id	sid	tid	token	lemma	pos
eurjchem-792	1	1	untitled	untitle	VERB
eurjchem-792	1	2	european	european	PROPN
eurjchem-792	1	3	journal	journal	PROPN
eurjchem-792	1	4	of	of	ADP
eurjchem-792	1	5	chemistry	chemistry	NOUN
eurjchem-792	1	6	4	4	NUM
eurjchem-792	1	7	(	(	PUNCT
eurjchem-792	1	8	4	4	NUM
eurjchem-792	1	9	)	)	PUNCT
eurjchem-792	1	10	(	(	PUNCT
eurjchem-792	1	11	2013	2013	NUM
eurjchem-792	1	12	)	)	PUNCT
eurjchem-792	1	13	329‐335	329‐335	PROPN
eurjchem-792	1	14	european	european	PROPN
eurjchem-792	1	15	journal	journal	PROPN
eurjchem-792	1	16	of	of	ADP
eurjchem-792	1	17	chemistry	chemistry	NOUN
eurjchem-792	1	18	issn	issn	PROPN
eurjchem-792	1	19	2153‐2249	2153‐2249	PROPN
eurjchem-792	1	20	(	(	PUNCT
eurjchem-792	1	21	print	print	NOUN
eurjchem-792	1	22	)	)	PUNCT
eurjchem-792	1	23	/	/	SYM
eurjchem-792	1	24	issn	issn	PROPN
eurjchem-792	1	25	2153‐2257	2153‐2257	NUM
eurjchem-792	1	26	(	(	PUNCT
eurjchem-792	1	27	online	online	ADJ
eurjchem-792	1	28	)	)	PUNCT
eurjchem-792	1	29			NOUN
eurjchem-792	1	30	2013	2013	NUM
eurjchem-792	1	31	eurjchem	eurjchem	PROPN
eurjchem-792	1	32	doi:10.5155	doi:10.5155	PROPN
eurjchem-792	1	33	/	/	SYM
eurjchem-792	1	34	eurjchem.4.4.329‐335.792	eurjchem.4.4.329‐335.792	NOUN
eurjchem-792	1	35	european	european	ADJ
eurjchem-792	1	36	journal	journal	PROPN
eurjchem-792	1	37	of	of	ADP
eurjchem-792	1	38	chemistry	chemistry	PROPN
eurjchem-792	1	39	journal	journal	PROPN
eurjchem-792	1	40	homepage	homepage	NOUN
eurjchem-792	1	41	:	:	PUNCT
eurjchem-792	1	42	www.eurjchem.com	www.eurjchem.com	X
eurjchem-792	1	43	synthesis	synthesis	NOUN
eurjchem-792	1	44	and	and	CCONJ
eurjchem-792	1	45	biological	biological	ADJ
eurjchem-792	1	46	evaluation	evaluation	NOUN
eurjchem-792	1	47	of	of	ADP
eurjchem-792	1	48	novel	novel	NOUN
eurjchem-792	1	49	β‐hydroxy	β‐hydroxy	PUNCT
eurjchem-792	1	50	benzimidazolyl	benzimidazolyl	ADJ
eurjchem-792	1	51	sulfone	sulfone	ADJ
eurjchem-792	1	52	fluoroquinolones	fluoroquinolone	NOUN
eurjchem-792	1	53	by	by	ADP
eurjchem-792	1	54	selective	selective	ADJ
eurjchem-792	1	55	oxidation	oxidation	NOUN
eurjchem-792	1	56	using	use	VERB
eurjchem-792	1	57	ammonium	ammonium	NOUN
eurjchem-792	1	58	molybdate	molybdate	NOUN
eurjchem-792	1	59	catalysed	catalyse	VERB
eurjchem-792	1	60	h2o2	h2o2	NOUN
eurjchem-792	1	61	batthini	batthini	NOUN
eurjchem-792	1	62	guruswamy	guruswamy	NOUN
eurjchem-792	1	63	a	a	PRON
eurjchem-792	1	64	,	,	PUNCT
eurjchem-792	1	65	*	*	PROPN
eurjchem-792	1	66	,	,	PUNCT
eurjchem-792	1	67	rama	rama	PROPN
eurjchem-792	1	68	krishnan	krishnan	PROPN
eurjchem-792	1	69	arul	arul	PROPN
eurjchem-792	1	70	a	a	PRON
eurjchem-792	1	71	,	,	PUNCT
eurjchem-792	1	72	muggu	muggu	PROPN
eurjchem-792	1	73	venkata	venkata	PROPN
eurjchem-792	1	74	satya	satya	PROPN
eurjchem-792	1	75	rama	rama	PROPN
eurjchem-792	1	76	krishna	krishna	PROPN
eurjchem-792	1	77	chaitanya	chaitanya	PROPN
eurjchem-792	1	78	b	b	PROPN
eurjchem-792	1	79	and	and	CCONJ
eurjchem-792	1	80	sai	sai	PROPN
eurjchem-792	1	81	subrahmanya	subrahmanya	PROPN
eurjchem-792	1	82	praveen	praveen	PROPN
eurjchem-792	1	83	kumar	kumar	PROPN
eurjchem-792	1	84	darsi	darsi	PROPN
eurjchem-792	1	85	b	b	PROPN
eurjchem-792	1	86	a	a	DET
eurjchem-792	1	87	neuland	neuland	NOUN
eurjchem-792	1	88	laboratories	laboratorie	VERB
eurjchem-792	1	89	research	research	NOUN
eurjchem-792	1	90	and	and	CCONJ
eurjchem-792	1	91	development	development	NOUN
eurjchem-792	1	92	center	center	NOUN
eurjchem-792	1	93	,	,	PUNCT
eurjchem-792	1	94	bonthapally	bonthapally	ADV
eurjchem-792	1	95	,	,	PUNCT
eurjchem-792	1	96	medak	medak	PROPN
eurjchem-792	1	97	,	,	PUNCT
eurjchem-792	1	98	andhra	andhra	PROPN
eurjchem-792	1	99	pradesh‐500313	pradesh‐500313	PROPN
eurjchem-792	1	100	,	,	PUNCT
eurjchem-792	1	101	india	india	PROPN
eurjchem-792	1	102	b	b	PROPN
eurjchem-792	1	103	department	department	PROPN
eurjchem-792	1	104	of	of	ADP
eurjchem-792	1	105	chemistry	chemistry	NOUN
eurjchem-792	1	106	,	,	PUNCT
eurjchem-792	1	107	jawaharlal	jawaharlal	PROPN
eurjchem-792	1	108	nehru	nehru	PROPN
eurjchem-792	1	109	technological	technological	PROPN
eurjchem-792	1	110	university	university	PROPN
eurjchem-792	1	111	hyderabad	hyderabad	PROPN
eurjchem-792	1	112	college	college	PROPN
eurjchem-792	1	113	of	of	ADP
eurjchem-792	1	114	engineering	engineering	PROPN
eurjchem-792	1	115	,	,	PUNCT
eurjchem-792	1	116	kukatpally	kukatpally	ADV
eurjchem-792	1	117	,	,	PUNCT
eurjchem-792	1	118	hyderabad‐500085	hyderabad‐500085	PROPN
eurjchem-792	1	119	,	,	PUNCT
eurjchem-792	1	120	india	india	PROPN
eurjchem-792	1	121	*	*	PUNCT
eurjchem-792	1	122	corresponding	correspond	VERB
eurjchem-792	1	123	author	author	NOUN
eurjchem-792	1	124	at	at	ADP
eurjchem-792	1	125	:	:	PUNCT
eurjchem-792	1	126	neuland	neuland	PROPN
eurjchem-792	1	127	laboratories	laboratories	PROPN
eurjchem-792	1	128	research	research	PROPN
eurjchem-792	1	129	&	&	CCONJ
eurjchem-792	1	130	development	development	PROPN
eurjchem-792	1	131	center	center	PROPN
eurjchem-792	1	132	,	,	PUNCT
eurjchem-792	1	133	bonthapally	bonthapally	ADV
eurjchem-792	1	134	,	,	PUNCT
eurjchem-792	1	135	medak	medak	PROPN
eurjchem-792	1	136	,	,	PUNCT
eurjchem-792	1	137	andhra	andhra	PROPN
eurjchem-792	1	138	pradesh‐500313	pradesh‐500313	PROPN
eurjchem-792	1	139	,	,	PUNCT
eurjchem-792	1	140	india	india	PROPN
eurjchem-792	1	141	.	.	PUNCT
eurjchem-792	2	1	tel	tel	PROPN
eurjchem-792	2	2	.	.	PUNCT
eurjchem-792	2	3	:	:	PUNCT
eurjchem-792	3	1	+91.086.54392608	+91.086.54392608	ADP
eurjchem-792	3	2	;	;	PUNCT
eurjchem-792	3	3	fax	fax	NOUN
eurjchem-792	3	4	:	:	PUNCT
eurjchem-792	3	5	+91.086.54392600	+91.086.54392600	NUM
eurjchem-792	3	6	.	.	PUNCT
eurjchem-792	3	7	e‐mail	e‐mail	PUNCT
eurjchem-792	3	8	address	address	NOUN
eurjchem-792	3	9	:	:	PUNCT
eurjchem-792	3	10	guruswamy2748@gmail.com	guruswamy2748@gmail.com	PROPN
eurjchem-792	3	11	(	(	PUNCT
eurjchem-792	3	12	b.	b.	PROPN
eurjchem-792	3	13	guruswamy	guruswamy	PROPN
eurjchem-792	3	14	)	)	PUNCT
eurjchem-792	3	15	.	.	PUNCT
eurjchem-792	4	1	article	article	NOUN
eurjchem-792	4	2	information	information	PROPN
eurjchem-792	4	3	abstract	abstract	ADV
eurjchem-792	4	4	received	receive	VERB
eurjchem-792	4	5	:	:	PUNCT
eurjchem-792	4	6	05	05	NUM
eurjchem-792	4	7	april	april	PROPN
eurjchem-792	4	8	2013	2013	NUM
eurjchem-792	4	9	received	receive	VERB
eurjchem-792	4	10	in	in	ADP
eurjchem-792	4	11	revised	revise	VERB
eurjchem-792	4	12	form	form	NOUN
eurjchem-792	4	13	:	:	PUNCT
eurjchem-792	4	14	12	12	NUM
eurjchem-792	4	15	july	july	PROPN
eurjchem-792	4	16	2013	2013	NUM
eurjchem-792	4	17	accepted	accept	VERB
eurjchem-792	4	18	:	:	PUNCT
eurjchem-792	4	19	12	12	NUM
eurjchem-792	4	20	july	july	PROPN
eurjchem-792	4	21	2013	2013	NUM
eurjchem-792	4	22	online	online	NOUN
eurjchem-792	4	23	:	:	PUNCT
eurjchem-792	4	24	31	31	NUM
eurjchem-792	4	25	december	december	PROPN
eurjchem-792	4	26	2013	2013	NUM
eurjchem-792	4	27	keywords	keyword	VERB
eurjchem-792	4	28	synthesis	synthesis	NOUN
eurjchem-792	4	29	of	of	ADP
eurjchem-792	4	30	new	new	ADJ
eurjchem-792	4	31	β‐hydroxy	β‐hydroxy	PUNCT
eurjchem-792	4	32	benzimidazolyl	benzimidazolyl	ADJ
eurjchem-792	4	33	sulfides	sulfide	NOUN
eurjchem-792	4	34	(	(	PUNCT
eurjchem-792	4	35	4a‐e	4a‐e	NOUN
eurjchem-792	4	36	)	)	PUNCT
eurjchem-792	4	37	and	and	CCONJ
eurjchem-792	4	38	β‐hydroxy	β‐hydroxy	PUNCT
eurjchem-792	4	39	benzimidazolyl	benzimidazolyl	ADJ
eurjchem-792	4	40	sulfones	sulfone	NOUN
eurjchem-792	4	41	(	(	PUNCT
eurjchem-792	4	42	5a‐e	5a‐e	PROPN
eurjchem-792	4	43	)	)	PUNCT
eurjchem-792	4	44	containing	contain	VERB
eurjchem-792	4	45	7‐piperazine	7‐piperazine	PROPN
eurjchem-792	4	46	fluoroquinolones	fluoroquinolone	NOUN
eurjchem-792	4	47	have	have	AUX
eurjchem-792	4	48	been	be	AUX
eurjchem-792	4	49	described	describe	VERB
eurjchem-792	4	50	and	and	CCONJ
eurjchem-792	4	51	evaluated	evaluate	VERB
eurjchem-792	4	52	for	for	ADP
eurjchem-792	4	53	their	their	PRON
eurjchem-792	4	54	antimicrobial	antimicrobial	ADJ
eurjchem-792	4	55	activity	activity	NOUN
eurjchem-792	4	56	.	.	PUNCT
eurjchem-792	5	1	benzoxazine	benzoxazine	NOUN
eurjchem-792	5	2	fluoroquinolone	fluoroquinolone	NOUN
eurjchem-792	5	3	carboxylic	carboxylic	ADJ
eurjchem-792	5	4	acid	acid	NOUN
eurjchem-792	5	5	,	,	PUNCT
eurjchem-792	5	6	1	1	NUM
eurjchem-792	5	7	,	,	PUNCT
eurjchem-792	5	8	on	on	ADP
eurjchem-792	5	9	reaction	reaction	NOUN
eurjchem-792	5	10	with	with	ADP
eurjchem-792	5	11	piperazine	piperazine	NOUN
eurjchem-792	5	12	in	in	ADP
eurjchem-792	5	13	presence	presence	NOUN
eurjchem-792	5	14	of	of	ADP
eurjchem-792	5	15	triethylamine	triethylamine	NOUN
eurjchem-792	5	16	in	in	ADP
eurjchem-792	5	17	acetonitrile	acetonitrile	NOUN
eurjchem-792	5	18	under	under	ADP
eurjchem-792	5	19	reflux	reflux	NOUN
eurjchem-792	5	20	resulted	result	VERB
eurjchem-792	5	21	7‐piperazine	7‐piperazine	NUM
eurjchem-792	5	22	bezoxazole	bezoxazole	VERB
eurjchem-792	5	23	fluoroquinolone	fluoroquinolone	NOUN
eurjchem-792	5	24	,	,	PUNCT
eurjchem-792	5	25	2	2	X
eurjchem-792	5	26	.	.	PUNCT
eurjchem-792	6	1	the	the	DET
eurjchem-792	6	2	latter	latter	ADJ
eurjchem-792	6	3	is	be	AUX
eurjchem-792	6	4	reacted	react	VERB
eurjchem-792	6	5	with	with	ADP
eurjchem-792	6	6	epichlorohydrine	epichlorohydrine	NOUN
eurjchem-792	6	7	in	in	ADP
eurjchem-792	6	8	presence	presence	NOUN
eurjchem-792	6	9	of	of	ADP
eurjchem-792	6	10	naoh	naoh	NOUN
eurjchem-792	6	11	in	in	ADP
eurjchem-792	6	12	acetone	acetone	NOUN
eurjchem-792	6	13	yielded	yield	VERB
eurjchem-792	6	14	corresponding	corresponding	ADJ
eurjchem-792	6	15	n‐substituted	n‐substitute	VERB
eurjchem-792	6	16	epoxide	epoxide	NOUN
eurjchem-792	6	17	,	,	PUNCT
eurjchem-792	6	18	3	3	NUM
eurjchem-792	6	19	,	,	PUNCT
eurjchem-792	6	20	with	with	ADP
eurjchem-792	6	21	retained	retain	VERB
eurjchem-792	6	22	chirality	chirality	NOUN
eurjchem-792	6	23	,	,	PUNCT
eurjchem-792	6	24	which	which	PRON
eurjchem-792	6	25	on	on	ADP
eurjchem-792	6	26	treatment	treatment	NOUN
eurjchem-792	6	27	with	with	ADP
eurjchem-792	6	28	5‐substituted‐2‐mercaptobenzimidazoles	5‐substituted‐2‐mercaptobenzimidazoles	NUM
eurjchem-792	6	29	given	give	VERB
eurjchem-792	6	30	the	the	DET
eurjchem-792	6	31	corresponding	correspond	VERB
eurjchem-792	6	32	β‐	β‐	ADJ
eurjchem-792	6	33	hydroxy	hydroxy	NOUN
eurjchem-792	6	34	bezimidazolyl	bezimidazolyl	NOUN
eurjchem-792	6	35	sulfides	sulfide	NOUN
eurjchem-792	6	36	(	(	PUNCT
eurjchem-792	6	37	4a‐e	4a‐e	NOUN
eurjchem-792	6	38	)	)	PUNCT
eurjchem-792	6	39	.	.	PUNCT
eurjchem-792	7	1	further	far	ADV
eurjchem-792	7	2	compounds	compound	VERB
eurjchem-792	7	3	4a‐e	4a‐e	PROPN
eurjchem-792	7	4	on	on	ADP
eurjchem-792	7	5	treatment	treatment	NOUN
eurjchem-792	7	6	with	with	ADP
eurjchem-792	7	7	h2o2	h2o2	NOUN
eurjchem-792	7	8	and	and	CCONJ
eurjchem-792	7	9	ammonium	ammonium	NOUN
eurjchem-792	7	10	molybdate	molybdate	NOUN
eurjchem-792	7	11	in	in	ADP
eurjchem-792	7	12	dichloromethane	dichloromethane	NOUN
eurjchem-792	7	13	yielded	yield	VERB
eurjchem-792	7	14	the	the	DET
eurjchem-792	7	15	β‐hydroxy	β‐hydroxy	PUNCT
eurjchem-792	7	16	bezimidazolyl	bezimidazolyl	ADJ
eurjchem-792	7	17	sulfones	sulfone	NOUN
eurjchem-792	7	18	,	,	PUNCT
eurjchem-792	7	19	5a‐	5a‐	NUM
eurjchem-792	7	20	e.	e.	PROPN
eurjchem-792	7	21	the	the	DET
eurjchem-792	7	22	antimicrobial	antimicrobial	ADJ
eurjchem-792	7	23	activity	activity	NOUN
eurjchem-792	7	24	of	of	ADP
eurjchem-792	7	25	newly	newly	ADV
eurjchem-792	7	26	synthesized	synthesize	VERB
eurjchem-792	7	27	compounds	compound	NOUN
eurjchem-792	7	28	along	along	ADP
eurjchem-792	7	29	with	with	ADP
eurjchem-792	7	30	levofloxacin	levofloxacin	PROPN
eurjchem-792	7	31	(	(	PUNCT
eurjchem-792	7	32	reference	reference	NOUN
eurjchem-792	7	33	drug	drug	NOUN
eurjchem-792	7	34	)	)	PUNCT
eurjchem-792	7	35	were	be	AUX
eurjchem-792	7	36	evaluated	evaluate	VERB
eurjchem-792	7	37	against	against	ADP
eurjchem-792	7	38	different	different	ADJ
eurjchem-792	7	39	microorganisms	microorganism	NOUN
eurjchem-792	7	40	and	and	CCONJ
eurjchem-792	7	41	found	find	VERB
eurjchem-792	7	42	many	many	ADJ
eurjchem-792	7	43	of	of	ADP
eurjchem-792	7	44	the	the	DET
eurjchem-792	7	45	evaluated	evaluate	VERB
eurjchem-792	7	46	compounds	compound	NOUN
eurjchem-792	7	47	have	have	AUX
eurjchem-792	7	48	been	be	AUX
eurjchem-792	7	49	exhibited	exhibit	VERB
eurjchem-792	7	50	remarkable	remarkable	ADJ
eurjchem-792	7	51	activity	activity	NOUN
eurjchem-792	7	52	.	.	PUNCT
eurjchem-792	8	1	levofloxacin	levofloxacin	PROPN
eurjchem-792	8	2	epichlorohydrine	epichlorohydrine	PROPN
eurjchem-792	8	3	antimicrobial	antimicrobial	ADJ
eurjchem-792	8	4	activity	activity	NOUN
eurjchem-792	8	5	ammonium	ammonium	NOUN
eurjchem-792	8	6	molybdate	molybdate	NOUN
eurjchem-792	8	7	β‐hydroxy	β‐hydroxy	PUNCT
eurjchem-792	8	8	benzimidazolyl	benzimidazolyl	ADJ
eurjchem-792	8	9	sulfones	sulfone	NOUN
eurjchem-792	8	10	chiral	chiral	ADJ
eurjchem-792	8	11	benzoxazole	benzoxazole	NOUN
eurjchem-792	8	12	fluoroquinolones	fluoroquinolone	NOUN
eurjchem-792	8	13	1	1	NUM
eurjchem-792	8	14	.	.	PUNCT
eurjchem-792	9	1	introduction	introduction	NOUN
eurjchem-792	9	2	fluoroquinolones	fluoroquinolone	NOUN
eurjchem-792	9	3	are	be	AUX
eurjchem-792	9	4	compounds	compound	NOUN
eurjchem-792	9	5	which	which	PRON
eurjchem-792	9	6	posses	posse	VERB
eurjchem-792	9	7	a	a	DET
eurjchem-792	9	8	wide	wide	ADJ
eurjchem-792	9	9	variety	variety	NOUN
eurjchem-792	9	10	of	of	ADP
eurjchem-792	9	11	therapeutically	therapeutically	ADV
eurjchem-792	9	12	interesting	interesting	ADJ
eurjchem-792	9	13	antibacterial	antibacterial	ADJ
eurjchem-792	9	14	activity	activity	NOUN
eurjchem-792	9	15	against	against	ADP
eurjchem-792	9	16	various	various	ADJ
eurjchem-792	9	17	gram‐positive	gram‐positive	ADJ
eurjchem-792	9	18	and	and	CCONJ
eurjchem-792	9	19	gram‐negative	gram‐negative	ADJ
eurjchem-792	9	20	bacteria	bacteria	NOUN
eurjchem-792	10	1	[	[	X
eurjchem-792	10	2	1,2	1,2	NUM
eurjchem-792	10	3	]	]	PUNCT
eurjchem-792	10	4	.	.	PUNCT
eurjchem-792	11	1	the	the	DET
eurjchem-792	11	2	board	board	NOUN
eurjchem-792	11	3	spectrum	spectrum	NOUN
eurjchem-792	11	4	of	of	ADP
eurjchem-792	11	5	antibiotic	antibiotic	ADJ
eurjchem-792	11	6	activity	activity	NOUN
eurjchem-792	11	7	of	of	ADP
eurjchem-792	11	8	these	these	DET
eurjchem-792	11	9	compounds	compound	NOUN
eurjchem-792	11	10	is	be	AUX
eurjchem-792	11	11	mainly	mainly	ADV
eurjchem-792	11	12	due	due	ADJ
eurjchem-792	11	13	to	to	ADP
eurjchem-792	11	14	the	the	DET
eurjchem-792	11	15	presence	presence	NOUN
eurjchem-792	11	16	of	of	ADP
eurjchem-792	11	17	a	a	DET
eurjchem-792	11	18	fluorine	fluorine	NOUN
eurjchem-792	11	19	atom	atom	NOUN
eurjchem-792	11	20	at	at	ADP
eurjchem-792	11	21	position	position	NOUN
eurjchem-792	11	22	c‐6	c‐6	NOUN
eurjchem-792	11	23	,	,	PUNCT
eurjchem-792	11	24	chemical	chemical	NOUN
eurjchem-792	11	25	modification	modification	NOUN
eurjchem-792	11	26	at	at	ADP
eurjchem-792	11	27	position	position	NOUN
eurjchem-792	11	28	c‐7	c‐7	NOUN
eurjchem-792	11	29	(	(	PUNCT
eurjchem-792	11	30	piperazine	piperazine	ADJ
eurjchem-792	11	31	moiety	moiety	NOUN
eurjchem-792	11	32	)	)	PUNCT
eurjchem-792	11	33	of	of	ADP
eurjchem-792	11	34	fluroquinolones	fluroquinolone	NOUN
eurjchem-792	11	35	ring	ring	NOUN
eurjchem-792	11	36	system	system	NOUN
eurjchem-792	11	37	[	[	X
eurjchem-792	11	38	3‐6	3‐6	NUM
eurjchem-792	11	39	]	]	PUNCT
eurjchem-792	11	40	.	.	PUNCT
eurjchem-792	12	1	literature	literature	NOUN
eurjchem-792	12	2	survey	survey	NOUN
eurjchem-792	12	3	and	and	CCONJ
eurjchem-792	12	4	structure	structure	NOUN
eurjchem-792	12	5	activity	activity	NOUN
eurjchem-792	12	6	relationship	relationship	NOUN
eurjchem-792	12	7	(	(	PUNCT
eurjchem-792	12	8	sar	sar	PROPN
eurjchem-792	12	9	)	)	PUNCT
eurjchem-792	12	10	analysis	analysis	NOUN
eurjchem-792	12	11	reveals	reveal	VERB
eurjchem-792	12	12	that	that	SCONJ
eurjchem-792	12	13	the	the	DET
eurjchem-792	12	14	substitution	substitution	NOUN
eurjchem-792	12	15	/	/	SYM
eurjchem-792	12	16	modifications	modification	NOUN
eurjchem-792	12	17	at	at	ADP
eurjchem-792	12	18	c‐7	c‐7	NOUN
eurjchem-792	12	19	position	position	NOUN
eurjchem-792	12	20	of	of	ADP
eurjchem-792	12	21	fluro‐	fluro‐	NOUN
eurjchem-792	12	22	quinolones	quinolone	NOUN
eurjchem-792	12	23	nucleus	nucleus	ADJ
eurjchem-792	12	24	lead	lead	VERB
eurjchem-792	12	25	to	to	ADP
eurjchem-792	12	26	the	the	DET
eurjchem-792	12	27	synthesis	synthesis	NOUN
eurjchem-792	12	28	of	of	ADP
eurjchem-792	12	29	new	new	ADJ
eurjchem-792	12	30	and	and	CCONJ
eurjchem-792	12	31	improved	improved	ADJ
eurjchem-792	12	32	fluoroquinolones	fluoroquinolone	NOUN
eurjchem-792	12	33	antibacterials	antibacterial	NOUN
eurjchem-792	12	34	[	[	X
eurjchem-792	12	35	7,8	7,8	NUM
eurjchem-792	12	36	]	]	PUNCT
eurjchem-792	12	37	with	with	ADP
eurjchem-792	12	38	enhanced	enhanced	ADJ
eurjchem-792	12	39	activity	activity	NOUN
eurjchem-792	12	40	similar	similar	ADJ
eurjchem-792	12	41	to	to	ADP
eurjchem-792	12	42	antibiotics	antibiotic	NOUN
eurjchem-792	12	43	like	like	ADP
eurjchem-792	12	44	levofloxacin	levofloxacin	NOUN
eurjchem-792	12	45	,	,	PUNCT
eurjchem-792	12	46	moxifloxacin	moxifloxacin	NUM
eurjchem-792	12	47	,	,	PUNCT
eurjchem-792	12	48	ciprofloxacin	ciprofloxacin	NOUN
eurjchem-792	12	49	,	,	PUNCT
eurjchem-792	12	50	ofloxacin	ofloxacin	NOUN
eurjchem-792	12	51	and	and	CCONJ
eurjchem-792	12	52	enrofloxacin	enrofloxacin	PROPN
eurjchem-792	12	53	(	(	PUNCT
eurjchem-792	12	54	figure	figure	NOUN
eurjchem-792	12	55	1	1	NUM
eurjchem-792	12	56	)	)	PUNCT
eurjchem-792	12	57	.	.	PUNCT
eurjchem-792	13	1	fluoro‐	fluoro‐	NOUN
eurjchem-792	13	2	quinolones	quinolone	NOUN
eurjchem-792	13	3	impair	impair	VERB
eurjchem-792	13	4	dna	dna	PROPN
eurjchem-792	13	5	gyrase	gyrase	NOUN
eurjchem-792	13	6	,	,	PUNCT
eurjchem-792	13	7	type	type	NOUN
eurjchem-792	13	8	iv	iv	NUM
eurjchem-792	13	9	topoisomerase	topoisomerase	ADJ
eurjchem-792	13	10	enzymes	enzyme	NOUN
eurjchem-792	13	11	and	and	CCONJ
eurjchem-792	13	12	inhibit	inhibit	VERB
eurjchem-792	13	13	the	the	DET
eurjchem-792	13	14	dna	dna	PROPN
eurjchem-792	13	15	replication	replication	NOUN
eurjchem-792	13	16	[	[	X
eurjchem-792	13	17	9,10	9,10	NUM
eurjchem-792	13	18	]	]	X
eurjchem-792	13	19	.	.	PUNCT
eurjchem-792	14	1	the	the	DET
eurjchem-792	14	2	main	main	ADJ
eurjchem-792	14	3	objective	objective	NOUN
eurjchem-792	14	4	in	in	ADP
eurjchem-792	14	5	fluroquinolone	fluroquinolone	NOUN
eurjchem-792	14	6	research	research	NOUN
eurjchem-792	14	7	include	include	VERB
eurjchem-792	14	8	improving	improve	VERB
eurjchem-792	14	9	the	the	DET
eurjchem-792	14	10	potency	potency	NOUN
eurjchem-792	14	11	and	and	CCONJ
eurjchem-792	14	12	activity	activity	NOUN
eurjchem-792	14	13	against	against	ADP
eurjchem-792	14	14	resistant	resistant	ADJ
eurjchem-792	14	15	microorganisms	microorganism	NOUN
eurjchem-792	14	16	[	[	X
eurjchem-792	14	17	11,12	11,12	NUM
eurjchem-792	14	18	]	]	PUNCT
eurjchem-792	14	19	.	.	PUNCT
eurjchem-792	15	1	mercaptobenzimidazoles	mercaptobenzimidazole	NOUN
eurjchem-792	15	2	and	and	CCONJ
eurjchem-792	15	3	its	its	PRON
eurjchem-792	15	4	derivatives	derivative	NOUN
eurjchem-792	15	5	are	be	AUX
eurjchem-792	15	6	heterocyclic	heterocyclic	ADJ
eurjchem-792	15	7	compounds	compound	NOUN
eurjchem-792	15	8	that	that	PRON
eurjchem-792	15	9	exhibit	exhibit	VERB
eurjchem-792	15	10	a	a	DET
eurjchem-792	15	11	wide	wide	ADJ
eurjchem-792	15	12	range	range	NOUN
eurjchem-792	15	13	of	of	ADP
eurjchem-792	15	14	medicinal	medicinal	ADJ
eurjchem-792	15	15	uses	use	NOUN
eurjchem-792	15	16	such	such	ADJ
eurjchem-792	15	17	as	as	ADP
eurjchem-792	15	18	anti‐cancer	anti‐cancer	NOUN
eurjchem-792	15	19	[	[	X
eurjchem-792	15	20	13	13	NUM
eurjchem-792	15	21	]	]	PUNCT
eurjchem-792	15	22	,	,	PUNCT
eurjchem-792	15	23	anti‐microbial	anti‐microbial	ADJ
eurjchem-792	16	1	[	[	X
eurjchem-792	16	2	14	14	NUM
eurjchem-792	16	3	]	]	PUNCT
eurjchem-792	16	4	,	,	PUNCT
eurjchem-792	16	5	anti‐viral	anti‐viral	ADJ
eurjchem-792	17	1	[	[	X
eurjchem-792	17	2	15	15	NUM
eurjchem-792	17	3	]	]	PUNCT
eurjchem-792	17	4	and	and	CCONJ
eurjchem-792	17	5	anti‐fungal	anti‐fungal	ADJ
eurjchem-792	17	6	[	[	X
eurjchem-792	17	7	16	16	NUM
eurjchem-792	17	8	]	]	PUNCT
eurjchem-792	17	9	activity	activity	NOUN
eurjchem-792	17	10	.	.	PUNCT
eurjchem-792	18	1	these	these	PRON
eurjchem-792	18	2	also	also	ADV
eurjchem-792	18	3	been	be	AUX
eurjchem-792	18	4	found	find	VERB
eurjchem-792	18	5	to	to	PART
eurjchem-792	18	6	be	be	AUX
eurjchem-792	18	7	an	an	DET
eurjchem-792	18	8	integral	integral	ADJ
eurjchem-792	18	9	part	part	NOUN
eurjchem-792	18	10	of	of	ADP
eurjchem-792	18	11	vitamin	vitamin	NOUN
eurjchem-792	18	12	b12	b12	NOUN
eurjchem-792	18	13	[	[	X
eurjchem-792	18	14	17	17	NUM
eurjchem-792	18	15	]	]	PUNCT
eurjchem-792	18	16	in	in	ADP
eurjchem-792	18	17	the	the	DET
eurjchem-792	18	18	form	form	NOUN
eurjchem-792	18	19	of	of	ADP
eurjchem-792	18	20	5,6‐dimethyl‐	5,6‐dimethyl‐	ADJ
eurjchem-792	18	21	1‐(α‐d‐ribofuranosyl	1‐(α‐d‐ribofuranosyl	NUM
eurjchem-792	18	22	)	)	PUNCT
eurjchem-792	18	23	benzimidazole	benzimidazole	NOUN
eurjchem-792	18	24	.	.	PUNCT
eurjchem-792	19	1	the	the	DET
eurjchem-792	19	2	medicinal	medicinal	ADJ
eurjchem-792	19	3	impor‐	impor‐	NOUN
eurjchem-792	19	4	tances	tance	NOUN
eurjchem-792	19	5	of	of	ADP
eurjchem-792	19	6	both	both	DET
eurjchem-792	19	7	7‐piperazine	7‐piperazine	NUM
eurjchem-792	19	8	fluoroquinolones	fluoroquinolone	NOUN
eurjchem-792	19	9	and	and	CCONJ
eurjchem-792	19	10	substituted	substitute	VERB
eurjchem-792	19	11	mercaptobenzimidazoles	mercaptobenzimidazole	NOUN
eurjchem-792	19	12	have	have	AUX
eurjchem-792	19	13	prompted	prompt	VERB
eurjchem-792	19	14	us	we	PRON
eurjchem-792	19	15	to	to	PART
eurjchem-792	19	16	synthesize	synthesize	VERB
eurjchem-792	19	17	a	a	DET
eurjchem-792	19	18	series	series	NOUN
eurjchem-792	19	19	of	of	ADP
eurjchem-792	19	20	novel	novel	NOUN
eurjchem-792	19	21	β‐hydroxy	β‐hydroxy	PUNCT
eurjchem-792	19	22	benzimidazolyl	benzimidazolyl	ADJ
eurjchem-792	19	23	sulfides	sulfide	NOUN
eurjchem-792	19	24	.	.	PUNCT
eurjchem-792	20	1	further	far	ADV
eurjchem-792	20	2	on	on	ADP
eurjchem-792	20	3	selective	selective	ADJ
eurjchem-792	20	4	oxidation	oxidation	NOUN
eurjchem-792	20	5	using	use	VERB
eurjchem-792	20	6	ammonium	ammonium	NOUN
eurjchem-792	20	7	molybdate	molybdate	NOUN
eurjchem-792	20	8	dissolved	dissolve	VERB
eurjchem-792	20	9	in	in	ADP
eurjchem-792	20	10	h2o2	h2o2	NOUN
eurjchem-792	20	11	[	[	X
eurjchem-792	20	12	18	18	NUM
eurjchem-792	20	13	]	]	PUNCT
eurjchem-792	20	14	,	,	PUNCT
eurjchem-792	20	15	yielded	yield	VERB
eurjchem-792	20	16	novel	novel	NOUN
eurjchem-792	20	17	β‐hydroxy	β‐hydroxy	PUNCT
eurjchem-792	20	18	benzimidazolyl	benzimidazolyl	ADJ
eurjchem-792	20	19	sulfones	sulfone	NOUN
eurjchem-792	20	20	containing	contain	VERB
eurjchem-792	20	21	7‐piperazine	7‐piperazine	NUM
eurjchem-792	20	22	fluroquinolones	fluroquinolone	NOUN
eurjchem-792	20	23	.	.	PUNCT
eurjchem-792	21	1	in	in	ADP
eurjchem-792	21	2	view	view	NOUN
eurjchem-792	21	3	of	of	ADP
eurjchem-792	21	4	these	these	DET
eurjchem-792	21	5	reports	report	NOUN
eurjchem-792	21	6	,	,	PUNCT
eurjchem-792	21	7	it	it	PRON
eurjchem-792	21	8	was	be	AUX
eurjchem-792	21	9	thought	think	VERB
eurjchem-792	21	10	worthwhile	worthwhile	ADJ
eurjchem-792	21	11	to	to	PART
eurjchem-792	21	12	synthesize	synthesize	VERB
eurjchem-792	21	13	and	and	CCONJ
eurjchem-792	21	14	investigate	investigate	VERB
eurjchem-792	21	15	the	the	DET
eurjchem-792	21	16	novel	novel	ADJ
eurjchem-792	21	17	7‐piperazinyl	7‐piperazinyl	NUM
eurjchem-792	21	18	fluoro‐	fluoro‐	NOUN
eurjchem-792	21	19	quinolones	quinolone	NOUN
eurjchem-792	21	20	.	.	PUNCT
eurjchem-792	22	1	present	present	ADJ
eurjchem-792	22	2	work	work	NOUN
eurjchem-792	22	3	is	be	AUX
eurjchem-792	22	4	concerned	concern	VERB
eurjchem-792	22	5	with	with	ADP
eurjchem-792	22	6	the	the	DET
eurjchem-792	22	7	synthesis	synthesis	NOUN
eurjchem-792	22	8	of	of	ADP
eurjchem-792	22	9	mercaptobenzimidazolyl	mercaptobenzimidazolyl	NOUN
eurjchem-792	22	10	substituted	substitute	VERB
eurjchem-792	22	11	7‐piperazine	7‐piperazine	PROPN
eurjchem-792	22	12	fluoro‐	fluoro‐	NOUN
eurjchem-792	22	13	quinolones	quinolone	NOUN
eurjchem-792	22	14	having	have	VERB
eurjchem-792	22	15	the	the	DET
eurjchem-792	22	16	objective	objective	NOUN
eurjchem-792	22	17	of	of	ADP
eurjchem-792	22	18	discovering	discover	VERB
eurjchem-792	22	19	novel	novel	ADJ
eurjchem-792	22	20	antimicrobial	antimicrobial	ADJ
eurjchem-792	22	21	agents	agent	NOUN
eurjchem-792	22	22	.	.	PUNCT
eurjchem-792	23	1	figure	figure	NOUN
eurjchem-792	23	2	1	1	NUM
eurjchem-792	23	3	.	.	PUNCT
eurjchem-792	24	1	fluroquinolone	fluroquinolone	ADJ
eurjchem-792	24	2	antibacterial	antibacterial	ADJ
eurjchem-792	24	3	agents	agent	NOUN
eurjchem-792	24	4	.	.	PUNCT
eurjchem-792	25	1	330	330	NUM
eurjchem-792	25	2	guruswamy	guruswamy	NOUN
eurjchem-792	25	3	et	et	PROPN
eurjchem-792	25	4	al	al	PROPN
eurjchem-792	25	5	.	.	PUNCT
eurjchem-792	25	6	/	/	SYM
eurjchem-792	25	7	european	european	PROPN
eurjchem-792	25	8	journal	journal	PROPN
eurjchem-792	25	9	of	of	ADP
eurjchem-792	25	10	chemistry	chemistry	NOUN
eurjchem-792	25	11	4	4	NUM
eurjchem-792	25	12	(	(	PUNCT
eurjchem-792	25	13	4	4	NUM
eurjchem-792	25	14	)	)	PUNCT
eurjchem-792	25	15	(	(	PUNCT
eurjchem-792	25	16	2013	2013	NUM
eurjchem-792	25	17	)	)	PUNCT
eurjchem-792	25	18	329‐335	329‐335	PROPN
eurjchem-792	25	19	scheme	scheme	NOUN
eurjchem-792	25	20	1	1	NUM
eurjchem-792	25	21	2	2	NUM
eurjchem-792	25	22	.	.	PUNCT
eurjchem-792	25	23	experimental	experimental	ADJ
eurjchem-792	25	24	2.1	2.1	NUM
eurjchem-792	25	25	.	.	PUNCT
eurjchem-792	26	1	instrumentation	instrumentation	NOUN
eurjchem-792	26	2	all	all	DET
eurjchem-792	26	3	the	the	DET
eurjchem-792	26	4	reagents	reagent	NOUN
eurjchem-792	26	5	and	and	CCONJ
eurjchem-792	26	6	solvents	solvent	NOUN
eurjchem-792	26	7	were	be	AUX
eurjchem-792	26	8	used	use	VERB
eurjchem-792	26	9	analytical	analytical	ADJ
eurjchem-792	26	10	grade	grade	NOUN
eurjchem-792	26	11	and	and	CCONJ
eurjchem-792	26	12	without	without	ADP
eurjchem-792	26	13	further	further	ADJ
eurjchem-792	26	14	purification	purification	NOUN
eurjchem-792	26	15	unless	unless	SCONJ
eurjchem-792	26	16	otherwise	otherwise	ADV
eurjchem-792	26	17	mentioned	mention	VERB
eurjchem-792	26	18	.	.	PUNCT
eurjchem-792	27	1	thin	thin	ADJ
eurjchem-792	27	2	layer	layer	NOUN
eurjchem-792	27	3	chromatography	chromatography	NOUN
eurjchem-792	27	4	(	(	PUNCT
eurjchem-792	27	5	tlc	tlc	NOUN
eurjchem-792	27	6	)	)	PUNCT
eurjchem-792	27	7	was	be	AUX
eurjchem-792	27	8	carried	carry	VERB
eurjchem-792	27	9	out	out	ADP
eurjchem-792	27	10	on	on	ADP
eurjchem-792	27	11	aluminium	aluminium	NOUN
eurjchem-792	27	12	sheets	sheet	NOUN
eurjchem-792	27	13	coated	coat	VERB
eurjchem-792	27	14	with	with	ADP
eurjchem-792	27	15	silica	silica	NOUN
eurjchem-792	27	16	gel	gel	NOUN
eurjchem-792	27	17	60	60	NUM
eurjchem-792	27	18	f254	f254	PROPN
eurjchem-792	27	19	(	(	PUNCT
eurjchem-792	27	20	merck	merck	PROPN
eurjchem-792	27	21	)	)	PUNCT
eurjchem-792	27	22	.	.	PUNCT
eurjchem-792	28	1	tlc	tlc	NOUN
eurjchem-792	28	2	plates	plate	NOUN
eurjchem-792	28	3	were	be	AUX
eurjchem-792	28	4	inspected	inspect	VERB
eurjchem-792	28	5	under	under	ADP
eurjchem-792	28	6	uv	uv	NOUN
eurjchem-792	28	7	light	light	NOUN
eurjchem-792	28	8	.	.	PUNCT
eurjchem-792	29	1	elemental	elemental	ADJ
eurjchem-792	29	2	analyses	analysis	NOUN
eurjchem-792	29	3	data	datum	NOUN
eurjchem-792	29	4	were	be	AUX
eurjchem-792	29	5	obtained	obtain	VERB
eurjchem-792	29	6	by	by	ADP
eurjchem-792	29	7	employing	employ	VERB
eurjchem-792	29	8	a	a	DET
eurjchem-792	29	9	perkin‐elmer	perkin‐elmer	PROPN
eurjchem-792	29	10	240c	240c	PROPN
eurjchem-792	29	11	analyzer	analyzer	NOUN
eurjchem-792	29	12	.	.	PUNCT
eurjchem-792	30	1	ir	ir	PROPN
eurjchem-792	30	2	spectra	spectra	PROPN
eurjchem-792	30	3	(	(	PUNCT
eurjchem-792	30	4	kbr	kbr	PROPN
eurjchem-792	30	5	pellets	pellet	NOUN
eurjchem-792	30	6	)	)	PUNCT
eurjchem-792	30	7	were	be	AUX
eurjchem-792	30	8	recorded	record	VERB
eurjchem-792	30	9	with	with	ADP
eurjchem-792	30	10	a	a	DET
eurjchem-792	30	11	perkin‐elmer‐1700	perkin‐elmer‐1700	NUM
eurjchem-792	30	12	spectro	spectro	PROPN
eurjchem-792	30	13	photo	photo	NOUN
eurjchem-792	30	14	meter	meter	NOUN
eurjchem-792	30	15	.	.	PUNCT
eurjchem-792	31	1	1h	1h	NUM
eurjchem-792	31	2	nmr	nmr	NOUN
eurjchem-792	31	3	and	and	CCONJ
eurjchem-792	31	4	13c	13c	NOUN
eurjchem-792	31	5	nmr	nmr	NOUN
eurjchem-792	31	6	spectra	spectra	NOUN
eurjchem-792	31	7	were	be	AUX
eurjchem-792	31	8	measured	measure	VERB
eurjchem-792	31	9	on	on	ADP
eurjchem-792	31	10	avance	avance	PROPN
eurjchem-792	31	11	bruker‐300	bruker‐300	PROPN
eurjchem-792	31	12	mhz	mhz	NOUN
eurjchem-792	31	13	spectrometer	spectrometer	NOUN
eurjchem-792	31	14	.	.	PUNCT
eurjchem-792	32	1	mass	mass	PROPN
eurjchem-792	32	2	spectrum	spectrum	PROPN
eurjchem-792	32	3	was	be	AUX
eurjchem-792	32	4	recorded	record	VERB
eurjchem-792	32	5	on	on	ADP
eurjchem-792	32	6	varian	varian	PROPN
eurjchem-792	32	7	300‐ms	300‐ms	NUM
eurjchem-792	32	8	spectrometer	spectrometer	NOUN
eurjchem-792	32	9	and	and	CCONJ
eurjchem-792	32	10	melting	melting	NOUN
eurjchem-792	32	11	points	point	NOUN
eurjchem-792	32	12	were	be	AUX
eurjchem-792	32	13	recorded	record	VERB
eurjchem-792	32	14	on	on	ADP
eurjchem-792	32	15	a	a	DET
eurjchem-792	32	16	polmon	polmon	ADJ
eurjchem-792	32	17	mp96	mp96	PROPN
eurjchem-792	32	18	.	.	PUNCT
eurjchem-792	33	1	specific	specific	ADJ
eurjchem-792	33	2	optical	optical	ADJ
eurjchem-792	33	3	rotation	rotation	NOUN
eurjchem-792	33	4	performed	perform	VERB
eurjchem-792	33	5	on	on	ADP
eurjchem-792	33	6	rudolf	rudolf	NOUN
eurjchem-792	33	7	model	model	NOUN
eurjchem-792	33	8	number	number	NOUN
eurjchem-792	33	9	420766apr/6w	420766apr/6w	NUM
eurjchem-792	33	10	polarimeter	polarimeter	NOUN
eurjchem-792	33	11	.	.	PUNCT
eurjchem-792	34	1	2.2	2.2	NUM
eurjchem-792	34	2	.	.	PUNCT
eurjchem-792	34	3	synthesis	synthesis	NOUN
eurjchem-792	34	4	2.2.1	2.2.1	NUM
eurjchem-792	34	5	.	.	PUNCT
eurjchem-792	35	1	(	(	PUNCT
eurjchem-792	35	2	s)‐9‐fluoro‐3,7‐dihydro‐3‐methyl‐7‐oxo‐10‐	s)‐9‐fluoro‐3,7‐dihydro‐3‐methyl‐7‐oxo‐10‐	NOUN
eurjchem-792	35	3	(	(	PUNCT
eurjchem-792	35	4	piperazin‐1‐yl)‐2h‐[1,4]oxazino[2,3,4‐ij]quinoline‐6‐	piperazin‐1‐yl)‐2h‐[1,4]oxazino[2,3,4‐ij]quinoline‐6‐	ADJ
eurjchem-792	35	5	carboxylic	carboxylic	ADJ
eurjchem-792	35	6	acid	acid	NOUN
eurjchem-792	35	7	(	(	PUNCT
eurjchem-792	35	8	2	2	NUM
eurjchem-792	35	9	)	)	PUNCT
eurjchem-792	35	10	to	to	ADP
eurjchem-792	35	11	a	a	DET
eurjchem-792	35	12	solution	solution	NOUN
eurjchem-792	35	13	of	of	ADP
eurjchem-792	35	14	compound	compound	NOUN
eurjchem-792	35	15	1	1	NUM
eurjchem-792	35	16	(	(	PUNCT
eurjchem-792	35	17	100.0	100.0	NUM
eurjchem-792	35	18	g	g	NOUN
eurjchem-792	35	19	,	,	PUNCT
eurjchem-792	35	20	356	356	NUM
eurjchem-792	35	21	mmol	mmol	NOUN
eurjchem-792	35	22	)	)	PUNCT
eurjchem-792	35	23	in	in	ADP
eurjchem-792	35	24	acetonitrile	acetonitrile	NOUN
eurjchem-792	35	25	(	(	PUNCT
eurjchem-792	35	26	500	500	NUM
eurjchem-792	35	27	ml	ml	NOUN
eurjchem-792	35	28	)	)	PUNCT
eurjchem-792	35	29	and	and	CCONJ
eurjchem-792	35	30	piperazine	piperazine	NOUN
eurjchem-792	35	31	(	(	PUNCT
eurjchem-792	35	32	45.92	45.92	NUM
eurjchem-792	35	33	g	g	NOUN
eurjchem-792	35	34	,	,	PUNCT
eurjchem-792	35	35	534	534	NUM
eurjchem-792	35	36	mmol	mmol	NOUN
eurjchem-792	35	37	)	)	PUNCT
eurjchem-792	35	38	was	be	AUX
eurjchem-792	35	39	stirred	stir	VERB
eurjchem-792	35	40	for	for	ADP
eurjchem-792	35	41	30	30	NUM
eurjchem-792	35	42	min	min	NOUN
eurjchem-792	35	43	at	at	ADP
eurjchem-792	35	44	25‐30	25‐30	PROPN
eurjchem-792	35	45	°	°	ADP
eurjchem-792	35	46	c	c	NOUN
eurjchem-792	35	47	,	,	PUNCT
eurjchem-792	35	48	added	add	VERB
eurjchem-792	35	49	triethylamine	triethylamine	NOUN
eurjchem-792	35	50	(	(	PUNCT
eurjchem-792	35	51	107.86	107.86	NUM
eurjchem-792	35	52	g	g	NOUN
eurjchem-792	35	53	,	,	PUNCT
eurjchem-792	35	54	1068	1068	NUM
eurjchem-792	35	55	mmol	mmol	NOUN
eurjchem-792	35	56	)	)	PUNCT
eurjchem-792	35	57	and	and	CCONJ
eurjchem-792	35	58	heated	heat	VERB
eurjchem-792	35	59	the	the	DET
eurjchem-792	35	60	reaction	reaction	NOUN
eurjchem-792	35	61	mass	mass	NOUN
eurjchem-792	35	62	to	to	PART
eurjchem-792	35	63	reflux	reflux	VERB
eurjchem-792	35	64	,	,	PUNCT
eurjchem-792	35	65	maintained	maintain	VERB
eurjchem-792	35	66	for	for	ADP
eurjchem-792	35	67	12	12	NUM
eurjchem-792	35	68	h	h	NOUN
eurjchem-792	35	69	,	,	PUNCT
eurjchem-792	35	70	progress	progress	NOUN
eurjchem-792	35	71	of	of	ADP
eurjchem-792	35	72	the	the	DET
eurjchem-792	35	73	reaction	reaction	NOUN
eurjchem-792	35	74	was	be	AUX
eurjchem-792	35	75	monitored	monitor	VERB
eurjchem-792	35	76	by	by	ADP
eurjchem-792	35	77	tlc	tlc	PROPN
eurjchem-792	35	78	.	.	PUNCT
eurjchem-792	36	1	the	the	DET
eurjchem-792	36	2	reaction	reaction	NOUN
eurjchem-792	36	3	mass	mass	NOUN
eurjchem-792	36	4	was	be	AUX
eurjchem-792	36	5	cooled	cool	VERB
eurjchem-792	36	6	to	to	ADP
eurjchem-792	36	7	25‐30	25‐30	NUM
eurjchem-792	36	8	°	°	SYM
eurjchem-792	36	9	c	c	NOUN
eurjchem-792	36	10	,	,	PUNCT
eurjchem-792	36	11	stirred	stir	VERB
eurjchem-792	36	12	for	for	ADP
eurjchem-792	36	13	1	1	NUM
eurjchem-792	36	14	h	h	NOUN
eurjchem-792	36	15	,	,	PUNCT
eurjchem-792	36	16	filtered	filter	VERB
eurjchem-792	36	17	the	the	DET
eurjchem-792	36	18	isolated	isolated	ADJ
eurjchem-792	36	19	compound	compound	NOUN
eurjchem-792	36	20	and	and	CCONJ
eurjchem-792	36	21	washed	wash	VERB
eurjchem-792	36	22	with	with	ADP
eurjchem-792	36	23	acetonitrile	acetonitrile	NOUN
eurjchem-792	36	24	.	.	PUNCT
eurjchem-792	37	1	the	the	DET
eurjchem-792	37	2	crude	crude	ADJ
eurjchem-792	37	3	solid	solid	NOUN
eurjchem-792	37	4	was	be	AUX
eurjchem-792	37	5	recrystallized	recrystallize	VERB
eurjchem-792	37	6	from	from	ADP
eurjchem-792	37	7	methanol	methanol	NOUN
eurjchem-792	37	8	to	to	PART
eurjchem-792	37	9	obtain	obtain	VERB
eurjchem-792	37	10	pure	pure	ADJ
eurjchem-792	37	11	compound	compound	NOUN
eurjchem-792	37	12	2	2	NUM
eurjchem-792	37	13	(	(	PUNCT
eurjchem-792	37	14	scheme	scheme	NOUN
eurjchem-792	37	15	1	1	NUM
eurjchem-792	37	16	)	)	PUNCT
eurjchem-792	37	17	.	.	PUNCT
eurjchem-792	38	1	yield	yield	NOUN
eurjchem-792	38	2	:	:	PUNCT
eurjchem-792	38	3	106.19	106.19	NUM
eurjchem-792	38	4	g	g	NOUN
eurjchem-792	38	5	(	(	PUNCT
eurjchem-792	38	6	86	86	NUM
eurjchem-792	38	7	%	%	NOUN
eurjchem-792	38	8	)	)	PUNCT
eurjchem-792	38	9	.	.	PUNCT
eurjchem-792	39	1	color	color	NOUN
eurjchem-792	39	2	:	:	PUNCT
eurjchem-792	39	3	pale	pale	ADJ
eurjchem-792	39	4	yellow	yellow	ADJ
eurjchem-792	39	5	powder	powder	NOUN
eurjchem-792	39	6	.	.	PUNCT
eurjchem-792	40	1	m.p	m.p	PROPN
eurjchem-792	40	2	.	.	PROPN
eurjchem-792	40	3	:	:	PUNCT
eurjchem-792	41	1	263‐265	263‐265	PROPN
eurjchem-792	41	2	°	°	NUM
eurjchem-792	41	3	c	c	X
eurjchem-792	41	4	.	.	PUNCT
eurjchem-792	42	1	ir	ir	PROPN
eurjchem-792	42	2	(	(	PUNCT
eurjchem-792	42	3	kbr	kbr	PROPN
eurjchem-792	42	4	,	,	PUNCT
eurjchem-792	42	5	v	v	NOUN
eurjchem-792	42	6	,	,	PUNCT
eurjchem-792	42	7	cm‐1	cm‐1	PROPN
eurjchem-792	42	8	):	):	PUNCT
eurjchem-792	42	9	3412	3412	NUM
eurjchem-792	42	10	(	(	PUNCT
eurjchem-792	42	11	nh	nh	NOUN
eurjchem-792	42	12	)	)	PUNCT
eurjchem-792	42	13	,	,	PUNCT
eurjchem-792	42	14	2814	2814	NUM
eurjchem-792	42	15	(	(	PUNCT
eurjchem-792	42	16	ch	ch	NOUN
eurjchem-792	42	17	)	)	PUNCT
eurjchem-792	42	18	,	,	PUNCT
eurjchem-792	42	19	1728	1728	NUM
eurjchem-792	42	20	(	(	PUNCT
eurjchem-792	42	21	c	c	NOUN
eurjchem-792	42	22	=	=	NOUN
eurjchem-792	42	23	o	o	NOUN
eurjchem-792	42	24	)	)	PUNCT
eurjchem-792	42	25	,	,	PUNCT
eurjchem-792	42	26	1617	1617	NUM
eurjchem-792	42	27	(	(	PUNCT
eurjchem-792	42	28	c	c	NOUN
eurjchem-792	42	29	=	=	NOUN
eurjchem-792	42	30	o	o	NOUN
eurjchem-792	42	31	)	)	PUNCT
eurjchem-792	42	32	.	.	PUNCT
eurjchem-792	43	1	1h	1h	NUM
eurjchem-792	43	2	nmr	nmr	NOUN
eurjchem-792	43	3	(	(	PUNCT
eurjchem-792	43	4	300	300	NUM
eurjchem-792	43	5	mhz	mhz	NOUN
eurjchem-792	43	6	,	,	PUNCT
eurjchem-792	43	7	dmso‐	dmso‐	NUM
eurjchem-792	43	8	d6	d6	NOUN
eurjchem-792	43	9	,	,	PUNCT
eurjchem-792	43	10	δ	δ	PROPN
eurjchem-792	43	11	,	,	PUNCT
eurjchem-792	43	12	ppm	ppm	NUM
eurjchem-792	43	13	):	):	PUNCT
eurjchem-792	43	14	1.22‐1.24	1.22‐1.24	NUM
eurjchem-792	43	15	(	(	PUNCT
eurjchem-792	43	16	d	d	PROPN
eurjchem-792	43	17	,	,	PUNCT
eurjchem-792	43	18	3h	3h	NUM
eurjchem-792	43	19	,	,	PUNCT
eurjchem-792	43	20	ch3	ch3	PROPN
eurjchem-792	43	21	,	,	PUNCT
eurjchem-792	43	22	j	j	PROPN
eurjchem-792	44	1	=	=	SYM
eurjchem-792	44	2	6.0	6.0	NUM
eurjchem-792	44	3	hz	hz	NOUN
eurjchem-792	44	4	)	)	PUNCT
eurjchem-792	44	5	,	,	PUNCT
eurjchem-792	44	6	2.48‐2.55	2.48‐2.55	NUM
eurjchem-792	44	7	(	(	PUNCT
eurjchem-792	44	8	m	m	PROPN
eurjchem-792	44	9	,	,	PUNCT
eurjchem-792	44	10	4h	4h	NOUN
eurjchem-792	44	11	,	,	PUNCT
eurjchem-792	44	12	2×ch2	2×ch2	ADJ
eurjchem-792	44	13	)	)	PUNCT
eurjchem-792	44	14	,	,	PUNCT
eurjchem-792	44	15	2.27	2.27	NUM
eurjchem-792	44	16	(	(	PUNCT
eurjchem-792	44	17	s	s	PROPN
eurjchem-792	44	18	,	,	PUNCT
eurjchem-792	44	19	1h	1h	NUM
eurjchem-792	44	20	,	,	PUNCT
eurjchem-792	44	21	nh	nh	PROPN
eurjchem-792	44	22	,	,	PUNCT
eurjchem-792	44	23	d2o	d2o	PROPN
eurjchem-792	44	24	exchangeable	exchangeable	ADJ
eurjchem-792	44	25	)	)	PUNCT
eurjchem-792	44	26	,	,	PUNCT
eurjchem-792	44	27	3.56‐3.62	3.56‐3.62	NUM
eurjchem-792	44	28	(	(	PUNCT
eurjchem-792	44	29	m	m	PROPN
eurjchem-792	44	30	,	,	PUNCT
eurjchem-792	44	31	4h	4h	NOUN
eurjchem-792	44	32	,	,	PUNCT
eurjchem-792	44	33	2×ch2	2×ch2	ADJ
eurjchem-792	44	34	)	)	PUNCT
eurjchem-792	44	35	,	,	PUNCT
eurjchem-792	44	36	3.97‐4.00	3.97‐4.00	NUM
eurjchem-792	44	37	(	(	PUNCT
eurjchem-792	44	38	m	m	PROPN
eurjchem-792	44	39	,	,	PUNCT
eurjchem-792	44	40	1h	1h	NUM
eurjchem-792	44	41	,	,	PUNCT
eurjchem-792	44	42	ch	ch	NOUN
eurjchem-792	44	43	)	)	PUNCT
eurjchem-792	44	44	,	,	PUNCT
eurjchem-792	44	45	4.54‐4.57	4.54‐4.57	NUM
eurjchem-792	44	46	(	(	PUNCT
eurjchem-792	44	47	m	m	PROPN
eurjchem-792	44	48	,	,	PUNCT
eurjchem-792	44	49	2h	2h	NUM
eurjchem-792	44	50	,	,	PUNCT
eurjchem-792	44	51	ch2	ch2	PROPN
eurjchem-792	44	52	)	)	PUNCT
eurjchem-792	44	53	,	,	PUNCT
eurjchem-792	44	54	7.48‐	7.48‐	NUM
eurjchem-792	44	55	7.32	7.32	NUM
eurjchem-792	44	56	(	(	PUNCT
eurjchem-792	44	57	d	d	PROPN
eurjchem-792	44	58	,	,	PUNCT
eurjchem-792	44	59	1h	1h	NUM
eurjchem-792	44	60	,	,	PUNCT
eurjchem-792	44	61	ar‐h	ar‐h	PROPN
eurjchem-792	44	62	,	,	PUNCT
eurjchem-792	44	63	j	j	PROPN
eurjchem-792	44	64	=	=	PROPN
eurjchem-792	44	65	12.0	12.0	NUM
eurjchem-792	44	66	hz	hz	NOUN
eurjchem-792	44	67	)	)	PUNCT
eurjchem-792	44	68	,	,	PUNCT
eurjchem-792	44	69	8.89	8.89	NUM
eurjchem-792	44	70	(	(	PUNCT
eurjchem-792	44	71	s	s	PROPN
eurjchem-792	44	72	,	,	PUNCT
eurjchem-792	44	73	1h	1h	NUM
eurjchem-792	44	74	,	,	PUNCT
eurjchem-792	44	75	c	c	NOUN
eurjchem-792	44	76	=	=	NOUN
eurjchem-792	44	77	ch	ch	NOUN
eurjchem-792	44	78	)	)	PUNCT
eurjchem-792	44	79	,	,	PUNCT
eurjchem-792	44	80	15.17	15.17	NUM
eurjchem-792	44	81	(	(	PUNCT
eurjchem-792	44	82	s	s	PROPN
eurjchem-792	44	83	,	,	PUNCT
eurjchem-792	44	84	1h	1h	NUM
eurjchem-792	44	85	,	,	PUNCT
eurjchem-792	44	86	cooh	cooh	NOUN
eurjchem-792	44	87	,	,	PUNCT
eurjchem-792	44	88	d2o	d2o	PROPN
eurjchem-792	44	89	exchangeable	exchangeable	ADJ
eurjchem-792	44	90	)	)	PUNCT
eurjchem-792	44	91	.	.	PUNCT
eurjchem-792	45	1	13c	13c	NOUN
eurjchem-792	45	2	nmr	nmr	NOUN
eurjchem-792	45	3	(	(	PUNCT
eurjchem-792	45	4	75	75	NUM
eurjchem-792	45	5	mhz	mhz	NOUN
eurjchem-792	45	6	,	,	PUNCT
eurjchem-792	45	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-792	45	8	,	,	PUNCT
eurjchem-792	45	9	δ	δ	PROPN
eurjchem-792	45	10	,	,	PUNCT
eurjchem-792	45	11	ppm	ppm	NUM
