id	sid	tid	token	lemma	pos
eurjchem-844	1	1	untitled	untitle	VERB
eurjchem-844	1	2	european	european	PROPN
eurjchem-844	1	3	journal	journal	PROPN
eurjchem-844	1	4	of	of	ADP
eurjchem-844	1	5	chemistry	chemistry	NOUN
eurjchem-844	1	6	4	4	NUM
eurjchem-844	1	7	(	(	PUNCT
eurjchem-844	1	8	4	4	NUM
eurjchem-844	1	9	)	)	PUNCT
eurjchem-844	1	10	(	(	PUNCT
eurjchem-844	1	11	2013	2013	NUM
eurjchem-844	1	12	)	)	PUNCT
eurjchem-844	1	13	444‐449	444‐449	PROPN
eurjchem-844	1	14	european	european	PROPN
eurjchem-844	1	15	journal	journal	PROPN
eurjchem-844	1	16	of	of	ADP
eurjchem-844	1	17	chemistry	chemistry	NOUN
eurjchem-844	1	18	issn	issn	PROPN
eurjchem-844	1	19	2153‐2249	2153‐2249	PROPN
eurjchem-844	1	20	(	(	PUNCT
eurjchem-844	1	21	print	print	NOUN
eurjchem-844	1	22	)	)	PUNCT
eurjchem-844	1	23	/	/	SYM
eurjchem-844	1	24	issn	issn	PROPN
eurjchem-844	1	25	2153‐2257	2153‐2257	NUM
eurjchem-844	1	26	(	(	PUNCT
eurjchem-844	1	27	online	online	ADJ
eurjchem-844	1	28	)	)	PUNCT
eurjchem-844	1	29			NOUN
eurjchem-844	2	1	2013	2013	NUM
eurjchem-844	2	2	eurjchem	eurjchem	PROPN
eurjchem-844	2	3	doi:10.5155	doi:10.5155	NOUN
eurjchem-844	2	4	/	/	SYM
eurjchem-844	2	5	eurjchem.4.4.444‐449.844	eurjchem.4.4.444‐449.844	NOUN
eurjchem-844	2	6	european	european	ADJ
eurjchem-844	2	7	journal	journal	PROPN
eurjchem-844	2	8	of	of	ADP
eurjchem-844	2	9	chemistry	chemistry	PROPN
eurjchem-844	2	10	journal	journal	PROPN
eurjchem-844	2	11	homepage	homepage	NOUN
eurjchem-844	2	12	:	:	PUNCT
eurjchem-844	2	13	www.eurjchem.com	www.eurjchem.com	X
eurjchem-844	2	14	development	development	NOUN
eurjchem-844	2	15	and	and	CCONJ
eurjchem-844	2	16	validation	validation	NOUN
eurjchem-844	2	17	of	of	ADP
eurjchem-844	2	18	a	a	DET
eurjchem-844	2	19	reversed	reverse	VERB
eurjchem-844	2	20	phase	phase	NOUN
eurjchem-844	2	21	liquid	liquid	ADJ
eurjchem-844	2	22	chromatographic	chromatographic	ADJ
eurjchem-844	2	23	method	method	NOUN
eurjchem-844	2	24	for	for	ADP
eurjchem-844	2	25	the	the	DET
eurjchem-844	2	26	determination	determination	NOUN
eurjchem-844	2	27	of	of	ADP
eurjchem-844	2	28	three	three	NUM
eurjchem-844	2	29	gliptins	gliptin	NOUN
eurjchem-844	2	30	and	and	CCONJ
eurjchem-844	2	31	metformin	metformin	NOUN
eurjchem-844	2	32	in	in	ADP
eurjchem-844	2	33	the	the	DET
eurjchem-844	2	34	presence	presence	NOUN
eurjchem-844	2	35	of	of	ADP
eurjchem-844	2	36	metformin	metformin	NOUN
eurjchem-844	2	37	impurity	impurity	NOUN
eurjchem-844	2	38	(	(	PUNCT
eurjchem-844	2	39	1‐cyanoguanidine	1‐cyanoguanidine	NUM
eurjchem-844	2	40	)	)	PUNCT
eurjchem-844	2	41	ramzia	ramzia	PROPN
eurjchem-844	2	42	ismail	ismail	PROPN
eurjchem-844	2	43	el‐bagary	el‐bagary	PROPN
eurjchem-844	2	44	a	a	PROPN
eurjchem-844	2	45	,	,	PUNCT
eurjchem-844	2	46	ehab	ehab	PROPN
eurjchem-844	2	47	farouk	farouk	PROPN
eurjchem-844	2	48	elkady	elkady	PROPN
eurjchem-844	2	49	a	a	PROPN
eurjchem-844	2	50	,	,	PUNCT
eurjchem-844	2	51	and	and	CCONJ
eurjchem-844	2	52	bassam	bassam	PROPN
eurjchem-844	2	53	mahfouz	mahfouz	PROPN
eurjchem-844	2	54	ayoub	ayoub	PROPN
eurjchem-844	2	55	b	b	PROPN
eurjchem-844	2	56	,	,	PUNCT
eurjchem-844	2	57	*	*	PUNCT
eurjchem-844	2	58	a	a	DET
eurjchem-844	2	59	pharmaceutical	pharmaceutical	ADJ
eurjchem-844	2	60	chemistry	chemistry	NOUN
eurjchem-844	2	61	department	department	NOUN
eurjchem-844	2	62	,	,	PUNCT
eurjchem-844	2	63	faculty	faculty	NOUN
eurjchem-844	2	64	of	of	ADP
eurjchem-844	2	65	pharmacy	pharmacy	NOUN
eurjchem-844	2	66	,	,	PUNCT
eurjchem-844	2	67	cairo	cairo	PROPN
eurjchem-844	2	68	university	university	PROPN
eurjchem-844	2	69	,	,	PUNCT
eurjchem-844	2	70	cairo	cairo	PROPN
eurjchem-844	2	71	11562	11562	NUM
eurjchem-844	2	72	,	,	PUNCT
eurjchem-844	2	73	egypt	egypt	PROPN
eurjchem-844	2	74	b	b	PROPN
eurjchem-844	2	75	pharmaceutical	pharmaceutical	ADJ
eurjchem-844	2	76	chemistry	chemistry	NOUN
eurjchem-844	2	77	department	department	NOUN
eurjchem-844	2	78	,	,	PUNCT
eurjchem-844	2	79	faculty	faculty	NOUN
eurjchem-844	2	80	of	of	ADP
eurjchem-844	2	81	pharmacy	pharmacy	NOUN
eurjchem-844	2	82	,	,	PUNCT
eurjchem-844	2	83	british	british	ADJ
eurjchem-844	2	84	university	university	PROPN
eurjchem-844	2	85	in	in	ADP
eurjchem-844	2	86	egypt	egypt	PROPN
eurjchem-844	2	87	,	,	PUNCT
eurjchem-844	2	88	el‐sherouk	el‐sherouk	PROPN
eurjchem-844	2	89	,	,	PUNCT
eurjchem-844	2	90	cairo	cairo	PROPN
eurjchem-844	2	91	11837	11837	NUM
eurjchem-844	2	92	,	,	PUNCT
eurjchem-844	2	93	egypt	egypt	PROPN
eurjchem-844	2	94	*	*	PUNCT
eurjchem-844	2	95	corresponding	correspond	VERB
eurjchem-844	2	96	author	author	NOUN
eurjchem-844	2	97	at	at	ADP
eurjchem-844	2	98	:	:	PUNCT
eurjchem-844	2	99	pharmaceutical	pharmaceutical	ADJ
eurjchem-844	2	100	chemistry	chemistry	NOUN
eurjchem-844	2	101	department	department	NOUN
eurjchem-844	2	102	,	,	PUNCT
eurjchem-844	2	103	faculty	faculty	NOUN
eurjchem-844	2	104	of	of	ADP
eurjchem-844	2	105	pharmacy	pharmacy	NOUN
eurjchem-844	2	106	,	,	PUNCT
eurjchem-844	2	107	british	british	ADJ
eurjchem-844	2	108	university	university	PROPN
eurjchem-844	2	109	in	in	ADP
eurjchem-844	2	110	egypt	egypt	PROPN
eurjchem-844	2	111	,	,	PUNCT
eurjchem-844	2	112	el‐sherouk	el‐sherouk	PROPN
eurjchem-844	2	113	,	,	PUNCT
eurjchem-844	2	114	cairo	cairo	PROPN
eurjchem-844	2	115	11837	11837	NUM
eurjchem-844	2	116	,	,	PUNCT
eurjchem-844	2	117	egypt	egypt	PROPN
eurjchem-844	2	118	.	.	PUNCT
eurjchem-844	3	1	tel	tel	PROPN
eurjchem-844	3	2	.	.	PUNCT
eurjchem-844	3	3	:	:	PUNCT
eurjchem-844	4	1	+2.012.25104337	+2.012.25104337	ADJ
eurjchem-844	4	2	;	;	PUNCT
eurjchem-844	4	3	fax	fax	NOUN
eurjchem-844	4	4	:	:	PUNCT
eurjchem-844	4	5	+2.022.4148452	+2.022.4148452	PROPN
eurjchem-844	4	6	.	.	PUNCT
eurjchem-844	4	7	e‐mail	e‐mail	PUNCT
eurjchem-844	5	1	address	address	NOUN
eurjchem-844	5	2	:	:	PUNCT
eurjchem-844	5	3	bassam.ayoub@bue.edu.eg	bassam.ayoub@bue.edu.eg	PROPN
eurjchem-844	5	4	(	(	PUNCT
eurjchem-844	5	5	b.m	b.m	PROPN
eurjchem-844	5	6	.	.	PROPN
eurjchem-844	5	7	ayoub	ayoub	PROPN
eurjchem-844	5	8	)	)	PUNCT
eurjchem-844	5	9	.	.	PUNCT
eurjchem-844	6	1	article	article	NOUN
eurjchem-844	6	2	information	information	PROPN
eurjchem-844	6	3	abstract	abstract	ADV
eurjchem-844	6	4	received	receive	VERB
eurjchem-844	6	5	:	:	PUNCT
eurjchem-844	6	6	04	04	NUM
eurjchem-844	6	7	june	june	PROPN
eurjchem-844	6	8	2013	2013	NUM
eurjchem-844	6	9	received	receive	VERB
eurjchem-844	6	10	in	in	ADP
eurjchem-844	6	11	revised	revise	VERB
eurjchem-844	6	12	form	form	NOUN
eurjchem-844	6	13	:	:	PUNCT
eurjchem-844	6	14	26	26	NUM
eurjchem-844	6	15	june	june	PROPN
eurjchem-844	6	16	2013	2013	NUM
eurjchem-844	6	17	accepted	accept	VERB
eurjchem-844	6	18	:	:	PUNCT
eurjchem-844	6	19	18	18	NUM
eurjchem-844	6	20	august	august	PROPN
eurjchem-844	6	21	2013	2013	NUM
eurjchem-844	6	22	online	online	NOUN
eurjchem-844	6	23	:	:	PUNCT
eurjchem-844	6	24	31	31	NUM
eurjchem-844	6	25	december	december	PROPN
eurjchem-844	6	26	2013	2013	NUM
eurjchem-844	6	27	keywords	keyword	VERB
eurjchem-844	6	28	a	a	DET
eurjchem-844	6	29	simple	simple	ADJ
eurjchem-844	6	30	and	and	CCONJ
eurjchem-844	6	31	precise	precise	ADJ
eurjchem-844	6	32	liquid	liquid	ADJ
eurjchem-844	6	33	chromatographic	chromatographic	ADJ
eurjchem-844	6	34	method	method	NOUN
eurjchem-844	6	35	has	have	AUX
eurjchem-844	6	36	been	be	AUX
eurjchem-844	6	37	developed	develop	VERB
eurjchem-844	6	38	and	and	CCONJ
eurjchem-844	6	39	validated	validate	VERB
eurjchem-844	6	40	for	for	ADP
eurjchem-844	6	41	the	the	DET
eurjchem-844	6	42	determination	determination	NOUN
eurjchem-844	6	43	of	of	ADP
eurjchem-844	6	44	either	either	DET
eurjchem-844	6	45	sitagliptin	sitagliptin	NOUN
eurjchem-844	6	46	(	(	PUNCT
eurjchem-844	6	47	stg	stg	NOUN
eurjchem-844	6	48	)	)	PUNCT
eurjchem-844	6	49	,	,	PUNCT
eurjchem-844	6	50	vildagliptin	vildagliptin	NOUN
eurjchem-844	6	51	(	(	PUNCT
eurjchem-844	6	52	vlg	vlg	PROPN
eurjchem-844	6	53	)	)	PUNCT
eurjchem-844	6	54	or	or	CCONJ
eurjchem-844	6	55	saxagliptin	saxagliptin	PROPN
eurjchem-844	6	56	hcl	hcl	PROPN
eurjchem-844	6	57	(	(	PUNCT
eurjchem-844	6	58	sxg	sxg	NOUN
eurjchem-844	6	59	)	)	PUNCT
eurjchem-844	6	60	and	and	CCONJ
eurjchem-844	6	61	metformin	metformin	PROPN
eurjchem-844	6	62	hcl	hcl	PROPN
eurjchem-844	6	63	(	(	PUNCT
eurjchem-844	6	64	met	meet	VERB
eurjchem-844	6	65	)	)	PUNCT
eurjchem-844	6	66	in	in	ADP
eurjchem-844	6	67	the	the	DET
eurjchem-844	6	68	presence	presence	NOUN
eurjchem-844	6	69	of	of	ADP
eurjchem-844	6	70	metformin	metformin	NOUN
eurjchem-844	6	71	degradation	degradation	NOUN
eurjchem-844	6	72	product	product	NOUN
eurjchem-844	6	73	,	,	PUNCT
eurjchem-844	6	74	1‐cyanoguanidine	1‐cyanoguanidine	NUM
eurjchem-844	6	75	(	(	PUNCT
eurjchem-844	6	76	cgn	cgn	PROPN
eurjchem-844	6	77	)	)	PUNCT
eurjchem-844	6	78	.	.	PUNCT
eurjchem-844	7	1	chromatographic	chromatographic	ADJ
eurjchem-844	7	2	separation	separation	NOUN
eurjchem-844	7	3	was	be	AUX
eurjchem-844	7	4	achieved	achieve	VERB
eurjchem-844	7	5	on	on	ADP
eurjchem-844	7	6	a	a	DET
eurjchem-844	7	7	symmetry	symmetry	NOUN
eurjchem-844	7	8	®	®	NOUN
eurjchem-844	7	9	cyanide	cyanide	NOUN
eurjchem-844	7	10	column	column	NOUN
eurjchem-844	7	11	(	(	PUNCT
eurjchem-844	7	12	150	150	NUM
eurjchem-844	7	13	mm	mm	NOUN
eurjchem-844	7	14	×	×	NOUN
eurjchem-844	7	15	4.6	4.6	NUM
eurjchem-844	7	16	mm	mm	NOUN
eurjchem-844	7	17	,	,	PUNCT
eurjchem-844	7	18	5	5	NUM
eurjchem-844	7	19	μm	μm	NUM
eurjchem-844	7	20	)	)	PUNCT
eurjchem-844	7	21	.	.	PUNCT
eurjchem-844	8	1	isocratic	isocratic	ADJ
eurjchem-844	8	2	elution	elution	NOUN
eurjchem-844	8	3	using	use	VERB
eurjchem-844	8	4	a	a	DET
eurjchem-844	8	5	mobile	mobile	ADJ
eurjchem-844	8	6	phase	phase	NOUN
eurjchem-844	8	7	of	of	ADP
eurjchem-844	8	8	potassium	potassium	NOUN
eurjchem-844	8	9	dihydrogen	dihydrogen	NOUN
eurjchem-844	8	10	phosphate	phosphate	NOUN
eurjchem-844	8	11	buffer	buffer	NOUN
eurjchem-844	8	12	(	(	PUNCT
eurjchem-844	8	13	ph	ph	NOUN
eurjchem-844	8	14	=	=	NOUN
eurjchem-844	8	15	4.6	4.6	NUM
eurjchem-844	8	16	)	)	PUNCT
eurjchem-844	8	17	‐	‐	ADJ
eurjchem-844	8	18	acetonitrile	acetonitrile	NOUN
eurjchem-844	8	19	(	(	PUNCT
eurjchem-844	8	20	30:70	30:70	NUM
eurjchem-844	8	21	,	,	PUNCT
eurjchem-844	8	22	v	v	NOUN
eurjchem-844	8	23	:	:	SYM
eurjchem-844	8	24	v	v	NOUN
eurjchem-844	8	25	)	)	PUNCT
eurjchem-844	8	26	at	at	ADP
eurjchem-844	8	27	a	a	DET
eurjchem-844	8	28	flow	flow	NOUN
eurjchem-844	8	29	rate	rate	NOUN
eurjchem-844	8	30	of	of	ADP
eurjchem-844	8	31	1	1	NUM
eurjchem-844	8	32	ml	ml	NOUN
eurjchem-844	8	33	/	/	SYM
eurjchem-844	8	34	min	min	NOUN
eurjchem-844	8	35	with	with	ADP
eurjchem-844	8	36	uv	uv	NOUN
eurjchem-844	8	37	detection	detection	NOUN
eurjchem-844	8	38	at	at	ADP
eurjchem-844	8	39	210	210	NUM
eurjchem-844	8	40	nm	nm	NOUN
eurjchem-844	8	41	was	be	AUX
eurjchem-844	8	42	performed	perform	VERB
eurjchem-844	8	43	.	.	PUNCT
eurjchem-844	9	1	the	the	DET
eurjchem-844	9	2	lc	lc	PROPN
eurjchem-844	9	3	method	method	NOUN
eurjchem-844	9	4	was	be	AUX
eurjchem-844	9	5	used	use	VERB
eurjchem-844	9	6	for	for	ADP
eurjchem-844	9	7	the	the	DET
eurjchem-844	9	8	simultaneous	simultaneous	ADJ
eurjchem-844	9	9	determination	determination	NOUN
eurjchem-844	9	10	of	of	ADP
eurjchem-844	9	11	stg	stg	PROPN
eurjchem-844	9	12	,	,	PUNCT
eurjchem-844	9	13	vlg	vlg	PROPN
eurjchem-844	9	14	,	,	PUNCT
eurjchem-844	9	15	sxg	sxg	NOUN
eurjchem-844	9	16	and	and	CCONJ
eurjchem-844	9	17	met	meet	VERB
eurjchem-844	9	18	in	in	ADP
eurjchem-844	9	19	the	the	DET
eurjchem-844	9	20	ranges	range	NOUN
eurjchem-844	9	21	of	of	ADP
eurjchem-844	9	22	5‐200	5‐200	PROPN
eurjchem-844	9	23	,	,	PUNCT
eurjchem-844	9	24	5‐200	5‐200	PROPN
eurjchem-844	9	25	,	,	PUNCT
eurjchem-844	9	26	0.5‐80.0	0.5‐80.0	NOUN
eurjchem-844	9	27	and	and	CCONJ
eurjchem-844	9	28	20‐800	20‐800	NUM
eurjchem-844	9	29	μg	μg	NOUN
eurjchem-844	9	30	/	/	SYM
eurjchem-844	9	31	ml	ml	NOUN
eurjchem-844	9	32	,	,	PUNCT
eurjchem-844	9	33	respectively	respectively	ADV
eurjchem-844	9	34	.	.	PUNCT
eurjchem-844	10	1	the	the	DET
eurjchem-844	10	2	results	result	NOUN
eurjchem-844	10	3	were	be	AUX
eurjchem-844	10	4	statistically	statistically	ADV
eurjchem-844	10	5	compared	compare	VERB
eurjchem-844	10	6	with	with	ADP
eurjchem-844	10	7	the	the	DET
eurjchem-844	10	8	reference	reference	NOUN
eurjchem-844	10	9	method	method	NOUN
eurjchem-844	10	10	for	for	ADP
eurjchem-844	10	11	each	each	DET
eurjchem-844	10	12	drug	drug	NOUN
eurjchem-844	10	13	using	use	VERB
eurjchem-844	10	14	one‐way	one‐way	NOUN
eurjchem-844	10	15	analysis	analysis	NOUN
eurjchem-844	10	16	of	of	ADP
eurjchem-844	10	17	variance	variance	NOUN
eurjchem-844	10	18	(	(	PUNCT
eurjchem-844	10	19	anova	anova	PROPN
eurjchem-844	10	20	)	)	PUNCT
eurjchem-844	10	21	.	.	PUNCT
eurjchem-844	11	1	the	the	DET
eurjchem-844	11	2	method	method	NOUN
eurjchem-844	11	3	developed	develop	VERB
eurjchem-844	11	4	was	be	AUX
eurjchem-844	11	5	satisfactorily	satisfactorily	ADV
eurjchem-844	11	6	applied	apply	VERB
eurjchem-844	11	7	to	to	ADP
eurjchem-844	11	8	the	the	DET
eurjchem-844	11	9	analysis	analysis	NOUN
eurjchem-844	11	10	of	of	ADP
eurjchem-844	11	11	the	the	DET
eurjchem-844	11	12	pharmaceutical	pharmaceutical	NOUN
eurjchem-844	11	13	formulations	formulation	NOUN
eurjchem-844	11	14	and	and	CCONJ
eurjchem-844	11	15	proved	prove	VERB
eurjchem-844	11	16	to	to	PART
eurjchem-844	11	17	be	be	AUX
eurjchem-844	11	18	specific	specific	ADJ
eurjchem-844	11	19	and	and	CCONJ
eurjchem-844	11	20	accurate	accurate	ADJ
eurjchem-844	11	21	for	for	ADP
eurjchem-844	11	22	the	the	DET
eurjchem-844	11	23	quality	quality	NOUN
eurjchem-844	11	24	control	control	NOUN
eurjchem-844	11	25	of	of	ADP
eurjchem-844	11	26	the	the	DET
eurjchem-844	11	27	cited	cite	VERB
eurjchem-844	11	28	drugs	drug	NOUN
eurjchem-844	11	29	in	in	ADP
eurjchem-844	11	30	pharmaceutical	pharmaceutical	ADJ
eurjchem-844	11	31	dosage	dosage	NOUN
eurjchem-844	11	32	forms	form	NOUN
eurjchem-844	11	33	.	.	PUNCT
eurjchem-844	12	1	sitagliptin	sitagliptin	PROPN
eurjchem-844	12	2	metformin	metformin	PROPN
eurjchem-844	12	3	saxagliptin	saxagliptin	NOUN
eurjchem-844	12	4	vildagliptin	vildagliptin	NOUN
eurjchem-844	12	5	liquid	liquid	ADJ
eurjchem-844	12	6	chromatography	chromatography	NOUN
eurjchem-844	12	7	stability	stability	NOUN
eurjchem-844	12	8	indicating	indicate	VERB
eurjchem-844	12	9	assay	assay	PROPN
eurjchem-844	12	10	1	1	NUM
eurjchem-844	12	11	.	.	PUNCT
eurjchem-844	12	12	introduction	introduction	NOUN
eurjchem-844	12	13	sitagliptin	sitagliptin	NOUN
eurjchem-844	12	14	(	(	PUNCT
eurjchem-844	12	15	figure	figure	NOUN
eurjchem-844	12	16	1a	1a	NOUN
eurjchem-844	12	17	)	)	PUNCT
eurjchem-844	12	18	,	,	PUNCT
eurjchem-844	12	19	vildagliptin	vildagliptin	PROPN
eurjchem-844	12	20	,	,	PUNCT
eurjchem-844	12	21	(	(	PUNCT
eurjchem-844	12	22	figure	figure	NOUN
eurjchem-844	12	23	1b	1b	NUM
eurjchem-844	12	24	)	)	PUNCT
eurjchem-844	12	25	,	,	PUNCT
eurjchem-844	12	26	and	and	CCONJ
eurjchem-844	12	27	saxagliptin	saxagliptin	NOUN
eurjchem-844	12	28	(	(	PUNCT
eurjchem-844	12	29	figure	figure	NOUN
eurjchem-844	12	30	1c	1c	NOUN
eurjchem-844	12	31	)	)	PUNCT
eurjchem-844	12	32	are	be	AUX
eurjchem-844	12	33	oral	oral	ADJ
eurjchem-844	12	34	hypoglycemic	hypoglycemic	ADJ
eurjchem-844	12	35	drugs	drug	NOUN
eurjchem-844	12	36	of	of	ADP
eurjchem-844	12	37	the	the	DET
eurjchem-844	12	38	dipeptidyl	dipeptidyl	NOUN
eurjchem-844	12	39	peptidase‐4	peptidase‐4	PROPN
eurjchem-844	12	40	(	(	PUNCT
eurjchem-844	12	41	dpp‐4	dpp‐4	NOUN
eurjchem-844	12	42	)	)	PUNCT
eurjchem-844	12	43	inhibitors	inhibitor	NOUN
eurjchem-844	12	44	class	class	NOUN
eurjchem-844	12	45	.	.	PUNCT
eurjchem-844	13	1	dpp‐4	dpp‐4	NOUN
eurjchem-844	13	2	inhibitors	inhibitor	NOUN
eurjchem-844	13	3	represent	represent	VERB
eurjchem-844	13	4	a	a	DET
eurjchem-844	13	5	new	new	ADJ
eurjchem-844	13	6	therapeutic	therapeutic	ADJ
eurjchem-844	13	7	approach	approach	NOUN
eurjchem-844	13	8	to	to	ADP
eurjchem-844	13	9	the	the	DET
eurjchem-844	13	10	treatment	treatment	NOUN
eurjchem-844	13	11	of	of	ADP
eurjchem-844	13	12	type‐2	type‐2	DET
eurjchem-844	13	13	diabetes	diabetes	NOUN
eurjchem-844	13	14	that	that	PRON
eurjchem-844	13	15	functions	function	NOUN
eurjchem-844	13	16	to	to	PART
eurjchem-844	13	17	stimulate	stimulate	VERB
eurjchem-844	13	18	glucose‐dependent	glucose‐dependent	NOUN
eurjchem-844	13	19	insulin	insulin	NOUN
eurjchem-844	13	20	release	release	NOUN
eurjchem-844	13	21	and	and	CCONJ
eurjchem-844	13	22	reduce	reduce	VERB
eurjchem-844	13	23	glucagons	glucagon	NOUN
eurjchem-844	13	24	levels	level	NOUN
eurjchem-844	13	25	.	.	PUNCT
eurjchem-844	14	1	this	this	PRON
eurjchem-844	14	2	is	be	AUX
eurjchem-844	14	3	done	do	VERB
eurjchem-844	14	4	through	through	ADP
eurjchem-844	14	5	inhibition	inhibition	NOUN
eurjchem-844	14	6	of	of	ADP
eurjchem-844	14	7	the	the	DET
eurjchem-844	14	8	inactivation	inactivation	NOUN
eurjchem-844	14	9	of	of	ADP
eurjchem-844	14	10	incretins	incretin	NOUN
eurjchem-844	14	11	,	,	PUNCT
eurjchem-844	14	12	particularly	particularly	ADV
eurjchem-844	14	13	glucagon‐like	glucagon‐like	ADP
eurjchem-844	14	14	peptide‐1	peptide‐1	PROPN
eurjchem-844	14	15	(	(	PUNCT
eurjchem-844	14	16	glp‐1	glp‐1	NOUN
