id	sid	tid	token	lemma	pos
eurjchem-843	1	1	untitled	untitle	VERB
eurjchem-843	1	2	european	european	PROPN
eurjchem-843	1	3	journal	journal	PROPN
eurjchem-843	1	4	of	of	ADP
eurjchem-843	1	5	chemistry	chemistry	NOUN
eurjchem-843	1	6	4	4	NUM
eurjchem-843	1	7	(	(	PUNCT
eurjchem-843	1	8	4	4	NUM
eurjchem-843	1	9	)	)	PUNCT
eurjchem-843	1	10	(	(	PUNCT
eurjchem-843	1	11	2013	2013	NUM
eurjchem-843	1	12	)	)	PUNCT
eurjchem-843	1	13	360‐365	360‐365	NUM
eurjchem-843	1	14	european	european	ADJ
eurjchem-843	1	15	journal	journal	PROPN
eurjchem-843	1	16	of	of	ADP
eurjchem-843	1	17	chemistry	chemistry	NOUN
eurjchem-843	1	18	issn	issn	PROPN
eurjchem-843	1	19	2153‐2249	2153‐2249	PROPN
eurjchem-843	1	20	(	(	PUNCT
eurjchem-843	1	21	print	print	NOUN
eurjchem-843	1	22	)	)	PUNCT
eurjchem-843	1	23	/	/	SYM
eurjchem-843	1	24	issn	issn	PROPN
eurjchem-843	1	25	2153‐2257	2153‐2257	NUM
eurjchem-843	1	26	(	(	PUNCT
eurjchem-843	1	27	online	online	ADJ
eurjchem-843	1	28	)	)	PUNCT
eurjchem-843	1	29			NOUN
eurjchem-843	1	30	2013	2013	NUM
eurjchem-843	1	31	eurjchem	eurjchem	PROPN
eurjchem-843	1	32	doi:10.5155	doi:10.5155	PROPN
eurjchem-843	1	33	/	/	SYM
eurjchem-843	1	34	eurjchem.4.4.360‐365.843	eurjchem.4.4.360‐365.843	PROPN
eurjchem-843	1	35	european	european	PROPN
eurjchem-843	1	36	journal	journal	PROPN
eurjchem-843	1	37	of	of	ADP
eurjchem-843	1	38	chemistry	chemistry	PROPN
eurjchem-843	1	39	journal	journal	PROPN
eurjchem-843	1	40	homepage	homepage	NOUN
eurjchem-843	1	41	:	:	PUNCT
eurjchem-843	1	42	www.eurjchem.com	www.eurjchem.com	X
eurjchem-843	1	43	simultaneous	simultaneous	ADJ
eurjchem-843	1	44	determination	determination	NOUN
eurjchem-843	1	45	of	of	ADP
eurjchem-843	1	46	sitagliptin	sitagliptin	NOUN
eurjchem-843	1	47	and	and	CCONJ
eurjchem-843	1	48	metformin	metformin	NOUN
eurjchem-843	1	49	in	in	ADP
eurjchem-843	1	50	ternary	ternary	ADJ
eurjchem-843	1	51	mixture	mixture	NOUN
eurjchem-843	1	52	with	with	ADP
eurjchem-843	1	53	sitagliptin	sitagliptin	NOUN
eurjchem-843	1	54	acid	acid	NOUN
eurjchem-843	1	55	degradation	degradation	NOUN
eurjchem-843	1	56	product	product	NOUN
eurjchem-843	1	57	ramzia	ramzia	PROPN
eurjchem-843	1	58	ismail	ismail	PROPN
eurjchem-843	1	59	el‐bagary	el‐bagary	PROPN
eurjchem-843	1	60	a	a	PROPN
eurjchem-843	1	61	,	,	PUNCT
eurjchem-843	1	62	ehab	ehab	PROPN
eurjchem-843	1	63	farouk	farouk	PROPN
eurjchem-843	1	64	elkady	elkady	PROPN
eurjchem-843	1	65	a	a	PROPN
eurjchem-843	1	66	,	,	PUNCT
eurjchem-843	1	67	and	and	CCONJ
eurjchem-843	1	68	bassam	bassam	PROPN
eurjchem-843	1	69	mahfouz	mahfouz	PROPN
eurjchem-843	1	70	ayoub	ayoub	PROPN
eurjchem-843	1	71	b	b	PROPN
eurjchem-843	1	72	,	,	PUNCT
eurjchem-843	1	73	*	*	PUNCT
eurjchem-843	1	74	a	a	DET
eurjchem-843	1	75	pharmaceutical	pharmaceutical	ADJ
eurjchem-843	1	76	chemistry	chemistry	NOUN
eurjchem-843	1	77	department	department	NOUN
eurjchem-843	1	78	,	,	PUNCT
eurjchem-843	1	79	faculty	faculty	NOUN
eurjchem-843	1	80	of	of	ADP
eurjchem-843	1	81	pharmacy	pharmacy	NOUN
eurjchem-843	1	82	,	,	PUNCT
eurjchem-843	1	83	cairo	cairo	PROPN
eurjchem-843	1	84	university	university	PROPN
eurjchem-843	1	85	,	,	PUNCT
eurjchem-843	1	86	cairo	cairo	PROPN
eurjchem-843	1	87	11562	11562	NUM
eurjchem-843	1	88	,	,	PUNCT
eurjchem-843	1	89	egypt	egypt	PROPN
eurjchem-843	1	90	b	b	PROPN
eurjchem-843	1	91	pharmaceutical	pharmaceutical	ADJ
eurjchem-843	1	92	chemistry	chemistry	NOUN
eurjchem-843	1	93	department	department	NOUN
eurjchem-843	1	94	,	,	PUNCT
eurjchem-843	1	95	faculty	faculty	NOUN
eurjchem-843	1	96	of	of	ADP
eurjchem-843	1	97	pharmacy	pharmacy	NOUN
eurjchem-843	1	98	,	,	PUNCT
eurjchem-843	1	99	british	british	ADJ
eurjchem-843	1	100	university	university	PROPN
eurjchem-843	1	101	in	in	ADP
eurjchem-843	1	102	egypt	egypt	PROPN
eurjchem-843	1	103	,	,	PUNCT
eurjchem-843	1	104	el‐sherouk	el‐sherouk	PROPN
eurjchem-843	1	105	,	,	PUNCT
eurjchem-843	1	106	cairo	cairo	PROPN
eurjchem-843	1	107	11837	11837	NUM
eurjchem-843	1	108	,	,	PUNCT
eurjchem-843	1	109	egypt	egypt	PROPN
eurjchem-843	1	110	*	*	PUNCT
eurjchem-843	1	111	corresponding	correspond	VERB
eurjchem-843	1	112	author	author	NOUN
eurjchem-843	1	113	at	at	ADP
eurjchem-843	1	114	:	:	PUNCT
eurjchem-843	1	115	pharmaceutical	pharmaceutical	ADJ
eurjchem-843	1	116	chemistry	chemistry	NOUN
eurjchem-843	1	117	department	department	NOUN
eurjchem-843	1	118	,	,	PUNCT
eurjchem-843	1	119	faculty	faculty	NOUN
eurjchem-843	1	120	of	of	ADP
eurjchem-843	1	121	pharmacy	pharmacy	NOUN
eurjchem-843	1	122	,	,	PUNCT
eurjchem-843	1	123	british	british	ADJ
eurjchem-843	1	124	university	university	PROPN
eurjchem-843	1	125	in	in	ADP
eurjchem-843	1	126	egypt	egypt	PROPN
eurjchem-843	1	127	,	,	PUNCT
eurjchem-843	1	128	el‐sherouk	el‐sherouk	PROPN
eurjchem-843	1	129	,	,	PUNCT
eurjchem-843	1	130	cairo	cairo	PROPN
eurjchem-843	1	131	11837	11837	NUM
eurjchem-843	1	132	,	,	PUNCT
eurjchem-843	1	133	egypt	egypt	PROPN
eurjchem-843	1	134	.	.	PUNCT
eurjchem-843	2	1	tel	tel	PROPN
eurjchem-843	2	2	.	.	PUNCT
eurjchem-843	2	3	:	:	PUNCT
eurjchem-843	3	1	+2.012.25104337	+2.012.25104337	ADJ
eurjchem-843	3	2	;	;	PUNCT
eurjchem-843	3	3	fax	fax	NOUN
eurjchem-843	3	4	:	:	PUNCT
eurjchem-843	3	5	+2.022.4148452	+2.022.4148452	PROPN
eurjchem-843	3	6	.	.	PUNCT
eurjchem-843	3	7	e‐mail	e‐mail	PUNCT
eurjchem-843	4	1	address	address	NOUN
eurjchem-843	4	2	:	:	PUNCT
eurjchem-843	4	3	bassam.ayoub@bue.edu.eg	bassam.ayoub@bue.edu.eg	PROPN
eurjchem-843	4	4	(	(	PUNCT
eurjchem-843	4	5	b.m	b.m	PROPN
eurjchem-843	4	6	.	.	PROPN
eurjchem-843	4	7	ayoub	ayoub	PROPN
eurjchem-843	4	8	)	)	PUNCT
eurjchem-843	4	9	.	.	PUNCT
eurjchem-843	5	1	article	article	NOUN
eurjchem-843	5	2	information	information	PROPN
eurjchem-843	5	3	abstract	abstract	ADV
eurjchem-843	5	4	received	receive	VERB
eurjchem-843	5	5	:	:	PUNCT
eurjchem-843	5	6	04	04	NUM
eurjchem-843	5	7	june	june	PROPN
eurjchem-843	5	8	2013	2013	NUM
eurjchem-843	5	9	received	receive	VERB
eurjchem-843	5	10	in	in	ADP
eurjchem-843	5	11	revised	revise	VERB
eurjchem-843	5	12	form	form	NOUN
eurjchem-843	5	13	:	:	PUNCT
eurjchem-843	5	14	28	28	NUM
eurjchem-843	5	15	june	june	PROPN
eurjchem-843	5	16	2013	2013	NUM
eurjchem-843	5	17	accepted	accept	VERB
eurjchem-843	5	18	:	:	PUNCT
eurjchem-843	5	19	05	05	NUM
eurjchem-843	5	20	july	july	PROPN
eurjchem-843	5	21	2013	2013	NUM
eurjchem-843	5	22	online	online	NOUN
eurjchem-843	5	23	:	:	PUNCT
eurjchem-843	5	24	31	31	NUM
eurjchem-843	5	25	december	december	PROPN
eurjchem-843	5	26	2013	2013	NUM
eurjchem-843	5	27	keywords	keyword	NOUN
eurjchem-843	5	28	in	in	ADP
eurjchem-843	5	29	this	this	DET
eurjchem-843	5	30	work	work	NOUN
eurjchem-843	5	31	,	,	PUNCT
eurjchem-843	5	32	the	the	DET
eurjchem-843	5	33	acidic	acidic	ADJ
eurjchem-843	5	34	degradation	degradation	NOUN
eurjchem-843	5	35	product	product	NOUN
eurjchem-843	5	36	of	of	ADP
eurjchem-843	5	37	sitagliptin	sitagliptin	NOUN
eurjchem-843	5	38	phosphate	phosphate	NOUN
eurjchem-843	5	39	monohydrate	monohydrate	NOUN
eurjchem-843	5	40	(	(	PUNCT
eurjchem-843	5	41	stg	stg	NOUN
eurjchem-843	5	42	)	)	PUNCT
eurjchem-843	5	43	was	be	AUX
eurjchem-843	5	44	synthesized	synthesize	VERB
eurjchem-843	5	45	,	,	PUNCT
eurjchem-843	5	46	separated	separate	VERB
eurjchem-843	5	47	and	and	CCONJ
eurjchem-843	5	48	its	its	PRON
eurjchem-843	5	49	structure	structure	NOUN
eurjchem-843	5	50	was	be	AUX
eurjchem-843	5	51	elucidated	elucidate	VERB
eurjchem-843	5	52	.	.	PUNCT
eurjchem-843	6	1	additionally	additionally	ADV
eurjchem-843	6	2	,	,	PUNCT
eurjchem-843	6	3	two	two	NUM
eurjchem-843	6	4	reversed‐phase	reversed‐phase	NOUN
eurjchem-843	6	5	liquid	liquid	ADJ
eurjchem-843	6	6	chromatographic	chromatographic	ADJ
eurjchem-843	6	7	(	(	PUNCT
eurjchem-843	6	8	rp‐lc	rp‐lc	NUM
eurjchem-843	6	9	)	)	PUNCT
eurjchem-843	6	10	methods	method	NOUN
eurjchem-843	6	11	have	have	AUX
eurjchem-843	6	12	been	be	AUX
eurjchem-843	6	13	developed	develop	VERB
eurjchem-843	6	14	for	for	ADP
eurjchem-843	6	15	the	the	DET
eurjchem-843	6	16	determination	determination	NOUN
eurjchem-843	6	17	of	of	ADP
eurjchem-843	6	18	stg	stg	PROPN
eurjchem-843	6	19	.	.	PUNCT
eurjchem-843	7	1	the	the	DET
eurjchem-843	7	2	first	first	ADJ
eurjchem-843	7	3	method	method	NOUN
eurjchem-843	7	4	comprised	comprise	VERB
eurjchem-843	7	5	the	the	DET
eurjchem-843	7	6	determination	determination	NOUN
eurjchem-843	7	7	of	of	ADP
eurjchem-843	7	8	stg	stg	PROPN
eurjchem-843	7	9	in	in	ADP
eurjchem-843	7	10	binary	binary	ADJ
eurjchem-843	7	11	mixture	mixture	NOUN
eurjchem-843	7	12	with	with	ADP
eurjchem-843	7	13	sitagliptin	sitagliptin	NOUN
eurjchem-843	7	14	acid	acid	NOUN
eurjchem-843	7	15	degradation	degradation	NOUN
eurjchem-843	7	16	product	product	NOUN
eurjchem-843	7	17	(	(	PUNCT
eurjchem-843	7	18	sdp	sdp	NOUN
eurjchem-843	7	19	)	)	PUNCT
eurjchem-843	7	20	in	in	ADP
eurjchem-843	7	21	laboratory	laboratory	NOUN
eurjchem-843	7	22	prepared	prepare	VERB
eurjchem-843	7	23	mixtures	mixture	NOUN
eurjchem-843	7	24	,	,	PUNCT
eurjchem-843	7	25	in	in	ADP
eurjchem-843	7	26	plasma	plasma	NOUN
eurjchem-843	7	27	and	and	CCONJ
eurjchem-843	7	28	in	in	ADP
eurjchem-843	7	29	dosage	dosage	NOUN
eurjchem-843	7	30	form	form	NOUN
eurjchem-843	7	31	.	.	PUNCT
eurjchem-843	8	1	this	this	DET
eurjchem-843	8	2	method	method	NOUN
eurjchem-843	8	3	was	be	AUX
eurjchem-843	8	4	based	base	VERB
eurjchem-843	8	5	on	on	ADP
eurjchem-843	8	6	isocratic	isocratic	ADJ
eurjchem-843	8	7	elution	elution	NOUN
eurjchem-843	8	8	using	use	VERB
eurjchem-843	8	9	a	a	DET
eurjchem-843	8	10	mobile	mobile	ADJ
eurjchem-843	8	11	phase	phase	NOUN
eurjchem-843	8	12	consisting	consist	VERB
eurjchem-843	8	13	of	of	ADP
eurjchem-843	8	14	potassium	potassium	NOUN
eurjchem-843	8	15	dihydrogen	dihydrogen	NOUN
eurjchem-843	8	16	phosphate	phosphate	NOUN
eurjchem-843	8	17	buffer	buffer	NOUN
eurjchem-843	8	18	(	(	PUNCT
eurjchem-843	8	19	ph	ph	NOUN
eurjchem-843	8	20	=	=	NOUN
eurjchem-843	8	21	4.6	4.6	NUM
eurjchem-843	8	22	)	)	PUNCT
eurjchem-843	8	23	‐	‐	ADJ
eurjchem-843	8	24	acetonitrile	acetonitrile	NOUN
eurjchem-843	8	25	(	(	PUNCT
eurjchem-843	8	26	30:70	30:70	NUM
eurjchem-843	8	27	,	,	PUNCT
eurjchem-843	8	28	v	v	NOUN
eurjchem-843	8	29	:	:	SYM
eurjchem-843	8	30	v	v	NOUN
eurjchem-843	8	31	)	)	PUNCT
eurjchem-843	8	32	with	with	ADP
eurjchem-843	8	33	fluorometric	fluorometric	ADJ
eurjchem-843	8	34	detection	detection	NOUN
eurjchem-843	8	35	.	.	PUNCT
eurjchem-843	9	1	the	the	DET
eurjchem-843	9	2	fluorometric	fluorometric	ADJ
eurjchem-843	9	3	detector	detector	NOUN
eurjchem-843	9	4	was	be	AUX
eurjchem-843	9	5	operated	operate	VERB
eurjchem-843	9	6	at	at	ADP
eurjchem-843	9	7	267	267	NUM
eurjchem-843	9	8	nm	nm	NOUN
eurjchem-843	9	9	for	for	ADP
eurjchem-843	9	10	excitation	excitation	NOUN
eurjchem-843	9	11	and	and	CCONJ
eurjchem-843	9	12	575	575	NUM
eurjchem-843	9	13	nm	nm	NOUN
eurjchem-843	9	14	for	for	ADP
eurjchem-843	9	15	emission	emission	NOUN
eurjchem-843	9	16	.	.	PUNCT
eurjchem-843	10	1	in	in	ADP
eurjchem-843	10	2	the	the	DET
eurjchem-843	10	3	second	second	ADJ
eurjchem-843	10	4	method	method	NOUN
eurjchem-843	10	5	,	,	PUNCT
eurjchem-843	10	6	the	the	DET
eurjchem-843	10	7	simultaneous	simultaneous	ADJ
eurjchem-843	10	8	determination	determination	NOUN
eurjchem-843	10	9	of	of	ADP
eurjchem-843	10	10	stg	stg	PROPN
eurjchem-843	10	11	and	and	CCONJ
eurjchem-843	10	12	metformin	metformin	PROPN
eurjchem-843	10	13	(	(	PUNCT
eurjchem-843	10	14	met	meet	VERB
eurjchem-843	10	15	)	)	PUNCT
eurjchem-843	10	16	in	in	ADP
eurjchem-843	10	17	the	the	DET
eurjchem-843	10	18	presence	presence	NOUN
eurjchem-843	10	19	of	of	ADP
eurjchem-843	10	20	sdp	sdp	NOUN
eurjchem-843	10	21	has	have	AUX
eurjchem-843	10	22	been	be	AUX
eurjchem-843	10	23	developed	develop	VERB
eurjchem-843	10	24	.	.	PUNCT
eurjchem-843	11	1	in	in	ADP
eurjchem-843	11	2	this	this	DET
eurjchem-843	11	3	method	method	NOUN
eurjchem-843	11	4	,	,	PUNCT
eurjchem-843	11	5	the	the	DET
eurjchem-843	11	6	ternary	ternary	ADJ
eurjchem-843	11	7	mixture	mixture	NOUN
eurjchem-843	11	8	of	of	ADP
eurjchem-843	11	9	stg	stg	PROPN
eurjchem-843	11	10	,	,	PUNCT
eurjchem-843	11	11	met	meet	VERB
eurjchem-843	11	12	and	and	CCONJ
eurjchem-843	11	13	sdp	sdp	NOUN
eurjchem-843	11	14	was	be	AUX
eurjchem-843	11	15	separated	separate	VERB
eurjchem-843	11	16	using	use	VERB
eurjchem-843	11	17	a	a	DET
eurjchem-843	11	18	mobile	mobile	ADJ
eurjchem-843	11	19	phase	phase	NOUN
eurjchem-843	11	20	consisting	consist	VERB
eurjchem-843	11	21	of	of	ADP
eurjchem-843	11	22	potassium	potassium	NOUN
eurjchem-843	11	23	dihydrogen	dihydrogen	NOUN
eurjchem-843	11	24	phosphate	phosphate	NOUN
eurjchem-843	11	25	buffer	buffer	NOUN
eurjchem-843	11	26	(	(	PUNCT
eurjchem-843	11	27	ph	ph	NOUN
eurjchem-843	11	28	=	=	NOUN
eurjchem-843	11	29	4.6	4.6	NUM
eurjchem-843	11	30	)	)	PUNCT
eurjchem-843	11	31	‐	‐	ADJ
eurjchem-843	11	32	acetonitrile	acetonitrile	NOUN
eurjchem-843	11	33	(	(	PUNCT
eurjchem-843	11	34	15:85	15:85	NUM
eurjchem-843	11	35	,	,	PUNCT
eurjchem-843	11	36	v	v	NOUN
eurjchem-843	11	37	:	:	SYM
eurjchem-843	11	38	v	v	NOUN
eurjchem-843	11	39	)	)	PUNCT
eurjchem-843	11	40	with	with	ADP
eurjchem-843	11	41	uv	uv	NOUN
eurjchem-843	11	42	detection	detection	NOUN
eurjchem-843	11	43	at	at	ADP
eurjchem-843	11	44	220	220	NUM
eurjchem-843	11	45	nm	nm	NOUN
eurjchem-843	11	46	.	.	PUNCT
eurjchem-843	12	1	chromatographic	chromatographic	ADJ
eurjchem-843	12	2	separation	separation	NOUN
eurjchem-843	12	3	in	in	ADP
eurjchem-843	12	4	the	the	DET
eurjchem-843	12	5	two	two	NUM
eurjchem-843	12	6	methods	method	NOUN
eurjchem-843	12	7	was	be	AUX
eurjchem-843	12	8	achieved	achieve	VERB
eurjchem-843	12	9	on	on	ADP
eurjchem-843	12	10	a	a	DET
eurjchem-843	12	11	symmetry	symmetry	NOUN
eurjchem-843	12	12	®	®	NOUN
eurjchem-843	12	13	waters	water	VERB
eurjchem-843	12	14	c18	c18	NOUN
eurjchem-843	12	15	column	column	NOUN
eurjchem-843	12	16	(	(	PUNCT
eurjchem-843	12	17	150	150	NUM
eurjchem-843	12	18	mm	mm	NOUN
eurjchem-843	12	19	×	×	NOUN
eurjchem-843	12	20	4.6	4.6	NUM
eurjchem-843	12	21	mm	mm	NOUN
eurjchem-843	12	22	,	,	PUNCT
eurjchem-843	12	23	5	5	NUM
eurjchem-843	12	24	μm	μm	NUM
eurjchem-843	12	25	)	)	PUNCT
eurjchem-843	12	26	.	.	PUNCT
eurjchem-843	13	1	the	the	DET
eurjchem-843	13	2	optimized	optimize	VERB
eurjchem-843	13	3	methods	method	NOUN
eurjchem-843	13	4	were	be	AUX
eurjchem-843	13	5	validated	validate	VERB
eurjchem-843	13	6	and	and	CCONJ
eurjchem-843	13	7	proved	prove	VERB
eurjchem-843	13	8	to	to	PART
eurjchem-843	13	9	be	be	AUX
eurjchem-843	13	10	specific	specific	ADJ
eurjchem-843	13	11	,	,	PUNCT
eurjchem-843	13	12	robust	robust	ADJ
eurjchem-843	13	13	and	and	CCONJ
eurjchem-843	13	14	accurate	accurate	ADJ
eurjchem-843	13	15	for	for	ADP
eurjchem-843	13	16	the	the	DET
eurjchem-843	13	17	quality	quality	NOUN
eurjchem-843	13	18	control	control	NOUN
eurjchem-843	13	19	of	of	ADP
eurjchem-843	13	20	the	the	DET
eurjchem-843	13	21	cited	cite	VERB
eurjchem-843	13	22	drugs	drug	NOUN
eurjchem-843	13	23	in	in	ADP
eurjchem-843	13	24	pharmaceutical	pharmaceutical	ADJ
eurjchem-843	13	25	preparations	preparation	NOUN
eurjchem-843	13	26	.	.	PUNCT
eurjchem-843	14	1	metformin	metformin	NOUN
eurjchem-843	14	2	sitagliptin	sitagliptin	PROPN
eurjchem-843	14	3	phosphate	phosphate	NOUN
eurjchem-843	14	4	stability	stability	NOUN
eurjchem-843	14	5	indicating	indicate	VERB
eurjchem-843	14	6	assay	assay	ADJ
eurjchem-843	14	7	pharmaceutical	pharmaceutical	ADJ
eurjchem-843	14	8	preparation	preparation	NOUN
eurjchem-843	14	9	sitagliptin	sitagliptin	NOUN
eurjchem-843	14	10	degradation	degradation	NOUN
eurjchem-843	14	11	product	product	NOUN
eurjchem-843	14	12	reversed‐phase	reversed‐phase	NOUN
eurjchem-843	14	13	liquid	liquid	ADJ
eurjchem-843	14	14	chromatography	chromatography	NOUN
eurjchem-843	14	15	1	1	NUM
eurjchem-843	14	16	.	.	PUNCT
eurjchem-843	15	1	introduction	introduction	NOUN
eurjchem-843	15	2	sitagliptin	sitagliptin	NOUN
eurjchem-843	15	3	(	(	PUNCT
eurjchem-843	15	4	stg	stg	NOUN
eurjchem-843	15	5	)	)	PUNCT
eurjchem-843	15	6	,	,	PUNCT
eurjchem-843	16	1	[	[	X
eurjchem-843	16	2	(	(	PUNCT
eurjchem-843	16	3	2r)‐1‐(2,4,5‐trifluorophenyl)‐4‐oxo‐4‐	2r)‐1‐(2,4,5‐trifluorophenyl)‐4‐oxo‐4‐	NUM
eurjchem-843	16	4	[	[	X
eurjchem-843	16	5	3‐(trifluoromethyl)‐5,6‐dihydro	3‐(trifluoromethyl)‐5,6‐dihydro	PROPN
eurjchem-843	17	1	[	[	X
eurjchem-843	17	2	1,2,4]triazolo	1,2,4]triazolo	NUM
eurjchem-843	17	3	[	[	X
eurjchem-843	17	4	4,3‐a]pyrazin‐	4,3‐a]pyrazin‐	NUM
eurjchem-843	17	5	7(8h)‐yl	7(8h)‐yl	NUM
eurjchem-843	17	6	]	]	PUNCT
eurjchem-843	17	7	butan‐2‐amine	butan‐2‐amine	X
eurjchem-843	17	8	]	]	PUNCT
eurjchem-843	17	9	(	(	PUNCT
eurjchem-843	17	10	figure	figure	NOUN
eurjchem-843	17	11	1a	1a	NOUN
eurjchem-843	17	12	)	)	PUNCT
eurjchem-843	17	13	,	,	PUNCT
eurjchem-843	17	14	is	be	AUX
eurjchem-843	17	15	an	an	DET
eurjchem-843	17	16	hypoglycemic	hypoglycemic	ADJ
eurjchem-843	17	17	drug	drug	NOUN
eurjchem-843	17	18	that	that	PRON
eurjchem-843	17	19	belongs	belong	VERB
eurjchem-843	17	20	to	to	ADP
eurjchem-843	17	21	dipeptidyl‐peptidase‐4	dipeptidyl‐peptidase‐4	VERB
eurjchem-843	17	22	inhibitor	inhibitor	NOUN
eurjchem-843	17	23	class	class	NOUN
eurjchem-843	17	24	which	which	PRON
eurjchem-843	17	25	stimulates	stimulate	VERB
eurjchem-843	17	26	glucose‐dependent	glucose‐dependent	ADJ
eurjchem-843	17	27	insulin	insulin	NOUN
eurjchem-843	17	28	release	release	NOUN
eurjchem-843	17	29	[	[	X
eurjchem-843	17	30	1‐3	1‐3	NUM
eurjchem-843	17	31	]	]	PUNCT
eurjchem-843	17	32	.	.	PUNCT
eurjchem-843	18	1	metformin	metformin	NOUN
eurjchem-843	18	2	(	(	PUNCT
eurjchem-843	18	3	met	meet	VERB
eurjchem-843	18	4	)	)	PUNCT
eurjchem-843	18	5	,	,	PUNCT
eurjchem-843	18	6	n	n	CCONJ
eurjchem-843	18	7	,	,	PUNCT
eurjchem-843	18	8	n‐dimethylimidodicarbonimidic	n‐dimethylimidodicarbonimidic	X
eurjchem-843	18	9	diamide	diamide	PROPN
eurjchem-843	18	10	(	(	PUNCT
eurjchem-843	18	11	figure	figure	NOUN
eurjchem-843	18	12	1b	1b	NUM
eurjchem-843	18	13	)	)	PUNCT
eurjchem-843	18	14	,	,	PUNCT
eurjchem-843	18	15	is	be	AUX
eurjchem-843	18	16	a	a	DET
eurjchem-843	18	17	biguanide	biguanide	NOUN
eurjchem-843	18	18	drug	drug	NOUN
eurjchem-843	18	19	that	that	PRON
eurjchem-843	18	20	stimulates	stimulate	VERB
eurjchem-843	18	21	glycolysis	glycolysis	NOUN
eurjchem-843	18	22	in	in	ADP
eurjchem-843	18	23	peripheral	peripheral	ADJ
eurjchem-843	18	24	tissues	tissue	NOUN
eurjchem-843	18	25	[	[	X
eurjchem-843	18	26	4	4	NUM
eurjchem-843	18	27	]	]	PUNCT
eurjchem-843	18	28	.	.	PUNCT
eurjchem-843	19	1	recently	recently	ADV
eurjchem-843	19	2	,	,	PUNCT
eurjchem-843	19	3	the	the	DET
eurjchem-843	19	4	combination	combination	NOUN
eurjchem-843	19	5	of	of	ADP
eurjchem-843	19	6	the	the	DET
eurjchem-843	19	7	two	two	NUM
eurjchem-843	19	8	drugs	drug	NOUN
eurjchem-843	19	9	has	have	AUX
eurjchem-843	19	10	been	be	AUX
eurjchem-843	19	11	recommended	recommend	VERB
eurjchem-843	19	12	in	in	ADP
eurjchem-843	19	13	the	the	DET
eurjchem-843	19	14	treatment	treatment	NOUN
eurjchem-843	19	15	of	of	ADP
eurjchem-843	19	16	diabetes	diabetes	NOUN
eurjchem-843	19	17	mellitus	mellitus	NOUN
eurjchem-843	19	18	to	to	PART
eurjchem-843	19	19	improve	improve	VERB
eurjchem-843	19	20	glycemic	glycemic	ADJ
eurjchem-843	19	21	control	control	NOUN
eurjchem-843	20	1	[	[	X
eurjchem-843	20	2	5	5	NUM
eurjchem-843	20	3	]	]	PUNCT
eurjchem-843	20	4	.	.	PUNCT
eurjchem-843	21	1	a	a	DET
eurjchem-843	21	2	few	few	ADJ
eurjchem-843	21	3	methods	method	NOUN
eurjchem-843	21	4	have	have	AUX
eurjchem-843	21	5	been	be	AUX
eurjchem-843	21	6	described	describe	VERB
eurjchem-843	21	7	for	for	ADP
eurjchem-843	21	8	the	the	DET
eurjchem-843	21	9	determination	determination	NOUN
eurjchem-843	21	10	of	of	ADP
eurjchem-843	21	11	stg	stg	PROPN
eurjchem-843	21	12	in	in	ADP
eurjchem-843	21	13	pharmaceutical	pharmaceutical	ADJ
eurjchem-843	21	14	preparations	preparation	NOUN
eurjchem-843	21	15	including	include	VERB
eurjchem-843	21	16	spectro‐	spectro‐	NOUN
eurjchem-843	21	17	photometry	photometry	NOUN
eurjchem-843	21	18	[	[	X
eurjchem-843	21	19	1,6	1,6	NUM
eurjchem-843	21	20	]	]	PUNCT
eurjchem-843	21	21	,	,	PUNCT
eurjchem-843	21	22	hplc	hplc	NOUN
eurjchem-843	21	23	[	[	X
eurjchem-843	21	24	2,3,7	2,3,7	NUM
eurjchem-843	21	25	]	]	PUNCT
eurjchem-843	21	26	and	and	CCONJ
eurjchem-843	21	27	fluorometry	fluorometry	NOUN
eurjchem-843	22	1	[	[	X
eurjchem-843	22	2	8	8	NUM
eurjchem-843	22	3	]	]	PUNCT
eurjchem-843	22	4	.	.	PUNCT
eurjchem-843	23	1	besides	besides	SCONJ
eurjchem-843	23	2	,	,	PUNCT
eurjchem-843	23	3	some	some	DET
eurjchem-843	23	4	methods	method	NOUN
eurjchem-843	23	5	have	have	AUX
eurjchem-843	23	6	been	be	AUX
eurjchem-843	23	7	reported	report	VERB
eurjchem-843	23	8	for	for	ADP
eurjchem-843	23	9	determination	determination	NOUN
eurjchem-843	23	10	of	of	ADP
eurjchem-843	23	11	met	meet	VERB
eurjchem-843	23	12	in	in	ADP
eurjchem-843	23	13	pharmaceutical	pharmaceutical	ADJ
eurjchem-843	23	14	preparations	preparation	NOUN
eurjchem-843	23	15	including	include	VERB
eurjchem-843	23	16	lc	lc	PROPN
eurjchem-843	23	17	/	/	SYM
eurjchem-843	23	18	ms	ms	PROPN
eurjchem-843	23	19	/	/	SYM
eurjchem-843	23	20	ms	ms	NOUN
eurjchem-843	23	21	[	[	X
eurjchem-843	23	22	4	4	NUM
eurjchem-843	23	23	]	]	PUNCT
eurjchem-843	23	24	and	and	CCONJ
eurjchem-843	23	25	hplc	hplc	NOUN
eurjchem-843	23	26	[	[	X
eurjchem-843	23	27	9‐11	9‐11	X
eurjchem-843	23	28	]	]	PUNCT
eurjchem-843	23	29	.	.	PUNCT
eurjchem-843	24	1	in	in	ADP
eurjchem-843	24	2	a	a	DET
eurjchem-843	24	3	previous	previous	ADJ
eurjchem-843	24	4	work	work	NOUN
eurjchem-843	24	5	by	by	ADP
eurjchem-843	24	6	the	the	DET
eurjchem-843	24	7	same	same	ADJ
eurjchem-843	24	8	authors	author	NOUN
eurjchem-843	24	9	of	of	ADP
eurjchem-843	24	10	the	the	DET
eurjchem-843	24	11	present	present	ADJ
eurjchem-843	24	12	work	work	NOUN
eurjchem-843	24	13	[	[	X
eurjchem-843	24	14	7	7	NUM
eurjchem-843	24	15	]	]	PUNCT
eurjchem-843	24	16	,	,	PUNCT
eurjchem-843	24	17	the	the	DET
eurjchem-843	24	18	determination	determination	NOUN
eurjchem-843	24	19	of	of	ADP
eurjchem-843	24	20	stg	stg	PROPN
eurjchem-843	24	21	was	be	AUX
eurjchem-843	24	22	carried	carry	VERB
eurjchem-843	24	23	out	out	ADP
eurjchem-843	24	24	alone	alone	ADV
eurjchem-843	24	25	and	and	CCONJ
eurjchem-843	24	26	was	be	AUX
eurjchem-843	24	27	also	also	ADV
eurjchem-843	24	28	simultaneously	simultaneously	ADV
eurjchem-843	24	29	determined	determine	VERB
eurjchem-843	24	30	with	with	ADP
eurjchem-843	24	31	met	meet	VERB
eurjchem-843	24	32	in	in	ADP
eurjchem-843	24	33	the	the	DET
eurjchem-843	24	34	presence	presence	NOUN
eurjchem-843	24	35	of	of	ADP
eurjchem-843	24	36	stg	stg	PROPN
eurjchem-843	24	37	alkaline	alkaline	NOUN
eurjchem-843	24	38	degradation	degradation	NOUN
eurjchem-843	24	39	product	product	NOUN
eurjchem-843	24	40	(	(	PUNCT
eurjchem-843	24	41	sdp	sdp	NOUN
eurjchem-843	24	42	)	)	PUNCT
eurjchem-843	24	43	.	.	PUNCT
eurjchem-843	25	1	however	however	ADV
eurjchem-843	25	2	,	,	PUNCT
eurjchem-843	25	3	the	the	DET
eurjchem-843	25	4	acid	acid	NOUN
eurjchem-843	25	5	degradation	degradation	NOUN
eurjchem-843	25	6	of	of	ADP
eurjchem-843	25	7	stg	stg	PROPN
eurjchem-843	25	8	could	could	AUX
eurjchem-843	25	9	not	not	PART
eurjchem-843	25	10	be	be	AUX
eurjchem-843	25	11	separated	separate	VERB
eurjchem-843	25	12	.	.	PUNCT
eurjchem-843	26	1	so	so	ADV
eurjchem-843	26	2	,	,	PUNCT
eurjchem-843	26	3	the	the	DET
eurjchem-843	26	4	aim	aim	NOUN
eurjchem-843	26	5	of	of	ADP
eurjchem-843	26	6	the	the	DET
eurjchem-843	26	7	present	present	ADJ
eurjchem-843	26	8	work	work	NOUN
eurjchem-843	26	9	presents	present	NOUN
eurjchem-843	26	10	was	be	AUX
eurjchem-843	26	11	to	to	PART
eurjchem-843	26	12	synthesize	synthesize	VERB
eurjchem-843	26	13	,	,	PUNCT
eurjchem-843	26	14	separate	separate	ADJ
eurjchem-843	26	15	and	and	CCONJ
eurjchem-843	26	16	study	study	VERB
eurjchem-843	26	17	the	the	DET
eurjchem-843	26	18	acidic	acidic	ADJ
eurjchem-843	26	19	degradation	degradation	NOUN
eurjchem-843	26	20	product	product	NOUN
eurjchem-843	26	21	of	of	ADP
eurjchem-843	26	22	stg	stg	PROPN
eurjchem-843	26	23	and	and	CCONJ
eurjchem-843	26	24	to	to	PART
eurjchem-843	26	25	develop	develop	VERB
eurjchem-843	26	26	lc	lc	NOUN
eurjchem-843	26	27	methods	method	NOUN
eurjchem-843	26	28	for	for	ADP
eurjchem-843	26	29	the	the	DET
eurjchem-843	26	30	determination	determination	NOUN
eurjchem-843	26	31	of	of	ADP
eurjchem-843	26	32	stg	stg	PROPN
eurjchem-843	26	33	either	either	CCONJ
eurjchem-843	26	34	in	in	ADP
eurjchem-843	26	35	binary	binary	ADJ
eurjchem-843	26	36	mixture	mixture	NOUN
eurjchem-843	26	37	with	with	ADP
eurjchem-843	26	38	its	its	PRON
eurjchem-843	26	39	acidic	acidic	ADJ
eurjchem-843	26	40	degradation	degradation	NOUN
eurjchem-843	26	41	product	product	NOUN
eurjchem-843	26	42	(	(	PUNCT
eurjchem-843	26	43	sdp	sdp	NOUN
eurjchem-843	26	44	)	)	PUNCT
eurjchem-843	26	45	or	or	CCONJ
eurjchem-843	26	46	in	in	ADP
eurjchem-843	26	47	ternary	ternary	ADJ
eurjchem-843	26	48	mixture	mixture	NOUN
eurjchem-843	26	49	with	with	ADP
eurjchem-843	26	50	met	meet	VERB
eurjchem-843	26	51	and	and	CCONJ
eurjchem-843	26	52	sdp	sdp	NOUN
eurjchem-843	26	53	.	.	PUNCT
eurjchem-843	27	1	in	in	ADP
eurjchem-843	27	2	the	the	DET
eurjchem-843	27	3	first	first	ADJ
eurjchem-843	27	4	method	method	NOUN
eurjchem-843	27	5	(	(	PUNCT
eurjchem-843	27	6	lc‐fluoro	lc‐fluoro	PROPN
eurjchem-843	27	7	)	)	PUNCT
eurjchem-843	27	8	,	,	PUNCT
eurjchem-843	27	9	stg	stg	PROPN
eurjchem-843	27	10	and	and	CCONJ
eurjchem-843	27	11	sdp	sdp	NOUN
eurjchem-843	27	12	was	be	AUX
eurjchem-843	27	13	determined	determine	VERB
eurjchem-843	27	14	applying	apply	VERB
eurjchem-843	27	15	fluorometric	fluorometric	ADJ