eurjchem-792	45	12	):	):	PUNCT
eurjchem-792	45	13	18.39	18.39	NUM
eurjchem-792	45	14	(	(	PUNCT
eurjchem-792	45	15	ch3	ch3	PROPN
eurjchem-792	45	16	)	)	PUNCT
eurjchem-792	45	17	,	,	PUNCT
eurjchem-792	45	18	51.46	51.46	NUM
eurjchem-792	45	19	(	(	PUNCT
eurjchem-792	45	20	2×ch2	2×ch2	ADJ
eurjchem-792	45	21	)	)	PUNCT
eurjchem-792	45	22	,	,	PUNCT
eurjchem-792	45	23	54.32	54.32	NUM
eurjchem-792	45	24	(	(	PUNCT
eurjchem-792	45	25	2×ch2	2×ch2	ADJ
eurjchem-792	45	26	)	)	PUNCT
eurjchem-792	45	27	,	,	PUNCT
eurjchem-792	45	28	58.71	58.71	NUM
eurjchem-792	45	29	(	(	PUNCT
eurjchem-792	45	30	ch	ch	NOUN
eurjchem-792	45	31	)	)	PUNCT
eurjchem-792	45	32	,	,	PUNCT
eurjchem-792	45	33	60.31	60.31	NUM
eurjchem-792	45	34	(	(	PUNCT
eurjchem-792	45	35	ch2	ch2	PROPN
eurjchem-792	45	36	)	)	PUNCT
eurjchem-792	45	37	,	,	PUNCT
eurjchem-792	45	38	103.41	103.41	NUM
eurjchem-792	45	39	(	(	PUNCT
eurjchem-792	45	40	ch	ch	NOUN
eurjchem-792	45	41	)	)	PUNCT
eurjchem-792	45	42	,	,	PUNCT
eurjchem-792	45	43	107.62	107.62	NUM
eurjchem-792	45	44	(	(	PUNCT
eurjchem-792	45	45	c	c	NOUN
eurjchem-792	45	46	)	)	PUNCT
eurjchem-792	45	47	,	,	PUNCT
eurjchem-792	45	48	120.34	120.34	NUM
eurjchem-792	45	49	(	(	PUNCT
eurjchem-792	45	50	c	c	NOUN
eurjchem-792	45	51	)	)	PUNCT
eurjchem-792	45	52	,	,	PUNCT
eurjchem-792	45	53	125.41	125.41	NUM
eurjchem-792	45	54	(	(	PUNCT
eurjchem-792	45	55	c	c	NOUN
eurjchem-792	45	56	)	)	PUNCT
eurjchem-792	45	57	,	,	PUNCT
eurjchem-792	45	58	131.08	131.08	NUM
eurjchem-792	45	59	(	(	PUNCT
eurjchem-792	45	60	c	c	NOUN
eurjchem-792	45	61	)	)	PUNCT
eurjchem-792	45	62	,	,	PUNCT
eurjchem-792	45	63	140.36	140.36	NUM
eurjchem-792	45	64	(	(	PUNCT
eurjchem-792	45	65	c	c	NOUN
eurjchem-792	45	66	)	)	PUNCT
eurjchem-792	45	67	,	,	PUNCT
eurjchem-792	45	68	146.54	146.54	NUM
eurjchem-792	45	69	(	(	PUNCT
eurjchem-792	45	70	c	c	NOUN
eurjchem-792	45	71	)	)	PUNCT
eurjchem-792	45	72	,	,	PUNCT
eurjchem-792	45	73	154.31	154.31	NUM
eurjchem-792	45	74	(	(	PUNCT
eurjchem-792	45	75	c	c	NOUN
eurjchem-792	45	76	)	)	PUNCT
eurjchem-792	45	77	,	,	PUNCT
eurjchem-792	45	78	157.29	157.29	NUM
eurjchem-792	45	79	(	(	PUNCT
eurjchem-792	45	80	ch	ch	NOUN
eurjchem-792	45	81	)	)	PUNCT
eurjchem-792	45	82	,	,	PUNCT
eurjchem-792	45	83	166.82	166.82	NUM
eurjchem-792	45	84	(	(	PUNCT
eurjchem-792	45	85	c	c	NOUN
eurjchem-792	45	86	=	=	NOUN
eurjchem-792	45	87	o	o	NOUN
eurjchem-792	45	88	)	)	PUNCT
eurjchem-792	45	89	,	,	PUNCT
eurjchem-792	45	90	177.09	177.09	NUM
eurjchem-792	45	91	(	(	PUNCT
eurjchem-792	45	92	c	c	NOUN
eurjchem-792	45	93	=	=	NOUN
eurjchem-792	45	94	o	o	NOUN
eurjchem-792	45	95	)	)	PUNCT
eurjchem-792	45	96	.	.	PUNCT
eurjchem-792	46	1	anal	anal	PROPN
eurjchem-792	46	2	.	.	PUNCT
eurjchem-792	46	3	calcd	calcd	NOUN
eurjchem-792	46	4	.	.	PUNCT
eurjchem-792	47	1	for	for	ADP
eurjchem-792	47	2	c17h18fn3o4	c17h18fn3o4	NOUN
eurjchem-792	47	3	:	:	PUNCT
eurjchem-792	47	4	c	c	X
eurjchem-792	47	5	,	,	PUNCT
eurjchem-792	47	6	58.78	58.78	NUM
eurjchem-792	47	7	;	;	PUNCT
eurjchem-792	47	8	h	h	NOUN
eurjchem-792	47	9	,	,	PUNCT
eurjchem-792	47	10	5.22	5.22	NUM
eurjchem-792	47	11	;	;	PUNCT
eurjchem-792	47	12	n	n	CCONJ
eurjchem-792	47	13	,	,	PUNCT
eurjchem-792	47	14	12.10	12.10	NUM
eurjchem-792	47	15	.	.	PUNCT
eurjchem-792	47	16	found	find	VERB
eurjchem-792	47	17	:	:	PUNCT
eurjchem-792	48	1	c	c	X
eurjchem-792	48	2	,	,	PUNCT
eurjchem-792	48	3	58.64	58.64	NUM
eurjchem-792	48	4	;	;	PUNCT
eurjchem-792	49	1	h	h	NOUN
eurjchem-792	49	2	,	,	PUNCT
eurjchem-792	49	3	5.09	5.09	NUM
eurjchem-792	49	4	;	;	PUNCT
eurjchem-792	49	5	n	n	CCONJ
eurjchem-792	49	6	,	,	PUNCT
eurjchem-792	49	7	12.01	12.01	NUM
eurjchem-792	49	8	%	%	NOUN
eurjchem-792	49	9	.	.	PUNCT
eurjchem-792	50	1	ms	ms	NOUN
eurjchem-792	50	2	(	(	PUNCT
eurjchem-792	50	3	m	m	PROPN
eurjchem-792	50	4	/	/	SYM
eurjchem-792	50	5	z	z	NOUN
eurjchem-792	50	6	):	):	PUNCT
eurjchem-792	50	7	348.07	348.07	NUM
eurjchem-792	50	8	(	(	PUNCT
eurjchem-792	50	9	m+	m+	NUM
eurjchem-792	50	10	)	)	PUNCT
eurjchem-792	50	11	.	.	PUNCT
eurjchem-792	51	1	[	[	X
eurjchem-792	51	2	α]d25	α]d25	NOUN
eurjchem-792	51	3	:	:	PUNCT
eurjchem-792	51	4	‐72.41	‐72.41	PROPN
eurjchem-792	51	5	(	(	PUNCT
eurjchem-792	51	6	c	c	NOUN
eurjchem-792	51	7	=	=	SYM
eurjchem-792	51	8	1.0	1.0	NUM
eurjchem-792	51	9	in	in	ADP
eurjchem-792	51	10	methanol	methanol	NOUN
eurjchem-792	51	11	:	:	PUNCT
eurjchem-792	51	12	methylene	methylene	NOUN
eurjchem-792	51	13	chloride	chloride	NOUN
eurjchem-792	51	14	,	,	PUNCT
eurjchem-792	51	15	1:1	1:1	NUM
eurjchem-792	51	16	)	)	PUNCT
eurjchem-792	51	17	.	.	PUNCT
eurjchem-792	52	1	2.2.2	2.2.2	X
eurjchem-792	52	2	.	.	PUNCT
eurjchem-792	53	1	(	(	PUNCT
eurjchem-792	53	2	s)‐9‐fluoro‐3,7‐dihydro‐3‐methyl‐10‐(4‐((oxiran‐2‐yl	s)‐9‐fluoro‐3,7‐dihydro‐3‐methyl‐10‐(4‐((oxiran‐2‐yl	PROPN
eurjchem-792	53	3	)	)	PUNCT
eurjchem-792	53	4	methyl)piperazin‐1‐yl)‐7‐oxo‐2h‐[1,4]oxazino[2,3,4‐ij	methyl)piperazin‐1‐yl)‐7‐oxo‐2h‐[1,4]oxazino[2,3,4‐ij	PROPN
eurjchem-792	53	5	]	]	PUNCT
eurjchem-792	53	6	quinoline‐6‐carboxylic	quinoline‐6‐carboxylic	PROPN
eurjchem-792	53	7	acid	acid	NOUN
eurjchem-792	53	8	(	(	PUNCT
eurjchem-792	53	9	3	3	NUM
eurjchem-792	53	10	)	)	PUNCT
eurjchem-792	53	11	to	to	ADP
eurjchem-792	53	12	a	a	DET
eurjchem-792	53	13	solution	solution	NOUN
eurjchem-792	53	14	of	of	ADP
eurjchem-792	53	15	compound	compound	NOUN
eurjchem-792	53	16	2	2	NUM
eurjchem-792	53	17	(	(	PUNCT
eurjchem-792	53	18	50.0	50.0	NUM
eurjchem-792	53	19	g	g	NOUN
eurjchem-792	53	20	,	,	PUNCT
eurjchem-792	53	21	123	123	NUM
eurjchem-792	53	22	mmol	mmol	NOUN
eurjchem-792	53	23	)	)	PUNCT
eurjchem-792	53	24	in	in	ADP
eurjchem-792	53	25	acetone	acetone	NOUN
eurjchem-792	53	26	(	(	PUNCT
eurjchem-792	53	27	250	250	NUM
eurjchem-792	53	28	ml	ml	NOUN
eurjchem-792	53	29	)	)	PUNCT
eurjchem-792	53	30	,	,	PUNCT
eurjchem-792	53	31	added	add	VERB
eurjchem-792	53	32	naoh	naoh	NOUN
eurjchem-792	53	33	(	(	PUNCT
eurjchem-792	53	34	12.3	12.3	NUM
eurjchem-792	53	35	g	g	NOUN
eurjchem-792	53	36	,	,	PUNCT
eurjchem-792	53	37	307	307	NUM
eurjchem-792	53	38	mmol	mmol	NOUN
eurjchem-792	53	39	)	)	PUNCT
eurjchem-792	53	40	followed	follow	VERB
eurjchem-792	53	41	by	by	ADP
eurjchem-792	53	42	epichlorohydrine	epichlorohydrine	PROPN
eurjchem-792	53	43	(	(	PUNCT
eurjchem-792	53	44	22.75	22.75	NUM
eurjchem-792	53	45	g	g	NOUN
eurjchem-792	53	46	,	,	PUNCT
eurjchem-792	53	47	0.246	0.246	NUM
eurjchem-792	53	48	mmol	mmol	NOUN
eurjchem-792	53	49	)	)	PUNCT
eurjchem-792	53	50	and	and	CCONJ
eurjchem-792	53	51	the	the	DET
eurjchem-792	53	52	reaction	reaction	NOUN
eurjchem-792	53	53	mixture	mixture	NOUN
eurjchem-792	53	54	was	be	AUX
eurjchem-792	53	55	maintained	maintain	VERB
eurjchem-792	53	56	for	for	ADP
eurjchem-792	53	57	4	4	NUM
eurjchem-792	53	58	h	h	NOUN
eurjchem-792	53	59	at	at	ADP
eurjchem-792	53	60	40‐45	40‐45	NUM
eurjchem-792	53	61	°	°	ADP
eurjchem-792	53	62	c	c	PROPN
eurjchem-792	53	63	,	,	PUNCT
eurjchem-792	53	64	at	at	ADP
eurjchem-792	53	65	the	the	DET
eurjchem-792	53	66	end	end	NOUN
eurjchem-792	53	67	of	of	ADP
eurjchem-792	53	68	this	this	DET
eurjchem-792	53	69	period	period	NOUN
eurjchem-792	53	70	,	,	PUNCT
eurjchem-792	53	71	the	the	DET
eurjchem-792	53	72	reaction	reaction	NOUN
eurjchem-792	53	73	mixture	mixture	NOUN
eurjchem-792	53	74	was	be	AUX
eurjchem-792	53	75	cooled	cool	VERB
eurjchem-792	53	76	to	to	ADP
eurjchem-792	53	77	25‐30	25‐30	NUM
eurjchem-792	53	78	°	°	ADP
eurjchem-792	53	79	c	c	NOUN
eurjchem-792	53	80	and	and	CCONJ
eurjchem-792	53	81	solvent	solvent	NOUN
eurjchem-792	53	82	was	be	AUX
eurjchem-792	53	83	distilled	distil	VERB
eurjchem-792	53	84	off	off	ADP
eurjchem-792	53	85	under	under	ADP
eurjchem-792	53	86	vacuum	vacuum	NOUN
eurjchem-792	53	87	.	.	PUNCT
eurjchem-792	54	1	the	the	DET
eurjchem-792	54	2	residue	residue	NOUN
eurjchem-792	54	3	was	be	AUX
eurjchem-792	54	4	dissolved	dissolve	VERB
eurjchem-792	54	5	in	in	ADP
eurjchem-792	54	6	water	water	NOUN
eurjchem-792	54	7	(	(	PUNCT
eurjchem-792	54	8	50.0	50.0	NUM
eurjchem-792	54	9	ml	ml	NOUN
eurjchem-792	54	10	)	)	PUNCT
eurjchem-792	54	11	and	and	CCONJ
eurjchem-792	54	12	adjusted	adjust	VERB
eurjchem-792	54	13	the	the	DET
eurjchem-792	54	14	ph	ph	NOUN
eurjchem-792	54	15	=	=	SYM
eurjchem-792	54	16	6.0‐7.0	6.0‐7.0	NUM
eurjchem-792	54	17	with	with	ADP
eurjchem-792	54	18	dil	dil	PROPN
eurjchem-792	54	19	.	.	PUNCT
eurjchem-792	55	1	hcl	hcl	PROPN
eurjchem-792	55	2	.	.	PUNCT
eurjchem-792	56	1	the	the	DET
eurjchem-792	56	2	separated	separate	VERB
eurjchem-792	56	3	solid	solid	ADJ
eurjchem-792	56	4	was	be	AUX
eurjchem-792	56	5	filtered	filter	VERB
eurjchem-792	56	6	,	,	PUNCT
eurjchem-792	56	7	washed	wash	VERB
eurjchem-792	56	8	with	with	ADP
eurjchem-792	56	9	water	water	NOUN
eurjchem-792	56	10	and	and	CCONJ
eurjchem-792	56	11	dried	dry	VERB
eurjchem-792	56	12	.	.	PUNCT
eurjchem-792	57	1	the	the	DET
eurjchem-792	57	2	crude	crude	ADJ
eurjchem-792	57	3	solid	solid	NOUN
eurjchem-792	57	4	was	be	AUX
eurjchem-792	57	5	recrystallized	recrystallize	VERB
eurjchem-792	57	6	from	from	ADP
eurjchem-792	57	7	ethyl	ethyl	PROPN
eurjchem-792	57	8	acetate	acetate	NOUN
eurjchem-792	57	9	to	to	PART
eurjchem-792	57	10	obtain	obtain	VERB
eurjchem-792	57	11	pure	pure	ADJ
eurjchem-792	57	12	compound	compound	NOUN
eurjchem-792	57	13	3	3	NUM
eurjchem-792	57	14	(	(	PUNCT
eurjchem-792	57	15	scheme	scheme	NOUN
eurjchem-792	57	16	1	1	NUM
eurjchem-792	57	17	)	)	PUNCT
eurjchem-792	57	18	.	.	PUNCT
eurjchem-792	58	1	yield	yield	NOUN
eurjchem-792	58	2	:	:	PUNCT
eurjchem-792	58	3	47.40	47.40	NUM
eurjchem-792	58	4	g	g	NOUN
eurjchem-792	58	5	(	(	PUNCT
eurjchem-792	58	6	81.6	81.6	NUM
eurjchem-792	58	7	%	%	NOUN
eurjchem-792	58	8	)	)	PUNCT
eurjchem-792	58	9	.	.	PUNCT
eurjchem-792	59	1	color	color	NOUN
eurjchem-792	59	2	:	:	PUNCT
eurjchem-792	59	3	off	off	ADP
eurjchem-792	59	4	white	white	ADJ
eurjchem-792	59	5	powder	powder	NOUN
eurjchem-792	59	6	.	.	PUNCT
eurjchem-792	60	1	m.p	m.p	PROPN
eurjchem-792	60	2	.	.	PROPN
eurjchem-792	60	3	:	:	PUNCT
eurjchem-792	61	1	210‐213	210‐213	PROPN
eurjchem-792	61	2	°	°	PROPN
eurjchem-792	61	3	c	c	PROPN
eurjchem-792	61	4	.	.	PUNCT
eurjchem-792	62	1	ir	ir	PROPN
eurjchem-792	62	2	(	(	PUNCT
eurjchem-792	62	3	kbr	kbr	PROPN
eurjchem-792	62	4	,	,	PUNCT
eurjchem-792	62	5	v	v	NOUN
eurjchem-792	62	6	,	,	PUNCT
eurjchem-792	62	7	cm‐1	cm‐1	PROPN
eurjchem-792	62	8	):	):	PUNCT
eurjchem-792	62	9	3042	3042	NUM
eurjchem-792	62	10	(	(	PUNCT
eurjchem-792	62	11	ch	ch	NOUN
eurjchem-792	62	12	)	)	PUNCT
eurjchem-792	62	13	,	,	PUNCT
eurjchem-792	62	14	1708	1708	NUM
eurjchem-792	62	15	(	(	PUNCT
eurjchem-792	62	16	c	c	NOUN
eurjchem-792	62	17	=	=	NOUN
eurjchem-792	62	18	o	o	NOUN
eurjchem-792	62	19	)	)	PUNCT
eurjchem-792	62	20	,	,	PUNCT
eurjchem-792	62	21	1624	1624	NUM
eurjchem-792	62	22	(	(	PUNCT
eurjchem-792	62	23	c	c	NOUN
eurjchem-792	62	24	=	=	NOUN
eurjchem-792	62	25	o	o	NOUN
eurjchem-792	62	26	)	)	PUNCT
eurjchem-792	62	27	.	.	PUNCT
eurjchem-792	63	1	1h	1h	NUM
eurjchem-792	63	2	nmr	nmr	NOUN
eurjchem-792	63	3	(	(	PUNCT
eurjchem-792	63	4	300	300	NUM
eurjchem-792	63	5	mhz	mhz	NOUN
eurjchem-792	63	6	,	,	PUNCT
eurjchem-792	63	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-792	63	8	,	,	PUNCT
eurjchem-792	63	9	δ	δ	PROPN
eurjchem-792	63	10	,	,	PUNCT
eurjchem-792	63	11	ppm	ppm	NUM
eurjchem-792	63	12	):	):	PUNCT
eurjchem-792	63	13	1.42‐1.44	1.42‐1.44	NUM
eurjchem-792	63	14	(	(	PUNCT
eurjchem-792	63	15	d	d	PROPN
eurjchem-792	63	16	,	,	PUNCT
eurjchem-792	63	17	3h	3h	NUM
eurjchem-792	63	18	,	,	PUNCT
eurjchem-792	63	19	ch3	ch3	PROPN
eurjchem-792	63	20	,	,	PUNCT
eurjchem-792	63	21	j	j	PROPN
eurjchem-792	63	22	=	=	SYM
eurjchem-792	63	23	6.0	6.0	NUM
eurjchem-792	63	24	hz	hz	NOUN
eurjchem-792	63	25	)	)	PUNCT
eurjchem-792	63	26	,	,	PUNCT
eurjchem-792	63	27	2.34‐2.48	2.34‐2.48	NUM
eurjchem-792	63	28	(	(	PUNCT
eurjchem-792	63	29	m	m	PROPN
eurjchem-792	63	30	,	,	PUNCT
eurjchem-792	63	31	4h	4h	NOUN
eurjchem-792	63	32	,	,	PUNCT
eurjchem-792	63	33	2×ch2	2×ch2	ADJ
eurjchem-792	63	34	)	)	PUNCT
eurjchem-792	63	35	,	,	PUNCT
eurjchem-792	63	36	2.49‐2.51	2.49‐2.51	NUM
eurjchem-792	63	37	(	(	PUNCT
eurjchem-792	63	38	m	m	PROPN
eurjchem-792	63	39	,	,	PUNCT
eurjchem-792	63	40	2h	2h	NUM
eurjchem-792	63	41	,	,	PUNCT
eurjchem-792	63	42	ch2	ch2	PROPN
eurjchem-792	63	43	)	)	PUNCT
eurjchem-792	63	44	,	,	PUNCT
eurjchem-792	63	45	3.23‐3.32	3.23‐3.32	NUM
eurjchem-792	63	46	(	(	PUNCT
eurjchem-792	63	47	m	m	PROPN
eurjchem-792	63	48	,	,	PUNCT
eurjchem-792	63	49	4h	4h	NOUN
eurjchem-792	63	50	,	,	PUNCT
eurjchem-792	63	51	2×ch2	2×ch2	ADJ
eurjchem-792	63	52	)	)	PUNCT
eurjchem-792	63	53	,	,	PUNCT
eurjchem-792	63	54	3.51‐3.54(d	3.51‐3.54(d	NUM
eurjchem-792	63	55	,	,	PUNCT
eurjchem-792	63	56	2h	2h	NUM
eurjchem-792	63	57	,	,	PUNCT
eurjchem-792	63	58	ch2	ch2	PROPN
eurjchem-792	63	59	,	,	PUNCT
eurjchem-792	63	60	j	j	PROPN
eurjchem-792	63	61	=	=	SYM
eurjchem-792	63	62	6.2	6.2	NUM
eurjchem-792	63	63	hz	hz	NOUN
eurjchem-792	63	64	)	)	PUNCT
eurjchem-792	63	65	,	,	PUNCT
eurjchem-792	63	66	4.33‐4.35	4.33‐4.35	NUM
eurjchem-792	63	67	(	(	PUNCT
eurjchem-792	63	68	d	d	PROPN
eurjchem-792	63	69	,	,	PUNCT
eurjchem-792	63	70	1h	1h	NUM
eurjchem-792	63	71	,	,	PUNCT
eurjchem-792	63	72	ch	ch	NOUN
eurjchem-792	63	73	,	,	PUNCT
eurjchem-792	63	74	j	j	PROPN
eurjchem-792	64	1	=	=	SYM
eurjchem-792	64	2	6.0	6.0	NUM
eurjchem-792	64	3	hz	hz	NOUN
eurjchem-792	64	4	)	)	PUNCT
eurjchem-792	64	5	,	,	PUNCT
eurjchem-792	64	6	4.55‐4.58	4.55‐4.58	NUM
eurjchem-792	64	7	(	(	PUNCT
eurjchem-792	64	8	d	d	NOUN
eurjchem-792	64	9	,	,	PUNCT
eurjchem-792	64	10	1h	1h	NUM
eurjchem-792	64	11	,	,	PUNCT
eurjchem-792	64	12	ch	ch	NOUN
eurjchem-792	64	13	,	,	PUNCT
eurjchem-792	64	14	j	j	PROPN
eurjchem-792	65	1	=	=	SYM
eurjchem-792	65	2	6.0	6.0	NUM
eurjchem-792	65	3	hz	hz	NOUN
eurjchem-792	65	4	)	)	PUNCT
eurjchem-792	65	5	,	,	PUNCT
eurjchem-792	65	6	4.89‐4.91	4.89‐4.91	NUM
eurjchem-792	65	7	(	(	PUNCT
eurjchem-792	65	8	d	d	NOUN
eurjchem-792	65	9	,	,	PUNCT
eurjchem-792	65	10	2h	2h	NUM
eurjchem-792	65	11	,	,	PUNCT
eurjchem-792	65	12	ch2	ch2	PROPN
eurjchem-792	65	13	,	,	PUNCT
eurjchem-792	65	14	j	j	PROPN
eurjchem-792	66	1	=	=	SYM
eurjchem-792	66	2	6.0	6.0	NUM
eurjchem-792	66	3	hz	hz	NOUN
eurjchem-792	66	4	)	)	PUNCT
eurjchem-792	66	5	,	,	PUNCT
eurjchem-792	66	6	7.52‐	7.52‐	NUM
eurjchem-792	66	7	7.56	7.56	NUM
eurjchem-792	66	8	(	(	PUNCT
eurjchem-792	66	9	d	d	PROPN
eurjchem-792	66	10	,	,	PUNCT
eurjchem-792	66	11	1h	1h	NUM
eurjchem-792	66	12	,	,	PUNCT
eurjchem-792	66	13	ar‐h	ar‐h	PROPN
eurjchem-792	66	14	,	,	PUNCT
eurjchem-792	66	15	j	j	PROPN
eurjchem-792	66	16	=	=	PROPN
eurjchem-792	66	17	12.0	12.0	NUM
eurjchem-792	66	18	hz	hz	NOUN
eurjchem-792	66	19	)	)	PUNCT
eurjchem-792	66	20	,	,	PUNCT
eurjchem-792	66	21	8.94	8.94	NUM
eurjchem-792	66	22	(	(	PUNCT
eurjchem-792	66	23	s	s	PROPN
eurjchem-792	66	24	,	,	PUNCT
eurjchem-792	66	25	1h	1h	NUM
eurjchem-792	66	26	,	,	PUNCT
eurjchem-792	66	27	c	c	NOUN
eurjchem-792	66	28	=	=	NOUN
eurjchem-792	66	29	ch	ch	NOUN
eurjchem-792	66	30	)	)	PUNCT
eurjchem-792	66	31	,	,	PUNCT
eurjchem-792	66	32	15.17	15.17	NUM
eurjchem-792	66	33	(	(	PUNCT
eurjchem-792	66	34	s	s	PROPN
eurjchem-792	66	35	,	,	PUNCT
eurjchem-792	66	36	1h	1h	NUM
eurjchem-792	66	37	,	,	PUNCT
eurjchem-792	66	38	cooh	cooh	NOUN
eurjchem-792	66	39	,	,	PUNCT
eurjchem-792	66	40	d2o	d2o	PROPN
eurjchem-792	66	41	exchangeable	exchangeable	ADJ
eurjchem-792	66	42	)	)	PUNCT
eurjchem-792	66	43	.	.	PUNCT
eurjchem-792	67	1	13c	13c	NOUN
eurjchem-792	67	2	nmr	nmr	NOUN
eurjchem-792	67	3	(	(	PUNCT
eurjchem-792	67	4	75	75	NUM
eurjchem-792	67	5	mhz	mhz	NOUN
eurjchem-792	67	6	,	,	PUNCT
eurjchem-792	67	7	dmso‐d6	dmso‐d6	NOUN
eurjchem-792	67	8	,	,	PUNCT
eurjchem-792	67	9	ppm	ppm	NOUN
eurjchem-792	67	10	,	,	PUNCT
eurjchem-792	67	11	δ	δ	PROPN
eurjchem-792	67	12	):	):	PUNCT
eurjchem-792	67	13	18.34	18.34	NUM
eurjchem-792	67	14	(	(	PUNCT
eurjchem-792	67	15	ch3	ch3	PROPN
eurjchem-792	67	16	)	)	PUNCT
eurjchem-792	67	17	,	,	PUNCT
eurjchem-792	67	18	45.29	45.29	NUM
eurjchem-792	67	19	(	(	PUNCT
eurjchem-792	67	20	ch2	ch2	PROPN
eurjchem-792	67	21	)	)	PUNCT
eurjchem-792	67	22	,	,	PUNCT
eurjchem-792	67	23	49.23	49.23	NUM
eurjchem-792	67	24	(	(	PUNCT
eurjchem-792	67	25	ch2	ch2	PROPN
eurjchem-792	67	26	)	)	PUNCT
eurjchem-792	67	27	,	,	PUNCT
eurjchem-792	67	28	50.72	50.72	NUM
eurjchem-792	67	29	(	(	PUNCT
eurjchem-792	67	30	2×ch2	2×ch2	ADJ
eurjchem-792	67	31	)	)	PUNCT
eurjchem-792	67	32	,	,	PUNCT
eurjchem-792	67	33	54.56	54.56	NUM
eurjchem-792	67	34	(	(	PUNCT
eurjchem-792	67	35	2×ch2	2×ch2	ADJ
eurjchem-792	67	36	)	)	PUNCT
eurjchem-792	67	37	,	,	PUNCT
eurjchem-792	67	38	55.25	55.25	NUM
eurjchem-792	67	39	(	(	PUNCT
eurjchem-792	67	40	ch	ch	NOUN
eurjchem-792	67	41	)	)	PUNCT
eurjchem-792	67	42	,	,	PUNCT
eurjchem-792	67	43	58.35	58.35	NUM
eurjchem-792	67	44	(	(	PUNCT
eurjchem-792	67	45	ch	ch	NOUN
eurjchem-792	67	46	)	)	PUNCT
eurjchem-792	67	47	,	,	PUNCT
eurjchem-792	67	48	61.61	61.61	NUM
eurjchem-792	67	49	(	(	PUNCT
eurjchem-792	67	50	ch	ch	NOUN
eurjchem-792	67	51	)	)	PUNCT
eurjchem-792	67	52	,	,	PUNCT
eurjchem-792	67	53	68.49	68.49	NUM
eurjchem-792	67	54	(	(	PUNCT
eurjchem-792	67	55	ch2	ch2	PROPN
eurjchem-792	67	56	)	)	PUNCT
eurjchem-792	67	57	,	,	PUNCT
eurjchem-792	67	58	107.32	107.32	NUM
eurjchem-792	67	59	(	(	PUNCT
eurjchem-792	67	60	ch	ch	NOUN
eurjchem-792	67	61	)	)	PUNCT
eurjchem-792	67	62	,	,	PUNCT
eurjchem-792	67	63	109.34	109.34	NUM
eurjchem-792	67	64	(	(	PUNCT
eurjchem-792	67	65	c	c	NOUN
eurjchem-792	67	66	)	)	PUNCT
eurjchem-792	67	67	,	,	PUNCT
eurjchem-792	67	68	120.13	120.13	NUM
eurjchem-792	67	69	(	(	PUNCT
eurjchem-792	67	70	c	c	NOUN
eurjchem-792	67	71	)	)	PUNCT
eurjchem-792	67	72	,	,	PUNCT
eurjchem-792	67	73	125.19	125.19	NUM
eurjchem-792	67	74	(	(	PUNCT
eurjchem-792	67	75	c	c	NOUN
eurjchem-792	67	76	)	)	PUNCT
eurjchem-792	67	77	,	,	PUNCT
eurjchem-792	67	78	130.44	130.44	NUM
eurjchem-792	67	79	(	(	PUNCT
eurjchem-792	67	80	c	c	NOUN
eurjchem-792	67	81	)	)	PUNCT
eurjchem-792	67	82	,	,	PUNCT
eurjchem-792	67	83	132.56	132.56	NUM
eurjchem-792	67	84	(	(	PUNCT
eurjchem-792	67	85	c	c	NOUN
eurjchem-792	67	86	)	)	PUNCT
eurjchem-792	67	87	,	,	PUNCT
eurjchem-792	67	88	140.68	140.68	NUM
eurjchem-792	67	89	(	(	PUNCT
eurjchem-792	67	90	c	c	NOUN
eurjchem-792	67	91	)	)	PUNCT
eurjchem-792	67	92	,	,	PUNCT
eurjchem-792	67	93	146.79	146.79	NUM
eurjchem-792	67	94	(	(	PUNCT
eurjchem-792	67	95	c	c	NOUN
eurjchem-792	67	96	)	)	PUNCT
eurjchem-792	67	97	,	,	PUNCT
eurjchem-792	67	98	154.28	154.28	NUM
eurjchem-792	67	99	(	(	PUNCT
eurjchem-792	67	100	ch	ch	NOUN
eurjchem-792	67	101	)	)	PUNCT
eurjchem-792	67	102	,	,	PUNCT
eurjchem-792	67	103	166.45	166.45	NUM
eurjchem-792	67	104	(	(	PUNCT
eurjchem-792	67	105	c	c	NOUN
eurjchem-792	67	106	=	=	NOUN
eurjchem-792	67	107	o	o	NOUN
eurjchem-792	67	108	)	)	PUNCT
eurjchem-792	67	109	,	,	PUNCT
eurjchem-792	67	110	176.77	176.77	NUM
eurjchem-792	67	111	(	(	PUNCT
eurjchem-792	67	112	c	c	NOUN
eurjchem-792	67	113	=	=	NOUN
eurjchem-792	67	114	o	o	NOUN
eurjchem-792	67	115	)	)	PUNCT
eurjchem-792	67	116	.	.	PUNCT
eurjchem-792	68	1	anal	anal	PROPN
eurjchem-792	68	2	.	.	PUNCT
eurjchem-792	68	3	calcd	calcd	NOUN
eurjchem-792	68	4	.	.	PUNCT
eurjchem-792	69	1	for	for	ADP
eurjchem-792	69	2	c20h22fn3o5	c20h22fn3o5	PROPN
eurjchem-792	69	3	:	:	PUNCT
eurjchem-792	69	4	c	c	X
eurjchem-792	69	5	,	,	PUNCT
eurjchem-792	69	6	59.55	59.55	NUM
eurjchem-792	69	7	;	;	PUNCT
eurjchem-792	69	8	h	h	NOUN
eurjchem-792	69	9	,	,	PUNCT
eurjchem-792	69	10	5.50	5.50	NUM
eurjchem-792	69	11	;	;	PUNCT
eurjchem-792	69	12	n	n	CCONJ
eurjchem-792	69	13	,	,	PUNCT
eurjchem-792	69	14	10.42	10.42	NUM
eurjchem-792	69	15	.	.	PUNCT
eurjchem-792	69	16	found	find	VERB
eurjchem-792	69	17	:	:	PUNCT
eurjchem-792	70	1	c	c	X
eurjchem-792	70	2	,	,	PUNCT
eurjchem-792	70	3	59.49	59.49	NUM
eurjchem-792	70	4	;	;	PUNCT
eurjchem-792	71	1	h	h	NOUN
eurjchem-792	71	2	,	,	PUNCT
eurjchem-792	71	3	5.60	5.60	NUM
eurjchem-792	71	4	;	;	PUNCT
eurjchem-792	71	5	n	n	CCONJ
eurjchem-792	71	6	,	,	PUNCT
eurjchem-792	71	7	10.64	10.64	NUM
eurjchem-792	71	8	%	%	NOUN
eurjchem-792	71	9	.	.	PUNCT
eurjchem-792	72	1	ms	ms	NOUN
eurjchem-792	72	2	(	(	PUNCT
eurjchem-792	72	3	m	m	PROPN
eurjchem-792	72	4	/	/	SYM
eurjchem-792	72	5	z	z	NOUN
eurjchem-792	72	6	):	):	PUNCT
eurjchem-792	72	7	404.02	404.02	NUM
eurjchem-792	72	8	(	(	PUNCT
eurjchem-792	72	9	m+	m+	NUM
eurjchem-792	72	10	)	)	PUNCT
eurjchem-792	72	11	.	.	PUNCT
eurjchem-792	73	1	[	[	X
eurjchem-792	73	2	α]d25	α]d25	NOUN
eurjchem-792	73	3	:	:	PUNCT
eurjchem-792	73	4	‐73.06	‐73.06	ADV
eurjchem-792	73	5	(	(	PUNCT
eurjchem-792	73	6	c	c	NOUN
eurjchem-792	73	7	=	=	SYM
eurjchem-792	73	8	1.0	1.0	NUM
eurjchem-792	73	9	in	in	ADP
eurjchem-792	73	10	methanol	methanol	NOUN
eurjchem-792	73	11	:	:	PUNCT
eurjchem-792	73	12	methylene	methylene	NOUN
eurjchem-792	73	13	chloride	chloride	NOUN
eurjchem-792	73	14	,	,	PUNCT
eurjchem-792	73	15	1:1	1:1	NUM
eurjchem-792	73	16	)	)	PUNCT
eurjchem-792	73	17	.	.	PUNCT
eurjchem-792	74	1	2.2.3	2.2.3	X
eurjchem-792	74	2	.	.	PUNCT
eurjchem-792	74	3	general	general	ADJ
eurjchem-792	74	4	procedure	procedure	NOUN
eurjchem-792	74	5	for	for	ADP
eurjchem-792	74	6	the	the	DET
eurjchem-792	74	7	synthesis	synthesis	NOUN
eurjchem-792	74	8	of	of	ADP
eurjchem-792	74	9	compounds	compound	NOUN
eurjchem-792	74	10	4a‐e	4a‐e	NOUN
eurjchem-792	74	11	to	to	ADP
eurjchem-792	74	12	a	a	DET
eurjchem-792	74	13	solution	solution	NOUN
eurjchem-792	74	14	of	of	ADP
eurjchem-792	74	15	substituted	substitute	VERB
eurjchem-792	74	16	mercaptobenzimidazoles	mercaptobenzimidazole	NOUN
eurjchem-792	74	17	(	(	PUNCT
eurjchem-792	74	18	13.53	13.53	NUM
eurjchem-792	74	19	mmol	mmol	NOUN
eurjchem-792	74	20	)	)	PUNCT
eurjchem-792	74	21	in	in	ADP
eurjchem-792	74	22	methanolic	methanolic	PROPN
eurjchem-792	74	23	naoh	naoh	NOUN
eurjchem-792	74	24	(	(	PUNCT
eurjchem-792	74	25	30.75	30.75	NUM
eurjchem-792	74	26	mmol	mmol	NOUN
eurjchem-792	74	27	)	)	PUNCT
eurjchem-792	74	28	was	be	AUX
eurjchem-792	74	29	added	add	VERB
eurjchem-792	74	30	to	to	PART
eurjchem-792	74	31	compound	compound	VERB
eurjchem-792	74	32	3	3	NUM
eurjchem-792	74	33	(	(	PUNCT
eurjchem-792	74	34	5.0	5.0	NUM
eurjchem-792	74	35	g	g	NOUN
eurjchem-792	74	36	,	,	PUNCT
eurjchem-792	74	37	12.30	12.30	NUM
eurjchem-792	74	38	mmol	mmol	NOUN
eurjchem-792	74	39	)	)	PUNCT
eurjchem-792	74	40	and	and	CCONJ
eurjchem-792	74	41	the	the	DET
eurjchem-792	74	42	reaction	reaction	NOUN
eurjchem-792	74	43	mixture	mixture	NOUN
eurjchem-792	74	44	was	be	AUX
eurjchem-792	74	45	stirred	stir	VERB
eurjchem-792	74	46	for	for	ADP
eurjchem-792	74	47	6	6	NUM
eurjchem-792	74	48	h	h	NOUN
eurjchem-792	74	49	at	at	ADP
eurjchem-792	74	50	room	room	NOUN
eurjchem-792	74	51	temperature	temperature	NOUN
eurjchem-792	74	52	and	and	CCONJ
eurjchem-792	74	53	monitored	monitor	VERB
eurjchem-792	74	54	the	the	DET
eurjchem-792	74	55	reaction	reaction	NOUN
eurjchem-792	74	56	by	by	ADP
eurjchem-792	74	57	tlc	tlc	PROPN
eurjchem-792	74	58	,	,	PUNCT
eurjchem-792	74	59	upon	upon	SCONJ
eurjchem-792	74	60	completion	completion	NOUN
eurjchem-792	74	61	of	of	ADP
eurjchem-792	74	62	the	the	DET
eurjchem-792	74	63	reaction	reaction	NOUN
eurjchem-792	74	64	,	,	PUNCT
eurjchem-792	74	65	methanol	methanol	NOUN
eurjchem-792	74	66	was	be	AUX
eurjchem-792	74	67	distilled	distil	VERB
eurjchem-792	74	68	off	off	ADP
eurjchem-792	74	69	under	under	ADP
eurjchem-792	74	70	reduced	reduce	VERB
eurjchem-792	74	71	pressure	pressure	NOUN
eurjchem-792	74	72	and	and	CCONJ
eurjchem-792	74	73	the	the	DET
eurjchem-792	74	74	resulted	resulted	ADJ
eurjchem-792	74	75	residue	residue	NOUN
eurjchem-792	74	76	was	be	AUX
eurjchem-792	74	77	dissolved	dissolve	VERB
eurjchem-792	74	78	in	in	ADP
eurjchem-792	74	79	water	water	NOUN
eurjchem-792	74	80	,	,	PUNCT
eurjchem-792	74	81	adjusted	adjust	VERB
eurjchem-792	74	82	the	the	DET
eurjchem-792	74	83	ph	ph	NOUN
eurjchem-792	74	84	=	=	SYM
eurjchem-792	74	85	6.0‐7.0	6.0‐7.0	NUM
eurjchem-792	74	86	with	with	ADP
eurjchem-792	74	87	dil	dil	PROPN
eurjchem-792	74	88	.	.	PUNCT
eurjchem-792	75	1	hcl	hcl	PROPN
eurjchem-792	76	1	and	and	CCONJ
eurjchem-792	76	2	extracted	extract	VERB
eurjchem-792	76	3	the	the	DET
eurjchem-792	76	4	product	product	NOUN
eurjchem-792	76	5	in	in	ADP
eurjchem-792	76	6	to	to	ADP
eurjchem-792	76	7	dichloromethane	dichloromethane	NOUN
eurjchem-792	76	8	.	.	PUNCT
eurjchem-792	77	1	the	the	DET
eurjchem-792	77	2	organic	organic	ADJ
eurjchem-792	77	3	layer	layer	NOUN
eurjchem-792	77	4	was	be	AUX
eurjchem-792	77	5	separated	separate	VERB
eurjchem-792	77	6	and	and	CCONJ
eurjchem-792	77	7	washed	wash	VERB
eurjchem-792	77	8	with	with	ADP
eurjchem-792	77	9	water	water	NOUN
eurjchem-792	77	10	followed	follow	VERB
eurjchem-792	77	11	by	by	ADP
eurjchem-792	77	12	20	20	NUM
eurjchem-792	77	13	%	%	NOUN
eurjchem-792	77	14	sodium	sodium	NOUN
eurjchem-792	77	15	chloride	chloride	NOUN
eurjchem-792	77	16	solution	solution	NOUN
eurjchem-792	77	17	,	,	PUNCT
eurjchem-792	77	18	dried	dry	VERB
eurjchem-792	77	19	over	over	ADP
eurjchem-792	77	20	anhydrous	anhydrous	ADJ
eurjchem-792	77	21	na2so4	na2so4	NOUN
eurjchem-792	77	22	.	.	PUNCT
eurjchem-792	78	1	the	the	DET
eurjchem-792	78	2	solvent	solvent	NOUN
eurjchem-792	78	3	was	be	AUX
eurjchem-792	78	4	distilled	distil	VERB
eurjchem-792	78	5	off	off	ADP
eurjchem-792	78	6	under	under	ADP
eurjchem-792	78	7	vacuum	vacuum	NOUN
eurjchem-792	78	8	to	to	PART
eurjchem-792	78	9	obtain	obtain	VERB
eurjchem-792	78	10	crude	crude	ADJ
eurjchem-792	78	11	4a‐e	4a‐e	NOUN
eurjchem-792	78	12	.	.	PUNCT
eurjchem-792	79	1	the	the	DET
eurjchem-792	79	2	crude	crude	ADJ
eurjchem-792	79	3	compounds	compound	NOUN
eurjchem-792	79	4	were	be	AUX
eurjchem-792	79	5	recrystallized	recrystallize	VERB
eurjchem-792	79	6	from	from	AUX
eurjchem-792	79	7	ethylacetate	ethylacetate	VERB
eurjchem-792	79	8	to	to	PART
eurjchem-792	79	9	obtain	obtain	VERB
eurjchem-792	79	10	the	the	DET
eurjchem-792	79	11	pure	pure	ADJ
eurjchem-792	79	12	title	title	NOUN
eurjchem-792	79	13	compounds	compound	NOUN
eurjchem-792	79	14	(	(	PUNCT
eurjchem-792	79	15	scheme	scheme	NOUN
eurjchem-792	79	16	2	2	NUM
eurjchem-792	79	17	)	)	PUNCT
eurjchem-792	79	18	.	.	PUNCT
eurjchem-792	80	1	(	(	PUNCT
eurjchem-792	80	2	s)‐10‐(4‐(3‐(1h‐benzo[d]imidazol‐2‐ylthio)‐2‐hydroxy	s)‐10‐(4‐(3‐(1h‐benzo[d]imidazol‐2‐ylthio)‐2‐hydroxy	PROPN
eurjchem-792	80	3	propyl)piperazin‐1‐yl)‐9‐fluoro‐3,7‐dihydro‐3‐methyl‐7‐oxo‐2h‐	propyl)piperazin‐1‐yl)‐9‐fluoro‐3,7‐dihydro‐3‐methyl‐7‐oxo‐2h‐	PROPN
eurjchem-792	80	4	[	[	X
eurjchem-792	80	5	1,4]oxazino[2,3,4‐ij]quinoline‐6‐carboxylic	1,4]oxazino[2,3,4‐ij]quinoline‐6‐carboxylic	NUM
eurjchem-792	80	6	acid	acid	NOUN
eurjchem-792	80	7	(	(	PUNCT
eurjchem-792	80	8	4a	4a	NUM
eurjchem-792	80	9	):	):	PUNCT
eurjchem-792	80	10	yield	yield	NOUN
eurjchem-792	80	11	:	:	PUNCT
eurjchem-792	80	12	5.59	5.59	NUM
eurjchem-792	80	13	g	g	NOUN
eurjchem-792	80	14	(	(	PUNCT
eurjchem-792	80	15	81.5	81.5	NUM
eurjchem-792	80	16	%	%	NOUN
eurjchem-792	80	17	)	)	PUNCT
eurjchem-792	80	18	.	.	PUNCT
eurjchem-792	81	1	color	color	NOUN
eurjchem-792	81	2	:	:	PUNCT
eurjchem-792	81	3	off	off	ADP
eurjchem-792	81	4	white	white	ADJ
eurjchem-792	81	5	powder	powder	NOUN
eurjchem-792	81	6	.	.	PUNCT
eurjchem-792	82	1	m.p	m.p	PROPN
eurjchem-792	82	2	.	.	PROPN
eurjchem-792	82	3	:	:	PUNCT
eurjchem-792	83	1	222‐225	222‐225	PROPN
eurjchem-792	83	2	°	°	SYM
eurjchem-792	83	3	c	c	VERB
eurjchem-792	83	4	.	.	PUNCT
eurjchem-792	84	1	ir	ir	PROPN
eurjchem-792	84	2	(	(	PUNCT
eurjchem-792	84	3	kbr	kbr	PROPN
eurjchem-792	84	4	,	,	PUNCT
eurjchem-792	84	5	v	v	NOUN
eurjchem-792	84	6	,	,	PUNCT
eurjchem-792	84	7	cm‐1	cm‐1	PROPN
eurjchem-792	84	8	):	):	PUNCT
eurjchem-792	84	9	3401	3401	NUM
eurjchem-792	84	10	(	(	PUNCT
eurjchem-792	84	11	oh	oh	INTJ
eurjchem-792	84	12	)	)	PUNCT
eurjchem-792	84	13	,	,	PUNCT
eurjchem-792	84	14	1721	1721	NUM
eurjchem-792	84	15	(	(	PUNCT
eurjchem-792	84	16	c	c	NOUN
eurjchem-792	84	17	=	=	NOUN
eurjchem-792	84	18	o	o	NOUN
eurjchem-792	84	19	)	)	PUNCT
eurjchem-792	84	20	,	,	PUNCT
eurjchem-792	84	21	1619	1619	NUM
eurjchem-792	84	22	(	(	PUNCT
eurjchem-792	84	23	c	c	NOUN
eurjchem-792	84	24	=	=	NOUN
eurjchem-792	84	25	o	o	NOUN
eurjchem-792	84	26	)	)	PUNCT
eurjchem-792	84	27	.	.	PUNCT
eurjchem-792	85	1	1h	1h	NUM
eurjchem-792	85	2	nmr	nmr	NOUN
eurjchem-792	85	3	(	(	PUNCT
eurjchem-792	85	4	300	300	NUM
eurjchem-792	85	5	mhz	mhz	NOUN
eurjchem-792	85	6	,	,	PUNCT
eurjchem-792	85	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-792	85	8	,	,	PUNCT
eurjchem-792	85	9	δ	δ	PROPN
eurjchem-792	85	10	,	,	PUNCT
eurjchem-792	85	11	ppm	ppm	NUM
eurjchem-792	85	12	):	):	PUNCT
eurjchem-792	85	13	1.39‐1.41	1.39‐1.41	NUM
eurjchem-792	85	14	(	(	PUNCT
eurjchem-792	85	15	d	d	PROPN
eurjchem-792	85	16	,	,	PUNCT
eurjchem-792	85	17	3h	3h	NUM
eurjchem-792	85	18	,	,	PUNCT
eurjchem-792	85	19	ch3	ch3	PROPN
eurjchem-792	85	20	,	,	PUNCT
eurjchem-792	85	21	j	j	PROPN
eurjchem-792	85	22	=	=	SYM
eurjchem-792	85	23	6.2	6.2	NUM
eurjchem-792	85	24	hz	hz	ADJ
eurjchem-792	85	25	)	)	PUNCT
eurjchem-792	85	26	2.52‐2.58	2.52‐2.58	PROPN
eurjchem-792	85	27	(	(	PUNCT
eurjchem-792	85	28	m	m	PROPN
eurjchem-792	85	29	,	,	PUNCT
eurjchem-792	85	30	4h	4h	NOUN
eurjchem-792	85	31	,	,	PUNCT
eurjchem-792	85	32	2×ch2	2×ch2	ADJ
eurjchem-792	85	33	)	)	PUNCT
eurjchem-792	85	34	,	,	PUNCT
eurjchem-792	85	35	2.71‐2.73	2.71‐2.73	PROPN
eurjchem-792	85	36	(	(	PUNCT
eurjchem-792	85	37	d	d	NOUN
eurjchem-792	85	38	,	,	PUNCT
eurjchem-792	85	39	2h	2h	NUM
eurjchem-792	85	40	,	,	PUNCT
eurjchem-792	85	41	ch2	ch2	PROPN
eurjchem-792	85	42	,	,	PUNCT
eurjchem-792	85	43	j	j	PROPN
eurjchem-792	85	44	=	=	SYM
eurjchem-792	85	45	6.0	6.0	NUM
eurjchem-792	85	46	hz	hz	NOUN
eurjchem-792	85	47	)	)	PUNCT
eurjchem-792	85	48	,	,	PUNCT
eurjchem-792	85	49	3.26‐3.28	3.26‐3.28	NUM
eurjchem-792	85	50	(	(	PUNCT
eurjchem-792	85	51	d	d	NOUN
eurjchem-792	85	52	,	,	PUNCT
eurjchem-792	85	53	2h	2h	NUM
eurjchem-792	85	54	,	,	PUNCT
eurjchem-792	85	55	ch2	ch2	PROPN
eurjchem-792	85	56	,	,	PUNCT
eurjchem-792	85	57	j	j	PROPN
eurjchem-792	85	58	=	=	SYM
eurjchem-792	85	59	6.0	6.0	NUM
eurjchem-792	85	60	hz	hz	NOUN
eurjchem-792	85	61	)	)	PUNCT
eurjchem-792	85	62	,	,	PUNCT
eurjchem-792	85	63	3.53‐3.60	3.53‐3.60	NUM
eurjchem-792	85	64	(	(	PUNCT
eurjchem-792	85	65	m	m	PROPN
eurjchem-792	85	66	,	,	PUNCT
eurjchem-792	85	67	4h	4h	NOUN
eurjchem-792	85	68	,	,	PUNCT
eurjchem-792	85	69	2×ch2	2×ch2	ADJ
eurjchem-792	85	70	)	)	PUNCT
eurjchem-792	85	71	,	,	PUNCT
eurjchem-792	85	72	3.62‐3.66	3.62‐3.66	NUM
eurjchem-792	85	73	(	(	PUNCT
eurjchem-792	85	74	m	m	PROPN
eurjchem-792	85	75	,	,	PUNCT
eurjchem-792	85	76	1h	1h	NUM
eurjchem-792	85	77	,	,	PUNCT
eurjchem-792	85	78	ch	ch	NOUN
eurjchem-792	85	79	)	)	PUNCT
eurjchem-792	85	80	,	,	PUNCT
eurjchem-792	85	81	4.31‐4.37	4.31‐4.37	PROPN
eurjchem-792	85	82	(	(	PUNCT
eurjchem-792	85	83	m	m	PROPN
eurjchem-792	85	84	,	,	PUNCT
eurjchem-792	85	85	1h	1h	NUM
eurjchem-792	85	86	,	,	PUNCT
eurjchem-792	85	87	ch	ch	NOUN
eurjchem-792	85	88	)	)	PUNCT
eurjchem-792	85	89	,	,	PUNCT
eurjchem-792	85	90	4.49‐4.51	4.49‐4.51	NUM
eurjchem-792	85	91	(	(	PUNCT
eurjchem-792	85	92	d	d	NOUN
eurjchem-792	85	93	,	,	PUNCT
eurjchem-792	85	94	2h	2h	NUM
eurjchem-792	85	95	,	,	PUNCT
eurjchem-792	85	96	ch2	ch2	PROPN
eurjchem-792	85	97	,	,	PUNCT
eurjchem-792	85	98	j	j	PROPN
eurjchem-792	86	1	=	=	SYM
eurjchem-792	86	2	6.0	6.0	NUM
eurjchem-792	86	3	hz	hz	NOUN
eurjchem-792	86	4	)	)	PUNCT
eurjchem-792	86	5	,	,	PUNCT
eurjchem-792	86	6	4.96	4.96	NUM
eurjchem-792	86	7	(	(	PUNCT
eurjchem-792	86	8	s	s	PROPN
eurjchem-792	86	9	,	,	PUNCT
eurjchem-792	86	10	1h	1h	NUM
eurjchem-792	86	11	,	,	PUNCT
eurjchem-792	86	12	oh	oh	INTJ
eurjchem-792	86	13	,	,	PUNCT
eurjchem-792	86	14	d2o	d2o	NOUN
eurjchem-792	86	15	exchangeable	exchangeable	ADJ
eurjchem-792	86	16	)	)	PUNCT
eurjchem-792	86	17	,	,	PUNCT
eurjchem-792	86	18	5.36	5.36	NUM
eurjchem-792	86	19	(	(	PUNCT
eurjchem-792	86	20	s	s	PROPN
eurjchem-792	86	21	,	,	PUNCT
eurjchem-792	86	22	1h	1h	NUM
eurjchem-792	86	23	,	,	PUNCT
eurjchem-792	86	24	nh	nh	PROPN
eurjchem-792	86	25	,	,	PUNCT
eurjchem-792	86	26	d2o	d2o	PROPN
eurjchem-792	86	27	exchangeable	exchangeable	ADJ
eurjchem-792	86	28	)	)	PUNCT
eurjchem-792	86	29	,	,	PUNCT
eurjchem-792	86	30	7.03‐7.08	7.03‐7.08	NUM
eurjchem-792	86	31	(	(	PUNCT
eurjchem-792	86	32	m	m	PROPN
eurjchem-792	86	33	,	,	PUNCT
eurjchem-792	86	34	2h	2h	NUM
eurjchem-792	86	35	,	,	PUNCT
eurjchem-792	86	36	ar‐h	ar‐h	NOUN
eurjchem-792	86	37	)	)	PUNCT
eurjchem-792	86	38	,	,	PUNCT
eurjchem-792	86	39	7.36‐7.37	7.36‐7.37	NUM
eurjchem-792	86	40	(	(	PUNCT
eurjchem-792	86	41	m	m	PROPN
eurjchem-792	86	42	,	,	PUNCT
eurjchem-792	86	43	2h	2h	NUM
eurjchem-792	86	44	,	,	PUNCT
eurjchem-792	86	45	ar‐	ar‐	PROPN
eurjchem-792	86	46	h	h	NOUN
eurjchem-792	86	47	)	)	PUNCT
eurjchem-792	86	48	,	,	PUNCT
eurjchem-792	86	49	7.47‐7.50	7.47‐7.50	NUM
eurjchem-792	86	50	(	(	PUNCT
eurjchem-792	86	51	d	d	PROPN
eurjchem-792	86	52	,	,	PUNCT
eurjchem-792	86	53	1h	1h	NUM
eurjchem-792	86	54	,	,	PUNCT
eurjchem-792	86	55	ar‐h	ar‐h	PROPN
eurjchem-792	86	56	,	,	PUNCT
eurjchem-792	86	57	j	j	PROPN
eurjchem-792	86	58	=	=	PROPN
eurjchem-792	86	59	12.0	12.0	NUM
eurjchem-792	86	60	hz	hz	NOUN
eurjchem-792	86	61	)	)	PUNCT
eurjchem-792	86	62	,	,	PUNCT
eurjchem-792	86	63	8.74	8.74	NUM
eurjchem-792	86	64	(	(	PUNCT
eurjchem-792	86	65	s	s	PROPN
eurjchem-792	86	66	,	,	PUNCT
eurjchem-792	86	67	1h	1h	NUM
eurjchem-792	86	68	,	,	PUNCT
eurjchem-792	86	69	c	c	NOUN
eurjchem-792	86	70	=	=	NOUN
eurjchem-792	86	71	ch	ch	NOUN
eurjchem-792	86	72	)	)	PUNCT
eurjchem-792	86	73	,	,	PUNCT
eurjchem-792	86	74	15.16	15.16	NUM
eurjchem-792	86	75	(	(	PUNCT
eurjchem-792	86	76	s	s	PROPN
eurjchem-792	86	77	,	,	PUNCT
eurjchem-792	86	78	1h	1h	NUM
eurjchem-792	86	79	,	,	PUNCT
eurjchem-792	86	80	cooh	cooh	NOUN
eurjchem-792	86	81	,	,	PUNCT
eurjchem-792	86	82	d2o	d2o	PROPN
eurjchem-792	86	83	exchangeable	exchangeable	ADJ
eurjchem-792	86	84	)	)	PUNCT
eurjchem-792	86	85	.	.	PUNCT
eurjchem-792	87	1	13c	13c	NOUN
eurjchem-792	87	2	nmr	nmr	NOUN
eurjchem-792	87	3	(	(	PUNCT
eurjchem-792	87	4	75	75	NUM
eurjchem-792	87	5	mhz	mhz	NOUN
eurjchem-792	87	6	,	,	PUNCT
eurjchem-792	87	7	dmso‐d6	dmso‐d6	NOUN
eurjchem-792	87	8	,	,	PUNCT
eurjchem-792	87	9	ppm	ppm	NOUN
eurjchem-792	87	10	,	,	PUNCT
eurjchem-792	87	11	δ	δ	PROPN
eurjchem-792	87	12	):	):	PUNCT
eurjchem-792	87	13	18.39	18.39	NUM
eurjchem-792	87	14	(	(	PUNCT
eurjchem-792	87	15	ch3	ch3	PROPN
eurjchem-792	87	16	)	)	PUNCT
eurjchem-792	87	17	,	,	PUNCT
eurjchem-792	87	18	47.24	47.24	NUM
eurjchem-792	87	19	(	(	PUNCT
eurjchem-792	87	20	ch2	ch2	PROPN
eurjchem-792	87	21	)	)	PUNCT
eurjchem-792	87	22	,	,	PUNCT
eurjchem-792	87	23	49.04	49.04	NUM
eurjchem-792	87	24	(	(	PUNCT
eurjchem-792	87	25	2×ch2	2×ch2	ADJ
eurjchem-792	87	26	)	)	PUNCT
eurjchem-792	87	27	,	,	PUNCT
eurjchem-792	87	28	55.30	55.30	NUM
eurjchem-792	87	29	(	(	PUNCT
eurjchem-792	87	30	2×ch2	2×ch2	ADJ
eurjchem-792	87	31	)	)	PUNCT
eurjchem-792	87	32	,	,	PUNCT
eurjchem-792	87	33	60.43	60.43	NUM
eurjchem-792	87	34	(	(	PUNCT
eurjchem-792	87	35	ch2	ch2	PROPN
eurjchem-792	87	36	)	)	PUNCT
eurjchem-792	87	37	,	,	PUNCT
eurjchem-792	87	38	62.31	62.31	NUM
eurjchem-792	87	39	(	(	PUNCT
eurjchem-792	87	40	ch	ch	NOUN
eurjchem-792	87	41	)	)	PUNCT
eurjchem-792	87	42	,	,	PUNCT
eurjchem-792	87	43	64.51	64.51	NUM
eurjchem-792	87	44	(	(	PUNCT
eurjchem-792	87	45	ch	ch	NOUN
eurjchem-792	87	46	)	)	PUNCT
eurjchem-792	87	47	,	,	PUNCT
eurjchem-792	87	48	68.77	68.77	NUM
eurjchem-792	87	49	(	(	PUNCT
eurjchem-792	87	50	ch2	ch2	PROPN
eurjchem-792	87	51	)	)	PUNCT
eurjchem-792	87	52	,	,	PUNCT
eurjchem-792	87	53	107.24	107.24	NUM
eurjchem-792	87	54	(	(	PUNCT
eurjchem-792	87	55	ch	ch	NOUN
eurjchem-792	87	56	)	)	PUNCT
eurjchem-792	87	57	,	,	PUNCT
eurjchem-792	87	58	109.21	109.21	NUM
eurjchem-792	87	59	(	(	PUNCT
eurjchem-792	87	60	c	c	NOUN
eurjchem-792	87	61	)	)	PUNCT
eurjchem-792	87	62	,	,	PUNCT
eurjchem-792	87	63	115.99	115.99	NUM
eurjchem-792	87	64	(	(	PUNCT
eurjchem-792	87	65	ch	ch	NOUN
eurjchem-792	87	66	)	)	PUNCT
eurjchem-792	87	67	,	,	PUNCT
eurjchem-792	87	68	120.96	120.96	NUM
eurjchem-792	87	69	(	(	PUNCT
eurjchem-792	87	70	c	c	NOUN
eurjchem-792	87	71	)	)	PUNCT
eurjchem-792	87	72	,	,	PUNCT
eurjchem-792	87	73	124.05	124.05	NUM
eurjchem-792	87	74	(	(	PUNCT
eurjchem-792	87	75	ch	ch	NOUN
eurjchem-792	87	76	)	)	PUNCT
eurjchem-792	87	77	,	,	PUNCT
eurjchem-792	87	78	130.77	130.77	NUM
eurjchem-792	87	79	(	(	PUNCT
eurjchem-792	87	80	c	c	NOUN
eurjchem-792	87	81	)	)	PUNCT
eurjchem-792	87	82	,	,	PUNCT
eurjchem-792	87	83	134.79	134.79	NUM
eurjchem-792	87	84	(	(	PUNCT
eurjchem-792	87	85	c	c	NOUN
eurjchem-792	87	86	)	)	PUNCT
eurjchem-792	87	87	,	,	PUNCT
eurjchem-792	87	88	140.96	140.96	NUM
eurjchem-792	87	89	(	(	PUNCT
eurjchem-792	87	90	c	c	NOUN
eurjchem-792	87	91	)	)	PUNCT
eurjchem-792	87	92	,	,	PUNCT
eurjchem-792	87	93	146.79	146.79	NUM
eurjchem-792	87	94	(	(	PUNCT
eurjchem-792	87	95	c	c	NOUN
eurjchem-792	87	96	)	)	PUNCT
eurjchem-792	87	97	,	,	PUNCT
eurjchem-792	87	98	152.50	152.50	NUM
eurjchem-792	87	99	(	(	PUNCT
eurjchem-792	87	100	c	c	NOUN
eurjchem-792	87	101	)	)	PUNCT
eurjchem-792	87	102	,	,	PUNCT
eurjchem-792	87	103	154.07	154.07	NUM
eurjchem-792	87	104	(	(	PUNCT
eurjchem-792	87	105	ch	ch	NOUN
eurjchem-792	87	106	)	)	PUNCT
eurjchem-792	87	107	,	,	PUNCT
eurjchem-792	87	108	166.39	166.39	NUM
eurjchem-792	87	109	(	(	PUNCT
eurjchem-792	87	110	c	c	NOUN
eurjchem-792	87	111	=	=	NOUN
eurjchem-792	87	112	o	o	NOUN
eurjchem-792	87	113	)	)	PUNCT
eurjchem-792	87	114	,	,	PUNCT
eurjchem-792	87	115	176.83	176.83	NUM
eurjchem-792	87	116	(	(	PUNCT
eurjchem-792	87	117	c	c	NOUN
eurjchem-792	87	118	=	=	NOUN
eurjchem-792	87	119	o	o	NOUN
eurjchem-792	87	120	)	)	PUNCT
eurjchem-792	87	121	.	.	PUNCT
eurjchem-792	88	1	anal	anal	PROPN
eurjchem-792	88	2	.	.	PUNCT
eurjchem-792	88	3	calcd	calcd	NOUN
eurjchem-792	88	4	.	.	PUNCT
eurjchem-792	89	1	for	for	SCONJ
eurjchem-792	89	2	c27h28fn5o5s	c27h28fn5o5s	PROPN
eurjchem-792	89	3	:	:	PUNCT
eurjchem-792	89	4	c	c	X
eurjchem-792	89	5	,	,	PUNCT
eurjchem-792	89	6	58.58	58.58	NUM
eurjchem-792	89	7	;	;	PUNCT
eurjchem-792	89	8	h	h	NOUN
eurjchem-792	89	9	,	,	PUNCT
eurjchem-792	89	10	5.10	5.10	NUM
eurjchem-792	89	11	;	;	PUNCT
eurjchem-792	89	12	n	n	CCONJ
eurjchem-792	89	13	,	,	PUNCT
eurjchem-792	89	14	12.56	12.56	NUM
eurjchem-792	89	15	.	.	PUNCT
eurjchem-792	89	16	found	find	VERB
eurjchem-792	89	17	:	:	PUNCT
eurjchem-792	90	1	c	c	X
eurjchem-792	90	2	,	,	PUNCT
eurjchem-792	90	3	58.46	58.46	NUM
eurjchem-792	90	4	;	;	PUNCT
eurjchem-792	90	5	h	h	NOUN
eurjchem-792	90	6	,	,	PUNCT
eurjchem-792	90	7	5.01	5.01	NUM
eurjchem-792	90	8	;	;	PUNCT
eurjchem-792	90	9	n	n	CCONJ
eurjchem-792	90	10	,	,	PUNCT
eurjchem-792	90	11	12.49	12.49	NUM
eurjchem-792	90	12	%	%	NOUN
eurjchem-792	90	13	.	.	PUNCT
eurjchem-792	91	1	ms	ms	NOUN
eurjchem-792	91	2	(	(	PUNCT
eurjchem-792	91	3	m	m	PROPN
eurjchem-792	91	4	/	/	SYM
eurjchem-792	91	5	z	z	NOUN
eurjchem-792	91	6	):	):	PUNCT
eurjchem-792	91	7	554.07	554.07	NUM
eurjchem-792	91	8	(	(	PUNCT
eurjchem-792	91	9	m+	m+	NUM
eurjchem-792	91	10	)	)	PUNCT
eurjchem-792	91	11	.	.	PUNCT
eurjchem-792	92	1	[	[	X
eurjchem-792	92	2	α]d25	α]d25	NOUN
eurjchem-792	92	3	:	:	PUNCT
eurjchem-792	92	4	‐91.68	‐91.68	PROPN
eurjchem-792	92	5	(	(	PUNCT
eurjchem-792	92	6	c	c	NOUN
eurjchem-792	92	7	=	=	SYM
eurjchem-792	92	8	1.0	1.0	NUM
eurjchem-792	92	9	in	in	ADP
eurjchem-792	92	10	methanol	methanol	NOUN
eurjchem-792	92	11	:	:	PUNCT
eurjchem-792	92	12	methylene	methylene	NOUN
eurjchem-792	92	13	chloride	chloride	NOUN
eurjchem-792	92	14	,	,	PUNCT
eurjchem-792	92	15	1:1	1:1	NUM
eurjchem-792	92	16	)	)	PUNCT
eurjchem-792	92	17	.	.	PUNCT
eurjchem-792	93	1	guruswamy	guruswamy	NOUN
