3	calcd	calcd	NOUN
eurjchem-782	45	4	.	.	PUNCT
eurjchem-782	46	1	for	for	ADP
eurjchem-782	46	2	c15h12o	c15h12o	PROPN
eurjchem-782	46	3	:	:	PUNCT
eurjchem-782	46	4	c	c	X
eurjchem-782	46	5	,	,	PUNCT
eurjchem-782	46	6	86.51	86.51	NUM
eurjchem-782	46	7	;	;	PUNCT
eurjchem-782	46	8	h	h	NOUN
eurjchem-782	46	9	,	,	PUNCT
eurjchem-782	46	10	5.81	5.81	NUM
eurjchem-782	46	11	.	.	PUNCT
eurjchem-782	46	12	found	find	VERB
eurjchem-782	46	13	:	:	PUNCT
eurjchem-782	47	1	c	c	X
eurjchem-782	47	2	,	,	PUNCT
eurjchem-782	47	3	86.48	86.48	NUM
eurjchem-782	47	4	;	;	PUNCT
eurjchem-782	47	5	h	h	X
eurjchem-782	47	6	,	,	PUNCT
eurjchem-782	47	7	5.85	5.85	NUM
eurjchem-782	47	8	%	%	NOUN
eurjchem-782	47	9	.	.	PUNCT
eurjchem-782	48	1	(	(	PUNCT
eurjchem-782	48	2	e)‐3‐phenyl‐1‐p‐tolylprop‐2‐en‐1‐one	e)‐3‐phenyl‐1‐p‐tolylprop‐2‐en‐1‐one	X
eurjchem-782	48	3	(	(	PUNCT
eurjchem-782	48	4	3b	3b	NUM
eurjchem-782	48	5	):	):	PUNCT
eurjchem-782	48	6	color	color	NOUN
eurjchem-782	48	7	:	:	PUNCT
eurjchem-782	48	8	light	light	ADJ
eurjchem-782	48	9	yellow	yellow	ADJ
eurjchem-782	48	10	solid	solid	ADJ
eurjchem-782	48	11	.	.	PUNCT
eurjchem-782	48	12	yield	yield	NOUN
eurjchem-782	48	13	:	:	PUNCT
eurjchem-782	48	14	66.35	66.35	NUM
eurjchem-782	48	15	%	%	NOUN
eurjchem-782	48	16	.	.	PUNCT
eurjchem-782	49	1	m.p	m.p	PROPN
eurjchem-782	49	2	.	.	PROPN
eurjchem-782	49	3	:	:	PUNCT
eurjchem-782	50	1	110‐112	110‐112	NUM
eurjchem-782	50	2	oc	oc	PROPN
eurjchem-782	50	3	.	.	PROPN
eurjchem-782	50	4	ir	ir	PROPN
eurjchem-782	50	5	(	(	PUNCT
eurjchem-782	50	6	kbr	kbr	PROPN
eurjchem-782	50	7	,	,	PUNCT
eurjchem-782	50	8	ν	ν	PROPN
eurjchem-782	50	9	,	,	PUNCT
eurjchem-782	50	10	cm‐1	cm‐1	PROPN
eurjchem-782	50	11	):	):	PUNCT
eurjchem-782	50	12	3128	3128	NUM
eurjchem-782	50	13	,	,	PUNCT
eurjchem-782	50	14	2965	2965	NUM
eurjchem-782	50	15	(	(	PUNCT
eurjchem-782	50	16	ar‐ch	ar‐ch	NUM
eurjchem-782	50	17	)	)	PUNCT
eurjchem-782	50	18	,	,	PUNCT
eurjchem-782	50	19	1670	1670	NUM
eurjchem-782	50	20	(	(	PUNCT
eurjchem-782	50	21	c	c	NOUN
eurjchem-782	50	22	=	=	NOUN
eurjchem-782	50	23	o	o	NOUN
eurjchem-782	50	24	)	)	PUNCT
eurjchem-782	50	25	,	,	PUNCT
eurjchem-782	50	26	1603	1603	NUM
eurjchem-782	50	27	(	(	PUNCT
eurjchem-782	50	28	c	c	NOUN
eurjchem-782	50	29	=	=	SYM
eurjchem-782	50	30	c	c	NOUN
eurjchem-782	50	31	)	)	PUNCT
eurjchem-782	50	32	.	.	PUNCT
eurjchem-782	51	1	1h	1h	NUM
eurjchem-782	51	2	nmr	nmr	NOUN
eurjchem-782	51	3	(	(	PUNCT
eurjchem-782	51	4	400	400	NUM
eurjchem-782	51	5	mhz	mhz	NOUN
eurjchem-782	51	6	,	,	PUNCT
eurjchem-782	51	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-782	51	8	,	,	PUNCT
eurjchem-782	51	9	δ	δ	PROPN
eurjchem-782	51	10	,	,	PUNCT
eurjchem-782	51	11	ppm	ppm	NUM
eurjchem-782	51	12	):	):	PUNCT
eurjchem-782	51	13	8.10	8.10	NUM
eurjchem-782	51	14	(	(	PUNCT
eurjchem-782	51	15	d	d	PROPN
eurjchem-782	51	16	,	,	PUNCT
eurjchem-782	51	17	1h	1h	NUM
eurjchem-782	51	18	,	,	PUNCT
eurjchem-782	51	19	j	j	PROPN
eurjchem-782	51	20	=	=	SYM
eurjchem-782	51	21	8.0	8.0	NUM
eurjchem-782	51	22	hz	hz	NOUN
eurjchem-782	51	23	,	,	PUNCT
eurjchem-782	51	24	β‐ch	β‐ch	NOUN
eurjchem-782	51	25	)	)	PUNCT
eurjchem-782	51	26	,	,	PUNCT
eurjchem-782	51	27	7.84‐7.33	7.84‐7.33	NUM
eurjchem-782	51	28	(	(	PUNCT
eurjchem-782	51	29	m	m	PROPN
eurjchem-782	51	30	,	,	PUNCT
eurjchem-782	51	31	9h	9h	NUM
eurjchem-782	51	32	,	,	PUNCT
eurjchem-782	51	33	ar‐h	ar‐h	NOUN
eurjchem-782	51	34	)	)	PUNCT
eurjchem-782	51	35	,	,	PUNCT
eurjchem-782	51	36	7.58	7.58	NUM
eurjchem-782	51	37	(	(	PUNCT
eurjchem-782	51	38	d	d	PROPN
eurjchem-782	51	39	,	,	PUNCT
eurjchem-782	51	40	1h	1h	NUM
eurjchem-782	51	41	,	,	PUNCT
eurjchem-782	51	42	j	j	PROPN
eurjchem-782	51	43	=	=	SYM
eurjchem-782	51	44	8.0	8.0	NUM
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eurjchem-782	51	46	,	,	PUNCT
eurjchem-782	51	47	α‐ch	α‐ch	PROPN
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eurjchem-782	51	49	,	,	PUNCT
eurjchem-782	51	50	2.34	2.34	NUM
eurjchem-782	51	51	(	(	PUNCT
eurjchem-782	51	52	s	s	PROPN
eurjchem-782	51	53	,	,	PUNCT
eurjchem-782	51	54	3h	3h	NUM
eurjchem-782	51	55	,	,	PUNCT
eurjchem-782	51	56	ch3	ch3	PROPN
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eurjchem-782	51	58	.	.	PUNCT
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eurjchem-782	52	2	nmr	nmr	NOUN
eurjchem-782	52	3	(	(	PUNCT
eurjchem-782	52	4	100	100	NUM
eurjchem-782	52	5	mhz	mhz	NOUN
eurjchem-782	52	6	,	,	PUNCT
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eurjchem-782	52	8	,	,	PUNCT
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eurjchem-782	52	10	,	,	PUNCT
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eurjchem-782	52	12	):	):	PUNCT
eurjchem-782	52	13	189.5	189.5	NUM
eurjchem-782	52	14	(	(	PUNCT
eurjchem-782	52	15	c‐1	c‐1	NOUN
eurjchem-782	52	16	)	)	PUNCT
eurjchem-782	52	17	,	,	PUNCT
eurjchem-782	52	18	145.3	145.3	NUM
eurjchem-782	52	19	(	(	PUNCT
eurjchem-782	52	20	c‐3	c‐3	NOUN
eurjchem-782	52	21	)	)	PUNCT
eurjchem-782	52	22	,	,	PUNCT
eurjchem-782	52	23	144.0	144.0	NUM
eurjchem-782	52	24	(	(	PUNCT
eurjchem-782	52	25	c‐4	c‐4	PROPN
eurjchem-782	52	26	'	'	PUNCT
eurjchem-782	52	27	)	)	PUNCT
eurjchem-782	52	28	,	,	PUNCT
eurjchem-782	52	29	135.2	135.2	NUM
eurjchem-782	52	30	(	(	PUNCT
eurjchem-782	52	31	c‐1	c‐1	NOUN
eurjchem-782	52	32	"	"	PUNCT
eurjchem-782	52	33	)	)	PUNCT
eurjchem-782	52	34	,	,	PUNCT
eurjchem-782	52	35	134.8	134.8	NUM
eurjchem-782	52	36	(	(	PUNCT
eurjchem-782	52	37	c‐1	c‐1	NOUN
eurjchem-782	52	38	'	'	PUNCT
eurjchem-782	52	39	)	)	PUNCT
eurjchem-782	52	40	,	,	PUNCT
eurjchem-782	52	41	129.8	129.8	NUM
eurjchem-782	52	42	(	(	PUNCT
eurjchem-782	52	43	c‐2	c‐2	NOUN
eurjchem-782	52	44	'	'	PUNCT
eurjchem-782	52	45	,	,	PUNCT
eurjchem-782	52	46	c‐6	c‐6	NOUN
eurjchem-782	52	47	'	'	PUNCT
eurjchem-782	52	48	)	)	PUNCT
eurjchem-782	52	49	,	,	PUNCT
eurjchem-782	52	50	129.5	129.5	NUM
eurjchem-782	52	51	(	(	PUNCT
eurjchem-782	52	52	c‐3	c‐3	NOUN
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eurjchem-782	52	54	,	,	PUNCT
eurjchem-782	52	55	c‐5	c‐5	NOUN
eurjchem-782	52	56	'	'	PUNCT
eurjchem-782	52	57	)	)	PUNCT
eurjchem-782	52	58	,	,	PUNCT
eurjchem-782	52	59	128.4	128.4	NUM
eurjchem-782	52	60	(	(	PUNCT
eurjchem-782	52	61	c‐3	c‐3	NOUN
eurjchem-782	52	62	"	"	PUNCT
eurjchem-782	52	63	,	,	PUNCT
eurjchem-782	52	64	c‐5	c‐5	NOUN
eurjchem-782	52	65	"	"	PUNCT
eurjchem-782	52	66	)	)	PUNCT
eurjchem-782	52	67	,	,	PUNCT
eurjchem-782	52	68	128.0	128.0	NUM
eurjchem-782	52	69	(	(	PUNCT
eurjchem-782	52	70	c‐2	c‐2	NOUN
eurjchem-782	52	71	"	"	PUNCT
eurjchem-782	52	72	,	,	PUNCT
eurjchem-782	52	73	c‐6	c‐6	NOUN
eurjchem-782	52	74	"	"	PUNCT
eurjchem-782	52	75	)	)	PUNCT
eurjchem-782	52	76	,	,	PUNCT
eurjchem-782	52	77	127.9	127.9	NUM
eurjchem-782	52	78	(	(	PUNCT
eurjchem-782	52	79	c‐4	c‐4	PROPN
eurjchem-782	52	80	"	"	PUNCT
eurjchem-782	52	81	)	)	PUNCT
eurjchem-782	52	82	,	,	PUNCT
eurjchem-782	52	83	121.3	121.3	NUM
eurjchem-782	52	84	(	(	PUNCT
eurjchem-782	52	85	c‐2	c‐2	NOUN
eurjchem-782	52	86	)	)	PUNCT
eurjchem-782	52	87	,	,	PUNCT
eurjchem-782	52	88	21.2	21.2	NUM
eurjchem-782	52	89	(	(	PUNCT
eurjchem-782	52	90	‐ch3	‐ch3	ADJ
eurjchem-782	52	91	)	)	PUNCT
eurjchem-782	52	92	.	.	PUNCT
eurjchem-782	53	1	ms	ms	PROPN
eurjchem-782	53	2	(	(	PUNCT
eurjchem-782	53	3	esi	esi	PROPN
eurjchem-782	53	4	,	,	PUNCT
eurjchem-782	53	5	m	m	PROPN
eurjchem-782	53	6	/	/	SYM
eurjchem-782	53	7	z	z	NOUN
eurjchem-782	53	8	):	):	PUNCT
eurjchem-782	53	9	222.10	222.10	NUM
eurjchem-782	53	10	(	(	PUNCT
eurjchem-782	53	11	m+	m+	NUM
eurjchem-782	53	12	)	)	PUNCT
eurjchem-782	53	13	.	.	PUNCT
eurjchem-782	54	1	anal	anal	PROPN
eurjchem-782	54	2	.	.	PUNCT
eurjchem-782	54	3	calcd	calcd	NOUN
eurjchem-782	54	4	.	.	PUNCT
eurjchem-782	55	1	for	for	ADP
eurjchem-782	55	2	c16h14o	c16h14o	NUM
eurjchem-782	55	3	:	:	PUNCT
eurjchem-782	55	4	c	c	X
eurjchem-782	55	5	,	,	PUNCT
eurjchem-782	55	6	86.45	86.45	NUM
eurjchem-782	55	7	;	;	PUNCT
eurjchem-782	55	8	h	h	NOUN
eurjchem-782	55	9	,	,	PUNCT
eurjchem-782	55	10	6.35	6.35	NUM
eurjchem-782	55	11	.	.	PUNCT
eurjchem-782	55	12	found	find	VERB
eurjchem-782	55	13	:	:	PUNCT
eurjchem-782	56	1	c	c	X
eurjchem-782	56	2	,	,	PUNCT
eurjchem-782	56	3	86.42	86.42	NUM
eurjchem-782	56	4	;	;	PUNCT
eurjchem-782	56	5	h	h	NOUN
eurjchem-782	56	6	,	,	PUNCT
eurjchem-782	56	7	6.33	6.33	NUM
eurjchem-782	56	8	%	%	NOUN
eurjchem-782	56	9	.	.	PUNCT
eurjchem-782	57	1	(	(	PUNCT
eurjchem-782	57	2	e)‐1‐(4‐methoxyphenyl)‐3‐phenylprop‐2‐en‐1‐one	e)‐1‐(4‐methoxyphenyl)‐3‐phenylprop‐2‐en‐1‐one	NOUN
eurjchem-782	57	3	(	(	PUNCT
eurjchem-782	57	4	3c	3c	NUM
eurjchem-782	57	5	):	):	PUNCT
eurjchem-782	57	6	color	color	NOUN
eurjchem-782	57	7	:	:	PUNCT
eurjchem-782	57	8	light	light	ADJ
eurjchem-782	57	9	yellow	yellow	ADJ
eurjchem-782	57	10	solid	solid	ADJ
eurjchem-782	57	11	.	.	PUNCT
eurjchem-782	57	12	yield	yield	NOUN
eurjchem-782	57	13	:	:	PUNCT
eurjchem-782	57	14	71.88	71.88	NUM
eurjchem-782	57	15	%	%	NOUN
eurjchem-782	57	16	.	.	PUNCT
eurjchem-782	58	1	m.p	m.p	PROPN
eurjchem-782	58	2	.	.	PROPN
eurjchem-782	58	3	:	:	PUNCT
eurjchem-782	59	1	128‐130	128‐130	PROPN
eurjchem-782	59	2	oc	oc	PROPN
eurjchem-782	59	3	.	.	PROPN
eurjchem-782	59	4	ir	ir	PROPN
eurjchem-782	59	5	(	(	PUNCT
eurjchem-782	59	6	kbr	kbr	PROPN
eurjchem-782	59	7	,	,	PUNCT
eurjchem-782	59	8	ν	ν	PROPN
eurjchem-782	59	9	,	,	PUNCT
eurjchem-782	59	10	cm‐1	cm‐1	PROPN
eurjchem-782	59	11	):	):	PUNCT
eurjchem-782	59	12	3135	3135	NUM
eurjchem-782	59	13	,	,	PUNCT
eurjchem-782	59	14	2973	2973	NUM
eurjchem-782	59	15	(	(	PUNCT
eurjchem-782	59	16	ar‐ch	ar‐ch	NUM
eurjchem-782	59	17	)	)	PUNCT
eurjchem-782	59	18	,	,	PUNCT
eurjchem-782	59	19	1667	1667	NUM
eurjchem-782	59	20	(	(	PUNCT
eurjchem-782	59	21	c	c	NOUN
eurjchem-782	59	22	=	=	NOUN
eurjchem-782	59	23	o	o	NOUN
eurjchem-782	59	24	)	)	PUNCT
eurjchem-782	59	25	,	,	PUNCT
eurjchem-782	59	26	1588	1588	NUM
eurjchem-782	59	27	(	(	PUNCT
eurjchem-782	59	28	c	c	NOUN
eurjchem-782	59	29	=	=	SYM
eurjchem-782	59	30	c	c	NOUN
eurjchem-782	59	31	)	)	PUNCT
eurjchem-782	59	32	.	.	PUNCT
eurjchem-782	60	1	1h	1h	NUM
eurjchem-782	60	2	nmr	nmr	NOUN
eurjchem-782	60	3	(	(	PUNCT
eurjchem-782	60	4	400	400	NUM
eurjchem-782	60	5	mhz	mhz	NOUN
eurjchem-782	60	6	,	,	PUNCT
eurjchem-782	60	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-782	60	8	,	,	PUNCT
eurjchem-782	60	9	δ	δ	PROPN
eurjchem-782	60	10	,	,	PUNCT
eurjchem-782	60	11	ppm	ppm	NUM
eurjchem-782	60	12	):	):	PUNCT
eurjchem-782	60	13	8.09	8.09	NUM
eurjchem-782	60	14	(	(	PUNCT
eurjchem-782	60	15	d	d	PROPN
eurjchem-782	60	16	,	,	PUNCT
eurjchem-782	60	17	1h	1h	NUM
eurjchem-782	60	18	,	,	PUNCT
eurjchem-782	60	19	j	j	PROPN
eurjchem-782	60	20	=	=	SYM
eurjchem-782	60	21	7.5	7.5	NUM
eurjchem-782	60	22	hz	hz	ADJ
eurjchem-782	60	23	,	,	PUNCT
eurjchem-782	60	24	β‐	β‐	ADJ
eurjchem-782	60	25	ch	ch	NOUN
eurjchem-782	60	26	)	)	PUNCT
eurjchem-782	60	27	,	,	PUNCT
eurjchem-782	60	28	7.88‐7.28	7.88‐7.28	NUM
eurjchem-782	60	29	(	(	PUNCT
eurjchem-782	60	30	m	m	PROPN
eurjchem-782	60	31	,	,	PUNCT
eurjchem-782	60	32	9h	9h	NUM
eurjchem-782	60	33	,	,	PUNCT
eurjchem-782	60	34	ar‐h	ar‐h	NOUN
eurjchem-782	60	35	)	)	PUNCT
eurjchem-782	60	36	,	,	PUNCT
eurjchem-782	60	37	7.61	7.61	NUM
eurjchem-782	60	38	(	(	PUNCT
eurjchem-782	60	39	d	d	PROPN
eurjchem-782	60	40	,	,	PUNCT
eurjchem-782	60	41	1h	1h	NUM
eurjchem-782	60	42	,	,	PUNCT
eurjchem-782	60	43	j	j	PROPN
eurjchem-782	60	44	=	=	SYM
eurjchem-782	60	45	7.9	7.9	NUM
eurjchem-782	60	46	hz	hz	NOUN
eurjchem-782	60	47	,	,	PUNCT
eurjchem-782	60	48	α‐ch	α‐ch	PROPN
eurjchem-782	60	49	)	)	PUNCT
eurjchem-782	60	50	,	,	PUNCT
eurjchem-782	60	51	3.83	3.83	NUM
eurjchem-782	60	52	(	(	PUNCT
eurjchem-782	60	53	s	s	PROPN
eurjchem-782	60	54	,	,	PUNCT
eurjchem-782	60	55	3h	3h	NUM
eurjchem-782	60	56	,	,	PUNCT
eurjchem-782	60	57	och3	och3	ADJ
eurjchem-782	60	58	)	)	PUNCT
eurjchem-782	60	59	.	.	PUNCT
eurjchem-782	61	1	13c	13c	NOUN
eurjchem-782	61	2	nmr	nmr	NOUN
eurjchem-782	61	3	(	(	PUNCT
eurjchem-782	61	4	100	100	NUM
eurjchem-782	61	5	mhz	mhz	NOUN
eurjchem-782	61	6	,	,	PUNCT
eurjchem-782	61	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-782	61	8	,	,	PUNCT
eurjchem-782	61	9	δ	δ	PROPN
eurjchem-782	61	10	,	,	PUNCT
eurjchem-782	61	11	ppm	ppm	NUM
eurjchem-782	61	12	):	):	PUNCT
eurjchem-782	61	13	189.3	189.3	NUM
eurjchem-782	61	14	(	(	PUNCT
eurjchem-782	61	15	c‐	c‐	NOUN
eurjchem-782	61	16	1	1	NUM
eurjchem-782	61	17	)	)	PUNCT
eurjchem-782	61	18	,	,	PUNCT
eurjchem-782	61	19	166.4	166.4	NUM
eurjchem-782	61	20	(	(	PUNCT
eurjchem-782	61	21	c‐4	c‐4	PROPN
eurjchem-782	61	22	'	'	PUNCT
eurjchem-782	61	23	)	)	PUNCT
eurjchem-782	61	24	,	,	PUNCT
eurjchem-782	61	25	145.6	145.6	NUM
eurjchem-782	61	26	(	(	PUNCT
eurjchem-782	61	27	c‐3	c‐3	NOUN
eurjchem-782	61	28	)	)	PUNCT
eurjchem-782	61	29	,	,	PUNCT
eurjchem-782	61	30	135.2	135.2	NUM
eurjchem-782	61	31	(	(	PUNCT
eurjchem-782	61	32	c‐1	c‐1	NOUN
eurjchem-782	61	33	"	"	PUNCT
eurjchem-782	61	34	)	)	PUNCT
eurjchem-782	61	35	,	,	PUNCT
eurjchem-782	61	36	131.0	131.0	NUM
eurjchem-782	61	37	(	(	PUNCT
eurjchem-782	61	38	c‐2	c‐2	NOUN
eurjchem-782	61	39	'	'	PUNCT
eurjchem-782	61	40	,	,	PUNCT
eurjchem-782	61	41	c‐6	c‐6	NOUN
eurjchem-782	61	42	'	'	PUNCT
eurjchem-782	61	43	)	)	PUNCT
eurjchem-782	61	44	,	,	PUNCT
eurjchem-782	61	45	130.2	130.2	NUM
eurjchem-782	61	46	(	(	PUNCT
eurjchem-782	61	47	c‐1	c‐1	NOUN
eurjchem-782	61	48	'	'	PUNCT
eurjchem-782	61	49	)	)	PUNCT
eurjchem-782	61	50	,	,	PUNCT
eurjchem-782	61	51	128.5	128.5	NUM
eurjchem-782	61	52	(	(	PUNCT
eurjchem-782	61	53	c‐3	c‐3	NOUN
eurjchem-782	61	54	"	"	PUNCT
eurjchem-782	61	55	,	,	PUNCT
eurjchem-782	61	56	c‐5	c‐5	NOUN
eurjchem-782	61	57	"	"	PUNCT
eurjchem-782	61	58	)	)	PUNCT
eurjchem-782	61	59	,	,	PUNCT
eurjchem-782	61	60	128.2	128.2	NUM
eurjchem-782	61	61	(	(	PUNCT
eurjchem-782	61	62	c‐2	c‐2	NOUN
eurjchem-782	61	63	"	"	PUNCT
eurjchem-782	61	64	,	,	PUNCT
eurjchem-782	61	65	c‐6	c‐6	NOUN
eurjchem-782	61	66	"	"	PUNCT
eurjchem-782	61	67	)	)	PUNCT
eurjchem-782	61	68	,	,	PUNCT
eurjchem-782	61	69	127.8	127.8	NUM
eurjchem-782	61	70	(	(	PUNCT
eurjchem-782	61	71	c‐4	c‐4	PROPN
eurjchem-782	61	72	"	"	PUNCT
eurjchem-782	61	73	)	)	PUNCT
eurjchem-782	61	74	,	,	PUNCT
eurjchem-782	61	75	121.3	121.3	NUM
eurjchem-782	61	76	(	(	PUNCT
eurjchem-782	61	77	c‐2	c‐2	NOUN
eurjchem-782	61	78	)	)	PUNCT
eurjchem-782	61	79	,	,	PUNCT
eurjchem-782	61	80	114.8	114.8	NUM
eurjchem-782	61	81	(	(	PUNCT
eurjchem-782	61	82	c‐3	c‐3	NOUN
eurjchem-782	61	83	'	'	PUNCT
eurjchem-782	61	84	,	,	PUNCT
eurjchem-782	61	85	c‐5	c‐5	NOUN
eurjchem-782	61	86	'	'	PUNCT
eurjchem-782	61	87	)	)	PUNCT
eurjchem-782	61	88	,	,	PUNCT
eurjchem-782	61	89	55.8	55.8	NUM
eurjchem-782	61	90	(	(	PUNCT
eurjchem-782	61	91	‐och3	‐och3	NOUN
eurjchem-782	61	92	)	)	PUNCT
eurjchem-782	61	93	.	.	PUNCT
eurjchem-782	62	1	ms	ms	PROPN
eurjchem-782	62	2	(	(	PUNCT
eurjchem-782	62	3	esi	esi	PROPN
eurjchem-782	62	4	,	,	PUNCT
eurjchem-782	62	5	m	m	PROPN
eurjchem-782	62	6	/	/	SYM
eurjchem-782	62	7	z	z	NOUN
eurjchem-782	62	8	):	):	PUNCT
eurjchem-782	62	9	238.10	238.10	NUM
eurjchem-782	62	10	(	(	PUNCT
eurjchem-782	62	11	m+	m+	NUM
eurjchem-782	62	12	)	)	PUNCT
eurjchem-782	62	13	.	.	PUNCT
eurjchem-782	63	1	anal	anal	PROPN
eurjchem-782	63	2	.	.	PUNCT
eurjchem-782	63	3	calcd	calcd	NOUN
eurjchem-782	63	4	.	.	PUNCT
eurjchem-782	64	1	for	for	ADP
eurjchem-782	64	2	c16h14o2	c16h14o2	PROPN
eurjchem-782	64	3	:	:	PUNCT
eurjchem-782	64	4	c	c	NOUN
eurjchem-782	64	5	,	,	PUNCT
eurjchem-782	64	6	80.65	80.65	NUM
eurjchem-782	64	7	;	;	PUNCT
eurjchem-782	64	8	h	h	NOUN
eurjchem-782	64	9	,	,	PUNCT
eurjchem-782	64	10	5.92	5.92	NUM
eurjchem-782	64	11	.	.	PUNCT
eurjchem-782	64	12	found	find	VERB
eurjchem-782	64	13	:	:	PUNCT
eurjchem-782	65	1	c	c	X
eurjchem-782	65	2	,	,	PUNCT
eurjchem-782	65	3	80.62	80.62	NUM
eurjchem-782	65	4	;	;	PUNCT
eurjchem-782	65	5	h	h	NOUN
eurjchem-782	65	6	,	,	PUNCT
eurjchem-782	65	7	5.88	5.88	NUM
eurjchem-782	65	8	%	%	NOUN
eurjchem-782	65	9	.	.	PUNCT
eurjchem-782	66	1	(	(	PUNCT
eurjchem-782	66	2	e)‐1‐(4‐(methylthio)phenyl)‐3‐phenylprop‐2‐en‐1‐one	e)‐1‐(4‐(methylthio)phenyl)‐3‐phenylprop‐2‐en‐1‐one	NOUN
eurjchem-782	66	3	(	(	PUNCT
eurjchem-782	66	4	3d	3d	NOUN
eurjchem-782	66	5	):	):	PUNCT
eurjchem-782	66	6	color	color	NOUN
eurjchem-782	66	7	:	:	PUNCT
eurjchem-782	66	8	light	light	ADJ
eurjchem-782	66	9	yellow	yellow	ADJ
eurjchem-782	66	10	solid	solid	ADJ
eurjchem-782	66	11	.	.	PUNCT
eurjchem-782	67	1	yield	yield	NOUN
eurjchem-782	67	2	:	:	PUNCT
eurjchem-782	67	3	73.50	73.50	NUM
eurjchem-782	67	4	%	%	NOUN
eurjchem-782	67	5	.	.	PUNCT
eurjchem-782	68	1	m.p	m.p	PROPN
eurjchem-782	68	2	.	.	PROPN
eurjchem-782	68	3	:	:	PUNCT
eurjchem-782	68	4	95‐97	95‐97	NUM
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eurjchem-782	68	6	.	.	PUNCT
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eurjchem-782	69	2	(	(	PUNCT
eurjchem-782	69	3	kbr	kbr	PROPN
eurjchem-782	69	4	,	,	PUNCT
eurjchem-782	69	5	ν	ν	PROPN
eurjchem-782	69	6	,	,	PUNCT
eurjchem-782	69	7	cm‐1	cm‐1	PROPN
eurjchem-782	69	8	):	):	PUNCT
eurjchem-782	69	9	3142	3142	NUM
eurjchem-782	69	10	,	,	PUNCT
eurjchem-782	69	11	2985	2985	NUM
eurjchem-782	69	12	(	(	PUNCT
eurjchem-782	69	13	ar‐ch	ar‐ch	NUM
eurjchem-782	69	14	)	)	PUNCT
eurjchem-782	69	15	,	,	PUNCT
eurjchem-782	69	16	1673	1673	NUM
eurjchem-782	69	17	(	(	PUNCT
eurjchem-782	69	18	c	c	NOUN
eurjchem-782	69	19	=	=	NOUN
eurjchem-782	69	20	o	o	NOUN
eurjchem-782	69	21	)	)	PUNCT
eurjchem-782	69	22	,	,	PUNCT
eurjchem-782	69	23	1591	1591	NUM
eurjchem-782	69	24	(	(	PUNCT
eurjchem-782	69	25	c	c	X
eurjchem-782	69	26	=	=	SYM
eurjchem-782	69	27	c	c	NOUN
eurjchem-782	69	28	)	)	PUNCT
eurjchem-782	69	29	.	.	PUNCT
eurjchem-782	70	1	1h	1h	NUM
eurjchem-782	70	2	nmr	nmr	NOUN
eurjchem-782	70	3	(	(	PUNCT
eurjchem-782	70	4	400	400	NUM
eurjchem-782	70	5	mhz	mhz	NOUN
eurjchem-782	70	6	,	,	PUNCT
eurjchem-782	70	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-782	70	8	,	,	PUNCT
eurjchem-782	70	9	δ	δ	PROPN
eurjchem-782	70	10	,	,	PUNCT
eurjchem-782	70	11	ppm	ppm	NUM
eurjchem-782	70	12	):	):	PUNCT
eurjchem-782	70	13	8.00	8.00	NUM
eurjchem-782	70	14	(	(	PUNCT
eurjchem-782	70	15	d	d	PROPN
eurjchem-782	70	16	,	,	PUNCT
eurjchem-782	70	17	1h	1h	NUM
eurjchem-782	70	18	,	,	PUNCT
eurjchem-782	70	19	j	j	PROPN
eurjchem-782	70	20	=	=	SYM
eurjchem-782	70	21	7.3	7.3	NUM
eurjchem-782	70	22	hz	hz	ADJ
eurjchem-782	70	23	,	,	PUNCT
eurjchem-782	70	24	β‐ch	β‐ch	NOUN
eurjchem-782	70	25	)	)	PUNCT
eurjchem-782	70	26	,	,	PUNCT
eurjchem-782	70	27	7.89‐7.25	7.89‐7.25	NUM
eurjchem-782	70	28	(	(	PUNCT
eurjchem-782	70	29	m	m	PROPN
eurjchem-782	70	30	,	,	PUNCT
eurjchem-782	70	31	9h	9h	NUM
eurjchem-782	70	32	,	,	PUNCT
eurjchem-782	70	33	ar‐h	ar‐h	NOUN
eurjchem-782	70	34	)	)	PUNCT
eurjchem-782	70	35	,	,	PUNCT
eurjchem-782	70	36	7.55	7.55	NUM
eurjchem-782	70	37	(	(	PUNCT
eurjchem-782	70	38	d	d	PROPN
eurjchem-782	70	39	,	,	PUNCT
eurjchem-782	70	40	1h	1h	NUM
eurjchem-782	70	41	,	,	PUNCT
eurjchem-782	70	42	j	j	PROPN
eurjchem-782	70	43	=	=	PROPN
eurjchem-782	70	44	8.2	8.2	NUM
eurjchem-782	70	45	hz	hz	NOUN
eurjchem-782	70	46	,	,	PUNCT
eurjchem-782	70	47	α‐ch	α‐ch	PROPN
eurjchem-782	70	48	)	)	PUNCT
eurjchem-782	70	49	,	,	PUNCT
eurjchem-782	70	50	2.55	2.55	NUM
eurjchem-782	70	51	(	(	PUNCT
eurjchem-782	70	52	s	s	PROPN
eurjchem-782	70	53	,	,	PUNCT
eurjchem-782	70	54	3h	3h	NUM
eurjchem-782	70	55	,	,	PUNCT
eurjchem-782	70	56	sch3	sch3	PROPN
eurjchem-782	70	57	)	)	PUNCT
eurjchem-782	70	58	.	.	PUNCT
eurjchem-782	71	1	13c	13c	NOUN
eurjchem-782	71	2	nmr	nmr	NOUN
eurjchem-782	71	3	(	(	PUNCT
eurjchem-782	71	4	100	100	NUM
eurjchem-782	71	5	mhz	mhz	NOUN
eurjchem-782	71	6	,	,	PUNCT
eurjchem-782	71	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-782	71	8	,	,	PUNCT
eurjchem-782	71	9	δ	δ	PROPN
eurjchem-782	71	10	,	,	PUNCT
eurjchem-782	71	11	ppm	ppm	NUM
eurjchem-782	71	12	):	):	PUNCT
eurjchem-782	71	13	189.5	189.5	NUM
eurjchem-782	71	14	(	(	PUNCT
eurjchem-782	71	15	c‐1	c‐1	NOUN
eurjchem-782	71	16	)	)	PUNCT
eurjchem-782	71	17	,	,	PUNCT
eurjchem-782	71	18	145.0	145.0	NUM
eurjchem-782	71	19	(	(	PUNCT
eurjchem-782	71	20	c‐4	c‐4	NOUN
eurjchem-782	71	21	'	'	NUM
eurjchem-782	71	22	)	)	PUNCT
eurjchem-782	71	23	,	,	PUNCT
eurjchem-782	71	24	145.0	145.0	NUM
eurjchem-782	71	25	(	(	PUNCT
eurjchem-782	71	26	c‐3	c‐3	NOUN
eurjchem-782	71	27	)	)	PUNCT
eurjchem-782	71	28	,	,	PUNCT
eurjchem-782	71	29	135.2	135.2	NUM
eurjchem-782	71	30	(	(	PUNCT
eurjchem-782	71	31	c‐1	c‐1	NOUN
eurjchem-782	71	32	"	"	PUNCT
eurjchem-782	71	33	)	)	PUNCT
eurjchem-782	71	34	,	,	PUNCT
eurjchem-782	71	35	134.3	134.3	NUM
eurjchem-782	71	36	(	(	PUNCT
eurjchem-782	71	37	c‐1	c‐1	NOUN
eurjchem-782	71	38	'	'	PUNCT
eurjchem-782	71	39	)	)	PUNCT
eurjchem-782	71	40	,	,	PUNCT
eurjchem-782	71	41	128.9	128.9	NUM
eurjchem-782	71	42	(	(	PUNCT
eurjchem-782	71	43	c‐2	c‐2	NOUN
eurjchem-782	71	44	'	'	PUNCT
eurjchem-782	71	45	,	,	PUNCT
eurjchem-782	71	46	c‐6	c‐6	NOUN
eurjchem-782	71	47	'	'	PUNCT
eurjchem-782	71	48	)	)	PUNCT
eurjchem-782	71	49	,	,	PUNCT
eurjchem-782	71	50	128.6	128.6	NUM
eurjchem-782	71	51	(	(	PUNCT
eurjchem-782	71	52	c‐3	c‐3	NOUN
eurjchem-782	71	53	"	"	PUNCT
eurjchem-782	71	54	,	,	PUNCT
eurjchem-782	71	55	c‐5	c‐5	NOUN
eurjchem-782	71	56	"	"	PUNCT
eurjchem-782	71	57	)	)	PUNCT
eurjchem-782	71	58	,	,	PUNCT
eurjchem-782	71	59	128.3	128.3	NUM
eurjchem-782	71	60	(	(	PUNCT
eurjchem-782	71	61	c‐2	c‐2	NOUN
eurjchem-782	71	62	"	"	PUNCT
eurjchem-782	71	63	,	,	PUNCT
eurjchem-782	71	64	c‐6	c‐6	NOUN
eurjchem-782	71	65	"	"	PUNCT
eurjchem-782	71	66	)	)	PUNCT
eurjchem-782	71	67	,	,	PUNCT
eurjchem-782	71	68	127.9	127.9	NUM
eurjchem-782	71	69	(	(	PUNCT
eurjchem-782	71	70	c‐4	c‐4	PROPN
eurjchem-782	71	71	"	"	PUNCT
eurjchem-782	71	72	)	)	PUNCT
eurjchem-782	71	73	,	,	PUNCT
eurjchem-782	71	74	127.3	127.3	NUM
eurjchem-782	71	75	(	(	PUNCT
eurjchem-782	71	76	c‐3	c‐3	NOUN
eurjchem-782	71	77	'	'	PUNCT
eurjchem-782	71	78	,	,	PUNCT
eurjchem-782	71	79	c‐5	c‐5	NOUN
eurjchem-782	71	80	'	'	PUNCT
eurjchem-782	71	81	)	)	PUNCT
eurjchem-782	71	82	,	,	PUNCT
eurjchem-782	71	83	121.3	121.3	NUM
eurjchem-782	71	84	(	(	PUNCT
eurjchem-782	71	85	c‐2	c‐2	NOUN
eurjchem-782	71	86	)	)	PUNCT
eurjchem-782	71	87	,	,	PUNCT
eurjchem-782	71	88	14.5	14.5	NUM
eurjchem-782	71	89	(	(	PUNCT
eurjchem-782	71	90	‐sch3	‐sch3	PROPN
eurjchem-782	71	91	)	)	PUNCT
eurjchem-782	71	92	.	.	PUNCT
eurjchem-782	72	1	ms	ms	PROPN
eurjchem-782	72	2	(	(	PUNCT
eurjchem-782	72	3	esi	esi	PROPN
eurjchem-782	72	4	,	,	PUNCT
eurjchem-782	72	5	m	m	PROPN
eurjchem-782	72	6	/	/	SYM
eurjchem-782	72	7	z	z	NOUN
eurjchem-782	72	8	):	):	PUNCT
eurjchem-782	72	9	254.07	254.07	NUM
eurjchem-782	72	10	(	(	PUNCT
eurjchem-782	72	11	m+	m+	NUM
eurjchem-782	72	12	)	)	PUNCT
eurjchem-782	72	13	.	.	PUNCT
eurjchem-782	73	1	anal	anal	PROPN
eurjchem-782	73	2	.	.	PUNCT
eurjchem-782	73	3	calcd	calcd	NOUN
eurjchem-782	73	4	.	.	PUNCT
eurjchem-782	74	1	for	for	ADP
eurjchem-782	74	2	c16h14os	c16h14o	NOUN
eurjchem-782	74	3	:	:	PUNCT
eurjchem-782	74	4	c	c	NOUN
eurjchem-782	74	5	,	,	PUNCT
eurjchem-782	74	6	75.55	75.55	NUM
eurjchem-782	74	7	;	;	PUNCT
eurjchem-782	74	8	h	h	NOUN
eurjchem-782	74	9	,	,	PUNCT
eurjchem-782	74	10	5.55	5.55	NUM
eurjchem-782	74	11	.	.	PUNCT
eurjchem-782	74	12	found	find	VERB
eurjchem-782	74	13	:	:	PUNCT
eurjchem-782	75	1	c	c	X
eurjchem-782	75	2	,	,	PUNCT
eurjchem-782	75	3	75.51	75.51	NUM
eurjchem-782	75	4	;	;	PUNCT
eurjchem-782	75	5	h	h	NOUN
eurjchem-782	75	6	,	,	PUNCT
eurjchem-782	75	7	5.53	5.53	NUM
eurjchem-782	75	8	%	%	NOUN
eurjchem-782	75	9	.	.	PUNCT
eurjchem-782	76	1	2.2.2	2.2.2	X
eurjchem-782	76	2	.	.	PUNCT
eurjchem-782	76	3	general	general	ADJ
eurjchem-782	76	4	procedure	procedure	NOUN
eurjchem-782	76	5	for	for	ADP
eurjchem-782	76	6	the	the	DET
eurjchem-782	76	7	synthesis	synthesis	NOUN
eurjchem-782	76	8	of	of	ADP
eurjchem-782	76	9	cyclopropyl	cyclopropyl	PROPN
eurjchem-782	76	10	ketones	ketone	NOUN
eurjchem-782	76	11	analogues	analogue	NOUN
eurjchem-782	76	12	(	(	PUNCT
eurjchem-782	76	13	4a‐d	4a‐d	NOUN
eurjchem-782	76	14	)	)	PUNCT
eurjchem-782	76	15	sodium	sodium	NOUN
eurjchem-782	76	16	hydride	hydride	NOUN
eurjchem-782	76	17	(	(	PUNCT
eurjchem-782	76	18	0.3	0.3	NUM
eurjchem-782	76	19	g	g	NOUN
eurjchem-782	76	20	,	,	PUNCT
eurjchem-782	76	21	0.0130	0.0130	NUM
eurjchem-782	76	22	mol	mol	NOUN
eurjchem-782	76	23	)	)	PUNCT
eurjchem-782	76	24	was	be	AUX
eurjchem-782	76	25	added	add	VERB
eurjchem-782	76	26	in	in	ADP
eurjchem-782	76	27	portions	portion	NOUN
eurjchem-782	76	28	to	to	ADP
eurjchem-782	76	29	the	the	DET
eurjchem-782	76	30	stirred	stirred	ADJ
eurjchem-782	76	31	suspensions	suspension	NOUN
eurjchem-782	76	32	of	of	ADP
eurjchem-782	76	33	trimethylsulfoxonium	trimethylsulfoxonium	NOUN
eurjchem-782	76	34	iodide	iodide	NOUN
eurjchem-782	76	35	(	(	PUNCT
eurjchem-782	76	36	2.8	2.8	NUM
eurjchem-782	76	37	g	g	NOUN
eurjchem-782	76	38	,	,	PUNCT
eurjchem-782	76	39	0.0130	0.0130	NUM
eurjchem-782	76	40	mol	mol	NOUN
eurjchem-782	76	41	)	)	PUNCT
eurjchem-782	76	42	in	in	ADP
eurjchem-782	76	43	dry	dry	ADJ
eurjchem-782	76	44	dmso	dmso	NOUN
eurjchem-782	76	45	(	(	PUNCT
eurjchem-782	76	46	20	20	NUM
eurjchem-782	76	47	ml	ml	NOUN
eurjchem-782	76	48	)	)	PUNCT
eurjchem-782	76	49	under	under	ADP
eurjchem-782	76	50	nitrogen	nitrogen	NOUN
eurjchem-782	76	51	gas	gas	NOUN
eurjchem-782	76	52	atmosphere	atmosphere	NOUN
eurjchem-782	76	53	.	.	PUNCT
eurjchem-782	77	1	the	the	DET
eurjchem-782	77	2	reaction	reaction	NOUN
eurjchem-782	77	3	mixture	mixture	NOUN
eurjchem-782	77	4	was	be	AUX
eurjchem-782	77	5	stirred	stir	VERB
eurjchem-782	77	6	for	for	ADP
eurjchem-782	77	7	10	10	NUM
eurjchem-782	77	8	min	min	NOUN
eurjchem-782	77	9	.	.	PROPN
eurjchem-782	78	1	at	at	ADP
eurjchem-782	78	2	25‐30	25‐30	NUM
eurjchem-782	78	3	oc	oc	ADP
eurjchem-782	78	4	(	(	PUNCT
eurjchem-782	78	5	until	until	SCONJ
eurjchem-782	78	6	the	the	DET
eurjchem-782	78	7	evaluation	evaluation	NOUN
eurjchem-782	78	8	of	of	ADP
eurjchem-782	78	9	the	the	DET
eurjchem-782	78	10	h2	h2	NOUN
eurjchem-782	78	11	gas	gas	NOUN
eurjchem-782	78	12	ceased	cease	VERB
eurjchem-782	78	13	)	)	PUNCT
eurjchem-782	78	14	.	.	PUNCT
eurjchem-782	79	1	chalcones	chalcone	NOUN
eurjchem-782	79	2	(	(	PUNCT
eurjchem-782	79	3	0.0130	0.0130	NUM
eurjchem-782	79	4	mol	mol	NOUN
eurjchem-782	79	5	)	)	PUNCT
eurjchem-782	79	6	in	in	ADP
eurjchem-782	79	7	dry	dry	ADJ
eurjchem-782	79	8	dmso	dmso	NOUN
eurjchem-782	79	9	(	(	PUNCT
eurjchem-782	79	10	15	15	NUM
eurjchem-782	79	11	ml	ml	NOUN
eurjchem-782	79	12	)	)	PUNCT
eurjchem-782	79	13	were	be	AUX
eurjchem-782	79	14	added	add	VERB
eurjchem-782	79	15	drop	drop	NOUN
eurjchem-782	79	16	wise	wise	ADJ
eurjchem-782	79	17	during	during	ADP
eurjchem-782	79	18	30min	30min	NOUN
eurjchem-782	79	19	.	.	PUNCT
eurjchem-782	80	1	to	to	ADP
eurjchem-782	80	2	the	the	DET
eurjchem-782	80	3	above	above	ADJ
eurjchem-782	80	4	solution	solution	NOUN