eurjchem-843	27	16	detection	detection	NOUN
eurjchem-843	27	17	based	base	VERB
eurjchem-843	27	18	on	on	ADP
eurjchem-843	27	19	the	the	DET
eurjchem-843	27	20	native	native	ADJ
eurjchem-843	27	21	fluorescence	fluorescence	NOUN
eurjchem-843	27	22	of	of	ADP
eurjchem-843	27	23	the	the	DET
eurjchem-843	27	24	drug	drug	NOUN
eurjchem-843	27	25	and	and	CCONJ
eurjchem-843	27	26	the	the	DET
eurjchem-843	27	27	acidic	acidic	ADJ
eurjchem-843	27	28	degradation	degradation	NOUN
eurjchem-843	27	29	product	product	NOUN
eurjchem-843	27	30	.	.	PUNCT
eurjchem-843	28	1	fluorometric	fluorometric	ADJ
eurjchem-843	28	2	detection	detection	NOUN
eurjchem-843	28	3	was	be	AUX
eurjchem-843	28	4	chosen	choose	VERB
eurjchem-843	28	5	for	for	ADP
eurjchem-843	28	6	its	its	PRON
eurjchem-843	28	7	better	well	ADJ
eurjchem-843	28	8	selectivity	selectivity	NOUN
eurjchem-843	28	9	than	than	ADP
eurjchem-843	28	10	uv	uv	NOUN
eurjchem-843	28	11	detection	detection	NOUN
eurjchem-843	28	12	.	.	PUNCT
eurjchem-843	29	1	in	in	ADP
eurjchem-843	29	2	the	the	DET
eurjchem-843	29	3	second	second	ADJ
eurjchem-843	29	4	method	method	NOUN
eurjchem-843	29	5	(	(	PUNCT
eurjchem-843	29	6	lc‐uv	lc‐uv	NUM
eurjchem-843	29	7	)	)	PUNCT
eurjchem-843	29	8	,	,	PUNCT
eurjchem-843	29	9	uv	uv	NOUN
eurjchem-843	29	10	detection	detection	NOUN
eurjchem-843	29	11	was	be	AUX
eurjchem-843	29	12	applied	apply	VERB
eurjchem-843	29	13	for	for	ADP
eurjchem-843	29	14	the	the	DET
eurjchem-843	29	15	determination	determination	NOUN
eurjchem-843	29	16	of	of	ADP
eurjchem-843	29	17	the	the	DET
eurjchem-843	29	18	ternary	ternary	ADJ
eurjchem-843	29	19	mixture	mixture	NOUN
eurjchem-843	29	20	due	due	ADP
eurjchem-843	29	21	to	to	ADP
eurjchem-843	29	22	the	the	DET
eurjchem-843	29	23	lack	lack	NOUN
eurjchem-843	29	24	of	of	ADP
eurjchem-843	29	25	native	native	ADJ
eurjchem-843	29	26	fluorescence	fluorescence	NOUN
eurjchem-843	29	27	for	for	ADP
eurjchem-843	29	28	met	meet	VERB
eurjchem-843	29	29	.	.	PUNCT
eurjchem-843	30	1	sdp	sdp	PROPN
eurjchem-843	30	2	was	be	AUX
eurjchem-843	30	3	prepared	prepare	VERB
eurjchem-843	30	4	,	,	PUNCT
eurjchem-843	30	5	separated	separate	VERB
eurjchem-843	30	6	and	and	CCONJ
eurjchem-843	30	7	its	its	PRON
eurjchem-843	30	8	structure	structure	NOUN
eurjchem-843	30	9	was	be	AUX
eurjchem-843	30	10	elucidated	elucidate	VERB
eurjchem-843	30	11	by	by	ADP
eurjchem-843	30	12	different	different	ADJ
eurjchem-843	30	13	spectroscopic	spectroscopic	ADJ
eurjchem-843	30	14	techniques	technique	NOUN
eurjchem-843	30	15	and	and	CCONJ
eurjchem-843	30	16	proved	prove	VERB
eurjchem-843	30	17	to	to	PART
eurjchem-843	30	18	be	be	AUX
eurjchem-843	30	19	;	;	PUNCT
eurjchem-843	30	20	3‐amino‐	3‐amino‐	NUM
eurjchem-843	30	21	4‐(2,4,5‐trifluorophenyl	4‐(2,4,5‐trifluorophenyl	NUM
eurjchem-843	30	22	)	)	PUNCT
eurjchem-843	30	23	butanoic	butanoic	NOUN
eurjchem-843	30	24	acid	acid	NOUN
eurjchem-843	30	25	,	,	PUNCT
eurjchem-843	30	26	(	(	PUNCT
eurjchem-843	30	27	figure	figure	NOUN
eurjchem-843	30	28	1c	1c	NOUN
eurjchem-843	30	29	)	)	PUNCT
eurjchem-843	30	30	.	.	PUNCT
eurjchem-843	31	1	(	(	PUNCT
eurjchem-843	31	2	a	a	X
eurjchem-843	31	3	)	)	PUNCT
eurjchem-843	31	4	(	(	PUNCT
eurjchem-843	31	5	b	b	X
eurjchem-843	31	6	)	)	PUNCT
eurjchem-843	31	7	(	(	PUNCT
eurjchem-843	31	8	c	c	X
eurjchem-843	31	9	)	)	PUNCT
eurjchem-843	31	10	figure	figure	NOUN
eurjchem-843	31	11	1	1	NUM
eurjchem-843	31	12	.	.	PUNCT
eurjchem-843	32	1	chemical	chemical	NOUN
eurjchem-843	32	2	structures	structure	NOUN
eurjchem-843	32	3	of	of	ADP
eurjchem-843	32	4	sitagliptin	sitagliptin	NOUN
eurjchem-843	32	5	(	(	PUNCT
eurjchem-843	32	6	a	a	NOUN
eurjchem-843	32	7	)	)	PUNCT
eurjchem-843	32	8	,	,	PUNCT
eurjchem-843	32	9	metformin	metformin	NOUN
eurjchem-843	32	10	(	(	PUNCT
eurjchem-843	32	11	b	b	NOUN
eurjchem-843	32	12	)	)	PUNCT
eurjchem-843	32	13	and	and	CCONJ
eurjchem-843	32	14	sitagliptin	sitagliptin	VERB
eurjchem-843	32	15	acidic	acidic	ADJ
eurjchem-843	32	16	degradation	degradation	NOUN
eurjchem-843	32	17	product	product	NOUN
eurjchem-843	32	18	(	(	PUNCT
eurjchem-843	32	19	c	c	NOUN
eurjchem-843	32	20	)	)	PUNCT
eurjchem-843	32	21	.	.	PUNCT
eurjchem-843	33	1	el‐bagary	el‐bagary	PROPN
eurjchem-843	33	2	et	et	PROPN
eurjchem-843	33	3	al	al	PROPN
eurjchem-843	33	4	.	.	PUNCT
eurjchem-843	33	5	/	/	SYM
eurjchem-843	33	6	european	european	PROPN
eurjchem-843	33	7	journal	journal	PROPN
eurjchem-843	33	8	of	of	ADP
eurjchem-843	33	9	chemistry	chemistry	NOUN
eurjchem-843	33	10	4	4	NUM
eurjchem-843	33	11	(	(	PUNCT
eurjchem-843	33	12	4	4	NUM
eurjchem-843	33	13	)	)	PUNCT
eurjchem-843	33	14	(	(	PUNCT
eurjchem-843	33	15	2013	2013	NUM
eurjchem-843	33	16	)	)	PUNCT
eurjchem-843	33	17	360‐365	360‐365	NOUN
eurjchem-843	33	18	361	361	NUM
eurjchem-843	33	19	2	2	NUM
eurjchem-843	33	20	.	.	PUNCT
eurjchem-843	33	21	experimental	experimental	ADJ
eurjchem-843	33	22	2.1	2.1	NUM
eurjchem-843	33	23	.	.	PUNCT
eurjchem-843	34	1	instrumentation	instrumentation	NOUN
eurjchem-843	34	2	the	the	DET
eurjchem-843	34	3	hplc	hplc	NOUN
eurjchem-843	34	4	system	system	NOUN
eurjchem-843	34	5	consisted	consist	VERB
eurjchem-843	34	6	of	of	ADP
eurjchem-843	34	7	a	a	DET
eurjchem-843	34	8	shimadzu	shimadzu	ADJ
eurjchem-843	34	9	lc‐20	lc‐20	NOUN
eurjchem-843	34	10	at	at	ADP
eurjchem-843	34	11	liquid	liquid	ADJ
eurjchem-843	34	12	chromatograph	chromatograph	NOUN
eurjchem-843	34	13	(	(	PUNCT
eurjchem-843	34	14	japan	japan	PROPN
eurjchem-843	34	15	)	)	PUNCT
eurjchem-843	34	16	using	use	VERB
eurjchem-843	34	17	a	a	DET
eurjchem-843	34	18	symmetry	symmetry	NOUN
eurjchem-843	34	19	®	®	NOUN
eurjchem-843	34	20	waters	water	VERB
eurjchem-843	34	21	c18	c18	NOUN
eurjchem-843	34	22	column	column	NOUN
eurjchem-843	34	23	(	(	PUNCT
eurjchem-843	34	24	150	150	NUM
eurjchem-843	34	25	mm	mm	NOUN
eurjchem-843	34	26	x	x	SYM
eurjchem-843	34	27	4.6	4.6	NUM
eurjchem-843	34	28	mm	mm	NOUN
eurjchem-843	34	29	,	,	PUNCT
eurjchem-843	34	30	5	5	NUM
eurjchem-843	34	31	µm	µm	NOUN
eurjchem-843	34	32	)	)	PUNCT
eurjchem-843	34	33	(	(	PUNCT
eurjchem-843	34	34	ireland	ireland	NOUN
eurjchem-843	34	35	)	)	PUNCT
eurjchem-843	34	36	.	.	PUNCT
eurjchem-843	35	1	the	the	DET
eurjchem-843	35	2	system	system	NOUN
eurjchem-843	35	3	was	be	AUX
eurjchem-843	35	4	equipped	equip	VERB
eurjchem-843	35	5	with	with	ADP
eurjchem-843	35	6	a	a	DET
eurjchem-843	35	7	flourometric	flourometric	NOUN
eurjchem-843	35	8	detector	detector	NOUN
eurjchem-843	35	9	(	(	PUNCT
eurjchem-843	35	10	rf‐551	rf‐551	PROPN
eurjchem-843	35	11	,	,	PUNCT
eurjchem-843	35	12	japan	japan	PROPN
eurjchem-843	35	13	)	)	PUNCT
eurjchem-843	35	14	,	,	PUNCT
eurjchem-843	35	15	uv‐	uv‐	PROPN
eurjchem-843	35	16	visible	visible	ADJ
eurjchem-843	35	17	detector	detector	NOUN
eurjchem-843	35	18	(	(	PUNCT
eurjchem-843	35	19	spd‐20a	spd‐20a	PROPN
eurjchem-843	35	20	,	,	PUNCT
eurjchem-843	35	21	japan	japan	PROPN
eurjchem-843	35	22	)	)	PUNCT
eurjchem-843	35	23	and	and	CCONJ
eurjchem-843	35	24	an	an	DET
eurjchem-843	35	25	auto	auto	NOUN
eurjchem-843	35	26	sampler	sampler	NOUN
eurjchem-843	35	27	(	(	PUNCT
eurjchem-843	35	28	sil‐	sil‐	NOUN
eurjchem-843	35	29	20a	20a	NOUN
eurjchem-843	35	30	,	,	PUNCT
eurjchem-843	35	31	shimadzu	shimadzu	NOUN
eurjchem-843	35	32	,	,	PUNCT
eurjchem-843	35	33	japan	japan	PROPN
eurjchem-843	35	34	)	)	PUNCT
eurjchem-843	35	35	.	.	PUNCT
eurjchem-843	36	1	an	an	PRON
eurjchem-843	36	2	elma	elma	PROPN
eurjchem-843	36	3	s100	s100	PROPN
eurjchem-843	36	4	ultrasonic	ultrasonic	ADJ
eurjchem-843	36	5	processor	processor	NOUN
eurjchem-843	36	6	model	model	NOUN
eurjchem-843	36	7	kbk	kbk	PROPN
eurjchem-843	36	8	4200	4200	NUM
eurjchem-843	36	9	(	(	PUNCT
eurjchem-843	36	10	germany	germany	PROPN
eurjchem-843	36	11	)	)	PUNCT
eurjchem-843	36	12	was	be	AUX
eurjchem-843	36	13	used	use	VERB
eurjchem-843	36	14	.	.	PUNCT
eurjchem-843	37	1	2.2	2.2	NUM
eurjchem-843	37	2	.	.	PUNCT
eurjchem-843	37	3	reagents	reagent	NOUN
eurjchem-843	37	4	and	and	CCONJ
eurjchem-843	37	5	reference	reference	NOUN
eurjchem-843	37	6	samples	sample	VERB
eurjchem-843	37	7	pharmaceutical	pharmaceutical	ADJ
eurjchem-843	37	8	grade	grade	NOUN
eurjchem-843	37	9	stg	stg	PROPN
eurjchem-843	37	10	,	,	PUNCT
eurjchem-843	37	11	certified	certify	VERB
eurjchem-843	37	12	to	to	PART
eurjchem-843	37	13	contain	contain	VERB
eurjchem-843	37	14	99.80	99.80	NUM
eurjchem-843	37	15	%	%	NOUN
eurjchem-843	37	16	,	,	PUNCT
eurjchem-843	37	17	januvia	januvia	PROPN
eurjchem-843	37	18	®	®	NOUN
eurjchem-843	37	19	tablets	tablet	NOUN
eurjchem-843	37	20	nominally	nominally	ADV
eurjchem-843	37	21	containing	contain	VERB
eurjchem-843	37	22	128.5	128.5	NUM
eurjchem-843	37	23	mg	mg	NOUN
eurjchem-843	37	24	of	of	ADP
eurjchem-843	37	25	stg	stg	PROPN
eurjchem-843	37	26	per	per	ADP
eurjchem-843	37	27	tablet	tablet	NOUN
eurjchem-843	37	28	(	(	PUNCT
eurjchem-843	37	29	batch	batch	VERB
eurjchem-843	37	30	no	no	NOUN
eurjchem-843	37	31	.	.	PUNCT
eurjchem-843	38	1	s0273	s0273	NUM
eurjchem-843	38	2	)	)	PUNCT
eurjchem-843	38	3	and	and	CCONJ
eurjchem-843	38	4	janumet	janumet	ADJ
eurjchem-843	38	5	®	®	NOUN
eurjchem-843	38	6	tablets	tablet	NOUN
eurjchem-843	38	7	nominally	nominally	ADV
eurjchem-843	38	8	containing	contain	VERB
eurjchem-843	38	9	64.25	64.25	NUM
eurjchem-843	38	10	mg	mg	NOUN
eurjchem-843	38	11	of	of	ADP
eurjchem-843	38	12	stg	stg	PROPN
eurjchem-843	38	13	and	and	CCONJ
eurjchem-843	38	14	1000	1000	NUM
eurjchem-843	38	15	mg	mg	NOUN
eurjchem-843	38	16	of	of	ADP
eurjchem-843	38	17	met	meet	VERB
eurjchem-843	38	18	per	per	ADP
eurjchem-843	38	19	tablet	tablet	NOUN
eurjchem-843	38	20	(	(	PUNCT
eurjchem-843	38	21	batch	batch	VERB
eurjchem-843	38	22	no	no	NOUN
eurjchem-843	38	23	.	.	NOUN
eurjchem-843	38	24	0426570	0426570	NUM
eurjchem-843	38	25	)	)	PUNCT
eurjchem-843	38	26	were	be	AUX
eurjchem-843	38	27	all	all	PRON
eurjchem-843	38	28	supplied	supply	VERB
eurjchem-843	38	29	from	from	ADP
eurjchem-843	38	30	merck	merck	PROPN
eurjchem-843	38	31	sharp	sharp	PROPN
eurjchem-843	38	32	and	and	CCONJ
eurjchem-843	38	33	dohme	dohme	PROPN
eurjchem-843	38	34	co.	co.	PROPN
eurjchem-843	38	35	(	(	PUNCT
eurjchem-843	38	36	cairo	cairo	PROPN
eurjchem-843	38	37	,	,	PUNCT
eurjchem-843	38	38	egypt	egypt	PROPN
eurjchem-843	38	39	)	)	PUNCT
eurjchem-843	38	40	.	.	PUNCT
eurjchem-843	39	1	inactive	inactive	ADJ
eurjchem-843	39	2	ingredients	ingredient	NOUN
eurjchem-843	39	3	of	of	ADP
eurjchem-843	39	4	januvia	januvia	PROPN
eurjchem-843	39	5	®	®	NOUN
eurjchem-843	39	6	tablets	tablet	NOUN
eurjchem-843	39	7	include	include	VERB
eurjchem-843	39	8	microcrystalline	microcrystalline	NOUN
eurjchem-843	39	9	cellulose	cellulose	NOUN
eurjchem-843	39	10	(	(	PUNCT
eurjchem-843	39	11	e460	e460	PROPN
eurjchem-843	39	12	)	)	PUNCT
eurjchem-843	39	13	,	,	PUNCT
eurjchem-843	39	14	calcium	calcium	NOUN
eurjchem-843	39	15	hydrogen	hydrogen	NOUN
eurjchem-843	39	16	phosphate	phosphate	NOUN
eurjchem-843	39	17	,	,	PUNCT
eurjchem-843	39	18	anhydrous	anhydrous	ADJ
eurjchem-843	39	19	(	(	PUNCT
eurjchem-843	39	20	e341	e341	PROPN
eurjchem-843	39	21	)	)	PUNCT
eurjchem-843	39	22	,	,	PUNCT
eurjchem-843	39	23	croscarmellose	croscarmellose	ADJ
eurjchem-843	39	24	sodium	sodium	NOUN
eurjchem-843	39	25	(	(	PUNCT
eurjchem-843	39	26	e468	e468	PROPN
eurjchem-843	39	27	)	)	PUNCT
eurjchem-843	39	28	,	,	PUNCT
eurjchem-843	39	29	magnesium	magnesium	NOUN
eurjchem-843	39	30	stearate	stearate	NOUN
eurjchem-843	39	31	(	(	PUNCT
eurjchem-843	39	32	e470b	e470b	PROPN
eurjchem-843	39	33	)	)	PUNCT
eurjchem-843	39	34	and	and	CCONJ
eurjchem-843	39	35	sodium	sodium	NOUN
eurjchem-843	39	36	stearyl	stearyl	NOUN
eurjchem-843	39	37	fumarate	fumarate	NOUN
eurjchem-843	39	38	,	,	PUNCT
eurjchem-843	39	39	polyvinyl	polyvinyl	NOUN
eurjchem-843	39	40	alcohol	alcohol	NOUN
eurjchem-843	39	41	,	,	PUNCT
eurjchem-843	39	42	macrogol	macrogol	VERB
eurjchem-843	39	43	3350	3350	NUM
eurjchem-843	39	44	,	,	PUNCT
eurjchem-843	39	45	talc	talc	NOUN
eurjchem-843	39	46	(	(	PUNCT
eurjchem-843	39	47	e553b	e553b	PROPN
eurjchem-843	39	48	)	)	PUNCT
eurjchem-843	39	49	,	,	PUNCT
eurjchem-843	39	50	titanium	titanium	NOUN
eurjchem-843	39	51	dioxide	dioxide	NOUN
eurjchem-843	39	52	(	(	PUNCT
eurjchem-843	39	53	e171	e171	NUM
eurjchem-843	39	54	)	)	PUNCT
eurjchem-843	39	55	,	,	PUNCT
eurjchem-843	39	56	red	red	ADJ
eurjchem-843	39	57	iron	iron	NOUN
eurjchem-843	39	58	oxide	oxide	NOUN
eurjchem-843	39	59	(	(	PUNCT
eurjchem-843	39	60	e172	e172	NUM
eurjchem-843	39	61	)	)	PUNCT
eurjchem-843	39	62	and	and	CCONJ
eurjchem-843	39	63	yellow	yellow	ADJ
eurjchem-843	39	64	iron	iron	NOUN
eurjchem-843	39	65	oxide	oxide	NOUN
eurjchem-843	39	66	(	(	PUNCT
eurjchem-843	39	67	e172	e172	NUM
eurjchem-843	39	68	)	)	PUNCT
eurjchem-843	39	69	.	.	PUNCT
eurjchem-843	40	1	whereas	whereas	SCONJ
eurjchem-843	40	2	those	those	PRON
eurjchem-843	40	3	of	of	ADP
eurjchem-843	40	4	janumet	janumet	ADJ
eurjchem-843	40	5	®	®	NOUN
eurjchem-843	40	6	tablets	tablet	NOUN
eurjchem-843	40	7	include	include	VERB
eurjchem-843	40	8	microcrystalline	microcrystalline	NOUN
eurjchem-843	40	9	cellulose	cellulose	NOUN
eurjchem-843	40	10	(	(	PUNCT
eurjchem-843	40	11	e460	e460	PROPN
eurjchem-843	40	12	)	)	PUNCT
eurjchem-843	40	13	,	,	PUNCT
eurjchem-843	40	14	povidone	povidone	NOUN
eurjchem-843	40	15	k29/32	k29/32	PROPN
eurjchem-843	40	16	(	(	PUNCT
eurjchem-843	40	17	e1201	e1201	NOUN
eurjchem-843	40	18	)	)	PUNCT
eurjchem-843	40	19	,	,	PUNCT
eurjchem-843	40	20	sodium	sodium	NOUN
eurjchem-843	40	21	lauril	lauril	NOUN
eurjchem-843	40	22	sulfate	sulfate	NOUN
eurjchem-843	40	23	,	,	PUNCT
eurjchem-843	40	24	sodium	sodium	NOUN
eurjchem-843	40	25	stearyl	stearyl	NOUN
eurjchem-843	40	26	fumarate	fumarate	NOUN
eurjchem-843	40	27	,	,	PUNCT
eurjchem-843	40	28	polyvinyl	polyvinyl	NOUN
eurjchem-843	40	29	alcohol	alcohol	NOUN
eurjchem-843	40	30	,	,	PUNCT
eurjchem-843	40	31	macrogol	macrogol	VERB
eurjchem-843	40	32	3350	3350	NUM
eurjchem-843	40	33	,	,	PUNCT
eurjchem-843	40	34	talc	talc	NOUN
eurjchem-843	40	35	(	(	PUNCT
eurjchem-843	40	36	e553b	e553b	PROPN
eurjchem-843	40	37	)	)	PUNCT
eurjchem-843	40	38	,	,	PUNCT
eurjchem-843	40	39	titanium	titanium	NOUN
eurjchem-843	40	40	dioxide	dioxide	NOUN
eurjchem-843	40	41	(	(	PUNCT
eurjchem-843	40	42	e171	e171	NUM
eurjchem-843	40	43	)	)	PUNCT
eurjchem-843	40	44	,	,	PUNCT
eurjchem-843	40	45	iron	iron	NOUN
eurjchem-843	40	46	oxide	oxide	NOUN
eurjchem-843	40	47	red	red	NOUN
eurjchem-843	40	48	(	(	PUNCT
eurjchem-843	40	49	e172	e172	PROPN
eurjchem-843	40	50	)	)	PUNCT
eurjchem-843	40	51	and	and	CCONJ
eurjchem-843	40	52	iron	iron	NOUN
eurjchem-843	40	53	oxide	oxide	NOUN
eurjchem-843	40	54	black	black	NOUN
eurjchem-843	40	55	(	(	PUNCT
eurjchem-843	40	56	e172	e172	PROPN
eurjchem-843	40	57	)	)	PUNCT
eurjchem-843	40	58	.	.	PUNCT
eurjchem-843	41	1	pharmaceutical	pharmaceutical	PROPN
eurjchem-843	41	2	grade	grade	NOUN
eurjchem-843	41	3	met	meet	VERB
eurjchem-843	41	4	,	,	PUNCT
eurjchem-843	41	5	certified	certify	VERB
eurjchem-843	41	6	to	to	PART
eurjchem-843	41	7	contain	contain	VERB
eurjchem-843	41	8	99.79	99.79	NUM
eurjchem-843	41	9	%	%	NOUN
eurjchem-843	41	10	was	be	AUX
eurjchem-843	41	11	kindly	kindly	ADV
eurjchem-843	41	12	supplied	supply	VERB
eurjchem-843	41	13	by	by	ADP
eurjchem-843	41	14	chemical	chemical	NOUN
eurjchem-843	41	15	industries	industry	NOUN
eurjchem-843	41	16	development	development	NOUN
eurjchem-843	41	17	(	(	PUNCT
eurjchem-843	41	18	cid	cid	PROPN
eurjchem-843	41	19	)	)	PUNCT
eurjchem-843	41	20	co.	co.	PROPN
eurjchem-843	41	21	(	(	PUNCT
eurjchem-843	41	22	giza	giza	PROPN
eurjchem-843	41	23	,	,	PUNCT
eurjchem-843	41	24	egypt	egypt	PROPN
eurjchem-843	41	25	)	)	PUNCT
eurjchem-843	41	26	.	.	PUNCT
eurjchem-843	42	1	hplc	hplc	NOUN
eurjchem-843	42	2	grade	grade	NOUN
eurjchem-843	42	3	acetonitrile	acetonitrile	NOUN
eurjchem-843	42	4	and	and	CCONJ
eurjchem-843	42	5	methanol	methanol	NOUN
eurjchem-843	42	6	were	be	AUX
eurjchem-843	42	7	purchased	purchase	VERB
eurjchem-843	42	8	from	from	ADP
eurjchem-843	42	9	fisher	fisher	PROPN
eurjchem-843	42	10	scientific	scientific	PROPN
eurjchem-843	42	11	(	(	PUNCT
eurjchem-843	42	12	loughborough	loughborough	PROPN
eurjchem-843	42	13	,	,	PUNCT
eurjchem-843	42	14	leicestershire	leicestershire	NOUN
eurjchem-843	42	15	,	,	PUNCT
eurjchem-843	42	16	uk	uk	PROPN
eurjchem-843	42	17	)	)	PUNCT
eurjchem-843	42	18	.	.	PUNCT
eurjchem-843	43	1	potassium	potassium	NOUN
eurjchem-843	43	2	dihydrogen	dihydrogen	NOUN
eurjchem-843	43	3	phosphate	phosphate	NOUN
eurjchem-843	43	4	and	and	CCONJ
eurjchem-843	43	5	orthophosphric	orthophosphric	ADJ
eurjchem-843	43	6	acid	acid	NOUN
eurjchem-843	43	7	(	(	PUNCT
eurjchem-843	43	8	85	85	NUM
eurjchem-843	43	9	%	%	NOUN
eurjchem-843	43	10	)	)	PUNCT
eurjchem-843	43	11	were	be	AUX
eurjchem-843	43	12	purchased	purchase	VERB
eurjchem-843	43	13	from	from	ADP
eurjchem-843	43	14	vwr	vwr	PROPN
eurjchem-843	43	15	chemicals	chemical	NOUN
eurjchem-843	43	16	(	(	PUNCT
eurjchem-843	43	17	pool	pool	NOUN
eurjchem-843	43	18	,	,	PUNCT
eurjchem-843	43	19	england	england	PROPN
eurjchem-843	43	20	)	)	PUNCT
eurjchem-843	43	21	.	.	PUNCT
eurjchem-843	44	1	bi‐distilled	bi‐distille	VERB
eurjchem-843	44	2	water	water	NOUN
eurjchem-843	44	3	was	be	AUX
eurjchem-843	44	4	produced	produce	VERB
eurjchem-843	44	5	in‐	in‐	ADJ
eurjchem-843	44	6	house	house	NOUN
eurjchem-843	44	7	(	(	PUNCT
eurjchem-843	44	8	aquatron	aquatron	VERB
eurjchem-843	44	9	water	water	NOUN
eurjchem-843	44	10	still	still	ADV
eurjchem-843	44	11	,	,	PUNCT
eurjchem-843	44	12	a4000d	a4000d	PROPN
eurjchem-843	44	13	,	,	PUNCT
eurjchem-843	44	14	uk	uk	PROPN
eurjchem-843	44	15	)	)	PUNCT
eurjchem-843	44	16	.	.	PUNCT
eurjchem-843	45	1	membrane	membrane	NOUN
eurjchem-843	45	2	filters	filter	NOUN
eurjchem-843	45	3	0.45	0.45	NUM
eurjchem-843	45	4	µm	µm	NOUN
eurjchem-843	45	5	from	from	ADP
eurjchem-843	45	6	teknokroma	teknokroma	NOUN
eurjchem-843	45	7	(	(	PUNCT
eurjchem-843	45	8	barcelona	barcelona	PROPN
eurjchem-843	45	9	,	,	PUNCT
eurjchem-843	45	10	spain	spain	PROPN
eurjchem-843	45	11	)	)	PUNCT
eurjchem-843	45	12	were	be	AUX
eurjchem-843	45	13	used	use	VERB
eurjchem-843	45	14	.	.	PUNCT
eurjchem-843	46	1	all	all	DET
eurjchem-843	46	2	other	other	ADJ
eurjchem-843	46	3	chemicals	chemical	NOUN
eurjchem-843	46	4	and	and	CCONJ
eurjchem-843	46	5	reagents	reagent	NOUN
eurjchem-843	46	6	used	use	VERB
eurjchem-843	46	7	were	be	AUX
eurjchem-843	46	8	of	of	ADP
eurjchem-843	46	9	analytical	analytical	ADJ
eurjchem-843	46	10	grade	grade	NOUN
eurjchem-843	46	11	unless	unless	SCONJ
eurjchem-843	46	12	indicated	indicate	VERB
eurjchem-843	46	13	otherwise	otherwise	ADV
eurjchem-843	46	14	.	.	PUNCT
eurjchem-843	47	1	standard	standard	ADJ
eurjchem-843	47	2	stock	stock	NOUN
eurjchem-843	47	3	solutions	solution	NOUN
eurjchem-843	47	4	of	of	ADP
eurjchem-843	47	5	each	each	DET
eurjchem-843	47	6	drug	drug	NOUN
eurjchem-843	47	7	(	(	PUNCT
eurjchem-843	47	8	1	1	NUM
eurjchem-843	47	9	mg	mg	NUM
eurjchem-843	47	10	/	/	SYM
eurjchem-843	47	11	ml	ml	NOUN
eurjchem-843	47	12	)	)	PUNCT
eurjchem-843	47	13	were	be	AUX
eurjchem-843	47	14	prepared	prepare	VERB
eurjchem-843	47	15	by	by	ADP
eurjchem-843	47	16	dissolving	dissolve	VERB
eurjchem-843	47	17	100	100	NUM
eurjchem-843	47	18	mg	mg	ADP
eurjchem-843	47	19	of	of	ADP
eurjchem-843	47	20	the	the	DET
eurjchem-843	47	21	drug	drug	NOUN
eurjchem-843	47	22	in	in	ADP
eurjchem-843	47	23	methanol	methanol	NOUN
eurjchem-843	47	24	and	and	CCONJ
eurjchem-843	47	25	completing	complete	VERB
eurjchem-843	47	26	the	the	DET
eurjchem-843	47	27	volume	volume	NOUN
eurjchem-843	47	28	to	to	ADP
eurjchem-843	47	29	100	100	NUM
eurjchem-843	47	30	ml	ml	NOUN
eurjchem-843	47	31	in	in	ADP
eurjchem-843	47	32	a	a	DET
eurjchem-843	47	33	volumetric	volumetric	NOUN
eurjchem-843	47	34	flask	flask	NOUN
eurjchem-843	47	35	and	and	CCONJ
eurjchem-843	47	36	then	then	ADV
eurjchem-843	47	37	the	the	DET
eurjchem-843	47	38	required	require	VERB
eurjchem-843	47	39	concentrations	concentration	NOUN
eurjchem-843	47	40	were	be	AUX
eurjchem-843	47	41	prepared	prepare	VERB
eurjchem-843	47	42	by	by	ADP
eurjchem-843	47	43	serial	serial	ADJ
eurjchem-843	47	44	dilutions	dilution	NOUN
eurjchem-843	47	45	.	.	PUNCT
eurjchem-843	48	1	2.3	2.3	NUM
eurjchem-843	48	2	.	.	PUNCT
eurjchem-843	49	1	plasma	plasma	NOUN
eurjchem-843	49	2	sample	sample	NOUN
eurjchem-843	49	3	preparation	preparation	NOUN
eurjchem-843	49	4	the	the	DET
eurjchem-843	49	5	spiked	spiked	ADJ
eurjchem-843	49	6	plasma	plasma	NOUN
eurjchem-843	49	7	samples	sample	NOUN
eurjchem-843	49	8	were	be	AUX
eurjchem-843	49	9	extracted	extract	VERB
eurjchem-843	49	10	after	after	ADP
eurjchem-843	49	11	precipitation	precipitation	NOUN
eurjchem-843	49	12	of	of	ADP
eurjchem-843	49	13	proteins	protein	NOUN
eurjchem-843	49	14	using	use	VERB
eurjchem-843	49	15	100	100	NUM
eurjchem-843	49	16	μl	μl	ADP
eurjchem-843	49	17	of	of	ADP
eurjchem-843	49	18	perchloric	perchloric	ADJ
eurjchem-843	49	19	acid	acid	NOUN
eurjchem-843	49	20	(	(	PUNCT
eurjchem-843	49	21	35	35	NUM
eurjchem-843	49	22	%	%	NOUN
eurjchem-843	49	23	,	,	PUNCT
eurjchem-843	49	24	w	w	NOUN
eurjchem-843	49	25	:	:	PUNCT
eurjchem-843	49	26	w	w	NOUN
eurjchem-843	49	27	)	)	PUNCT
eurjchem-843	49	28	.	.	PUNCT
eurjchem-843	50	1	then	then	ADV
eurjchem-843	50	2	,	,	PUNCT
eurjchem-843	50	3	the	the	DET
eurjchem-843	50	4	mixture	mixture	NOUN
eurjchem-843	50	5	was	be	AUX
eurjchem-843	50	6	vortex‐mixed	vortex‐mixe	VERB
eurjchem-843	50	7	and	and	CCONJ
eurjchem-843	50	8	centrifuged	centrifuged	ADJ
eurjchem-843	50	9	(	(	PUNCT
eurjchem-843	50	10	2	2	NUM
eurjchem-843	50	11	and	and	CCONJ
eurjchem-843	50	12	3	3	NUM
eurjchem-843	50	13	min	min	NOUN
eurjchem-843	50	14	,	,	PUNCT
eurjchem-843	50	15	respectively	respectively	ADV
eurjchem-843	50	16	)	)	PUNCT
eurjchem-843	50	17	.	.	PUNCT
eurjchem-843	51	1	the	the	DET
eurjchem-843	51	2	supernatant	supernatant	NOUN
eurjchem-843	51	3	was	be	AUX
eurjchem-843	51	4	separated	separate	VERB
eurjchem-843	51	5	and	and	CCONJ
eurjchem-843	51	6	transferred	transfer	VERB
eurjchem-843	51	7	to	to	ADP
eurjchem-843	51	8	another	another	DET
eurjchem-843	51	9	tube	tube	NOUN
eurjchem-843	51	10	and	and	CCONJ
eurjchem-843	51	11	a	a	DET
eurjchem-843	51	12	25	25	NUM
eurjchem-843	51	13	μl	μl	NOUN
eurjchem-843	51	14	volume	volume	NOUN
eurjchem-843	51	15	was	be	AUX
eurjchem-843	51	16	injected	inject	VERB
eurjchem-843	51	17	into	into	ADP
eurjchem-843	51	18	the	the	DET
eurjchem-843	51	19	chromatograph	chromatograph	NOUN
eurjchem-843	51	20	.	.	PUNCT
eurjchem-843	52	1	2.4	2.4	NUM
eurjchem-843	52	2	.	.	PUNCT
eurjchem-843	52	3	preparation	preparation	NOUN
eurjchem-843	52	4	of	of	ADP
eurjchem-843	52	5	the	the	DET
eurjchem-843	52	6	acidic	acidic	ADJ
eurjchem-843	52	7	degradation	degradation	NOUN
eurjchem-843	52	8	product	product	NOUN
eurjchem-843	52	9	an	an	DET
eurjchem-843	52	10	amount	amount	NOUN
eurjchem-843	52	11	of	of	ADP
eurjchem-843	52	12	1	1	NUM
eurjchem-843	52	13	g	g	NOUN
eurjchem-843	52	14	of	of	ADP
eurjchem-843	52	15	stg	stg	PROPN
eurjchem-843	52	16	bulk	bulk	ADJ
eurjchem-843	52	17	powder	powder	NOUN
eurjchem-843	52	18	was	be	AUX
eurjchem-843	52	19	dissolved	dissolve	VERB
eurjchem-843	52	20	in	in	ADP
eurjchem-843	52	21	250	250	NUM
eurjchem-843	52	22	ml	ml	NOUN
eurjchem-843	52	23	of	of	ADP
eurjchem-843	52	24	6	6	NUM
eurjchem-843	52	25	n	n	CCONJ
eurjchem-843	52	26	aqueous	aqueous	ADJ
eurjchem-843	52	27	hydrochloric	hydrochloric	ADJ
eurjchem-843	52	28	acid	acid	NOUN
eurjchem-843	52	29	then	then	ADV
eurjchem-843	52	30	the	the	DET
eurjchem-843	52	31	solution	solution	NOUN
eurjchem-843	52	32	was	be	AUX
eurjchem-843	52	33	heated	heat	VERB
eurjchem-843	52	34	for	for	ADP
eurjchem-843	52	35	8	8	NUM
eurjchem-843	52	36	h	h	NOUN
eurjchem-843	52	37	on	on	ADP
eurjchem-843	52	38	a	a	DET
eurjchem-843	52	39	boiling	boil	VERB
eurjchem-843	52	40	water	water	NOUN
eurjchem-843	52	41	bath	bath	NOUN
eurjchem-843	52	42	,	,	PUNCT
eurjchem-843	52	43	then	then	ADV
eurjchem-843	52	44	cooled	cool	VERB
eurjchem-843	52	45	and	and	CCONJ
eurjchem-843	52	46	neutralized	neutralize	VERB
eurjchem-843	52	47	by	by	ADP
eurjchem-843	52	48	6	6	NUM
eurjchem-843	52	49	n	n	DET
eurjchem-843	52	50	aqueous	aqueous	ADJ
eurjchem-843	52	51	sodium	sodium	NOUN
eurjchem-843	52	52	hydroxide	hydroxide	NOUN
eurjchem-843	52	53	.	.	PUNCT
eurjchem-843	53	1	the	the	DET
eurjchem-843	53	2	formed	form	VERB
eurjchem-843	53	3	precipitate	precipitate	NOUN
eurjchem-843	53	4	was	be	AUX
eurjchem-843	53	5	filtered	filter	VERB
eurjchem-843	53	6	,	,	PUNCT
eurjchem-843	53	7	washed	wash	VERB
eurjchem-843	53	8	several	several	ADJ
eurjchem-843	53	9	times	time	NOUN
eurjchem-843	53	10	and	and	CCONJ
eurjchem-843	53	11	dried	dry	VERB
eurjchem-843	53	12	.	.	PUNCT
eurjchem-843	54	1	complete	complete	ADJ
eurjchem-843	54	2	degradation	degradation	NOUN
eurjchem-843	54	3	was	be	AUX
eurjchem-843	54	4	confirmed	confirm	VERB
eurjchem-843	54	5	using	use	VERB
eurjchem-843	54	6	tlc	tlc	NOUN
eurjchem-843	54	7	plates	plate	NOUN
eurjchem-843	54	8	and	and	CCONJ
eurjchem-843	54	9	its	its	PRON
eurjchem-843	54	10	structure	structure	NOUN
eurjchem-843	54	11	was	be	AUX
eurjchem-843	54	12	then	then	ADV
eurjchem-843	54	13	elucidated	elucidate	VERB
eurjchem-843	54	14	by	by	ADP
eurjchem-843	54	15	different	different	ADJ
eurjchem-843	54	16	spectroscopic	spectroscopic	ADJ
eurjchem-843	54	17	techniques	technique	NOUN
eurjchem-843	54	18	.	.	PUNCT
eurjchem-843	55	1	2.5	2.5	NUM
eurjchem-843	55	2	.	.	PUNCT
eurjchem-843	56	1	chromatographic	chromatographic	ADJ
eurjchem-843	56	2	conditions	condition	NOUN
eurjchem-843	56	3	2.5.1	2.5.1	NUM
eurjchem-843	56	4	.	.	PUNCT