eurjchem-844	14	17	)	)	PUNCT
eurjchem-844	14	18	and	and	CCONJ
eurjchem-844	14	19	gastric	gastric	ADJ
eurjchem-844	14	20	inhibitory	inhibitory	ADJ
eurjchem-844	14	21	polypeptide	polypeptide	ADJ
eurjchem-844	14	22	(	(	PUNCT
eurjchem-844	14	23	gip	gip	NOUN
eurjchem-844	14	24	)	)	PUNCT
eurjchem-844	15	1	[	[	X
eurjchem-844	15	2	1	1	NUM
eurjchem-844	15	3	]	]	PUNCT
eurjchem-844	15	4	.	.	PUNCT
eurjchem-844	16	1	few	few	ADJ
eurjchem-844	16	2	methods	method	NOUN
eurjchem-844	16	3	have	have	AUX
eurjchem-844	16	4	been	be	AUX
eurjchem-844	16	5	described	describe	VERB
eurjchem-844	16	6	for	for	ADP
eurjchem-844	16	7	the	the	DET
eurjchem-844	16	8	determination	determination	NOUN
eurjchem-844	16	9	of	of	ADP
eurjchem-844	16	10	stg	stg	PROPN
eurjchem-844	16	11	in	in	ADP
eurjchem-844	16	12	pharmaceutical	pharmaceutical	ADJ
eurjchem-844	16	13	preparations	preparation	NOUN
eurjchem-844	16	14	or	or	CCONJ
eurjchem-844	16	15	biological	biological	ADJ
eurjchem-844	16	16	fluids	fluid	NOUN
eurjchem-844	16	17	including	include	VERB
eurjchem-844	16	18	spectrophotometry	spectrophotometry	NOUN
eurjchem-844	16	19	[	[	X
eurjchem-844	16	20	2	2	NUM
eurjchem-844	16	21	]	]	PUNCT
eurjchem-844	16	22	and	and	CCONJ
eurjchem-844	16	23	high	high	ADJ
eurjchem-844	16	24	performance	performance	NOUN
eurjchem-844	16	25	liquid	liquid	NOUN
eurjchem-844	16	26	chromatography	chromatography	NOUN
eurjchem-844	16	27	(	(	PUNCT
eurjchem-844	16	28	hplc	hplc	PROPN
eurjchem-844	16	29	)	)	PUNCT
eurjchem-844	17	1	[	[	X
eurjchem-844	17	2	1,3	1,3	NUM
eurjchem-844	17	3	]	]	PUNCT
eurjchem-844	17	4	.	.	PUNCT
eurjchem-844	18	1	a	a	DET
eurjchem-844	18	2	liquid	liquid	ADJ
eurjchem-844	18	3	chromatographic	chromatographic	ADJ
eurjchem-844	18	4	(	(	PUNCT
eurjchem-844	18	5	lc	lc	NOUN
eurjchem-844	18	6	)	)	PUNCT
eurjchem-844	18	7	method	method	NOUN
eurjchem-844	18	8	was	be	AUX
eurjchem-844	18	9	reported	report	VERB
eurjchem-844	18	10	for	for	ADP
eurjchem-844	18	11	the	the	DET
eurjchem-844	18	12	determination	determination	NOUN
eurjchem-844	18	13	of	of	ADP
eurjchem-844	18	14	stg	stg	PROPN
eurjchem-844	18	15	in	in	ADP
eurjchem-844	18	16	ternary	ternary	ADJ
eurjchem-844	18	17	mixture	mixture	NOUN
eurjchem-844	18	18	with	with	ADP
eurjchem-844	18	19	met	meet	VERB
eurjchem-844	18	20	and	and	CCONJ
eurjchem-844	18	21	sitagliptin	sitagliptin	NOUN
eurjchem-844	18	22	degradation	degradation	NOUN
eurjchem-844	18	23	product	product	NOUN
eurjchem-844	18	24	[	[	X
eurjchem-844	18	25	4	4	NUM
eurjchem-844	18	26	]	]	PUNCT
eurjchem-844	18	27	.	.	PUNCT
eurjchem-844	19	1	for	for	ADP
eurjchem-844	19	2	vdg	vdg	PROPN
eurjchem-844	19	3	,	,	PUNCT
eurjchem-844	19	4	literature	literature	NOUN
eurjchem-844	19	5	survey	survey	NOUN
eurjchem-844	19	6	reveals	reveal	VERB
eurjchem-844	19	7	that	that	SCONJ
eurjchem-844	19	8	only	only	ADV
eurjchem-844	19	9	one	one	NUM
eurjchem-844	19	10	spectroscopic	spectroscopic	ADJ
eurjchem-844	19	11	method	method	NOUN
eurjchem-844	19	12	and	and	CCONJ
eurjchem-844	19	13	one	one	NUM
eurjchem-844	19	14	lc	lc	NOUN
eurjchem-844	19	15	method	method	NOUN
eurjchem-844	19	16	were	be	AUX
eurjchem-844	19	17	reported	report	VERB
eurjchem-844	19	18	for	for	ADP
eurjchem-844	19	19	its	its	PRON
eurjchem-844	19	20	determination	determination	NOUN
eurjchem-844	19	21	[	[	X
eurjchem-844	19	22	5,6	5,6	NUM
eurjchem-844	19	23	]	]	X
eurjchem-844	19	24	.	.	PUNCT
eurjchem-844	20	1	sxg	sxg	PROPN
eurjchem-844	20	2	is	be	AUX
eurjchem-844	20	3	recently	recently	ADV
eurjchem-844	20	4	approved	approve	VERB
eurjchem-844	20	5	for	for	ADP
eurjchem-844	20	6	the	the	DET
eurjchem-844	20	7	treatment	treatment	NOUN
eurjchem-844	20	8	of	of	ADP
eurjchem-844	20	9	type‐2	type‐2	PRON
eurjchem-844	20	10	diabetes	diabetes	NOUN
eurjchem-844	20	11	mellitus	mellitus	NOUN
eurjchem-844	21	1	[	[	X
eurjchem-844	21	2	7	7	NUM
eurjchem-844	21	3	]	]	PUNCT
eurjchem-844	21	4	.	.	PUNCT
eurjchem-844	22	1	literature	literature	NOUN
eurjchem-844	22	2	survey	survey	NOUN
eurjchem-844	22	3	reveals	reveal	VERB
eurjchem-844	22	4	that	that	SCONJ
eurjchem-844	22	5	only	only	ADV
eurjchem-844	22	6	one	one	NUM
eurjchem-844	22	7	lc‐ms	lc‐ms	NUM
eurjchem-844	22	8	/	/	SYM
eurjchem-844	22	9	ms	ms	NOUN
eurjchem-844	23	1	[	[	X
eurjchem-844	23	2	8	8	NUM
eurjchem-844	23	3	]	]	PUNCT
eurjchem-844	23	4	and	and	CCONJ
eurjchem-844	23	5	one	one	NUM
eurjchem-844	23	6	spectrophotometric	spectrophotometric	ADJ
eurjchem-844	23	7	method	method	NOUN
eurjchem-844	23	8	have	have	AUX
eurjchem-844	23	9	been	be	AUX
eurjchem-844	23	10	reported	report	VERB
eurjchem-844	23	11	for	for	ADP
eurjchem-844	23	12	its	its	PRON
eurjchem-844	23	13	determination	determination	NOUN
eurjchem-844	23	14	[	[	X
eurjchem-844	23	15	9	9	NUM
eurjchem-844	23	16	]	]	PUNCT
eurjchem-844	23	17	.	.	PUNCT
eurjchem-844	24	1	metformin	metformin	NOUN
eurjchem-844	24	2	(	(	PUNCT
eurjchem-844	24	3	figure	figure	NOUN
eurjchem-844	24	4	1d	1d	NUM
eurjchem-844	24	5	)	)	PUNCT
eurjchem-844	24	6	,	,	PUNCT
eurjchem-844	24	7	is	be	AUX
eurjchem-844	24	8	a	a	DET
eurjchem-844	24	9	biguanide	biguanide	NOUN
eurjchem-844	24	10	hypoglycemic	hypoglycemic	ADJ
eurjchem-844	24	11	drug	drug	NOUN
eurjchem-844	24	12	that	that	PRON
eurjchem-844	24	13	is	be	AUX
eurjchem-844	24	14	regarded	regard	VERB
eurjchem-844	24	15	as	as	ADP
eurjchem-844	24	16	the	the	DET
eurjchem-844	24	17	main	main	ADJ
eurjchem-844	24	18	compound	compound	NOUN
eurjchem-844	24	19	in	in	ADP
eurjchem-844	24	20	mixed	mixed	ADJ
eurjchem-844	24	21	therapies	therapy	NOUN
eurjchem-844	24	22	of	of	ADP
eurjchem-844	24	23	oral	oral	ADJ
eurjchem-844	24	24	hypoglycemics	hypoglycemic	NOUN
eurjchem-844	24	25	.	.	PUNCT
eurjchem-844	25	1	literature	literature	NOUN
eurjchem-844	25	2	survey	survey	NOUN
eurjchem-844	25	3	reveals	reveal	VERB
eurjchem-844	25	4	some	some	DET
eurjchem-844	25	5	methods	method	NOUN
eurjchem-844	25	6	for	for	ADP
eurjchem-844	25	7	the	the	DET
eurjchem-844	25	8	determination	determination	NOUN
eurjchem-844	25	9	of	of	ADP
eurjchem-844	25	10	met	meet	VERB
eurjchem-844	25	11	in	in	ADP
eurjchem-844	25	12	mixtures	mixture	NOUN
eurjchem-844	25	13	including	include	VERB
eurjchem-844	25	14	lc	lc	PROPN
eurjchem-844	25	15	/	/	SYM
eurjchem-844	25	16	ms	ms	PROPN
eurjchem-844	25	17	/	/	SYM
eurjchem-844	25	18	ms	ms	NOUN
eurjchem-844	26	1	[	[	X
eurjchem-844	26	2	10	10	NUM
eurjchem-844	26	3	]	]	PUNCT
eurjchem-844	26	4	and	and	CCONJ
eurjchem-844	26	5	hplc	hplc	PROPN
eurjchem-844	27	1	[	[	X
eurjchem-844	27	2	11‐14	11‐14	NUM
eurjchem-844	27	3	]	]	PUNCT
eurjchem-844	27	4	.	.	PUNCT
eurjchem-844	28	1	1‐cyanoganidine	1‐cyanoganidine	NUM
eurjchem-844	28	2	(	(	PUNCT
eurjchem-844	28	3	cgn	cgn	PROPN
eurjchem-844	28	4	)	)	PUNCT
eurjchem-844	28	5	is	be	AUX
eurjchem-844	28	6	a	a	DET
eurjchem-844	28	7	potential	potential	ADJ
eurjchem-844	28	8	impurity	impurity	NOUN
eurjchem-844	28	9	of	of	ADP
eurjchem-844	28	10	metformin	metformin	NOUN
eurjchem-844	28	11	hydrochloride	hydrochloride	NOUN
eurjchem-844	28	12	,	,	PUNCT
eurjchem-844	28	13	which	which	PRON
eurjchem-844	28	14	is	be	AUX
eurjchem-844	28	15	reported	report	VERB
eurjchem-844	28	16	in	in	ADP
eurjchem-844	28	17	usp	usp	PROPN
eurjchem-844	28	18	and	and	CCONJ
eurjchem-844	28	19	bp	bp	PROPN
eurjchem-844	28	20	(	(	PUNCT
eurjchem-844	28	21	figure	figure	NOUN
eurjchem-844	28	22	1e	1e	NOUN
eurjchem-844	28	23	)	)	PUNCT
eurjchem-844	29	1	[	[	X
eurjchem-844	29	2	15,16	15,16	NUM
eurjchem-844	29	3	]	]	PUNCT
eurjchem-844	29	4	.	.	PUNCT
eurjchem-844	30	1	only	only	ADV
eurjchem-844	30	2	one	one	NUM
eurjchem-844	30	3	lc	lc	NOUN
eurjchem-844	30	4	method	method	NOUN
eurjchem-844	30	5	has	have	AUX
eurjchem-844	30	6	been	be	AUX
eurjchem-844	30	7	reported	report	VERB
eurjchem-844	30	8	for	for	ADP
eurjchem-844	30	9	the	the	DET
eurjchem-844	30	10	determination	determination	NOUN
eurjchem-844	30	11	of	of	ADP
eurjchem-844	30	12	met	meet	VERB
eurjchem-844	30	13	in	in	ADP
eurjchem-844	30	14	the	the	DET
eurjchem-844	30	15	presence	presence	NOUN
eurjchem-844	30	16	of	of	ADP
eurjchem-844	30	17	cgn	cgn	PROPN
eurjchem-844	30	18	[	[	X
eurjchem-844	30	19	16	16	NUM
eurjchem-844	30	20	]	]	PUNCT
eurjchem-844	30	21	.	.	PUNCT
eurjchem-844	31	1	(	(	PUNCT
eurjchem-844	31	2	a	a	X
eurjchem-844	31	3	)	)	PUNCT
eurjchem-844	31	4	(	(	PUNCT
eurjchem-844	31	5	b	b	X
eurjchem-844	31	6	)	)	PUNCT
eurjchem-844	31	7	(	(	PUNCT
eurjchem-844	31	8	c	c	X
eurjchem-844	31	9	)	)	PUNCT
eurjchem-844	31	10	(	(	PUNCT
eurjchem-844	31	11	d	d	X
eurjchem-844	31	12	)	)	PUNCT
eurjchem-844	31	13	(	(	PUNCT
eurjchem-844	31	14	e	e	NOUN
eurjchem-844	31	15	)	)	PUNCT
eurjchem-844	31	16	figure	figure	NOUN
eurjchem-844	31	17	1	1	NUM
eurjchem-844	31	18	.	.	PUNCT
eurjchem-844	32	1	chemical	chemical	NOUN
eurjchem-844	32	2	structures	structure	NOUN
eurjchem-844	32	3	of	of	ADP
eurjchem-844	32	4	the	the	DET
eurjchem-844	32	5	drugs	drug	NOUN
eurjchem-844	32	6	;	;	PUNCT
eurjchem-844	32	7	(	(	PUNCT
eurjchem-844	32	8	a	a	X
eurjchem-844	32	9	)	)	PUNCT
eurjchem-844	32	10	sitagliptin	sitagliptin	NOUN
eurjchem-844	32	11	,	,	PUNCT
eurjchem-844	32	12	[	[	X
eurjchem-844	32	13	(	(	PUNCT
eurjchem-844	32	14	2r)‐1‐(2,4,5‐	2r)‐1‐(2,4,5‐	NUM
eurjchem-844	32	15	trifluorophenyl)‐4‐oxo‐4‐[3‐(trifluoromethyl)‐5,6‐dihydro	trifluorophenyl)‐4‐oxo‐4‐[3‐(trifluoromethyl)‐5,6‐dihydro	PROPN
eurjchem-844	33	1	[	[	X
eurjchem-844	33	2	1,2,4	1,2,4	X
eurjchem-844	33	3	]	]	X
eurjchem-844	33	4	triazolo	triazolo	NOUN
eurjchem-844	34	1	[	[	X
eurjchem-844	34	2	4,3‐a	4,3‐a	NOUN
eurjchem-844	34	3	]	]	X
eurjchem-844	34	4	pyrazin‐7(8h)‐yl	pyrazin‐7(8h)‐yl	PROPN
eurjchem-844	34	5	]	]	PUNCT
eurjchem-844	34	6	butan‐2‐amine	butan‐2‐amine	X
eurjchem-844	34	7	]	]	PUNCT
eurjchem-844	34	8	;	;	PUNCT
eurjchem-844	34	9	(	(	PUNCT
eurjchem-844	34	10	b	b	X
eurjchem-844	34	11	)	)	PUNCT
eurjchem-844	34	12	vildagliptin	vildagliptin	NOUN
eurjchem-844	34	13	,	,	PUNCT
eurjchem-844	34	14	s‐1‐[n‐(3‐	s‐1‐[n‐(3‐	X
eurjchem-844	34	15	hydroxy‐1‐adamantyl	hydroxy‐1‐adamantyl	NOUN
eurjchem-844	34	16	)	)	PUNCT
eurjchem-844	34	17	glycyl	glycyl	NOUN
eurjchem-844	34	18	]	]	PUNCT
eurjchem-844	34	19	pyrrolidine‐2‐carbonitrile	pyrrolidine‐2‐carbonitrile	NUM
eurjchem-844	34	20	;	;	PUNCT
eurjchem-844	34	21	(	(	PUNCT
eurjchem-844	34	22	c	c	X
eurjchem-844	34	23	)	)	PUNCT
eurjchem-844	34	24	saxagliptin	saxagliptin	NOUN
eurjchem-844	34	25	,	,	PUNCT
eurjchem-844	34	26	(	(	PUNCT
eurjchem-844	34	27	1s,3s,5s)‐2‐[(2s)‐2‐amino‐2‐(3‐hydroxy‐1‐adamantyl)acetyl]‐2‐azabicyclo	1s,3s,5s)‐2‐[(2s)‐2‐amino‐2‐(3‐hydroxy‐1‐adamantyl)acetyl]‐2‐azabicyclo	NUM
eurjchem-844	34	28	[	[	PUNCT
eurjchem-844	34	29	3.1.0	3.1.0	NUM
eurjchem-844	34	30	]	]	X
eurjchem-844	34	31	hexane‐3‐carbonitrile	hexane‐3‐carbonitrile	NUM
eurjchem-844	34	32	;	;	PUNCT
eurjchem-844	34	33	(	(	PUNCT
eurjchem-844	34	34	d	d	X
eurjchem-844	34	35	)	)	PUNCT
eurjchem-844	34	36	metformin	metformin	NOUN
eurjchem-844	34	37	,	,	PUNCT
eurjchem-844	34	38	n	n	CCONJ
eurjchem-844	34	39	,	,	PUNCT
eurjchem-844	34	40	n‐dimethylimidodicarbon	n‐dimethylimidodicarbon	PUNCT
eurjchem-844	34	41	imidic	imidic	ADJ
eurjchem-844	34	42	diamide	diamide	NOUN
eurjchem-844	34	43	;	;	PUNCT
eurjchem-844	34	44	(	(	PUNCT
eurjchem-844	34	45	e	e	NOUN
eurjchem-844	34	46	)	)	PUNCT
eurjchem-844	34	47	cyanoguanidine	cyanoguanidine	NOUN
eurjchem-844	34	48	.	.	PUNCT
eurjchem-844	35	1	el‐bagary	el‐bagary	PROPN
eurjchem-844	35	2	et	et	PROPN
eurjchem-844	35	3	al	al	PROPN
eurjchem-844	35	4	.	.	PUNCT
eurjchem-844	35	5	/	/	SYM
eurjchem-844	35	6	european	european	PROPN
eurjchem-844	35	7	journal	journal	PROPN
eurjchem-844	35	8	of	of	ADP
eurjchem-844	35	9	chemistry	chemistry	NOUN
eurjchem-844	35	10	4	4	NUM
eurjchem-844	35	11	(	(	PUNCT
eurjchem-844	35	12	4	4	NUM
eurjchem-844	35	13	)	)	PUNCT
eurjchem-844	35	14	(	(	PUNCT
eurjchem-844	35	15	2013	2013	NUM
eurjchem-844	35	16	)	)	PUNCT
eurjchem-844	35	17	444‐449	444‐449	NOUN
eurjchem-844	35	18	445	445	NUM
eurjchem-844	36	1	the	the	DET
eurjchem-844	36	2	aim	aim	NOUN
eurjchem-844	36	3	of	of	ADP
eurjchem-844	36	4	the	the	DET
eurjchem-844	36	5	present	present	ADJ
eurjchem-844	36	6	work	work	NOUN
eurjchem-844	36	7	was	be	AUX
eurjchem-844	36	8	to	to	PART
eurjchem-844	36	9	develop	develop	VERB
eurjchem-844	36	10	and	and	CCONJ
eurjchem-844	36	11	validate	validate	VERB
eurjchem-844	36	12	one	one	NUM
eurjchem-844	36	13	simple	simple	ADJ
eurjchem-844	36	14	reversed	reverse	VERB
eurjchem-844	36	15	phase	phase	NOUN
eurjchem-844	36	16	liquid	liquid	NOUN
eurjchem-844	36	17	chromatographic	chromatographic	ADJ
eurjchem-844	36	18	(	(	PUNCT
eurjchem-844	36	19	rp‐lc	rp‐lc	NOUN
eurjchem-844	36	20	)	)	PUNCT
eurjchem-844	36	21	method	method	NOUN
eurjchem-844	36	22	that	that	PRON
eurjchem-844	36	23	could	could	AUX
eurjchem-844	36	24	be	be	AUX
eurjchem-844	36	25	applied	apply	VERB
eurjchem-844	36	26	for	for	ADP
eurjchem-844	36	27	the	the	DET
eurjchem-844	36	28	simultaneous	simultaneous	ADJ
eurjchem-844	36	29	determination	determination	NOUN
eurjchem-844	36	30	of	of	ADP
eurjchem-844	36	31	each	each	PRON
eurjchem-844	36	32	of	of	ADP
eurjchem-844	36	33	the	the	DET
eurjchem-844	36	34	three	three	NUM
eurjchem-844	36	35	commonly	commonly	ADV
eurjchem-844	36	36	used	use	VERB
eurjchem-844	36	37	gliptins	gliptin	NOUN
eurjchem-844	36	38	;	;	PUNCT
eurjchem-844	36	39	stg	stg	PROPN
eurjchem-844	36	40	,	,	PUNCT
eurjchem-844	36	41	vdg	vdg	NOUN
eurjchem-844	36	42	and	and	CCONJ
eurjchem-844	36	43	sxg	sxg	NOUN
eurjchem-844	36	44	and	and	CCONJ
eurjchem-844	36	45	met	meet	VERB
eurjchem-844	36	46	in	in	ADP
eurjchem-844	36	47	their	their	PRON
eurjchem-844	36	48	ternary	ternary	ADJ
eurjchem-844	36	49	mixture	mixture	NOUN
eurjchem-844	36	50	with	with	ADP
eurjchem-844	36	51	met	meet	VERB
eurjchem-844	36	52	degradation	degradation	NOUN
eurjchem-844	36	53	product	product	NOUN
eurjchem-844	36	54	,	,	PUNCT
eurjchem-844	36	55	cgn	cgn	PROPN
eurjchem-844	36	56	(	(	PUNCT
eurjchem-844	36	57	stability	stability	NOUN
eurjchem-844	36	58	indicating	indicate	VERB
eurjchem-844	36	59	assay	assay	VERB
eurjchem-844	36	60	for	for	ADP
eurjchem-844	36	61	met	meet	VERB
eurjchem-844	36	62	)	)	PUNCT
eurjchem-844	36	63	.	.	PUNCT
eurjchem-844	37	1	2	2	X
eurjchem-844	37	2	.	.	X
eurjchem-844	37	3	experimental	experimental	ADJ
eurjchem-844	37	4	2.1	2.1	NUM
eurjchem-844	37	5	.	.	PUNCT
eurjchem-844	38	1	instrumentation	instrumentation	NOUN
eurjchem-844	38	2	the	the	DET
eurjchem-844	38	3	hplc	hplc	NOUN
eurjchem-844	38	4	system	system	NOUN
eurjchem-844	38	5	consisted	consist	VERB
eurjchem-844	38	6	of	of	ADP
eurjchem-844	38	7	a	a	DET
eurjchem-844	38	8	shimadzu	shimadzu	ADJ
eurjchem-844	38	9	lc‐20	lc‐20	NOUN
eurjchem-844	38	10	at	at	ADP
eurjchem-844	38	11	liquid	liquid	ADJ
eurjchem-844	38	12	chromatograph	chromatograph	NOUN
eurjchem-844	38	13	(	(	PUNCT
eurjchem-844	38	14	japan	japan	PROPN
eurjchem-844	38	15	)	)	PUNCT
eurjchem-844	38	16	using	use	VERB
eurjchem-844	38	17	a	a	DET
eurjchem-844	38	18	symmetry	symmetry	NOUN
eurjchem-844	38	19	®	®	NOUN
eurjchem-844	38	20	cyanide	cyanide	NOUN
eurjchem-844	38	21	column	column	NOUN
eurjchem-844	38	22	(	(	PUNCT
eurjchem-844	38	23	150	150	NUM
eurjchem-844	38	24	mm	mm	NOUN
eurjchem-844	38	25	×	×	NOUN
eurjchem-844	38	26	4.6	4.6	NUM
eurjchem-844	38	27	mm	mm	NOUN
eurjchem-844	38	28	,	,	PUNCT
eurjchem-844	38	29	5	5	NUM
eurjchem-844	38	30	μm	μm	NOUN
eurjchem-844	38	31	)	)	PUNCT
eurjchem-844	38	32	(	(	PUNCT
eurjchem-844	38	33	ireland	ireland	NOUN
eurjchem-844	38	34	)	)	PUNCT
eurjchem-844	38	35	.	.	PUNCT
eurjchem-844	39	1	the	the	DET
eurjchem-844	39	2	system	system	NOUN
eurjchem-844	39	3	was	be	AUX
eurjchem-844	39	4	equipped	equip	VERB
eurjchem-844	39	5	with	with	ADP
eurjchem-844	39	6	a	a	DET
eurjchem-844	39	7	uv‐visible	uv‐visible	ADJ
eurjchem-844	39	8	detector	detector	NOUN
eurjchem-844	39	9	(	(	PUNCT
eurjchem-844	39	10	spd‐20a	spd‐20a	PROPN
eurjchem-844	39	11	,	,	PUNCT
eurjchem-844	39	12	japan	japan	PROPN
eurjchem-844	39	13	)	)	PUNCT
eurjchem-844	39	14	and	and	CCONJ
eurjchem-844	39	15	an	an	DET
eurjchem-844	39	16	auto	auto	NOUN
eurjchem-844	39	17	sampler	sampler	NOUN
eurjchem-844	39	18	(	(	PUNCT
eurjchem-844	39	19	sil‐20a	sil‐20a	NOUN
eurjchem-844	39	20	,	,	PUNCT
eurjchem-844	39	21	shimadzu	shimadzu	NOUN
eurjchem-844	39	22	,	,	PUNCT
eurjchem-844	39	23	japan	japan	PROPN
eurjchem-844	39	24	)	)	PUNCT
eurjchem-844	39	25	.	.	PUNCT
eurjchem-844	40	1	an	an	PRON
eurjchem-844	40	2	elma	elma	PROPN
eurjchem-844	40	3	s100	s100	PROPN
eurjchem-844	40	4	ultrasonic	ultrasonic	ADJ
eurjchem-844	40	5	processor	processor	NOUN
eurjchem-844	40	6	model	model	NOUN
eurjchem-844	40	7	kbk	kbk	PROPN
eurjchem-844	40	8	4200	4200	NUM
eurjchem-844	40	9	(	(	PUNCT
eurjchem-844	40	10	germany	germany	PROPN
eurjchem-844	40	11	)	)	PUNCT
eurjchem-844	40	12	was	be	AUX
eurjchem-844	40	13	used	use	VERB
eurjchem-844	40	14	for	for	ADP
eurjchem-844	40	15	the	the	DET
eurjchem-844	40	16	degassing	degassing	NOUN
eurjchem-844	40	17	of	of	ADP
eurjchem-844	40	18	the	the	DET
eurjchem-844	40	19	mobile	mobile	ADJ
eurjchem-844	40	20	phases	phase	NOUN
eurjchem-844	40	21	.	.	PUNCT
eurjchem-844	41	1	2.2	2.2	NUM
eurjchem-844	41	2	.	.	PUNCT
eurjchem-844	41	3	reagents	reagent	NOUN