eurjchem-792	93	2	et	et	PROPN
eurjchem-792	93	3	al	al	PROPN
eurjchem-792	93	4	.	.	PUNCT
eurjchem-792	93	5	/	/	SYM
eurjchem-792	93	6	european	european	PROPN
eurjchem-792	93	7	journal	journal	PROPN
eurjchem-792	93	8	of	of	ADP
eurjchem-792	93	9	chemistry	chemistry	NOUN
eurjchem-792	93	10	4	4	NUM
eurjchem-792	93	11	(	(	PUNCT
eurjchem-792	93	12	4	4	NUM
eurjchem-792	93	13	)	)	PUNCT
eurjchem-792	93	14	(	(	PUNCT
eurjchem-792	93	15	2013	2013	NUM
eurjchem-792	93	16	)	)	PUNCT
eurjchem-792	93	17	329‐335	329‐335	PROPN
eurjchem-792	93	18	331	331	NUM
eurjchem-792	93	19	scheme	scheme	NOUN
eurjchem-792	93	20	2	2	NUM
eurjchem-792	93	21	(	(	PUNCT
eurjchem-792	93	22	s)‐10‐(4‐(3‐(5‐methyl‐1h‐benzo[d]imidazol‐2‐yl	s)‐10‐(4‐(3‐(5‐methyl‐1h‐benzo[d]imidazol‐2‐yl	ADJ
eurjchem-792	93	23	thio)‐2‐	thio)‐2‐	NOUN
eurjchem-792	93	24	hydroxypropyl)piperazin‐1‐yl)‐9‐fluoro‐3,7‐dihydro‐3‐methyl‐7‐	hydroxypropyl)piperazin‐1‐yl)‐9‐fluoro‐3,7‐dihydro‐3‐methyl‐7‐	PROPN
eurjchem-792	93	25	oxo‐2h‐[1,4]oxazino[2,3,4‐ij]quinoline‐6‐carboxylic	oxo‐2h‐[1,4]oxazino[2,3,4‐ij]quinoline‐6‐carboxylic	PROPN
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eurjchem-792	93	27	(	(	PUNCT
eurjchem-792	93	28	4b	4b	PROPN
eurjchem-792	93	29	):	):	PUNCT
eurjchem-792	93	30	yield	yield	NOUN
eurjchem-792	93	31	:	:	PUNCT
eurjchem-792	93	32	5.79	5.79	NUM
eurjchem-792	93	33	g	g	NOUN
eurjchem-792	93	34	(	(	PUNCT
eurjchem-792	93	35	82.3	82.3	NUM
eurjchem-792	93	36	%	%	NOUN
eurjchem-792	93	37	)	)	PUNCT
eurjchem-792	93	38	.	.	PUNCT
eurjchem-792	94	1	color	color	NOUN
eurjchem-792	94	2	:	:	PUNCT
eurjchem-792	94	3	off	off	ADP
eurjchem-792	94	4	white	white	ADJ
eurjchem-792	94	5	powder	powder	NOUN
eurjchem-792	94	6	.	.	PUNCT
eurjchem-792	95	1	m.p	m.p	PROPN
eurjchem-792	95	2	.	.	PROPN
eurjchem-792	95	3	:	:	PUNCT
eurjchem-792	96	1	238‐240	238‐240	NUM
eurjchem-792	96	2	°	°	PROPN
eurjchem-792	96	3	c	c	PROPN
eurjchem-792	96	4	.	.	PUNCT
eurjchem-792	97	1	ir	ir	PROPN
eurjchem-792	97	2	(	(	PUNCT
eurjchem-792	97	3	kbr	kbr	PROPN
eurjchem-792	97	4	,	,	PUNCT
eurjchem-792	97	5	v	v	NOUN
eurjchem-792	97	6	,	,	PUNCT
eurjchem-792	97	7	cm‐1	cm‐1	PROPN
eurjchem-792	97	8	):	):	PUNCT
eurjchem-792	97	9	3401	3401	NUM
eurjchem-792	97	10	(	(	PUNCT
eurjchem-792	97	11	oh	oh	INTJ
eurjchem-792	97	12	)	)	PUNCT
eurjchem-792	97	13	,	,	PUNCT
eurjchem-792	97	14	1707	1707	NUM
eurjchem-792	97	15	(	(	PUNCT
eurjchem-792	97	16	c	c	NOUN
eurjchem-792	97	17	=	=	NOUN
eurjchem-792	97	18	o	o	NOUN
eurjchem-792	97	19	)	)	PUNCT
eurjchem-792	97	20	,	,	PUNCT
eurjchem-792	97	21	1624	1624	NUM
eurjchem-792	97	22	(	(	PUNCT
eurjchem-792	97	23	c	c	NOUN
eurjchem-792	97	24	=	=	NOUN
eurjchem-792	97	25	o	o	NOUN
eurjchem-792	97	26	)	)	PUNCT
eurjchem-792	97	27	.	.	PUNCT
eurjchem-792	98	1	1h	1h	NUM
eurjchem-792	98	2	nmr	nmr	NOUN
eurjchem-792	98	3	(	(	PUNCT
eurjchem-792	98	4	300	300	NUM
eurjchem-792	98	5	mhz	mhz	NOUN
eurjchem-792	98	6	,	,	PUNCT
eurjchem-792	98	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-792	98	8	,	,	PUNCT
eurjchem-792	98	9	δ	δ	PROPN
eurjchem-792	98	10	,	,	PUNCT
eurjchem-792	98	11	ppm	ppm	NUM
eurjchem-792	98	12	):	):	PUNCT
eurjchem-792	98	13	1.43‐1.45	1.43‐1.45	NUM
eurjchem-792	98	14	(	(	PUNCT
eurjchem-792	98	15	d	d	PROPN
eurjchem-792	98	16	,	,	PUNCT
eurjchem-792	98	17	3h	3h	NUM
eurjchem-792	98	18	,	,	PUNCT
eurjchem-792	98	19	ch3	ch3	PROPN
eurjchem-792	98	20	,	,	PUNCT
eurjchem-792	98	21	j	j	PROPN
eurjchem-792	98	22	=	=	SYM
eurjchem-792	98	23	6.2	6.2	NUM
eurjchem-792	98	24	hz	hz	NOUN
eurjchem-792	98	25	)	)	PUNCT
eurjchem-792	98	26	,	,	PUNCT
eurjchem-792	98	27	2.43	2.43	NUM
eurjchem-792	98	28	(	(	PUNCT
eurjchem-792	98	29	s	s	PROPN
eurjchem-792	98	30	,	,	PUNCT
eurjchem-792	98	31	3h	3h	NUM
eurjchem-792	98	32	,	,	PUNCT
eurjchem-792	98	33	ar‐ch3	ar‐ch3	ADJ
eurjchem-792	98	34	)	)	PUNCT
eurjchem-792	98	35	,	,	PUNCT
eurjchem-792	98	36	2.69‐2.73	2.69‐2.73	NUM
eurjchem-792	98	37	(	(	PUNCT
eurjchem-792	98	38	m	m	PROPN
eurjchem-792	98	39	,	,	PUNCT
eurjchem-792	98	40	4h	4h	NOUN
eurjchem-792	98	41	,	,	PUNCT
eurjchem-792	98	42	2×ch2	2×ch2	ADJ
eurjchem-792	98	43	)	)	PUNCT
eurjchem-792	98	44	,	,	PUNCT
eurjchem-792	98	45	2.75‐2.77	2.75‐2.77	NUM
eurjchem-792	98	46	(	(	PUNCT
eurjchem-792	98	47	d	d	NOUN
eurjchem-792	98	48	,	,	PUNCT
eurjchem-792	98	49	2h	2h	NUM
eurjchem-792	98	50	,	,	PUNCT
eurjchem-792	98	51	ch2	ch2	PROPN
eurjchem-792	98	52	,	,	PUNCT
eurjchem-792	98	53	j	j	PROPN
eurjchem-792	99	1	=	=	SYM
eurjchem-792	99	2	6.0	6.0	NUM
eurjchem-792	99	3	hz	hz	NOUN
eurjchem-792	99	4	)	)	PUNCT
eurjchem-792	99	5	,	,	PUNCT
eurjchem-792	99	6	3.13‐3.15	3.13‐3.15	NUM
eurjchem-792	99	7	(	(	PUNCT
eurjchem-792	99	8	d	d	PROPN
eurjchem-792	99	9	,	,	PUNCT
eurjchem-792	99	10	2h	2h	NUM
eurjchem-792	99	11	,	,	PUNCT
eurjchem-792	99	12	ch2	ch2	PROPN
eurjchem-792	99	13	,	,	PUNCT
eurjchem-792	99	14	j	j	PROPN
eurjchem-792	99	15	=	=	SYM
eurjchem-792	99	16	6.0	6.0	NUM
eurjchem-792	99	17	hz	hz	NOUN
eurjchem-792	99	18	)	)	PUNCT
eurjchem-792	99	19	,	,	PUNCT
eurjchem-792	99	20	3.62‐	3.62‐	NUM
eurjchem-792	99	21	3.68	3.68	NUM
eurjchem-792	99	22	(	(	PUNCT
eurjchem-792	99	23	m	m	PROPN
eurjchem-792	99	24	,	,	PUNCT
eurjchem-792	99	25	4h	4h	NOUN
eurjchem-792	99	26	,	,	PUNCT
eurjchem-792	99	27	2×ch2	2×ch2	ADJ
eurjchem-792	99	28	)	)	PUNCT
eurjchem-792	99	29	,	,	PUNCT
eurjchem-792	99	30	3.71‐3.76	3.71‐3.76	NUM
eurjchem-792	99	31	(	(	PUNCT
eurjchem-792	99	32	m	m	PROPN
eurjchem-792	99	33	,	,	PUNCT
eurjchem-792	99	34	1h	1h	NUM
eurjchem-792	99	35	,	,	PUNCT
eurjchem-792	99	36	ch	ch	NOUN
eurjchem-792	99	37	)	)	PUNCT
eurjchem-792	99	38	,	,	PUNCT
eurjchem-792	99	39	4.35‐4.39	4.35‐4.39	NUM
eurjchem-792	99	40	(	(	PUNCT
eurjchem-792	99	41	m	m	PROPN
eurjchem-792	99	42	,	,	PUNCT
eurjchem-792	99	43	1h	1h	NUM
eurjchem-792	99	44	,	,	PUNCT
eurjchem-792	99	45	ch	ch	NOUN
eurjchem-792	99	46	)	)	PUNCT
eurjchem-792	99	47	,	,	PUNCT
eurjchem-792	99	48	4.56‐4.58	4.56‐4.58	NUM
eurjchem-792	99	49	(	(	PUNCT
eurjchem-792	99	50	d	d	NOUN
eurjchem-792	99	51	,	,	PUNCT
eurjchem-792	99	52	2h	2h	NUM
eurjchem-792	99	53	,	,	PUNCT
eurjchem-792	99	54	ch2	ch2	PROPN
eurjchem-792	99	55	,	,	PUNCT
eurjchem-792	99	56	j	j	PROPN
eurjchem-792	100	1	=	=	SYM
eurjchem-792	100	2	6.0	6.0	NUM
eurjchem-792	100	3	hz	hz	NOUN
eurjchem-792	100	4	)	)	PUNCT
eurjchem-792	100	5	,	,	PUNCT
eurjchem-792	100	6	5.12	5.12	NUM
eurjchem-792	100	7	(	(	PUNCT
eurjchem-792	100	8	s	s	PROPN
eurjchem-792	100	9	,	,	PUNCT
eurjchem-792	100	10	1h	1h	NUM
eurjchem-792	100	11	,	,	PUNCT
eurjchem-792	100	12	oh	oh	INTJ
eurjchem-792	100	13	,	,	PUNCT
eurjchem-792	100	14	d2o	d2o	NOUN
eurjchem-792	100	15	exchangeable	exchangeable	ADJ
eurjchem-792	100	16	)	)	PUNCT
eurjchem-792	100	17	,	,	PUNCT
eurjchem-792	100	18	5.54	5.54	NUM
eurjchem-792	100	19	(	(	PUNCT
eurjchem-792	100	20	s	s	PROPN
eurjchem-792	100	21	,	,	PUNCT
eurjchem-792	100	22	1h	1h	NUM
eurjchem-792	100	23	,	,	PUNCT
eurjchem-792	100	24	nh	nh	PROPN
eurjchem-792	100	25	,	,	PUNCT
eurjchem-792	100	26	d2o	d2o	PROPN
eurjchem-792	100	27	exchangeable	exchangeable	ADJ
eurjchem-792	100	28	)	)	PUNCT
eurjchem-792	100	29	,	,	PUNCT
eurjchem-792	100	30	7.22‐7.25	7.22‐7.25	NUM
eurjchem-792	100	31	(	(	PUNCT
eurjchem-792	100	32	d	d	PROPN
eurjchem-792	100	33	,	,	PUNCT
eurjchem-792	100	34	1h	1h	NUM
eurjchem-792	100	35	,	,	PUNCT
eurjchem-792	100	36	ar‐h	ar‐h	PROPN
eurjchem-792	100	37	,	,	PUNCT
eurjchem-792	100	38	j	j	PROPN
eurjchem-792	100	39	=	=	SYM
eurjchem-792	100	40	9.0	9.0	NUM
eurjchem-792	100	41	hz	hz	NOUN
eurjchem-792	100	42	)	)	PUNCT
eurjchem-792	100	43	,	,	PUNCT
eurjchem-792	100	44	7.31	7.31	NUM
eurjchem-792	100	45	(	(	PUNCT
eurjchem-792	100	46	s	s	PROPN
eurjchem-792	100	47	,	,	PUNCT
eurjchem-792	100	48	1h	1h	NUM
eurjchem-792	100	49	,	,	PUNCT
eurjchem-792	100	50	ar‐h	ar‐h	NOUN
eurjchem-792	100	51	)	)	PUNCT
eurjchem-792	100	52	,	,	PUNCT
eurjchem-792	100	53	7.45‐7.61	7.45‐7.61	NUM
eurjchem-792	100	54	(	(	PUNCT
eurjchem-792	100	55	m	m	PROPN
eurjchem-792	100	56	,	,	PUNCT
eurjchem-792	100	57	2h	2h	NUM
eurjchem-792	100	58	,	,	PUNCT
eurjchem-792	100	59	ar‐	ar‐	PROPN
eurjchem-792	100	60	h	h	NOUN
eurjchem-792	100	61	)	)	PUNCT
eurjchem-792	100	62	,	,	PUNCT
eurjchem-792	100	63	8.97	8.97	NUM
eurjchem-792	100	64	(	(	PUNCT
eurjchem-792	100	65	s	s	PROPN
eurjchem-792	100	66	,	,	PUNCT
eurjchem-792	100	67	1h	1h	NUM
eurjchem-792	100	68	,	,	PUNCT
eurjchem-792	100	69	c	c	NOUN
eurjchem-792	100	70	=	=	NOUN
eurjchem-792	100	71	ch	ch	NOUN
eurjchem-792	100	72	)	)	PUNCT
eurjchem-792	100	73	,	,	PUNCT
eurjchem-792	100	74	15.08	15.08	NUM
eurjchem-792	100	75	(	(	PUNCT
eurjchem-792	100	76	s	s	PROPN
eurjchem-792	100	77	,	,	PUNCT
eurjchem-792	100	78	1h	1h	NUM
eurjchem-792	100	79	,	,	PUNCT
eurjchem-792	100	80	cooh	cooh	NOUN
eurjchem-792	100	81	,	,	PUNCT
eurjchem-792	100	82	d2o	d2o	PROPN
eurjchem-792	100	83	exchangeable	exchangeable	ADJ
eurjchem-792	100	84	)	)	PUNCT
eurjchem-792	100	85	.	.	PUNCT
eurjchem-792	101	1	13c	13c	NOUN
eurjchem-792	101	2	nmr	nmr	NOUN
eurjchem-792	101	3	(	(	PUNCT
eurjchem-792	101	4	75	75	NUM
eurjchem-792	101	5	mhz	mhz	NOUN
eurjchem-792	101	6	,	,	PUNCT
eurjchem-792	101	7	dmso‐d6	dmso‐d6	NOUN
eurjchem-792	101	8	,	,	PUNCT
eurjchem-792	101	9	ppm	ppm	NOUN
eurjchem-792	101	10	,	,	PUNCT
eurjchem-792	101	11	δ	δ	PROPN
eurjchem-792	101	12	):	):	PUNCT
eurjchem-792	101	13	18.46	18.46	NUM
eurjchem-792	101	14	(	(	PUNCT
eurjchem-792	101	15	ch3	ch3	PROPN
eurjchem-792	101	16	)	)	PUNCT
eurjchem-792	101	17	,	,	PUNCT
eurjchem-792	101	18	26.8	26.8	NUM
eurjchem-792	101	19	(	(	PUNCT
eurjchem-792	101	20	ch3	ch3	PROPN
eurjchem-792	101	21	)	)	PUNCT
eurjchem-792	101	22	,	,	PUNCT
eurjchem-792	101	23	46.34	46.34	NUM
eurjchem-792	101	24	(	(	PUNCT
eurjchem-792	101	25	ch2	ch2	PROPN
eurjchem-792	101	26	)	)	PUNCT
eurjchem-792	101	27	,	,	PUNCT
eurjchem-792	101	28	50.26	50.26	NUM
eurjchem-792	101	29	(	(	PUNCT
eurjchem-792	101	30	2×ch2	2×ch2	ADJ
eurjchem-792	101	31	)	)	PUNCT
eurjchem-792	101	32	,	,	PUNCT
eurjchem-792	101	33	54.89	54.89	NUM
eurjchem-792	101	34	(	(	PUNCT
eurjchem-792	101	35	2×ch2	2×ch2	ADJ
eurjchem-792	101	36	)	)	PUNCT
eurjchem-792	101	37	,	,	PUNCT
eurjchem-792	101	38	60.52	60.52	NUM
eurjchem-792	101	39	(	(	PUNCT
eurjchem-792	101	40	ch2	ch2	PROPN
eurjchem-792	101	41	)	)	PUNCT
eurjchem-792	101	42	,	,	PUNCT
eurjchem-792	101	43	62.18	62.18	NUM
eurjchem-792	101	44	(	(	PUNCT
eurjchem-792	101	45	ch	ch	NOUN
eurjchem-792	101	46	)	)	PUNCT
eurjchem-792	101	47	,	,	PUNCT
eurjchem-792	101	48	64.49	64.49	NUM
eurjchem-792	101	49	(	(	PUNCT
eurjchem-792	101	50	ch	ch	NOUN
eurjchem-792	101	51	)	)	PUNCT
eurjchem-792	101	52	,	,	PUNCT
eurjchem-792	101	53	68.91	68.91	NUM
eurjchem-792	101	54	(	(	PUNCT
eurjchem-792	101	55	ch2	ch2	PROPN
eurjchem-792	101	56	)	)	PUNCT
eurjchem-792	101	57	,	,	PUNCT
eurjchem-792	101	58	107.51	107.51	NUM
eurjchem-792	101	59	(	(	PUNCT
eurjchem-792	101	60	ch	ch	NOUN
eurjchem-792	101	61	)	)	PUNCT
eurjchem-792	101	62	,	,	PUNCT
eurjchem-792	101	63	109.83	109.83	NUM
eurjchem-792	101	64	(	(	PUNCT
eurjchem-792	101	65	c	c	NOUN
eurjchem-792	101	66	)	)	PUNCT
eurjchem-792	101	67	,	,	PUNCT
eurjchem-792	101	68	114.09	114.09	NUM
eurjchem-792	101	69	(	(	PUNCT
eurjchem-792	101	70	ch	ch	NOUN
eurjchem-792	101	71	)	)	PUNCT
eurjchem-792	101	72	,	,	PUNCT
eurjchem-792	101	73	120.33	120.33	NUM
eurjchem-792	101	74	(	(	PUNCT
eurjchem-792	101	75	c	c	NOUN
eurjchem-792	101	76	)	)	PUNCT
eurjchem-792	101	77	,	,	PUNCT
eurjchem-792	101	78	124.18	124.18	NUM
eurjchem-792	101	79	(	(	PUNCT
eurjchem-792	101	80	ch	ch	NOUN
eurjchem-792	101	81	)	)	PUNCT
eurjchem-792	101	82	,	,	PUNCT
eurjchem-792	101	83	130.46	130.46	NUM
eurjchem-792	101	84	(	(	PUNCT
eurjchem-792	101	85	c	c	NOUN
eurjchem-792	101	86	)	)	PUNCT
eurjchem-792	101	87	,	,	PUNCT
eurjchem-792	101	88	134.79	134.79	NUM
eurjchem-792	101	89	(	(	PUNCT
eurjchem-792	101	90	c	c	NOUN
eurjchem-792	101	91	)	)	PUNCT
eurjchem-792	101	92	,	,	PUNCT
eurjchem-792	101	93	140.96	140.96	NUM
eurjchem-792	101	94	(	(	PUNCT
eurjchem-792	101	95	c	c	NOUN
eurjchem-792	101	96	)	)	PUNCT
eurjchem-792	101	97	,	,	PUNCT
eurjchem-792	101	98	146.79	146.79	NUM
eurjchem-792	101	99	(	(	PUNCT
eurjchem-792	101	100	c	c	NOUN
eurjchem-792	101	101	)	)	PUNCT
eurjchem-792	101	102	,	,	PUNCT
eurjchem-792	101	103	152.50	152.50	NUM
eurjchem-792	101	104	(	(	PUNCT
eurjchem-792	101	105	c	c	NOUN
eurjchem-792	101	106	)	)	PUNCT
eurjchem-792	101	107	,	,	PUNCT
eurjchem-792	101	108	154.07	154.07	NUM
eurjchem-792	101	109	(	(	PUNCT
eurjchem-792	101	110	ch	ch	NOUN
eurjchem-792	101	111	)	)	PUNCT
eurjchem-792	101	112	,	,	PUNCT
eurjchem-792	101	113	166.39	166.39	NUM
eurjchem-792	101	114	(	(	PUNCT
eurjchem-792	101	115	c	c	NOUN
eurjchem-792	101	116	=	=	NOUN
eurjchem-792	101	117	o	o	NOUN
eurjchem-792	101	118	)	)	PUNCT
eurjchem-792	101	119	,	,	PUNCT
eurjchem-792	101	120	176.83	176.83	NUM
eurjchem-792	101	121	(	(	PUNCT
eurjchem-792	101	122	c	c	NOUN
eurjchem-792	101	123	=	=	NOUN
eurjchem-792	101	124	o	o	NOUN
eurjchem-792	101	125	)	)	PUNCT
eurjchem-792	101	126	.	.	PUNCT
eurjchem-792	102	1	anal	anal	PROPN
eurjchem-792	102	2	.	.	PUNCT
eurjchem-792	102	3	calcd	calcd	NOUN
eurjchem-792	102	4	.	.	PUNCT
eurjchem-792	103	1	for	for	ADP
eurjchem-792	103	2	c28h30fn5o5s	c28h30fn5o5s	ADJ
eurjchem-792	103	3	:	:	PUNCT
eurjchem-792	103	4	c	c	X
eurjchem-792	103	5	,	,	PUNCT
eurjchem-792	103	6	59.25	59.25	NUM
eurjchem-792	103	7	;	;	PUNCT
eurjchem-792	103	8	h	h	NOUN
eurjchem-792	103	9	,	,	PUNCT
eurjchem-792	103	10	5.33	5.33	NUM
eurjchem-792	103	11	;	;	PUNCT
eurjchem-792	103	12	n	n	CCONJ
eurjchem-792	103	13	,	,	PUNCT
eurjchem-792	103	14	12.34	12.34	NUM
eurjchem-792	103	15	.	.	PUNCT
eurjchem-792	103	16	found	find	VERB
eurjchem-792	103	17	:	:	PUNCT
eurjchem-792	104	1	c	c	X
eurjchem-792	104	2	,	,	PUNCT
eurjchem-792	104	3	59.12	59.12	NUM
eurjchem-792	104	4	;	;	PUNCT
eurjchem-792	104	5	h	h	NOUN
eurjchem-792	104	6	,	,	PUNCT
eurjchem-792	104	7	5.24	5.24	NUM
eurjchem-792	104	8	;	;	PUNCT
eurjchem-792	104	9	n	n	CCONJ
eurjchem-792	104	10	,	,	PUNCT
eurjchem-792	104	11	12.20	12.20	NUM
eurjchem-792	104	12	%	%	NOUN
eurjchem-792	104	13	.	.	PUNCT
eurjchem-792	105	1	ms	ms	NOUN
eurjchem-792	105	2	(	(	PUNCT
eurjchem-792	105	3	m	m	PROPN
eurjchem-792	105	4	/	/	SYM
eurjchem-792	105	5	z	z	NOUN
eurjchem-792	105	6	):	):	PUNCT
eurjchem-792	105	7	568.10	568.10	NUM
eurjchem-792	105	8	(	(	PUNCT
eurjchem-792	105	9	m+	m+	NUM
eurjchem-792	105	10	)	)	PUNCT
eurjchem-792	105	11	.	.	PUNCT
eurjchem-792	106	1	[	[	X
eurjchem-792	106	2	α]d25	α]d25	NOUN
eurjchem-792	106	3	:	:	PUNCT
eurjchem-792	106	4	‐88.10	‐88.10	PROPN
eurjchem-792	106	5	(	(	PUNCT
eurjchem-792	106	6	c	c	NOUN
eurjchem-792	106	7	=	=	SYM
eurjchem-792	106	8	1.0	1.0	NUM
eurjchem-792	106	9	in	in	ADP
eurjchem-792	106	10	methanol	methanol	NOUN
eurjchem-792	106	11	:	:	PUNCT
eurjchem-792	106	12	methylene	methylene	NOUN
eurjchem-792	106	13	chloride	chloride	NOUN
eurjchem-792	106	14	,	,	PUNCT
eurjchem-792	106	15	1:1	1:1	NUM
eurjchem-792	106	16	)	)	PUNCT
eurjchem-792	106	17	.	.	PUNCT
eurjchem-792	107	1	(	(	PUNCT
eurjchem-792	107	2	s)‐10‐(4‐(3‐(5‐methoxy‐1h‐benzo[d]imidazol‐2‐ylthio)‐2‐	s)‐10‐(4‐(3‐(5‐methoxy‐1h‐benzo[d]imidazol‐2‐ylthio)‐2‐	PROPN
eurjchem-792	107	3	hydroxypropyl)piperazin‐1‐yl)‐9‐fluoro‐3,7‐dihydro‐3‐methyl‐7‐	hydroxypropyl)piperazin‐1‐yl)‐9‐fluoro‐3,7‐dihydro‐3‐methyl‐7‐	PROPN
eurjchem-792	107	4	oxo‐2h‐[1,4]oxazino[2,3,4‐ij]quinoline‐6‐carboxylic	oxo‐2h‐[1,4]oxazino[2,3,4‐ij]quinoline‐6‐carboxylic	PROPN
eurjchem-792	107	5	acid	acid	PROPN
eurjchem-792	107	6	(	(	PUNCT
eurjchem-792	107	7	4c	4c	NOUN
eurjchem-792	107	8	):	):	PUNCT
eurjchem-792	107	9	yield	yield	NOUN
eurjchem-792	107	10	:	:	PUNCT
eurjchem-792	107	11	5.53	5.53	NUM
eurjchem-792	107	12	g	g	NOUN
eurjchem-792	107	13	(	(	PUNCT
eurjchem-792	107	14	76.6	76.6	NUM
eurjchem-792	107	15	%	%	NOUN
eurjchem-792	107	16	)	)	PUNCT
eurjchem-792	107	17	.	.	PUNCT
eurjchem-792	108	1	color	color	NOUN
eurjchem-792	108	2	:	:	PUNCT
eurjchem-792	108	3	off	off	ADP
eurjchem-792	108	4	white	white	ADJ
eurjchem-792	108	5	powder	powder	NOUN
eurjchem-792	108	6	.	.	PUNCT
eurjchem-792	109	1	m.p	m.p	PROPN
eurjchem-792	109	2	.	.	PROPN
eurjchem-792	109	3	:	:	PUNCT
eurjchem-792	110	1	234‐238	234‐238	NUM
eurjchem-792	110	2	°	°	PROPN
eurjchem-792	110	3	c	c	X
eurjchem-792	110	4	.	.	PUNCT
eurjchem-792	111	1	ir	ir	PROPN
eurjchem-792	111	2	(	(	PUNCT
eurjchem-792	111	3	kbr	kbr	PROPN
eurjchem-792	111	4	,	,	PUNCT
eurjchem-792	111	5	v	v	NOUN
eurjchem-792	111	6	,	,	PUNCT
eurjchem-792	111	7	cm‐1	cm‐1	PROPN
eurjchem-792	111	8	):	):	PUNCT
eurjchem-792	111	9	3399	3399	NUM
eurjchem-792	111	10	(	(	PUNCT
eurjchem-792	111	11	oh	oh	INTJ
eurjchem-792	111	12	)	)	PUNCT
eurjchem-792	111	13	,	,	PUNCT
eurjchem-792	111	14	1708	1708	NUM
eurjchem-792	111	15	(	(	PUNCT
eurjchem-792	111	16	c	c	NOUN
eurjchem-792	111	17	=	=	NOUN
eurjchem-792	111	18	o	o	NOUN
eurjchem-792	111	19	)	)	PUNCT
eurjchem-792	111	20	,	,	PUNCT
eurjchem-792	111	21	1624	1624	NUM
eurjchem-792	111	22	(	(	PUNCT
eurjchem-792	111	23	c	c	NOUN
eurjchem-792	111	24	=	=	NOUN
eurjchem-792	111	25	o	o	NOUN
eurjchem-792	111	26	)	)	PUNCT
eurjchem-792	111	27	.	.	PUNCT
eurjchem-792	112	1	1h	1h	NUM
eurjchem-792	112	2	nmr	nmr	NOUN
eurjchem-792	112	3	(	(	PUNCT
eurjchem-792	112	4	300	300	NUM
eurjchem-792	112	5	mhz	mhz	NOUN
eurjchem-792	112	6	,	,	PUNCT
eurjchem-792	112	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-792	112	8	,	,	PUNCT
eurjchem-792	112	9	δ	δ	PROPN
eurjchem-792	112	10	,	,	PUNCT
eurjchem-792	112	11	ppm	ppm	NUM
eurjchem-792	112	12	):	):	PUNCT
eurjchem-792	112	13	1.43‐1.45	1.43‐1.45	NUM
eurjchem-792	112	14	(	(	PUNCT
eurjchem-792	112	15	d	d	PROPN
eurjchem-792	112	16	,	,	PUNCT
eurjchem-792	112	17	3h	3h	NUM
eurjchem-792	112	18	,	,	PUNCT
eurjchem-792	112	19	ch3	ch3	PROPN
eurjchem-792	112	20	,	,	PUNCT
eurjchem-792	112	21	j	j	PROPN
eurjchem-792	112	22	=	=	SYM
eurjchem-792	112	23	6.2	6.2	NUM
eurjchem-792	112	24	hz	hz	NOUN
eurjchem-792	112	25	)	)	PUNCT
eurjchem-792	112	26	,	,	PUNCT
eurjchem-792	112	27	2.58‐2.63	2.58‐2.63	NUM
eurjchem-792	112	28	(	(	PUNCT
eurjchem-792	112	29	m	m	PROPN
eurjchem-792	112	30	,	,	PUNCT
eurjchem-792	112	31	4h	4h	NOUN
eurjchem-792	112	32	,	,	PUNCT
eurjchem-792	112	33	2×ch2	2×ch2	ADJ
eurjchem-792	112	34	)	)	PUNCT
eurjchem-792	112	35	,	,	PUNCT
eurjchem-792	112	36	2.68‐2.70	2.68‐2.70	NUM
eurjchem-792	112	37	(	(	PUNCT
eurjchem-792	112	38	d	d	PROPN
eurjchem-792	112	39	,	,	PUNCT
eurjchem-792	112	40	2h	2h	NUM
eurjchem-792	112	41	,	,	PUNCT
eurjchem-792	112	42	ch2	ch2	PROPN
eurjchem-792	112	43	,	,	PUNCT
eurjchem-792	112	44	j	j	PROPN
eurjchem-792	113	1	=	=	SYM
eurjchem-792	113	2	6.0	6.0	NUM
eurjchem-792	113	3	hz	hz	NOUN
eurjchem-792	113	4	)	)	PUNCT
eurjchem-792	113	5	,	,	PUNCT
eurjchem-792	113	6	3.18‐3.20	3.18‐3.20	NUM
eurjchem-792	113	7	(	(	PUNCT
eurjchem-792	113	8	d	d	PROPN
eurjchem-792	113	9	,	,	PUNCT
eurjchem-792	113	10	2h	2h	NUM
eurjchem-792	113	11	,	,	PUNCT
eurjchem-792	113	12	ch2	ch2	PROPN
eurjchem-792	113	13	,	,	PUNCT
eurjchem-792	113	14	j	j	PROPN
eurjchem-792	113	15	=	=	SYM
eurjchem-792	113	16	6.0	6.0	NUM
eurjchem-792	113	17	hz	hz	NOUN
eurjchem-792	113	18	)	)	PUNCT
eurjchem-792	113	19	,	,	PUNCT
eurjchem-792	113	20	3.56‐3.61	3.56‐3.61	NUM
eurjchem-792	113	21	(	(	PUNCT
eurjchem-792	113	22	m	m	PROPN
eurjchem-792	113	23	,	,	PUNCT
eurjchem-792	113	24	4h	4h	NOUN
eurjchem-792	113	25	,	,	PUNCT
eurjchem-792	113	26	2×ch2	2×ch2	ADJ
eurjchem-792	113	27	)	)	PUNCT
eurjchem-792	113	28	,	,	PUNCT
eurjchem-792	113	29	3.76‐3.81	3.76‐3.81	NUM
eurjchem-792	113	30	(	(	PUNCT
eurjchem-792	113	31	m	m	PROPN
eurjchem-792	113	32	,	,	PUNCT
eurjchem-792	113	33	1h	1h	NUM
eurjchem-792	113	34	,	,	PUNCT
eurjchem-792	113	35	ch	ch	NOUN
eurjchem-792	113	36	)	)	PUNCT
eurjchem-792	113	37	,	,	PUNCT
eurjchem-792	113	38	3.86	3.86	NUM
eurjchem-792	113	39	(	(	PUNCT
eurjchem-792	113	40	s	s	PROPN
eurjchem-792	113	41	,	,	PUNCT
eurjchem-792	113	42	3h	3h	NUM
eurjchem-792	113	43	,	,	PUNCT
eurjchem-792	113	44	och3	och3	ADJ
eurjchem-792	113	45	)	)	PUNCT
eurjchem-792	113	46	,	,	PUNCT
eurjchem-792	113	47	4.41‐4.45	4.41‐4.45	NUM
eurjchem-792	113	48	(	(	PUNCT
eurjchem-792	113	49	m	m	PROPN
eurjchem-792	113	50	,	,	PUNCT
eurjchem-792	113	51	1h	1h	NUM
eurjchem-792	113	52	,	,	PUNCT
eurjchem-792	113	53	ch	ch	NOUN
eurjchem-792	113	54	)	)	PUNCT
eurjchem-792	113	55	,	,	PUNCT
eurjchem-792	113	56	4.61‐4.63	4.61‐4.63	X
eurjchem-792	113	57	(	(	PUNCT
eurjchem-792	113	58	d	d	NOUN
eurjchem-792	113	59	,	,	PUNCT
eurjchem-792	113	60	2h	2h	NUM
eurjchem-792	113	61	,	,	PUNCT
eurjchem-792	113	62	ch2	ch2	PROPN
eurjchem-792	113	63	,	,	PUNCT
eurjchem-792	113	64	j	j	PROPN
eurjchem-792	114	1	=	=	SYM
eurjchem-792	114	2	6.0	6.0	NUM
eurjchem-792	114	3	hz	hz	NOUN
eurjchem-792	114	4	)	)	PUNCT
eurjchem-792	114	5	,	,	PUNCT
eurjchem-792	114	6	4.97	4.97	NUM
eurjchem-792	114	7	(	(	PUNCT
eurjchem-792	114	8	s	s	PROPN
eurjchem-792	114	9	,	,	PUNCT
eurjchem-792	114	10	1h	1h	NUM
eurjchem-792	114	11	,	,	PUNCT
eurjchem-792	114	12	oh	oh	INTJ
eurjchem-792	114	13	,	,	PUNCT
eurjchem-792	114	14	d2o	d2o	NOUN
eurjchem-792	114	15	exchangeable	exchangeable	ADJ
eurjchem-792	114	16	)	)	PUNCT
eurjchem-792	114	17	,	,	PUNCT
eurjchem-792	114	18	5.31	5.31	NUM
eurjchem-792	114	19	(	(	PUNCT
eurjchem-792	114	20	s	s	PROPN
eurjchem-792	114	21	,	,	PUNCT
eurjchem-792	114	22	1h	1h	NUM
eurjchem-792	114	23	,	,	PUNCT
eurjchem-792	114	24	nh	nh	PROPN
eurjchem-792	114	25	,	,	PUNCT
eurjchem-792	114	26	d2o	d2o	PROPN
eurjchem-792	114	27	exchangeable	exchangeable	ADJ
eurjchem-792	114	28	)	)	PUNCT
eurjchem-792	114	29	,	,	PUNCT
eurjchem-792	114	30	7.00‐7.03	7.00‐7.03	NUM
eurjchem-792	114	31	(	(	PUNCT
eurjchem-792	114	32	d	d	PROPN
eurjchem-792	114	33	,	,	PUNCT
eurjchem-792	114	34	1h	1h	NUM
eurjchem-792	114	35	,	,	PUNCT
eurjchem-792	114	36	ar‐h	ar‐h	PROPN
eurjchem-792	114	37	j	j	PROPN
eurjchem-792	115	1	=	=	SYM
eurjchem-792	115	2	9.0	9.0	NUM
eurjchem-792	115	3	hz	hz	NOUN
eurjchem-792	115	4	)	)	PUNCT
eurjchem-792	115	5	,	,	PUNCT
eurjchem-792	115	6	7.10	7.10	NUM
eurjchem-792	115	7	(	(	PUNCT
eurjchem-792	115	8	s	s	PROPN
eurjchem-792	115	9	,	,	PUNCT
eurjchem-792	115	10	1h	1h	NUM
eurjchem-792	115	11	,	,	PUNCT
eurjchem-792	115	12	ar‐h	ar‐h	NOUN
eurjchem-792	115	13	)	)	PUNCT
eurjchem-792	115	14	,	,	PUNCT
eurjchem-792	115	15	7.53‐7.63	7.53‐7.63	NUM
eurjchem-792	115	16	(	(	PUNCT
eurjchem-792	115	17	m	m	PROPN
eurjchem-792	115	18	,	,	PUNCT
eurjchem-792	115	19	2h	2h	NUM
eurjchem-792	115	20	,	,	PUNCT
eurjchem-792	115	21	ar‐	ar‐	PROPN
eurjchem-792	115	22	h	h	NOUN
eurjchem-792	115	23	)	)	PUNCT
eurjchem-792	115	24	,	,	PUNCT
eurjchem-792	115	25	8.98	8.98	NUM
eurjchem-792	115	26	(	(	PUNCT
eurjchem-792	115	27	s	s	PROPN
eurjchem-792	115	28	,	,	PUNCT
eurjchem-792	115	29	1h	1h	NUM
eurjchem-792	115	30	,	,	PUNCT
eurjchem-792	115	31	c	c	NOUN
eurjchem-792	115	32	=	=	NOUN
eurjchem-792	115	33	ch	ch	NOUN
eurjchem-792	115	34	)	)	PUNCT
eurjchem-792	115	35	,	,	PUNCT
eurjchem-792	115	36	15.14	15.14	NUM
eurjchem-792	115	37	(	(	PUNCT
eurjchem-792	115	38	s	s	PROPN
eurjchem-792	115	39	,	,	PUNCT
eurjchem-792	115	40	1h	1h	NUM
eurjchem-792	115	41	,	,	PUNCT
eurjchem-792	115	42	cooh	cooh	NOUN
eurjchem-792	115	43	,	,	PUNCT
eurjchem-792	115	44	d2o	d2o	PROPN
eurjchem-792	115	45	exchangeable	exchangeable	ADJ
eurjchem-792	115	46	)	)	PUNCT
eurjchem-792	115	47	.	.	PUNCT
eurjchem-792	116	1	13c	13c	NOUN
eurjchem-792	116	2	nmr	nmr	NOUN
eurjchem-792	116	3	(	(	PUNCT
eurjchem-792	116	4	75	75	NUM
eurjchem-792	116	5	mhz	mhz	NOUN
eurjchem-792	116	6	,	,	PUNCT
eurjchem-792	116	7	dmso‐d6	dmso‐d6	NOUN
eurjchem-792	116	8	,	,	PUNCT
eurjchem-792	116	9	ppm	ppm	NOUN
eurjchem-792	116	10	,	,	PUNCT
eurjchem-792	116	11	δ	δ	PROPN
eurjchem-792	116	12	):	):	PUNCT
eurjchem-792	116	13	18.41	18.41	NUM
eurjchem-792	116	14	(	(	PUNCT
eurjchem-792	116	15	ch3	ch3	PROPN
eurjchem-792	116	16	)	)	PUNCT
eurjchem-792	116	17	,	,	PUNCT
eurjchem-792	116	18	47.10	47.10	NUM
eurjchem-792	116	19	(	(	PUNCT
eurjchem-792	116	20	ch2	ch2	PROPN
eurjchem-792	116	21	)	)	PUNCT
eurjchem-792	116	22	,	,	PUNCT
eurjchem-792	116	23	51.24	51.24	NUM
eurjchem-792	116	24	(	(	PUNCT
eurjchem-792	116	25	2×ch2	2×ch2	ADJ
eurjchem-792	116	26	)	)	PUNCT
eurjchem-792	116	27	,	,	PUNCT
eurjchem-792	116	28	55.18	55.18	NUM
eurjchem-792	116	29	(	(	PUNCT
eurjchem-792	116	30	2×ch2	2×ch2	ADJ
eurjchem-792	116	31	)	)	PUNCT
eurjchem-792	116	32	,	,	PUNCT
eurjchem-792	116	33	58.36	58.36	NUM
eurjchem-792	116	34	(	(	PUNCT
eurjchem-792	116	35	och3	och3	ADJ
eurjchem-792	116	36	)	)	PUNCT
eurjchem-792	116	37	,	,	PUNCT
eurjchem-792	116	38	60.56	60.56	NUM
eurjchem-792	116	39	(	(	PUNCT
eurjchem-792	116	40	ch	ch	NOUN
eurjchem-792	116	41	)	)	PUNCT
eurjchem-792	116	42	,	,	PUNCT
eurjchem-792	116	43	62.12	62.12	NUM
eurjchem-792	116	44	(	(	PUNCT
eurjchem-792	116	45	ch	ch	NOUN
eurjchem-792	116	46	)	)	PUNCT
eurjchem-792	116	47	,	,	PUNCT
eurjchem-792	116	48	64.56	64.56	NUM
eurjchem-792	116	49	(	(	PUNCT
eurjchem-792	116	50	ch	ch	NOUN
eurjchem-792	116	51	)	)	PUNCT
eurjchem-792	116	52	,	,	PUNCT
eurjchem-792	116	53	68.74	68.74	NUM
eurjchem-792	116	54	(	(	PUNCT
eurjchem-792	116	55	ch2	ch2	PROPN
eurjchem-792	116	56	)	)	PUNCT
eurjchem-792	116	57	,	,	PUNCT
eurjchem-792	116	58	102.21	102.21	NUM
eurjchem-792	116	59	(	(	PUNCT
eurjchem-792	116	60	ch	ch	NOUN
eurjchem-792	116	61	)	)	PUNCT
eurjchem-792	116	62	,	,	PUNCT
eurjchem-792	116	63	107.31	107.31	NUM
eurjchem-792	116	64	(	(	PUNCT
eurjchem-792	116	65	ch	ch	NOUN
eurjchem-792	116	66	)	)	PUNCT
eurjchem-792	116	67	,	,	PUNCT
eurjchem-792	116	68	108.31	108.31	NUM
eurjchem-792	116	69	(	(	PUNCT
eurjchem-792	116	70	ch	ch	NOUN
eurjchem-792	116	71	)	)	PUNCT
eurjchem-792	116	72	,	,	PUNCT
eurjchem-792	116	73	110.41	110.41	NUM
eurjchem-792	116	74	(	(	PUNCT
eurjchem-792	116	75	c	c	NOUN
eurjchem-792	116	76	)	)	PUNCT
eurjchem-792	116	77	,	,	PUNCT
eurjchem-792	116	78	117.54	117.54	NUM
eurjchem-792	116	79	(	(	PUNCT
eurjchem-792	116	80	ch	ch	NOUN
eurjchem-792	116	81	)	)	PUNCT
eurjchem-792	116	82	,	,	PUNCT
eurjchem-792	116	83	125.31	125.31	NUM
eurjchem-792	116	84	(	(	PUNCT
eurjchem-792	116	85	c	c	NOUN
eurjchem-792	116	86	)	)	PUNCT
eurjchem-792	116	87	,	,	PUNCT
eurjchem-792	116	88	129.47	129.47	NUM
eurjchem-792	116	89	(	(	PUNCT
eurjchem-792	116	90	c	c	NOUN
eurjchem-792	116	91	)	)	PUNCT
eurjchem-792	116	92	,	,	PUNCT
eurjchem-792	116	93	135.27	135.27	NUM
eurjchem-792	116	94	(	(	PUNCT
eurjchem-792	116	95	c	c	NOUN
eurjchem-792	116	96	)	)	PUNCT
eurjchem-792	116	97	,	,	PUNCT
eurjchem-792	116	98	141.07	141.07	NUM
eurjchem-792	116	99	(	(	PUNCT
eurjchem-792	116	100	c	c	NOUN
eurjchem-792	116	101	)	)	PUNCT
eurjchem-792	116	102	,	,	PUNCT
eurjchem-792	116	103	146.53	146.53	NUM
eurjchem-792	116	104	(	(	PUNCT
eurjchem-792	116	105	c	c	NOUN
eurjchem-792	116	106	)	)	PUNCT
eurjchem-792	116	107	,	,	PUNCT
eurjchem-792	116	108	149.11	149.11	NUM
eurjchem-792	116	109	(	(	PUNCT
eurjchem-792	116	110	c	c	NOUN
eurjchem-792	116	111	)	)	PUNCT
eurjchem-792	116	112	,	,	PUNCT
eurjchem-792	116	113	152.28	152.28	NUM
eurjchem-792	116	114	(	(	PUNCT
eurjchem-792	116	115	c	c	NOUN
eurjchem-792	116	116	)	)	PUNCT
eurjchem-792	116	117	,	,	PUNCT
eurjchem-792	116	118	154.32	154.32	NUM
eurjchem-792	116	119	(	(	PUNCT
eurjchem-792	116	120	ch	ch	NOUN
eurjchem-792	116	121	)	)	PUNCT
eurjchem-792	116	122	,	,	PUNCT
eurjchem-792	116	123	158.41	158.41	NUM
eurjchem-792	116	124	(	(	PUNCT
eurjchem-792	116	125	c	c	NOUN
eurjchem-792	116	126	)	)	PUNCT
eurjchem-792	116	127	,	,	PUNCT
eurjchem-792	116	128	166.56	166.56	NUM
eurjchem-792	116	129	(	(	PUNCT
eurjchem-792	116	130	c	c	NOUN
eurjchem-792	116	131	=	=	NOUN
eurjchem-792	116	132	o	o	NOUN
eurjchem-792	116	133	)	)	PUNCT
eurjchem-792	116	134	,	,	PUNCT
eurjchem-792	116	135	177.02	177.02	NUM
eurjchem-792	116	136	(	(	PUNCT
eurjchem-792	116	137	c	c	NOUN
eurjchem-792	116	138	=	=	NOUN
eurjchem-792	116	139	o	o	NOUN
eurjchem-792	116	140	)	)	PUNCT
eurjchem-792	116	141	.	.	PUNCT
eurjchem-792	117	1	anal	anal	PROPN
eurjchem-792	117	2	.	.	PUNCT
eurjchem-792	117	3	calcd	calcd	NOUN
eurjchem-792	117	4	.	.	PUNCT
eurjchem-792	118	1	for	for	ADP
eurjchem-792	118	2	c28h30fn5o6s	c28h30fn5o6s	NOUN
eurjchem-792	118	3	:	:	PUNCT
eurjchem-792	118	4	c	c	X
eurjchem-792	118	5	,	,	PUNCT
eurjchem-792	118	6	57.62	57.62	NUM
eurjchem-792	118	7	;	;	PUNCT
eurjchem-792	118	8	h	h	NOUN
eurjchem-792	118	9	,	,	PUNCT
eurjchem-792	118	10	5.18	5.18	NUM
eurjchem-792	118	11	;	;	PUNCT
eurjchem-792	118	12	n	n	CCONJ
eurjchem-792	118	13	,	,	PUNCT
eurjchem-792	118	14	12.00	12.00	NUM
eurjchem-792	118	15	.	.	PUNCT
eurjchem-792	118	16	found	find	VERB
eurjchem-792	118	17	:	:	PUNCT
eurjchem-792	119	1	c	c	X
eurjchem-792	119	2	,	,	PUNCT
eurjchem-792	119	3	57.56	57.56	NUM
eurjchem-792	119	4	;	;	PUNCT
eurjchem-792	119	5	h	h	NOUN
eurjchem-792	119	6	,	,	PUNCT
eurjchem-792	119	7	5.07	5.07	NUM
eurjchem-792	119	8	;	;	PUNCT
eurjchem-792	119	9	n	n	CCONJ
eurjchem-792	119	10	,	,	PUNCT
eurjchem-792	119	11	11.87	11.87	NUM
eurjchem-792	119	12	%	%	NOUN
eurjchem-792	119	13	.	.	PUNCT
eurjchem-792	120	1	ms	ms	NOUN
eurjchem-792	120	2	(	(	PUNCT
eurjchem-792	120	3	m	m	PROPN
eurjchem-792	120	4	/	/	SYM
eurjchem-792	120	5	z	z	NOUN
eurjchem-792	120	6	):	):	PUNCT
eurjchem-792	120	7	584.10	584.10	NUM
eurjchem-792	120	8	(	(	PUNCT
eurjchem-792	120	9	m+	m+	NUM
eurjchem-792	120	10	)	)	PUNCT
eurjchem-792	120	11	.	.	PUNCT
eurjchem-792	121	1	[	[	X
eurjchem-792	121	2	α]d25	α]d25	NOUN
eurjchem-792	121	3	:	:	PUNCT
eurjchem-792	121	4	‐64.80	‐64.80	PROPN
eurjchem-792	121	5	(	(	PUNCT
eurjchem-792	121	6	c	c	X
eurjchem-792	121	7	=	=	SYM
eurjchem-792	121	8	1.0	1.0	NUM
eurjchem-792	121	9	in	in	ADP
eurjchem-792	121	10	methanol	methanol	NOUN
eurjchem-792	121	11	:	:	PUNCT
eurjchem-792	121	12	methylene	methylene	NOUN
eurjchem-792	121	13	chloride	chloride	NOUN
eurjchem-792	121	14	,	,	PUNCT
eurjchem-792	121	15	1:1	1:1	NUM
eurjchem-792	121	16	)	)	PUNCT
eurjchem-792	121	17	.	.	PUNCT
eurjchem-792	122	1	(	(	PUNCT
eurjchem-792	122	2	s)‐10‐(4‐(3‐(5‐(difluoromethoxy)‐1h‐benzo[d]imidazol‐2‐	s)‐10‐(4‐(3‐(5‐(difluoromethoxy)‐1h‐benzo[d]imidazol‐2‐	VERB
eurjchem-792	122	3	ylthio)‐2‐hydroxypropyl)piperazin‐1‐yl)‐9‐fluoro‐3,7‐dihydro‐3‐	ylthio)‐2‐hydroxypropyl)piperazin‐1‐yl)‐9‐fluoro‐3,7‐dihydro‐3‐	NOUN
eurjchem-792	122	4	methyl‐7‐oxo‐2h‐[1,4]oxazino[2,3,4‐ij]quinoline‐6‐carboxylic	methyl‐7‐oxo‐2h‐[1,4]oxazino[2,3,4‐ij]quinoline‐6‐carboxylic	NOUN
eurjchem-792	122	5	acid	acid	NOUN
eurjchem-792	122	6	(	(	PUNCT
eurjchem-792	122	7	4d	4d	NUM
eurjchem-792	122	8	):	):	PUNCT
eurjchem-792	122	9	yield	yield	NOUN
eurjchem-792	122	10	:	:	PUNCT
eurjchem-792	122	11	6.41	6.41	NUM
eurjchem-792	122	12	g	g	NOUN
eurjchem-792	122	13	(	(	PUNCT
eurjchem-792	122	14	74.8	74.8	NUM
eurjchem-792	122	15	%	%	NOUN
eurjchem-792	122	16	)	)	PUNCT
eurjchem-792	122	17	.	.	PUNCT
eurjchem-792	123	1	color	color	NOUN
eurjchem-792	123	2	:	:	PUNCT
eurjchem-792	123	3	off	off	ADP
eurjchem-792	123	4	white	white	ADJ
eurjchem-792	123	5	powder	powder	NOUN
eurjchem-792	123	6	.	.	PUNCT
eurjchem-792	124	1	m.p	m.p	PROPN
eurjchem-792	124	2	.	.	PROPN
eurjchem-792	124	3	:	:	PUNCT
eurjchem-792	125	1	222‐225	222‐225	PROPN
eurjchem-792	125	2	°	°	SYM
eurjchem-792	125	3	c	c	VERB
eurjchem-792	125	4	.	.	PUNCT
eurjchem-792	126	1	ir	ir	PROPN
eurjchem-792	126	2	(	(	PUNCT
eurjchem-792	126	3	kbr	kbr	PROPN
eurjchem-792	126	4	,	,	PUNCT
eurjchem-792	126	5	v	v	NOUN
eurjchem-792	126	6	,	,	PUNCT
eurjchem-792	126	7	cm‐1	cm‐1	PROPN
eurjchem-792	126	8	):	):	PUNCT
eurjchem-792	126	9	3400	3400	NUM
eurjchem-792	126	10	(	(	PUNCT
eurjchem-792	126	11	oh	oh	INTJ
eurjchem-792	126	12	)	)	PUNCT
eurjchem-792	126	13	,	,	PUNCT
eurjchem-792	126	14	1709	1709	NUM
eurjchem-792	126	15	(	(	PUNCT
eurjchem-792	126	16	c	c	NOUN
eurjchem-792	126	17	=	=	NOUN
eurjchem-792	126	18	o	o	NOUN
eurjchem-792	126	19	)	)	PUNCT
eurjchem-792	126	20	,	,	PUNCT
eurjchem-792	126	21	1623	1623	NUM
eurjchem-792	126	22	(	(	PUNCT
eurjchem-792	126	23	c	c	NOUN
eurjchem-792	126	24	=	=	NOUN
eurjchem-792	126	25	o	o	NOUN
eurjchem-792	126	26	)	)	PUNCT
eurjchem-792	126	27	.	.	PUNCT
eurjchem-792	127	1	1h‐nmr	1h‐nmr	NUM
eurjchem-792	127	2	(	(	PUNCT
eurjchem-792	127	3	300	300	NUM
eurjchem-792	127	4	mhz	mhz	NOUN
eurjchem-792	127	5	,	,	PUNCT
eurjchem-792	127	6	dmso‐d6	dmso‐d6	PROPN
eurjchem-792	127	7	,	,	PUNCT
eurjchem-792	127	8	δ	δ	PROPN
eurjchem-792	127	9	,	,	PUNCT
eurjchem-792	127	10	ppm	ppm	NUM
eurjchem-792	127	11	):	):	PUNCT
eurjchem-792	127	12	1.43‐1.45	1.43‐1.45	NUM
eurjchem-792	127	13	(	(	PUNCT
eurjchem-792	127	14	d	d	PROPN
eurjchem-792	127	15	,	,	PUNCT
eurjchem-792	127	16	3h	3h	NUM
eurjchem-792	127	17	,	,	PUNCT
eurjchem-792	127	18	ch3	ch3	PROPN
eurjchem-792	127	19	,	,	PUNCT
eurjchem-792	127	20	j	j	PROPN
eurjchem-792	127	21	=	=	SYM
eurjchem-792	127	22	6.2	6.2	NUM
eurjchem-792	127	23	hz	hz	NOUN
eurjchem-792	127	24	)	)	PUNCT
eurjchem-792	127	25	,	,	PUNCT
eurjchem-792	127	26	2.48‐2.53	2.48‐2.53	NUM
eurjchem-792	127	27	(	(	PUNCT
eurjchem-792	127	28	m	m	PROPN
eurjchem-792	127	29	,	,	PUNCT
eurjchem-792	127	30	4h	4h	NOUN
eurjchem-792	127	31	,	,	PUNCT
eurjchem-792	127	32	2×ch2	2×ch2	ADJ
eurjchem-792	127	33	)	)	PUNCT
eurjchem-792	127	34	,	,	PUNCT
eurjchem-792	127	35	2.81‐2.83	2.81‐2.83	NUM
eurjchem-792	127	36	(	(	PUNCT
eurjchem-792	127	37	d	d	NOUN
eurjchem-792	127	38	,	,	PUNCT
eurjchem-792	127	39	2h	2h	NUM
eurjchem-792	127	40	,	,	PUNCT
eurjchem-792	127	41	ch2	ch2	PROPN
eurjchem-792	127	42	,	,	PUNCT
eurjchem-792	127	43	j	j	PROPN
eurjchem-792	128	1	=	=	SYM
eurjchem-792	128	2	6.0	6.0	NUM
eurjchem-792	128	3	hz	hz	NOUN
eurjchem-792	128	4	)	)	PUNCT
eurjchem-792	128	5	,	,	PUNCT
eurjchem-792	128	6	3.20‐3.22	3.20‐3.22	NUM
eurjchem-792	128	7	(	(	PUNCT
eurjchem-792	128	8	d	d	NOUN
eurjchem-792	128	9	,	,	PUNCT
eurjchem-792	128	10	2h	2h	NUM
eurjchem-792	128	11	,	,	PUNCT
eurjchem-792	128	12	ch2	ch2	PROPN
eurjchem-792	128	13	,	,	PUNCT
eurjchem-792	128	14	j	j	PROPN
eurjchem-792	128	15	=	=	SYM
eurjchem-792	128	16	6.0	6.0	NUM
eurjchem-792	128	17	hz	hz	NOUN
eurjchem-792	128	18	)	)	PUNCT
eurjchem-792	128	19	,	,	PUNCT
eurjchem-792	128	20	3.52‐3.57	3.52‐3.57	NUM
eurjchem-792	128	21	(	(	PUNCT
eurjchem-792	128	22	m	m	PROPN
eurjchem-792	128	23	,	,	PUNCT
eurjchem-792	128	24	4h	4h	NOUN
eurjchem-792	128	25	,	,	PUNCT
eurjchem-792	128	26	2×ch2	2×ch2	ADJ
eurjchem-792	128	27	)	)	PUNCT
eurjchem-792	128	28	,	,	PUNCT
eurjchem-792	128	29	3.66‐3.70	3.66‐3.70	NUM
eurjchem-792	128	30	(	(	PUNCT
eurjchem-792	128	31	m	m	PROPN
eurjchem-792	128	32	,	,	PUNCT
eurjchem-792	128	33	1h	1h	NUM
eurjchem-792	128	34	,	,	PUNCT
eurjchem-792	128	35	ch	ch	NOUN
eurjchem-792	128	36	)	)	PUNCT
eurjchem-792	128	37	,	,	PUNCT
eurjchem-792	128	38	4.37‐4.41	4.37‐4.41	PROPN
eurjchem-792	128	39	(	(	PUNCT
eurjchem-792	128	40	m	m	PROPN
eurjchem-792	128	41	,	,	PUNCT
eurjchem-792	128	42	1h	1h	NUM
eurjchem-792	128	43	,	,	PUNCT
eurjchem-792	128	44	ch	ch	NOUN
eurjchem-792	128	45	)	)	PUNCT
eurjchem-792	128	46	,	,	PUNCT
eurjchem-792	128	47	4.58‐4.60	4.58‐4.60	NUM
eurjchem-792	128	48	(	(	PUNCT
eurjchem-792	128	49	d	d	NOUN
eurjchem-792	128	50	,	,	PUNCT
eurjchem-792	128	51	2h	2h	NUM
eurjchem-792	128	52	,	,	PUNCT
eurjchem-792	128	53	ch2	ch2	PROPN
eurjchem-792	128	54	,	,	PUNCT
eurjchem-792	128	55	j	j	PROPN
eurjchem-792	129	1	=	=	SYM
eurjchem-792	129	2	6.0	6.0	NUM
eurjchem-792	129	3	hz	hz	NOUN
eurjchem-792	129	4	)	)	PUNCT
eurjchem-792	129	5	,	,	PUNCT
eurjchem-792	129	6	5.12	5.12	NUM
eurjchem-792	129	7	(	(	PUNCT
eurjchem-792	129	8	s	s	PROPN
eurjchem-792	129	9	,	,	PUNCT
eurjchem-792	129	10	1h	1h	NUM
eurjchem-792	129	11	,	,	PUNCT
eurjchem-792	129	12	oh	oh	INTJ
eurjchem-792	129	13	,	,	PUNCT
eurjchem-792	129	14	d2o	d2o	NOUN
eurjchem-792	129	15	exchangeable	exchangeable	ADJ
eurjchem-792	129	16	)	)	PUNCT
eurjchem-792	129	17	,	,	PUNCT
eurjchem-792	129	18	5.53	5.53	NUM
eurjchem-792	129	19	(	(	PUNCT
eurjchem-792	129	20	s	s	PROPN
eurjchem-792	129	21	,	,	PUNCT
eurjchem-792	129	22	1h	1h	NUM
eurjchem-792	129	23	,	,	PUNCT
eurjchem-792	129	24	nh	nh	PROPN
eurjchem-792	129	25	,	,	PUNCT
eurjchem-792	129	26	d2o	d2o	PROPN
eurjchem-792	129	27	exchangeable	exchangeable	ADJ
eurjchem-792	129	28	)	)	PUNCT
eurjchem-792	129	29	,	,	PUNCT
eurjchem-792	129	30	6.98	6.98	NUM
eurjchem-792	129	31	(	(	PUNCT
eurjchem-792	129	32	m	m	PROPN
eurjchem-792	129	33	,	,	PUNCT
eurjchem-792	129	34	1h	1h	NUM
eurjchem-792	129	35	,	,	PUNCT
eurjchem-792	129	36	ar‐h	ar‐h	NOUN
eurjchem-792	129	37	)	)	PUNCT
eurjchem-792	129	38	,	,	PUNCT
eurjchem-792	129	39	7.23‐7.26	7.23‐7.26	NUM
eurjchem-792	129	40	(	(	PUNCT
eurjchem-792	129	41	m	m	PROPN
eurjchem-792	129	42	,	,	PUNCT
eurjchem-792	129	43	2h	2h	NUM
eurjchem-792	129	44	,	,	PUNCT
eurjchem-792	129	45	ar‐h	ar‐h	NOUN
eurjchem-792	129	46	)	)	PUNCT
eurjchem-792	129	47	,	,	PUNCT
eurjchem-792	129	48	7.42	7.42	NUM
eurjchem-792	129	49	(	(	PUNCT
eurjchem-792	129	50	s	s	PROPN
eurjchem-792	129	51	,	,	PUNCT
eurjchem-792	129	52	1h	1h	NUM
eurjchem-792	129	53	,	,	PUNCT
eurjchem-792	129	54	chf2	chf2	PROPN
eurjchem-792	129	55	)	)	PUNCT
eurjchem-792	129	56	,	,	PUNCT
eurjchem-792	129	57	7.55‐7.59	7.55‐7.59	NUM
eurjchem-792	129	58	(	(	PUNCT
eurjchem-792	129	59	d	d	PROPN
eurjchem-792	129	60	,	,	PUNCT
eurjchem-792	129	61	1h	1h	NUM
eurjchem-792	129	62	,	,	PUNCT
eurjchem-792	129	63	ar‐h	ar‐h	PROPN
eurjchem-792	129	64	,	,	PUNCT
eurjchem-792	129	65	j	j	PROPN
eurjchem-792	129	66	=	=	PROPN
eurjchem-792	129	67	12.0	12.0	NUM
eurjchem-792	129	68	hz	hz	NOUN
eurjchem-792	129	69	)	)	PUNCT
eurjchem-792	129	70	,	,	PUNCT
eurjchem-792	129	71	8.98	8.98	NUM
eurjchem-792	129	72	(	(	PUNCT
eurjchem-792	129	73	s	s	PROPN
eurjchem-792	129	74	,	,	PUNCT
eurjchem-792	129	75	1h	1h	NUM
eurjchem-792	129	76	,	,	PUNCT
eurjchem-792	129	77	c	c	NOUN
eurjchem-792	129	78	=	=	NOUN
eurjchem-792	129	79	ch	ch	NOUN
eurjchem-792	129	80	)	)	PUNCT
eurjchem-792	129	81	,	,	PUNCT
eurjchem-792	129	82	15.17	15.17	NUM
eurjchem-792	129	83	(	(	PUNCT
eurjchem-792	129	84	s	s	PROPN
eurjchem-792	129	85	,	,	PUNCT
eurjchem-792	129	86	1h	1h	NUM
eurjchem-792	129	87	,	,	PUNCT
eurjchem-792	129	88	cooh	cooh	NOUN
eurjchem-792	129	89	,	,	PUNCT
eurjchem-792	129	90	d2o	d2o	PROPN
eurjchem-792	129	91	exchangeable	exchangeable	ADJ
eurjchem-792	129	92	)	)	PUNCT
eurjchem-792	129	93	.	.	PUNCT
eurjchem-792	130	1	13c	13c	NOUN
eurjchem-792	130	2	nmr	nmr	NOUN
eurjchem-792	130	3	(	(	PUNCT
eurjchem-792	130	4	75	75	NUM
eurjchem-792	130	5	mhz	mhz	NOUN
eurjchem-792	130	6	,	,	PUNCT
eurjchem-792	130	7	dmso‐d6	dmso‐d6	NOUN
eurjchem-792	130	8	,	,	PUNCT
eurjchem-792	130	9	ppm	ppm	NOUN
eurjchem-792	130	10	,	,	PUNCT
eurjchem-792	130	11	δ	δ	PROPN
eurjchem-792	130	12	):	):	PUNCT
eurjchem-792	130	13	18.41	18.41	NUM
eurjchem-792	130	14	(	(	PUNCT
eurjchem-792	130	15	ch3	ch3	PROPN
eurjchem-792	130	16	)	)	PUNCT
eurjchem-792	130	17	,	,	PUNCT
eurjchem-792	130	18	47.48	47.48	NUM
eurjchem-792	130	19	(	(	PUNCT
eurjchem-792	130	20	ch2	ch2	PROPN
eurjchem-792	130	21	)	)	PUNCT
eurjchem-792	130	22	,	,	PUNCT
eurjchem-792	130	23	50.36	50.36	NUM
eurjchem-792	130	24	(	(	PUNCT
eurjchem-792	130	25	2×ch2	2×ch2	ADJ
eurjchem-792	130	26	)	)	PUNCT
eurjchem-792	130	27	,	,	PUNCT
eurjchem-792	130	28	55.11	55.11	NUM
eurjchem-792	130	29	(	(	PUNCT
eurjchem-792	130	30	2×ch2	2×ch2	ADJ
eurjchem-792	130	31	)	)	PUNCT
eurjchem-792	130	32	,	,	PUNCT
eurjchem-792	130	33	60.24	60.24	NUM
eurjchem-792	130	34	(	(	PUNCT
eurjchem-792	130	35	ch2	ch2	PROPN
eurjchem-792	130	36	)	)	PUNCT
eurjchem-792	130	37	,	,	PUNCT
eurjchem-792	130	38	62.31	62.31	NUM
eurjchem-792	130	39	(	(	PUNCT
eurjchem-792	130	40	ch	ch	NOUN
eurjchem-792	130	41	)	)	PUNCT
eurjchem-792	130	42	,	,	PUNCT
eurjchem-792	130	43	64.62	64.62	NUM
eurjchem-792	130	44	(	(	PUNCT
eurjchem-792	130	45	ch	ch	NOUN
eurjchem-792	130	46	)	)	PUNCT
eurjchem-792	130	47	,	,	PUNCT
eurjchem-792	130	48	68.56	68.56	NUM
eurjchem-792	130	49	(	(	PUNCT
eurjchem-792	130	50	ch2	ch2	PROPN
eurjchem-792	130	51	)	)	PUNCT
eurjchem-792	130	52	,	,	PUNCT