eurjchem-843	57	1	lc‐fluoro	lc‐fluoro	PROPN
eurjchem-843	57	2	method	method	NOUN
eurjchem-843	57	3	chromatographic	chromatographic	ADJ
eurjchem-843	57	4	separation	separation	NOUN
eurjchem-843	57	5	was	be	AUX
eurjchem-843	57	6	achieved	achieve	VERB
eurjchem-843	57	7	on	on	ADP
eurjchem-843	57	8	a	a	DET
eurjchem-843	57	9	symmetry	symmetry	NOUN
eurjchem-843	57	10	®	®	NOUN
eurjchem-843	57	11	waters	water	VERB
eurjchem-843	57	12	c18	c18	NOUN
eurjchem-843	57	13	column	column	NOUN
eurjchem-843	57	14	(	(	PUNCT
eurjchem-843	57	15	150	150	NUM
eurjchem-843	57	16	mm	mm	NOUN
eurjchem-843	57	17	×	×	NOUN
eurjchem-843	57	18	4.6	4.6	NUM
eurjchem-843	57	19	mm	mm	NOUN
eurjchem-843	57	20	,	,	PUNCT
eurjchem-843	57	21	5	5	NUM
eurjchem-843	57	22	μm	μm	NOUN
eurjchem-843	57	23	)	)	PUNCT
eurjchem-843	57	24	applying	apply	VERB
eurjchem-843	57	25	an	an	DET
eurjchem-843	57	26	isocratic	isocratic	ADJ
eurjchem-843	57	27	elution	elution	NOUN
eurjchem-843	57	28	based	base	VERB
eurjchem-843	57	29	on	on	ADP
eurjchem-843	57	30	potassium	potassium	NOUN
eurjchem-843	57	31	dihydrogen	dihydrogen	NOUN
eurjchem-843	57	32	phosphate	phosphate	NOUN
eurjchem-843	57	33	buffer	buffer	NOUN
eurjchem-843	57	34	(	(	PUNCT
eurjchem-843	57	35	ph	ph	NOUN
eurjchem-843	57	36	=	=	NOUN
eurjchem-843	57	37	4.6	4.6	NUM
eurjchem-843	57	38	)	)	PUNCT
eurjchem-843	57	39	‐	‐	ADJ
eurjchem-843	57	40	acetonitrile	acetonitrile	NOUN
eurjchem-843	57	41	(	(	PUNCT
eurjchem-843	57	42	30:70	30:70	NUM
eurjchem-843	57	43	,	,	PUNCT
eurjchem-843	57	44	v	v	NOUN
eurjchem-843	57	45	:	:	SYM
eurjchem-843	57	46	v	v	NOUN
eurjchem-843	57	47	)	)	PUNCT
eurjchem-843	57	48	as	as	ADP
eurjchem-843	57	49	a	a	DET
eurjchem-843	57	50	mobile	mobile	ADJ
eurjchem-843	57	51	phase	phase	NOUN
eurjchem-843	57	52	.	.	PUNCT
eurjchem-843	58	1	the	the	DET
eurjchem-843	58	2	fluorometric	fluorometric	ADJ
eurjchem-843	58	3	detector	detector	NOUN
eurjchem-843	58	4	was	be	AUX
eurjchem-843	58	5	operated	operate	VERB
eurjchem-843	58	6	at	at	ADP
eurjchem-843	58	7	267	267	NUM
eurjchem-843	58	8	nm	nm	NOUN
eurjchem-843	58	9	for	for	ADP
eurjchem-843	58	10	excitation	excitation	NOUN
eurjchem-843	58	11	and	and	CCONJ
eurjchem-843	58	12	575	575	NUM
eurjchem-843	58	13	nm	nm	NOUN
eurjchem-843	58	14	for	for	ADP
eurjchem-843	58	15	emission	emission	NOUN
eurjchem-843	58	16	.	.	PUNCT
eurjchem-843	59	1	the	the	DET
eurjchem-843	59	2	buffer	buffer	NOUN
eurjchem-843	59	3	solution	solution	NOUN
eurjchem-843	59	4	was	be	AUX
eurjchem-843	59	5	filtered	filter	VERB
eurjchem-843	59	6	through	through	ADP
eurjchem-843	59	7	0.45	0.45	NUM
eurjchem-843	59	8	µm	µm	ADP
eurjchem-843	59	9	membrane	membrane	NOUN
eurjchem-843	59	10	filter	filter	NOUN
eurjchem-843	59	11	and	and	CCONJ
eurjchem-843	59	12	degassed	degas	VERB
eurjchem-843	59	13	for	for	ADP
eurjchem-843	59	14	30	30	NUM
eurjchem-843	59	15	min	min	NOUN
eurjchem-843	59	16	in	in	ADP
eurjchem-843	59	17	an	an	DET
eurjchem-843	59	18	ultrasonic	ultrasonic	ADJ
eurjchem-843	59	19	bath	bath	NOUN
eurjchem-843	59	20	prior	prior	ADV
eurjchem-843	59	21	to	to	ADP
eurjchem-843	59	22	its	its	PRON
eurjchem-843	59	23	use	use	NOUN
eurjchem-843	59	24	.	.	PUNCT
eurjchem-843	60	1	the	the	DET
eurjchem-843	60	2	mobile	mobile	ADJ
eurjchem-843	60	3	phase	phase	NOUN
eurjchem-843	60	4	was	be	AUX
eurjchem-843	60	5	pumped	pump	VERB
eurjchem-843	60	6	through	through	ADP
eurjchem-843	60	7	the	the	DET
eurjchem-843	60	8	column	column	NOUN
eurjchem-843	60	9	at	at	ADP
eurjchem-843	60	10	a	a	DET
eurjchem-843	60	11	flow	flow	NOUN
eurjchem-843	60	12	rate	rate	NOUN
eurjchem-843	60	13	of	of	ADP
eurjchem-843	60	14	1	1	NUM
eurjchem-843	60	15	ml	ml	NOUN
eurjchem-843	60	16	/	/	SYM
eurjchem-843	60	17	min	min	NOUN
eurjchem-843	60	18	.	.	PROPN
eurjchem-843	60	19	analyses	analysis	NOUN
eurjchem-843	60	20	were	be	AUX
eurjchem-843	60	21	performed	perform	VERB
eurjchem-843	60	22	at	at	ADP
eurjchem-843	60	23	ambient	ambient	ADJ
eurjchem-843	60	24	temperature	temperature	NOUN
eurjchem-843	60	25	and	and	CCONJ
eurjchem-843	60	26	the	the	DET
eurjchem-843	60	27	injection	injection	NOUN
eurjchem-843	60	28	volume	volume	NOUN
eurjchem-843	60	29	was	be	AUX
eurjchem-843	60	30	25	25	NUM
eurjchem-843	60	31	µl	µl	NOUN
eurjchem-843	60	32	.	.	PUNCT
eurjchem-843	61	1	2.5.2	2.5.2	NUM
eurjchem-843	61	2	.	.	NOUN
eurjchem-843	61	3	lc‐uv	lc‐uv	PROPN
eurjchem-843	61	4	method	method	PROPN
eurjchem-843	61	5	chromatographic	chromatographic	ADJ
eurjchem-843	61	6	separation	separation	NOUN
eurjchem-843	61	7	was	be	AUX
eurjchem-843	61	8	achieved	achieve	VERB
eurjchem-843	61	9	on	on	ADP
eurjchem-843	61	10	a	a	DET
eurjchem-843	61	11	symmetry	symmetry	NOUN
eurjchem-843	61	12	®	®	NOUN
eurjchem-843	61	13	waters	water	VERB
eurjchem-843	61	14	c18	c18	NOUN
eurjchem-843	61	15	column	column	NOUN
eurjchem-843	61	16	(	(	PUNCT
eurjchem-843	61	17	150	150	NUM
eurjchem-843	61	18	mm	mm	NOUN
eurjchem-843	61	19	×	×	NOUN
eurjchem-843	61	20	4.6	4.6	NUM
eurjchem-843	61	21	mm	mm	NOUN
eurjchem-843	61	22	,	,	PUNCT
eurjchem-843	61	23	5	5	NUM
eurjchem-843	61	24	μm	μm	NOUN
eurjchem-843	61	25	)	)	PUNCT
eurjchem-843	61	26	applying	apply	VERB
eurjchem-843	61	27	an	an	DET
eurjchem-843	61	28	isocratic	isocratic	ADJ
eurjchem-843	61	29	elution	elution	NOUN
eurjchem-843	61	30	based	base	VERB
eurjchem-843	61	31	on	on	ADP
eurjchem-843	61	32	potassium	potassium	NOUN
eurjchem-843	61	33	dihydrogen	dihydrogen	NOUN
eurjchem-843	61	34	phosphate	phosphate	NOUN
eurjchem-843	61	35	buffer	buffer	NOUN
eurjchem-843	61	36	(	(	PUNCT
eurjchem-843	61	37	ph	ph	NOUN
eurjchem-843	61	38	=	=	NOUN
eurjchem-843	61	39	4.6	4.6	NUM
eurjchem-843	61	40	)	)	PUNCT
eurjchem-843	61	41	‐	‐	ADJ
eurjchem-843	61	42	acetonitrile	acetonitrile	NOUN
eurjchem-843	61	43	(	(	PUNCT
eurjchem-843	61	44	15:85	15:85	NUM
eurjchem-843	61	45	,	,	PUNCT
eurjchem-843	61	46	v	v	NOUN
eurjchem-843	61	47	:	:	SYM
eurjchem-843	61	48	v	v	NOUN
eurjchem-843	61	49	)	)	PUNCT
eurjchem-843	61	50	as	as	ADP
eurjchem-843	61	51	a	a	DET
eurjchem-843	61	52	mobile	mobile	ADJ
eurjchem-843	61	53	phase	phase	NOUN
eurjchem-843	61	54	.	.	PUNCT
eurjchem-843	62	1	the	the	DET
eurjchem-843	62	2	uv	uv	NOUN
eurjchem-843	62	3	detector	detector	NOUN
eurjchem-843	62	4	was	be	AUX
eurjchem-843	62	5	operated	operate	VERB
eurjchem-843	62	6	at	at	ADP
eurjchem-843	62	7	220	220	NUM
eurjchem-843	62	8	nm	nm	NOUN
eurjchem-843	62	9	.	.	PUNCT
eurjchem-843	63	1	the	the	DET
eurjchem-843	63	2	buffer	buffer	NOUN
eurjchem-843	63	3	solution	solution	NOUN
eurjchem-843	63	4	was	be	AUX
eurjchem-843	63	5	filtered	filter	VERB
eurjchem-843	63	6	through	through	ADP
eurjchem-843	63	7	0.45	0.45	NUM
eurjchem-843	63	8	µm	µm	ADP
eurjchem-843	63	9	membrane	membrane	NOUN
eurjchem-843	63	10	filter	filter	NOUN
eurjchem-843	63	11	and	and	CCONJ
eurjchem-843	63	12	degassed	degas	VERB
eurjchem-843	63	13	for	for	ADP
eurjchem-843	63	14	30	30	NUM
eurjchem-843	63	15	min	min	NOUN
eurjchem-843	63	16	in	in	ADP
eurjchem-843	63	17	an	an	DET
eurjchem-843	63	18	ultrasonic	ultrasonic	ADJ
eurjchem-843	63	19	bath	bath	NOUN
eurjchem-843	63	20	prior	prior	ADV
eurjchem-843	63	21	to	to	ADP
eurjchem-843	63	22	its	its	PRON
eurjchem-843	63	23	use	use	NOUN
eurjchem-843	63	24	.	.	PUNCT
eurjchem-843	64	1	the	the	DET
eurjchem-843	64	2	mobile	mobile	ADJ
eurjchem-843	64	3	phase	phase	NOUN
eurjchem-843	64	4	was	be	AUX
eurjchem-843	64	5	pumped	pump	VERB
eurjchem-843	64	6	through	through	ADP
eurjchem-843	64	7	the	the	DET
eurjchem-843	64	8	column	column	NOUN
eurjchem-843	64	9	at	at	ADP
eurjchem-843	64	10	a	a	DET
eurjchem-843	64	11	flow	flow	NOUN
eurjchem-843	64	12	rate	rate	NOUN
eurjchem-843	64	13	of	of	ADP
eurjchem-843	64	14	1	1	NUM
eurjchem-843	64	15	ml	ml	NOUN
eurjchem-843	64	16	/	/	SYM
eurjchem-843	64	17	min	min	NOUN
eurjchem-843	64	18	.	.	PROPN
eurjchem-843	64	19	analyses	analysis	NOUN
eurjchem-843	64	20	were	be	AUX
eurjchem-843	64	21	performed	perform	VERB
eurjchem-843	64	22	at	at	ADP
eurjchem-843	64	23	ambient	ambient	ADJ
eurjchem-843	64	24	temperature	temperature	NOUN
eurjchem-843	64	25	and	and	CCONJ
eurjchem-843	64	26	the	the	DET
eurjchem-843	64	27	injection	injection	NOUN
eurjchem-843	64	28	volume	volume	NOUN
eurjchem-843	64	29	was	be	AUX
eurjchem-843	64	30	25	25	NUM
eurjchem-843	64	31	µl	µl	NOUN
eurjchem-843	64	32	.	.	PUNCT
eurjchem-843	65	1	2.6	2.6	NUM
eurjchem-843	65	2	.	.	PUNCT
eurjchem-843	66	1	sample	sample	NOUN
eurjchem-843	66	2	preparation	preparation	NOUN
eurjchem-843	66	3	twenty	twenty	NUM
eurjchem-843	66	4	tablets	tablet	NOUN
eurjchem-843	66	5	of	of	ADP
eurjchem-843	66	6	januvia	januvia	PROPN
eurjchem-843	66	7	®	®	PROPN
eurjchem-843	66	8	and	and	CCONJ
eurjchem-843	66	9	janumet	janumet	ADJ
eurjchem-843	66	10	®	®	NOUN
eurjchem-843	66	11	were	be	AUX
eurjchem-843	66	12	separately	separately	ADV
eurjchem-843	66	13	weighed	weigh	VERB
eurjchem-843	66	14	.	.	PUNCT
eurjchem-843	67	1	an	an	DET
eurjchem-843	67	2	accurately	accurately	ADV
eurjchem-843	67	3	weighed	weigh	VERB
eurjchem-843	67	4	amount	amount	NOUN
eurjchem-843	67	5	of	of	ADP
eurjchem-843	67	6	the	the	DET
eurjchem-843	67	7	finely	finely	ADV
eurjchem-843	67	8	powdered	powder	VERB
eurjchem-843	67	9	januvia	januvia	NOUN
eurjchem-843	67	10	®	®	NOUN
eurjchem-843	67	11	tablets	tablet	NOUN
eurjchem-843	67	12	equivalent	equivalent	ADJ
eurjchem-843	67	13	to	to	ADP
eurjchem-843	67	14	100	100	NUM
eurjchem-843	67	15	mg	mg	NOUN
eurjchem-843	67	16	of	of	ADP
eurjchem-843	67	17	stg	stg	PROPN
eurjchem-843	67	18	and	and	CCONJ
eurjchem-843	67	19	a	a	DET
eurjchem-843	67	20	quantity	quantity	NOUN
eurjchem-843	67	21	of	of	ADP
eurjchem-843	67	22	the	the	DET
eurjchem-843	67	23	powdered	powdered	ADJ
eurjchem-843	67	24	janumet	janumet	NOUN
eurjchem-843	67	25	®	®	NOUN
eurjchem-843	67	26	tablets	tablet	NOUN
eurjchem-843	67	27	equivalent	equivalent	ADJ
eurjchem-843	67	28	to	to	ADP
eurjchem-843	67	29	(	(	PUNCT
eurjchem-843	67	30	6.425	6.425	NUM
eurjchem-843	67	31	mg	mg	NOUN
eurjchem-843	67	32	)	)	PUNCT
eurjchem-843	67	33	stg	stg	PROPN
eurjchem-843	67	34	and	and	CCONJ
eurjchem-843	67	35	(	(	PUNCT
eurjchem-843	67	36	100	100	NUM
eurjchem-843	67	37	mg	mg	NOUN
eurjchem-843	67	38	)	)	PUNCT
eurjchem-843	67	39	met	meet	VERB
eurjchem-843	67	40	were	be	AUX
eurjchem-843	67	41	separately	separately	ADV
eurjchem-843	67	42	made	make	VERB
eurjchem-843	67	43	up	up	ADP
eurjchem-843	67	44	to	to	PART
eurjchem-843	67	45	100	100	NUM
eurjchem-843	67	46	ml	ml	NOUN
eurjchem-843	67	47	with	with	ADP
eurjchem-843	67	48	methanol	methanol	NOUN
eurjchem-843	67	49	and	and	CCONJ
eurjchem-843	67	50	sonicated	sonicate	VERB
eurjchem-843	67	51	to	to	PART
eurjchem-843	67	52	dissolve	dissolve	VERB
eurjchem-843	67	53	.	.	PUNCT
eurjchem-843	68	1	the	the	DET
eurjchem-843	68	2	solutions	solution	NOUN
eurjchem-843	68	3	were	be	AUX
eurjchem-843	68	4	filtered	filter	VERB
eurjchem-843	68	5	followed	follow	VERB
eurjchem-843	68	6	by	by	ADP
eurjchem-843	68	7	serial	serial	ADJ
eurjchem-843	68	8	dilutions	dilution	NOUN
eurjchem-843	68	9	to	to	ADP
eurjchem-843	68	10	the	the	DET
eurjchem-843	68	11	required	require	VERB
eurjchem-843	68	12	concentrations	concentration	NOUN
eurjchem-843	68	13	for	for	ADP
eurjchem-843	68	14	each	each	DET
eurjchem-843	68	15	experiment	experiment	NOUN
eurjchem-843	68	16	.	.	PUNCT
eurjchem-843	69	1	2.7	2.7	NUM
eurjchem-843	69	2	.	.	PUNCT
eurjchem-843	69	3	procedure	procedure	NOUN
eurjchem-843	69	4	2.7.1	2.7.1	NUM
eurjchem-843	69	5	.	.	PUNCT
eurjchem-843	70	1	linearity	linearity	NOUN
eurjchem-843	70	2	and	and	CCONJ
eurjchem-843	70	3	repeatability	repeatability	NOUN
eurjchem-843	70	4	2.7.1.1	2.7.1.1	NUM
eurjchem-843	70	5	.	.	PUNCT
eurjchem-843	71	1	lc‐fluoro	lc‐fluoro	PROPN
eurjchem-843	71	2	method	method	NOUN
eurjchem-843	71	3	accurately	accurately	ADV
eurjchem-843	71	4	measured	measure	VERB
eurjchem-843	71	5	aliquots	aliquot	NOUN
eurjchem-843	71	6	of	of	ADP
eurjchem-843	71	7	stg	stg	NOUN
eurjchem-843	71	8	stock	stock	NOUN
eurjchem-843	71	9	solution	solution	NOUN
eurjchem-843	71	10	equivalent	equivalent	ADJ
eurjchem-843	71	11	to	to	ADP
eurjchem-843	71	12	50‐2000	50‐2000	NUM
eurjchem-843	71	13	µg	µg	ADV
eurjchem-843	71	14	were	be	AUX
eurjchem-843	71	15	transferred	transfer	VERB
eurjchem-843	71	16	into	into	ADP
eurjchem-843	71	17	a	a	DET
eurjchem-843	71	18	series	series	NOUN
eurjchem-843	71	19	of	of	ADP
eurjchem-843	71	20	10	10	NUM
eurjchem-843	71	21	ml	ml	NOUN
eurjchem-843	71	22	volumetric	volumetric	ADJ
eurjchem-843	71	23	flasks	flask	NOUN
eurjchem-843	71	24	and	and	CCONJ
eurjchem-843	71	25	then	then	ADV
eurjchem-843	71	26	completed	complete	VERB
eurjchem-843	71	27	to	to	PART
eurjchem-843	71	28	volume	volume	VERB
eurjchem-843	71	29	with	with	ADP
eurjchem-843	71	30	methanol	methanol	NOUN
eurjchem-843	71	31	.	.	PUNCT
eurjchem-843	72	1	a	a	DET
eurjchem-843	72	2	volume	volume	NOUN
eurjchem-843	72	3	of	of	ADP
eurjchem-843	72	4	25	25	NUM
eurjchem-843	72	5	µl	µl	NOUN
eurjchem-843	72	6	of	of	ADP
eurjchem-843	72	7	each	each	DET
eurjchem-843	72	8	solution	solution	NOUN
eurjchem-843	72	9	was	be	AUX
eurjchem-843	72	10	injected	inject	VERB
eurjchem-843	72	11	into	into	ADP
eurjchem-843	72	12	the	the	DET
eurjchem-843	72	13	chromatograph	chromatograph	NOUN
eurjchem-843	72	14	.	.	PUNCT
eurjchem-843	73	1	the	the	DET
eurjchem-843	73	2	conditions	condition	NOUN
eurjchem-843	73	3	including	include	VERB
eurjchem-843	73	4	the	the	DET
eurjchem-843	73	5	mobile	mobile	ADJ
eurjchem-843	73	6	phase	phase	NOUN
eurjchem-843	73	7	at	at	ADP
eurjchem-843	73	8	a	a	DET
eurjchem-843	73	9	flow	flow	NOUN
eurjchem-843	73	10	rate	rate	NOUN
eurjchem-843	73	11	1	1	NUM
eurjchem-843	73	12	ml	ml	NOUN
eurjchem-843	73	13	/	/	SYM
eurjchem-843	73	14	min	min	NOUN
eurjchem-843	73	15	,	,	PUNCT
eurjchem-843	73	16	fluorometric	fluorometric	ADJ
eurjchem-843	73	17	detection	detection	NOUN
eurjchem-843	73	18	(	(	PUNCT
eurjchem-843	73	19	λex	λex	NOUN
eurjchem-843	73	20	:	:	PUNCT
eurjchem-843	73	21	267	267	NUM
eurjchem-843	73	22	nm	nm	NOUN
eurjchem-843	73	23	,	,	PUNCT
eurjchem-843	73	24	λem	λem	ADJ
eurjchem-843	73	25	:	:	PUNCT
eurjchem-843	73	26	575	575	NUM
eurjchem-843	73	27	nm	nm	NOUN
eurjchem-843	73	28	)	)	PUNCT
eurjchem-843	73	29	and	and	CCONJ
eurjchem-843	73	30	run	run	VERB
eurjchem-843	73	31	time	time	NOUN
eurjchem-843	73	32	program	program	NOUN
eurjchem-843	73	33	for	for	ADP
eurjchem-843	73	34	10	10	NUM
eurjchem-843	73	35	min	min	NOUN
eurjchem-843	73	36	were	be	AUX
eurjchem-843	73	37	adjusted	adjust	VERB
eurjchem-843	73	38	.	.	PUNCT
eurjchem-843	74	1	a	a	DET
eurjchem-843	74	2	calibration	calibration	NOUN
eurjchem-843	74	3	curve	curve	NOUN
eurjchem-843	74	4	was	be	AUX
eurjchem-843	74	5	obtained	obtain	VERB
eurjchem-843	74	6	by	by	ADP
eurjchem-843	74	7	plotting	plot	VERB
eurjchem-843	74	8	area	area	NOUN
eurjchem-843	74	9	under	under	ADP
eurjchem-843	74	10	the	the	DET
eurjchem-843	74	11	peak	peak	NOUN
eurjchem-843	74	12	(	(	PUNCT
eurjchem-843	74	13	aup	aup	PROPN
eurjchem-843	74	14	)	)	PUNCT
eurjchem-843	74	15	against	against	ADP
eurjchem-843	74	16	concentration	concentration	NOUN
eurjchem-843	74	17	(	(	PUNCT
eurjchem-843	74	18	c	c	NOUN
eurjchem-843	74	19	)	)	PUNCT
eurjchem-843	74	20	.	.	PUNCT
eurjchem-843	75	1	the	the	DET
eurjchem-843	75	2	repeatability	repeatability	NOUN
eurjchem-843	75	3	of	of	ADP
eurjchem-843	75	4	the	the	DET
eurjchem-843	75	5	method	method	NOUN
eurjchem-843	75	6	was	be	AUX
eurjchem-843	75	7	assessed	assess	VERB
eurjchem-843	75	8	by	by	ADP
eurjchem-843	75	9	analyzing	analyze	VERB
eurjchem-843	75	10	a	a	DET
eurjchem-843	75	11	mixture	mixture	NOUN
eurjchem-843	75	12	containing	contain	VERB
eurjchem-843	75	13	30	30	NUM
eurjchem-843	75	14	and	and	CCONJ
eurjchem-843	75	15	100	100	NUM
eurjchem-843	75	16	µg	µg	ADJ
eurjchem-843	75	17	/	/	SYM
eurjchem-843	75	18	ml	ml	NOUN
eurjchem-843	75	19	of	of	ADP
eurjchem-843	75	20	sdp	sdp	NOUN
eurjchem-843	75	21	and	and	CCONJ
eurjchem-843	75	22	stg	stg	NOUN
eurjchem-843	75	23	,	,	PUNCT
eurjchem-843	75	24	respectively	respectively	ADV
eurjchem-843	75	25	(	(	PUNCT
eurjchem-843	75	26	n	n	NOUN
eurjchem-843	75	27	=	=	SYM
eurjchem-843	75	28	6	6	NUM
eurjchem-843	75	29	)	)	PUNCT
eurjchem-843	75	30	.	.	PUNCT
eurjchem-843	76	1	the	the	DET
eurjchem-843	76	2	precision	precision	NOUN
eurjchem-843	76	3	(	(	PUNCT
eurjchem-843	76	4	%	%	INTJ
eurjchem-843	76	5	r.s.d	r.s.d	NOUN
eurjchem-843	76	6	.	.	PUNCT
eurjchem-843	76	7	)	)	PUNCT
eurjchem-843	77	1	values	value	NOUN
eurjchem-843	77	2	of	of	ADP
eurjchem-843	77	3	peak	peak	NOUN
eurjchem-843	77	4	areas	area	NOUN
eurjchem-843	77	5	and	and	CCONJ
eurjchem-843	77	6	retention	retention	NOUN
eurjchem-843	77	7	times	time	NOUN
eurjchem-843	77	8	were	be	AUX
eurjchem-843	77	9	calculated	calculate	VERB
eurjchem-843	77	10	,	,	PUNCT
eurjchem-843	77	11	table	table	NOUN
eurjchem-843	77	12	1	1	NUM
eurjchem-843	77	13	.	.	PUNCT
eurjchem-843	78	1	2.7.1.1.1	2.7.1.1.1	X
eurjchem-843	78	2	.	.	PUNCT
eurjchem-843	78	3	lc‐fluoro	lc‐fluoro	PROPN
eurjchem-843	78	4	method	method	NOUN
eurjchem-843	78	5	in	in	ADP
eurjchem-843	78	6	plasma	plasma	NOUN
eurjchem-843	78	7	accurately	accurately	ADV
eurjchem-843	78	8	measured	measure	VERB
eurjchem-843	78	9	aliquots	aliquot	NOUN
eurjchem-843	78	10	of	of	ADP
eurjchem-843	78	11	plasma	plasma	NOUN
eurjchem-843	78	12	samples	sample	NOUN
eurjchem-843	78	13	equivalent	equivalent	ADJ
eurjchem-843	78	14	to	to	ADP
eurjchem-843	78	15	0.25‐8.00	0.25‐8.00	PROPN
eurjchem-843	78	16	µg	µg	ADP
eurjchem-843	78	17	stg	stg	PROPN
eurjchem-843	78	18	were	be	AUX
eurjchem-843	78	19	prepared	prepare	VERB
eurjchem-843	78	20	after	after	ADP
eurjchem-843	78	21	its	its	PRON
eurjchem-843	78	22	extraction	extraction	NOUN
eurjchem-843	78	23	as	as	SCONJ
eurjchem-843	78	24	mentioned	mention	VERB
eurjchem-843	78	25	under	under	ADP
eurjchem-843	78	26	section	section	NOUN
eurjchem-843	78	27	2.3	2.3	NUM
eurjchem-843	78	28	with	with	ADP
eurjchem-843	78	29	the	the	DET
eurjchem-843	78	30	same	same	ADJ
eurjchem-843	78	31	conditions	condition	NOUN
eurjchem-843	78	32	under	under	ADP
eurjchem-843	78	33	section	section	NOUN
eurjchem-843	78	34	2.7.1.1	2.7.1.1	NUM
eurjchem-843	78	35	.	.	PUNCT
eurjchem-843	79	1	a	a	DET
eurjchem-843	79	2	calibration	calibration	NOUN
eurjchem-843	79	3	curve	curve	NOUN
eurjchem-843	79	4	was	be	AUX
eurjchem-843	79	5	obtained	obtain	VERB
eurjchem-843	79	6	by	by	ADP
eurjchem-843	79	7	plotting	plot	VERB
eurjchem-843	79	8	area	area	NOUN
eurjchem-843	79	9	under	under	ADP
eurjchem-843	79	10	the	the	DET
eurjchem-843	79	11	peak	peak	NOUN
eurjchem-843	79	12	(	(	PUNCT
eurjchem-843	79	13	aup	aup	PROPN
eurjchem-843	79	14	)	)	PUNCT
eurjchem-843	79	15	against	against	ADP
eurjchem-843	79	16	concentration	concentration	NOUN
eurjchem-843	79	17	(	(	PUNCT
eurjchem-843	79	18	c	c	NOUN
eurjchem-843	79	19	)	)	PUNCT
eurjchem-843	79	20	.	.	PUNCT
eurjchem-843	80	1	the	the	DET
eurjchem-843	80	2	repeatability	repeatability	NOUN
eurjchem-843	80	3	of	of	ADP
eurjchem-843	80	4	the	the	DET
eurjchem-843	80	5	method	method	NOUN
eurjchem-843	80	6	was	be	AUX
eurjchem-843	80	7	assessed	assess	VERB
eurjchem-843	80	8	by	by	ADP
eurjchem-843	80	9	analyzing	analyze	VERB
eurjchem-843	80	10	a	a	DET
eurjchem-843	80	11	mixture	mixture	NOUN
eurjchem-843	80	12	containing	contain	VERB
eurjchem-843	80	13	1.5	1.5	NUM
eurjchem-843	80	14	and	and	CCONJ
eurjchem-843	80	15	5.0	5.0	NUM
eurjchem-843	80	16	µg	µg	NOUN
eurjchem-843	80	17	/	/	SYM
eurjchem-843	80	18	ml	ml	NOUN
eurjchem-843	80	19	of	of	ADP
eurjchem-843	80	20	sdp	sdp	NOUN
eurjchem-843	80	21	and	and	CCONJ
eurjchem-843	80	22	stg	stg	NOUN
eurjchem-843	80	23	,	,	PUNCT
eurjchem-843	80	24	respectively	respectively	ADV
eurjchem-843	80	25	(	(	PUNCT
eurjchem-843	80	26	n	n	NOUN
eurjchem-843	80	27	=	=	SYM
eurjchem-843	80	28	6	6	NUM
eurjchem-843	80	29	)	)	PUNCT
eurjchem-843	80	30	.	.	PUNCT
eurjchem-843	81	1	the	the	DET
eurjchem-843	81	2	precision	precision	NOUN
eurjchem-843	81	3	(	(	PUNCT
eurjchem-843	81	4	%	%	INTJ
eurjchem-843	81	5	r.s.d	r.s.d	NOUN
eurjchem-843	81	6	.	.	PUNCT
eurjchem-843	81	7	)	)	PUNCT
eurjchem-843	81	8	was	be	AUX
eurjchem-843	81	9	calculated	calculate	VERB
eurjchem-843	81	10	,	,	PUNCT
eurjchem-843	81	11	table	table	NOUN
eurjchem-843	81	12	1	1	NUM
eurjchem-843	81	13	.	.	PUNCT
eurjchem-843	81	14	362	362	NUM
eurjchem-843	81	15	yazar	yazar	NOUN
eurjchem-843	81	16	et	et	PROPN
eurjchem-843	81	17	al	al	PROPN
eurjchem-843	81	18	.	.	PUNCT
eurjchem-843	81	19	/	/	SYM
eurjchem-843	81	20	european	european	PROPN
eurjchem-843	81	21	journal	journal	PROPN
eurjchem-843	81	22	of	of	ADP
eurjchem-843	81	23	chemistry	chemistry	NOUN
eurjchem-843	81	24	4	4	NUM
eurjchem-843	81	25	(	(	PUNCT
eurjchem-843	81	26	4	4	NUM
eurjchem-843	81	27	)	)	PUNCT
eurjchem-843	81	28	(	(	PUNCT
eurjchem-843	81	29	2013	2013	NUM
eurjchem-843	81	30	)	)	PUNCT
eurjchem-843	81	31	360‐365	360‐365	NOUN
eurjchem-843	81	32	table	table	NOUN
eurjchem-843	81	33	1	1	NUM
eurjchem-843	81	34	.	.	PUNCT
eurjchem-843	81	35	system	system	NOUN
eurjchem-843	81	36	suitability	suitability	NOUN
eurjchem-843	81	37	tests	test	VERB
eurjchem-843	81	38	for	for	ADP
eurjchem-843	81	39	lc‐fluoro	lc‐fluoro	PROPN
eurjchem-843	81	40	method	method	NOUN
eurjchem-843	81	41	for	for	ADP
eurjchem-843	81	42	the	the	DET
eurjchem-843	81	43	determination	determination	NOUN
eurjchem-843	81	44	of	of	ADP
eurjchem-843	81	45	sitagliptin	sitagliptin	NOUN
eurjchem-843	81	46	in	in	ADP
eurjchem-843	81	47	binary	binary	ADJ
eurjchem-843	81	48	mixture	mixture	NOUN
eurjchem-843	81	49	with	with	ADP
eurjchem-843	81	50	its	its	PRON
eurjchem-843	81	51	acidic	acidic	ADJ
eurjchem-843	81	52	degradation	degradation	NOUN
eurjchem-843	81	53	product	product	NOUN
eurjchem-843	81	54	.	.	PUNCT
eurjchem-843	82	1	item	item	NOUN
eurjchem-843	82	2	*	*	PUNCT
eurjchem-843	82	3	in	in	ADP
eurjchem-843	82	4	laboratory	laboratory	NOUN
eurjchem-843	82	5	mix	mix	NOUN
eurjchem-843	82	6	in	in	ADP
eurjchem-843	82	7	plasma	plasma	NOUN
eurjchem-843	82	8	stg	stg	PROPN
eurjchem-843	82	9	sdp	sdp	PROPN
eurjchem-843	82	10	stg	stg	PROPN
eurjchem-843	82	11	sdp	sdp	PROPN
eurjchem-843	82	12	n	n	PROPN
eurjchem-843	82	13	860	860	NUM
eurjchem-843	82	14	1024	1024	NUM
eurjchem-843	82	15	784	784	NUM
eurjchem-843	82	16	2578	2578	NUM
eurjchem-843	82	17	r	r	NOUN
eurjchem-843	82	18	6.29	6.29	NUM
eurjchem-843	82	19	6.29	6.29	NUM
eurjchem-843	82	20	7.6	7.6	NUM
eurjchem-843	82	21	7.6	7.6	NUM
eurjchem-843	82	22	t	t	PROPN
eurjchem-843	82	23	1.14	1.14	NUM
eurjchem-843	82	24	1.19	1.19	NUM
eurjchem-843	82	25	1.02	1.02	NUM
eurjchem-843	82	26	1.05	1.05	NUM
eurjchem-843	82	27	%	%	NOUN
eurjchem-843	82	28	r.s.d	r.s.d	NOUN
eurjchem-843	82	29	.	.	PUNCT
eurjchem-843	83	1	of	of	ADP
eurjchem-843	83	2	6	6	NUM
eurjchem-843	83	3	injections	injection	NOUN
eurjchem-843	83	4	peak	peak	NOUN
eurjchem-843	83	5	area	area	NOUN
eurjchem-843	83	6	0.38	0.38	NUM
eurjchem-843	83	7	0.43	0.43	NUM
eurjchem-843	83	8	0.48	0.48	NUM
eurjchem-843	83	9	0.36	0.36	NUM
eurjchem-843	83	10	retention	retention	NOUN
eurjchem-843	83	11	time	time	NOUN
eurjchem-843	83	12	0.27	0.27	NUM
eurjchem-843	83	13	0.44	0.44	NUM
eurjchem-843	83	14	0.57	0.57	NUM
eurjchem-843	83	15	0.22	0.22	NUM
eurjchem-843	83	16	*	*	PUNCT
eurjchem-843	83	17	n	n	X
eurjchem-843	83	18	(	(	PUNCT
eurjchem-843	83	19	number	number	NOUN
eurjchem-843	83	20	of	of	ADP
eurjchem-843	83	21	theoretical	theoretical	ADJ
eurjchem-843	83	22	plates	plate	NOUN
eurjchem-843	83	23	)	)	PUNCT
eurjchem-843	83	24	,	,	PUNCT
eurjchem-843	83	25	r	r	NOUN
eurjchem-843	83	26	(	(	PUNCT
eurjchem-843	83	27	peak	peak	NOUN
eurjchem-843	83	28	resolution	resolution	NOUN
eurjchem-843	83	29	factor	factor	NOUN
eurjchem-843	83	30	)	)	PUNCT
eurjchem-843	83	31	,	,	PUNCT
eurjchem-843	83	32	t	t	PROPN
eurjchem-843	83	33	(	(	PUNCT
eurjchem-843	83	34	tailing	tail	VERB
eurjchem-843	83	35	of	of	ADP
eurjchem-843	83	36	chromatographic	chromatographic	ADJ
eurjchem-843	83	37	peak	peak	NOUN
eurjchem-843	83	38	)	)	PUNCT
eurjchem-843	83	39	,	,	PUNCT
eurjchem-843	83	40	and	and	CCONJ
eurjchem-843	83	41	repeatability	repeatability	NOUN
eurjchem-843	83	42	as	as	ADP
eurjchem-843	83	43	%	%	NOUN
eurjchem-843	83	44	r.s.d	r.s.d	NOUN
eurjchem-843	83	45	.	.	PUNCT
eurjchem-843	84	1	of	of	ADP
eurjchem-843	84	2	peak	peak	NOUN
eurjchem-843	84	3	area	area	NOUN
eurjchem-843	84	4	for	for	ADP
eurjchem-843	84	5	six	six	NUM
eurjchem-843	84	6	injections	injection	NOUN
eurjchem-843	84	7	and	and	CCONJ
eurjchem-843	84	8	reproducibility	reproducibility	NOUN
eurjchem-843	84	9	of	of	ADP
eurjchem-843	84	10	retention	retention	NOUN
eurjchem-843	84	11	as	as	ADP
eurjchem-843	84	12	%	%	NOUN
eurjchem-843	84	13	r.s.d	r.s.d	NOUN
eurjchem-843	84	14	.	.	PUNCT
eurjchem-843	85	1	of	of	ADP
eurjchem-843	85	2	retention	retention	NOUN
eurjchem-843	85	3	time	time	NOUN
eurjchem-843	85	4	.	.	PUNCT
eurjchem-843	86	1	table	table	NOUN
eurjchem-843	86	2	2	2	NUM
eurjchem-843	86	3	.	.	X
eurjchem-843	86	4	system	system	NOUN
eurjchem-843	86	5	suitability	suitability	NOUN
eurjchem-843	86	6	tests	test	VERB
eurjchem-843	86	7	for	for	ADP
eurjchem-843	86	8	lc‐uv	lc‐uv	NUM
eurjchem-843	86	9	method	method	NOUN
eurjchem-843	86	10	for	for	ADP
eurjchem-843	86	11	the	the	DET
eurjchem-843	86	12	simultaneous	simultaneous	ADJ
eurjchem-843	86	13	determination	determination	NOUN
eurjchem-843	86	14	of	of	ADP
eurjchem-843	86	15	sitagliptin	sitagliptin	NOUN
eurjchem-843	86	16	and	and	CCONJ
eurjchem-843	86	17	metformin	metformin	NOUN
eurjchem-843	86	18	in	in	ADP
eurjchem-843	86	19	the	the	DET
eurjchem-843	86	20	presence	presence	NOUN
eurjchem-843	86	21	of	of	ADP
eurjchem-843	86	22	sitagliptin	sitagliptin	NOUN
eurjchem-843	86	23	acidic	acidic	ADJ
eurjchem-843	86	24	degradation	degradation	NOUN