eurjchem-782	80	5	.	.	PUNCT
eurjchem-782	81	1	the	the	DET
eurjchem-782	81	2	reaction	reaction	NOUN
eurjchem-782	81	3	mass	mass	NOUN
eurjchem-782	81	4	was	be	AUX
eurjchem-782	81	5	stirred	stir	VERB
eurjchem-782	81	6	at	at	ADP
eurjchem-782	81	7	26‐28	26‐28	NUM
eurjchem-782	81	8	oc	oc	NOUN
eurjchem-782	81	9	for	for	ADP
eurjchem-782	81	10	2h	2h	NUM
eurjchem-782	81	11	.	.	PUNCT
eurjchem-782	82	1	and	and	CCONJ
eurjchem-782	82	2	raised	raise	VERB
eurjchem-782	82	3	the	the	DET
eurjchem-782	82	4	temperature	temperature	NOUN
eurjchem-782	82	5	to	to	ADP
eurjchem-782	82	6	50‐60	50‐60	NUM
eurjchem-782	82	7	oc	oc	NOUN
eurjchem-782	82	8	for	for	ADP
eurjchem-782	82	9	1h	1h	NUM
eurjchem-782	82	10	.	.	PUNCT
eurjchem-782	83	1	the	the	DET
eurjchem-782	83	2	completion	completion	NOUN
eurjchem-782	83	3	of	of	ADP
eurjchem-782	83	4	the	the	DET
eurjchem-782	83	5	reaction	reaction	NOUN
eurjchem-782	83	6	was	be	AUX
eurjchem-782	83	7	confirmed	confirm	VERB
eurjchem-782	83	8	by	by	ADP
eurjchem-782	83	9	tlc	tlc	NOUN
eurjchem-782	83	10	and	and	CCONJ
eurjchem-782	83	11	the	the	DET
eurjchem-782	83	12	reaction	reaction	NOUN
eurjchem-782	83	13	mixture	mixture	NOUN
eurjchem-782	83	14	was	be	AUX
eurjchem-782	83	15	poured	pour	VERB
eurjchem-782	83	16	into	into	ADP
eurjchem-782	83	17	water	water	NOUN
eurjchem-782	83	18	(	(	PUNCT
eurjchem-782	83	19	20	20	NUM
eurjchem-782	83	20	ml	ml	NOUN
eurjchem-782	83	21	)	)	PUNCT
eurjchem-782	83	22	.	.	PUNCT
eurjchem-782	84	1	the	the	DET
eurjchem-782	84	2	precipitated	precipitate	VERB
eurjchem-782	84	3	gummy	gummy	ADJ
eurjchem-782	84	4	residue	residue	NOUN
eurjchem-782	84	5	was	be	AUX
eurjchem-782	84	6	extracted	extract	VERB
eurjchem-782	84	7	into	into	ADP
eurjchem-782	84	8	chloroform	chloroform	NOUN
eurjchem-782	84	9	.	.	PUNCT
eurjchem-782	85	1	the	the	DET
eurjchem-782	85	2	combined	combine	VERB
eurjchem-782	85	3	organic	organic	ADJ
eurjchem-782	85	4	layer	layer	NOUN
eurjchem-782	85	5	was	be	AUX
eurjchem-782	85	6	washed	wash	VERB
eurjchem-782	85	7	with	with	ADP
eurjchem-782	85	8	water	water	NOUN
eurjchem-782	85	9	,	,	PUNCT
eurjchem-782	85	10	dried	dry	VERB
eurjchem-782	85	11	over	over	ADP
eurjchem-782	85	12	anhyd	anhyd	NOUN
eurjchem-782	85	13	.	.	PUNCT
eurjchem-782	86	1	na2so4	na2so4	NOUN
eurjchem-782	86	2	and	and	CCONJ
eurjchem-782	86	3	concentrated	concentrate	VERB
eurjchem-782	86	4	under	under	ADP
eurjchem-782	86	5	reduced	reduced	ADJ
eurjchem-782	86	6	pressure	pressure	NOUN
eurjchem-782	86	7	.	.	PUNCT
eurjchem-782	87	1	the	the	DET
eurjchem-782	87	2	products	product	NOUN
eurjchem-782	87	3	were	be	AUX
eurjchem-782	87	4	recrystallized	recrystallize	VERB
eurjchem-782	87	5	from	from	ADP
eurjchem-782	87	6	ethanol	ethanol	NOUN
eurjchem-782	87	7	(	(	PUNCT
eurjchem-782	87	8	scheme	scheme	NOUN
eurjchem-782	87	9	1	1	NUM
eurjchem-782	87	10	)	)	PUNCT
eurjchem-782	87	11	.	.	PUNCT
eurjchem-782	88	1	phenyl	phenyl	NOUN
eurjchem-782	88	2	(	(	PUNCT
eurjchem-782	88	3	2‐phenylcyclopropyl)methanone	2‐phenylcyclopropyl)methanone	NUM
eurjchem-782	88	4	(	(	PUNCT
eurjchem-782	88	5	4a	4a	NUM
eurjchem-782	88	6	):	):	PUNCT
eurjchem-782	88	7	color	color	NOUN
eurjchem-782	88	8	:	:	PUNCT
eurjchem-782	88	9	dark	dark	ADJ
eurjchem-782	88	10	brown	brown	ADJ
eurjchem-782	88	11	semisolid	semisolid	NOUN
eurjchem-782	88	12	.	.	PUNCT
eurjchem-782	89	1	yield	yield	NOUN
eurjchem-782	89	2	:	:	PUNCT
eurjchem-782	89	3	77.63	77.63	NUM
eurjchem-782	89	4	%	%	NOUN
eurjchem-782	89	5	.	.	PUNCT
eurjchem-782	90	1	ir	ir	PROPN
eurjchem-782	90	2	(	(	PUNCT
eurjchem-782	90	3	kbr	kbr	PROPN
eurjchem-782	90	4	,	,	PUNCT
eurjchem-782	90	5	ν	ν	PROPN
eurjchem-782	90	6	,	,	PUNCT
eurjchem-782	90	7	cm‐1	cm‐1	PROPN
eurjchem-782	90	8	):	):	PUNCT
eurjchem-782	90	9	3160	3160	NUM
eurjchem-782	90	10	,	,	PUNCT
eurjchem-782	90	11	2953	2953	NUM
eurjchem-782	90	12	(	(	PUNCT
eurjchem-782	90	13	ar‐ch	ar‐ch	NUM
eurjchem-782	90	14	)	)	PUNCT
eurjchem-782	90	15	,	,	PUNCT
eurjchem-782	90	16	1671	1671	NUM
eurjchem-782	90	17	(	(	PUNCT
eurjchem-782	90	18	c	c	NOUN
eurjchem-782	90	19	=	=	NOUN
eurjchem-782	90	20	o	o	NOUN
eurjchem-782	90	21	)	)	PUNCT
eurjchem-782	90	22	.	.	PUNCT
eurjchem-782	91	1	1h	1h	NUM
eurjchem-782	91	2	nmr	nmr	NOUN
eurjchem-782	91	3	(	(	PUNCT
eurjchem-782	91	4	400	400	NUM
eurjchem-782	91	5	mhz	mhz	NOUN
eurjchem-782	91	6	,	,	PUNCT
eurjchem-782	91	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-782	91	8	,	,	PUNCT
eurjchem-782	91	9	δ	δ	PROPN
eurjchem-782	91	10	,	,	PUNCT
eurjchem-782	91	11	ppm	ppm	NOUN
eurjchem-782	91	12	):	):	PUNCT
eurjchem-782	91	13	7.95‐7.25	7.95‐7.25	PROPN
eurjchem-782	91	14	(	(	PUNCT
eurjchem-782	91	15	m	m	PROPN
eurjchem-782	91	16	,	,	PUNCT
eurjchem-782	91	17	10h	10h	NUM
eurjchem-782	91	18	,	,	PUNCT
eurjchem-782	91	19	ar‐h	ar‐h	PROPN
eurjchem-782	91	20	)	)	PUNCT
eurjchem-782	91	21	,	,	PUNCT
eurjchem-782	91	22	2.10‐2.02	2.10‐2.02	NUM
eurjchem-782	91	23	(	(	PUNCT
eurjchem-782	91	24	m	m	PROPN
eurjchem-782	91	25	,	,	PUNCT
eurjchem-782	91	26	2h	2h	NUM
eurjchem-782	91	27	,	,	PUNCT
eurjchem-782	91	28	cyclopro‐ch	cyclopro‐ch	NUM
eurjchem-782	91	29	)	)	PUNCT
eurjchem-782	91	30	,	,	PUNCT
eurjchem-782	91	31	0.78	0.78	NUM
eurjchem-782	91	32	(	(	PUNCT
eurjchem-782	91	33	d	d	NOUN
eurjchem-782	91	34	,	,	PUNCT
eurjchem-782	91	35	2h	2h	NUM
eurjchem-782	91	36	,	,	PUNCT
eurjchem-782	91	37	c4‐ch2	c4‐ch2	PROPN
eurjchem-782	91	38	)	)	PUNCT
eurjchem-782	91	39	.	.	PUNCT
eurjchem-782	92	1	13c	13c	NOUN
eurjchem-782	92	2	nmr	nmr	NOUN
eurjchem-782	92	3	(	(	PUNCT
eurjchem-782	92	4	100	100	NUM
eurjchem-782	92	5	mhz	mhz	NOUN
eurjchem-782	92	6	,	,	PUNCT
eurjchem-782	92	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-782	92	8	,	,	PUNCT
eurjchem-782	92	9	δ	δ	PROPN
eurjchem-782	92	10	,	,	PUNCT
eurjchem-782	92	11	ppm	ppm	NUM
eurjchem-782	92	12	):	):	PUNCT
eurjchem-782	92	13	192.2	192.2	NUM
eurjchem-782	92	14	(	(	PUNCT
eurjchem-782	92	15	c‐	c‐	NOUN
eurjchem-782	92	16	1	1	NUM
eurjchem-782	92	17	)	)	PUNCT
eurjchem-782	92	18	,	,	PUNCT
eurjchem-782	92	19	141.7	141.7	NUM
eurjchem-782	92	20	(	(	PUNCT
eurjchem-782	92	21	c‐1	c‐1	NOUN
eurjchem-782	92	22	"	"	PUNCT
eurjchem-782	92	23	)	)	PUNCT
eurjchem-782	92	24	,	,	PUNCT
eurjchem-782	92	25	136.3	136.3	NUM
eurjchem-782	92	26	(	(	PUNCT
eurjchem-782	92	27	c‐1	c‐1	NOUN
eurjchem-782	92	28	'	'	PUNCT
eurjchem-782	92	29	)	)	PUNCT
eurjchem-782	92	30	,	,	PUNCT
eurjchem-782	92	31	133.0	133.0	NUM
eurjchem-782	92	32	(	(	PUNCT
eurjchem-782	92	33	c‐4	c‐4	PROPN
eurjchem-782	92	34	'	'	PUNCT
eurjchem-782	92	35	)	)	PUNCT
eurjchem-782	92	36	,	,	PUNCT
eurjchem-782	92	37	128.9	128.9	NUM
eurjchem-782	92	38	(	(	PUNCT
eurjchem-782	92	39	c‐2	c‐2	NOUN
eurjchem-782	92	40	'	'	PUNCT
eurjchem-782	92	41	,	,	PUNCT
eurjchem-782	92	42	c‐6	c‐6	NOUN
eurjchem-782	92	43	'	'	PROPN
eurjchem-782	92	44	,	,	PUNCT
eurjchem-782	92	45	c‐	c‐	NOUN
eurjchem-782	92	46	2	2	NUM
eurjchem-782	92	47	"	"	PUNCT
eurjchem-782	92	48	,	,	PUNCT
eurjchem-782	92	49	c‐6	c‐6	NOUN
eurjchem-782	92	50	"	"	PUNCT
eurjchem-782	92	51	)	)	PUNCT
eurjchem-782	92	52	,	,	PUNCT
eurjchem-782	92	53	128.6	128.6	NUM
eurjchem-782	92	54	(	(	PUNCT
eurjchem-782	92	55	c‐3	c‐3	NOUN
eurjchem-782	92	56	'	'	PUNCT
eurjchem-782	92	57	,	,	PUNCT
eurjchem-782	92	58	c‐5	c‐5	NOUN
eurjchem-782	92	59	'	'	PUNCT
eurjchem-782	92	60	)	)	PUNCT
eurjchem-782	92	61	,	,	PUNCT
eurjchem-782	92	62	128.3	128.3	NUM
eurjchem-782	92	63	(	(	PUNCT
eurjchem-782	92	64	c‐3	c‐3	NOUN
eurjchem-782	92	65	"	"	PUNCT
eurjchem-782	92	66	,	,	PUNCT
eurjchem-782	92	67	c‐5	c‐5	NOUN
eurjchem-782	92	68	"	"	PUNCT
eurjchem-782	92	69	)	)	PUNCT
eurjchem-782	92	70	,	,	PUNCT
eurjchem-782	92	71	125.1	125.1	NUM
eurjchem-782	92	72	(	(	PUNCT
eurjchem-782	92	73	c‐4	c‐4	PROPN
eurjchem-782	92	74	"	"	PUNCT
eurjchem-782	92	75	)	)	PUNCT
eurjchem-782	92	76	,	,	PUNCT
eurjchem-782	92	77	27.0	27.0	NUM
eurjchem-782	92	78	(	(	PUNCT
eurjchem-782	92	79	c‐2	c‐2	NOUN
eurjchem-782	92	80	)	)	PUNCT
eurjchem-782	92	81	,	,	PUNCT
eurjchem-782	92	82	25.4	25.4	NUM
eurjchem-782	92	83	(	(	PUNCT
eurjchem-782	92	84	c‐3	c‐3	NOUN
eurjchem-782	92	85	)	)	PUNCT
eurjchem-782	92	86	,	,	PUNCT
eurjchem-782	92	87	12.4	12.4	NUM
eurjchem-782	92	88	(	(	PUNCT
eurjchem-782	92	89	c‐4	c‐4	PROPN
eurjchem-782	92	90	)	)	PUNCT
eurjchem-782	92	91	.	.	PUNCT
eurjchem-782	93	1	ms	ms	PROPN
eurjchem-782	93	2	(	(	PUNCT
eurjchem-782	93	3	esi	esi	PROPN
eurjchem-782	93	4	,	,	PUNCT
eurjchem-782	93	5	m	m	PROPN
eurjchem-782	93	6	/	/	SYM
eurjchem-782	93	7	z	z	NOUN
eurjchem-782	93	8	):	):	PUNCT
eurjchem-782	93	9	222.11	222.11	NUM
eurjchem-782	93	10	(	(	PUNCT
eurjchem-782	93	11	m+	m+	NUM
eurjchem-782	93	12	)	)	PUNCT
eurjchem-782	93	13	.	.	PUNCT
eurjchem-782	94	1	anal	anal	PROPN
eurjchem-782	94	2	.	.	PUNCT
eurjchem-782	94	3	calcd	calcd	NOUN
eurjchem-782	94	4	.	.	PUNCT
eurjchem-782	95	1	for	for	ADP
eurjchem-782	95	2	c16h14o	c16h14o	NUM
eurjchem-782	95	3	:	:	PUNCT
eurjchem-782	95	4	c	c	X
eurjchem-782	95	5	,	,	PUNCT
eurjchem-782	95	6	86.45	86.45	NUM
eurjchem-782	95	7	;	;	PUNCT
eurjchem-782	95	8	h	h	NOUN
eurjchem-782	95	9	,	,	PUNCT
eurjchem-782	95	10	6.35	6.35	NUM
eurjchem-782	95	11	.	.	PUNCT
eurjchem-782	95	12	found	find	VERB
eurjchem-782	95	13	:	:	PUNCT
eurjchem-782	96	1	c	c	X
eurjchem-782	96	2	,	,	PUNCT
eurjchem-782	96	3	86.43	86.43	NUM
eurjchem-782	96	4	;	;	PUNCT
eurjchem-782	96	5	h	h	NOUN
eurjchem-782	96	6	,	,	PUNCT
eurjchem-782	96	7	6.32	6.32	NUM
eurjchem-782	96	8	%	%	NOUN
eurjchem-782	96	9	.	.	PUNCT
eurjchem-782	97	1	umesha	umesha	PROPN
eurjchem-782	97	2	and	and	CCONJ
eurjchem-782	97	3	basavaraju	basavaraju	NOUN
eurjchem-782	97	4	/	/	SYM
eurjchem-782	97	5	european	european	ADJ
eurjchem-782	97	6	journal	journal	PROPN
eurjchem-782	97	7	of	of	ADP
eurjchem-782	97	8	chemistry	chemistry	NOUN
eurjchem-782	97	9	4	4	NUM
eurjchem-782	97	10	(	(	PUNCT
eurjchem-782	97	11	3	3	NUM
eurjchem-782	97	12	)	)	PUNCT
eurjchem-782	97	13	(	(	PUNCT
eurjchem-782	97	14	2013	2013	NUM
eurjchem-782	97	15	)	)	PUNCT
eurjchem-782	97	16	235‐239	235‐239	NUM
eurjchem-782	97	17	237	237	NUM
eurjchem-782	97	18	(	(	PUNCT
eurjchem-782	97	19	2‐phenylcyclopropyl)(p‐tolyl)methanone	2‐phenylcyclopropyl)(p‐tolyl)methanone	NUM
eurjchem-782	97	20	(	(	PUNCT
eurjchem-782	97	21	4b	4b	PROPN
eurjchem-782	97	22	):	):	PUNCT
eurjchem-782	97	23	color	color	NOUN
eurjchem-782	97	24	:	:	PUNCT
eurjchem-782	97	25	dark	dark	ADJ
eurjchem-782	97	26	brown	brown	ADJ
eurjchem-782	97	27	semisolid	semisolid	NOUN
eurjchem-782	97	28	.	.	PUNCT
eurjchem-782	98	1	yield	yield	NOUN
eurjchem-782	98	2	:	:	PUNCT
eurjchem-782	98	3	88.55	88.55	NUM
eurjchem-782	98	4	%	%	NOUN
eurjchem-782	98	5	.	.	PUNCT
eurjchem-782	99	1	ir	ir	PROPN
eurjchem-782	99	2	(	(	PUNCT
eurjchem-782	99	3	kbr	kbr	PROPN
eurjchem-782	99	4	,	,	PUNCT
eurjchem-782	99	5	ν	ν	PROPN
eurjchem-782	99	6	,	,	PUNCT
eurjchem-782	99	7	cm‐1	cm‐1	PROPN
eurjchem-782	99	8	):	):	PUNCT
eurjchem-782	99	9	3155	3155	NUM
eurjchem-782	99	10	,	,	PUNCT
eurjchem-782	99	11	2948	2948	NUM
eurjchem-782	99	12	(	(	PUNCT
eurjchem-782	99	13	ar‐ch	ar‐ch	NUM
eurjchem-782	99	14	)	)	PUNCT
eurjchem-782	99	15	,	,	PUNCT
eurjchem-782	99	16	1677	1677	NUM
eurjchem-782	99	17	(	(	PUNCT
eurjchem-782	99	18	c	c	NOUN
eurjchem-782	99	19	=	=	NOUN
eurjchem-782	99	20	o	o	NOUN
eurjchem-782	99	21	)	)	PUNCT
eurjchem-782	99	22	.	.	PUNCT
eurjchem-782	100	1	1h	1h	NUM
eurjchem-782	100	2	nmr	nmr	NOUN
eurjchem-782	100	3	(	(	PUNCT
eurjchem-782	100	4	400	400	NUM
eurjchem-782	100	5	mhz	mhz	NOUN
eurjchem-782	100	6	,	,	PUNCT
eurjchem-782	100	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-782	100	8	,	,	PUNCT
eurjchem-782	100	9	δ	δ	PROPN
eurjchem-782	100	10	,	,	PUNCT
eurjchem-782	100	11	ppm	ppm	NUM
eurjchem-782	100	12	):	):	PUNCT
eurjchem-782	100	13	8.01	8.01	NUM
eurjchem-782	100	14	‐7.28	‐7.28	NOUN
eurjchem-782	100	15	(	(	PUNCT
eurjchem-782	100	16	m	m	PROPN
eurjchem-782	100	17	,	,	PUNCT
eurjchem-782	100	18	9h	9h	NUM
eurjchem-782	100	19	,	,	PUNCT
eurjchem-782	100	20	ar‐h	ar‐h	NOUN
eurjchem-782	100	21	)	)	PUNCT
eurjchem-782	100	22	,	,	PUNCT
eurjchem-782	100	23	2.34	2.34	NUM
eurjchem-782	100	24	(	(	PUNCT
eurjchem-782	100	25	s	s	PROPN
eurjchem-782	100	26	,	,	PUNCT
eurjchem-782	100	27	3h	3h	NUM
eurjchem-782	100	28	,	,	PUNCT
eurjchem-782	100	29	ch3	ch3	PROPN
eurjchem-782	100	30	)	)	PUNCT
eurjchem-782	100	31	,	,	PUNCT
eurjchem-782	100	32	2.18‐2.00	2.18‐2.00	NUM
eurjchem-782	100	33	(	(	PUNCT
eurjchem-782	100	34	m	m	PROPN
eurjchem-782	100	35	,	,	PUNCT
eurjchem-782	100	36	2h	2h	NUM
eurjchem-782	100	37	,	,	PUNCT
eurjchem-782	100	38	cyclopro‐ch	cyclopro‐ch	NUM
eurjchem-782	100	39	)	)	PUNCT
eurjchem-782	100	40	,	,	PUNCT
eurjchem-782	100	41	0.81	0.81	NUM
eurjchem-782	100	42	(	(	PUNCT
eurjchem-782	100	43	d	d	NOUN
eurjchem-782	100	44	,	,	PUNCT
eurjchem-782	100	45	2h	2h	NUM
eurjchem-782	100	46	,	,	PUNCT
eurjchem-782	100	47	c4‐ch2	c4‐ch2	PROPN
eurjchem-782	100	48	)	)	PUNCT
eurjchem-782	100	49	.	.	PUNCT
eurjchem-782	101	1	13c	13c	NOUN
eurjchem-782	101	2	nmr	nmr	NOUN
eurjchem-782	101	3	(	(	PUNCT
eurjchem-782	101	4	100	100	NUM
eurjchem-782	101	5	mhz	mhz	NOUN
eurjchem-782	101	6	,	,	PUNCT
eurjchem-782	101	7	dmso‐	dmso‐	NUM
eurjchem-782	101	8	d6	d6	NOUN
eurjchem-782	101	9	,	,	PUNCT
eurjchem-782	101	10	δ	δ	PROPN
eurjchem-782	101	11	,	,	PUNCT
eurjchem-782	101	12	ppm	ppm	NUM
eurjchem-782	101	13	):	):	PUNCT
eurjchem-782	101	14	192.3	192.3	NUM
eurjchem-782	101	15	(	(	PUNCT
eurjchem-782	101	16	c‐1	c‐1	NOUN
eurjchem-782	101	17	)	)	PUNCT
eurjchem-782	101	18	,	,	PUNCT
eurjchem-782	101	19	142.7	142.7	NUM
eurjchem-782	101	20	(	(	PUNCT
eurjchem-782	101	21	c‐4	c‐4	NOUN
eurjchem-782	101	22	'	'	PUNCT
eurjchem-782	101	23	)	)	PUNCT
eurjchem-782	101	24	,	,	PUNCT
eurjchem-782	101	25	141.9	141.9	NUM
eurjchem-782	101	26	(	(	PUNCT
eurjchem-782	101	27	c‐1	c‐1	NOUN
eurjchem-782	101	28	"	"	PUNCT
eurjchem-782	101	29	)	)	PUNCT
eurjchem-782	101	30	,	,	PUNCT
eurjchem-782	101	31	133.8	133.8	NUM
eurjchem-782	101	32	(	(	PUNCT
eurjchem-782	101	33	c‐1	c‐1	NOUN
eurjchem-782	101	34	'	'	PUNCT
eurjchem-782	101	35	)	)	PUNCT
eurjchem-782	101	36	,	,	PUNCT
eurjchem-782	101	37	128.9	128.9	NUM
eurjchem-782	101	38	(	(	PUNCT
eurjchem-782	101	39	c‐3	c‐3	NOUN
eurjchem-782	101	40	'	'	PUNCT
eurjchem-782	101	41	,	,	PUNCT
eurjchem-782	101	42	c‐5	c‐5	NOUN
eurjchem-782	101	43	'	'	PUNCT
eurjchem-782	101	44	)	)	PUNCT
eurjchem-782	101	45	,	,	PUNCT
eurjchem-782	101	46	128.6	128.6	NUM
eurjchem-782	101	47	(	(	PUNCT
eurjchem-782	101	48	c‐2	c‐2	NOUN
eurjchem-782	101	49	'	'	PUNCT
eurjchem-782	101	50	,	,	PUNCT
eurjchem-782	101	51	c‐6	c‐6	NOUN
eurjchem-782	101	52	'	'	PUNCT
eurjchem-782	101	53	)	)	PUNCT
eurjchem-782	101	54	,	,	PUNCT
eurjchem-782	101	55	128.3	128.3	NUM
eurjchem-782	101	56	(	(	PUNCT
eurjchem-782	101	57	c‐3	c‐3	NOUN
eurjchem-782	101	58	"	"	PUNCT
eurjchem-782	101	59	,	,	PUNCT
eurjchem-782	101	60	c‐5	c‐5	NOUN
eurjchem-782	101	61	"	"	PUNCT
eurjchem-782	101	62	)	)	PUNCT
eurjchem-782	101	63	,	,	PUNCT
eurjchem-782	101	64	125.3	125.3	NUM
eurjchem-782	101	65	(	(	PUNCT
eurjchem-782	101	66	c‐	c‐	NOUN
eurjchem-782	101	67	4	4	NUM
eurjchem-782	101	68	"	"	PUNCT
eurjchem-782	101	69	)	)	PUNCT
eurjchem-782	101	70	,	,	PUNCT
eurjchem-782	101	71	125.0	125.0	NUM
eurjchem-782	101	72	(	(	PUNCT
eurjchem-782	101	73	c‐2	c‐2	NOUN
eurjchem-782	101	74	"	"	PUNCT
eurjchem-782	101	75	)	)	PUNCT
eurjchem-782	101	76	,	,	PUNCT
eurjchem-782	101	77	27.2	27.2	NUM
eurjchem-782	101	78	(	(	PUNCT
eurjchem-782	101	79	c‐2	c‐2	NOUN
eurjchem-782	101	80	)	)	PUNCT
eurjchem-782	101	81	,	,	PUNCT
eurjchem-782	101	82	25.4	25.4	NUM
eurjchem-782	101	83	(	(	PUNCT
eurjchem-782	101	84	c‐3	c‐3	NOUN
eurjchem-782	101	85	)	)	PUNCT
eurjchem-782	101	86	,	,	PUNCT
eurjchem-782	101	87	21.5	21.5	NUM
eurjchem-782	101	88	(	(	PUNCT
eurjchem-782	101	89	‐ch3	‐ch3	ADJ
eurjchem-782	101	90	)	)	PUNCT
eurjchem-782	101	91	,	,	PUNCT
eurjchem-782	101	92	14.8	14.8	NUM
eurjchem-782	101	93	(	(	PUNCT
eurjchem-782	101	94	c‐4	c‐4	PROPN
eurjchem-782	101	95	)	)	PUNCT
eurjchem-782	101	96	.	.	PUNCT
eurjchem-782	102	1	ms	ms	PROPN
eurjchem-782	102	2	(	(	PUNCT
eurjchem-782	102	3	esi	esi	PROPN
eurjchem-782	102	4	,	,	PUNCT
eurjchem-782	102	5	m	m	PROPN
eurjchem-782	102	6	/	/	SYM
eurjchem-782	102	7	z	z	NOUN
eurjchem-782	102	8	):	):	PUNCT
eurjchem-782	102	9	236.12	236.12	NUM
eurjchem-782	102	10	(	(	PUNCT
eurjchem-782	102	11	m+	m+	NUM
eurjchem-782	102	12	)	)	PUNCT
eurjchem-782	102	13	.	.	PUNCT
eurjchem-782	103	1	anal	anal	PROPN
eurjchem-782	103	2	.	.	PUNCT
eurjchem-782	103	3	calcd	calcd	NOUN
eurjchem-782	103	4	.	.	PUNCT
eurjchem-782	104	1	for	for	ADP
eurjchem-782	104	2	c17h16o	c17h16o	NOUN
eurjchem-782	104	3	:	:	PUNCT
eurjchem-782	104	4	c	c	X
eurjchem-782	104	5	,	,	PUNCT
eurjchem-782	104	6	86.40	86.40	NUM
eurjchem-782	104	7	;	;	PUNCT
eurjchem-782	104	8	h	h	NOUN
eurjchem-782	104	9	,	,	PUNCT
eurjchem-782	104	10	6.82	6.82	NUM
eurjchem-782	104	11	.	.	PUNCT
eurjchem-782	104	12	found	find	VERB
eurjchem-782	104	13	:	:	PUNCT
eurjchem-782	105	1	c	c	X
eurjchem-782	105	2	,	,	PUNCT
eurjchem-782	105	3	86.41	86.41	NUM
eurjchem-782	105	4	;	;	PUNCT
eurjchem-782	105	5	h	h	NOUN
eurjchem-782	105	6	,	,	PUNCT
eurjchem-782	105	7	6.79	6.79	NUM
eurjchem-782	105	8	%	%	NOUN
eurjchem-782	105	9	.	.	PUNCT
eurjchem-782	106	1	(	(	PUNCT
eurjchem-782	106	2	4‐methoxyphenyl)(2‐phenylcyclopropyl)methanone	4‐methoxyphenyl)(2‐phenylcyclopropyl)methanone	NOUN
eurjchem-782	106	3	(	(	PUNCT
eurjchem-782	106	4	4c	4c	NOUN
eurjchem-782	106	5	):	):	PUNCT
eurjchem-782	106	6	color	color	NOUN
eurjchem-782	106	7	:	:	PUNCT
eurjchem-782	106	8	dark	dark	ADJ
eurjchem-782	106	9	brown	brown	ADJ
eurjchem-782	106	10	semisolid	semisolid	NOUN
eurjchem-782	106	11	.	.	PUNCT
eurjchem-782	107	1	yield	yield	NOUN
eurjchem-782	107	2	:	:	PUNCT
eurjchem-782	107	3	74.30	74.30	NUM
eurjchem-782	107	4	%	%	NOUN
eurjchem-782	107	5	.	.	PUNCT
eurjchem-782	108	1	ir	ir	PROPN
eurjchem-782	108	2	(	(	PUNCT
eurjchem-782	108	3	kbr	kbr	PROPN
eurjchem-782	108	4	,	,	PUNCT
eurjchem-782	108	5	ν	ν	PROPN
eurjchem-782	108	6	,	,	PUNCT
eurjchem-782	108	7	cm‐1	cm‐1	PROPN
eurjchem-782	108	8	):	):	PUNCT
eurjchem-782	108	9	3163	3163	NUM
eurjchem-782	108	10	,	,	PUNCT
eurjchem-782	108	11	2955	2955	NUM
eurjchem-782	108	12	(	(	PUNCT
eurjchem-782	108	13	ar‐ch	ar‐ch	NUM
eurjchem-782	108	14	)	)	PUNCT
eurjchem-782	108	15	,	,	PUNCT
eurjchem-782	108	16	1676	1676	NUM
eurjchem-782	108	17	(	(	PUNCT
eurjchem-782	108	18	c	c	NOUN
eurjchem-782	108	19	=	=	NOUN
eurjchem-782	108	20	o	o	NOUN
eurjchem-782	108	21	)	)	PUNCT
eurjchem-782	108	22	.	.	PUNCT
eurjchem-782	109	1	1h	1h	NUM
eurjchem-782	109	2	nmr	nmr	NOUN
eurjchem-782	109	3	(	(	PUNCT
eurjchem-782	109	4	400	400	NUM
eurjchem-782	109	5	mhz	mhz	NOUN
eurjchem-782	109	6	,	,	PUNCT
eurjchem-782	109	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-782	109	8	,	,	PUNCT
eurjchem-782	109	9	δ	δ	PROPN
eurjchem-782	109	10	,	,	PUNCT
eurjchem-782	109	11	ppm	ppm	NOUN
eurjchem-782	109	12	):	):	PUNCT
eurjchem-782	109	13	7.95‐7.31	7.95‐7.31	NUM
eurjchem-782	109	14	(	(	PUNCT
eurjchem-782	109	15	m	m	PROPN
eurjchem-782	109	16	,	,	PUNCT
eurjchem-782	109	17	9h	9h	NUM
eurjchem-782	109	18	,	,	PUNCT
eurjchem-782	109	19	ar‐h	ar‐h	NOUN
eurjchem-782	109	20	)	)	PUNCT
eurjchem-782	109	21	,	,	PUNCT
eurjchem-782	109	22	3.85	3.85	NUM
eurjchem-782	109	23	(	(	PUNCT
eurjchem-782	109	24	s	s	PROPN
eurjchem-782	109	25	,	,	PUNCT
eurjchem-782	109	26	3h	3h	NUM
eurjchem-782	109	27	,	,	PUNCT
eurjchem-782	109	28	och3	och3	ADJ
eurjchem-782	109	29	)	)	PUNCT
eurjchem-782	109	30	,	,	PUNCT
eurjchem-782	109	31	2.20‐2.03	2.20‐2.03	NUM
eurjchem-782	109	32	(	(	PUNCT
eurjchem-782	109	33	m	m	PROPN
eurjchem-782	109	34	,	,	PUNCT
eurjchem-782	109	35	2h	2h	NUM
eurjchem-782	109	36	,	,	PUNCT
eurjchem-782	109	37	cyclopro‐ch	cyclopro‐ch	NUM
eurjchem-782	109	38	)	)	PUNCT
eurjchem-782	109	39	,	,	PUNCT
eurjchem-782	109	40	0.80	0.80	NUM
eurjchem-782	109	41	(	(	PUNCT
eurjchem-782	109	42	d	d	NOUN
eurjchem-782	109	43	,	,	PUNCT
eurjchem-782	109	44	2h	2h	NUM
eurjchem-782	109	45	,	,	PUNCT
eurjchem-782	109	46	c4‐ch2	c4‐ch2	PROPN
eurjchem-782	109	47	)	)	PUNCT
eurjchem-782	109	48	.	.	PUNCT
eurjchem-782	110	1	13c	13c	NOUN
eurjchem-782	110	2	nmr	nmr	NOUN
eurjchem-782	110	3	(	(	PUNCT
eurjchem-782	110	4	100	100	NUM
eurjchem-782	110	5	mhz	mhz	NOUN
eurjchem-782	110	6	,	,	PUNCT
eurjchem-782	110	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-782	110	8	,	,	PUNCT
eurjchem-782	110	9	δ	δ	PROPN
eurjchem-782	110	10	,	,	PUNCT
eurjchem-782	110	11	ppm	ppm	NUM
eurjchem-782	110	12	):	):	PUNCT
eurjchem-782	110	13	192.0	192.0	NUM
eurjchem-782	110	14	(	(	PUNCT
eurjchem-782	110	15	c‐1	c‐1	NOUN
eurjchem-782	110	16	)	)	PUNCT
eurjchem-782	110	17	,	,	PUNCT
eurjchem-782	110	18	165.2	165.2	NUM
eurjchem-782	110	19	(	(	PUNCT
eurjchem-782	110	20	c‐4	c‐4	PROPN
eurjchem-782	110	21	'	'	PUNCT
eurjchem-782	110	22	)	)	PUNCT
eurjchem-782	110	23	,	,	PUNCT
eurjchem-782	110	24	141.7	141.7	NUM
eurjchem-782	110	25	(	(	PUNCT
eurjchem-782	110	26	c‐4	c‐4	PROPN
eurjchem-782	110	27	"	"	PUNCT
eurjchem-782	110	28	)	)	PUNCT
eurjchem-782	110	29	,	,	PUNCT
eurjchem-782	110	30	129.9	129.9	NUM
eurjchem-782	110	31	(	(	PUNCT
eurjchem-782	110	32	c‐2	c‐2	NOUN
eurjchem-782	110	33	'	'	PUNCT
eurjchem-782	110	34	,	,	PUNCT
eurjchem-782	110	35	c‐6	c‐6	NOUN
eurjchem-782	110	36	'	'	PUNCT
eurjchem-782	110	37	)	)	PUNCT
eurjchem-782	110	38	,	,	PUNCT
eurjchem-782	110	39	129.3	129.3	NUM
eurjchem-782	110	40	(	(	PUNCT
eurjchem-782	110	41	c‐1	c‐1	NOUN
eurjchem-782	110	42	'	'	PUNCT
eurjchem-782	110	43	)	)	PUNCT
eurjchem-782	110	44	,	,	PUNCT
eurjchem-782	110	45	128.3	128.3	NUM
eurjchem-782	110	46	(	(	PUNCT
eurjchem-782	110	47	c‐3	c‐3	NOUN
eurjchem-782	110	48	"	"	PUNCT
eurjchem-782	110	49	,	,	PUNCT
eurjchem-782	110	50	c‐5	c‐5	NOUN
eurjchem-782	110	51	"	"	PUNCT
eurjchem-782	110	52	)	)	PUNCT
eurjchem-782	110	53	,	,	PUNCT
eurjchem-782	110	54	125.4	125.4	NUM
eurjchem-782	110	55	(	(	PUNCT
eurjchem-782	110	56	c‐2	c‐2	NOUN
eurjchem-782	110	57	"	"	PUNCT
eurjchem-782	110	58	,	,	PUNCT
eurjchem-782	110	59	c‐6	c‐6	NOUN
eurjchem-782	110	60	"	"	PUNCT
eurjchem-782	110	61	)	)	PUNCT
eurjchem-782	110	62	,	,	PUNCT
eurjchem-782	110	63	121.0	121.0	NUM
eurjchem-782	110	64	(	(	PUNCT
eurjchem-782	110	65	c‐4	c‐4	PROPN
eurjchem-782	110	66	"	"	PUNCT
eurjchem-782	110	67	)	)	PUNCT
eurjchem-782	110	68	,	,	PUNCT
eurjchem-782	110	69	114.5	114.5	NUM
eurjchem-782	110	70	(	(	PUNCT
eurjchem-782	110	71	c‐3	c‐3	NOUN
eurjchem-782	110	72	'	'	PUNCT
eurjchem-782	110	73	,	,	PUNCT
eurjchem-782	110	74	c‐5	c‐5	NOUN
eurjchem-782	110	75	'	'	PUNCT
eurjchem-782	110	76	)	)	PUNCT
eurjchem-782	110	77	,	,	PUNCT
eurjchem-782	110	78	55.7	55.7	NUM
eurjchem-782	110	79	(	(	PUNCT
eurjchem-782	110	80	‐och3	‐och3	NOUN
eurjchem-782	110	81	)	)	PUNCT
eurjchem-782	110	82	,	,	PUNCT
eurjchem-782	110	83	27.3	27.3	NUM
eurjchem-782	110	84	(	(	PUNCT
eurjchem-782	110	85	c‐2	c‐2	NOUN
eurjchem-782	110	86	)	)	PUNCT
eurjchem-782	110	87	,	,	PUNCT
eurjchem-782	110	88	25.5	25.5	NUM
eurjchem-782	110	89	(	(	PUNCT
eurjchem-782	110	90	c‐3	c‐3	NOUN
eurjchem-782	110	91	)	)	PUNCT
eurjchem-782	110	92	,	,	PUNCT
eurjchem-782	110	93	14.4	14.4	NUM
eurjchem-782	110	94	(	(	PUNCT
eurjchem-782	110	95	c‐4	c‐4	PROPN
eurjchem-782	110	96	)	)	PUNCT
eurjchem-782	110	97	.	.	PUNCT
eurjchem-782	111	1	ms	ms	PROPN
eurjchem-782	111	2	(	(	PUNCT
eurjchem-782	111	3	esi	esi	PROPN
eurjchem-782	111	4	,	,	PUNCT
eurjchem-782	111	5	m	m	PROPN
eurjchem-782	111	6	/	/	SYM
eurjchem-782	111	7	z	z	NOUN
eurjchem-782	111	8	):	):	PUNCT
eurjchem-782	111	9	252.14	252.14	NUM
eurjchem-782	111	10	(	(	PUNCT
eurjchem-782	111	11	m+	m+	NUM
eurjchem-782	111	12	)	)	PUNCT
eurjchem-782	111	13	.	.	PUNCT
eurjchem-782	112	1	anal	anal	PROPN
eurjchem-782	112	2	.	.	PUNCT
eurjchem-782	112	3	calcd	calcd	NOUN
eurjchem-782	112	4	.	.	PUNCT
eurjchem-782	113	1	for	for	ADP
eurjchem-782	113	2	c17h16o2	c17h16o2	NOUN
eurjchem-782	113	3	;	;	PUNCT
eurjchem-782	113	4	c	c	X
eurjchem-782	113	5	,	,	PUNCT
eurjchem-782	113	6	80.93	80.93	NUM
eurjchem-782	113	7	;	;	PUNCT
eurjchem-782	113	8	h	h	NOUN
eurjchem-782	113	9	,	,	PUNCT
eurjchem-782	113	10	6.39	6.39	NUM
eurjchem-782	113	11	.	.	PUNCT
eurjchem-782	113	12	found	find	VERB
eurjchem-782	113	13	:	:	PUNCT
eurjchem-782	114	1	c	c	X
eurjchem-782	114	2	,	,	PUNCT
eurjchem-782	114	3	80.90	80.90	NUM
eurjchem-782	114	4	;	;	PUNCT
eurjchem-782	114	5	h	h	NOUN
eurjchem-782	114	6	,	,	PUNCT
eurjchem-782	114	7	6.35	6.35	NUM
eurjchem-782	114	8	%	%	NOUN
eurjchem-782	114	9	.	.	PUNCT
eurjchem-782	115	1	(	(	PUNCT
eurjchem-782	115	2	4‐(methylthio)phenyl)(2‐phenylcyclopropyl)methanone	4‐(methylthio)phenyl)(2‐phenylcyclopropyl)methanone	X
eurjchem-782	115	3	(	(	PUNCT
eurjchem-782	115	4	4d	4d	NUM
eurjchem-782	115	5	):	):	PUNCT
eurjchem-782	115	6	color	color	NOUN
eurjchem-782	115	7	:	:	PUNCT
eurjchem-782	115	8	dark	dark	ADJ
eurjchem-782	115	9	brown	brown	ADJ
eurjchem-782	115	10	semisolid	semisolid	NOUN
eurjchem-782	115	11	.	.	PUNCT
eurjchem-782	116	1	yield	yield	NOUN
eurjchem-782	116	2	:	:	PUNCT
eurjchem-782	116	3	71.80	71.80	NUM
eurjchem-782	116	4	%	%	NOUN
eurjchem-782	116	5	.	.	PUNCT
eurjchem-782	117	1	ir	ir	PROPN
eurjchem-782	117	2	(	(	PUNCT
eurjchem-782	117	3	kbr	kbr	PROPN
eurjchem-782	117	4	,	,	PUNCT
eurjchem-782	117	5	ν	ν	PROPN
eurjchem-782	117	6	,	,	PUNCT
eurjchem-782	117	7	cm‐1	cm‐1	PROPN
eurjchem-782	117	8	):	):	PUNCT
eurjchem-782	117	9	3178	3178	NUM
eurjchem-782	117	10	,	,	PUNCT
eurjchem-782	117	11	2965	2965	NUM
eurjchem-782	117	12	(	(	PUNCT
eurjchem-782	117	13	ar‐ch	ar‐ch	NUM
eurjchem-782	117	14	)	)	PUNCT
eurjchem-782	117	15	,	,	PUNCT
eurjchem-782	117	16	1687	1687	NUM
eurjchem-782	117	17	(	(	PUNCT
eurjchem-782	117	18	c	c	NOUN
eurjchem-782	117	19	=	=	NOUN
eurjchem-782	117	20	o	o	NOUN
eurjchem-782	117	21	)	)	PUNCT
eurjchem-782	117	22	.	.	PUNCT
eurjchem-782	118	1	1h	1h	NUM
eurjchem-782	118	2	nmr	nmr	NOUN
eurjchem-782	118	3	(	(	PUNCT
eurjchem-782	118	4	400	400	NUM
eurjchem-782	118	5	mhz	mhz	NOUN
eurjchem-782	118	6	,	,	PUNCT
eurjchem-782	118	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-782	118	8	,	,	PUNCT
eurjchem-782	118	9	δ	δ	PROPN
eurjchem-782	118	10	,	,	PUNCT
eurjchem-782	118	11	ppm	ppm	NOUN
eurjchem-782	118	12	):	):	PUNCT
eurjchem-782	118	13	7.97‐7.26	7.97‐7.26	NUM
eurjchem-782	118	14	(	(	PUNCT
eurjchem-782	118	15	m	m	PROPN
eurjchem-782	118	16	,	,	PUNCT
eurjchem-782	118	17	9h	9h	NUM
eurjchem-782	118	18	,	,	PUNCT
eurjchem-782	118	19	ar‐h	ar‐h	NOUN
eurjchem-782	118	20	)	)	PUNCT
eurjchem-782	118	21	,	,	PUNCT
eurjchem-782	118	22	2.53	2.53	NUM
eurjchem-782	118	23	(	(	PUNCT
eurjchem-782	118	24	s	s	PROPN
eurjchem-782	118	25	,	,	PUNCT
eurjchem-782	118	26	3h	3h	NUM
eurjchem-782	118	27	,	,	PUNCT
eurjchem-782	118	28	sch3	sch3	PROPN
eurjchem-782	118	29	)	)	PUNCT
eurjchem-782	118	30	,	,	PUNCT
eurjchem-782	118	31	2.21‐2.05	2.21‐2.05	NUM
eurjchem-782	118	32	(	(	PUNCT
eurjchem-782	118	33	m	m	PROPN
eurjchem-782	118	34	,	,	PUNCT
eurjchem-782	118	35	2h	2h	NUM
eurjchem-782	118	36	,	,	PUNCT