eurjchem-844	41	4	and	and	CCONJ
eurjchem-844	41	5	reference	reference	NOUN
eurjchem-844	41	6	samples	sample	NOUN
eurjchem-844	41	7	pharmaceutical	pharmaceutical	ADJ
eurjchem-844	41	8	grade	grade	NOUN
eurjchem-844	41	9	stg	stg	PROPN
eurjchem-844	41	10	monohydrate	monohydrate	NOUN
eurjchem-844	41	11	,	,	PUNCT
eurjchem-844	41	12	certified	certify	VERB
eurjchem-844	41	13	to	to	PART
eurjchem-844	41	14	contain	contain	VERB
eurjchem-844	41	15	99.80	99.80	NUM
eurjchem-844	41	16	%	%	NOUN
eurjchem-844	41	17	,	,	PUNCT
eurjchem-844	41	18	janumet	janumet	ADJ
eurjchem-844	41	19	®	®	NOUN
eurjchem-844	41	20	tablets	tablet	NOUN
eurjchem-844	41	21	nominally	nominally	ADV
eurjchem-844	41	22	containing	contain	VERB
eurjchem-844	41	23	64.25	64.25	NUM
eurjchem-844	41	24	mg	mg	NOUN
eurjchem-844	41	25	of	of	ADP
eurjchem-844	41	26	stg	stg	PROPN
eurjchem-844	41	27	and	and	CCONJ
eurjchem-844	41	28	1000	1000	NUM
eurjchem-844	41	29	mg	mg	NOUN
eurjchem-844	41	30	of	of	ADP
eurjchem-844	41	31	met	meet	VERB
eurjchem-844	41	32	per	per	ADP
eurjchem-844	41	33	tablet	tablet	NOUN
eurjchem-844	41	34	were	be	AUX
eurjchem-844	41	35	all	all	PRON
eurjchem-844	41	36	kindly	kindly	ADV
eurjchem-844	41	37	supplied	supply	VERB
eurjchem-844	41	38	from	from	ADP
eurjchem-844	41	39	merck	merck	PROPN
eurjchem-844	41	40	sharp	sharp	PROPN
eurjchem-844	41	41	and	and	CCONJ
eurjchem-844	41	42	dohme	dohme	PROPN
eurjchem-844	41	43	co.	co.	PROPN
eurjchem-844	41	44	(	(	PUNCT
eurjchem-844	41	45	cairo	cairo	PROPN
eurjchem-844	41	46	,	,	PUNCT
eurjchem-844	41	47	egypt	egypt	PROPN
eurjchem-844	41	48	)	)	PUNCT
eurjchem-844	41	49	.	.	PUNCT
eurjchem-844	42	1	pharmaceutical	pharmaceutical	PROPN
eurjchem-844	42	2	grade	grade	PROPN
eurjchem-844	42	3	vdg	vdg	PROPN
eurjchem-844	42	4	,	,	PUNCT
eurjchem-844	42	5	certified	certify	VERB
eurjchem-844	42	6	to	to	PART
eurjchem-844	42	7	contain	contain	VERB
eurjchem-844	42	8	99.70	99.70	NUM
eurjchem-844	42	9	%	%	NOUN
eurjchem-844	42	10	and	and	CCONJ
eurjchem-844	42	11	eucreas	eucreas	ADJ
eurjchem-844	42	12	®	®	NOUN
eurjchem-844	42	13	tablets	tablet	NOUN
eurjchem-844	42	14	nominally	nominally	ADV
eurjchem-844	42	15	containing	contain	VERB
eurjchem-844	42	16	50	50	NUM
eurjchem-844	42	17	mg	mg	NOUN
eurjchem-844	42	18	vdg	vdg	NOUN
eurjchem-844	42	19	and	and	CCONJ
eurjchem-844	42	20	500	500	NUM
eurjchem-844	42	21	mg	mg	NOUN
eurjchem-844	42	22	of	of	ADP
eurjchem-844	42	23	met	meet	VERB
eurjchem-844	42	24	per	per	ADP
eurjchem-844	42	25	tablet	tablet	NOUN
eurjchem-844	42	26	were	be	AUX
eurjchem-844	42	27	kindly	kindly	ADV
eurjchem-844	42	28	supplied	supply	VERB
eurjchem-844	42	29	from	from	ADP
eurjchem-844	42	30	novartis	novartis	PROPN
eurjchem-844	42	31	europharm	europharm	NOUN
eurjchem-844	42	32	limited	limit	VERB
eurjchem-844	42	33	company	company	NOUN
eurjchem-844	42	34	(	(	PUNCT
eurjchem-844	42	35	london	london	PROPN
eurjchem-844	42	36	,	,	PUNCT
eurjchem-844	42	37	u.k	u.k	PROPN
eurjchem-844	42	38	.	.	PROPN
eurjchem-844	42	39	)	)	PUNCT
eurjchem-844	42	40	.	.	PUNCT
eurjchem-844	43	1	pharmaceutical	pharmaceutical	NOUN
eurjchem-844	43	2	grade	grade	PROPN
eurjchem-844	43	3	sxg	sxg	NOUN
eurjchem-844	43	4	,	,	PUNCT
eurjchem-844	43	5	certified	certify	VERB
eurjchem-844	43	6	to	to	PART
eurjchem-844	43	7	contain	contain	VERB
eurjchem-844	43	8	99.85	99.85	NUM
eurjchem-844	43	9	%	%	NOUN
eurjchem-844	43	10	and	and	CCONJ
eurjchem-844	43	11	kombiglyze	kombiglyze	NOUN
eurjchem-844	43	12	®	®	NOUN
eurjchem-844	43	13	tablets	tablet	NOUN
eurjchem-844	43	14	nominally	nominally	ADV
eurjchem-844	43	15	containing	contain	VERB
eurjchem-844	43	16	5.58	5.58	NUM
eurjchem-844	43	17	mg	mg	NOUN
eurjchem-844	43	18	of	of	ADP
eurjchem-844	43	19	sxg	sxg	NOUN
eurjchem-844	43	20	and	and	CCONJ
eurjchem-844	43	21	500	500	NUM
eurjchem-844	43	22	mg	mg	NOUN
eurjchem-844	43	23	of	of	ADP
eurjchem-844	43	24	met	meet	VERB
eurjchem-844	43	25	per	per	ADP
eurjchem-844	43	26	tablet	tablet	NOUN
eurjchem-844	43	27	were	be	AUX
eurjchem-844	43	28	kindly	kindly	ADV
eurjchem-844	43	29	supplied	supply	VERB
eurjchem-844	43	30	by	by	ADP
eurjchem-844	43	31	bristol‐myers	bristol‐myer	NOUN
eurjchem-844	43	32	squibb	squibb	PROPN
eurjchem-844	43	33	/	/	SYM
eurjchem-844	43	34	astra	astra	PROPN
eurjchem-844	43	35	zeneca	zeneca	PROPN
eurjchem-844	43	36	eeig	eeig	PROPN
eurjchem-844	43	37	(	(	PUNCT
eurjchem-844	43	38	united	united	ADJ
eurjchem-844	43	39	kingdom	kingdom	PROPN
eurjchem-844	43	40	)	)	PUNCT
eurjchem-844	43	41	.	.	PUNCT
eurjchem-844	44	1	pharmaceutical	pharmaceutical	PROPN
eurjchem-844	44	2	grade	grade	NOUN
eurjchem-844	44	3	met	meet	VERB
eurjchem-844	44	4	,	,	PUNCT
eurjchem-844	44	5	certified	certify	VERB
eurjchem-844	44	6	to	to	PART
eurjchem-844	44	7	contain	contain	VERB
eurjchem-844	44	8	99.79	99.79	NUM
eurjchem-844	44	9	%	%	NOUN
eurjchem-844	44	10	was	be	AUX
eurjchem-844	44	11	kindly	kindly	ADV
eurjchem-844	44	12	supplied	supply	VERB
eurjchem-844	44	13	by	by	ADP
eurjchem-844	44	14	chemical	chemical	NOUN
eurjchem-844	44	15	industries	industry	NOUN
eurjchem-844	44	16	development	development	NOUN
eurjchem-844	44	17	(	(	PUNCT
eurjchem-844	44	18	cid	cid	PROPN
eurjchem-844	44	19	)	)	PUNCT
eurjchem-844	44	20	co.	co.	PROPN
eurjchem-844	44	21	(	(	PUNCT
eurjchem-844	44	22	giza	giza	PROPN
eurjchem-844	44	23	,	,	PUNCT
eurjchem-844	44	24	egypt	egypt	PROPN
eurjchem-844	44	25	)	)	PUNCT
eurjchem-844	44	26	.	.	PUNCT
eurjchem-844	45	1	cgn	cgn	PROPN
eurjchem-844	45	2	was	be	AUX
eurjchem-844	45	3	brought	bring	VERB
eurjchem-844	45	4	from	from	ADP
eurjchem-844	45	5	fluka	fluka	PROPN
eurjchem-844	45	6	(	(	PUNCT
eurjchem-844	45	7	steinheim	steinheim	PROPN
eurjchem-844	45	8	,	,	PUNCT
eurjchem-844	45	9	germany	germany	PROPN
eurjchem-844	45	10	)	)	PUNCT
eurjchem-844	45	11	.	.	PUNCT
eurjchem-844	46	1	methanol	methanol	NOUN
eurjchem-844	46	2	(	(	PUNCT
eurjchem-844	46	3	hipersolv	hipersolv	NOUN
eurjchem-844	46	4	for	for	ADP
eurjchem-844	46	5	hplc	hplc	NOUN
eurjchem-844	46	6	)	)	PUNCT
eurjchem-844	46	7	,	,	PUNCT
eurjchem-844	46	8	acetonitrile	acetonitrile	NOUN
eurjchem-844	46	9	(	(	PUNCT
eurjchem-844	46	10	hipersolv	hipersolv	NOUN
eurjchem-844	46	11	)	)	PUNCT
eurjchem-844	46	12	were	be	AUX
eurjchem-844	46	13	purchased	purchase	VERB
eurjchem-844	46	14	from	from	ADP
eurjchem-844	46	15	fisher	fisher	PROPN
eurjchem-844	46	16	scientific	scientific	PROPN
eurjchem-844	46	17	(	(	PUNCT
eurjchem-844	46	18	loughborough	loughborough	PROPN
eurjchem-844	46	19	,	,	PUNCT
eurjchem-844	46	20	leicestershire	leicestershire	NOUN
eurjchem-844	46	21	,	,	PUNCT
eurjchem-844	46	22	uk	uk	PROPN
eurjchem-844	46	23	)	)	PUNCT
eurjchem-844	46	24	.	.	PUNCT
eurjchem-844	47	1	potassium	potassium	NOUN
eurjchem-844	47	2	dihydrogen	dihydrogen	NOUN
eurjchem-844	47	3	phosphate	phosphate	NOUN
eurjchem-844	47	4	and	and	CCONJ
eurjchem-844	47	5	orthophosphric	orthophosphric	ADJ
eurjchem-844	47	6	acid	acid	NOUN
eurjchem-844	47	7	(	(	PUNCT
eurjchem-844	47	8	85	85	NUM
eurjchem-844	47	9	%	%	NOUN
eurjchem-844	47	10	)	)	PUNCT
eurjchem-844	47	11	were	be	AUX
eurjchem-844	47	12	obtained	obtain	VERB
eurjchem-844	47	13	from	from	ADP
eurjchem-844	47	14	vwr	vwr	PROPN
eurjchem-844	47	15	chemicals	chemical	NOUN
eurjchem-844	47	16	(	(	PUNCT
eurjchem-844	47	17	pool	pool	NOUN
eurjchem-844	47	18	,	,	PUNCT
eurjchem-844	47	19	england	england	PROPN
eurjchem-844	47	20	)	)	PUNCT
eurjchem-844	47	21	.	.	PUNCT
eurjchem-844	48	1	bi‐	bi‐	NOUN
eurjchem-844	48	2	distilled	distil	VERB
eurjchem-844	48	3	water	water	NOUN
eurjchem-844	48	4	was	be	AUX
eurjchem-844	48	5	produced	produce	VERB
eurjchem-844	48	6	in‐house	in‐house	NOUN
eurjchem-844	48	7	(	(	PUNCT
eurjchem-844	48	8	aquatron	aquatron	VERB
eurjchem-844	48	9	water	water	NOUN
eurjchem-844	48	10	still	still	ADV
eurjchem-844	48	11	,	,	PUNCT
eurjchem-844	48	12	a4000d	a4000d	PROPN
eurjchem-844	48	13	,	,	PUNCT
eurjchem-844	48	14	uk	uk	PROPN
eurjchem-844	48	15	)	)	PUNCT
eurjchem-844	48	16	.	.	PUNCT
eurjchem-844	49	1	membrane	membrane	NOUN
eurjchem-844	49	2	filters	filter	NOUN
eurjchem-844	49	3	0.45	0.45	NUM
eurjchem-844	49	4	µm	µm	NOUN
eurjchem-844	49	5	from	from	ADP
eurjchem-844	49	6	teknokroma	teknokroma	NOUN
eurjchem-844	49	7	(	(	PUNCT
eurjchem-844	49	8	barcelona	barcelona	PROPN
eurjchem-844	49	9	,	,	PUNCT
eurjchem-844	49	10	spain	spain	PROPN
eurjchem-844	49	11	)	)	PUNCT
eurjchem-844	49	12	were	be	AUX
eurjchem-844	49	13	used	use	VERB
eurjchem-844	49	14	.	.	PUNCT
eurjchem-844	50	1	all	all	DET
eurjchem-844	50	2	other	other	ADJ
eurjchem-844	50	3	chemicals	chemical	NOUN
eurjchem-844	50	4	and	and	CCONJ
eurjchem-844	50	5	reagents	reagent	NOUN
eurjchem-844	50	6	used	use	VERB
eurjchem-844	50	7	were	be	AUX
eurjchem-844	50	8	of	of	ADP
eurjchem-844	50	9	analytical	analytical	ADJ
eurjchem-844	50	10	grade	grade	NOUN
eurjchem-844	50	11	unless	unless	SCONJ
eurjchem-844	50	12	indicated	indicate	VERB
eurjchem-844	50	13	otherwise	otherwise	ADV
eurjchem-844	50	14	.	.	PUNCT
eurjchem-844	51	1	standard	standard	ADJ
eurjchem-844	51	2	stock	stock	NOUN
eurjchem-844	51	3	solutions	solution	NOUN
eurjchem-844	51	4	of	of	ADP
eurjchem-844	51	5	each	each	DET
eurjchem-844	51	6	drug	drug	NOUN
eurjchem-844	51	7	(	(	PUNCT
eurjchem-844	51	8	1	1	NUM
eurjchem-844	51	9	mg	mg	NUM
eurjchem-844	51	10	/	/	SYM
eurjchem-844	51	11	ml	ml	NOUN
eurjchem-844	51	12	)	)	PUNCT
eurjchem-844	51	13	were	be	AUX
eurjchem-844	51	14	prepared	prepare	VERB
eurjchem-844	51	15	by	by	ADP
eurjchem-844	51	16	dissolving	dissolve	VERB
eurjchem-844	51	17	100	100	NUM
eurjchem-844	51	18	mg	mg	ADP
eurjchem-844	51	19	of	of	ADP
eurjchem-844	51	20	the	the	DET
eurjchem-844	51	21	drug	drug	NOUN
eurjchem-844	51	22	in	in	ADP
eurjchem-844	51	23	methanol	methanol	NOUN
eurjchem-844	51	24	in	in	ADP
eurjchem-844	51	25	a	a	DET
eurjchem-844	51	26	100	100	NUM
eurjchem-844	51	27	ml	ml	NOUN
eurjchem-844	51	28	volumetric	volumetric	ADJ
eurjchem-844	51	29	flask	flask	NOUN
eurjchem-844	51	30	and	and	CCONJ
eurjchem-844	51	31	then	then	ADV
eurjchem-844	51	32	completed	complete	VERB
eurjchem-844	51	33	to	to	PART
eurjchem-844	51	34	volume	volume	VERB
eurjchem-844	51	35	with	with	ADP
eurjchem-844	51	36	methanol	methanol	NOUN
eurjchem-844	51	37	.	.	PUNCT
eurjchem-844	52	1	then	then	ADV
eurjchem-844	52	2	required	require	VERB
eurjchem-844	52	3	concentrations	concentration	NOUN
eurjchem-844	52	4	were	be	AUX
eurjchem-844	52	5	prepared	prepare	VERB
eurjchem-844	52	6	by	by	ADP
eurjchem-844	52	7	serial	serial	ADJ
eurjchem-844	52	8	dilutions	dilution	NOUN
eurjchem-844	52	9	with	with	ADP
eurjchem-844	52	10	methanol	methanol	NOUN
eurjchem-844	52	11	of	of	ADP
eurjchem-844	52	12	these	these	DET
eurjchem-844	52	13	stock	stock	NOUN
eurjchem-844	52	14	solutions	solution	NOUN
eurjchem-844	52	15	.	.	PUNCT
eurjchem-844	53	1	2.3	2.3	NUM
eurjchem-844	53	2	.	.	PUNCT
eurjchem-844	53	3	chromatographic	chromatographic	ADJ
eurjchem-844	53	4	conditions	condition	NOUN
eurjchem-844	53	5	chromatographic	chromatographic	ADJ
eurjchem-844	53	6	separation	separation	NOUN
eurjchem-844	53	7	was	be	AUX
eurjchem-844	53	8	achieved	achieve	VERB
eurjchem-844	53	9	on	on	ADP
eurjchem-844	53	10	a	a	DET
eurjchem-844	53	11	symmetry	symmetry	NOUN
eurjchem-844	53	12	®	®	NOUN
eurjchem-844	53	13	cyanide	cyanide	NOUN
eurjchem-844	53	14	column	column	NOUN
eurjchem-844	53	15	(	(	PUNCT
eurjchem-844	53	16	150	150	NUM
eurjchem-844	53	17	mm	mm	NOUN
eurjchem-844	53	18	×	×	NOUN
eurjchem-844	53	19	4.6	4.6	NUM
eurjchem-844	53	20	mm	mm	NOUN
eurjchem-844	53	21	,	,	PUNCT
eurjchem-844	53	22	5	5	NUM
eurjchem-844	53	23	μm	μm	NUM
eurjchem-844	53	24	)	)	PUNCT
eurjchem-844	53	25	.	.	PUNCT
eurjchem-844	54	1	isocratic	isocratic	ADJ
eurjchem-844	54	2	elution	elution	NOUN
eurjchem-844	54	3	using	use	VERB
eurjchem-844	54	4	a	a	DET
eurjchem-844	54	5	mobile	mobile	ADJ
eurjchem-844	54	6	phase	phase	NOUN
eurjchem-844	54	7	consisting	consist	VERB
eurjchem-844	54	8	of	of	ADP
eurjchem-844	54	9	potassium	potassium	NOUN
eurjchem-844	54	10	dihydrogen	dihydrogen	NOUN
eurjchem-844	54	11	phosphate	phosphate	NOUN
eurjchem-844	54	12	buffer	buffer	NOUN
eurjchem-844	54	13	(	(	PUNCT
eurjchem-844	54	14	ph	ph	NOUN
eurjchem-844	54	15	=	=	NOUN
eurjchem-844	54	16	4.6	4.6	NUM
eurjchem-844	54	17	)	)	PUNCT
eurjchem-844	54	18	‐	‐	ADJ
eurjchem-844	54	19	acetonitrile	acetonitrile	NOUN
eurjchem-844	54	20	(	(	PUNCT
eurjchem-844	54	21	30:70	30:70	NUM
eurjchem-844	54	22	,	,	PUNCT
eurjchem-844	54	23	v	v	NOUN
eurjchem-844	54	24	:	:	SYM
eurjchem-844	54	25	v	v	NOUN
eurjchem-844	54	26	)	)	PUNCT
eurjchem-844	54	27	with	with	ADP
eurjchem-844	54	28	uv	uv	NOUN
eurjchem-844	54	29	detection	detection	NOUN
eurjchem-844	54	30	at	at	ADP
eurjchem-844	54	31	210	210	NUM
eurjchem-844	54	32	nm	nm	NOUN
eurjchem-844	54	33	was	be	AUX
eurjchem-844	54	34	performed	perform	VERB
eurjchem-844	54	35	.	.	PUNCT
eurjchem-844	55	1	the	the	DET
eurjchem-844	55	2	buffer	buffer	NOUN
eurjchem-844	55	3	solution	solution	NOUN
eurjchem-844	55	4	was	be	AUX
eurjchem-844	55	5	filtered	filter	VERB
eurjchem-844	55	6	through	through	ADP
eurjchem-844	55	7	0.45	0.45	NUM
eurjchem-844	55	8	µm	µm	ADP
eurjchem-844	55	9	membrane	membrane	NOUN
eurjchem-844	55	10	filter	filter	NOUN
eurjchem-844	55	11	and	and	CCONJ
eurjchem-844	55	12	degassed	degas	VERB
eurjchem-844	55	13	for	for	ADP
eurjchem-844	55	14	30	30	NUM
eurjchem-844	55	15	min	min	NOUN
eurjchem-844	55	16	in	in	ADP
eurjchem-844	55	17	an	an	DET
eurjchem-844	55	18	ultrasonic	ultrasonic	ADJ
eurjchem-844	55	19	bath	bath	NOUN
eurjchem-844	55	20	prior	prior	ADV
eurjchem-844	55	21	to	to	ADP
eurjchem-844	55	22	use	use	NOUN
eurjchem-844	55	23	.	.	PUNCT
eurjchem-844	56	1	the	the	DET
eurjchem-844	56	2	mobile	mobile	ADJ
eurjchem-844	56	3	phase	phase	NOUN
eurjchem-844	56	4	was	be	AUX
eurjchem-844	56	5	pumped	pump	VERB
eurjchem-844	56	6	through	through	ADP
eurjchem-844	56	7	the	the	DET
eurjchem-844	56	8	column	column	NOUN
eurjchem-844	56	9	at	at	ADP
eurjchem-844	56	10	a	a	DET
eurjchem-844	56	11	flow	flow	NOUN
eurjchem-844	56	12	rate	rate	NOUN
eurjchem-844	56	13	of	of	ADP
eurjchem-844	56	14	1	1	NUM
eurjchem-844	56	15	ml	ml	NOUN
eurjchem-844	56	16	/	/	SYM
eurjchem-844	56	17	min	min	NOUN
eurjchem-844	56	18	.	.	PROPN
eurjchem-844	56	19	analyses	analysis	NOUN
eurjchem-844	56	20	were	be	AUX
eurjchem-844	56	21	performed	perform	VERB
eurjchem-844	56	22	at	at	ADP
eurjchem-844	56	23	ambient	ambient	ADJ
eurjchem-844	56	24	temperature	temperature	NOUN
eurjchem-844	56	25	and	and	CCONJ
eurjchem-844	56	26	the	the	DET
eurjchem-844	56	27	injection	injection	NOUN
eurjchem-844	56	28	volume	volume	NOUN
eurjchem-844	56	29	was	be	AUX
eurjchem-844	56	30	25	25	NUM
eurjchem-844	56	31	µl	µl	NOUN
eurjchem-844	56	32	.	.	PUNCT
eurjchem-844	57	1	2.4	2.4	NUM
eurjchem-844	57	2	.	.	PUNCT
eurjchem-844	58	1	samples	sample	NOUN
eurjchem-844	58	2	’	'	PUNCT
eurjchem-844	58	3	preparation	preparation	NOUN
eurjchem-844	58	4	twenty	twenty	NUM
eurjchem-844	58	5	tablets	tablet	NOUN
eurjchem-844	58	6	of	of	ADP
eurjchem-844	58	7	each	each	DET
eurjchem-844	58	8	pharmaceutical	pharmaceutical	ADJ
eurjchem-844	58	9	preparation	preparation	NOUN
eurjchem-844	58	10	were	be	AUX
eurjchem-844	58	11	weighed	weigh	VERB
eurjchem-844	58	12	.	.	PUNCT
eurjchem-844	59	1	an	an	DET
eurjchem-844	59	2	accurately	accurately	ADV
eurjchem-844	59	3	weighed	weigh	VERB
eurjchem-844	59	4	amount	amount	NOUN
eurjchem-844	59	5	of	of	ADP
eurjchem-844	59	6	the	the	DET
eurjchem-844	59	7	finely	finely	ADV
eurjchem-844	59	8	powdered	powdered	ADJ
eurjchem-844	59	9	janumet	janumet	ADJ
eurjchem-844	59	10	®	®	NOUN
eurjchem-844	59	11	,	,	PUNCT
eurjchem-844	59	12	eucreas	eucrea	NOUN
eurjchem-844	59	13	®	®	NOUN
eurjchem-844	59	14	and	and	CCONJ
eurjchem-844	59	15	kombiglyze	kombiglyze	VERB
eurjchem-844	59	16	®	®	NOUN
eurjchem-844	59	17	tablets	tablet	NOUN
eurjchem-844	59	18	equivalent	equivalent	ADJ
eurjchem-844	59	19	to	to	ADP
eurjchem-844	59	20	(	(	PUNCT
eurjchem-844	59	21	64.25	64.25	NUM
eurjchem-844	59	22	mg	mg	NOUN
eurjchem-844	59	23	of	of	ADP
eurjchem-844	59	24	stg	stg	PROPN
eurjchem-844	59	25	and	and	CCONJ
eurjchem-844	59	26	1000	1000	NUM
eurjchem-844	59	27	mg	mg	NOUN
eurjchem-844	59	28	of	of	ADP
eurjchem-844	59	29	met	meet	VERB
eurjchem-844	59	30	)	)	PUNCT
eurjchem-844	59	31	,	,	PUNCT
eurjchem-844	59	32	(	(	PUNCT
eurjchem-844	59	33	equivalent	equivalent	ADJ
eurjchem-844	59	34	to	to	ADP
eurjchem-844	59	35	100	100	NUM
eurjchem-844	59	36	mg	mg	ADP
eurjchem-844	59	37	of	of	ADP
eurjchem-844	59	38	vdg	vdg	NOUN
eurjchem-844	59	39	and	and	CCONJ
eurjchem-844	59	40	1000	1000	NUM
eurjchem-844	59	41	mg	mg	NOUN
eurjchem-844	59	42	of	of	ADP
eurjchem-844	59	43	met	meet	VERB
eurjchem-844	59	44	)	)	PUNCT
eurjchem-844	59	45	and	and	CCONJ
eurjchem-844	59	46	(	(	PUNCT
eurjchem-844	59	47	equivalent	equivalent	ADJ
eurjchem-844	59	48	to	to	ADP
eurjchem-844	59	49	11.16	11.16	NUM
eurjchem-844	59	50	mg	mg	NOUN
eurjchem-844	59	51	of	of	ADP
eurjchem-844	59	52	sxg	sxg	NOUN
eurjchem-844	59	53	and	and	CCONJ
eurjchem-844	59	54	1000	1000	NUM
eurjchem-844	59	55	mg	mg	NOUN
eurjchem-844	59	56	of	of	ADP
eurjchem-844	59	57	met	meet	VERB
eurjchem-844	59	58	)	)	PUNCT