eurjchem-843	86	25	product	product	NOUN
eurjchem-843	86	26	.	.	PUNCT
eurjchem-843	87	1	item	item	NOUN
eurjchem-843	87	2	*	*	PUNCT
eurjchem-843	87	3	stg	stg	ADJ
eurjchem-843	87	4	degradation	degradation	NOUN
eurjchem-843	87	5	product	product	NOUN
eurjchem-843	87	6	stg	stg	PROPN
eurjchem-843	87	7	met	meet	VERB
eurjchem-843	87	8	n	n	PROPN
eurjchem-843	87	9	1022	1022	NUM
eurjchem-843	87	10	3136	3136	NUM
eurjchem-843	87	11	1733	1733	NUM
eurjchem-843	87	12	r	r	NOUN
eurjchem-843	87	13	6.5	6.5	NUM
eurjchem-843	87	14	2.1	2.1	NUM
eurjchem-843	87	15	2.1	2.1	NUM
eurjchem-843	87	16	t	t	NOUN
eurjchem-843	87	17	1.09	1.09	NUM
eurjchem-843	87	18	1.01	1.01	NUM
eurjchem-843	87	19	1.05	1.05	NUM
eurjchem-843	87	20	%	%	NOUN
eurjchem-843	87	21	r.s.d	r.s.d	NOUN
eurjchem-843	87	22	.	.	PUNCT
eurjchem-843	88	1	of	of	ADP
eurjchem-843	88	2	6	6	NUM
eurjchem-843	88	3	injections	injection	NOUN
eurjchem-843	88	4	peak	peak	NOUN
eurjchem-843	88	5	area	area	NOUN
eurjchem-843	88	6	0.46	0.46	NUM
eurjchem-843	88	7	0.59	0.59	NUM
eurjchem-843	88	8	0.47	0.47	NUM
eurjchem-843	88	9	retention	retention	NOUN
eurjchem-843	88	10	time	time	NOUN
eurjchem-843	88	11	0.66	0.66	NUM
eurjchem-843	88	12	0.22	0.22	NUM
eurjchem-843	88	13	0.28	0.28	NUM
eurjchem-843	88	14	*	*	PUNCT
eurjchem-843	88	15	n	n	PRON
eurjchem-843	88	16	(	(	PUNCT
eurjchem-843	88	17	number	number	NOUN
eurjchem-843	88	18	of	of	ADP
eurjchem-843	88	19	theoretical	theoretical	ADJ
eurjchem-843	88	20	plates	plate	NOUN
eurjchem-843	88	21	)	)	PUNCT
eurjchem-843	88	22	,	,	PUNCT
eurjchem-843	88	23	r	r	NOUN
eurjchem-843	88	24	(	(	PUNCT
eurjchem-843	88	25	peak	peak	NOUN
eurjchem-843	88	26	resolution	resolution	NOUN
eurjchem-843	88	27	factor	factor	NOUN
eurjchem-843	88	28	)	)	PUNCT
eurjchem-843	88	29	,	,	PUNCT
eurjchem-843	88	30	t	t	PROPN
eurjchem-843	88	31	(	(	PUNCT
eurjchem-843	88	32	tailing	tail	VERB
eurjchem-843	88	33	of	of	ADP
eurjchem-843	88	34	chromatographic	chromatographic	ADJ
eurjchem-843	88	35	peak	peak	NOUN
eurjchem-843	88	36	)	)	PUNCT
eurjchem-843	88	37	,	,	PUNCT
eurjchem-843	88	38	and	and	CCONJ
eurjchem-843	88	39	repeatability	repeatability	NOUN
eurjchem-843	88	40	as	as	ADP
eurjchem-843	88	41	%	%	NOUN
eurjchem-843	88	42	r.s.d	r.s.d	NOUN
eurjchem-843	88	43	.	.	PUNCT
eurjchem-843	89	1	of	of	ADP
eurjchem-843	89	2	peak	peak	NOUN
eurjchem-843	89	3	area	area	NOUN
eurjchem-843	89	4	for	for	ADP
eurjchem-843	89	5	six	six	NUM
eurjchem-843	89	6	injections	injection	NOUN
eurjchem-843	89	7	and	and	CCONJ
eurjchem-843	89	8	reproducibility	reproducibility	NOUN
eurjchem-843	89	9	of	of	ADP
eurjchem-843	89	10	retention	retention	NOUN
eurjchem-843	89	11	as	as	ADP
eurjchem-843	89	12	%	%	NOUN
eurjchem-843	89	13	r.s.d	r.s.d	NOUN
eurjchem-843	89	14	.	.	PUNCT
eurjchem-843	90	1	of	of	ADP
eurjchem-843	90	2	retention	retention	NOUN
eurjchem-843	90	3	time	time	NOUN
eurjchem-843	90	4	.	.	PUNCT
eurjchem-843	91	1	2.7.1.2	2.7.1.2	NUM
eurjchem-843	91	2	.	.	NOUN
eurjchem-843	91	3	lc‐uv	lc‐uv	NOUN
eurjchem-843	91	4	method	method	PROPN
eurjchem-843	91	5	accurately	accurately	ADV
eurjchem-843	91	6	measured	measure	VERB
eurjchem-843	91	7	aliquots	aliquot	NOUN
eurjchem-843	91	8	of	of	ADP
eurjchem-843	91	9	stock	stock	NOUN
eurjchem-843	91	10	solutions	solution	NOUN
eurjchem-843	91	11	equivalent	equivalent	ADJ
eurjchem-843	91	12	to	to	ADP
eurjchem-843	91	13	50‐1600	50‐1600	NUM
eurjchem-843	91	14	µg	µg	ADP
eurjchem-843	91	15	stg	stg	PROPN
eurjchem-843	91	16	and	and	CCONJ
eurjchem-843	91	17	250‐8000	250‐8000	NUM
eurjchem-843	91	18	µg	µg	ADV
eurjchem-843	91	19	met	meet	VERB
eurjchem-843	91	20	were	be	AUX
eurjchem-843	91	21	separately	separately	ADV
eurjchem-843	91	22	transferred	transfer	VERB
eurjchem-843	91	23	into	into	ADP
eurjchem-843	91	24	two	two	NUM
eurjchem-843	91	25	series	series	NOUN
eurjchem-843	91	26	of	of	ADP
eurjchem-843	91	27	10	10	NUM
eurjchem-843	91	28	ml	ml	NOUN
eurjchem-843	91	29	volumetric	volumetric	ADJ
eurjchem-843	91	30	flasks	flask	NOUN
eurjchem-843	91	31	and	and	CCONJ
eurjchem-843	91	32	then	then	ADV
eurjchem-843	91	33	completed	complete	VERB
eurjchem-843	91	34	to	to	PART
eurjchem-843	91	35	volume	volume	VERB
eurjchem-843	91	36	with	with	ADP
eurjchem-843	91	37	methanol	methanol	NOUN
eurjchem-843	91	38	.	.	PUNCT
eurjchem-843	92	1	a	a	DET
eurjchem-843	92	2	volume	volume	NOUN
eurjchem-843	92	3	of	of	ADP
eurjchem-843	92	4	25	25	NUM
eurjchem-843	92	5	µl	µl	NOUN
eurjchem-843	92	6	of	of	ADP
eurjchem-843	92	7	each	each	DET
eurjchem-843	92	8	solution	solution	NOUN
eurjchem-843	92	9	was	be	AUX
eurjchem-843	92	10	injected	inject	VERB
eurjchem-843	92	11	into	into	ADP
eurjchem-843	92	12	the	the	DET
eurjchem-843	92	13	chromatograph	chromatograph	NOUN
eurjchem-843	92	14	.	.	PUNCT
eurjchem-843	93	1	the	the	DET
eurjchem-843	93	2	conditions	condition	NOUN
eurjchem-843	93	3	including	include	VERB
eurjchem-843	93	4	the	the	DET
eurjchem-843	93	5	mobile	mobile	ADJ
eurjchem-843	93	6	phase	phase	NOUN
eurjchem-843	93	7	at	at	ADP
eurjchem-843	93	8	a	a	DET
eurjchem-843	93	9	flow	flow	NOUN
eurjchem-843	93	10	rate	rate	NOUN
eurjchem-843	93	11	1	1	NUM
eurjchem-843	93	12	ml	ml	NOUN
eurjchem-843	93	13	/	/	SYM
eurjchem-843	93	14	min	min	NOUN
eurjchem-843	93	15	,	,	PUNCT
eurjchem-843	93	16	detection	detection	NOUN
eurjchem-843	93	17	at	at	ADP
eurjchem-843	93	18	220	220	NUM
eurjchem-843	93	19	nm	nm	NOUN
eurjchem-843	93	20	and	and	CCONJ
eurjchem-843	93	21	run	run	VERB
eurjchem-843	93	22	time	time	NOUN
eurjchem-843	93	23	program	program	NOUN
eurjchem-843	93	24	for	for	ADP
eurjchem-843	93	25	10	10	NUM
eurjchem-843	93	26	min	min	NOUN
eurjchem-843	93	27	were	be	AUX
eurjchem-843	93	28	adjusted	adjust	VERB
eurjchem-843	93	29	.	.	PUNCT
eurjchem-843	94	1	a	a	DET
eurjchem-843	94	2	calibration	calibration	NOUN
eurjchem-843	94	3	curve	curve	NOUN
eurjchem-843	94	4	for	for	ADP
eurjchem-843	94	5	each	each	DET
eurjchem-843	94	6	compound	compound	NOUN
eurjchem-843	94	7	was	be	AUX
eurjchem-843	94	8	obtained	obtain	VERB
eurjchem-843	94	9	by	by	ADP
eurjchem-843	94	10	plotting	plot	VERB
eurjchem-843	94	11	area	area	NOUN
eurjchem-843	94	12	under	under	ADP
eurjchem-843	94	13	the	the	DET
eurjchem-843	94	14	peak	peak	NOUN
eurjchem-843	94	15	(	(	PUNCT
eurjchem-843	94	16	aup	aup	PROPN
eurjchem-843	94	17	)	)	PUNCT
eurjchem-843	94	18	against	against	ADP
eurjchem-843	94	19	concentration	concentration	NOUN
eurjchem-843	94	20	(	(	PUNCT
eurjchem-843	94	21	c	c	NOUN
eurjchem-843	94	22	)	)	PUNCT
eurjchem-843	94	23	.	.	PUNCT
eurjchem-843	95	1	the	the	DET
eurjchem-843	95	2	repeatability	repeatability	NOUN
eurjchem-843	95	3	of	of	ADP
eurjchem-843	95	4	the	the	DET
eurjchem-843	95	5	method	method	NOUN
eurjchem-843	95	6	was	be	AUX
eurjchem-843	95	7	assessed	assess	VERB
eurjchem-843	95	8	by	by	ADP
eurjchem-843	95	9	analyzing	analyze	VERB
eurjchem-843	95	10	a	a	DET
eurjchem-843	95	11	mixture	mixture	NOUN
eurjchem-843	95	12	containing	contain	VERB
eurjchem-843	95	13	25.7	25.7	NUM
eurjchem-843	95	14	,	,	PUNCT
eurjchem-843	95	15	400.0	400.0	NUM
eurjchem-843	95	16	and	and	CCONJ
eurjchem-843	95	17	7.7	7.7	NUM
eurjchem-843	95	18	µg	µg	NOUN
eurjchem-843	95	19	/	/	SYM
eurjchem-843	95	20	ml	ml	NOUN
eurjchem-843	95	21	of	of	ADP
eurjchem-843	95	22	stg	stg	NOUN
eurjchem-843	95	23	,	,	PUNCT
eurjchem-843	95	24	met	meet	VERB
eurjchem-843	95	25	and	and	CCONJ
eurjchem-843	95	26	sdp	sdp	NOUN
eurjchem-843	95	27	,	,	PUNCT
eurjchem-843	95	28	respectively	respectively	ADV
eurjchem-843	95	29	(	(	PUNCT
eurjchem-843	95	30	n	n	NOUN
eurjchem-843	95	31	=	=	SYM
eurjchem-843	95	32	6	6	NUM
eurjchem-843	95	33	)	)	PUNCT
eurjchem-843	95	34	.	.	PUNCT
eurjchem-843	96	1	this	this	DET
eurjchem-843	96	2	mixture	mixture	NOUN
eurjchem-843	96	3	was	be	AUX
eurjchem-843	96	4	considered	consider	VERB
eurjchem-843	96	5	as	as	ADP
eurjchem-843	96	6	the	the	DET
eurjchem-843	96	7	working	work	VERB
eurjchem-843	96	8	standard	standard	ADJ
eurjchem-843	96	9	solution	solution	NOUN
eurjchem-843	96	10	.	.	PUNCT
eurjchem-843	97	1	the	the	DET
eurjchem-843	97	2	precision	precision	NOUN
eurjchem-843	97	3	(	(	PUNCT
eurjchem-843	97	4	%	%	INTJ
eurjchem-843	97	5	r.s.d	r.s.d	NOUN
eurjchem-843	97	6	.	.	PUNCT
eurjchem-843	97	7	)	)	PUNCT
eurjchem-843	98	1	values	value	NOUN
eurjchem-843	98	2	of	of	ADP
eurjchem-843	98	3	peak	peak	NOUN
eurjchem-843	98	4	areas	area	NOUN
eurjchem-843	98	5	and	and	CCONJ
eurjchem-843	98	6	retention	retention	NOUN
eurjchem-843	98	7	times	time	NOUN
eurjchem-843	98	8	were	be	AUX
eurjchem-843	98	9	calculated	calculate	VERB
eurjchem-843	98	10	for	for	ADP
eurjchem-843	98	11	each	each	DET
eurjchem-843	98	12	compound	compound	NOUN
eurjchem-843	98	13	,	,	PUNCT
eurjchem-843	98	14	table	table	NOUN
eurjchem-843	98	15	2	2	NUM
eurjchem-843	98	16	.	.	PUNCT
eurjchem-843	98	17	2.7.2	2.7.2	NUM
eurjchem-843	98	18	.	.	X
eurjchem-843	99	1	assay	assay	PROPN
eurjchem-843	99	2	of	of	ADP
eurjchem-843	99	3	laboratory	laboratory	NOUN
eurjchem-843	99	4	prepared	prepare	VERB
eurjchem-843	99	5	mixtures	mixture	NOUN
eurjchem-843	99	6	,	,	PUNCT
eurjchem-843	99	7	plasma	plasma	NOUN
eurjchem-843	99	8	and	and	CCONJ
eurjchem-843	99	9	januvia	januvia	NOUN
eurjchem-843	99	10	®	®	NOUN
eurjchem-843	99	11	tablets	tablet	VERB
eurjchem-843	99	12	the	the	DET
eurjchem-843	99	13	procedure	procedure	NOUN
eurjchem-843	99	14	mentioned	mention	VERB
eurjchem-843	99	15	under	under	ADP
eurjchem-843	99	16	section	section	NOUN
eurjchem-843	99	17	2.7.1.1	2.7.1.1	NUM
eurjchem-843	99	18	was	be	AUX
eurjchem-843	99	19	repeated	repeat	VERB
eurjchem-843	99	20	using	use	VERB
eurjchem-843	99	21	concentrations	concentration	NOUN
eurjchem-843	99	22	equivalent	equivalent	ADJ
eurjchem-843	99	23	to	to	ADP
eurjchem-843	99	24	10‐185	10‐185	NUM
eurjchem-843	99	25	µg	µg	NOUN
eurjchem-843	99	26	/	/	SYM
eurjchem-843	99	27	ml	ml	ADP
eurjchem-843	99	28	stg	stg	NOUN
eurjchem-843	99	29	and	and	CCONJ
eurjchem-843	99	30	3‐55	3‐55	NUM
eurjchem-843	99	31	µg	µg	ADJ
eurjchem-843	99	32	/	/	SYM
eurjchem-843	99	33	ml	ml	NOUN
eurjchem-843	99	34	sdp	sdp	NOUN
eurjchem-843	99	35	(	(	PUNCT
eurjchem-843	99	36	10	10	NUM
eurjchem-843	99	37	%	%	NOUN
eurjchem-843	99	38	to	to	PART
eurjchem-843	99	39	30	30	NUM
eurjchem-843	99	40	%	%	NOUN
eurjchem-843	99	41	of	of	ADP
eurjchem-843	99	42	stg	stg	PROPN
eurjchem-843	99	43	,	,	PUNCT
eurjchem-843	99	44	w	w	NOUN
eurjchem-843	99	45	:	:	SYM
eurjchem-843	99	46	w	w	NOUN
eurjchem-843	99	47	)	)	PUNCT
eurjchem-843	99	48	and	and	CCONJ
eurjchem-843	99	49	equivalent	equivalent	ADJ
eurjchem-843	99	50	to	to	ADP
eurjchem-843	99	51	1.0‐7.5	1.0‐7.5	NUM
eurjchem-843	99	52	µg	µg	ADJ
eurjchem-843	99	53	/	/	SYM
eurjchem-843	99	54	ml	ml	ADP
eurjchem-843	99	55	stg	stg	NOUN
eurjchem-843	99	56	and	and	CCONJ
eurjchem-843	99	57	0.3‐2.0	0.3‐2.0	NUM
eurjchem-843	99	58	µg	µg	NOUN
eurjchem-843	99	59	/	/	SYM
eurjchem-843	99	60	ml	ml	ADV
eurjchem-843	99	61	sdp	sdp	NOUN
eurjchem-843	99	62	(	(	PUNCT
eurjchem-843	99	63	10	10	NUM
eurjchem-843	99	64	%	%	NOUN
eurjchem-843	99	65	to	to	PART
eurjchem-843	99	66	30	30	NUM
eurjchem-843	99	67	%	%	NOUN
eurjchem-843	99	68	of	of	ADP
eurjchem-843	99	69	stg	stg	PROPN
eurjchem-843	99	70	,	,	PUNCT
eurjchem-843	99	71	w	w	NOUN
eurjchem-843	99	72	:	:	PUNCT
eurjchem-843	99	73	w	w	NOUN
eurjchem-843	99	74	)	)	PUNCT
eurjchem-843	99	75	.	.	PUNCT
eurjchem-843	100	1	for	for	ADP
eurjchem-843	100	2	the	the	DET
eurjchem-843	100	3	determination	determination	NOUN
eurjchem-843	100	4	of	of	ADP
eurjchem-843	100	5	stg	stg	PROPN
eurjchem-843	100	6	in	in	ADP
eurjchem-843	100	7	januvia	januvia	PROPN
eurjchem-843	100	8	®	®	NOUN
eurjchem-843	100	9	tablets	tablet	NOUN
eurjchem-843	100	10	,	,	PUNCT
eurjchem-843	100	11	the	the	DET
eurjchem-843	100	12	sample	sample	NOUN
eurjchem-843	100	13	solution	solution	NOUN
eurjchem-843	100	14	prepared	prepare	VERB
eurjchem-843	100	15	under	under	ADP
eurjchem-843	100	16	section	section	NOUN
eurjchem-843	100	17	2.6	2.6	NUM
eurjchem-843	100	18	was	be	AUX
eurjchem-843	100	19	serially	serially	ADV
eurjchem-843	100	20	diluted	dilute	VERB
eurjchem-843	100	21	and	and	CCONJ
eurjchem-843	100	22	then	then	ADV
eurjchem-843	100	23	injected	inject	VERB
eurjchem-843	100	24	in	in	ADP
eurjchem-843	100	25	triplicates	triplicate	NOUN
eurjchem-843	100	26	.	.	PUNCT
eurjchem-843	101	1	the	the	DET
eurjchem-843	101	2	concentrations	concentration	NOUN
eurjchem-843	101	3	of	of	ADP
eurjchem-843	101	4	stg	stg	PROPN
eurjchem-843	101	5	were	be	AUX
eurjchem-843	101	6	calculated	calculate	VERB
eurjchem-843	101	7	using	use	VERB
eurjchem-843	101	8	calibration	calibration	NOUN
eurjchem-843	101	9	equation	equation	NOUN
eurjchem-843	101	10	.	.	PUNCT
eurjchem-843	102	1	2.7.3	2.7.3	X
eurjchem-843	102	2	.	.	PUNCT
eurjchem-843	103	1	assay	assay	PROPN
eurjchem-843	103	2	of	of	ADP
eurjchem-843	103	3	laboratory	laboratory	NOUN
eurjchem-843	103	4	prepared	prepare	VERB
eurjchem-843	103	5	mixtures	mixture	NOUN
eurjchem-843	103	6	and	and	CCONJ
eurjchem-843	103	7	janumet	janumet	ADJ
eurjchem-843	103	8	®	®	NOUN
eurjchem-843	103	9	tablets	tablet	VERB
eurjchem-843	103	10	the	the	DET
eurjchem-843	103	11	procedure	procedure	NOUN
eurjchem-843	103	12	mentioned	mention	VERB
eurjchem-843	103	13	under	under	ADP
eurjchem-843	103	14	section	section	NOUN
eurjchem-843	103	15	2.7.1.2	2.7.1.2	NUM
eurjchem-843	103	16	was	be	AUX
eurjchem-843	103	17	repeated	repeat	VERB
eurjchem-843	103	18	for	for	ADP
eurjchem-843	103	19	the	the	DET
eurjchem-843	103	20	determination	determination	NOUN
eurjchem-843	103	21	of	of	ADP
eurjchem-843	103	22	laboratory	laboratory	NOUN
eurjchem-843	103	23	prepared	prepare	VERB
eurjchem-843	103	24	mixtures	mixture	NOUN
eurjchem-843	103	25	equivalent	equivalent	ADJ
eurjchem-843	103	26	to	to	ADP
eurjchem-843	103	27	10‐45	10‐45	NUM
eurjchem-843	103	28	µg	µg	ADJ
eurjchem-843	103	29	/	/	SYM
eurjchem-843	103	30	ml	ml	NOUN
eurjchem-843	103	31	stg	stg	NOUN
eurjchem-843	103	32	,	,	PUNCT
eurjchem-843	103	33	155.6‐700.4	155.6‐700.4	NUM
eurjchem-843	103	34	µg	µg	NOUN
eurjchem-843	103	35	/	/	SYM
eurjchem-843	103	36	ml	ml	VERB
eurjchem-843	103	37	met	meet	VERB
eurjchem-843	103	38	and	and	CCONJ
eurjchem-843	103	39	3.0‐13.5	3.0‐13.5	NUM
eurjchem-843	103	40	µg	µg	ADJ
eurjchem-843	103	41	/	/	SYM
eurjchem-843	103	42	ml	ml	NOUN
eurjchem-843	103	43	sdp	sdp	NOUN
eurjchem-843	103	44	(	(	PUNCT
eurjchem-843	103	45	10	10	NUM
eurjchem-843	103	46	%	%	NOUN
eurjchem-843	103	47	to	to	PART
eurjchem-843	103	48	30	30	NUM
eurjchem-843	103	49	%	%	NOUN
eurjchem-843	103	50	of	of	ADP
eurjchem-843	103	51	stg	stg	PROPN
eurjchem-843	103	52	,	,	PUNCT
eurjchem-843	103	53	w	w	NOUN
eurjchem-843	103	54	:	:	PUNCT
eurjchem-843	103	55	w	w	NOUN
eurjchem-843	103	56	)	)	PUNCT
eurjchem-843	103	57	.	.	PUNCT
eurjchem-843	104	1	for	for	ADP
eurjchem-843	104	2	the	the	DET
eurjchem-843	104	3	determination	determination	NOUN
eurjchem-843	104	4	of	of	ADP
eurjchem-843	104	5	the	the	DET
eurjchem-843	104	6	examined	examine	VERB
eurjchem-843	104	7	drugs	drug	NOUN
eurjchem-843	104	8	in	in	ADP
eurjchem-843	104	9	janumet	janumet	ADJ
eurjchem-843	104	10	®	®	NOUN
eurjchem-843	104	11	tablets	tablet	NOUN
eurjchem-843	104	12	,	,	PUNCT
eurjchem-843	104	13	the	the	DET
eurjchem-843	104	14	sample	sample	NOUN
eurjchem-843	104	15	solution	solution	NOUN
eurjchem-843	104	16	prepared	prepare	VERB
eurjchem-843	104	17	under	under	ADP
eurjchem-843	104	18	section	section	NOUN
eurjchem-843	104	19	2.6	2.6	NUM
eurjchem-843	104	20	was	be	AUX
eurjchem-843	104	21	serially	serially	ADV
eurjchem-843	104	22	diluted	dilute	VERB
eurjchem-843	104	23	to	to	PART
eurjchem-843	104	24	prepare	prepare	VERB
eurjchem-843	104	25	solutions	solution	NOUN
eurjchem-843	104	26	equivalent	equivalent	ADJ
eurjchem-843	104	27	to	to	ADP
eurjchem-843	104	28	10‐45	10‐45	NUM
eurjchem-843	104	29	,	,	PUNCT
eurjchem-843	104	30	155.6‐700.4	155.6‐700.4	NUM
eurjchem-843	104	31	µg	µg	NOUN
eurjchem-843	104	32	/	/	SYM
eurjchem-843	104	33	ml	ml	NOUN
eurjchem-843	104	34	of	of	ADP
eurjchem-843	104	35	stg	stg	PROPN
eurjchem-843	104	36	and	and	CCONJ
eurjchem-843	104	37	met	meet	VERB
eurjchem-843	104	38	,	,	PUNCT
eurjchem-843	104	39	respectively	respectively	ADV
eurjchem-843	104	40	;	;	PUNCT
eurjchem-843	104	41	and	and	CCONJ
eurjchem-843	104	42	then	then	ADV
eurjchem-843	104	43	injected	inject	VERB
eurjchem-843	104	44	in	in	ADP
eurjchem-843	104	45	triplicates	triplicate	NOUN
eurjchem-843	104	46	.	.	PUNCT
eurjchem-843	105	1	the	the	DET
eurjchem-843	105	2	concentrations	concentration	NOUN
eurjchem-843	105	3	of	of	ADP
eurjchem-843	105	4	the	the	DET
eurjchem-843	105	5	examined	examine	VERB
eurjchem-843	105	6	drugs	drug	NOUN
eurjchem-843	105	7	were	be	AUX
eurjchem-843	105	8	calculated	calculate	VERB
eurjchem-843	105	9	using	use	VERB
eurjchem-843	105	10	calibration	calibration	NOUN
eurjchem-843	105	11	equations	equation	NOUN
eurjchem-843	105	12	.	.	PUNCT
eurjchem-843	106	1	3	3	X
eurjchem-843	106	2	.	.	NOUN
eurjchem-843	106	3	results	result	NOUN
eurjchem-843	106	4	and	and	CCONJ
eurjchem-843	106	5	discussion	discussion	NOUN
eurjchem-843	106	6	sdp	sdp	NOUN
eurjchem-843	106	7	was	be	AUX
eurjchem-843	106	8	prepared	prepare	VERB
eurjchem-843	106	9	after	after	ADP
eurjchem-843	106	10	acidic	acidic	ADJ
eurjchem-843	106	11	hydrolysis	hydrolysis	NOUN
eurjchem-843	106	12	of	of	ADP
eurjchem-843	106	13	the	the	DET
eurjchem-843	106	14	amide	amide	NOUN
eurjchem-843	106	15	bond	bond	NOUN
eurjchem-843	106	16	of	of	ADP
eurjchem-843	106	17	the	the	DET
eurjchem-843	106	18	intact	intact	ADJ
eurjchem-843	106	19	drug	drug	NOUN
eurjchem-843	106	20	.	.	PUNCT
eurjchem-843	107	1	complete	complete	ADJ
eurjchem-843	107	2	degradation	degradation	NOUN
eurjchem-843	107	3	was	be	AUX
eurjchem-843	107	4	confirmed	confirm	VERB
eurjchem-843	107	5	using	use	VERB
eurjchem-843	107	6	tlc	tlc	NOUN
eurjchem-843	107	7	plates	plate	NOUN
eurjchem-843	107	8	.	.	PUNCT
eurjchem-843	108	1	structure	structure	NOUN
eurjchem-843	108	2	elucidation	elucidation	NOUN
eurjchem-843	108	3	of	of	ADP
eurjchem-843	108	4	the	the	DET
eurjchem-843	108	5	obtained	obtain	VERB
eurjchem-843	108	6	secondary	secondary	ADJ
eurjchem-843	108	7	amine	amine	NOUN
eurjchem-843	108	8	was	be	AUX
eurjchem-843	108	9	confirmed	confirm	VERB
eurjchem-843	108	10	using	use	VERB
eurjchem-843	108	11	infra‐red	infra‐re	VERB
eurjchem-843	108	12	,	,	PUNCT
eurjchem-843	108	13	mass	mass	ADJ
eurjchem-843	108	14	and	and	CCONJ
eurjchem-843	108	15	1h	1h	NUM
eurjchem-843	108	16	nmr	nmr	NOUN
eurjchem-843	108	17	spectroscopic	spectroscopic	NOUN
eurjchem-843	108	18	techniques	technique	NOUN
eurjchem-843	108	19	and	and	CCONJ
eurjchem-843	108	20	proved	prove	VERB
eurjchem-843	108	21	to	to	PART
eurjchem-843	108	22	be	be	AUX
eurjchem-843	108	23	:	:	PUNCT
eurjchem-843	108	24	3‐amino‐4‐(2,4,5‐	3‐amino‐4‐(2,4,5‐	NUM
eurjchem-843	108	25	trifluorophenyl	trifluorophenyl	NOUN
eurjchem-843	108	26	)	)	PUNCT
eurjchem-843	108	27	butanoic	butanoic	NOUN
eurjchem-843	108	28	acid	acid	NOUN
eurjchem-843	108	29	.	.	PUNCT
eurjchem-843	109	1	it	it	PRON
eurjchem-843	109	2	is	be	AUX
eurjchem-843	109	3	worth	worth	ADJ
eurjchem-843	109	4	noting	note	VERB
eurjchem-843	109	5	that	that	SCONJ
eurjchem-843	109	6	the	the	DET
eurjchem-843	109	7	other	other	ADJ
eurjchem-843	109	8	hydrolysis	hydrolysis	NOUN
eurjchem-843	109	9	product	product	NOUN
eurjchem-843	109	10	which	which	PRON
eurjchem-843	109	11	is	be	AUX
eurjchem-843	109	12	:	:	PUNCT
eurjchem-843	109	13	3‐(trifluoromethyl)‐5,6,7,8‐tetra	3‐(trifluoromethyl)‐5,6,7,8‐tetra	NUM
eurjchem-843	109	14	hydro‐[1,2,4]triazolo[4,3‐a]pyrazine	hydro‐[1,2,4]triazolo[4,3‐a]pyrazine	PRON
eurjchem-843	109	15	could	could	AUX
eurjchem-843	109	16	not	not	PART
eurjchem-843	109	17	be	be	AUX
eurjchem-843	109	18	separated	separate	VERB
eurjchem-843	109	19	from	from	ADP
eurjchem-843	109	20	the	the	DET
eurjchem-843	109	21	reaction	reaction	NOUN
eurjchem-843	109	22	medium	medium	NOUN
eurjchem-843	109	23	with	with	ADP
eurjchem-843	109	24	the	the	DET
eurjchem-843	109	25	acid	acid	NOUN
eurjchem-843	110	1	but	but	CCONJ
eurjchem-843	110	2	it	it	PRON
eurjchem-843	110	3	was	be	AUX
eurjchem-843	110	4	studied	study	VERB
eurjchem-843	110	5	in	in	ADP
eurjchem-843	110	6	a	a	DET
eurjchem-843	110	7	previous	previous	ADJ
eurjchem-843	110	8	work	work	NOUN
eurjchem-843	110	9	by	by	ADP
eurjchem-843	110	10	the	the	DET
eurjchem-843	110	11	same	same	ADJ
eurjchem-843	110	12	authors	author	NOUN
eurjchem-843	110	13	of	of	ADP
eurjchem-843	110	14	this	this	DET
eurjchem-843	110	15	work	work	NOUN
eurjchem-843	110	16	[	[	X
eurjchem-843	110	17	7	7	NUM
eurjchem-843	110	18	]	]	PUNCT
eurjchem-843	110	19	.	.	PUNCT
eurjchem-843	111	1	the	the	DET
eurjchem-843	111	2	ir	ir	PROPN
eurjchem-843	111	3	spectrum	spectrum	NOUN
eurjchem-843	111	4	of	of	ADP
eurjchem-843	111	5	sdp	sdp	NOUN
eurjchem-843	111	6	showed	show	VERB
eurjchem-843	111	7	the	the	DET
eurjchem-843	111	8	shift	shift	NOUN
eurjchem-843	111	9	of	of	ADP
eurjchem-843	111	10	the	the	DET
eurjchem-843	111	11	characteristic	characteristic	ADJ
eurjchem-843	111	12	peak	peak	NOUN
eurjchem-843	111	13	of	of	ADP
eurjchem-843	111	14	the	the	DET
eurjchem-843	111	15	carbonyl	carbonyl	NOUN
eurjchem-843	111	16	group	group	NOUN
eurjchem-843	111	17	of	of	ADP
eurjchem-843	111	18	the	the	DET
eurjchem-843	111	19	amide	amide	NOUN
eurjchem-843	111	20	bond	bond	NOUN
eurjchem-843	111	21	at	at	ADP
eurjchem-843	111	22	1639	1639	NUM
eurjchem-843	111	23	to	to	ADP
eurjchem-843	111	24	1697	1697	NUM
eurjchem-843	111	25	cm‐1	cm‐1	NOUN
eurjchem-843	111	26	which	which	PRON
eurjchem-843	111	27	is	be	AUX
eurjchem-843	111	28	the	the	DET
eurjchem-843	111	29	characteristic	characteristic	ADJ
eurjchem-843	111	30	peak	peak	NOUN
eurjchem-843	111	31	of	of	ADP
eurjchem-843	111	32	the	the	DET
eurjchem-843	111	33	carbonyl	carbonyl	NOUN
eurjchem-843	111	34	group	group	NOUN
eurjchem-843	111	35	of	of	ADP
eurjchem-843	111	36	the	the	DET
eurjchem-843	111	37	carboxylic	carboxylic	ADJ
eurjchem-843	111	38	acid	acid	NOUN
eurjchem-843	111	39	in	in	ADP
eurjchem-843	111	40	addition	addition	NOUN
eurjchem-843	111	41	to	to	ADP
eurjchem-843	111	42	the	the	DET
eurjchem-843	111	43	appearance	appearance	NOUN
eurjchem-843	111	44	of	of	ADP
eurjchem-843	111	45	the	the	DET
eurjchem-843	111	46	characteristic	characteristic	ADJ
eurjchem-843	111	47	broad	broad	ADJ
eurjchem-843	111	48	peak	peak	NOUN
eurjchem-843	111	49	of	of	ADP
eurjchem-843	111	50	the	the	DET
eurjchem-843	111	51	oh	oh	INTJ
eurjchem-843	111	52	of	of	ADP
eurjchem-843	111	53	the	the	DET
eurjchem-843	111	54	carboxylic	carboxylic	ADJ
eurjchem-843	111	55	group	group	NOUN
eurjchem-843	111	56	.	.	PUNCT
eurjchem-843	112	1	the	the	DET
eurjchem-843	112	2	characteristic	characteristic	ADJ
eurjchem-843	112	3	forked	fork	VERB
eurjchem-843	112	4	band	band	NOUN
eurjchem-843	112	5	of	of	ADP
eurjchem-843	112	6	the	the	DET
eurjchem-843	112	7	amino	amino	NOUN
eurjchem-843	112	8	group	group	NOUN
eurjchem-843	112	9	appears	appear	VERB
eurjchem-843	112	10	at	at	ADP
eurjchem-843	112	11	about	about	ADV
eurjchem-843	112	12	3100	3100	NUM
eurjchem-843	112	13	cm‐1	cm‐1	NOUN
eurjchem-843	112	14	due	due	ADP
eurjchem-843	112	15	to	to	ADP
eurjchem-843	112	16	the	the	DET
eurjchem-843	112	17	effect	effect	NOUN
eurjchem-843	112	18	of	of	ADP
eurjchem-843	112	19	hydrogen	hydrogen	NOUN
eurjchem-843	112	20	bonding	bonding	NOUN
eurjchem-843	112	21	with	with	ADP
eurjchem-843	112	22	the	the	DET
eurjchem-843	112	23	neighboring	neighboring	NOUN
eurjchem-843	112	24	fluoride	fluoride	NOUN
eurjchem-843	112	25	atom	atom	NOUN
eurjchem-843	112	26	,	,	PUNCT
eurjchem-843	112	27	which	which	PRON
eurjchem-843	112	28	is	be	AUX
eurjchem-843	112	29	a	a	DET
eurjchem-843	112	30	strong	strong	ADJ
eurjchem-843	112	31	hydrogen	hydrogen	NOUN
eurjchem-843	112	32	bond	bond	NOUN
eurjchem-843	112	33	acceptor	acceptor	NOUN
eurjchem-843	112	34	.	.	PUNCT
eurjchem-843	113	1	besides	besides	SCONJ
eurjchem-843	113	2	,	,	PUNCT
eurjchem-843	113	3	mass	mass	ADJ
eurjchem-843	113	4	spectroscopy	spectroscopy	NOUN
eurjchem-843	113	5	confirmed	confirm	VERB
eurjchem-843	113	6	the	the	DET
eurjchem-843	113	7	complete	complete	ADJ
eurjchem-843	113	8	hydrolysis	hydrolysis	NOUN
eurjchem-843	113	9	of	of	ADP
eurjchem-843	113	10	stg	stg	NOUN
eurjchem-843	113	11	showing	show	VERB
eurjchem-843	113	12	the	the	DET
eurjchem-843	113	13	molecular	molecular	ADJ
eurjchem-843	113	14	weight	weight	NOUN
eurjchem-843	113	15	of	of	ADP
eurjchem-843	113	16	the	the	DET
eurjchem-843	113	17	obtained	obtain	VERB
eurjchem-843	113	18	sdp	sdp	NOUN
eurjchem-843	113	19	at	at	ADP
eurjchem-843	113	20	233	233	NUM
eurjchem-843	113	21	m	m	NOUN
eurjchem-843	113	22	/	/	SYM
eurjchem-843	113	23	z.	z.	PROPN
eurjchem-843	113	24	finally	finally	ADV
eurjchem-843	113	25	,	,	PUNCT
eurjchem-843	113	26	1h	1h	NUM
eurjchem-843	113	27	nmr	nmr	NOUN
eurjchem-843	113	28	showed	show	VERB
eurjchem-843	113	29	the	the	DET
eurjchem-843	113	30	appearance	appearance	NOUN
eurjchem-843	113	31	of	of	ADP
eurjchem-843	113	32	the	the	DET
eurjchem-843	113	33	h	h	NOUN
eurjchem-843	113	34	at	at	ADP
eurjchem-843	113	35	12.4	12.4	NUM
eurjchem-843	113	36	ppm	ppm	NUM
eurjchem-843	113	37	which	which	PRON
eurjchem-843	113	38	confirmed	confirm	VERB
eurjchem-843	113	39	the	the	DET
eurjchem-843	113	40	acid	acid	NOUN
eurjchem-843	113	41	product	product	NOUN
eurjchem-843	113	42	and	and	CCONJ
eurjchem-843	113	43	also	also	ADV
eurjchem-843	113	44	showed	show	VERB
eurjchem-843	113	45	the	the	DET
eurjchem-843	113	46	absence	absence	NOUN
eurjchem-843	113	47	of	of	ADP
eurjchem-843	113	48	the	the	DET
eurjchem-843	113	49	heterocyclic	heterocyclic	ADJ
eurjchem-843	113	50	hydrogens	hydrogen	NOUN