eurjchem-782	118	37	cyclopro‐ch	cyclopro‐ch	NUM
eurjchem-782	118	38	)	)	PUNCT
eurjchem-782	118	39	,	,	PUNCT
eurjchem-782	118	40	0.83	0.83	NUM
eurjchem-782	118	41	(	(	PUNCT
eurjchem-782	118	42	d	d	PROPN
eurjchem-782	118	43	,	,	PUNCT
eurjchem-782	118	44	2h	2h	NUM
eurjchem-782	118	45	,	,	PUNCT
eurjchem-782	118	46	c4‐ch2	c4‐ch2	PROPN
eurjchem-782	118	47	)	)	PUNCT
eurjchem-782	118	48	.	.	PUNCT
eurjchem-782	119	1	13c	13c	NOUN
eurjchem-782	119	2	nmr	nmr	NOUN
eurjchem-782	119	3	(	(	PUNCT
eurjchem-782	119	4	100	100	NUM
eurjchem-782	119	5	mhz	mhz	NOUN
eurjchem-782	119	6	,	,	PUNCT
eurjchem-782	119	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-782	119	8	,	,	PUNCT
eurjchem-782	119	9	δ	δ	PROPN
eurjchem-782	119	10	,	,	PUNCT
eurjchem-782	119	11	ppm	ppm	NUM
eurjchem-782	119	12	):	):	PUNCT
eurjchem-782	119	13	192.3	192.3	NUM
eurjchem-782	119	14	(	(	PUNCT
eurjchem-782	119	15	c‐1	c‐1	NOUN
eurjchem-782	119	16	)	)	PUNCT
eurjchem-782	119	17	,	,	PUNCT
eurjchem-782	119	18	143.9	143.9	NUM
eurjchem-782	119	19	(	(	PUNCT
eurjchem-782	119	20	c‐4	c‐4	PROPN
eurjchem-782	119	21	'	'	PUNCT
eurjchem-782	119	22	)	)	PUNCT
eurjchem-782	119	23	,	,	PUNCT
eurjchem-782	119	24	141.7	141.7	NUM
eurjchem-782	119	25	(	(	PUNCT
eurjchem-782	119	26	c‐1	c‐1	NOUN
eurjchem-782	119	27	"	"	PUNCT
eurjchem-782	119	28	)	)	PUNCT
eurjchem-782	119	29	,	,	PUNCT
eurjchem-782	119	30	133.3	133.3	NUM
eurjchem-782	119	31	(	(	PUNCT
eurjchem-782	119	32	c‐1	c‐1	NOUN
eurjchem-782	119	33	'	'	PUNCT
eurjchem-782	119	34	)	)	PUNCT
eurjchem-782	119	35	,	,	PUNCT
eurjchem-782	119	36	132.0	132.0	NUM
eurjchem-782	119	37	(	(	PUNCT
eurjchem-782	119	38	c‐2	c‐2	NOUN
eurjchem-782	119	39	'	'	PUNCT
eurjchem-782	119	40	,	,	PUNCT
eurjchem-782	119	41	c‐6	c‐6	NOUN
eurjchem-782	119	42	'	'	PUNCT
eurjchem-782	119	43	)	)	PUNCT
eurjchem-782	119	44	,	,	PUNCT
eurjchem-782	119	45	128.5	128.5	NUM
eurjchem-782	119	46	(	(	PUNCT
eurjchem-782	119	47	c‐3	c‐3	NOUN
eurjchem-782	119	48	"	"	PUNCT
eurjchem-782	119	49	,	,	PUNCT
eurjchem-782	119	50	c‐5	c‐5	NOUN
eurjchem-782	119	51	"	"	PUNCT
eurjchem-782	119	52	)	)	PUNCT
eurjchem-782	119	53	,	,	PUNCT
eurjchem-782	119	54	126.3	126.3	NUM
eurjchem-782	119	55	(	(	PUNCT
eurjchem-782	119	56	c‐3	c‐3	NOUN
eurjchem-782	119	57	'	'	PUNCT
eurjchem-782	119	58	,	,	PUNCT
eurjchem-782	119	59	c‐5	c‐5	NOUN
eurjchem-782	119	60	'	'	PUNCT
eurjchem-782	119	61	)	)	PUNCT
eurjchem-782	119	62	,	,	PUNCT
eurjchem-782	119	63	125.2	125.2	NUM
eurjchem-782	119	64	(	(	PUNCT
eurjchem-782	119	65	c‐4	c‐4	PROPN
eurjchem-782	119	66	"	"	PUNCT
eurjchem-782	119	67	)	)	PUNCT
eurjchem-782	119	68	,	,	PUNCT
eurjchem-782	119	69	125.0	125.0	NUM
eurjchem-782	119	70	(	(	PUNCT
eurjchem-782	119	71	c‐2	c‐2	NOUN
eurjchem-782	119	72	"	"	PUNCT
eurjchem-782	119	73	,	,	PUNCT
eurjchem-782	119	74	c‐6	c‐6	NOUN
eurjchem-782	119	75	"	"	PUNCT
eurjchem-782	119	76	)	)	PUNCT
eurjchem-782	119	77	,	,	PUNCT
eurjchem-782	119	78	27.3	27.3	NUM
eurjchem-782	119	79	(	(	PUNCT
eurjchem-782	119	80	c‐2	c‐2	NOUN
eurjchem-782	119	81	)	)	PUNCT
eurjchem-782	119	82	,	,	PUNCT
eurjchem-782	119	83	25.4	25.4	NUM
eurjchem-782	119	84	(	(	PUNCT
eurjchem-782	119	85	c‐	c‐	NOUN
eurjchem-782	119	86	3	3	NUM
eurjchem-782	119	87	)	)	PUNCT
eurjchem-782	119	88	,	,	PUNCT
eurjchem-782	119	89	‐14.5(‐sch3	‐14.5(‐sch3	NOUN
eurjchem-782	119	90	)	)	PUNCT
eurjchem-782	119	91	,	,	PUNCT
eurjchem-782	119	92	14.1	14.1	NUM
eurjchem-782	119	93	(	(	PUNCT
eurjchem-782	119	94	c‐4	c‐4	PROPN
eurjchem-782	119	95	)	)	PUNCT
eurjchem-782	119	96	.	.	PUNCT
eurjchem-782	120	1	ms	ms	PROPN
eurjchem-782	120	2	(	(	PUNCT
eurjchem-782	120	3	esi	esi	PROPN
eurjchem-782	120	4	,	,	PUNCT
eurjchem-782	120	5	m	m	PROPN
eurjchem-782	120	6	/	/	SYM
eurjchem-782	120	7	z	z	NOUN
eurjchem-782	120	8	):	):	PUNCT
eurjchem-782	120	9	268.13	268.13	NUM
eurjchem-782	120	10	(	(	PUNCT
eurjchem-782	120	11	m+	m+	NUM
eurjchem-782	120	12	)	)	PUNCT
eurjchem-782	120	13	.	.	PUNCT
eurjchem-782	121	1	anal	anal	PROPN
eurjchem-782	121	2	.	.	PUNCT
eurjchem-782	121	3	calcd	calcd	NOUN
eurjchem-782	121	4	.	.	PUNCT
eurjchem-782	122	1	for	for	ADP
eurjchem-782	122	2	c17h16os	c17h16os	PROPN
eurjchem-782	122	3	:	:	PUNCT
eurjchem-782	122	4	c	c	X
eurjchem-782	122	5	,	,	PUNCT
eurjchem-782	122	6	76.08	76.08	NUM
eurjchem-782	122	7	;	;	PUNCT
eurjchem-782	122	8	h	h	NOUN
eurjchem-782	122	9	,	,	PUNCT
eurjchem-782	122	10	6.01	6.01	NUM
eurjchem-782	122	11	.	.	PUNCT
eurjchem-782	122	12	found	find	VERB
eurjchem-782	122	13	:	:	PUNCT
eurjchem-782	123	1	c	c	X
eurjchem-782	123	2	,	,	PUNCT
eurjchem-782	123	3	76.05	76.05	NUM
eurjchem-782	123	4	;	;	PUNCT
eurjchem-782	123	5	h	h	NOUN
eurjchem-782	123	6	,	,	PUNCT
eurjchem-782	123	7	6.03	6.03	NUM
eurjchem-782	123	8	%	%	NOUN
eurjchem-782	123	9	.	.	PUNCT
eurjchem-782	124	1	2.2.3	2.2.3	X
eurjchem-782	124	2	.	.	PUNCT
eurjchem-782	124	3	general	general	ADJ
eurjchem-782	124	4	procedure	procedure	NOUN
eurjchem-782	124	5	for	for	ADP
eurjchem-782	124	6	the	the	DET
eurjchem-782	124	7	synthesis	synthesis	NOUN
eurjchem-782	124	8	of	of	ADP
eurjchem-782	124	9	tetralones	tetralone	NOUN
eurjchem-782	124	10	(	(	PUNCT
eurjchem-782	124	11	5a‐	5a‐	NUM
eurjchem-782	124	12	d	d	X
eurjchem-782	124	13	)	)	PUNCT
eurjchem-782	124	14	cyclopropyl	cyclopropyl	PROPN
eurjchem-782	124	15	ketones	ketone	NOUN
eurjchem-782	124	16	(	(	PUNCT
eurjchem-782	124	17	0.0080	0.0080	NUM
eurjchem-782	124	18	mol	mol	NOUN
eurjchem-782	124	19	)	)	PUNCT
eurjchem-782	124	20	were	be	AUX
eurjchem-782	124	21	dissolved	dissolve	VERB
eurjchem-782	124	22	in	in	ADP
eurjchem-782	124	23	dry	dry	ADJ
eurjchem-782	124	24	dichloromethane	dichloromethane	NOUN
eurjchem-782	124	25	(	(	PUNCT
eurjchem-782	124	26	50	50	NUM
eurjchem-782	124	27	ml	ml	NOUN
eurjchem-782	124	28	)	)	PUNCT
eurjchem-782	124	29	.	.	PUNCT
eurjchem-782	125	1	acetic	acetic	ADJ
eurjchem-782	125	2	anhydride	anhydride	NOUN
eurjchem-782	125	3	(	(	PUNCT
eurjchem-782	125	4	0.8	0.8	NUM
eurjchem-782	125	5	g	g	NOUN
eurjchem-782	125	6	,	,	PUNCT
eurjchem-782	125	7	0.0080	0.0080	NUM
eurjchem-782	125	8	mol	mol	NOUN
eurjchem-782	125	9	)	)	PUNCT
eurjchem-782	125	10	and	and	CCONJ
eurjchem-782	125	11	anhydrous	anhydrous	ADJ
eurjchem-782	125	12	stannic	stannic	ADJ
eurjchem-782	125	13	chloride	chloride	NOUN
eurjchem-782	125	14	(	(	PUNCT
eurjchem-782	125	15	0.8	0.8	NUM
eurjchem-782	125	16	g	g	NOUN
eurjchem-782	125	17	,	,	PUNCT
eurjchem-782	125	18	0.0080	0.0080	NUM
eurjchem-782	125	19	mol	mol	NOUN
eurjchem-782	125	20	)	)	PUNCT
eurjchem-782	125	21	were	be	AUX
eurjchem-782	125	22	added	add	VERB
eurjchem-782	125	23	under	under	ADP
eurjchem-782	125	24	nitrogen	nitrogen	NOUN
eurjchem-782	125	25	gas	gas	NOUN
eurjchem-782	125	26	atmosphere	atmosphere	NOUN
eurjchem-782	125	27	.	.	PUNCT
eurjchem-782	126	1	the	the	DET
eurjchem-782	126	2	resultant	resultant	NOUN
eurjchem-782	126	3	reaction	reaction	NOUN
eurjchem-782	126	4	mixture	mixture	NOUN
eurjchem-782	126	5	was	be	AUX
eurjchem-782	126	6	stirred	stir	VERB
eurjchem-782	126	7	at	at	ADP
eurjchem-782	126	8	25‐28	25‐28	ADV
eurjchem-782	126	9	oc	oc	NOUN
eurjchem-782	126	10	for	for	ADP
eurjchem-782	126	11	3h	3h	NUM
eurjchem-782	126	12	.	.	PUNCT
eurjchem-782	127	1	the	the	DET
eurjchem-782	127	2	completion	completion	NOUN
eurjchem-782	127	3	of	of	ADP
eurjchem-782	127	4	reaction	reaction	NOUN
eurjchem-782	127	5	was	be	AUX
eurjchem-782	127	6	known	know	VERB
eurjchem-782	127	7	by	by	ADP
eurjchem-782	127	8	tlc	tlc	PROPN
eurjchem-782	127	9	.	.	PUNCT
eurjchem-782	128	1	the	the	DET
eurjchem-782	128	2	reaction	reaction	NOUN
eurjchem-782	128	3	mixture	mixture	NOUN
eurjchem-782	128	4	was	be	AUX
eurjchem-782	128	5	poured	pour	VERB
eurjchem-782	128	6	into	into	ADP
eurjchem-782	128	7	5	5	NUM
eurjchem-782	128	8	%	%	NOUN
eurjchem-782	128	9	naoh	naoh	NOUN
eurjchem-782	128	10	solution	solution	NOUN
eurjchem-782	128	11	(	(	PUNCT
eurjchem-782	128	12	20	20	NUM
eurjchem-782	128	13	ml	ml	NOUN
eurjchem-782	128	14	)	)	PUNCT
eurjchem-782	128	15	.	.	PUNCT
eurjchem-782	129	1	the	the	DET
eurjchem-782	129	2	product	product	NOUN
eurjchem-782	129	3	was	be	AUX
eurjchem-782	129	4	extracted	extract	VERB
eurjchem-782	129	5	into	into	ADP
eurjchem-782	129	6	dichloromethane	dichloromethane	NOUN
eurjchem-782	129	7	.	.	PUNCT
eurjchem-782	130	1	the	the	DET
eurjchem-782	130	2	organic	organic	ADJ
eurjchem-782	130	3	layer	layer	NOUN
eurjchem-782	130	4	was	be	AUX
eurjchem-782	130	5	washed	wash	VERB
eurjchem-782	130	6	with	with	ADP
eurjchem-782	130	7	water	water	NOUN
eurjchem-782	130	8	,	,	PUNCT
eurjchem-782	130	9	dried	dry	VERB
eurjchem-782	130	10	over	over	ADP
eurjchem-782	130	11	anhyd	anhyd	NOUN
eurjchem-782	130	12	.	.	PUNCT
eurjchem-782	131	1	na2so4	na2so4	NOUN
eurjchem-782	131	2	and	and	CCONJ
eurjchem-782	131	3	concentrated	concentrate	VERB
eurjchem-782	131	4	under	under	ADP
eurjchem-782	131	5	vacuum	vacuum	NOUN
eurjchem-782	131	6	using	use	VERB
eurjchem-782	131	7	a	a	DET
eurjchem-782	131	8	rotary	rotary	ADJ
eurjchem-782	131	9	evaporator	evaporator	NOUN
eurjchem-782	131	10	to	to	PART
eurjchem-782	131	11	give	give	VERB
eurjchem-782	131	12	brown	brown	ADJ
eurjchem-782	131	13	residue	residue	NOUN
eurjchem-782	131	14	.	.	PUNCT
eurjchem-782	132	1	the	the	DET
eurjchem-782	132	2	product	product	NOUN
eurjchem-782	132	3	was	be	AUX
eurjchem-782	132	4	purified	purify	VERB
eurjchem-782	132	5	by	by	ADP
eurjchem-782	132	6	column	column	NOUN
eurjchem-782	132	7	chromatography	chromatography	NOUN
eurjchem-782	132	8	using	use	VERB
eurjchem-782	132	9	silica	silica	NOUN
eurjchem-782	132	10	gel	gel	NOUN
eurjchem-782	132	11	(	(	PUNCT
eurjchem-782	132	12	60‐	60‐	NUM
eurjchem-782	132	13	120	120	NUM
eurjchem-782	132	14	mesh	mesh	NOUN
eurjchem-782	132	15	)	)	PUNCT
eurjchem-782	132	16	as	as	ADP
eurjchem-782	132	17	adsorbent	adsorbent	NOUN
eurjchem-782	132	18	and	and	CCONJ
eurjchem-782	132	19	benzene	benzene	NOUN
eurjchem-782	132	20	as	as	ADP
eurjchem-782	132	21	eluent	eluent	NOUN
eurjchem-782	132	22	.	.	PUNCT
eurjchem-782	133	1	the	the	DET
eurjchem-782	133	2	benzene	benzene	NOUN
eurjchem-782	133	3	solution	solution	NOUN
eurjchem-782	133	4	was	be	AUX
eurjchem-782	133	5	concentrated	concentrate	VERB
eurjchem-782	133	6	to	to	ADP
eurjchem-782	133	7	a	a	DET
eurjchem-782	133	8	small	small	ADJ
eurjchem-782	133	9	volume	volume	NOUN
eurjchem-782	133	10	(	(	PUNCT
eurjchem-782	133	11	20	20	NUM
eurjchem-782	133	12	ml	ml	NOUN
eurjchem-782	133	13	)	)	PUNCT
eurjchem-782	133	14	and	and	CCONJ
eurjchem-782	133	15	hexane	hexane	NOUN
eurjchem-782	133	16	(	(	PUNCT
eurjchem-782	133	17	100	100	NUM
eurjchem-782	133	18	ml	ml	NOUN
eurjchem-782	133	19	)	)	PUNCT
eurjchem-782	133	20	was	be	AUX
eurjchem-782	133	21	added	add	VERB
eurjchem-782	133	22	drop	drop	NOUN
eurjchem-782	133	23	wise	wise	ADJ
eurjchem-782	133	24	to	to	PART
eurjchem-782	133	25	give	give	VERB
eurjchem-782	133	26	products	product	NOUN
eurjchem-782	133	27	in	in	ADP
eurjchem-782	133	28	good	good	ADJ
eurjchem-782	133	29	yields	yield	NOUN
eurjchem-782	133	30	.	.	PUNCT
eurjchem-782	134	1	they	they	PRON
eurjchem-782	134	2	were	be	AUX
eurjchem-782	134	3	recrystallized	recrystallize	VERB
eurjchem-782	134	4	from	from	ADP
eurjchem-782	134	5	ethanol	ethanol	NOUN
eurjchem-782	134	6	(	(	PUNCT
eurjchem-782	134	7	scheme	scheme	NOUN
eurjchem-782	134	8	1	1	NUM
eurjchem-782	134	9	)	)	PUNCT
eurjchem-782	134	10	.	.	PUNCT
eurjchem-782	135	1	4‐phenyl‐3,4‐dihydronaphthalen‐1(2h)‐one	4‐phenyl‐3,4‐dihydronaphthalen‐1(2h)‐one	NOUN
eurjchem-782	135	2	(	(	PUNCT
eurjchem-782	135	3	5a	5a	NUM
eurjchem-782	135	4	):	):	PUNCT
eurjchem-782	135	5	color	color	NOUN
eurjchem-782	135	6	:	:	PUNCT
eurjchem-782	135	7	dark	dark	ADJ
eurjchem-782	135	8	semisolid	semisolid	NOUN
eurjchem-782	135	9	.	.	PUNCT
eurjchem-782	136	1	yield	yield	NOUN
eurjchem-782	136	2	:	:	PUNCT
eurjchem-782	136	3	75.56	75.56	NUM
eurjchem-782	136	4	%	%	NOUN
eurjchem-782	136	5	.	.	PUNCT
eurjchem-782	137	1	ir	ir	PROPN
eurjchem-782	137	2	(	(	PUNCT
eurjchem-782	137	3	kbr	kbr	PROPN
eurjchem-782	137	4	,	,	PUNCT
eurjchem-782	137	5	ν	ν	PROPN
eurjchem-782	137	6	,	,	PUNCT
eurjchem-782	137	7	cm‐1	cm‐1	PROPN
eurjchem-782	137	8	):	):	PUNCT
eurjchem-782	137	9	3112	3112	NUM
eurjchem-782	137	10	,	,	PUNCT
eurjchem-782	137	11	2934	2934	NUM
eurjchem-782	137	12	(	(	PUNCT
eurjchem-782	137	13	ar‐ch	ar‐ch	NUM
eurjchem-782	137	14	)	)	PUNCT
eurjchem-782	137	15	,	,	PUNCT
eurjchem-782	137	16	1685	1685	NUM
eurjchem-782	137	17	(	(	PUNCT
eurjchem-782	137	18	c	c	NOUN
eurjchem-782	137	19	=	=	NOUN
eurjchem-782	137	20	o	o	NOUN
eurjchem-782	137	21	)	)	PUNCT
eurjchem-782	137	22	.	.	PUNCT
eurjchem-782	138	1	1h	1h	NUM
eurjchem-782	138	2	nmr	nmr	NOUN
eurjchem-782	138	3	(	(	PUNCT
eurjchem-782	138	4	400	400	NUM
eurjchem-782	138	5	mhz	mhz	NOUN
eurjchem-782	138	6	,	,	PUNCT
eurjchem-782	138	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-782	138	8	,	,	PUNCT
eurjchem-782	138	9	δ	δ	PROPN
eurjchem-782	138	10	,	,	PUNCT
eurjchem-782	138	11	ppm	ppm	NOUN
eurjchem-782	138	12	):	):	PUNCT
eurjchem-782	138	13	7.81‐7.22	7.81‐7.22	NUM
eurjchem-782	138	14	(	(	PUNCT
eurjchem-782	138	15	m	m	PROPN
eurjchem-782	138	16	,	,	PUNCT
eurjchem-782	138	17	9h	9h	NUM
eurjchem-782	138	18	,	,	PUNCT
eurjchem-782	138	19	ar‐h	ar‐h	NOUN
eurjchem-782	138	20	)	)	PUNCT
eurjchem-782	138	21	,	,	PUNCT
eurjchem-782	138	22	4.05	4.05	NUM
eurjchem-782	138	23	(	(	PUNCT
eurjchem-782	138	24	t	t	PROPN
eurjchem-782	138	25	,	,	PUNCT
eurjchem-782	138	26	1h	1h	NUM
eurjchem-782	138	27	,	,	PUNCT
eurjchem-782	138	28	ch	ch	NOUN
eurjchem-782	138	29	)	)	PUNCT
eurjchem-782	138	30	,	,	PUNCT
eurjchem-782	138	31	2.65‐2.21	2.65‐2.21	NUM
eurjchem-782	138	32	(	(	PUNCT
eurjchem-782	138	33	m	m	PROPN
eurjchem-782	138	34	,	,	PUNCT
eurjchem-782	138	35	4h	4h	NOUN
eurjchem-782	138	36	,	,	PUNCT
eurjchem-782	138	37	ch2	ch2	PROPN
eurjchem-782	138	38	)	)	PUNCT
eurjchem-782	138	39	.	.	PUNCT
eurjchem-782	139	1	13c	13c	NOUN
eurjchem-782	139	2	nmr	nmr	NOUN
eurjchem-782	139	3	(	(	PUNCT
eurjchem-782	139	4	100	100	NUM
eurjchem-782	139	5	mhz	mhz	NOUN
eurjchem-782	139	6	,	,	PUNCT
eurjchem-782	139	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-782	139	8	,	,	PUNCT
eurjchem-782	139	9	δ	δ	PROPN
eurjchem-782	139	10	,	,	PUNCT
eurjchem-782	139	11	ppm	ppm	NUM
eurjchem-782	139	12	):	):	PUNCT
eurjchem-782	139	13	198.3	198.3	NUM
eurjchem-782	139	14	(	(	PUNCT
eurjchem-782	139	15	c‐1	c‐1	NOUN
eurjchem-782	139	16	)	)	PUNCT
eurjchem-782	139	17	,	,	PUNCT
eurjchem-782	139	18	145.3	145.3	NUM
eurjchem-782	139	19	(	(	PUNCT
eurjchem-782	139	20	c‐1	c‐1	NOUN
eurjchem-782	139	21	'	'	PUNCT
eurjchem-782	139	22	)	)	PUNCT
eurjchem-782	139	23	,	,	PUNCT
eurjchem-782	139	24	140.5	140.5	NUM
eurjchem-782	139	25	(	(	PUNCT
eurjchem-782	139	26	c‐5a	c‐5a	PROPN
eurjchem-782	139	27	)	)	PUNCT
eurjchem-782	139	28	,	,	PUNCT
eurjchem-782	139	29	134.1	134.1	NUM
eurjchem-782	139	30	(	(	PUNCT
eurjchem-782	139	31	c‐8a	c‐8a	NOUN
eurjchem-782	139	32	)	)	PUNCT
eurjchem-782	139	33	,	,	PUNCT
eurjchem-782	139	34	133.8	133.8	NUM
eurjchem-782	139	35	(	(	PUNCT
eurjchem-782	139	36	c‐6	c‐6	NOUN
eurjchem-782	139	37	)	)	PUNCT
eurjchem-782	139	38	,	,	PUNCT
eurjchem-782	139	39	129.5	129.5	NUM
eurjchem-782	139	40	(	(	PUNCT
eurjchem-782	139	41	c‐3	c‐3	NOUN
eurjchem-782	139	42	'	'	PUNCT
eurjchem-782	139	43	,	,	PUNCT
eurjchem-782	139	44	c‐5	c‐5	NOUN
eurjchem-782	139	45	'	'	PUNCT
eurjchem-782	139	46	)	)	PUNCT
eurjchem-782	139	47	,	,	PUNCT
eurjchem-782	139	48	128.1	128.1	NUM
eurjchem-782	139	49	(	(	PUNCT
eurjchem-782	139	50	c‐2	c‐2	NOUN
eurjchem-782	139	51	'	'	PUNCT
eurjchem-782	139	52	,	,	PUNCT
eurjchem-782	139	53	c‐6	c‐6	NOUN
eurjchem-782	139	54	'	'	PUNCT
eurjchem-782	139	55	)	)	PUNCT
eurjchem-782	139	56	,	,	PUNCT
eurjchem-782	139	57	128.0	128.0	NUM
eurjchem-782	139	58	(	(	PUNCT
eurjchem-782	139	59	c‐5	c‐5	NOUN
eurjchem-782	139	60	,	,	PUNCT
eurjchem-782	139	61	c‐8	c‐8	NOUN
eurjchem-782	139	62	)	)	PUNCT
eurjchem-782	139	63	,	,	PUNCT
eurjchem-782	139	64	126.5	126.5	NUM
eurjchem-782	139	65	(	(	PUNCT
eurjchem-782	139	66	c‐7	c‐7	NOUN
eurjchem-782	139	67	)	)	PUNCT
eurjchem-782	139	68	,	,	PUNCT
eurjchem-782	139	69	126.2	126.2	NUM
eurjchem-782	139	70	(	(	PUNCT
eurjchem-782	139	71	c‐4	c‐4	PROPN
eurjchem-782	139	72	'	'	PUNCT
eurjchem-782	139	73	)	)	PUNCT
eurjchem-782	139	74	,	,	PUNCT
eurjchem-782	139	75	45.0	45.0	NUM
eurjchem-782	139	76	(	(	PUNCT
eurjchem-782	139	77	c‐4	c‐4	PROPN
eurjchem-782	139	78	)	)	PUNCT
eurjchem-782	139	79	,	,	PUNCT
eurjchem-782	139	80	37.3	37.3	NUM
eurjchem-782	139	81	(	(	PUNCT
eurjchem-782	139	82	c‐2	c‐2	NOUN
eurjchem-782	139	83	)	)	PUNCT
eurjchem-782	139	84	,	,	PUNCT
eurjchem-782	139	85	31.6	31.6	NUM
eurjchem-782	139	86	(	(	PUNCT
eurjchem-782	139	87	c‐3	c‐3	NOUN
eurjchem-782	139	88	)	)	PUNCT
eurjchem-782	139	89	.	.	PUNCT
eurjchem-782	140	1	ms	ms	PROPN
eurjchem-782	140	2	(	(	PUNCT
eurjchem-782	140	3	esi	esi	PROPN
eurjchem-782	140	4	,	,	PUNCT
eurjchem-782	140	5	m	m	PROPN
eurjchem-782	140	6	/	/	SYM
eurjchem-782	140	7	z	z	NOUN
eurjchem-782	140	8	):	):	PUNCT
eurjchem-782	140	9	222.00	222.00	NUM
eurjchem-782	140	10	(	(	PUNCT
eurjchem-782	140	11	m+	m+	NUM
eurjchem-782	140	12	)	)	PUNCT
eurjchem-782	140	13	.	.	PUNCT
eurjchem-782	141	1	anal	anal	PROPN
eurjchem-782	141	2	.	.	PUNCT
eurjchem-782	141	3	calcd	calcd	NOUN
eurjchem-782	141	4	.	.	PUNCT
eurjchem-782	142	1	for	for	ADP
eurjchem-782	142	2	c16h14o	c16h14o	NUM
eurjchem-782	142	3	:	:	PUNCT
eurjchem-782	142	4	c	c	X
eurjchem-782	142	5	,	,	PUNCT
eurjchem-782	142	6	86.45	86.45	NUM
eurjchem-782	142	7	;	;	PUNCT
eurjchem-782	142	8	h	h	NOUN
eurjchem-782	142	9	,	,	PUNCT
eurjchem-782	142	10	6.35	6.35	NUM
eurjchem-782	142	11	.	.	PUNCT
eurjchem-782	142	12	found	find	VERB
eurjchem-782	142	13	:	:	PUNCT
eurjchem-782	143	1	c	c	X
eurjchem-782	143	2	,	,	PUNCT
eurjchem-782	143	3	86.41	86.41	NUM
eurjchem-782	143	4	;	;	PUNCT
eurjchem-782	143	5	h	h	NOUN
eurjchem-782	143	6	,	,	PUNCT
eurjchem-782	143	7	6.33	6.33	NUM
eurjchem-782	143	8	%	%	NOUN
eurjchem-782	143	9	.	.	PUNCT
eurjchem-782	144	1	6‐methyl‐4‐phenyl‐3,4‐dihydronaphthalen‐1(2h)‐one	6‐methyl‐4‐phenyl‐3,4‐dihydronaphthalen‐1(2h)‐one	NUM
eurjchem-782	144	2	(	(	PUNCT
eurjchem-782	144	3	5b	5b	NUM
eurjchem-782	144	4	):	):	PUNCT
eurjchem-782	144	5	color	color	NOUN
eurjchem-782	144	6	:	:	PUNCT
eurjchem-782	144	7	dark	dark	ADJ
eurjchem-782	144	8	semisolid	semisolid	NOUN
eurjchem-782	144	9	.	.	PUNCT
eurjchem-782	145	1	yield	yield	NOUN
eurjchem-782	145	2	:	:	PUNCT
eurjchem-782	145	3	66.14	66.14	NUM
eurjchem-782	145	4	%	%	NOUN
eurjchem-782	145	5	.	.	PUNCT
eurjchem-782	146	1	ir	ir	PROPN
eurjchem-782	146	2	(	(	PUNCT
eurjchem-782	146	3	kbr	kbr	PROPN
eurjchem-782	146	4	,	,	PUNCT
eurjchem-782	146	5	ν	ν	PROPN
eurjchem-782	146	6	,	,	PUNCT
eurjchem-782	146	7	cm‐1	cm‐1	PROPN
eurjchem-782	146	8	):	):	PUNCT
eurjchem-782	146	9	3124‐	3124‐	NUM
eurjchem-782	146	10	2943	2943	NUM
eurjchem-782	146	11	(	(	PUNCT
eurjchem-782	146	12	ar‐ch	ar‐ch	NUM
eurjchem-782	146	13	)	)	PUNCT
eurjchem-782	146	14	,	,	PUNCT
eurjchem-782	146	15	1694	1694	NUM
eurjchem-782	146	16	(	(	PUNCT
eurjchem-782	146	17	c	c	NOUN
eurjchem-782	146	18	=	=	NOUN
eurjchem-782	146	19	o	o	NOUN
eurjchem-782	146	20	)	)	PUNCT
eurjchem-782	146	21	.	.	PUNCT
eurjchem-782	147	1	1h	1h	NUM
eurjchem-782	147	2	nmr	nmr	NOUN
eurjchem-782	147	3	(	(	PUNCT
eurjchem-782	147	4	400	400	NUM
eurjchem-782	147	5	mhz	mhz	NOUN
eurjchem-782	147	6	,	,	PUNCT
eurjchem-782	147	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-782	147	8	,	,	PUNCT
eurjchem-782	147	9	δ	δ	PROPN
eurjchem-782	147	10	,	,	PUNCT
eurjchem-782	147	11	ppm	ppm	NOUN
eurjchem-782	147	12	):	):	PUNCT
eurjchem-782	147	13	7.85‐7.20	7.85‐7.20	NUM
eurjchem-782	147	14	(	(	PUNCT
eurjchem-782	147	15	m	m	PROPN
eurjchem-782	147	16	,	,	PUNCT
eurjchem-782	147	17	8h	8h	NUM
eurjchem-782	147	18	,	,	PUNCT
eurjchem-782	147	19	ar‐h	ar‐h	PROPN
eurjchem-782	147	20	)	)	PUNCT
eurjchem-782	147	21	,	,	PUNCT
eurjchem-782	147	22	4.10	4.10	NUM
eurjchem-782	147	23	(	(	PUNCT
eurjchem-782	147	24	t	t	PROPN
eurjchem-782	147	25	,	,	PUNCT
eurjchem-782	147	26	1h	1h	NUM
eurjchem-782	147	27	,	,	PUNCT
eurjchem-782	147	28	ch	ch	NOUN
eurjchem-782	147	29	)	)	PUNCT
eurjchem-782	147	30	,	,	PUNCT
eurjchem-782	147	31	2.63‐2.20	2.63‐2.20	NUM
eurjchem-782	147	32	(	(	PUNCT
eurjchem-782	147	33	m	m	PROPN
eurjchem-782	147	34	,	,	PUNCT
eurjchem-782	147	35	4h	4h	NOUN
eurjchem-782	147	36	,	,	PUNCT
eurjchem-782	147	37	ch2	ch2	PROPN
eurjchem-782	147	38	)	)	PUNCT
eurjchem-782	147	39	,	,	PUNCT
eurjchem-782	147	40	2.31	2.31	NUM
eurjchem-782	147	41	(	(	PUNCT
eurjchem-782	147	42	s	s	PROPN
eurjchem-782	147	43	,	,	PUNCT
eurjchem-782	147	44	3h	3h	NUM
eurjchem-782	147	45	,	,	PUNCT
eurjchem-782	147	46	ch3	ch3	PROPN
eurjchem-782	147	47	)	)	PUNCT
eurjchem-782	147	48	.	.	PUNCT
eurjchem-782	148	1	13c	13c	NOUN
eurjchem-782	148	2	nmr	nmr	NOUN
eurjchem-782	148	3	(	(	PUNCT
eurjchem-782	148	4	100	100	NUM
eurjchem-782	148	5	mhz	mhz	NOUN
eurjchem-782	148	6	,	,	PUNCT
eurjchem-782	148	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-782	148	8	,	,	PUNCT
eurjchem-782	148	9	δ	δ	PROPN
eurjchem-782	148	10	,	,	PUNCT
eurjchem-782	148	11	ppm	ppm	NUM
eurjchem-782	148	12	):	):	PUNCT
eurjchem-782	148	13	198.0	198.0	NUM
eurjchem-782	148	14	(	(	PUNCT
eurjchem-782	148	15	c‐1	c‐1	NOUN
eurjchem-782	148	16	)	)	PUNCT
eurjchem-782	148	17	,	,	PUNCT
eurjchem-782	148	18	145.3	145.3	NUM
eurjchem-782	148	19	(	(	PUNCT
eurjchem-782	148	20	c‐1	c‐1	NOUN
eurjchem-782	148	21	'	'	PUNCT
eurjchem-782	148	22	)	)	PUNCT
eurjchem-782	148	23	,	,	PUNCT
eurjchem-782	148	24	143.5	143.5	NUM
eurjchem-782	148	25	(	(	PUNCT
eurjchem-782	148	26	c‐6	c‐6	NOUN
eurjchem-782	148	27	)	)	PUNCT
eurjchem-782	148	28	,	,	PUNCT
eurjchem-782	148	29	140.2	140.2	NUM
eurjchem-782	148	30	(	(	PUNCT
eurjchem-782	148	31	c‐5a	c‐5a	PROPN
eurjchem-782	148	32	)	)	PUNCT
eurjchem-782	148	33	,	,	PUNCT
eurjchem-782	148	34	131.0	131.0	NUM
eurjchem-782	148	35	(	(	PUNCT
eurjchem-782	148	36	c‐8a	c‐8a	NOUN
eurjchem-782	148	37	)	)	PUNCT
eurjchem-782	148	38	,	,	PUNCT
eurjchem-782	148	39	129.5	129.5	NUM
eurjchem-782	148	40	(	(	PUNCT
eurjchem-782	148	41	c‐3	c‐3	NOUN
eurjchem-782	148	42	'	'	PUNCT
eurjchem-782	148	43	,	,	PUNCT
eurjchem-782	148	44	c‐5	c‐5	NOUN
eurjchem-782	148	45	'	'	PUNCT
eurjchem-782	148	46	)	)	PUNCT
eurjchem-782	148	47	,	,	PUNCT
eurjchem-782	148	48	128.1	128.1	NUM
eurjchem-782	148	49	(	(	PUNCT
eurjchem-782	148	50	c‐2	c‐2	NOUN
eurjchem-782	148	51	'	'	PUNCT
eurjchem-782	148	52	,	,	PUNCT
eurjchem-782	148	53	c‐6	c‐6	NOUN
eurjchem-782	148	54	'	'	PUNCT
eurjchem-782	148	55	)	)	PUNCT
eurjchem-782	148	56	,	,	PUNCT
eurjchem-782	148	57	128.0	128.0	NUM
eurjchem-782	148	58	(	(	PUNCT
eurjchem-782	148	59	c‐5	c‐5	NOUN
eurjchem-782	148	60	)	)	PUNCT
eurjchem-782	148	61	,	,	PUNCT
eurjchem-782	148	62	126.5	126.5	NUM
eurjchem-782	148	63	(	(	PUNCT
eurjchem-782	148	64	c‐7	c‐7	NOUN
eurjchem-782	148	65	)	)	PUNCT
eurjchem-782	148	66	,	,	PUNCT
eurjchem-782	148	67	126.1	126.1	NUM
eurjchem-782	148	68	(	(	PUNCT
eurjchem-782	148	69	c‐4	c‐4	PROPN
eurjchem-782	148	70	'	'	PUNCT
eurjchem-782	148	71	)	)	PUNCT
eurjchem-782	148	72	,	,	PUNCT
eurjchem-782	148	73	125.6	125.6	NUM
eurjchem-782	148	74	(	(	PUNCT
eurjchem-782	148	75	c‐8	c‐8	NOUN
eurjchem-782	148	76	)	)	PUNCT
eurjchem-782	148	77	,	,	PUNCT
eurjchem-782	148	78	45.1	45.1	NUM
eurjchem-782	148	79	(	(	PUNCT
eurjchem-782	148	80	c‐4	c‐4	PROPN
eurjchem-782	148	81	)	)	PUNCT
eurjchem-782	148	82	,	,	PUNCT
eurjchem-782	148	83	37.1	37.1	NUM
eurjchem-782	148	84	(	(	PUNCT
eurjchem-782	148	85	c‐2	c‐2	NOUN
eurjchem-782	148	86	)	)	PUNCT
eurjchem-782	148	87	,	,	PUNCT
eurjchem-782	148	88	31.5	31.5	NUM
eurjchem-782	148	89	(	(	PUNCT
eurjchem-782	148	90	c‐	c‐	NOUN
eurjchem-782	148	91	3	3	NUM
eurjchem-782	148	92	)	)	PUNCT
eurjchem-782	148	93	,	,	PUNCT
eurjchem-782	148	94	21.5	21.5	NUM
eurjchem-782	148	95	(	(	PUNCT
eurjchem-782	148	96	‐ch3	‐ch3	ADJ
eurjchem-782	148	97	)	)	PUNCT
eurjchem-782	148	98	.	.	PUNCT
eurjchem-782	149	1	ms	ms	PROPN
eurjchem-782	149	2	(	(	PUNCT
eurjchem-782	149	3	esi	esi	PROPN
eurjchem-782	149	4	,	,	PUNCT
eurjchem-782	149	5	m	m	PROPN
eurjchem-782	149	6	/	/	SYM
eurjchem-782	149	7	z	z	NOUN
eurjchem-782	149	8	):	):	PUNCT
eurjchem-782	149	9	236.09	236.09	NUM
eurjchem-782	149	10	(	(	PUNCT
eurjchem-782	149	11	m+	m+	NUM
eurjchem-782	149	12	)	)	PUNCT
eurjchem-782	149	13	.	.	PUNCT
eurjchem-782	150	1	anal	anal	PROPN
eurjchem-782	150	2	.	.	PUNCT
eurjchem-782	150	3	calcd	calcd	NOUN
eurjchem-782	150	4	.	.	PUNCT
eurjchem-782	151	1	for	for	ADP
eurjchem-782	151	2	c17h16o	c17h16o	NOUN
eurjchem-782	151	3	:	:	PUNCT
eurjchem-782	151	4	c	c	X
eurjchem-782	151	5	,	,	PUNCT
eurjchem-782	151	6	86.40	86.40	NUM
eurjchem-782	151	7	;	;	PUNCT
eurjchem-782	151	8	h	h	NOUN
eurjchem-782	151	9	,	,	PUNCT
eurjchem-782	151	10	6.82	6.82	NUM
eurjchem-782	151	11	.	.	PUNCT
eurjchem-782	151	12	found	find	VERB
eurjchem-782	151	13	:	:	PUNCT
eurjchem-782	152	1	c	c	X
eurjchem-782	152	2	,	,	PUNCT
eurjchem-782	152	3	86.39	86.39	NUM
eurjchem-782	152	4	;	;	PUNCT
eurjchem-782	152	5	h	h	NOUN
eurjchem-782	152	6	,	,	PUNCT
eurjchem-782	152	7	6.85	6.85	NUM
eurjchem-782	152	8	%	%	NOUN
eurjchem-782	152	9	.	.	PUNCT
eurjchem-782	153	1	6‐methoxy‐4‐phenyl‐3,4‐dihydronaphthalen‐1(2h)‐one	6‐methoxy‐4‐phenyl‐3,4‐dihydronaphthalen‐1(2h)‐one	NUM
eurjchem-782	153	2	(	(	PUNCT
eurjchem-782	153	3	5c	5c	NUM
eurjchem-782	153	4	):	):	PUNCT
eurjchem-782	153	5	color	color	NOUN
eurjchem-782	153	6	:	:	PUNCT
eurjchem-782	153	7	dark	dark	ADJ
eurjchem-782	153	8	semisolid	semisolid	NOUN
eurjchem-782	153	9	.	.	PUNCT
eurjchem-782	154	1	yield	yield	NOUN
eurjchem-782	154	2	:	:	PUNCT
eurjchem-782	154	3	81.61	81.61	NUM
eurjchem-782	154	4	%	%	NOUN
eurjchem-782	154	5	.	.	PUNCT
eurjchem-782	155	1	ir	ir	PROPN
eurjchem-782	155	2	(	(	PUNCT
eurjchem-782	155	3	kbr	kbr	PROPN
eurjchem-782	155	4	,	,	PUNCT
eurjchem-782	155	5	ν	ν	PROPN
eurjchem-782	155	6	,	,	PUNCT
eurjchem-782	155	7	cm‐1	cm‐1	PROPN
eurjchem-782	155	8	):	):	PUNCT
eurjchem-782	155	9	3125	3125	NUM
eurjchem-782	155	10	,	,	PUNCT
eurjchem-782	155	11	2946	2946	NUM
eurjchem-782	155	12	(	(	PUNCT
eurjchem-782	155	13	ar‐ch	ar‐ch	NUM
eurjchem-782	155	14	)	)	PUNCT
eurjchem-782	155	15	,	,	PUNCT
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eurjchem-782	155	17	(	(	PUNCT
eurjchem-782	155	18	c	c	NOUN
eurjchem-782	155	19	=	=	NOUN
eurjchem-782	155	20	o	o	NOUN
eurjchem-782	155	21	)	)	PUNCT
eurjchem-782	155	22	.	.	PUNCT
eurjchem-782	156	1	1h	1h	NUM
eurjchem-782	156	2	nmr	nmr	NOUN
eurjchem-782	156	3	(	(	PUNCT
eurjchem-782	156	4	400	400	NUM
eurjchem-782	156	5	mhz	mhz	NOUN
eurjchem-782	156	6	,	,	PUNCT
eurjchem-782	156	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-782	156	8	,	,	PUNCT
eurjchem-782	156	9	δ	δ	PROPN
eurjchem-782	156	10	,	,	PUNCT
eurjchem-782	156	11	ppm	ppm	NUM
eurjchem-782	156	12	):	):	PUNCT
eurjchem-782	156	13	7.90‐7.18	7.90‐7.18	X
eurjchem-782	156	14	(	(	PUNCT
eurjchem-782	156	15	m	m	PROPN