eurjchem-844	59	59	respectively	respectively	ADV
eurjchem-844	59	60	were	be	AUX
eurjchem-844	59	61	made	make	VERB
eurjchem-844	59	62	up	up	ADP
eurjchem-844	59	63	to	to	PART
eurjchem-844	59	64	100	100	NUM
eurjchem-844	59	65	ml	ml	NOUN
eurjchem-844	59	66	with	with	ADP
eurjchem-844	59	67	methanol	methanol	NOUN
eurjchem-844	59	68	.	.	PUNCT
eurjchem-844	60	1	the	the	DET
eurjchem-844	60	2	solutions	solution	NOUN
eurjchem-844	60	3	were	be	AUX
eurjchem-844	60	4	sonicated	sonicate	VERB
eurjchem-844	60	5	for	for	ADP
eurjchem-844	60	6	15	15	NUM
eurjchem-844	60	7	min	min	NOUN
eurjchem-844	60	8	and	and	CCONJ
eurjchem-844	60	9	filtered	filter	VERB
eurjchem-844	60	10	followed	follow	VERB
eurjchem-844	60	11	by	by	ADP
eurjchem-844	60	12	serial	serial	ADJ
eurjchem-844	60	13	dilution	dilution	NOUN
eurjchem-844	60	14	to	to	ADP
eurjchem-844	60	15	the	the	DET
eurjchem-844	60	16	required	require	VERB
eurjchem-844	60	17	concentrations	concentration	NOUN
eurjchem-844	60	18	for	for	ADP
eurjchem-844	60	19	each	each	DET
eurjchem-844	60	20	experiment	experiment	NOUN
eurjchem-844	60	21	.	.	PUNCT
eurjchem-844	61	1	2.5	2.5	NUM
eurjchem-844	61	2	.	.	PUNCT
eurjchem-844	61	3	procedure	procedure	NOUN
eurjchem-844	61	4	2.5.1	2.5.1	NUM
eurjchem-844	61	5	.	.	PUNCT
eurjchem-844	62	1	linearity	linearity	NOUN
eurjchem-844	62	2	and	and	CCONJ
eurjchem-844	62	3	repeatability	repeatability	NOUN
eurjchem-844	62	4	accurately	accurately	ADV
eurjchem-844	62	5	measured	measure	VERB
eurjchem-844	62	6	aliquots	aliquot	NOUN
eurjchem-844	62	7	of	of	ADP
eurjchem-844	62	8	working	work	VERB
eurjchem-844	62	9	standard	standard	ADJ
eurjchem-844	62	10	solutions	solution	NOUN
eurjchem-844	62	11	equivalent	equivalent	ADJ
eurjchem-844	62	12	to	to	ADP
eurjchem-844	62	13	50‐2000	50‐2000	NUM
eurjchem-844	62	14	µg	µg	NOUN
eurjchem-844	62	15	stg	stg	NOUN
eurjchem-844	62	16	,	,	PUNCT
eurjchem-844	62	17	50‐2000	50‐2000	NUM
eurjchem-844	62	18	µg	µg	PRON
eurjchem-844	62	19	vlg	vlg	PROPN
eurjchem-844	62	20	,	,	PUNCT
eurjchem-844	62	21	5.0‐	5.0‐	NUM
eurjchem-844	62	22	800	800	NUM
eurjchem-844	62	23	µg	µg	ADP
eurjchem-844	62	24	sxg	sxg	NOUN
eurjchem-844	62	25	and	and	CCONJ
eurjchem-844	62	26	0.2‐8.0	0.2‐8.0	PROPN
eurjchem-844	62	27	mg	mg	PROPN
eurjchem-844	62	28	met	meet	VERB
eurjchem-844	62	29	were	be	AUX
eurjchem-844	62	30	separately	separately	ADV
eurjchem-844	62	31	transferred	transfer	VERB
eurjchem-844	62	32	into	into	ADP
eurjchem-844	62	33	four	four	NUM
eurjchem-844	62	34	series	series	NOUN
eurjchem-844	62	35	of	of	ADP
eurjchem-844	62	36	10	10	NUM
eurjchem-844	62	37	ml	ml	NOUN
eurjchem-844	62	38	volumetric	volumetric	ADJ
eurjchem-844	62	39	flasks	flask	NOUN
eurjchem-844	62	40	and	and	CCONJ
eurjchem-844	62	41	then	then	ADV
eurjchem-844	62	42	completed	complete	VERB
eurjchem-844	62	43	to	to	PART
eurjchem-844	62	44	volume	volume	VERB
eurjchem-844	62	45	with	with	ADP
eurjchem-844	62	46	methanol	methanol	NOUN
eurjchem-844	62	47	.	.	PUNCT
eurjchem-844	63	1	a	a	DET
eurjchem-844	63	2	volume	volume	NOUN
eurjchem-844	63	3	of	of	ADP
eurjchem-844	63	4	25	25	NUM
eurjchem-844	63	5	µl	µl	NOUN
eurjchem-844	63	6	of	of	ADP
eurjchem-844	63	7	each	each	DET
eurjchem-844	63	8	solution	solution	NOUN
eurjchem-844	63	9	was	be	AUX
eurjchem-844	63	10	injected	inject	VERB
eurjchem-844	63	11	into	into	ADP
eurjchem-844	63	12	the	the	DET
eurjchem-844	63	13	chromatograph	chromatograph	NOUN
eurjchem-844	63	14	.	.	PUNCT
eurjchem-844	64	1	the	the	DET
eurjchem-844	64	2	chromatographic	chromatographic	ADJ
eurjchem-844	64	3	conditions	condition	NOUN
eurjchem-844	64	4	mentioned	mention	VERB
eurjchem-844	64	5	in	in	ADP
eurjchem-844	64	6	section	section	NOUN
eurjchem-844	64	7	2.3	2.3	NUM
eurjchem-844	64	8	including	include	VERB
eurjchem-844	64	9	the	the	DET
eurjchem-844	64	10	mobile	mobile	ADJ
eurjchem-844	64	11	phase	phase	NOUN
eurjchem-844	64	12	at	at	ADP
eurjchem-844	64	13	a	a	DET
eurjchem-844	64	14	flow	flow	NOUN
eurjchem-844	64	15	rate	rate	NOUN
eurjchem-844	64	16	1	1	NUM
eurjchem-844	64	17	ml	ml	NOUN
eurjchem-844	64	18	/	/	SYM
eurjchem-844	64	19	min	min	NOUN
eurjchem-844	64	20	,	,	PUNCT
eurjchem-844	64	21	detection	detection	NOUN
eurjchem-844	64	22	at	at	ADP
eurjchem-844	64	23	210	210	NUM
eurjchem-844	64	24	nm	nm	NOUN
eurjchem-844	64	25	and	and	CCONJ
eurjchem-844	64	26	run	run	VERB
eurjchem-844	64	27	time	time	NOUN
eurjchem-844	64	28	program	program	NOUN
eurjchem-844	64	29	for	for	ADP
eurjchem-844	64	30	10	10	NUM
eurjchem-844	64	31	min	min	NOUN
eurjchem-844	64	32	were	be	AUX
eurjchem-844	64	33	adjusted	adjust	VERB
eurjchem-844	64	34	.	.	PUNCT
eurjchem-844	65	1	the	the	DET
eurjchem-844	65	2	calibration	calibration	NOUN
eurjchem-844	65	3	curves	curve	NOUN
eurjchem-844	65	4	were	be	AUX
eurjchem-844	65	5	obtained	obtain	VERB
eurjchem-844	65	6	by	by	ADP
eurjchem-844	65	7	plotting	plot	VERB
eurjchem-844	65	8	area	area	NOUN
eurjchem-844	65	9	under	under	ADP
eurjchem-844	65	10	the	the	DET
eurjchem-844	65	11	peaks	peak	NOUN
eurjchem-844	65	12	(	(	PUNCT
eurjchem-844	65	13	aup	aup	PROPN
eurjchem-844	65	14	)	)	PUNCT
eurjchem-844	65	15	against	against	ADP
eurjchem-844	65	16	concentrations	concentration	NOUN
eurjchem-844	65	17	(	(	PUNCT
eurjchem-844	65	18	c	c	NOUN
eurjchem-844	65	19	)	)	PUNCT
eurjchem-844	65	20	.	.	PUNCT
eurjchem-844	66	1	the	the	DET
eurjchem-844	66	2	repeatability	repeatability	NOUN
eurjchem-844	66	3	of	of	ADP
eurjchem-844	66	4	the	the	DET
eurjchem-844	66	5	method	method	NOUN
eurjchem-844	66	6	was	be	AUX
eurjchem-844	66	7	assessed	assess	VERB
eurjchem-844	66	8	by	by	ADP
eurjchem-844	66	9	analyzing	analyze	VERB
eurjchem-844	66	10	a	a	DET
eurjchem-844	66	11	mixture	mixture	NOUN
eurjchem-844	66	12	containing	contain	VERB
eurjchem-844	66	13	32.1	32.1	NUM
eurjchem-844	66	14	μg	μg	NOUN
eurjchem-844	66	15	/	/	SYM
eurjchem-844	66	16	ml	ml	PROPN
eurjchem-844	66	17	of	of	ADP
eurjchem-844	66	18	stg	stg	NOUN
eurjchem-844	66	19	,	,	PUNCT
eurjchem-844	66	20	150	150	NUM
eurjchem-844	66	21	μg	μg	NOUN
eurjchem-844	66	22	/	/	SYM
eurjchem-844	66	23	ml	ml	PROPN
eurjchem-844	66	24	of	of	ADP
eurjchem-844	66	25	cgn	cgn	PROPN
eurjchem-844	66	26	and	and	CCONJ
eurjchem-844	66	27	500	500	NUM
eurjchem-844	66	28	μg	μg	NOUN
eurjchem-844	66	29	/	/	SYM
eurjchem-844	66	30	ml	ml	PROPN
eurjchem-844	66	31	of	of	ADP
eurjchem-844	66	32	met	meet	VERB
eurjchem-844	66	33	(	(	PUNCT
eurjchem-844	66	34	n	n	NOUN
eurjchem-844	66	35	=	=	SYM
eurjchem-844	66	36	6	6	NUM
eurjchem-844	66	37	)	)	PUNCT
eurjchem-844	66	38	.	.	PUNCT
eurjchem-844	67	1	the	the	DET
eurjchem-844	67	2	precision	precision	NOUN
eurjchem-844	67	3	(	(	PUNCT
eurjchem-844	67	4	%	%	INTJ
eurjchem-844	67	5	r.s.d	r.s.d	NOUN
eurjchem-844	67	6	.	.	PUNCT
eurjchem-844	67	7	)	)	PUNCT
eurjchem-844	67	8	was	be	AUX
eurjchem-844	67	9	calculated	calculate	VERB
eurjchem-844	67	10	(	(	PUNCT
eurjchem-844	67	11	table	table	NOUN
eurjchem-844	67	12	1	1	NUM
eurjchem-844	67	13	)	)	PUNCT
eurjchem-844	67	14	and	and	CCONJ
eurjchem-844	67	15	analyzing	analyze	VERB
eurjchem-844	67	16	a	a	DET
eurjchem-844	67	17	mixture	mixture	NOUN
eurjchem-844	67	18	containing	contain	VERB
eurjchem-844	67	19	50	50	NUM
eurjchem-844	67	20	μg	μg	NOUN
eurjchem-844	67	21	/	/	SYM
eurjchem-844	67	22	ml	ml	PROPN
eurjchem-844	67	23	of	of	ADP
eurjchem-844	67	24	vdg	vdg	NOUN
eurjchem-844	67	25	,	,	PUNCT
eurjchem-844	67	26	150	150	NUM
eurjchem-844	67	27	μg	μg	NOUN
eurjchem-844	67	28	/	/	SYM
eurjchem-844	67	29	ml	ml	PROPN
eurjchem-844	67	30	of	of	ADP
eurjchem-844	67	31	cgn	cgn	PROPN
eurjchem-844	67	32	and	and	CCONJ
eurjchem-844	67	33	500	500	NUM
eurjchem-844	67	34	μg	μg	NOUN
eurjchem-844	67	35	/	/	SYM
eurjchem-844	67	36	ml	ml	PROPN
eurjchem-844	67	37	of	of	ADP
eurjchem-844	67	38	met	meet	VERB
eurjchem-844	67	39	(	(	PUNCT
eurjchem-844	67	40	n	n	NOUN
eurjchem-844	67	41	=	=	SYM
eurjchem-844	67	42	6	6	NUM
eurjchem-844	67	43	)	)	PUNCT
eurjchem-844	67	44	.	.	PUNCT
eurjchem-844	68	1	the	the	DET
eurjchem-844	68	2	precision	precision	NOUN
eurjchem-844	68	3	(	(	PUNCT
eurjchem-844	68	4	%	%	INTJ
eurjchem-844	68	5	r.s.d	r.s.d	NOUN
eurjchem-844	68	6	.	.	PUNCT
eurjchem-844	68	7	)	)	PUNCT
eurjchem-844	68	8	was	be	AUX
eurjchem-844	68	9	calculated	calculate	VERB
eurjchem-844	68	10	(	(	PUNCT
eurjchem-844	68	11	table	table	NOUN
eurjchem-844	68	12	2	2	NUM
eurjchem-844	68	13	)	)	PUNCT
eurjchem-844	68	14	.	.	PUNCT
eurjchem-844	69	1	and	and	CCONJ
eurjchem-844	69	2	analyzing	analyze	VERB
eurjchem-844	69	3	a	a	DET
eurjchem-844	69	4	mixture	mixture	NOUN
eurjchem-844	69	5	containing	contain	VERB
eurjchem-844	69	6	5.6	5.6	NUM
eurjchem-844	69	7	μg	μg	NOUN
eurjchem-844	69	8	/	/	SYM
eurjchem-844	69	9	ml	ml	PROPN
eurjchem-844	69	10	of	of	ADP
eurjchem-844	69	11	sxg	sxg	NOUN
eurjchem-844	69	12	,	,	PUNCT
eurjchem-844	69	13	150	150	NUM
eurjchem-844	69	14	μg	μg	NOUN
eurjchem-844	69	15	/	/	SYM
eurjchem-844	69	16	ml	ml	PROPN
eurjchem-844	69	17	of	of	ADP
eurjchem-844	69	18	cgn	cgn	PROPN
eurjchem-844	69	19	and	and	CCONJ
eurjchem-844	69	20	500	500	NUM
eurjchem-844	69	21	µg	µg	NOUN
eurjchem-844	69	22	/	/	SYM
eurjchem-844	69	23	ml	ml	NOUN
eurjchem-844	69	24	of	of	ADP
eurjchem-844	69	25	met	meet	VERB
eurjchem-844	69	26	(	(	PUNCT
eurjchem-844	69	27	n	n	NOUN
eurjchem-844	69	28	=	=	SYM
eurjchem-844	69	29	6	6	NUM
eurjchem-844	69	30	)	)	PUNCT
eurjchem-844	69	31	.	.	PUNCT
eurjchem-844	70	1	the	the	DET
eurjchem-844	70	2	precision	precision	NOUN
eurjchem-844	70	3	(	(	PUNCT
eurjchem-844	70	4	%	%	INTJ
eurjchem-844	70	5	r.s.d	r.s.d	NOUN
eurjchem-844	70	6	.	.	PUNCT
eurjchem-844	70	7	)	)	PUNCT
eurjchem-844	70	8	was	be	AUX
eurjchem-844	70	9	calculated	calculate	VERB
eurjchem-844	70	10	(	(	PUNCT
eurjchem-844	70	11	table	table	NOUN
eurjchem-844	70	12	3	3	NUM
eurjchem-844	70	13	)	)	PUNCT
eurjchem-844	70	14	.	.	PUNCT
eurjchem-844	71	1	table	table	NOUN
eurjchem-844	71	2	1	1	NUM
eurjchem-844	71	3	.	.	PUNCT
eurjchem-844	72	1	system	system	NOUN
eurjchem-844	72	2	suitability	suitability	NOUN
eurjchem-844	72	3	tests	test	NOUN
eurjchem-844	72	4	of	of	ADP
eurjchem-844	72	5	the	the	DET
eurjchem-844	72	6	proposed	propose	VERB
eurjchem-844	72	7	lc	lc	NOUN
eurjchem-844	72	8	method	method	NOUN
eurjchem-844	72	9	for	for	ADP
eurjchem-844	72	10	the	the	DET
eurjchem-844	72	11	simultaneous	simultaneous	ADJ
eurjchem-844	72	12	determination	determination	NOUN
eurjchem-844	72	13	of	of	ADP
eurjchem-844	72	14	sitagliptin	sitagliptin	NOUN
eurjchem-844	72	15	,	,	PUNCT
eurjchem-844	72	16	metformin	metformin	NOUN
eurjchem-844	72	17	and	and	CCONJ
eurjchem-844	72	18	metformin	metformin	NOUN
eurjchem-844	72	19	degradation	degradation	NOUN
eurjchem-844	72	20	product	product	NOUN
eurjchem-844	72	21	.	.	PUNCT
eurjchem-844	73	1	item	item	NOUN
eurjchem-844	73	2	met	meet	VERB
eurjchem-844	73	3	degradation	degradation	NOUN
eurjchem-844	73	4	product	product	NOUN
eurjchem-844	73	5	stg	stg	PROPN
eurjchem-844	73	6	met	meet	VERB
eurjchem-844	73	7	n	n	PROPN
eurjchem-844	73	8	4096	4096	NUM
eurjchem-844	73	9	1984	1984	NUM
eurjchem-844	73	10	1296	1296	NUM
eurjchem-844	73	11	r	r	NOUN
eurjchem-844	73	12	4.8	4.8	NUM
eurjchem-844	73	13	4.1	4.1	NUM
eurjchem-844	73	14	4.1	4.1	NUM
eurjchem-844	73	15	t	t	NOUN
eurjchem-844	73	16	1.01	1.01	NUM
eurjchem-844	73	17	1.00	1.00	NUM
eurjchem-844	73	18	1.05	1.05	NUM
eurjchem-844	73	19	%	%	NOUN
eurjchem-844	73	20	r.s.d	r.s.d	NOUN
eurjchem-844	73	21	.	.	PUNCT
eurjchem-844	74	1	of	of	ADP
eurjchem-844	74	2	6	6	NUM
eurjchem-844	74	3	injections	injection	NOUN
eurjchem-844	74	4	peak	peak	NOUN
eurjchem-844	74	5	area	area	NOUN
eurjchem-844	74	6	0.62	0.62	NUM
eurjchem-844	74	7	0.23	0.23	NUM
eurjchem-844	74	8	0.54	0.54	NUM
eurjchem-844	74	9	retention	retention	NOUN
eurjchem-844	74	10	time	time	NOUN
eurjchem-844	74	11	0.82	0.82	NUM
eurjchem-844	74	12	0.19	0.19	NUM
eurjchem-844	74	13	0.33	0.33	NUM
eurjchem-844	74	14	*	*	PUNCT
eurjchem-844	74	15	n	n	CCONJ
eurjchem-844	74	16	:	:	PUNCT
eurjchem-844	74	17	number	number	NOUN
eurjchem-844	74	18	of	of	ADP
eurjchem-844	74	19	theoretical	theoretical	ADJ
eurjchem-844	74	20	plates	plate	NOUN
eurjchem-844	74	21	,	,	PUNCT
eurjchem-844	74	22	r	r	NOUN
eurjchem-844	74	23	:	:	PUNCT
eurjchem-844	74	24	peak	peak	NOUN
eurjchem-844	74	25	resolution	resolution	NOUN
eurjchem-844	74	26	factor	factor	NOUN
eurjchem-844	74	27	,	,	PUNCT
eurjchem-844	74	28	t	t	PROPN
eurjchem-844	74	29	:	:	PUNCT
eurjchem-844	74	30	ttailing	ttailing	NOUN
eurjchem-844	74	31	of	of	ADP
eurjchem-844	74	32	chromatographic	chromatographic	ADJ
eurjchem-844	74	33	peak	peak	NOUN
eurjchem-844	74	34	,	,	PUNCT
eurjchem-844	74	35	and	and	CCONJ
eurjchem-844	74	36	repeatability	repeatability	NOUN
eurjchem-844	74	37	as	as	ADP
eurjchem-844	74	38	percent	percent	NOUN
eurjchem-844	74	39	relative	relative	ADJ
eurjchem-844	74	40	standard	standard	ADJ
eurjchem-844	74	41	deviation	deviation	NOUN
eurjchem-844	74	42	%	%	NOUN
eurjchem-844	74	43	r.s.d	r.s.d	NOUN
eurjchem-844	74	44	.	.	PUNCT
eurjchem-844	75	1	of	of	ADP
eurjchem-844	75	2	peak	peak	NOUN
eurjchem-844	75	3	area	area	NOUN
eurjchem-844	75	4	for	for	ADP
eurjchem-844	75	5	six	six	NUM
eurjchem-844	75	6	injections	injection	NOUN
eurjchem-844	75	7	and	and	CCONJ
eurjchem-844	75	8	reproducibility	reproducibility	NOUN
eurjchem-844	75	9	of	of	ADP
eurjchem-844	75	10	retention	retention	NOUN
eurjchem-844	75	11	as	as	ADP
eurjchem-844	75	12	%	%	NOUN
eurjchem-844	75	13	r.s.d	r.s.d	NOUN
eurjchem-844	75	14	.	.	PUNCT
eurjchem-844	76	1	of	of	ADP
eurjchem-844	76	2	retention	retention	NOUN
eurjchem-844	76	3	time	time	NOUN
eurjchem-844	76	4	.	.	PUNCT
eurjchem-844	77	1	table	table	NOUN
eurjchem-844	77	2	2	2	NUM
eurjchem-844	77	3	.	.	X
eurjchem-844	77	4	system	system	NOUN
eurjchem-844	77	5	suitability	suitability	NOUN
eurjchem-844	77	6	tests	test	NOUN
eurjchem-844	77	7	of	of	ADP
eurjchem-844	77	8	the	the	DET
eurjchem-844	77	9	proposed	propose	VERB
eurjchem-844	77	10	lc	lc	NOUN
eurjchem-844	77	11	method	method	NOUN
eurjchem-844	77	12	for	for	ADP
eurjchem-844	77	13	the	the	DET
eurjchem-844	77	14	simultaneous	simultaneous	ADJ
eurjchem-844	77	15	determination	determination	NOUN
eurjchem-844	77	16	of	of	ADP
eurjchem-844	77	17	vildagliptin	vildagliptin	PROPN
eurjchem-844	77	18	,	,	PUNCT
eurjchem-844	77	19	metformin	metformin	NOUN
eurjchem-844	77	20	and	and	CCONJ
eurjchem-844	77	21	metformin	metformin	NOUN
eurjchem-844	77	22	degradation	degradation	NOUN
eurjchem-844	77	23	product	product	NOUN
eurjchem-844	77	24	.	.	PUNCT
eurjchem-844	78	1	item	item	NOUN
eurjchem-844	78	2	met	meet	VERB
eurjchem-844	78	3	degradation	degradation	NOUN
eurjchem-844	78	4	product	product	NOUN
eurjchem-844	78	5	vlg	vlg	PROPN
eurjchem-844	78	6	met	meet	VERB
eurjchem-844	78	7	n	n	PROPN
eurjchem-844	78	8	4096	4096	NUM
eurjchem-844	78	9	2175	2175	NUM
eurjchem-844	78	10	1296	1296	NUM
eurjchem-844	78	11	r	r	NOUN
eurjchem-844	78	12	6.7	6.7	NUM
eurjchem-844	78	13	2.5	2.5	NUM
eurjchem-844	78	14	2.5	2.5	NUM
eurjchem-844	78	15	t	t	NOUN
eurjchem-844	78	16	1.00	1.00	NUM
eurjchem-844	78	17	1.02	1.02	NUM
eurjchem-844	78	18	1.05	1.05	NUM
eurjchem-844	78	19	%	%	NOUN
eurjchem-844	78	20	r.s.d	r.s.d	NOUN
eurjchem-844	78	21	.	.	PUNCT
eurjchem-844	79	1	of	of	ADP
eurjchem-844	79	2	6	6	NUM
eurjchem-844	79	3	injections	injection	NOUN
eurjchem-844	79	4	peak	peak	NOUN
eurjchem-844	79	5	area	area	NOUN
eurjchem-844	79	6	0.55	0.55	NUM
eurjchem-844	79	7	0.72	0.72	NUM
eurjchem-844	79	8	0.44	0.44	NUM
eurjchem-844	79	9	retention	retention	NOUN
eurjchem-844	79	10	time	time	NOUN
eurjchem-844	79	11	0.49	0.49	NUM
eurjchem-844	79	12	0.11	0.11	NUM
eurjchem-844	79	13	0.25	0.25	NUM
eurjchem-844	79	14	*	*	PUNCT
eurjchem-844	79	15	n	n	CCONJ
eurjchem-844	79	16	:	:	PUNCT
eurjchem-844	79	17	number	number	NOUN
eurjchem-844	79	18	of	of	ADP
eurjchem-844	79	19	theoretical	theoretical	ADJ
eurjchem-844	79	20	plates	plate	NOUN
eurjchem-844	79	21	,	,	PUNCT
eurjchem-844	79	22	r	r	NOUN
eurjchem-844	79	23	:	:	PUNCT
eurjchem-844	79	24	peak	peak	NOUN
eurjchem-844	79	25	resolution	resolution	NOUN
eurjchem-844	79	26	factor	factor	NOUN
eurjchem-844	79	27	,	,	PUNCT
eurjchem-844	79	28	t	t	PROPN
eurjchem-844	79	29	:	:	PUNCT
eurjchem-844	79	30	tailing	tailing	NOUN
eurjchem-844	79	31	of	of	ADP
eurjchem-844	79	32	chromatographic	chromatographic	ADJ
eurjchem-844	79	33	peak	peak	NOUN
eurjchem-844	79	34	,	,	PUNCT
eurjchem-844	79	35	and	and	CCONJ
eurjchem-844	79	36	repeatability	repeatability	NOUN
eurjchem-844	79	37	as	as	ADP
eurjchem-844	79	38	%	%	NOUN
eurjchem-844	79	39	r.s.d	r.s.d	NOUN
eurjchem-844	79	40	.	.	PUNCT
eurjchem-844	80	1	of	of	ADP
eurjchem-844	80	2	peak	peak	NOUN
eurjchem-844	80	3	area	area	NOUN
eurjchem-844	80	4	for	for	ADP
eurjchem-844	80	5	six	six	NUM
eurjchem-844	80	6	injections	injection	NOUN
eurjchem-844	80	7	and	and	CCONJ
eurjchem-844	80	8	reproducibility	reproducibility	NOUN
eurjchem-844	80	9	of	of	ADP
eurjchem-844	80	10	retention	retention	NOUN
eurjchem-844	80	11	as	as	ADP
eurjchem-844	80	12	%	%	NOUN
eurjchem-844	80	13	r.s.d	r.s.d	NOUN
eurjchem-844	80	14	.	.	PUNCT
eurjchem-844	81	1	of	of	ADP
eurjchem-844	81	2	retention	retention	NOUN
eurjchem-844	81	3	time	time	NOUN
eurjchem-844	81	4	.	.	PUNCT