eurjchem-792	130	53	103.12	103.12	NUM
eurjchem-792	130	54	(	(	PUNCT
eurjchem-792	130	55	ch	ch	NOUN
eurjchem-792	130	56	)	)	PUNCT
eurjchem-792	130	57	,	,	PUNCT
eurjchem-792	130	58	108.09	108.09	NUM
eurjchem-792	130	59	(	(	PUNCT
eurjchem-792	130	60	ch	ch	NOUN
eurjchem-792	130	61	)	)	PUNCT
eurjchem-792	130	62	,	,	PUNCT
eurjchem-792	130	63	110.23	110.23	NUM
eurjchem-792	130	64	(	(	PUNCT
eurjchem-792	130	65	ch	ch	NOUN
eurjchem-792	130	66	)	)	PUNCT
eurjchem-792	130	67	,	,	PUNCT
eurjchem-792	130	68	110.85	110.85	NUM
eurjchem-792	130	69	(	(	PUNCT
eurjchem-792	130	70	c	c	NOUN
eurjchem-792	130	71	)	)	PUNCT
eurjchem-792	130	72	,	,	PUNCT
eurjchem-792	130	73	118.61(ch	118.61(ch	NOUN
eurjchem-792	130	74	)	)	PUNCT
eurjchem-792	130	75	,	,	PUNCT
eurjchem-792	130	76	120.34	120.34	NUM
eurjchem-792	130	77	(	(	PUNCT
eurjchem-792	130	78	c	c	NOUN
eurjchem-792	130	79	)	)	PUNCT
eurjchem-792	130	80	,	,	PUNCT
eurjchem-792	130	81	130.41	130.41	NUM
eurjchem-792	130	82	(	(	PUNCT
eurjchem-792	130	83	c	c	NOUN
eurjchem-792	130	84	)	)	PUNCT
eurjchem-792	130	85	,	,	PUNCT
eurjchem-792	130	86	133.45	133.45	NUM
eurjchem-792	130	87	(	(	PUNCT
eurjchem-792	130	88	c	c	NOUN
eurjchem-792	130	89	)	)	PUNCT
eurjchem-792	130	90	,	,	PUNCT
eurjchem-792	130	91	142.56	142.56	NUM
eurjchem-792	130	92	(	(	PUNCT
eurjchem-792	130	93	c	c	NOUN
eurjchem-792	130	94	)	)	PUNCT
eurjchem-792	130	95	,	,	PUNCT
eurjchem-792	130	96	148.35	148.35	NUM
eurjchem-792	130	97	(	(	PUNCT
eurjchem-792	130	98	c	c	NOUN
eurjchem-792	130	99	)	)	PUNCT
eurjchem-792	130	100	,	,	PUNCT
eurjchem-792	130	101	152.36	152.36	NUM
eurjchem-792	130	102	(	(	PUNCT
eurjchem-792	130	103	c	c	NOUN
eurjchem-792	130	104	)	)	PUNCT
eurjchem-792	130	105	,	,	PUNCT
eurjchem-792	130	106	154.60	154.60	NUM
eurjchem-792	130	107	(	(	PUNCT
eurjchem-792	130	108	c	c	NOUN
eurjchem-792	130	109	)	)	PUNCT
eurjchem-792	130	110	,	,	PUNCT
eurjchem-792	130	111	158.62	158.62	NUM
eurjchem-792	130	112	(	(	PUNCT
eurjchem-792	130	113	c	c	NOUN
eurjchem-792	130	114	)	)	PUNCT
eurjchem-792	130	115	,	,	PUNCT
eurjchem-792	130	116	166.84	166.84	NUM
eurjchem-792	130	117	(	(	PUNCT
eurjchem-792	130	118	c	c	NOUN
eurjchem-792	130	119	=	=	NOUN
eurjchem-792	130	120	o	o	NOUN
eurjchem-792	130	121	)	)	PUNCT
eurjchem-792	130	122	,	,	PUNCT
eurjchem-792	130	123	177.26	177.26	NUM
eurjchem-792	130	124	(	(	PUNCT
eurjchem-792	130	125	c	c	NOUN
eurjchem-792	130	126	=	=	NOUN
eurjchem-792	130	127	o	o	NOUN
eurjchem-792	130	128	)	)	PUNCT
eurjchem-792	130	129	.	.	PUNCT
eurjchem-792	131	1	anal	anal	PROPN
eurjchem-792	131	2	.	.	PUNCT
eurjchem-792	131	3	calcd	calcd	NOUN
eurjchem-792	131	4	.	.	PUNCT
eurjchem-792	132	1	for	for	ADP
eurjchem-792	132	2	c28h28f3n5o6s	c28h28f3n5o6s	PROPN
eurjchem-792	132	3	:	:	PUNCT
eurjchem-792	132	4	c	c	X
eurjchem-792	132	5	,	,	PUNCT
eurjchem-792	132	6	54.28	54.28	NUM
eurjchem-792	132	7	;	;	PUNCT
eurjchem-792	132	8	h	h	NOUN
eurjchem-792	132	9	,	,	PUNCT
eurjchem-792	132	10	4.55	4.55	NUM
eurjchem-792	132	11	;	;	PUNCT
eurjchem-792	132	12	n	n	CCONJ
eurjchem-792	132	13	,	,	PUNCT
eurjchem-792	132	14	11.30	11.30	NUM
eurjchem-792	132	15	.	.	PUNCT
eurjchem-792	133	1	found	find	VERB
eurjchem-792	133	2	:	:	PUNCT
eurjchem-792	134	1	c	c	X
eurjchem-792	134	2	,	,	PUNCT
eurjchem-792	134	3	54.13	54.13	NUM
eurjchem-792	134	4	;	;	PUNCT
eurjchem-792	134	5	h	h	NOUN
eurjchem-792	134	6	,	,	PUNCT
eurjchem-792	134	7	4.40	4.40	NUM
eurjchem-792	134	8	;	;	PUNCT
eurjchem-792	134	9	n	n	CCONJ
eurjchem-792	134	10	,	,	PUNCT
eurjchem-792	134	11	11.18	11.18	NUM
eurjchem-792	134	12	%	%	NOUN
eurjchem-792	134	13	.	.	PUNCT
eurjchem-792	135	1	ms	ms	NOUN
eurjchem-792	135	2	(	(	PUNCT
eurjchem-792	135	3	m	m	PROPN
eurjchem-792	135	4	/	/	SYM
eurjchem-792	135	5	z	z	NOUN
eurjchem-792	135	6	):	):	PUNCT
eurjchem-792	135	7	588.05	588.05	NUM
eurjchem-792	135	8	(	(	PUNCT
eurjchem-792	135	9	m+	m+	NUM
eurjchem-792	135	10	)	)	PUNCT
eurjchem-792	135	11	.	.	PUNCT
eurjchem-792	136	1	[	[	X
eurjchem-792	136	2	α]d25	α]d25	NOUN
eurjchem-792	136	3	:	:	PUNCT
eurjchem-792	136	4	‐	‐	NOUN
eurjchem-792	136	5	36.10	36.10	NUM
eurjchem-792	136	6	(	(	PUNCT
eurjchem-792	136	7	c	c	NOUN
eurjchem-792	136	8	=	=	SYM
eurjchem-792	136	9	1.0	1.0	NUM
eurjchem-792	136	10	in	in	ADP
eurjchem-792	136	11	methanol	methanol	NOUN
eurjchem-792	136	12	:	:	PUNCT
eurjchem-792	136	13	methylene	methylene	NOUN
eurjchem-792	136	14	chloride	chloride	NOUN
eurjchem-792	136	15	,	,	PUNCT
eurjchem-792	136	16	1:1	1:1	NUM
eurjchem-792	136	17	)	)	PUNCT
eurjchem-792	136	18	.	.	PUNCT
eurjchem-792	137	1	(	(	PUNCT
eurjchem-792	137	2	s)‐10‐(4‐(3‐(5‐chloro‐1h‐benzo[d]imidazol‐2‐ylthio)‐2‐	s)‐10‐(4‐(3‐(5‐chloro‐1h‐benzo[d]imidazol‐2‐ylthio)‐2‐	PROPN
eurjchem-792	137	3	hydroxypropyl)piperazin‐1‐yl)‐9‐fluoro‐3,7‐dihydro‐3‐methyl‐7‐	hydroxypropyl)piperazin‐1‐yl)‐9‐fluoro‐3,7‐dihydro‐3‐methyl‐7‐	PROPN
eurjchem-792	137	4	oxo‐2h‐[1,4]oxazino[2,3,4‐ij]quinoline‐6‐carboxylic	oxo‐2h‐[1,4]oxazino[2,3,4‐ij]quinoline‐6‐carboxylic	PROPN
eurjchem-792	137	5	acid	acid	PROPN
eurjchem-792	137	6	(	(	PUNCT
eurjchem-792	137	7	4e	4e	NOUN
eurjchem-792	137	8	):	):	PUNCT
eurjchem-792	137	9	yield	yield	NOUN
eurjchem-792	137	10	:	:	PUNCT
eurjchem-792	137	11	6.13	6.13	NUM
eurjchem-792	137	12	g	g	NOUN
eurjchem-792	137	13	(	(	PUNCT
eurjchem-792	137	14	84.1	84.1	NUM
eurjchem-792	137	15	%	%	NOUN
eurjchem-792	137	16	)	)	PUNCT
eurjchem-792	137	17	.	.	PUNCT
eurjchem-792	138	1	color	color	NOUN
eurjchem-792	138	2	:	:	PUNCT
eurjchem-792	138	3	off	off	ADP
eurjchem-792	138	4	white	white	ADJ
eurjchem-792	138	5	powder	powder	NOUN
eurjchem-792	138	6	.	.	PUNCT
eurjchem-792	139	1	m.p	m.p	PROPN
eurjchem-792	139	2	.	.	PROPN
eurjchem-792	139	3	:	:	PUNCT
eurjchem-792	140	1	242‐245	242‐245	NUM
eurjchem-792	140	2	°	°	PRON
eurjchem-792	140	3	c	c	PROPN
eurjchem-792	140	4	.	.	PUNCT
eurjchem-792	141	1	ir	ir	PROPN
eurjchem-792	141	2	(	(	PUNCT
eurjchem-792	141	3	kbr	kbr	PROPN
eurjchem-792	141	4	,	,	PUNCT
eurjchem-792	141	5	v	v	NOUN
eurjchem-792	141	6	,	,	PUNCT
eurjchem-792	141	7	cm‐1	cm‐1	PROPN
eurjchem-792	141	8	):	):	PUNCT
eurjchem-792	141	9	3420	3420	NUM
eurjchem-792	141	10	(	(	PUNCT
eurjchem-792	141	11	oh	oh	INTJ
eurjchem-792	141	12	)	)	PUNCT
eurjchem-792	141	13	,	,	PUNCT
eurjchem-792	141	14	1706	1706	NUM
eurjchem-792	141	15	(	(	PUNCT
eurjchem-792	141	16	c	c	NOUN
eurjchem-792	141	17	=	=	NOUN
eurjchem-792	141	18	o	o	NOUN
eurjchem-792	141	19	)	)	PUNCT
eurjchem-792	141	20	,	,	PUNCT
eurjchem-792	141	21	1623	1623	NUM
eurjchem-792	141	22	(	(	PUNCT
eurjchem-792	141	23	c	c	NOUN
eurjchem-792	141	24	=	=	NOUN
eurjchem-792	141	25	o	o	NOUN
eurjchem-792	141	26	)	)	PUNCT
eurjchem-792	141	27	.	.	PUNCT
eurjchem-792	142	1	1h	1h	NUM
eurjchem-792	142	2	nmr	nmr	NOUN
eurjchem-792	142	3	(	(	PUNCT
eurjchem-792	142	4	300	300	NUM
eurjchem-792	142	5	mhz	mhz	NOUN
eurjchem-792	142	6	,	,	PUNCT
eurjchem-792	142	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-792	142	8	,	,	PUNCT
eurjchem-792	142	9	δ	δ	PROPN
eurjchem-792	142	10	,	,	PUNCT
eurjchem-792	142	11	ppm	ppm	NUM
eurjchem-792	142	12	):	):	PUNCT
eurjchem-792	142	13	1.43‐1.45	1.43‐1.45	NUM
eurjchem-792	142	14	(	(	PUNCT
eurjchem-792	142	15	d	d	PROPN
eurjchem-792	142	16	,	,	PUNCT
eurjchem-792	142	17	3h	3h	NUM
eurjchem-792	142	18	,	,	PUNCT
eurjchem-792	142	19	ch3	ch3	PROPN
eurjchem-792	142	20	,	,	PUNCT
eurjchem-792	142	21	j	j	PROPN
eurjchem-792	142	22	=	=	SYM
eurjchem-792	142	23	6.2	6.2	NUM
eurjchem-792	142	24	hz	hz	NOUN
eurjchem-792	142	25	)	)	PUNCT
eurjchem-792	142	26	,	,	PUNCT
eurjchem-792	142	27	2.61‐2.67	2.61‐2.67	NUM
eurjchem-792	142	28	(	(	PUNCT
eurjchem-792	142	29	m	m	PROPN
eurjchem-792	142	30	,	,	PUNCT
eurjchem-792	142	31	4h	4h	NOUN
eurjchem-792	142	32	,	,	PUNCT
eurjchem-792	142	33	2×ch2	2×ch2	ADJ
eurjchem-792	142	34	)	)	PUNCT
eurjchem-792	142	35	,	,	PUNCT
eurjchem-792	142	36	2.72‐2.74	2.72‐2.74	NUM
eurjchem-792	142	37	(	(	PUNCT
eurjchem-792	142	38	d	d	PROPN
eurjchem-792	142	39	,	,	PUNCT
eurjchem-792	142	40	2h	2h	NUM
eurjchem-792	142	41	,	,	PUNCT
eurjchem-792	142	42	ch2	ch2	PROPN
eurjchem-792	142	43	,	,	PUNCT
eurjchem-792	142	44	j	j	PROPN
eurjchem-792	143	1	=	=	SYM
eurjchem-792	143	2	6.0	6.0	NUM
eurjchem-792	143	3	hz	hz	NOUN
eurjchem-792	143	4	)	)	PUNCT
eurjchem-792	143	5	,	,	PUNCT
eurjchem-792	143	6	3.32‐3.24	3.32‐3.24	NUM
eurjchem-792	143	7	(	(	PUNCT
eurjchem-792	143	8	d	d	NOUN
eurjchem-792	143	9	,	,	PUNCT
eurjchem-792	143	10	2h	2h	NUM
eurjchem-792	143	11	,	,	PUNCT
eurjchem-792	143	12	ch2	ch2	PROPN
eurjchem-792	143	13	,	,	PUNCT
eurjchem-792	143	14	j	j	PROPN
eurjchem-792	143	15	=	=	SYM
eurjchem-792	143	16	6.0	6.0	NUM
eurjchem-792	143	17	hz	hz	NOUN
eurjchem-792	143	18	)	)	PUNCT
eurjchem-792	143	19	,	,	PUNCT
eurjchem-792	143	20	3.61‐3.67	3.61‐3.67	NUM
eurjchem-792	143	21	(	(	PUNCT
eurjchem-792	143	22	m	m	PROPN
eurjchem-792	143	23	,	,	PUNCT
eurjchem-792	143	24	4h	4h	NOUN
eurjchem-792	143	25	,	,	PUNCT
eurjchem-792	143	26	2×ch2	2×ch2	ADJ
eurjchem-792	143	27	)	)	PUNCT
eurjchem-792	143	28	,	,	PUNCT
eurjchem-792	143	29	3.68‐3.73	3.68‐3.73	NUM
eurjchem-792	143	30	(	(	PUNCT
eurjchem-792	143	31	m	m	PROPN
eurjchem-792	143	32	,	,	PUNCT
eurjchem-792	143	33	1h	1h	NUM
eurjchem-792	143	34	,	,	PUNCT
eurjchem-792	143	35	ch	ch	NOUN
eurjchem-792	143	36	)	)	PUNCT
eurjchem-792	143	37	,	,	PUNCT
eurjchem-792	143	38	4.49‐4.56	4.49‐4.56	NUM
eurjchem-792	143	39	(	(	PUNCT
eurjchem-792	143	40	m	m	PROPN
eurjchem-792	143	41	,	,	PUNCT
eurjchem-792	143	42	1h	1h	NUM
eurjchem-792	143	43	,	,	PUNCT
eurjchem-792	143	44	ch	ch	NOUN
eurjchem-792	143	45	)	)	PUNCT
eurjchem-792	143	46	,	,	PUNCT
eurjchem-792	143	47	4.66‐4.68	4.66‐4.68	NUM
eurjchem-792	143	48	(	(	PUNCT
eurjchem-792	143	49	d	d	NOUN
eurjchem-792	143	50	,	,	PUNCT
eurjchem-792	143	51	2h	2h	NUM
eurjchem-792	143	52	,	,	PUNCT
eurjchem-792	143	53	ch2	ch2	PROPN
eurjchem-792	143	54	,	,	PUNCT
eurjchem-792	143	55	j	j	PROPN
eurjchem-792	144	1	=	=	SYM
eurjchem-792	144	2	6.0	6.0	NUM
eurjchem-792	144	3	hz	hz	NOUN
eurjchem-792	144	4	)	)	PUNCT
eurjchem-792	144	5	,	,	PUNCT
eurjchem-792	144	6	5.07	5.07	NUM
eurjchem-792	144	7	(	(	PUNCT
eurjchem-792	144	8	s	s	PROPN
eurjchem-792	144	9	,	,	PUNCT
eurjchem-792	144	10	1h	1h	NUM
eurjchem-792	144	11	,	,	PUNCT
eurjchem-792	144	12	oh	oh	INTJ
eurjchem-792	144	13	,	,	PUNCT
eurjchem-792	144	14	d2o	d2o	NOUN
eurjchem-792	144	15	exchangeable	exchangeable	ADJ
eurjchem-792	144	16	)	)	PUNCT
eurjchem-792	144	17	,	,	PUNCT
eurjchem-792	144	18	5.48	5.48	NUM
eurjchem-792	144	19	(	(	PUNCT
eurjchem-792	144	20	s	s	PROPN
eurjchem-792	144	21	,	,	PUNCT
eurjchem-792	144	22	1h	1h	NUM
eurjchem-792	144	23	,	,	PUNCT
eurjchem-792	144	24	nh	nh	PROPN
eurjchem-792	144	25	,	,	PUNCT
eurjchem-792	144	26	d2o	d2o	PROPN
eurjchem-792	144	27	exchangeable	exchangeable	ADJ
eurjchem-792	144	28	)	)	PUNCT
eurjchem-792	144	29	,	,	PUNCT
eurjchem-792	144	30	7.28‐7.31	7.28‐7.31	NUM
eurjchem-792	144	31	(	(	PUNCT
eurjchem-792	144	32	m	m	PROPN
eurjchem-792	144	33	,	,	PUNCT
eurjchem-792	144	34	1h	1h	NUM
eurjchem-792	144	35	,	,	PUNCT
eurjchem-792	144	36	ar‐h	ar‐h	NOUN
eurjchem-792	144	37	)	)	PUNCT
eurjchem-792	144	38	,	,	PUNCT
eurjchem-792	144	39	7.53‐7.60	7.53‐7.60	NUM
eurjchem-792	144	40	(	(	PUNCT
eurjchem-792	144	41	m	m	PROPN
eurjchem-792	144	42	,	,	PUNCT
eurjchem-792	144	43	3h	3h	NUM
eurjchem-792	144	44	,	,	PUNCT
eurjchem-792	144	45	ar‐h	ar‐h	NOUN
eurjchem-792	144	46	)	)	PUNCT
eurjchem-792	144	47	,	,	PUNCT
eurjchem-792	144	48	8.97	8.97	NUM
eurjchem-792	144	49	(	(	PUNCT
eurjchem-792	144	50	s	s	PROPN
eurjchem-792	144	51	,	,	PUNCT
eurjchem-792	144	52	1h	1h	NUM
eurjchem-792	144	53	,	,	PUNCT
eurjchem-792	144	54	c	c	NOUN
eurjchem-792	144	55	=	=	NOUN
eurjchem-792	144	56	ch	ch	NOUN
eurjchem-792	144	57	)	)	PUNCT
eurjchem-792	144	58	,	,	PUNCT
eurjchem-792	144	59	15.12	15.12	NUM
eurjchem-792	144	60	(	(	PUNCT
eurjchem-792	144	61	s	s	PROPN
eurjchem-792	144	62	,	,	PUNCT
eurjchem-792	144	63	1h	1h	NUM
eurjchem-792	144	64	,	,	PUNCT
eurjchem-792	144	65	cooh	cooh	NOUN
eurjchem-792	144	66	,	,	PUNCT
eurjchem-792	144	67	d2o	d2o	PROPN
eurjchem-792	144	68	exchangeable	exchangeable	ADJ
eurjchem-792	144	69	)	)	PUNCT
eurjchem-792	144	70	.	.	PUNCT
eurjchem-792	145	1	13c	13c	NOUN
eurjchem-792	145	2	nmr	nmr	NOUN
eurjchem-792	145	3	(	(	PUNCT
eurjchem-792	145	4	75	75	NUM
eurjchem-792	145	5	mhz	mhz	NOUN
eurjchem-792	145	6	,	,	PUNCT
eurjchem-792	145	7	dmso‐d6	dmso‐d6	NOUN
eurjchem-792	145	8	,	,	PUNCT
eurjchem-792	145	9	ppm	ppm	NOUN
eurjchem-792	145	10	,	,	PUNCT
eurjchem-792	145	11	δ	δ	PROPN
eurjchem-792	145	12	):	):	PUNCT
eurjchem-792	145	13	18.39	18.39	NUM
eurjchem-792	145	14	(	(	PUNCT
eurjchem-792	145	15	ch3	ch3	PROPN
eurjchem-792	145	16	)	)	PUNCT
eurjchem-792	145	17	,	,	PUNCT
eurjchem-792	145	18	47.36	47.36	NUM
eurjchem-792	145	19	(	(	PUNCT
eurjchem-792	145	20	ch2	ch2	PROPN
eurjchem-792	145	21	)	)	PUNCT
eurjchem-792	145	22	,	,	PUNCT
eurjchem-792	145	23	50.07	50.07	NUM
eurjchem-792	145	24	(	(	PUNCT
eurjchem-792	145	25	2×ch2	2×ch2	ADJ
eurjchem-792	145	26	)	)	PUNCT
eurjchem-792	145	27	,	,	PUNCT
eurjchem-792	145	28	54.91(2×ch2	54.91(2×ch2	NUM
eurjchem-792	145	29	)	)	PUNCT
eurjchem-792	145	30	,	,	PUNCT
eurjchem-792	145	31	60.43	60.43	NUM
eurjchem-792	145	32	(	(	PUNCT
eurjchem-792	145	33	ch2	ch2	PROPN
eurjchem-792	145	34	)	)	PUNCT
eurjchem-792	145	35	,	,	PUNCT
eurjchem-792	145	36	62.14	62.14	NUM
eurjchem-792	145	37	(	(	PUNCT
eurjchem-792	145	38	ch	ch	NOUN
eurjchem-792	145	39	)	)	PUNCT
eurjchem-792	145	40	,	,	PUNCT
eurjchem-792	145	41	64.51(ch	64.51(ch	PROPN
eurjchem-792	145	42	)	)	PUNCT
eurjchem-792	145	43	,	,	PUNCT
eurjchem-792	145	44	68.77	68.77	NUM
eurjchem-792	145	45	(	(	PUNCT
eurjchem-792	145	46	ch2	ch2	PROPN
eurjchem-792	145	47	)	)	PUNCT
eurjchem-792	145	48	,	,	PUNCT
eurjchem-792	145	49	107.27	107.27	NUM
eurjchem-792	145	50	(	(	PUNCT
eurjchem-792	145	51	ch	ch	NOUN
eurjchem-792	145	52	)	)	PUNCT
eurjchem-792	145	53	,	,	PUNCT
eurjchem-792	145	54	109.43	109.43	NUM
eurjchem-792	145	55	(	(	PUNCT
eurjchem-792	145	56	c	c	NOUN
eurjchem-792	145	57	)	)	PUNCT
eurjchem-792	145	58	,	,	PUNCT
eurjchem-792	145	59	113.57	113.57	NUM
eurjchem-792	145	60	(	(	PUNCT
eurjchem-792	145	61	ch	ch	NOUN
eurjchem-792	145	62	)	)	PUNCT
eurjchem-792	145	63	,	,	PUNCT
eurjchem-792	145	64	114.99	114.99	NUM
eurjchem-792	145	65	(	(	PUNCT
eurjchem-792	145	66	ch	ch	NOUN
eurjchem-792	145	67	)	)	PUNCT
eurjchem-792	145	68	,	,	PUNCT
eurjchem-792	145	69	120.96	120.96	NUM
eurjchem-792	145	70	(	(	PUNCT
eurjchem-792	145	71	c	c	NOUN
eurjchem-792	145	72	)	)	PUNCT
eurjchem-792	145	73	,	,	PUNCT
eurjchem-792	145	74	125.19	125.19	NUM
eurjchem-792	145	75	(	(	PUNCT
eurjchem-792	145	76	ch	ch	NOUN
eurjchem-792	145	77	)	)	PUNCT
eurjchem-792	145	78	,	,	PUNCT
eurjchem-792	145	79	130.77	130.77	NUM
eurjchem-792	145	80	(	(	PUNCT
eurjchem-792	145	81	c	c	NOUN
eurjchem-792	145	82	)	)	PUNCT
eurjchem-792	145	83	,	,	PUNCT
eurjchem-792	145	84	134.79	134.79	NUM
eurjchem-792	145	85	(	(	PUNCT
eurjchem-792	145	86	c	c	NOUN
eurjchem-792	145	87	)	)	PUNCT
eurjchem-792	145	88	,	,	PUNCT
eurjchem-792	145	89	136.99	136.99	NUM
eurjchem-792	145	90	(	(	PUNCT
eurjchem-792	145	91	c	c	NOUN
eurjchem-792	145	92	)	)	PUNCT
eurjchem-792	145	93	,	,	PUNCT
eurjchem-792	145	94	140.96	140.96	NUM
eurjchem-792	145	95	(	(	PUNCT
eurjchem-792	145	96	c	c	NOUN
eurjchem-792	145	97	)	)	PUNCT
eurjchem-792	145	98	,	,	PUNCT
eurjchem-792	145	99	146.79	146.79	NUM
eurjchem-792	145	100	(	(	PUNCT
eurjchem-792	145	101	c	c	NOUN
eurjchem-792	145	102	)	)	PUNCT
eurjchem-792	145	103	,	,	PUNCT
eurjchem-792	145	104	152.50	152.50	NUM
eurjchem-792	145	105	(	(	PUNCT
eurjchem-792	145	106	ch	ch	NOUN
eurjchem-792	145	107	)	)	PUNCT
eurjchem-792	145	108	,	,	PUNCT
eurjchem-792	145	109	166.39	166.39	NUM
eurjchem-792	145	110	(	(	PUNCT
eurjchem-792	145	111	c	c	NOUN
eurjchem-792	145	112	=	=	NOUN
eurjchem-792	145	113	o	o	NOUN
eurjchem-792	145	114	)	)	PUNCT
eurjchem-792	145	115	,	,	PUNCT
eurjchem-792	145	116	176.83	176.83	NUM
eurjchem-792	145	117	(	(	PUNCT
eurjchem-792	145	118	c	c	NOUN
eurjchem-792	145	119	=	=	NOUN
eurjchem-792	145	120	o	o	NOUN
eurjchem-792	145	121	)	)	PUNCT
eurjchem-792	145	122	.	.	PUNCT
eurjchem-792	146	1	anal	anal	PROPN
eurjchem-792	146	2	.	.	PUNCT
eurjchem-792	146	3	calcd	calcd	NOUN
eurjchem-792	146	4	.	.	PUNCT
eurjchem-792	147	1	for	for	ADP
eurjchem-792	147	2	c27h27clfn5o5s	c27h27clfn5o5s	NUM
eurjchem-792	147	3	:	:	PUNCT
eurjchem-792	147	4	c	c	X
eurjchem-792	147	5	,	,	PUNCT
eurjchem-792	147	6	55.15	55.15	NUM
eurjchem-792	147	7	;	;	PUNCT
eurjchem-792	147	8	h	h	NOUN
eurjchem-792	147	9	,	,	PUNCT
eurjchem-792	147	10	4.63	4.63	NUM
eurjchem-792	147	11	;	;	PUNCT
eurjchem-792	147	12	n	n	CCONJ
eurjchem-792	147	13	,	,	PUNCT
eurjchem-792	147	14	11.91	11.91	NUM
eurjchem-792	147	15	.	.	PUNCT
eurjchem-792	147	16	found	find	VERB
eurjchem-792	147	17	:	:	PUNCT
eurjchem-792	148	1	c	c	X
eurjchem-792	148	2	,	,	PUNCT
eurjchem-792	148	3	54.96	54.96	NUM
eurjchem-792	148	4	;	;	PUNCT
eurjchem-792	148	5	h	h	NOUN
eurjchem-792	148	6	,	,	PUNCT
eurjchem-792	148	7	4.52	4.52	NUM
eurjchem-792	148	8	;	;	PUNCT
eurjchem-792	148	9	n	n	CCONJ
eurjchem-792	148	10	,	,	PUNCT
eurjchem-792	148	11	11.79	11.79	NUM
eurjchem-792	148	12	%	%	NOUN
eurjchem-792	148	13	.	.	PUNCT
eurjchem-792	149	1	ms	ms	NOUN
eurjchem-792	149	2	(	(	PUNCT
eurjchem-792	149	3	m	m	PROPN
eurjchem-792	149	4	/	/	SYM
eurjchem-792	149	5	z	z	NOUN
eurjchem-792	149	6	):	):	PUNCT
eurjchem-792	149	7	588.65	588.65	NUM
eurjchem-792	149	8	(	(	PUNCT
eurjchem-792	149	9	m+	m+	NUM
eurjchem-792	149	10	)	)	PUNCT
eurjchem-792	149	11	.	.	PUNCT
eurjchem-792	150	1	[	[	X
eurjchem-792	150	2	α]d25	α]d25	NOUN
eurjchem-792	150	3	:	:	PUNCT
eurjchem-792	150	4	‐74.78	‐74.78	PROPN
eurjchem-792	150	5	(	(	PUNCT
eurjchem-792	150	6	c	c	NOUN
eurjchem-792	150	7	=	=	SYM
eurjchem-792	150	8	1.0	1.0	NUM
eurjchem-792	150	9	in	in	ADP
eurjchem-792	150	10	methanol	methanol	NOUN
eurjchem-792	150	11	:	:	PUNCT
eurjchem-792	150	12	methylene	methylene	NOUN
eurjchem-792	150	13	chloride	chloride	NOUN
eurjchem-792	150	14	,	,	PUNCT
eurjchem-792	150	15	1:1	1:1	NUM
eurjchem-792	150	16	)	)	PUNCT
eurjchem-792	150	17	.	.	PUNCT
eurjchem-792	151	1	2.2.4	2.2.4	NUM
eurjchem-792	151	2	.	.	PUNCT
eurjchem-792	151	3	general	general	ADJ
eurjchem-792	151	4	procedure	procedure	NOUN
eurjchem-792	151	5	for	for	ADP
eurjchem-792	151	6	the	the	DET
eurjchem-792	151	7	preparation	preparation	NOUN
eurjchem-792	151	8	of	of	ADP
eurjchem-792	151	9	5a‐e	5a‐e	PROPN
eurjchem-792	151	10	to	to	ADP
eurjchem-792	151	11	a	a	DET
eurjchem-792	151	12	solution	solution	NOUN
eurjchem-792	151	13	of	of	ADP
eurjchem-792	151	14	compounds	compound	NOUN
eurjchem-792	151	15	4a‐e	4a‐e	NOUN
eurjchem-792	151	16	(	(	PUNCT
eurjchem-792	151	17	9.03	9.03	NUM
eurjchem-792	151	18	mmol	mmol	NOUN
eurjchem-792	151	19	)	)	PUNCT
eurjchem-792	151	20	in	in	ADP
eurjchem-792	151	21	dichloromethane	dichloromethane	NOUN
eurjchem-792	151	22	(	(	PUNCT
eurjchem-792	151	23	25	25	NUM
eurjchem-792	151	24	ml	ml	NOUN
eurjchem-792	151	25	)	)	PUNCT
eurjchem-792	151	26	and	and	CCONJ
eurjchem-792	151	27	tetrabutyl	tetrabutyl	NOUN
eurjchem-792	151	28	ammonium	ammonium	NOUN
eurjchem-792	151	29	bromide	bromide	NOUN
eurjchem-792	151	30	(	(	PUNCT
eurjchem-792	151	31	0.1	0.1	NUM
eurjchem-792	151	32	g	g	NOUN
eurjchem-792	151	33	)	)	PUNCT
eurjchem-792	151	34	was	be	AUX
eurjchem-792	151	35	added	add	VERB
eurjchem-792	151	36	to	to	ADP
eurjchem-792	151	37	a	a	DET
eurjchem-792	151	38	solution	solution	NOUN
eurjchem-792	151	39	of	of	ADP
eurjchem-792	151	40	ammonium	ammonium	NOUN
eurjchem-792	151	41	molybdate	molybdate	NOUN
eurjchem-792	151	42	(	(	PUNCT
eurjchem-792	151	43	0.2	0.2	NUM
eurjchem-792	151	44	g	g	NOUN
eurjchem-792	151	45	)	)	PUNCT
eurjchem-792	151	46	in	in	ADP
eurjchem-792	151	47	30	30	NUM
eurjchem-792	151	48	%	%	NOUN
eurjchem-792	151	49	hydrogen	hydrogen	NOUN
eurjchem-792	151	50	peroxide	peroxide	NOUN
eurjchem-792	151	51	(	(	PUNCT
eurjchem-792	151	52	45.14	45.14	NUM
eurjchem-792	151	53	mmol	mmol	NOUN
eurjchem-792	151	54	)	)	PUNCT
eurjchem-792	151	55	drop	drop	NOUN
eurjchem-792	151	56	wise	wise	ADJ
eurjchem-792	151	57	at	at	ADP
eurjchem-792	151	58	0‐5	0‐5	NOUN
eurjchem-792	151	59	°	°	ADP
eurjchem-792	151	60	c	c	NOUN
eurjchem-792	151	61	and	and	CCONJ
eurjchem-792	151	62	maintained	maintain	VERB
eurjchem-792	151	63	for	for	ADP
eurjchem-792	151	64	4	4	NUM
eurjchem-792	151	65	h	h	NOUN
eurjchem-792	151	66	at	at	ADP
eurjchem-792	151	67	10‐15	10‐15	NUM
eurjchem-792	151	68	°	°	ADP
eurjchem-792	151	69	c	c	NOUN
eurjchem-792	151	70	and	and	CCONJ
eurjchem-792	151	71	monitor	monitor	VERB
eurjchem-792	151	72	the	the	DET
eurjchem-792	151	73	reaction	reaction	NOUN
eurjchem-792	151	74	by	by	ADP
eurjchem-792	151	75	tlc	tlc	PROPN
eurjchem-792	151	76	.	.	PUNCT
eurjchem-792	152	1	after	after	SCONJ
eurjchem-792	152	2	completion	completion	NOUN
eurjchem-792	152	3	of	of	ADP
eurjchem-792	152	4	reaction	reaction	NOUN
eurjchem-792	152	5	organic	organic	ADJ
eurjchem-792	152	6	layer	layer	NOUN
eurjchem-792	152	7	was	be	AUX
eurjchem-792	152	8	separated	separate	VERB
eurjchem-792	152	9	,	,	PUNCT
eurjchem-792	152	10	washed	wash	VERB
eurjchem-792	152	11	with	with	ADP
eurjchem-792	152	12	20	20	NUM
eurjchem-792	152	13	%	%	NOUN
eurjchem-792	152	14	nacl	nacl	NOUN
eurjchem-792	152	15	solution	solution	NOUN
eurjchem-792	152	16	(	(	PUNCT
eurjchem-792	152	17	20	20	NUM
eurjchem-792	152	18	ml	ml	NOUN
eurjchem-792	152	19	)	)	PUNCT
eurjchem-792	152	20	,	,	PUNCT
eurjchem-792	152	21	dried	dry	VERB
eurjchem-792	152	22	over	over	ADP
eurjchem-792	152	23	anhydrous	anhydrous	ADJ
eurjchem-792	152	24	na2so4	na2so4	NOUN
eurjchem-792	152	25	and	and	CCONJ
eurjchem-792	152	26	the	the	DET
eurjchem-792	152	27	solvent	solvent	NOUN
eurjchem-792	152	28	was	be	AUX
eurjchem-792	152	29	distilled	distil	VERB
eurjchem-792	152	30	off	off	ADP
eurjchem-792	152	31	under	under	ADP
eurjchem-792	152	32	vacuum	vacuum	NOUN
eurjchem-792	152	33	to	to	PART
eurjchem-792	152	34	obtain	obtain	VERB
eurjchem-792	152	35	a	a	DET
eurjchem-792	152	36	crude	crude	ADJ
eurjchem-792	152	37	5a‐e	5a‐e	NOUN
eurjchem-792	152	38	,	,	PUNCT
eurjchem-792	152	39	the	the	DET
eurjchem-792	152	40	crude	crude	ADJ
eurjchem-792	152	41	compounds	compound	NOUN
eurjchem-792	152	42	were	be	AUX
eurjchem-792	152	43	recrystallized	recrystallize	VERB
eurjchem-792	152	44	from	from	AUX
eurjchem-792	152	45	ethylacetate	ethylacetate	VERB
eurjchem-792	152	46	to	to	PART
eurjchem-792	152	47	obtain	obtain	VERB
eurjchem-792	152	48	the	the	DET
eurjchem-792	152	49	pure	pure	ADJ
eurjchem-792	152	50	title	title	NOUN
eurjchem-792	152	51	compounds	compound	NOUN
eurjchem-792	152	52	(	(	PUNCT
eurjchem-792	152	53	scheme	scheme	NOUN
eurjchem-792	152	54	3	3	NUM
eurjchem-792	152	55	)	)	PUNCT
eurjchem-792	152	56	.	.	PUNCT
eurjchem-792	153	1	(	(	PUNCT
eurjchem-792	153	2	s)‐10‐(4‐(3‐(1h‐benzo[d]imidazol‐2‐yl	s)‐10‐(4‐(3‐(1h‐benzo[d]imidazol‐2‐yl	PUNCT
eurjchem-792	153	3	sulfonyl)‐2‐hydroxy	sulfonyl)‐2‐hydroxy	PROPN
eurjchem-792	153	4	propyl)piperazin‐1‐yl)‐9‐fluoro‐3,7‐dihydro‐3‐methyl‐7‐oxo‐2h‐	propyl)piperazin‐1‐yl)‐9‐fluoro‐3,7‐dihydro‐3‐methyl‐7‐oxo‐2h‐	PROPN
eurjchem-792	153	5	[	[	X
eurjchem-792	153	6	1,4]oxazino[2,3,4‐ij]quinoline‐6‐carboxylic	1,4]oxazino[2,3,4‐ij]quinoline‐6‐carboxylic	NUM
eurjchem-792	153	7	acid	acid	NOUN
eurjchem-792	153	8	(	(	PUNCT
eurjchem-792	153	9	5a	5a	NUM
eurjchem-792	153	10	):	):	PUNCT
eurjchem-792	153	11	yield	yield	NOUN
eurjchem-792	153	12	:	:	PUNCT
eurjchem-792	153	13	4.40	4.40	NUM
eurjchem-792	153	14	g	g	NOUN
eurjchem-792	153	15	(	(	PUNCT
eurjchem-792	153	16	83.4	83.4	NUM
eurjchem-792	153	17	%	%	NOUN
eurjchem-792	153	18	)	)	PUNCT
eurjchem-792	153	19	.	.	PUNCT
eurjchem-792	154	1	color	color	NOUN
eurjchem-792	154	2	:	:	PUNCT
eurjchem-792	154	3	off	off	ADP
eurjchem-792	154	4	white	white	PROPN
eurjchem-792	154	5	solid	solid	PROPN
eurjchem-792	154	6	.	.	PUNCT
eurjchem-792	155	1	m.p	m.p	PROPN
eurjchem-792	155	2	.	.	PROPN
eurjchem-792	155	3	:	:	PUNCT
eurjchem-792	156	1	200‐203	200‐203	NUM
eurjchem-792	156	2	°	°	SYM
eurjchem-792	156	3	c	c	X
eurjchem-792	156	4	.	.	PUNCT
eurjchem-792	157	1	ir	ir	PROPN
eurjchem-792	157	2	(	(	PUNCT
eurjchem-792	157	3	kbr	kbr	PROPN
eurjchem-792	157	4	,	,	PUNCT
eurjchem-792	157	5	v	v	NOUN
eurjchem-792	157	6	,	,	PUNCT
eurjchem-792	157	7	cm‐1	cm‐1	PROPN
eurjchem-792	157	8	):	):	PUNCT
eurjchem-792	157	9	3418	3418	NUM
eurjchem-792	157	10	(	(	PUNCT
eurjchem-792	157	11	oh	oh	INTJ
eurjchem-792	157	12	)	)	PUNCT
eurjchem-792	157	13	,	,	PUNCT
eurjchem-792	157	14	1718	1718	NUM
eurjchem-792	157	15	(	(	PUNCT
eurjchem-792	157	16	c	c	NOUN
eurjchem-792	157	17	=	=	NOUN
eurjchem-792	157	18	o	o	NOUN
eurjchem-792	157	19	)	)	PUNCT
eurjchem-792	157	20	,	,	PUNCT
eurjchem-792	157	21	1621	1621	NUM
eurjchem-792	157	22	(	(	PUNCT
eurjchem-792	157	23	c	c	NOUN
eurjchem-792	157	24	=	=	NOUN
eurjchem-792	157	25	o	o	NOUN
eurjchem-792	157	26	)	)	PUNCT
eurjchem-792	157	27	.	.	PUNCT
eurjchem-792	158	1	1h	1h	NUM
eurjchem-792	158	2	nmr	nmr	NOUN
eurjchem-792	158	3	(	(	PUNCT
eurjchem-792	158	4	300	300	NUM
eurjchem-792	158	5	mhz	mhz	NOUN
eurjchem-792	158	6	,	,	PUNCT
eurjchem-792	158	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-792	158	8	,	,	PUNCT
eurjchem-792	158	9	δ	δ	PROPN
eurjchem-792	158	10	,	,	PUNCT
eurjchem-792	158	11	ppm	ppm	NUM
eurjchem-792	158	12	):	):	PUNCT
eurjchem-792	158	13	1.40‐1.42	1.40‐1.42	NUM
eurjchem-792	158	14	(	(	PUNCT
eurjchem-792	158	15	d	d	PROPN
eurjchem-792	158	16	,	,	PUNCT
eurjchem-792	158	17	3h	3h	NUM
eurjchem-792	158	18	,	,	PUNCT
eurjchem-792	158	19	ch3	ch3	PROPN
eurjchem-792	158	20	,	,	PUNCT
eurjchem-792	158	21	j	j	PROPN
eurjchem-792	158	22	=	=	SYM
eurjchem-792	158	23	6.2	6.2	NUM
eurjchem-792	158	24	hz	hz	NOUN
eurjchem-792	158	25	)	)	PUNCT
eurjchem-792	158	26	2.46‐2.51	2.46‐2.51	PROPN
eurjchem-792	158	27	(	(	PUNCT
eurjchem-792	158	28	m	m	PROPN
eurjchem-792	158	29	,	,	PUNCT
eurjchem-792	158	30	4h	4h	NOUN
eurjchem-792	158	31	,	,	PUNCT
eurjchem-792	158	32	2×ch2	2×ch2	ADJ
eurjchem-792	158	33	)	)	PUNCT
eurjchem-792	158	34	,	,	PUNCT
eurjchem-792	158	35	2.64‐2.66	2.64‐2.66	NUM
eurjchem-792	158	36	(	(	PUNCT
eurjchem-792	158	37	d	d	NOUN
eurjchem-792	158	38	,	,	PUNCT
eurjchem-792	158	39	2h	2h	NUM
eurjchem-792	158	40	,	,	PUNCT
eurjchem-792	158	41	ch2	ch2	PROPN
eurjchem-792	158	42	,	,	PUNCT
eurjchem-792	158	43	j	j	PROPN
eurjchem-792	158	44	=	=	SYM
eurjchem-792	158	45	6.0	6.0	NUM
eurjchem-792	158	46	hz	hz	NOUN
eurjchem-792	158	47	)	)	PUNCT
eurjchem-792	158	48	,	,	PUNCT
eurjchem-792	158	49	3.60‐3.66	3.60‐3.66	NUM
eurjchem-792	158	50	(	(	PUNCT
eurjchem-792	158	51	m	m	PROPN
eurjchem-792	158	52	,	,	PUNCT
eurjchem-792	158	53	4h	4h	NOUN
eurjchem-792	158	54	,	,	PUNCT
eurjchem-792	158	55	2×ch2	2×ch2	ADJ
eurjchem-792	158	56	)	)	PUNCT
eurjchem-792	158	57	,	,	PUNCT
eurjchem-792	158	58	3.71‐3.76	3.71‐3.76	NUM
eurjchem-792	158	59	(	(	PUNCT
eurjchem-792	158	60	m	m	PROPN
eurjchem-792	158	61	,	,	PUNCT
eurjchem-792	158	62	1h	1h	NUM
eurjchem-792	158	63	,	,	PUNCT
eurjchem-792	158	64	ch	ch	NOUN
eurjchem-792	158	65	)	)	PUNCT
eurjchem-792	158	66	,	,	PUNCT
eurjchem-792	158	67	3.83.85	3.83.85	NUM
eurjchem-792	158	68	(	(	PUNCT
eurjchem-792	158	69	d	d	PROPN
eurjchem-792	158	70	,	,	PUNCT
eurjchem-792	158	71	2h	2h	NUM
eurjchem-792	158	72	,	,	PUNCT
eurjchem-792	158	73	ch2	ch2	PROPN
eurjchem-792	158	74	,	,	PUNCT
eurjchem-792	158	75	j	j	PROPN
eurjchem-792	158	76	=	=	SYM
eurjchem-792	158	77	6.0	6.0	NUM
eurjchem-792	158	78	hz	hz	NOUN
eurjchem-792	158	79	)	)	PUNCT
eurjchem-792	158	80	,	,	PUNCT
eurjchem-792	158	81	4.41‐4.46	4.41‐4.46	NUM
eurjchem-792	158	82	(	(	PUNCT
eurjchem-792	158	83	m	m	PROPN
eurjchem-792	158	84	,	,	PUNCT
eurjchem-792	158	85	1h	1h	NUM
eurjchem-792	158	86	,	,	PUNCT
eurjchem-792	158	87	ch	ch	NOUN
eurjchem-792	158	88	)	)	PUNCT
eurjchem-792	158	89	,	,	PUNCT
eurjchem-792	158	90	4.53‐4.55	4.53‐4.55	NUM
eurjchem-792	158	91	(	(	PUNCT
eurjchem-792	158	92	d	d	NOUN
eurjchem-792	158	93	,	,	PUNCT
eurjchem-792	158	94	2h	2h	NUM
eurjchem-792	158	95	,	,	PUNCT
eurjchem-792	158	96	ch2	ch2	PROPN
eurjchem-792	158	97	,	,	PUNCT
eurjchem-792	158	98	j	j	PROPN
eurjchem-792	158	99	=	=	SYM
eurjchem-792	158	100	6.0	6.0	NUM
eurjchem-792	158	101	hz	hz	NOUN
eurjchem-792	158	102	)	)	PUNCT
eurjchem-792	158	103	,	,	PUNCT
eurjchem-792	158	104	4.89	4.89	NUM
eurjchem-792	158	105	(	(	PUNCT
eurjchem-792	158	106	s	s	PROPN
eurjchem-792	158	107	,	,	PUNCT
eurjchem-792	158	108	1h	1h	NUM
eurjchem-792	158	109	,	,	PUNCT
eurjchem-792	158	110	oh	oh	INTJ
eurjchem-792	158	111	,	,	PUNCT
eurjchem-792	158	112	d2o	d2o	NOUN
eurjchem-792	158	113	exchangeable	exchangeable	ADJ
eurjchem-792	158	114	)	)	PUNCT
eurjchem-792	158	115	,	,	PUNCT
eurjchem-792	158	116	5.24	5.24	NUM
eurjchem-792	158	117	(	(	PUNCT
eurjchem-792	158	118	s	s	PROPN
eurjchem-792	158	119	,	,	PUNCT
eurjchem-792	158	120	1h	1h	NUM
eurjchem-792	158	121	,	,	PUNCT
eurjchem-792	158	122	nh	nh	PROPN
eurjchem-792	158	123	,	,	PUNCT
eurjchem-792	158	124	d2o	d2o	PROPN
eurjchem-792	158	125	exchangeable	exchangeable	ADJ
eurjchem-792	158	126	)	)	PUNCT
eurjchem-792	158	127	,	,	PUNCT
eurjchem-792	158	128	7.11‐7.16	7.11‐7.16	NUM
eurjchem-792	158	129	(	(	PUNCT
eurjchem-792	158	130	m	m	PROPN
eurjchem-792	158	131	,	,	PUNCT
eurjchem-792	158	132	2h	2h	NUM
eurjchem-792	158	133	,	,	PUNCT
eurjchem-792	158	134	ar‐h	ar‐h	NOUN
eurjchem-792	158	135	)	)	PUNCT
eurjchem-792	158	136	,	,	PUNCT
eurjchem-792	158	137	7.39‐7.43	7.39‐7.43	NUM
eurjchem-792	158	138	(	(	PUNCT
eurjchem-792	158	139	m	m	PROPN
eurjchem-792	158	140	,	,	PUNCT
eurjchem-792	158	141	2h	2h	NUM
eurjchem-792	158	142	,	,	PUNCT
eurjchem-792	158	143	ar‐	ar‐	PROPN
eurjchem-792	158	144	h	h	NOUN
eurjchem-792	158	145	)	)	PUNCT
eurjchem-792	158	146	,	,	PUNCT
eurjchem-792	158	147	7.56‐7.60	7.56‐7.60	NUM
eurjchem-792	158	148	(	(	PUNCT
eurjchem-792	158	149	d	d	PROPN
eurjchem-792	158	150	,	,	PUNCT
eurjchem-792	158	151	1h	1h	NUM
eurjchem-792	158	152	,	,	PUNCT
eurjchem-792	158	153	ar‐h	ar‐h	PROPN
eurjchem-792	158	154	j	j	PROPN
eurjchem-792	159	1	=	=	SYM
eurjchem-792	159	2	12.0	12.0	NUM
eurjchem-792	159	3	hz	hz	NOUN
eurjchem-792	159	4	)	)	PUNCT
eurjchem-792	159	5	,	,	PUNCT
eurjchem-792	159	6	8.84	8.84	NUM
eurjchem-792	159	7	(	(	PUNCT
eurjchem-792	159	8	s	s	PROPN
eurjchem-792	159	9	,	,	PUNCT
eurjchem-792	159	10	1h	1h	NUM
eurjchem-792	159	11	,	,	PUNCT
eurjchem-792	159	12	c	c	NOUN
eurjchem-792	159	13	=	=	NOUN
eurjchem-792	159	14	ch	ch	NOUN
eurjchem-792	159	15	)	)	PUNCT
eurjchem-792	159	16	,	,	PUNCT
eurjchem-792	159	17	15.12	15.12	NUM
eurjchem-792	159	18	(	(	PUNCT
eurjchem-792	159	19	s	s	PROPN
eurjchem-792	159	20	,	,	PUNCT
eurjchem-792	159	21	1h	1h	NUM
eurjchem-792	159	22	,	,	PUNCT
eurjchem-792	159	23	cooh	cooh	NOUN
eurjchem-792	159	24	,	,	PUNCT
eurjchem-792	159	25	d2o	d2o	PROPN
eurjchem-792	159	26	exchangeable	exchangeable	ADJ
eurjchem-792	159	27	)	)	PUNCT
eurjchem-792	159	28	.	.	PUNCT
eurjchem-792	160	1	13c	13c	NOUN
eurjchem-792	160	2	nmr	nmr	NOUN
eurjchem-792	160	3	(	(	PUNCT
eurjchem-792	160	4	75	75	NUM
eurjchem-792	160	5	mhz	mhz	NOUN
eurjchem-792	160	6	,	,	PUNCT
eurjchem-792	160	7	dmso‐d6	dmso‐d6	NOUN
eurjchem-792	160	8	,	,	PUNCT
eurjchem-792	160	9	ppm	ppm	NOUN
eurjchem-792	160	10	,	,	PUNCT
eurjchem-792	160	11	δ	δ	PROPN
eurjchem-792	160	12	):	):	PUNCT
eurjchem-792	160	13	18.41	18.41	NUM
eurjchem-792	160	14	(	(	PUNCT
eurjchem-792	160	15	ch3	ch3	PROPN
eurjchem-792	160	16	)	)	PUNCT
eurjchem-792	160	17	,	,	PUNCT
eurjchem-792	160	18	50.16	50.16	NUM
eurjchem-792	160	19	(	(	PUNCT
eurjchem-792	160	20	2×ch2	2×ch2	ADJ
eurjchem-792	160	21	)	)	PUNCT
eurjchem-792	160	22	,	,	PUNCT
eurjchem-792	160	23	54.51	54.51	NUM
eurjchem-792	160	24	(	(	PUNCT
eurjchem-792	160	25	2×ch2	2×ch2	ADJ
eurjchem-792	160	26	)	)	PUNCT
eurjchem-792	160	27	,	,	PUNCT
eurjchem-792	160	28	60.28	60.28	NUM
eurjchem-792	160	29	(	(	PUNCT
eurjchem-792	160	30	ch2	ch2	PROPN
eurjchem-792	160	31	)	)	PUNCT
eurjchem-792	160	32	,	,	PUNCT
eurjchem-792	160	33	62.41	62.41	NUM
eurjchem-792	160	34	(	(	PUNCT
eurjchem-792	160	35	ch	ch	NOUN
eurjchem-792	160	36	)	)	PUNCT
eurjchem-792	160	37	,	,	PUNCT
eurjchem-792	160	38	64.51	64.51	NUM
eurjchem-792	160	39	(	(	PUNCT
eurjchem-792	160	40	ch	ch	NOUN
eurjchem-792	160	41	)	)	PUNCT
eurjchem-792	160	42	,	,	PUNCT
eurjchem-792	160	43	65.78	65.78	NUM
eurjchem-792	160	44	(	(	PUNCT
eurjchem-792	160	45	ch2	ch2	PROPN
eurjchem-792	160	46	)	)	PUNCT
eurjchem-792	160	47	,	,	PUNCT
eurjchem-792	160	48	68.77	68.77	NUM
eurjchem-792	160	49	(	(	PUNCT
eurjchem-792	160	50	ch2	ch2	PROPN
eurjchem-792	160	51	)	)	PUNCT
eurjchem-792	160	52	,	,	PUNCT
eurjchem-792	160	53	108.23	108.23	NUM
eurjchem-792	160	54	(	(	PUNCT
eurjchem-792	160	55	ch	ch	NOUN
eurjchem-792	160	56	)	)	PUNCT
eurjchem-792	160	57	,	,	PUNCT
eurjchem-792	160	58	109.36	109.36	NUM
eurjchem-792	160	59	(	(	PUNCT
eurjchem-792	160	60	c	c	NOUN
eurjchem-792	160	61	)	)	PUNCT
eurjchem-792	160	62	,	,	PUNCT
eurjchem-792	160	63	115.36	115.36	NUM
eurjchem-792	160	64	(	(	PUNCT
eurjchem-792	160	65	ch	ch	NOUN
eurjchem-792	160	66	)	)	PUNCT
eurjchem-792	160	67	,	,	PUNCT
eurjchem-792	160	68	119.48	119.48	NUM
eurjchem-792	160	69	(	(	PUNCT
eurjchem-792	160	70	c	c	NOUN
eurjchem-792	160	71	)	)	PUNCT
eurjchem-792	160	72	,	,	PUNCT
eurjchem-792	160	73	123.92	123.92	NUM
eurjchem-792	160	74	(	(	PUNCT
eurjchem-792	160	75	ch	ch	NOUN
eurjchem-792	160	76	)	)	PUNCT
eurjchem-792	160	77	,	,	PUNCT
eurjchem-792	160	78	131.23	131.23	NUM
eurjchem-792	160	79	(	(	PUNCT
eurjchem-792	160	80	c	c	NOUN
eurjchem-792	160	81	)	)	PUNCT
eurjchem-792	160	82	,	,	PUNCT
eurjchem-792	160	83	135.33	135.33	NUM
eurjchem-792	160	84	(	(	PUNCT
eurjchem-792	160	85	c	c	NOUN
eurjchem-792	160	86	)	)	PUNCT
eurjchem-792	160	87	,	,	PUNCT
eurjchem-792	160	88	141.63	141.63	NUM
eurjchem-792	160	89	(	(	PUNCT
eurjchem-792	160	90	c	c	NOUN
eurjchem-792	160	91	)	)	PUNCT
eurjchem-792	160	92	,	,	PUNCT
eurjchem-792	160	93	146.34	146.34	NUM
eurjchem-792	160	94	(	(	PUNCT
eurjchem-792	160	95	c	c	NOUN
eurjchem-792	160	96	)	)	PUNCT
eurjchem-792	160	97	,	,	PUNCT
eurjchem-792	160	98	151.53	151.53	NUM
eurjchem-792	160	99	(	(	PUNCT
eurjchem-792	160	100	c	c	NOUN
eurjchem-792	160	101	)	)	PUNCT
eurjchem-792	160	102	,	,	PUNCT
eurjchem-792	160	103	154.62	154.62	NUM
eurjchem-792	160	104	(	(	PUNCT
eurjchem-792	160	105	ch	ch	NOUN
eurjchem-792	160	106	)	)	PUNCT
eurjchem-792	160	107	,	,	PUNCT
eurjchem-792	160	108	332	332	NUM
eurjchem-792	160	109	guruswamy	guruswamy	NOUN
eurjchem-792	160	110	et	et	PROPN
eurjchem-792	160	111	al	al	PROPN
eurjchem-792	160	112	.	.	PUNCT
eurjchem-792	160	113	/	/	SYM
eurjchem-792	160	114	european	european	PROPN
eurjchem-792	160	115	journal	journal	PROPN
eurjchem-792	160	116	of	of	ADP
eurjchem-792	160	117	chemistry	chemistry	NOUN
eurjchem-792	160	118	4	4	NUM
eurjchem-792	160	119	(	(	PUNCT
eurjchem-792	160	120	4	4	NUM
eurjchem-792	160	121	)	)	PUNCT
eurjchem-792	160	122	(	(	PUNCT
eurjchem-792	160	123	2013	2013	NUM
eurjchem-792	160	124	)	)	PUNCT
eurjchem-792	160	125	329‐335	329‐335	PROPN
eurjchem-792	160	126	scheme	scheme	NOUN
eurjchem-792	160	127	3	3	NUM
eurjchem-792	160	128	166.73	166.73	NUM
eurjchem-792	160	129	(	(	PUNCT
eurjchem-792	160	130	c	c	NOUN
eurjchem-792	160	131	=	=	NOUN
eurjchem-792	160	132	o	o	NOUN
eurjchem-792	160	133	)	)	PUNCT
eurjchem-792	160	134	,	,	PUNCT
eurjchem-792	160	135	177.07	177.07	NUM
eurjchem-792	160	136	(	(	PUNCT
eurjchem-792	160	137	c	c	NOUN
eurjchem-792	160	138	=	=	NOUN
eurjchem-792	160	139	o	o	NOUN
eurjchem-792	160	140	)	)	PUNCT
eurjchem-792	160	141	.	.	PUNCT
eurjchem-792	161	1	anal	anal	PROPN
eurjchem-792	161	2	.	.	PUNCT
eurjchem-792	161	3	calcd	calcd	NOUN
eurjchem-792	161	4	.	.	PUNCT
eurjchem-792	162	1	for	for	SCONJ
eurjchem-792	162	2	c27h28fn5o7s	c27h28fn5o7s	PROPN
eurjchem-792	162	3	:	:	PUNCT
eurjchem-792	162	4	c	c	X
eurjchem-792	162	5	,	,	PUNCT
eurjchem-792	162	6	55.38	55.38	NUM
eurjchem-792	162	7	;	;	PUNCT
eurjchem-792	162	8	h	h	NOUN
eurjchem-792	162	9	,	,	PUNCT
eurjchem-792	162	10	4.82	4.82	NUM
eurjchem-792	162	11	;	;	PUNCT
eurjchem-792	162	12	n	n	CCONJ
eurjchem-792	162	13	,	,	PUNCT
eurjchem-792	162	14	11.96	11.96	NUM
eurjchem-792	162	15	.	.	PUNCT
eurjchem-792	162	16	found	find	VERB
eurjchem-792	162	17	:	:	PUNCT
eurjchem-792	163	1	c	c	X
eurjchem-792	163	2	,	,	PUNCT
eurjchem-792	163	3	55.13	55.13	NUM
eurjchem-792	163	4	;	;	PUNCT
eurjchem-792	163	5	h	h	NOUN
eurjchem-792	163	6	,	,	PUNCT
eurjchem-792	163	7	4.71	4.71	NUM
eurjchem-792	163	8	;	;	PUNCT
eurjchem-792	163	9	n	n	CCONJ
eurjchem-792	163	10	,	,	PUNCT
eurjchem-792	163	11	11.80	11.80	NUM
eurjchem-792	163	12	%	%	NOUN
eurjchem-792	163	13	.	.	PUNCT
eurjchem-792	164	1	ms	ms	NOUN
eurjchem-792	164	2	(	(	PUNCT
eurjchem-792	164	3	m	m	PROPN
eurjchem-792	164	4	/	/	SYM
eurjchem-792	164	5	z	z	NOUN
eurjchem-792	164	6	):	):	PUNCT
eurjchem-792	164	7	586.07	586.07	NUM
eurjchem-792	164	8	(	(	PUNCT
eurjchem-792	164	9	m+	m+	NUM
eurjchem-792	164	10	)	)	PUNCT
eurjchem-792	164	11	.	.	PUNCT
eurjchem-792	165	1	specific	specific	ADJ
eurjchem-792	165	2	optical	optical	ADJ
eurjchem-792	165	3	rotation	rotation	NOUN
eurjchem-792	165	4	:	:	PUNCT
eurjchem-792	166	1	[	[	X
eurjchem-792	166	2	α]d25	α]d25	NOUN
eurjchem-792	166	3	:	:	PUNCT
eurjchem-792	166	4	‐83.24	‐83.24	PROPN
eurjchem-792	166	5	(	(	PUNCT
eurjchem-792	166	6	c	c	NOUN
eurjchem-792	166	7	=	=	SYM
eurjchem-792	166	8	1.0	1.0	NUM
eurjchem-792	166	9	in	in	ADP
eurjchem-792	166	10	methanol	methanol	NOUN
eurjchem-792	166	11	:	:	PUNCT
eurjchem-792	166	12	methylene	methylene	NOUN
eurjchem-792	166	13	chloride	chloride	NOUN
eurjchem-792	166	14	,	,	PUNCT
eurjchem-792	166	15	1:1	1:1	NUM
eurjchem-792	166	16	)	)	PUNCT
eurjchem-792	166	17	.	.	PUNCT
eurjchem-792	167	1	(	(	PUNCT
eurjchem-792	167	2	s)‐10‐(4‐(3‐(5‐methyl‐1h‐benzo[d]imidazol‐2‐ylsulfonyl)‐2‐	s)‐10‐(4‐(3‐(5‐methyl‐1h‐benzo[d]imidazol‐2‐ylsulfonyl)‐2‐	X
eurjchem-792	167	3	hydroxypropyl)piperazin‐1‐yl)‐9‐fluoro‐3,7‐dihydro‐3‐methyl‐7‐	hydroxypropyl)piperazin‐1‐yl)‐9‐fluoro‐3,7‐dihydro‐3‐methyl‐7‐	X
eurjchem-792	167	4	oxo‐2h‐[1,4]oxazino[2,3,4‐ij]quinoline‐6‐carboxylic	oxo‐2h‐[1,4]oxazino[2,3,4‐ij]quinoline‐6‐carboxylic	PROPN
eurjchem-792	167	5	acid	acid	PROPN
eurjchem-792	167	6	(	(	PUNCT
eurjchem-792	167	7	5b	5b	NUM
eurjchem-792	167	8	):	):	PUNCT
eurjchem-792	167	9	yield	yield	NOUN
eurjchem-792	167	10	:	:	PUNCT
eurjchem-792	167	11	4.15	4.15	NUM
eurjchem-792	167	12	g	g	NOUN
eurjchem-792	167	13	(	(	PUNCT
eurjchem-792	167	14	78.6	78.6	NUM
eurjchem-792	167	15	%	%	NOUN
eurjchem-792	167	16	)	)	PUNCT
eurjchem-792	167	17	.	.	PUNCT
eurjchem-792	168	1	color	color	NOUN
eurjchem-792	168	2	:	:	PUNCT
eurjchem-792	168	3	off	off	ADP
eurjchem-792	168	4	white	white	PROPN
eurjchem-792	168	5	solid	solid	PROPN
eurjchem-792	168	6	.	.	PUNCT
eurjchem-792	169	1	m.p	m.p	PROPN
eurjchem-792	169	2	.	.	PROPN
eurjchem-792	169	3	:	:	PUNCT
eurjchem-792	170	1	212‐215	212‐215	NUM
eurjchem-792	170	2	°	°	PROPN
eurjchem-792	170	3	c	c	X
eurjchem-792	170	4	.	.	PUNCT
eurjchem-792	171	1	ir	ir	PROPN
eurjchem-792	171	2	(	(	PUNCT
eurjchem-792	171	3	kbr	kbr	PROPN
eurjchem-792	171	4	,	,	PUNCT
eurjchem-792	171	5	v	v	NOUN
eurjchem-792	171	6	,	,	PUNCT
eurjchem-792	171	7	cm‐1	cm‐1	PROPN
eurjchem-792	171	8	):	):	PUNCT
eurjchem-792	171	9	3422	3422	NUM
eurjchem-792	171	10	(	(	PUNCT
eurjchem-792	171	11	oh	oh	INTJ
eurjchem-792	171	12	)	)	PUNCT
eurjchem-792	171	13	,	,	PUNCT
eurjchem-792	171	14	1710	1710	NUM
eurjchem-792	171	15	(	(	PUNCT
eurjchem-792	171	16	c	c	NOUN
eurjchem-792	171	17	=	=	NOUN
eurjchem-792	171	18	o	o	NOUN
eurjchem-792	171	19	)	)	PUNCT
eurjchem-792	171	20	,	,	PUNCT
eurjchem-792	171	21	1619	1619	NUM
eurjchem-792	171	22	(	(	PUNCT
eurjchem-792	171	23	c	c	NOUN
eurjchem-792	171	24	=	=	NOUN
eurjchem-792	171	25	o	o	NOUN
eurjchem-792	171	26	)	)	PUNCT
eurjchem-792	171	27	.	.	PUNCT
eurjchem-792	172	1	1h	1h	NUM
eurjchem-792	172	2	nmr	nmr	NOUN