eurjchem-782	156	16	,	,	PUNCT
eurjchem-782	156	17	8h	8h	NUM
eurjchem-782	156	18	,	,	PUNCT
eurjchem-782	156	19	ar‐h	ar‐h	PROPN
eurjchem-782	156	20	)	)	PUNCT
eurjchem-782	156	21	,	,	PUNCT
eurjchem-782	156	22	4.02	4.02	NUM
eurjchem-782	156	23	(	(	PUNCT
eurjchem-782	156	24	t	t	PROPN
eurjchem-782	156	25	,	,	PUNCT
eurjchem-782	156	26	1h	1h	NUM
eurjchem-782	156	27	,	,	PUNCT
eurjchem-782	156	28	ch	ch	NOUN
eurjchem-782	156	29	)	)	PUNCT
eurjchem-782	156	30	,	,	PUNCT
eurjchem-782	156	31	3.84	3.84	NUM
eurjchem-782	156	32	(	(	PUNCT
eurjchem-782	156	33	s	s	PROPN
eurjchem-782	156	34	,	,	PUNCT
eurjchem-782	156	35	3h	3h	NUM
eurjchem-782	156	36	,	,	PUNCT
eurjchem-782	156	37	och3	och3	ADJ
eurjchem-782	156	38	)	)	PUNCT
eurjchem-782	156	39	,	,	PUNCT
eurjchem-782	156	40	2.60‐2.18	2.60‐2.18	NUM
eurjchem-782	156	41	(	(	PUNCT
eurjchem-782	156	42	m	m	PROPN
eurjchem-782	156	43	,	,	PUNCT
eurjchem-782	156	44	4h	4h	NOUN
eurjchem-782	156	45	,	,	PUNCT
eurjchem-782	156	46	ch2	ch2	PROPN
eurjchem-782	156	47	)	)	PUNCT
eurjchem-782	156	48	.	.	PUNCT
eurjchem-782	157	1	13c	13c	NOUN
eurjchem-782	157	2	nmr	nmr	NOUN
eurjchem-782	157	3	(	(	PUNCT
eurjchem-782	157	4	100	100	NUM
eurjchem-782	157	5	mhz	mhz	NOUN
eurjchem-782	157	6	,	,	PUNCT
eurjchem-782	157	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-782	157	8	,	,	PUNCT
eurjchem-782	157	9	δ	δ	PROPN
eurjchem-782	157	10	,	,	PUNCT
eurjchem-782	157	11	ppm	ppm	NUM
eurjchem-782	157	12	):	):	PUNCT
eurjchem-782	157	13	198.1	198.1	NUM
eurjchem-782	157	14	(	(	PUNCT
eurjchem-782	157	15	c‐1	c‐1	NOUN
eurjchem-782	157	16	)	)	PUNCT
eurjchem-782	157	17	,	,	PUNCT
eurjchem-782	157	18	165.3	165.3	NUM
eurjchem-782	157	19	(	(	PUNCT
eurjchem-782	157	20	c‐6	c‐6	NOUN
eurjchem-782	157	21	)	)	PUNCT
eurjchem-782	157	22	,	,	PUNCT
eurjchem-782	157	23	145.8	145.8	NUM
eurjchem-782	157	24	(	(	PUNCT
eurjchem-782	157	25	c‐1	c‐1	NOUN
eurjchem-782	157	26	'	'	PUNCT
eurjchem-782	157	27	)	)	PUNCT
eurjchem-782	157	28	,	,	PUNCT
eurjchem-782	157	29	141.9	141.9	NUM
eurjchem-782	157	30	(	(	PUNCT
eurjchem-782	157	31	c‐5a	c‐5a	PROPN
eurjchem-782	157	32	)	)	PUNCT
eurjchem-782	157	33	,	,	PUNCT
eurjchem-782	157	34	130.5	130.5	NUM
eurjchem-782	157	35	(	(	PUNCT
eurjchem-782	157	36	c‐8	c‐8	NOUN
eurjchem-782	157	37	)	)	PUNCT
eurjchem-782	157	38	,	,	PUNCT
eurjchem-782	157	39	129.7	129.7	NUM
eurjchem-782	157	40	(	(	PUNCT
eurjchem-782	157	41	c‐3	c‐3	NOUN
eurjchem-782	157	42	'	'	PUNCT
eurjchem-782	157	43	,	,	PUNCT
eurjchem-782	157	44	c‐5	c‐5	NOUN
eurjchem-782	157	45	'	'	PUNCT
eurjchem-782	157	46	)	)	PUNCT
eurjchem-782	157	47	,	,	PUNCT
eurjchem-782	157	48	128.0	128.0	NUM
eurjchem-782	157	49	(	(	PUNCT
eurjchem-782	157	50	c‐2	c‐2	NOUN
eurjchem-782	157	51	'	'	PUNCT
eurjchem-782	157	52	,	,	PUNCT
eurjchem-782	157	53	c‐6	c‐6	NOUN
eurjchem-782	157	54	'	'	PUNCT
eurjchem-782	157	55	)	)	PUNCT
eurjchem-782	157	56	,	,	PUNCT
eurjchem-782	157	57	126.5	126.5	NUM
eurjchem-782	157	58	(	(	PUNCT
eurjchem-782	157	59	c‐8a	c‐8a	NOUN
eurjchem-782	157	60	)	)	PUNCT
eurjchem-782	157	61	,	,	PUNCT
eurjchem-782	157	62	126.0	126.0	NUM
eurjchem-782	157	63	(	(	PUNCT
eurjchem-782	157	64	c‐4	c‐4	PROPN
eurjchem-782	157	65	'	'	PUNCT
eurjchem-782	157	66	)	)	PUNCT
eurjchem-782	157	67	,	,	PUNCT
eurjchem-782	157	68	111.6	111.6	NUM
eurjchem-782	157	69	(	(	PUNCT
eurjchem-782	157	70	c‐7	c‐7	NOUN
eurjchem-782	157	71	)	)	PUNCT
eurjchem-782	157	72	,	,	PUNCT
eurjchem-782	157	73	104.9	104.9	NUM
eurjchem-782	157	74	(	(	PUNCT
eurjchem-782	157	75	c‐5	c‐5	NOUN
eurjchem-782	157	76	)	)	PUNCT
eurjchem-782	157	77	,	,	PUNCT
eurjchem-782	157	78	55.3	55.3	NUM
eurjchem-782	157	79	(	(	PUNCT
eurjchem-782	157	80	‐och3	‐och3	NOUN
eurjchem-782	157	81	)	)	PUNCT
eurjchem-782	157	82	,	,	PUNCT
eurjchem-782	157	83	45.6	45.6	NUM
eurjchem-782	157	84	(	(	PUNCT
eurjchem-782	157	85	c‐4	c‐4	PROPN
eurjchem-782	157	86	)	)	PUNCT
eurjchem-782	157	87	,	,	PUNCT
eurjchem-782	157	88	37.9	37.9	NUM
eurjchem-782	157	89	(	(	PUNCT
eurjchem-782	157	90	c‐2	c‐2	NOUN
eurjchem-782	157	91	)	)	PUNCT
eurjchem-782	157	92	,	,	PUNCT
eurjchem-782	157	93	31.5	31.5	NUM
eurjchem-782	157	94	(	(	PUNCT
eurjchem-782	157	95	c‐3	c‐3	NOUN
eurjchem-782	157	96	)	)	PUNCT
eurjchem-782	157	97	.	.	PUNCT
eurjchem-782	158	1	ms	ms	PROPN
eurjchem-782	158	2	(	(	PUNCT
eurjchem-782	158	3	esi	esi	PROPN
eurjchem-782	158	4	,	,	PUNCT
eurjchem-782	158	5	m	m	PROPN
eurjchem-782	158	6	/	/	SYM
eurjchem-782	158	7	z	z	NOUN
eurjchem-782	158	8	):	):	PUNCT
eurjchem-782	158	9	252.13	252.13	NUM
eurjchem-782	158	10	(	(	PUNCT
eurjchem-782	158	11	m+	m+	NUM
eurjchem-782	158	12	)	)	PUNCT
eurjchem-782	158	13	.	.	PUNCT
eurjchem-782	159	1	anal	anal	PROPN
eurjchem-782	159	2	.	.	PUNCT
eurjchem-782	159	3	calcd	calcd	NOUN
eurjchem-782	159	4	.	.	PUNCT
eurjchem-782	160	1	for	for	SCONJ
eurjchem-782	160	2	c17h16o2	c17h16o2	NOUN
eurjchem-782	160	3	:	:	PUNCT
eurjchem-782	160	4	c	c	X
eurjchem-782	160	5	,	,	PUNCT
eurjchem-782	160	6	80.93	80.93	NUM
eurjchem-782	160	7	;	;	PUNCT
eurjchem-782	160	8	h	h	NOUN
eurjchem-782	160	9	,	,	PUNCT
eurjchem-782	160	10	6.39	6.39	NUM
eurjchem-782	160	11	.	.	PUNCT
eurjchem-782	160	12	found	find	VERB
eurjchem-782	160	13	:	:	PUNCT
eurjchem-782	161	1	c	c	X
eurjchem-782	161	2	,	,	PUNCT
eurjchem-782	161	3	80.90	80.90	NUM
eurjchem-782	161	4	;	;	PUNCT
eurjchem-782	161	5	h	h	NOUN
eurjchem-782	161	6	,	,	PUNCT
eurjchem-782	161	7	6.41	6.41	NUM
eurjchem-782	161	8	%	%	NOUN
eurjchem-782	161	9	.	.	PUNCT
eurjchem-782	162	1	6‐(methylthio)‐4‐phenyl‐3,4‐dihydronaphthalen‐1(2h)‐one	6‐(methylthio)‐4‐phenyl‐3,4‐dihydronaphthalen‐1(2h)‐one	NUM
eurjchem-782	162	2	(	(	PUNCT
eurjchem-782	162	3	5d	5d	NUM
eurjchem-782	162	4	):	):	PUNCT
eurjchem-782	162	5	color	color	NOUN
eurjchem-782	162	6	:	:	PUNCT
eurjchem-782	162	7	dark	dark	ADJ
eurjchem-782	162	8	semisolid	semisolid	NOUN
eurjchem-782	162	9	.	.	PUNCT
eurjchem-782	163	1	yield	yield	NOUN
eurjchem-782	163	2	:	:	PUNCT
eurjchem-782	163	3	93.40	93.40	NUM
eurjchem-782	163	4	%	%	NOUN
eurjchem-782	163	5	.	.	PUNCT
eurjchem-782	164	1	ir	ir	PROPN
eurjchem-782	164	2	(	(	PUNCT
eurjchem-782	164	3	kbr	kbr	PROPN
eurjchem-782	164	4	,	,	PUNCT
eurjchem-782	164	5	ν	ν	PROPN
eurjchem-782	164	6	,	,	PUNCT
eurjchem-782	164	7	cm‐1	cm‐1	PROPN
eurjchem-782	164	8	):	):	PUNCT
eurjchem-782	164	9	3133	3133	NUM
eurjchem-782	164	10	,	,	PUNCT
eurjchem-782	164	11	2965	2965	NUM
eurjchem-782	164	12	(	(	PUNCT
eurjchem-782	164	13	ar‐ch	ar‐ch	NUM
eurjchem-782	164	14	)	)	PUNCT
eurjchem-782	164	15	,	,	PUNCT
eurjchem-782	164	16	1687	1687	NUM
eurjchem-782	164	17	(	(	PUNCT
eurjchem-782	164	18	c	c	NOUN
eurjchem-782	164	19	=	=	NOUN
eurjchem-782	164	20	o	o	NOUN
eurjchem-782	164	21	)	)	PUNCT
eurjchem-782	164	22	.	.	PUNCT
eurjchem-782	165	1	1h	1h	NUM
eurjchem-782	165	2	nmr	nmr	NOUN
eurjchem-782	165	3	(	(	PUNCT
eurjchem-782	165	4	400	400	NUM
eurjchem-782	165	5	mhz	mhz	NOUN
eurjchem-782	165	6	,	,	PUNCT
eurjchem-782	165	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-782	165	8	,	,	PUNCT
eurjchem-782	165	9	δ	δ	PROPN
eurjchem-782	165	10	,	,	PUNCT
eurjchem-782	165	11	ppm	ppm	NUM
eurjchem-782	165	12	):	):	PUNCT
eurjchem-782	165	13	7.87‐7.12	7.87‐7.12	NUM
eurjchem-782	165	14	(	(	PUNCT
eurjchem-782	165	15	m	m	PROPN
eurjchem-782	165	16	,	,	PUNCT
eurjchem-782	165	17	8h	8h	NUM
eurjchem-782	165	18	,	,	PUNCT
eurjchem-782	165	19	ar‐h	ar‐h	PROPN
eurjchem-782	165	20	)	)	PUNCT
eurjchem-782	165	21	,	,	PUNCT
eurjchem-782	165	22	4.00	4.00	NUM
eurjchem-782	165	23	(	(	PUNCT
eurjchem-782	165	24	t	t	PROPN
eurjchem-782	165	25	,	,	PUNCT
eurjchem-782	165	26	1h	1h	NUM
eurjchem-782	165	27	,	,	PUNCT
eurjchem-782	165	28	ch	ch	NOUN
eurjchem-782	165	29	)	)	PUNCT
eurjchem-782	165	30	,	,	PUNCT
eurjchem-782	165	31	2.65‐2.21	2.65‐2.21	NUM
eurjchem-782	165	32	(	(	PUNCT
eurjchem-782	165	33	m	m	PROPN
eurjchem-782	165	34	,	,	PUNCT
eurjchem-782	165	35	4h	4h	NOUN
eurjchem-782	165	36	,	,	PUNCT
eurjchem-782	165	37	ch2	ch2	PROPN
eurjchem-782	165	38	)	)	PUNCT
eurjchem-782	165	39	,	,	PUNCT
eurjchem-782	165	40	2.53	2.53	NUM
eurjchem-782	165	41	(	(	PUNCT
eurjchem-782	165	42	s	s	PROPN
eurjchem-782	165	43	,	,	PUNCT
eurjchem-782	165	44	3h	3h	NUM
eurjchem-782	165	45	,	,	PUNCT
eurjchem-782	165	46	sch3	sch3	PROPN
eurjchem-782	165	47	)	)	PUNCT
eurjchem-782	165	48	.	.	PUNCT
eurjchem-782	166	1	13c	13c	NOUN
eurjchem-782	166	2	nmr	nmr	NOUN
eurjchem-782	166	3	(	(	PUNCT
eurjchem-782	166	4	100	100	NUM
eurjchem-782	166	5	mhz	mhz	NOUN
eurjchem-782	166	6	,	,	PUNCT
eurjchem-782	166	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-782	166	8	,	,	PUNCT
eurjchem-782	166	9	δ	δ	PROPN
eurjchem-782	166	10	,	,	PUNCT
eurjchem-782	166	11	ppm	ppm	NUM
eurjchem-782	166	12	):	):	PUNCT
eurjchem-782	166	13	198.3	198.3	NUM
eurjchem-782	166	14	(	(	PUNCT
eurjchem-782	166	15	c‐1	c‐1	NOUN
eurjchem-782	166	16	)	)	PUNCT
eurjchem-782	166	17	,	,	PUNCT
eurjchem-782	166	18	145.9	145.9	NUM
eurjchem-782	166	19	(	(	PUNCT
eurjchem-782	166	20	c‐1	c‐1	NOUN
eurjchem-782	166	21	'	'	PUNCT
eurjchem-782	166	22	)	)	PUNCT
eurjchem-782	166	23	,	,	PUNCT
eurjchem-782	166	24	143.8	143.8	NUM
eurjchem-782	166	25	(	(	PUNCT
eurjchem-782	166	26	c‐6	c‐6	NOUN
eurjchem-782	166	27	)	)	PUNCT
eurjchem-782	166	28	,	,	PUNCT
eurjchem-782	166	29	140.7	140.7	NUM
eurjchem-782	166	30	(	(	PUNCT
eurjchem-782	166	31	c‐5a	c‐5a	PROPN
eurjchem-782	166	32	)	)	PUNCT
eurjchem-782	166	33	,	,	PUNCT
eurjchem-782	166	34	130.6	130.6	NUM
eurjchem-782	166	35	(	(	PUNCT
eurjchem-782	166	36	c‐8a	c‐8a	NOUN
eurjchem-782	166	37	)	)	PUNCT
eurjchem-782	166	38	,	,	PUNCT
eurjchem-782	166	39	129.5	129.5	NUM
eurjchem-782	166	40	(	(	PUNCT
eurjchem-782	166	41	c‐8	c‐8	NOUN
eurjchem-782	166	42	)	)	PUNCT
eurjchem-782	166	43	,	,	PUNCT
eurjchem-782	166	44	129.2	129.2	NUM
eurjchem-782	166	45	(	(	PUNCT
eurjchem-782	166	46	c‐3	c‐3	NOUN
eurjchem-782	166	47	'	'	PUNCT
eurjchem-782	166	48	,	,	PUNCT
eurjchem-782	166	49	c‐5	c‐5	NOUN
eurjchem-782	166	50	'	'	PUNCT
eurjchem-782	166	51	)	)	PUNCT
eurjchem-782	166	52	,	,	PUNCT
eurjchem-782	166	53	128.4	128.4	NUM
eurjchem-782	166	54	(	(	PUNCT
eurjchem-782	166	55	c‐2	c‐2	NOUN
eurjchem-782	166	56	'	'	PUNCT
eurjchem-782	166	57	,	,	PUNCT
eurjchem-782	166	58	c‐6	c‐6	NOUN
eurjchem-782	166	59	'	'	PUNCT
eurjchem-782	166	60	)	)	PUNCT
eurjchem-782	166	61	,	,	PUNCT
eurjchem-782	166	62	126.3	126.3	NUM
eurjchem-782	166	63	(	(	PUNCT
eurjchem-782	166	64	c‐4	c‐4	PROPN
eurjchem-782	166	65	'	'	PUNCT
eurjchem-782	166	66	)	)	PUNCT
eurjchem-782	166	67	,	,	PUNCT
eurjchem-782	166	68	124.2	124.2	NUM
eurjchem-782	166	69	(	(	PUNCT
eurjchem-782	166	70	c‐7	c‐7	NOUN
eurjchem-782	166	71	)	)	PUNCT
eurjchem-782	166	72	,	,	PUNCT
eurjchem-782	166	73	123.1	123.1	NUM
eurjchem-782	166	74	(	(	PUNCT
eurjchem-782	166	75	c‐5	c‐5	NOUN
eurjchem-782	166	76	)	)	PUNCT
eurjchem-782	166	77	,	,	PUNCT
eurjchem-782	166	78	44.1	44.1	NUM
eurjchem-782	166	79	(	(	PUNCT
eurjchem-782	166	80	c‐4	c‐4	PROPN
eurjchem-782	166	81	)	)	PUNCT
eurjchem-782	166	82	,	,	PUNCT
eurjchem-782	166	83	37.5	37.5	NUM
eurjchem-782	166	84	(	(	PUNCT
eurjchem-782	166	85	c‐2	c‐2	NOUN
eurjchem-782	166	86	)	)	PUNCT
eurjchem-782	166	87	,	,	PUNCT
eurjchem-782	166	88	31.9	31.9	NUM
eurjchem-782	166	89	(	(	PUNCT
eurjchem-782	166	90	c‐	c‐	NOUN
eurjchem-782	166	91	3	3	NUM
eurjchem-782	166	92	)	)	PUNCT
eurjchem-782	166	93	,	,	PUNCT
eurjchem-782	166	94	14.6	14.6	NUM
eurjchem-782	166	95	(	(	PUNCT
eurjchem-782	166	96	‐sch3	‐sch3	PROPN
eurjchem-782	166	97	)	)	PUNCT
eurjchem-782	166	98	.	.	PUNCT
eurjchem-782	167	1	ms	ms	PROPN
eurjchem-782	167	2	(	(	PUNCT
eurjchem-782	167	3	esi	esi	PROPN
eurjchem-782	167	4	,	,	PUNCT
eurjchem-782	167	5	m	m	PROPN
eurjchem-782	167	6	/	/	SYM
eurjchem-782	167	7	z	z	NOUN
eurjchem-782	167	8	):	):	PUNCT
eurjchem-782	167	9	268.15	268.15	NUM
eurjchem-782	167	10	(	(	PUNCT
eurjchem-782	167	11	m+	m+	NUM
eurjchem-782	167	12	)	)	PUNCT
eurjchem-782	167	13	.	.	PUNCT
eurjchem-782	168	1	anal	anal	PROPN
eurjchem-782	168	2	.	.	PUNCT
eurjchem-782	168	3	calcd	calcd	NOUN
eurjchem-782	168	4	.	.	PUNCT
eurjchem-782	169	1	for	for	ADP
eurjchem-782	169	2	c17h16os	c17h16os	PROPN
eurjchem-782	169	3	:	:	PUNCT
eurjchem-782	169	4	c	c	X
eurjchem-782	169	5	,	,	PUNCT
eurjchem-782	169	6	76.08	76.08	NUM
eurjchem-782	169	7	;	;	PUNCT
eurjchem-782	169	8	h	h	NOUN
eurjchem-782	169	9	,	,	PUNCT
eurjchem-782	169	10	6.01	6.01	NUM
eurjchem-782	169	11	.	.	PUNCT
eurjchem-782	169	12	found	find	VERB
eurjchem-782	169	13	:	:	PUNCT
eurjchem-782	170	1	c	c	X
eurjchem-782	170	2	,	,	PUNCT
eurjchem-782	170	3	76.05	76.05	NUM
eurjchem-782	170	4	;	;	PUNCT
eurjchem-782	170	5	h	h	NOUN
eurjchem-782	170	6	,	,	PUNCT
eurjchem-782	170	7	6.05	6.05	NUM
eurjchem-782	170	8	%	%	NOUN
eurjchem-782	170	9	.	.	PUNCT
eurjchem-782	171	1	2.2.4	2.2.4	X
eurjchem-782	171	2	.	.	PUNCT
eurjchem-782	171	3	general	general	ADJ
eurjchem-782	171	4	procedure	procedure	NOUN
eurjchem-782	171	5	for	for	ADP
eurjchem-782	171	6	the	the	DET
eurjchem-782	171	7	synthesis	synthesis	NOUN
eurjchem-782	171	8	of	of	ADP
eurjchem-782	171	9	substituted	substitute	VERB
eurjchem-782	171	10	hydroxyl	hydroxyl	NOUN
eurjchem-782	171	11	methylene	methylene	NOUN
eurjchem-782	171	12	tetralones	tetralone	NOUN
eurjchem-782	171	13	(	(	PUNCT
eurjchem-782	171	14	6a‐d	6a‐d	NOUN
eurjchem-782	171	15	)	)	PUNCT
eurjchem-782	171	16	sodium	sodium	NOUN
eurjchem-782	171	17	hydride	hydride	NOUN
eurjchem-782	171	18	(	(	PUNCT
eurjchem-782	171	19	1.2	1.2	NUM
eurjchem-782	171	20	g	g	NOUN
eurjchem-782	171	21	,	,	PUNCT
eurjchem-782	171	22	0.0508	0.0508	NUM
eurjchem-782	171	23	mol	mol	NOUN
eurjchem-782	171	24	)	)	PUNCT
eurjchem-782	171	25	was	be	AUX
eurjchem-782	171	26	added	add	VERB
eurjchem-782	171	27	to	to	ADP
eurjchem-782	171	28	a	a	DET
eurjchem-782	171	29	mixture	mixture	NOUN
eurjchem-782	171	30	of	of	ADP
eurjchem-782	171	31	absolute	absolute	ADJ
eurjchem-782	171	32	ethanol	ethanol	NOUN
eurjchem-782	171	33	(	(	PUNCT
eurjchem-782	171	34	10	10	NUM
eurjchem-782	171	35	ml	ml	NOUN
eurjchem-782	171	36	)	)	PUNCT
eurjchem-782	171	37	and	and	CCONJ
eurjchem-782	171	38	dry	dry	ADJ
eurjchem-782	171	39	benzene	benzene	NOUN
eurjchem-782	171	40	(	(	PUNCT
eurjchem-782	171	41	150	150	NUM
eurjchem-782	171	42	ml	ml	NOUN
eurjchem-782	171	43	)	)	PUNCT
eurjchem-782	171	44	and	and	CCONJ
eurjchem-782	171	45	stirred	stir	VERB
eurjchem-782	171	46	for	for	ADP
eurjchem-782	171	47	1h	1h	NUM
eurjchem-782	171	48	.	.	PUNCT
eurjchem-782	172	1	ethyle	ethyle	NOUN
eurjchem-782	172	2	formate	formate	NOUN
eurjchem-782	172	3	(	(	PUNCT
eurjchem-782	172	4	10	10	NUM
eurjchem-782	172	5	ml	ml	NOUN
eurjchem-782	172	6	)	)	PUNCT
eurjchem-782	172	7	was	be	AUX
eurjchem-782	172	8	added	add	VERB
eurjchem-782	172	9	dropwise	dropwise	NOUN
eurjchem-782	172	10	to	to	ADP
eurjchem-782	172	11	the	the	DET
eurjchem-782	172	12	above	above	ADJ
eurjchem-782	172	13	reaction	reaction	NOUN
eurjchem-782	172	14	mixture	mixture	NOUN
eurjchem-782	172	15	and	and	CCONJ
eurjchem-782	172	16	stirred	stir	VERB
eurjchem-782	172	17	for	for	ADP
eurjchem-782	172	18	another	another	DET
eurjchem-782	172	19	1h	1h	NUM
eurjchem-782	172	20	,	,	PUNCT
eurjchem-782	172	21	followed	follow	VERB
eurjchem-782	172	22	by	by	ADP
eurjchem-782	172	23	dropwise	dropwise	NOUN
eurjchem-782	172	24	addition	addition	NOUN
eurjchem-782	172	25	of	of	ADP
eurjchem-782	172	26	tetralones	tetralone	NOUN
eurjchem-782	172	27	(	(	PUNCT
eurjchem-782	172	28	5.1	5.1	NUM
eurjchem-782	172	29	g	g	NOUN
eurjchem-782	172	30	,	,	PUNCT
eurjchem-782	172	31	0.0138	0.0138	NUM
eurjchem-782	172	32	mol	mol	NUM
eurjchem-782	172	33	)	)	PUNCT
eurjchem-782	172	34	,	,	PUNCT
eurjchem-782	172	35	in	in	ADP
eurjchem-782	172	36	dry	dry	ADJ
eurjchem-782	172	37	benzene	benzene	NOUN
eurjchem-782	172	38	(	(	PUNCT
eurjchem-782	172	39	100	100	NUM
eurjchem-782	172	40	ml	ml	NOUN
eurjchem-782	172	41	)	)	PUNCT
eurjchem-782	172	42	over	over	ADP
eurjchem-782	172	43	a	a	DET
eurjchem-782	172	44	period	period	NOUN
eurjchem-782	172	45	of	of	ADP
eurjchem-782	172	46	1h	1h	NUM
eurjchem-782	172	47	.	.	PUNCT
eurjchem-782	173	1	after	after	ADP
eurjchem-782	173	2	stirring	stir	VERB
eurjchem-782	173	3	the	the	DET
eurjchem-782	173	4	red	red	ADJ
eurjchem-782	173	5	coloured	coloured	ADJ
eurjchem-782	173	6	mixture	mixture	NOUN
eurjchem-782	173	7	at	at	ADP
eurjchem-782	173	8	room	room	NOUN
eurjchem-782	173	9	temperature	temperature	NOUN
eurjchem-782	173	10	for	for	ADP
eurjchem-782	173	11	2h	2h	NUM
eurjchem-782	173	12	,	,	PUNCT
eurjchem-782	173	13	it	it	PRON
eurjchem-782	173	14	was	be	AUX
eurjchem-782	173	15	poured	pour	VERB
eurjchem-782	173	16	into	into	ADP
eurjchem-782	173	17	2n	2n	ADJ
eurjchem-782	173	18	h2so4	h2so4	PROPN
eurjchem-782	173	19	(	(	PUNCT
eurjchem-782	173	20	100	100	NUM
eurjchem-782	173	21	ml	ml	NOUN
eurjchem-782	173	22	)	)	PUNCT
eurjchem-782	173	23	in	in	ADP
eurjchem-782	173	24	ice	ice	NOUN
eurjchem-782	173	25	.	.	PUNCT
eurjchem-782	174	1	the	the	DET
eurjchem-782	174	2	separated	separated	ADJ
eurjchem-782	174	3	organic	organic	ADJ
eurjchem-782	174	4	layer	layer	NOUN
eurjchem-782	174	5	was	be	AUX
eurjchem-782	174	6	washed	wash	VERB
eurjchem-782	174	7	with	with	ADP
eurjchem-782	174	8	water	water	NOUN
eurjchem-782	174	9	(	(	PUNCT
eurjchem-782	174	10	3x50	3x50	NUM
eurjchem-782	174	11	ml	ml	NOUN
eurjchem-782	174	12	)	)	PUNCT
eurjchem-782	174	13	and	and	CCONJ
eurjchem-782	174	14	extracted	extract	VERB
eurjchem-782	174	15	into	into	ADP
eurjchem-782	174	16	saturated	saturated	ADJ
eurjchem-782	174	17	sodium	sodium	NOUN
eurjchem-782	174	18	bicarbonate	bicarbonate	NOUN
eurjchem-782	174	19	solution	solution	NOUN
eurjchem-782	174	20	(	(	PUNCT
eurjchem-782	174	21	3x50	3x50	NUM
eurjchem-782	174	22	ml	ml	NOUN
eurjchem-782	174	23	)	)	PUNCT
eurjchem-782	174	24	,	,	PUNCT
eurjchem-782	174	25	followed	follow	VERB
eurjchem-782	174	26	by	by	ADP
eurjchem-782	174	27	1	1	NUM
eurjchem-782	174	28	%	%	NOUN
eurjchem-782	174	29	sodium	sodium	NOUN
eurjchem-782	174	30	hydroxide	hydroxide	NOUN
eurjchem-782	174	31	solution	solution	NOUN
eurjchem-782	174	32	(	(	PUNCT
eurjchem-782	174	33	3x50	3x50	NUM
eurjchem-782	174	34	ml	ml	NOUN
eurjchem-782	174	35	)	)	PUNCT
eurjchem-782	174	36	.	.	PUNCT
eurjchem-782	175	1	the	the	DET
eurjchem-782	175	2	sodium	sodium	NOUN
eurjchem-782	175	3	hydroxide	hydroxide	NOUN
eurjchem-782	175	4	extract	extract	NOUN
eurjchem-782	175	5	was	be	AUX
eurjchem-782	175	6	acidified	acidify	VERB
eurjchem-782	175	7	with	with	ADP
eurjchem-782	175	8	2n	2n	NUM
eurjchem-782	175	9	h2so4	h2so4	PROPN
eurjchem-782	175	10	gave	give	VERB
eurjchem-782	175	11	products	product	NOUN
eurjchem-782	175	12	in	in	ADP
eurjchem-782	175	13	good	good	ADJ
eurjchem-782	175	14	yields	yield	NOUN
eurjchem-782	175	15	.	.	PUNCT
eurjchem-782	176	1	they	they	PRON
eurjchem-782	176	2	were	be	AUX
eurjchem-782	176	3	recrystallized	recrystallize	VERB
eurjchem-782	176	4	from	from	ADP
eurjchem-782	176	5	ethanol	ethanol	NOUN
eurjchem-782	176	6	(	(	PUNCT
eurjchem-782	176	7	scheme	scheme	NOUN
eurjchem-782	176	8	1	1	NUM
eurjchem-782	176	9	)	)	PUNCT
eurjchem-782	176	10	.	.	PUNCT
eurjchem-782	177	1	(	(	PUNCT
eurjchem-782	177	2	z)‐2‐(hydroxymethylene)‐4‐phenyl‐3,4‐dihydronaphthalen‐	z)‐2‐(hydroxymethylene)‐4‐phenyl‐3,4‐dihydronaphthalen‐	NOUN
eurjchem-782	177	3	1(2h)‐one	1(2h)‐one	NUM
eurjchem-782	177	4	(	(	PUNCT
eurjchem-782	177	5	6a	6a	NOUN
eurjchem-782	177	6	):	):	PUNCT
eurjchem-782	177	7	color	color	NOUN
eurjchem-782	177	8	:	:	PUNCT
eurjchem-782	177	9	dark	dark	PROPN
eurjchem-782	177	10	brown	brown	PROPN
eurjchem-782	177	11	solid	solid	ADJ
eurjchem-782	177	12	.	.	PUNCT
eurjchem-782	177	13	yield	yield	NOUN
eurjchem-782	177	14	:	:	PUNCT
eurjchem-782	177	15	79.09	79.09	NUM
eurjchem-782	177	16	%	%	NOUN
eurjchem-782	177	17	.	.	PUNCT
eurjchem-782	178	1	m.p	m.p	PROPN
eurjchem-782	178	2	.	.	PROPN
eurjchem-782	178	3	:	:	PUNCT
eurjchem-782	179	1	135‐137	135‐137	NUM
eurjchem-782	179	2	oc	oc	PROPN
eurjchem-782	179	3	.	.	PUNCT
eurjchem-782	179	4	yield	yield	NOUN
eurjchem-782	179	5	:	:	PUNCT
eurjchem-782	179	6	79.80	79.80	NUM
eurjchem-782	179	7	%	%	NOUN
eurjchem-782	179	8	.	.	PUNCT
eurjchem-782	180	1	ir	ir	PROPN
eurjchem-782	180	2	(	(	PUNCT
eurjchem-782	180	3	kbr	kbr	PROPN
eurjchem-782	180	4	,	,	PUNCT
eurjchem-782	180	5	ν	ν	PROPN
eurjchem-782	180	6	,	,	PUNCT
eurjchem-782	180	7	cm‐1	cm‐1	PROPN
eurjchem-782	180	8	):	):	PUNCT
eurjchem-782	180	9	3255	3255	NUM
eurjchem-782	180	10	(	(	PUNCT
eurjchem-782	180	11	o‐h	o‐h	PROPN
eurjchem-782	180	12	)	)	PUNCT
eurjchem-782	180	13	,	,	PUNCT
eurjchem-782	180	14	3154	3154	NUM
eurjchem-782	180	15	,	,	PUNCT
eurjchem-782	180	16	2952	2952	NUM
eurjchem-782	180	17	(	(	PUNCT
eurjchem-782	180	18	ar‐ch	ar‐ch	NUM
eurjchem-782	180	19	)	)	PUNCT
eurjchem-782	180	20	,	,	PUNCT
eurjchem-782	180	21	1690	1690	NUM
eurjchem-782	180	22	(	(	PUNCT
eurjchem-782	180	23	c	c	NOUN
eurjchem-782	180	24	=	=	NOUN
eurjchem-782	180	25	o	o	NOUN
eurjchem-782	180	26	)	)	PUNCT
eurjchem-782	180	27	.	.	PUNCT
eurjchem-782	181	1	1h	1h	NUM
eurjchem-782	181	2	nmr	nmr	NOUN
eurjchem-782	181	3	(	(	PUNCT
eurjchem-782	181	4	400	400	NUM
eurjchem-782	181	5	mhz	mhz	NOUN
eurjchem-782	181	6	,	,	PUNCT
eurjchem-782	181	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-782	181	8	,	,	PUNCT
eurjchem-782	181	9	δ	δ	PROPN
eurjchem-782	181	10	,	,	PUNCT
eurjchem-782	181	11	ppm	ppm	NUM
eurjchem-782	181	12	):	):	PUNCT
eurjchem-782	181	13	5.7	5.7	NUM
eurjchem-782	181	14	(	(	PUNCT
eurjchem-782	181	15	s	s	PROPN
eurjchem-782	181	16	,	,	PUNCT
eurjchem-782	181	17	1h	1h	NUM
eurjchem-782	181	18	,	,	PUNCT
eurjchem-782	181	19	oh	oh	INTJ
eurjchem-782	181	20	vinyl	vinyl	NOUN
eurjchem-782	181	21	)	)	PUNCT
eurjchem-782	181	22	,	,	PUNCT
eurjchem-782	181	23	7.75‐7.22	7.75‐7.22	NUM
eurjchem-782	181	24	(	(	PUNCT
eurjchem-782	181	25	m	m	PROPN
eurjchem-782	181	26	,	,	PUNCT
eurjchem-782	181	27	9h	9h	NUM
eurjchem-782	181	28	,	,	PUNCT
eurjchem-782	181	29	ar‐h	ar‐h	NOUN
eurjchem-782	181	30	)	)	PUNCT
eurjchem-782	181	31	,	,	PUNCT
eurjchem-782	181	32	5.53	5.53	NUM
eurjchem-782	181	33	(	(	PUNCT
eurjchem-782	181	34	s	s	PROPN
eurjchem-782	181	35	,	,	PUNCT
eurjchem-782	181	36	1h	1h	NUM
eurjchem-782	181	37	,	,	PUNCT
eurjchem-782	181	38	choh	choh	NOUN
eurjchem-782	181	39	)	)	PUNCT
eurjchem-782	181	40	,	,	PUNCT
eurjchem-782	181	41	4.10	4.10	NUM
eurjchem-782	181	42	(	(	PUNCT
eurjchem-782	181	43	t	t	PROPN
eurjchem-782	181	44	,	,	PUNCT
eurjchem-782	181	45	1h	1h	NUM
eurjchem-782	181	46	,	,	PUNCT
eurjchem-782	181	47	ch	ch	NOUN
eurjchem-782	181	48	)	)	PUNCT
eurjchem-782	181	49	,	,	PUNCT
eurjchem-782	181	50	2.71	2.71	NUM
eurjchem-782	181	51	(	(	PUNCT
eurjchem-782	181	52	d	d	NOUN
eurjchem-782	181	53	,	,	PUNCT
eurjchem-782	181	54	2h	2h	NUM
eurjchem-782	181	55	,	,	PUNCT
eurjchem-782	181	56	ch2	ch2	PROPN
eurjchem-782	181	57	)	)	PUNCT
eurjchem-782	181	58	.	.	PUNCT
eurjchem-782	182	1	13c	13c	NOUN
eurjchem-782	182	2	nmr	nmr	NOUN
eurjchem-782	182	3	(	(	PUNCT
eurjchem-782	182	4	100	100	NUM
eurjchem-782	182	5	mhz	mhz	NOUN
eurjchem-782	182	6	,	,	PUNCT
eurjchem-782	182	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-782	182	8	,	,	PUNCT
eurjchem-782	182	9	δ	δ	PROPN
eurjchem-782	182	10	,	,	PUNCT
eurjchem-782	182	11	ppm	ppm	NUM
eurjchem-782	182	12	):	):	PUNCT
eurjchem-782	182	13	183.6	183.6	NUM
eurjchem-782	182	14	(	(	PUNCT
eurjchem-782	182	15	c‐1	c‐1	NOUN
eurjchem-782	182	16	)	)	PUNCT
eurjchem-782	182	17	,	,	PUNCT
eurjchem-782	182	18	172.9	172.9	NUM
eurjchem-782	182	19	(	(	PUNCT
eurjchem-782	182	20	c‐9	c‐9	PROPN
eurjchem-782	182	21	)	)	PUNCT
eurjchem-782	182	22	,	,	PUNCT
eurjchem-782	182	23	143.4	143.4	NUM
eurjchem-782	182	24	(	(	PUNCT
eurjchem-782	182	25	c‐1	c‐1	NOUN
eurjchem-782	182	26	'	'	PUNCT
eurjchem-782	182	27	)	)	PUNCT
eurjchem-782	182	28	,	,	PUNCT
eurjchem-782	182	29	141.9	141.9	NUM
eurjchem-782	182	30	(	(	PUNCT
eurjchem-782	182	31	c‐5a	c‐5a	PROPN
eurjchem-782	182	32	)	)	PUNCT
eurjchem-782	182	33	,	,	PUNCT
eurjchem-782	182	34	135.2	135.2	NUM
eurjchem-782	182	35	(	(	PUNCT
eurjchem-782	182	36	c‐6	c‐6	NOUN
eurjchem-782	182	37	)	)	PUNCT
eurjchem-782	182	38	,	,	PUNCT
eurjchem-782	182	39	133.0	133.0	NUM
eurjchem-782	182	40	(	(	PUNCT
eurjchem-782	182	41	c‐8a	c‐8a	NOUN
eurjchem-782	182	42	)	)	PUNCT
eurjchem-782	182	43	,	,	PUNCT
eurjchem-782	182	44	129.4	129.4	NUM
eurjchem-782	182	45	(	(	PUNCT
eurjchem-782	182	46	c‐3	c‐3	NOUN
eurjchem-782	182	47	'	'	PUNCT
eurjchem-782	182	48	,	,	PUNCT
eurjchem-782	182	49	c‐5	c‐5	NOUN
eurjchem-782	182	50	'	'	PUNCT
eurjchem-782	182	51	)	)	PUNCT
eurjchem-782	182	52	,	,	PUNCT
eurjchem-782	182	53	128.9	128.9	NUM
eurjchem-782	182	54	(	(	PUNCT
eurjchem-782	182	55	c‐5	c‐5	NOUN
eurjchem-782	182	56	)	)	PUNCT
eurjchem-782	182	57	,	,	PUNCT
eurjchem-782	182	58	128.5	128.5	NUM
eurjchem-782	182	59	(	(	PUNCT
eurjchem-782	182	60	c‐2	c‐2	NOUN
eurjchem-782	182	61	'	'	PUNCT
eurjchem-782	182	62	,	,	PUNCT
eurjchem-782	182	63	c‐6	c‐6	NOUN
eurjchem-782	182	64	'	'	PUNCT
eurjchem-782	182	65	)	)	PUNCT
eurjchem-782	182	66	,	,	PUNCT
eurjchem-782	182	67	127.8	127.8	NUM
eurjchem-782	182	68	(	(	PUNCT
eurjchem-782	182	69	c‐8	c‐8	NOUN
eurjchem-782	182	70	)	)	PUNCT
eurjchem-782	182	71	,	,	PUNCT
eurjchem-782	182	72	126.9	126.9	NUM
eurjchem-782	182	73	(	(	PUNCT
eurjchem-782	182	74	c‐7	c‐7	NOUN
eurjchem-782	182	75	)	)	PUNCT
eurjchem-782	182	76	,	,	PUNCT
eurjchem-782	182	77	126.4	126.4	NUM
eurjchem-782	182	78	(	(	PUNCT
eurjchem-782	182	79	c‐4	c‐4	PROPN
eurjchem-782	182	80	'	'	NUM
eurjchem-782	182	81	)	)	PUNCT
eurjchem-782	182	82	,	,	PUNCT
eurjchem-782	182	83	117.3	117.3	NUM
eurjchem-782	182	84	(	(	PUNCT
eurjchem-782	182	85	c‐2	c‐2	NOUN
eurjchem-782	182	86	)	)	PUNCT
eurjchem-782	182	87	,	,	PUNCT
eurjchem-782	182	88	42.9	42.9	NUM
eurjchem-782	182	89	(	(	PUNCT
eurjchem-782	182	90	c‐4	c‐4	PROPN
eurjchem-782	182	91	)	)	PUNCT
eurjchem-782	182	92	,	,	PUNCT
eurjchem-782	182	93	29.7	29.7	NUM
eurjchem-782	182	94	(	(	PUNCT
eurjchem-782	182	95	c‐3	c‐3	NOUN
eurjchem-782	182	96	)	)	PUNCT
eurjchem-782	182	97	.	.	PUNCT
eurjchem-782	183	1	ms	ms	PROPN
eurjchem-782	183	2	(	(	PUNCT
eurjchem-782	183	3	esi	esi	PROPN
eurjchem-782	183	4	,	,	PUNCT
eurjchem-782	183	5	m	m	PROPN
eurjchem-782	183	6	/	/	SYM
eurjchem-782	183	7	z	z	NOUN
eurjchem-782	183	8	):	):	PUNCT
eurjchem-782	183	9	250.13	250.13	NUM
eurjchem-782	183	10	(	(	PUNCT
eurjchem-782	183	11	m+	m+	NUM
eurjchem-782	183	12	)	)	PUNCT
eurjchem-782	183	13	.	.	PUNCT
eurjchem-782	184	1	anal	anal	PROPN
eurjchem-782	184	2	.	.	PUNCT
eurjchem-782	184	3	calcd	calcd	NOUN
eurjchem-782	184	4	.	.	PUNCT
eurjchem-782	185	1	for	for	ADP
eurjchem-782	185	2	c17h14o2	c17h14o2	NOUN
eurjchem-782	185	3	:	:	PUNCT
eurjchem-782	185	4	c	c	NOUN
eurjchem-782	185	5	,	,	PUNCT
eurjchem-782	185	6	81.58	81.58	NUM
eurjchem-782	185	7	;	;	PUNCT
eurjchem-782	185	8	h	h	X
eurjchem-782	185	9	,	,	PUNCT
eurjchem-782	185	10	5.64	5.64	NUM
eurjchem-782	185	11	.	.	PUNCT
eurjchem-782	185	12	found	find	VERB
eurjchem-782	185	13	:	:	PUNCT
eurjchem-782	186	1	c	c	X
eurjchem-782	186	2	,	,	PUNCT