eurjchem-843	113	51	which	which	PRON
eurjchem-843	113	52	ensure	ensure	VERB
eurjchem-843	113	53	the	the	DET
eurjchem-843	113	54	degradation	degradation	NOUN
eurjchem-843	113	55	.	.	PUNCT
eurjchem-843	114	1	3.1	3.1	NUM
eurjchem-843	114	2	.	.	PUNCT
eurjchem-843	114	3	methods	method	NOUN
eurjchem-843	114	4	development	development	VERB
eurjchem-843	114	5	3.1.1	3.1.1	NUM
eurjchem-843	114	6	.	.	PUNCT
eurjchem-843	115	1	lc‐fluoro	lc‐fluoro	PROPN
eurjchem-843	115	2	method	method	VERB
eurjchem-843	115	3	various	various	ADJ
eurjchem-843	115	4	reversed‐phase	reversed‐phase	NOUN
eurjchem-843	115	5	columns	column	NOUN
eurjchem-843	115	6	,	,	PUNCT
eurjchem-843	115	7	isocratic	isocratic	ADJ
eurjchem-843	115	8	mobile	mobile	ADJ
eurjchem-843	115	9	phase	phase	NOUN
eurjchem-843	115	10	systems	system	NOUN
eurjchem-843	115	11	and	and	CCONJ
eurjchem-843	115	12	different	different	ADJ
eurjchem-843	115	13	ph	ph	ADJ
eurjchem-843	115	14	values	value	NOUN
eurjchem-843	115	15	of	of	ADP
eurjchem-843	115	16	the	the	DET
eurjchem-843	115	17	buffer	buffer	NOUN
eurjchem-843	115	18	were	be	AUX
eurjchem-843	115	19	attempted	attempt	VERB
eurjchem-843	115	20	.	.	PUNCT
eurjchem-843	116	1	isocratic	isocratic	ADJ
eurjchem-843	116	2	elution	elution	NOUN
eurjchem-843	116	3	based	base	VERB
eurjchem-843	116	4	on	on	ADP
eurjchem-843	116	5	potassium	potassium	NOUN
eurjchem-843	116	6	dihydrogen	dihydrogen	NOUN
eurjchem-843	116	7	phosphate	phosphate	NOUN
eurjchem-843	116	8	buffer	buffer	NOUN
eurjchem-843	116	9	(	(	PUNCT
eurjchem-843	116	10	ph	ph	NOUN
eurjchem-843	116	11	=	=	NOUN
eurjchem-843	116	12	4.6	4.6	NUM
eurjchem-843	116	13	)	)	PUNCT
eurjchem-843	116	14	‐	‐	ADJ
eurjchem-843	116	15	acetonitrile	acetonitrile	NOUN
eurjchem-843	116	16	(	(	PUNCT
eurjchem-843	116	17	30:70	30:70	NUM
eurjchem-843	116	18	,	,	PUNCT
eurjchem-843	116	19	v	v	NOUN
eurjchem-843	116	20	:	:	SYM
eurjchem-843	116	21	v	v	NOUN
eurjchem-843	116	22	)	)	PUNCT
eurjchem-843	116	23	was	be	AUX
eurjchem-843	116	24	applied	apply	VERB
eurjchem-843	116	25	as	as	ADP
eurjchem-843	116	26	stg	stg	PROPN
eurjchem-843	116	27	and	and	CCONJ
eurjchem-843	116	28	sdp	sdp	NOUN
eurjchem-843	116	29	were	be	AUX
eurjchem-843	116	30	eluted	elute	VERB
eurjchem-843	116	31	in	in	ADP
eurjchem-843	116	32	a	a	DET
eurjchem-843	116	33	reasonable	reasonable	ADJ
eurjchem-843	116	34	time	time	NOUN
eurjchem-843	116	35	and	and	CCONJ
eurjchem-843	116	36	good	good	ADJ
eurjchem-843	116	37	peak	peak	NOUN
eurjchem-843	116	38	shape	shape	NOUN
eurjchem-843	116	39	with	with	ADP
eurjchem-843	116	40	this	this	DET
eurjchem-843	116	41	mobile	mobile	ADJ
eurjchem-843	116	42	phase	phase	NOUN
eurjchem-843	116	43	at	at	ADP
eurjchem-843	116	44	a	a	DET
eurjchem-843	116	45	flow	flow	NOUN
eurjchem-843	116	46	rate	rate	NOUN
eurjchem-843	116	47	1	1	NUM
eurjchem-843	116	48	ml	ml	NOUN
eurjchem-843	116	49	/	/	SYM
eurjchem-843	116	50	min	min	NOUN
eurjchem-843	116	51	.	.	PUNCT
eurjchem-843	117	1	the	the	DET
eurjchem-843	117	2	fluorometric	fluorometric	ADJ
eurjchem-843	117	3	detector	detector	NOUN
eurjchem-843	117	4	was	be	AUX
eurjchem-843	117	5	operated	operate	VERB
eurjchem-843	117	6	at	at	ADP
eurjchem-843	117	7	267	267	NUM
eurjchem-843	117	8	nm	nm	NOUN
eurjchem-843	117	9	for	for	ADP
eurjchem-843	117	10	excitation	excitation	NOUN
eurjchem-843	117	11	and	and	CCONJ
eurjchem-843	117	12	575	575	NUM
eurjchem-843	117	13	nm	nm	NOUN
eurjchem-843	117	14	for	for	ADP
eurjchem-843	117	15	emission	emission	NOUN
eurjchem-843	117	16	where	where	SCONJ
eurjchem-843	117	17	high	high	ADJ
eurjchem-843	117	18	detector	detector	NOUN
eurjchem-843	117	19	sensitivity	sensitivity	NOUN
eurjchem-843	117	20	was	be	AUX
eurjchem-843	117	21	achieved	achieve	VERB
eurjchem-843	117	22	at	at	ADP
eurjchem-843	117	23	these	these	DET
eurjchem-843	117	24	wavelengths	wavelength	NOUN
eurjchem-843	117	25	.	.	PUNCT
eurjchem-843	118	1	the	the	DET
eurjchem-843	118	2	retention	retention	NOUN
eurjchem-843	118	3	times	time	NOUN
eurjchem-843	118	4	were	be	AUX
eurjchem-843	118	5	3.9	3.9	NUM
eurjchem-843	118	6	and	and	CCONJ
eurjchem-843	118	7	6.1	6.1	NUM
eurjchem-843	118	8	min	min	NOUN
eurjchem-843	118	9	for	for	ADP
eurjchem-843	118	10	sdp	sdp	NOUN
eurjchem-843	118	11	and	and	CCONJ
eurjchem-843	118	12	stg	stg	NOUN
eurjchem-843	118	13	,	,	PUNCT
eurjchem-843	118	14	respectively	respectively	ADV
eurjchem-843	118	15	as	as	SCONJ
eurjchem-843	118	16	shown	show	VERB
eurjchem-843	118	17	in	in	ADP
eurjchem-843	118	18	figure	figure	NOUN
eurjchem-843	118	19	2	2	NUM
eurjchem-843	118	20	and	and	CCONJ
eurjchem-843	118	21	the	the	DET
eurjchem-843	118	22	retention	retention	NOUN
eurjchem-843	118	23	times	time	NOUN
eurjchem-843	118	24	were	be	AUX
eurjchem-843	118	25	3.8	3.8	NUM
eurjchem-843	118	26	and	and	CCONJ
eurjchem-843	118	27	6.3	6.3	NUM
eurjchem-843	118	28	min	min	NOUN
eurjchem-843	118	29	for	for	ADP
eurjchem-843	118	30	sdp	sdp	NOUN
eurjchem-843	118	31	and	and	CCONJ
eurjchem-843	118	32	stg	stg	NOUN
eurjchem-843	118	33	,	,	PUNCT
eurjchem-843	118	34	respectively	respectively	ADV
eurjchem-843	118	35	in	in	ADP
eurjchem-843	118	36	plasma	plasma	NOUN
eurjchem-843	118	37	as	as	SCONJ
eurjchem-843	118	38	shown	show	VERB
eurjchem-843	118	39	in	in	ADP
eurjchem-843	118	40	figures	figure	NOUN
eurjchem-843	118	41	3	3	NUM
eurjchem-843	118	42	and	and	CCONJ
eurjchem-843	118	43	4	4	NUM
eurjchem-843	118	44	.	.	X
eurjchem-843	119	1	3.1.2	3.1.2	NUM
eurjchem-843	119	2	.	.	NOUN
eurjchem-843	119	3	lc‐uv	lc‐uv	PROPN
eurjchem-843	119	4	method	method	PROPN
eurjchem-843	119	5	during	during	ADP
eurjchem-843	119	6	the	the	DET
eurjchem-843	119	7	optimization	optimization	NOUN
eurjchem-843	119	8	cycle	cycle	NOUN
eurjchem-843	119	9	,	,	PUNCT
eurjchem-843	119	10	several	several	ADJ
eurjchem-843	119	11	chromatographic	chromatographic	ADJ
eurjchem-843	119	12	conditions	condition	NOUN
eurjchem-843	119	13	were	be	AUX
eurjchem-843	119	14	attempted	attempt	VERB
eurjchem-843	119	15	using	use	VERB
eurjchem-843	119	16	symmetry	symmetry	NOUN
eurjchem-843	119	17	®	®	NOUN
eurjchem-843	119	18	waters	water	VERB
eurjchem-843	119	19	c18	c18	NOUN
eurjchem-843	119	20	column	column	NOUN
eurjchem-843	119	21	(	(	PUNCT
eurjchem-843	119	22	150	150	NUM
eurjchem-843	119	23	mm	mm	NOUN
eurjchem-843	119	24	x	x	SYM
eurjchem-843	119	25	4.6	4.6	NUM
eurjchem-843	119	26	mm	mm	NOUN
eurjchem-843	119	27	,	,	PUNCT
eurjchem-843	119	28	5	5	NUM
eurjchem-843	119	29	µm	µm	NOUN
eurjchem-843	119	30	)	)	PUNCT
eurjchem-843	119	31	.	.	PUNCT
eurjchem-843	120	1	the	the	DET
eurjchem-843	120	2	c18	c18	NOUN
eurjchem-843	120	3	column	column	NOUN
eurjchem-843	120	4	was	be	AUX
eurjchem-843	120	5	chosen	choose	VERB
eurjchem-843	120	6	for	for	ADP
eurjchem-843	120	7	its	its	PRON
eurjchem-843	120	8	availability	availability	NOUN
eurjchem-843	120	9	in	in	ADP
eurjchem-843	120	10	most	most	ADJ
eurjchem-843	120	11	quality	quality	NOUN
eurjchem-843	120	12	control	control	NOUN
eurjchem-843	120	13	laboratories	laboratory	NOUN
eurjchem-843	120	14	.	.	PUNCT
eurjchem-843	121	1	various	various	ADJ
eurjchem-843	121	2	mobile	mobile	ADJ
eurjchem-843	121	3	phase	phase	NOUN
eurjchem-843	121	4	compositions	composition	NOUN
eurjchem-843	121	5	containing	contain	VERB
eurjchem-843	121	6	different	different	ADJ
eurjchem-843	121	7	ratios	ratio	NOUN
eurjchem-843	121	8	of	of	ADP
eurjchem-843	121	9	organic	organic	ADJ
eurjchem-843	121	10	and	and	CCONJ
eurjchem-843	121	11	aqueous	aqueous	ADJ
eurjchem-843	121	12	phases	phase	NOUN
eurjchem-843	121	13	were	be	AUX
eurjchem-843	121	14	tried	try	VERB
eurjchem-843	121	15	in	in	ADP
eurjchem-843	121	16	an	an	DET
eurjchem-843	121	17	isocratic	isocratic	ADJ
eurjchem-843	121	18	mode	mode	NOUN
eurjchem-843	121	19	.	.	PUNCT
eurjchem-843	122	1	el‐bagary	el‐bagary	PROPN
eurjchem-843	122	2	et	et	PROPN
eurjchem-843	122	3	al	al	PROPN
eurjchem-843	122	4	.	.	PUNCT
eurjchem-843	122	5	/	/	SYM
eurjchem-843	122	6	european	european	PROPN
eurjchem-843	122	7	journal	journal	PROPN
eurjchem-843	122	8	of	of	ADP
eurjchem-843	122	9	chemistry	chemistry	NOUN
eurjchem-843	122	10	4	4	NUM
eurjchem-843	122	11	(	(	PUNCT
eurjchem-843	122	12	4	4	NUM
eurjchem-843	122	13	)	)	PUNCT
eurjchem-843	122	14	(	(	PUNCT
eurjchem-843	122	15	2013	2013	NUM
eurjchem-843	122	16	)	)	PUNCT
eurjchem-843	122	17	360‐365	360‐365	NUM
eurjchem-843	122	18	363	363	NUM
eurjchem-843	122	19	table	table	NOUN
eurjchem-843	122	20	3	3	NUM
eurjchem-843	122	21	.	.	PUNCT
eurjchem-843	122	22	results	result	NOUN
eurjchem-843	122	23	obtained	obtain	VERB
eurjchem-843	122	24	by	by	ADP
eurjchem-843	122	25	lc‐flouro	lc‐flouro	NOUN
eurjchem-843	122	26	method	method	NOUN
eurjchem-843	122	27	for	for	ADP
eurjchem-843	122	28	the	the	DET
eurjchem-843	122	29	determination	determination	NOUN
eurjchem-843	122	30	of	of	ADP
eurjchem-843	122	31	sitagliptin	sitagliptin	NOUN
eurjchem-843	122	32	in	in	ADP
eurjchem-843	122	33	binary	binary	ADJ
eurjchem-843	122	34	mixture	mixture	NOUN
eurjchem-843	122	35	with	with	ADP
eurjchem-843	122	36	its	its	PRON
eurjchem-843	122	37	acidic	acidic	ADJ
eurjchem-843	122	38	degradation	degradation	NOUN
eurjchem-843	122	39	product	product	NOUN
eurjchem-843	122	40	.	.	PUNCT
eurjchem-843	123	1	item	item	NOUN
eurjchem-843	123	2	*	*	PUNCT
eurjchem-843	123	3	stg	stg	X
eurjchem-843	123	4	stg	stg	X
eurjchem-843	123	5	in	in	ADP
eurjchem-843	123	6	plasma	plasma	NOUN
eurjchem-843	123	7	retention	retention	NOUN
eurjchem-843	123	8	time	time	NOUN
eurjchem-843	123	9	6.1	6.1	NUM
eurjchem-843	123	10	6.3	6.3	NUM
eurjchem-843	123	11	excitation	excitation	NOUN
eurjchem-843	123	12	wavelength	wavelength	NOUN
eurjchem-843	123	13	of	of	ADP
eurjchem-843	123	14	detection	detection	NOUN
eurjchem-843	123	15	267	267	NUM
eurjchem-843	123	16	nm	nm	NOUN
eurjchem-843	123	17	267	267	NUM
eurjchem-843	123	18	nm	nm	ADJ
eurjchem-843	123	19	emission	emission	NOUN
eurjchem-843	123	20	wavelength	wavelength	NOUN
eurjchem-843	123	21	of	of	ADP
eurjchem-843	123	22	detection	detection	NOUN
eurjchem-843	123	23	575	575	NUM
eurjchem-843	123	24	nm	nm	NUM
eurjchem-843	123	25	575	575	NUM
eurjchem-843	123	26	nm	nm	ADJ
eurjchem-843	123	27	range	range	NOUN
eurjchem-843	123	28	of	of	ADP
eurjchem-843	123	29	linearity	linearity	NOUN
eurjchem-843	123	30	5‐200	5‐200	PROPN
eurjchem-843	123	31	μg	μg	PROPN
eurjchem-843	123	32	/	/	SYM
eurjchem-843	123	33	ml	ml	PROPN
eurjchem-843	123	34	0.25‐8	0.25‐8	PROPN
eurjchem-843	123	35	μg	μg	PROPN
eurjchem-843	123	36	/	/	SYM
eurjchem-843	123	37	ml	ml	NOUN
eurjchem-843	123	38	regression	regression	NOUN
eurjchem-843	123	39	equation	equation	NOUN
eurjchem-843	123	40	area×10‐3	area×10‐3	NOUN
eurjchem-843	123	41	=	=	PUNCT
eurjchem-843	124	1	0.6710	0.6710	NUM
eurjchem-843	124	2	c	c	X
eurjchem-843	124	3	(	(	PUNCT
eurjchem-843	124	4	μg	μg	PROPN
eurjchem-843	124	5	/	/	SYM
eurjchem-843	124	6	ml)‐	ml)‐	PROPN
eurjchem-843	124	7	0.2104	0.2104	NUM
eurjchem-843	124	8	area	area	NOUN
eurjchem-843	124	9	×	×	NOUN
eurjchem-843	124	10	10‐4	10‐4	NUM
eurjchem-843	124	11	=	=	PUNCT
eurjchem-843	124	12	2.7479	2.7479	NUM
eurjchem-843	124	13	c	c	X
eurjchem-843	124	14	(	(	PUNCT
eurjchem-843	124	15	μg	μg	NOUN
eurjchem-843	124	16	/	/	SYM
eurjchem-843	124	17	ml	ml	NOUN
eurjchem-843	124	18	)	)	PUNCT
eurjchem-843	124	19	+	+	CCONJ
eurjchem-843	124	20	0.0155	0.0155	NUM
eurjchem-843	124	21	regression	regression	NOUN
eurjchem-843	124	22	coefficient	coefficient	NOUN
eurjchem-843	124	23	(	(	PUNCT
eurjchem-843	124	24	r2	r2	PROPN
eurjchem-843	124	25	)	)	PUNCT
eurjchem-843	124	26	1.0	1.0	NUM
eurjchem-843	124	27	0.9998	0.9998	NUM
eurjchem-843	124	28	lod	lod	PROPN
eurjchem-843	124	29	1.04	1.04	NUM
eurjchem-843	124	30	μg	μg	NOUN
eurjchem-843	124	31	/	/	SYM
eurjchem-843	124	32	ml	ml	PROPN
eurjchem-843	124	33	0.05	0.05	NUM
eurjchem-843	124	34	μg	μg	NOUN
eurjchem-843	124	35	/	/	SYM
eurjchem-843	124	36	ml	ml	PROPN
eurjchem-843	124	37	loq	loq	PROPN
eurjchem-843	124	38	3.48	3.48	NUM
eurjchem-843	124	39	μg	μg	PROPN
eurjchem-843	124	40	/	/	SYM
eurjchem-843	124	41	ml	ml	PROPN
eurjchem-843	124	42	0.16	0.16	NUM
eurjchem-843	124	43	μg	μg	PROPN
eurjchem-843	124	44	/	/	SYM
eurjchem-843	124	45	ml	ml	PROPN
eurjchem-843	124	46	sb	sb	PROPN
eurjchem-843	124	47	1.39	1.39	NUM
eurjchem-843	124	48	×	×	NOUN
eurjchem-843	124	49	10‐3	10‐3	NUM
eurjchem-843	124	50	6.3×10‐2	6.3×10‐2	NUM
eurjchem-843	124	51	sa	sa	NOUN
eurjchem-843	124	52	0.19	0.19	NUM
eurjchem-843	124	53	0.29	0.29	NUM
eurjchem-843	124	54	confidence	confidence	NOUN
eurjchem-843	124	55	limit	limit	NOUN
eurjchem-843	124	56	of	of	ADP
eurjchem-843	124	57	the	the	DET
eurjchem-843	124	58	slope	slope	NOUN
eurjchem-843	124	59	0.6710±0.13	0.6710±0.13	PROPN
eurjchem-843	124	60	2.7479±0.80	2.7479±0.80	ADJ
eurjchem-843	124	61	confidence	confidence	NOUN
eurjchem-843	124	62	limit	limit	NOUN
eurjchem-843	124	63	of	of	ADP
eurjchem-843	124	64	the	the	DET
eurjchem-843	124	65	intercept	intercept	NOUN
eurjchem-843	124	66	‐0.2104±0.29×10‐3	‐0.2104±0.29×10‐3	NOUN
eurjchem-843	124	67	0.0155±0.10×10‐2	0.0155±0.10×10‐2	PROPN
eurjchem-843	124	68	standard	standard	ADJ
eurjchem-843	124	69	error	error	NOUN
eurjchem-843	124	70	of	of	ADP
eurjchem-843	124	71	the	the	DET
eurjchem-843	124	72	estimation	estimation	NOUN
eurjchem-843	124	73	0.24	0.24	NUM
eurjchem-843	124	74	0.4165	0.4165	NUM
eurjchem-843	124	75	precision	precision	NOUN
eurjchem-843	124	76	intra‐day	intra‐day	NOUN
eurjchem-843	124	77	%	%	NOUN
eurjchem-843	124	78	r.s.d	r.s.d	NOUN
eurjchem-843	124	79	.	.	PUNCT
eurjchem-843	125	1	0.12‐0.58	0.12‐0.58	NOUN
eurjchem-843	125	2	0.24‐0.61	0.24‐0.61	NUM
eurjchem-843	125	3	inter‐day	inter‐day	NOUN
eurjchem-843	125	4	%	%	X
eurjchem-843	125	5	r.s.d	r.s.d	VERB
eurjchem-843	125	6	.	.	PUNCT
eurjchem-843	126	1	0.83‐1.53	0.83‐1.53	NOUN
eurjchem-843	127	1	0.72‐1.21	0.72‐1.21	PROPN
eurjchem-843	127	2	drug	drug	NOUN
eurjchem-843	127	3	in	in	ADP
eurjchem-843	127	4	dosage	dosage	NOUN
eurjchem-843	127	5	form	form	NOUN
eurjchem-843	127	6	100.39±1.43	100.39±1.43	NUM
eurjchem-843	127	7	accuracy	accuracy	NOUN
eurjchem-843	127	8	drug	drug	NOUN
eurjchem-843	127	9	in	in	ADP
eurjchem-843	127	10	laboratory	laboratory	NOUN
eurjchem-843	127	11	prepared	prepare	VERB
eurjchem-843	127	12	mixture	mixture	NOUN
eurjchem-843	127	13	99.65±1.0	99.65±1.0	PROPN
eurjchem-843	127	14	100.81±1.65	100.81±1.65	NUM
eurjchem-843	127	15	drug	drug	NOUN
eurjchem-843	127	16	added	add	VERB
eurjchem-843	127	17	99.62±1.56	99.62±1.56	NUM
eurjchem-843	127	18	*	*	PUNCT
eurjchem-843	127	19	%	%	INTJ
eurjchem-843	127	20	r.s.d	r.s.d	NOUN
eurjchem-843	127	21	.	.	PUNCT
eurjchem-843	127	22	:	:	PUNCT
eurjchem-843	128	1	percent	percent	NOUN
eurjchem-843	128	2	relative	relative	ADJ
eurjchem-843	128	3	standard	standard	ADJ
eurjchem-843	128	4	deviation	deviation	NOUN
eurjchem-843	128	5	,	,	PUNCT
eurjchem-843	128	6	lod	lod	PROPN
eurjchem-843	128	7	:	:	PUNCT
eurjchem-843	128	8	limit	limit	NOUN
eurjchem-843	128	9	of	of	ADP
eurjchem-843	128	10	detection	detection	NOUN
eurjchem-843	128	11	,	,	PUNCT
eurjchem-843	128	12	loq	loq	PROPN
eurjchem-843	128	13	:	:	PUNCT
eurjchem-843	128	14	limit	limit	NOUN
eurjchem-843	128	15	of	of	ADP
eurjchem-843	128	16	quantification	quantification	NOUN
eurjchem-843	128	17	.	.	PUNCT
eurjchem-843	129	1	it	it	PRON
eurjchem-843	129	2	was	be	AUX
eurjchem-843	129	3	found	find	VERB
eurjchem-843	129	4	that	that	SCONJ
eurjchem-843	129	5	85	85	NUM
eurjchem-843	129	6	%	%	NOUN
eurjchem-843	129	7	of	of	ADP
eurjchem-843	129	8	organic	organic	ADJ
eurjchem-843	129	9	modifier	modifier	NOUN
eurjchem-843	129	10	was	be	AUX
eurjchem-843	129	11	needed	need	VERB
eurjchem-843	129	12	to	to	PART
eurjchem-843	129	13	elute	elute	VERB
eurjchem-843	129	14	all	all	DET
eurjchem-843	129	15	peaks	peak	NOUN
eurjchem-843	129	16	within	within	ADP
eurjchem-843	129	17	10	10	NUM
eurjchem-843	129	18	min	min	NOUN
eurjchem-843	129	19	.	.	PROPN
eurjchem-843	129	20	acetonitrile	acetonitrile	NOUN
eurjchem-843	129	21	was	be	AUX
eurjchem-843	129	22	found	find	VERB
eurjchem-843	129	23	optimum	optimum	ADJ
eurjchem-843	129	24	for	for	ADP
eurjchem-843	129	25	the	the	DET
eurjchem-843	129	26	elution	elution	NOUN
eurjchem-843	129	27	.	.	PUNCT
eurjchem-843	130	1	besides	besides	SCONJ
eurjchem-843	130	2	,	,	PUNCT
eurjchem-843	130	3	different	different	ADJ
eurjchem-843	130	4	buffers	buffer	NOUN
eurjchem-843	130	5	at	at	ADP
eurjchem-843	130	6	different	different	ADJ
eurjchem-843	130	7	ph	ph	ADJ
eurjchem-843	130	8	values	value	NOUN
eurjchem-843	130	9	were	be	AUX
eurjchem-843	130	10	attempted	attempt	VERB
eurjchem-843	130	11	along	along	ADP
eurjchem-843	130	12	with	with	ADP
eurjchem-843	130	13	acetonitrile	acetonitrile	NOUN
eurjchem-843	130	14	.	.	PUNCT
eurjchem-843	131	1	therefore	therefore	ADV
eurjchem-843	131	2	,	,	PUNCT
eurjchem-843	131	3	a	a	DET
eurjchem-843	131	4	mobile	mobile	ADJ
eurjchem-843	131	5	phase	phase	NOUN
eurjchem-843	131	6	consisting	consist	VERB
eurjchem-843	131	7	of	of	ADP
eurjchem-843	131	8	potassium	potassium	NOUN
eurjchem-843	131	9	dihydrogen	dihydrogen	NOUN
eurjchem-843	131	10	phosphate	phosphate	NOUN
eurjchem-843	131	11	buffer	buffer	NOUN
eurjchem-843	131	12	(	(	PUNCT
eurjchem-843	131	13	ph	ph	NOUN
eurjchem-843	131	14	=	=	NOUN
eurjchem-843	131	15	4.6	4.6	NUM
eurjchem-843	131	16	)	)	PUNCT
eurjchem-843	131	17	‐	‐	ADJ
eurjchem-843	131	18	acetonitrile	acetonitrile	NOUN
eurjchem-843	131	19	(	(	PUNCT
eurjchem-843	131	20	15:85	15:85	NUM
eurjchem-843	131	21	,	,	PUNCT
eurjchem-843	131	22	v	v	NOUN
eurjchem-843	131	23	:	:	SYM
eurjchem-843	131	24	v	v	NOUN
eurjchem-843	131	25	)	)	PUNCT
eurjchem-843	131	26	and	and	CCONJ
eurjchem-843	131	27	pumped	pump	VERB
eurjchem-843	131	28	at	at	ADP
eurjchem-843	131	29	a	a	DET
eurjchem-843	131	30	flow	flow	NOUN
eurjchem-843	131	31	rate	rate	NOUN
eurjchem-843	131	32	of	of	ADP
eurjchem-843	131	33	1.0	1.0	NUM
eurjchem-843	131	34	ml	ml	NOUN
eurjchem-843	131	35	/	/	SYM
eurjchem-843	131	36	min	min	NOUN
eurjchem-843	131	37	,	,	PUNCT
eurjchem-843	131	38	in	in	ADP
eurjchem-843	131	39	an	an	DET
eurjchem-843	131	40	isocratic	isocratic	ADJ
eurjchem-843	131	41	mode	mode	NOUN
eurjchem-843	131	42	,	,	PUNCT
eurjchem-843	131	43	gave	give	VERB
eurjchem-843	131	44	good	good	ADJ
eurjchem-843	131	45	separation	separation	NOUN
eurjchem-843	131	46	of	of	ADP
eurjchem-843	131	47	the	the	DET
eurjchem-843	131	48	three	three	NUM
eurjchem-843	131	49	compounds	compound	NOUN
eurjchem-843	131	50	.	.	PUNCT
eurjchem-843	132	1	detection	detection	NOUN
eurjchem-843	132	2	was	be	AUX
eurjchem-843	132	3	carried	carry	VERB
eurjchem-843	132	4	out	out	ADP
eurjchem-843	132	5	at	at	ADP
eurjchem-843	132	6	220	220	NUM
eurjchem-843	132	7	nm	nm	NOUN
eurjchem-843	132	8	to	to	PART
eurjchem-843	132	9	obtain	obtain	VERB
eurjchem-843	132	10	sufficient	sufficient	ADJ
eurjchem-843	132	11	peak	peak	NOUN
eurjchem-843	132	12	intensity	intensity	NOUN
eurjchem-843	132	13	for	for	ADP
eurjchem-843	132	14	both	both	DET
eurjchem-843	132	15	drugs	drug	NOUN
eurjchem-843	132	16	and	and	CCONJ
eurjchem-843	132	17	sdg	sdg	NOUN
eurjchem-843	132	18	.	.	PUNCT
eurjchem-843	133	1	the	the	DET
eurjchem-843	133	2	retention	retention	NOUN
eurjchem-843	133	3	times	time	NOUN
eurjchem-843	133	4	were	be	AUX
eurjchem-843	133	5	3.0	3.0	NUM
eurjchem-843	133	6	,	,	PUNCT
eurjchem-843	133	7	5.6	5.6	NUM
eurjchem-843	133	8	and	and	CCONJ
eurjchem-843	133	9	6.5	6.5	NUM
eurjchem-843	133	10	min	min	NOUN
eurjchem-843	133	11	for	for	ADP
eurjchem-843	133	12	sdp	sdp	NOUN
eurjchem-843	133	13	,	,	PUNCT
eurjchem-843	133	14	stg	stg	PROPN
eurjchem-843	133	15	and	and	CCONJ
eurjchem-843	133	16	met	meet	VERB
eurjchem-843	133	17	,	,	PUNCT
eurjchem-843	133	18	respectively	respectively	ADV
eurjchem-843	133	19	as	as	ADP
eurjchem-843	133	20	in	in	ADP
eurjchem-843	133	21	figures	figure	NOUN
eurjchem-843	133	22	5	5	NUM
eurjchem-843	133	23	and	and	CCONJ
eurjchem-843	133	24	6	6	NUM
eurjchem-843	133	25	.	.	X
eurjchem-843	133	26	figure	figure	NOUN
eurjchem-843	133	27	2	2	NUM
eurjchem-843	133	28	.	.	PUNCT
eurjchem-843	134	1	a	a	DET
eurjchem-843	134	2	typical	typical	ADJ
eurjchem-843	134	3	lc	lc	NOUN
eurjchem-843	134	4	chromatogram	chromatogram	NOUN
eurjchem-843	134	5	with	with	ADP
eurjchem-843	134	6	fluorometric	fluorometric	ADJ
eurjchem-843	134	7	detection	detection	NOUN
eurjchem-843	134	8	of	of	ADP
eurjchem-843	134	9	25	25	NUM
eurjchem-843	134	10	µl	µl	ADP
eurjchem-843	134	11	injector	injector	NOUN
eurjchem-843	134	12	of	of	ADP
eurjchem-843	134	13	synthetic	synthetic	ADJ
eurjchem-843	134	14	binary	binary	ADJ
eurjchem-843	134	15	mixture	mixture	NOUN
eurjchem-843	134	16	of	of	ADP
eurjchem-843	134	17	sitagliptin	sitagliptin	NOUN
eurjchem-843	134	18	acidic	acidic	ADJ
eurjchem-843	134	19	degradation	degradation	NOUN
eurjchem-843	134	20	product	product	NOUN
eurjchem-843	134	21	(	(	PUNCT
eurjchem-843	134	22	30	30	NUM
eurjchem-843	134	23	µg	µg	NOUN
eurjchem-843	134	24	/	/	SYM
eurjchem-843	134	25	ml	ml	NOUN
eurjchem-843	134	26	)	)	PUNCT
eurjchem-843	134	27	(	(	PUNCT
eurjchem-843	134	28	a	a	X
eurjchem-843	134	29	)	)	PUNCT
eurjchem-843	134	30	and	and	CCONJ
eurjchem-843	134	31	sitagliptin	sitagliptin	NOUN
eurjchem-843	134	32	(	(	PUNCT
eurjchem-843	134	33	100	100	NUM
eurjchem-843	134	34	µg	µg	NOUN
eurjchem-843	134	35	/	/	SYM
eurjchem-843	134	36	ml	ml	NOUN
eurjchem-843	134	37	)	)	PUNCT
eurjchem-843	134	38	(	(	PUNCT
eurjchem-843	134	39	b	b	NOUN
eurjchem-843	134	40	)	)	PUNCT
eurjchem-843	134	41	.	.	PUNCT
eurjchem-843	135	1	figure	figure	VERB
eurjchem-843	135	2	3	3	NUM
eurjchem-843	135	3	.	.	PUNCT
eurjchem-843	136	1	a	a	DET
eurjchem-843	136	2	typical	typical	ADJ
eurjchem-843	136	3	lc	lc	NOUN
eurjchem-843	136	4	chromatogram	chromatogram	NOUN
eurjchem-843	136	5	with	with	ADP
eurjchem-843	136	6	fluorometric	fluorometric	ADJ
eurjchem-843	136	7	detection	detection	NOUN
eurjchem-843	136	8	of	of	ADP
eurjchem-843	136	9	25	25	NUM
eurjchem-843	136	10	µl	µl	ADP
eurjchem-843	136	11	injector	injector	NOUN
eurjchem-843	136	12	of	of	ADP
eurjchem-843	136	13	synthetic	synthetic	ADJ
eurjchem-843	136	14	binary	binary	ADJ
eurjchem-843	136	15	mixture	mixture	NOUN
eurjchem-843	136	16	of	of	ADP
eurjchem-843	136	17	sitagliptin	sitagliptin	NOUN
eurjchem-843	136	18	acidic	acidic	ADJ
eurjchem-843	136	19	degradation	degradation	NOUN
eurjchem-843	136	20	product	product	NOUN
eurjchem-843	136	21	(	(	PUNCT
eurjchem-843	136	22	1.5	1.5	NUM
eurjchem-843	136	23	µg	µg	NOUN
eurjchem-843	136	24	/	/	SYM
eurjchem-843	136	25	ml	ml	NOUN
eurjchem-843	136	26	)	)	PUNCT
eurjchem-843	136	27	(	(	PUNCT
eurjchem-843	136	28	a	a	X
eurjchem-843	136	29	)	)	PUNCT
eurjchem-843	136	30	and	and	CCONJ
eurjchem-843	136	31	sitagliptin	sitagliptin	NOUN
eurjchem-843	136	32	(	(	PUNCT
eurjchem-843	136	33	5	5	NUM
eurjchem-843	136	34	µg	µg	ADV
eurjchem-843	136	35	/	/	SYM
eurjchem-843	136	36	ml	ml	NOUN
eurjchem-843	136	37	)	)	PUNCT
eurjchem-843	136	38	(	(	PUNCT
eurjchem-843	136	39	b	b	NOUN
eurjchem-843	136	40	)	)	PUNCT
eurjchem-843	136	41	in	in	ADP
eurjchem-843	136	42	plasma	plasma	NOUN
eurjchem-843	136	43	.	.	PUNCT
eurjchem-843	137	1	3.1.3	3.1.3	X
eurjchem-843	137	2	.	.	PUNCT
eurjchem-843	137	3	system	system	NOUN
eurjchem-843	137	4	suitability	suitability	NOUN
eurjchem-843	137	5	tests	test	VERB
eurjchem-843	137	6	system	system	NOUN
eurjchem-843	137	7	suitability	suitability	NOUN
eurjchem-843	137	8	tests	test	NOUN
eurjchem-843	137	9	are	be	AUX
eurjchem-843	137	10	used	use	VERB
eurjchem-843	137	11	to	to	PART
eurjchem-843	137	12	verify	verify	VERB
eurjchem-843	137	13	that	that	SCONJ
eurjchem-843	137	14	the	the	DET
eurjchem-843	137	15	resolution	resolution	NOUN
eurjchem-843	137	16	and	and	CCONJ
eurjchem-843	137	17	reproducibility	reproducibility	NOUN
eurjchem-843	137	18	were	be	AUX
eurjchem-843	137	19	adequate	adequate	ADJ
eurjchem-843	137	20	for	for	SCONJ
eurjchem-843	137	21	the	the	DET
eurjchem-843	137	22	analysis	analysis	NOUN
eurjchem-843	137	23	performed	perform	VERB
eurjchem-843	137	24	.	.	PUNCT
eurjchem-843	138	1	the	the	DET
eurjchem-843	138	2	parameters	parameter	NOUN
eurjchem-843	138	3	of	of	ADP
eurjchem-843	138	4	these	these	DET
eurjchem-843	138	5	tests	test	NOUN
eurjchem-843	138	6	are	be	AUX
eurjchem-843	138	7	column	column	NOUN
eurjchem-843	138	8	efficiency	efficiency	NOUN
eurjchem-843	138	9	(	(	PUNCT
eurjchem-843	138	10	number	number	NOUN
eurjchem-843	138	11	of	of	ADP
eurjchem-843	138	12	theoretical	theoretical	ADJ
eurjchem-843	138	13	plates	plate	NOUN
eurjchem-843	138	14	)	)	PUNCT
eurjchem-843	138	15	,	,	PUNCT
eurjchem-843	138	16	tailing	tail	VERB
eurjchem-843	138	17	of	of	ADP
eurjchem-843	138	18	chromatographic	chromatographic	ADJ
eurjchem-843	138	19	peak	peak	NOUN
eurjchem-843	138	20	,	,	PUNCT
eurjchem-843	138	21	peak	peak	NOUN
eurjchem-843	138	22	resolution	resolution	NOUN
eurjchem-843	138	23	factor	factor	NOUN
eurjchem-843	138	24	,	,	PUNCT
eurjchem-843	138	25	and	and	CCONJ
eurjchem-843	138	26	repeatability	repeatability	NOUN
eurjchem-843	138	27	as	as	ADP
eurjchem-843	138	28	%	%	NOUN
eurjchem-843	138	29	r.s.d	r.s.d	NOUN
eurjchem-843	138	30	.	.	PUNCT
eurjchem-843	139	1	of	of	ADP
eurjchem-843	139	2	peak	peak	NOUN
eurjchem-843	139	3	area	area	NOUN
eurjchem-843	139	4	for	for	ADP
eurjchem-843	139	5	six	six	NUM
eurjchem-843	139	6	injections	injection	NOUN
eurjchem-843	139	7	and	and	CCONJ
eurjchem-843	139	8	reproducibility	reproducibility	NOUN
eurjchem-843	139	9	of	of	ADP
eurjchem-843	139	10	retention	retention	NOUN
eurjchem-843	139	11	as	as	ADP
eurjchem-843	139	12	%	%	NOUN
eurjchem-843	139	13	r.s.d	r.s.d	NOUN
eurjchem-843	139	14	.	.	PUNCT
eurjchem-843	140	1	of	of	ADP
eurjchem-843	140	2	retention	retention	NOUN
eurjchem-843	140	3	time	time	NOUN