eurjchem-792	172	3	(	(	PUNCT
eurjchem-792	172	4	300	300	NUM
eurjchem-792	172	5	mhz	mhz	NOUN
eurjchem-792	172	6	,	,	PUNCT
eurjchem-792	172	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-792	172	8	,	,	PUNCT
eurjchem-792	172	9	δ	δ	PROPN
eurjchem-792	172	10	,	,	PUNCT
eurjchem-792	172	11	ppm	ppm	NUM
eurjchem-792	172	12	):	):	PUNCT
eurjchem-792	172	13	1.41‐1.43	1.41‐1.43	NUM
eurjchem-792	172	14	(	(	PUNCT
eurjchem-792	172	15	d	d	PROPN
eurjchem-792	172	16	,	,	PUNCT
eurjchem-792	172	17	3h	3h	NUM
eurjchem-792	172	18	,	,	PUNCT
eurjchem-792	172	19	ch3	ch3	PROPN
eurjchem-792	172	20	,	,	PUNCT
eurjchem-792	172	21	j	j	PROPN
eurjchem-792	172	22	=	=	SYM
eurjchem-792	172	23	6.2	6.2	NUM
eurjchem-792	172	24	hz	hz	NOUN
eurjchem-792	172	25	)	)	PUNCT
eurjchem-792	172	26	,	,	PUNCT
eurjchem-792	172	27	2.47	2.47	NUM
eurjchem-792	172	28	(	(	PUNCT
eurjchem-792	172	29	s	s	PROPN
eurjchem-792	172	30	,	,	PUNCT
eurjchem-792	172	31	3h	3h	NUM
eurjchem-792	172	32	,	,	PUNCT
eurjchem-792	172	33	ar‐ch3	ar‐ch3	ADJ
eurjchem-792	172	34	)	)	PUNCT
eurjchem-792	172	35	,	,	PUNCT
eurjchem-792	172	36	2.53‐2.55	2.53‐2.55	NUM
eurjchem-792	172	37	(	(	PUNCT
eurjchem-792	172	38	m	m	PROPN
eurjchem-792	172	39	,	,	PUNCT
eurjchem-792	172	40	4h	4h	NOUN
eurjchem-792	172	41	,	,	PUNCT
eurjchem-792	172	42	2×ch2	2×ch2	ADJ
eurjchem-792	172	43	)	)	PUNCT
eurjchem-792	172	44	,	,	PUNCT
eurjchem-792	172	45	2.59‐2.61	2.59‐2.61	NUM
eurjchem-792	172	46	(	(	PUNCT
eurjchem-792	172	47	d	d	NOUN
eurjchem-792	172	48	,	,	PUNCT
eurjchem-792	172	49	2h	2h	NUM
eurjchem-792	172	50	,	,	PUNCT
eurjchem-792	172	51	ch2	ch2	PROPN
eurjchem-792	172	52	,	,	PUNCT
eurjchem-792	172	53	j	j	PROPN
eurjchem-792	173	1	=	=	SYM
eurjchem-792	173	2	6.0	6.0	NUM
eurjchem-792	173	3	hz	hz	NOUN
eurjchem-792	173	4	)	)	PUNCT
eurjchem-792	173	5	,	,	PUNCT
eurjchem-792	173	6	3.58‐3.64	3.58‐3.64	NUM
eurjchem-792	173	7	(	(	PUNCT
eurjchem-792	173	8	m	m	PROPN
eurjchem-792	173	9	,	,	PUNCT
eurjchem-792	173	10	4h	4h	NOUN
eurjchem-792	173	11	,	,	PUNCT
eurjchem-792	173	12	2×ch2	2×ch2	ADJ
eurjchem-792	173	13	)	)	PUNCT
eurjchem-792	173	14	,	,	PUNCT
eurjchem-792	173	15	3.77‐3.81	3.77‐3.81	NUM
eurjchem-792	173	16	(	(	PUNCT
eurjchem-792	173	17	m	m	PROPN
eurjchem-792	173	18	,	,	PUNCT
eurjchem-792	173	19	1h	1h	NUM
eurjchem-792	173	20	,	,	PUNCT
eurjchem-792	173	21	ch	ch	NOUN
eurjchem-792	173	22	)	)	PUNCT
eurjchem-792	173	23	,	,	PUNCT
eurjchem-792	173	24	3.85‐3.87	3.85‐3.87	NUM
eurjchem-792	173	25	(	(	PUNCT
eurjchem-792	173	26	d	d	NOUN
eurjchem-792	173	27	,	,	PUNCT
eurjchem-792	173	28	2h	2h	NUM
eurjchem-792	173	29	,	,	PUNCT
eurjchem-792	173	30	ch2	ch2	PROPN
eurjchem-792	173	31	,	,	PUNCT
eurjchem-792	173	32	j	j	PROPN
eurjchem-792	173	33	=	=	SYM
eurjchem-792	173	34	6.0	6.0	NUM
eurjchem-792	173	35	hz	hz	NOUN
eurjchem-792	173	36	)	)	PUNCT
eurjchem-792	173	37	,	,	PUNCT
eurjchem-792	173	38	4.56‐4.60	4.56‐4.60	NUM
eurjchem-792	173	39	(	(	PUNCT
eurjchem-792	173	40	m	m	PROPN
eurjchem-792	173	41	,	,	PUNCT
eurjchem-792	173	42	1h	1h	NUM
eurjchem-792	173	43	,	,	PUNCT
eurjchem-792	173	44	ch	ch	NOUN
eurjchem-792	173	45	)	)	PUNCT
eurjchem-792	173	46	,	,	PUNCT
eurjchem-792	173	47	4.61‐4.63(d	4.61‐4.63(d	NUM
eurjchem-792	173	48	,	,	PUNCT
eurjchem-792	173	49	2h	2h	NUM
eurjchem-792	173	50	,	,	PUNCT
eurjchem-792	173	51	ch2	ch2	PROPN
eurjchem-792	173	52	,	,	PUNCT
eurjchem-792	173	53	j	j	PROPN
eurjchem-792	173	54	=	=	SYM
eurjchem-792	173	55	6.0	6.0	NUM
eurjchem-792	173	56	hz	hz	NOUN
eurjchem-792	173	57	)	)	PUNCT
eurjchem-792	173	58	,	,	PUNCT
eurjchem-792	173	59	4.94	4.94	NUM
eurjchem-792	173	60	(	(	PUNCT
eurjchem-792	173	61	s	s	PROPN
eurjchem-792	173	62	,	,	PUNCT
eurjchem-792	173	63	1h	1h	NUM
eurjchem-792	173	64	,	,	PUNCT
eurjchem-792	173	65	oh	oh	INTJ
eurjchem-792	173	66	,	,	PUNCT
eurjchem-792	173	67	d2o	d2o	NOUN
eurjchem-792	173	68	exchangeable	exchangeable	ADJ
eurjchem-792	173	69	)	)	PUNCT
eurjchem-792	173	70	,	,	PUNCT
eurjchem-792	173	71	5.61	5.61	NUM
eurjchem-792	173	72	(	(	PUNCT
eurjchem-792	173	73	s	s	PROPN
eurjchem-792	173	74	,	,	PUNCT
eurjchem-792	173	75	1h	1h	NUM
eurjchem-792	173	76	,	,	PUNCT
eurjchem-792	173	77	nh	nh	PROPN
eurjchem-792	173	78	,	,	PUNCT
eurjchem-792	173	79	d2o	d2o	PROPN
eurjchem-792	173	80	exchangeable	exchangeable	ADJ
eurjchem-792	173	81	)	)	PUNCT
eurjchem-792	173	82	,	,	PUNCT
eurjchem-792	173	83	7.18‐7.21	7.18‐7.21	PROPN
eurjchem-792	173	84	(	(	PUNCT
eurjchem-792	173	85	m	m	PROPN
eurjchem-792	173	86	,	,	PUNCT
eurjchem-792	173	87	1h	1h	NUM
eurjchem-792	173	88	,	,	PUNCT
eurjchem-792	173	89	ar‐h	ar‐h	NOUN
eurjchem-792	173	90	)	)	PUNCT
eurjchem-792	173	91	,	,	PUNCT
eurjchem-792	173	92	7.24‐7.27	7.24‐7.27	NUM
eurjchem-792	173	93	(	(	PUNCT
eurjchem-792	173	94	m,1h	m,1h	PROPN
eurjchem-792	173	95	,	,	PUNCT
eurjchem-792	173	96	ar‐h	ar‐h	NOUN
eurjchem-792	173	97	)	)	PUNCT
eurjchem-792	173	98	,	,	PUNCT
eurjchem-792	173	99	7.39‐7.43	7.39‐7.43	NUM
eurjchem-792	173	100	(	(	PUNCT
eurjchem-792	173	101	m	m	PROPN
eurjchem-792	173	102	,	,	PUNCT
eurjchem-792	173	103	1h	1h	NUM
eurjchem-792	173	104	,	,	PUNCT
eurjchem-792	173	105	ar‐h	ar‐h	NOUN
eurjchem-792	173	106	)	)	PUNCT
eurjchem-792	173	107	,	,	PUNCT
eurjchem-792	173	108	7.54‐7.58	7.54‐7.58	NUM
eurjchem-792	173	109	(	(	PUNCT
eurjchem-792	173	110	d	d	PROPN
eurjchem-792	173	111	,	,	PUNCT
eurjchem-792	173	112	1h	1h	NUM
eurjchem-792	173	113	,	,	PUNCT
eurjchem-792	173	114	ar‐h	ar‐h	PROPN
eurjchem-792	173	115	,	,	PUNCT
eurjchem-792	173	116	j	j	PROPN
eurjchem-792	173	117	=	=	PROPN
eurjchem-792	173	118	12.0	12.0	NUM
eurjchem-792	173	119	hz	hz	NOUN
eurjchem-792	173	120	)	)	PUNCT
eurjchem-792	173	121	,	,	PUNCT
eurjchem-792	173	122	8.91	8.91	NUM
eurjchem-792	173	123	(	(	PUNCT
eurjchem-792	173	124	s	s	PROPN
eurjchem-792	173	125	,	,	PUNCT
eurjchem-792	173	126	1h	1h	NUM
eurjchem-792	173	127	,	,	PUNCT
eurjchem-792	173	128	c	c	NOUN
eurjchem-792	173	129	=	=	NOUN
eurjchem-792	173	130	ch	ch	NOUN
eurjchem-792	173	131	)	)	PUNCT
eurjchem-792	173	132	,	,	PUNCT
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eurjchem-792	173	134	(	(	PUNCT
eurjchem-792	173	135	s	s	PROPN
eurjchem-792	173	136	,	,	PUNCT
eurjchem-792	173	137	1h	1h	NUM
eurjchem-792	173	138	,	,	PUNCT
eurjchem-792	173	139	cooh	cooh	NOUN
eurjchem-792	173	140	,	,	PUNCT
eurjchem-792	173	141	d2o	d2o	PROPN
eurjchem-792	173	142	exchangeable	exchangeable	ADJ
eurjchem-792	173	143	)	)	PUNCT
eurjchem-792	173	144	.	.	PUNCT
eurjchem-792	174	1	13c	13c	NOUN
eurjchem-792	174	2	nmr	nmr	NOUN
eurjchem-792	174	3	(	(	PUNCT
eurjchem-792	174	4	75	75	NUM
eurjchem-792	174	5	mhz	mhz	NOUN
eurjchem-792	174	6	,	,	PUNCT
eurjchem-792	174	7	dmso‐d6	dmso‐d6	NOUN
eurjchem-792	174	8	,	,	PUNCT
eurjchem-792	174	9	ppm	ppm	NOUN
eurjchem-792	174	10	,	,	PUNCT
eurjchem-792	174	11	δ	δ	PROPN
eurjchem-792	174	12	):	):	PUNCT
eurjchem-792	174	13	18.39	18.39	NUM
eurjchem-792	174	14	(	(	PUNCT
eurjchem-792	174	15	ch3	ch3	PROPN
eurjchem-792	174	16	)	)	PUNCT
eurjchem-792	174	17	,	,	PUNCT
eurjchem-792	174	18	26.73	26.73	NUM
eurjchem-792	174	19	(	(	PUNCT
eurjchem-792	174	20	ch3	ch3	PROPN
eurjchem-792	174	21	)	)	PUNCT
eurjchem-792	174	22	,	,	PUNCT
eurjchem-792	174	23	50.35	50.35	NUM
eurjchem-792	174	24	(	(	PUNCT
eurjchem-792	174	25	2×ch2	2×ch2	ADJ
eurjchem-792	174	26	)	)	PUNCT
eurjchem-792	174	27	,	,	PUNCT
eurjchem-792	174	28	54.33	54.33	NUM
eurjchem-792	174	29	(	(	PUNCT
eurjchem-792	174	30	2×ch2	2×ch2	ADJ
eurjchem-792	174	31	)	)	PUNCT
eurjchem-792	174	32	,	,	PUNCT
eurjchem-792	174	33	59.93	59.93	NUM
eurjchem-792	174	34	(	(	PUNCT
eurjchem-792	174	35	ch2	ch2	PROPN
eurjchem-792	174	36	)	)	PUNCT
eurjchem-792	174	37	,	,	PUNCT
eurjchem-792	174	38	62.26	62.26	NUM
eurjchem-792	174	39	(	(	PUNCT
eurjchem-792	174	40	ch	ch	NOUN
eurjchem-792	174	41	)	)	PUNCT
eurjchem-792	174	42	,	,	PUNCT
eurjchem-792	174	43	64.36	64.36	NUM
eurjchem-792	174	44	(	(	PUNCT
eurjchem-792	174	45	ch	ch	NOUN
eurjchem-792	174	46	)	)	PUNCT
eurjchem-792	174	47	,	,	PUNCT
eurjchem-792	174	48	66.03	66.03	NUM
eurjchem-792	174	49	(	(	PUNCT
eurjchem-792	174	50	ch2	ch2	PROPN
eurjchem-792	174	51	)	)	PUNCT
eurjchem-792	174	52	,	,	PUNCT
eurjchem-792	174	53	6.81	6.81	NUM
eurjchem-792	174	54	(	(	PUNCT
eurjchem-792	174	55	ch2	ch2	PROPN
eurjchem-792	174	56	)	)	PUNCT
eurjchem-792	174	57	,	,	PUNCT
eurjchem-792	174	58	108.41	108.41	NUM
eurjchem-792	174	59	(	(	PUNCT
eurjchem-792	174	60	ch	ch	NOUN
eurjchem-792	174	61	)	)	PUNCT
eurjchem-792	174	62	,	,	PUNCT
eurjchem-792	174	63	109.73	109.73	NUM
eurjchem-792	174	64	(	(	PUNCT
eurjchem-792	174	65	c	c	NOUN
eurjchem-792	174	66	)	)	PUNCT
eurjchem-792	174	67	,	,	PUNCT
eurjchem-792	174	68	115.01	115.01	NUM
eurjchem-792	174	69	(	(	PUNCT
eurjchem-792	174	70	ch	ch	NOUN
eurjchem-792	174	71	)	)	PUNCT
eurjchem-792	174	72	,	,	PUNCT
eurjchem-792	174	73	119.96	119.96	NUM
eurjchem-792	174	74	(	(	PUNCT
eurjchem-792	174	75	c	c	NOUN
eurjchem-792	174	76	)	)	PUNCT
eurjchem-792	174	77	,	,	PUNCT
eurjchem-792	174	78	123.56	123.56	NUM
eurjchem-792	174	79	(	(	PUNCT
eurjchem-792	174	80	ch	ch	NOUN
eurjchem-792	174	81	)	)	PUNCT
eurjchem-792	174	82	,	,	PUNCT
eurjchem-792	174	83	124.53	124.53	NUM
eurjchem-792	174	84	(	(	PUNCT
eurjchem-792	174	85	ch	ch	NOUN
eurjchem-792	174	86	)	)	PUNCT
eurjchem-792	174	87	,	,	PUNCT
eurjchem-792	174	88	130.95	130.95	NUM
eurjchem-792	174	89	(	(	PUNCT
eurjchem-792	174	90	c	c	NOUN
eurjchem-792	174	91	)	)	PUNCT
eurjchem-792	174	92	,	,	PUNCT
eurjchem-792	174	93	134.76	134.76	NUM
eurjchem-792	174	94	(	(	PUNCT
eurjchem-792	174	95	c	c	NOUN
eurjchem-792	174	96	)	)	PUNCT
eurjchem-792	174	97	,	,	PUNCT
eurjchem-792	174	98	140.68	140.68	NUM
eurjchem-792	174	99	(	(	PUNCT
eurjchem-792	174	100	c	c	NOUN
eurjchem-792	174	101	)	)	PUNCT
eurjchem-792	174	102	,	,	PUNCT
eurjchem-792	174	103	145.53	145.53	NUM
eurjchem-792	174	104	(	(	PUNCT
eurjchem-792	174	105	c	c	NOUN
eurjchem-792	174	106	)	)	PUNCT
eurjchem-792	174	107	,	,	PUNCT
eurjchem-792	174	108	152.26	152.26	NUM
eurjchem-792	174	109	(	(	PUNCT
eurjchem-792	174	110	c	c	NOUN
eurjchem-792	174	111	)	)	PUNCT
eurjchem-792	174	112	,	,	PUNCT
eurjchem-792	174	113	154.58	154.58	NUM
eurjchem-792	174	114	(	(	PUNCT
eurjchem-792	174	115	c	c	NOUN
eurjchem-792	174	116	)	)	PUNCT
eurjchem-792	174	117	,	,	PUNCT
eurjchem-792	174	118	166.58	166.58	NUM
eurjchem-792	174	119	(	(	PUNCT
eurjchem-792	174	120	c	c	NOUN
eurjchem-792	174	121	=	=	NOUN
eurjchem-792	174	122	o	o	NOUN
eurjchem-792	174	123	)	)	PUNCT
eurjchem-792	174	124	,	,	PUNCT
eurjchem-792	174	125	176.83	176.83	NUM
eurjchem-792	174	126	(	(	PUNCT
eurjchem-792	174	127	c	c	NOUN
eurjchem-792	174	128	=	=	NOUN
eurjchem-792	174	129	o	o	NOUN
eurjchem-792	174	130	)	)	PUNCT
eurjchem-792	174	131	.	.	PUNCT
eurjchem-792	175	1	anal	anal	PROPN
eurjchem-792	175	2	.	.	PUNCT
eurjchem-792	175	3	calcd	calcd	NOUN
eurjchem-792	175	4	.	.	PUNCT
eurjchem-792	176	1	for	for	ADP
eurjchem-792	176	2	c28h30fn5o7s	c28h30fn5o7s	NOUN
eurjchem-792	176	3	:	:	PUNCT
eurjchem-792	176	4	c	c	X
eurjchem-792	176	5	,	,	PUNCT
eurjchem-792	176	6	56.08	56.08	NUM
eurjchem-792	176	7	;	;	PUNCT
eurjchem-792	176	8	h	h	NOUN
eurjchem-792	176	9	,	,	PUNCT
eurjchem-792	176	10	5.04	5.04	NUM
eurjchem-792	176	11	;	;	PUNCT
eurjchem-792	176	12	n	n	CCONJ
eurjchem-792	176	13	,	,	PUNCT
eurjchem-792	176	14	11.68	11.68	NUM
eurjchem-792	176	15	.	.	PUNCT
eurjchem-792	176	16	found	find	VERB
eurjchem-792	176	17	:	:	PUNCT
eurjchem-792	177	1	c	c	X
eurjchem-792	177	2	,	,	PUNCT
eurjchem-792	177	3	55.93	55.93	NUM
eurjchem-792	177	4	;	;	PUNCT
eurjchem-792	178	1	h	h	NOUN
eurjchem-792	178	2	,	,	PUNCT
eurjchem-792	178	3	4.92	4.92	NUM
eurjchem-792	178	4	;	;	PUNCT
eurjchem-792	178	5	n	n	CCONJ
eurjchem-792	178	6	,	,	PUNCT
eurjchem-792	178	7	11.58	11.58	NUM
eurjchem-792	178	8	%	%	NOUN
eurjchem-792	178	9	.	.	PUNCT
eurjchem-792	179	1	ms	ms	NOUN
eurjchem-792	179	2	(	(	PUNCT
eurjchem-792	179	3	m	m	PROPN
eurjchem-792	179	4	/	/	SYM
eurjchem-792	179	5	z	z	NOUN
eurjchem-792	179	6	):	):	PUNCT
eurjchem-792	179	7	600.12	600.12	NUM
eurjchem-792	179	8	(	(	PUNCT
eurjchem-792	179	9	m+	m+	NUM
eurjchem-792	179	10	)	)	PUNCT
eurjchem-792	179	11	.	.	PUNCT
eurjchem-792	180	1	[	[	X
eurjchem-792	180	2	α]d25	α]d25	NOUN
eurjchem-792	180	3	:	:	PUNCT
eurjchem-792	180	4	‐49.74	‐49.74	X
eurjchem-792	180	5	(	(	PUNCT
eurjchem-792	180	6	c	c	NOUN
eurjchem-792	180	7	=	=	SYM
eurjchem-792	180	8	1.0	1.0	NUM
eurjchem-792	180	9	in	in	ADP
eurjchem-792	180	10	methanol	methanol	NOUN
eurjchem-792	180	11	:	:	PUNCT
eurjchem-792	180	12	methylene	methylene	NOUN
eurjchem-792	180	13	chloride	chloride	NOUN
eurjchem-792	180	14	,	,	PUNCT
eurjchem-792	180	15	1:1	1:1	NUM
eurjchem-792	180	16	)	)	PUNCT
eurjchem-792	180	17	.	.	PUNCT
eurjchem-792	181	1	(	(	PUNCT
eurjchem-792	181	2	s)‐10‐(4‐(3‐(5‐methoxy‐1h‐benzo[d]imidazol‐2‐ylsulfonyl)‐	s)‐10‐(4‐(3‐(5‐methoxy‐1h‐benzo[d]imidazol‐2‐ylsulfonyl)‐	NOUN
eurjchem-792	181	3	2‐hydroxypropyl	2‐hydroxypropyl	NUM
eurjchem-792	181	4	)	)	PUNCT
eurjchem-792	181	5	piperazin‐1‐yl)‐9‐fluoro‐3,7‐dihydro‐3‐methyl‐	piperazin‐1‐yl)‐9‐fluoro‐3,7‐dihydro‐3‐methyl‐	NOUN
eurjchem-792	181	6	7‐oxo‐2h‐[1,4]oxazino[2,3,4‐ij]quinoline‐6‐carboxylic	7‐oxo‐2h‐[1,4]oxazino[2,3,4‐ij]quinoline‐6‐carboxylic	NUM
eurjchem-792	181	7	acid	acid	NOUN
eurjchem-792	181	8	(	(	PUNCT
eurjchem-792	181	9	5c	5c	NUM
eurjchem-792	181	10	):	):	PUNCT
eurjchem-792	181	11	yield	yield	NOUN
eurjchem-792	181	12	:	:	PUNCT
eurjchem-792	181	13	4.23	4.23	NUM
eurjchem-792	181	14	g	g	NOUN
eurjchem-792	181	15	(	(	PUNCT
eurjchem-792	181	16	80.4	80.4	NUM
eurjchem-792	181	17	%	%	NOUN
eurjchem-792	181	18	)	)	PUNCT
eurjchem-792	181	19	.	.	PUNCT
eurjchem-792	182	1	color	color	NOUN
eurjchem-792	182	2	:	:	PUNCT
eurjchem-792	182	3	off	off	ADP
eurjchem-792	182	4	white	white	ADJ
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eurjchem-792	182	6	.	.	PUNCT
eurjchem-792	183	1	m.p	m.p	PROPN
eurjchem-792	183	2	.	.	PROPN
eurjchem-792	183	3	:	:	PUNCT
eurjchem-792	184	1	216‐218	216‐218	NUM
eurjchem-792	184	2	°	°	SYM
eurjchem-792	184	3	c	c	X
eurjchem-792	184	4	.	.	PUNCT
eurjchem-792	185	1	ir	ir	PROPN
eurjchem-792	185	2	(	(	PUNCT
eurjchem-792	185	3	kbr	kbr	PROPN
eurjchem-792	185	4	,	,	PUNCT
eurjchem-792	185	5	v	v	NOUN
eurjchem-792	185	6	,	,	PUNCT
eurjchem-792	185	7	cm‐1	cm‐1	PROPN
eurjchem-792	185	8	):	):	PUNCT
eurjchem-792	185	9	3412	3412	NUM
eurjchem-792	185	10	(	(	PUNCT
eurjchem-792	185	11	oh	oh	INTJ
eurjchem-792	185	12	)	)	PUNCT
eurjchem-792	185	13	,	,	PUNCT
eurjchem-792	185	14	1709	1709	NUM
eurjchem-792	185	15	(	(	PUNCT
eurjchem-792	185	16	c	c	NOUN
eurjchem-792	185	17	=	=	NOUN
eurjchem-792	185	18	o	o	NOUN
eurjchem-792	185	19	)	)	PUNCT
eurjchem-792	185	20	,	,	PUNCT
eurjchem-792	185	21	1618	1618	NUM
eurjchem-792	185	22	(	(	PUNCT
eurjchem-792	185	23	c	c	NOUN
eurjchem-792	185	24	=	=	NOUN
eurjchem-792	185	25	o	o	NOUN
eurjchem-792	185	26	)	)	PUNCT
eurjchem-792	185	27	.	.	PUNCT
eurjchem-792	186	1	1h	1h	NUM
eurjchem-792	186	2	nmr	nmr	NOUN
eurjchem-792	186	3	(	(	PUNCT
eurjchem-792	186	4	300	300	NUM
eurjchem-792	186	5	mhz	mhz	NOUN
eurjchem-792	186	6	,	,	PUNCT
eurjchem-792	186	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-792	186	8	,	,	PUNCT
eurjchem-792	186	9	δ	δ	PROPN
eurjchem-792	186	10	,	,	PUNCT
eurjchem-792	186	11	ppm	ppm	NUM
eurjchem-792	186	12	):	):	PUNCT
eurjchem-792	186	13	1.40‐1.42	1.40‐1.42	NUM
eurjchem-792	186	14	(	(	PUNCT
eurjchem-792	186	15	d	d	PROPN
eurjchem-792	186	16	,	,	PUNCT
eurjchem-792	186	17	3h	3h	NUM
eurjchem-792	186	18	,	,	PUNCT
eurjchem-792	186	19	ch3	ch3	PROPN
eurjchem-792	186	20	,	,	PUNCT
eurjchem-792	186	21	j	j	PROPN
eurjchem-792	186	22	=	=	SYM
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eurjchem-792	186	24	hz	hz	NOUN
eurjchem-792	186	25	)	)	PUNCT
eurjchem-792	186	26	,	,	PUNCT
eurjchem-792	186	27	2.49‐2.55	2.49‐2.55	NUM
eurjchem-792	186	28	(	(	PUNCT
eurjchem-792	186	29	m	m	PROPN
eurjchem-792	186	30	,	,	PUNCT
eurjchem-792	186	31	4h	4h	NOUN
eurjchem-792	186	32	,	,	PUNCT
eurjchem-792	186	33	2×ch2	2×ch2	ADJ
eurjchem-792	186	34	)	)	PUNCT
eurjchem-792	186	35	,	,	PUNCT
eurjchem-792	186	36	2.72‐7.74	2.72‐7.74	NUM
eurjchem-792	186	37	(	(	PUNCT
eurjchem-792	186	38	d	d	NOUN
eurjchem-792	186	39	,	,	PUNCT
eurjchem-792	186	40	2h	2h	NUM
eurjchem-792	186	41	,	,	PUNCT
eurjchem-792	186	42	ch2	ch2	PROPN
eurjchem-792	186	43	,	,	PUNCT
eurjchem-792	186	44	j	j	PROPN
eurjchem-792	187	1	=	=	SYM
eurjchem-792	187	2	6.0	6.0	NUM
eurjchem-792	187	3	hz	hz	NOUN
eurjchem-792	187	4	)	)	PUNCT
eurjchem-792	187	5	,	,	PUNCT
eurjchem-792	187	6	3.62‐3.66	3.62‐3.66	NUM
eurjchem-792	187	7	(	(	PUNCT
eurjchem-792	187	8	m	m	PROPN
eurjchem-792	187	9	,	,	PUNCT
eurjchem-792	187	10	4h	4h	NOUN
eurjchem-792	187	11	,	,	PUNCT
eurjchem-792	187	12	2×ch2	2×ch2	ADJ
eurjchem-792	187	13	)	)	PUNCT
eurjchem-792	187	14	,	,	PUNCT
eurjchem-792	187	15	3.71‐3.75	3.71‐3.75	PROPN
eurjchem-792	187	16	(	(	PUNCT
eurjchem-792	187	17	m	m	PROPN
eurjchem-792	187	18	,	,	PUNCT
eurjchem-792	187	19	1h	1h	NUM
eurjchem-792	187	20	,	,	PUNCT
eurjchem-792	187	21	ch	ch	NOUN
eurjchem-792	187	22	)	)	PUNCT
eurjchem-792	187	23	,	,	PUNCT
eurjchem-792	187	24	3.80‐3.82	3.80‐3.82	NUM
eurjchem-792	187	25	(	(	PUNCT
eurjchem-792	187	26	d	d	NOUN
eurjchem-792	187	27	,	,	PUNCT
eurjchem-792	187	28	2h	2h	NUM
eurjchem-792	187	29	,	,	PUNCT
eurjchem-792	187	30	ch2	ch2	PROPN
eurjchem-792	187	31	,	,	PUNCT
eurjchem-792	187	32	j	j	PROPN
eurjchem-792	187	33	=	=	SYM
eurjchem-792	187	34	6.0	6.0	NUM
eurjchem-792	187	35	hz	hz	NOUN
eurjchem-792	187	36	)	)	PUNCT
eurjchem-792	187	37	,	,	PUNCT
eurjchem-792	187	38	4.01	4.01	NUM
eurjchem-792	187	39	(	(	PUNCT
eurjchem-792	187	40	s	s	PROPN
eurjchem-792	187	41	,	,	PUNCT
eurjchem-792	187	42	3h	3h	NUM
eurjchem-792	187	43	,	,	PUNCT
eurjchem-792	187	44	och3	och3	ADJ
eurjchem-792	187	45	)	)	PUNCT
eurjchem-792	187	46	,	,	PUNCT
eurjchem-792	187	47	4.51‐4.55	4.51‐4.55	NUM
eurjchem-792	187	48	(	(	PUNCT
eurjchem-792	187	49	m	m	PROPN
eurjchem-792	187	50	,	,	PUNCT
eurjchem-792	187	51	1h	1h	NUM
eurjchem-792	187	52	,	,	PUNCT
eurjchem-792	187	53	ch	ch	NOUN
eurjchem-792	187	54	)	)	PUNCT
eurjchem-792	187	55	,	,	PUNCT
eurjchem-792	187	56	4.58‐4.60	4.58‐4.60	NUM
eurjchem-792	187	57	(	(	PUNCT
eurjchem-792	187	58	d	d	NOUN
eurjchem-792	187	59	,	,	PUNCT
eurjchem-792	187	60	2h	2h	NUM
eurjchem-792	187	61	,	,	PUNCT
eurjchem-792	187	62	ch2	ch2	PROPN
eurjchem-792	187	63	,	,	PUNCT
eurjchem-792	187	64	j	j	PROPN
eurjchem-792	188	1	=	=	SYM
eurjchem-792	188	2	6.0	6.0	NUM
eurjchem-792	188	3	hz	hz	NOUN
eurjchem-792	188	4	)	)	PUNCT
eurjchem-792	188	5	,	,	PUNCT
eurjchem-792	188	6	5.07	5.07	NUM
eurjchem-792	188	7	(	(	PUNCT
eurjchem-792	188	8	s	s	PROPN
eurjchem-792	188	9	,	,	PUNCT
eurjchem-792	188	10	1h	1h	NUM
eurjchem-792	188	11	,	,	PUNCT
eurjchem-792	188	12	oh	oh	INTJ
eurjchem-792	188	13	,	,	PUNCT
eurjchem-792	188	14	d2o	d2o	NOUN
eurjchem-792	188	15	exchangeable	exchangeable	ADJ
eurjchem-792	188	16	)	)	PUNCT
eurjchem-792	188	17	,	,	PUNCT
eurjchem-792	188	18	5.48	5.48	NUM
eurjchem-792	188	19	(	(	PUNCT
eurjchem-792	188	20	s	s	PROPN
eurjchem-792	188	21	,	,	PUNCT
eurjchem-792	188	22	1h	1h	NUM
eurjchem-792	188	23	,	,	PUNCT
eurjchem-792	188	24	nh	nh	PROPN
eurjchem-792	188	25	,	,	PUNCT
eurjchem-792	188	26	d2o	d2o	PROPN
eurjchem-792	188	27	exchangeable	exchangeable	ADJ
eurjchem-792	188	28	)	)	PUNCT
eurjchem-792	188	29	,	,	PUNCT
eurjchem-792	188	30	7.11‐7.13	7.11‐7.13	NUM
eurjchem-792	188	31	(	(	PUNCT
eurjchem-792	188	32	d	d	PROPN
eurjchem-792	188	33	,	,	PUNCT
eurjchem-792	188	34	1h	1h	NUM
eurjchem-792	188	35	,	,	PUNCT
eurjchem-792	188	36	ar‐h	ar‐h	PROPN
eurjchem-792	188	37	,	,	PUNCT
eurjchem-792	188	38	j	j	PROPN
eurjchem-792	188	39	=	=	SYM
eurjchem-792	188	40	9.0	9.0	NUM
eurjchem-792	188	41	hz	hz	NOUN
eurjchem-792	188	42	)	)	PUNCT
eurjchem-792	188	43	,	,	PUNCT
eurjchem-792	188	44	7.21‐7.23	7.21‐7.23	NUM
eurjchem-792	188	45	(	(	PUNCT
eurjchem-792	188	46	m	m	PROPN
eurjchem-792	188	47	,	,	PUNCT
eurjchem-792	188	48	1h	1h	NUM
eurjchem-792	188	49	,	,	PUNCT
eurjchem-792	188	50	ar‐h	ar‐h	NOUN
eurjchem-792	188	51	)	)	PUNCT
eurjchem-792	188	52	,	,	PUNCT
eurjchem-792	188	53	7.53‐7.63	7.53‐7.63	NUM
eurjchem-792	188	54	(	(	PUNCT
eurjchem-792	188	55	m	m	PROPN
eurjchem-792	188	56	,	,	PUNCT
eurjchem-792	188	57	2h	2h	NUM
eurjchem-792	188	58	,	,	PUNCT
eurjchem-792	188	59	ar‐h	ar‐h	NOUN
eurjchem-792	188	60	)	)	PUNCT
eurjchem-792	188	61	,	,	PUNCT
eurjchem-792	188	62	8.93	8.93	NUM
eurjchem-792	188	63	(	(	PUNCT
eurjchem-792	188	64	s	s	PROPN
eurjchem-792	188	65	,	,	PUNCT
eurjchem-792	188	66	1h	1h	NUM
eurjchem-792	188	67	,	,	PUNCT
eurjchem-792	188	68	c	c	NOUN
eurjchem-792	188	69	=	=	NOUN
eurjchem-792	188	70	ch	ch	NOUN
eurjchem-792	188	71	)	)	PUNCT
eurjchem-792	188	72	,	,	PUNCT
eurjchem-792	188	73	15.12	15.12	NUM
eurjchem-792	188	74	(	(	PUNCT
eurjchem-792	188	75	s	s	PROPN
eurjchem-792	188	76	,	,	PUNCT
eurjchem-792	188	77	1h	1h	NUM
eurjchem-792	188	78	,	,	PUNCT
eurjchem-792	188	79	cooh	cooh	NOUN
eurjchem-792	188	80	,	,	PUNCT
eurjchem-792	188	81	d2o	d2o	PROPN
eurjchem-792	188	82	exchangeable	exchangeable	ADJ
eurjchem-792	188	83	)	)	PUNCT
eurjchem-792	188	84	.	.	PUNCT
eurjchem-792	189	1	13c	13c	NOUN
eurjchem-792	189	2	nmr	nmr	NOUN
eurjchem-792	189	3	(	(	PUNCT
eurjchem-792	189	4	75	75	NUM
eurjchem-792	189	5	mhz	mhz	NOUN
eurjchem-792	189	6	,	,	PUNCT
eurjchem-792	189	7	dmso‐d6	dmso‐d6	NOUN
eurjchem-792	189	8	,	,	PUNCT
eurjchem-792	189	9	ppm	ppm	NOUN
eurjchem-792	189	10	,	,	PUNCT
eurjchem-792	189	11	δ	δ	PROPN
eurjchem-792	189	12	):	):	PUNCT
eurjchem-792	189	13	18.41	18.41	NUM
eurjchem-792	189	14	(	(	PUNCT
eurjchem-792	189	15	ch3	ch3	PROPN
eurjchem-792	189	16	)	)	PUNCT
eurjchem-792	189	17	,	,	PUNCT
eurjchem-792	189	18	50.48	50.48	NUM
eurjchem-792	189	19	(	(	PUNCT
eurjchem-792	189	20	2×ch2	2×ch2	ADJ
eurjchem-792	189	21	)	)	PUNCT
eurjchem-792	189	22	,	,	PUNCT
eurjchem-792	189	23	54.76	54.76	NUM
eurjchem-792	189	24	(	(	PUNCT
eurjchem-792	189	25	2×ch2	2×ch2	ADJ
eurjchem-792	189	26	)	)	PUNCT
eurjchem-792	189	27	,	,	PUNCT
eurjchem-792	189	28	56.82	56.82	NUM
eurjchem-792	189	29	(	(	PUNCT
eurjchem-792	189	30	ch2	ch2	PROPN
eurjchem-792	189	31	)	)	PUNCT
eurjchem-792	189	32	,	,	PUNCT
eurjchem-792	189	33	58.42	58.42	NUM
eurjchem-792	189	34	(	(	PUNCT
eurjchem-792	189	35	och3	och3	ADJ
eurjchem-792	189	36	)	)	PUNCT
eurjchem-792	189	37	,	,	PUNCT
eurjchem-792	189	38	62.34	62.34	NUM
eurjchem-792	189	39	(	(	PUNCT
eurjchem-792	189	40	ch	ch	NOUN
eurjchem-792	189	41	)	)	PUNCT
eurjchem-792	189	42	,	,	PUNCT
eurjchem-792	189	43	64.56	64.56	NUM
eurjchem-792	189	44	(	(	PUNCT
eurjchem-792	189	45	ch	ch	NOUN
eurjchem-792	189	46	)	)	PUNCT
eurjchem-792	189	47	,	,	PUNCT
eurjchem-792	189	48	66.50	66.50	NUM
eurjchem-792	189	49	(	(	PUNCT
eurjchem-792	189	50	ch2	ch2	PROPN
eurjchem-792	189	51	)	)	PUNCT
eurjchem-792	189	52	,	,	PUNCT
eurjchem-792	189	53	68.61(ch2	68.61(ch2	NUM
eurjchem-792	189	54	)	)	PUNCT
eurjchem-792	189	55	,	,	PUNCT
eurjchem-792	189	56	103.27	103.27	NUM
eurjchem-792	189	57	(	(	PUNCT
eurjchem-792	189	58	ch	ch	NOUN
eurjchem-792	189	59	)	)	PUNCT
eurjchem-792	189	60	,	,	PUNCT
eurjchem-792	189	61	108.72	108.72	NUM
eurjchem-792	189	62	(	(	PUNCT
eurjchem-792	189	63	ch	ch	NOUN
eurjchem-792	189	64	)	)	PUNCT
eurjchem-792	189	65	,	,	PUNCT
eurjchem-792	189	66	109.67	109.67	NUM
eurjchem-792	189	67	(	(	PUNCT
eurjchem-792	189	68	ch	ch	NOUN
eurjchem-792	189	69	)	)	PUNCT
eurjchem-792	189	70	,	,	PUNCT
eurjchem-792	189	71	110.38	110.38	NUM
eurjchem-792	189	72	(	(	PUNCT
eurjchem-792	189	73	c	c	NOUN
eurjchem-792	189	74	)	)	PUNCT
eurjchem-792	189	75	,	,	PUNCT
eurjchem-792	189	76	118.66	118.66	NUM
eurjchem-792	189	77	(	(	PUNCT
eurjchem-792	189	78	ch	ch	NOUN
eurjchem-792	189	79	)	)	PUNCT
eurjchem-792	189	80	,	,	PUNCT
eurjchem-792	189	81	120.46	120.46	NUM
eurjchem-792	189	82	(	(	PUNCT
eurjchem-792	189	83	c	c	NOUN
eurjchem-792	189	84	)	)	PUNCT
eurjchem-792	189	85	,	,	PUNCT
eurjchem-792	189	86	129.37	129.37	NUM
eurjchem-792	189	87	(	(	PUNCT
eurjchem-792	189	88	c	c	NOUN
eurjchem-792	189	89	)	)	PUNCT
eurjchem-792	189	90	,	,	PUNCT
eurjchem-792	189	91	133.56	133.56	NUM
eurjchem-792	189	92	(	(	PUNCT
eurjchem-792	189	93	c	c	NOUN
eurjchem-792	189	94	)	)	PUNCT
eurjchem-792	189	95	,	,	PUNCT
eurjchem-792	189	96	141.38	141.38	NUM
eurjchem-792	189	97	(	(	PUNCT
eurjchem-792	189	98	c	c	NOUN
eurjchem-792	189	99	)	)	PUNCT
eurjchem-792	189	100	,	,	PUNCT
eurjchem-792	189	101	147.71	147.71	NUM
eurjchem-792	189	102	(	(	PUNCT
eurjchem-792	189	103	c	c	NOUN
eurjchem-792	189	104	)	)	PUNCT
eurjchem-792	189	105	,	,	PUNCT
eurjchem-792	189	106	152.39	152.39	NUM
eurjchem-792	189	107	(	(	PUNCT
eurjchem-792	189	108	c	c	NOUN
eurjchem-792	189	109	)	)	PUNCT
eurjchem-792	189	110	,	,	PUNCT
eurjchem-792	189	111	154.64	154.64	NUM
eurjchem-792	189	112	(	(	PUNCT
eurjchem-792	189	113	c	c	NOUN
eurjchem-792	189	114	)	)	PUNCT
eurjchem-792	189	115	,	,	PUNCT
eurjchem-792	189	116	158.41	158.41	NUM
eurjchem-792	189	117	(	(	PUNCT
eurjchem-792	189	118	c	c	NOUN
eurjchem-792	189	119	)	)	PUNCT
eurjchem-792	189	120	,	,	PUNCT
eurjchem-792	189	121	166.63	166.63	NUM
eurjchem-792	189	122	(	(	PUNCT
eurjchem-792	189	123	c	c	NOUN
eurjchem-792	189	124	=	=	NOUN
eurjchem-792	189	125	o	o	NOUN
eurjchem-792	189	126	)	)	PUNCT
eurjchem-792	189	127	,	,	PUNCT
eurjchem-792	189	128	176.74	176.74	NUM
eurjchem-792	189	129	(	(	PUNCT
eurjchem-792	189	130	c	c	NOUN
eurjchem-792	189	131	=	=	NOUN
eurjchem-792	189	132	o	o	NOUN
eurjchem-792	189	133	)	)	PUNCT
eurjchem-792	189	134	.	.	PUNCT
eurjchem-792	190	1	anal	anal	PROPN
eurjchem-792	190	2	.	.	PUNCT
eurjchem-792	190	3	calcd	calcd	NOUN
eurjchem-792	190	4	.	.	PUNCT
eurjchem-792	191	1	for	for	SCONJ
eurjchem-792	191	2	c28h30fn5o8s	c28h30fn5o8s	ADJ
eurjchem-792	191	3	:	:	PUNCT
eurjchem-792	191	4	c	c	X
eurjchem-792	191	5	,	,	PUNCT
eurjchem-792	191	6	54.63	54.63	NUM
eurjchem-792	191	7	;	;	PUNCT
eurjchem-792	191	8	h	h	NOUN
eurjchem-792	191	9	,	,	PUNCT
eurjchem-792	191	10	4.91	4.91	NUM
eurjchem-792	191	11	;	;	PUNCT
eurjchem-792	191	12	n	n	CCONJ
eurjchem-792	191	13	,	,	PUNCT
eurjchem-792	191	14	11.38	11.38	NUM
eurjchem-792	191	15	.	.	PUNCT
eurjchem-792	191	16	found	find	VERB
eurjchem-792	191	17	:	:	PUNCT
eurjchem-792	192	1	c	c	X
eurjchem-792	192	2	,	,	PUNCT
eurjchem-792	192	3	54.48	54.48	NUM
eurjchem-792	192	4	;	;	PUNCT
eurjchem-792	192	5	h	h	NOUN
eurjchem-792	192	6	,	,	PUNCT
eurjchem-792	192	7	4.80	4.80	NUM
eurjchem-792	192	8	;	;	PUNCT
eurjchem-792	192	9	n	n	CCONJ
eurjchem-792	192	10	,	,	PUNCT
eurjchem-792	192	11	11.24	11.24	NUM
eurjchem-792	192	12	%	%	NOUN
eurjchem-792	192	13	.	.	PUNCT
eurjchem-792	193	1	ms	ms	NOUN
eurjchem-792	193	2	(	(	PUNCT
eurjchem-792	193	3	m	m	PROPN
eurjchem-792	193	4	/	/	SYM
eurjchem-792	193	5	z	z	NOUN
eurjchem-792	193	6	):	):	PUNCT
eurjchem-792	193	7	616.05	616.05	NUM
eurjchem-792	193	8	(	(	PUNCT
eurjchem-792	193	9	m+	m+	NUM
eurjchem-792	193	10	)	)	PUNCT
eurjchem-792	193	11	.	.	PUNCT
eurjchem-792	194	1	[	[	X
eurjchem-792	194	2	α]d25	α]d25	NOUN
eurjchem-792	194	3	:	:	PUNCT
eurjchem-792	194	4	‐	‐	SYM
eurjchem-792	194	5	44.80	44.80	NUM
eurjchem-792	194	6	(	(	PUNCT
eurjchem-792	194	7	c	c	NOUN
eurjchem-792	194	8	=	=	SYM
eurjchem-792	194	9	1.0	1.0	NUM
eurjchem-792	194	10	in	in	ADP
eurjchem-792	194	11	methanol	methanol	NOUN
eurjchem-792	194	12	:	:	PUNCT
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eurjchem-792	194	14	chloride	chloride	NOUN
eurjchem-792	194	15	,	,	PUNCT
eurjchem-792	194	16	1:1	1:1	NUM
eurjchem-792	194	17	)	)	PUNCT
eurjchem-792	194	18	.	.	PUNCT
eurjchem-792	195	1	(	(	PUNCT
eurjchem-792	195	2	s)‐10‐(4‐(3‐(5‐(difluoromethoxy)‐1h‐benzo[d]imidazol‐2‐	s)‐10‐(4‐(3‐(5‐(difluoromethoxy)‐1h‐benzo[d]imidazol‐2‐	PROPN
eurjchem-792	195	3	ylsulfonyl)‐2‐hydroxypropyl)piperazin‐1‐yl)‐9‐fluoro‐3,7‐	ylsulfonyl)‐2‐hydroxypropyl)piperazin‐1‐yl)‐9‐fluoro‐3,7‐	PROPN
eurjchem-792	195	4	dihydro‐3‐methyl‐7‐oxo‐2h‐[1,4]oxazino[2,3,4‐ij]quinoline‐6‐	dihydro‐3‐methyl‐7‐oxo‐2h‐[1,4]oxazino[2,3,4‐ij]quinoline‐6‐	NOUN
eurjchem-792	195	5	carboxylic	carboxylic	ADJ
eurjchem-792	195	6	acid	acid	NOUN
eurjchem-792	195	7	(	(	PUNCT
eurjchem-792	195	8	5d	5d	NUM
eurjchem-792	195	9	):	):	PUNCT
eurjchem-792	195	10	yield	yield	NOUN
eurjchem-792	195	11	:	:	PUNCT
eurjchem-792	195	12	4.17	4.17	NUM
eurjchem-792	195	13	g	g	NOUN
eurjchem-792	195	14	(	(	PUNCT
eurjchem-792	195	15	79.5	79.5	NUM
eurjchem-792	195	16	%	%	NOUN
eurjchem-792	195	17	)	)	PUNCT
eurjchem-792	195	18	.	.	PUNCT
eurjchem-792	196	1	color	color	NOUN
eurjchem-792	196	2	:	:	PUNCT
eurjchem-792	196	3	off	off	ADP
eurjchem-792	196	4	white	white	PROPN
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eurjchem-792	196	6	.	.	PUNCT
eurjchem-792	197	1	m.p	m.p	PROPN
eurjchem-792	197	2	.	.	PROPN
eurjchem-792	197	3	:	:	PUNCT
eurjchem-792	198	1	208‐210	208‐210	NUM
eurjchem-792	198	2	°	°	ADP
eurjchem-792	198	3	c	c	X
eurjchem-792	198	4	.	.	PUNCT
eurjchem-792	199	1	ir	ir	PROPN
eurjchem-792	199	2	(	(	PUNCT
eurjchem-792	199	3	kbr	kbr	PROPN
eurjchem-792	199	4	,	,	PUNCT
eurjchem-792	199	5	v	v	NOUN
eurjchem-792	199	6	,	,	PUNCT
eurjchem-792	199	7	cm‐1	cm‐1	PROPN
eurjchem-792	199	8	):	):	PUNCT
eurjchem-792	199	9	3412	3412	NUM
eurjchem-792	199	10	(	(	PUNCT
eurjchem-792	199	11	oh	oh	INTJ
eurjchem-792	199	12	)	)	PUNCT
eurjchem-792	199	13	,	,	PUNCT
eurjchem-792	199	14	1708	1708	NUM
eurjchem-792	199	15	(	(	PUNCT
eurjchem-792	199	16	c	c	NOUN
eurjchem-792	199	17	=	=	NOUN
eurjchem-792	199	18	o	o	NOUN
eurjchem-792	199	19	)	)	PUNCT
eurjchem-792	199	20	,	,	PUNCT
eurjchem-792	199	21	1619	1619	NUM
eurjchem-792	199	22	(	(	PUNCT
eurjchem-792	199	23	c	c	NOUN
eurjchem-792	199	24	=	=	NOUN
eurjchem-792	199	25	o	o	NOUN
eurjchem-792	199	26	)	)	PUNCT
eurjchem-792	199	27	.	.	PUNCT
eurjchem-792	200	1	1h	1h	NUM
eurjchem-792	200	2	nmr	nmr	NOUN
eurjchem-792	200	3	(	(	PUNCT
eurjchem-792	200	4	300	300	NUM
eurjchem-792	200	5	mhz	mhz	NOUN
eurjchem-792	200	6	,	,	PUNCT
eurjchem-792	200	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-792	200	8	,	,	PUNCT
eurjchem-792	200	9	δ	δ	PROPN
eurjchem-792	200	10	,	,	PUNCT
eurjchem-792	200	11	ppm	ppm	NUM
eurjchem-792	200	12	):	):	PUNCT
eurjchem-792	200	13	1.38‐	1.38‐	NUM
eurjchem-792	200	14	1.40	1.40	NUM
eurjchem-792	200	15	(	(	PUNCT
eurjchem-792	200	16	d	d	PROPN
eurjchem-792	200	17	,	,	PUNCT
eurjchem-792	200	18	3h	3h	NUM
eurjchem-792	200	19	,	,	PUNCT
eurjchem-792	200	20	ch3	ch3	PROPN
eurjchem-792	200	21	,	,	PUNCT
eurjchem-792	200	22	j	j	PROPN
eurjchem-792	200	23	=	=	SYM
eurjchem-792	200	24	6.2	6.2	NUM
eurjchem-792	200	25	hz	hz	NOUN
eurjchem-792	200	26	)	)	PUNCT
eurjchem-792	200	27	,	,	PUNCT
eurjchem-792	200	28	2.56‐2.61	2.56‐2.61	NUM
eurjchem-792	200	29	(	(	PUNCT
eurjchem-792	200	30	m	m	PROPN
eurjchem-792	200	31	,	,	PUNCT
eurjchem-792	200	32	4h	4h	NOUN
eurjchem-792	200	33	,	,	PUNCT
eurjchem-792	200	34	2×ch2	2×ch2	ADJ
eurjchem-792	200	35	)	)	PUNCT
eurjchem-792	200	36	,	,	PUNCT
eurjchem-792	200	37	2.79‐2.81	2.79‐2.81	NUM
eurjchem-792	200	38	(	(	PUNCT
eurjchem-792	200	39	d	d	NOUN
eurjchem-792	200	40	,	,	PUNCT
eurjchem-792	200	41	2h	2h	NUM
eurjchem-792	200	42	,	,	PUNCT
eurjchem-792	200	43	ch2	ch2	PROPN
eurjchem-792	200	44	,	,	PUNCT
eurjchem-792	200	45	j	j	PROPN
eurjchem-792	201	1	=	=	SYM
eurjchem-792	201	2	6.0	6.0	NUM
eurjchem-792	201	3	hz	hz	NOUN
eurjchem-792	201	4	)	)	PUNCT
eurjchem-792	201	5	,	,	PUNCT
eurjchem-792	201	6	3.55‐3.61	3.55‐3.61	NUM
eurjchem-792	201	7	(	(	PUNCT
eurjchem-792	201	8	m	m	PROPN
eurjchem-792	201	9	,	,	PUNCT
eurjchem-792	201	10	4h	4h	NOUN
eurjchem-792	201	11	,	,	PUNCT
eurjchem-792	201	12	2×ch2	2×ch2	ADJ
eurjchem-792	201	13	)	)	PUNCT
eurjchem-792	201	14	,	,	PUNCT
eurjchem-792	201	15	3.71‐3.74	3.71‐3.74	NUM
eurjchem-792	201	16	(	(	PUNCT
eurjchem-792	201	17	m	m	PROPN
eurjchem-792	201	18	,	,	PUNCT
eurjchem-792	201	19	1h	1h	NUM
eurjchem-792	201	20	,	,	PUNCT
eurjchem-792	201	21	ch	ch	NOUN
eurjchem-792	201	22	)	)	PUNCT
eurjchem-792	201	23	,	,	PUNCT
eurjchem-792	201	24	3.81‐3.83	3.81‐3.83	PROPN
eurjchem-792	201	25	(	(	PUNCT
eurjchem-792	201	26	d	d	NOUN
eurjchem-792	201	27	,	,	PUNCT
eurjchem-792	201	28	2h	2h	NUM
eurjchem-792	201	29	,	,	PUNCT
eurjchem-792	201	30	ch2	ch2	PROPN
eurjchem-792	201	31	,	,	PUNCT
eurjchem-792	201	32	j	j	PROPN
eurjchem-792	201	33	=	=	SYM
eurjchem-792	201	34	6.0	6.0	NUM
eurjchem-792	201	35	hz	hz	NOUN
eurjchem-792	201	36	)	)	PUNCT
eurjchem-792	201	37	,	,	PUNCT
eurjchem-792	201	38	4.42‐4.46	4.42‐4.46	NUM
eurjchem-792	201	39	(	(	PUNCT
eurjchem-792	201	40	m	m	PROPN
eurjchem-792	201	41	,	,	PUNCT
eurjchem-792	201	42	1h	1h	NUM
eurjchem-792	201	43	,	,	PUNCT
eurjchem-792	201	44	ch	ch	NOUN
eurjchem-792	201	45	)	)	PUNCT
eurjchem-792	201	46	,	,	PUNCT
eurjchem-792	201	47	4.62‐4.64	4.62‐4.64	NUM
eurjchem-792	201	48	(	(	PUNCT
eurjchem-792	201	49	d	d	PROPN
eurjchem-792	201	50	,	,	PUNCT
eurjchem-792	201	51	2h	2h	NUM
eurjchem-792	201	52	,	,	PUNCT
eurjchem-792	201	53	ch2	ch2	PROPN
eurjchem-792	201	54	,	,	PUNCT
eurjchem-792	201	55	j	j	PROPN
eurjchem-792	202	1	=	=	SYM
eurjchem-792	202	2	6.0	6.0	NUM
eurjchem-792	202	3	hz	hz	NOUN
eurjchem-792	202	4	)	)	PUNCT
eurjchem-792	202	5	,	,	PUNCT
eurjchem-792	202	6	4.99	4.99	NUM
eurjchem-792	202	7	(	(	PUNCT
eurjchem-792	202	8	s	s	PROPN
eurjchem-792	202	9	,	,	PUNCT
eurjchem-792	202	10	1h	1h	NUM
eurjchem-792	202	11	,	,	PUNCT
eurjchem-792	202	12	oh	oh	INTJ
eurjchem-792	202	13	,	,	PUNCT
eurjchem-792	202	14	d2o	d2o	NOUN
eurjchem-792	202	15	exchangeable	exchangeable	ADJ
eurjchem-792	202	16	)	)	PUNCT
eurjchem-792	202	17	,	,	PUNCT
eurjchem-792	202	18	5.36	5.36	NUM
eurjchem-792	202	19	(	(	PUNCT
eurjchem-792	202	20	s	s	PROPN
eurjchem-792	202	21	,	,	PUNCT
eurjchem-792	202	22	1h	1h	NUM
eurjchem-792	202	23	,	,	PUNCT
eurjchem-792	202	24	nh	nh	PROPN
eurjchem-792	202	25	,	,	PUNCT
eurjchem-792	202	26	d2o	d2o	PROPN
eurjchem-792	202	27	exchangeable	exchangeable	ADJ
eurjchem-792	202	28	)	)	PUNCT
eurjchem-792	202	29	,	,	PUNCT
eurjchem-792	202	30	7.02‐7.03	7.02‐7.03	NUM
eurjchem-792	202	31	(	(	PUNCT
eurjchem-792	202	32	m	m	PROPN
eurjchem-792	202	33	,	,	PUNCT
eurjchem-792	202	34	1h	1h	NUM
eurjchem-792	202	35	,	,	PUNCT
eurjchem-792	202	36	ar‐h	ar‐h	NOUN
eurjchem-792	202	37	)	)	PUNCT
eurjchem-792	202	38	,	,	PUNCT
eurjchem-792	202	39	7.34‐7.38	7.34‐7.38	NUM
eurjchem-792	202	40	(	(	PUNCT
eurjchem-792	202	41	m	m	PROPN
eurjchem-792	202	42	,	,	PUNCT
eurjchem-792	202	43	2h	2h	NUM
eurjchem-792	202	44	,	,	PUNCT
eurjchem-792	202	45	ar‐h	ar‐h	NOUN
eurjchem-792	202	46	)	)	PUNCT
eurjchem-792	202	47	,	,	PUNCT
eurjchem-792	202	48	7.41	7.41	NUM
eurjchem-792	202	49	(	(	PUNCT
eurjchem-792	202	50	s	s	PROPN
eurjchem-792	202	51	,	,	PUNCT
eurjchem-792	202	52	1h	1h	NUM
eurjchem-792	202	53	,	,	PUNCT
eurjchem-792	202	54	ar‐h	ar‐h	NOUN
eurjchem-792	202	55	)	)	PUNCT
eurjchem-792	202	56	,	,	PUNCT
eurjchem-792	202	57	7.57‐	7.57‐	NUM
eurjchem-792	202	58	7.61	7.61	NUM
eurjchem-792	202	59	(	(	PUNCT
eurjchem-792	202	60	m	m	PROPN
eurjchem-792	202	61	,	,	PUNCT
eurjchem-792	202	62	1h	1h	NUM
eurjchem-792	202	63	,	,	PUNCT
eurjchem-792	202	64	ar‐h	ar‐h	NOUN
eurjchem-792	202	65	)	)	PUNCT
eurjchem-792	202	66	,	,	PUNCT
eurjchem-792	202	67	8.86	8.86	NUM
eurjchem-792	202	68	(	(	PUNCT
eurjchem-792	202	69	s	s	PROPN
eurjchem-792	202	70	,	,	PUNCT
eurjchem-792	202	71	1h	1h	NUM
eurjchem-792	202	72	,	,	PUNCT
eurjchem-792	202	73	c	c	NOUN
eurjchem-792	202	74	=	=	NOUN
eurjchem-792	202	75	ch	ch	NOUN
eurjchem-792	202	76	)	)	PUNCT
eurjchem-792	202	77	,	,	PUNCT
eurjchem-792	202	78	15.11	15.11	NUM
eurjchem-792	202	79	(	(	PUNCT
eurjchem-792	202	80	s	s	PROPN
eurjchem-792	202	81	,	,	PUNCT
eurjchem-792	202	82	1h	1h	NUM
eurjchem-792	202	83	,	,	PUNCT
eurjchem-792	202	84	cooh	cooh	NOUN
eurjchem-792	202	85	,	,	PUNCT
eurjchem-792	202	86	d2o	d2o	PROPN
eurjchem-792	202	87	exchangeable	exchangeable	ADJ
eurjchem-792	202	88	)	)	PUNCT
eurjchem-792	202	89	.	.	PUNCT
eurjchem-792	203	1	13c	13c	NOUN
eurjchem-792	203	2	nmr	nmr	NOUN
eurjchem-792	203	3	(	(	PUNCT
eurjchem-792	203	4	75	75	NUM
eurjchem-792	203	5	mhz	mhz	NOUN
eurjchem-792	203	6	,	,	PUNCT
eurjchem-792	203	7	dmso‐d6	dmso‐d6	NOUN
eurjchem-792	203	8	,	,	PUNCT
eurjchem-792	203	9	ppm	ppm	NOUN
eurjchem-792	203	10	,	,	PUNCT
eurjchem-792	203	11	δ	δ	PROPN
eurjchem-792	203	12	):	):	PUNCT
eurjchem-792	203	13	18.37	18.37	NUM
eurjchem-792	203	14	(	(	PUNCT
eurjchem-792	203	15	ch3	ch3	PROPN
eurjchem-792	203	16	)	)	PUNCT
eurjchem-792	203	17	,	,	PUNCT
eurjchem-792	203	18	50.41(2×ch2	50.41(2×ch2	NUM
eurjchem-792	203	19	)	)	PUNCT
eurjchem-792	203	20	,	,	PUNCT
eurjchem-792	203	21	54.68	54.68	NUM
eurjchem-792	203	22	(	(	PUNCT
eurjchem-792	203	23	2×ch2	2×ch2	ADJ
eurjchem-792	203	24	)	)	PUNCT
eurjchem-792	203	25	,	,	PUNCT
eurjchem-792	203	26	60.31	60.31	NUM
eurjchem-792	203	27	(	(	PUNCT
eurjchem-792	203	28	ch2	ch2	PROPN
eurjchem-792	203	29	)	)	PUNCT
eurjchem-792	203	30	,	,	PUNCT
eurjchem-792	203	31	62.18	62.18	NUM
eurjchem-792	203	32	(	(	PUNCT
eurjchem-792	203	33	ch	ch	NOUN
eurjchem-792	203	34	)	)	PUNCT
eurjchem-792	203	35	,	,	PUNCT
eurjchem-792	203	36	64.58	64.58	NUM
eurjchem-792	203	37	(	(	PUNCT
eurjchem-792	203	38	ch	ch	NOUN
eurjchem-792	203	39	)	)	PUNCT
eurjchem-792	203	40	,	,	PUNCT
eurjchem-792	203	41	66.50	66.50	NUM
eurjchem-792	203	42	(	(	PUNCT
eurjchem-792	203	43	ch2	ch2	PROPN
eurjchem-792	203	44	)	)	PUNCT
eurjchem-792	203	45	,	,	PUNCT
eurjchem-792	203	46	68.73	68.73	NUM
eurjchem-792	203	47	(	(	PUNCT
eurjchem-792	203	48	ch2	ch2	PROPN
eurjchem-792	203	49	)	)	PUNCT
eurjchem-792	203	50	,	,	PUNCT
eurjchem-792	203	51	102.31	102.31	NUM
eurjchem-792	203	52	(	(	PUNCT
eurjchem-792	203	53	ch	ch	NOUN
eurjchem-792	203	54	)	)	PUNCT
eurjchem-792	203	55	,	,	PUNCT
eurjchem-792	203	56	107.88	107.88	NUM
eurjchem-792	203	57	(	(	PUNCT
eurjchem-792	203	58	ch	ch	NOUN
eurjchem-792	203	59	)	)	PUNCT
eurjchem-792	203	60	,	,	PUNCT
eurjchem-792	203	61	109.43	109.43	NUM
eurjchem-792	203	62	(	(	PUNCT
eurjchem-792	203	63	ch	ch	NOUN
eurjchem-792	203	64	)	)	PUNCT
eurjchem-792	203	65	,	,	PUNCT
eurjchem-792	203	66	110.63	110.63	NUM
eurjchem-792	203	67	(	(	PUNCT
eurjchem-792	203	68	c	c	NOUN
eurjchem-792	203	69	)	)	PUNCT
eurjchem-792	203	70	,	,	PUNCT
eurjchem-792	203	71	118.54	118.54	NUM
eurjchem-792	203	72	(	(	PUNCT
eurjchem-792	203	73	ch	ch	NOUN
eurjchem-792	203	74	)	)	PUNCT
eurjchem-792	203	75	,	,	PUNCT
eurjchem-792	203	76	119.94	119.94	NUM
eurjchem-792	203	77	(	(	PUNCT
eurjchem-792	203	78	c	c	NOUN
eurjchem-792	203	79	)	)	PUNCT
eurjchem-792	203	80	,	,	PUNCT
eurjchem-792	203	81	129.81	129.81	NUM
eurjchem-792	203	82	(	(	PUNCT
eurjchem-792	203	83	c	c	NOUN
eurjchem-792	203	84	)	)	PUNCT
eurjchem-792	203	85	,	,	PUNCT
eurjchem-792	203	86	133.01	133.01	NUM
eurjchem-792	203	87	(	(	PUNCT
eurjchem-792	203	88	c	c	NOUN
eurjchem-792	203	89	)	)	PUNCT
eurjchem-792	203	90	,	,	PUNCT
eurjchem-792	203	91	142.62	142.62	NUM
eurjchem-792	203	92	(	(	PUNCT
eurjchem-792	203	93	c	c	NOUN
eurjchem-792	203	94	)	)	PUNCT
eurjchem-792	203	95	,	,	PUNCT
eurjchem-792	203	96	148.35	148.35	NUM
eurjchem-792	203	97	(	(	PUNCT
eurjchem-792	203	98	c	c	NOUN
eurjchem-792	203	99	)	)	PUNCT
eurjchem-792	203	100	,	,	PUNCT
eurjchem-792	203	101	152.17	152.17	NUM
eurjchem-792	203	102	(	(	PUNCT
eurjchem-792	203	103	c	c	NOUN
eurjchem-792	203	104	)	)	PUNCT
eurjchem-792	203	105	,	,	PUNCT
eurjchem-792	203	106	154.38	154.38	NUM
eurjchem-792	203	107	(	(	PUNCT
eurjchem-792	203	108	c	c	NOUN
eurjchem-792	203	109	)	)	PUNCT
eurjchem-792	203	110	,	,	PUNCT
eurjchem-792	203	111	158.49	158.49	NUM
eurjchem-792	203	112	(	(	PUNCT
eurjchem-792	203	113	c	c	NOUN
eurjchem-792	203	114	)	)	PUNCT
eurjchem-792	203	115	,	,	PUNCT
eurjchem-792	203	116	164.28	164.28	NUM
eurjchem-792	203	117	(	(	PUNCT
eurjchem-792	203	118	chf2	chf2	PROPN
eurjchem-792	203	119	)	)	PUNCT
eurjchem-792	203	120	,	,	PUNCT
eurjchem-792	203	121	166.52	166.52	NUM
eurjchem-792	203	122	(	(	PUNCT
eurjchem-792	203	123	c	c	NOUN
eurjchem-792	203	124	=	=	NOUN