eurjchem-782	186	3	81.56	81.56	NUM
eurjchem-782	186	4	;	;	PUNCT
eurjchem-782	186	5	h	h	NOUN
eurjchem-782	186	6	,	,	PUNCT
eurjchem-782	186	7	5.61	5.61	NUM
eurjchem-782	186	8	%	%	NOUN
eurjchem-782	186	9	.	.	PUNCT
eurjchem-782	187	1	(	(	PUNCT
eurjchem-782	187	2	z)‐2‐(hydroxymethylene)‐6‐methyl‐4‐phenyl‐3,4‐dihydro	z)‐2‐(hydroxymethylene)‐6‐methyl‐4‐phenyl‐3,4‐dihydro	NUM
eurjchem-782	187	3	naphthalen‐1(2h)‐one	naphthalen‐1(2h)‐one	NOUN
eurjchem-782	187	4	(	(	PUNCT
eurjchem-782	187	5	6b	6b	NOUN
eurjchem-782	187	6	):	):	PUNCT
eurjchem-782	187	7	color	color	NOUN
eurjchem-782	187	8	:	:	PUNCT
eurjchem-782	187	9	dark	dark	PROPN
eurjchem-782	187	10	brown	brown	PROPN
eurjchem-782	187	11	solid	solid	ADJ
eurjchem-782	187	12	.	.	PUNCT
eurjchem-782	187	13	yield	yield	NOUN
eurjchem-782	187	14	:	:	PUNCT
eurjchem-782	187	15	89.08	89.08	NUM
eurjchem-782	187	16	%	%	NOUN
eurjchem-782	187	17	.	.	PUNCT
eurjchem-782	188	1	m.p	m.p	PROPN
eurjchem-782	188	2	.	.	PROPN
eurjchem-782	188	3	:	:	PUNCT
eurjchem-782	189	1	129‐131	129‐131	NUM
eurjchem-782	189	2	oc	oc	PROPN
eurjchem-782	189	3	.	.	PROPN
eurjchem-782	189	4	ir	ir	PROPN
eurjchem-782	189	5	(	(	PUNCT
eurjchem-782	189	6	kbr	kbr	PROPN
eurjchem-782	189	7	,	,	PUNCT
eurjchem-782	189	8	ν	ν	PROPN
eurjchem-782	189	9	,	,	PUNCT
eurjchem-782	189	10	cm‐1	cm‐1	PROPN
eurjchem-782	189	11	):	):	PUNCT
eurjchem-782	189	12	3253	3253	NUM
eurjchem-782	189	13	(	(	PUNCT
eurjchem-782	189	14	o‐h	o‐h	PROPN
eurjchem-782	189	15	)	)	PUNCT
eurjchem-782	189	16	,	,	PUNCT
eurjchem-782	189	17	3152	3152	NUM
eurjchem-782	189	18	,	,	PUNCT
eurjchem-782	189	19	2951	2951	NUM
eurjchem-782	189	20	(	(	PUNCT
eurjchem-782	189	21	ar‐ch	ar‐ch	NUM
eurjchem-782	189	22	)	)	PUNCT
eurjchem-782	189	23	,	,	PUNCT
eurjchem-782	189	24	1690	1690	NUM
eurjchem-782	189	25	(	(	PUNCT
eurjchem-782	189	26	c	c	NOUN
eurjchem-782	189	27	=	=	NOUN
eurjchem-782	189	28	o	o	NOUN
eurjchem-782	189	29	)	)	PUNCT
eurjchem-782	189	30	.	.	PUNCT
eurjchem-782	190	1	1h	1h	NUM
eurjchem-782	190	2	nmr	nmr	NOUN
eurjchem-782	190	3	(	(	PUNCT
eurjchem-782	190	4	400	400	NUM
eurjchem-782	190	5	mhz	mhz	NOUN
eurjchem-782	190	6	,	,	PUNCT
eurjchem-782	190	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-782	190	8	,	,	PUNCT
eurjchem-782	190	9	δ	δ	PROPN
eurjchem-782	190	10	,	,	PUNCT
eurjchem-782	190	11	ppm	ppm	NUM
eurjchem-782	190	12	):	):	PUNCT
eurjchem-782	190	13	5.6	5.6	NUM
eurjchem-782	190	14	(	(	PUNCT
eurjchem-782	190	15	s	s	PROPN
eurjchem-782	190	16	,	,	PUNCT
eurjchem-782	190	17	1h	1h	NUM
eurjchem-782	190	18	,	,	PUNCT
eurjchem-782	190	19	oh	oh	INTJ
eurjchem-782	190	20	,	,	PUNCT
eurjchem-782	190	21	vinyl	vinyl	NOUN
eurjchem-782	190	22	)	)	PUNCT
eurjchem-782	190	23	,	,	PUNCT
eurjchem-782	190	24	7.76‐7.22	7.76‐7.22	NUM
eurjchem-782	190	25	(	(	PUNCT
eurjchem-782	190	26	m	m	PROPN
eurjchem-782	190	27	,	,	PUNCT
eurjchem-782	190	28	8h	8h	NUM
eurjchem-782	190	29	,	,	PUNCT
eurjchem-782	190	30	ar‐h	ar‐h	PROPN
eurjchem-782	190	31	)	)	PUNCT
eurjchem-782	190	32	,	,	PUNCT
eurjchem-782	190	33	5.51	5.51	NUM
eurjchem-782	190	34	(	(	PUNCT
eurjchem-782	190	35	s	s	PROPN
eurjchem-782	190	36	,	,	PUNCT
eurjchem-782	190	37	1h	1h	NUM
eurjchem-782	190	38	,	,	PUNCT
eurjchem-782	190	39	choh	choh	NOUN
eurjchem-782	190	40	)	)	PUNCT
eurjchem-782	190	41	,	,	PUNCT
eurjchem-782	190	42	4.15	4.15	NUM
eurjchem-782	190	43	(	(	PUNCT
eurjchem-782	190	44	t	t	PROPN
eurjchem-782	190	45	,	,	PUNCT
eurjchem-782	190	46	1h	1h	NUM
eurjchem-782	190	47	,	,	PUNCT
eurjchem-782	190	48	ch	ch	NOUN
eurjchem-782	190	49	)	)	PUNCT
eurjchem-782	190	50	,	,	PUNCT
eurjchem-782	190	51	2.86	2.86	NUM
eurjchem-782	190	52	(	(	PUNCT
eurjchem-782	190	53	s	s	PROPN
eurjchem-782	190	54	,	,	PUNCT
eurjchem-782	190	55	3h	3h	NUM
eurjchem-782	190	56	,	,	PUNCT
eurjchem-782	190	57	ch3	ch3	PROPN
eurjchem-782	190	58	)	)	PUNCT
eurjchem-782	190	59	,	,	PUNCT
eurjchem-782	190	60	2.74	2.74	NUM
eurjchem-782	190	61	(	(	PUNCT
eurjchem-782	190	62	d	d	NOUN
eurjchem-782	190	63	,	,	PUNCT
eurjchem-782	190	64	2h	2h	NUM
eurjchem-782	190	65	,	,	PUNCT
eurjchem-782	190	66	ch2	ch2	PROPN
eurjchem-782	190	67	)	)	PUNCT
eurjchem-782	190	68	.	.	PUNCT
eurjchem-782	191	1	13c	13c	NOUN
eurjchem-782	191	2	nmr	nmr	NOUN
eurjchem-782	191	3	(	(	PUNCT
eurjchem-782	191	4	100	100	NUM
eurjchem-782	191	5	mhz	mhz	NOUN
eurjchem-782	191	6	,	,	PUNCT
eurjchem-782	191	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-782	191	8	,	,	PUNCT
eurjchem-782	191	9	δ	δ	PROPN
eurjchem-782	191	10	,	,	PUNCT
eurjchem-782	191	11	ppm	ppm	NUM
eurjchem-782	191	12	):	):	PUNCT
eurjchem-782	191	13	183.5	183.5	NUM
eurjchem-782	191	14	(	(	PUNCT
eurjchem-782	191	15	c‐1	c‐1	NOUN
eurjchem-782	191	16	)	)	PUNCT
eurjchem-782	191	17	,	,	PUNCT
eurjchem-782	191	18	173.6	173.6	NUM
eurjchem-782	191	19	(	(	PUNCT
eurjchem-782	191	20	c‐9	c‐9	PROPN
eurjchem-782	191	21	)	)	PUNCT
eurjchem-782	191	22	,	,	PUNCT
eurjchem-782	191	23	144.5	144.5	NUM
eurjchem-782	191	24	(	(	PUNCT
eurjchem-782	191	25	c‐6	c‐6	NOUN
eurjchem-782	191	26	)	)	PUNCT
eurjchem-782	191	27	,	,	PUNCT
eurjchem-782	191	28	143.1	143.1	NUM
eurjchem-782	191	29	(	(	PUNCT
eurjchem-782	191	30	c‐1	c‐1	NOUN
eurjchem-782	191	31	'	'	PUNCT
eurjchem-782	191	32	)	)	PUNCT
eurjchem-782	191	33	,	,	PUNCT
eurjchem-782	191	34	141.9	141.9	NUM
eurjchem-782	191	35	(	(	PUNCT
eurjchem-782	191	36	c‐5a	c‐5a	PROPN
eurjchem-782	191	37	)	)	PUNCT
eurjchem-782	191	38	,	,	PUNCT
eurjchem-782	191	39	130.5	130.5	NUM
eurjchem-782	191	40	(	(	PUNCT
eurjchem-782	191	41	c‐8	c‐8	NOUN
eurjchem-782	191	42	)	)	PUNCT
eurjchem-782	191	43	,	,	PUNCT
eurjchem-782	191	44	130.1	130.1	NUM
eurjchem-782	191	45	(	(	PUNCT
eurjchem-782	191	46	c‐	c‐	NOUN
eurjchem-782	191	47	8a	8a	NUM
eurjchem-782	191	48	)	)	PUNCT
eurjchem-782	191	49	,	,	PUNCT
eurjchem-782	191	50	129.9	129.9	NUM
eurjchem-782	191	51	(	(	PUNCT
eurjchem-782	191	52	c‐3	c‐3	NOUN
eurjchem-782	191	53	'	'	PUNCT
eurjchem-782	191	54	,	,	PUNCT
eurjchem-782	191	55	c‐5	c‐5	NOUN
eurjchem-782	191	56	'	'	PUNCT
eurjchem-782	191	57	)	)	PUNCT
eurjchem-782	191	58	,	,	PUNCT
eurjchem-782	191	59	128.6	128.6	NUM
eurjchem-782	191	60	(	(	PUNCT
eurjchem-782	191	61	c‐5	c‐5	NOUN
eurjchem-782	191	62	)	)	PUNCT
eurjchem-782	191	63	,	,	PUNCT
eurjchem-782	191	64	128.4	128.4	NUM
eurjchem-782	191	65	(	(	PUNCT
eurjchem-782	191	66	c‐2	c‐2	NOUN
eurjchem-782	191	67	'	'	PUNCT
eurjchem-782	191	68	,	,	PUNCT
eurjchem-782	191	69	c‐6	c‐6	NOUN
eurjchem-782	191	70	'	'	PUNCT
eurjchem-782	191	71	)	)	PUNCT
eurjchem-782	191	72	,	,	PUNCT
eurjchem-782	191	73	127.0	127.0	NUM
eurjchem-782	191	74	(	(	PUNCT
eurjchem-782	191	75	c‐	c‐	NOUN
eurjchem-782	191	76	7	7	NUM
eurjchem-782	191	77	)	)	PUNCT
eurjchem-782	191	78	,	,	PUNCT
eurjchem-782	191	79	126.4	126.4	NUM
eurjchem-782	191	80	(	(	PUNCT
eurjchem-782	191	81	c‐4	c‐4	PROPN
eurjchem-782	191	82	'	'	NUM
eurjchem-782	191	83	)	)	PUNCT
eurjchem-782	191	84	,	,	PUNCT
eurjchem-782	191	85	117.9	117.9	NUM
eurjchem-782	191	86	(	(	PUNCT
eurjchem-782	191	87	c‐2	c‐2	NOUN
eurjchem-782	191	88	)	)	PUNCT
eurjchem-782	191	89	,	,	PUNCT
eurjchem-782	191	90	42.5	42.5	NUM
eurjchem-782	191	91	(	(	PUNCT
eurjchem-782	191	92	c‐4	c‐4	PROPN
eurjchem-782	191	93	)	)	PUNCT
eurjchem-782	191	94	,	,	PUNCT
eurjchem-782	191	95	29.8	29.8	NUM
eurjchem-782	191	96	(	(	PUNCT
eurjchem-782	191	97	c‐3	c‐3	NOUN
eurjchem-782	191	98	)	)	PUNCT
eurjchem-782	191	99	,	,	PUNCT
eurjchem-782	191	100	29.5(‐ch3	29.5(‐ch3	NUM
eurjchem-782	191	101	)	)	PUNCT
eurjchem-782	191	102	.	.	PUNCT
eurjchem-782	192	1	ms	ms	PROPN
eurjchem-782	192	2	(	(	PUNCT
eurjchem-782	192	3	esi	esi	PROPN
eurjchem-782	192	4	,	,	PUNCT
eurjchem-782	192	5	m	m	PROPN
eurjchem-782	192	6	/	/	SYM
eurjchem-782	192	7	z	z	NOUN
eurjchem-782	192	8	):	):	PUNCT
eurjchem-782	192	9	264.12	264.12	NUM
eurjchem-782	192	10	(	(	PUNCT
eurjchem-782	192	11	m+	m+	NUM
eurjchem-782	192	12	)	)	PUNCT
eurjchem-782	192	13	.	.	PUNCT
eurjchem-782	193	1	anal	anal	PROPN
eurjchem-782	193	2	.	.	PUNCT
eurjchem-782	193	3	calcd	calcd	NOUN
eurjchem-782	193	4	.	.	PUNCT
eurjchem-782	194	1	for	for	SCONJ
eurjchem-782	194	2	c18h16o2	c18h16o2	PROPN
eurjchem-782	194	3	:	:	PUNCT
eurjchem-782	194	4	c	c	X
eurjchem-782	194	5	,	,	PUNCT
eurjchem-782	194	6	81.79	81.79	NUM
eurjchem-782	194	7	;	;	PUNCT
eurjchem-782	194	8	h	h	NOUN
eurjchem-782	194	9	,	,	PUNCT
eurjchem-782	194	10	6.10	6.10	NUM
eurjchem-782	194	11	.	.	PUNCT
eurjchem-782	194	12	found	find	VERB
eurjchem-782	194	13	:	:	PUNCT
eurjchem-782	195	1	c	c	X
eurjchem-782	195	2	,	,	PUNCT
eurjchem-782	195	3	81.75	81.75	NUM
eurjchem-782	195	4	;	;	PUNCT
eurjchem-782	195	5	h	h	NOUN
eurjchem-782	195	6	,	,	PUNCT
eurjchem-782	195	7	6.13	6.13	NUM
eurjchem-782	195	8	%	%	NOUN
eurjchem-782	195	9	.	.	PUNCT
eurjchem-782	196	1	(	(	PUNCT
eurjchem-782	196	2	z)‐2‐(hydroxymethylene)‐6‐methoxy‐4‐phenyl‐3,4‐dihydro	z)‐2‐(hydroxymethylene)‐6‐methoxy‐4‐phenyl‐3,4‐dihydro	PROPN
eurjchem-782	196	3	naphthalen‐1(2h)‐one	naphthalen‐1(2h)‐one	NUM
eurjchem-782	196	4	(	(	PUNCT
eurjchem-782	196	5	6c	6c	NOUN
eurjchem-782	196	6	):	):	PUNCT
eurjchem-782	196	7	color	color	NOUN
eurjchem-782	196	8	:	:	PUNCT
eurjchem-782	196	9	dark	dark	PROPN
eurjchem-782	196	10	brown	brown	PROPN
eurjchem-782	196	11	solid	solid	ADJ
eurjchem-782	196	12	.	.	PUNCT
eurjchem-782	196	13	yield	yield	NOUN
eurjchem-782	196	14	:	:	PUNCT
eurjchem-782	196	15	65.32	65.32	NUM
eurjchem-782	196	16	%	%	NOUN
eurjchem-782	196	17	.	.	PUNCT
eurjchem-782	197	1	m.p	m.p	PROPN
eurjchem-782	197	2	.	.	PROPN
eurjchem-782	197	3	:	:	PUNCT
eurjchem-782	198	1	140‐142	140‐142	NUM
eurjchem-782	198	2	oc	oc	PROPN
eurjchem-782	198	3	.	.	PROPN
eurjchem-782	198	4	ir	ir	PROPN
eurjchem-782	198	5	(	(	PUNCT
eurjchem-782	198	6	kbr	kbr	PROPN
eurjchem-782	198	7	,	,	PUNCT
eurjchem-782	198	8	ν	ν	PROPN
eurjchem-782	198	9	,	,	PUNCT
eurjchem-782	198	10	cm‐1	cm‐1	PROPN
eurjchem-782	198	11	):	):	PUNCT
eurjchem-782	198	12	3251	3251	NUM
eurjchem-782	198	13	(	(	PUNCT
eurjchem-782	198	14	o‐h	o‐h	PROPN
eurjchem-782	198	15	)	)	PUNCT
eurjchem-782	198	16	,	,	PUNCT
eurjchem-782	198	17	3156	3156	NUM
eurjchem-782	198	18	,	,	PUNCT
eurjchem-782	198	19	2958	2958	NUM
eurjchem-782	198	20	(	(	PUNCT
eurjchem-782	198	21	ar‐ch	ar‐ch	NOUN
eurjchem-782	198	22	)	)	PUNCT
eurjchem-782	198	23	,	,	PUNCT
eurjchem-782	198	24	1672	1672	NUM
eurjchem-782	198	25	(	(	PUNCT
eurjchem-782	198	26	c	c	NOUN
eurjchem-782	198	27	=	=	NOUN
eurjchem-782	198	28	o	o	NOUN
eurjchem-782	198	29	)	)	PUNCT
eurjchem-782	198	30	.	.	PUNCT
eurjchem-782	199	1	1h	1h	NUM
eurjchem-782	199	2	nmr	nmr	NOUN
eurjchem-782	199	3	(	(	PUNCT
eurjchem-782	199	4	400	400	NUM
eurjchem-782	199	5	mhz	mhz	NOUN
eurjchem-782	199	6	,	,	PUNCT
eurjchem-782	199	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-782	199	8	,	,	PUNCT
eurjchem-782	199	9	δ	δ	PROPN
eurjchem-782	199	10	,	,	PUNCT
eurjchem-782	199	11	ppm	ppm	NUM
eurjchem-782	199	12	):	):	PUNCT
eurjchem-782	199	13	5.8	5.8	NUM
eurjchem-782	199	14	(	(	PUNCT
eurjchem-782	199	15	s	s	PROPN
eurjchem-782	199	16	,	,	PUNCT
eurjchem-782	199	17	1h	1h	NUM
eurjchem-782	199	18	,	,	PUNCT
eurjchem-782	199	19	oh	oh	INTJ
eurjchem-782	199	20	vinyl	vinyl	NOUN
eurjchem-782	199	21	)	)	PUNCT
eurjchem-782	199	22	,	,	PUNCT
eurjchem-782	199	23	7.79‐7.26	7.79‐7.26	NUM
eurjchem-782	199	24	(	(	PUNCT
eurjchem-782	199	25	m	m	PROPN
eurjchem-782	199	26	,	,	PUNCT
eurjchem-782	199	27	8h	8h	NUM
eurjchem-782	199	28	,	,	PUNCT
eurjchem-782	199	29	ar‐h	ar‐h	PROPN
eurjchem-782	199	30	)	)	PUNCT
eurjchem-782	199	31	,	,	PUNCT
eurjchem-782	199	32	5.51	5.51	NUM
eurjchem-782	199	33	(	(	PUNCT
eurjchem-782	199	34	s	s	PROPN
eurjchem-782	199	35	,	,	PUNCT
eurjchem-782	199	36	1h	1h	NUM
eurjchem-782	199	37	,	,	PUNCT
eurjchem-782	199	38	choh	choh	NOUN
eurjchem-782	199	39	)	)	PUNCT
eurjchem-782	199	40	,	,	PUNCT
eurjchem-782	199	41	4.11	4.11	NUM
eurjchem-782	199	42	(	(	PUNCT
eurjchem-782	199	43	t	t	PROPN
eurjchem-782	199	44	,	,	PUNCT
eurjchem-782	199	45	1h	1h	NUM
eurjchem-782	199	46	,	,	PUNCT
eurjchem-782	199	47	ch	ch	NOUN
eurjchem-782	199	48	)	)	PUNCT
eurjchem-782	199	49	,	,	PUNCT
eurjchem-782	199	50	3.87	3.87	NUM
eurjchem-782	199	51	(	(	PUNCT
eurjchem-782	199	52	s	s	PROPN
eurjchem-782	199	53	,	,	PUNCT
eurjchem-782	199	54	3h	3h	NUM
eurjchem-782	199	55	,	,	PUNCT
eurjchem-782	199	56	och3	och3	ADJ
eurjchem-782	199	57	)	)	PUNCT
eurjchem-782	199	58	,	,	PUNCT
eurjchem-782	199	59	2.76	2.76	NUM
eurjchem-782	199	60	(	(	PUNCT
eurjchem-782	199	61	d	d	PROPN
eurjchem-782	199	62	,	,	PUNCT
eurjchem-782	199	63	2h	2h	NUM
eurjchem-782	199	64	,	,	PUNCT
eurjchem-782	199	65	ch2	ch2	PROPN
eurjchem-782	199	66	)	)	PUNCT
eurjchem-782	199	67	.	.	PUNCT
eurjchem-782	200	1	13c	13c	NOUN
eurjchem-782	200	2	nmr	nmr	NOUN
eurjchem-782	200	3	(	(	PUNCT
eurjchem-782	200	4	100	100	NUM
eurjchem-782	200	5	mhz	mhz	NOUN
eurjchem-782	200	6	,	,	PUNCT
eurjchem-782	200	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-782	200	8	,	,	PUNCT
eurjchem-782	200	9	δ	δ	PROPN
eurjchem-782	200	10	,	,	PUNCT
eurjchem-782	200	11	ppm	ppm	NUM
eurjchem-782	200	12	):	):	PUNCT
eurjchem-782	200	13	183.4	183.4	NUM
eurjchem-782	200	14	(	(	PUNCT
eurjchem-782	200	15	c‐1	c‐1	NOUN
eurjchem-782	200	16	)	)	PUNCT
eurjchem-782	200	17	,	,	PUNCT
eurjchem-782	200	18	172.6	172.6	NUM
eurjchem-782	200	19	(	(	PUNCT
eurjchem-782	200	20	c‐9	c‐9	PROPN
eurjchem-782	200	21	)	)	PUNCT
eurjchem-782	200	22	,	,	PUNCT
eurjchem-782	200	23	166.7	166.7	NUM
eurjchem-782	200	24	(	(	PUNCT
eurjchem-782	200	25	c‐6	c‐6	NOUN
eurjchem-782	200	26	)	)	PUNCT
eurjchem-782	200	27	,	,	PUNCT
eurjchem-782	200	28	143.3	143.3	NUM
eurjchem-782	200	29	(	(	PUNCT
eurjchem-782	200	30	c‐1	c‐1	NOUN
eurjchem-782	200	31	'	'	PUNCT
eurjchem-782	200	32	)	)	PUNCT
eurjchem-782	200	33	,	,	PUNCT
eurjchem-782	200	34	142.4	142.4	NUM
eurjchem-782	200	35	(	(	PUNCT
eurjchem-782	200	36	c‐5a	c‐5a	PROPN
eurjchem-782	200	37	)	)	PUNCT
eurjchem-782	200	38	,	,	PUNCT
eurjchem-782	200	39	129.9(c‐8	129.9(c‐8	PROPN
eurjchem-782	200	40	)	)	PUNCT
eurjchem-782	200	41	,	,	PUNCT
eurjchem-782	200	42	129.4	129.4	NUM
eurjchem-782	200	43	(	(	PUNCT
eurjchem-782	200	44	c‐3	c‐3	NOUN
eurjchem-782	200	45	'	'	PUNCT
eurjchem-782	200	46	,	,	PUNCT
eurjchem-782	200	47	c‐5	c‐5	NOUN
eurjchem-782	200	48	'	'	PUNCT
eurjchem-782	200	49	)	)	PUNCT
eurjchem-782	200	50	,	,	PUNCT
eurjchem-782	200	51	128.7	128.7	NUM
eurjchem-782	200	52	(	(	PUNCT
eurjchem-782	200	53	c‐2	c‐2	NOUN
eurjchem-782	200	54	'	'	PUNCT
eurjchem-782	200	55	,	,	PUNCT
eurjchem-782	200	56	c‐6	c‐6	NOUN
eurjchem-782	200	57	'	'	PUNCT
eurjchem-782	200	58	)	)	PUNCT
eurjchem-782	200	59	,	,	PUNCT
eurjchem-782	200	60	126.4	126.4	NUM
eurjchem-782	200	61	(	(	PUNCT
eurjchem-782	200	62	c‐4	c‐4	PROPN
eurjchem-782	200	63	'	'	NUM
eurjchem-782	200	64	)	)	PUNCT
eurjchem-782	200	65	,	,	PUNCT
eurjchem-782	200	66	125.9	125.9	NUM
eurjchem-782	200	67	(	(	PUNCT
eurjchem-782	200	68	c‐8a	c‐8a	PROPN
eurjchem-782	200	69	)	)	PUNCT
eurjchem-782	200	70	,	,	PUNCT
eurjchem-782	200	71	117.3	117.3	NUM
eurjchem-782	200	72	(	(	PUNCT
eurjchem-782	200	73	c‐2	c‐2	NOUN
eurjchem-782	200	74	)	)	PUNCT
eurjchem-782	200	75	,	,	PUNCT
eurjchem-782	200	76	112.5	112.5	NUM
eurjchem-782	200	77	(	(	PUNCT
eurjchem-782	200	78	c‐7	c‐7	NOUN
eurjchem-782	200	79	)	)	PUNCT
eurjchem-782	200	80	,	,	PUNCT
eurjchem-782	200	81	105.8	105.8	NUM
eurjchem-782	200	82	(	(	PUNCT
eurjchem-782	200	83	c‐5	c‐5	NOUN
eurjchem-782	200	84	)	)	PUNCT
eurjchem-782	200	85	,	,	PUNCT
eurjchem-782	200	86	‐55.9	‐55.9	PROPN
eurjchem-782	200	87	(	(	PUNCT
eurjchem-782	200	88	‐och3	‐och3	NOUN
eurjchem-782	200	89	)	)	PUNCT
eurjchem-782	200	90	,	,	PUNCT
eurjchem-782	200	91	42.8	42.8	NUM
eurjchem-782	200	92	(	(	PUNCT
eurjchem-782	200	93	c‐4	c‐4	PROPN
eurjchem-782	200	94	)	)	PUNCT
eurjchem-782	200	95	,	,	PUNCT
eurjchem-782	200	96	29.4	29.4	NUM
eurjchem-782	200	97	(	(	PUNCT
eurjchem-782	200	98	c‐3	c‐3	NOUN
eurjchem-782	200	99	)	)	PUNCT
eurjchem-782	200	100	.	.	PUNCT
eurjchem-782	201	1	238	238	NUM
eurjchem-782	201	2	umesha	umesha	ADJ
eurjchem-782	201	3	and	and	CCONJ
eurjchem-782	201	4	basavaraju	basavaraju	NOUN
eurjchem-782	201	5	/	/	SYM
eurjchem-782	201	6	european	european	ADJ
eurjchem-782	201	7	journal	journal	PROPN
eurjchem-782	201	8	of	of	ADP
eurjchem-782	201	9	chemistry	chemistry	NOUN
eurjchem-782	201	10	4	4	NUM
eurjchem-782	201	11	(	(	PUNCT
eurjchem-782	201	12	3	3	NUM
eurjchem-782	201	13	)	)	PUNCT
eurjchem-782	201	14	(	(	PUNCT
eurjchem-782	201	15	2013	2013	NUM
eurjchem-782	201	16	)	)	PUNCT
eurjchem-782	201	17	235‐239	235‐239	NUM
eurjchem-782	201	18	ms	ms	NOUN
eurjchem-782	201	19	(	(	PUNCT
eurjchem-782	201	20	esi	esi	PROPN
eurjchem-782	201	21	,	,	PUNCT
eurjchem-782	201	22	m	m	PROPN
eurjchem-782	201	23	/	/	SYM
eurjchem-782	201	24	z	z	NOUN
eurjchem-782	201	25	):	):	PUNCT
eurjchem-782	201	26	280.14	280.14	NUM
eurjchem-782	201	27	(	(	PUNCT
eurjchem-782	201	28	m+	m+	NUM
eurjchem-782	201	29	)	)	PUNCT
eurjchem-782	201	30	.	.	PUNCT
eurjchem-782	202	1	anal	anal	PROPN
eurjchem-782	202	2	.	.	PUNCT
eurjchem-782	202	3	calcd	calcd	NOUN
eurjchem-782	202	4	.	.	PUNCT
eurjchem-782	203	1	for	for	ADP
eurjchem-782	203	2	c18h16o3	c18h16o3	PROPN
eurjchem-782	203	3	:	:	PUNCT
eurjchem-782	203	4	c	c	X
eurjchem-782	203	5	,	,	PUNCT
eurjchem-782	203	6	77.12	77.12	NUM
eurjchem-782	203	7	;	;	PUNCT
eurjchem-782	203	8	h	h	X
eurjchem-782	203	9	,	,	PUNCT
eurjchem-782	203	10	5.75	5.75	NUM
eurjchem-782	203	11	.	.	PUNCT
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eurjchem-782	203	13	:	:	PUNCT
eurjchem-782	204	1	c	c	X
eurjchem-782	204	2	,	,	PUNCT
eurjchem-782	204	3	77.15	77.15	NUM
eurjchem-782	204	4	;	;	PUNCT
eurjchem-782	204	5	h	h	NOUN
eurjchem-782	204	6	,	,	PUNCT
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eurjchem-782	204	8	%	%	NOUN
eurjchem-782	204	9	.	.	PUNCT
eurjchem-782	205	1	(	(	PUNCT
eurjchem-782	205	2	z)‐2‐(hydroxymethylene)‐6‐(methylthio)‐4‐phenyl‐3,4‐	z)‐2‐(hydroxymethylene)‐6‐(methylthio)‐4‐phenyl‐3,4‐	NUM
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eurjchem-782	205	4	(	(	PUNCT
eurjchem-782	205	5	6d	6d	NUM
eurjchem-782	205	6	):	):	PUNCT
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eurjchem-782	205	8	:	:	PUNCT
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eurjchem-782	205	12	.	.	PUNCT
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eurjchem-782	205	14	:	:	PUNCT
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eurjchem-782	206	1	m.p	m.p	PROPN
eurjchem-782	206	2	.	.	PROPN
eurjchem-782	206	3	:	:	PUNCT
eurjchem-782	207	1	145‐147	145‐147	PROPN
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eurjchem-782	207	3	.	.	PROPN
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eurjchem-782	207	5	(	(	PUNCT
eurjchem-782	207	6	kbr	kbr	PROPN
eurjchem-782	207	7	,	,	PUNCT
eurjchem-782	207	8	ν	ν	PROPN
eurjchem-782	207	9	,	,	PUNCT
eurjchem-782	207	10	cm‐1	cm‐1	PROPN
eurjchem-782	207	11	):	):	PUNCT
eurjchem-782	207	12	3258	3258	NUM
eurjchem-782	207	13	(	(	PUNCT
eurjchem-782	207	14	o‐h	o‐h	PROPN
eurjchem-782	207	15	)	)	PUNCT
eurjchem-782	207	16	,	,	PUNCT
eurjchem-782	207	17	3159‐2952	3159‐2952	NUM
eurjchem-782	207	18	(	(	PUNCT
eurjchem-782	207	19	ar‐ch	ar‐ch	NUM
eurjchem-782	207	20	)	)	PUNCT
eurjchem-782	207	21	,	,	PUNCT
eurjchem-782	207	22	1678	1678	NUM
eurjchem-782	207	23	(	(	PUNCT
eurjchem-782	207	24	c	c	NOUN
eurjchem-782	207	25	=	=	NOUN
eurjchem-782	207	26	o	o	NOUN
eurjchem-782	207	27	)	)	PUNCT
eurjchem-782	207	28	.	.	PUNCT
eurjchem-782	208	1	1h	1h	NUM
eurjchem-782	208	2	nmr	nmr	NOUN
eurjchem-782	208	3	(	(	PUNCT
eurjchem-782	208	4	400	400	NUM
eurjchem-782	208	5	mhz	mhz	NOUN
eurjchem-782	208	6	,	,	PUNCT
eurjchem-782	208	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-782	208	8	,	,	PUNCT
eurjchem-782	208	9	δ	δ	PROPN
eurjchem-782	208	10	,	,	PUNCT
eurjchem-782	208	11	ppm	ppm	NUM
eurjchem-782	208	12	):	):	PUNCT
eurjchem-782	208	13	5.6	5.6	NUM
eurjchem-782	208	14	(	(	PUNCT
eurjchem-782	208	15	s	s	PROPN
eurjchem-782	208	16	,	,	PUNCT
eurjchem-782	208	17	1h	1h	NUM
eurjchem-782	208	18	,	,	PUNCT
eurjchem-782	208	19	oh	oh	INTJ
eurjchem-782	208	20	vinyl	vinyl	NOUN
eurjchem-782	208	21	)	)	PUNCT
eurjchem-782	208	22	,	,	PUNCT
eurjchem-782	208	23	7.75‐7.27	7.75‐7.27	X
eurjchem-782	208	24	(	(	PUNCT
eurjchem-782	208	25	m	m	PROPN
eurjchem-782	208	26	,	,	PUNCT
eurjchem-782	208	27	8h	8h	NUM
eurjchem-782	208	28	,	,	PUNCT
eurjchem-782	208	29	ar‐h	ar‐h	PROPN
eurjchem-782	208	30	)	)	PUNCT
eurjchem-782	208	31	,	,	PUNCT
eurjchem-782	208	32	5.49	5.49	NUM
eurjchem-782	208	33	(	(	PUNCT
eurjchem-782	208	34	s	s	PROPN
eurjchem-782	208	35	,	,	PUNCT
eurjchem-782	208	36	1h	1h	NUM
eurjchem-782	208	37	,	,	PUNCT
eurjchem-782	208	38	choh	choh	NOUN
eurjchem-782	208	39	)	)	PUNCT
eurjchem-782	208	40	,	,	PUNCT
eurjchem-782	208	41	4.09	4.09	NUM
eurjchem-782	208	42	(	(	PUNCT
eurjchem-782	208	43	t	t	PROPN
eurjchem-782	208	44	,	,	PUNCT
eurjchem-782	208	45	1h	1h	NUM
eurjchem-782	208	46	,	,	PUNCT
eurjchem-782	208	47	ch	ch	NOUN
eurjchem-782	208	48	)	)	PUNCT
eurjchem-782	208	49	,	,	PUNCT
eurjchem-782	208	50	2.61	2.61	NUM
eurjchem-782	208	51	(	(	PUNCT
eurjchem-782	208	52	s	s	PROPN
eurjchem-782	208	53	,	,	PUNCT
eurjchem-782	208	54	3h	3h	NUM
eurjchem-782	208	55	,	,	PUNCT
eurjchem-782	208	56	sch3	sch3	PROPN
eurjchem-782	208	57	)	)	PUNCT
eurjchem-782	208	58	,	,	PUNCT
eurjchem-782	208	59	2.78	2.78	NUM
eurjchem-782	208	60	(	(	PUNCT
eurjchem-782	208	61	d	d	PROPN
eurjchem-782	208	62	,	,	PUNCT
eurjchem-782	208	63	2h	2h	NUM
eurjchem-782	208	64	,	,	PUNCT
eurjchem-782	208	65	ch2	ch2	PROPN
eurjchem-782	208	66	)	)	PUNCT
eurjchem-782	208	67	.	.	PUNCT
eurjchem-782	209	1	13c	13c	NOUN
eurjchem-782	209	2	nmr	nmr	NOUN
eurjchem-782	209	3	(	(	PUNCT
eurjchem-782	209	4	100	100	NUM
eurjchem-782	209	5	mhz	mhz	NOUN
eurjchem-782	209	6	,	,	PUNCT
eurjchem-782	209	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-782	209	8	,	,	PUNCT
eurjchem-782	209	9	δ	δ	PROPN
eurjchem-782	209	10	,	,	PUNCT
eurjchem-782	209	11	ppm	ppm	NUM
eurjchem-782	209	12	):	):	PUNCT
eurjchem-782	209	13	183.6	183.6	NUM
eurjchem-782	209	14	(	(	PUNCT
eurjchem-782	209	15	c‐1	c‐1	NOUN
eurjchem-782	209	16	)	)	PUNCT
eurjchem-782	209	17	,	,	PUNCT
eurjchem-782	209	18	172.5	172.5	NUM
eurjchem-782	209	19	(	(	PUNCT
eurjchem-782	209	20	c‐9	c‐9	NOUN
eurjchem-782	209	21	)	)	PUNCT
eurjchem-782	209	22	,	,	PUNCT
eurjchem-782	209	23	145.9	145.9	NUM
eurjchem-782	209	24	(	(	PUNCT
eurjchem-782	209	25	c‐6	c‐6	NOUN
eurjchem-782	209	26	)	)	PUNCT
eurjchem-782	209	27	,	,	PUNCT
eurjchem-782	209	28	143.3	143.3	NUM
eurjchem-782	209	29	(	(	PUNCT
eurjchem-782	209	30	c‐1	c‐1	NOUN
eurjchem-782	209	31	'	'	PUNCT
eurjchem-782	209	32	)	)	PUNCT
eurjchem-782	209	33	,	,	PUNCT
eurjchem-782	209	34	141.9	141.9	NUM
eurjchem-782	209	35	(	(	PUNCT
eurjchem-782	209	36	c‐5a	c‐5a	PROPN
eurjchem-782	209	37	)	)	PUNCT
eurjchem-782	209	38	,	,	PUNCT
eurjchem-782	209	39	130.7	130.7	NUM
eurjchem-782	209	40	(	(	PUNCT
eurjchem-782	209	41	c‐8	c‐8	NOUN
eurjchem-782	209	42	)	)	PUNCT
eurjchem-782	209	43	,	,	PUNCT
eurjchem-782	209	44	129.6	129.6	NUM
eurjchem-782	209	45	(	(	PUNCT
eurjchem-782	209	46	c‐8a	c‐8a	NOUN
eurjchem-782	209	47	)	)	PUNCT
eurjchem-782	209	48	,	,	PUNCT
eurjchem-782	209	49	129.2	129.2	NUM
eurjchem-782	209	50	(	(	PUNCT
eurjchem-782	209	51	c‐3	c‐3	NOUN
eurjchem-782	209	52	'	'	PUNCT
eurjchem-782	209	53	,	,	PUNCT
eurjchem-782	209	54	c‐5	c‐5	NOUN
eurjchem-782	209	55	'	'	PUNCT
eurjchem-782	209	56	)	)	PUNCT
eurjchem-782	209	57	,	,	PUNCT
eurjchem-782	209	58	128.7	128.7	NUM
eurjchem-782	209	59	(	(	PUNCT
eurjchem-782	209	60	c‐2	c‐2	NOUN
eurjchem-782	209	61	'	'	PUNCT
eurjchem-782	209	62	,	,	PUNCT
eurjchem-782	209	63	c‐6	c‐6	NOUN
eurjchem-782	209	64	'	'	PUNCT
eurjchem-782	209	65	)	)	PUNCT
eurjchem-782	209	66	,	,	PUNCT
eurjchem-782	209	67	126.7	126.7	NUM
eurjchem-782	209	68	(	(	PUNCT
eurjchem-782	209	69	c‐4	c‐4	PROPN
eurjchem-782	209	70	'	'	PUNCT
eurjchem-782	209	71	)	)	PUNCT
eurjchem-782	209	72	,	,	PUNCT
eurjchem-782	209	73	124.8	124.8	NUM
eurjchem-782	209	74	(	(	PUNCT
eurjchem-782	209	75	c‐7	c‐7	NOUN
eurjchem-782	209	76	)	)	PUNCT
eurjchem-782	209	77	,	,	PUNCT
eurjchem-782	209	78	123.9	123.9	NUM
eurjchem-782	209	79	(	(	PUNCT
eurjchem-782	209	80	c‐5	c‐5	NOUN
eurjchem-782	209	81	)	)	PUNCT
eurjchem-782	209	82	,	,	PUNCT
eurjchem-782	209	83	117.4	117.4	NUM
eurjchem-782	209	84	(	(	PUNCT
eurjchem-782	209	85	c‐2	c‐2	NOUN
eurjchem-782	209	86	)	)	PUNCT
eurjchem-782	209	87	,	,	PUNCT
eurjchem-782	209	88	42.3	42.3	NUM
eurjchem-782	209	89	(	(	PUNCT
eurjchem-782	209	90	c‐4	c‐4	PROPN
eurjchem-782	209	91	)	)	PUNCT
eurjchem-782	209	92	,	,	PUNCT
eurjchem-782	209	93	29.4	29.4	NUM
eurjchem-782	209	94	(	(	PUNCT
eurjchem-782	209	95	c‐3	c‐3	NOUN
eurjchem-782	209	96	)	)	PUNCT
eurjchem-782	209	97	,	,	PUNCT
eurjchem-782	209	98	14.8	14.8	NUM
eurjchem-782	209	99	(	(	PUNCT
eurjchem-782	209	100	‐	‐	PROPN
eurjchem-782	209	101	sch3	sch3	NOUN
eurjchem-782	209	102	)	)	PUNCT
eurjchem-782	209	103	.	.	PUNCT
eurjchem-782	210	1	ms	ms	PROPN
eurjchem-782	210	2	(	(	PUNCT
eurjchem-782	210	3	esi	esi	PROPN
eurjchem-782	210	4	,	,	PUNCT
eurjchem-782	210	5	m	m	PROPN
eurjchem-782	210	6	/	/	SYM
eurjchem-782	210	7	z	z	NOUN
eurjchem-782	210	8	):	):	PUNCT
eurjchem-782	210	9	296.07	296.07	NUM
eurjchem-782	210	10	(	(	PUNCT
eurjchem-782	210	11	m+	m+	NUM
eurjchem-782	210	12	)	)	PUNCT
eurjchem-782	210	13	.	.	PUNCT
eurjchem-782	211	1	anal	anal	PROPN
eurjchem-782	211	2	.	.	PUNCT
eurjchem-782	211	3	calcd	calcd	NOUN
eurjchem-782	211	4	.	.	PUNCT
eurjchem-782	212	1	for	for	ADP
eurjchem-782	212	2	c18h16o2s	c18h16o2s	NOUN
eurjchem-782	212	3	:	:	PUNCT
eurjchem-782	212	4	c	c	X
eurjchem-782	212	5	,	,	PUNCT
eurjchem-782	212	6	72.94	72.94	NUM
eurjchem-782	212	7	;	;	PUNCT
eurjchem-782	212	8	h	h	NOUN
eurjchem-782	212	9	,	,	PUNCT
eurjchem-782	212	10	5.44	5.44	NUM
eurjchem-782	212	11	.	.	PUNCT
eurjchem-782	212	12	found	find	VERB
eurjchem-782	212	13	:	:	PUNCT
eurjchem-782	213	1	c	c	X
eurjchem-782	213	2	,	,	PUNCT
eurjchem-782	213	3	72.91	72.91	NUM
eurjchem-782	213	4	;	;	PUNCT
eurjchem-782	213	5	h	h	NOUN
eurjchem-782	213	6	,	,	PUNCT
eurjchem-782	213	7	5.42	5.42	NUM
eurjchem-782	213	8	%	%	NOUN
eurjchem-782	213	9	.	.	PUNCT
eurjchem-782	214	1	2.2.5	2.2.5	X
eurjchem-782	214	2	.	.	PUNCT
eurjchem-782	214	3	general	general	ADJ
eurjchem-782	214	4	procedure	procedure	NOUN
eurjchem-782	214	5	for	for	ADP
eurjchem-782	214	6	the	the	DET
eurjchem-782	214	7	synthesis	synthesis	NOUN
eurjchem-782	214	8	of	of	ADP
eurjchem-782	214	9	novel	novel	ADJ
eurjchem-782	214	10	diaza	diaza	NOUN
eurjchem-782	214	11	analogues	analogue	NOUN
eurjchem-782	214	12	of	of	ADP
eurjchem-782	214	13	podophyllotoxin	podophyllotoxin	PROPN
eurjchem-782	214	14	(	(	PUNCT
eurjchem-782	214	15	7a‐d	7a‐d	NOUN
eurjchem-782	214	16	)	)	PUNCT
eurjchem-782	214	17	a	a	DET
eurjchem-782	214	18	mixture	mixture	NOUN
eurjchem-782	214	19	of	of	ADP
eurjchem-782	214	20	hydroxymethylene	hydroxymethylene	ADJ
eurjchem-782	214	21	tetralones	tetralone	NOUN