eurjchem-844	82	1	table	table	NOUN
eurjchem-844	82	2	3	3	NUM
eurjchem-844	82	3	.	.	X
eurjchem-844	82	4	system	system	NOUN
eurjchem-844	82	5	suitability	suitability	NOUN
eurjchem-844	82	6	tests	test	NOUN
eurjchem-844	82	7	of	of	ADP
eurjchem-844	82	8	the	the	DET
eurjchem-844	82	9	proposed	propose	VERB
eurjchem-844	82	10	lc	lc	NOUN
eurjchem-844	82	11	method	method	NOUN
eurjchem-844	82	12	for	for	ADP
eurjchem-844	82	13	the	the	DET
eurjchem-844	82	14	simultaneous	simultaneous	ADJ
eurjchem-844	82	15	determination	determination	NOUN
eurjchem-844	82	16	of	of	ADP
eurjchem-844	82	17	saxagliptin	saxagliptin	PROPN
eurjchem-844	82	18	,	,	PUNCT
eurjchem-844	82	19	metformin	metformin	NOUN
eurjchem-844	82	20	and	and	CCONJ
eurjchem-844	82	21	metformin	metformin	NOUN
eurjchem-844	82	22	degradation	degradation	NOUN
eurjchem-844	82	23	product	product	NOUN
eurjchem-844	82	24	.	.	PUNCT
eurjchem-844	83	1	item	item	NOUN
eurjchem-844	83	2	met	meet	VERB
eurjchem-844	83	3	degradation	degradation	NOUN
eurjchem-844	83	4	product	product	NOUN
eurjchem-844	83	5	sxg	sxg	NOUN
eurjchem-844	83	6	met	meet	VERB
eurjchem-844	83	7	n	n	DET
eurjchem-844	83	8	4096	4096	NUM
eurjchem-844	83	9	2704	2704	NUM
eurjchem-844	83	10	1296	1296	NUM
eurjchem-844	83	11	r	r	NOUN
eurjchem-844	83	12	5.3	5.3	NUM
eurjchem-844	83	13	3.2	3.2	NUM
eurjchem-844	83	14	3.2	3.2	NUM
eurjchem-844	83	15	t	t	NOUN
eurjchem-844	83	16	1.00	1.00	NUM
eurjchem-844	83	17	1.04	1.04	NUM
eurjchem-844	83	18	1.05	1.05	NUM
eurjchem-844	83	19	%	%	NOUN
eurjchem-844	83	20	r.s.d	r.s.d	NOUN
eurjchem-844	83	21	.	.	PUNCT
eurjchem-844	84	1	of	of	ADP
eurjchem-844	84	2	6	6	NUM
eurjchem-844	84	3	injections	injection	NOUN
eurjchem-844	84	4	peak	peak	NOUN
eurjchem-844	84	5	area	area	NOUN
eurjchem-844	84	6	0.48	0.48	NUM
eurjchem-844	84	7	0.51	0.51	NUM
eurjchem-844	84	8	0.88	0.88	NUM
eurjchem-844	84	9	retention	retention	NOUN
eurjchem-844	84	10	time	time	NOUN
eurjchem-844	84	11	0.76	0.76	NUM
eurjchem-844	84	12	0.27	0.27	NUM
eurjchem-844	84	13	0.38	0.38	NUM
eurjchem-844	84	14	*	*	PUNCT
eurjchem-844	84	15	n	n	CCONJ
eurjchem-844	84	16	:	:	PUNCT
eurjchem-844	84	17	number	number	NOUN
eurjchem-844	84	18	of	of	ADP
eurjchem-844	84	19	theoretical	theoretical	ADJ
eurjchem-844	84	20	plates	plate	NOUN
eurjchem-844	84	21	,	,	PUNCT
eurjchem-844	84	22	r	r	NOUN
eurjchem-844	84	23	:	:	PUNCT
eurjchem-844	84	24	peak	peak	NOUN
eurjchem-844	84	25	resolution	resolution	NOUN
eurjchem-844	84	26	factor	factor	NOUN
eurjchem-844	84	27	,	,	PUNCT
eurjchem-844	84	28	t	t	PROPN
eurjchem-844	84	29	:	:	PUNCT
eurjchem-844	84	30	tailing	tailing	NOUN
eurjchem-844	84	31	of	of	ADP
eurjchem-844	84	32	chromatographic	chromatographic	ADJ
eurjchem-844	84	33	peak	peak	NOUN
eurjchem-844	84	34	,	,	PUNCT
eurjchem-844	84	35	and	and	CCONJ
eurjchem-844	84	36	repeatability	repeatability	NOUN
eurjchem-844	84	37	as	as	ADP
eurjchem-844	84	38	%	%	NOUN
eurjchem-844	84	39	r.s.d	r.s.d	NOUN
eurjchem-844	84	40	.	.	PUNCT
eurjchem-844	85	1	of	of	ADP
eurjchem-844	85	2	peak	peak	NOUN
eurjchem-844	85	3	area	area	NOUN
eurjchem-844	85	4	for	for	ADP
eurjchem-844	85	5	six	six	NUM
eurjchem-844	85	6	injections	injection	NOUN
eurjchem-844	85	7	and	and	CCONJ
eurjchem-844	85	8	reproducibility	reproducibility	NOUN
eurjchem-844	85	9	of	of	ADP
eurjchem-844	85	10	retention	retention	NOUN
eurjchem-844	85	11	as	as	ADP
eurjchem-844	85	12	%	%	NOUN
eurjchem-844	85	13	r.s.d	r.s.d	NOUN
eurjchem-844	85	14	.	.	PUNCT
eurjchem-844	86	1	of	of	ADP
eurjchem-844	86	2	retention	retention	NOUN
eurjchem-844	86	3	time	time	NOUN
eurjchem-844	86	4	.	.	PUNCT
eurjchem-844	87	1	2.5.2	2.5.2	X
eurjchem-844	87	2	.	.	PUNCT
eurjchem-844	88	1	assay	assay	NOUN
eurjchem-844	88	2	of	of	ADP
eurjchem-844	88	3	drugs	drug	NOUN
eurjchem-844	88	4	in	in	ADP
eurjchem-844	88	5	laboratory	laboratory	NOUN
eurjchem-844	88	6	prepared	prepare	VERB
eurjchem-844	88	7	mixtures	mixture	NOUN
eurjchem-844	88	8	and	and	CCONJ
eurjchem-844	88	9	in	in	ADP
eurjchem-844	88	10	pharmaceutical	pharmaceutical	ADJ
eurjchem-844	88	11	dosage	dosage	NOUN
eurjchem-844	88	12	forms	form	VERB
eurjchem-844	88	13	the	the	DET
eurjchem-844	88	14	procedure	procedure	NOUN
eurjchem-844	88	15	mentioned	mention	VERB
eurjchem-844	88	16	in	in	ADP
eurjchem-844	88	17	section	section	NOUN
eurjchem-844	88	18	2.5.1	2.5.1	NUM
eurjchem-844	88	19	was	be	AUX
eurjchem-844	88	20	repeated	repeat	VERB
eurjchem-844	88	21	using	use	VERB
eurjchem-844	88	22	three	three	NUM
eurjchem-844	88	23	sets	set	NOUN
eurjchem-844	88	24	of	of	ADP
eurjchem-844	88	25	laboratory	laboratory	NOUN
eurjchem-844	88	26	prepared	prepare	VERB
eurjchem-844	88	27	mixtures	mixture	NOUN
eurjchem-844	88	28	equivalent	equivalent	ADJ
eurjchem-844	88	29	to	to	ADP
eurjchem-844	88	30	either	either	DET
eurjchem-844	88	31	13‐48	13‐48	NUM
eurjchem-844	88	32	μg	μg	PROPN
eurjchem-844	88	33	/	/	SYM
eurjchem-844	88	34	ml	ml	PROPN
eurjchem-844	88	35	stg	stg	PROPN
eurjchem-844	88	36	,	,	PUNCT
eurjchem-844	88	37	20‐75	20‐75	NUM
eurjchem-844	88	38	μg	μg	PROPN
eurjchem-844	88	39	/	/	SYM
eurjchem-844	88	40	ml	ml	ADP
eurjchem-844	88	41	vlg	vlg	NOUN
eurjchem-844	88	42	or	or	CCONJ
eurjchem-844	88	43	2.0‐8.5	2.0‐8.5	NUM
eurjchem-844	88	44	μg	μg	PROPN
eurjchem-844	88	45	/	/	SYM
eurjchem-844	88	46	ml	ml	PROPN
eurjchem-844	88	47	446	446	NUM
eurjchem-844	88	48	el‐bagary	el‐bagary	ADJ
eurjchem-844	88	49	et	et	PROPN
eurjchem-844	88	50	al	al	PROPN
eurjchem-844	88	51	.	.	PUNCT
eurjchem-844	88	52	/	/	SYM
eurjchem-844	88	53	european	european	PROPN
eurjchem-844	88	54	journal	journal	PROPN
eurjchem-844	88	55	of	of	ADP
eurjchem-844	88	56	chemistry	chemistry	NOUN
eurjchem-844	88	57	4	4	NUM
eurjchem-844	88	58	(	(	PUNCT
eurjchem-844	88	59	4	4	NUM
eurjchem-844	88	60	)	)	PUNCT
eurjchem-844	88	61	(	(	PUNCT
eurjchem-844	88	62	2013	2013	NUM
eurjchem-844	88	63	)	)	PUNCT
eurjchem-844	88	64	444‐449	444‐449	PROPN
eurjchem-844	88	65	sxg	sxg	NOUN
eurjchem-844	88	66	and	and	CCONJ
eurjchem-844	88	67	200‐750	200‐750	NUM
eurjchem-844	88	68	μg	μg	NOUN
eurjchem-844	88	69	/	/	SYM
eurjchem-844	88	70	ml	ml	VERB
eurjchem-844	88	71	met	meet	VERB
eurjchem-844	88	72	.	.	PUNCT
eurjchem-844	89	1	for	for	ADP
eurjchem-844	89	2	the	the	DET
eurjchem-844	89	3	determination	determination	NOUN
eurjchem-844	89	4	of	of	ADP
eurjchem-844	89	5	the	the	DET
eurjchem-844	89	6	examined	examine	VERB
eurjchem-844	89	7	drugs	drug	NOUN
eurjchem-844	89	8	in	in	ADP
eurjchem-844	89	9	tablets	tablet	NOUN
eurjchem-844	89	10	,	,	PUNCT
eurjchem-844	89	11	the	the	DET
eurjchem-844	89	12	sample	sample	NOUN
eurjchem-844	89	13	solutions	solution	NOUN
eurjchem-844	89	14	prepared	prepare	VERB
eurjchem-844	89	15	under	under	ADP
eurjchem-844	89	16	section	section	NOUN
eurjchem-844	89	17	2.4	2.4	NUM
eurjchem-844	89	18	were	be	AUX
eurjchem-844	89	19	serially	serially	ADV
eurjchem-844	89	20	diluted	dilute	VERB
eurjchem-844	89	21	to	to	PART
eurjchem-844	89	22	prepare	prepare	VERB
eurjchem-844	89	23	solutions	solution	NOUN
eurjchem-844	89	24	equivalent	equivalent	ADJ
eurjchem-844	89	25	to	to	ADP
eurjchem-844	89	26	6.5‐32.0	6.5‐32.0	NUM
eurjchem-844	89	27	and	and	CCONJ
eurjchem-844	89	28	100‐500	100‐500	NUM
eurjchem-844	89	29	μg	μg	NOUN
eurjchem-844	89	30	/	/	SYM
eurjchem-844	89	31	ml	ml	PROPN
eurjchem-844	89	32	of	of	ADP
eurjchem-844	89	33	stg	stg	PROPN
eurjchem-844	89	34	and	and	CCONJ
eurjchem-844	89	35	met	meet	VERB
eurjchem-844	89	36	,	,	PUNCT
eurjchem-844	89	37	respectively	respectively	ADV
eurjchem-844	89	38	;	;	PUNCT
eurjchem-844	89	39	and	and	CCONJ
eurjchem-844	89	40	equivalent	equivalent	ADJ
eurjchem-844	89	41	to	to	ADP
eurjchem-844	89	42	10‐50	10‐50	NUM
eurjchem-844	89	43	and	and	CCONJ
eurjchem-844	89	44	100‐500	100‐500	NUM
eurjchem-844	89	45	μg	μg	NOUN
eurjchem-844	89	46	/	/	SYM
eurjchem-844	89	47	ml	ml	PROPN
eurjchem-844	89	48	of	of	ADP
eurjchem-844	89	49	vld	vld	PROPN
eurjchem-844	89	50	and	and	CCONJ
eurjchem-844	89	51	met	meet	VERB
eurjchem-844	89	52	,	,	PUNCT
eurjchem-844	89	53	respectively	respectively	ADV
eurjchem-844	89	54	;	;	PUNCT
eurjchem-844	89	55	and	and	CCONJ
eurjchem-844	89	56	equivalent	equivalent	ADJ
eurjchem-844	89	57	to	to	ADP
eurjchem-844	89	58	1.0‐5.5	1.0‐5.5	NUM
eurjchem-844	89	59	and	and	CCONJ
eurjchem-844	89	60	100‐	100‐	NUM
eurjchem-844	89	61	500	500	NUM
eurjchem-844	89	62	μg	μg	NOUN
eurjchem-844	89	63	/	/	SYM
eurjchem-844	89	64	ml	ml	PROPN
eurjchem-844	89	65	of	of	ADP
eurjchem-844	89	66	sxg	sxg	NOUN
eurjchem-844	89	67	and	and	CCONJ
eurjchem-844	89	68	met	meet	VERB
eurjchem-844	89	69	,	,	PUNCT
eurjchem-844	89	70	respectively	respectively	ADV
eurjchem-844	89	71	;	;	PUNCT
eurjchem-844	89	72	and	and	CCONJ
eurjchem-844	89	73	then	then	ADV
eurjchem-844	89	74	injected	inject	VERB
eurjchem-844	89	75	in	in	ADP
eurjchem-844	89	76	triplicates	triplicate	NOUN
eurjchem-844	89	77	.	.	PUNCT
eurjchem-844	90	1	the	the	DET
eurjchem-844	90	2	concentrations	concentration	NOUN
eurjchem-844	90	3	of	of	ADP
eurjchem-844	90	4	the	the	DET
eurjchem-844	90	5	examined	examine	VERB
eurjchem-844	90	6	drugs	drug	NOUN
eurjchem-844	90	7	were	be	AUX
eurjchem-844	90	8	calculated	calculate	VERB
eurjchem-844	90	9	by	by	ADP
eurjchem-844	90	10	the	the	DET
eurjchem-844	90	11	corresponding	correspond	VERB
eurjchem-844	90	12	calibration	calibration	NOUN
eurjchem-844	90	13	equations	equation	NOUN
eurjchem-844	90	14	.	.	PUNCT
eurjchem-844	91	1	3	3	X
eurjchem-844	91	2	.	.	NOUN
eurjchem-844	91	3	results	result	NOUN
eurjchem-844	91	4	and	and	CCONJ
eurjchem-844	91	5	discussion	discussion	NOUN
eurjchem-844	91	6	hplc	hplc	NOUN
eurjchem-844	91	7	greatly	greatly	ADV
eurjchem-844	91	8	reduces	reduce	VERB
eurjchem-844	91	9	the	the	DET
eurjchem-844	91	10	analysis	analysis	NOUN
eurjchem-844	91	11	time	time	NOUN
eurjchem-844	91	12	and	and	CCONJ
eurjchem-844	91	13	allows	allow	VERB
eurjchem-844	91	14	for	for	ADP
eurjchem-844	91	15	the	the	DET
eurjchem-844	91	16	determination	determination	NOUN
eurjchem-844	91	17	of	of	ADP
eurjchem-844	91	18	many	many	ADJ
eurjchem-844	91	19	individual	individual	ADJ
eurjchem-844	91	20	components	component	NOUN
eurjchem-844	91	21	in	in	ADP
eurjchem-844	91	22	a	a	DET
eurjchem-844	91	23	mixture	mixture	NOUN
eurjchem-844	91	24	using	use	VERB
eurjchem-844	91	25	one	one	NUM
eurjchem-844	91	26	single	single	ADJ
eurjchem-844	91	27	procedure	procedure	NOUN
eurjchem-844	91	28	[	[	X
eurjchem-844	91	29	17	17	NUM
eurjchem-844	91	30	]	]	PUNCT
eurjchem-844	91	31	.	.	PUNCT
eurjchem-844	92	1	no	no	DET
eurjchem-844	92	2	previous	previous	ADJ
eurjchem-844	92	3	method	method	NOUN
eurjchem-844	92	4	was	be	AUX
eurjchem-844	92	5	reported	report	VERB
eurjchem-844	92	6	for	for	ADP
eurjchem-844	92	7	the	the	DET
eurjchem-844	92	8	lc	lc	NOUN
eurjchem-844	92	9	determination	determination	NOUN
eurjchem-844	92	10	of	of	ADP
eurjchem-844	92	11	either	either	DET
eurjchem-844	92	12	stg	stg	PROPN
eurjchem-844	92	13	,	,	PUNCT
eurjchem-844	92	14	vdg	vdg	NOUN
eurjchem-844	92	15	or	or	CCONJ
eurjchem-844	92	16	sxg	sxg	NOUN
eurjchem-844	92	17	in	in	ADP
eurjchem-844	92	18	their	their	PRON
eurjchem-844	92	19	ternary	ternary	ADJ
eurjchem-844	92	20	mixture	mixture	NOUN
eurjchem-844	92	21	with	with	ADP
eurjchem-844	92	22	met	meet	VERB
eurjchem-844	92	23	and	and	CCONJ
eurjchem-844	92	24	cgn	cgn	PROPN
eurjchem-844	92	25	.	.	PUNCT
eurjchem-844	93	1	cgn	cgn	PROPN
eurjchem-844	93	2	is	be	AUX
eurjchem-844	93	3	a	a	DET
eurjchem-844	93	4	known	know	VERB
eurjchem-844	93	5	impurity	impurity	NOUN
eurjchem-844	93	6	with	with	ADP
eurjchem-844	93	7	a	a	DET
eurjchem-844	93	8	limit	limit	NOUN
eurjchem-844	93	9	of	of	ADP
eurjchem-844	93	10	not	not	PART
eurjchem-844	93	11	more	more	ADJ
eurjchem-844	93	12	than	than	ADP
eurjchem-844	93	13	0.02	0.02	NUM
eurjchem-844	93	14	%	%	NOUN
eurjchem-844	93	15	,	,	PUNCT
eurjchem-844	93	16	it	it	PRON
eurjchem-844	93	17	is	be	AUX
eurjchem-844	93	18	also	also	ADV
eurjchem-844	93	19	called	call	VERB
eurjchem-844	93	20	dicyandiamide	dicyandiamide	ADV
eurjchem-844	93	21	,	,	PUNCT
eurjchem-844	93	22	is	be	AUX
eurjchem-844	93	23	the	the	DET
eurjchem-844	93	24	dimer	dimer	NOUN
eurjchem-844	93	25	of	of	ADP
eurjchem-844	93	26	cyanamide	cyanamide	NOUN
eurjchem-844	93	27	.	.	PUNCT
eurjchem-844	94	1	efficient	efficient	ADJ
eurjchem-844	94	2	control	control	NOUN
eurjchem-844	94	3	of	of	ADP
eurjchem-844	94	4	these	these	DET
eurjchem-844	94	5	unwanted	unwanted	ADJ
eurjchem-844	94	6	compounds	compound	NOUN
eurjchem-844	94	7	in	in	ADP
eurjchem-844	94	8	a	a	DET
eurjchem-844	94	9	formulation	formulation	NOUN
eurjchem-844	94	10	is	be	AUX
eurjchem-844	94	11	necessary	necessary	ADJ
eurjchem-844	94	12	[	[	X
eurjchem-844	94	13	15	15	NUM
eurjchem-844	94	14	]	]	SYM
eurjchem-844	94	15	.	.	PUNCT
eurjchem-844	95	1	3.1	3.1	NUM
eurjchem-844	95	2	.	.	PUNCT
eurjchem-844	95	3	method	method	PROPN
eurjchem-844	95	4	development	development	PROPN
eurjchem-844	95	5	different	different	ADJ
eurjchem-844	95	6	chromatographic	chromatographic	ADJ
eurjchem-844	95	7	systems	system	NOUN
eurjchem-844	95	8	including	include	VERB
eurjchem-844	95	9	different	different	ADJ
eurjchem-844	95	10	c18	c18	NOUN
eurjchem-844	95	11	columns	column	NOUN
eurjchem-844	95	12	and	and	CCONJ
eurjchem-844	95	13	different	different	ADJ
eurjchem-844	95	14	mobile	mobile	ADJ
eurjchem-844	95	15	phases	phase	NOUN
eurjchem-844	95	16	at	at	ADP
eurjchem-844	95	17	different	different	ADJ
eurjchem-844	95	18	ph	ph	ADJ
eurjchem-844	95	19	values	value	NOUN
eurjchem-844	95	20	were	be	AUX
eurjchem-844	95	21	attempted	attempt	VERB
eurjchem-844	95	22	.	.	PUNCT
eurjchem-844	96	1	unfortunately	unfortunately	ADV
eurjchem-844	96	2	,	,	PUNCT
eurjchem-844	96	3	simultaneous	simultaneous	ADJ
eurjchem-844	96	4	elution	elution	NOUN
eurjchem-844	96	5	of	of	ADP
eurjchem-844	96	6	the	the	DET
eurjchem-844	96	7	ternary	ternary	ADJ
eurjchem-844	96	8	mixtures	mixture	NOUN
eurjchem-844	96	9	at	at	ADP
eurjchem-844	96	10	reasonable	reasonable	ADJ
eurjchem-844	96	11	time	time	NOUN
eurjchem-844	96	12	could	could	AUX
eurjchem-844	96	13	not	not	PART
eurjchem-844	96	14	be	be	AUX
eurjchem-844	96	15	achieved	achieve	VERB
eurjchem-844	96	16	.	.	PUNCT
eurjchem-844	97	1	recently	recently	ADV
eurjchem-844	97	2	,	,	PUNCT
eurjchem-844	97	3	cyano	cyano	NOUN
eurjchem-844	97	4	columns	column	NOUN
eurjchem-844	97	5	have	have	AUX
eurjchem-844	97	6	been	be	AUX
eurjchem-844	97	7	used	use	VERB
eurjchem-844	97	8	for	for	ADP
eurjchem-844	97	9	the	the	DET
eurjchem-844	97	10	separation	separation	NOUN
eurjchem-844	97	11	and	and	CCONJ
eurjchem-844	97	12	quantitation	quantitation	NOUN
eurjchem-844	97	13	of	of	ADP
eurjchem-844	97	14	drugs	drug	NOUN
eurjchem-844	97	15	[	[	X
eurjchem-844	97	16	18‐21	18‐21	NUM
eurjchem-844	97	17	]	]	PUNCT
eurjchem-844	97	18	.	.	PUNCT
eurjchem-844	98	1	using	use	VERB
eurjchem-844	98	2	a	a	DET
eurjchem-844	98	3	mobile	mobile	ADJ
eurjchem-844	98	4	phase	phase	NOUN
eurjchem-844	98	5	of	of	ADP
eurjchem-844	98	6	acidic	acidic	ADJ
eurjchem-844	98	7	ph	ph	NOUN
eurjchem-844	98	8	value	value	NOUN
eurjchem-844	98	9	,	,	PUNCT
eurjchem-844	98	10	c18	c18	NOUN
eurjchem-844	98	11	column	column	NOUN
eurjchem-844	98	12	was	be	AUX
eurjchem-844	98	13	consequently	consequently	ADV
eurjchem-844	98	14	replaced	replace	VERB
eurjchem-844	98	15	with	with	ADP
eurjchem-844	98	16	a	a	DET
eurjchem-844	98	17	cyano	cyano	NOUN
eurjchem-844	98	18	column	column	NOUN
eurjchem-844	98	19	in	in	ADP
eurjchem-844	98	20	order	order	NOUN
eurjchem-844	98	21	to	to	PART
eurjchem-844	98	22	separate	separate	VERB
eurjchem-844	98	23	mixture	mixture	NOUN
eurjchem-844	98	24	components	component	NOUN
eurjchem-844	98	25	.	.	PUNCT
eurjchem-844	99	1	for	for	ADP
eurjchem-844	99	2	the	the	DET
eurjchem-844	99	3	cyano‐bonded	cyano‐bonde	VERB
eurjchem-844	99	4	phase	phase	NOUN
eurjchem-844	99	5	column	column	NOUN
eurjchem-844	99	6	,	,	PUNCT
eurjchem-844	99	7	the	the	DET
eurjchem-844	99	8	weak	weak	ADJ
eurjchem-844	99	9	polar	polar	ADJ
eurjchem-844	99	10	cyano	cyano	NOUN
eurjchem-844	99	11	groups	group	NOUN
eurjchem-844	99	12	,	,	PUNCT
eurjchem-844	99	13	together	together	ADV
eurjchem-844	99	14	with	with	ADP
eurjchem-844	99	15	the	the	DET
eurjchem-844	99	16	short	short	ADJ
eurjchem-844	99	17	hydrocarbon	hydrocarbon	NOUN
eurjchem-844	99	18	chains	chain	NOUN
eurjchem-844	99	19	allow	allow	VERB
eurjchem-844	99	20	a	a	DET
eurjchem-844	99	21	mixed	mixed	ADJ
eurjchem-844	99	22	mechanism	mechanism	NOUN
eurjchem-844	99	23	of	of	ADP
eurjchem-844	99	24	separation	separation	NOUN
eurjchem-844	99	25	[	[	X
eurjchem-844	99	26	22	22	NUM
eurjchem-844	99	27	]	]	PUNCT
eurjchem-844	99	28	,	,	PUNCT
eurjchem-844	99	29	and	and	CCONJ
eurjchem-844	99	30	hence	hence	ADV
eurjchem-844	99	31	give	give	VERB
eurjchem-844	99	32	reasonable	reasonable	ADJ
eurjchem-844	99	33	retention	retention	NOUN
eurjchem-844	99	34	times	time	NOUN
eurjchem-844	99	35	for	for	ADP
eurjchem-844	99	36	the	the	DET
eurjchem-844	99	37	three	three	NUM
eurjchem-844	99	38	components	component	NOUN
eurjchem-844	99	39	under	under	ADP
eurjchem-844	99	40	investigation	investigation	NOUN
eurjchem-844	99	41	in	in	ADP
eurjchem-844	99	42	every	every	DET
eurjchem-844	99	43	mixture	mixture	NOUN