eurjchem-843	140	4	.	.	PUNCT
eurjchem-843	141	1	the	the	DET
eurjchem-843	141	2	results	result	NOUN
eurjchem-843	141	3	of	of	ADP
eurjchem-843	141	4	these	these	DET
eurjchem-843	141	5	tests	test	NOUN
eurjchem-843	141	6	for	for	ADP
eurjchem-843	141	7	the	the	DET
eurjchem-843	141	8	two	two	NUM
eurjchem-843	141	9	proposed	propose	VERB
eurjchem-843	141	10	methods	method	NOUN
eurjchem-843	141	11	are	be	AUX
eurjchem-843	141	12	listed	list	VERB
eurjchem-843	141	13	in	in	ADP
eurjchem-843	141	14	tables	table	NOUN
eurjchem-843	141	15	1	1	NUM
eurjchem-843	141	16	and	and	CCONJ
eurjchem-843	141	17	2	2	NUM
eurjchem-843	141	18	.	.	X
eurjchem-843	141	19	figure	figure	NOUN
eurjchem-843	141	20	4	4	NUM
eurjchem-843	141	21	.	.	PUNCT
eurjchem-843	142	1	a	a	DET
eurjchem-843	142	2	typical	typical	ADJ
eurjchem-843	142	3	lc	lc	NOUN
eurjchem-843	142	4	chromatogram	chromatogram	NOUN
eurjchem-843	142	5	with	with	ADP
eurjchem-843	142	6	fluorometric	fluorometric	ADJ
eurjchem-843	142	7	detection	detection	NOUN
eurjchem-843	142	8	of	of	ADP
eurjchem-843	142	9	25	25	NUM
eurjchem-843	142	10	µl	µl	ADP
eurjchem-843	142	11	injector	injector	NOUN
eurjchem-843	142	12	of	of	ADP
eurjchem-843	142	13	januvia	januvia	PROPN
eurjchem-843	142	14	®	®	NOUN
eurjchem-843	142	15	sample	sample	NOUN
eurjchem-843	142	16	solution	solution	NOUN
eurjchem-843	142	17	(	(	PUNCT
eurjchem-843	142	18	30	30	NUM
eurjchem-843	142	19	µg	µg	NOUN
eurjchem-843	142	20	/	/	SYM
eurjchem-843	142	21	ml	ml	NOUN
eurjchem-843	142	22	)	)	PUNCT
eurjchem-843	142	23	.	.	PUNCT
eurjchem-843	143	1	figure	figure	NOUN
eurjchem-843	143	2	5	5	NUM
eurjchem-843	143	3	.	.	PUNCT
eurjchem-843	144	1	a	a	DET
eurjchem-843	144	2	typical	typical	ADJ
eurjchem-843	144	3	lc	lc	NOUN
eurjchem-843	144	4	chromatogram	chromatogram	NOUN
eurjchem-843	144	5	of	of	ADP
eurjchem-843	144	6	25	25	NUM
eurjchem-843	144	7	µl	µl	ADP
eurjchem-843	144	8	injector	injector	NOUN
eurjchem-843	144	9	of	of	ADP
eurjchem-843	144	10	synthetic	synthetic	ADJ
eurjchem-843	144	11	ternary	ternary	ADJ
eurjchem-843	144	12	mixture	mixture	NOUN
eurjchem-843	144	13	of	of	ADP
eurjchem-843	144	14	sitagliptin	sitagliptin	NOUN
eurjchem-843	144	15	acidic	acidic	ADJ
eurjchem-843	144	16	degradation	degradation	NOUN
eurjchem-843	144	17	product	product	NOUN
eurjchem-843	144	18	(	(	PUNCT
eurjchem-843	144	19	7.7	7.7	NUM
eurjchem-843	144	20	µg	µg	NOUN
eurjchem-843	144	21	/	/	SYM
eurjchem-843	144	22	ml	ml	NOUN
eurjchem-843	144	23	)	)	PUNCT
eurjchem-843	144	24	(	(	PUNCT
eurjchem-843	144	25	a	a	X
eurjchem-843	144	26	)	)	PUNCT
eurjchem-843	144	27	,	,	PUNCT
eurjchem-843	144	28	sitagliptin	sitagliptin	NOUN
eurjchem-843	144	29	(	(	PUNCT
eurjchem-843	144	30	25.7	25.7	NUM
eurjchem-843	144	31	µg	µg	NOUN
eurjchem-843	144	32	/	/	SYM
eurjchem-843	144	33	ml	ml	NOUN
eurjchem-843	144	34	)	)	PUNCT
eurjchem-843	144	35	(	(	PUNCT
eurjchem-843	144	36	b	b	NOUN
eurjchem-843	144	37	)	)	PUNCT
eurjchem-843	144	38	,	,	PUNCT
eurjchem-843	144	39	and	and	CCONJ
eurjchem-843	144	40	metformin	metformin	NOUN
eurjchem-843	144	41	(	(	PUNCT
eurjchem-843	144	42	400	400	NUM
eurjchem-843	144	43	µg	µg	NOUN
eurjchem-843	144	44	/	/	SYM
eurjchem-843	144	45	ml	ml	NOUN
eurjchem-843	144	46	)	)	PUNCT
eurjchem-843	144	47	(	(	PUNCT
eurjchem-843	144	48	c	c	NOUN
eurjchem-843	144	49	)	)	PUNCT
eurjchem-843	144	50	.	.	PUNCT
eurjchem-843	145	1	3.2	3.2	NUM
eurjchem-843	145	2	.	.	PUNCT
eurjchem-843	145	3	methods	method	NOUN
eurjchem-843	145	4	validation	validation	NOUN
eurjchem-843	145	5	3.2.1	3.2.1	NUM
eurjchem-843	145	6	.	.	PUNCT
eurjchem-843	146	1	linearity	linearity	PROPN
eurjchem-843	146	2	3.2.1.1	3.2.1.1	PROPN
eurjchem-843	146	3	.	.	PUNCT
eurjchem-843	147	1	lc‐fluoro	lc‐fluoro	PROPN
eurjchem-843	147	2	method	method	VERB
eurjchem-843	147	3	a	a	DET
eurjchem-843	147	4	linear	linear	ADJ
eurjchem-843	147	5	relationship	relationship	NOUN
eurjchem-843	147	6	between	between	ADP
eurjchem-843	147	7	area	area	NOUN
eurjchem-843	147	8	under	under	ADP
eurjchem-843	147	9	the	the	DET
eurjchem-843	147	10	peak	peak	NOUN
eurjchem-843	147	11	(	(	PUNCT
eurjchem-843	147	12	aup	aup	PROPN
eurjchem-843	147	13	)	)	PUNCT
eurjchem-843	147	14	and	and	CCONJ
eurjchem-843	147	15	stg	stg	NOUN
eurjchem-843	147	16	concentration	concentration	NOUN
eurjchem-843	147	17	(	(	PUNCT
eurjchem-843	147	18	c	c	X
eurjchem-843	147	19	)	)	PUNCT
eurjchem-843	147	20	was	be	AUX
eurjchem-843	147	21	obtained	obtain	VERB
eurjchem-843	147	22	.	.	PUNCT
eurjchem-843	148	1	the	the	DET
eurjchem-843	148	2	regression	regression	NOUN
eurjchem-843	148	3	equation	equation	NOUN
eurjchem-843	148	4	was	be	AUX
eurjchem-843	148	5	computed	compute	VERB
eurjchem-843	148	6	,	,	PUNCT
eurjchem-843	148	7	table	table	NOUN
eurjchem-843	148	8	3	3	NUM
eurjchem-843	148	9	.	.	PUNCT
eurjchem-843	149	1	the	the	DET
eurjchem-843	149	2	linearity	linearity	NOUN
eurjchem-843	149	3	of	of	ADP
eurjchem-843	149	4	the	the	DET
eurjchem-843	149	5	calibration	calibration	NOUN
eurjchem-843	149	6	curve	curve	NOUN
eurjchem-843	149	7	was	be	AUX
eurjchem-843	149	8	validated	validate	VERB
eurjchem-843	149	9	by	by	ADP
eurjchem-843	149	10	the	the	DET
eurjchem-843	149	11	high	high	ADJ
eurjchem-843	149	12	value	value	NOUN
eurjchem-843	149	13	of	of	ADP
eurjchem-843	149	14	correlation	correlation	NOUN
eurjchem-843	149	15	coefficient	coefficient	NOUN
eurjchem-843	149	16	.	.	PUNCT
eurjchem-843	150	1	364	364	NUM
eurjchem-843	150	2	yazar	yazar	NOUN
eurjchem-843	150	3	et	et	PROPN
eurjchem-843	150	4	al	al	PROPN
eurjchem-843	150	5	.	.	PUNCT
eurjchem-843	150	6	/	/	SYM
eurjchem-843	150	7	european	european	PROPN
eurjchem-843	150	8	journal	journal	PROPN
eurjchem-843	150	9	of	of	ADP
eurjchem-843	150	10	chemistry	chemistry	NOUN
eurjchem-843	150	11	4	4	NUM
eurjchem-843	150	12	(	(	PUNCT
eurjchem-843	150	13	4	4	NUM
eurjchem-843	150	14	)	)	PUNCT
eurjchem-843	150	15	(	(	PUNCT
eurjchem-843	150	16	2013	2013	NUM
eurjchem-843	150	17	)	)	PUNCT
eurjchem-843	150	18	360‐365	360‐365	NOUN
eurjchem-843	150	19	table	table	NOUN
eurjchem-843	150	20	4	4	NUM
eurjchem-843	150	21	.	.	PUNCT
eurjchem-843	150	22	results	result	NOUN
eurjchem-843	150	23	obtained	obtain	VERB
eurjchem-843	150	24	by	by	ADP
eurjchem-843	150	25	lc‐uv	lc‐uv	NUM
eurjchem-843	150	26	method	method	NOUN
eurjchem-843	150	27	for	for	ADP
eurjchem-843	150	28	the	the	DET
eurjchem-843	150	29	simultaneous	simultaneous	ADJ
eurjchem-843	150	30	determination	determination	NOUN
eurjchem-843	150	31	of	of	ADP
eurjchem-843	150	32	sitagliptin	sitagliptin	NOUN
eurjchem-843	150	33	and	and	CCONJ
eurjchem-843	150	34	metformin	metformin	NOUN
eurjchem-843	150	35	in	in	ADP
eurjchem-843	150	36	the	the	DET
eurjchem-843	150	37	presence	presence	NOUN
eurjchem-843	150	38	of	of	ADP
eurjchem-843	150	39	sitagliptin	sitagliptin	NOUN
eurjchem-843	150	40	acidic	acidic	ADJ
eurjchem-843	150	41	degradation	degradation	NOUN
eurjchem-843	150	42	product	product	NOUN
eurjchem-843	150	43	.	.	PUNCT
eurjchem-843	151	1	item	item	NOUN
eurjchem-843	151	2	*	*	PUNCT
eurjchem-843	151	3	sitagliptin	sitagliptin	PROPN
eurjchem-843	151	4	metformin	metformin	NOUN
eurjchem-843	151	5	retention	retention	NOUN
eurjchem-843	151	6	time	time	NOUN
eurjchem-843	151	7	5.6	5.6	NUM
eurjchem-843	151	8	6.5	6.5	NUM
eurjchem-843	151	9	wavelength	wavelength	NOUN
eurjchem-843	151	10	of	of	ADP
eurjchem-843	151	11	detection	detection	NOUN
eurjchem-843	151	12	220	220	NUM
eurjchem-843	151	13	nm	nm	NOUN
eurjchem-843	151	14	220	220	NUM
eurjchem-843	151	15	nm	nm	ADJ
eurjchem-843	151	16	range	range	NOUN
eurjchem-843	151	17	of	of	ADP
eurjchem-843	151	18	linearity	linearity	NOUN
eurjchem-843	151	19	5‐160	5‐160	NUM
eurjchem-843	151	20	μg	μg	NOUN
eurjchem-843	151	21	/	/	SYM
eurjchem-843	151	22	ml	ml	PROPN
eurjchem-843	151	23	25‐800	25‐800	PROPN
eurjchem-843	151	24	μg	μg	PROPN
eurjchem-843	151	25	/	/	SYM
eurjchem-843	151	26	ml	ml	ADP
eurjchem-843	151	27	regression	regression	NOUN
eurjchem-843	151	28	equation	equation	NOUN
eurjchem-843	151	29	area	area	NOUN
eurjchem-843	151	30	×	×	PROPN
eurjchem-843	151	31	10‐5	10‐5	NUM
eurjchem-843	151	32	=	=	SYM
eurjchem-843	151	33	0.1285	0.1285	NUM
eurjchem-843	151	34	c	c	X
eurjchem-843	151	35	(	(	PUNCT
eurjchem-843	151	36	μg	μg	PROPN
eurjchem-843	151	37	/	/	SYM
eurjchem-843	151	38	ml	ml	NOUN
eurjchem-843	151	39	)	)	PUNCT
eurjchem-843	151	40	‐	‐	NOUN
eurjchem-843	151	41	0.0098	0.0098	NUM
eurjchem-843	151	42	area	area	NOUN
eurjchem-843	151	43	×	×	PROPN
eurjchem-843	151	44	10‐6	10‐6	NUM
eurjchem-843	151	45	=	=	SYM
eurjchem-843	151	46	0.1191	0.1191	NUM
eurjchem-843	151	47	c	c	X
eurjchem-843	151	48	(	(	PUNCT
eurjchem-843	151	49	μg	μg	PROPN
eurjchem-843	151	50	/	/	SYM
eurjchem-843	151	51	ml	ml	NOUN
eurjchem-843	151	52	)	)	PUNCT
eurjchem-843	152	1	+	+	CCONJ
eurjchem-843	152	2	0.6991	0.6991	NUM
eurjchem-843	152	3	regression	regression	NOUN
eurjchem-843	152	4	coefficient	coefficient	NOUN
eurjchem-843	152	5	(	(	PUNCT
eurjchem-843	152	6	r2	r2	PROPN
eurjchem-843	152	7	)	)	PUNCT
eurjchem-843	152	8	1.0	1.0	NUM
eurjchem-843	152	9	0.9999	0.9999	NUM
eurjchem-843	152	10	lod	lod	PROPN
eurjchem-843	152	11	1.39	1.39	NUM
eurjchem-843	152	12	μg	μg	NOUN
eurjchem-843	152	13	/	/	SYM
eurjchem-843	152	14	ml	ml	PROPN
eurjchem-843	152	15	5.78	5.78	NUM
eurjchem-843	152	16	μg	μg	NOUN
eurjchem-843	152	17	/	/	SYM
eurjchem-843	152	18	ml	ml	NOUN
eurjchem-843	152	19	loq	loq	PROPN
eurjchem-843	152	20	4.63	4.63	NUM
eurjchem-843	152	21	μg	μg	PROPN
eurjchem-843	152	22	/	/	SYM
eurjchem-843	152	23	ml	ml	PROPN
eurjchem-843	152	24	19.26	19.26	NUM
eurjchem-843	152	25	μg	μg	NOUN
eurjchem-843	152	26	/	/	SYM
eurjchem-843	152	27	ml	ml	PROPN
eurjchem-843	152	28	sb	sb	PROPN
eurjchem-843	152	29	4.48×10‐4	4.48×10‐4	NUM
eurjchem-843	152	30	5.9×10‐4	5.9×10‐4	PROPN
eurjchem-843	152	31	sa	sa	PROPN
eurjchem-843	152	32	0.04	0.04	NUM
eurjchem-843	152	33	0.27	0.27	NUM
eurjchem-843	152	34	confidence	confidence	NOUN
eurjchem-843	152	35	limit	limit	NOUN
eurjchem-843	152	36	of	of	ADP
eurjchem-843	152	37	the	the	DET
eurjchem-843	152	38	slope	slope	NOUN
eurjchem-843	152	39	0.1285±5.14×10‐3	0.1285±5.14×10‐3	PROPN
eurjchem-843	152	40	0.1191±3.2×10‐2	0.1191±3.2×10‐2	NUM
eurjchem-843	152	41	confidence	confidence	NOUN
eurjchem-843	152	42	limit	limit	NOUN
eurjchem-843	152	43	of	of	ADP
eurjchem-843	152	44	the	the	DET
eurjchem-843	152	45	intercept	intercept	NOUN
eurjchem-843	152	46	‐0.0098	‐0.0098	NUM
eurjchem-843	152	47	±0.04×10‐4	±0.04×10‐4	NOUN
eurjchem-843	152	48	0.6991±4.12×10‐4	0.6991±4.12×10‐4	NOUN
eurjchem-843	152	49	standard	standard	ADJ
eurjchem-843	152	50	error	error	NOUN
eurjchem-843	152	51	of	of	ADP
eurjchem-843	152	52	the	the	DET
eurjchem-843	152	53	estimation	estimation	NOUN
eurjchem-843	152	54	0.0035	0.0035	NUM
eurjchem-843	152	55	0.39	0.39	NUM
eurjchem-843	152	56	precision	precision	NOUN
eurjchem-843	152	57	intra‐day	intra‐day	NOUN
eurjchem-843	152	58	%	%	INTJ
eurjchem-843	152	59	r.s.d	r.s.d	VERB
eurjchem-843	152	60	.	.	PUNCT
eurjchem-843	153	1	0.14‐0.47	0.14‐0.47	NOUN
eurjchem-843	154	1	0.08‐0.57	0.08‐0.57	NUM
eurjchem-843	154	2	inter‐day	inter‐day	NOUN
eurjchem-843	154	3	%	%	X
eurjchem-843	154	4	r.s.d	r.s.d	VERB
eurjchem-843	154	5	.	.	PUNCT
eurjchem-843	155	1	0.21‐1.35	0.21‐1.35	NUM
eurjchem-843	155	2	0.24‐1.13	0.24‐1.13	NUM
eurjchem-843	155	3	drug	drug	NOUN
eurjchem-843	155	4	in	in	ADP
eurjchem-843	155	5	dosage	dosage	NOUN
eurjchem-843	155	6	form	form	NOUN
eurjchem-843	155	7	100.24±1.63	100.24±1.63	NOUN
eurjchem-843	155	8	100.55±1.31	100.55±1.31	NUM
eurjchem-843	155	9	accuracy	accuracy	NOUN
eurjchem-843	155	10	drug	drug	NOUN
eurjchem-843	155	11	in	in	ADP
eurjchem-843	155	12	laboratory	laboratory	NOUN
eurjchem-843	155	13	mixture	mixture	NOUN
eurjchem-843	155	14	99.72±1.50	99.72±1.50	PROPN
eurjchem-843	155	15	99.70±1.74	99.70±1.74	PROPN
eurjchem-843	155	16	drug	drug	NOUN
eurjchem-843	155	17	added	add	VERB
eurjchem-843	155	18	100.50±1.61	100.50±1.61	NUM
eurjchem-843	155	19	100.13±1.63	100.13±1.63	NUM
eurjchem-843	156	1	*	*	PUNCT
eurjchem-843	156	2	%	%	INTJ
eurjchem-843	156	3	r.s.d	r.s.d	NOUN
eurjchem-843	156	4	.	.	PUNCT
eurjchem-843	156	5	:	:	PUNCT
eurjchem-843	157	1	percent	percent	NOUN
eurjchem-843	157	2	relative	relative	ADJ
eurjchem-843	157	3	standard	standard	ADJ
eurjchem-843	157	4	deviation	deviation	NOUN
eurjchem-843	157	5	,	,	PUNCT
eurjchem-843	157	6	lod	lod	PROPN
eurjchem-843	157	7	:	:	PUNCT
eurjchem-843	157	8	limit	limit	NOUN
eurjchem-843	157	9	of	of	ADP
eurjchem-843	157	10	detection	detection	NOUN
eurjchem-843	157	11	,	,	PUNCT
eurjchem-843	157	12	loq	loq	PROPN
eurjchem-843	157	13	:	:	PUNCT
eurjchem-843	157	14	limit	limit	NOUN
eurjchem-843	157	15	of	of	ADP
eurjchem-843	157	16	quantification	quantification	NOUN
eurjchem-843	157	17	.	.	PUNCT
eurjchem-843	158	1	figure	figure	NOUN
eurjchem-843	158	2	6	6	NUM
eurjchem-843	158	3	.	.	PUNCT
eurjchem-843	159	1	a	a	DET
eurjchem-843	159	2	typical	typical	ADJ
eurjchem-843	159	3	lc	lc	NOUN
eurjchem-843	159	4	chromatogram	chromatogram	NOUN
eurjchem-843	159	5	of	of	ADP
eurjchem-843	159	6	25	25	NUM
eurjchem-843	159	7	µl	µl	ADP
eurjchem-843	159	8	injector	injector	NOUN
eurjchem-843	159	9	of	of	ADP
eurjchem-843	159	10	janumet	janumet	ADJ
eurjchem-843	159	11	®	®	NOUN
eurjchem-843	159	12	sample	sample	NOUN
eurjchem-843	159	13	solution	solution	NOUN
eurjchem-843	159	14	,	,	PUNCT
eurjchem-843	159	15	sitagliptin	sitagliptin	NOUN
eurjchem-843	159	16	(	(	PUNCT
eurjchem-843	159	17	25.7	25.7	NUM
eurjchem-843	159	18	µg	µg	NOUN
eurjchem-843	159	19	/	/	SYM
eurjchem-843	159	20	ml	ml	NOUN
eurjchem-843	159	21	)	)	PUNCT
eurjchem-843	159	22	(	(	PUNCT
eurjchem-843	159	23	a	a	X
eurjchem-843	159	24	)	)	PUNCT
eurjchem-843	159	25	and	and	CCONJ
eurjchem-843	159	26	metformin	metformin	NOUN
eurjchem-843	159	27	(	(	PUNCT
eurjchem-843	159	28	400	400	NUM
eurjchem-843	159	29	µg	µg	NOUN
eurjchem-843	159	30	/	/	SYM
eurjchem-843	159	31	ml	ml	NOUN
eurjchem-843	159	32	)	)	PUNCT
eurjchem-843	159	33	(	(	PUNCT
eurjchem-843	159	34	b	b	NOUN
eurjchem-843	159	35	)	)	PUNCT
eurjchem-843	159	36	.	.	PUNCT
eurjchem-843	160	1	the	the	DET
eurjchem-843	160	2	analytical	analytical	ADJ
eurjchem-843	160	3	data	datum	NOUN
eurjchem-843	160	4	of	of	ADP
eurjchem-843	160	5	the	the	DET
eurjchem-843	160	6	calibration	calibration	NOUN
eurjchem-843	160	7	curve	curve	NOUN
eurjchem-843	160	8	including	include	VERB
eurjchem-843	160	9	standard	standard	ADJ
eurjchem-843	160	10	deviations	deviation	NOUN
eurjchem-843	160	11	for	for	ADP
eurjchem-843	160	12	the	the	DET
eurjchem-843	160	13	slope	slope	NOUN
eurjchem-843	160	14	and	and	CCONJ
eurjchem-843	160	15	intercept	intercept	PROPN
eurjchem-843	160	16	(	(	PUNCT
eurjchem-843	160	17	sb	sb	PROPN
eurjchem-843	160	18	,	,	PUNCT
eurjchem-843	160	19	sa	sa	PROPN
eurjchem-843	160	20	)	)	PUNCT
eurjchem-843	160	21	are	be	AUX
eurjchem-843	160	22	summarized	summarize	VERB
eurjchem-843	160	23	in	in	ADP
eurjchem-843	160	24	table	table	NOUN
eurjchem-843	160	25	3	3	NUM
eurjchem-843	160	26	.	.	PUNCT
eurjchem-843	161	1	3.2.1.2	3.2.1.2	NUM
eurjchem-843	161	2	.	.	NOUN
eurjchem-843	161	3	lc‐uv	lc‐uv	PROPN
eurjchem-843	162	1	method	method	PROPN
eurjchem-843	162	2	linearity	linearity	PROPN
eurjchem-843	162	3	was	be	AUX
eurjchem-843	162	4	studied	study	VERB
eurjchem-843	162	5	for	for	ADP
eurjchem-843	162	6	stg	stg	PROPN
eurjchem-843	162	7	and	and	CCONJ
eurjchem-843	162	8	met	meet	VERB
eurjchem-843	162	9	.	.	PUNCT
eurjchem-843	163	1	a	a	DET
eurjchem-843	163	2	linear	linear	ADJ
eurjchem-843	163	3	relationship	relationship	NOUN
eurjchem-843	163	4	between	between	ADP
eurjchem-843	163	5	area	area	NOUN
eurjchem-843	163	6	under	under	ADP
eurjchem-843	163	7	the	the	DET
eurjchem-843	163	8	peak	peak	NOUN
eurjchem-843	163	9	(	(	PUNCT
eurjchem-843	163	10	aup	aup	PROPN
eurjchem-843	163	11	)	)	PUNCT
eurjchem-843	163	12	and	and	CCONJ
eurjchem-843	163	13	components	component	NOUN
eurjchem-843	163	14	’	'	PUNCT
eurjchem-843	163	15	concentrations	concentration	NOUN
eurjchem-843	163	16	(	(	PUNCT
eurjchem-843	163	17	c	c	X
eurjchem-843	163	18	)	)	PUNCT
eurjchem-843	163	19	was	be	AUX
eurjchem-843	163	20	obtained	obtain	VERB
eurjchem-843	163	21	.	.	PUNCT
eurjchem-843	164	1	the	the	DET
eurjchem-843	164	2	regression	regression	NOUN
eurjchem-843	164	3	equation	equation	NOUN
eurjchem-843	164	4	for	for	ADP
eurjchem-843	164	5	each	each	DET
eurjchem-843	164	6	drug	drug	NOUN
eurjchem-843	164	7	was	be	AUX
eurjchem-843	164	8	also	also	ADV
eurjchem-843	164	9	computed	compute	VERB
eurjchem-843	164	10	,	,	PUNCT
eurjchem-843	164	11	table	table	NOUN
eurjchem-843	164	12	4	4	NUM
eurjchem-843	164	13	.	.	PUNCT
eurjchem-843	165	1	the	the	DET
eurjchem-843	165	2	linearity	linearity	NOUN
eurjchem-843	165	3	of	of	ADP
eurjchem-843	165	4	the	the	DET
eurjchem-843	165	5	calibration	calibration	NOUN
eurjchem-843	165	6	curves	curve	NOUN
eurjchem-843	165	7	were	be	AUX
eurjchem-843	165	8	validated	validate	VERB
eurjchem-843	165	9	by	by	ADP
eurjchem-843	165	10	the	the	DET
eurjchem-843	165	11	high	high	ADJ
eurjchem-843	165	12	value	value	NOUN
eurjchem-843	165	13	of	of	ADP
eurjchem-843	165	14	correlation	correlation	NOUN
eurjchem-843	165	15	coefficients	coefficient	NOUN
eurjchem-843	165	16	.	.	PUNCT
eurjchem-843	166	1	the	the	DET
eurjchem-843	166	2	analytical	analytical	ADJ
eurjchem-843	166	3	data	datum	NOUN
eurjchem-843	166	4	of	of	ADP
eurjchem-843	166	5	the	the	DET
eurjchem-843	166	6	calibration	calibration	NOUN
eurjchem-843	166	7	curves	curve	NOUN
eurjchem-843	166	8	including	include	VERB
eurjchem-843	166	9	standard	standard	ADJ
eurjchem-843	166	10	deviations	deviation	NOUN
eurjchem-843	166	11	for	for	ADP
eurjchem-843	166	12	the	the	DET
eurjchem-843	166	13	slope	slope	NOUN
eurjchem-843	166	14	and	and	CCONJ
eurjchem-843	166	15	intercept	intercept	PROPN
eurjchem-843	166	16	(	(	PUNCT
eurjchem-843	166	17	sb	sb	PROPN
eurjchem-843	166	18	,	,	PUNCT
eurjchem-843	166	19	sa	sa	PROPN
eurjchem-843	166	20	)	)	PUNCT
eurjchem-843	166	21	are	be	AUX
eurjchem-843	166	22	summarized	summarize	VERB
eurjchem-843	166	23	in	in	ADP
eurjchem-843	166	24	table	table	NOUN
eurjchem-843	166	25	4	4	NUM
eurjchem-843	166	26	.	.	X
eurjchem-843	166	27	3.2.2	3.2.2	NUM
eurjchem-843	166	28	.	.	PUNCT
eurjchem-843	167	1	accuracy	accuracy	NOUN
eurjchem-843	167	2	3.2.2.1	3.2.2.1	NUM
eurjchem-843	167	3	.	.	PUNCT
eurjchem-843	168	1	lc‐fluoro	lc‐fluoro	PROPN
eurjchem-843	168	2	method	method	NOUN
eurjchem-843	168	3	accuracy	accuracy	NOUN
eurjchem-843	168	4	of	of	ADP
eurjchem-843	168	5	the	the	DET
eurjchem-843	168	6	results	result	NOUN
eurjchem-843	168	7	was	be	AUX
eurjchem-843	168	8	calculated	calculate	VERB
eurjchem-843	168	9	by	by	ADP
eurjchem-843	168	10	%	%	NOUN
eurjchem-843	168	11	recovery	recovery	NOUN
eurjchem-843	168	12	of	of	ADP
eurjchem-843	168	13	5	5	NUM
eurjchem-843	168	14	different	different	ADJ
eurjchem-843	168	15	concentrations	concentration	NOUN
eurjchem-843	168	16	of	of	ADP
eurjchem-843	168	17	stg	stg	PROPN
eurjchem-843	168	18	in	in	ADP
eurjchem-843	168	19	laboratory‐prepared	laboratory‐prepared	ADJ
eurjchem-843	168	20	mixtures	mixture	NOUN
eurjchem-843	168	21	with	with	ADP
eurjchem-843	168	22	sdp	sdp	NOUN
eurjchem-843	168	23	(	(	PUNCT
eurjchem-843	168	24	10	10	NUM
eurjchem-843	168	25	to	to	PART
eurjchem-843	168	26	30	30	NUM
eurjchem-843	168	27	%	%	NOUN
eurjchem-843	168	28	of	of	ADP
eurjchem-843	168	29	stg	stg	PROPN
eurjchem-843	168	30	,	,	PUNCT
eurjchem-843	168	31	w	w	NOUN
eurjchem-843	168	32	:	:	SYM
eurjchem-843	168	33	w	w	NOUN
eurjchem-843	168	34	)	)	PUNCT
eurjchem-843	168	35	and	and	CCONJ
eurjchem-843	168	36	also	also	ADV
eurjchem-843	168	37	by	by	ADP
eurjchem-843	168	38	standard	standard	ADJ
eurjchem-843	168	39	addition	addition	NOUN
eurjchem-843	168	40	technique	technique	NOUN
eurjchem-843	168	41	applied	apply	VERB
eurjchem-843	168	42	for	for	ADP
eurjchem-843	168	43	januvia	januvia	NOUN
eurjchem-843	168	44	®	®	NOUN
eurjchem-843	168	45	tablets	tablet	NOUN
eurjchem-843	168	46	,	,	PUNCT
eurjchem-843	168	47	all	all	PRON
eurjchem-843	168	48	carried	carry	VERB
eurjchem-843	168	49	out	out	ADP
eurjchem-843	168	50	in	in	ADP
eurjchem-843	168	51	triplicates	triplicate	NOUN
eurjchem-843	168	52	.	.	PUNCT
eurjchem-843	169	1	the	the	DET
eurjchem-843	169	2	results	result	NOUN
eurjchem-843	169	3	obtained	obtain	VERB
eurjchem-843	169	4	including	include	VERB
eurjchem-843	169	5	the	the	DET
eurjchem-843	169	6	mean	mean	NOUN
eurjchem-843	169	7	of	of	ADP
eurjchem-843	169	8	the	the	DET
eurjchem-843	169	9	recovery	recovery	NOUN
eurjchem-843	169	10	and	and	CCONJ
eurjchem-843	169	11	standard	standard	ADJ
eurjchem-843	169	12	deviation	deviation	NOUN
eurjchem-843	169	13	are	be	AUX
eurjchem-843	169	14	displayed	display	VERB
eurjchem-843	169	15	in	in	ADP
eurjchem-843	169	16	table	table	NOUN
eurjchem-843	169	17	3	3	NUM
eurjchem-843	169	18	.	.	PUNCT
eurjchem-843	169	19	3.2.2.2	3.2.2.2	NUM
eurjchem-843	169	20	.	.	PROPN
eurjchem-843	169	21	lc‐uv	lc‐uv	PROPN
eurjchem-843	170	1	method	method	PROPN
eurjchem-843	170	2	accuracy	accuracy	NOUN
eurjchem-843	170	3	of	of	ADP
eurjchem-843	170	4	the	the	DET
eurjchem-843	170	5	results	result	NOUN
eurjchem-843	170	6	was	be	AUX
eurjchem-843	170	7	calculated	calculate	VERB
eurjchem-843	170	8	by	by	ADP
eurjchem-843	170	9	%	%	INTJ
eurjchem-843	170	10	recovery	recovery	NOUN
eurjchem-843	170	11	of	of	ADP
eurjchem-843	170	12	five	five	NUM
eurjchem-843	170	13	different	different	ADJ
eurjchem-843	170	14	concentrations	concentration	NOUN
eurjchem-843	170	15	of	of	ADP
eurjchem-843	170	16	the	the	DET
eurjchem-843	170	17	laboratory	laboratory	NOUN
eurjchem-843	170	18	prepared	prepare	VERB
eurjchem-843	170	19	mixtures	mixture	NOUN
eurjchem-843	170	20	of	of	ADP
eurjchem-843	170	21	the	the	DET
eurjchem-843	170	22	two	two	NUM
eurjchem-843	170	23	drugs	drug	NOUN
eurjchem-843	170	24	with	with	ADP
eurjchem-843	170	25	sdp	sdp	NOUN
eurjchem-843	170	26	and	and	CCONJ
eurjchem-843	170	27	also	also	ADV
eurjchem-843	170	28	by	by	ADP
eurjchem-843	170	29	standard	standard	ADJ
eurjchem-843	170	30	addition	addition	NOUN
eurjchem-843	170	31	technique	technique	NOUN
eurjchem-843	170	32	applied	apply	VERB
eurjchem-843	170	33	for	for	ADP
eurjchem-843	170	34	janumet	janumet	ADJ
eurjchem-843	170	35	®	®	NOUN
eurjchem-843	170	36	tablets	tablet	NOUN
eurjchem-843	170	37	,	,	PUNCT
eurjchem-843	170	38	all	all	PRON
eurjchem-843	170	39	carried	carry	VERB
eurjchem-843	170	40	out	out	ADP
eurjchem-843	170	41	in	in	ADP
eurjchem-843	170	42	triplicates	triplicate	NOUN
eurjchem-843	170	43	.	.	PUNCT
eurjchem-843	171	1	the	the	DET
eurjchem-843	171	2	results	result	NOUN
eurjchem-843	171	3	obtained	obtain	VERB
eurjchem-843	171	4	including	include	VERB
eurjchem-843	171	5	the	the	DET
eurjchem-843	171	6	mean	mean	NOUN
eurjchem-843	171	7	of	of	ADP
eurjchem-843	171	8	the	the	DET
eurjchem-843	171	9	recovery	recovery	NOUN
eurjchem-843	171	10	and	and	CCONJ
eurjchem-843	171	11	standard	standard	ADJ
eurjchem-843	171	12	deviation	deviation	NOUN
eurjchem-843	171	13	are	be	AUX
eurjchem-843	171	14	displayed	display	VERB
eurjchem-843	171	15	in	in	ADP
eurjchem-843	171	16	table	table	NOUN
eurjchem-843	171	17	4	4	NUM
eurjchem-843	171	18	.	.	PUNCT
eurjchem-843	172	1	3.2.3	3.2.3	NUM
eurjchem-843	172	2	.	.	X
eurjchem-843	172	3	precision	precision	PROPN
eurjchem-843	172	4	3.2.3.1	3.2.3.1	PROPN
eurjchem-843	172	5	.	.	PUNCT
eurjchem-843	172	6	lc‐fluoro	lc‐fluoro	PROPN
eurjchem-843	172	7	method	method	NOUN
eurjchem-843	172	8	precision	precision	NOUN
eurjchem-843	172	9	was	be	AUX
eurjchem-843	172	10	estimated	estimate	VERB
eurjchem-843	172	11	by	by	ADP
eurjchem-843	172	12	repeatability	repeatability	NOUN
eurjchem-843	172	13	.	.	PUNCT
eurjchem-843	173	1	the	the	DET
eurjchem-843	173	2	repeatability	repeatability	NOUN
eurjchem-843	173	3	was	be	AUX
eurjchem-843	173	4	assessed	assess	VERB
eurjchem-843	173	5	by	by	ADP
eurjchem-843	173	6	analyzing	analyze	VERB
eurjchem-843	173	7	a	a	DET
eurjchem-843	173	8	mixture	mixture	NOUN
eurjchem-843	173	9	containing	contain	VERB
eurjchem-843	173	10	30	30	NUM
eurjchem-843	173	11	and	and	CCONJ
eurjchem-843	173	12	100	100	NUM
eurjchem-843	173	13	µg	µg	ADJ
eurjchem-843	173	14	/	/	SYM
eurjchem-843	173	15	ml	ml	NOUN
eurjchem-843	173	16	of	of	ADP
eurjchem-843	173	17	spd	spd	NOUN
eurjchem-843	173	18	and	and	CCONJ
eurjchem-843	173	19	stg	stg	NOUN
eurjchem-843	173	20	,	,	PUNCT
eurjchem-843	173	21	respectively	respectively	ADV
eurjchem-843	173	22	(	(	PUNCT
eurjchem-843	173	23	n	n	NOUN
eurjchem-843	173	24	=	=	SYM
eurjchem-843	173	25	6	6	NUM
eurjchem-843	173	26	)	)	PUNCT
eurjchem-843	173	27	.	.	PUNCT
eurjchem-843	174	1	the	the	DET
eurjchem-843	174	2	values	value	NOUN
eurjchem-843	174	3	of	of	ADP
eurjchem-843	174	4	repeatability	repeatability	NOUN
eurjchem-843	174	5	,	,	PUNCT
eurjchem-843	174	6	intra‐day	intra‐day	NOUN
eurjchem-843	174	7	and	and	CCONJ
eurjchem-843	174	8	inter‐day	inter‐day	PROPN
eurjchem-843	174	9	precision	precision	NOUN
eurjchem-843	174	10	(	(	PUNCT
eurjchem-843	174	11	using	use	VERB
eurjchem-843	174	12	3	3	NUM
eurjchem-843	174	13	different	different	ADJ
eurjchem-843	174	14	concentrations	concentration	NOUN
eurjchem-843	174	15	in	in	ADP
eurjchem-843	174	16	triplicates	triplicate	NOUN
eurjchem-843	174	17	for	for	ADP
eurjchem-843	174	18	three	three	NUM
eurjchem-843	174	19	consecutive	consecutive	ADJ
eurjchem-843	174	20	days	day	NOUN
eurjchem-843	174	21	)	)	PUNCT
eurjchem-843	174	22	for	for	ADP
eurjchem-843	174	23	stg	stg	PROPN
eurjchem-843	174	24	are	be	AUX
eurjchem-843	174	25	displayed	display	VERB
eurjchem-843	174	26	in	in	ADP
eurjchem-843	174	27	tables	table	NOUN
eurjchem-843	174	28	1	1	NUM