eurjchem-782	214	22	(	(	PUNCT
eurjchem-782	214	23	0.0145	0.0145	NUM
eurjchem-782	214	24	mol	mol	NOUN
eurjchem-782	214	25	)	)	PUNCT
eurjchem-782	214	26	and	and	CCONJ
eurjchem-782	214	27	hydrazine	hydrazine	NOUN
eurjchem-782	214	28	hydrate	hydrate	NOUN
eurjchem-782	214	29	(	(	PUNCT
eurjchem-782	214	30	0.5	0.5	NUM
eurjchem-782	214	31	g	g	NOUN
eurjchem-782	214	32	,	,	PUNCT
eurjchem-782	214	33	0.0145	0.0145	NUM
eurjchem-782	214	34	mol	mol	NOUN
eurjchem-782	214	35	)	)	PUNCT
eurjchem-782	214	36	in	in	ADP
eurjchem-782	214	37	absolute	absolute	ADJ
eurjchem-782	214	38	ethanol	ethanol	NOUN
eurjchem-782	214	39	was	be	AUX
eurjchem-782	214	40	refluxed	refluxe	VERB
eurjchem-782	214	41	for	for	ADP
eurjchem-782	214	42	3h	3h	NUM
eurjchem-782	214	43	.	.	PUNCT
eurjchem-782	215	1	the	the	DET
eurjchem-782	215	2	excess	excess	NOUN
eurjchem-782	215	3	of	of	ADP
eurjchem-782	215	4	solvent	solvent	NOUN
eurjchem-782	215	5	was	be	AUX
eurjchem-782	215	6	removed	remove	VERB
eurjchem-782	215	7	under	under	ADP
eurjchem-782	215	8	reduced	reduced	ADJ
eurjchem-782	215	9	pressure	pressure	NOUN
eurjchem-782	215	10	.	.	PUNCT
eurjchem-782	216	1	the	the	DET
eurjchem-782	216	2	solid	solid	ADJ
eurjchem-782	216	3	thus	thus	ADV
eurjchem-782	216	4	obtained	obtain	VERB
eurjchem-782	216	5	were	be	AUX
eurjchem-782	216	6	collected	collect	VERB
eurjchem-782	216	7	and	and	CCONJ
eurjchem-782	216	8	recrystallized	recrystallize	VERB
eurjchem-782	216	9	from	from	ADP
eurjchem-782	216	10	ethanol	ethanol	NOUN
eurjchem-782	216	11	(	(	PUNCT
eurjchem-782	216	12	scheme	scheme	NOUN
eurjchem-782	216	13	1	1	NUM
eurjchem-782	216	14	)	)	PUNCT
eurjchem-782	216	15	.	.	PUNCT
eurjchem-782	217	1	5‐phenyl‐4,5‐dihydro‐2h‐benzo[g]indazole	5‐phenyl‐4,5‐dihydro‐2h‐benzo[g]indazole	NUM
eurjchem-782	217	2	(	(	PUNCT
eurjchem-782	217	3	7a	7a	NUM
eurjchem-782	217	4	):	):	PUNCT
eurjchem-782	217	5	color	color	NOUN
eurjchem-782	217	6	:	:	PUNCT
eurjchem-782	217	7	dark	dark	PROPN
eurjchem-782	217	8	brown	brown	PROPN
eurjchem-782	217	9	solid	solid	ADJ
eurjchem-782	217	10	.	.	PUNCT
eurjchem-782	217	11	yield	yield	NOUN
eurjchem-782	217	12	:	:	PUNCT
eurjchem-782	217	13	77.36	77.36	NUM
eurjchem-782	217	14	%	%	NOUN
eurjchem-782	217	15	.	.	PUNCT
eurjchem-782	218	1	m.p	m.p	PROPN
eurjchem-782	218	2	.	.	PROPN
eurjchem-782	218	3	:	:	PUNCT
eurjchem-782	219	1	151‐153	151‐153	NUM
eurjchem-782	219	2	oc	oc	X
eurjchem-782	219	3	.	.	PROPN
eurjchem-782	219	4	ir	ir	PROPN
eurjchem-782	219	5	(	(	PUNCT
eurjchem-782	219	6	kbr	kbr	PROPN
eurjchem-782	219	7	,	,	PUNCT
eurjchem-782	219	8	ν	ν	PROPN
eurjchem-782	219	9	,	,	PUNCT
eurjchem-782	219	10	cm‐1	cm‐1	PROPN
eurjchem-782	219	11	):	):	PUNCT
eurjchem-782	219	12	3269	3269	NUM
eurjchem-782	219	13	(	(	PUNCT
eurjchem-782	219	14	n‐h	n‐h	NUM
eurjchem-782	219	15	)	)	PUNCT
eurjchem-782	219	16	,	,	PUNCT
eurjchem-782	219	17	3144	3144	NUM
eurjchem-782	219	18	,	,	PUNCT
eurjchem-782	219	19	2969	2969	NUM
eurjchem-782	219	20	(	(	PUNCT
eurjchem-782	219	21	ar‐ch	ar‐ch	NOUN
eurjchem-782	219	22	)	)	PUNCT
eurjchem-782	219	23	.	.	PUNCT
eurjchem-782	220	1	1h	1h	NUM
eurjchem-782	220	2	nmr	nmr	NOUN
eurjchem-782	220	3	(	(	PUNCT
eurjchem-782	220	4	400	400	NUM
eurjchem-782	220	5	mhz	mhz	NOUN
eurjchem-782	220	6	,	,	PUNCT
eurjchem-782	220	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-782	220	8	,	,	PUNCT
eurjchem-782	220	9	δ	δ	PROPN
eurjchem-782	220	10	,	,	PUNCT
eurjchem-782	220	11	ppm	ppm	NOUN
eurjchem-782	220	12	):	):	PUNCT
eurjchem-782	220	13	12.60	12.60	NUM
eurjchem-782	220	14	(	(	PUNCT
eurjchem-782	220	15	s	s	PROPN
eurjchem-782	220	16	,	,	PUNCT
eurjchem-782	220	17	1h	1h	NUM
eurjchem-782	220	18	,	,	PUNCT
eurjchem-782	220	19	nh	nh	PROPN
eurjchem-782	220	20	)	)	PUNCT
eurjchem-782	220	21	,	,	PUNCT
eurjchem-782	220	22	7.65‐7.23	7.65‐7.23	NUM
eurjchem-782	220	23	(	(	PUNCT
eurjchem-782	220	24	m	m	PROPN
eurjchem-782	220	25	,	,	PUNCT
eurjchem-782	220	26	9h	9h	NUM
eurjchem-782	220	27	,	,	PUNCT
eurjchem-782	220	28	ar‐h	ar‐h	NOUN
eurjchem-782	220	29	)	)	PUNCT
eurjchem-782	220	30	,	,	PUNCT
eurjchem-782	220	31	7.53	7.53	NUM
eurjchem-782	220	32	(	(	PUNCT
eurjchem-782	220	33	s	s	PROPN
eurjchem-782	220	34	,	,	PUNCT
eurjchem-782	220	35	1h	1h	NUM
eurjchem-782	220	36	,	,	PUNCT
eurjchem-782	220	37	pyrazole‐ch	pyrazole‐ch	NOUN
eurjchem-782	220	38	)	)	PUNCT
eurjchem-782	220	39	,	,	PUNCT
eurjchem-782	220	40	4.42	4.42	NUM
eurjchem-782	220	41	(	(	PUNCT
eurjchem-782	220	42	t	t	PROPN
eurjchem-782	220	43	,	,	PUNCT
eurjchem-782	220	44	1h	1h	NUM
eurjchem-782	220	45	,	,	PUNCT
eurjchem-782	220	46	ch	ch	NOUN
eurjchem-782	220	47	)	)	PUNCT
eurjchem-782	220	48	,	,	PUNCT
eurjchem-782	220	49	3.29	3.29	NUM
eurjchem-782	220	50	(	(	PUNCT
eurjchem-782	220	51	d	d	PROPN
eurjchem-782	220	52	,	,	PUNCT
eurjchem-782	220	53	d	d	PROPN
eurjchem-782	220	54	,	,	PUNCT
eurjchem-782	220	55	2h	2h	NUM
eurjchem-782	220	56	,	,	PUNCT
eurjchem-782	220	57	ch2	ch2	PROPN
eurjchem-782	220	58	)	)	PUNCT
eurjchem-782	220	59	.	.	PUNCT
eurjchem-782	221	1	13c	13c	NOUN
eurjchem-782	221	2	nmr	nmr	NOUN
eurjchem-782	221	3	(	(	PUNCT
eurjchem-782	221	4	100	100	NUM
eurjchem-782	221	5	mhz	mhz	NOUN
eurjchem-782	221	6	,	,	PUNCT
eurjchem-782	221	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-782	221	8	,	,	PUNCT
eurjchem-782	221	9	δ	δ	PROPN
eurjchem-782	221	10	,	,	PUNCT
eurjchem-782	221	11	ppm	ppm	NUM
eurjchem-782	221	12	):	):	PUNCT
eurjchem-782	221	13	144.5	144.5	NUM
eurjchem-782	221	14	(	(	PUNCT
eurjchem-782	221	15	c‐1	c‐1	NOUN
eurjchem-782	221	16	)	)	PUNCT
eurjchem-782	221	17	,	,	PUNCT
eurjchem-782	221	18	143.2	143.2	NUM
eurjchem-782	221	19	(	(	PUNCT
eurjchem-782	221	20	c‐1	c‐1	NOUN
eurjchem-782	221	21	'	'	PUNCT
eurjchem-782	221	22	)	)	PUNCT
eurjchem-782	221	23	,	,	PUNCT
eurjchem-782	221	24	140.9	140.9	NUM
eurjchem-782	221	25	(	(	PUNCT
eurjchem-782	221	26	c‐5a	c‐5a	PROPN
eurjchem-782	221	27	)	)	PUNCT
eurjchem-782	221	28	,	,	PUNCT
eurjchem-782	221	29	133.5	133.5	NUM
eurjchem-782	221	30	(	(	PUNCT
eurjchem-782	221	31	c‐9	c‐9	NOUN
eurjchem-782	221	32	)	)	PUNCT
eurjchem-782	221	33	,	,	PUNCT
eurjchem-782	221	34	129.3	129.3	NUM
eurjchem-782	221	35	(	(	PUNCT
eurjchem-782	221	36	c‐3	c‐3	NOUN
eurjchem-782	221	37	'	'	PUNCT
eurjchem-782	221	38	,	,	PUNCT
eurjchem-782	221	39	c‐5	c‐5	NOUN
eurjchem-782	221	40	'	'	PUNCT
eurjchem-782	221	41	)	)	PUNCT
eurjchem-782	221	42	,	,	PUNCT
eurjchem-782	221	43	128.9	128.9	NUM
eurjchem-782	221	44	(	(	PUNCT
eurjchem-782	221	45	c‐8a	c‐8a	NOUN
eurjchem-782	221	46	)	)	PUNCT
eurjchem-782	221	47	,	,	PUNCT
eurjchem-782	221	48	128.4	128.4	NUM
eurjchem-782	221	49	(	(	PUNCT
eurjchem-782	221	50	c‐2	c‐2	NOUN
eurjchem-782	221	51	'	'	PUNCT
eurjchem-782	221	52	,	,	PUNCT
eurjchem-782	221	53	c‐6	c‐6	NOUN
eurjchem-782	221	54	'	'	PUNCT
eurjchem-782	221	55	)	)	PUNCT
eurjchem-782	221	56	,	,	PUNCT
eurjchem-782	221	57	126.7	126.7	NUM
eurjchem-782	221	58	(	(	PUNCT
eurjchem-782	221	59	c‐4	c‐4	PROPN
eurjchem-782	221	60	'	'	PUNCT
eurjchem-782	221	61	)	)	PUNCT
eurjchem-782	221	62	,	,	PUNCT
eurjchem-782	221	63	126.5	126.5	NUM
eurjchem-782	221	64	(	(	PUNCT
eurjchem-782	221	65	c‐7	c‐7	NOUN
eurjchem-782	221	66	)	)	PUNCT
eurjchem-782	221	67	,	,	PUNCT
eurjchem-782	221	68	126.1	126.1	NUM
eurjchem-782	221	69	(	(	PUNCT
eurjchem-782	221	70	c‐6	c‐6	NOUN
eurjchem-782	221	71	)	)	PUNCT
eurjchem-782	221	72	,	,	PUNCT
eurjchem-782	221	73	123.1	123.1	NUM
eurjchem-782	221	74	(	(	PUNCT
eurjchem-782	221	75	c‐8	c‐8	NOUN
eurjchem-782	221	76	)	)	PUNCT
eurjchem-782	221	77	,	,	PUNCT
eurjchem-782	221	78	120.0	120.0	NUM
eurjchem-782	221	79	(	(	PUNCT
eurjchem-782	221	80	c‐5a	c‐5a	PROPN
eurjchem-782	221	81	)	)	PUNCT
eurjchem-782	221	82	,	,	PUNCT
eurjchem-782	221	83	114.9	114.9	NUM
eurjchem-782	221	84	(	(	PUNCT
eurjchem-782	221	85	c‐2	c‐2	NOUN
eurjchem-782	221	86	)	)	PUNCT
eurjchem-782	221	87	,	,	PUNCT
eurjchem-782	221	88	45.8	45.8	NUM
eurjchem-782	221	89	(	(	PUNCT
eurjchem-782	221	90	c‐4	c‐4	PROPN
eurjchem-782	221	91	)	)	PUNCT
eurjchem-782	221	92	,	,	PUNCT
eurjchem-782	221	93	37.3	37.3	NUM
eurjchem-782	221	94	(	(	PUNCT
eurjchem-782	221	95	c‐3	c‐3	NOUN
eurjchem-782	221	96	)	)	PUNCT
eurjchem-782	221	97	.	.	PUNCT
eurjchem-782	222	1	ms	ms	PROPN
eurjchem-782	222	2	(	(	PUNCT
eurjchem-782	222	3	esi	esi	PROPN
eurjchem-782	222	4	,	,	PUNCT
eurjchem-782	222	5	m	m	PROPN
eurjchem-782	222	6	/	/	SYM
eurjchem-782	222	7	z	z	NOUN
eurjchem-782	222	8	):	):	PUNCT
eurjchem-782	222	9	246.09	246.09	NUM
eurjchem-782	222	10	(	(	PUNCT
eurjchem-782	222	11	m+	m+	NUM
eurjchem-782	222	12	)	)	PUNCT
eurjchem-782	222	13	.	.	PUNCT
eurjchem-782	223	1	anal	anal	PROPN
eurjchem-782	223	2	.	.	PUNCT
eurjchem-782	223	3	calcd	calcd	NOUN
eurjchem-782	223	4	.	.	PUNCT
eurjchem-782	224	1	for	for	ADP
eurjchem-782	224	2	c17h14n2	c17h14n2	PROPN
eurjchem-782	224	3	:	:	PUNCT
eurjchem-782	224	4	c	c	X
eurjchem-782	224	5	,	,	PUNCT
eurjchem-782	224	6	82.90	82.90	NUM
eurjchem-782	224	7	;	;	PUNCT
eurjchem-782	224	8	h	h	NOUN
eurjchem-782	224	9	,	,	PUNCT
eurjchem-782	224	10	5.73	5.73	NUM
eurjchem-782	224	11	;	;	PUNCT
eurjchem-782	224	12	n	n	CCONJ
eurjchem-782	224	13	,	,	PUNCT
eurjchem-782	224	14	11.37	11.37	NUM
eurjchem-782	224	15	.	.	PUNCT
eurjchem-782	224	16	found	find	VERB
eurjchem-782	224	17	:	:	PUNCT
eurjchem-782	225	1	c	c	X
eurjchem-782	225	2	,	,	PUNCT
eurjchem-782	225	3	82.86	82.86	NUM
eurjchem-782	225	4	;	;	PUNCT
eurjchem-782	225	5	h	h	NOUN
eurjchem-782	225	6	,	,	PUNCT
eurjchem-782	225	7	5.70	5.70	NUM
eurjchem-782	225	8	;	;	PUNCT
eurjchem-782	225	9	n	n	CCONJ
eurjchem-782	225	10	,	,	PUNCT
eurjchem-782	225	11	11.35	11.35	NUM
eurjchem-782	225	12	%	%	NOUN
eurjchem-782	225	13	.	.	PUNCT
eurjchem-782	226	1	7‐methyl‐5‐phenyl‐4,5‐dihydro‐2h‐benzo[g]indazole	7‐methyl‐5‐phenyl‐4,5‐dihydro‐2h‐benzo[g]indazole	NUM
eurjchem-782	226	2	(	(	PUNCT
eurjchem-782	226	3	7b	7b	NUM
eurjchem-782	226	4	):	):	PUNCT
eurjchem-782	226	5	color	color	NOUN
eurjchem-782	226	6	:	:	PUNCT
eurjchem-782	226	7	dark	dark	PROPN
eurjchem-782	226	8	brown	brown	PROPN
eurjchem-782	226	9	solid	solid	ADJ
eurjchem-782	226	10	.	.	PUNCT
eurjchem-782	226	11	yield	yield	NOUN
eurjchem-782	226	12	:	:	PUNCT
eurjchem-782	226	13	82.65	82.65	NUM
eurjchem-782	226	14	%	%	NOUN
eurjchem-782	226	15	.	.	PUNCT
eurjchem-782	227	1	m.p	m.p	PROPN
eurjchem-782	227	2	.	.	PROPN
eurjchem-782	227	3	:	:	PUNCT
eurjchem-782	228	1	148‐150	148‐150	PROPN
eurjchem-782	228	2	oc	oc	PROPN
eurjchem-782	228	3	.	.	PROPN
eurjchem-782	229	1	ir	ir	PROPN
eurjchem-782	229	2	(	(	PUNCT
eurjchem-782	229	3	kbr	kbr	PROPN
eurjchem-782	229	4	,	,	PUNCT
eurjchem-782	229	5	ν	ν	PROPN
eurjchem-782	229	6	,	,	PUNCT
eurjchem-782	229	7	cm‐1	cm‐1	PROPN
eurjchem-782	229	8	):	):	PUNCT
eurjchem-782	229	9	3265	3265	NUM
eurjchem-782	229	10	(	(	PUNCT
eurjchem-782	229	11	n‐h	n‐h	NUM
eurjchem-782	229	12	)	)	PUNCT
eurjchem-782	229	13	,	,	PUNCT
eurjchem-782	229	14	3142	3142	NUM
eurjchem-782	229	15	,	,	PUNCT
eurjchem-782	229	16	2968	2968	NUM
eurjchem-782	229	17	(	(	PUNCT
eurjchem-782	229	18	ar‐ch	ar‐ch	NOUN
eurjchem-782	229	19	)	)	PUNCT
eurjchem-782	229	20	.	.	PUNCT
eurjchem-782	230	1	1h	1h	NUM
eurjchem-782	230	2	nmr	nmr	NOUN
eurjchem-782	230	3	(	(	PUNCT
eurjchem-782	230	4	400	400	NUM
eurjchem-782	230	5	mhz	mhz	NOUN
eurjchem-782	230	6	,	,	PUNCT
eurjchem-782	230	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-782	230	8	,	,	PUNCT
eurjchem-782	230	9	δ	δ	PROPN
eurjchem-782	230	10	,	,	PUNCT
eurjchem-782	230	11	ppm	ppm	NUM
eurjchem-782	230	12	):	):	PUNCT
eurjchem-782	230	13	12.64	12.64	NUM
eurjchem-782	230	14	(	(	PUNCT
eurjchem-782	230	15	s	s	PROPN
eurjchem-782	230	16	,	,	PUNCT
eurjchem-782	230	17	1h	1h	NUM
eurjchem-782	230	18	,	,	PUNCT
eurjchem-782	230	19	nh	nh	PROPN
eurjchem-782	230	20	)	)	PUNCT
eurjchem-782	230	21	,	,	PUNCT
eurjchem-782	230	22	7.64‐7.26	7.64‐7.26	NUM
eurjchem-782	230	23	(	(	PUNCT
eurjchem-782	230	24	m	m	PROPN
eurjchem-782	230	25	,	,	PUNCT
eurjchem-782	230	26	8h	8h	PROPN
eurjchem-782	230	27	,	,	PUNCT
eurjchem-782	230	28	ar‐	ar‐	PROPN
eurjchem-782	230	29	h	h	NOUN
eurjchem-782	230	30	)	)	PUNCT
eurjchem-782	230	31	,	,	PUNCT
eurjchem-782	230	32	7.52	7.52	NUM
eurjchem-782	230	33	(	(	PUNCT
eurjchem-782	230	34	s	s	PROPN
eurjchem-782	230	35	,	,	PUNCT
eurjchem-782	230	36	1h	1h	NUM
eurjchem-782	230	37	,	,	PUNCT
eurjchem-782	230	38	pyrazole‐ch	pyrazole‐ch	NOUN
eurjchem-782	230	39	)	)	PUNCT
eurjchem-782	230	40	,	,	PUNCT
eurjchem-782	230	41	4.44	4.44	NUM
eurjchem-782	230	42	(	(	PUNCT
eurjchem-782	230	43	t	t	PROPN
eurjchem-782	230	44	,	,	PUNCT
eurjchem-782	230	45	1h	1h	NUM
eurjchem-782	230	46	,	,	PUNCT
eurjchem-782	230	47	ch	ch	NOUN
eurjchem-782	230	48	)	)	PUNCT
eurjchem-782	230	49	,	,	PUNCT
eurjchem-782	230	50	3.25	3.25	NUM
eurjchem-782	230	51	(	(	PUNCT
eurjchem-782	230	52	d	d	NOUN
eurjchem-782	230	53	,	,	PUNCT
eurjchem-782	230	54	d	d	PROPN
eurjchem-782	230	55	,	,	PUNCT
eurjchem-782	230	56	2h	2h	NUM
eurjchem-782	230	57	,	,	PUNCT
eurjchem-782	230	58	ch2	ch2	PROPN
eurjchem-782	230	59	)	)	PUNCT
eurjchem-782	230	60	,	,	PUNCT
eurjchem-782	230	61	2.82	2.82	NUM
eurjchem-782	230	62	(	(	PUNCT
eurjchem-782	230	63	s	s	PROPN
eurjchem-782	230	64	,	,	PUNCT
eurjchem-782	230	65	3h	3h	NUM
eurjchem-782	230	66	,	,	PUNCT
eurjchem-782	230	67	ch3	ch3	PROPN
eurjchem-782	230	68	)	)	PUNCT
eurjchem-782	230	69	.	.	PUNCT
eurjchem-782	231	1	13c	13c	NOUN
eurjchem-782	231	2	nmr	nmr	NOUN
eurjchem-782	231	3	(	(	PUNCT
eurjchem-782	231	4	100	100	NUM
eurjchem-782	231	5	mhz	mhz	NOUN
eurjchem-782	231	6	,	,	PUNCT
eurjchem-782	231	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-782	231	8	,	,	PUNCT
eurjchem-782	231	9	δ	δ	PROPN
eurjchem-782	231	10	,	,	PUNCT
eurjchem-782	231	11	ppm	ppm	NUM
eurjchem-782	231	12	):	):	PUNCT
eurjchem-782	231	13	144.2	144.2	NUM
eurjchem-782	231	14	(	(	PUNCT
eurjchem-782	231	15	c‐1	c‐1	NOUN
eurjchem-782	231	16	)	)	PUNCT
eurjchem-782	231	17	,	,	PUNCT
eurjchem-782	231	18	143.2	143.2	NUM
eurjchem-782	231	19	(	(	PUNCT
eurjchem-782	231	20	c‐1	c‐1	NOUN
eurjchem-782	231	21	'	'	PUNCT
eurjchem-782	231	22	)	)	PUNCT
eurjchem-782	231	23	,	,	PUNCT
eurjchem-782	231	24	140.6	140.6	NUM
eurjchem-782	231	25	(	(	PUNCT
eurjchem-782	231	26	c‐5a	c‐5a	PROPN
eurjchem-782	231	27	)	)	PUNCT
eurjchem-782	231	28	,	,	PUNCT
eurjchem-782	231	29	138.7	138.7	NUM
eurjchem-782	231	30	(	(	PUNCT
eurjchem-782	231	31	c‐6	c‐6	NOUN
eurjchem-782	231	32	)	)	PUNCT
eurjchem-782	231	33	,	,	PUNCT
eurjchem-782	231	34	133.5	133.5	NUM
eurjchem-782	231	35	(	(	PUNCT
eurjchem-782	231	36	c‐9	c‐9	NOUN
eurjchem-782	231	37	)	)	PUNCT
eurjchem-782	231	38	,	,	PUNCT
eurjchem-782	231	39	130.9	130.9	NUM
eurjchem-782	231	40	(	(	PUNCT
eurjchem-782	231	41	c‐5	c‐5	NOUN
eurjchem-782	231	42	)	)	PUNCT
eurjchem-782	231	43	,	,	PUNCT
eurjchem-782	231	44	129.2	129.2	NUM
eurjchem-782	231	45	(	(	PUNCT
eurjchem-782	231	46	c‐3	c‐3	NOUN
eurjchem-782	231	47	'	'	PUNCT
eurjchem-782	231	48	,	,	PUNCT
eurjchem-782	231	49	c‐5	c‐5	NOUN
eurjchem-782	231	50	'	'	PUNCT
eurjchem-782	231	51	)	)	PUNCT
eurjchem-782	231	52	,	,	PUNCT
eurjchem-782	231	53	128.6	128.6	NUM
eurjchem-782	231	54	(	(	PUNCT
eurjchem-782	231	55	c‐2	c‐2	NOUN
eurjchem-782	231	56	'	'	PUNCT
eurjchem-782	231	57	,	,	PUNCT
eurjchem-782	231	58	c‐6	c‐6	NOUN
eurjchem-782	231	59	'	'	PUNCT
eurjchem-782	231	60	)	)	PUNCT
eurjchem-782	231	61	,	,	PUNCT
eurjchem-782	231	62	127.8	127.8	NUM
eurjchem-782	231	63	(	(	PUNCT
eurjchem-782	231	64	c‐8	c‐8	NOUN
eurjchem-782	231	65	)	)	PUNCT
eurjchem-782	231	66	,	,	PUNCT
eurjchem-782	231	67	127.1	127.1	NUM
eurjchem-782	231	68	(	(	PUNCT
eurjchem-782	231	69	c‐7	c‐7	NOUN
eurjchem-782	231	70	)	)	PUNCT
eurjchem-782	231	71	,	,	PUNCT
eurjchem-782	231	72	126.2	126.2	NUM
eurjchem-782	231	73	(	(	PUNCT
eurjchem-782	231	74	c‐4	c‐4	PROPN
eurjchem-782	231	75	'	'	PUNCT
eurjchem-782	231	76	)	)	PUNCT
eurjchem-782	231	77	,	,	PUNCT
eurjchem-782	231	78	125.6	125.6	NUM
eurjchem-782	231	79	(	(	PUNCT
eurjchem-782	231	80	c‐8a	c‐8a	NOUN
eurjchem-782	231	81	)	)	PUNCT
eurjchem-782	231	82	,	,	PUNCT
eurjchem-782	231	83	114.6	114.6	NUM
eurjchem-782	231	84	(	(	PUNCT
eurjchem-782	231	85	c‐2	c‐2	NOUN
eurjchem-782	231	86	)	)	PUNCT
eurjchem-782	231	87	,	,	PUNCT
eurjchem-782	231	88	46.8	46.8	NUM
eurjchem-782	231	89	(	(	PUNCT
eurjchem-782	231	90	c‐4	c‐4	PROPN
eurjchem-782	231	91	)	)	PUNCT
eurjchem-782	231	92	,	,	PUNCT
eurjchem-782	231	93	37.5	37.5	NUM
eurjchem-782	231	94	(	(	PUNCT
eurjchem-782	231	95	c‐3	c‐3	NOUN
eurjchem-782	231	96	)	)	PUNCT
eurjchem-782	231	97	,	,	PUNCT
eurjchem-782	231	98	21.64	21.64	NUM
eurjchem-782	231	99	(	(	PUNCT
eurjchem-782	231	100	‐ch3	‐ch3	ADJ
eurjchem-782	231	101	)	)	PUNCT
eurjchem-782	231	102	.	.	PUNCT
eurjchem-782	232	1	ms	ms	PROPN
eurjchem-782	232	2	(	(	PUNCT
eurjchem-782	232	3	esi	esi	PROPN
eurjchem-782	232	4	,	,	PUNCT
eurjchem-782	232	5	m	m	PROPN
eurjchem-782	232	6	/	/	SYM
eurjchem-782	232	7	z	z	NOUN
eurjchem-782	232	8	):	):	PUNCT
eurjchem-782	232	9	260.14	260.14	NUM
eurjchem-782	232	10	(	(	PUNCT
eurjchem-782	232	11	m+	m+	NUM
eurjchem-782	232	12	)	)	PUNCT
eurjchem-782	232	13	.	.	PUNCT
eurjchem-782	233	1	anal	anal	PROPN
eurjchem-782	233	2	.	.	PUNCT
eurjchem-782	233	3	calcd	calcd	NOUN
eurjchem-782	233	4	.	.	PUNCT
eurjchem-782	234	1	for	for	SCONJ
eurjchem-782	234	2	c18h16n2	c18h16n2	NOUN
eurjchem-782	234	3	:	:	PUNCT
eurjchem-782	234	4	c	c	X
eurjchem-782	234	5	,	,	PUNCT
eurjchem-782	234	6	83.04	83.04	NUM
eurjchem-782	234	7	;	;	PUNCT
eurjchem-782	234	8	h	h	NOUN
eurjchem-782	234	9	,	,	PUNCT
eurjchem-782	234	10	6.19	6.19	NUM
eurjchem-782	234	11	;	;	PUNCT
eurjchem-782	234	12	n	n	CCONJ
eurjchem-782	234	13	,	,	PUNCT
eurjchem-782	234	14	10.76	10.76	NUM
eurjchem-782	234	15	.	.	PUNCT
eurjchem-782	234	16	found	find	VERB
eurjchem-782	234	17	:	:	PUNCT
eurjchem-782	234	18	c	c	X
eurjchem-782	234	19	,	,	PUNCT
eurjchem-782	234	20	83.00	83.00	NUM
eurjchem-782	234	21	;	;	PUNCT
eurjchem-782	234	22	h	h	NOUN
eurjchem-782	234	23	,	,	PUNCT
eurjchem-782	234	24	6.20	6.20	NUM
eurjchem-782	234	25	;	;	PUNCT
eurjchem-782	234	26	n	n	CCONJ
eurjchem-782	234	27	,	,	PUNCT
eurjchem-782	234	28	10.79	10.79	NUM
eurjchem-782	234	29	%	%	NOUN
eurjchem-782	234	30	.	.	PUNCT
eurjchem-782	235	1	7‐methoxy‐5‐phenyl‐4,5‐dihydro‐2h‐benzo[g]indazole	7‐methoxy‐5‐phenyl‐4,5‐dihydro‐2h‐benzo[g]indazole	NUM
eurjchem-782	235	2	(	(	PUNCT
eurjchem-782	235	3	7c	7c	NOUN
eurjchem-782	235	4	):	):	PUNCT
eurjchem-782	235	5	color	color	NOUN
eurjchem-782	235	6	:	:	PUNCT
eurjchem-782	235	7	dark	dark	ADJ
eurjchem-782	235	8	brown	brown	PROPN
eurjchem-782	235	9	solid	solid	ADJ
eurjchem-782	235	10	.	.	PUNCT
eurjchem-782	235	11	yield	yield	NOUN
eurjchem-782	235	12	:	:	PUNCT
eurjchem-782	235	13	68.83	68.83	NUM
eurjchem-782	235	14	%	%	NOUN
eurjchem-782	235	15	.	.	PUNCT
eurjchem-782	236	1	m.p	m.p	PROPN
eurjchem-782	236	2	.	.	PROPN
eurjchem-782	236	3	:	:	PUNCT
eurjchem-782	237	1	135‐137	135‐137	NUM
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eurjchem-782	237	3	.	.	PROPN
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eurjchem-782	237	5	(	(	PUNCT
eurjchem-782	237	6	kbr	kbr	PROPN
eurjchem-782	237	7	,	,	PUNCT
eurjchem-782	237	8	ν	ν	PROPN
eurjchem-782	237	9	,	,	PUNCT
eurjchem-782	237	10	cm‐1	cm‐1	PROPN
eurjchem-782	237	11	):	):	PUNCT
eurjchem-782	237	12	3269	3269	NUM
eurjchem-782	237	13	(	(	PUNCT
eurjchem-782	237	14	n‐h	n‐h	NUM
eurjchem-782	237	15	)	)	PUNCT
eurjchem-782	237	16	,	,	PUNCT
eurjchem-782	237	17	3147	3147	NUM
eurjchem-782	237	18	,	,	PUNCT
eurjchem-782	237	19	2969	2969	NUM
eurjchem-782	237	20	(	(	PUNCT
eurjchem-782	237	21	ar‐ch	ar‐ch	NOUN
eurjchem-782	237	22	)	)	PUNCT
eurjchem-782	237	23	.	.	PUNCT
eurjchem-782	238	1	1h	1h	NUM
eurjchem-782	238	2	nmr	nmr	NOUN
eurjchem-782	238	3	(	(	PUNCT
eurjchem-782	238	4	400	400	NUM
eurjchem-782	238	5	mhz	mhz	NOUN
eurjchem-782	238	6	,	,	PUNCT
eurjchem-782	238	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-782	238	8	,	,	PUNCT
eurjchem-782	238	9	δ	δ	PROPN
eurjchem-782	238	10	,	,	PUNCT
eurjchem-782	238	11	ppm	ppm	NUM
eurjchem-782	238	12	):	):	PUNCT
eurjchem-782	238	13	12.59	12.59	NUM
eurjchem-782	238	14	(	(	PUNCT
eurjchem-782	238	15	s	s	PROPN
eurjchem-782	238	16	,	,	PUNCT
eurjchem-782	238	17	1h	1h	NUM
eurjchem-782	238	18	,	,	PUNCT
eurjchem-782	238	19	nh	nh	PROPN
eurjchem-782	238	20	)	)	PUNCT
eurjchem-782	238	21	,	,	PUNCT
eurjchem-782	238	22	7.68‐7.25	7.68‐7.25	NUM
eurjchem-782	238	23	(	(	PUNCT
eurjchem-782	238	24	m	m	PROPN
eurjchem-782	238	25	,	,	PUNCT
eurjchem-782	238	26	8h	8h	PROPN
eurjchem-782	238	27	,	,	PUNCT
eurjchem-782	238	28	ar‐	ar‐	PROPN
eurjchem-782	238	29	h	h	NOUN
eurjchem-782	238	30	)	)	PUNCT
eurjchem-782	238	31	,	,	PUNCT
eurjchem-782	238	32	7.55	7.55	NUM
eurjchem-782	238	33	(	(	PUNCT
eurjchem-782	238	34	s	s	PROPN
eurjchem-782	238	35	,	,	PUNCT
eurjchem-782	238	36	1h	1h	NUM
eurjchem-782	238	37	,	,	PUNCT
eurjchem-782	238	38	pyrazole‐ch	pyrazole‐ch	NOUN
eurjchem-782	238	39	)	)	PUNCT
eurjchem-782	238	40	,	,	PUNCT
eurjchem-782	238	41	4.39	4.39	NUM
eurjchem-782	238	42	(	(	PUNCT
eurjchem-782	238	43	t	t	PROPN
eurjchem-782	238	44	,	,	PUNCT
eurjchem-782	238	45	1h	1h	NUM
eurjchem-782	238	46	,	,	PUNCT
eurjchem-782	238	47	ch	ch	NOUN
eurjchem-782	238	48	)	)	PUNCT
eurjchem-782	238	49	,	,	PUNCT
eurjchem-782	238	50	3.26	3.26	NUM
eurjchem-782	238	51	(	(	PUNCT
eurjchem-782	238	52	d	d	NOUN
eurjchem-782	238	53	,	,	PUNCT
eurjchem-782	238	54	d	d	NOUN
eurjchem-782	238	55	,	,	PUNCT
eurjchem-782	238	56	2h	2h	NUM
eurjchem-782	238	57	,	,	PUNCT
eurjchem-782	238	58	ch2	ch2	PROPN
eurjchem-782	238	59	)	)	PUNCT
eurjchem-782	238	60	,	,	PUNCT
eurjchem-782	238	61	3.81	3.81	NUM
eurjchem-782	238	62	(	(	PUNCT
eurjchem-782	238	63	s	s	PROPN
eurjchem-782	238	64	,	,	PUNCT
eurjchem-782	238	65	3h	3h	NUM
eurjchem-782	238	66	,	,	PUNCT
eurjchem-782	238	67	och3	och3	ADJ
eurjchem-782	238	68	)	)	PUNCT
eurjchem-782	238	69	.	.	PUNCT
eurjchem-782	239	1	13c	13c	NOUN
eurjchem-782	239	2	nmr	nmr	NOUN
eurjchem-782	239	3	(	(	PUNCT
eurjchem-782	239	4	100	100	NUM
eurjchem-782	239	5	mhz	mhz	NOUN
eurjchem-782	239	6	,	,	PUNCT
eurjchem-782	239	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-782	239	8	,	,	PUNCT
eurjchem-782	239	9	δ	δ	PROPN
eurjchem-782	239	10	,	,	PUNCT
eurjchem-782	239	11	ppm	ppm	NUM
eurjchem-782	239	12	):	):	PUNCT
eurjchem-782	239	13	161.3	161.3	NUM
eurjchem-782	239	14	(	(	PUNCT
eurjchem-782	239	15	c‐6	c‐6	NOUN
eurjchem-782	239	16	)	)	PUNCT
eurjchem-782	239	17	,	,	PUNCT
eurjchem-782	239	18	144.6	144.6	NUM
eurjchem-782	239	19	(	(	PUNCT
eurjchem-782	239	20	c‐1	c‐1	NOUN
eurjchem-782	239	21	)	)	PUNCT
eurjchem-782	239	22	,	,	PUNCT
eurjchem-782	239	23	143.7	143.7	NUM
eurjchem-782	239	24	(	(	PUNCT
eurjchem-782	239	25	c‐1	c‐1	NOUN
eurjchem-782	239	26	'	'	PUNCT
eurjchem-782	239	27	)	)	PUNCT
eurjchem-782	239	28	,	,	PUNCT
eurjchem-782	239	29	141.9	141.9	NUM
eurjchem-782	239	30	(	(	PUNCT
eurjchem-782	239	31	c‐5a	c‐5a	PROPN
eurjchem-782	239	32	)	)	PUNCT
eurjchem-782	239	33	,	,	PUNCT
eurjchem-782	239	34	133.5	133.5	NUM
eurjchem-782	239	35	(	(	PUNCT
eurjchem-782	239	36	c‐9	c‐9	NOUN
eurjchem-782	239	37	)	)	PUNCT
eurjchem-782	239	38	,	,	PUNCT
eurjchem-782	239	39	129.3	129.3	NUM
eurjchem-782	239	40	(	(	PUNCT
eurjchem-782	239	41	c‐3	c‐3	NOUN
eurjchem-782	239	42	'	'	PUNCT
eurjchem-782	239	43	,	,	PUNCT
eurjchem-782	239	44	c‐5	c‐5	NOUN
eurjchem-782	239	45	'	'	PUNCT
eurjchem-782	239	46	)	)	PUNCT
eurjchem-782	239	47	,	,	PUNCT
eurjchem-782	239	48	129.0	129.0	NUM
eurjchem-782	239	49	(	(	PUNCT
eurjchem-782	239	50	c‐8	c‐8	NOUN
eurjchem-782	239	51	)	)	PUNCT
eurjchem-782	239	52	,	,	PUNCT
eurjchem-782	239	53	128.4	128.4	NUM
eurjchem-782	239	54	(	(	PUNCT
eurjchem-782	239	55	c‐2	c‐2	NOUN
eurjchem-782	239	56	'	'	PUNCT
eurjchem-782	239	57	,	,	PUNCT
eurjchem-782	239	58	c‐6	c‐6	NOUN
eurjchem-782	239	59	'	'	PUNCT
eurjchem-782	239	60	)	)	PUNCT
eurjchem-782	239	61	,	,	PUNCT
eurjchem-782	239	62	126.5	126.5	NUM
eurjchem-782	239	63	(	(	PUNCT
eurjchem-782	239	64	c‐4	c‐4	PROPN
eurjchem-782	239	65	'	'	PUNCT
eurjchem-782	239	66	)	)	PUNCT
eurjchem-782	239	67	,	,	PUNCT
eurjchem-782	239	68	121.3	121.3	NUM
eurjchem-782	239	69	(	(	PUNCT
eurjchem-782	239	70	c‐8a	c‐8a	PROPN
eurjchem-782	239	71	)	)	PUNCT
eurjchem-782	239	72	,	,	PUNCT
eurjchem-782	239	73	114.6	114.6	NUM
eurjchem-782	239	74	(	(	PUNCT
eurjchem-782	239	75	c‐2	c‐2	NOUN
eurjchem-782	239	76	)	)	PUNCT
eurjchem-782	239	77	,	,	PUNCT
eurjchem-782	239	78	112.5	112.5	NUM
eurjchem-782	239	79	(	(	PUNCT
eurjchem-782	239	80	c‐5	c‐5	NOUN
eurjchem-782	239	81	)	)	PUNCT
eurjchem-782	239	82	,	,	PUNCT
eurjchem-782	239	83	112.4	112.4	NUM
eurjchem-782	239	84	(	(	PUNCT
eurjchem-782	239	85	c‐7	c‐7	NOUN
eurjchem-782	239	86	)	)	PUNCT
eurjchem-782	239	87	,	,	PUNCT
eurjchem-782	239	88	55.6	55.6	NUM
eurjchem-782	239	89	(	(	PUNCT
eurjchem-782	239	90	‐	‐	NOUN
eurjchem-782	239	91	och3	och3	ADJ
eurjchem-782	239	92	)	)	PUNCT
eurjchem-782	239	93	,	,	PUNCT
eurjchem-782	239	94	46.7	46.7	NUM
eurjchem-782	239	95	(	(	PUNCT
eurjchem-782	239	96	c‐4	c‐4	PROPN
eurjchem-782	239	97	)	)	PUNCT
eurjchem-782	239	98	,	,	PUNCT
eurjchem-782	239	99	37.1	37.1	NUM
eurjchem-782	239	100	(	(	PUNCT
eurjchem-782	239	101	c‐3	c‐3	NOUN
eurjchem-782	239	102	)	)	PUNCT
eurjchem-782	239	103	.	.	PUNCT
eurjchem-782	240	1	ms	ms	PROPN
eurjchem-782	240	2	(	(	PUNCT
eurjchem-782	240	3	esi	esi	PROPN
eurjchem-782	240	4	,	,	PUNCT
eurjchem-782	240	5	m	m	PROPN
eurjchem-782	240	6	/	/	SYM
eurjchem-782	240	7	z	z	NOUN
eurjchem-782	240	8	):	):	PUNCT
eurjchem-782	240	9	276.13	276.13	NUM
eurjchem-782	240	10	(	(	PUNCT
eurjchem-782	240	11	m+	m+	NUM
eurjchem-782	240	12	)	)	PUNCT
eurjchem-782	240	13	.	.	PUNCT
eurjchem-782	241	1	anal	anal	PROPN
eurjchem-782	241	2	.	.	PUNCT
eurjchem-782	241	3	calcd	calcd	NOUN
eurjchem-782	241	4	.	.	PUNCT
eurjchem-782	242	1	for	for	SCONJ
eurjchem-782	242	2	c18h16n2o	c18h16n2o	NOUN
eurjchem-782	242	3	:	:	PUNCT
eurjchem-782	242	4	c	c	X
eurjchem-782	242	5	,	,	PUNCT
eurjchem-782	242	6	78.24	78.24	NUM
eurjchem-782	242	7	;	;	PUNCT
eurjchem-782	242	8	h	h	NOUN
eurjchem-782	242	9	,	,	PUNCT
eurjchem-782	242	10	5.84	5.84	NUM
eurjchem-782	242	11	;	;	PUNCT
eurjchem-782	242	12	n	n	CCONJ
eurjchem-782	242	13	,	,	PUNCT
eurjchem-782	242	14	10.14	10.14	NUM
eurjchem-782	242	15	.	.	PUNCT
eurjchem-782	242	16	found	find	VERB
eurjchem-782	242	17	:	:	PUNCT
eurjchem-782	243	1	c	c	X
eurjchem-782	243	2	,	,	PUNCT
eurjchem-782	243	3	78.22	78.22	NUM
eurjchem-782	243	4	;	;	PUNCT
eurjchem-782	243	5	h	h	NOUN
eurjchem-782	243	6	,	,	PUNCT
eurjchem-782	243	7	5.85	5.85	NUM
eurjchem-782	243	8	;	;	PUNCT
eurjchem-782	243	9	n	n	CCONJ
eurjchem-782	243	10	,	,	PUNCT
eurjchem-782	243	11	10.11	10.11	NUM
eurjchem-782	243	12	%	%	NOUN
eurjchem-782	243	13	.	.	PUNCT
eurjchem-782	244	1	7‐(methylthio)‐5‐phenyl‐4,5‐dihydro‐2h‐benzo[g]indazole	7‐(methylthio)‐5‐phenyl‐4,5‐dihydro‐2h‐benzo[g]indazole	NOUN
eurjchem-782	244	2	(	(	PUNCT
eurjchem-782	244	3	7d	7d	NUM
eurjchem-782	244	4	):	):	PUNCT
eurjchem-782	244	5	color	color	NOUN
eurjchem-782	244	6	:	:	PUNCT