eurjchem-844	99	44	when	when	SCONJ
eurjchem-844	99	45	operating	operate	VERB
eurjchem-844	99	46	under	under	ADP
eurjchem-844	99	47	optimum	optimum	ADJ
eurjchem-844	99	48	conditions	condition	NOUN
eurjchem-844	99	49	.	.	PUNCT
eurjchem-844	100	1	isocratic	isocratic	ADJ
eurjchem-844	100	2	elution	elution	NOUN
eurjchem-844	100	3	based	base	VERB
eurjchem-844	100	4	on	on	ADP
eurjchem-844	100	5	potassium	potassium	NOUN
eurjchem-844	100	6	dihydrogen	dihydrogen	NOUN
eurjchem-844	100	7	phosphate	phosphate	NOUN
eurjchem-844	100	8	buffer	buffer	NOUN
eurjchem-844	100	9	(	(	PUNCT
eurjchem-844	100	10	ph	ph	NOUN
eurjchem-844	100	11	=	=	NOUN
eurjchem-844	100	12	4.6	4.6	NUM
eurjchem-844	100	13	)	)	PUNCT
eurjchem-844	100	14	‐	‐	ADJ
eurjchem-844	100	15	acetonitrile	acetonitrile	NOUN
eurjchem-844	100	16	(	(	PUNCT
eurjchem-844	100	17	30:70	30:70	NUM
eurjchem-844	100	18	,	,	PUNCT
eurjchem-844	100	19	v	v	NOUN
eurjchem-844	100	20	:	:	SYM
eurjchem-844	100	21	v	v	NOUN
eurjchem-844	100	22	)	)	PUNCT
eurjchem-844	100	23	was	be	AUX
eurjchem-844	100	24	applied	apply	VERB
eurjchem-844	100	25	.	.	PUNCT
eurjchem-844	101	1	minimum	minimum	ADJ
eurjchem-844	101	2	retention	retention	NOUN
eurjchem-844	101	3	times	time	NOUN
eurjchem-844	101	4	were	be	AUX
eurjchem-844	101	5	obtained	obtain	VERB
eurjchem-844	101	6	at	at	ADP
eurjchem-844	101	7	a	a	DET
eurjchem-844	101	8	flow	flow	NOUN
eurjchem-844	101	9	rate	rate	NOUN
eurjchem-844	101	10	1	1	NUM
eurjchem-844	101	11	ml	ml	NOUN
eurjchem-844	101	12	/	/	SYM
eurjchem-844	101	13	min	min	NOUN
eurjchem-844	101	14	.	.	PUNCT
eurjchem-844	102	1	the	the	DET
eurjchem-844	102	2	uv	uv	NOUN
eurjchem-844	102	3	detector	detector	NOUN
eurjchem-844	102	4	was	be	AUX
eurjchem-844	102	5	operated	operate	VERB
eurjchem-844	102	6	at	at	ADP
eurjchem-844	102	7	210	210	NUM
eurjchem-844	102	8	nm	nm	NOUN
eurjchem-844	102	9	where	where	SCONJ
eurjchem-844	102	10	good	good	ADJ
eurjchem-844	102	11	detector	detector	NOUN
eurjchem-844	102	12	sensitivity	sensitivity	NOUN
eurjchem-844	102	13	was	be	AUX
eurjchem-844	102	14	achieved	achieve	VERB
eurjchem-844	102	15	for	for	ADP
eurjchem-844	102	16	all	all	DET
eurjchem-844	102	17	the	the	DET
eurjchem-844	102	18	examined	examine	VERB
eurjchem-844	102	19	drugs	drug	NOUN
eurjchem-844	102	20	.	.	PUNCT
eurjchem-844	103	1	the	the	DET
eurjchem-844	103	2	retention	retention	NOUN
eurjchem-844	103	3	times	time	NOUN
eurjchem-844	103	4	were	be	AUX
eurjchem-844	103	5	6.0	6.0	NUM
eurjchem-844	103	6	,	,	PUNCT
eurjchem-844	103	7	7.1	7.1	NUM
eurjchem-844	103	8	,	,	PUNCT
eurjchem-844	103	9	6.5	6.5	NUM
eurjchem-844	103	10	,	,	PUNCT
eurjchem-844	103	11	9.1	9.1	NUM
eurjchem-844	103	12	and	and	CCONJ
eurjchem-844	103	13	4.1	4.1	NUM
eurjchem-844	103	14	min	min	NOUN
eurjchem-844	103	15	for	for	ADP
eurjchem-844	103	16	stg	stg	PROPN
eurjchem-844	103	17	,	,	PUNCT
eurjchem-844	103	18	vld	vld	PROPN
eurjchem-844	103	19	,	,	PUNCT
eurjchem-844	103	20	sxg	sxg	NOUN
eurjchem-844	103	21	,	,	PUNCT
eurjchem-844	103	22	met	meet	VERB
eurjchem-844	103	23	and	and	CCONJ
eurjchem-844	103	24	cgn	cgn	PROPN
eurjchem-844	103	25	,	,	PUNCT
eurjchem-844	103	26	respectively	respectively	ADV
eurjchem-844	103	27	;	;	PUNCT
eurjchem-844	103	28	as	as	SCONJ
eurjchem-844	103	29	presented	present	VERB
eurjchem-844	103	30	in	in	ADP
eurjchem-844	103	31	figure	figure	NOUN
eurjchem-844	103	32	2‐	2‐	NUM
eurjchem-844	103	33	7	7	NUM
eurjchem-844	103	34	.	.	PUNCT
eurjchem-844	103	35	figure	figure	NOUN
eurjchem-844	103	36	2	2	NUM
eurjchem-844	103	37	.	.	PUNCT
eurjchem-844	104	1	a	a	DET
eurjchem-844	104	2	typical	typical	ADJ
eurjchem-844	104	3	lc	lc	NOUN
eurjchem-844	104	4	chromatogram	chromatogram	NOUN
eurjchem-844	104	5	of	of	ADP
eurjchem-844	104	6	25	25	NUM
eurjchem-844	104	7	µl	µl	ADP
eurjchem-844	104	8	injector	injector	NOUN
eurjchem-844	104	9	of	of	ADP
eurjchem-844	104	10	the	the	DET
eurjchem-844	104	11	synthetic	synthetic	ADJ
eurjchem-844	104	12	ternary	ternary	ADJ
eurjchem-844	104	13	mixture	mixture	NOUN
eurjchem-844	104	14	,	,	PUNCT
eurjchem-844	104	15	(	(	PUNCT
eurjchem-844	104	16	a	a	X
eurjchem-844	104	17	)	)	PUNCT
eurjchem-844	104	18	metformin	metformin	NOUN
eurjchem-844	104	19	hydrochloride	hydrochloride	NOUN
eurjchem-844	104	20	(	(	PUNCT
eurjchem-844	104	21	500	500	NUM
eurjchem-844	104	22	μg	μg	NOUN
eurjchem-844	104	23	/	/	SYM
eurjchem-844	104	24	ml	ml	NOUN
eurjchem-844	104	25	)	)	PUNCT
eurjchem-844	104	26	,	,	PUNCT
eurjchem-844	104	27	(	(	PUNCT
eurjchem-844	104	28	b	b	X
eurjchem-844	104	29	)	)	PUNCT
eurjchem-844	104	30	sitagliptin	sitagliptin	NOUN
eurjchem-844	104	31	(	(	PUNCT
eurjchem-844	104	32	32.1	32.1	NUM
eurjchem-844	104	33	μg	μg	NOUN
eurjchem-844	104	34	/	/	SYM
eurjchem-844	104	35	ml	ml	NOUN
eurjchem-844	104	36	)	)	PUNCT
eurjchem-844	104	37	and	and	CCONJ
eurjchem-844	104	38	(	(	PUNCT
eurjchem-844	104	39	c	c	NOUN
eurjchem-844	104	40	)	)	PUNCT
eurjchem-844	104	41	cyanoguanidine	cyanoguanidine	NOUN
eurjchem-844	104	42	(	(	PUNCT
eurjchem-844	104	43	150	150	NUM
eurjchem-844	104	44	μg	μg	NOUN
eurjchem-844	104	45	/	/	SYM
eurjchem-844	104	46	ml	ml	NOUN
eurjchem-844	104	47	)	)	PUNCT
eurjchem-844	104	48	.	.	PUNCT
eurjchem-844	105	1	3.2	3.2	NUM
eurjchem-844	105	2	.	.	PUNCT
eurjchem-844	106	1	system	system	NOUN
eurjchem-844	106	2	suitability	suitability	NOUN
eurjchem-844	106	3	tests	test	NOUN
eurjchem-844	106	4	according	accord	VERB
eurjchem-844	106	5	to	to	ADP
eurjchem-844	106	6	united	united	PROPN
eurjchem-844	106	7	states	states	PROPN
eurjchem-844	106	8	pharmacopeia	pharmacopeia	PROPN
eurjchem-844	106	9	(	(	PUNCT
eurjchem-844	106	10	usp	usp	NOUN
eurjchem-844	106	11	)	)	PUNCT
eurjchem-844	107	1	[	[	X
eurjchem-844	107	2	23	23	NUM
eurjchem-844	107	3	]	]	PUNCT
eurjchem-844	107	4	,	,	PUNCT
eurjchem-844	107	5	system	system	NOUN
eurjchem-844	107	6	suitability	suitability	NOUN
eurjchem-844	107	7	tests	test	NOUN
eurjchem-844	107	8	are	be	AUX
eurjchem-844	107	9	an	an	DET
eurjchem-844	107	10	integral	integral	ADJ
eurjchem-844	107	11	part	part	NOUN
eurjchem-844	107	12	of	of	ADP
eurjchem-844	107	13	liquid	liquid	ADJ
eurjchem-844	107	14	chromatographic	chromatographic	ADJ
eurjchem-844	107	15	methods	method	NOUN
eurjchem-844	107	16	in	in	ADP
eurjchem-844	107	17	the	the	DET
eurjchem-844	107	18	course	course	NOUN
eurjchem-844	107	19	of	of	ADP
eurjchem-844	107	20	optimizing	optimize	VERB
eurjchem-844	107	21	the	the	DET
eurjchem-844	107	22	conditions	condition	NOUN
eurjchem-844	107	23	of	of	ADP
eurjchem-844	107	24	the	the	DET
eurjchem-844	107	25	proposed	propose	VERB
eurjchem-844	107	26	method	method	NOUN
eurjchem-844	107	27	.	.	PUNCT
eurjchem-844	108	1	in	in	ADP
eurjchem-844	108	2	the	the	DET
eurjchem-844	108	3	proposed	propose	VERB
eurjchem-844	108	4	lc	lc	NOUN
eurjchem-844	108	5	method	method	NOUN
eurjchem-844	108	6	,	,	PUNCT
eurjchem-844	108	7	system	system	NOUN
eurjchem-844	108	8	suitability	suitability	NOUN
eurjchem-844	108	9	tests	test	NOUN
eurjchem-844	108	10	are	be	AUX
eurjchem-844	108	11	used	use	VERB
eurjchem-844	108	12	to	to	PART
eurjchem-844	108	13	verify	verify	VERB
eurjchem-844	108	14	that	that	DET
eurjchem-844	108	15	resolution	resolution	NOUN
eurjchem-844	108	16	and	and	CCONJ
eurjchem-844	108	17	reproducibility	reproducibility	NOUN
eurjchem-844	108	18	were	be	AUX
eurjchem-844	108	19	adequate	adequate	ADJ
eurjchem-844	108	20	for	for	ADP
eurjchem-844	108	21	analysis	analysis	NOUN
eurjchem-844	108	22	performed	perform	VERB
eurjchem-844	108	23	.	.	PUNCT
eurjchem-844	109	1	different	different	ADJ
eurjchem-844	109	2	parameters	parameter	NOUN
eurjchem-844	109	3	affecting	affect	VERB
eurjchem-844	109	4	the	the	DET
eurjchem-844	109	5	chromatographic	chromatographic	ADJ
eurjchem-844	109	6	separation	separation	NOUN
eurjchem-844	109	7	were	be	AUX
eurjchem-844	109	8	studied	study	VERB
eurjchem-844	109	9	.	.	PUNCT
eurjchem-844	110	1	the	the	DET
eurjchem-844	110	2	parameters	parameter	NOUN
eurjchem-844	110	3	of	of	ADP
eurjchem-844	110	4	this	this	DET
eurjchem-844	110	5	test	test	NOUN
eurjchem-844	110	6	are	be	AUX
eurjchem-844	110	7	column	column	NOUN
eurjchem-844	110	8	efficiency	efficiency	NOUN
eurjchem-844	110	9	(	(	PUNCT
eurjchem-844	110	10	number	number	NOUN
eurjchem-844	110	11	of	of	ADP
eurjchem-844	110	12	theoretical	theoretical	ADJ
eurjchem-844	110	13	plates	plate	NOUN
eurjchem-844	110	14	)	)	PUNCT
eurjchem-844	110	15	,	,	PUNCT
eurjchem-844	110	16	tailing	tail	VERB
eurjchem-844	110	17	of	of	ADP
eurjchem-844	110	18	chromatographic	chromatographic	ADJ
eurjchem-844	110	19	peak	peak	NOUN
eurjchem-844	110	20	,	,	PUNCT
eurjchem-844	110	21	peak	peak	NOUN
eurjchem-844	110	22	resolution	resolution	NOUN
eurjchem-844	110	23	factor	factor	NOUN
eurjchem-844	110	24	,	,	PUNCT
eurjchem-844	110	25	and	and	CCONJ
eurjchem-844	110	26	repeatability	repeatability	NOUN
eurjchem-844	110	27	as	as	ADP
eurjchem-844	110	28	%	%	NOUN
eurjchem-844	110	29	r.s.d	r.s.d	NOUN
eurjchem-844	110	30	.	.	PUNCT
eurjchem-844	111	1	of	of	ADP
eurjchem-844	111	2	peak	peak	NOUN
eurjchem-844	111	3	areas	area	NOUN
eurjchem-844	111	4	for	for	ADP
eurjchem-844	111	5	six	six	NUM
eurjchem-844	111	6	injections	injection	NOUN
eurjchem-844	111	7	and	and	CCONJ
eurjchem-844	111	8	reproducibility	reproducibility	NOUN
eurjchem-844	111	9	of	of	ADP
eurjchem-844	111	10	retention	retention	NOUN
eurjchem-844	111	11	times	time	NOUN
eurjchem-844	111	12	.	.	PUNCT
eurjchem-844	112	1	the	the	DET
eurjchem-844	112	2	results	result	NOUN
eurjchem-844	112	3	of	of	ADP
eurjchem-844	112	4	these	these	DET
eurjchem-844	112	5	tests	test	NOUN
eurjchem-844	112	6	are	be	AUX
eurjchem-844	112	7	listed	list	VERB
eurjchem-844	112	8	in	in	ADP
eurjchem-844	112	9	tables	table	NOUN
eurjchem-844	112	10	1‐3	1‐3	PROPN
eurjchem-844	112	11	.	.	PUNCT
eurjchem-844	113	1	figure	figure	NOUN
eurjchem-844	113	2	3	3	NUM
eurjchem-844	113	3	.	.	PUNCT
eurjchem-844	114	1	a	a	DET
eurjchem-844	114	2	typical	typical	ADJ
eurjchem-844	114	3	lc	lc	NOUN
eurjchem-844	114	4	chromatogram	chromatogram	NOUN
eurjchem-844	114	5	of	of	ADP
eurjchem-844	114	6	25	25	NUM
eurjchem-844	114	7	µl	µl	ADP
eurjchem-844	114	8	injector	injector	NOUN
eurjchem-844	114	9	of	of	ADP
eurjchem-844	114	10	the	the	DET
eurjchem-844	114	11	synthetic	synthetic	ADJ
eurjchem-844	114	12	ternary	ternary	ADJ
eurjchem-844	114	13	mixture	mixture	NOUN
eurjchem-844	114	14	,	,	PUNCT
eurjchem-844	114	15	(	(	PUNCT
eurjchem-844	114	16	a	a	X
eurjchem-844	114	17	)	)	PUNCT
eurjchem-844	114	18	metformin	metformin	NOUN
eurjchem-844	114	19	hydrochloride	hydrochloride	NOUN
eurjchem-844	114	20	(	(	PUNCT
eurjchem-844	114	21	500	500	NUM
eurjchem-844	114	22	μg	μg	NOUN
eurjchem-844	114	23	/	/	SYM
eurjchem-844	114	24	ml	ml	NOUN
eurjchem-844	114	25	)	)	PUNCT
eurjchem-844	114	26	,	,	PUNCT
eurjchem-844	114	27	(	(	PUNCT
eurjchem-844	114	28	b	b	X
eurjchem-844	114	29	)	)	PUNCT
eurjchem-844	114	30	vildagliptin	vildagliptin	NOUN
eurjchem-844	114	31	(	(	PUNCT
eurjchem-844	114	32	50	50	NUM
eurjchem-844	114	33	μg	μg	NOUN
eurjchem-844	114	34	/	/	SYM
eurjchem-844	114	35	ml	ml	NOUN
eurjchem-844	114	36	)	)	PUNCT
eurjchem-844	114	37	and	and	CCONJ
eurjchem-844	114	38	(	(	PUNCT
eurjchem-844	114	39	c	c	NOUN
eurjchem-844	114	40	)	)	PUNCT
eurjchem-844	114	41	cyanoguanidine	cyanoguanidine	NOUN
eurjchem-844	114	42	(	(	PUNCT
eurjchem-844	114	43	150	150	NUM
eurjchem-844	114	44	μg	μg	NOUN
eurjchem-844	114	45	/	/	SYM
eurjchem-844	114	46	ml	ml	NOUN
eurjchem-844	114	47	)	)	PUNCT
eurjchem-844	114	48	.	.	PUNCT
eurjchem-844	115	1	figure	figure	VERB
eurjchem-844	115	2	4	4	NUM
eurjchem-844	115	3	.	.	PUNCT
eurjchem-844	116	1	a	a	DET
eurjchem-844	116	2	typical	typical	ADJ
eurjchem-844	116	3	lc	lc	NOUN
eurjchem-844	116	4	chromatogram	chromatogram	NOUN
eurjchem-844	116	5	of	of	ADP
eurjchem-844	116	6	25	25	NUM
eurjchem-844	116	7	µl	µl	ADP
eurjchem-844	116	8	injector	injector	NOUN
eurjchem-844	116	9	of	of	ADP
eurjchem-844	116	10	the	the	DET
eurjchem-844	116	11	synthetic	synthetic	ADJ
eurjchem-844	116	12	ternary	ternary	ADJ
eurjchem-844	116	13	mixture	mixture	NOUN
eurjchem-844	116	14	,	,	PUNCT
eurjchem-844	116	15	(	(	PUNCT
eurjchem-844	116	16	a	a	X
eurjchem-844	116	17	)	)	PUNCT
eurjchem-844	116	18	metformin	metformin	NOUN
eurjchem-844	116	19	hydrochloride	hydrochloride	NOUN
eurjchem-844	116	20	(	(	PUNCT
eurjchem-844	116	21	500	500	NUM
eurjchem-844	116	22	μg	μg	NOUN
eurjchem-844	116	23	/	/	SYM
eurjchem-844	116	24	ml	ml	NOUN
eurjchem-844	116	25	)	)	PUNCT
eurjchem-844	116	26	,	,	PUNCT
eurjchem-844	116	27	(	(	PUNCT
eurjchem-844	116	28	b	b	X
eurjchem-844	116	29	)	)	PUNCT
eurjchem-844	116	30	saxagliptin	saxagliptin	NOUN
eurjchem-844	116	31	hydrochloride	hydrochloride	NOUN
eurjchem-844	116	32	(	(	PUNCT
eurjchem-844	116	33	5.6	5.6	NUM
eurjchem-844	116	34	μg	μg	NOUN
eurjchem-844	116	35	/	/	SYM
eurjchem-844	116	36	ml	ml	PROPN
eurjchem-844	116	37	)	)	PUNCT
eurjchem-844	116	38	and	and	CCONJ
eurjchem-844	116	39	(	(	PUNCT
eurjchem-844	116	40	c	c	NOUN
eurjchem-844	116	41	)	)	PUNCT
eurjchem-844	116	42	cyanoguanidine	cyanoguanidine	NOUN
eurjchem-844	116	43	(	(	PUNCT
eurjchem-844	116	44	150	150	NUM
eurjchem-844	116	45	μg	μg	NOUN
eurjchem-844	116	46	/	/	SYM
eurjchem-844	116	47	ml	ml	NOUN
eurjchem-844	116	48	)	)	PUNCT
eurjchem-844	116	49	.	.	PUNCT
eurjchem-844	117	1	figure	figure	NOUN
eurjchem-844	117	2	5	5	NUM
eurjchem-844	117	3	.	.	PUNCT
eurjchem-844	118	1	a	a	DET
eurjchem-844	118	2	typical	typical	ADJ
eurjchem-844	118	3	lc	lc	NOUN
eurjchem-844	118	4	chromatogram	chromatogram	NOUN
eurjchem-844	118	5	of	of	ADP
eurjchem-844	118	6	25	25	NUM
eurjchem-844	118	7	µl	µl	ADP
eurjchem-844	118	8	injector	injector	NOUN
eurjchem-844	118	9	of	of	ADP
eurjchem-844	118	10	janumet	janumet	ADJ
eurjchem-844	118	11	®	®	NOUN
eurjchem-844	118	12	sample	sample	NOUN
eurjchem-844	118	13	solution	solution	NOUN
eurjchem-844	118	14	,	,	PUNCT
eurjchem-844	118	15	(	(	PUNCT
eurjchem-844	118	16	a	a	X
eurjchem-844	118	17	)	)	PUNCT
eurjchem-844	118	18	metformin	metformin	NOUN
eurjchem-844	118	19	hydrochloride	hydrochloride	NOUN
eurjchem-844	118	20	(	(	PUNCT
eurjchem-844	118	21	500	500	NUM
eurjchem-844	118	22	μg	μg	NOUN
eurjchem-844	118	23	/	/	SYM
eurjchem-844	118	24	ml	ml	NOUN
eurjchem-844	118	25	)	)	PUNCT
eurjchem-844	118	26	and	and	CCONJ
eurjchem-844	118	27	(	(	PUNCT
eurjchem-844	118	28	b	b	NOUN
eurjchem-844	118	29	)	)	PUNCT
eurjchem-844	118	30	sitagliptin	sitagliptin	NOUN
eurjchem-844	118	31	(	(	PUNCT
eurjchem-844	118	32	32.1	32.1	NUM
eurjchem-844	118	33	μg	μg	NOUN
eurjchem-844	118	34	/	/	SYM
eurjchem-844	118	35	ml	ml	NOUN
eurjchem-844	118	36	)	)	PUNCT
eurjchem-844	118	37	.	.	PUNCT
eurjchem-844	119	1	3.3	3.3	NUM
eurjchem-844	119	2	.	.	PUNCT
eurjchem-844	120	1	method	method	NOUN
eurjchem-844	120	2	validation	validation	NOUN
eurjchem-844	120	3	3.3.1	3.3.1	PROPN
eurjchem-844	120	4	.	.	PUNCT
eurjchem-844	121	1	linearity	linearity	NOUN
eurjchem-844	121	2	linearity	linearity	PROPN
eurjchem-844	121	3	was	be	AUX
eurjchem-844	121	4	studied	study	VERB
eurjchem-844	121	5	for	for	ADP
eurjchem-844	121	6	stg	stg	PROPN
eurjchem-844	121	7	,	,	PUNCT
eurjchem-844	121	8	vdg	vdg	PROPN
eurjchem-844	121	9	,	,	PUNCT
eurjchem-844	121	10	sxg	sxg	NOUN
eurjchem-844	121	11	and	and	CCONJ
eurjchem-844	121	12	met	meet	VERB
eurjchem-844	121	13	.	.	PUNCT
eurjchem-844	122	1	a	a	DET
eurjchem-844	122	2	linear	linear	ADJ
eurjchem-844	122	3	relationship	relationship	NOUN
eurjchem-844	122	4	between	between	ADP
eurjchem-844	122	5	area	area	NOUN
eurjchem-844	122	6	under	under	ADP
eurjchem-844	122	7	the	the	DET
eurjchem-844	122	8	peak	peak	NOUN
eurjchem-844	122	9	(	(	PUNCT
eurjchem-844	122	10	aup	aup	PROPN
eurjchem-844	122	11	)	)	PUNCT
eurjchem-844	122	12	and	and	CCONJ
eurjchem-844	122	13	component	component	NOUN
eurjchem-844	122	14	concentration	concentration	NOUN
eurjchem-844	122	15	(	(	PUNCT
eurjchem-844	122	16	c	c	NOUN
eurjchem-844	122	17	)	)	PUNCT
eurjchem-844	122	18	was	be	AUX
eurjchem-844	122	19	obtained	obtain	VERB
eurjchem-844	122	20	.	.	PUNCT
eurjchem-844	123	1	the	the	DET
eurjchem-844	123	2	regression	regression	NOUN
eurjchem-844	123	3	equations	equation	NOUN
eurjchem-844	123	4	were	be	AUX
eurjchem-844	123	5	also	also	ADV
eurjchem-844	123	6	computed	compute	VERB
eurjchem-844	123	7	.	.	PUNCT
eurjchem-844	124	1	the	the	DET
eurjchem-844	124	2	linearity	linearity	NOUN
eurjchem-844	124	3	of	of	ADP
eurjchem-844	124	4	the	the	DET
eurjchem-844	124	5	calibration	calibration	NOUN
eurjchem-844	124	6	curves	curve	NOUN
eurjchem-844	124	7	were	be	AUX
eurjchem-844	124	8	validated	validate	VERB
eurjchem-844	124	9	by	by	ADP
eurjchem-844	124	10	the	the	DET
eurjchem-844	124	11	high	high	ADJ
eurjchem-844	124	12	value	value	NOUN
eurjchem-844	124	13	of	of	ADP
eurjchem-844	124	14	correlation	correlation	NOUN
eurjchem-844	124	15	coefficients	coefficient	NOUN
eurjchem-844	124	16	.	.	PUNCT
eurjchem-844	125	1	the	the	DET
eurjchem-844	125	2	analytical	analytical	ADJ
eurjchem-844	125	3	data	datum	NOUN
eurjchem-844	125	4	of	of	ADP
eurjchem-844	125	5	the	the	DET
eurjchem-844	125	6	calibration	calibration	NOUN
eurjchem-844	125	7	curves	curve	NOUN