eurjchem-792	203	125	o	o	NOUN
eurjchem-792	203	126	)	)	PUNCT
eurjchem-792	203	127	,	,	PUNCT
eurjchem-792	203	128	176.79	176.79	NUM
eurjchem-792	203	129	(	(	PUNCT
eurjchem-792	203	130	c	c	NOUN
eurjchem-792	203	131	=	=	NOUN
eurjchem-792	203	132	o	o	NOUN
eurjchem-792	203	133	)	)	PUNCT
eurjchem-792	203	134	.	.	PUNCT
eurjchem-792	204	1	anal	anal	PROPN
eurjchem-792	204	2	.	.	PUNCT
eurjchem-792	204	3	calcd	calcd	NOUN
eurjchem-792	204	4	.	.	PUNCT
eurjchem-792	205	1	for	for	SCONJ
eurjchem-792	205	2	c28h28f3n5o8s	c28h28f3n5o8s	ADJ
eurjchem-792	205	3	:	:	PUNCT
eurjchem-792	205	4	c	c	X
eurjchem-792	205	5	,	,	PUNCT
eurjchem-792	205	6	51.61	51.61	NUM
eurjchem-792	205	7	;	;	PUNCT
eurjchem-792	205	8	h	h	NOUN
eurjchem-792	205	9	,	,	PUNCT
eurjchem-792	205	10	4.33	4.33	NUM
eurjchem-792	205	11	;	;	PUNCT
eurjchem-792	205	12	n	n	CCONJ
eurjchem-792	205	13	,	,	PUNCT
eurjchem-792	205	14	10.75	10.75	NUM
eurjchem-792	205	15	.	.	PUNCT
eurjchem-792	205	16	found	find	VERB
eurjchem-792	205	17	:	:	PUNCT
eurjchem-792	206	1	c	c	X
eurjchem-792	206	2	,	,	PUNCT
eurjchem-792	206	3	51.48	51.48	NUM
eurjchem-792	206	4	;	;	PUNCT
eurjchem-792	206	5	h	h	NOUN
eurjchem-792	206	6	,	,	PUNCT
eurjchem-792	206	7	4.20	4.20	NUM
eurjchem-792	206	8	;	;	PUNCT
eurjchem-792	206	9	n	n	CCONJ
eurjchem-792	206	10	,	,	PUNCT
eurjchem-792	206	11	10.62	10.62	NUM
eurjchem-792	206	12	%	%	NOUN
eurjchem-792	206	13	.	.	PUNCT
eurjchem-792	207	1	ms	ms	NOUN
eurjchem-792	207	2	(	(	PUNCT
eurjchem-792	207	3	m	m	PROPN
eurjchem-792	207	4	/	/	SYM
eurjchem-792	207	5	z	z	NOUN
eurjchem-792	207	6	):	):	PUNCT
eurjchem-792	207	7	652.11	652.11	NUM
eurjchem-792	207	8	(	(	PUNCT
eurjchem-792	207	9	m+	m+	NUM
eurjchem-792	207	10	)	)	PUNCT
eurjchem-792	207	11	.	.	PUNCT
eurjchem-792	208	1	[	[	X
eurjchem-792	208	2	α]d25	α]d25	NOUN
eurjchem-792	208	3	:	:	PUNCT
eurjchem-792	208	4	‐54.10	‐54.10	PROPN
eurjchem-792	208	5	(	(	PUNCT
eurjchem-792	208	6	c	c	NOUN
eurjchem-792	208	7	=	=	SYM
eurjchem-792	208	8	1.0	1.0	NUM
eurjchem-792	208	9	in	in	ADP
eurjchem-792	208	10	methanol	methanol	NOUN
eurjchem-792	208	11	:	:	PUNCT
eurjchem-792	208	12	methylene	methylene	NOUN
eurjchem-792	208	13	chloride	chloride	NOUN
eurjchem-792	208	14	,	,	PUNCT
eurjchem-792	208	15	1:1	1:1	NUM
eurjchem-792	208	16	)	)	PUNCT
eurjchem-792	208	17	.	.	PUNCT
eurjchem-792	209	1	(	(	PUNCT
eurjchem-792	209	2	s)‐10‐(4‐(3‐(5‐chloro‐1h‐benzo[d]imidazol‐2‐ylsulfonyl)‐2‐	s)‐10‐(4‐(3‐(5‐chloro‐1h‐benzo[d]imidazol‐2‐ylsulfonyl)‐2‐	ADV
eurjchem-792	209	3	hydroxypropyl)piperazin‐1‐yl)‐9‐fluoro‐3,7‐dihydro‐3‐methyl‐7‐	hydroxypropyl)piperazin‐1‐yl)‐9‐fluoro‐3,7‐dihydro‐3‐methyl‐7‐	PROPN
eurjchem-792	209	4	oxo‐2h‐[1,4]oxazino[2,3,4‐ij]quinoline‐6‐carboxylic	oxo‐2h‐[1,4]oxazino[2,3,4‐ij]quinoline‐6‐carboxylic	PROPN
eurjchem-792	209	5	acid	acid	PROPN
eurjchem-792	209	6	(	(	PUNCT
eurjchem-792	209	7	5e	5e	NOUN
eurjchem-792	209	8	):	):	PUNCT
eurjchem-792	209	9	yield	yield	NOUN
eurjchem-792	209	10	:	:	PUNCT
eurjchem-792	209	11	4.60	4.60	NUM
eurjchem-792	209	12	g	g	NOUN
eurjchem-792	209	13	(	(	PUNCT
eurjchem-792	209	14	86.8	86.8	NUM
eurjchem-792	209	15	%	%	NOUN
eurjchem-792	209	16	)	)	PUNCT
eurjchem-792	209	17	.	.	PUNCT
eurjchem-792	210	1	color	color	NOUN
eurjchem-792	210	2	:	:	PUNCT
eurjchem-792	210	3	off	off	ADP
eurjchem-792	210	4	white	white	ADJ
eurjchem-792	210	5	powder	powder	NOUN
eurjchem-792	210	6	.	.	PUNCT
eurjchem-792	211	1	m.p	m.p	PROPN
eurjchem-792	211	2	.	.	PROPN
eurjchem-792	211	3	:	:	PUNCT
eurjchem-792	212	1	197‐199	197‐199	NUM
eurjchem-792	212	2	°	°	SYM
eurjchem-792	212	3	c	c	X
eurjchem-792	212	4	.	.	PUNCT
eurjchem-792	213	1	ir	ir	PROPN
eurjchem-792	213	2	(	(	PUNCT
eurjchem-792	213	3	kbr	kbr	PROPN
eurjchem-792	213	4	,	,	PUNCT
eurjchem-792	213	5	v	v	NOUN
eurjchem-792	213	6	,	,	PUNCT
eurjchem-792	213	7	cm‐1	cm‐1	PROPN
eurjchem-792	213	8	):	):	PUNCT
eurjchem-792	213	9	3416	3416	NUM
eurjchem-792	213	10	(	(	PUNCT
eurjchem-792	213	11	oh	oh	INTJ
eurjchem-792	213	12	)	)	PUNCT
eurjchem-792	213	13	,	,	PUNCT
eurjchem-792	213	14	1708	1708	NUM
eurjchem-792	213	15	(	(	PUNCT
eurjchem-792	213	16	c	c	NOUN
eurjchem-792	213	17	=	=	NOUN
eurjchem-792	213	18	o	o	NOUN
eurjchem-792	213	19	)	)	PUNCT
eurjchem-792	213	20	,	,	PUNCT
eurjchem-792	213	21	1619	1619	NUM
eurjchem-792	213	22	(	(	PUNCT
eurjchem-792	213	23	c	c	NOUN
eurjchem-792	213	24	=	=	NOUN
eurjchem-792	213	25	o	o	NOUN
eurjchem-792	213	26	)	)	PUNCT
eurjchem-792	213	27	.	.	PUNCT
eurjchem-792	214	1	1h	1h	NUM
eurjchem-792	214	2	nmr	nmr	NOUN
eurjchem-792	214	3	(	(	PUNCT
eurjchem-792	214	4	300	300	NUM
eurjchem-792	214	5	mhz	mhz	NOUN
eurjchem-792	214	6	,	,	PUNCT
eurjchem-792	214	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-792	214	8	,	,	PUNCT
eurjchem-792	214	9	δ	δ	PROPN
eurjchem-792	214	10	,	,	PUNCT
eurjchem-792	214	11	ppm	ppm	NUM
eurjchem-792	214	12	):	):	PUNCT
eurjchem-792	214	13	1.39‐1.41	1.39‐1.41	NUM
eurjchem-792	214	14	(	(	PUNCT
eurjchem-792	214	15	d	d	PROPN
eurjchem-792	214	16	,	,	PUNCT
eurjchem-792	214	17	3h	3h	NUM
eurjchem-792	214	18	,	,	PUNCT
eurjchem-792	214	19	ch3	ch3	PROPN
eurjchem-792	214	20	,	,	PUNCT
eurjchem-792	214	21	j	j	PROPN
eurjchem-792	214	22	=	=	SYM
eurjchem-792	214	23	6.2	6.2	NUM
eurjchem-792	214	24	hz	hz	NOUN
eurjchem-792	214	25	)	)	PUNCT
eurjchem-792	214	26	,	,	PUNCT
eurjchem-792	214	27	2.71‐2.75	2.71‐2.75	NUM
eurjchem-792	214	28	(	(	PUNCT
eurjchem-792	214	29	m	m	PROPN
eurjchem-792	214	30	,	,	PUNCT
eurjchem-792	214	31	4h	4h	NOUN
eurjchem-792	214	32	,	,	PUNCT
eurjchem-792	214	33	2×ch2	2×ch2	ADJ
eurjchem-792	214	34	)	)	PUNCT
eurjchem-792	214	35	,	,	PUNCT
eurjchem-792	214	36	2.78‐2.80	2.78‐2.80	NUM
eurjchem-792	214	37	(	(	PUNCT
eurjchem-792	214	38	d	d	NOUN
eurjchem-792	214	39	,	,	PUNCT
eurjchem-792	214	40	2h	2h	NUM
eurjchem-792	214	41	,	,	PUNCT
eurjchem-792	214	42	ch2	ch2	PROPN
eurjchem-792	214	43	,	,	PUNCT
eurjchem-792	214	44	j	j	PROPN
eurjchem-792	214	45	=	=	SYM
eurjchem-792	214	46	6.0	6.0	NUM
eurjchem-792	214	47	hz	hz	NOUN
eurjchem-792	214	48	)	)	PUNCT
eurjchem-792	214	49	,	,	PUNCT
eurjchem-792	214	50	3.69‐3.73	3.69‐3.73	NUM
eurjchem-792	214	51	(	(	PUNCT
eurjchem-792	214	52	m	m	PROPN
eurjchem-792	214	53	,	,	PUNCT
eurjchem-792	214	54	4h	4h	NOUN
eurjchem-792	214	55	,	,	PUNCT
eurjchem-792	214	56	2×ch2	2×ch2	ADJ
eurjchem-792	214	57	)	)	PUNCT
eurjchem-792	214	58	,	,	PUNCT
eurjchem-792	214	59	3.76‐3.80	3.76‐3.80	NUM
eurjchem-792	214	60	(	(	PUNCT
eurjchem-792	214	61	m	m	PROPN
eurjchem-792	214	62	,	,	PUNCT
eurjchem-792	214	63	1h	1h	NUM
eurjchem-792	214	64	,	,	PUNCT
eurjchem-792	214	65	ch	ch	NOUN
eurjchem-792	214	66	)	)	PUNCT
eurjchem-792	214	67	,	,	PUNCT
eurjchem-792	214	68	3.84‐3.86	3.84‐3.86	NUM
eurjchem-792	214	69	(	(	PUNCT
eurjchem-792	214	70	d	d	NOUN
eurjchem-792	214	71	,	,	PUNCT
eurjchem-792	214	72	2h	2h	NUM
eurjchem-792	214	73	,	,	PUNCT
eurjchem-792	214	74	ch2	ch2	PROPN
eurjchem-792	214	75	,	,	PUNCT
eurjchem-792	214	76	j	j	PROPN
eurjchem-792	214	77	=	=	SYM
eurjchem-792	214	78	6.0	6.0	NUM
eurjchem-792	214	79	hz	hz	NOUN
eurjchem-792	214	80	)	)	PUNCT
eurjchem-792	214	81	,	,	PUNCT
eurjchem-792	214	82	4.53‐4.57	4.53‐4.57	NUM
eurjchem-792	214	83	(	(	PUNCT
eurjchem-792	214	84	m	m	PROPN
eurjchem-792	214	85	,	,	PUNCT
eurjchem-792	214	86	1h	1h	NUM
eurjchem-792	214	87	,	,	PUNCT
eurjchem-792	214	88	ch	ch	NOUN
eurjchem-792	214	89	)	)	PUNCT
eurjchem-792	214	90	,	,	PUNCT
eurjchem-792	214	91	4.69‐4.71	4.69‐4.71	NUM
eurjchem-792	214	92	(	(	PUNCT
eurjchem-792	214	93	d	d	PROPN
eurjchem-792	214	94	,	,	PUNCT
eurjchem-792	214	95	2h	2h	NUM
eurjchem-792	214	96	,	,	PUNCT
eurjchem-792	214	97	ch	ch	NOUN
eurjchem-792	214	98	,	,	PUNCT
eurjchem-792	214	99	j	j	PROPN
eurjchem-792	215	1	=	=	SYM
eurjchem-792	215	2	6.0	6.0	NUM
eurjchem-792	215	3	hz	hz	NOUN
eurjchem-792	215	4	)	)	PUNCT
eurjchem-792	215	5	,	,	PUNCT
eurjchem-792	215	6	5.07	5.07	NUM
eurjchem-792	215	7	(	(	PUNCT
eurjchem-792	215	8	s	s	PROPN
eurjchem-792	215	9	,	,	PUNCT
eurjchem-792	215	10	1h	1h	NUM
eurjchem-792	215	11	,	,	PUNCT
eurjchem-792	215	12	oh	oh	INTJ
eurjchem-792	215	13	,	,	PUNCT
eurjchem-792	215	14	d2o	d2o	NOUN
eurjchem-792	215	15	exchangeable	exchangeable	ADJ
eurjchem-792	215	16	)	)	PUNCT
eurjchem-792	215	17	,	,	PUNCT
eurjchem-792	215	18	5.48	5.48	NUM
eurjchem-792	215	19	(	(	PUNCT
eurjchem-792	215	20	s	s	PROPN
eurjchem-792	215	21	,	,	PUNCT
eurjchem-792	215	22	1h	1h	NUM
eurjchem-792	215	23	,	,	PUNCT
eurjchem-792	215	24	oh	oh	INTJ
eurjchem-792	215	25	,	,	PUNCT
eurjchem-792	215	26	d2o	d2o	NOUN
eurjchem-792	215	27	exchangeable	exchangeable	ADJ
eurjchem-792	215	28	)	)	PUNCT
eurjchem-792	215	29	,	,	PUNCT
eurjchem-792	215	30	7.24‐7.28	7.24‐7.28	NUM
eurjchem-792	215	31	(	(	PUNCT
eurjchem-792	215	32	m	m	PROPN
eurjchem-792	215	33	,	,	PUNCT
eurjchem-792	215	34	1h	1h	NUM
eurjchem-792	215	35	,	,	PUNCT
eurjchem-792	215	36	ar‐h	ar‐h	NOUN
eurjchem-792	215	37	)	)	PUNCT
eurjchem-792	215	38	,	,	PUNCT
eurjchem-792	215	39	7.48‐7.53	7.48‐7.53	NUM
eurjchem-792	215	40	(	(	PUNCT
eurjchem-792	215	41	m	m	PROPN
eurjchem-792	215	42	,	,	PUNCT
eurjchem-792	215	43	2h	2h	NUM
eurjchem-792	215	44	,	,	PUNCT
eurjchem-792	215	45	ar‐h	ar‐h	NOUN
eurjchem-792	215	46	)	)	PUNCT
eurjchem-792	215	47	,	,	PUNCT
eurjchem-792	215	48	7.58‐7.62	7.58‐7.62	NUM
eurjchem-792	215	49	(	(	PUNCT
eurjchem-792	215	50	d	d	PROPN
eurjchem-792	215	51	,	,	PUNCT
eurjchem-792	215	52	1h	1h	NUM
eurjchem-792	215	53	,	,	PUNCT
eurjchem-792	215	54	ar‐h	ar‐h	PROPN
eurjchem-792	215	55	,	,	PUNCT
eurjchem-792	215	56	j	j	PROPN
eurjchem-792	215	57	=	=	PROPN
eurjchem-792	215	58	12.0	12.0	NUM
eurjchem-792	215	59	hz	hz	NOUN
eurjchem-792	215	60	)	)	PUNCT
eurjchem-792	215	61	,	,	PUNCT
eurjchem-792	215	62	8.89	8.89	NUM
eurjchem-792	215	63	(	(	PUNCT
eurjchem-792	215	64	s	s	PROPN
eurjchem-792	215	65	,	,	PUNCT
eurjchem-792	215	66	1h	1h	NUM
eurjchem-792	215	67	,	,	PUNCT
eurjchem-792	215	68	c	c	NOUN
eurjchem-792	215	69	=	=	NOUN
eurjchem-792	215	70	ch	ch	NOUN
eurjchem-792	215	71	)	)	PUNCT
eurjchem-792	215	72	,	,	PUNCT
eurjchem-792	215	73	15.10	15.10	NUM
eurjchem-792	215	74	(	(	PUNCT
eurjchem-792	215	75	s	s	PROPN
eurjchem-792	215	76	,	,	PUNCT
eurjchem-792	215	77	1h	1h	NUM
eurjchem-792	215	78	,	,	PUNCT
eurjchem-792	215	79	cooh	cooh	NOUN
eurjchem-792	215	80	,	,	PUNCT
eurjchem-792	215	81	d2o	d2o	PROPN
eurjchem-792	215	82	exchangeable	exchangeable	ADJ
eurjchem-792	215	83	)	)	PUNCT
eurjchem-792	215	84	.	.	PUNCT
eurjchem-792	216	1	13c	13c	NOUN
eurjchem-792	216	2	nmr	nmr	NOUN
eurjchem-792	216	3	(	(	PUNCT
eurjchem-792	216	4	75	75	NUM
eurjchem-792	216	5	mhz	mhz	NOUN
eurjchem-792	216	6	,	,	PUNCT
eurjchem-792	216	7	dmso‐d6	dmso‐d6	NOUN
eurjchem-792	216	8	,	,	PUNCT
eurjchem-792	216	9	ppm	ppm	NOUN
eurjchem-792	216	10	,	,	PUNCT
eurjchem-792	216	11	δ	δ	PROPN
eurjchem-792	216	12	):	):	PUNCT
eurjchem-792	216	13	18.39	18.39	NUM
eurjchem-792	216	14	(	(	PUNCT
eurjchem-792	216	15	ch3	ch3	PROPN
eurjchem-792	216	16	)	)	PUNCT
eurjchem-792	216	17	,	,	PUNCT
eurjchem-792	216	18	51.08	51.08	NUM
eurjchem-792	216	19	(	(	PUNCT
eurjchem-792	216	20	2×ch2	2×ch2	ADJ
eurjchem-792	216	21	)	)	PUNCT
eurjchem-792	216	22	,	,	PUNCT
eurjchem-792	216	23	54.84	54.84	NUM
eurjchem-792	216	24	(	(	PUNCT
eurjchem-792	216	25	2×ch2	2×ch2	ADJ
eurjchem-792	216	26	)	)	PUNCT
eurjchem-792	216	27	,	,	PUNCT
eurjchem-792	216	28	60.12	60.12	NUM
eurjchem-792	216	29	(	(	PUNCT
eurjchem-792	216	30	ch2	ch2	PROPN
eurjchem-792	216	31	)	)	PUNCT
eurjchem-792	216	32	,	,	PUNCT
eurjchem-792	216	33	62.49	62.49	NUM
eurjchem-792	216	34	(	(	PUNCT
eurjchem-792	216	35	ch	ch	NOUN
eurjchem-792	216	36	)	)	PUNCT
eurjchem-792	216	37	,	,	PUNCT
eurjchem-792	216	38	64.51	64.51	NUM
eurjchem-792	216	39	(	(	PUNCT
eurjchem-792	216	40	ch	ch	NOUN
eurjchem-792	216	41	)	)	PUNCT
eurjchem-792	216	42	,	,	PUNCT
eurjchem-792	216	43	66.24	66.24	NUM
eurjchem-792	216	44	(	(	PUNCT
eurjchem-792	216	45	ch2	ch2	PROPN
eurjchem-792	216	46	)	)	PUNCT
eurjchem-792	216	47	,	,	PUNCT
eurjchem-792	216	48	68.62	68.62	NUM
eurjchem-792	216	49	(	(	PUNCT
eurjchem-792	216	50	ch2	ch2	PROPN
eurjchem-792	216	51	)	)	PUNCT
eurjchem-792	216	52	,	,	PUNCT
eurjchem-792	216	53	108.18	108.18	NUM
eurjchem-792	216	54	(	(	PUNCT
eurjchem-792	216	55	ch	ch	NOUN
eurjchem-792	216	56	)	)	PUNCT
eurjchem-792	216	57	,	,	PUNCT
eurjchem-792	216	58	109.25	109.25	NUM
eurjchem-792	216	59	(	(	PUNCT
eurjchem-792	216	60	c	c	NOUN
eurjchem-792	216	61	)	)	PUNCT
eurjchem-792	216	62	,	,	PUNCT
eurjchem-792	216	63	114.27	114.27	NUM
eurjchem-792	216	64	(	(	PUNCT
eurjchem-792	216	65	ch	ch	NOUN
eurjchem-792	216	66	)	)	PUNCT
eurjchem-792	216	67	,	,	PUNCT
eurjchem-792	216	68	114.99	114.99	NUM
eurjchem-792	216	69	(	(	PUNCT
eurjchem-792	216	70	ch	ch	NOUN
eurjchem-792	216	71	)	)	PUNCT
eurjchem-792	216	72	,	,	PUNCT
eurjchem-792	216	73	119.53	119.53	NUM
eurjchem-792	216	74	(	(	PUNCT
eurjchem-792	216	75	c	c	NOUN
eurjchem-792	216	76	)	)	PUNCT
eurjchem-792	216	77	,	,	PUNCT
eurjchem-792	216	78	124.32	124.32	NUM
eurjchem-792	216	79	(	(	PUNCT
eurjchem-792	216	80	ch	ch	NOUN
eurjchem-792	216	81	)	)	PUNCT
eurjchem-792	216	82	,	,	PUNCT
eurjchem-792	216	83	131.21	131.21	NUM
eurjchem-792	216	84	(	(	PUNCT
eurjchem-792	216	85	c	c	NOUN
eurjchem-792	216	86	)	)	PUNCT
eurjchem-792	216	87	,	,	PUNCT
eurjchem-792	216	88	134.76	134.76	NUM
eurjchem-792	216	89	(	(	PUNCT
eurjchem-792	216	90	c	c	NOUN
eurjchem-792	216	91	)	)	PUNCT
eurjchem-792	216	92	,	,	PUNCT
eurjchem-792	216	93	137.26	137.26	NUM
eurjchem-792	216	94	(	(	PUNCT
eurjchem-792	216	95	c	c	NOUN
eurjchem-792	216	96	)	)	PUNCT
eurjchem-792	216	97	,	,	PUNCT
eurjchem-792	216	98	141.14	141.14	NUM
eurjchem-792	216	99	(	(	PUNCT
eurjchem-792	216	100	c	c	NOUN
eurjchem-792	216	101	)	)	PUNCT
eurjchem-792	216	102	,	,	PUNCT
eurjchem-792	216	103	146.52	146.52	NUM
eurjchem-792	216	104	(	(	PUNCT
eurjchem-792	216	105	c	c	NOUN
eurjchem-792	216	106	)	)	PUNCT
eurjchem-792	216	107	,	,	PUNCT
eurjchem-792	216	108	152.32	152.32	NUM
eurjchem-792	216	109	(	(	PUNCT
eurjchem-792	216	110	ch	ch	NOUN
eurjchem-792	216	111	)	)	PUNCT
eurjchem-792	216	112	,	,	PUNCT
eurjchem-792	216	113	166.48	166.48	NUM
eurjchem-792	216	114	(	(	PUNCT
eurjchem-792	216	115	c	c	NOUN
eurjchem-792	216	116	=	=	NOUN
eurjchem-792	216	117	o	o	NOUN
eurjchem-792	216	118	)	)	PUNCT
eurjchem-792	216	119	,	,	PUNCT
eurjchem-792	216	120	176.58	176.58	NUM
eurjchem-792	216	121	(	(	PUNCT
eurjchem-792	216	122	c	c	NOUN
eurjchem-792	216	123	=	=	NOUN
eurjchem-792	216	124	o	o	NOUN
eurjchem-792	216	125	)	)	PUNCT
eurjchem-792	216	126	.	.	PUNCT
eurjchem-792	217	1	anal	anal	PROPN
eurjchem-792	217	2	.	.	PUNCT
eurjchem-792	217	3	calcd	calcd	NOUN
eurjchem-792	217	4	.	.	PUNCT
eurjchem-792	218	1	for	for	ADP
eurjchem-792	218	2	c27h27clfn5o7s	c27h27clfn5o7s	NOUN
eurjchem-792	218	3	:	:	PUNCT
eurjchem-792	218	4	c	c	X
eurjchem-792	218	5	,	,	PUNCT
eurjchem-792	218	6	52.30	52.30	NUM
eurjchem-792	218	7	;	;	PUNCT
eurjchem-792	218	8	h	h	NOUN
eurjchem-792	218	9	,	,	PUNCT
eurjchem-792	218	10	4.39	4.39	NUM
eurjchem-792	218	11	;	;	PUNCT
eurjchem-792	218	12	n	n	CCONJ
eurjchem-792	218	13	,	,	PUNCT
eurjchem-792	218	14	11.29	11.29	NUM
eurjchem-792	218	15	.	.	PUNCT
eurjchem-792	218	16	found	find	VERB
eurjchem-792	218	17	:	:	PUNCT
eurjchem-792	219	1	c	c	X
eurjchem-792	219	2	,	,	PUNCT
eurjchem-792	219	3	52.17	52.17	NUM
eurjchem-792	219	4	;	;	PUNCT
eurjchem-792	219	5	h	h	NOUN
eurjchem-792	219	6	,	,	PUNCT
eurjchem-792	219	7	4.24	4.24	NUM
eurjchem-792	219	8	;	;	PUNCT
eurjchem-792	219	9	n	n	CCONJ
eurjchem-792	219	10	,	,	PUNCT
eurjchem-792	219	11	11.18	11.18	NUM
eurjchem-792	219	12	%	%	NOUN
eurjchem-792	219	13	.	.	PUNCT
eurjchem-792	220	1	es	es	X
eurjchem-792	220	2	(	(	PUNCT
eurjchem-792	220	3	m	m	PROPN
eurjchem-792	220	4	/	/	SYM
eurjchem-792	220	5	z	z	NOUN
eurjchem-792	220	6	):	):	PUNCT
eurjchem-792	220	7	620.61	620.61	NUM
eurjchem-792	220	8	(	(	PUNCT
eurjchem-792	220	9	m+	m+	NUM
eurjchem-792	220	10	)	)	PUNCT
eurjchem-792	220	11	.	.	PUNCT
eurjchem-792	221	1	[	[	X
eurjchem-792	221	2	α]d25	α]d25	NUM
eurjchem-792	221	3	:	:	PUNCT
eurjchem-792	221	4	‐61.29	‐61.29	NOUN
eurjchem-792	221	5	(	(	PUNCT
eurjchem-792	221	6	c	c	NOUN
eurjchem-792	221	7	=	=	SYM
eurjchem-792	221	8	1.0	1.0	NUM
eurjchem-792	221	9	in	in	ADP
eurjchem-792	221	10	methanol	methanol	NOUN
eurjchem-792	221	11	:	:	PUNCT
eurjchem-792	221	12	methylene	methylene	NOUN
eurjchem-792	221	13	chloride	chloride	NOUN
eurjchem-792	221	14	,	,	PUNCT
eurjchem-792	221	15	1:1	1:1	NUM
eurjchem-792	221	16	)	)	PUNCT
eurjchem-792	221	17	.	.	PUNCT
eurjchem-792	222	1	2.3	2.3	NUM
eurjchem-792	222	2	.	.	PUNCT
eurjchem-792	223	1	biological	biological	ADJ
eurjchem-792	223	2	evaluation	evaluation	NOUN
eurjchem-792	223	3	2.3.1	2.3.1	NUM
eurjchem-792	223	4	.	.	PUNCT
eurjchem-792	223	5	antibacterial	antibacterial	ADJ
eurjchem-792	223	6	activity	activity	NOUN
eurjchem-792	223	7	the	the	DET
eurjchem-792	223	8	compounds	compound	NOUN
eurjchem-792	223	9	2	2	NUM
eurjchem-792	223	10	,	,	PUNCT
eurjchem-792	223	11	3	3	NUM
eurjchem-792	223	12	,	,	PUNCT
eurjchem-792	223	13	4a‐e	4a‐e	NOUN
eurjchem-792	223	14	and	and	CCONJ
eurjchem-792	223	15	5a‐e	5a‐e	NOUN
eurjchem-792	223	16	were	be	AUX
eurjchem-792	223	17	assayed	assayed	ADJ
eurjchem-792	223	18	for	for	ADP
eurjchem-792	223	19	antibacterial	antibacterial	ADJ
eurjchem-792	223	20	activity	activity	NOUN
eurjchem-792	223	21	against	against	ADP
eurjchem-792	223	22	three	three	NUM
eurjchem-792	223	23	representative	representative	ADJ
eurjchem-792	223	24	gram‐	gram‐	NOUN
eurjchem-792	223	25	positive	positive	ADJ
eurjchem-792	223	26	organisms	organism	NOUN
eurjchem-792	223	27	viz	viz	VERB
eurjchem-792	223	28	.	.	PUNCT
eurjchem-792	224	1	bacillus	bacillus	NOUN
eurjchem-792	224	2	subtilis	subtili	NOUN
eurjchem-792	224	3	(	(	PUNCT
eurjchem-792	224	4	mtcc	mtcc	NOUN
eurjchem-792	224	5	441	441	NUM
eurjchem-792	224	6	)	)	PUNCT
eurjchem-792	224	7	,	,	PUNCT
eurjchem-792	224	8	staphylococcus	staphylococcus	NOUN
eurjchem-792	224	9	aureus	aureus	NOUN
eurjchem-792	224	10	(	(	PUNCT
eurjchem-792	224	11	mtcc	mtcc	NOUN
eurjchem-792	224	12	96	96	NUM
eurjchem-792	224	13	)	)	PUNCT
eurjchem-792	224	14	,	,	PUNCT
eurjchem-792	224	15	staphylococcus	staphylococcus	NOUN
eurjchem-792	224	16	epidermidis	epidermidi	NOUN
eurjchem-792	224	17	and	and	CCONJ
eurjchem-792	224	18	three	three	NUM
eurjchem-792	224	19	gram‐negative	gram‐negative	ADJ
eurjchem-792	224	20	organisms	organism	NOUN
eurjchem-792	224	21	viz	viz	X
eurjchem-792	224	22	escherichia	escherichia	NOUN
eurjchem-792	224	23	coli	coli	NOUN
eurjchem-792	224	24	(	(	PUNCT
eurjchem-792	224	25	mtcc	mtcc	NOUN
eurjchem-792	224	26	443	443	NUM
eurjchem-792	224	27	)	)	PUNCT
eurjchem-792	224	28	,	,	PUNCT
eurjchem-792	224	29	pseudomonas	pseudomona	VERB
eurjchem-792	224	30	aeruginosa	aeruginosa	NOUN
eurjchem-792	224	31	(	(	PUNCT
eurjchem-792	224	32	mtcc	mtcc	NOUN
eurjchem-792	224	33	741	741	NUM
eurjchem-792	224	34	)	)	PUNCT
eurjchem-792	224	35	and	and	CCONJ
eurjchem-792	224	36	klebsiella	klebsiella	NOUN
eurjchem-792	224	37	pneumoniae	pneumoniae	ADJ
eurjchem-792	224	38	(	(	PUNCT
eurjchem-792	224	39	mtcc	mtcc	NOUN
eurjchem-792	224	40	618	618	NUM
eurjchem-792	224	41	)	)	PUNCT
eurjchem-792	224	42	by	by	ADP
eurjchem-792	224	43	broth	broth	ADJ
eurjchem-792	224	44	dilution	dilution	NOUN
eurjchem-792	224	45	method	method	NOUN
eurjchem-792	224	46	recommended	recommend	VERB
eurjchem-792	224	47	by	by	ADP
eurjchem-792	224	48	national	national	ADJ
eurjchem-792	224	49	committee	committee	PROPN
eurjchem-792	224	50	for	for	ADP
eurjchem-792	224	51	clinical	clinical	ADJ
eurjchem-792	224	52	laboratory	laboratory	NOUN
eurjchem-792	224	53	(	(	PUNCT
eurjchem-792	224	54	nccl	nccl	ADJ
eurjchem-792	224	55	)	)	PUNCT
eurjchem-792	224	56	standards	standard	NOUN
eurjchem-792	225	1	[	[	X
eurjchem-792	225	2	19	19	NUM
eurjchem-792	225	3	]	]	PUNCT
eurjchem-792	225	4	.	.	PUNCT
eurjchem-792	226	1	levofloxacin	levofloxacin	PROPN
eurjchem-792	226	2	was	be	AUX
eurjchem-792	226	3	used	use	VERB
eurjchem-792	226	4	as	as	ADP
eurjchem-792	226	5	reference	reference	NOUN
eurjchem-792	226	6	standard	standard	NOUN
eurjchem-792	226	7	.	.	PUNCT
eurjchem-792	227	1	the	the	DET
eurjchem-792	227	2	minimum	minimum	ADJ
eurjchem-792	227	3	inhibitory	inhibitory	ADJ
eurjchem-792	227	4	concentration	concentration	NOUN
eurjchem-792	227	5	(	(	PUNCT
eurjchem-792	227	6	mic	mic	ADJ
eurjchem-792	227	7	)	)	PUNCT
eurjchem-792	227	8	values	value	NOUN
eurjchem-792	227	9	are	be	AUX
eurjchem-792	227	10	presented	present	VERB
eurjchem-792	227	11	in	in	ADP
eurjchem-792	227	12	table	table	NOUN
eurjchem-792	227	13	1	1	NUM
eurjchem-792	227	14	.	.	NOUN
eurjchem-792	227	15	2.3.2	2.3.2	NUM
eurjchem-792	227	16	.	.	PUNCT
eurjchem-792	227	17	antifungal	antifungal	ADJ
eurjchem-792	227	18	activity	activity	NOUN
eurjchem-792	227	19	in	in	ADP
eurjchem-792	227	20	vitro	vitro	X
eurjchem-792	227	21	antifungal	antifungal	ADJ
eurjchem-792	227	22	activity	activity	NOUN
eurjchem-792	227	23	of	of	ADP
eurjchem-792	227	24	the	the	DET
eurjchem-792	227	25	newly	newly	ADV
eurjchem-792	227	26	synthesized	synthesize	VERB
eurjchem-792	227	27	compounds	compound	NOUN
eurjchem-792	227	28	ware	ware	NOUN
eurjchem-792	227	29	studied	study	VERB
eurjchem-792	227	30	against	against	ADP
eurjchem-792	227	31	the	the	DET
eurjchem-792	227	32	fungal	fungal	ADJ
eurjchem-792	227	33	strains	strain	NOUN
eurjchem-792	227	34	,	,	PUNCT
eurjchem-792	227	35	candida	candida	NOUN
eurjchem-792	227	36	albicans	albican	NOUN
eurjchem-792	227	37	(	(	PUNCT
eurjchem-792	227	38	mtcc	mtcc	NOUN
eurjchem-792	227	39	227	227	NUM
eurjchem-792	227	40	)	)	PUNCT
eurjchem-792	227	41	,	,	PUNCT
eurjchem-792	227	42	candida	candida	PROPN
eurjchem-792	227	43	rugosa	rugosa	NOUN
eurjchem-792	227	44	(	(	PUNCT
eurjchem-792	227	45	ncim	ncim	NOUN
eurjchem-792	227	46	3467	3467	NUM
eurjchem-792	227	47	)	)	PUNCT
eurjchem-792	227	48	,	,	PUNCT
eurjchem-792	227	49	aspergillus	aspergillus	NOUN
eurjchem-792	227	50	flavus	flavus	NOUN
eurjchem-792	227	51	(	(	PUNCT
eurjchem-792	227	52	mtcc	mtcc	NOUN
eurjchem-792	227	53	277	277	NUM
eurjchem-792	227	54	)	)	PUNCT
eurjchem-792	227	55	and	and	CCONJ
eurjchem-792	227	56	saccharomyces	saccharomyce	NOUN
eurjchem-792	227	57	cervisiae	cervisiae	NOUN
eurjchem-792	227	58	(	(	PUNCT
eurjchem-792	227	59	mtcc	mtcc	NOUN
eurjchem-792	227	60	36	36	NUM
eurjchem-792	227	61	)	)	PUNCT
eurjchem-792	227	62	of	of	ADP
eurjchem-792	227	63	yeasts	yeast	NOUN
eurjchem-792	227	64	by	by	ADP
eurjchem-792	227	65	agar	agar	NOUN
eurjchem-792	227	66	well	well	ADJ
eurjchem-792	227	67	diffusion	diffusion	NOUN
eurjchem-792	227	68	method	method	NOUN
eurjchem-792	227	69	[	[	X
eurjchem-792	227	70	20	20	NUM
eurjchem-792	227	71	]	]	PUNCT
eurjchem-792	227	72	in	in	ADP
eurjchem-792	227	73	100	100	NUM
eurjchem-792	227	74	and	and	CCONJ
eurjchem-792	227	75	150	150	NUM
eurjchem-792	227	76	µg	µg	ADJ
eurjchem-792	227	77	/	/	SYM
eurjchem-792	227	78	ml	ml	NOUN
eurjchem-792	227	79	concentrations	concentration	NOUN
eurjchem-792	227	80	.	.	PUNCT
eurjchem-792	228	1	guruswamy	guruswamy	NOUN
eurjchem-792	228	2	et	et	PROPN
eurjchem-792	228	3	al	al	PROPN
eurjchem-792	228	4	.	.	PUNCT
eurjchem-792	228	5	/	/	SYM
eurjchem-792	228	6	european	european	PROPN
eurjchem-792	228	7	journal	journal	PROPN
eurjchem-792	228	8	of	of	ADP
eurjchem-792	228	9	chemistry	chemistry	NOUN
eurjchem-792	228	10	4	4	NUM
eurjchem-792	228	11	(	(	PUNCT
eurjchem-792	228	12	4	4	NUM
eurjchem-792	228	13	)	)	PUNCT
eurjchem-792	228	14	(	(	PUNCT
eurjchem-792	228	15	2013	2013	NUM
eurjchem-792	228	16	)	)	PUNCT
eurjchem-792	228	17	329‐335	329‐335	NOUN
eurjchem-792	228	18	333	333	NUM
eurjchem-792	228	19	table	table	NOUN
eurjchem-792	228	20	1	1	NUM
eurjchem-792	228	21	.	.	PUNCT
eurjchem-792	229	1	minimum	minimum	ADJ
eurjchem-792	229	2	inhibitory	inhibitory	ADJ
eurjchem-792	229	3	concentration	concentration	NOUN
eurjchem-792	229	4	(	(	PUNCT
eurjchem-792	229	5	mic	mic	ADJ
eurjchem-792	229	6	)	)	PUNCT
eurjchem-792	229	7	values	value	NOUN
eurjchem-792	229	8	of	of	ADP
eurjchem-792	229	9	compounds	compound	NOUN
eurjchem-792	229	10	2	2	NUM
eurjchem-792	229	11	,	,	PUNCT
eurjchem-792	229	12	3	3	NUM
eurjchem-792	229	13	,	,	PUNCT
eurjchem-792	229	14	4a‐e	4a‐e	NOUN
eurjchem-792	229	15	and	and	CCONJ
eurjchem-792	229	16	5a‐e	5a‐e	PROPN
eurjchem-792	229	17	.	.	PUNCT
eurjchem-792	230	1	sample	sample	NOUN
eurjchem-792	230	2	no	no	DET
eurjchem-792	230	3	test	test	NOUN
eurjchem-792	230	4	compounds	compound	VERB
eurjchem-792	230	5	microorganisms	microorganism	NOUN
eurjchem-792	230	6	and	and	CCONJ
eurjchem-792	230	7	minimum	minimum	ADJ
eurjchem-792	230	8	inhibitory	inhibitory	ADJ
eurjchem-792	230	9	concentration	concentration	NOUN
eurjchem-792	230	10	(	(	PUNCT
eurjchem-792	230	11	mic	mic	ADJ
eurjchem-792	230	12	)	)	PUNCT
eurjchem-792	231	1	µg	µg	ADJ
eurjchem-792	231	2	/	/	SYM
eurjchem-792	231	3	ml	ml	PROPN
eurjchem-792	231	4	b.	b.	PROPN
eurjchem-792	231	5	subtilis	subtilis	PROPN
eurjchem-792	231	6	s.	s.	PROPN
eurjchem-792	231	7	aureus	aureus	PROPN
eurjchem-792	231	8	s.	s.	PROPN
eurjchem-792	231	9	epidermidis	epidermidis	PROPN
eurjchem-792	231	10	e.	e.	PROPN
eurjchem-792	231	11	coli	coli	PROPN
eurjchem-792	231	12	p.	p.	NOUN
eurjchem-792	231	13	aeruginosa	aeruginosa	PROPN
eurjchem-792	232	1	k.	k.	PROPN
eurjchem-792	232	2	pneumoniae	pneumoniae	ADJ
eurjchem-792	232	3	1	1	NUM
eurjchem-792	232	4	2	2	NUM
eurjchem-792	232	5	6.9	6.9	NUM
eurjchem-792	232	6	0.75	0.75	NUM
eurjchem-792	232	7	1.20	1.20	NUM
eurjchem-792	232	8	0.75	0.75	NUM
eurjchem-792	232	9	2.20	2.20	NUM
eurjchem-792	232	10	2.20	2.20	NUM
eurjchem-792	232	11	2	2	NUM
eurjchem-792	232	12	3	3	NUM
eurjchem-792	232	13	7.5	7.5	NUM
eurjchem-792	232	14	6.17	6.17	NUM
eurjchem-792	232	15	7.37	7.37	NUM
eurjchem-792	232	16	7.37	7.37	NUM
eurjchem-792	232	17	6.68	6.68	NUM
eurjchem-792	232	18	3.75	3.75	NUM
eurjchem-792	232	19	3	3	NUM
eurjchem-792	232	20	4a	4a	NOUN
eurjchem-792	232	21	2.64	2.64	NUM
eurjchem-792	232	22	0.66	0.66	NUM
eurjchem-792	232	23	0.84	0.84	NUM
eurjchem-792	232	24	7.22	7.22	NUM
eurjchem-792	232	25	2.16	2.16	NUM
eurjchem-792	232	26	4.32	4.32	NUM
eurjchem-792	232	27	4	4	NUM
eurjchem-792	232	28	4b	4b	NOUN
eurjchem-792	232	29	2.34	2.34	NUM
eurjchem-792	232	30	3.24	3.24	NUM
eurjchem-792	232	31	4.12	4.12	NUM
eurjchem-792	232	32	6.34	6.34	NUM
eurjchem-792	232	33	1.18	1.18	NUM
eurjchem-792	232	34	6.42	6.42	NUM
eurjchem-792	232	35	5	5	NUM
eurjchem-792	232	36	4c	4c	NOUN
eurjchem-792	232	37	1.58	1.58	NUM
eurjchem-792	232	38	0.92	0.92	NUM
eurjchem-792	232	39	0.62	0.62	NUM
eurjchem-792	232	40	1.58	1.58	NUM
eurjchem-792	232	41	0.88	0.88	NUM
eurjchem-792	232	42	1.58	1.58	NUM
eurjchem-792	232	43	6	6	NUM
eurjchem-792	232	44	4d	4d	NUM
eurjchem-792	232	45	1.28	1.28	NUM
eurjchem-792	232	46	0.68	0.68	NUM
eurjchem-792	232	47	0.94	0.94	NUM
eurjchem-792	232	48	1.20	1.20	NUM
eurjchem-792	232	49	0.72	0.72	NUM
eurjchem-792	232	50	2.84	2.84	NUM
eurjchem-792	232	51	7	7	NUM
eurjchem-792	232	52	4e	4e	NOUN
eurjchem-792	232	53	2.28	2.28	NUM
eurjchem-792	232	54	1.74	1.74	NUM
eurjchem-792	232	55	1.20	1.20	NUM
eurjchem-792	232	56	1.58	1.58	NUM
eurjchem-792	232	57	0.58	0.58	NUM
eurjchem-792	232	58	4.62	4.62	NUM
eurjchem-792	232	59	8	8	NUM
eurjchem-792	232	60	5a	5a	NUM
eurjchem-792	232	61	0.96	0.96	NUM
eurjchem-792	232	62	0.34	0.34	NUM
eurjchem-792	232	63	0.34	0.34	NUM
eurjchem-792	232	64	0.58	0.58	NUM
eurjchem-792	232	65	0.24	0.24	NUM
eurjchem-792	232	66	0.84	0.84	NUM
eurjchem-792	232	67	9	9	NUM
eurjchem-792	232	68	5b	5b	NUM
eurjchem-792	232	69	1.34	1.34	NUM
eurjchem-792	232	70	0.34	0.34	NUM
eurjchem-792	232	71	0.42	0.42	NUM
eurjchem-792	232	72	0.78	0.78	NUM
eurjchem-792	232	73	0.58	0.58	NUM
eurjchem-792	232	74	0.68	0.68	NUM
eurjchem-792	232	75	10	10	NUM
eurjchem-792	232	76	5c	5c	NUM
eurjchem-792	232	77	0.52	0.52	NUM
eurjchem-792	232	78	0.32	0.32	NUM
eurjchem-792	232	79	0.18	0.18	NUM
eurjchem-792	232	80	0.36	0.36	NUM
eurjchem-792	232	81	0.22	0.22	NUM
eurjchem-792	232	82	0.48	0.48	NUM
eurjchem-792	232	83	11	11	NUM
eurjchem-792	232	84	5d	5d	NUM
eurjchem-792	232	85	0.84	0.84	NUM
eurjchem-792	232	86	0.34	0.34	NUM
eurjchem-792	232	87	0.18	0.18	NUM
eurjchem-792	232	88	0.28	0.28	NUM
eurjchem-792	232	89	0.18	0.18	NUM
eurjchem-792	232	90	0.74	0.74	NUM
eurjchem-792	232	91	12	12	NUM
eurjchem-792	232	92	5e	5e	NOUN
eurjchem-792	232	93	1.28	1.28	NUM
eurjchem-792	232	94	0.64	0.64	NUM
eurjchem-792	232	95	0.62	0.62	NUM
eurjchem-792	232	96	0.58	0.58	NUM
eurjchem-792	232	97	0.72	0.72	NUM
eurjchem-792	232	98	1.18	1.18	NUM
eurjchem-792	232	99	13	13	NUM
eurjchem-792	232	100	levofloxacin	levofloxacin	NOUN
eurjchem-792	232	101	0.78	0.78	NUM
eurjchem-792	232	102	0.19	0.19	NUM
eurjchem-792	232	103	0.19	0.19	NUM
eurjchem-792	232	104	0.19	0.19	NUM
eurjchem-792	232	105	0.19	0.19	NUM
eurjchem-792	232	106	1.56	1.56	NUM
eurjchem-792	232	107	table	table	NOUN
eurjchem-792	232	108	2	2	NUM
eurjchem-792	232	109	.	.	PUNCT
eurjchem-792	232	110	zone	zone	NOUN
eurjchem-792	232	111	of	of	ADP
eurjchem-792	232	112	inhibition	inhibition	NOUN
eurjchem-792	232	113	of	of	ADP
eurjchem-792	232	114	compounds	compound	NOUN
eurjchem-792	232	115	2	2	NUM
eurjchem-792	232	116	,	,	PUNCT
eurjchem-792	232	117	3	3	NUM
eurjchem-792	232	118	,	,	PUNCT
eurjchem-792	232	119	4a‐e	4a‐e	NOUN
eurjchem-792	232	120	and	and	CCONJ
eurjchem-792	232	121	5a‐e	5a‐e	NOUN
eurjchem-792	232	122	in	in	ADP
eurjchem-792	232	123	mm	mm	PROPN
eurjchem-792	232	124	at	at	ADP
eurjchem-792	232	125	100	100	NUM
eurjchem-792	232	126	and	and	CCONJ
eurjchem-792	232	127	150	150	NUM
eurjchem-792	232	128	µg	µg	ADJ
eurjchem-792	232	129	/	/	SYM
eurjchem-792	232	130	ml	ml	NOUN
eurjchem-792	232	131	concentrations	concentration	NOUN
eurjchem-792	232	132	*	*	PUNCT
eurjchem-792	232	133	.	.	PUNCT
eurjchem-792	233	1	sample	sample	VERB
eurjchem-792	233	2	no	no	DET
eurjchem-792	233	3	test	test	NOUN
eurjchem-792	233	4	compounds	compound	VERB
eurjchem-792	233	5	c.	c.	NOUN
eurjchem-792	233	6	albicans	albican	VERB
eurjchem-792	233	7	100	100	NUM
eurjchem-792	233	8	µg	µg	NOUN
eurjchem-792	233	9	/	/	SYM
eurjchem-792	233	10	ml	ml	NOUN
eurjchem-792	233	11	150	150	NUM
eurjchem-792	233	12	µg	µg	NOUN
eurjchem-792	233	13	/	/	SYM
eurjchem-792	233	14	ml	ml	NOUN
eurjchem-792	233	15	1	1	NUM
eurjchem-792	233	16	2	2	NUM
eurjchem-792	233	17	‐	‐	NOUN
eurjchem-792	233	18	6	6	NUM
eurjchem-792	233	19	2	2	NUM
eurjchem-792	233	20	3	3	NUM
eurjchem-792	233	21	‐	‐	NOUN
eurjchem-792	233	22	7	7	NUM
eurjchem-792	233	23	3	3	NUM
eurjchem-792	233	24	4a	4a	NOUN
eurjchem-792	233	25	‐	‐	VERB
eurjchem-792	233	26	4	4	NUM
eurjchem-792	233	27	4	4	NUM
eurjchem-792	233	28	4b	4b	NOUN
eurjchem-792	233	29	‐	‐	VERB
eurjchem-792	233	30	5	5	NUM
eurjchem-792	233	31	5	5	NUM
eurjchem-792	233	32	4c	4c	NOUN
eurjchem-792	233	33	‐	‐	ADV
eurjchem-792	233	34	5	5	NUM
eurjchem-792	233	35	6	6	NUM
eurjchem-792	233	36	4d	4d	NOUN
eurjchem-792	233	37	‐	‐	VERB
eurjchem-792	233	38	7	7	NUM
eurjchem-792	233	39	7	7	NUM
eurjchem-792	233	40	4e	4e	NOUN
eurjchem-792	233	41	‐	‐	VERB
eurjchem-792	233	42	7	7	NUM
eurjchem-792	233	43	8	8	NUM
eurjchem-792	233	44	5a	5a	NUM
eurjchem-792	233	45	‐	‐	VERB
eurjchem-792	233	46	6	6	NUM
eurjchem-792	233	47	9	9	NUM
eurjchem-792	233	48	5b	5b	NOUN
eurjchem-792	233	49	‐	‐	VERB
eurjchem-792	233	50	7	7	NUM
eurjchem-792	233	51	10	10	NUM
eurjchem-792	233	52	5c	5c	NUM
eurjchem-792	233	53	‐	‐	ADV
eurjchem-792	233	54	7	7	NUM
eurjchem-792	233	55	11	11	NUM
eurjchem-792	233	56	5d	5d	NUM
eurjchem-792	233	57	‐	‐	VERB
eurjchem-792	233	58	9	9	NUM
eurjchem-792	233	59	12	12	NUM
eurjchem-792	233	60	5e	5e	NOUN
eurjchem-792	233	61	‐	‐	VERB
eurjchem-792	233	62	9	9	NUM
eurjchem-792	233	63	13	13	NUM
eurjchem-792	233	64	levofloxacin	levofloxacin	NOUN
eurjchem-792	233	65	‐	‐	ADV
eurjchem-792	233	66	4	4	NUM
eurjchem-792	233	67	“	"	PUNCT
eurjchem-792	233	68	‐	‐	PROPN
eurjchem-792	233	69	“	"	PUNCT
eurjchem-792	233	70	=	=	NOUN
eurjchem-792	233	71	not	not	PART
eurjchem-792	233	72	active	active	ADJ
eurjchem-792	233	73	.	.	PUNCT
eurjchem-792	234	1	the	the	DET
eurjchem-792	234	2	potato	potato	NOUN
eurjchem-792	234	3	dextrose	dextrose	NOUN
eurjchem-792	234	4	agar	agar	NOUN
eurjchem-792	234	5	(	(	PUNCT
eurjchem-792	234	6	pda	pda	NOUN
eurjchem-792	234	7	)	)	PUNCT
eurjchem-792	234	8	medium	medium	NOUN
eurjchem-792	234	9	was	be	AUX
eurjchem-792	234	10	suspended	suspend	VERB
eurjchem-792	234	11	in	in	ADP
eurjchem-792	234	12	distilled	distil	VERB
eurjchem-792	234	13	water	water	NOUN
eurjchem-792	234	14	(	(	PUNCT
eurjchem-792	234	15	39	39	NUM
eurjchem-792	234	16	g	g	NOUN
eurjchem-792	234	17	in	in	ADP
eurjchem-792	234	18	1000	1000	NUM
eurjchem-792	234	19	ml	ml	NOUN
eurjchem-792	234	20	)	)	PUNCT
eurjchem-792	234	21	and	and	CCONJ
eurjchem-792	234	22	heated	heat	VERB
eurjchem-792	234	23	to	to	ADP
eurjchem-792	234	24	boiling	boil	VERB
eurjchem-792	234	25	until	until	SCONJ
eurjchem-792	234	26	it	it	PRON
eurjchem-792	234	27	dissolved	dissolve	VERB
eurjchem-792	234	28	completely	completely	ADV
eurjchem-792	234	29	,	,	PUNCT
eurjchem-792	234	30	the	the	DET
eurjchem-792	234	31	medium	medium	ADJ
eurjchem-792	234	32	and	and	CCONJ
eurjchem-792	234	33	petri	petri	ADJ
eurjchem-792	234	34	dishes	dish	NOUN
eurjchem-792	234	35	were	be	AUX
eurjchem-792	234	36	autoclaved	autoclave	VERB
eurjchem-792	234	37	at	at	ADP
eurjchem-792	234	38	pressure	pressure	NOUN
eurjchem-792	234	39	of	of	ADP
eurjchem-792	234	40	15	15	NUM
eurjchem-792	234	41	psi	psi	NOUN
eurjchem-792	234	42	for	for	ADP
eurjchem-792	234	43	20	20	NUM
eurjchem-792	234	44	min	min	NOUN
eurjchem-792	234	45	.	.	NOUN
eurjchem-792	234	46	agar	agar	NOUN
eurjchem-792	234	47	well	well	ADJ
eurjchem-792	234	48	bioassay	bioassay	NOUN
eurjchem-792	234	49	was	be	AUX
eurjchem-792	234	50	employed	employ	VERB
eurjchem-792	234	51	for	for	ADP
eurjchem-792	234	52	antifungal	antifungal	ADJ
eurjchem-792	234	53	activity	activity	NOUN
eurjchem-792	234	54	.	.	PUNCT
eurjchem-792	235	1	the	the	DET
eurjchem-792	235	2	medium	medium	NOUN
eurjchem-792	235	3	was	be	AUX
eurjchem-792	235	4	poured	pour	VERB
eurjchem-792	235	5	into	into	ADP
eurjchem-792	235	6	sterile	sterile	ADJ
eurjchem-792	235	7	petri	petri	ADJ
eurjchem-792	235	8	dishes	dish	NOUN
eurjchem-792	235	9	under	under	ADP
eurjchem-792	235	10	aseptic	aseptic	ADJ
eurjchem-792	235	11	conditions	condition	NOUN
eurjchem-792	235	12	in	in	ADP
eurjchem-792	235	13	a	a	DET
eurjchem-792	235	14	laminar	laminar	ADJ
eurjchem-792	235	15	air	air	NOUN
eurjchem-792	235	16	flow	flow	NOUN
eurjchem-792	235	17	chamber	chamber	NOUN
eurjchem-792	235	18	.	.	PUNCT
eurjchem-792	236	1	when	when	SCONJ
eurjchem-792	236	2	the	the	DET
eurjchem-792	236	3	medium	medium	NOUN
eurjchem-792	236	4	in	in	ADP
eurjchem-792	236	5	the	the	DET
eurjchem-792	236	6	plates	plate	NOUN
eurjchem-792	236	7	solidified	solidify	VERB
eurjchem-792	236	8	,	,	PUNCT
eurjchem-792	236	9	0.5	0.5	NUM
eurjchem-792	236	10	ml	ml	NOUN
eurjchem-792	236	11	of	of	ADP
eurjchem-792	236	12	(	(	PUNCT
eurjchem-792	236	13	week	week	NOUN
eurjchem-792	236	14	old	old	ADJ
eurjchem-792	236	15	)	)	PUNCT
eurjchem-792	236	16	culture	culture	NOUN
eurjchem-792	236	17	of	of	ADP
eurjchem-792	236	18	test	test	NOUN
eurjchem-792	236	19	organism	organism	NOUN
eurjchem-792	236	20	was	be	AUX
eurjchem-792	236	21	inoculated	inoculate	VERB
eurjchem-792	236	22	and	and	CCONJ
eurjchem-792	236	23	uniformly	uniformly	ADV
eurjchem-792	236	24	spread	spread	VERB
eurjchem-792	236	25	over	over	ADP
eurjchem-792	236	26	the	the	DET
eurjchem-792	236	27	agar	agar	NOUN
eurjchem-792	236	28	surface	surface	NOUN
eurjchem-792	236	29	with	with	ADP
eurjchem-792	236	30	a	a	DET
eurjchem-792	236	31	sterile	sterile	ADJ
eurjchem-792	236	32	l‐shaped	l‐shaped	PUNCT
eurjchem-792	236	33	rod	rod	NOUN
eurjchem-792	236	34	.	.	PUNCT
eurjchem-792	237	1	solutions	solution	NOUN
eurjchem-792	237	2	were	be	AUX
eurjchem-792	237	3	prepared	prepare	VERB
eurjchem-792	237	4	by	by	ADP
eurjchem-792	237	5	dissolving	dissolve	VERB
eurjchem-792	237	6	the	the	DET
eurjchem-792	237	7	compound	compound	NOUN
eurjchem-792	237	8	in	in	ADP
eurjchem-792	237	9	dmso	dmso	NOUN
eurjchem-792	237	10	at	at	ADP
eurjchem-792	237	11	different	different	ADJ
eurjchem-792	237	12	concentrations	concentration	NOUN
eurjchem-792	237	13	.	.	PUNCT
eurjchem-792	238	1	after	after	ADP
eurjchem-792	238	2	inoculation	inoculation	NOUN
eurjchem-792	238	3	,	,	PUNCT
eurjchem-792	238	4	wells	well	NOUN
eurjchem-792	238	5	were	be	AUX
eurjchem-792	238	6	scooped	scoop	VERB
eurjchem-792	238	7	out	out	ADP
eurjchem-792	238	8	with	with	ADP
eurjchem-792	238	9	6	6	NUM
eurjchem-792	238	10	mm	mm	NOUN
eurjchem-792	238	11	sterile	sterile	ADJ
eurjchem-792	238	12	cork	cork	NOUN
eurjchem-792	238	13	borer	borer	NOUN
eurjchem-792	238	14	and	and	CCONJ
eurjchem-792	238	15	the	the	DET
eurjchem-792	238	16	lids	lid	NOUN
eurjchem-792	238	17	of	of	ADP
eurjchem-792	238	18	the	the	DET
eurjchem-792	238	19	dishes	dish	NOUN
eurjchem-792	238	20	were	be	AUX
eurjchem-792	238	21	replaced	replace	VERB
eurjchem-792	238	22	.	.	PUNCT
eurjchem-792	239	1	to	to	ADP
eurjchem-792	239	2	each	each	DET
eurjchem-792	239	3	well	well	ADV
eurjchem-792	239	4	different	different	ADJ
eurjchem-792	239	5	concentrations	concentration	NOUN
eurjchem-792	239	6	of	of	ADP
eurjchem-792	239	7	test	test	NOUN
eurjchem-792	239	8	solutions	solution	NOUN
eurjchem-792	239	9	were	be	AUX
eurjchem-792	239	10	added	add	VERB
eurjchem-792	239	11	.	.	PUNCT
eurjchem-792	240	1	controls	control	NOUN
eurjchem-792	240	2	were	be	AUX
eurjchem-792	240	3	maintained	maintain	VERB
eurjchem-792	240	4	.	.	PUNCT
eurjchem-792	241	1	the	the	DET
eurjchem-792	241	2	treated	treat	VERB
eurjchem-792	241	3	and	and	CCONJ
eurjchem-792	241	4	the	the	DET
eurjchem-792	241	5	controls	control	NOUN
eurjchem-792	241	6	were	be	AUX
eurjchem-792	241	7	kept	keep	VERB
eurjchem-792	241	8	at	at	ADP
eurjchem-792	241	9	27	27	NUM
eurjchem-792	241	10	°	°	NOUN
eurjchem-792	241	11	c	c	NOUN
eurjchem-792	241	12	for	for	SCONJ
eurjchem-792	241	13	48	48	NUM
eurjchem-792	241	14	h.	h.	NOUN
eurjchem-792	241	15	inhibition	inhibition	NOUN
eurjchem-792	241	16	zones	zone	NOUN
eurjchem-792	241	17	were	be	AUX
eurjchem-792	241	18	measured	measure	VERB
eurjchem-792	241	19	,	,	PUNCT
eurjchem-792	241	20	the	the	DET
eurjchem-792	241	21	diameter	diameter	NOUN
eurjchem-792	241	22	calculated	calculate	VERB
eurjchem-792	241	23	in	in	ADP
eurjchem-792	241	24	millimetre	millimetre	PROPN
eurjchem-792	241	25	.	.	PUNCT
eurjchem-792	242	1	some	some	PRON
eurjchem-792	242	2	of	of	ADP
eurjchem-792	242	3	newly	newly	ADV
eurjchem-792	242	4	synthesized	synthesize	VERB
eurjchem-792	242	5	compounds	compound	NOUN
eurjchem-792	242	6	shown	show	VERB
eurjchem-792	242	7	excellent	excellent	ADJ
eurjchem-792	242	8	to	to	ADP
eurjchem-792	242	9	good	good	ADJ
eurjchem-792	242	10	activity	activity	NOUN
eurjchem-792	242	11	against	against	ADP
eurjchem-792	242	12	candida	candida	NOUN
eurjchem-792	242	13	albicans	albican	NOUN
eurjchem-792	242	14	(	(	PUNCT
eurjchem-792	242	15	mtcc	mtcc	NOUN
eurjchem-792	242	16	227	227	NUM
eurjchem-792	242	17	)	)	PUNCT
eurjchem-792	242	18	only	only	ADV
eurjchem-792	242	19	at	at	ADP
eurjchem-792	242	20	150	150	NUM
eurjchem-792	242	21	μg	μg	NOUN
eurjchem-792	242	22	concentrations	concentration	NOUN
eurjchem-792	242	23	and	and	CCONJ
eurjchem-792	242	24	inactive	inactive	ADJ
eurjchem-792	242	25	against	against	ADP
eurjchem-792	242	26	100	100	NUM
eurjchem-792	242	27	µg	µg	NOUN
eurjchem-792	242	28	concentration	concentration	NOUN
eurjchem-792	242	29	,	,	PUNCT
eurjchem-792	242	30	these	these	DET
eurjchem-792	242	31	compounds	compound	NOUN
eurjchem-792	242	32	did	do	AUX
eurjchem-792	242	33	n’t	not	PART
eurjchem-792	242	34	shown	show	VERB
eurjchem-792	242	35	any	any	DET
eurjchem-792	242	36	appreciable	appreciable	ADJ
eurjchem-792	242	37	activity	activity	NOUN