eurjchem-843	174	29	and	and	CCONJ
eurjchem-843	174	30	3	3	NUM
eurjchem-843	174	31	.	.	X
eurjchem-843	174	32	3.2.3.2	3.2.3.2	NUM
eurjchem-843	174	33	.	.	NOUN
eurjchem-843	174	34	lc‐uv	lc‐uv	PROPN
eurjchem-843	174	35	method	method	VERB
eurjchem-843	174	36	the	the	DET
eurjchem-843	174	37	repeatability	repeatability	NOUN
eurjchem-843	174	38	was	be	AUX
eurjchem-843	174	39	assessed	assess	VERB
eurjchem-843	174	40	by	by	ADP
eurjchem-843	174	41	analyzing	analyze	VERB
eurjchem-843	174	42	a	a	DET
eurjchem-843	174	43	mixture	mixture	NOUN
eurjchem-843	174	44	containing	contain	VERB
eurjchem-843	174	45	25.7	25.7	NUM
eurjchem-843	174	46	,	,	PUNCT
eurjchem-843	174	47	400.0	400.0	NUM
eurjchem-843	174	48	and	and	CCONJ
eurjchem-843	174	49	7.7	7.7	NUM
eurjchem-843	174	50	µg	µg	NOUN
eurjchem-843	174	51	/	/	SYM
eurjchem-843	174	52	ml	ml	NOUN
eurjchem-843	174	53	of	of	ADP
eurjchem-843	174	54	stg	stg	NOUN
eurjchem-843	174	55	,	,	PUNCT
eurjchem-843	174	56	met	meet	VERB
eurjchem-843	174	57	and	and	CCONJ
eurjchem-843	174	58	sdp	sdp	NOUN
eurjchem-843	174	59	,	,	PUNCT
eurjchem-843	174	60	respectively	respectively	ADV
eurjchem-843	174	61	(	(	PUNCT
eurjchem-843	174	62	n	n	NOUN
eurjchem-843	174	63	=	=	SYM
eurjchem-843	174	64	6	6	NUM
eurjchem-843	174	65	)	)	PUNCT
eurjchem-843	174	66	.	.	PUNCT
eurjchem-843	175	1	the	the	DET
eurjchem-843	175	2	values	value	NOUN
eurjchem-843	175	3	of	of	ADP
eurjchem-843	175	4	repeatability	repeatability	NOUN
eurjchem-843	175	5	for	for	ADP
eurjchem-843	175	6	stg	stg	NOUN
eurjchem-843	175	7	and	and	CCONJ
eurjchem-843	175	8	met	meet	VERB
eurjchem-843	175	9	peaks	peak	NOUN
eurjchem-843	175	10	,	,	PUNCT
eurjchem-843	175	11	intra‐day	intra‐day	NOUN
eurjchem-843	175	12	and	and	CCONJ
eurjchem-843	175	13	inter‐day	inter‐day	PROPN
eurjchem-843	175	14	precision	precision	NOUN
eurjchem-843	175	15	(	(	PUNCT
eurjchem-843	175	16	using	use	VERB
eurjchem-843	175	17	3	3	NUM
eurjchem-843	175	18	different	different	ADJ
eurjchem-843	175	19	concentrations	concentration	NOUN
eurjchem-843	175	20	in	in	ADP
eurjchem-843	175	21	triplicates	triplicate	NOUN
eurjchem-843	175	22	for	for	ADP
eurjchem-843	175	23	three	three	NUM
eurjchem-843	175	24	consecutive	consecutive	ADJ
eurjchem-843	175	25	days	day	NOUN
eurjchem-843	175	26	)	)	PUNCT
eurjchem-843	175	27	are	be	AUX
eurjchem-843	175	28	displayed	display	VERB
eurjchem-843	175	29	,	,	PUNCT
eurjchem-843	175	30	tables	table	NOUN
eurjchem-843	175	31	2	2	NUM
eurjchem-843	175	32	and	and	CCONJ
eurjchem-843	175	33	4	4	NUM
eurjchem-843	175	34	.	.	X
eurjchem-843	176	1	3.2.4	3.2.4	NUM
eurjchem-843	176	2	.	.	PUNCT
eurjchem-843	177	1	specificity	specificity	NOUN
eurjchem-843	177	2	specificity	specificity	NOUN
eurjchem-843	177	3	is	be	AUX
eurjchem-843	177	4	the	the	DET
eurjchem-843	177	5	ability	ability	NOUN
eurjchem-843	177	6	of	of	ADP
eurjchem-843	177	7	the	the	DET
eurjchem-843	177	8	analytical	analytical	ADJ
eurjchem-843	177	9	method	method	NOUN
eurjchem-843	177	10	to	to	PART
eurjchem-843	177	11	measure	measure	VERB
eurjchem-843	177	12	the	the	DET
eurjchem-843	177	13	analyte	analyte	NOUN
eurjchem-843	177	14	response	response	NOUN
eurjchem-843	177	15	in	in	ADP
eurjchem-843	177	16	the	the	DET
eurjchem-843	177	17	presence	presence	NOUN
eurjchem-843	177	18	of	of	ADP
eurjchem-843	177	19	interferences	interference	NOUN
eurjchem-843	177	20	including	include	VERB
eurjchem-843	177	21	degradation	degradation	NOUN
eurjchem-843	177	22	products	product	NOUN
eurjchem-843	177	23	and	and	CCONJ
eurjchem-843	177	24	related	related	ADJ
eurjchem-843	177	25	substances	substance	NOUN
eurjchem-843	177	26	.	.	PUNCT
eurjchem-843	178	1	the	the	DET
eurjchem-843	178	2	proposed	propose	VERB
eurjchem-843	178	3	methods	method	NOUN
eurjchem-843	178	4	were	be	AUX
eurjchem-843	178	5	used	use	VERB
eurjchem-843	178	6	for	for	ADP
eurjchem-843	178	7	the	the	DET
eurjchem-843	178	8	determination	determination	NOUN
eurjchem-843	178	9	of	of	ADP
eurjchem-843	178	10	stg	stg	PROPN
eurjchem-843	178	11	alone	alone	ADJ
eurjchem-843	178	12	or	or	CCONJ
eurjchem-843	178	13	the	the	DET
eurjchem-843	178	14	mixture	mixture	NOUN
eurjchem-843	178	15	of	of	ADP
eurjchem-843	178	16	stg	stg	PROPN
eurjchem-843	178	17	and	and	CCONJ
eurjchem-843	178	18	met	meet	VERB
eurjchem-843	178	19	in	in	ADP
eurjchem-843	178	20	the	the	DET
eurjchem-843	178	21	presence	presence	NOUN
eurjchem-843	178	22	of	of	ADP
eurjchem-843	178	23	sdp	sdp	NOUN
eurjchem-843	178	24	;	;	PUNCT
eurjchem-843	178	25	the	the	DET
eurjchem-843	178	26	acid	acid	NOUN
eurjchem-843	178	27	degradation	degradation	NOUN
eurjchem-843	178	28	of	of	ADP
eurjchem-843	178	29	stg	stg	PROPN
eurjchem-843	178	30	.	.	PUNCT
eurjchem-843	179	1	besides	besides	SCONJ
eurjchem-843	179	2	,	,	PUNCT
eurjchem-843	179	3	the	the	DET
eurjchem-843	179	4	chromatograms	chromatogram	NOUN
eurjchem-843	179	5	of	of	ADP
eurjchem-843	179	6	the	the	DET
eurjchem-843	179	7	samples	sample	NOUN
eurjchem-843	179	8	were	be	AUX
eurjchem-843	179	9	checked	check	VERB
eurjchem-843	179	10	for	for	ADP
eurjchem-843	179	11	the	the	DET
eurjchem-843	179	12	appearance	appearance	NOUN
eurjchem-843	179	13	of	of	ADP
eurjchem-843	179	14	any	any	DET
eurjchem-843	179	15	extra	extra	ADJ
eurjchem-843	179	16	peaks	peak	NOUN
eurjchem-843	179	17	.	.	PUNCT
eurjchem-843	180	1	no	no	DET
eurjchem-843	180	2	chromatographic	chromatographic	ADJ
eurjchem-843	180	3	interference	interference	NOUN
eurjchem-843	180	4	from	from	ADP
eurjchem-843	180	5	any	any	PRON
eurjchem-843	180	6	of	of	ADP
eurjchem-843	180	7	the	the	DET
eurjchem-843	180	8	excipients	excipient	NOUN
eurjchem-843	180	9	was	be	AUX
eurjchem-843	180	10	found	find	VERB
eurjchem-843	180	11	at	at	ADP
eurjchem-843	180	12	the	the	DET
eurjchem-843	180	13	retention	retention	NOUN
eurjchem-843	180	14	times	time	NOUN
eurjchem-843	180	15	of	of	ADP
eurjchem-843	180	16	the	the	DET
eurjchem-843	180	17	examined	examine	VERB
eurjchem-843	180	18	compounds	compound	NOUN
eurjchem-843	180	19	.	.	PUNCT
eurjchem-843	181	1	in	in	ADP
eurjchem-843	181	2	addition	addition	NOUN
eurjchem-843	181	3	,	,	PUNCT
eurjchem-843	181	4	the	the	DET
eurjchem-843	181	5	chromatogram	chromatogram	NOUN
eurjchem-843	181	6	of	of	ADP
eurjchem-843	181	7	each	each	DET
eurjchem-843	181	8	compound	compound	NOUN
eurjchem-843	181	9	in	in	ADP
eurjchem-843	181	10	the	the	DET
eurjchem-843	181	11	sample	sample	NOUN
eurjchem-843	181	12	solution	solution	NOUN
eurjchem-843	181	13	was	be	AUX
eurjchem-843	181	14	found	find	VERB
eurjchem-843	181	15	identical	identical	ADJ
eurjchem-843	181	16	to	to	ADP
eurjchem-843	181	17	the	the	DET
eurjchem-843	181	18	chromatogram	chromatogram	NOUN
eurjchem-843	181	19	received	receive	VERB
eurjchem-843	181	20	by	by	ADP
eurjchem-843	181	21	the	the	DET
eurjchem-843	181	22	standard	standard	ADJ
eurjchem-843	181	23	solution	solution	NOUN
eurjchem-843	181	24	at	at	ADP
eurjchem-843	181	25	the	the	DET
eurjchem-843	181	26	wavelengths	wavelength	NOUN
eurjchem-843	181	27	applied	apply	VERB
eurjchem-843	181	28	.	.	PUNCT
eurjchem-843	182	1	these	these	DET
eurjchem-843	182	2	results	result	NOUN
eurjchem-843	182	3	demonstrate	demonstrate	VERB
eurjchem-843	182	4	the	the	DET
eurjchem-843	182	5	absence	absence	NOUN
eurjchem-843	182	6	of	of	ADP
eurjchem-843	182	7	interference	interference	NOUN
eurjchem-843	182	8	from	from	ADP
eurjchem-843	182	9	other	other	ADJ
eurjchem-843	182	10	materials	material	NOUN
eurjchem-843	182	11	in	in	ADP
eurjchem-843	182	12	the	the	DET
eurjchem-843	182	13	pharmaceutical	pharmaceutical	NOUN
eurjchem-843	182	14	formulations	formulation	NOUN
eurjchem-843	182	15	and	and	CCONJ
eurjchem-843	182	16	therefore	therefore	ADV
eurjchem-843	182	17	confirm	confirm	VERB
eurjchem-843	182	18	the	the	DET
eurjchem-843	182	19	specificity	specificity	NOUN
eurjchem-843	182	20	of	of	ADP
eurjchem-843	182	21	the	the	DET
eurjchem-843	182	22	two	two	NUM
eurjchem-843	182	23	proposed	propose	VERB
eurjchem-843	182	24	methods	method	NOUN
eurjchem-843	182	25	.	.	PUNCT
eurjchem-843	183	1	3.2.5	3.2.5	X
eurjchem-843	183	2	.	.	PUNCT
eurjchem-843	184	1	robustness	robustness	NOUN
eurjchem-843	184	2	3.2.5.1	3.2.5.1	PROPN
eurjchem-843	184	3	.	.	PUNCT
eurjchem-843	185	1	lc‐fluoro	lc‐fluoro	PROPN
eurjchem-843	185	2	method	method	NOUN
eurjchem-843	185	3	robustness	robustness	NOUN
eurjchem-843	185	4	was	be	AUX
eurjchem-843	185	5	performed	perform	VERB
eurjchem-843	185	6	by	by	ADP
eurjchem-843	185	7	deliberately	deliberately	ADV
eurjchem-843	185	8	changing	change	VERB
eurjchem-843	185	9	the	the	DET
eurjchem-843	185	10	chromatographic	chromatographic	ADJ
eurjchem-843	185	11	conditions	condition	NOUN
eurjchem-843	185	12	.	.	PUNCT
eurjchem-843	186	1	el‐bagary	el‐bagary	PROPN
eurjchem-843	186	2	et	et	PROPN
eurjchem-843	186	3	al	al	PROPN
eurjchem-843	186	4	.	.	PUNCT
eurjchem-843	186	5	/	/	SYM
eurjchem-843	186	6	european	european	PROPN
eurjchem-843	186	7	journal	journal	PROPN
eurjchem-843	186	8	of	of	ADP
eurjchem-843	186	9	chemistry	chemistry	NOUN
eurjchem-843	186	10	4	4	NUM
eurjchem-843	186	11	(	(	PUNCT
eurjchem-843	186	12	4	4	NUM
eurjchem-843	186	13	)	)	PUNCT
eurjchem-843	186	14	(	(	PUNCT
eurjchem-843	186	15	2013	2013	NUM
eurjchem-843	186	16	)	)	PUNCT
eurjchem-843	186	17	360‐365	360‐365	NUM
eurjchem-843	186	18	365	365	NUM
eurjchem-843	186	19	table	table	NOUN
eurjchem-843	186	20	5	5	NUM
eurjchem-843	186	21	.	.	PUNCT
eurjchem-843	187	1	statistical	statistical	ADJ
eurjchem-843	187	2	comparison	comparison	NOUN
eurjchem-843	187	3	between	between	ADP
eurjchem-843	187	4	the	the	DET
eurjchem-843	187	5	results	result	NOUN
eurjchem-843	187	6	of	of	ADP
eurjchem-843	187	7	proposed	propose	VERB
eurjchem-843	187	8	methods	method	NOUN
eurjchem-843	187	9	and	and	CCONJ
eurjchem-843	187	10	the	the	DET
eurjchem-843	187	11	reference	reference	NOUN
eurjchem-843	187	12	method	method	NOUN
eurjchem-843	187	13	for	for	ADP
eurjchem-843	187	14	the	the	DET
eurjchem-843	187	15	determination	determination	NOUN
eurjchem-843	187	16	of	of	ADP
eurjchem-843	187	17	sitagliptin	sitagliptin	NOUN
eurjchem-843	187	18	.	.	PUNCT
eurjchem-843	188	1	statistical	statistical	ADJ
eurjchem-843	188	2	term	term	NOUN
eurjchem-843	188	3	a	a	DET
eurjchem-843	188	4	reference	reference	NOUN
eurjchem-843	188	5	method	method	NOUN
eurjchem-843	188	6	b	b	NOUN
eurjchem-843	188	7	lc‐fluoro	lc‐fluoro	PROPN
eurjchem-843	188	8	lc‐fluoro	lc‐fluoro	PROPN
eurjchem-843	188	9	plasma	plasma	NOUN
eurjchem-843	188	10	lc‐uv	lc‐uv	NOUN
eurjchem-843	188	11	mean	mean	NOUN
eurjchem-843	188	12	100.5	100.5	NUM
eurjchem-843	189	1	99.65	99.65	NUM
eurjchem-843	189	2	100.81	100.81	NUM
eurjchem-843	189	3	99.72	99.72	NUM
eurjchem-843	189	4	±s.d	±s.d	PROPN
eurjchem-843	189	5	.	.	PUNCT
eurjchem-843	190	1	1.39	1.39	NUM
eurjchem-843	190	2	1.00	1.00	NUM
eurjchem-843	190	3	1.65	1.65	NUM
eurjchem-843	190	4	1.50	1.50	NUM
eurjchem-843	190	5	±s.e	±s.e	NOUN
eurjchem-843	190	6	.	.	PROPN
eurjchem-843	190	7	0.62	0.62	NUM
eurjchem-843	190	8	0.45	0.45	NUM
eurjchem-843	190	9	0.74	0.74	NUM
eurjchem-843	190	10	0.67	0.67	NUM
eurjchem-843	190	11	%	%	NOUN
eurjchem-843	190	12	r.s.d	r.s.d	NOUN
eurjchem-843	190	13	.	.	PUNCT
eurjchem-843	191	1	1.38	1.38	NUM
eurjchem-843	191	2	1.00	1.00	NUM
eurjchem-843	191	3	1.64	1.64	NUM
eurjchem-843	191	4	1.50	1.50	NUM
eurjchem-843	191	5	n	n	PRON
eurjchem-843	191	6	5	5	NUM
eurjchem-843	191	7	5	5	NUM
eurjchem-843	191	8	5	5	NUM
eurjchem-843	191	9	5	5	NUM
eurjchem-843	191	10	v	v	ADP
eurjchem-843	191	11	1.93	1.93	NUM
eurjchem-843	191	12	1.00	1.00	NUM
eurjchem-843	191	13	2.72	2.72	NUM
eurjchem-843	191	14	2.25	2.25	NUM
eurjchem-843	191	15	t	t	NOUN
eurjchem-843	191	16	(	(	PUNCT
eurjchem-843	191	17	2.306	2.306	NUM
eurjchem-843	191	18	)	)	PUNCT
eurjchem-843	191	19	c	c	NOUN
eurjchem-843	191	20	‐	‐	NOUN
eurjchem-843	191	21	1.10	1.10	NUM
eurjchem-843	191	22	0.32	0.32	NUM
eurjchem-843	191	23	0.85	0.85	NUM
eurjchem-843	191	24	a	a	DET
eurjchem-843	191	25	s.d	s.d	PROPN
eurjchem-843	191	26	.	.	PUNCT
eurjchem-843	191	27	:	:	PUNCT
eurjchem-843	191	28	standard	standard	ADJ
eurjchem-843	191	29	deviation	deviation	NOUN
eurjchem-843	191	30	,	,	PUNCT
eurjchem-843	191	31	s.e	s.e	PROPN
eurjchem-843	191	32	.	.	PROPN
eurjchem-843	191	33	:	:	PUNCT
eurjchem-843	191	34	standard	standard	ADJ
eurjchem-843	191	35	error	error	NOUN
eurjchem-843	191	36	,	,	PUNCT
eurjchem-843	191	37	%	%	INTJ
eurjchem-843	191	38	r.s.d	r.s.d	NOUN
eurjchem-843	191	39	.	.	PUNCT
eurjchem-843	191	40	:	:	PUNCT
eurjchem-843	191	41	relative	relative	ADJ
eurjchem-843	191	42	standard	standard	ADJ
eurjchem-843	191	43	deviation	deviation	NOUN
eurjchem-843	191	44	,	,	PUNCT
eurjchem-843	191	45	n	n	CCONJ
eurjchem-843	191	46	:	:	PUNCT
eurjchem-843	191	47	number	number	NOUN
eurjchem-843	191	48	of	of	ADP
eurjchem-843	191	49	samples	sample	NOUN
eurjchem-843	191	50	,	,	PUNCT
eurjchem-843	191	51	v	v	NOUN
eurjchem-843	191	52	:	:	PUNCT
eurjchem-843	191	53	variance	variance	NOUN
eurjchem-843	191	54	.	.	PUNCT
eurjchem-843	192	1	b	b	X
eurjchem-843	192	2	reference	reference	NOUN
eurjchem-843	192	3	method	method	NOUN
eurjchem-843	192	4	:	:	PUNCT
eurjchem-843	192	5	aliquots	aliquot	NOUN
eurjchem-843	192	6	of	of	ADP
eurjchem-843	192	7	standard	standard	ADJ
eurjchem-843	192	8	solutions	solution	NOUN
eurjchem-843	192	9	in	in	ADP
eurjchem-843	192	10	distilled	distil	VERB
eurjchem-843	192	11	water	water	NOUN
eurjchem-843	192	12	containing	contain	VERB
eurjchem-843	192	13	2‐10	2‐10	NUM
eurjchem-843	192	14	μg	μg	PROPN
eurjchem-843	192	15	/	/	SYM
eurjchem-843	192	16	ml	ml	PROPN
eurjchem-843	192	17	stg	stg	PROPN
eurjchem-843	192	18	were	be	AUX
eurjchem-843	192	19	measured	measure	VERB
eurjchem-843	192	20	at	at	ADP
eurjchem-843	192	21	220	220	NUM
eurjchem-843	192	22	nm	nm	NOUN
eurjchem-843	192	23	using	use	VERB
eurjchem-843	192	24	water	water	NOUN
eurjchem-843	192	25	as	as	ADP
eurjchem-843	192	26	a	a	DET
eurjchem-843	192	27	blank	blank	NOUN
eurjchem-843	193	1	[	[	X
eurjchem-843	193	2	1	1	NUM
eurjchem-843	193	3	]	]	PUNCT
eurjchem-843	193	4	.	.	PUNCT
eurjchem-843	194	1	no	no	DET
eurjchem-843	194	2	significant	significant	ADJ
eurjchem-843	194	3	difference	difference	NOUN
eurjchem-843	194	4	between	between	ADP
eurjchem-843	194	5	groups	group	NOUN
eurjchem-843	194	6	by	by	ADP
eurjchem-843	194	7	using	use	VERB
eurjchem-843	194	8	one	one	NUM
eurjchem-843	194	9	way	way	NOUN
eurjchem-843	194	10	anova	anova	X
eurjchem-843	194	11	with	with	ADP
eurjchem-843	194	12	f	f	PROPN
eurjchem-843	194	13	=	=	PROPN
eurjchem-843	194	14	0.84	0.84	NUM
eurjchem-843	194	15	and	and	CCONJ
eurjchem-843	194	16	p	p	NOUN
eurjchem-843	194	17	=	=	NOUN
eurjchem-843	194	18	0.49	0.49	NUM
eurjchem-843	194	19	.	.	PUNCT
eurjchem-843	195	1	c	c	NOUN
eurjchem-843	195	2	figure	figure	NOUN
eurjchem-843	195	3	in	in	ADP
eurjchem-843	195	4	parentheses	parenthesis	NOUN
eurjchem-843	195	5	are	be	AUX
eurjchem-843	195	6	the	the	DET
eurjchem-843	195	7	theoretical	theoretical	ADJ
eurjchem-843	195	8	t	t	NOUN
eurjchem-843	195	9	value	value	NOUN
eurjchem-843	195	10	at	at	ADP
eurjchem-843	195	11	(	(	PUNCT
eurjchem-843	195	12	p	p	X
eurjchem-843	195	13	=	=	NOUN
eurjchem-843	195	14	0.05	0.05	NUM
eurjchem-843	195	15	)	)	PUNCT
eurjchem-843	195	16	.	.	PUNCT
eurjchem-843	196	1	table	table	NOUN
eurjchem-843	196	2	6	6	NUM
eurjchem-843	196	3	.	.	PUNCT
eurjchem-843	197	1	statistical	statistical	ADJ
eurjchem-843	197	2	comparison	comparison	NOUN
eurjchem-843	197	3	between	between	ADP
eurjchem-843	197	4	the	the	DET
eurjchem-843	197	5	proposed	propose	VERB
eurjchem-843	197	6	method	method	NOUN
eurjchem-843	197	7	and	and	CCONJ
eurjchem-843	197	8	the	the	DET
eurjchem-843	197	9	reference	reference	NOUN
eurjchem-843	197	10	method	method	NOUN
eurjchem-843	197	11	for	for	ADP
eurjchem-843	197	12	the	the	DET
eurjchem-843	197	13	determination	determination	NOUN
eurjchem-843	197	14	of	of	ADP
eurjchem-843	197	15	metformin	metformin	NOUN
eurjchem-843	197	16	.	.	PUNCT
eurjchem-843	198	1	statistical	statistical	ADJ
eurjchem-843	198	2	term	term	NOUN
eurjchem-843	198	3	a	a	DET
eurjchem-843	198	4	reference	reference	NOUN
eurjchem-843	198	5	method	method	NOUN
eurjchem-843	198	6	b	b	PROPN
eurjchem-843	198	7	hplc	hplc	NOUN
eurjchem-843	198	8	method	method	NOUN
eurjchem-843	198	9	mean	mean	VERB
eurjchem-843	198	10	100.4	100.4	NUM
eurjchem-843	198	11	99.70	99.70	NUM
eurjchem-843	198	12	±s.d	±s.d	PROPN
eurjchem-843	198	13	.	.	PUNCT
eurjchem-843	199	1	0.28	0.28	NUM
eurjchem-843	199	2	1.74	1.74	NUM
eurjchem-843	199	3	±s.e	±s.e	NOUN
eurjchem-843	199	4	.	.	PUNCT
eurjchem-843	199	5	0.13	0.13	NUM
eurjchem-843	199	6	0.78	0.78	NUM
eurjchem-843	199	7	%	%	NOUN
eurjchem-843	199	8	r.s.d	r.s.d	NOUN
eurjchem-843	199	9	.	.	PUNCT
eurjchem-843	200	1	0.28	0.28	NUM
eurjchem-843	200	2	1.75	1.75	NUM
eurjchem-843	200	3	n	n	NOUN
eurjchem-843	200	4	5	5	NUM
eurjchem-843	200	5	5	5	NUM
eurjchem-843	200	6	v	v	ADP
eurjchem-843	200	7	0.08	0.08	NUM
eurjchem-843	200	8	3.03	3.03	NUM
eurjchem-843	200	9	t	t	NOUN
eurjchem-843	200	10	(	(	PUNCT
eurjchem-843	200	11	2.306	2.306	NUM
eurjchem-843	200	12	)	)	PUNCT
eurjchem-843	200	13	c	c	NOUN
eurjchem-843	200	14	‐	‐	ADP
eurjchem-843	200	15	0.89	0.89	NUM
eurjchem-843	200	16	a	a	DET
eurjchem-843	200	17	s.d	s.d	PROPN
eurjchem-843	200	18	.	.	PUNCT
eurjchem-843	200	19	:	:	PUNCT
eurjchem-843	200	20	standard	standard	ADJ
eurjchem-843	200	21	deviation	deviation	NOUN
eurjchem-843	200	22	,	,	PUNCT
eurjchem-843	200	23	s.e	s.e	PROPN
eurjchem-843	200	24	.	.	PROPN
eurjchem-843	200	25	:	:	PUNCT
eurjchem-843	200	26	standard	standard	ADJ
eurjchem-843	200	27	error	error	NOUN
eurjchem-843	200	28	,	,	PUNCT
eurjchem-843	200	29	%	%	INTJ
eurjchem-843	200	30	r.s.d	r.s.d	NOUN
eurjchem-843	200	31	.	.	PUNCT
eurjchem-843	200	32	:	:	PUNCT
eurjchem-843	200	33	relative	relative	ADJ
eurjchem-843	200	34	standard	standard	ADJ
eurjchem-843	200	35	deviation	deviation	NOUN
eurjchem-843	200	36	,	,	PUNCT
eurjchem-843	200	37	n	n	CCONJ
eurjchem-843	200	38	:	:	PUNCT
eurjchem-843	200	39	number	number	NOUN
eurjchem-843	200	40	of	of	ADP
eurjchem-843	200	41	samples	sample	NOUN
eurjchem-843	200	42	,	,	PUNCT
eurjchem-843	200	43	v	v	NOUN
eurjchem-843	200	44	:	:	PUNCT
eurjchem-843	200	45	variance	variance	NOUN
eurjchem-843	200	46	.	.	PUNCT
eurjchem-843	201	1	b	b	X
eurjchem-843	201	2	reference	reference	NOUN
eurjchem-843	201	3	method	method	NOUN
eurjchem-843	201	4	:	:	PUNCT
eurjchem-843	201	5	aliquots	aliquot	NOUN
eurjchem-843	201	6	of	of	ADP
eurjchem-843	201	7	standard	standard	ADJ
eurjchem-843	201	8	solutions	solution	NOUN
eurjchem-843	201	9	in	in	ADP
eurjchem-843	201	10	distilled	distil	VERB
eurjchem-843	201	11	water	water	NOUN
eurjchem-843	201	12	containing	contain	VERB
eurjchem-843	201	13	2‐12	2‐12	NUM
eurjchem-843	201	14	μg	μg	NOUN
eurjchem-843	201	15	/	/	SYM
eurjchem-843	201	16	ml	ml	VERB
eurjchem-843	201	17	met	meet	VERB
eurjchem-843	201	18	were	be	AUX
eurjchem-843	201	19	measured	measure	VERB
eurjchem-843	201	20	at	at	ADP
eurjchem-843	201	21	232	232	NUM
eurjchem-843	201	22	nm	nm	NOUN
eurjchem-843	201	23	using	use	VERB
eurjchem-843	201	24	water	water	NOUN
eurjchem-843	201	25	as	as	ADP
eurjchem-843	201	26	a	a	DET
eurjchem-843	201	27	blank	blank	NOUN
eurjchem-843	201	28	[	[	X
eurjchem-843	201	29	12	12	NUM
eurjchem-843	201	30	]	]	PUNCT
eurjchem-843	201	31	.	.	PUNCT
eurjchem-843	202	1	no	no	DET
eurjchem-843	202	2	significant	significant	ADJ
eurjchem-843	202	3	difference	difference	NOUN
eurjchem-843	202	4	between	between	ADP
eurjchem-843	202	5	groups	group	NOUN
eurjchem-843	202	6	by	by	ADP
eurjchem-843	202	7	using	use	VERB
eurjchem-843	202	8	one	one	NUM
eurjchem-843	202	9	way	way	NOUN
eurjchem-843	202	10	anova	anova	X
eurjchem-843	202	11	with	with	ADP
eurjchem-843	202	12	f	f	PROPN
eurjchem-843	202	13	=	=	SYM
eurjchem-843	202	14	0.79	0.79	NUM
eurjchem-843	202	15	and	and	CCONJ
eurjchem-843	202	16	p	p	NOUN
eurjchem-843	202	17	=	=	PROPN
eurjchem-843	202	18	0.4	0.4	NUM
eurjchem-843	202	19	.	.	PUNCT
eurjchem-843	203	1	c	c	PROPN
eurjchem-843	203	2	figure	figure	NOUN
eurjchem-843	203	3	in	in	ADP
eurjchem-843	203	4	parentheses	parenthesis	NOUN
eurjchem-843	203	5	are	be	AUX
eurjchem-843	203	6	the	the	DET
eurjchem-843	203	7	theoretical	theoretical	ADJ
eurjchem-843	203	8	t	t	NOUN
eurjchem-843	203	9	value	value	NOUN
eurjchem-843	203	10	at	at	ADP
eurjchem-843	203	11	(	(	PUNCT
eurjchem-843	203	12	p	p	X
eurjchem-843	203	13	=	=	NOUN
eurjchem-843	203	14	0.05	0.05	NUM
eurjchem-843	203	15	)	)	PUNCT
eurjchem-843	203	16	.	.	PUNCT
eurjchem-843	204	1	the	the	DET
eurjchem-843	204	2	most	most	ADV
eurjchem-843	204	3	important	important	ADJ
eurjchem-843	204	4	parameter	parameter	NOUN
eurjchem-843	204	5	to	to	PART
eurjchem-843	204	6	be	be	AUX
eurjchem-843	204	7	studied	study	VERB
eurjchem-843	204	8	was	be	AUX
eurjchem-843	204	9	the	the	DET
eurjchem-843	204	10	resolution	resolution	NOUN
eurjchem-843	204	11	factor	factor	NOUN
eurjchem-843	204	12	between	between	ADP
eurjchem-843	204	13	the	the	DET
eurjchem-843	204	14	two	two	NUM
eurjchem-843	204	15	peaks	peak	NOUN
eurjchem-843	204	16	of	of	ADP
eurjchem-843	204	17	sdp	sdp	NOUN
eurjchem-843	204	18	and	and	CCONJ
eurjchem-843	204	19	stg	stg	PROPN
eurjchem-843	204	20	.	.	PUNCT
eurjchem-843	205	1	the	the	DET
eurjchem-843	205	2	flow	flow	NOUN
eurjchem-843	205	3	rate	rate	NOUN
eurjchem-843	205	4	of	of	ADP
eurjchem-843	205	5	the	the	DET
eurjchem-843	205	6	mobile	mobile	ADJ
eurjchem-843	205	7	phase	phase	NOUN
eurjchem-843	205	8	was	be	AUX
eurjchem-843	205	9	changed	change	VERB
eurjchem-843	205	10	from	from	ADP
eurjchem-843	205	11	1	1	NUM
eurjchem-843	205	12	ml	ml	NOUN
eurjchem-843	205	13	/	/	SYM
eurjchem-843	205	14	min	min	NOUN
eurjchem-843	205	15	to	to	PART
eurjchem-843	205	16	0.8	0.8	NUM
eurjchem-843	205	17	ml	ml	NOUN
eurjchem-843	205	18	/	/	SYM
eurjchem-843	205	19	min	min	NOUN
eurjchem-843	205	20	and	and	CCONJ
eurjchem-843	205	21	1.2	1.2	NUM
eurjchem-843	205	22	ml	ml	NOUN
eurjchem-843	205	23	/	/	SYM
eurjchem-843	205	24	min	min	NOUN
eurjchem-843	205	25	,	,	PUNCT
eurjchem-843	205	26	where	where	SCONJ
eurjchem-843	205	27	resolution	resolution	NOUN
eurjchem-843	205	28	factors	factor	NOUN
eurjchem-843	205	29	obtained	obtain	VERB
eurjchem-843	205	30	were	be	AUX
eurjchem-843	205	31	6.29	6.29	NUM
eurjchem-843	205	32	,	,	PUNCT
eurjchem-843	205	33	6.14	6.14	NUM
eurjchem-843	205	34	and	and	CCONJ
eurjchem-843	205	35	6.08	6.08	NUM
eurjchem-843	205	36	,	,	PUNCT
eurjchem-843	205	37	respectively	respectively	ADV
eurjchem-843	205	38	.	.	PUNCT
eurjchem-843	206	1	the	the	DET
eurjchem-843	206	2	ratio	ratio	NOUN
eurjchem-843	206	3	of	of	ADP
eurjchem-843	206	4	acetonitrile	acetonitrile	NOUN
eurjchem-843	206	5	was	be	AUX
eurjchem-843	206	6	changed	change	VERB
eurjchem-843	206	7	from	from	ADP
eurjchem-843	206	8	70	70	NUM
eurjchem-843	206	9	%	%	NOUN
eurjchem-843	206	10	to	to	PART
eurjchem-843	206	11	72	72	NUM
eurjchem-843	206	12	%	%	NOUN
eurjchem-843	206	13	and	and	CCONJ
eurjchem-843	206	14	68	68	NUM
eurjchem-843	206	15	%	%	NOUN
eurjchem-843	206	16	,	,	PUNCT
eurjchem-843	206	17	where	where	SCONJ
eurjchem-843	206	18	resolution	resolution	NOUN
eurjchem-843	206	19	factors	factor	NOUN
eurjchem-843	206	20	obtained	obtain	VERB
eurjchem-843	206	21	were	be	AUX
eurjchem-843	206	22	6.29	6.29	NUM
eurjchem-843	206	23	,	,	PUNCT
eurjchem-843	206	24	6.34	6.34	NUM
eurjchem-843	206	25	and	and	CCONJ
eurjchem-843	206	26	6.07	6.07	NUM
eurjchem-843	206	27	,	,	PUNCT
eurjchem-843	206	28	respectively	respectively	ADV
eurjchem-843	206	29	.	.	PUNCT
eurjchem-843	207	1	finally	finally	ADV
eurjchem-843	207	2	,	,	PUNCT
eurjchem-843	207	3	the	the	DET
eurjchem-843	207	4	value	value	NOUN
eurjchem-843	207	5	of	of	ADP
eurjchem-843	207	6	ph	ph	NOUN
eurjchem-843	207	7	of	of	ADP
eurjchem-843	207	8	the	the	DET
eurjchem-843	207	9	phosphate	phosphate	ADJ
eurjchem-843	207	10	buffer	buffer	NOUN
eurjchem-843	207	11	was	be	AUX
eurjchem-843	207	12	varied	varied	ADJ
eurjchem-843	207	13	from	from	ADP
eurjchem-843	207	14	4.6	4.6	NUM
eurjchem-843	207	15	to	to	ADP
eurjchem-843	207	16	4.5	4.5	NUM
eurjchem-843	207	17	and	and	CCONJ
eurjchem-843	207	18	4.7	4.7	NUM
eurjchem-843	207	19	,	,	PUNCT
eurjchem-843	207	20	where	where	SCONJ
eurjchem-843	207	21	resolution	resolution	NOUN
eurjchem-843	207	22	factors	factor	NOUN
eurjchem-843	207	23	obtained	obtain	VERB
eurjchem-843	207	24	were	be	AUX
eurjchem-843	207	25	6.29	6.29	NUM
eurjchem-843	207	26	,	,	PUNCT
eurjchem-843	207	27	6.39	6.39	NUM
eurjchem-843	207	28	and	and	CCONJ
eurjchem-843	207	29	6.48	6.48	NUM
eurjchem-843	207	30	,	,	PUNCT
eurjchem-843	207	31	respectively	respectively	ADV
eurjchem-843	207	32	.	.	PUNCT
eurjchem-843	208	1	as	as	SCONJ
eurjchem-843	208	2	can	can	AUX
eurjchem-843	208	3	be	be	AUX
eurjchem-843	208	4	seen	see	VERB
eurjchem-843	208	5	from	from	ADP
eurjchem-843	208	6	these	these	DET
eurjchem-843	208	7	results	result	NOUN
eurjchem-843	208	8	,	,	PUNCT
eurjchem-843	208	9	good	good	ADJ
eurjchem-843	208	10	values	value	NOUN
eurjchem-843	208	11	of	of	ADP
eurjchem-843	208	12	the	the	DET
eurjchem-843	208	13	resolution	resolution	NOUN
eurjchem-843	208	14	factor	factor	NOUN
eurjchem-843	208	15	were	be	AUX
eurjchem-843	208	16	obtained	obtain	VERB
eurjchem-843	208	17	for	for	ADP
eurjchem-843	208	18	all	all	DET
eurjchem-843	208	19	these	these	DET
eurjchem-843	208	20	variations	variation	NOUN
eurjchem-843	208	21	,	,	PUNCT
eurjchem-843	208	22	indicating	indicate	VERB
eurjchem-843	208	23	good	good	ADJ
eurjchem-843	208	24	robustness	robustness	NOUN
eurjchem-843	208	25	of	of	ADP
eurjchem-843	208	26	the	the	DET
eurjchem-843	208	27	proposed	propose	VERB
eurjchem-843	208	28	lc	lc	NOUN