eurjchem-844	125	8	including	include	VERB
eurjchem-844	125	9	standard	standard	ADJ
eurjchem-844	125	10	deviations	deviation	NOUN
eurjchem-844	125	11	for	for	ADP
eurjchem-844	125	12	the	the	DET
eurjchem-844	125	13	slope	slope	NOUN
eurjchem-844	125	14	and	and	CCONJ
eurjchem-844	125	15	intercept	intercept	PROPN
eurjchem-844	125	16	(	(	PUNCT
eurjchem-844	125	17	sb	sb	PROPN
eurjchem-844	125	18	,	,	PUNCT
eurjchem-844	125	19	sa	sa	PROPN
eurjchem-844	125	20	)	)	PUNCT
eurjchem-844	125	21	are	be	AUX
eurjchem-844	125	22	summarized	summarize	VERB
eurjchem-844	125	23	in	in	ADP
eurjchem-844	125	24	tables	table	NOUN
eurjchem-844	125	25	4	4	NUM
eurjchem-844	125	26	and	and	CCONJ
eurjchem-844	125	27	5	5	NUM
eurjchem-844	125	28	.	.	X
eurjchem-844	125	29	el‐bagary	el‐bagary	PROPN
eurjchem-844	125	30	et	et	PROPN
eurjchem-844	125	31	al	al	PROPN
eurjchem-844	125	32	.	.	PUNCT
eurjchem-844	125	33	/	/	SYM
eurjchem-844	125	34	european	european	PROPN
eurjchem-844	125	35	journal	journal	PROPN
eurjchem-844	125	36	of	of	ADP
eurjchem-844	125	37	chemistry	chemistry	NOUN
eurjchem-844	125	38	4	4	NUM
eurjchem-844	125	39	(	(	PUNCT
eurjchem-844	125	40	4	4	NUM
eurjchem-844	125	41	)	)	PUNCT
eurjchem-844	125	42	(	(	PUNCT
eurjchem-844	125	43	2013	2013	NUM
eurjchem-844	125	44	)	)	PUNCT
eurjchem-844	125	45	444‐449	444‐449	PROPN
eurjchem-844	125	46	447	447	NUM
eurjchem-844	125	47	table	table	NOUN
eurjchem-844	125	48	4	4	NUM
eurjchem-844	125	49	.	.	PUNCT
eurjchem-844	125	50	results	result	NOUN
eurjchem-844	125	51	obtained	obtain	VERB
eurjchem-844	125	52	by	by	ADP
eurjchem-844	125	53	lc	lc	PROPN
eurjchem-844	125	54	method	method	NOUN
eurjchem-844	125	55	for	for	ADP
eurjchem-844	125	56	the	the	DET
eurjchem-844	125	57	determination	determination	NOUN
eurjchem-844	125	58	of	of	ADP
eurjchem-844	125	59	metformin	metformin	NOUN
eurjchem-844	125	60	in	in	ADP
eurjchem-844	125	61	binary	binary	ADJ
eurjchem-844	125	62	mixture	mixture	NOUN
eurjchem-844	125	63	with	with	ADP
eurjchem-844	125	64	sitagliptin	sitagliptin	NOUN
eurjchem-844	125	65	or	or	CCONJ
eurjchem-844	125	66	vildagliptin	vildagliptin	NOUN
eurjchem-844	125	67	or	or	CCONJ
eurjchem-844	125	68	saxagliptin	saxagliptin	NOUN
eurjchem-844	125	69	.	.	PUNCT
eurjchem-844	126	1	item	item	PROPN
eurjchem-844	126	2	*	*	PUNCT
eurjchem-844	127	1	metformin	metformin	NOUN
eurjchem-844	127	2	retention	retention	NOUN
eurjchem-844	127	3	time	time	NOUN
eurjchem-844	127	4	9.1	9.1	NUM
eurjchem-844	127	5	wavelength	wavelength	NOUN
eurjchem-844	127	6	of	of	ADP
eurjchem-844	127	7	detection	detection	NOUN
eurjchem-844	127	8	,	,	PUNCT
eurjchem-844	127	9	nm	nm	ADJ
eurjchem-844	127	10	210	210	NUM
eurjchem-844	127	11	range	range	NOUN
eurjchem-844	127	12	of	of	ADP
eurjchem-844	127	13	linearity	linearity	NOUN
eurjchem-844	127	14	,	,	PUNCT
eurjchem-844	127	15	μg	μg	PROPN
eurjchem-844	127	16	/	/	SYM
eurjchem-844	127	17	ml	ml	PROPN
eurjchem-844	127	18	20‐800	20‐800	NUM
eurjchem-844	127	19	regression	regression	NOUN
eurjchem-844	127	20	equation	equation	NOUN
eurjchem-844	127	21	area	area	NOUN
eurjchem-844	127	22	×	×	PROPN
eurjchem-844	127	23	10‐6	10‐6	NUM
eurjchem-844	127	24	=	=	SYM
eurjchem-844	128	1	0.0630	0.0630	NUM
eurjchem-844	128	2	cμg	cμg	NOUN
eurjchem-844	128	3	/	/	SYM
eurjchem-844	128	4	ml	ml	NOUN
eurjchem-844	129	1	+	+	CCONJ
eurjchem-844	129	2	0.4827	0.4827	NUM
eurjchem-844	129	3	regression	regression	NOUN
eurjchem-844	129	4	coefficient	coefficient	NOUN
eurjchem-844	129	5	(	(	PUNCT
eurjchem-844	129	6	r2	r2	PROPN
eurjchem-844	129	7	)	)	PUNCT
eurjchem-844	129	8	0.9998	0.9998	NUM
eurjchem-844	129	9	lod	lod	PROPN
eurjchem-844	129	10	,	,	PUNCT
eurjchem-844	129	11	μg	μg	PROPN
eurjchem-844	129	12	/	/	SYM
eurjchem-844	129	13	ml	ml	PROPN
eurjchem-844	129	14	12.26	12.26	NUM
eurjchem-844	129	15	loq	loq	PROPN
eurjchem-844	129	16	,	,	PUNCT
eurjchem-844	129	17	μg	μg	PROPN
eurjchem-844	129	18	/	/	SYM
eurjchem-844	129	19	ml	ml	PROPN
eurjchem-844	129	20	19.7	19.7	NUM
eurjchem-844	129	21	sb	sb	PROPN
eurjchem-844	129	22	1.6×10‐3	1.6×10‐3	PROPN
eurjchem-844	129	23	sa	sa	PROPN
eurjchem-844	129	24	1.4×10‐1	1.4×10‐1	NUM
eurjchem-844	129	25	confidence	confidence	NOUN
eurjchem-844	129	26	limit	limit	NOUN
eurjchem-844	129	27	of	of	ADP
eurjchem-844	129	28	the	the	DET
eurjchem-844	129	29	slope	slope	NOUN
eurjchem-844	129	30	0.0630±0.09×10‐1	0.0630±0.09×10‐1	NOUN
eurjchem-844	129	31	confidence	confidence	NOUN
eurjchem-844	129	32	limit	limit	NOUN
eurjchem-844	129	33	of	of	ADP
eurjchem-844	129	34	the	the	DET
eurjchem-844	129	35	intercept	intercept	NOUN
eurjchem-844	129	36	0.4827±0.77×10‐3	0.4827±0.77×10‐3	PROPN
eurjchem-844	129	37	standard	standard	ADJ
eurjchem-844	129	38	error	error	NOUN
eurjchem-844	129	39	of	of	ADP
eurjchem-844	129	40	the	the	DET
eurjchem-844	129	41	estimation	estimation	NOUN
eurjchem-844	129	42	0.22	0.22	NUM
eurjchem-844	129	43	intraday	intraday	NOUN
eurjchem-844	129	44	%	%	NOUN
eurjchem-844	129	45	r.s.d	r.s.d	NOUN
eurjchem-844	129	46	.	.	PUNCT
eurjchem-844	130	1	0.29‐0.67	0.29‐0.67	NUM
eurjchem-844	130	2	interday	interday	NOUN
eurjchem-844	130	3	%	%	NOUN
eurjchem-844	130	4	r.s.d	r.s.d	VERB
eurjchem-844	130	5	.	.	PUNCT
eurjchem-844	131	1	0.13‐1.1	0.13‐1.1	PROPN
eurjchem-844	131	2	drug	drug	PROPN
eurjchem-844	131	3	in	in	ADP
eurjchem-844	131	4	laboratory	laboratory	NOUN
eurjchem-844	131	5	mixture	mixture	NOUN
eurjchem-844	131	6	100.29±1.65	100.29±1.65	NUM
eurjchem-844	131	7	with	with	ADP
eurjchem-844	131	8	stg	stg	PROPN
eurjchem-844	131	9	100.57±0.90	100.57±0.90	NUM
eurjchem-844	131	10	with	with	ADP
eurjchem-844	131	11	vlg	vlg	PROPN
eurjchem-844	131	12	100.23±0.91	100.23±0.91	NUM
eurjchem-844	131	13	with	with	ADP
eurjchem-844	131	14	sxg	sxg	ADJ
eurjchem-844	131	15	drug	drug	NOUN
eurjchem-844	131	16	in	in	ADP
eurjchem-844	131	17	dosage	dosage	NOUN
eurjchem-844	131	18	form	form	NOUN
eurjchem-844	131	19	99.71±1.68	99.71±1.68	PROPN
eurjchem-844	131	20	(	(	PUNCT
eurjchem-844	131	21	janumet	janumet	PROPN
eurjchem-844	131	22	®	®	PROPN
eurjchem-844	131	23	)	)	PUNCT
eurjchem-844	131	24	99.95±1.20	99.95±1.20	NUM
eurjchem-844	131	25	(	(	PUNCT
eurjchem-844	131	26	eucreas	eucrea	NOUN
eurjchem-844	131	27	®	®	NOUN
eurjchem-844	131	28	)	)	PUNCT
eurjchem-844	131	29	100.14±1.19	100.14±1.19	NUM
eurjchem-844	131	30	(	(	PUNCT
eurjchem-844	131	31	kombiglyze	kombiglyze	PROPN
eurjchem-844	131	32	®	®	NOUN
eurjchem-844	131	33	)	)	PUNCT
eurjchem-844	131	34	drug	drug	NOUN
eurjchem-844	131	35	added	add	VERB
eurjchem-844	131	36	100.26±1.48	100.26±1.48	NOUN
eurjchem-844	131	37	(	(	PUNCT
eurjchem-844	131	38	janumet	janumet	PROPN
eurjchem-844	131	39	®	®	PROPN
eurjchem-844	131	40	)	)	PUNCT
eurjchem-844	131	41	99.99±1.01	99.99±1.01	NUM
eurjchem-844	131	42	(	(	PUNCT
eurjchem-844	131	43	eucreas	eucreas	ADJ
eurjchem-844	131	44	®	®	NOUN
eurjchem-844	131	45	)	)	PUNCT
eurjchem-844	131	46	99.73±1.24	99.73±1.24	PROPN
eurjchem-844	131	47	(	(	PUNCT
eurjchem-844	131	48	kombiglyze	kombiglyze	PROPN
eurjchem-844	131	49	®	®	PROPN
eurjchem-844	131	50	)	)	PUNCT
eurjchem-844	131	51	*	*	PUNCT
eurjchem-844	132	1	lod	lod	PROPN
eurjchem-844	132	2	:	:	PUNCT
eurjchem-844	132	3	limit	limit	NOUN
eurjchem-844	132	4	of	of	ADP
eurjchem-844	132	5	detection	detection	NOUN
eurjchem-844	132	6	,	,	PUNCT
eurjchem-844	132	7	loq	loq	PROPN
eurjchem-844	132	8	:	:	PUNCT
eurjchem-844	132	9	limit	limit	NOUN
eurjchem-844	132	10	of	of	ADP
eurjchem-844	132	11	quantification	quantification	NOUN
eurjchem-844	132	12	,	,	PUNCT
eurjchem-844	132	13	%	%	INTJ
eurjchem-844	132	14	r.s.d	r.s.d	NOUN
eurjchem-844	132	15	.	.	PUNCT
eurjchem-844	132	16	:	:	PUNCT
eurjchem-844	133	1	percent	percent	NOUN
eurjchem-844	133	2	relative	relative	ADJ
eurjchem-844	133	3	standard	standard	ADJ
eurjchem-844	133	4	deviation	deviation	NOUN
eurjchem-844	133	5	.	.	PUNCT
eurjchem-844	134	1	table	table	NOUN
eurjchem-844	134	2	5	5	NUM
eurjchem-844	134	3	.	.	PUNCT
eurjchem-844	135	1	results	result	NOUN
eurjchem-844	135	2	obtained	obtain	VERB
eurjchem-844	135	3	by	by	ADP
eurjchem-844	135	4	lc	lc	PROPN
eurjchem-844	135	5	method	method	NOUN
eurjchem-844	135	6	for	for	ADP
eurjchem-844	135	7	the	the	DET
eurjchem-844	135	8	determination	determination	NOUN
eurjchem-844	135	9	of	of	ADP
eurjchem-844	135	10	sitagliptin	sitagliptin	NOUN
eurjchem-844	135	11	,	,	PUNCT
eurjchem-844	135	12	vildagliptin	vildagliptin	NOUN
eurjchem-844	135	13	and	and	CCONJ
eurjchem-844	135	14	saxagliptin	saxagliptin	PROPN
eurjchem-844	135	15	.	.	PUNCT
eurjchem-844	136	1	item	item	PROPN
eurjchem-844	136	2	sitagliptin	sitagliptin	PROPN
eurjchem-844	136	3	vildagliptin	vildagliptin	NOUN
eurjchem-844	136	4	saxagliptin	saxagliptin	NOUN
eurjchem-844	136	5	retention	retention	NOUN
eurjchem-844	136	6	time	time	NOUN
eurjchem-844	136	7	6.0	6.0	NUM
eurjchem-844	136	8	7.1	7.1	NUM
eurjchem-844	136	9	6.5	6.5	NUM
eurjchem-844	136	10	wavelength	wavelength	NOUN
eurjchem-844	136	11	of	of	ADP
eurjchem-844	136	12	detection	detection	NOUN
eurjchem-844	136	13	,	,	PUNCT
eurjchem-844	136	14	nm	nm	NOUN
eurjchem-844	136	15	210	210	NUM
eurjchem-844	136	16	210	210	NUM
eurjchem-844	136	17	210	210	NUM
eurjchem-844	136	18	range	range	NOUN
eurjchem-844	136	19	of	of	ADP
eurjchem-844	136	20	linearity	linearity	NOUN
eurjchem-844	136	21	,	,	PUNCT
eurjchem-844	136	22	μg	μg	PROPN
eurjchem-844	136	23	/	/	SYM
eurjchem-844	136	24	ml	ml	NOUN
eurjchem-844	137	1	5‐200	5‐200	PROPN
eurjchem-844	137	2	5‐200	5‐200	NUM
eurjchem-844	137	3	0.5‐80	0.5‐80	VERB
eurjchem-844	137	4	regression	regression	NOUN
eurjchem-844	137	5	equation	equation	NOUN
eurjchem-844	137	6	area×10‐5	area×10‐5	NOUN
eurjchem-844	137	7	=	=	SYM
eurjchem-844	137	8	0.1013	0.1013	NUM
eurjchem-844	137	9	cμg	cμg	ADJ
eurjchem-844	137	10	/	/	SYM
eurjchem-844	137	11	ml+	ml+	NOUN
eurjchem-844	137	12	0.0736	0.0736	NUM
eurjchem-844	137	13	area×10‐5	area×10‐5	NOUN
eurjchem-844	137	14	=	=	PUNCT
eurjchem-844	137	15	0.1126	0.1126	NUM
eurjchem-844	137	16	cμg	cμg	NOUN
eurjchem-844	137	17	/	/	SYM
eurjchem-844	137	18	ml	ml	NOUN
eurjchem-844	138	1	+	+	CCONJ
eurjchem-844	138	2	0.4040	0.4040	NUM
eurjchem-844	138	3	area×10‐5	area×10‐5	ADJ
eurjchem-844	138	4	=	=	PUNCT
eurjchem-844	138	5	0.1495	0.1495	NUM
eurjchem-844	138	6	cμg	cμg	NOUN
eurjchem-844	138	7	/	/	SYM
eurjchem-844	138	8	ml	ml	NOUN
eurjchem-844	138	9	+	+	CCONJ
eurjchem-844	138	10	0.0114	0.0114	NUM
eurjchem-844	138	11	regression	regression	NOUN
eurjchem-844	138	12	coefficient	coefficient	NOUN
eurjchem-844	138	13	(	(	PUNCT
eurjchem-844	138	14	r2	r2	PROPN
eurjchem-844	138	15	)	)	PUNCT
eurjchem-844	138	16	0.9998	0.9998	NUM
eurjchem-844	138	17	0.9996	0.9996	NUM
eurjchem-844	138	18	0.9987	0.9987	NUM
eurjchem-844	138	19	lod	lod	NOUN
eurjchem-844	138	20	,	,	PUNCT
eurjchem-844	138	21	μg	μg	PROPN
eurjchem-844	138	22	/	/	SYM
eurjchem-844	138	23	ml	ml	PROPN
eurjchem-844	138	24	1.48	1.48	NUM
eurjchem-844	138	25	0.53	0.53	NUM
eurjchem-844	138	26	0.10	0.10	NUM
eurjchem-844	138	27	loq	loq	PROPN
eurjchem-844	138	28	,	,	PUNCT
eurjchem-844	138	29	μg	μg	PROPN
eurjchem-844	138	30	/	/	SYM
eurjchem-844	138	31	ml	ml	PROPN
eurjchem-844	138	32	4.94	4.94	NUM
eurjchem-844	138	33	1.78	1.78	NUM
eurjchem-844	138	34	0.42	0.42	NUM
eurjchem-844	138	35	sb	sb	NOUN
eurjchem-844	138	36	1.16×10‐4	1.16×10‐4	PROPN
eurjchem-844	138	37	1.6×10‐4	1.6×10‐4	PROPN
eurjchem-844	138	38	1.8×10‐4	1.8×10‐4	PROPN
eurjchem-844	138	39	sa	sa	PROPN
eurjchem-844	139	1	0.17	0.17	NUM
eurjchem-844	139	2	0.22	0.22	NUM
eurjchem-844	139	3	0.25	0.25	NUM
eurjchem-844	139	4	confidence	confidence	NOUN
eurjchem-844	139	5	limit	limit	NOUN
eurjchem-844	139	6	of	of	ADP
eurjchem-844	139	7	the	the	DET
eurjchem-844	139	8	slope	slope	NOUN
eurjchem-844	139	9	0.1013±0.02	0.1013±0.02	PROPN
eurjchem-844	139	10	0.1126±0.02	0.1126±0.02	PROPN
eurjchem-844	139	11	0.1495±0.04	0.1495±0.04	NOUN
eurjchem-844	139	12	confidence	confidence	NOUN
eurjchem-844	139	13	limit	limit	NOUN
eurjchem-844	139	14	of	of	ADP
eurjchem-844	139	15	the	the	DET
eurjchem-844	139	16	intercept	intercept	NOUN
eurjchem-844	139	17	0.0736±0.09×10‐4	0.0736±0.09×10‐4	PROPN
eurjchem-844	139	18	0.4040±0.65×10‐4	0.4040±0.65×10‐4	PROPN
eurjchem-844	139	19	0.0114±0.02×10‐4	0.0114±0.02×10‐4	PROPN
eurjchem-844	139	20	standard	standard	ADJ
eurjchem-844	139	21	error	error	NOUN
eurjchem-844	139	22	of	of	ADP
eurjchem-844	139	23	the	the	DET
eurjchem-844	139	24	estimation	estimation	NOUN
eurjchem-844	139	25	0.19	0.19	NUM
eurjchem-844	139	26	0.27	0.27	NUM
eurjchem-844	139	27	0.31	0.31	NUM
eurjchem-844	139	28	intraday	intraday	NOUN
eurjchem-844	139	29	%	%	NOUN
eurjchem-844	139	30	r.s.d	r.s.d	NOUN
eurjchem-844	139	31	.	.	PUNCT
eurjchem-844	140	1	0.29‐0.58	0.29‐0.58	PROPN
eurjchem-844	140	2	0.21‐0.42	0.21‐0.42	NUM
eurjchem-844	141	1	0.43‐0.68	0.43‐0.68	PROPN
eurjchem-844	141	2	interday	interday	PROPN
eurjchem-844	141	3	%	%	INTJ
eurjchem-844	141	4	r.s.d	r.s.d	VERB
eurjchem-844	141	5	.	.	PUNCT
eurjchem-844	142	1	0.31‐1.14	0.31‐1.14	NOUN
eurjchem-844	142	2	0.23‐0.92	0.23‐0.92	NUM
eurjchem-844	142	3	0.56‐1.31	0.56‐1.31	NOUN
eurjchem-844	142	4	drug	drug	NOUN
eurjchem-844	142	5	in	in	ADP
eurjchem-844	142	6	laboratory	laboratory	NOUN
eurjchem-844	142	7	mixture	mixture	NOUN
eurjchem-844	142	8	100.32±1.44	100.32±1.44	NUM
eurjchem-844	142	9	100.17±1.41	100.17±1.41	NUM
eurjchem-844	142	10	100.01±1.51	100.01±1.51	NUM
eurjchem-844	142	11	drug	drug	NOUN
eurjchem-844	142	12	in	in	ADP
eurjchem-844	142	13	dosage	dosage	NOUN
eurjchem-844	142	14	form	form	NOUN
eurjchem-844	142	15	100.13±1.15	100.13±1.15	NUM
eurjchem-844	142	16	99.95±1.60	99.95±1.60	NUM
eurjchem-844	142	17	99.85±1.68	99.85±1.68	NUM
eurjchem-844	142	18	drug	drug	NOUN
eurjchem-844	142	19	added	add	VERB
eurjchem-844	142	20	100.52±1.21	100.52±1.21	NUM
eurjchem-844	142	21	100.24±1.65	100.24±1.65	NUM
eurjchem-844	142	22	99.53±1.46	99.53±1.46	NUM
eurjchem-844	142	23	*	*	PUNCT
eurjchem-844	142	24	lod	lod	PROPN
eurjchem-844	142	25	:	:	PUNCT
eurjchem-844	142	26	limit	limit	NOUN
eurjchem-844	142	27	of	of	ADP
eurjchem-844	142	28	detection	detection	NOUN
eurjchem-844	142	29	,	,	PUNCT
eurjchem-844	142	30	loq	loq	PROPN
eurjchem-844	142	31	:	:	PUNCT
eurjchem-844	142	32	limit	limit	NOUN
eurjchem-844	142	33	of	of	ADP
eurjchem-844	142	34	quantification	quantification	NOUN
eurjchem-844	142	35	,	,	PUNCT
eurjchem-844	142	36	%	%	INTJ
eurjchem-844	142	37	r.s.d	r.s.d	NOUN
eurjchem-844	142	38	.	.	PUNCT
eurjchem-844	142	39	:	:	PUNCT
eurjchem-844	143	1	percent	percent	NOUN
eurjchem-844	143	2	relative	relative	ADJ
eurjchem-844	143	3	standard	standard	ADJ
eurjchem-844	143	4	deviation	deviation	NOUN
eurjchem-844	143	5	.	.	PUNCT
eurjchem-844	144	1	figure	figure	NOUN
eurjchem-844	144	2	6	6	NUM
eurjchem-844	144	3	.	.	PUNCT
eurjchem-844	145	1	a	a	DET
eurjchem-844	145	2	typical	typical	ADJ
eurjchem-844	145	3	lc	lc	NOUN
eurjchem-844	145	4	chromatogram	chromatogram	NOUN
eurjchem-844	145	5	of	of	ADP
eurjchem-844	145	6	25	25	NUM
eurjchem-844	145	7	µl	µl	ADP
eurjchem-844	145	8	injector	injector	NOUN
eurjchem-844	145	9	of	of	ADP
eurjchem-844	145	10	eucreas	eucrea	NOUN
eurjchem-844	145	11	®	®	NOUN
eurjchem-844	145	12	sample	sample	NOUN
eurjchem-844	145	13	solution	solution	NOUN
eurjchem-844	145	14	,	,	PUNCT
eurjchem-844	145	15	(	(	PUNCT
eurjchem-844	145	16	a	a	X
eurjchem-844	145	17	)	)	PUNCT
eurjchem-844	145	18	metformin	metformin	NOUN
eurjchem-844	145	19	hydrochloride	hydrochloride	NOUN
eurjchem-844	145	20	(	(	PUNCT
eurjchem-844	145	21	500	500	NUM
eurjchem-844	145	22	μg	μg	NOUN
eurjchem-844	145	23	/	/	SYM
eurjchem-844	145	24	ml	ml	NOUN
eurjchem-844	145	25	)	)	PUNCT
eurjchem-844	145	26	and	and	CCONJ
eurjchem-844	145	27	(	(	PUNCT
eurjchem-844	145	28	b	b	NOUN
eurjchem-844	145	29	)	)	PUNCT
eurjchem-844	145	30	vildagliptin	vildagliptin	NOUN
eurjchem-844	145	31	(	(	PUNCT
eurjchem-844	145	32	50	50	NUM
eurjchem-844	145	33	μg	μg	NOUN
eurjchem-844	145	34	/	/	SYM
eurjchem-844	145	35	ml	ml	NOUN
eurjchem-844	145	36	)	)	PUNCT
eurjchem-844	145	37	.	.	PUNCT
eurjchem-844	146	1	3.3.2	3.3.2	NUM
eurjchem-844	146	2	.	.	PUNCT
eurjchem-844	146	3	accuracy	accuracy	NOUN
eurjchem-844	146	4	accuracy	accuracy	NOUN
eurjchem-844	146	5	of	of	ADP
eurjchem-844	146	6	the	the	DET
eurjchem-844	146	7	results	result	NOUN
eurjchem-844	146	8	was	be	AUX
eurjchem-844	146	9	calculated	calculate	VERB
eurjchem-844	146	10	by	by	ADP
eurjchem-844	146	11	%	%	NOUN
eurjchem-844	146	12	recovery	recovery	NOUN
eurjchem-844	146	13	of	of	ADP
eurjchem-844	146	14	five	five	NUM
eurjchem-844	146	15	different	different	ADJ
eurjchem-844	146	16	solutions	solution	NOUN
eurjchem-844	146	17	of	of	ADP
eurjchem-844	146	18	the	the	DET
eurjchem-844	146	19	laboratory	laboratory	NOUN
eurjchem-844	146	20	prepared	prepare	VERB
eurjchem-844	146	21	mixtures	mixture	NOUN
eurjchem-844	146	22	of	of	ADP
eurjchem-844	146	23	stg	stg	PROPN
eurjchem-844	146	24	,	,	PUNCT
eurjchem-844	146	25	vld	vld	NOUN
eurjchem-844	146	26	and	and	CCONJ
eurjchem-844	146	27	sxg	sxg	NOUN
eurjchem-844	146	28	in	in	ADP
eurjchem-844	146	29	their	their	PRON
eurjchem-844	146	30	ternary	ternary	ADJ
eurjchem-844	146	31	mixture	mixture	NOUN
eurjchem-844	146	32	with	with	ADP
eurjchem-844	146	33	met	meet	VERB