eurjchem-792	242	38	against	against	ADP
eurjchem-792	242	39	other	other	ADJ
eurjchem-792	242	40	fungal	fungal	ADJ
eurjchem-792	242	41	strains	strain	NOUN
eurjchem-792	242	42	.	.	PUNCT
eurjchem-792	243	1	the	the	DET
eurjchem-792	243	2	results	result	NOUN
eurjchem-792	243	3	of	of	ADP
eurjchem-792	243	4	the	the	DET
eurjchem-792	243	5	activity	activity	NOUN
eurjchem-792	243	6	against	against	ADP
eurjchem-792	243	7	candida	candida	NOUN
eurjchem-792	243	8	albicans	albican	NOUN
eurjchem-792	243	9	are	be	AUX
eurjchem-792	243	10	tabulated	tabulate	VERB
eurjchem-792	243	11	in	in	ADP
eurjchem-792	243	12	table	table	NOUN
eurjchem-792	243	13	2	2	NUM
eurjchem-792	243	14	.	.	NOUN
eurjchem-792	243	15	3	3	NUM
eurjchem-792	243	16	.	.	NOUN
eurjchem-792	243	17	results	result	NOUN
eurjchem-792	243	18	and	and	CCONJ
eurjchem-792	243	19	discussion	discussion	VERB
eurjchem-792	243	20	the	the	DET
eurjchem-792	243	21	synthetic	synthetic	ADJ
eurjchem-792	243	22	strategies	strategy	NOUN
eurjchem-792	243	23	adopted	adopt	VERB
eurjchem-792	243	24	to	to	PART
eurjchem-792	243	25	obtain	obtain	VERB
eurjchem-792	243	26	the	the	DET
eurjchem-792	243	27	target	target	NOUN
eurjchem-792	243	28	compounds	compound	NOUN
eurjchem-792	243	29	are	be	AUX
eurjchem-792	243	30	depicted	depict	VERB
eurjchem-792	243	31	in	in	ADP
eurjchem-792	243	32	schemes	scheme	NOUN
eurjchem-792	243	33	1	1	NUM
eurjchem-792	243	34	,	,	PUNCT
eurjchem-792	243	35	2	2	NUM
eurjchem-792	243	36	and	and	CCONJ
eurjchem-792	243	37	3	3	NUM
eurjchem-792	243	38	.	.	PUNCT
eurjchem-792	244	1	initially	initially	ADV
eurjchem-792	244	2	(	(	PUNCT
eurjchem-792	244	3	3s)‐	3s)‐	PROPN
eurjchem-792	244	4	9,10‐difluoro‐3‐methyl‐7‐oxo‐3,7‐dihydro‐2h‐[1,4]oxazino[2,3	9,10‐difluoro‐3‐methyl‐7‐oxo‐3,7‐dihydro‐2h‐[1,4]oxazino[2,3	NUM
eurjchem-792	244	5	,	,	PUNCT
eurjchem-792	244	6	4‐ij]quinoline‐6‐carboxylic	4‐ij]quinoline‐6‐carboxylic	ADV
eurjchem-792	244	7	acid	acid	ADJ
eurjchem-792	244	8	,	,	PUNCT
eurjchem-792	244	9	1	1	NUM
eurjchem-792	244	10	,	,	PUNCT
eurjchem-792	244	11	on	on	ADP
eurjchem-792	244	12	reaction	reaction	NOUN
eurjchem-792	244	13	with	with	ADP
eurjchem-792	244	14	piperizine	piperizine	NOUN
eurjchem-792	244	15	in	in	ADP
eurjchem-792	244	16	presence	presence	NOUN
eurjchem-792	244	17	of	of	ADP
eurjchem-792	244	18	triethylamine	triethylamine	NOUN
eurjchem-792	244	19	in	in	ADP
eurjchem-792	244	20	acetonitrile	acetonitrile	NOUN
eurjchem-792	244	21	under	under	ADP
eurjchem-792	244	22	reflux	reflux	NOUN
eurjchem-792	244	23	given	give	VERB
eurjchem-792	244	24	the	the	PRON
eurjchem-792	244	25	previously	previously	ADV
eurjchem-792	244	26	reported	report	VERB
eurjchem-792	244	27	[	[	X
eurjchem-792	244	28	21	21	NUM
eurjchem-792	244	29	]	]	X
eurjchem-792	244	30	(	(	PUNCT
eurjchem-792	244	31	s)‐9‐fluoro‐3,7‐dihydro‐3‐	s)‐9‐fluoro‐3,7‐dihydro‐3‐	ADJ
eurjchem-792	244	32	methyl‐7‐oxo‐10‐(piperazin‐1‐yl)‐2h‐[1,4]oxazino[2,3,4‐	methyl‐7‐oxo‐10‐(piperazin‐1‐yl)‐2h‐[1,4]oxazino[2,3,4‐	NOUN
eurjchem-792	244	33	ij	ij	NOUN
eurjchem-792	244	34	]	]	X
eurjchem-792	244	35	quinoline‐6‐carboxylic	quinoline‐6‐carboxylic	ADJ
eurjchem-792	244	36	acid	acid	NOUN
eurjchem-792	244	37	2	2	NUM
eurjchem-792	244	38	on	on	ADP
eurjchem-792	244	39	treatment	treatment	NOUN
eurjchem-792	244	40	with	with	ADP
eurjchem-792	244	41	epichlro‐	epichlro‐	NOUN
eurjchem-792	244	42	hydrine	hydrine	NOUN
eurjchem-792	244	43	in	in	ADP
eurjchem-792	244	44	presence	presence	NOUN
eurjchem-792	244	45	of	of	ADP
eurjchem-792	244	46	naoh	naoh	NOUN
eurjchem-792	244	47	in	in	ADP
eurjchem-792	244	48	acetone	acetone	NOUN
eurjchem-792	244	49	at	at	ADP
eurjchem-792	244	50	40‐45	40‐45	NUM
eurjchem-792	244	51	°	°	PROPN
eurjchem-792	244	52	c	c	PROPN
eurjchem-792	244	53	gave	give	VERB
eurjchem-792	244	54	the	the	DET
eurjchem-792	244	55	corresponding	correspond	VERB
eurjchem-792	244	56	9‐fluoro‐3,7‐dihydro‐3‐methyl‐10‐(4‐((oxiran‐	9‐fluoro‐3,7‐dihydro‐3‐methyl‐10‐(4‐((oxiran‐	NOUN
eurjchem-792	244	57	2‐yl)methyl)piperazin‐1‐yl)‐7‐oxo‐2h‐[1,4]oxazino[2,3,4‐ij	2‐yl)methyl)piperazin‐1‐yl)‐7‐oxo‐2h‐[1,4]oxazino[2,3,4‐ij	PRON
eurjchem-792	244	58	]	]	X
eurjchem-792	244	59	quinoline‐6‐carboxylic	quinoline‐6‐carboxylic	PROPN
eurjchem-792	244	60	acid	acid	NOUN
eurjchem-792	244	61	,	,	PUNCT
eurjchem-792	244	62	3	3	NUM
eurjchem-792	244	63	,	,	PUNCT
eurjchem-792	244	64	as	as	SCONJ
eurjchem-792	244	65	shown	show	VERB
eurjchem-792	244	66	in	in	ADP
eurjchem-792	244	67	scheme	scheme	NOUN
eurjchem-792	244	68	1	1	NUM
eurjchem-792	244	69	.	.	PUNCT
eurjchem-792	245	1	the	the	DET
eurjchem-792	245	2	structure	structure	NOUN
eurjchem-792	245	3	of	of	ADP
eurjchem-792	245	4	compound	compound	NOUN
eurjchem-792	245	5	3	3	NUM
eurjchem-792	245	6	was	be	AUX
eurjchem-792	245	7	determined	determine	VERB
eurjchem-792	245	8	on	on	ADP
eurjchem-792	245	9	the	the	DET
eurjchem-792	245	10	basis	basis	NOUN
eurjchem-792	245	11	of	of	ADP
eurjchem-792	245	12	its	its	PRON
eurjchem-792	245	13	spectral	spectral	ADJ
eurjchem-792	245	14	data	datum	NOUN
eurjchem-792	245	15	.	.	PUNCT
eurjchem-792	246	1	the	the	DET
eurjchem-792	246	2	ir	ir	PROPN
eurjchem-792	246	3	(	(	PUNCT
eurjchem-792	246	4	kbr	kbr	PROPN
eurjchem-792	246	5	)	)	PUNCT
eurjchem-792	246	6	spectrum	spectrum	NOUN
eurjchem-792	246	7	of	of	ADP
eurjchem-792	246	8	compound	compound	NOUN
eurjchem-792	246	9	3	3	NUM
eurjchem-792	246	10	has	have	AUX
eurjchem-792	246	11	shown	show	VERB
eurjchem-792	246	12	absorptions	absorption	NOUN
eurjchem-792	246	13	at	at	ADP
eurjchem-792	246	14	1708	1708	NUM
eurjchem-792	246	15	and	and	CCONJ
eurjchem-792	246	16	1624	1624	NUM
eurjchem-792	246	17	cm‐1	cm‐1	NOUN
eurjchem-792	246	18	assignable	assignable	ADJ
eurjchem-792	246	19	to	to	ADP
eurjchem-792	246	20	two	two	NUM
eurjchem-792	246	21	carbonyl	carbonyl	NOUN
eurjchem-792	246	22	groups	group	NOUN
eurjchem-792	246	23	as	as	ADP
eurjchem-792	246	24	diagnostic	diagnostic	ADJ
eurjchem-792	246	25	absorptions	absorption	NOUN
eurjchem-792	246	26	.	.	PUNCT
eurjchem-792	247	1	typical	typical	ADJ
eurjchem-792	247	2	aliphatic	aliphatic	ADJ
eurjchem-792	247	3	shift	shift	NOUN
eurjchem-792	247	4	alignment	alignment	NOUN
eurjchem-792	247	5	in	in	ADP
eurjchem-792	247	6	1h	1h	NUM
eurjchem-792	247	7	nmr	nmr	NOUN
eurjchem-792	247	8	spectrum	spectrum	NOUN
eurjchem-792	247	9	at	at	ADP
eurjchem-792	247	10	1.42‐1.44	1.42‐1.44	NUM
eurjchem-792	247	11	ppm	ppm	ADJ
eurjchem-792	247	12	,	,	PUNCT
eurjchem-792	247	13	3	3	NUM
eurjchem-792	247	14	protons	proton	NOUN
eurjchem-792	247	15	as	as	ADP
eurjchem-792	247	16	doublet	doublet	PROPN
eurjchem-792	247	17	has	have	AUX
eurjchem-792	247	18	shown	show	VERB
eurjchem-792	247	19	the	the	DET
eurjchem-792	247	20	methyl	methyl	NOUN
eurjchem-792	247	21	protons	proton	NOUN
eurjchem-792	247	22	adjacent	adjacent	ADJ
eurjchem-792	247	23	to	to	ADP
eurjchem-792	247	24	asymmetric	asymmetric	ADJ
eurjchem-792	247	25	carbon	carbon	NOUN
eurjchem-792	247	26	of	of	ADP
eurjchem-792	247	27	oxazine	oxazine	NOUN
eurjchem-792	247	28	ring	ring	NOUN
eurjchem-792	247	29	.	.	PUNCT
eurjchem-792	248	1	chemical	chemical	ADJ
eurjchem-792	248	2	shifts	shift	NOUN
eurjchem-792	248	3	at	at	ADP
eurjchem-792	248	4	3.51‐3.53	3.51‐3.53	PROPN
eurjchem-792	248	5	ppm	ppm	NOUN
eurjchem-792	248	6	(	(	PUNCT
eurjchem-792	248	7	d	d	NOUN
eurjchem-792	248	8	,	,	PUNCT
eurjchem-792	248	9	2h	2h	NUM
eurjchem-792	248	10	)	)	PUNCT
eurjchem-792	248	11	,	,	PUNCT
eurjchem-792	248	12	4.33‐4.38	4.33‐4.38	X
eurjchem-792	248	13	ppm	ppm	NOUN
eurjchem-792	248	14	(	(	PUNCT
eurjchem-792	248	15	m	m	PROPN
eurjchem-792	248	16	,	,	PUNCT
eurjchem-792	248	17	1h	1h	NUM
eurjchem-792	248	18	)	)	PUNCT
eurjchem-792	248	19	confirms	confirm	VERB
eurjchem-792	248	20	the	the	DET
eurjchem-792	248	21	epoxide	epoxide	NOUN
eurjchem-792	248	22	ring	ring	NOUN
eurjchem-792	248	23	protons	proton	NOUN
eurjchem-792	248	24	.	.	PUNCT
eurjchem-792	249	1	however	however	ADV
eurjchem-792	249	2	,	,	PUNCT
eurjchem-792	249	3	the	the	DET
eurjchem-792	249	4	chemical	chemical	NOUN
eurjchem-792	249	5	shift	shift	NOUN
eurjchem-792	249	6	at	at	ADP
eurjchem-792	249	7	7.52‐7.56	7.52‐7.56	NUM
eurjchem-792	249	8	(	(	PUNCT
eurjchem-792	249	9	d	d	PROPN
eurjchem-792	249	10	,	,	PUNCT
eurjchem-792	249	11	1h	1h	NUM
eurjchem-792	249	12	)	)	PUNCT
eurjchem-792	249	13	with	with	ADP
eurjchem-792	249	14	coupling	couple	VERB
eurjchem-792	249	15	constant	constant	ADJ
eurjchem-792	249	16	12.0	12.0	NUM
eurjchem-792	249	17	hz	hz	VERB
eurjchem-792	249	18	indicated	indicate	VERB
eurjchem-792	249	19	proton	proton	NOUN
eurjchem-792	249	20	coupled	couple	VERB
eurjchem-792	249	21	with	with	ADP
eurjchem-792	249	22	adjacent	adjacent	ADJ
eurjchem-792	249	23	fluorine	fluorine	NOUN
eurjchem-792	249	24	atom	atom	NOUN
eurjchem-792	249	25	and	and	CCONJ
eurjchem-792	249	26	broad	broad	ADJ
eurjchem-792	249	27	singlet	singlet	NOUN
eurjchem-792	249	28	at	at	ADP
eurjchem-792	249	29	15.17	15.17	NUM
eurjchem-792	249	30	ppm	ppm	NOUN
eurjchem-792	249	31	exchangeable	exchangeable	ADJ
eurjchem-792	249	32	with	with	ADP
eurjchem-792	249	33	d2o	d2o	PROPN
eurjchem-792	249	34	confirmed	confirm	VERB
eurjchem-792	249	35	the	the	DET
eurjchem-792	249	36	presence	presence	NOUN
eurjchem-792	249	37	of	of	ADP
eurjchem-792	249	38	carboxylic	carboxylic	ADJ
eurjchem-792	249	39	acid	acid	NOUN
eurjchem-792	249	40	.	.	PUNCT
eurjchem-792	250	1	in	in	ADP
eurjchem-792	250	2	13c	13c	NUM
eurjchem-792	250	3	nmr	nmr	NOUN
eurjchem-792	250	4	chemical	chemical	NOUN
eurjchem-792	250	5	shift	shift	NOUN
eurjchem-792	250	6	at	at	ADP
eurjchem-792	250	7	18.34	18.34	NUM
eurjchem-792	250	8	ppm	ppm	NOUN
eurjchem-792	250	9	indicated	indicate	VERB
eurjchem-792	250	10	the	the	DET
eurjchem-792	250	11	methyl	methyl	NOUN
eurjchem-792	250	12	group	group	NOUN
eurjchem-792	250	13	and	and	CCONJ
eurjchem-792	250	14	signal	signal	VERB
eurjchem-792	250	15	at	at	ADP
eurjchem-792	250	16	146.51	146.51	NUM
eurjchem-792	250	17	ppm	ppm	NOUN
eurjchem-792	250	18	shown	show	VERB
eurjchem-792	250	19	the	the	DET
eurjchem-792	250	20	carbon	carbon	NOUN
eurjchem-792	250	21	attached	attach	VERB
eurjchem-792	250	22	to	to	ADP
eurjchem-792	250	23	fluorine	fluorine	NOUN
eurjchem-792	250	24	.	.	PUNCT
eurjchem-792	251	1	enone	enone	NOUN
eurjchem-792	251	2	carbon	carbon	NOUN
eurjchem-792	251	3	resonated	resonate	VERB
eurjchem-792	251	4	downfield	downfield	VERB
eurjchem-792	251	5	than	than	ADP
eurjchem-792	251	6	all	all	DET
eurjchem-792	251	7	other	other	ADJ
eurjchem-792	251	8	carbons	carbon	NOUN
eurjchem-792	251	9	at	at	ADP
eurjchem-792	251	10	176.77	176.77	NUM
eurjchem-792	251	11	ppm	ppm	NOUN
eurjchem-792	251	12	,	,	PUNCT
eurjchem-792	251	13	where	where	SCONJ
eurjchem-792	251	14	as	as	ADP
eurjchem-792	251	15	carboxylic	carboxylic	ADJ
eurjchem-792	251	16	acid	acid	NOUN
eurjchem-792	251	17	carbon	carbon	NOUN
eurjchem-792	251	18	resonated	resonate	VERB
eurjchem-792	251	19	at	at	ADP
eurjchem-792	251	20	166.45	166.45	NUM
eurjchem-792	251	21	ppm	ppm	NOUN
eurjchem-792	251	22	.	.	PUNCT
eurjchem-792	252	1	molecular	molecular	ADJ
eurjchem-792	252	2	mass	mass	NOUN
eurjchem-792	252	3	of	of	ADP
eurjchem-792	252	4	compound	compound	NOUN
eurjchem-792	252	5	3	3	NUM
eurjchem-792	252	6	has	have	VERB
eurjchem-792	252	7	m	m	PROPN
eurjchem-792	252	8	/	/	SYM
eurjchem-792	252	9	z	z	PROPN
eurjchem-792	252	10	404.02	404.02	NUM
eurjchem-792	252	11	(	(	PUNCT
eurjchem-792	252	12	m	m	NOUN
eurjchem-792	252	13	+	+	ADJ
eurjchem-792	252	14	)	)	PUNCT
eurjchem-792	252	15	indicates	indicate	VERB
eurjchem-792	252	16	the	the	DET
eurjchem-792	252	17	molecular	molecular	ADJ
eurjchem-792	252	18	weight	weight	NOUN
eurjchem-792	252	19	m	m	PROPN
eurjchem-792	252	20	/	/	SYM
eurjchem-792	252	21	z	z	PROPN
eurjchem-792	252	22	403.4	403.4	NUM
eurjchem-792	252	23	.	.	PUNCT
eurjchem-792	253	1	the	the	DET
eurjchem-792	253	2	results	result	NOUN
eurjchem-792	253	3	of	of	ADP
eurjchem-792	253	4	elemental	elemental	ADJ
eurjchem-792	253	5	analysis	analysis	NOUN
eurjchem-792	253	6	for	for	ADP
eurjchem-792	253	7	c	c	NOUN
eurjchem-792	253	8	,	,	PUNCT
eurjchem-792	253	9	h	h	NOUN
eurjchem-792	253	10	and	and	CCONJ
eurjchem-792	253	11	n	n	PROPN
eurjchem-792	253	12	were	be	AUX
eurjchem-792	253	13	within	within	ADP
eurjchem-792	253	14	±	±	NUM
eurjchem-792	253	15	0.4	0.4	NUM
eurjchem-792	253	16	%	%	NOUN
eurjchem-792	253	17	of	of	ADP
eurjchem-792	253	18	the	the	DET
eurjchem-792	253	19	theoretical	theoretical	ADJ
eurjchem-792	253	20	values	value	NOUN
eurjchem-792	253	21	.	.	PUNCT
eurjchem-792	254	1	the	the	DET
eurjchem-792	254	2	specific	specific	ADJ
eurjchem-792	254	3	optical	optical	ADJ
eurjchem-792	254	4	rotation	rotation	NOUN
eurjchem-792	254	5	‐73.06	‐73.06	CCONJ
eurjchem-792	254	6	shown	show	VERB
eurjchem-792	254	7	that	that	SCONJ
eurjchem-792	254	8	the	the	DET
eurjchem-792	254	9	compound	compound	NOUN
eurjchem-792	254	10	3	3	NUM
eurjchem-792	254	11	is	be	AUX
eurjchem-792	254	12	chiral	chiral	ADJ
eurjchem-792	254	13	.	.	PUNCT
eurjchem-792	255	1	further	far	ADV
eurjchem-792	255	2	,	,	PUNCT
eurjchem-792	255	3	the	the	DET
eurjchem-792	255	4	nucleophilic	nucleophilic	ADJ
eurjchem-792	255	5	opening	opening	NOUN
eurjchem-792	255	6	of	of	ADP
eurjchem-792	255	7	epoxide	epoxide	NOUN
eurjchem-792	255	8	,	,	PUNCT
eurjchem-792	255	9	3	3	NUM
eurjchem-792	255	10	,	,	PUNCT
eurjchem-792	255	11	was	be	AUX
eurjchem-792	255	12	carried	carry	VERB
eurjchem-792	255	13	out	out	ADP
eurjchem-792	255	14	with	with	ADP
eurjchem-792	255	15	substituted	substitute	VERB
eurjchem-792	255	16	2‐mercaptobenzimidazole	2‐mercaptobenzimidazole	NOUN
eurjchem-792	255	17	in	in	ADP
eurjchem-792	255	18	alcoholic	alcoholic	ADJ
eurjchem-792	255	19	naoh	naoh	NOUN
eurjchem-792	255	20	solution	solution	NOUN
eurjchem-792	255	21	at	at	ADP
eurjchem-792	255	22	room	room	NOUN
eurjchem-792	255	23	temperature	temperature	NOUN
eurjchem-792	255	24	for	for	ADP
eurjchem-792	255	25	6	6	NUM
eurjchem-792	255	26	h	h	NOUN
eurjchem-792	255	27	,	,	PUNCT
eurjchem-792	255	28	leads	lead	VERB
eurjchem-792	255	29	to	to	ADP
eurjchem-792	255	30	formation	formation	NOUN
eurjchem-792	255	31	of	of	ADP
eurjchem-792	255	32	7‐(4‐(3‐(1h‐benzo[d]imidazol‐2‐ylthio)‐2‐hydroxypropyl	7‐(4‐(3‐(1h‐benzo[d]imidazol‐2‐ylthio)‐2‐hydroxypropyl	NUM
eurjchem-792	255	33	)	)	PUNCT
eurjchem-792	256	1	piperazin‐1‐yl)‐1‐cyclopropyl‐6‐fluoro‐4‐oxo‐1,4‐dihydro	piperazin‐1‐yl)‐1‐cyclopropyl‐6‐fluoro‐4‐oxo‐1,4‐dihydro	PROPN
eurjchem-792	256	2	quinoline‐3‐carboxylic	quinoline‐3‐carboxylic	PROPN
eurjchem-792	256	3	acid	acid	NOUN
eurjchem-792	256	4	,	,	PUNCT
eurjchem-792	256	5	4a‐e	4a‐e	NOUN
eurjchem-792	256	6	,	,	PUNCT
eurjchem-792	256	7	depicted	depict	VERB
eurjchem-792	256	8	in	in	ADP
eurjchem-792	256	9	scheme	scheme	NOUN
eurjchem-792	256	10	2	2	NUM
eurjchem-792	256	11	.	.	PUNCT
eurjchem-792	257	1	the	the	DET
eurjchem-792	257	2	synthesis	synthesis	NOUN
eurjchem-792	257	3	of	of	ADP
eurjchem-792	257	4	compounds	compound	NOUN
eurjchem-792	257	5	4a‐e	4a‐e	PROPN
eurjchem-792	257	6	was	be	AUX
eurjchem-792	257	7	confirmed	confirm	VERB
eurjchem-792	257	8	by	by	ADP
eurjchem-792	257	9	ir	ir	PROPN
eurjchem-792	257	10	,	,	PUNCT
eurjchem-792	257	11	1h	1h	NUM
eurjchem-792	257	12	nmr	nmr	NOUN
eurjchem-792	257	13	,	,	PUNCT
eurjchem-792	257	14	13c	13c	NOUN
eurjchem-792	257	15	nmr	nmr	NOUN
eurjchem-792	257	16	,	,	PUNCT
eurjchem-792	257	17	mass	mass	NOUN
eurjchem-792	257	18	spectrum	spectrum	NOUN
eurjchem-792	257	19	and	and	CCONJ
eurjchem-792	257	20	elemental	elemental	ADJ
eurjchem-792	257	21	analysis	analysis	NOUN
eurjchem-792	257	22	.	.	PUNCT
eurjchem-792	258	1	the	the	DET
eurjchem-792	258	2	compound	compound	PROPN
eurjchem-792	258	3	4a	4a	PROPN
eurjchem-792	258	4	ir	ir	PROPN
eurjchem-792	258	5	(	(	PUNCT
eurjchem-792	258	6	kbr	kbr	PROPN
eurjchem-792	258	7	)	)	PUNCT
eurjchem-792	258	8	spectrum	spectrum	NOUN
eurjchem-792	258	9	shown	show	VERB
eurjchem-792	258	10	absorption	absorption	NOUN
eurjchem-792	258	11	at	at	ADP
eurjchem-792	258	12	3401	3401	NUM
eurjchem-792	258	13	cm‐	cm‐	NOUN
eurjchem-792	258	14	1	1	NUM
eurjchem-792	258	15	is	be	AUX
eurjchem-792	258	16	indicated	indicate	VERB
eurjchem-792	258	17	the	the	DET
eurjchem-792	258	18	presence	presence	NOUN
eurjchem-792	258	19	of	of	ADP
eurjchem-792	258	20	oh	oh	INTJ
eurjchem-792	258	21	group	group	NOUN
eurjchem-792	258	22	and	and	CCONJ
eurjchem-792	258	23	absorption	absorption	NOUN
eurjchem-792	258	24	at	at	ADP
eurjchem-792	258	25	1721	1721	NUM
eurjchem-792	258	26	and	and	CCONJ
eurjchem-792	258	27	1619	1619	NUM
eurjchem-792	258	28	cm‐1	cm‐1	NOUN
eurjchem-792	258	29	shown	show	VERB
eurjchem-792	258	30	the	the	DET
eurjchem-792	258	31	presence	presence	NOUN
eurjchem-792	258	32	of	of	ADP
eurjchem-792	258	33	both	both	DET
eurjchem-792	258	34	carbonyl	carbonyl	NOUN
eurjchem-792	258	35	groups	group	NOUN
eurjchem-792	258	36	.	.	PUNCT
eurjchem-792	259	1	chemical	chemical	ADJ
eurjchem-792	259	2	shift	shift	NOUN
eurjchem-792	259	3	in	in	ADP
eurjchem-792	259	4	1h	1h	NUM
eurjchem-792	259	5	nmr	nmr	NOUN
eurjchem-792	259	6	spectrum	spectrum	NOUN
eurjchem-792	259	7	at	at	ADP
eurjchem-792	259	8	1.39‐1.41	1.39‐1.41	NUM
eurjchem-792	259	9	ppm	ppm	NOUN
eurjchem-792	259	10	,	,	PUNCT
eurjchem-792	259	11	3	3	NUM
eurjchem-792	259	12	protons	proton	NOUN
eurjchem-792	259	13	as	as	ADV
eurjchem-792	259	14	doublet	doublet	ADJ
eurjchem-792	259	15	with	with	ADP
eurjchem-792	259	16	coupling	couple	VERB
eurjchem-792	259	17	constant	constant	ADJ
eurjchem-792	259	18	6.0	6.0	NUM
eurjchem-792	259	19	hz	hz	VERB
eurjchem-792	259	20	shown	show	VERB
eurjchem-792	259	21	the	the	DET
eurjchem-792	259	22	presence	presence	NOUN
eurjchem-792	259	23	of	of	ADP
eurjchem-792	259	24	methyl	methyl	NOUN
eurjchem-792	259	25	group	group	NOUN
eurjchem-792	259	26	of	of	ADP
eurjchem-792	259	27	oxazine	oxazine	NOUN
eurjchem-792	259	28	ring	ring	NOUN
eurjchem-792	259	29	.	.	PUNCT
eurjchem-792	260	1	proton	proton	NOUN
eurjchem-792	260	2	shifts	shift	NOUN
eurjchem-792	260	3	at	at	ADP
eurjchem-792	260	4	4.96	4.96	NUM
eurjchem-792	260	5	and	and	CCONJ
eurjchem-792	260	6	5.36	5.36	NUM
eurjchem-792	260	7	ppm	ppm	NOUN
eurjchem-792	260	8	as	as	ADP
eurjchem-792	260	9	broad	broad	ADJ
eurjchem-792	260	10	singlet	singlet	NOUN
eurjchem-792	260	11	and	and	CCONJ
eurjchem-792	260	12	exchangeable	exchangeable	ADJ
eurjchem-792	260	13	with	with	ADP
eurjchem-792	260	14	d2o	d2o	PROPN
eurjchem-792	260	15	proved	prove	VERB
eurjchem-792	260	16	that	that	SCONJ
eurjchem-792	260	17	the	the	DET
eurjchem-792	260	18	presence	presence	NOUN
eurjchem-792	260	19	of	of	ADP
eurjchem-792	260	20	oh	oh	INTJ
eurjchem-792	260	21	and	and	CCONJ
eurjchem-792	260	22	nh	nh	PROPN
eurjchem-792	260	23	groups	group	NOUN
eurjchem-792	260	24	,	,	PUNCT
eurjchem-792	260	25	further	further	ADJ
eurjchem-792	260	26	chemical	chemical	ADJ
eurjchem-792	260	27	shifts	shift	NOUN
eurjchem-792	260	28	between	between	ADP
eurjchem-792	260	29	7.00	7.00	NUM
eurjchem-792	260	30	to	to	ADP
eurjchem-792	260	31	7.50	7.50	NUM
eurjchem-792	260	32	ppm	ppm	NOUN
eurjchem-792	260	33	in	in	ADP
eurjchem-792	260	34	aromatic	aromatic	ADJ
eurjchem-792	260	35	region	region	NOUN
eurjchem-792	260	36	indicated	indicate	VERB
eurjchem-792	260	37	the	the	DET
eurjchem-792	260	38	presence	presence	NOUN
eurjchem-792	260	39	of	of	ADP
eurjchem-792	260	40	benzimidazolyl	benzimidazolyl	ADJ
eurjchem-792	260	41	moity	moity	NOUN
eurjchem-792	260	42	.	.	PUNCT
eurjchem-792	261	1	in	in	ADP
eurjchem-792	261	2	13c	13c	NUM
eurjchem-792	261	3	nmr	nmr	NOUN
eurjchem-792	261	4	chemical	chemical	NOUN
eurjchem-792	261	5	shift	shift	NOUN
eurjchem-792	261	6	at	at	ADP
eurjchem-792	261	7	18.34	18.34	NUM
eurjchem-792	261	8	ppm	ppm	NOUN
eurjchem-792	261	9	indicated	indicate	VERB
eurjchem-792	261	10	the	the	DET
eurjchem-792	261	11	chiral	chiral	ADJ
eurjchem-792	261	12	ch3	ch3	PROPN
eurjchem-792	261	13	group	group	PROPN
eurjchem-792	261	14	and	and	CCONJ
eurjchem-792	261	15	chemical	chemical	NOUN
eurjchem-792	261	16	shift	shift	NOUN
eurjchem-792	261	17	at	at	ADP
eurjchem-792	261	18	47.24	47.24	NUM
eurjchem-792	261	19	ppm	ppm	NOUN
eurjchem-792	261	20	indicated	indicate	VERB
eurjchem-792	261	21	the	the	DET
eurjchem-792	261	22	methylene	methylene	NOUN
eurjchem-792	261	23	carbon	carbon	NOUN
eurjchem-792	261	24	attached	attach	VERB
eurjchem-792	261	25	to	to	ADP
eurjchem-792	261	26	benzimidazolyl	benzimidazolyl	PROPN
eurjchem-792	261	27	thiol	thiol	PROPN
eurjchem-792	261	28	moiety	moiety	NOUN
eurjchem-792	261	29	.	.	PUNCT
eurjchem-792	262	1	334	334	NUM
eurjchem-792	262	2	guruswamy	guruswamy	NOUN
eurjchem-792	262	3	et	et	PROPN
eurjchem-792	262	4	al	al	PROPN
eurjchem-792	262	5	.	.	PUNCT
eurjchem-792	262	6	/	/	SYM
eurjchem-792	262	7	european	european	PROPN
eurjchem-792	262	8	journal	journal	PROPN
eurjchem-792	262	9	of	of	ADP
eurjchem-792	262	10	chemistry	chemistry	NOUN
eurjchem-792	262	11	4	4	NUM
eurjchem-792	262	12	(	(	PUNCT
eurjchem-792	262	13	4	4	NUM
eurjchem-792	262	14	)	)	PUNCT
eurjchem-792	262	15	(	(	PUNCT
eurjchem-792	262	16	2013	2013	NUM
eurjchem-792	262	17	)	)	PUNCT
eurjchem-792	262	18	329‐335	329‐335	PROPN
eurjchem-792	262	19	table	table	NOUN
eurjchem-792	262	20	3	3	NUM
eurjchem-792	262	21	.	.	X
eurjchem-792	262	22	synthesis	synthesis	NOUN
eurjchem-792	262	23	of	of	ADP
eurjchem-792	262	24	various	various	ADJ
eurjchem-792	262	25	substituted	substitute	VERB
eurjchem-792	262	26	mercaptobenzimdazole	mercaptobenzimdazole	NOUN
eurjchem-792	262	27	sulfides	sulfide	VERB
eurjchem-792	262	28	4a‐e	4a‐e	NOUN
eurjchem-792	262	29	.	.	PUNCT
eurjchem-792	263	1	n	n	PRON
eurjchem-792	264	1	o	o	NOUN
eurjchem-792	265	1	oh	oh	INTJ
eurjchem-792	265	2	o	o	X
eurjchem-792	265	3	f	f	PROPN
eurjchem-792	265	4	n	n	CCONJ
eurjchem-792	265	5	n	n	ADV
eurjchem-792	266	1	oh	oh	INTJ
eurjchem-792	266	2	s	s	NOUN
eurjchem-792	266	3	n	n	CCONJ
eurjchem-792	266	4	n	n	NOUN
eurjchem-792	266	5	h	h	NOUN
eurjchem-792	267	1	r	r	NOUN
eurjchem-792	267	2	o	o	NOUN
eurjchem-792	267	3	sample	sample	NOUN
eurjchem-792	267	4	no	no	DET
eurjchem-792	267	5	r	r	NOUN
eurjchem-792	267	6	product	product	NOUN
eurjchem-792	267	7	yield	yield	NOUN
eurjchem-792	267	8	(	(	PUNCT
eurjchem-792	267	9	%	%	NOUN
eurjchem-792	267	10	)	)	PUNCT
eurjchem-792	267	11	1	1	NUM
eurjchem-792	267	12	h	h	NOUN
eurjchem-792	267	13	4a	4a	NOUN
eurjchem-792	267	14	81.5	81.5	NUM
eurjchem-792	267	15	2	2	NUM
eurjchem-792	267	16	ch3	ch3	PROPN
eurjchem-792	267	17	4b	4b	NOUN
eurjchem-792	267	18	82.3	82.3	NUM
eurjchem-792	267	19	3	3	NUM
eurjchem-792	267	20	och3	och3	ADJ
eurjchem-792	267	21	4c	4c	NOUN
eurjchem-792	267	22	76.6	76.6	NUM
eurjchem-792	267	23	4	4	NUM
eurjchem-792	267	24	och2f2	och2f2	NOUN
eurjchem-792	267	25	4d	4d	NOUN
eurjchem-792	267	26	74.8	74.8	NUM
eurjchem-792	267	27	5	5	NUM
eurjchem-792	267	28	cl	cl	NOUN
eurjchem-792	267	29	4e	4e	NOUN
eurjchem-792	267	30	84.1	84.1	NUM
eurjchem-792	267	31	table	table	NOUN
eurjchem-792	267	32	4	4	NUM
eurjchem-792	267	33	.	.	PUNCT
eurjchem-792	267	34	synthesis	synthesis	NOUN
eurjchem-792	267	35	of	of	ADP
eurjchem-792	267	36	various	various	ADJ
eurjchem-792	267	37	substituted	substitute	VERB
eurjchem-792	267	38	mercaptobenzimdazolyl	mercaptobenzimdazolyl	NOUN
eurjchem-792	267	39	sulfones	sulfone	NOUN
eurjchem-792	267	40	,	,	PUNCT
eurjchem-792	267	41	5a‐e	5a‐e	PROPN
eurjchem-792	267	42	,	,	PUNCT
eurjchem-792	267	43	from	from	ADP
eurjchem-792	267	44	corresponding	corresponding	ADJ
eurjchem-792	267	45	sulfides	sulfide	NOUN
eurjchem-792	267	46	using	use	VERB
eurjchem-792	267	47	ammonium	ammonium	NOUN
eurjchem-792	267	48	molybdate	molybdate	NOUN
eurjchem-792	267	49	catalysed	catalyse	VERB
eurjchem-792	267	50	hydrogen	hydrogen	NOUN
eurjchem-792	267	51	peroxide	peroxide	NOUN
eurjchem-792	267	52	.	.	PUNCT
eurjchem-792	268	1	sample	sample	NOUN
eurjchem-792	268	2	no	no	DET
eurjchem-792	268	3	r	r	NOUN
eurjchem-792	268	4	reactant	reactant	NOUN
eurjchem-792	268	5	product	product	NOUN
eurjchem-792	268	6	yield	yield	NOUN
eurjchem-792	268	7	(	(	PUNCT
eurjchem-792	268	8	%	%	NOUN
eurjchem-792	268	9	)	)	PUNCT
eurjchem-792	268	10	1	1	NUM
eurjchem-792	268	11	h	h	NOUN
eurjchem-792	268	12	4a	4a	NOUN
eurjchem-792	268	13	5a	5a	NUM
eurjchem-792	268	14	83.4	83.4	NUM
eurjchem-792	268	15	2	2	NUM
eurjchem-792	268	16	ch3	ch3	PROPN
eurjchem-792	268	17	4b	4b	PROPN
eurjchem-792	268	18	5b	5b	VERB
eurjchem-792	268	19	78.6	78.6	NUM
eurjchem-792	268	20	3	3	NUM
eurjchem-792	268	21	och3	och3	ADJ
eurjchem-792	268	22	4c	4c	NOUN
eurjchem-792	268	23	5c	5c	NOUN
eurjchem-792	268	24	80.4	80.4	NUM
eurjchem-792	268	25	4	4	NUM
eurjchem-792	268	26	och2f2	och2f2	NOUN
eurjchem-792	268	27	4d	4d	NUM
eurjchem-792	268	28	5d	5d	NUM
eurjchem-792	268	29	79.5	79.5	NUM
eurjchem-792	268	30	5	5	NUM
eurjchem-792	268	31	cl	cl	NOUN
eurjchem-792	268	32	4e	4e	NOUN
eurjchem-792	268	33	5e	5e	NOUN
eurjchem-792	268	34	86.8	86.8	NUM
eurjchem-792	268	35	further	far	ADV
eurjchem-792	268	36	,	,	PUNCT
eurjchem-792	268	37	enone	enone	NOUN
eurjchem-792	268	38	carbon	carbon	NOUN
eurjchem-792	268	39	resonated	resonate	VERB
eurjchem-792	268	40	downfield	downfield	VERB
eurjchem-792	268	41	than	than	SCONJ
eurjchem-792	268	42	all	all	DET
eurjchem-792	268	43	the	the	DET
eurjchem-792	268	44	carbons	carbon	NOUN
eurjchem-792	268	45	at	at	ADP
eurjchem-792	268	46	176.83	176.83	NUM
eurjchem-792	268	47	ppm	ppm	NOUN
eurjchem-792	268	48	where	where	SCONJ
eurjchem-792	268	49	as	as	ADP
eurjchem-792	268	50	carboxylic	carboxylic	ADJ
eurjchem-792	268	51	acid	acid	NOUN
eurjchem-792	268	52	carbon	carbon	NOUN
eurjchem-792	268	53	resonated	resonate	VERB
eurjchem-792	268	54	at	at	ADP
eurjchem-792	268	55	166.39	166.39	NUM
eurjchem-792	268	56	ppm	ppm	NOUN
eurjchem-792	268	57	further	far	ADV
eurjchem-792	268	58	proved	prove	VERB
eurjchem-792	268	59	the	the	DET
eurjchem-792	268	60	presence	presence	NOUN
eurjchem-792	268	61	of	of	ADP
eurjchem-792	268	62	both	both	DET
eurjchem-792	268	63	carbonyl	carbonyl	NOUN
eurjchem-792	268	64	carbons	carbon	NOUN
eurjchem-792	268	65	.	.	PUNCT
eurjchem-792	269	1	molecular	molecular	ADJ
eurjchem-792	269	2	mass	mass	NOUN
eurjchem-792	269	3	of	of	ADP
eurjchem-792	269	4	compound	compound	NOUN
eurjchem-792	269	5	4a	4a	NOUN
eurjchem-792	269	6	in	in	ADP
eurjchem-792	269	7	the	the	DET
eurjchem-792	269	8	mass	mass	NOUN
eurjchem-792	269	9	spectrum	spectrum	NOUN
eurjchem-792	269	10	shown	show	VERB
eurjchem-792	269	11	m	m	PROPN
eurjchem-792	269	12	/	/	SYM
eurjchem-792	269	13	z	z	PROPN
eurjchem-792	269	14	554.07	554.07	NUM
eurjchem-792	269	15	(	(	PUNCT
eurjchem-792	269	16	m	m	PROPN
eurjchem-792	269	17	+	+	ADJ
eurjchem-792	269	18	)	)	PUNCT
eurjchem-792	269	19	indicated	indicate	VERB
eurjchem-792	269	20	the	the	DET
eurjchem-792	269	21	molecular	molecular	ADJ
eurjchem-792	269	22	weight	weight	NOUN
eurjchem-792	269	23	of	of	ADP
eurjchem-792	269	24	compound	compound	NOUN
eurjchem-792	269	25	i.e.	i.e.	X
eurjchem-792	269	26	m	m	VERB
eurjchem-792	269	27	/	/	SYM
eurjchem-792	269	28	z	z	PROPN
eurjchem-792	269	29	553.60	553.60	NUM
eurjchem-792	269	30	.	.	PUNCT
eurjchem-792	270	1	the	the	DET
eurjchem-792	270	2	results	result	NOUN
eurjchem-792	270	3	of	of	ADP
eurjchem-792	270	4	elemental	elemental	ADJ
eurjchem-792	270	5	analysis	analysis	NOUN
eurjchem-792	270	6	for	for	ADP
eurjchem-792	270	7	c	c	NOUN
eurjchem-792	270	8	,	,	PUNCT
eurjchem-792	270	9	h	h	NOUN
eurjchem-792	270	10	and	and	CCONJ
eurjchem-792	270	11	n	n	PROPN
eurjchem-792	270	12	were	be	AUX
eurjchem-792	270	13	within	within	ADP
eurjchem-792	270	14	±0.4	±0.4	PROPN
eurjchem-792	270	15	%	%	NOUN
eurjchem-792	270	16	of	of	ADP
eurjchem-792	270	17	the	the	DET
eurjchem-792	270	18	theoretical	theoretical	ADJ
eurjchem-792	270	19	values	value	NOUN
eurjchem-792	270	20	.	.	PUNCT
eurjchem-792	271	1	the	the	DET
eurjchem-792	271	2	specific	specific	ADJ
eurjchem-792	271	3	optical	optical	ADJ
eurjchem-792	271	4	rotation	rotation	NOUN
eurjchem-792	271	5	[	[	X
eurjchem-792	271	6	α]d25	α]d25	NOUN
eurjchem-792	271	7	:	:	PUNCT
eurjchem-792	271	8	‐91.68	‐91.68	PROPN
eurjchem-792	271	9	proven	prove	VERB
eurjchem-792	271	10	that	that	SCONJ
eurjchem-792	271	11	the	the	DET
eurjchem-792	271	12	compound	compound	NOUN
eurjchem-792	271	13	4a	4a	NOUN
eurjchem-792	271	14	is	be	AUX
eurjchem-792	271	15	chiral	chiral	ADJ
eurjchem-792	271	16	.	.	PUNCT
eurjchem-792	272	1	similar	similar	ADJ
eurjchem-792	272	2	reactions	reaction	NOUN
eurjchem-792	272	3	have	have	AUX
eurjchem-792	272	4	been	be	AUX
eurjchem-792	272	5	carried	carry	VERB
eurjchem-792	272	6	out	out	ADP
eurjchem-792	272	7	with	with	ADP
eurjchem-792	272	8	various	various	ADJ
eurjchem-792	272	9	substituted	substitute	VERB
eurjchem-792	272	10	mercapto	mercapto	NOUN
eurjchem-792	272	11	benzimdazoles	benzimdazole	NOUN
eurjchem-792	272	12	dipicted	dipicte	VERB
eurjchem-792	272	13	in	in	ADP
eurjchem-792	272	14	table	table	NOUN
eurjchem-792	272	15	3	3	NUM
eurjchem-792	272	16	.	.	PUNCT
eurjchem-792	272	17	initially	initially	ADV
eurjchem-792	272	18	,	,	PUNCT
eurjchem-792	272	19	compounds	compound	VERB
eurjchem-792	272	20	4a‐e	4a‐e	PROPN
eurjchem-792	272	21	was	be	AUX
eurjchem-792	272	22	allowed	allow	VERB
eurjchem-792	272	23	to	to	PART
eurjchem-792	272	24	react	react	VERB
eurjchem-792	272	25	with	with	ADP
eurjchem-792	272	26	sodium	sodium	NOUN
eurjchem-792	272	27	hypochlorite	hypochlorite	NOUN
eurjchem-792	272	28	in	in	ADP
eurjchem-792	272	29	methylene	methylene	ADJ
eurjchem-792	272	30	chloride	chloride	NOUN
eurjchem-792	272	31	with	with	ADP
eurjchem-792	272	32	different	different	ADJ
eurjchem-792	272	33	mole	mole	NOUN
eurjchem-792	272	34	ratios	ratio	NOUN
eurjchem-792	272	35	and	and	CCONJ
eurjchem-792	272	36	temperatures	temperature	NOUN
eurjchem-792	272	37	,	,	PUNCT
eurjchem-792	272	38	observed	observe	VERB
eurjchem-792	272	39	the	the	DET
eurjchem-792	272	40	resulted	resulted	ADJ
eurjchem-792	272	41	product	product	NOUN
eurjchem-792	272	42	is	be	AUX
eurjchem-792	272	43	mixture	mixture	NOUN
eurjchem-792	272	44	of	of	ADP
eurjchem-792	272	45	sulfoxide	sulfoxide	NOUN
eurjchem-792	272	46	and	and	CCONJ
eurjchem-792	272	47	sulfone	sulfone	NOUN
eurjchem-792	272	48	,	,	PUNCT
eurjchem-792	272	49	the	the	DET
eurjchem-792	272	50	same	same	ADJ
eurjchem-792	272	51	oxidation	oxidation	NOUN
eurjchem-792	272	52	reaction	reaction	NOUN
eurjchem-792	272	53	carried	carry	VERB
eurjchem-792	272	54	out	out	ADP
eurjchem-792	272	55	using	use	VERB
eurjchem-792	272	56	potassium	potassium	NOUN
eurjchem-792	272	57	peroxomonosulfate	peroxomonosulfate	NOUN
eurjchem-792	272	58	(	(	PUNCT
eurjchem-792	272	59	oxone	oxone	NOUN
eurjchem-792	272	60	)	)	PUNCT
eurjchem-792	272	61	but	but	CCONJ
eurjchem-792	272	62	results	result	NOUN
eurjchem-792	272	63	are	be	AUX
eurjchem-792	272	64	not	not	PART
eurjchem-792	272	65	encouraging	encouraging	ADJ
eurjchem-792	272	66	.	.	PUNCT
eurjchem-792	273	1	further	further	ADJ
eurjchem-792	273	2	attempts	attempt	NOUN
eurjchem-792	273	3	made	make	VERB
eurjchem-792	273	4	using	use	VERB
eurjchem-792	273	5	hydrogen	hydrogen	NOUN
eurjchem-792	273	6	peroxide	peroxide	NOUN
eurjchem-792	273	7	observed	observe	VERB
eurjchem-792	273	8	that	that	SCONJ
eurjchem-792	273	9	reaction	reaction	NOUN
eurjchem-792	273	10	is	be	AUX
eurjchem-792	273	11	taken	take	VERB
eurjchem-792	273	12	longer	long	ADJ
eurjchem-792	273	13	hours	hour	NOUN
eurjchem-792	273	14	and	and	CCONJ
eurjchem-792	273	15	formation	formation	NOUN
eurjchem-792	273	16	of	of	ADP
eurjchem-792	273	17	other	other	ADJ
eurjchem-792	273	18	side	side	NOUN
eurjchem-792	273	19	products	product	NOUN
eurjchem-792	273	20	predominately	predominately	ADV
eurjchem-792	273	21	corresponding	correspond	VERB
eurjchem-792	273	22	sulfoxide	sulfoxide	NOUN
eurjchem-792	273	23	,	,	PUNCT
eurjchem-792	273	24	when	when	SCONJ
eurjchem-792	273	25	the	the	DET
eurjchem-792	273	26	same	same	ADJ
eurjchem-792	273	27	reactions	reaction	NOUN
eurjchem-792	273	28	are	be	AUX
eurjchem-792	273	29	carried	carry	VERB
eurjchem-792	273	30	out	out	ADP
eurjchem-792	273	31	using	use	VERB
eurjchem-792	273	32	ammonium	ammonium	NOUN
eurjchem-792	273	33	molybdate	molybdate	NOUN
eurjchem-792	273	34	catalysed	catalyse	VERB
eurjchem-792	273	35	h2o2	h2o2	NOUN
eurjchem-792	273	36	in	in	ADP
eurjchem-792	273	37	presence	presence	NOUN
eurjchem-792	273	38	of	of	ADP
eurjchem-792	273	39	phase	phase	NOUN
eurjchem-792	273	40	transfer	transfer	NOUN
eurjchem-792	273	41	catalyst	catalyst	NOUN
eurjchem-792	273	42	like	like	ADP
eurjchem-792	273	43	tetrabutyl	tetrabutyl	NOUN
eurjchem-792	273	44	ammonium	ammonium	NOUN
eurjchem-792	273	45	bromide	bromide	NOUN
eurjchem-792	273	46	surprisingly	surprisingly	ADV
eurjchem-792	273	47	reaction	reaction	NOUN
eurjchem-792	273	48	is	be	AUX
eurjchem-792	273	49	completed	complete	VERB
eurjchem-792	273	50	within	within	ADP
eurjchem-792	273	51	4.0	4.0	NUM
eurjchem-792	273	52	h	h	NOUN
eurjchem-792	273	53	and	and	CCONJ
eurjchem-792	273	54	resulted	result	VERB
eurjchem-792	273	55	product	product	NOUN
eurjchem-792	273	56	is	be	AUX
eurjchem-792	273	57	selectively	selectively	ADV
eurjchem-792	273	58	desired	desire	VERB
eurjchem-792	273	59	sulfone	sulfone	NOUN
eurjchem-792	273	60	.	.	PUNCT
eurjchem-792	274	1	the	the	DET
eurjchem-792	274	2	chemical	chemical	NOUN
eurjchem-792	274	3	reaction	reaction	NOUN
eurjchem-792	274	4	depicted	depict	VERB
eurjchem-792	274	5	in	in	ADP
eurjchem-792	274	6	scheme	scheme	NOUN
eurjchem-792	274	7	3	3	NUM
eurjchem-792	274	8	.	.	PUNCT
eurjchem-792	275	1	the	the	DET
eurjchem-792	275	2	structure	structure	NOUN
eurjchem-792	275	3	of	of	ADP
eurjchem-792	275	4	compound	compound	NOUN
eurjchem-792	275	5	5a	5a	NUM
eurjchem-792	275	6	was	be	AUX
eurjchem-792	275	7	determined	determine	VERB
eurjchem-792	275	8	on	on	ADP
eurjchem-792	275	9	the	the	DET
eurjchem-792	275	10	basis	basis	NOUN
eurjchem-792	275	11	of	of	ADP
eurjchem-792	275	12	its	its	PRON
eurjchem-792	275	13	spectral	spectral	ADJ
eurjchem-792	275	14	data	datum	NOUN
eurjchem-792	275	15	.	.	PUNCT
eurjchem-792	276	1	its	its	PRON
eurjchem-792	276	2	ir	ir	PROPN
eurjchem-792	276	3	(	(	PUNCT
eurjchem-792	276	4	kbr	kbr	PROPN
eurjchem-792	276	5	)	)	PUNCT
eurjchem-792	276	6	spectrum	spectrum	NOUN
eurjchem-792	276	7	contains	contain	VERB
eurjchem-792	276	8	sharp	sharp	ADJ
eurjchem-792	276	9	absorption	absorption	NOUN
eurjchem-792	276	10	bands	band	NOUN
eurjchem-792	276	11	at	at	ADP
eurjchem-792	276	12	1718	1718	NUM
eurjchem-792	276	13	and	and	CCONJ
eurjchem-792	276	14	1621	1621	NUM
eurjchem-792	276	15	cm‐1	cm‐1	PROPN
eurjchem-792	276	16	indicated	indicate	VERB
eurjchem-792	276	17	the	the	DET
eurjchem-792	276	18	presence	presence	NOUN
eurjchem-792	276	19	of	of	ADP
eurjchem-792	276	20	carbonyl	carbonyl	NOUN
eurjchem-792	276	21	groups	group	NOUN
eurjchem-792	276	22	.	.	PUNCT
eurjchem-792	277	1	1h	1h	NUM
eurjchem-792	277	2	nmr	nmr	PROPN
eurjchem-792	277	3	spectra	spectra	NOUN
eurjchem-792	277	4	in	in	ADP
eurjchem-792	277	5	dmso‐d6	dmso‐d6	PROPN
eurjchem-792	277	6	shown	show	VERB
eurjchem-792	277	7	the	the	DET
eurjchem-792	277	8	absence	absence	NOUN
eurjchem-792	277	9	of	of	ADP
eurjchem-792	277	10	methylene	methylene	ADJ
eurjchem-792	277	11	protons	proton	NOUN
eurjchem-792	277	12	at	at	ADP
eurjchem-792	277	13	2.64‐2.66	2.64‐2.66	NUM
eurjchem-792	277	14	ppm	ppm	NOUN
eurjchem-792	277	15	and	and	CCONJ
eurjchem-792	277	16	shifted	shift	VERB
eurjchem-792	277	17	to	to	ADP
eurjchem-792	277	18	little	little	ADJ
eurjchem-792	277	19	down	down	ADP
eurjchem-792	277	20	field	field	NOUN
eurjchem-792	277	21	to	to	ADP
eurjchem-792	277	22	3.83‐3.85	3.83‐3.85	NUM
eurjchem-792	277	23	ppm	ppm	NOUN
eurjchem-792	277	24	proved	prove	VERB
eurjchem-792	277	25	the	the	DET
eurjchem-792	277	26	absence	absence	NOUN
eurjchem-792	277	27	of	of	ADP
eurjchem-792	277	28	starting	start	VERB
eurjchem-792	277	29	sufide	sufide	ADV
eurjchem-792	277	30	.	.	PUNCT
eurjchem-792	278	1	chemical	chemical	ADJ
eurjchem-792	278	2	shift	shift	NOUN
eurjchem-792	278	3	at	at	ADP
eurjchem-792	278	4	15.12	15.12	NUM
eurjchem-792	278	5	ppm	ppm	NOUN
eurjchem-792	278	6	as	as	ADP
eurjchem-792	278	7	broad	broad	ADJ
eurjchem-792	278	8	singlet	singlet	ADJ
eurjchem-792	278	9	d2o	d2o	NOUN
eurjchem-792	278	10	exchangeable	exchangeable	ADJ
eurjchem-792	278	11	proton	proton	NOUN
eurjchem-792	278	12	indicated	indicate	VERB
eurjchem-792	278	13	the	the	DET
eurjchem-792	278	14	presence	presence	NOUN
eurjchem-792	278	15	of	of	ADP
eurjchem-792	278	16	carboxylic	carboxylic	ADJ
eurjchem-792	278	17	acid	acid	NOUN
eurjchem-792	278	18	which	which	PRON
eurjchem-792	278	19	is	be	AUX
eurjchem-792	278	20	essential	essential	ADJ
eurjchem-792	278	21	to	to	PART
eurjchem-792	278	22	exhibit	exhibit	VERB
eurjchem-792	278	23	the	the	DET
eurjchem-792	278	24	antimicrobial	antimicrobial	ADJ
eurjchem-792	278	25	activity	activity	NOUN
eurjchem-792	278	26	.	.	PUNCT
eurjchem-792	279	1	however	however	ADV
eurjchem-792	279	2	absence	absence	VERB
eurjchem-792	279	3	the	the	DET
eurjchem-792	279	4	carbon	carbon	NOUN
eurjchem-792	279	5	chemical	chemical	NOUN
eurjchem-792	279	6	shift	shift	NOUN
eurjchem-792	279	7	at	at	ADP
eurjchem-792	279	8	47.12	47.12	NUM
eurjchem-792	279	9	ppm	ppm	NOUN
eurjchem-792	279	10	and	and	CCONJ
eurjchem-792	279	11	appeared	appear	VERB
eurjchem-792	279	12	at	at	ADP
eurjchem-792	279	13	64.51	64.51	NUM
eurjchem-792	279	14	ppm	ppm	NOUN
eurjchem-792	279	15	confirmed	confirm	VERB
eurjchem-792	279	16	the	the	DET
eurjchem-792	279	17	formation	formation	NOUN
eurjchem-792	279	18	of	of	ADP
eurjchem-792	279	19	sulfone	sulfone	NOUN
eurjchem-792	279	20	.	.	PUNCT
eurjchem-792	280	1	the	the	DET
eurjchem-792	280	2	molecular	molecular	ADJ
eurjchem-792	280	3	mass	mass	NOUN
eurjchem-792	280	4	of	of	ADP
eurjchem-792	280	5	compound	compound	NOUN
eurjchem-792	280	6	shown	show	VERB
eurjchem-792	280	7	in	in	ADP
eurjchem-792	280	8	the	the	DET
eurjchem-792	280	9	mass	mass	NOUN
eurjchem-792	280	10	spectrum	spectrum	NOUN
eurjchem-792	280	11	as	as	ADP
eurjchem-792	280	12	m	m	NOUN
eurjchem-792	280	13	/	/	SYM
eurjchem-792	280	14	z	z	PROPN
eurjchem-792	280	15	586.07	586.07	NUM
eurjchem-792	280	16	(	(	PUNCT
eurjchem-792	280	17	m+	m+	NOUN
eurjchem-792	280	18	)	)	PUNCT
eurjchem-792	280	19	indicated	indicate	VERB
eurjchem-792	280	20	its	its	PRON
eurjchem-792	280	21	molecular	molecular	ADJ
eurjchem-792	280	22	weight	weight	NOUN
eurjchem-792	280	23	m	m	PROPN
eurjchem-792	280	24	/	/	SYM
eurjchem-792	280	25	z	z	PROPN
eurjchem-792	280	26	585.60	585.60	NUM
eurjchem-792	280	27	.	.	PUNCT
eurjchem-792	281	1	the	the	DET
eurjchem-792	281	2	results	result	NOUN
eurjchem-792	281	3	of	of	ADP
eurjchem-792	281	4	elemental	elemental	ADJ
eurjchem-792	281	5	analysis	analysis	NOUN
eurjchem-792	281	6	for	for	ADP
eurjchem-792	281	7	c	c	NOUN
eurjchem-792	281	8	,	,	PUNCT
eurjchem-792	281	9	h	h	NOUN
eurjchem-792	281	10	and	and	CCONJ
eurjchem-792	281	11	n	n	PROPN
eurjchem-792	281	12	were	be	AUX
eurjchem-792	281	13	within	within	ADP
eurjchem-792	281	14	±0.4	±0.4	PROPN
eurjchem-792	281	15	%	%	NOUN
eurjchem-792	281	16	of	of	ADP
eurjchem-792	281	17	the	the	DET
eurjchem-792	281	18	theoretical	theoretical	ADJ
eurjchem-792	281	19	values	value	NOUN
eurjchem-792	281	20	.	.	PUNCT
eurjchem-792	282	1	the	the	DET
eurjchem-792	282	2	specific	specific	ADJ
eurjchem-792	282	3	optical	optical	ADJ
eurjchem-792	282	4	rotation	rotation	NOUN
eurjchem-792	282	5	[	[	X
eurjchem-792	282	6	α]d25	α]d25	NOUN
eurjchem-792	282	7	:	:	PUNCT
eurjchem-792	282	8	‐84.24	‐84.24	NUM
eurjchem-792	282	9	proven	prove	VERB
eurjchem-792	282	10	that	that	SCONJ
eurjchem-792	282	11	the	the	DET
eurjchem-792	282	12	compound	compound	NOUN
eurjchem-792	282	13	5a	5a	NOUN
eurjchem-792	282	14	is	be	AUX
eurjchem-792	282	15	chiral	chiral	ADJ
eurjchem-792	282	16	.	.	PUNCT