eurjchem-843	208	29	method	method	NOUN
eurjchem-843	208	30	.	.	PUNCT
eurjchem-843	209	1	3.2.5.2	3.2.5.2	NUM
eurjchem-843	209	2	.	.	NOUN
eurjchem-843	209	3	lc‐uv	lc‐uv	PROPN
eurjchem-843	209	4	method	method	VERB
eurjchem-843	209	5	the	the	DET
eurjchem-843	209	6	most	most	ADV
eurjchem-843	209	7	important	important	ADJ
eurjchem-843	209	8	parameter	parameter	NOUN
eurjchem-843	209	9	to	to	PART
eurjchem-843	209	10	be	be	AUX
eurjchem-843	209	11	studied	study	VERB
eurjchem-843	209	12	was	be	AUX
eurjchem-843	209	13	the	the	DET
eurjchem-843	209	14	resolution	resolution	NOUN
eurjchem-843	209	15	factor	factor	NOUN
eurjchem-843	209	16	between	between	ADP
eurjchem-843	209	17	the	the	DET
eurjchem-843	209	18	two	two	NUM
eurjchem-843	209	19	peaks	peak	NOUN
eurjchem-843	209	20	of	of	ADP
eurjchem-843	209	21	sdp	sdp	NOUN
eurjchem-843	209	22	and	and	CCONJ
eurjchem-843	209	23	stg	stg	PROPN
eurjchem-843	209	24	and	and	CCONJ
eurjchem-843	209	25	also	also	ADV
eurjchem-843	209	26	between	between	ADP
eurjchem-843	209	27	the	the	DET
eurjchem-843	209	28	two	two	NUM
eurjchem-843	209	29	peaks	peak	NOUN
eurjchem-843	209	30	of	of	ADP
eurjchem-843	209	31	stg	stg	PROPN
eurjchem-843	209	32	and	and	CCONJ
eurjchem-843	209	33	met	meet	VERB
eurjchem-843	209	34	.	.	PUNCT
eurjchem-843	210	1	the	the	DET
eurjchem-843	210	2	flow	flow	NOUN
eurjchem-843	210	3	rate	rate	NOUN
eurjchem-843	210	4	of	of	ADP
eurjchem-843	210	5	the	the	DET
eurjchem-843	210	6	mobile	mobile	ADJ
eurjchem-843	210	7	phase	phase	NOUN
eurjchem-843	210	8	was	be	AUX
eurjchem-843	210	9	changed	change	VERB
eurjchem-843	210	10	from	from	ADP
eurjchem-843	210	11	1	1	NUM
eurjchem-843	210	12	ml	ml	NOUN
eurjchem-843	210	13	/	/	SYM
eurjchem-843	210	14	min	min	NOUN
eurjchem-843	210	15	to	to	PART
eurjchem-843	210	16	0.8	0.8	NUM
eurjchem-843	210	17	ml	ml	NOUN
eurjchem-843	210	18	/	/	SYM
eurjchem-843	210	19	min	min	NOUN
eurjchem-843	210	20	and	and	CCONJ
eurjchem-843	210	21	1.2	1.2	NUM
eurjchem-843	210	22	ml	ml	NOUN
eurjchem-843	210	23	/	/	SYM
eurjchem-843	210	24	min	min	NOUN
eurjchem-843	210	25	,	,	PUNCT
eurjchem-843	210	26	where	where	SCONJ
eurjchem-843	210	27	resolution	resolution	NOUN
eurjchem-843	210	28	factors	factor	NOUN
eurjchem-843	210	29	obtained	obtain	VERB
eurjchem-843	210	30	were	be	AUX
eurjchem-843	210	31	(	(	PUNCT
eurjchem-843	210	32	6.5	6.5	NUM
eurjchem-843	210	33	,	,	PUNCT
eurjchem-843	210	34	2.1	2.1	NUM
eurjchem-843	210	35	)	)	PUNCT
eurjchem-843	210	36	,	,	PUNCT
eurjchem-843	210	37	(	(	PUNCT
eurjchem-843	210	38	6.36	6.36	NUM
eurjchem-843	210	39	,	,	PUNCT
eurjchem-843	210	40	2.14	2.14	NUM
eurjchem-843	210	41	)	)	PUNCT
eurjchem-843	210	42	and	and	CCONJ
eurjchem-843	210	43	(	(	PUNCT
eurjchem-843	210	44	6.44	6.44	NUM
eurjchem-843	210	45	,	,	PUNCT
eurjchem-843	210	46	1.95	1.95	NUM
eurjchem-843	210	47	)	)	PUNCT
eurjchem-843	210	48	,	,	PUNCT
eurjchem-843	210	49	respectively	respectively	ADV
eurjchem-843	210	50	.	.	PUNCT
eurjchem-843	211	1	the	the	DET
eurjchem-843	211	2	ratio	ratio	NOUN
eurjchem-843	211	3	of	of	ADP
eurjchem-843	211	4	acetonitrile	acetonitrile	NOUN
eurjchem-843	211	5	was	be	AUX
eurjchem-843	211	6	changed	change	VERB
eurjchem-843	211	7	from	from	ADP
eurjchem-843	211	8	85	85	NUM
eurjchem-843	211	9	%	%	NOUN
eurjchem-843	211	10	to	to	ADP
eurjchem-843	211	11	87	87	NUM
eurjchem-843	211	12	%	%	NOUN
eurjchem-843	211	13	and	and	CCONJ
eurjchem-843	211	14	83	83	NUM
eurjchem-843	211	15	%	%	NOUN
eurjchem-843	211	16	,	,	PUNCT
eurjchem-843	211	17	where	where	SCONJ
eurjchem-843	211	18	resolution	resolution	NOUN
eurjchem-843	211	19	factors	factor	NOUN
eurjchem-843	211	20	obtained	obtain	VERB
eurjchem-843	211	21	were	be	AUX
eurjchem-843	211	22	(	(	PUNCT
eurjchem-843	211	23	6.5	6.5	NUM
eurjchem-843	211	24	,	,	PUNCT
eurjchem-843	211	25	2.1	2.1	NUM
eurjchem-843	211	26	)	)	PUNCT
eurjchem-843	211	27	,	,	PUNCT
eurjchem-843	211	28	(	(	PUNCT
eurjchem-843	211	29	5.98	5.98	NUM
eurjchem-843	211	30	,	,	PUNCT
eurjchem-843	211	31	1.89	1.89	NUM
eurjchem-843	211	32	)	)	PUNCT
eurjchem-843	211	33	,	,	PUNCT
eurjchem-843	211	34	(	(	PUNCT
eurjchem-843	211	35	6.66	6.66	NUM
eurjchem-843	211	36	,	,	PUNCT
eurjchem-843	211	37	1.91	1.91	NUM
eurjchem-843	211	38	)	)	PUNCT
eurjchem-843	211	39	,	,	PUNCT
eurjchem-843	211	40	respectively	respectively	ADV
eurjchem-843	211	41	.	.	PUNCT
eurjchem-843	212	1	finally	finally	ADV
eurjchem-843	212	2	,	,	PUNCT
eurjchem-843	212	3	the	the	DET
eurjchem-843	212	4	value	value	NOUN
eurjchem-843	212	5	of	of	ADP
eurjchem-843	212	6	ph	ph	NOUN
eurjchem-843	212	7	of	of	ADP
eurjchem-843	212	8	the	the	DET
eurjchem-843	212	9	phosphate	phosphate	ADJ
eurjchem-843	212	10	buffer	buffer	NOUN
eurjchem-843	212	11	was	be	AUX
eurjchem-843	212	12	varied	varied	ADJ
eurjchem-843	212	13	from	from	ADP
eurjchem-843	212	14	4.6	4.6	NUM
eurjchem-843	212	15	to	to	ADP
eurjchem-843	212	16	4.5	4.5	NUM
eurjchem-843	212	17	and	and	CCONJ
eurjchem-843	212	18	4.7	4.7	NUM
eurjchem-843	212	19	,	,	PUNCT
eurjchem-843	212	20	where	where	SCONJ
eurjchem-843	212	21	resolution	resolution	NOUN
eurjchem-843	212	22	factors	factor	NOUN
eurjchem-843	212	23	obtained	obtain	VERB
eurjchem-843	212	24	were	be	AUX
eurjchem-843	212	25	(	(	PUNCT
eurjchem-843	212	26	6.5	6.5	NUM
eurjchem-843	212	27	,	,	PUNCT
eurjchem-843	212	28	2.1	2.1	NUM
eurjchem-843	212	29	)	)	PUNCT
eurjchem-843	212	30	,	,	PUNCT
eurjchem-843	212	31	(	(	PUNCT
eurjchem-843	212	32	6.33	6.33	NUM
eurjchem-843	212	33	,	,	PUNCT
eurjchem-843	212	34	2.12	2.12	NUM
eurjchem-843	212	35	)	)	PUNCT
eurjchem-843	212	36	and	and	CCONJ
eurjchem-843	212	37	(	(	PUNCT
eurjchem-843	212	38	6.18	6.18	NUM
eurjchem-843	212	39	,	,	PUNCT
eurjchem-843	212	40	2.16	2.16	NUM
eurjchem-843	212	41	)	)	PUNCT
eurjchem-843	212	42	,	,	PUNCT
eurjchem-843	212	43	respectively	respectively	ADV
eurjchem-843	212	44	.	.	PUNCT
eurjchem-843	213	1	as	as	SCONJ
eurjchem-843	213	2	can	can	AUX
eurjchem-843	213	3	be	be	AUX
eurjchem-843	213	4	seen	see	VERB
eurjchem-843	213	5	from	from	ADP
eurjchem-843	213	6	these	these	DET
eurjchem-843	213	7	results	result	NOUN
eurjchem-843	213	8	,	,	PUNCT
eurjchem-843	213	9	good	good	ADJ
eurjchem-843	213	10	values	value	NOUN
eurjchem-843	213	11	of	of	ADP
eurjchem-843	213	12	the	the	DET
eurjchem-843	213	13	resolution	resolution	NOUN
eurjchem-843	213	14	factor	factor	NOUN
eurjchem-843	213	15	were	be	AUX
eurjchem-843	213	16	obtained	obtain	VERB
eurjchem-843	213	17	for	for	ADP
eurjchem-843	213	18	all	all	DET
eurjchem-843	213	19	these	these	DET
eurjchem-843	213	20	variations	variation	NOUN
eurjchem-843	213	21	,	,	PUNCT
eurjchem-843	213	22	indicating	indicate	VERB
eurjchem-843	213	23	good	good	ADJ
eurjchem-843	213	24	robustness	robustness	NOUN
eurjchem-843	213	25	of	of	ADP
eurjchem-843	213	26	the	the	DET
eurjchem-843	213	27	proposed	propose	VERB
eurjchem-843	213	28	lc	lc	NOUN
eurjchem-843	213	29	method	method	NOUN
eurjchem-843	213	30	.	.	PUNCT
eurjchem-843	214	1	3.2.6	3.2.6	X
eurjchem-843	214	2	.	.	PUNCT
eurjchem-843	214	3	limit	limit	NOUN
eurjchem-843	214	4	of	of	ADP
eurjchem-843	214	5	detection	detection	NOUN
eurjchem-843	214	6	and	and	CCONJ
eurjchem-843	214	7	limit	limit	NOUN
eurjchem-843	214	8	of	of	ADP
eurjchem-843	214	9	quantification	quantification	NOUN
eurjchem-843	214	10	limit	limit	NOUN
eurjchem-843	214	11	of	of	ADP
eurjchem-843	214	12	detection	detection	NOUN
eurjchem-843	214	13	(	(	PUNCT
eurjchem-843	214	14	lod	lod	PROPN
eurjchem-843	214	15	)	)	PUNCT
eurjchem-843	214	16	which	which	PRON
eurjchem-843	214	17	represents	represent	VERB
eurjchem-843	214	18	the	the	DET
eurjchem-843	214	19	concentration	concentration	NOUN
eurjchem-843	214	20	of	of	ADP
eurjchem-843	214	21	analyte	analyte	NOUN
eurjchem-843	214	22	at	at	ADP
eurjchem-843	214	23	s	s	PROPN
eurjchem-843	214	24	/	/	SYM
eurjchem-843	214	25	n	n	PRON
eurjchem-843	214	26	ratio	ratio	NOUN
eurjchem-843	214	27	of	of	ADP
eurjchem-843	214	28	3	3	NUM
eurjchem-843	214	29	and	and	CCONJ
eurjchem-843	214	30	limit	limit	NOUN
eurjchem-843	214	31	of	of	ADP
eurjchem-843	214	32	quantification	quantification	NOUN
eurjchem-843	214	33	(	(	PUNCT
eurjchem-843	214	34	loq	loq	PROPN
eurjchem-843	214	35	)	)	PUNCT
eurjchem-843	214	36	at	at	ADP
eurjchem-843	214	37	which	which	PRON
eurjchem-843	214	38	s	s	PROPN
eurjchem-843	214	39	/	/	SYM
eurjchem-843	214	40	n	n	PRON
eurjchem-843	214	41	is	be	AUX
eurjchem-843	214	42	10	10	NUM
eurjchem-843	214	43	were	be	AUX
eurjchem-843	214	44	determined	determine	VERB
eurjchem-843	214	45	experimentally	experimentally	ADV
eurjchem-843	214	46	for	for	ADP
eurjchem-843	214	47	the	the	DET
eurjchem-843	214	48	proposed	propose	VERB
eurjchem-843	214	49	methods	method	NOUN
eurjchem-843	214	50	and	and	CCONJ
eurjchem-843	214	51	results	result	NOUN
eurjchem-843	214	52	are	be	AUX
eurjchem-843	214	53	given	give	VERB
eurjchem-843	214	54	in	in	ADP
eurjchem-843	214	55	tables	table	NOUN
eurjchem-843	214	56	3	3	NUM
eurjchem-843	214	57	and	and	CCONJ
eurjchem-843	214	58	4	4	NUM
eurjchem-843	214	59	.	.	X
eurjchem-843	214	60	3.2.7	3.2.7	NUM
eurjchem-843	214	61	.	.	PUNCT
eurjchem-843	215	1	statistical	statistical	ADJ
eurjchem-843	215	2	analysis	analysis	NOUN
eurjchem-843	215	3	a	a	DET
eurjchem-843	215	4	statistical	statistical	ADJ
eurjchem-843	215	5	analysis	analysis	NOUN
eurjchem-843	215	6	of	of	ADP
eurjchem-843	215	7	the	the	DET
eurjchem-843	215	8	results	result	NOUN
eurjchem-843	215	9	obtained	obtain	VERB
eurjchem-843	215	10	by	by	ADP
eurjchem-843	215	11	the	the	DET
eurjchem-843	215	12	proposed	propose	VERB
eurjchem-843	215	13	methods	method	NOUN
eurjchem-843	215	14	and	and	CCONJ
eurjchem-843	215	15	the	the	DET
eurjchem-843	215	16	reference	reference	NOUN
eurjchem-843	215	17	methods	method	NOUN
eurjchem-843	215	18	was	be	AUX
eurjchem-843	215	19	carried	carry	VERB
eurjchem-843	215	20	out	out	ADP
eurjchem-843	215	21	by	by	ADP
eurjchem-843	215	22	“	"	PUNCT
eurjchem-843	215	23	spss	spss	ADJ
eurjchem-843	215	24	statistical	statistical	ADJ
eurjchem-843	215	25	package	package	NOUN
eurjchem-843	215	26	version	version	NOUN
eurjchem-843	215	27	11	11	NUM
eurjchem-843	215	28	”	"	PUNCT
eurjchem-843	215	29	.	.	PUNCT
eurjchem-843	216	1	the	the	DET
eurjchem-843	216	2	significant	significant	ADJ
eurjchem-843	216	3	difference	difference	NOUN
eurjchem-843	216	4	between	between	ADP
eurjchem-843	216	5	groups	group	NOUN
eurjchem-843	216	6	was	be	AUX
eurjchem-843	216	7	tested	test	VERB
eurjchem-843	216	8	by	by	ADP
eurjchem-843	216	9	one	one	NUM
eurjchem-843	216	10	way	way	NOUN
eurjchem-843	216	11	anova	anova	X
eurjchem-843	216	12	(	(	PUNCT
eurjchem-843	216	13	f‐	f‐	NOUN
eurjchem-843	216	14	test	test	NOUN
eurjchem-843	216	15	)	)	PUNCT
eurjchem-843	216	16	at	at	ADP
eurjchem-843	216	17	p	p	NOUN
eurjchem-843	216	18	=	=	NOUN
eurjchem-843	216	19	0.05	0.05	NUM
eurjchem-843	216	20	as	as	SCONJ
eurjchem-843	216	21	shown	show	VERB
eurjchem-843	216	22	in	in	ADP
eurjchem-843	216	23	tables	table	NOUN
eurjchem-843	216	24	5	5	NUM
eurjchem-843	216	25	and	and	CCONJ
eurjchem-843	216	26	6	6	NUM
eurjchem-843	216	27	.	.	PUNCT
eurjchem-843	217	1	the	the	DET
eurjchem-843	217	2	test	test	NOUN
eurjchem-843	217	3	ascertained	ascertain	VERB
eurjchem-843	217	4	that	that	SCONJ
eurjchem-843	217	5	there	there	PRON
eurjchem-843	217	6	was	be	VERB
eurjchem-843	217	7	no	no	DET
eurjchem-843	217	8	significant	significant	ADJ
eurjchem-843	217	9	difference	difference	NOUN
eurjchem-843	217	10	among	among	ADP
eurjchem-843	217	11	the	the	DET
eurjchem-843	217	12	methods	method	NOUN
eurjchem-843	217	13	.	.	PUNCT
eurjchem-843	218	1	4	4	X
eurjchem-843	218	2	.	.	X
eurjchem-843	218	3	conclusion	conclusion	NOUN
eurjchem-843	218	4	the	the	DET
eurjchem-843	218	5	two	two	NUM
eurjchem-843	218	6	proposed	propose	VERB
eurjchem-843	218	7	lc	lc	NOUN
eurjchem-843	218	8	methods	method	NOUN
eurjchem-843	218	9	proved	prove	VERB
eurjchem-843	218	10	to	to	PART
eurjchem-843	218	11	be	be	AUX
eurjchem-843	218	12	simple	simple	ADJ
eurjchem-843	218	13	,	,	PUNCT
eurjchem-843	218	14	accurate	accurate	ADJ
eurjchem-843	218	15	and	and	CCONJ
eurjchem-843	218	16	reproducible	reproducible	ADJ
eurjchem-843	218	17	for	for	ADP
eurjchem-843	218	18	the	the	DET
eurjchem-843	218	19	determination	determination	NOUN
eurjchem-843	218	20	of	of	ADP
eurjchem-843	218	21	stg	stg	PROPN
eurjchem-843	218	22	either	either	CCONJ
eurjchem-843	218	23	alone	alone	ADJ
eurjchem-843	218	24	or	or	CCONJ
eurjchem-843	218	25	in	in	ADP
eurjchem-843	218	26	combination	combination	NOUN
eurjchem-843	218	27	with	with	ADP
eurjchem-843	218	28	met	meet	VERB
eurjchem-843	218	29	in	in	ADP
eurjchem-843	218	30	the	the	DET
eurjchem-843	218	31	presence	presence	NOUN
eurjchem-843	218	32	of	of	ADP
eurjchem-843	218	33	stg	stg	PROPN
eurjchem-843	218	34	acidic	acidic	ADJ
eurjchem-843	218	35	degradation	degradation	NOUN
eurjchem-843	218	36	product	product	NOUN
eurjchem-843	218	37	in	in	ADP
eurjchem-843	218	38	reasonable	reasonable	ADJ
eurjchem-843	218	39	run	run	NOUN
eurjchem-843	218	40	times	time	NOUN
eurjchem-843	218	41	.	.	PUNCT
eurjchem-843	219	1	the	the	DET
eurjchem-843	219	2	two	two	NUM
eurjchem-843	219	3	methods	method	NOUN
eurjchem-843	219	4	were	be	AUX
eurjchem-843	219	5	validated	validate	VERB
eurjchem-843	219	6	showing	show	VERB
eurjchem-843	219	7	satisfactory	satisfactory	ADJ
eurjchem-843	219	8	data	datum	NOUN
eurjchem-843	219	9	for	for	ADP
eurjchem-843	219	10	all	all	DET
eurjchem-843	219	11	the	the	DET
eurjchem-843	219	12	method	method	NOUN
eurjchem-843	219	13	validation	validation	NOUN
eurjchem-843	219	14	parameters	parameter	NOUN
eurjchem-843	219	15	tested	test	VERB
eurjchem-843	219	16	.	.	PUNCT
eurjchem-843	220	1	the	the	DET
eurjchem-843	220	2	developed	develop	VERB
eurjchem-843	220	3	methods	method	NOUN
eurjchem-843	220	4	are	be	AUX
eurjchem-843	220	5	stability	stability	NOUN
eurjchem-843	220	6	indicating	indicate	VERB
eurjchem-843	220	7	and	and	CCONJ
eurjchem-843	220	8	can	can	AUX
eurjchem-843	220	9	be	be	AUX
eurjchem-843	220	10	conveniently	conveniently	ADV
eurjchem-843	220	11	used	use	VERB
eurjchem-843	220	12	by	by	ADP
eurjchem-843	220	13	quality	quality	NOUN
eurjchem-843	220	14	control	control	NOUN
eurjchem-843	220	15	laboratories	laboratory	NOUN
eurjchem-843	220	16	.	.	PUNCT
eurjchem-843	221	1	references	reference	NOUN
eurjchem-843	221	2	[	[	X
eurjchem-843	221	3	1	1	NUM
eurjchem-843	221	4	]	]	PUNCT
eurjchem-843	221	5	.	.	PUNCT
eurjchem-843	222	1	sekaran	sekaran	PROPN
eurjchem-843	222	2	,	,	PUNCT
eurjchem-843	222	3	b.	b.	PROPN
eurjchem-843	222	4	;	;	PUNCT
eurjchem-843	222	5	rani	rani	PROPN
eurjchem-843	222	6	,	,	PUNCT
eurjchem-843	222	7	p.	p.	NOUN
eurjchem-843	222	8	int	int	NOUN
eurjchem-843	222	9	.	.	PUNCT
eurjchem-843	223	1	j.	j.	PROPN
eurjchem-843	223	2	pharm	pharm	PROPN
eurjchem-843	223	3	.	.	PUNCT
eurjchem-843	224	1	pharm	pharm	PROPN
eurjchem-843	224	2	.	.	PUNCT
eurjchem-843	225	1	sci	sci	PROPN
eurjchem-843	225	2	.	.	PROPN
eurjchem-843	225	3	2010	2010	NUM
eurjchem-843	225	4	,	,	PUNCT
eurjchem-843	225	5	2	2	NUM
eurjchem-843	225	6	,	,	PUNCT
eurjchem-843	225	7	138‐142	138‐142	NUM
eurjchem-843	225	8	.	.	PUNCT
eurjchem-843	226	1	[	[	X
eurjchem-843	226	2	2	2	NUM
eurjchem-843	226	3	]	]	PUNCT
eurjchem-843	226	4	.	.	PUNCT
eurjchem-843	227	1	nirogi	nirogi	PROPN
eurjchem-843	227	2	,	,	PUNCT
eurjchem-843	227	3	r.	r.	PROPN
eurjchem-843	227	4	;	;	PUNCT
eurjchem-843	227	5	kandikere	kandikere	PROPN
eurjchem-843	227	6	,	,	PUNCT
eurjchem-843	227	7	v.	v.	PROPN
eurjchem-843	227	8	;	;	PUNCT
eurjchem-843	227	9	mudigonda	mudigonda	NOUN
eurjchem-843	227	10	,	,	PUNCT
eurjchem-843	227	11	k.	k.	PROPN
eurjchem-843	227	12	;	;	PUNCT
eurjchem-843	227	13	komarneni	komarneni	PROPN
eurjchem-843	227	14	,	,	PUNCT
eurjchem-843	227	15	p.	p.	NOUN
eurjchem-843	227	16	;	;	PUNCT
eurjchem-843	227	17	aleti	aleti	PROPN
eurjchem-843	227	18	,	,	PUNCT
eurjchem-843	227	19	r.	r.	PROPN
eurjchem-843	227	20	;	;	PUNCT
eurjchem-843	227	21	boggavarapu	boggavarapu	PROPN
eurjchem-843	227	22	,	,	PUNCT
eurjchem-843	227	23	r.	r.	PROPN
eurjchem-843	227	24	biomed	biome	VERB
eurjchem-843	227	25	.	.	PUNCT
eurjchem-843	228	1	chromatogr	chromatogr	PROPN
eurjchem-843	228	2	.	.	PUNCT
eurjchem-843	229	1	2008	2008	NUM
eurjchem-843	229	2	,	,	PUNCT
eurjchem-843	229	3	22	22	NUM
eurjchem-843	229	4	,	,	PUNCT
eurjchem-843	229	5	214‐222	214‐222	NUM
eurjchem-843	229	6	.	.	PUNCT
eurjchem-843	230	1	[	[	X
eurjchem-843	230	2	3	3	NUM
eurjchem-843	230	3	]	]	PUNCT
eurjchem-843	230	4	.	.	PUNCT
eurjchem-843	231	1	zeng	zeng	PROPN
eurjchem-843	231	2	,	,	PUNCT
eurjchem-843	231	3	w.	w.	PROPN
eurjchem-843	231	4	;	;	PUNCT
eurjchem-843	231	5	musson	musson	PROPN
eurjchem-843	231	6	,	,	PUNCT
eurjchem-843	231	7	d.	d.	PROPN
eurjchem-843	231	8	;	;	PUNCT
eurjchem-843	231	9	fisher	fisher	PROPN
eurjchem-843	231	10	,	,	PUNCT
eurjchem-843	231	11	a.	a.	NOUN
eurjchem-843	231	12	;	;	PUNCT
eurjchem-843	231	13	chen	chen	PROPN
eurjchem-843	231	14	,	,	PUNCT
eurjchem-843	231	15	l.	l.	PROPN
eurjchem-843	231	16	;	;	PUNCT
eurjchem-843	231	17	schwartz	schwartz	PROPN
eurjchem-843	231	18	,	,	PUNCT
eurjchem-843	231	19	m.	m.	NOUN
eurjchem-843	231	20	;	;	PUNCT
eurjchem-843	231	21	woolf	woolf	PROPN
eurjchem-843	231	22	,	,	PUNCT
eurjchem-843	231	23	e.	e.	PROPN
eurjchem-843	231	24	;	;	PUNCT
eurjchem-843	231	25	wang	wang	PROPN
eurjchem-843	231	26	,	,	PUNCT
eurjchem-843	231	27	a.	a.	PROPN
eurjchem-843	231	28	j.	j.	PROPN
eurjchem-843	231	29	pharm	pharm	PROPN
eurjchem-843	231	30	.	.	PUNCT
eurjchem-843	231	31	biomed	biome	VERB
eurjchem-843	231	32	.	.	PUNCT
eurjchem-843	232	1	anal	anal	PROPN
eurjchem-843	232	2	.	.	PUNCT
eurjchem-843	233	1	2008	2008	NUM
eurjchem-843	233	2	,	,	PUNCT
eurjchem-843	233	3	46	46	NUM
eurjchem-843	233	4	,	,	PUNCT
eurjchem-843	233	5	534‐542	534‐542	NUM
eurjchem-843	233	6	.	.	PUNCT
eurjchem-843	234	1	[	[	X
eurjchem-843	234	2	4	4	NUM
eurjchem-843	234	3	]	]	PUNCT
eurjchem-843	234	4	.	.	PUNCT
eurjchem-843	235	1	sengupta	sengupta	NOUN
eurjchem-843	235	2	,	,	PUNCT
eurjchem-843	235	3	p.	p.	NOUN
eurjchem-843	235	4	;	;	PUNCT
eurjchem-843	235	5	bhaumik	bhaumik	ADJ
eurjchem-843	235	6	,	,	PUNCT
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eurjchem-843	235	8	;	;	PUNCT
eurjchem-843	235	9	ghosh	ghosh	PROPN
eurjchem-843	235	10	,	,	PUNCT
eurjchem-843	235	11	a.	a.	PROPN
eurjchem-843	235	12	;	;	PUNCT
eurjchem-843	235	13	chatterjee	chatterjee	PROPN
eurjchem-843	235	14	,	,	PUNCT
eurjchem-843	235	15	b.	b.	PROPN
eurjchem-843	235	16	;	;	PUNCT
eurjchem-843	235	17	bose	bose	PROPN
eurjchem-843	235	18	,	,	PUNCT
eurjchem-843	235	19	a.	a.	NOUN
eurjchem-843	235	20	;	;	PUNCT
eurjchem-843	235	21	pal	pal	NOUN
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eurjchem-843	235	23	t.	t.	PROPN
eurjchem-843	235	24	k.	k.	PROPN
eurjchem-843	235	25	chromatographia	chromatographia	PROPN
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eurjchem-843	235	27	,	,	PUNCT
eurjchem-843	235	28	69	69	NUM
eurjchem-843	235	29	,	,	PUNCT
eurjchem-843	235	30	1243‐1250	1243‐1250	NUM
eurjchem-843	235	31	.	.	PUNCT
eurjchem-843	236	1	[	[	X
eurjchem-843	236	2	5	5	NUM
eurjchem-843	236	3	]	]	PUNCT
eurjchem-843	236	4	.	.	PUNCT
eurjchem-843	236	5	salsali	salsali	PROPN
eurjchem-843	236	6	,	,	PUNCT
eurjchem-843	236	7	a.	a.	NOUN
eurjchem-843	236	8	;	;	PUNCT
eurjchem-843	236	9	pratley	pratley	PROPN
eurjchem-843	236	10	,	,	PUNCT
eurjchem-843	236	11	r.	r.	PROPN
eurjchem-843	236	12	nat	nat	PROPN
eurjchem-843	236	13	.	.	PUNCT
eurjchem-843	237	1	rev	rev	PROPN
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eurjchem-843	238	2	,	,	PUNCT
eurjchem-843	238	3	3	3	NUM
eurjchem-843	238	4	,	,	PUNCT
eurjchem-843	238	5	450‐451	450‐451	NUM
eurjchem-843	238	6	.	.	PUNCT
eurjchem-843	239	1	[	[	X
eurjchem-843	239	2	6	6	NUM
eurjchem-843	239	3	]	]	PUNCT
eurjchem-843	239	4	.	.	PUNCT
eurjchem-843	240	1	el‐bagary	el‐bagary	PROPN
eurjchem-843	240	2	,	,	PUNCT
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eurjchem-843	240	5	elkady	elkady	PROPN
eurjchem-843	240	6	,	,	PUNCT
eurjchem-843	240	7	e.	e.	PROPN
eurjchem-843	240	8	;	;	PUNCT
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eurjchem-843	240	10	,	,	PUNCT
eurjchem-843	240	11	b.	b.	PROPN
eurjchem-843	240	12	int	int	PROPN
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eurjchem-843	242	2	.	.	PROPN
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eurjchem-843	242	4	,	,	PUNCT
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eurjchem-843	242	6	,	,	PUNCT
eurjchem-843	242	7	55‐61	55‐61	NUM
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eurjchem-843	243	1	[	[	X
eurjchem-843	243	2	7	7	NUM
eurjchem-843	243	3	]	]	PUNCT
eurjchem-843	243	4	.	.	PUNCT
eurjchem-843	244	1	el‐bagary	el‐bagary	PROPN
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eurjchem-843	244	6	,	,	PUNCT
eurjchem-843	244	7	e.	e.	PROPN
eurjchem-843	244	8	;	;	PUNCT
eurjchem-843	244	9	ayoub	ayoub	PROPN
eurjchem-843	244	10	,	,	PUNCT
eurjchem-843	244	11	b.	b.	PROPN
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eurjchem-843	244	14	,	,	PUNCT
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eurjchem-843	244	16	,	,	PUNCT
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eurjchem-843	245	1	[	[	X
eurjchem-843	245	2	8	8	NUM
eurjchem-843	245	3	]	]	PUNCT
eurjchem-843	245	4	.	.	PUNCT
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eurjchem-843	246	4	;	;	PUNCT
eurjchem-843	246	5	elkady	elkady	PROPN
eurjchem-843	246	6	,	,	PUNCT
eurjchem-843	246	7	e.	e.	PROPN
eurjchem-843	246	8	;	;	PUNCT
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eurjchem-843	246	10	,	,	PUNCT
eurjchem-843	246	11	b.	b.	PROPN
eurjchem-843	246	12	int	int	PROPN
eurjchem-843	246	13	.	.	PUNCT
eurjchem-843	247	1	j.	j.	PROPN
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eurjchem-843	247	3	.	.	PUNCT
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eurjchem-843	248	2	.	.	PROPN
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eurjchem-843	248	4	,	,	PUNCT
eurjchem-843	248	5	7	7	NUM
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eurjchem-843	248	8	.	.	PUNCT
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eurjchem-843	249	2	9	9	NUM
eurjchem-843	249	3	]	]	PUNCT
eurjchem-843	249	4	.	.	PUNCT
eurjchem-843	249	5	ali	ali	PROPN
eurjchem-843	249	6	,	,	PUNCT
eurjchem-843	249	7	a.	a.	PROPN
eurjchem-843	249	8	;	;	PUNCT
eurjchem-843	249	9	duraidi	duraidi	PROPN
eurjchem-843	249	10	,	,	PUNCT
eurjchem-843	249	11	i.	i.	NOUN
eurjchem-843	249	12	;	;	PUNCT
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eurjchem-843	249	14	,	,	PUNCT
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eurjchem-843	249	16	;	;	PUNCT
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eurjchem-843	249	18	,	,	PUNCT
eurjchem-843	249	19	e.	e.	PROPN
eurjchem-843	249	20	j.	j.	PROPN
eurjchem-843	249	21	aoac	aoac	PROPN
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eurjchem-843	250	2	,	,	PUNCT
eurjchem-843	250	3	92	92	NUM
eurjchem-843	250	4	,	,	PUNCT
eurjchem-843	250	5	119‐	119‐	NUM
eurjchem-843	250	6	124	124	NUM
eurjchem-843	250	7	.	.	PUNCT
eurjchem-843	251	1	[	[	X
eurjchem-843	251	2	10	10	NUM
eurjchem-843	251	3	]	]	PUNCT
eurjchem-843	251	4	.	.	PUNCT
eurjchem-843	252	1	porta	porta	PROPN
eurjchem-843	252	2	,	,	PUNCT
eurjchem-843	252	3	v.	v.	PROPN
eurjchem-843	252	4	;	;	PUNCT
eurjchem-843	252	5	schramm	schramm	PROPN
eurjchem-843	252	6	,	,	PUNCT
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eurjchem-843	252	8	;	;	PUNCT
eurjchem-843	252	9	kano	kano	PROPN
eurjchem-843	252	10	,	,	PUNCT
eurjchem-843	252	11	e.	e.	PROPN
eurjchem-843	252	12	;	;	PUNCT
eurjchem-843	252	13	koono	koono	PROPN
eurjchem-843	252	14	,	,	PUNCT
eurjchem-843	252	15	e.	e.	PROPN
eurjchem-843	252	16	;	;	PUNCT
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eurjchem-843	252	20	;	;	PUNCT
eurjchem-843	252	21	fukuda	fukuda	PROPN
eurjchem-843	252	22	,	,	PUNCT
eurjchem-843	252	23	k.	k.	PROPN
eurjchem-843	252	24	;	;	PUNCT
eurjchem-843	252	25	serra	serra	PROPN
eurjchem-843	252	26	,	,	PUNCT
eurjchem-843	252	27	c.	c.	PROPN
eurjchem-843	252	28	j.	j.	PROPN
eurjchem-843	252	29	pharm	pharm	PROPN
eurjchem-843	252	30	.	.	PUNCT
eurjchem-843	253	1	biomed	biome	VERB
eurjchem-843	253	2	.	.	PUNCT
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eurjchem-843	254	2	.	.	PUNCT
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eurjchem-843	254	4	,	,	PUNCT
eurjchem-843	254	5	46	46	NUM
eurjchem-843	254	6	,	,	PUNCT
eurjchem-843	254	7	143‐147	143‐147	NUM
eurjchem-843	254	8	.	.	PUNCT
eurjchem-843	255	1	[	[	X
eurjchem-843	255	2	11	11	NUM
eurjchem-843	255	3	]	]	PUNCT
eurjchem-843	255	4	.	.	PUNCT
eurjchem-843	256	1	zhong	zhong	PROPN
eurjchem-843	256	2	,	,	PUNCT
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eurjchem-843	256	4	;	;	PUNCT
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eurjchem-843	256	6	,	,	PUNCT
eurjchem-843	256	7	x.	x.	NOUN
eurjchem-843	256	8	;	;	PUNCT
eurjchem-843	256	9	sun	sun	PROPN
eurjchem-843	256	10	,	,	PUNCT
eurjchem-843	256	11	h.	h.	PROPN
eurjchem-843	256	12	yaowu‐fenxi‐zazhi	yaowu‐fenxi‐zazhi	PROPN
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eurjchem-843	256	14	,	,	PUNCT
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eurjchem-843	256	16	,	,	PUNCT
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eurjchem-843	256	18	.	.	PUNCT
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eurjchem-843	257	2	12	12	NUM
eurjchem-843	257	3	]	]	PUNCT
eurjchem-843	257	4	.	.	PUNCT
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eurjchem-843	258	4	.	.	PUNCT
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eurjchem-843	260	10	;	;	PUNCT
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