eurjchem-782	244	7	dark	dark	ADJ
eurjchem-782	244	8	brown	brown	PROPN
eurjchem-782	244	9	solid	solid	ADJ
eurjchem-782	244	10	.	.	PUNCT
eurjchem-782	244	11	yield	yield	NOUN
eurjchem-782	244	12	:	:	PUNCT
eurjchem-782	244	13	63.90	63.90	NUM
eurjchem-782	244	14	%	%	NOUN
eurjchem-782	244	15	.	.	PUNCT
eurjchem-782	245	1	m.p	m.p	PROPN
eurjchem-782	245	2	.	.	PROPN
eurjchem-782	245	3	:	:	PUNCT
eurjchem-782	246	1	145‐147	145‐147	PROPN
eurjchem-782	246	2	oc	oc	PROPN
eurjchem-782	246	3	.	.	PROPN
eurjchem-782	246	4	ir	ir	PROPN
eurjchem-782	246	5	(	(	PUNCT
eurjchem-782	246	6	kbr	kbr	PROPN
eurjchem-782	246	7	,	,	PUNCT
eurjchem-782	246	8	ν	ν	PROPN
eurjchem-782	246	9	,	,	PUNCT
eurjchem-782	246	10	cm‐1	cm‐1	PROPN
eurjchem-782	246	11	):	):	PUNCT
eurjchem-782	246	12	3265	3265	NUM
eurjchem-782	246	13	(	(	PUNCT
eurjchem-782	246	14	n‐h	n‐h	NUM
eurjchem-782	246	15	)	)	PUNCT
eurjchem-782	246	16	,	,	PUNCT
eurjchem-782	246	17	3143	3143	NUM
eurjchem-782	246	18	,	,	PUNCT
eurjchem-782	246	19	2968	2968	NUM
eurjchem-782	246	20	(	(	PUNCT
eurjchem-782	246	21	ar‐ch	ar‐ch	NOUN
eurjchem-782	246	22	)	)	PUNCT
eurjchem-782	246	23	.	.	PUNCT
eurjchem-782	247	1	1h	1h	NUM
eurjchem-782	247	2	nmr	nmr	NOUN
eurjchem-782	247	3	(	(	PUNCT
eurjchem-782	247	4	400	400	NUM
eurjchem-782	247	5	mhz	mhz	NOUN
eurjchem-782	247	6	,	,	PUNCT
eurjchem-782	247	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-782	247	8	,	,	PUNCT
eurjchem-782	247	9	δ	δ	PROPN
eurjchem-782	247	10	,	,	PUNCT
eurjchem-782	247	11	ppm	ppm	NUM
eurjchem-782	247	12	):	):	PUNCT
eurjchem-782	247	13	12.55	12.55	NUM
eurjchem-782	247	14	(	(	PUNCT
eurjchem-782	247	15	s	s	PROPN
eurjchem-782	247	16	,	,	PUNCT
eurjchem-782	247	17	1h	1h	NUM
eurjchem-782	247	18	,	,	PUNCT
eurjchem-782	247	19	nh	nh	PROPN
eurjchem-782	247	20	)	)	PUNCT
eurjchem-782	247	21	,	,	PUNCT
eurjchem-782	247	22	7.61‐7.29	7.61‐7.29	NUM
eurjchem-782	247	23	(	(	PUNCT
eurjchem-782	247	24	m	m	PROPN
eurjchem-782	247	25	,	,	PUNCT
eurjchem-782	247	26	8h	8h	PROPN
eurjchem-782	247	27	,	,	PUNCT
eurjchem-782	247	28	ar‐	ar‐	PROPN
eurjchem-782	247	29	h	h	NOUN
eurjchem-782	247	30	)	)	PUNCT
eurjchem-782	247	31	,	,	PUNCT
eurjchem-782	247	32	7.51	7.51	NUM
eurjchem-782	247	33	(	(	PUNCT
eurjchem-782	247	34	s	s	PROPN
eurjchem-782	247	35	,	,	PUNCT
eurjchem-782	247	36	1h	1h	NUM
eurjchem-782	247	37	,	,	PUNCT
eurjchem-782	247	38	pyrazole‐ch	pyrazole‐ch	NOUN
eurjchem-782	247	39	)	)	PUNCT
eurjchem-782	247	40	,	,	PUNCT
eurjchem-782	247	41	4.35	4.35	NUM
eurjchem-782	247	42	(	(	PUNCT
eurjchem-782	247	43	t	t	PROPN
eurjchem-782	247	44	,	,	PUNCT
eurjchem-782	247	45	1h	1h	NUM
eurjchem-782	247	46	,	,	PUNCT
eurjchem-782	247	47	ch	ch	NOUN
eurjchem-782	247	48	)	)	PUNCT
eurjchem-782	247	49	,	,	PUNCT
eurjchem-782	247	50	3.21	3.21	NUM
eurjchem-782	247	51	(	(	PUNCT
eurjchem-782	247	52	d	d	NOUN
eurjchem-782	247	53	,	,	PUNCT
eurjchem-782	247	54	d	d	PROPN
eurjchem-782	247	55	,	,	PUNCT
eurjchem-782	247	56	2h	2h	NUM
eurjchem-782	247	57	,	,	PUNCT
eurjchem-782	247	58	ch2	ch2	PROPN
eurjchem-782	247	59	)	)	PUNCT
eurjchem-782	247	60	,	,	PUNCT
eurjchem-782	247	61	2.49	2.49	NUM
eurjchem-782	247	62	(	(	PUNCT
eurjchem-782	247	63	s	s	PROPN
eurjchem-782	247	64	,	,	PUNCT
eurjchem-782	247	65	3h	3h	NUM
eurjchem-782	247	66	,	,	PUNCT
eurjchem-782	247	67	sch3	sch3	PROPN
eurjchem-782	247	68	)	)	PUNCT
eurjchem-782	247	69	.	.	PUNCT
eurjchem-782	248	1	13c	13c	NOUN
eurjchem-782	248	2	nmr	nmr	NOUN
eurjchem-782	248	3	(	(	PUNCT
eurjchem-782	248	4	100	100	NUM
eurjchem-782	248	5	mhz	mhz	NOUN
eurjchem-782	248	6	,	,	PUNCT
eurjchem-782	248	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-782	248	8	,	,	PUNCT
eurjchem-782	248	9	δ	δ	PROPN
eurjchem-782	248	10	,	,	PUNCT
eurjchem-782	248	11	ppm	ppm	NUM
eurjchem-782	248	12	):	):	PUNCT
eurjchem-782	248	13	144.3	144.3	NUM
eurjchem-782	248	14	(	(	PUNCT
eurjchem-782	248	15	c‐1	c‐1	NOUN
eurjchem-782	248	16	)	)	PUNCT
eurjchem-782	248	17	,	,	PUNCT
eurjchem-782	248	18	143.2	143.2	NUM
eurjchem-782	248	19	(	(	PUNCT
eurjchem-782	248	20	c‐1	c‐1	NOUN
eurjchem-782	248	21	'	'	PUNCT
eurjchem-782	248	22	)	)	PUNCT
eurjchem-782	248	23	,	,	PUNCT
eurjchem-782	248	24	140.9	140.9	NUM
eurjchem-782	248	25	(	(	PUNCT
eurjchem-782	248	26	c‐5a	c‐5a	PROPN
eurjchem-782	248	27	)	)	PUNCT
eurjchem-782	248	28	,	,	PUNCT
eurjchem-782	248	29	139.5	139.5	NUM
eurjchem-782	248	30	(	(	PUNCT
eurjchem-782	248	31	c‐6	c‐6	NOUN
eurjchem-782	248	32	)	)	PUNCT
eurjchem-782	248	33	,	,	PUNCT
eurjchem-782	248	34	133.6	133.6	NUM
eurjchem-782	248	35	(	(	PUNCT
eurjchem-782	248	36	c‐9	c‐9	PROPN
eurjchem-782	248	37	)	)	PUNCT
eurjchem-782	248	38	,	,	PUNCT
eurjchem-782	248	39	129.4	129.4	NUM
eurjchem-782	248	40	(	(	PUNCT
eurjchem-782	248	41	c‐3	c‐3	NOUN
eurjchem-782	248	42	'	'	PUNCT
eurjchem-782	248	43	,	,	PUNCT
eurjchem-782	248	44	c‐5	c‐5	NOUN
eurjchem-782	248	45	'	'	PUNCT
eurjchem-782	248	46	)	)	PUNCT
eurjchem-782	248	47	,	,	PUNCT
eurjchem-782	248	48	128.4	128.4	NUM
eurjchem-782	248	49	(	(	PUNCT
eurjchem-782	248	50	c‐8	c‐8	NOUN
eurjchem-782	248	51	)	)	PUNCT
eurjchem-782	248	52	,	,	PUNCT
eurjchem-782	248	53	128.3	128.3	NUM
eurjchem-782	248	54	(	(	PUNCT
eurjchem-782	248	55	c‐2	c‐2	NOUN
eurjchem-782	248	56	'	'	PUNCT
eurjchem-782	248	57	,	,	PUNCT
eurjchem-782	248	58	c‐6	c‐6	NOUN
eurjchem-782	248	59	'	'	PUNCT
eurjchem-782	248	60	)	)	PUNCT
eurjchem-782	248	61	,	,	PUNCT
eurjchem-782	248	62	126.5	126.5	NUM
eurjchem-782	248	63	(	(	PUNCT
eurjchem-782	248	64	c‐4	c‐4	PROPN
eurjchem-782	248	65	'	'	PUNCT
eurjchem-782	248	66	)	)	PUNCT
eurjchem-782	248	67	,	,	PUNCT
eurjchem-782	248	68	125.5	125.5	NUM
eurjchem-782	248	69	(	(	PUNCT
eurjchem-782	248	70	c‐8a	c‐8a	NOUN
eurjchem-782	248	71	)	)	PUNCT
eurjchem-782	248	72	,	,	PUNCT
eurjchem-782	248	73	124.4	124.4	NUM
eurjchem-782	248	74	(	(	PUNCT
eurjchem-782	248	75	c‐7	c‐7	NOUN
eurjchem-782	248	76	)	)	PUNCT
eurjchem-782	248	77	,	,	PUNCT
eurjchem-782	248	78	123.9	123.9	NUM
eurjchem-782	248	79	(	(	PUNCT
eurjchem-782	248	80	c‐5	c‐5	NOUN
eurjchem-782	248	81	)	)	PUNCT
eurjchem-782	248	82	,	,	PUNCT
eurjchem-782	248	83	114.7	114.7	NUM
eurjchem-782	248	84	(	(	PUNCT
eurjchem-782	248	85	c‐2	c‐2	NOUN
eurjchem-782	248	86	)	)	PUNCT
eurjchem-782	248	87	,	,	PUNCT
eurjchem-782	248	88	45.5	45.5	NUM
eurjchem-782	248	89	(	(	PUNCT
eurjchem-782	248	90	c‐4	c‐4	PROPN
eurjchem-782	248	91	)	)	PUNCT
eurjchem-782	248	92	,	,	PUNCT
eurjchem-782	248	93	37.6	37.6	NUM
eurjchem-782	248	94	(	(	PUNCT
eurjchem-782	248	95	c‐3	c‐3	NOUN
eurjchem-782	248	96	)	)	PUNCT
eurjchem-782	248	97	,	,	PUNCT
eurjchem-782	248	98	14.7	14.7	NUM
eurjchem-782	248	99	(	(	PUNCT
eurjchem-782	248	100	‐sch3	‐sch3	NOUN
eurjchem-782	248	101	)	)	PUNCT
eurjchem-782	248	102	.	.	PUNCT
eurjchem-782	249	1	ms	ms	PROPN
eurjchem-782	249	2	(	(	PUNCT
eurjchem-782	249	3	esi	esi	PROPN
eurjchem-782	249	4	,	,	PUNCT
eurjchem-782	249	5	m	m	PROPN
eurjchem-782	249	6	/	/	SYM
eurjchem-782	249	7	z	z	NOUN
eurjchem-782	249	8	):	):	PUNCT
eurjchem-782	249	9	292.11	292.11	NUM
eurjchem-782	249	10	(	(	PUNCT
eurjchem-782	249	11	m+	m+	NUM
eurjchem-782	249	12	)	)	PUNCT
eurjchem-782	249	13	.	.	PUNCT
eurjchem-782	250	1	anal	anal	PROPN
eurjchem-782	250	2	.	.	PUNCT
eurjchem-782	250	3	calcd	calcd	NOUN
eurjchem-782	250	4	.	.	PUNCT
eurjchem-782	251	1	for	for	ADP
eurjchem-782	251	2	c18h16n2s	c18h16n2s	NOUN
eurjchem-782	251	3	:	:	PUNCT
eurjchem-782	251	4	c	c	X
eurjchem-782	251	5	,	,	PUNCT
eurjchem-782	251	6	73.94	73.94	NUM
eurjchem-782	251	7	;	;	PUNCT
eurjchem-782	251	8	h	h	NOUN
eurjchem-782	251	9	,	,	PUNCT
eurjchem-782	251	10	5.52	5.52	NUM
eurjchem-782	251	11	;	;	PUNCT
eurjchem-782	251	12	n	n	CCONJ
eurjchem-782	251	13	,	,	PUNCT
eurjchem-782	251	14	9.58	9.58	NUM
eurjchem-782	251	15	.	.	PUNCT
eurjchem-782	251	16	found	find	VERB
eurjchem-782	251	17	:	:	PUNCT
eurjchem-782	252	1	c	c	X
eurjchem-782	252	2	,	,	PUNCT
eurjchem-782	252	3	73.93	73.93	NUM
eurjchem-782	252	4	;	;	PUNCT
eurjchem-782	252	5	h	h	NOUN
eurjchem-782	252	6	,	,	PUNCT
eurjchem-782	252	7	5.50	5.50	NUM
eurjchem-782	252	8	;	;	PUNCT
eurjchem-782	252	9	n	n	CCONJ
eurjchem-782	252	10	,	,	PUNCT
eurjchem-782	252	11	9.55	9.55	NUM
eurjchem-782	252	12	%	%	NOUN
eurjchem-782	252	13	.	.	PUNCT
eurjchem-782	253	1	3	3	X
eurjchem-782	253	2	.	.	NOUN
eurjchem-782	253	3	results	result	NOUN
eurjchem-782	253	4	and	and	CCONJ
eurjchem-782	253	5	discussion	discussion	VERB
eurjchem-782	253	6	the	the	DET
eurjchem-782	253	7	synthesis	synthesis	NOUN
eurjchem-782	253	8	of	of	ADP
eurjchem-782	253	9	novel	novel	ADJ
eurjchem-782	253	10	diaza	diaza	NOUN
eurjchem-782	253	11	analogues	analogue	NOUN
eurjchem-782	253	12	of	of	ADP
eurjchem-782	253	13	podophyllotoxin	podophyllotoxin	NOUN
eurjchem-782	253	14	has	have	AUX
eurjchem-782	253	15	been	be	AUX
eurjchem-782	253	16	carried	carry	VERB
eurjchem-782	253	17	out	out	ADP
eurjchem-782	253	18	by	by	ADP
eurjchem-782	253	19	chalcone	chalcone	NOUN
eurjchem-782	253	20	route	route	NOUN
eurjchem-782	253	21	(	(	PUNCT
eurjchem-782	253	22	scheme	scheme	NOUN
eurjchem-782	253	23	1	1	NUM
eurjchem-782	253	24	)	)	PUNCT
eurjchem-782	253	25	.	.	PUNCT
eurjchem-782	254	1	the	the	DET
eurjchem-782	254	2	benzylideneacetophenones	benzylideneacetophenone	NOUN
eurjchem-782	254	3	(	(	PUNCT
eurjchem-782	254	4	chalcones	chalcones	PROPN
eurjchem-782	254	5	)	)	PUNCT
eurjchem-782	254	6	(	(	PUNCT
eurjchem-782	254	7	3a‐d	3a‐d	ADV
eurjchem-782	254	8	)	)	PUNCT
eurjchem-782	254	9	were	be	AUX
eurjchem-782	254	10	prepared	prepare	VERB
eurjchem-782	254	11	in	in	ADP
eurjchem-782	254	12	high	high	ADJ
eurjchem-782	254	13	yields	yield	NOUN
eurjchem-782	254	14	by	by	ADP
eurjchem-782	254	15	claisen‐schmidt	claisen‐schmidt	ADJ
eurjchem-782	254	16	reaction	reaction	NOUN
eurjchem-782	254	17	of	of	ADP
eurjchem-782	254	18	acetophenones	acetophenone	NOUN
eurjchem-782	254	19	(	(	PUNCT
eurjchem-782	254	20	1a‐d	1a‐d	NOUN
eurjchem-782	254	21	)	)	PUNCT
eurjchem-782	254	22	with	with	ADP
eurjchem-782	254	23	benzaldehyde	benzaldehyde	NOUN
eurjchem-782	254	24	(	(	PUNCT
eurjchem-782	254	25	2	2	NUM
eurjchem-782	254	26	)	)	PUNCT
eurjchem-782	254	27	in	in	ADP
eurjchem-782	254	28	the	the	DET
eurjchem-782	254	29	presence	presence	NOUN
eurjchem-782	254	30	of	of	ADP
eurjchem-782	254	31	sodium	sodium	NOUN
eurjchem-782	254	32	hydroxide	hydroxide	NOUN
eurjchem-782	254	33	in	in	ADP
eurjchem-782	254	34	water‐ethanol	water‐ethanol	ADJ
eurjchem-782	254	35	mixture	mixture	NOUN
eurjchem-782	254	36	[	[	X
eurjchem-782	254	37	13,14	13,14	NUM
eurjchem-782	254	38	]	]	PUNCT
eurjchem-782	254	39	.	.	PUNCT
eurjchem-782	255	1	the	the	DET
eurjchem-782	255	2	structures	structure	NOUN
eurjchem-782	255	3	of	of	ADP
eurjchem-782	255	4	the	the	DET
eurjchem-782	255	5	chalcones	chalcone	NOUN
eurjchem-782	255	6	were	be	AUX
eurjchem-782	255	7	confirmed	confirm	VERB
eurjchem-782	255	8	by	by	ADP
eurjchem-782	255	9	ir	ir	PROPN
eurjchem-782	255	10	and	and	CCONJ
eurjchem-782	255	11	1h	1h	NUM
eurjchem-782	255	12	nmr	nmr	PROPN
eurjchem-782	255	13	spectral	spectral	ADJ
eurjchem-782	255	14	studies	study	NOUN
eurjchem-782	255	15	.	.	PUNCT
eurjchem-782	256	1	ir	ir	PROPN
eurjchem-782	256	2	spectra	spectra	PROPN
eurjchem-782	256	3	of	of	ADP
eurjchem-782	256	4	compounds	compound	NOUN
eurjchem-782	256	5	(	(	PUNCT
eurjchem-782	256	6	3a‐d	3a‐d	ADV
eurjchem-782	256	7	)	)	PUNCT
eurjchem-782	256	8	showed	show	VERB
eurjchem-782	256	9	the	the	DET
eurjchem-782	256	10	c	c	NOUN
eurjchem-782	256	11	=	=	NOUN
eurjchem-782	256	12	c	c	NOUN
eurjchem-782	256	13	stretching	stretch	VERB
eurjchem-782	256	14	frequency	frequency	NOUN
eurjchem-782	256	15	in	in	ADP
eurjchem-782	256	16	the	the	DET
eurjchem-782	256	17	range	range	NOUN
eurjchem-782	256	18	1626‐1613	1626‐1613	NUM
eurjchem-782	256	19	cm‐1	cm‐1	NOUN
eurjchem-782	256	20	and	and	CCONJ
eurjchem-782	256	21	1h	1h	NUM
eurjchem-782	256	22	nmr	nmr	NOUN
eurjchem-782	256	23	showed	show	VERB
eurjchem-782	256	24	the	the	DET
eurjchem-782	256	25	absence	absence	NOUN
eurjchem-782	256	26	of	of	ADP
eurjchem-782	256	27	aldehyde	aldehyde	NOUN
eurjchem-782	256	28	proton	proton	NOUN
eurjchem-782	256	29	at	at	ADP
eurjchem-782	256	30	9.83	9.83	NUM
eurjchem-782	256	31	ppm	ppm	NOUN
eurjchem-782	256	32	.	.	PUNCT
eurjchem-782	257	1	the	the	DET
eurjchem-782	257	2	cyclopropyl	cyclopropyl	PROPN
eurjchem-782	257	3	ketones	ketone	NOUN
eurjchem-782	257	4	(	(	PUNCT
eurjchem-782	257	5	4a‐d	4a‐d	NOUN
eurjchem-782	257	6	)	)	PUNCT
eurjchem-782	257	7	were	be	AUX
eurjchem-782	257	8	prepared	prepare	VERB
eurjchem-782	257	9	in	in	ADP
eurjchem-782	257	10	good	good	ADJ
eurjchem-782	257	11	yields	yield	NOUN
eurjchem-782	257	12	by	by	ADP
eurjchem-782	257	13	the	the	DET
eurjchem-782	257	14	reaction	reaction	NOUN
eurjchem-782	257	15	of	of	ADP
eurjchem-782	257	16	chalcones	chalcone	NOUN
eurjchem-782	257	17	(	(	PUNCT
eurjchem-782	257	18	3a‐d	3a‐d	ADV
eurjchem-782	257	19	)	)	PUNCT
eurjchem-782	257	20	with	with	ADP
eurjchem-782	257	21	trimethylsulfoxonium	trimethylsulfoxonium	NOUN
eurjchem-782	257	22	iodide	iodide	NOUN
eurjchem-782	257	23	in	in	ADP
eurjchem-782	257	24	the	the	DET
eurjchem-782	257	25	presence	presence	NOUN
eurjchem-782	257	26	of	of	ADP
eurjchem-782	257	27	sodium	sodium	NOUN
eurjchem-782	257	28	hydride	hydride	NOUN
eurjchem-782	257	29	in	in	ADP
eurjchem-782	257	30	dry	dry	ADJ
eurjchem-782	257	31	dmso	dmso	NOUN
eurjchem-782	257	32	[	[	X
eurjchem-782	257	33	15,16	15,16	NUM
eurjchem-782	257	34	]	]	PUNCT
eurjchem-782	257	35	.	.	PUNCT
eurjchem-782	258	1	the	the	DET
eurjchem-782	258	2	sodium	sodium	NOUN
eurjchem-782	258	3	hydride	hydride	NOUN
eurjchem-782	258	4	acts	act	VERB
eurjchem-782	258	5	as	as	ADP
eurjchem-782	258	6	a	a	DET
eurjchem-782	258	7	base	base	NOUN
eurjchem-782	258	8	which	which	PRON
eurjchem-782	258	9	abstracts	abstract	VERB
eurjchem-782	258	10	a	a	DET
eurjchem-782	258	11	proton	proton	NOUN
eurjchem-782	258	12	from	from	ADP
eurjchem-782	258	13	the	the	DET
eurjchem-782	258	14	methyl	methyl	NOUN
eurjchem-782	258	15	group	group	NOUN
eurjchem-782	258	16	in	in	ADP
eurjchem-782	258	17	trimethylsulfoxonium	trimethylsulfoxonium	NOUN
eurjchem-782	258	18	iodide	iodide	NOUN
eurjchem-782	258	19	to	to	PART
eurjchem-782	258	20	form	form	VERB
eurjchem-782	258	21	a	a	DET
eurjchem-782	258	22	dimethylsulfoxonium	dimethylsulfoxonium	NOUN
eurjchem-782	258	23	methylide	methylide	NOUN
eurjchem-782	258	24	.	.	PUNCT
eurjchem-782	259	1	it	it	PRON
eurjchem-782	259	2	attacks	attack	VERB
eurjchem-782	259	3	nucleophilically	nucleophilically	ADV
eurjchem-782	259	4	the	the	DET
eurjchem-782	259	5	β‐carbom	β‐carbom	PUNCT
eurjchem-782	259	6	atom	atom	NOUN
eurjchem-782	259	7	of	of	ADP
eurjchem-782	259	8	the	the	DET
eurjchem-782	259	9	chalcone	chalcone	NOUN
eurjchem-782	259	10	which	which	PRON
eurjchem-782	259	11	acts	act	VERB
eurjchem-782	259	12	as	as	SCONJ
eurjchem-782	259	13	michael	michael	PROPN
eurjchem-782	259	14	receptors	receptor	NOUN
eurjchem-782	259	15	to	to	PART
eurjchem-782	259	16	form	form	VERB
eurjchem-782	259	17	an	an	DET
eurjchem-782	259	18	enolate	enolate	ADJ
eurjchem-782	259	19	ion	ion	NOUN
eurjchem-782	259	20	,	,	PUNCT
eurjchem-782	259	21	which	which	PRON
eurjchem-782	259	22	undergoes	undergo	VERB
eurjchem-782	259	23	nucleophilic	nucleophilic	ADJ
eurjchem-782	259	24	attack	attack	NOUN
eurjchem-782	259	25	on	on	ADP
eurjchem-782	259	26	the	the	DET
eurjchem-782	259	27	methylene	methylene	NOUN
eurjchem-782	259	28	carbon	carbon	NOUN
eurjchem-782	259	29	atom	atom	NOUN
eurjchem-782	259	30	bearing	bear	VERB
eurjchem-782	259	31	the	the	DET
eurjchem-782	259	32	dimethylsulfoxonium	dimethylsulfoxonium	NOUN
eurjchem-782	259	33	cation	cation	NOUN
eurjchem-782	259	34	intramolecularly	intramolecularly	ADV
eurjchem-782	259	35	finally	finally	ADV
eurjchem-782	259	36	to	to	PART
eurjchem-782	259	37	form	form	VERB
eurjchem-782	259	38	the	the	DET
eurjchem-782	259	39	desired	desire	VERB
eurjchem-782	259	40	cyclopropyl	cyclopropyl	PROPN
eurjchem-782	259	41	ketone	ketone	NOUN
eurjchem-782	259	42	.	.	PUNCT
eurjchem-782	260	1	the	the	DET
eurjchem-782	260	2	structure	structure	NOUN
eurjchem-782	260	3	of	of	ADP
eurjchem-782	260	4	compounds	compound	NOUN
eurjchem-782	260	5	(	(	PUNCT
eurjchem-782	260	6	4a‐d	4a‐d	NOUN
eurjchem-782	260	7	)	)	PUNCT
eurjchem-782	260	8	was	be	AUX
eurjchem-782	260	9	confirmed	confirm	VERB
eurjchem-782	260	10	by	by	ADP
eurjchem-782	260	11	ir	ir	PROPN
eurjchem-782	260	12	spectra	spectra	PROPN
eurjchem-782	260	13	.	.	PUNCT
eurjchem-782	261	1	in	in	ADP
eurjchem-782	261	2	its	its	PRON
eurjchem-782	261	3	ir	ir	PROPN
eurjchem-782	261	4	spectra	spectra	NOUN
eurjchem-782	261	5	exhibited	exhibit	VERB
eurjchem-782	261	6	c	c	NOUN
eurjchem-782	261	7	=	=	NOUN
eurjchem-782	261	8	o	o	NOUN
eurjchem-782	261	9	stretching	stretch	VERB
eurjchem-782	261	10	band	band	NOUN
eurjchem-782	261	11	in	in	ADP
eurjchem-782	261	12	the	the	DET
eurjchem-782	261	13	range	range	NOUN
eurjchem-782	261	14	1687‐1671	1687‐1671	PROPN
eurjchem-782	261	15	cm‐1	cm‐1	NOUN
eurjchem-782	261	16	and	and	CCONJ
eurjchem-782	261	17	1h	1h	NUM
eurjchem-782	261	18	nmr	nmr	NOUN
eurjchem-782	261	19	showed	show	VERB
eurjchem-782	261	20	the	the	DET
eurjchem-782	261	21	cyclopropane	cyclopropane	NOUN
eurjchem-782	261	22	ch2	ch2	NOUN
eurjchem-782	261	23	and	and	CCONJ
eurjchem-782	261	24	ch	ch	NOUN
eurjchem-782	261	25	peak	peak	NOUN
eurjchem-782	261	26	at	at	ADP
eurjchem-782	261	27	the	the	DET
eurjchem-782	261	28	range	range	NOUN
eurjchem-782	261	29	2.21‐	2.21‐	NUM
eurjchem-782	261	30	2.00	2.00	NUM
eurjchem-782	261	31	and	and	CCONJ
eurjchem-782	261	32	0.83‐0.78	0.83‐0.78	PRON
eurjchem-782	261	33	ppm	ppm	VERB
eurjchem-782	261	34	respectively	respectively	ADV
eurjchem-782	261	35	.	.	PUNCT
eurjchem-782	262	1	tetralones	tetralone	NOUN
eurjchem-782	262	2	(	(	PUNCT
eurjchem-782	262	3	5a‐d	5a‐d	ADV
eurjchem-782	262	4	)	)	PUNCT
eurjchem-782	262	5	were	be	AUX
eurjchem-782	262	6	prepared	prepare	VERB
eurjchem-782	262	7	in	in	ADP
eurjchem-782	262	8	good	good	ADJ
eurjchem-782	262	9	yields	yield	NOUN
eurjchem-782	262	10	by	by	ADP
eurjchem-782	262	11	the	the	DET
eurjchem-782	262	12	friedel‐craft	friedel‐craft	NOUN
eurjchem-782	262	13	’s	’s	PART
eurjchem-782	262	14	intramolecular	intramolecular	ADJ
eurjchem-782	262	15	cyclization	cyclization	NOUN
eurjchem-782	262	16	reaction	reaction	NOUN
eurjchem-782	262	17	of	of	ADP
eurjchem-782	262	18	cyclopropyle	cyclopropyle	NOUN
eurjchem-782	262	19	ketones	ketone	NOUN
eurjchem-782	262	20	(	(	PUNCT
eurjchem-782	262	21	4a‐d	4a‐d	NOUN
eurjchem-782	262	22	)	)	PUNCT
eurjchem-782	262	23	in	in	ADP
eurjchem-782	262	24	the	the	DET
eurjchem-782	262	25	presence	presence	NOUN
eurjchem-782	262	26	of	of	ADP
eurjchem-782	262	27	anhyd	anhyd	NOUN
eurjchem-782	262	28	.	.	PUNCT
eurjchem-782	263	1	stannic	stannic	ADJ
eurjchem-782	263	2	chloride	chloride	NOUN
eurjchem-782	263	3	and	and	CCONJ
eurjchem-782	263	4	acetic	acetic	ADJ
eurjchem-782	263	5	anhydride	anhydride	NOUN
eurjchem-782	263	6	in	in	ADP
eurjchem-782	263	7	dry	dry	ADJ
eurjchem-782	263	8	dichloromethane	dichloromethane	NOUN
eurjchem-782	263	9	[	[	X
eurjchem-782	263	10	17	17	NUM
eurjchem-782	263	11	]	]	PUNCT
eurjchem-782	263	12	.	.	PUNCT
eurjchem-782	264	1	the	the	DET
eurjchem-782	264	2	cyclopropyl	cyclopropyl	PROPN
eurjchem-782	264	3	ketones	ketone	NOUN
eurjchem-782	264	4	undergoes	undergo	VERB
eurjchem-782	264	5	electrophilic	electrophilic	ADJ
eurjchem-782	264	6	ring	ring	NOUN
eurjchem-782	264	7	opening	opening	NOUN
eurjchem-782	264	8	in	in	ADP
eurjchem-782	264	9	the	the	DET
eurjchem-782	264	10	presence	presence	NOUN
eurjchem-782	264	11	of	of	ADP
eurjchem-782	264	12	lewis	lewis	PROPN
eurjchem-782	264	13	acid	acid	PROPN
eurjchem-782	264	14	to	to	PART
eurjchem-782	264	15	give	give	VERB
eurjchem-782	264	16	benzylcarbocationic	benzylcarbocationic	ADJ
eurjchem-782	264	17	intermediate	intermediate	ADJ
eurjchem-782	264	18	which	which	PRON
eurjchem-782	264	19	is	be	AUX
eurjchem-782	264	20	intramolecularly	intramolecularly	ADV
eurjchem-782	264	21	attacked	attack	VERB
eurjchem-782	264	22	by	by	ADP
eurjchem-782	264	23	aryl	aryl	NOUN
eurjchem-782	264	24	ring	ring	NOUN
eurjchem-782	264	25	π‐electrons	π‐electron	NOUN
eurjchem-782	264	26	resulting	result	VERB
eurjchem-782	264	27	in	in	ADP
eurjchem-782	264	28	the	the	DET
eurjchem-782	264	29	formation	formation	NOUN
eurjchem-782	264	30	of	of	ADP
eurjchem-782	264	31	a	a	DET
eurjchem-782	264	32	six	six	NUM
eurjchem-782	264	33	membered	membere	VERB
eurjchem-782	264	34	ring	ring	NOUN
eurjchem-782	264	35	with	with	ADP
eurjchem-782	264	36	a	a	DET
eurjchem-782	264	37	pendant	pendant	ADJ
eurjchem-782	264	38	carbocation	carbocation	NOUN
eurjchem-782	264	39	.	.	PUNCT
eurjchem-782	265	1	this	this	PRON
eurjchem-782	265	2	readily	readily	ADV
eurjchem-782	265	3	gives	give	VERB
eurjchem-782	265	4	up	up	ADP
eurjchem-782	265	5	proton	proton	NOUN
eurjchem-782	265	6	to	to	PART
eurjchem-782	265	7	form	form	VERB
eurjchem-782	265	8	tetralones	tetralone	NOUN
eurjchem-782	265	9	.	.	PUNCT
eurjchem-782	266	1	acetic	acetic	ADJ
eurjchem-782	266	2	anhydride	anhydride	NOUN
eurjchem-782	266	3	which	which	PRON
eurjchem-782	266	4	facilitates	facilitate	VERB
eurjchem-782	266	5	the	the	DET
eurjchem-782	266	6	formation	formation	NOUN
eurjchem-782	266	7	of	of	ADP
eurjchem-782	266	8	desired	desire	VERB
eurjchem-782	266	9	tetralones	tetralone	NOUN
eurjchem-782	266	10	.	.	PUNCT
eurjchem-782	267	1	in	in	ADP
eurjchem-782	267	2	its	its	PRON
eurjchem-782	267	3	ir	ir	PROPN
eurjchem-782	267	4	spectra	spectra	PROPN
eurjchem-782	267	5	appeared	appear	VERB
eurjchem-782	267	6	absorption	absorption	NOUN
eurjchem-782	267	7	bands	band	NOUN
eurjchem-782	267	8	in	in	ADP
eurjchem-782	267	9	the	the	DET
eurjchem-782	267	10	range	range	NOUN
eurjchem-782	267	11	3133‐2934	3133‐2934	NUM
eurjchem-782	267	12	cm‐1	cm‐1	NOUN
eurjchem-782	267	13	and	and	CCONJ
eurjchem-782	267	14	1705‐1685	1705‐1685	NUM
eurjchem-782	267	15	cm‐1	cm‐1	NOUN
eurjchem-782	267	16	corresponds	correspond	VERB
eurjchem-782	267	17	to	to	ADP
eurjchem-782	267	18	aromatic	aromatic	ADJ
eurjchem-782	267	19	and	and	CCONJ
eurjchem-782	267	20	c	c	NOUN
eurjchem-782	267	21	=	=	NOUN
eurjchem-782	267	22	o	o	NOUN
eurjchem-782	267	23	stretching	stretch	VERB
eurjchem-782	267	24	frequencies	frequency	NOUN
eurjchem-782	267	25	and	and	CCONJ
eurjchem-782	267	26	1h	1h	NUM
eurjchem-782	267	27	nmr	nmr	NOUN
eurjchem-782	267	28	of	of	ADP
eurjchem-782	267	29	the	the	DET
eurjchem-782	267	30	ring	ring	PROPN
eurjchem-782	267	31	b	b	PROPN
eurjchem-782	267	32	proton	proton	NOUN
eurjchem-782	267	33	appears	appear	VERB
eurjchem-782	267	34	in	in	ADP
eurjchem-782	267	35	the	the	DET
eurjchem-782	267	36	range	range	NOUN
eurjchem-782	267	37	2.65‐2.18	2.65‐2.18	NUM
eurjchem-782	267	38	ppm	ppm	NOUN
eurjchem-782	267	39	.	.	PUNCT
eurjchem-782	268	1	they	they	PRON
eurjchem-782	268	2	are	be	AUX
eurjchem-782	268	3	key	key	ADJ
eurjchem-782	268	4	intermediates	intermediate	NOUN
eurjchem-782	268	5	for	for	ADP
eurjchem-782	268	6	the	the	DET
eurjchem-782	268	7	preparation	preparation	NOUN
eurjchem-782	268	8	of	of	ADP
eurjchem-782	268	9	the	the	DET
eurjchem-782	268	10	novel	novel	ADJ
eurjchem-782	268	11	diaza	diaza	NOUN
eurjchem-782	268	12	analogues	analogue	NOUN
eurjchem-782	268	13	of	of	ADP
eurjchem-782	268	14	podophyllotoxin	podophyllotoxin	PROPN
eurjchem-782	268	15	.	.	PUNCT
eurjchem-782	269	1	the	the	DET
eurjchem-782	269	2	tetralones	tetralone	NOUN
eurjchem-782	269	3	on	on	ADP
eurjchem-782	269	4	formylation	formylation	NOUN
eurjchem-782	269	5	to	to	PART
eurjchem-782	269	6	give	give	VERB
eurjchem-782	269	7	substituted	substitute	VERB
eurjchem-782	269	8	hydroxyl‐	hydroxyl‐	PROPN
eurjchem-782	269	9	methylene	methylene	NOUN
eurjchem-782	269	10	tetralones	tetralone	NOUN
eurjchem-782	269	11	(	(	PUNCT
eurjchem-782	269	12	6a‐d	6a‐d	NOUN
eurjchem-782	269	13	)	)	PUNCT
eurjchem-782	270	1	[	[	X
eurjchem-782	270	2	18	18	NUM
eurjchem-782	270	3	]	]	PUNCT
eurjchem-782	270	4	.	.	PUNCT
eurjchem-782	271	1	formation	formation	NOUN
eurjchem-782	271	2	of	of	ADP
eurjchem-782	271	3	the	the	DET
eurjchem-782	271	4	presently	presently	ADV
eurjchem-782	271	5	synthesized	synthesize	VERB
eurjchem-782	271	6	tetralones	tetralone	NOUN
eurjchem-782	271	7	with	with	ADP
eurjchem-782	271	8	ethyl	ethyl	PROPN
eurjchem-782	271	9	formate	formate	NOUN
eurjchem-782	271	10	using	use	VERB
eurjchem-782	271	11	sodium	sodium	NOUN
eurjchem-782	271	12	hydride	hydride	NOUN
eurjchem-782	271	13	as	as	SCONJ
eurjchem-782	271	14	the	the	DET
eurjchem-782	271	15	base	base	NOUN
eurjchem-782	271	16	at	at	ADP
eurjchem-782	271	17	room	room	NOUN
eurjchem-782	271	18	temperature	temperature	NOUN
eurjchem-782	271	19	gave	give	VERB
eurjchem-782	271	20	single	single	ADJ
eurjchem-782	271	21	products	product	NOUN
eurjchem-782	271	22	in	in	ADP
eurjchem-782	271	23	good	good	ADJ
eurjchem-782	271	24	yields	yield	NOUN
eurjchem-782	271	25	.	.	PUNCT
eurjchem-782	272	1	the	the	DET
eurjchem-782	272	2	β‐dicarbonyl	β‐dicarbonyl	PUNCT
eurjchem-782	272	3	compound	compound	NOUN
eurjchem-782	272	4	,	,	PUNCT
eurjchem-782	272	5	which	which	PRON
eurjchem-782	272	6	exist	exist	VERB
eurjchem-782	272	7	in	in	ADP
eurjchem-782	272	8	the	the	DET
eurjchem-782	272	9	enol	enol	NOUN
eurjchem-782	272	10	form	form	NOUN
eurjchem-782	272	11	show	show	VERB
eurjchem-782	272	12	the	the	DET
eurjchem-782	272	13	carbonyl	carbonyl	NOUN
eurjchem-782	272	14	absorption	absorption	NOUN
eurjchem-782	272	15	in	in	ADP
eurjchem-782	272	16	the	the	DET
eurjchem-782	272	17	region	region	NOUN
eurjchem-782	272	18	1640‐1610	1640‐1610	NUM
eurjchem-782	272	19	cm‐1	cm‐1	NOUN
eurjchem-782	272	20	.	.	PUNCT
eurjchem-782	273	1	generally	generally	ADV
eurjchem-782	273	2	1,3‐diketones	1,3‐diketone	VERB
eurjchem-782	273	3	absorption	absorption	NOUN
eurjchem-782	273	4	peak	peak	NOUN
eurjchem-782	273	5	with	with	ADP
eurjchem-782	273	6	high	high	ADJ
eurjchem-782	273	7	intensity	intensity	NOUN
eurjchem-782	273	8	at	at	ADP
eurjchem-782	273	9	1715	1715	NUM
eurjchem-782	273	10	cm‐1	cm‐1	NOUN
eurjchem-782	273	11	.	.	PUNCT
eurjchem-782	274	1	enols	enol	NOUN
eurjchem-782	274	2	containing	contain	VERB
eurjchem-782	274	3	this	this	DET
eurjchem-782	274	4	grouping	grouping	NOUN
eurjchem-782	274	5	,	,	PUNCT
eurjchem-782	274	6	but	but	CCONJ
eurjchem-782	274	7	the	the	DET
eurjchem-782	274	8	shift	shift	NOUN
eurjchem-782	274	9	that	that	PRON
eurjchem-782	274	10	occurs	occur	VERB
eurjchem-782	274	11	in	in	ADP
eurjchem-782	274	12	these	these	DET
eurjchem-782	274	13	compounds	compound	NOUN
eurjchem-782	274	14	is	be	AUX
eurjchem-782	274	15	attributed	attribute	VERB
eurjchem-782	274	16	to	to	ADP
eurjchem-782	274	17	the	the	DET
eurjchem-782	274	18	intramolecular	intramolecular	ADJ
eurjchem-782	274	19	hydrogen	hydrogen	NOUN
eurjchem-782	274	20	bonding	bonding	NOUN
eurjchem-782	274	21	(	(	PUNCT
eurjchem-782	274	22	figure	figure	NOUN
eurjchem-782	274	23	2	2	NUM