eurjchem-792	283	1	the	the	DET
eurjchem-792	283	2	above	above	ADJ
eurjchem-792	283	3	reaction	reaction	NOUN
eurjchem-792	283	4	has	have	AUX
eurjchem-792	283	5	been	be	AUX
eurjchem-792	283	6	carried	carry	VERB
eurjchem-792	283	7	out	out	ADP
eurjchem-792	283	8	with	with	ADP
eurjchem-792	283	9	various	various	ADJ
eurjchem-792	283	10	n‐	n‐	NOUN
eurjchem-792	283	11	substituted	substitute	VERB
eurjchem-792	283	12	β‐hydroxy	β‐hydroxy	PUNCT
eurjchem-792	283	13	benzimidazolyl	benzimidazolyl	ADJ
eurjchem-792	283	14	sulfides	sulfide	NOUN
eurjchem-792	283	15	to	to	PART
eurjchem-792	283	16	convert	convert	VERB
eurjchem-792	283	17	into	into	ADP
eurjchem-792	283	18	corresponding	corresponding	ADJ
eurjchem-792	283	19	sulfones	sulfone	NOUN
eurjchem-792	283	20	using	use	VERB
eurjchem-792	283	21	ammonium	ammonium	NOUN
eurjchem-792	283	22	molybdate	molybdate	NOUN
eurjchem-792	283	23	catalysed	catalyse	VERB
eurjchem-792	283	24	h2o2	h2o2	NOUN
eurjchem-792	283	25	as	as	SCONJ
eurjchem-792	283	26	mentioned	mention	VERB
eurjchem-792	283	27	in	in	ADP
eurjchem-792	283	28	table	table	NOUN
eurjchem-792	283	29	4	4	NUM
eurjchem-792	283	30	.	.	PUNCT
eurjchem-792	284	1	all	all	DET
eurjchem-792	284	2	the	the	DET
eurjchem-792	284	3	newly	newly	ADV
eurjchem-792	284	4	synthesized	synthesize	VERB
eurjchem-792	284	5	compounds	compound	NOUN
eurjchem-792	284	6	2	2	NUM
eurjchem-792	284	7	,	,	PUNCT
eurjchem-792	284	8	3	3	NUM
eurjchem-792	284	9	,	,	PUNCT
eurjchem-792	284	10	4a‐e	4a‐e	NOUN
eurjchem-792	284	11	and	and	CCONJ
eurjchem-792	284	12	5a‐e	5a‐e	NOUN
eurjchem-792	284	13	were	be	AUX
eurjchem-792	284	14	tested	test	VERB
eurjchem-792	284	15	invitro	invitro	ADV
eurjchem-792	284	16	against	against	ADP
eurjchem-792	284	17	gram‐positive	gram‐positive	ADJ
eurjchem-792	284	18	organisms	organism	NOUN
eurjchem-792	284	19	viz	viz	VERB
eurjchem-792	284	20	.	.	PUNCT
eurjchem-792	285	1	bacillus	bacillus	NOUN
eurjchem-792	285	2	subtilis	subtili	NOUN
eurjchem-792	285	3	(	(	PUNCT
eurjchem-792	285	4	mtcc	mtcc	NOUN
eurjchem-792	285	5	441	441	NUM
eurjchem-792	285	6	)	)	PUNCT
eurjchem-792	285	7	,	,	PUNCT
eurjchem-792	285	8	staphylococcus	staphylococcus	NOUN
eurjchem-792	285	9	aureus	aureus	NOUN
eurjchem-792	285	10	(	(	PUNCT
eurjchem-792	285	11	mtcc	mtcc	NOUN
eurjchem-792	285	12	96	96	NUM
eurjchem-792	285	13	)	)	PUNCT
eurjchem-792	285	14	,	,	PUNCT
eurjchem-792	285	15	staphylococcus	staphylococcus	NOUN
eurjchem-792	285	16	epidermidis	epidermidi	NOUN
eurjchem-792	285	17	and	and	CCONJ
eurjchem-792	285	18	gram‐negative	gram‐negative	ADJ
eurjchem-792	285	19	organisms	organism	NOUN
eurjchem-792	285	20	viz	viz	VERB
eurjchem-792	285	21	.	.	PUNCT
eurjchem-792	285	22	escherichia	escherichia	NOUN
eurjchem-792	285	23	coli	coli	NOUN
eurjchem-792	285	24	(	(	PUNCT
eurjchem-792	285	25	mtcc	mtcc	NOUN
eurjchem-792	285	26	443	443	NUM
eurjchem-792	285	27	)	)	PUNCT
eurjchem-792	285	28	,	,	PUNCT
eurjchem-792	285	29	pseudomonas	pseudomona	VERB
eurjchem-792	285	30	aeruginosa	aeruginosa	NOUN
eurjchem-792	285	31	(	(	PUNCT
eurjchem-792	285	32	mtcc	mtcc	NOUN
eurjchem-792	285	33	741	741	NUM
eurjchem-792	285	34	)	)	PUNCT
eurjchem-792	285	35	,	,	PUNCT
eurjchem-792	285	36	and	and	CCONJ
eurjchem-792	285	37	klebsiella	klebsiella	NOUN
eurjchem-792	285	38	pneumoniae	pneumoniae	ADJ
eurjchem-792	285	39	(	(	PUNCT
eurjchem-792	285	40	mtcc	mtcc	NOUN
eurjchem-792	285	41	618	618	NUM
eurjchem-792	285	42	)	)	PUNCT
eurjchem-792	285	43	and	and	CCONJ
eurjchem-792	285	44	also	also	ADV
eurjchem-792	285	45	synthesized	synthesize	VERB
eurjchem-792	285	46	compounds	compound	NOUN
eurjchem-792	285	47	were	be	AUX
eurjchem-792	285	48	screened	screen	VERB
eurjchem-792	285	49	invitro	invitro	ADV
eurjchem-792	285	50	for	for	ADP
eurjchem-792	285	51	antifungal	antifungal	ADJ
eurjchem-792	285	52	activity	activity	NOUN
eurjchem-792	285	53	aganist	aganist	ADJ
eurjchem-792	285	54	candida	candida	NOUN
eurjchem-792	285	55	albicans	albican	NOUN
eurjchem-792	285	56	(	(	PUNCT
eurjchem-792	285	57	mtcc	mtcc	NOUN
eurjchem-792	285	58	227	227	NUM
eurjchem-792	285	59	)	)	PUNCT
eurjchem-792	285	60	,	,	PUNCT
eurjchem-792	285	61	candida	candida	PROPN
eurjchem-792	285	62	rugosa	rugosa	NOUN
eurjchem-792	285	63	(	(	PUNCT
eurjchem-792	285	64	ncim	ncim	NOUN
eurjchem-792	285	65	3467	3467	NUM
eurjchem-792	285	66	)	)	PUNCT
eurjchem-792	285	67	,	,	PUNCT
eurjchem-792	285	68	aspergillus	aspergillus	NOUN
eurjchem-792	285	69	flavus	flavus	NOUN
eurjchem-792	285	70	(	(	PUNCT
eurjchem-792	285	71	mtcc	mtcc	NOUN
eurjchem-792	285	72	277	277	NUM
eurjchem-792	285	73	)	)	PUNCT
eurjchem-792	285	74	,	,	PUNCT
eurjchem-792	285	75	and	and	CCONJ
eurjchem-792	285	76	aspergillus	aspergillus	NOUN
eurjchem-792	285	77	niger	niger	NOUN
eurjchem-792	285	78	(	(	PUNCT
eurjchem-792	285	79	mtcc	mtcc	NOUN
eurjchem-792	285	80	282	282	NUM
eurjchem-792	285	81	)	)	PUNCT
eurjchem-792	285	82	.	.	PUNCT
eurjchem-792	286	1	saccharomyces	saccharomyce	NOUN
eurjchem-792	286	2	cervisiae	cervisiae	NOUN
eurjchem-792	286	3	(	(	PUNCT
eurjchem-792	286	4	mtcc	mtcc	NOUN
eurjchem-792	286	5	36	36	NUM
eurjchem-792	286	6	)	)	PUNCT
eurjchem-792	286	7	of	of	ADP
eurjchem-792	286	8	yeasts	yeast	NOUN
eurjchem-792	286	9	.	.	PUNCT
eurjchem-792	287	1	most	most	ADJ
eurjchem-792	287	2	of	of	ADP
eurjchem-792	287	3	the	the	DET
eurjchem-792	287	4	evaluated	evaluate	VERB
eurjchem-792	287	5	compounds	compound	NOUN
eurjchem-792	287	6	exhibited	exhibit	VERB
eurjchem-792	287	7	remarkable	remarkable	ADJ
eurjchem-792	287	8	antimicrobial	antimicrobial	ADJ
eurjchem-792	287	9	activity	activity	NOUN
eurjchem-792	287	10	.	.	PUNCT
eurjchem-792	288	1	4	4	X
eurjchem-792	288	2	.	.	X
eurjchem-792	288	3	conclusion	conclusion	NOUN
eurjchem-792	288	4	in	in	ADP
eurjchem-792	288	5	conclusion	conclusion	NOUN
eurjchem-792	288	6	,	,	PUNCT
eurjchem-792	288	7	synthesis	synthesis	NOUN
eurjchem-792	288	8	of	of	ADP
eurjchem-792	288	9	new	new	ADJ
eurjchem-792	288	10	β‐hydroxy	β‐hydroxy	PUNCT
eurjchem-792	288	11	benzimidazolyl	benzimidazolyl	ADJ
eurjchem-792	288	12	sulphides	sulphide	NOUN
eurjchem-792	288	13	,	,	PUNCT
eurjchem-792	288	14	4a‐e	4a‐e	NOUN
eurjchem-792	288	15	,	,	PUNCT
eurjchem-792	288	16	and	and	CCONJ
eurjchem-792	288	17	corresponding	corresponding	ADJ
eurjchem-792	288	18	sulfones	sulfone	NOUN
eurjchem-792	288	19	,	,	PUNCT
eurjchem-792	288	20	5a‐e	5a‐e	PROPN
eurjchem-792	288	21	,	,	PUNCT
eurjchem-792	288	22	containing	contain	VERB
eurjchem-792	288	23	7‐piperzine	7‐piperzine	NUM
eurjchem-792	288	24	fluoroquinolones	fluoroquinolone	NOUN
eurjchem-792	288	25	in	in	ADP
eurjchem-792	288	26	presence	presence	NOUN
eurjchem-792	288	27	of	of	ADP
eurjchem-792	288	28	ammonium	ammonium	NOUN
eurjchem-792	288	29	molybdate	molybdate	NOUN
eurjchem-792	288	30	catalysed	catalyse	VERB
eurjchem-792	288	31	h2o2	h2o2	NOUN
eurjchem-792	288	32	has	have	AUX
eurjchem-792	288	33	been	be	AUX
eurjchem-792	288	34	described	describe	VERB
eurjchem-792	288	35	.	.	PUNCT
eurjchem-792	289	1	the	the	DET
eurjchem-792	289	2	reaction	reaction	NOUN
eurjchem-792	289	3	was	be	AUX
eurjchem-792	289	4	very	very	ADV
eurjchem-792	289	5	simple	simple	ADJ
eurjchem-792	289	6	,	,	PUNCT
eurjchem-792	289	7	highly	highly	ADV
eurjchem-792	289	8	selective	selective	ADJ
eurjchem-792	289	9	towards	towards	ADP
eurjchem-792	289	10	formation	formation	NOUN
eurjchem-792	289	11	of	of	ADP
eurjchem-792	289	12	sulfones	sulfone	NOUN
eurjchem-792	289	13	and	and	CCONJ
eurjchem-792	289	14	reproducible	reproducible	VERB
eurjchem-792	289	15	.	.	PUNCT
eurjchem-792	290	1	all	all	DET
eurjchem-792	290	2	the	the	DET
eurjchem-792	290	3	newly	newly	ADV
eurjchem-792	290	4	synthesized	synthesize	VERB
eurjchem-792	290	5	compounds	compound	NOUN
eurjchem-792	290	6	have	have	AUX
eurjchem-792	290	7	been	be	AUX
eurjchem-792	290	8	evaluated	evaluate	VERB
eurjchem-792	290	9	for	for	ADP
eurjchem-792	290	10	their	their	PRON
eurjchem-792	290	11	antimicrobial	antimicrobial	ADJ
eurjchem-792	290	12	activity	activity	NOUN
eurjchem-792	290	13	against	against	ADP
eurjchem-792	290	14	bacteria	bacteria	NOUN
eurjchem-792	290	15	and	and	CCONJ
eurjchem-792	290	16	fungi	fungus	NOUN
eurjchem-792	290	17	and	and	CCONJ
eurjchem-792	290	18	found	find	VERB
eurjchem-792	290	19	potent	potent	ADJ
eurjchem-792	290	20	against	against	ADP
eurjchem-792	290	21	given	give	VERB
eurjchem-792	290	22	bacteria	bacteria	NOUN
eurjchem-792	290	23	and	and	CCONJ
eurjchem-792	290	24	fungi	fungus	NOUN
eurjchem-792	290	25	strains	strain	NOUN
eurjchem-792	290	26	.	.	PUNCT
eurjchem-792	291	1	compounds	compound	VERB
eurjchem-792	291	2	5d	5d	NUM
eurjchem-792	291	3	,	,	PUNCT
eurjchem-792	291	4	5c	5c	NUM
eurjchem-792	291	5	,	,	PUNCT
eurjchem-792	291	6	and	and	CCONJ
eurjchem-792	291	7	5b	5b	NOUN
eurjchem-792	291	8	are	be	AUX
eurjchem-792	291	9	exhibited	exhibit	VERB
eurjchem-792	291	10	excellent	excellent	ADJ
eurjchem-792	291	11	anti	anti	ADJ
eurjchem-792	291	12	bacterial	bacterial	ADJ
eurjchem-792	291	13	activity	activity	NOUN
eurjchem-792	291	14	against	against	ADP
eurjchem-792	291	15	gram‐positive	gram‐positive	ADJ
eurjchem-792	291	16	organisms	organism	NOUN
eurjchem-792	291	17	viz	viz	VERB
eurjchem-792	291	18	.	.	PUNCT
eurjchem-792	292	1	bacillus	bacillus	NOUN
eurjchem-792	292	2	subtilis	subtili	NOUN
eurjchem-792	292	3	(	(	PUNCT
eurjchem-792	292	4	mtcc	mtcc	NOUN
eurjchem-792	292	5	441	441	NUM
eurjchem-792	292	6	)	)	PUNCT
eurjchem-792	292	7	,	,	PUNCT
eurjchem-792	292	8	staphylococcus	staphylococcus	NOUN
eurjchem-792	292	9	aureus	aureus	NOUN
eurjchem-792	292	10	(	(	PUNCT
eurjchem-792	292	11	mtcc	mtcc	NOUN
eurjchem-792	292	12	96	96	NUM
eurjchem-792	292	13	)	)	PUNCT
eurjchem-792	292	14	,	,	PUNCT
eurjchem-792	292	15	staphylococcus	staphylococcus	NOUN
eurjchem-792	292	16	epidermidis	epidermidi	NOUN
eurjchem-792	292	17	and	and	CCONJ
eurjchem-792	292	18	gram‐negative	gram‐negative	ADJ
eurjchem-792	292	19	organisms	organism	NOUN
eurjchem-792	292	20	viz	viz	VERB
eurjchem-792	292	21	pseudomonas	pseudomonas	PROPN
eurjchem-792	292	22	aeruginosa	aeruginosa	NOUN
eurjchem-792	292	23	(	(	PUNCT
eurjchem-792	292	24	mtcc	mtcc	NOUN
eurjchem-792	292	25	741	741	NUM
eurjchem-792	292	26	)	)	PUNCT
eurjchem-792	292	27	and	and	CCONJ
eurjchem-792	292	28	klebsiella	klebsiella	NOUN
eurjchem-792	292	29	pneumoniae	pneumoniae	ADJ
eurjchem-792	292	30	(	(	PUNCT
eurjchem-792	292	31	mtcc	mtcc	NOUN
eurjchem-792	292	32	618	618	NUM
eurjchem-792	292	33	)	)	PUNCT
eurjchem-792	292	34	.	.	PUNCT
eurjchem-792	293	1	compounds	compound	VERB
eurjchem-792	293	2	4d	4d	NUM
eurjchem-792	293	3	and	and	CCONJ
eurjchem-792	293	4	5c	5c	NUM
eurjchem-792	293	5	have	have	AUX
eurjchem-792	293	6	shown	show	VERB
eurjchem-792	293	7	good	good	ADJ
eurjchem-792	293	8	activity	activity	NOUN
eurjchem-792	293	9	and	and	CCONJ
eurjchem-792	293	10	remaining	remain	VERB
eurjchem-792	293	11	compounds	compound	NOUN
eurjchem-792	293	12	shown	show	VERB
eurjchem-792	293	13	moderate	moderate	ADJ
eurjchem-792	293	14	to	to	ADP
eurjchem-792	293	15	poor	poor	ADJ
eurjchem-792	293	16	activity	activity	NOUN
eurjchem-792	293	17	compared	compare	VERB
eurjchem-792	293	18	with	with	ADP
eurjchem-792	293	19	levofloxacin	levofloxacin	PROPN
eurjchem-792	293	20	(	(	PUNCT
eurjchem-792	293	21	reference	reference	NOUN
eurjchem-792	293	22	drug	drug	NOUN
eurjchem-792	293	23	)	)	PUNCT
eurjchem-792	293	24	but	but	CCONJ
eurjchem-792	293	25	all	all	DET
eurjchem-792	293	26	the	the	DET
eurjchem-792	293	27	compounds	compound	NOUN
eurjchem-792	293	28	shown	show	VERB
eurjchem-792	293	29	equal	equal	ADJ
eurjchem-792	293	30	or	or	CCONJ
eurjchem-792	293	31	less	less	ADJ
eurjchem-792	293	32	activity	activity	NOUN
eurjchem-792	293	33	against	against	ADP
eurjchem-792	293	34	escherichia	escherichia	NOUN
eurjchem-792	293	35	coli	coli	NOUN
eurjchem-792	293	36	(	(	PUNCT
eurjchem-792	293	37	mtcc	mtcc	NOUN
eurjchem-792	293	38	443	443	NUM
eurjchem-792	293	39	)	)	PUNCT
eurjchem-792	293	40	.	.	PUNCT
eurjchem-792	294	1	guruswamy	guruswamy	NOUN
eurjchem-792	294	2	et	et	PROPN
eurjchem-792	294	3	al	al	PROPN
eurjchem-792	294	4	.	.	PUNCT
eurjchem-792	294	5	/	/	SYM
eurjchem-792	294	6	european	european	PROPN
eurjchem-792	294	7	journal	journal	PROPN
eurjchem-792	294	8	of	of	ADP
eurjchem-792	294	9	chemistry	chemistry	NOUN
eurjchem-792	294	10	4	4	NUM
eurjchem-792	294	11	(	(	PUNCT
eurjchem-792	294	12	4	4	NUM
eurjchem-792	294	13	)	)	PUNCT
eurjchem-792	294	14	(	(	PUNCT
eurjchem-792	294	15	2013	2013	NUM
eurjchem-792	294	16	)	)	PUNCT
eurjchem-792	294	17	329‐335	329‐335	PROPN
eurjchem-792	294	18	335	335	NUM
eurjchem-792	294	19	however	however	ADV
eurjchem-792	294	20	,	,	PUNCT
eurjchem-792	294	21	sulfones	sulfone	NOUN
eurjchem-792	294	22	,	,	PUNCT
eurjchem-792	294	23	5a‐e	5a‐e	PROPN
eurjchem-792	294	24	,	,	PUNCT
eurjchem-792	294	25	shown	show	VERB
eurjchem-792	294	26	superior	superior	ADJ
eurjchem-792	294	27	activity	activity	NOUN
eurjchem-792	294	28	than	than	ADP
eurjchem-792	294	29	corresponding	correspond	VERB
eurjchem-792	294	30	sulfides	sulfide	NOUN
eurjchem-792	294	31	.	.	PUNCT
eurjchem-792	295	1	in	in	ADP
eurjchem-792	295	2	the	the	DET
eurjchem-792	295	3	same	same	ADJ
eurjchem-792	295	4	way	way	NOUN
eurjchem-792	295	5	compounds	compound	VERB
eurjchem-792	295	6	5d	5d	PROPN
eurjchem-792	295	7	and	and	CCONJ
eurjchem-792	295	8	5e	5e	NOUN
eurjchem-792	295	9	were	be	AUX
eurjchem-792	295	10	shown	show	VERB
eurjchem-792	295	11	excellent	excellent	ADJ
eurjchem-792	295	12	antifungal	antifungal	ADJ
eurjchem-792	295	13	activity	activity	NOUN
eurjchem-792	295	14	against	against	ADP
eurjchem-792	295	15	c.	c.	NOUN
eurjchem-792	295	16	albicans	albican	NOUN
eurjchem-792	295	17	and	and	CCONJ
eurjchem-792	295	18	4d	4d	NUM
eurjchem-792	295	19	and	and	CCONJ
eurjchem-792	295	20	4e	4e	NOUN
eurjchem-792	295	21	also	also	ADV
eurjchem-792	295	22	exhibited	exhibit	VERB
eurjchem-792	295	23	good	good	ADJ
eurjchem-792	295	24	antifungal	antifungal	ADJ
eurjchem-792	295	25	activity	activity	NOUN
eurjchem-792	295	26	comparatively	comparatively	ADV
eurjchem-792	295	27	other	other	ADJ
eurjchem-792	295	28	newly	newly	ADV
eurjchem-792	295	29	synthesized	synthesize	VERB
eurjchem-792	295	30	compounds	compound	NOUN
eurjchem-792	295	31	in	in	ADP
eurjchem-792	295	32	150	150	NUM
eurjchem-792	295	33	µg	µg	ADJ
eurjchem-792	295	34	/	/	SYM
eurjchem-792	295	35	ml	ml	NOUN
eurjchem-792	295	36	concentration	concentration	NOUN
eurjchem-792	295	37	comparisons	comparison	NOUN
eurjchem-792	295	38	with	with	ADP
eurjchem-792	295	39	levofloxacin	levofloxacin	PROPN
eurjchem-792	295	40	.	.	PUNCT
eurjchem-792	296	1	whereas	whereas	SCONJ
eurjchem-792	296	2	no	no	DET
eurjchem-792	296	3	compound	compound	NOUN
eurjchem-792	296	4	exhibited	exhibit	VERB
eurjchem-792	296	5	antifungal	antifungal	ADJ
eurjchem-792	296	6	activity	activity	NOUN
eurjchem-792	296	7	in	in	ADP
eurjchem-792	296	8	100	100	NUM
eurjchem-792	296	9	µg	µg	ADJ
eurjchem-792	296	10	/	/	SYM
eurjchem-792	296	11	ml	ml	NOUN
eurjchem-792	296	12	concentration	concentration	NOUN
eurjchem-792	296	13	including	include	VERB
eurjchem-792	296	14	reference	reference	NOUN
eurjchem-792	296	15	drug	drug	NOUN
eurjchem-792	296	16	.	.	PUNCT
eurjchem-792	297	1	acknowledgements	acknowledgement	NOUN
eurjchem-792	297	2	the	the	DET
eurjchem-792	297	3	authors	author	NOUN
eurjchem-792	297	4	express	express	VERB
eurjchem-792	297	5	their	their	PRON
eurjchem-792	297	6	sincere	sincere	ADJ
eurjchem-792	297	7	thanks	thank	NOUN
eurjchem-792	297	8	to	to	PART
eurjchem-792	297	9	neuland	neuland	VERB
eurjchem-792	297	10	laboratories	laboratory	NOUN
eurjchem-792	297	11	limited	limit	VERB
eurjchem-792	297	12	,	,	PUNCT
eurjchem-792	297	13	hyderabad	hyderabad	PROPN
eurjchem-792	297	14	(	(	PUNCT
eurjchem-792	297	15	a.p	a.p	PROPN
eurjchem-792	297	16	.	.	PROPN
eurjchem-792	297	17	)	)	PUNCT
eurjchem-792	297	18	,	,	PUNCT
eurjchem-792	297	19	india	india	PROPN
eurjchem-792	297	20	for	for	ADP
eurjchem-792	297	21	supporting	support	VERB
eurjchem-792	297	22	this	this	DET
eurjchem-792	297	23	research	research	NOUN
eurjchem-792	297	24	work	work	NOUN
eurjchem-792	297	25	and	and	CCONJ
eurjchem-792	297	26	indian	indian	PROPN
eurjchem-792	297	27	institute	institute	PROPN
eurjchem-792	297	28	of	of	ADP
eurjchem-792	297	29	chemical	chemical	PROPN
eurjchem-792	297	30	technology	technology	NOUN
eurjchem-792	297	31	(	(	PUNCT
eurjchem-792	297	32	iict	iict	PROPN
eurjchem-792	297	33	)	)	PUNCT
eurjchem-792	297	34	,	,	PUNCT
eurjchem-792	297	35	hyderabad	hyderabad	NOUN
eurjchem-792	297	36	for	for	ADP
eurjchem-792	297	37	providing	provide	VERB
eurjchem-792	297	38	data	datum	NOUN
eurjchem-792	297	39	of	of	ADP
eurjchem-792	297	40	anti‐microbial	anti‐microbial	ADJ
eurjchem-792	297	41	screening	screening	NOUN
eurjchem-792	297	42	.	.	PUNCT
eurjchem-792	298	1	authors	author	NOUN
eurjchem-792	298	2	also	also	ADV
eurjchem-792	298	3	thankful	thankful	ADJ
eurjchem-792	298	4	to	to	ADP
eurjchem-792	298	5	authorities	authority	NOUN
eurjchem-792	298	6	of	of	ADP
eurjchem-792	298	7	jawaharlal	jawaharlal	PROPN
eurjchem-792	298	8	nehru	nehru	PROPN
eurjchem-792	298	9	technological	technological	ADJ
eurjchem-792	298	10	university	university	NOUN
eurjchem-792	298	11	,	,	PUNCT
eurjchem-792	298	12	kukatpally	kukatpally	ADV
eurjchem-792	298	13	,	,	PUNCT
eurjchem-792	298	14	hyderabad	hyderabad	PROPN
eurjchem-792	298	15	(	(	PUNCT
eurjchem-792	298	16	a.p	a.p	PROPN
eurjchem-792	298	17	.	.	PROPN
eurjchem-792	298	18	)	)	PUNCT
eurjchem-792	298	19	,	,	PUNCT
eurjchem-792	298	20	india	india	PROPN
eurjchem-792	298	21	.	.	PUNCT
eurjchem-792	298	22	references	reference	NOUN
eurjchem-792	298	23	[	[	X
eurjchem-792	298	24	1	1	NUM
eurjchem-792	298	25	]	]	PUNCT
eurjchem-792	298	26	.	.	PUNCT
eurjchem-792	299	1	renau	renau	PROPN
eurjchem-792	299	2	,	,	PUNCT
eurjchem-792	299	3	t.	t.	PROPN
eurjchem-792	299	4	e.	e.	PROPN
eurjchem-792	299	5	;	;	PUNCT
eurjchem-792	299	6	sanchez	sanchez	PROPN
eurjchem-792	299	7	,	,	PUNCT
eurjchem-792	299	8	j.	j.	PROPN
eurjchem-792	299	9	p.	p.	PROPN
eurjchem-792	299	10	;	;	PUNCT
eurjchem-792	299	11	shapiro	shapiro	PROPN
eurjchem-792	299	12	,	,	PUNCT
eurjchem-792	299	13	m.	m.	NOUN
eurjchem-792	299	14	a.	a.	PROPN
eurjchem-792	299	15	;	;	PUNCT
eurjchem-792	299	16	dever	dever	PROPN
eurjchem-792	299	17	,	,	PUNCT
eurjchem-792	299	18	j.	j.	PROPN
eurjchem-792	299	19	a.	a.	PROPN
eurjchem-792	299	20	;	;	PUNCT
eurjchem-792	299	21	gracheck	gracheck	PROPN
eurjchem-792	299	22	,	,	PUNCT
eurjchem-792	299	23	s.	s.	PROPN
eurjchem-792	299	24	j.	j.	PROPN
eurjchem-792	299	25	;	;	PUNCT
eurjchem-792	299	26	domagala	domagala	PROPN
eurjchem-792	299	27	,	,	PUNCT
eurjchem-792	299	28	j.	j.	PROPN
eurjchem-792	299	29	m.	m.	PROPN
eurjchem-792	299	30	j.	j.	PROPN
eurjchem-792	299	31	med	med	PROPN
eurjchem-792	299	32	.	.	PROPN
eurjchem-792	299	33	chem	chem	PROPN
eurjchem-792	299	34	.	.	PUNCT
eurjchem-792	300	1	1995	1995	NUM
eurjchem-792	300	2	,	,	PUNCT
eurjchem-792	300	3	38	38	NUM
eurjchem-792	300	4	,	,	PUNCT
eurjchem-792	300	5	2974‐2977	2974‐2977	NUM
eurjchem-792	300	6	.	.	PUNCT
eurjchem-792	301	1	[	[	X
eurjchem-792	301	2	2	2	NUM
eurjchem-792	301	3	]	]	PUNCT
eurjchem-792	301	4	.	.	PUNCT
eurjchem-792	302	1	mascellino	mascellino	PROPN
eurjchem-792	302	2	,	,	PUNCT
eurjchem-792	302	3	m.	m.	NOUN
eurjchem-792	302	4	t.	t.	PROPN
eurjchem-792	302	5	;	;	PUNCT
eurjchem-792	302	6	ferinelli	ferinelli	PROPN
eurjchem-792	302	7	,	,	PUNCT
eurjchem-792	302	8	s.	s.	PROPN
eurjchem-792	302	9	;	;	PUNCT
eurjchem-792	302	10	iegri	iegri	PROPN
eurjchem-792	302	11	,	,	PUNCT
eurjchem-792	302	12	f.	f.	PROPN
eurjchem-792	302	13	;	;	PUNCT
eurjchem-792	302	14	iona	iona	PROPN
eurjchem-792	302	15	,	,	PUNCT
eurjchem-792	302	16	e.	e.	PROPN
eurjchem-792	302	17	;	;	PUNCT
eurjchem-792	302	18	desimone	desimone	PROPN
eurjchem-792	302	19	,	,	PUNCT
eurjchem-792	302	20	c.	c.	PROPN
eurjchem-792	302	21	drugs	drug	NOUN
eurjchem-792	302	22	expert	expert	NOUN
eurjchem-792	302	23	.	.	PUNCT
eurjchem-792	303	1	clin	clin	PROPN
eurjchem-792	303	2	.	.	PUNCT
eurjchem-792	304	1	res	re	NOUN
eurjchem-792	304	2	.	.	PROPN
eurjchem-792	305	1	1998	1998	NUM
eurjchem-792	305	2	,	,	PUNCT
eurjchem-792	305	3	24	24	NUM
eurjchem-792	305	4	,	,	PUNCT
eurjchem-792	305	5	139‐151	139‐151	NUM
eurjchem-792	305	6	.	.	PUNCT
eurjchem-792	306	1	[	[	X
eurjchem-792	306	2	3	3	NUM
eurjchem-792	306	3	]	]	PUNCT
eurjchem-792	306	4	.	.	PUNCT
eurjchem-792	307	1	shen	shen	PROPN
eurjchem-792	307	2	,	,	PUNCT
eurjchem-792	307	3	l.	l.	PROPN
eurjchem-792	307	4	l.	l.	PROPN
eurjchem-792	307	5	;	;	PUNCT
eurjchem-792	307	6	mitscher	mitscher	NOUN
eurjchem-792	307	7	,	,	PUNCT
eurjchem-792	307	8	l.	l.	PROPN
eurjchem-792	307	9	a.	a.	PROPN
eurjchem-792	307	10	;	;	PUNCT
eurjchem-792	307	11	sharma	sharma	PROPN
eurjchem-792	307	12	,	,	PUNCT
eurjchem-792	307	13	p.	p.	NOUN
eurjchem-792	307	14	n.	n.	NOUN
eurjchem-792	307	15	;	;	PUNCT
eurjchem-792	307	16	copper	copper	NOUN
eurjchem-792	307	17	,	,	PUNCT
eurjchem-792	307	18	c.	c.	PROPN
eurjchem-792	307	19	s.	s.	PROPN
eurjchem-792	307	20	;	;	PUNCT
eurjchem-792	307	21	rosen	rosen	PROPN
eurjchem-792	307	22	,	,	PUNCT
eurjchem-792	307	23	t.	t.	PROPN
eurjchem-792	307	24	;	;	PUNCT
eurjchem-792	307	25	pernet	pernet	PROPN
eurjchem-792	307	26	,	,	PUNCT
eurjchem-792	307	27	a.	a.	NOUN
eurjchem-792	307	28	g.	g.	PROPN
eurjchem-792	307	29	biochemistry	biochemistry	PROPN
eurjchem-792	307	30	1989	1989	NUM
eurjchem-792	307	31	,	,	PUNCT
eurjchem-792	307	32	28	28	NUM
eurjchem-792	307	33	,	,	PUNCT
eurjchem-792	307	34	3886‐3894	3886‐3894	NUM
eurjchem-792	307	35	.	.	PUNCT
eurjchem-792	308	1	[	[	X
eurjchem-792	308	2	4	4	NUM
eurjchem-792	308	3	]	]	PUNCT
eurjchem-792	308	4	.	.	PUNCT
eurjchem-792	309	1	kondo	kondo	PROPN
eurjchem-792	309	2	,	,	PUNCT
eurjchem-792	309	3	h.	h.	PROPN
eurjchem-792	309	4	;	;	PUNCT
eurjchem-792	309	5	sakamoto	sakamoto	PROPN
eurjchem-792	309	6	,	,	PUNCT
eurjchem-792	309	7	f.	f.	PROPN
eurjchem-792	309	8	;	;	PUNCT
eurjchem-792	309	9	koders	koder	NOUN
eurjchem-792	309	10	,	,	PUNCT
eurjchem-792	309	11	y.	y.	PROPN
eurjchem-792	309	12	;	;	PUNCT
eurjchem-792	309	13	tsukamoto	tsukamoto	NOUN
eurjchem-792	309	14	,	,	PUNCT
eurjchem-792	309	15	g.	g.	PROPN
eurjchem-792	309	16	j.	j.	PROPN
eurjchem-792	309	17	med	med	PROPN
eurjchem-792	309	18	.	.	PROPN
eurjchem-792	309	19	chem	chem	PROPN
eurjchem-792	309	20	.	.	PUNCT
eurjchem-792	310	1	1986	1986	NUM
eurjchem-792	310	2	,	,	PUNCT
eurjchem-792	310	3	29	29	NUM
eurjchem-792	310	4	,	,	PUNCT
eurjchem-792	310	5	2020‐2024	2020‐2024	NUM
eurjchem-792	310	6	.	.	PUNCT
eurjchem-792	311	1	[	[	X
eurjchem-792	311	2	5	5	NUM
eurjchem-792	311	3	]	]	PUNCT
eurjchem-792	311	4	.	.	PUNCT
eurjchem-792	312	1	sheu	sheu	PROPN
eurjchem-792	312	2	,	,	PUNCT
eurjchem-792	312	3	j.	j.	PROPN
eurjchem-792	312	4	y.	y.	PROPN
eurjchem-792	312	5	;	;	PUNCT
eurjchem-792	312	6	chen	chen	PROPN
eurjchem-792	312	7	,	,	PUNCT
eurjchem-792	312	8	y.	y.	PROPN
eurjchem-792	312	9	l.	l.	PROPN
eurjchem-792	312	10	;	;	PUNCT
eurjchem-792	312	11	tzeng	tzeng	PROPN
eurjchem-792	312	12	,	,	PUNCT
eurjchem-792	312	13	c.	c.	PROPN
eurjchem-792	312	14	c.	c.	PROPN
eurjchem-792	312	15	helv	helv	PROPN
eurjchem-792	312	16	.	.	PUNCT
eurjchem-792	313	1	chim	chim	PROPN
eurjchem-792	313	2	.	.	PUNCT
eurjchem-792	314	1	acta	acta	PROPN
eurjchem-792	314	2	.	.	PUNCT
eurjchem-792	315	1	2003	2003	NUM
eurjchem-792	315	2	,	,	PUNCT
eurjchem-792	315	3	86	86	NUM
eurjchem-792	315	4	,	,	PUNCT
eurjchem-792	315	5	2481‐	2481‐	NUM
eurjchem-792	315	6	2489	2489	NUM
eurjchem-792	315	7	.	.	PUNCT
eurjchem-792	316	1	[	[	X
eurjchem-792	316	2	6	6	NUM
eurjchem-792	316	3	]	]	PUNCT
eurjchem-792	316	4	.	.	PUNCT
eurjchem-792	317	1	zhao	zhao	PROPN
eurjchem-792	317	2	,	,	PUNCT
eurjchem-792	317	3	x.	x.	PROPN
eurjchem-792	317	4	;	;	PUNCT
eurjchem-792	317	5	wang	wang	PROPN
eurjchem-792	317	6	,	,	PUNCT
eurjchem-792	317	7	j.	j.	PROPN
eurjchem-792	317	8	y.	y.	PROPN
eurjchem-792	317	9	;	;	PUNCT
eurjchem-792	317	10	xu	xu	PROPN
eurjchem-792	317	11	,	,	PUNCT
eurjchem-792	317	12	c.	c.	PROPN
eurjchem-792	317	13	;	;	PUNCT
eurjchem-792	317	14	dong	dong	PROPN
eurjchem-792	317	15	,	,	PUNCT
eurjchem-792	317	16	y.	y.	PROPN
eurjchem-792	317	17	;	;	PUNCT
eurjchem-792	317	18	zhou	zhou	PROPN
eurjchem-792	317	19	,	,	PUNCT
eurjchem-792	317	20	j.	j.	PROPN
eurjchem-792	317	21	;	;	PUNCT
eurjchem-792	317	22	domagala	domagala	PROPN
eurjchem-792	317	23	,	,	PUNCT
eurjchem-792	317	24	j.	j.	PROPN
eurjchem-792	317	25	;	;	PUNCT
eurjchem-792	317	26	drlica	drlica	PROPN
eurjchem-792	317	27	,	,	PUNCT
eurjchem-792	317	28	k.	k.	PROPN
eurjchem-792	317	29	antimicrob	antimicrob	PROPN
eurjchem-792	317	30	.	.	PUNCT
eurjchem-792	318	1	agents	agents	PROPN
eurjchem-792	318	2	chemother	chemother	PROPN
eurjchem-792	318	3	.	.	PUNCT
eurjchem-792	319	1	1998	1998	NUM
eurjchem-792	319	2	,	,	PUNCT
eurjchem-792	319	3	42	42	NUM
eurjchem-792	319	4	,	,	PUNCT
eurjchem-792	319	5	956‐958	956‐958	NUM
eurjchem-792	319	6	.	.	PUNCT
eurjchem-792	320	1	[	[	X
eurjchem-792	320	2	7	7	NUM
eurjchem-792	320	3	]	]	PUNCT
eurjchem-792	320	4	.	.	PUNCT
eurjchem-792	321	1	jafri	jafri	PROPN
eurjchem-792	321	2	,	,	PUNCT
eurjchem-792	321	3	h.	h.	PROPN
eurjchem-792	321	4	s.	s.	PROPN
eurjchem-792	321	5	;	;	PUNCT
eurjchem-792	321	6	mccracken	mccracken	PROPN
eurjchem-792	321	7	,	,	PUNCT
eurjchem-792	321	8	g.	g.	PROPN
eurjchem-792	321	9	h.	h.	PROPN
eurjchem-792	321	10	drugs	drugs	PROPN
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eurjchem-792	321	12	,	,	PUNCT
eurjchem-792	321	13	58	58	NUM
eurjchem-792	321	14	,	,	PUNCT
eurjchem-792	321	15	43‐48	43‐48	NUM
eurjchem-792	321	16	.	.	PUNCT
eurjchem-792	322	1	[	[	X
eurjchem-792	322	2	8	8	NUM
eurjchem-792	322	3	]	]	SYM
eurjchem-792	322	4	.	.	PUNCT
eurjchem-792	322	5	andriole	andriole	PROPN
eurjchem-792	322	6	,	,	PUNCT
eurjchem-792	322	7	t.	t.	PROPN
eurjchem-792	322	8	v.	v.	CCONJ
eurjchem-792	322	9	drugs	drug	NOUN
eurjchem-792	322	10	1999	1999	NUM
eurjchem-792	322	11	,	,	PUNCT
eurjchem-792	322	12	58	58	NUM
eurjchem-792	322	13	,	,	PUNCT
eurjchem-792	322	14	1‐4	1‐4	NUM
eurjchem-792	322	15	.	.	PUNCT
eurjchem-792	323	1	[	[	X
eurjchem-792	323	2	9	9	NUM
eurjchem-792	323	3	]	]	PUNCT
eurjchem-792	323	4	.	.	PUNCT
eurjchem-792	324	1	drlica	drlica	PROPN
eurjchem-792	324	2	,	,	PUNCT
eurjchem-792	324	3	k.	k.	PROPN
eurjchem-792	324	4	;	;	PUNCT
eurjchem-792	324	5	zhao	zhao	PROPN
eurjchem-792	324	6	,	,	PUNCT
eurjchem-792	324	7	x.	x.	PROPN
eurjchem-792	324	8	microbiol	microbiol	PROPN
eurjchem-792	324	9	.	.	PUNCT
eurjchem-792	325	1	mol	mol	PROPN
eurjchem-792	325	2	.	.	PUNCT
eurjchem-792	326	1	biol	biol	PROPN
eurjchem-792	326	2	.	.	PUNCT
eurjchem-792	327	1	rev	rev	PROPN
eurjchem-792	327	2	.	.	PROPN
eurjchem-792	327	3	1997	1997	NUM
eurjchem-792	327	4	,	,	PUNCT
eurjchem-792	327	5	61	61	NUM
eurjchem-792	327	6	,	,	PUNCT
eurjchem-792	327	7	377‐392	377‐392	NUM
eurjchem-792	327	8	.	.	PUNCT
eurjchem-792	328	1	[	[	X
eurjchem-792	328	2	10	10	NUM
eurjchem-792	328	3	]	]	PUNCT
eurjchem-792	328	4	.	.	PUNCT
eurjchem-792	328	5	mitscher	mitscher	NOUN
eurjchem-792	328	6	,	,	PUNCT
eurjchem-792	328	7	l.	l.	PROPN
eurjchem-792	328	8	a.	a.	PROPN
eurjchem-792	328	9	chem	chem	PROPN
eurjchem-792	328	10	.	.	PUNCT
eurjchem-792	329	1	rev	rev	PROPN
eurjchem-792	329	2	.	.	PROPN
eurjchem-792	329	3	,	,	PUNCT
eurjchem-792	329	4	2005	2005	NUM
eurjchem-792	329	5	,	,	PUNCT
eurjchem-792	329	6	105	105	NUM
eurjchem-792	329	7	,	,	PUNCT
eurjchem-792	329	8	559‐592	559‐592	NUM
eurjchem-792	329	9	.	.	PUNCT
eurjchem-792	330	1	[	[	X
eurjchem-792	330	2	11	11	NUM
eurjchem-792	330	3	]	]	PUNCT
eurjchem-792	330	4	.	.	PUNCT
eurjchem-792	330	5	garcia	garcia	PROPN
eurjchem-792	330	6	,	,	PUNCT
eurjchem-792	330	7	g.	g.	PROPN
eurjchem-792	330	8	f.	f.	PROPN
eurjchem-792	330	9	;	;	PUNCT
eurjchem-792	330	10	cercenado	cercenado	PROPN
eurjchem-792	330	11	,	,	PUNCT
eurjchem-792	330	12	e.	e.	PROPN
eurjchem-792	330	13	;	;	PUNCT
eurjchem-792	330	14	martin	martin	PROPN
eurjchem-792	330	15	,	,	PUNCT
eurjchem-792	330	16	p.	p.	PROPN
eurjchem-792	330	17	j.	j.	PROPN
eurjchem-792	330	18	;	;	PUNCT
eurjchem-792	330	19	cuevas	cuevas	PROPN
eurjchem-792	330	20	,	,	PUNCT
eurjchem-792	330	21	o.	o.	PROPN
eurjchem-792	330	22	;	;	PUNCT
eurjchem-792	330	23	bouza	bouza	PROPN
eurjchem-792	330	24	,	,	PUNCT
eurjchem-792	330	25	e.	e.	PROPN
eurjchem-792	330	26	j.	j.	PROPN
eurjchem-792	330	27	antimicrob	antimicrob	PROPN
eurjchem-792	330	28	.	.	PUNCT
eurjchem-792	331	1	chemother	chemother	PROPN
eurjchem-792	331	2	.	.	PUNCT
eurjchem-792	332	1	2001	2001	NUM
eurjchem-792	332	2	,	,	PUNCT
eurjchem-792	332	3	47	47	NUM
eurjchem-792	332	4	,	,	PUNCT
eurjchem-792	332	5	681‐684	681‐684	NUM
eurjchem-792	332	6	.	.	PUNCT
eurjchem-792	333	1	[	[	X
eurjchem-792	333	2	12	12	NUM
eurjchem-792	333	3	]	]	PUNCT
eurjchem-792	333	4	.	.	PUNCT
eurjchem-792	334	1	kim	kim	PROPN
eurjchem-792	334	2	,	,	PUNCT
eurjchem-792	334	3	j.	j.	PROPN
eurjchem-792	334	4	h.	h.	PROPN
eurjchem-792	334	5	;	;	PUNCT
eurjchem-792	334	6	kang	kang	PROPN
eurjchem-792	334	7	,	,	PUNCT
eurjchem-792	334	8	j.	j.	PROPN
eurjchem-792	334	9	a.	a.	PROPN
eurjchem-792	334	10	;	;	PUNCT
eurjchem-792	334	11	kim	kim	PROPN
eurjchem-792	334	12	,	,	PUNCT
eurjchem-792	334	13	y.	y.	PROPN
eurjchem-792	334	14	g.	g.	PROPN
eurjchem-792	334	15	;	;	PUNCT
eurjchem-792	334	16	kim	kim	PROPN
eurjchem-792	334	17	,	,	PUNCT
eurjchem-792	334	18	j.	j.	PROPN
eurjchem-792	334	19	w.	w.	PROPN
eurjchem-792	334	20	;	;	PUNCT
eurjchem-792	334	21	lee	lee	PROPN
eurjchem-792	334	22	,	,	PUNCT
eurjchem-792	334	23	j.	j.	PROPN
eurjchem-792	334	24	h.	h.	PROPN
eurjchem-792	334	25	;	;	PUNCT
eurjchem-792	334	26	kim	kim	PROPN
eurjchem-792	334	27	,	,	PUNCT
eurjchem-792	334	28	b.	b.	PROPN
eurjchem-792	334	29	k.	k.	PROPN
eurjchem-792	334	30	antimicrob	antimicrob	PROPN
eurjchem-792	334	31	.	.	PUNCT
eurjchem-792	335	1	agents	agents	PROPN
eurjchem-792	335	2	chemother	chemother	PROPN
eurjchem-792	335	3	.	.	PUNCT
eurjchem-792	336	1	1997	1997	NUM
eurjchem-792	336	2	,	,	PUNCT
eurjchem-792	336	3	41	41	NUM
eurjchem-792	336	4	,	,	PUNCT
eurjchem-792	336	5	2209‐2213	2209‐2213	NUM
eurjchem-792	336	6	.	.	PUNCT
eurjchem-792	337	1	[	[	X
eurjchem-792	337	2	13	13	NUM
eurjchem-792	337	3	]	]	PUNCT
eurjchem-792	337	4	.	.	PUNCT
eurjchem-792	338	1	meena	meena	PROPN
eurjchem-792	338	2	,	,	PUNCT
eurjchem-792	338	3	c.	c.	PROPN
eurjchem-792	338	4	j.	j.	PROPN
eurjchem-792	338	5	pharm	pharm	PROPN
eurjchem-792	338	6	.	.	PUNCT
eurjchem-792	339	1	res	re	NOUN
eurjchem-792	339	2	.	.	PROPN
eurjchem-792	339	3	2012	2012	NUM
eurjchem-792	339	4	,	,	PUNCT
eurjchem-792	339	5	25	25	NUM
eurjchem-792	339	6	,	,	PUNCT
eurjchem-792	339	7	324‐326	324‐326	NUM
eurjchem-792	339	8	.	.	PUNCT
eurjchem-792	340	1	[	[	X
eurjchem-792	340	2	14	14	NUM
eurjchem-792	340	3	]	]	PUNCT
eurjchem-792	340	4	.	.	PUNCT
eurjchem-792	341	1	huang	huang	PROPN
eurjchem-792	341	2	,	,	PUNCT
eurjchem-792	341	3	w.	w.	PROPN
eurjchem-792	341	4	;	;	PUNCT
eurjchem-792	341	5	zhao	zhao	PROPN
eurjchem-792	341	6	,	,	PUNCT
eurjchem-792	341	7	p.	p.	PROPN
eurjchem-792	341	8	l.	l.	PROPN
eurjchem-792	341	9	;	;	PUNCT
eurjchem-792	341	10	liu	liu	PROPN
eurjchem-792	341	11	,	,	PUNCT
eurjchem-792	341	12	c.	c.	PROPN
eurjchem-792	341	13	l.	l.	PROPN
eurjchem-792	341	14	;	;	PUNCT
eurjchem-792	341	15	chen	chen	PROPN
eurjchem-792	341	16	,	,	PUNCT
eurjchem-792	341	17	q.	q.	PROPN
eurjchem-792	341	18	;	;	PUNCT
eurjchem-792	341	19	liu	liu	PROPN
eurjchem-792	341	20	,	,	PUNCT
eurjchem-792	341	21	z.	z.	PROPN
eurjchem-792	341	22	m.	m.	PROPN
eurjchem-792	341	23	;	;	PUNCT
eurjchem-792	341	24	yang	yang	PROPN
eurjchem-792	341	25	,	,	PUNCT
eurjchem-792	341	26	g.	g.	PROPN
eurjchem-792	341	27	f.	f.	PROPN
eurjchem-792	341	28	j.	j.	PROPN
eurjchem-792	341	29	agr	agr	PROPN
eurjchem-792	341	30	.	.	PUNCT
eurjchem-792	342	1	food	food	NOUN
eurjchem-792	342	2	chem	chem	NOUN
eurjchem-792	342	3	.	.	PUNCT
eurjchem-792	343	1	2007	2007	NUM
eurjchem-792	343	2	,	,	PUNCT
eurjchem-792	343	3	55	55	NUM
eurjchem-792	343	4	,	,	PUNCT
eurjchem-792	343	5	3004‐3010	3004‐3010	NUM
eurjchem-792	343	6	.	.	PUNCT
eurjchem-792	344	1	[	[	X
eurjchem-792	344	2	15	15	NUM
eurjchem-792	344	3	]	]	PUNCT
eurjchem-792	344	4	.	.	PUNCT
eurjchem-792	345	1	john	john	PROPN
eurjchem-792	345	2	,	,	PUNCT
eurjchem-792	345	3	r.	r.	PROPN
eurjchem-792	345	4	p.	p.	PROPN
eurjchem-792	345	5	;	;	PUNCT
eurjchem-792	345	6	maurizio	maurizio	PROPN
eurjchem-792	345	7	,	,	PUNCT
eurjchem-792	345	8	d.	d.	PROPN
eurjchem-792	345	9	p.	p.	PROPN
eurjchem-792	345	10	;	;	PUNCT
eurjchem-792	345	11	wiley	wiley	PROPN
eurjchem-792	345	12	,	,	PUNCT
eurjchem-792	345	13	a.	a.	NOUN
eurjchem-792	345	14	;	;	PUNCT
eurjchem-792	345	15	schell	schell	PROPN
eurjchem-792	345	16	,	,	PUNCT
eurjchem-792	345	17	r.	r.	PROPN
eurjchem-792	345	18	r.	r.	PROPN
eurjchem-792	345	19	antimicrob	antimicrob	PROPN
eurjchem-792	345	20	.	.	PUNCT
eurjchem-792	346	1	agents	agents	PROPN
eurjchem-792	346	2	chemother	chemother	PROPN
eurjchem-792	346	3	.	.	PUNCT
eurjchem-792	347	1	1998	1998	NUM
eurjchem-792	347	2	,	,	PUNCT
eurjchem-792	347	3	42	42	NUM
eurjchem-792	347	4	,	,	PUNCT
eurjchem-792	347	5	2503‐2510	2503‐2510	NUM
eurjchem-792	347	6	.	.	PUNCT
eurjchem-792	348	1	[	[	X
eurjchem-792	348	2	16	16	NUM
eurjchem-792	348	3	]	]	PUNCT
eurjchem-792	348	4	.	.	PUNCT
eurjchem-792	349	1	barbara	barbara	PROPN
eurjchem-792	349	2	,	,	PUNCT
eurjchem-792	349	3	g	g	PROPN
eurjchem-792	349	4	;	;	PUNCT
eurjchem-792	349	5	tatiana	tatiana	PROPN
eurjchem-792	349	6	,	,	PUNCT
eurjchem-792	349	7	f.	f.	PROPN
eurjchem-792	349	8	;	;	PUNCT
eurjchem-792	349	9	thomas	thomas	PROPN
eurjchem-792	349	10	,	,	PUNCT
eurjchem-792	349	11	l.	l.	PROPN
eurjchem-792	349	12	g.	g.	PROPN
eurjchem-792	349	13	bioorg	bioorg	PROPN
eurjchem-792	349	14	.	.	PUNCT
eurjchem-792	350	1	med	med	PROPN
eurjchem-792	350	2	.	.	PROPN
eurjchem-792	350	3	chem	chem	PROPN
eurjchem-792	350	4	.	.	PUNCT
eurjchem-792	350	5	,	,	PUNCT
eurjchem-792	350	6	2004	2004	NUM
eurjchem-792	350	7	,	,	PUNCT
eurjchem-792	350	8	12	12	NUM
eurjchem-792	350	9	,	,	PUNCT
eurjchem-792	350	10	103‐112	103‐112	PROPN
eurjchem-792	350	11	.	.	PUNCT
eurjchem-792	351	1	[	[	X
eurjchem-792	351	2	17	17	NUM
eurjchem-792	351	3	]	]	PUNCT
eurjchem-792	351	4	.	.	PUNCT
eurjchem-792	352	1	campbell	campbell	PROPN
eurjchem-792	352	2	,	,	PUNCT
eurjchem-792	352	3	m.	m.	PROPN
eurjchem-792	352	4	j.	j.	PROPN
eurjchem-792	352	5	m.	m.	PROPN
eurjchem-792	352	6	;	;	PUNCT
eurjchem-792	352	7	grzeskowiak	grzeskowiak	PROPN
eurjchem-792	352	8	,	,	PUNCT
eurjchem-792	352	9	r.	r.	PROPN
eurjchem-792	352	10	;	;	PUNCT
eurjchem-792	352	11	juneja	juneja	PROPN
eurjchem-792	352	12	,	,	PUNCT
eurjchem-792	352	13	g.	g.	PROPN
eurjchem-792	352	14	s.	s.	PROPN
eurjchem-792	352	15	j.	j.	PROPN
eurjchem-792	352	16	inorg	inorg	PROPN
eurjchem-792	352	17	.	.	PUNCT
eurjchem-792	353	1	nucl	nucl	PROPN
eurjchem-792	353	2	.	.	PUNCT
eurjchem-792	354	1	chem	chem	PROPN
eurjchem-792	354	2	.	.	PUNCT
eurjchem-792	355	1	1978	1978	NUM
eurjchem-792	355	2	,	,	PUNCT
eurjchem-792	355	3	40	40	NUM
eurjchem-792	355	4	,	,	PUNCT
eurjchem-792	355	5	1507‐1511	1507‐1511	NUM
eurjchem-792	355	6	.	.	PUNCT
eurjchem-792	356	1	[	[	X
eurjchem-792	356	2	18	18	NUM
eurjchem-792	356	3	]	]	SYM
eurjchem-792	356	4	.	.	PUNCT
eurjchem-792	357	1	ono	ono	PROPN
eurjchem-792	357	2	,	,	PUNCT
eurjchem-792	357	3	k.	k.	PROPN
eurjchem-792	357	4	;	;	PUNCT
eurjchem-792	357	5	yoshida	yoshida	PROPN
eurjchem-792	357	6	,	,	PUNCT
eurjchem-792	357	7	a.	a.	PROPN
eurjchem-792	357	8	;	;	PUNCT
eurjchem-792	357	9	saito	saito	PROPN
eurjchem-792	357	10	,	,	PUNCT
eurjchem-792	357	11	n.	n.	NOUN
eurjchem-792	357	12	;	;	PUNCT
eurjchem-792	357	13	fujishima	fujishima	PROPN
eurjchem-792	357	14	,	,	PUNCT
eurjchem-792	357	15	t.	t.	PROPN
eurjchem-792	357	16	;	;	PUNCT
eurjchem-792	357	17	honzawa	honzawa	PROPN
eurjchem-792	357	18	,	,	PUNCT
eurjchem-792	357	19	s.	s.	PROPN
eurjchem-792	357	20	;	;	PUNCT
eurjchem-792	357	21	suhara	suhara	NOUN
eurjchem-792	357	22	,	,	PUNCT
eurjchem-792	357	23	y.	y.	PROPN
eurjchem-792	357	24	;	;	PUNCT
eurjchem-792	357	25	kishimoto	kishimoto	PROPN
eurjchem-792	357	26	,	,	PUNCT
eurjchem-792	357	27	s.	s.	PROPN
eurjchem-792	357	28	;	;	PUNCT
eurjchem-792	357	29	sugiura	sugiura	NOUN
eurjchem-792	357	30	,	,	PUNCT
eurjchem-792	357	31	t.	t.	PROPN
eurjchem-792	357	32	;	;	PUNCT
eurjchem-792	357	33	waku	waku	PROPN
eurjchem-792	357	34	,	,	PUNCT
eurjchem-792	357	35	k.	k.	PROPN
eurjchem-792	357	36	;	;	PUNCT
eurjchem-792	357	37	takayama	takayama	PROPN
eurjchem-792	357	38	,	,	PUNCT
eurjchem-792	357	39	h.	h.	PROPN
eurjchem-792	357	40	;	;	PUNCT
eurjchem-792	357	41	kittaka	kittaka	PROPN
eurjchem-792	357	42	,	,	PUNCT
eurjchem-792	357	43	a.	a.	PROPN
eurjchem-792	357	44	j.	j.	PROPN
eurjchem-792	357	45	org	org	PROPN
eurjchem-792	357	46	.	.	PUNCT
eurjchem-792	357	47	chem	chem	PROPN
eurjchem-792	357	48	.	.	PUNCT
eurjchem-792	358	1	2003	2003	NUM
eurjchem-792	358	2	,	,	PUNCT
eurjchem-792	358	3	68	68	NUM
eurjchem-792	358	4	,	,	PUNCT
eurjchem-792	358	5	7407‐7415	7407‐7415	NUM
eurjchem-792	358	6	.	.	PUNCT
eurjchem-792	359	1	[	[	X
eurjchem-792	359	2	19	19	NUM
eurjchem-792	359	3	]	]	PUNCT
eurjchem-792	359	4	.	.	PUNCT
eurjchem-792	360	1	villanova	villanova	PROPN
eurjchem-792	360	2	,	,	PUNCT
eurjchem-792	360	3	p.	p.	NOUN
eurjchem-792	360	4	a.	a.	NOUN
eurjchem-792	360	5	performance	performance	NOUN
eurjchem-792	360	6	standards	standard	NOUN
eurjchem-792	360	7	for	for	ADP
eurjchem-792	360	8	antimicrobial	antimicrobial	ADJ
eurjchem-792	360	9	disk	disk	NOUN
eurjchem-792	360	10	susceptibility	susceptibility	NOUN
eurjchem-792	360	11	tests	test	NOUN
eurjchem-792	360	12	,	,	PUNCT
eurjchem-792	360	13	5th	5th	ADJ
eurjchem-792	360	14	edition	edition	NOUN
eurjchem-792	360	15	,	,	PUNCT
eurjchem-792	360	16	approved	approve	VERB
eurjchem-792	360	17	standard	standard	ADJ
eurjchem-792	360	18	m7‐a5	m7‐a5	NOUN
eurjchem-792	360	19	,	,	PUNCT
eurjchem-792	360	20	nccls	nccls	NOUN
eurjchem-792	360	21	,	,	PUNCT
eurjchem-792	360	22	2000	2000	NUM
eurjchem-792	360	23	.	.	PUNCT
eurjchem-792	361	1	[	[	X
eurjchem-792	361	2	20	20	NUM
eurjchem-792	361	3	]	]	PUNCT
eurjchem-792	361	4	.	.	PUNCT
eurjchem-792	362	1	linday	linday	PROPN
eurjchem-792	362	2	,	,	PUNCT
eurjchem-792	362	3	m.	m.	NOUN
eurjchem-792	362	4	e.	e.	PROPN
eurjchem-792	362	5	practical	practical	ADJ
eurjchem-792	362	6	introduction	introduction	NOUN
eurjchem-792	362	7	to	to	ADP
eurjchem-792	362	8	microbiology	microbiology	NOUN
eurjchem-792	362	9	,	,	PUNCT
eurjchem-792	362	10	e	e	PROPN
eurjchem-792	362	11	and	and	CCONJ
eurjchem-792	362	12	f.	f.	PROPN
eurjchem-792	362	13	n.	n.	PROPN
eurjchem-792	362	14	spon	spon	PROPN
eurjchem-792	362	15	ltd	ltd	PROPN
eurjchem-792	362	16	.	.	PROPN
eurjchem-792	362	17	,	,	PUNCT
eurjchem-792	362	18	united	united	PROPN
eurjchem-792	362	19	kingdom	kingdom	PROPN
eurjchem-792	362	20	,	,	PUNCT
eurjchem-792	362	21	1962	1962	NUM
eurjchem-792	362	22	.	.	PUNCT
eurjchem-792	363	1	[	[	X
eurjchem-792	363	2	21	21	NUM
eurjchem-792	363	3	]	]	PUNCT
eurjchem-792	363	4	.	.	PUNCT
eurjchem-792	364	1	hayakawa	hayakawa	PROPN
eurjchem-792	364	2	,	,	PUNCT
eurjchem-792	364	3	i.	i.	PROPN
eurjchem-792	364	4	;	;	PUNCT
eurjchem-792	364	5	hiramitsu	hiramitsu	ADJ
eurjchem-792	364	6	,	,	PUNCT
eurjchem-792	364	7	t.	t.	PROPN
eurjchem-792	364	8	;	;	PUNCT
eurjchem-792	364	9	tanaka	tanaka	PROPN
eurjchem-792	364	10	,	,	PUNCT
eurjchem-792	364	11	y.	y.	PROPN
eurjchem-792	364	12	chem	chem	PROPN
eurjchem-792	364	13	.	.	PUNCT
eurjchem-792	365	1	pharm	pharm	NOUN
eurjchem-792	365	2	.	.	PUNCT
eurjchem-792	366	1	bull	bull	PROPN
eurjchem-792	366	2	.	.	PUNCT
eurjchem-792	367	1	1984	1984	NUM
eurjchem-792	367	2	,	,	PUNCT
eurjchem-792	367	3	32	32	NUM
eurjchem-792	367	4	,	,	PUNCT
eurjchem-792	367	5	4907‐4913	4907‐4913	NUM
eurjchem-792	367	6	.	.	PUNCT