eurjchem-782	274	24	)	)	PUNCT
eurjchem-782	274	25	.	.	PUNCT
eurjchem-782	275	1	figure	figure	NOUN
eurjchem-782	275	2	2	2	NUM
eurjchem-782	275	3	.	.	PUNCT
eurjchem-782	275	4	β‐dicarbonyl	β‐dicarbonyl	PUNCT
eurjchem-782	276	1	compound	compound	NOUN
eurjchem-782	276	2	which	which	PRON
eurjchem-782	276	3	exist	exist	VERB
eurjchem-782	276	4	in	in	ADP
eurjchem-782	276	5	the	the	DET
eurjchem-782	276	6	enol	enol	NOUN
eurjchem-782	276	7	form	form	NOUN
eurjchem-782	276	8	.	.	PUNCT
eurjchem-782	277	1	at	at	ADP
eurjchem-782	277	2	the	the	DET
eurjchem-782	277	3	same	same	ADJ
eurjchem-782	277	4	time	time	NOUN
eurjchem-782	277	5	,	,	PUNCT
eurjchem-782	277	6	the	the	DET
eurjchem-782	277	7	true	true	ADJ
eurjchem-782	277	8	alcoholic	alcoholic	ADJ
eurjchem-782	277	9	hydroxyl	hydroxyl	NOUN
eurjchem-782	277	10	band	band	NOUN
eurjchem-782	277	11	near	near	ADP
eurjchem-782	277	12	3700	3700	NUM
eurjchem-782	277	13	cm‐1	cm‐1	NOUN
eurjchem-782	277	14	is	be	AUX
eurjchem-782	277	15	absent	absent	ADJ
eurjchem-782	277	16	in	in	ADP
eurjchem-782	277	17	enols	enol	NOUN
eurjchem-782	277	18	,	,	PUNCT
eurjchem-782	277	19	but	but	CCONJ
eurjchem-782	277	20	there	there	PRON
eurjchem-782	277	21	is	be	VERB
eurjchem-782	277	22	a	a	DET
eurjchem-782	277	23	band	band	NOUN
eurjchem-782	277	24	near	near	ADP
eurjchem-782	277	25	3258‐	3258‐	NUM
eurjchem-782	277	26	3251	3251	NUM
eurjchem-782	277	27	cm‐1	cm‐1	NOUN
eurjchem-782	277	28	(	(	PUNCT
eurjchem-782	277	29	s	s	NOUN
eurjchem-782	277	30	)	)	PUNCT
eurjchem-782	277	31	which	which	PRON
eurjchem-782	277	32	is	be	AUX
eurjchem-782	277	33	attributed	attribute	VERB
eurjchem-782	277	34	to	to	ADP
eurjchem-782	277	35	the	the	DET
eurjchem-782	277	36	chelated	chelated	ADJ
eurjchem-782	277	37	hydroxyl	hydroxyl	NOUN
eurjchem-782	277	38	group	group	NOUN
eurjchem-782	277	39	.	.	PUNCT
eurjchem-782	278	1	1h	1h	NUM
eurjchem-782	278	2	nmr	nmr	NOUN
eurjchem-782	278	3	showed	show	VERB
eurjchem-782	278	4	the	the	DET
eurjchem-782	278	5	vinylic	vinylic	ADJ
eurjchem-782	278	6	proton	proton	NOUN
eurjchem-782	278	7	absorption	absorption	NOUN
eurjchem-782	278	8	at	at	ADP
eurjchem-782	278	9	5.80‐	5.80‐	NUM
eurjchem-782	278	10	5.60	5.60	NUM
eurjchem-782	278	11	ppm	ppm	NOUN
eurjchem-782	278	12	.	.	PUNCT
eurjchem-782	279	1	the	the	DET
eurjchem-782	279	2	diaza	diaza	PROPN
eurjchem-782	279	3	analogues	analogue	NOUN
eurjchem-782	279	4	of	of	ADP
eurjchem-782	279	5	podophyllotoxin	podophyllotoxin	PROPN
eurjchem-782	279	6	(	(	PUNCT
eurjchem-782	279	7	7a‐d	7a‐d	NOUN
eurjchem-782	279	8	)	)	PUNCT
eurjchem-782	279	9	were	be	AUX
eurjchem-782	279	10	umesha	umesha	ADJ
eurjchem-782	279	11	and	and	CCONJ
eurjchem-782	279	12	basavaraju	basavaraju	NOUN
eurjchem-782	279	13	/	/	SYM
eurjchem-782	279	14	european	european	ADJ
eurjchem-782	279	15	journal	journal	PROPN
eurjchem-782	279	16	of	of	ADP
eurjchem-782	279	17	chemistry	chemistry	NOUN
eurjchem-782	279	18	4	4	NUM
eurjchem-782	279	19	(	(	PUNCT
eurjchem-782	279	20	3	3	NUM
eurjchem-782	279	21	)	)	PUNCT
eurjchem-782	279	22	(	(	PUNCT
eurjchem-782	279	23	2013	2013	NUM
eurjchem-782	279	24	)	)	PUNCT
eurjchem-782	279	25	235‐239	235‐239	NUM
eurjchem-782	279	26	239	239	NUM
eurjchem-782	279	27	synthesized	synthesize	VERB
eurjchem-782	279	28	in	in	ADP
eurjchem-782	279	29	high	high	ADJ
eurjchem-782	279	30	yields	yield	NOUN
eurjchem-782	279	31	by	by	ADP
eurjchem-782	279	32	the	the	DET
eurjchem-782	279	33	condensation	condensation	NOUN
eurjchem-782	279	34	of	of	ADP
eurjchem-782	279	35	hydroxylmethylene	hydroxylmethylene	ADJ
eurjchem-782	279	36	tetralones	tetralone	NOUN
eurjchem-782	279	37	and	and	CCONJ
eurjchem-782	279	38	hydrazine	hydrazine	NOUN
eurjchem-782	279	39	hydrate	hydrate	NOUN
eurjchem-782	279	40	in	in	ADP
eurjchem-782	279	41	absolute	absolute	ADJ
eurjchem-782	279	42	ethanol	ethanol	NOUN
eurjchem-782	279	43	[	[	X
eurjchem-782	279	44	19	19	NUM
eurjchem-782	279	45	]	]	PUNCT
eurjchem-782	279	46	.	.	PUNCT
eurjchem-782	280	1	the	the	DET
eurjchem-782	280	2	products	product	NOUN
eurjchem-782	280	3	were	be	AUX
eurjchem-782	280	4	purified	purify	VERB
eurjchem-782	280	5	by	by	ADP
eurjchem-782	280	6	column	column	NOUN
eurjchem-782	280	7	chromatography	chromatography	NOUN
eurjchem-782	280	8	by	by	ADP
eurjchem-782	280	9	using	use	VERB
eurjchem-782	280	10	benzene‐ethyl	benzene‐ethyl	PROPN
eurjchem-782	280	11	acetate	acetate	NOUN
eurjchem-782	280	12	mixture	mixture	NOUN
eurjchem-782	280	13	as	as	ADP
eurjchem-782	280	14	eluent	eluent	NOUN
eurjchem-782	280	15	and	and	CCONJ
eurjchem-782	280	16	silica	silica	NOUN
eurjchem-782	280	17	gel	gel	NOUN
eurjchem-782	280	18	as	as	ADP
eurjchem-782	280	19	an	an	DET
eurjchem-782	280	20	adsorbent	adsorbent	NOUN
eurjchem-782	280	21	or	or	CCONJ
eurjchem-782	280	22	recrystallization	recrystallization	NOUN
eurjchem-782	280	23	from	from	ADP
eurjchem-782	280	24	ethanol	ethanol	NOUN
eurjchem-782	280	25	.	.	PUNCT
eurjchem-782	281	1	the	the	DET
eurjchem-782	281	2	compounds	compound	NOUN
eurjchem-782	281	3	(	(	PUNCT
eurjchem-782	281	4	7a‐d	7a‐d	NOUN
eurjchem-782	281	5	)	)	PUNCT
eurjchem-782	281	6	exhibited	exhibit	VERB
eurjchem-782	281	7	nh	nh	PROPN
eurjchem-782	281	8	stretching	stretch	VERB
eurjchem-782	281	9	band	band	NOUN
eurjchem-782	281	10	at	at	ADP
eurjchem-782	281	11	3269‐3265	3269‐3265	NUM
eurjchem-782	281	12	cm‐1	cm‐1	NOUN
eurjchem-782	281	13	and	and	CCONJ
eurjchem-782	281	14	proton	proton	NOUN
eurjchem-782	281	15	nmr	nmr	NOUN
eurjchem-782	281	16	showed	show	VERB
eurjchem-782	281	17	singlet	singlet	ADJ
eurjchem-782	281	18	nh	nh	PROPN
eurjchem-782	281	19	peak	peak	NOUN
eurjchem-782	281	20	at	at	ADP
eurjchem-782	281	21	12.64‐12.55	12.64‐12.55	NUM
eurjchem-782	281	22	ppm	ppm	NOUN
eurjchem-782	281	23	.	.	PUNCT
eurjchem-782	282	1	based	base	VERB
eurjchem-782	282	2	on	on	ADP
eurjchem-782	282	3	this	this	PRON
eurjchem-782	282	4	,	,	PUNCT
eurjchem-782	282	5	the	the	DET
eurjchem-782	282	6	synthesized	synthesize	VERB
eurjchem-782	282	7	compounds	compound	NOUN
eurjchem-782	282	8	were	be	AUX
eurjchem-782	282	9	confirmed	confirm	VERB
eurjchem-782	282	10	.	.	PUNCT
eurjchem-782	283	1	4	4	X
eurjchem-782	283	2	.	.	X
eurjchem-782	283	3	conclusion	conclusion	NOUN
eurjchem-782	283	4	in	in	ADP
eurjchem-782	283	5	summary	summary	NOUN
eurjchem-782	283	6	,	,	PUNCT
eurjchem-782	283	7	a	a	DET
eurjchem-782	283	8	convenient	convenient	ADJ
eurjchem-782	283	9	synthesis	synthesis	NOUN
eurjchem-782	283	10	of	of	ADP
eurjchem-782	283	11	novel	novel	ADJ
eurjchem-782	283	12	diaza	diaza	NOUN
eurjchem-782	283	13	analogues	analogue	NOUN
eurjchem-782	283	14	of	of	ADP
eurjchem-782	283	15	podophyllotoxin	podophyllotoxin	NOUN
eurjchem-782	283	16	has	have	AUX
eurjchem-782	283	17	been	be	AUX
eurjchem-782	283	18	developed	develop	VERB
eurjchem-782	283	19	.	.	PUNCT
eurjchem-782	284	1	this	this	DET
eurjchem-782	284	2	procedure	procedure	NOUN
eurjchem-782	284	3	provides	provide	VERB
eurjchem-782	284	4	good	good	ADJ
eurjchem-782	284	5	yields	yield	NOUN
eurjchem-782	284	6	of	of	ADP
eurjchem-782	284	7	podophyllotoxin	podophyllotoxin	PROPN
eurjchem-782	284	8	analogues	analogue	NOUN
eurjchem-782	284	9	.	.	PUNCT
eurjchem-782	285	1	this	this	PRON
eurjchem-782	285	2	constitutes	constitute	VERB
eurjchem-782	285	3	one	one	NUM
eurjchem-782	285	4	of	of	ADP
eurjchem-782	285	5	the	the	DET
eurjchem-782	285	6	synthetic	synthetic	ADJ
eurjchem-782	285	7	methods	method	NOUN
eurjchem-782	285	8	by	by	ADP
eurjchem-782	285	9	doing	do	VERB
eurjchem-782	285	10	structural	structural	ADJ
eurjchem-782	285	11	modifications	modification	NOUN
eurjchem-782	285	12	to	to	PART
eurjchem-782	285	13	podophyllotoxin	podophyllotoxin	VERB
eurjchem-782	285	14	for	for	ADP
eurjchem-782	285	15	novel	novel	ADJ
eurjchem-782	285	16	diaza	diaza	NOUN
eurjchem-782	285	17	analogues	analogue	NOUN
eurjchem-782	285	18	of	of	ADP
eurjchem-782	285	19	podophyllotoxin	podophyllotoxin	PROPN
eurjchem-782	285	20	.	.	PUNCT
eurjchem-782	286	1	acknowledgement	acknowledgement	NOUN
eurjchem-782	286	2	the	the	DET
eurjchem-782	286	3	authors	author	NOUN
eurjchem-782	286	4	are	be	AUX
eurjchem-782	286	5	thankful	thankful	ADJ
eurjchem-782	286	6	to	to	ADP
eurjchem-782	286	7	indian	indian	PROPN
eurjchem-782	286	8	institute	institute	PROPN
eurjchem-782	286	9	of	of	ADP
eurjchem-782	286	10	technology	technology	PROPN
eurjchem-782	286	11	,	,	PUNCT
eurjchem-782	286	12	bombay	bombay	PROPN
eurjchem-782	286	13	for	for	ADP
eurjchem-782	286	14	providing	provide	VERB
eurjchem-782	286	15	spectral	spectral	ADJ
eurjchem-782	286	16	data	datum	NOUN
eurjchem-782	286	17	.	.	PUNCT
eurjchem-782	287	1	references	reference	NOUN
eurjchem-782	287	2	[	[	X
eurjchem-782	287	3	1	1	NUM
eurjchem-782	287	4	]	]	PUNCT
eurjchem-782	287	5	.	.	PUNCT
eurjchem-782	288	1	shi‐wu	shi‐wu	PROPN
eurjchem-782	288	2	,	,	PUNCT
eurjchem-782	288	3	c.	c.	PROPN
eurjchem-782	288	4	;	;	PUNCT
eurjchem-782	288	5	yun‐hua	yun‐hua	PROPN
eurjchem-782	288	6	,	,	PUNCT
eurjchem-782	288	7	w.	w.	PROPN
eurjchem-782	288	8	;	;	PUNCT
eurjchem-782	288	9	yan	yan	PROPN
eurjchem-782	288	10	,	,	PUNCT
eurjchem-782	288	11	j.	j.	PROPN
eurjchem-782	288	12	;	;	PUNCT
eurjchem-782	288	13	xuan	xuan	PROPN
eurjchem-782	288	14	,	,	PUNCT
eurjchem-782	288	15	t.	t.	PROPN
eurjchem-782	288	16	;	;	PUNCT
eurjchem-782	288	17	yong‐tang	yong‐tang	PROPN
eurjchem-782	288	18	,	,	PUNCT
eurjchem-782	288	19	z.	z.	PROPN
eurjchem-782	288	20	;	;	PUNCT
eurjchem-782	288	21	du‐qiang	du‐qiang	PROPN
eurjchem-782	288	22	,	,	PUNCT
eurjchem-782	288	23	l.	l.	PROPN
eurjchem-782	288	24	;	;	PUNCT
eurjchem-782	288	25	yong‐qiang	yong‐qiang	PROPN
eurjchem-782	288	26	,	,	PUNCT
eurjchem-782	288	27	t.	t.	PROPN
eurjchem-782	288	28	bioorg	bioorg	PROPN
eurjchem-782	288	29	.	.	PUNCT
eurjchem-782	289	1	med	med	PROPN
eurjchem-782	289	2	.	.	PROPN
eurjchem-782	289	3	chem	chem	PROPN
eurjchem-782	289	4	.	.	PUNCT
eurjchem-782	290	1	lett	lett	PROPN
eurjchem-782	290	2	.	.	PUNCT
eurjchem-782	291	1	2007	2007	NUM
eurjchem-782	291	2	,	,	PUNCT
eurjchem-782	291	3	17	17	NUM
eurjchem-782	291	4	,	,	PUNCT
eurjchem-782	291	5	2091‐	2091‐	NUM
eurjchem-782	291	6	2095	2095	NUM
eurjchem-782	291	7	.	.	PUNCT
eurjchem-782	292	1	[	[	X
eurjchem-782	292	2	2	2	NUM
eurjchem-782	292	3	]	]	PUNCT
eurjchem-782	292	4	.	.	PUNCT
eurjchem-782	293	1	mohammed	mohammed	PROPN
eurjchem-782	293	2	,	,	PUNCT
eurjchem-782	293	3	m.	m.	NOUN
eurjchem-782	293	4	m.	m.	PROPN
eurjchem-782	293	5	d.	d.	PROPN
eurjchem-782	293	6	;	;	PUNCT
eurjchem-782	293	7	chen	chen	PROPN
eurjchem-782	293	8	,	,	PUNCT
eurjchem-782	293	9	m.	m.	NOUN
eurjchem-782	293	10	;	;	PUNCT
eurjchem-782	293	11	zhai	zhai	PROPN
eurjchem-782	293	12	,	,	PUNCT
eurjchem-782	293	13	l.	l.	PROPN
eurjchem-782	293	14	;	;	PUNCT
eurjchem-782	293	15	ibrahim	ibrahim	PROPN
eurjchem-782	293	16	,	,	PUNCT
eurjchem-782	293	17	n.	n.	PROPN
eurjchem-782	293	18	a.	a.	PROPN
eurjchem-782	293	19	eur	eur	PROPN
eurjchem-782	293	20	.	.	PUNCT
eurjchem-782	294	1	j.	j.	PROPN
eurjchem-782	294	2	chem	chem	PROPN
eurjchem-782	294	3	.	.	PUNCT
eurjchem-782	295	1	2010	2010	NUM
eurjchem-782	295	2	,	,	PUNCT
eurjchem-782	295	3	1(2	1(2	NUM
eurjchem-782	295	4	)	)	PUNCT
eurjchem-782	295	5	,	,	PUNCT
eurjchem-782	295	6	110‐114	110‐114	NUM
eurjchem-782	295	7	.	.	PUNCT
eurjchem-782	296	1	[	[	X
eurjchem-782	296	2	3	3	NUM
eurjchem-782	296	3	]	]	PUNCT
eurjchem-782	296	4	.	.	PUNCT
eurjchem-782	297	1	zhu	zhu	PROPN
eurjchem-782	297	2	,	,	PUNCT
eurjchem-782	297	3	x.	x.	PROPN
eurjchem-782	297	4	k.	k.	PROPN
eurjchem-782	297	5	;	;	PUNCT
eurjchem-782	297	6	guan	guan	PROPN
eurjchem-782	297	7	,	,	PUNCT
eurjchem-782	297	8	j.	j.	PROPN
eurjchem-782	297	9	;	;	PUNCT
eurjchem-782	297	10	xiao	xiao	PROPN
eurjchem-782	297	11	,	,	PUNCT
eurjchem-782	297	12	z.	z.	PROPN
eurjchem-782	297	13	;	;	PUNCT
eurjchem-782	297	14	cosentino	cosentino	PROPN
eurjchem-782	297	15	,	,	PUNCT
eurjchem-782	297	16	m.	m.	NOUN
eurjchem-782	297	17	;	;	PUNCT
eurjchem-782	297	18	lee	lee	PROPN
eurjchem-782	297	19	,	,	PUNCT
eurjchem-782	297	20	k.	k.	PROPN
eurjchem-782	297	21	h.	h.	PROPN
eurjchem-782	297	22	bioorg	bioorg	PROPN
eurjchem-782	297	23	.	.	PUNCT
eurjchem-782	298	1	med	med	PROPN
eurjchem-782	298	2	.	.	PUNCT
eurjchem-782	298	3	chem	chem	PROPN
eurjchem-782	298	4	.	.	PUNCT
eurjchem-782	299	1	2004	2004	NUM
eurjchem-782	299	2	,	,	PUNCT
eurjchem-782	299	3	12	12	NUM
eurjchem-782	299	4	,	,	PUNCT
eurjchem-782	299	5	4267‐4273	4267‐4273	NUM
eurjchem-782	299	6	.	.	PUNCT
eurjchem-782	300	1	[	[	X
eurjchem-782	300	2	4	4	NUM
eurjchem-782	300	3	]	]	PUNCT
eurjchem-782	300	4	.	.	PUNCT
eurjchem-782	301	1	lee	lee	PROPN
eurjchem-782	301	2	,	,	PUNCT
eurjchem-782	301	3	k.	k.	PROPN
eurjchem-782	301	4	h.	h.	PROPN
eurjchem-782	301	5	acs	acs	PROPN
eurjchem-782	301	6	symp	symp	PROPN
eurjchem-782	301	7	.	.	PUNCT
eurjchem-782	302	1	ser	ser	PROPN
eurjchem-782	302	2	.	.	PROPN
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eurjchem-782	302	4	,	,	PUNCT
eurjchem-782	302	5	170‐190	170‐190	NUM
eurjchem-782	302	6	.	.	PUNCT
eurjchem-782	303	1	[	[	X
eurjchem-782	303	2	5	5	NUM
eurjchem-782	303	3	]	]	PUNCT
eurjchem-782	303	4	.	.	PUNCT
eurjchem-782	304	1	macrae	macrae	PROPN
eurjchem-782	304	2	,	,	PUNCT
eurjchem-782	304	3	w.	w.	PROPN
eurjchem-782	304	4	d.	d.	PROPN
eurjchem-782	304	5	;	;	PUNCT
eurjchem-782	304	6	hudson	hudson	PROPN
eurjchem-782	304	7	,	,	PUNCT
eurjchem-782	304	8	j.	j.	PROPN
eurjchem-782	304	9	b.	b.	PROPN
eurjchem-782	304	10	;	;	PUNCT
eurjchem-782	304	11	towers	tower	NOUN
eurjchem-782	304	12	,	,	PUNCT
eurjchem-782	304	13	b.	b.	PROPN
eurjchem-782	304	14	h.	h.	PROPN
eurjchem-782	304	15	n.	n.	PROPN
eurjchem-782	304	16	planta	planta	PROPN
eurjchem-782	304	17	med	med	PROPN
eurjchem-782	304	18	.	.	PUNCT
eurjchem-782	304	19	1993	1993	NUM
eurjchem-782	304	20	,	,	PUNCT
eurjchem-782	304	21	55	55	NUM
eurjchem-782	304	22	,	,	PUNCT
eurjchem-782	304	23	531‐535	531‐535	NUM
eurjchem-782	304	24	.	.	PUNCT
eurjchem-782	305	1	[	[	X
eurjchem-782	305	2	6	6	NUM
eurjchem-782	305	3	]	]	PUNCT
eurjchem-782	305	4	.	.	PUNCT
eurjchem-782	306	1	imbert	imbert	PROPN
eurjchem-782	306	2	,	,	PUNCT
eurjchem-782	306	3	t.	t.	PROPN
eurjchem-782	306	4	f.	f.	PROPN
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eurjchem-782	306	6	.	.	PUNCT
eurjchem-782	307	1	1998	1998	NUM
eurjchem-782	307	2	,	,	PUNCT
eurjchem-782	307	3	80	80	NUM
eurjchem-782	307	4	,	,	PUNCT
eurjchem-782	307	5	207‐222	207‐222	NOUN
eurjchem-782	307	6	.	.	PUNCT
eurjchem-782	308	1	[	[	X
eurjchem-782	308	2	7	7	NUM
eurjchem-782	308	3	]	]	PUNCT
eurjchem-782	308	4	.	.	PUNCT
eurjchem-782	308	5	hemakumar	hemakumar	PROPN
eurjchem-782	308	6	,	,	PUNCT
eurjchem-782	308	7	k.	k.	PROPN
eurjchem-782	308	8	h.	h.	PROPN
eurjchem-782	308	9	;	;	PUNCT
eurjchem-782	308	10	sathisha	sathisha	PROPN
eurjchem-782	308	11	,	,	PUNCT
eurjchem-782	308	12	a.	a.	PROPN
eurjchem-782	308	13	d.	d.	PROPN
eurjchem-782	308	14	;	;	PUNCT
eurjchem-782	308	15	basavaraju	basavaraju	PROPN
eurjchem-782	308	16	,	,	PUNCT
eurjchem-782	308	17	y.	y.	PROPN
eurjchem-782	308	18	b.	b.	PROPN
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eurjchem-782	308	21	.	.	PUNCT
eurjchem-782	308	22	2008	2008	NUM
eurjchem-782	308	23	,	,	PUNCT
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eurjchem-782	308	25	,	,	PUNCT
eurjchem-782	308	26	114‐119	114‐119	NUM
eurjchem-782	308	27	.	.	PUNCT
eurjchem-782	309	1	[	[	X
eurjchem-782	309	2	8	8	NUM
eurjchem-782	309	3	]	]	PUNCT
eurjchem-782	309	4	.	.	PUNCT
eurjchem-782	310	1	jardine	jardine	PROPN
eurjchem-782	310	2	,	,	PUNCT
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eurjchem-782	310	4	;	;	PUNCT
eurjchem-782	310	5	carrady	carrady	PROPN
eurjchem-782	310	6	,	,	PUNCT
eurjchem-782	310	7	j.	j.	PROPN
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eurjchem-782	310	9	;	;	PUNCT
eurjchem-782	310	10	dourous	dourous	ADJ
eurjchem-782	310	11	,	,	PUNCT
eurjchem-782	310	12	j.	j.	PROPN
eurjchem-782	310	13	d.	d.	PROPN
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eurjchem-782	310	21	,	,	PUNCT
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eurjchem-782	310	24	,	,	PUNCT
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eurjchem-782	310	27	,	,	PUNCT
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eurjchem-782	310	30	.	.	PUNCT
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eurjchem-782	310	34	.	.	PUNCT
eurjchem-782	311	1	319‐351	319‐351	NUM
eurjchem-782	311	2	.	.	PUNCT
eurjchem-782	312	1	[	[	X
eurjchem-782	312	2	9	9	NUM
eurjchem-782	312	3	]	]	PUNCT
eurjchem-782	312	4	.	.	PUNCT
eurjchem-782	313	1	lee	lee	PROPN
eurjchem-782	313	2	,	,	PUNCT
eurjchem-782	313	3	k.	k.	PROPN
eurjchem-782	313	4	h.	h.	PROPN
eurjchem-782	313	5	;	;	PUNCT
eurjchem-782	313	6	beers	beer	NOUN
eurjchem-782	313	7	,	,	PUNCT
eurjchem-782	313	8	s.	s.	PROPN
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eurjchem-782	313	10	;	;	PUNCT
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eurjchem-782	313	12	,	,	PUNCT
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eurjchem-782	313	14	;	;	PUNCT
eurjchem-782	313	15	wang	wang	PROPN
eurjchem-782	313	16	,	,	PUNCT
eurjchem-782	313	17	z.	z.	PROPN
eurjchem-782	313	18	q.	q.	PROPN
eurjchem-782	313	19	;	;	PUNCT
eurjchem-782	313	20	kuo	kuo	PROPN
eurjchem-782	313	21	,	,	PUNCT
eurjchem-782	313	22	y.	y.	PROPN
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eurjchem-782	313	24	;	;	PUNCT
eurjchem-782	313	25	li	li	PROPN
eurjchem-782	313	26	,	,	PUNCT
eurjchem-782	313	27	l.	l.	PROPN
eurjchem-782	313	28	;	;	PUNCT
eurjchem-782	313	29	liu	liu	PROPN
eurjchem-782	313	30	,	,	PUNCT
eurjchem-782	313	31	s.	s.	PROPN
eurjchem-782	313	32	y.	y.	PROPN
eurjchem-782	313	33	;	;	PUNCT
eurjchem-782	313	34	chang	chang	PROPN
eurjchem-782	313	35	,	,	PUNCT
eurjchem-782	313	36	j.	j.	PROPN
eurjchem-782	313	37	y.	y.	PROPN
eurjchem-782	313	38	;	;	PUNCT
eurjchem-782	313	39	han	han	PROPN
eurjchem-782	313	40	,	,	PUNCT
eurjchem-782	313	41	f.	f.	PROPN
eurjchem-782	313	42	s.	s.	PROPN
eurjchem-782	313	43	;	;	PUNCT
eurjchem-782	313	44	chang	chang	PROPN
eurjchem-782	313	45	,	,	PUNCT
eurjchem-782	313	46	y.	y.	PROPN
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eurjchem-782	313	50	.	.	PROPN
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eurjchem-782	313	52	.	.	PUNCT
eurjchem-782	314	1	1990	1990	NUM
eurjchem-782	314	2	,	,	PUNCT
eurjchem-782	314	3	33	33	NUM
eurjchem-782	314	4	,	,	PUNCT
eurjchem-782	314	5	1365‐1368	1365‐1368	NUM
eurjchem-782	314	6	.	.	PUNCT
eurjchem-782	315	1	[	[	X
eurjchem-782	315	2	10	10	NUM
eurjchem-782	315	3	]	]	PUNCT
eurjchem-782	315	4	.	.	PUNCT
eurjchem-782	316	1	stehlin	stehlin	PROPN
eurjchem-782	316	2	,	,	PUNCT
eurjchem-782	316	3	h.	h.	PROPN
eurjchem-782	316	4	;	;	PUNCT
eurjchem-782	316	5	von	von	PROPN
eurjchem-782	316	6	wartburg	wartburg	PROPN
eurjchem-782	316	7	,	,	PUNCT
eurjchem-782	316	8	a.	a.	NOUN
eurjchem-782	316	9	prog	prog	PROPN
eurjchem-782	316	10	.	.	PUNCT
eurjchem-782	317	1	drug	drug	NOUN
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eurjchem-782	317	3	.	.	PUNCT
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eurjchem-782	317	5	,	,	PUNCT
eurjchem-782	317	6	33	33	NUM
eurjchem-782	317	7	,	,	PUNCT
eurjchem-782	317	8	169‐266	169‐266	NUM
eurjchem-782	317	9	.	.	PUNCT
eurjchem-782	318	1	[	[	X
eurjchem-782	318	2	11	11	NUM
eurjchem-782	318	3	]	]	PUNCT
eurjchem-782	318	4	.	.	PUNCT
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eurjchem-782	319	2	,	,	PUNCT
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eurjchem-782	319	4	;	;	PUNCT
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eurjchem-782	319	6	,	,	PUNCT
eurjchem-782	319	7	k.	k.	PROPN
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eurjchem-782	319	9	;	;	PUNCT
eurjchem-782	319	10	paidakula	paidakula	PROPN
eurjchem-782	319	11	,	,	PUNCT
eurjchem-782	319	12	s.	s.	PROPN
eurjchem-782	319	13	;	;	PUNCT
eurjchem-782	319	14	nagula	nagula	PROPN
eurjchem-782	319	15	,	,	PUNCT
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eurjchem-782	319	17	;	;	PUNCT
eurjchem-782	319	18	shiva	shiva	PROPN
eurjchem-782	319	19	,	,	PUNCT
eurjchem-782	319	20	k.	k.	PROPN
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eurjchem-782	319	23	.	.	PUNCT
eurjchem-782	320	1	med	med	PROPN
eurjchem-782	320	2	.	.	PROPN
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eurjchem-782	320	4	.	.	PUNCT
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eurjchem-782	321	2	.	.	PUNCT
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eurjchem-782	322	2	,	,	PUNCT
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eurjchem-782	322	4	,	,	PUNCT
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eurjchem-782	322	6	.	.	PUNCT
eurjchem-782	323	1	[	[	X
eurjchem-782	323	2	12	12	NUM
eurjchem-782	323	3	]	]	PUNCT
eurjchem-782	323	4	.	.	PUNCT
eurjchem-782	324	1	kelly	kelly	PROPN
eurjchem-782	324	2	,	,	PUNCT
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eurjchem-782	324	5	;	;	PUNCT
eurjchem-782	324	6	hart	hart	PROPN
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eurjchem-782	324	12	.	.	PUNCT
eurjchem-782	325	1	j.	j.	PROPN
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eurjchem-782	325	4	.	.	PUNCT
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eurjchem-782	325	6	,	,	PUNCT
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eurjchem-782	325	10	.	.	PUNCT
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eurjchem-782	326	3	]	]	SYM
eurjchem-782	326	4	.	.	PUNCT
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eurjchem-782	326	9	;	;	PUNCT
eurjchem-782	326	10	hannaford	hannaford	PROPN
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eurjchem-782	327	1	[	[	X
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eurjchem-782	327	3	]	]	PUNCT
eurjchem-782	327	4	.	.	PUNCT
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eurjchem-782	328	11	;	;	PUNCT
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eurjchem-782	328	13	,	,	PUNCT
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eurjchem-782	328	15	m.	m.	NOUN
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eurjchem-782	328	17	comm	comm	NOUN
eurjchem-782	328	18	.	.	PUNCT
eurjchem-782	329	1	1990	1990	NUM
eurjchem-782	329	2	,	,	PUNCT
eurjchem-782	329	3	20	20	NUM
eurjchem-782	329	4	,	,	PUNCT
eurjchem-782	329	5	1273‐1277	1273‐1277	NUM
eurjchem-782	329	6	.	.	PUNCT
eurjchem-782	330	1	[	[	X
eurjchem-782	330	2	15	15	NUM
eurjchem-782	330	3	]	]	PUNCT
eurjchem-782	330	4	.	.	PUNCT
eurjchem-782	331	1	doyle	doyle	PROPN
eurjchem-782	331	2	,	,	PUNCT
eurjchem-782	331	3	m.	m.	NOUN
eurjchem-782	331	4	p.	p.	PROPN
eurjchem-782	331	5	;	;	PUNCT
eurjchem-782	331	6	hu	hu	PROPN
eurjchem-782	331	7	,	,	PUNCT
eurjchem-782	331	8	w.	w.	PROPN
eurjchem-782	331	9	adv	adv	PROPN
eurjchem-782	331	10	.	.	PUNCT
eurjchem-782	331	11	synth	synth	PROPN
eurjchem-782	331	12	.	.	PUNCT
eurjchem-782	332	1	catal	catal	PROPN
eurjchem-782	332	2	.	.	PUNCT
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eurjchem-782	333	2	,	,	PUNCT
eurjchem-782	333	3	343	343	NUM
eurjchem-782	333	4	,	,	PUNCT
eurjchem-782	333	5	299‐302	299‐302	PROPN
eurjchem-782	333	6	.	.	PUNCT
eurjchem-782	334	1	[	[	X
eurjchem-782	334	2	16	16	NUM
eurjchem-782	334	3	]	]	PUNCT
eurjchem-782	334	4	.	.	PUNCT
eurjchem-782	335	1	davies	davy	NOUN
eurjchem-782	335	2	,	,	PUNCT
eurjchem-782	335	3	h.	h.	PROPN
eurjchem-782	335	4	m.	m.	PROPN
eurjchem-782	335	5	l.	l.	PROPN
eurjchem-782	335	6	;	;	PUNCT
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eurjchem-782	335	8	,	,	PUNCT
eurjchem-782	335	9	r.	r.	PROPN
eurjchem-782	335	10	l.	l.	PROPN
eurjchem-782	335	11	;	;	PUNCT
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eurjchem-782	335	13	,	,	PUNCT
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eurjchem-782	335	15	j.	j.	PROPN
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eurjchem-782	335	18	,	,	PUNCT
eurjchem-782	335	19	p.	p.	PROPN
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eurjchem-782	335	24	m.	m.	PROPN
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eurjchem-782	336	2	,	,	PUNCT
eurjchem-782	336	3	65	65	NUM
eurjchem-782	336	4	,	,	PUNCT
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eurjchem-782	336	6	.	.	PUNCT
eurjchem-782	337	1	[	[	X
eurjchem-782	337	2	17	17	NUM
eurjchem-782	337	3	]	]	PUNCT
eurjchem-782	337	4	.	.	PUNCT
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eurjchem-782	338	2	,	,	PUNCT
eurjchem-782	338	3	m.	m.	PROPN
eurjchem-782	338	4	b.	b.	PROPN
eurjchem-782	338	5	;	;	PUNCT
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eurjchem-782	338	7	,	,	PUNCT
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eurjchem-782	338	9	b.	b.	PROPN
eurjchem-782	338	10	bulg	bulg	PROPN
eurjchem-782	338	11	.	.	PUNCT
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eurjchem-782	339	2	.	.	PUNCT
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eurjchem-782	340	2	.	.	PUNCT
eurjchem-782	341	1	2005	2005	NUM
eurjchem-782	341	2	,	,	PUNCT
eurjchem-782	341	3	37	37	NUM
eurjchem-782	341	4	,	,	PUNCT
eurjchem-782	341	5	135‐	135‐	NUM
eurjchem-782	341	6	139	139	NUM
eurjchem-782	341	7	.	.	PUNCT
eurjchem-782	342	1	[	[	X
eurjchem-782	342	2	18	18	NUM
eurjchem-782	342	3	]	]	PUNCT
eurjchem-782	342	4	.	.	PUNCT
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eurjchem-782	343	2	,	,	PUNCT
eurjchem-782	343	3	m.	m.	PROPN
eurjchem-782	343	4	c.	c.	PROPN
eurjchem-782	343	5	;	;	PUNCT
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eurjchem-782	343	7	,	,	PUNCT
eurjchem-782	343	8	y.	y.	PROPN
eurjchem-782	343	9	b.	b.	PROPN
eurjchem-782	343	10	ind	ind	PROPN
eurjchem-782	343	11	.	.	PUNCT
eurjchem-782	344	1	j.	j.	PROPN
eurjchem-782	344	2	hetero	hetero	PROPN
eurjchem-782	344	3	.	.	PUNCT
eurjchem-782	345	1	chem	chem	PROPN
eurjchem-782	345	2	.	.	PUNCT
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eurjchem-782	346	2	,	,	PUNCT
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eurjchem-782	346	4	,	,	PUNCT
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eurjchem-782	346	6	.	.	PUNCT
eurjchem-782	347	1	[	[	X
eurjchem-782	347	2	19	19	NUM
eurjchem-782	347	3	]	]	PUNCT
eurjchem-782	347	4	.	.	PUNCT
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eurjchem-782	348	2	,	,	PUNCT
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eurjchem-782	348	4	;	;	PUNCT
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eurjchem-782	348	6	,	,	PUNCT
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eurjchem-782	348	12	,	,	PUNCT
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eurjchem-782	348	14	;	;	PUNCT
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eurjchem-782	348	25	.	.	PUNCT
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eurjchem-782	349	2	,	,	PUNCT
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eurjchem-782	349	4	,	,	PUNCT
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