eurjchem-844	146	34	and	and	CCONJ
eurjchem-844	146	35	cgn	cgn	PROPN
eurjchem-844	146	36	and	and	CCONJ
eurjchem-844	146	37	also	also	ADV
eurjchem-844	146	38	by	by	ADP
eurjchem-844	146	39	standard	standard	ADJ
eurjchem-844	146	40	addition	addition	NOUN
eurjchem-844	146	41	technique	technique	NOUN
eurjchem-844	146	42	for	for	ADP
eurjchem-844	146	43	janumet	janumet	ADJ
eurjchem-844	146	44	®	®	NOUN
eurjchem-844	146	45	,	,	PUNCT
eurjchem-844	146	46	eucreas	eucrea	NOUN
eurjchem-844	146	47	®	®	NOUN
eurjchem-844	146	48	and	and	CCONJ
eurjchem-844	146	49	kombiglyze	kombiglyze	VERB
eurjchem-844	146	50	®	®	NOUN
eurjchem-844	146	51	tablets	tablet	NOUN
eurjchem-844	146	52	.	.	PUNCT
eurjchem-844	147	1	the	the	DET
eurjchem-844	147	2	results	result	NOUN
eurjchem-844	147	3	obtained	obtain	VERB
eurjchem-844	147	4	including	include	VERB
eurjchem-844	147	5	the	the	DET
eurjchem-844	147	6	mean	mean	NOUN
eurjchem-844	147	7	of	of	ADP
eurjchem-844	147	8	the	the	DET
eurjchem-844	147	9	recovery	recovery	NOUN
eurjchem-844	147	10	and	and	CCONJ
eurjchem-844	147	11	standard	standard	ADJ
eurjchem-844	147	12	deviation	deviation	NOUN
eurjchem-844	147	13	are	be	AUX
eurjchem-844	147	14	displayed	display	VERB
eurjchem-844	147	15	in	in	ADP
eurjchem-844	147	16	tables	table	NOUN
eurjchem-844	147	17	4	4	NUM
eurjchem-844	147	18	and	and	CCONJ
eurjchem-844	147	19	5	5	NUM
eurjchem-844	147	20	.	.	X
eurjchem-844	147	21	3.3.3	3.3.3	NUM
eurjchem-844	147	22	.	.	PUNCT
eurjchem-844	147	23	precision	precision	VERB
eurjchem-844	147	24	the	the	DET
eurjchem-844	147	25	repeatability	repeatability	NOUN
eurjchem-844	147	26	of	of	ADP
eurjchem-844	147	27	the	the	DET
eurjchem-844	147	28	method	method	NOUN
eurjchem-844	147	29	was	be	AUX
eurjchem-844	147	30	assessed	assess	VERB
eurjchem-844	147	31	by	by	ADP
eurjchem-844	147	32	six	six	NUM
eurjchem-844	147	33	determinations	determination	NOUN
eurjchem-844	147	34	for	for	ADP
eurjchem-844	147	35	each	each	PRON
eurjchem-844	147	36	of	of	ADP
eurjchem-844	147	37	the	the	DET
eurjchem-844	147	38	three	three	NUM
eurjchem-844	147	39	concentrations	concentration	NOUN
eurjchem-844	147	40	of	of	ADP
eurjchem-844	147	41	the	the	DET
eurjchem-844	147	42	laboratory	laboratory	NOUN
eurjchem-844	147	43	prepared	prepare	VERB
eurjchem-844	147	44	mixture	mixture	NOUN
eurjchem-844	147	45	of	of	ADP
eurjchem-844	147	46	stg	stg	PROPN
eurjchem-844	147	47	(	(	PUNCT
eurjchem-844	147	48	25.7	25.7	NUM
eurjchem-844	147	49	,	,	PUNCT
eurjchem-844	147	50	32.1	32.1	NUM
eurjchem-844	147	51	,	,	PUNCT
eurjchem-844	147	52	and	and	CCONJ
eurjchem-844	147	53	38.5	38.5	NUM
eurjchem-844	147	54	μg	μg	NOUN
eurjchem-844	147	55	/	/	SYM
eurjchem-844	147	56	ml	ml	NOUN
eurjchem-844	147	57	)	)	PUNCT
eurjchem-844	147	58	with	with	ADP
eurjchem-844	147	59	met	meet	VERB
eurjchem-844	147	60	(	(	PUNCT
eurjchem-844	147	61	400	400	NUM
eurjchem-844	147	62	,	,	PUNCT
eurjchem-844	147	63	500	500	NUM
eurjchem-844	147	64	,	,	PUNCT
eurjchem-844	147	65	and	and	CCONJ
eurjchem-844	147	66	600	600	NUM
eurjchem-844	147	67	μg	μg	NOUN
eurjchem-844	147	68	/	/	SYM
eurjchem-844	147	69	ml	ml	NOUN
eurjchem-844	147	70	)	)	PUNCT
eurjchem-844	147	71	and	and	CCONJ
eurjchem-844	147	72	cgn	cgn	PROPN
eurjchem-844	147	73	(	(	PUNCT
eurjchem-844	147	74	120	120	NUM
eurjchem-844	147	75	,	,	PUNCT
eurjchem-844	147	76	150	150	NUM
eurjchem-844	147	77	,	,	PUNCT
eurjchem-844	147	78	and	and	CCONJ
eurjchem-844	147	79	180	180	NUM
eurjchem-844	147	80	μg	μg	NOUN
eurjchem-844	147	81	/	/	SYM
eurjchem-844	147	82	ml	ml	NOUN
eurjchem-844	147	83	)	)	PUNCT
eurjchem-844	147	84	representing	represent	VERB
eurjchem-844	147	85	80	80	NUM
eurjchem-844	147	86	,	,	PUNCT
eurjchem-844	147	87	100	100	NUM
eurjchem-844	147	88	and	and	CCONJ
eurjchem-844	147	89	120	120	NUM
eurjchem-844	147	90	%	%	NOUN
eurjchem-844	147	91	,	,	PUNCT
eurjchem-844	147	92	respectively	respectively	ADV
eurjchem-844	147	93	,	,	PUNCT
eurjchem-844	147	94	and	and	CCONJ
eurjchem-844	147	95	three	three	NUM
eurjchem-844	147	96	concentrations	concentration	NOUN
eurjchem-844	147	97	of	of	ADP
eurjchem-844	147	98	the	the	DET
eurjchem-844	147	99	laboratory	laboratory	NOUN
eurjchem-844	147	100	prepared	prepare	VERB
eurjchem-844	147	101	mixture	mixture	NOUN
eurjchem-844	147	102	of	of	ADP
eurjchem-844	147	103	vlg	vlg	PROPN
eurjchem-844	147	104	(	(	PUNCT
eurjchem-844	147	105	40	40	NUM
eurjchem-844	147	106	,	,	PUNCT
eurjchem-844	147	107	50	50	NUM
eurjchem-844	147	108	,	,	PUNCT
eurjchem-844	147	109	and	and	CCONJ
eurjchem-844	147	110	60	60	NUM
eurjchem-844	147	111	μg	μg	NOUN
eurjchem-844	147	112	/	/	SYM
eurjchem-844	147	113	ml	ml	NOUN
eurjchem-844	147	114	)	)	PUNCT
eurjchem-844	147	115	with	with	ADP
eurjchem-844	147	116	met	meet	VERB
eurjchem-844	147	117	(	(	PUNCT
eurjchem-844	147	118	400	400	NUM
eurjchem-844	147	119	,	,	PUNCT
eurjchem-844	147	120	500	500	NUM
eurjchem-844	147	121	,	,	PUNCT
eurjchem-844	147	122	and	and	CCONJ
eurjchem-844	147	123	600	600	NUM
eurjchem-844	147	124	μg	μg	NOUN
eurjchem-844	147	125	/	/	SYM
eurjchem-844	147	126	ml	ml	NOUN
eurjchem-844	147	127	)	)	PUNCT
eurjchem-844	147	128	and	and	CCONJ
eurjchem-844	147	129	cgn	cgn	PROPN
eurjchem-844	147	130	(	(	PUNCT
eurjchem-844	147	131	120	120	NUM
eurjchem-844	147	132	,	,	PUNCT
eurjchem-844	147	133	150	150	NUM
eurjchem-844	147	134	,	,	PUNCT
eurjchem-844	147	135	and	and	CCONJ
eurjchem-844	147	136	180	180	NUM
eurjchem-844	147	137	μg	μg	NOUN
eurjchem-844	147	138	/	/	SYM
eurjchem-844	147	139	ml	ml	NOUN
eurjchem-844	147	140	)	)	PUNCT
eurjchem-844	147	141	representing	represent	VERB
eurjchem-844	147	142	80	80	NUM
eurjchem-844	147	143	,	,	PUNCT
eurjchem-844	147	144	100	100	NUM
eurjchem-844	147	145	,	,	PUNCT
eurjchem-844	147	146	and	and	CCONJ
eurjchem-844	147	147	120	120	NUM
eurjchem-844	147	148	%	%	NOUN
eurjchem-844	147	149	,	,	PUNCT
eurjchem-844	147	150	respectively	respectively	ADV
eurjchem-844	147	151	,	,	PUNCT
eurjchem-844	147	152	and	and	CCONJ
eurjchem-844	147	153	three	three	NUM
eurjchem-844	147	154	concentrations	concentration	NOUN
eurjchem-844	147	155	of	of	ADP
eurjchem-844	147	156	the	the	DET
eurjchem-844	147	157	laboratory	laboratory	NOUN
eurjchem-844	147	158	prepared	prepare	VERB
eurjchem-844	147	159	mixture	mixture	NOUN
eurjchem-844	147	160	of	of	ADP
eurjchem-844	147	161	sxg	sxg	NOUN
eurjchem-844	147	162	(	(	PUNCT
eurjchem-844	147	163	4.5	4.5	NUM
eurjchem-844	147	164	,	,	PUNCT
eurjchem-844	147	165	5.6	5.6	NUM
eurjchem-844	147	166	,	,	PUNCT
eurjchem-844	147	167	and	and	CCONJ
eurjchem-844	147	168	6.7	6.7	NUM
eurjchem-844	147	169	μg	μg	NOUN
eurjchem-844	147	170	/	/	SYM
eurjchem-844	147	171	ml	ml	NOUN
eurjchem-844	147	172	)	)	PUNCT
eurjchem-844	147	173	with	with	ADP
eurjchem-844	147	174	met	meet	VERB
eurjchem-844	147	175	(	(	PUNCT
eurjchem-844	147	176	400	400	NUM
eurjchem-844	147	177	,	,	PUNCT
eurjchem-844	147	178	500	500	NUM
eurjchem-844	147	179	,	,	PUNCT
eurjchem-844	147	180	and	and	CCONJ
eurjchem-844	147	181	600	600	NUM
eurjchem-844	147	182	μg	μg	NOUN
eurjchem-844	147	183	/	/	SYM
eurjchem-844	147	184	ml	ml	NOUN
eurjchem-844	147	185	)	)	PUNCT
eurjchem-844	147	186	and	and	CCONJ
eurjchem-844	147	187	cgn	cgn	PROPN
eurjchem-844	147	188	(	(	PUNCT
eurjchem-844	147	189	120	120	NUM
eurjchem-844	147	190	,	,	PUNCT
eurjchem-844	147	191	150	150	NUM
eurjchem-844	147	192	,	,	PUNCT
eurjchem-844	147	193	and	and	CCONJ
eurjchem-844	147	194	180	180	NUM
eurjchem-844	147	195	μg	μg	NOUN
eurjchem-844	147	196	/	/	SYM
eurjchem-844	147	197	ml	ml	NOUN
eurjchem-844	147	198	)	)	PUNCT
eurjchem-844	147	199	representing	represent	VERB
eurjchem-844	147	200	80	80	NUM
eurjchem-844	147	201	,	,	PUNCT
eurjchem-844	147	202	100	100	NUM
eurjchem-844	147	203	,	,	PUNCT
eurjchem-844	147	204	120	120	NUM
eurjchem-844	147	205	%	%	NOUN
eurjchem-844	147	206	,	,	PUNCT
eurjchem-844	147	207	respectively	respectively	ADV
eurjchem-844	147	208	.	.	PUNCT
eurjchem-844	148	1	the	the	DET
eurjchem-844	148	2	repeatability	repeatability	NOUN
eurjchem-844	148	3	of	of	ADP
eurjchem-844	148	4	sample	sample	NOUN
eurjchem-844	148	5	application	application	NOUN
eurjchem-844	148	6	and	and	CCONJ
eurjchem-844	148	7	measurement	measurement	NOUN
eurjchem-844	148	8	of	of	ADP
eurjchem-844	148	9	peak	peak	NOUN
eurjchem-844	148	10	area	area	NOUN
eurjchem-844	148	11	for	for	ADP
eurjchem-844	148	12	active	active	ADJ
eurjchem-844	148	13	compound	compound	NOUN
eurjchem-844	148	14	were	be	AUX
eurjchem-844	148	15	expressed	express	VERB
eurjchem-844	148	16	in	in	ADP
eurjchem-844	148	17	terms	term	NOUN
eurjchem-844	148	18	of	of	ADP
eurjchem-844	148	19	percentage	percentage	NOUN
eurjchem-844	148	20	relative	relative	ADJ
eurjchem-844	148	21	standard	standard	ADJ
eurjchem-844	148	22	deviation	deviation	NOUN
eurjchem-844	148	23	(	(	PUNCT
eurjchem-844	148	24	%	%	INTJ
eurjchem-844	148	25	r.s.d	r.s.d	NOUN
eurjchem-844	148	26	.	.	PUNCT
eurjchem-844	148	27	)	)	PUNCT
eurjchem-844	148	28	and	and	CCONJ
eurjchem-844	148	29	found	find	VERB
eurjchem-844	148	30	to	to	PART
eurjchem-844	148	31	be	be	AUX
eurjchem-844	148	32	less	less	ADJ
eurjchem-844	148	33	than	than	ADP
eurjchem-844	148	34	1	1	NUM
eurjchem-844	148	35	%	%	NOUN
eurjchem-844	148	36	in	in	ADP
eurjchem-844	148	37	the	the	DET
eurjchem-844	148	38	three	three	NUM
eurjchem-844	148	39	concentrations	concentration	NOUN
eurjchem-844	148	40	.	.	PUNCT
eurjchem-844	149	1	results	result	NOUN
eurjchem-844	149	2	for	for	ADP
eurjchem-844	149	3	the	the	DET
eurjchem-844	149	4	determination	determination	NOUN
eurjchem-844	149	5	of	of	ADP
eurjchem-844	149	6	precision	precision	NOUN
eurjchem-844	149	7	are	be	AUX
eurjchem-844	149	8	displayed	display	VERB
eurjchem-844	149	9	in	in	ADP
eurjchem-844	149	10	tables	table	NOUN
eurjchem-844	149	11	1‐5	1‐5	NUM
eurjchem-844	149	12	.	.	PUNCT
eurjchem-844	150	1	3.3.4	3.3.4	NUM
eurjchem-844	150	2	.	.	PUNCT
eurjchem-844	150	3	specificity	specificity	NOUN
eurjchem-844	150	4	specificity	specificity	NOUN
eurjchem-844	150	5	is	be	AUX
eurjchem-844	150	6	the	the	DET
eurjchem-844	150	7	ability	ability	NOUN
eurjchem-844	150	8	of	of	ADP
eurjchem-844	150	9	the	the	DET
eurjchem-844	150	10	analytical	analytical	ADJ
eurjchem-844	150	11	method	method	NOUN
eurjchem-844	150	12	to	to	PART
eurjchem-844	150	13	measure	measure	VERB
eurjchem-844	150	14	the	the	DET
eurjchem-844	150	15	analyte	analyte	NOUN
eurjchem-844	150	16	response	response	NOUN
eurjchem-844	150	17	in	in	ADP
eurjchem-844	150	18	the	the	DET
eurjchem-844	150	19	presence	presence	NOUN
eurjchem-844	150	20	of	of	ADP
eurjchem-844	150	21	interferences	interference	NOUN
eurjchem-844	150	22	including	include	VERB
eurjchem-844	150	23	degradation	degradation	NOUN
eurjchem-844	150	24	products	product	NOUN
eurjchem-844	150	25	and	and	CCONJ
eurjchem-844	150	26	related	related	ADJ
eurjchem-844	150	27	substances	substance	NOUN
eurjchem-844	150	28	.	.	PUNCT
eurjchem-844	151	1	448	448	NUM
eurjchem-844	151	2	el‐bagary	el‐bagary	ADJ
eurjchem-844	151	3	et	et	PROPN
eurjchem-844	151	4	al	al	PROPN
eurjchem-844	151	5	.	.	PUNCT
eurjchem-844	151	6	/	/	SYM
eurjchem-844	151	7	european	european	PROPN
eurjchem-844	151	8	journal	journal	PROPN
eurjchem-844	151	9	of	of	ADP
eurjchem-844	151	10	chemistry	chemistry	NOUN
eurjchem-844	151	11	4	4	NUM
eurjchem-844	151	12	(	(	PUNCT
eurjchem-844	151	13	4	4	NUM
eurjchem-844	151	14	)	)	PUNCT
eurjchem-844	151	15	(	(	PUNCT
eurjchem-844	151	16	2013	2013	NUM
eurjchem-844	151	17	)	)	PUNCT
eurjchem-844	151	18	444‐449	444‐449	PROPN
eurjchem-844	151	19	table	table	NOUN
eurjchem-844	151	20	6	6	NUM
eurjchem-844	151	21	.	.	PUNCT
eurjchem-844	151	22	statistical	statistical	ADJ
eurjchem-844	151	23	comparison	comparison	NOUN
eurjchem-844	151	24	between	between	ADP
eurjchem-844	151	25	the	the	DET
eurjchem-844	151	26	results	result	NOUN
eurjchem-844	151	27	of	of	ADP
eurjchem-844	151	28	the	the	DET
eurjchem-844	151	29	proposed	propose	VERB
eurjchem-844	151	30	lc	lc	NOUN
eurjchem-844	151	31	method	method	NOUN
eurjchem-844	151	32	and	and	CCONJ
eurjchem-844	151	33	the	the	DET
eurjchem-844	151	34	reference	reference	NOUN
eurjchem-844	151	35	method	method	NOUN
eurjchem-844	151	36	for	for	ADP
eurjchem-844	151	37	the	the	DET
eurjchem-844	151	38	determination	determination	NOUN
eurjchem-844	151	39	of	of	ADP
eurjchem-844	151	40	metformin	metformin	NOUN
eurjchem-844	151	41	.	.	PUNCT
eurjchem-844	152	1	statistical	statistical	ADJ
eurjchem-844	152	2	term	term	NOUN
eurjchem-844	152	3	a	a	DET
eurjchem-844	152	4	reference	reference	NOUN
eurjchem-844	152	5	method	method	NOUN
eurjchem-844	152	6	b	b	PROPN
eurjchem-844	152	7	proposed	propose	VERB
eurjchem-844	152	8	method	method	NOUN
eurjchem-844	152	9	mean	mean	VERB
eurjchem-844	152	10	100.4	100.4	NUM
eurjchem-844	152	11	100.36	100.36	NUM
eurjchem-844	152	12	s.d	s.d	PROPN
eurjchem-844	152	13	.	.	PROPN
eurjchem-844	152	14	0.28	0.28	NUM
eurjchem-844	152	15	1.15	1.15	NUM
eurjchem-844	152	16	s.e	s.e	PROPN
eurjchem-844	152	17	.	.	PROPN
eurjchem-844	152	18	0.13	0.13	NUM
eurjchem-844	152	19	0.51	0.51	NUM
eurjchem-844	152	20	%	%	NOUN
eurjchem-844	152	21	r.s.d	r.s.d	NOUN
eurjchem-844	152	22	.	.	PUNCT
eurjchem-844	153	1	0.28	0.28	NUM
eurjchem-844	153	2	1.15	1.15	NUM
eurjchem-844	153	3	n	n	NUM
eurjchem-844	153	4	5	5	NUM
eurjchem-844	153	5	5	5	NUM
eurjchem-844	153	6	v	v	NUM
eurjchem-844	153	7	0.08	0.08	NUM
eurjchem-844	153	8	1.32	1.32	NUM
eurjchem-844	153	9	t	t	NOUN
eurjchem-844	153	10	(	(	PUNCT
eurjchem-844	153	11	2.306	2.306	NUM
eurjchem-844	153	12	)	)	PUNCT
eurjchem-844	153	13	c	c	NOUN
eurjchem-844	153	14	‐	‐	SYM
eurjchem-844	153	15	0.08	0.08	NUM
eurjchem-844	153	16	a	a	DET
eurjchem-844	153	17	s.d	s.d	PROPN
eurjchem-844	153	18	.	.	PUNCT
eurjchem-844	153	19	:	:	PUNCT
eurjchem-844	153	20	standard	standard	ADJ
eurjchem-844	153	21	deviation	deviation	NOUN
eurjchem-844	153	22	,	,	PUNCT
eurjchem-844	153	23	s.e	s.e	PROPN
eurjchem-844	153	24	.	.	PROPN
eurjchem-844	153	25	:	:	PUNCT
eurjchem-844	153	26	standard	standard	ADJ
eurjchem-844	153	27	error	error	NOUN
eurjchem-844	153	28	,	,	PUNCT
eurjchem-844	153	29	%	%	INTJ
eurjchem-844	153	30	r.s.d	r.s.d	NOUN
eurjchem-844	153	31	.	.	PUNCT
eurjchem-844	153	32	:	:	PUNCT
eurjchem-844	153	33	relative	relative	ADJ
eurjchem-844	153	34	standard	standard	ADJ
eurjchem-844	153	35	deviation	deviation	NOUN
eurjchem-844	153	36	,	,	PUNCT
eurjchem-844	153	37	n	n	CCONJ
eurjchem-844	153	38	:	:	PUNCT
eurjchem-844	153	39	number	number	NOUN
eurjchem-844	153	40	of	of	ADP
eurjchem-844	153	41	samples	sample	NOUN
eurjchem-844	153	42	,	,	PUNCT
eurjchem-844	153	43	v	v	NOUN
eurjchem-844	153	44	:	:	PUNCT
eurjchem-844	153	45	variance	variance	NOUN
eurjchem-844	153	46	.	.	PUNCT
eurjchem-844	154	1	b	b	X
eurjchem-844	154	2	reference	reference	NOUN
eurjchem-844	154	3	method	method	NOUN
eurjchem-844	154	4	for	for	ADP
eurjchem-844	154	5	the	the	DET
eurjchem-844	154	6	spectrophotometric	spectrophotometric	ADJ
eurjchem-844	154	7	determination	determination	NOUN
eurjchem-844	154	8	of	of	ADP
eurjchem-844	154	9	metformin	metformin	NOUN
eurjchem-844	154	10	in	in	ADP
eurjchem-844	154	11	the	the	DET
eurjchem-844	154	12	indian	indian	ADJ
eurjchem-844	154	13	pharmacopeia	pharmacopeia	NOUN
eurjchem-844	154	14	[	[	X
eurjchem-844	154	15	24	24	NUM
eurjchem-844	154	16	]	]	PUNCT
eurjchem-844	154	17	.	.	PUNCT
eurjchem-844	155	1	c	c	NOUN
eurjchem-844	155	2	figures	figure	NOUN
eurjchem-844	155	3	in	in	ADP
eurjchem-844	155	4	parentheses	parenthesis	NOUN
eurjchem-844	155	5	are	be	AUX
eurjchem-844	155	6	the	the	DET
eurjchem-844	155	7	theoretical	theoretical	ADJ
eurjchem-844	155	8	t	t	NOUN
eurjchem-844	155	9	value	value	NOUN
eurjchem-844	155	10	at	at	ADP
eurjchem-844	155	11	(	(	PUNCT
eurjchem-844	155	12	p	p	X
eurjchem-844	155	13	=	=	NOUN
eurjchem-844	155	14	0.05	0.05	NUM
eurjchem-844	155	15	)	)	PUNCT
eurjchem-844	155	16	.	.	PUNCT
eurjchem-844	156	1	no	no	DET
eurjchem-844	156	2	significant	significant	ADJ
eurjchem-844	156	3	difference	difference	NOUN
eurjchem-844	156	4	between	between	ADP
eurjchem-844	156	5	groups	group	NOUN
eurjchem-844	156	6	by	by	ADP
eurjchem-844	156	7	using	use	VERB
eurjchem-844	156	8	one	one	NUM
eurjchem-844	156	9	way	way	NOUN
eurjchem-844	156	10	anova	anova	X
eurjchem-844	156	11	with	with	ADP
eurjchem-844	156	12	f	f	PROPN
eurjchem-844	156	13	=	=	NOUN
eurjchem-844	156	14	0.01	0.01	NUM
eurjchem-844	156	15	and	and	CCONJ
eurjchem-844	156	16	p	p	X
eurjchem-844	156	17	=	=	PROPN
eurjchem-844	156	18	0.94	0.94	NUM
eurjchem-844	156	19	.	.	PUNCT
eurjchem-844	156	20	table	table	NOUN
eurjchem-844	156	21	7	7	NUM
eurjchem-844	156	22	.	.	PUNCT
eurjchem-844	157	1	statistical	statistical	ADJ
eurjchem-844	157	2	comparison	comparison	NOUN
eurjchem-844	157	3	between	between	ADP
eurjchem-844	157	4	the	the	DET
eurjchem-844	157	5	results	result	NOUN
eurjchem-844	157	6	of	of	ADP
eurjchem-844	157	7	the	the	DET
eurjchem-844	157	8	lc	lc	NOUN
eurjchem-844	157	9	method	method	NOUN
eurjchem-844	157	10	and	and	CCONJ
eurjchem-844	157	11	the	the	DET
eurjchem-844	157	12	reference	reference	NOUN
eurjchem-844	157	13	methods	method	NOUN
eurjchem-844	157	14	for	for	ADP
eurjchem-844	157	15	the	the	DET
eurjchem-844	157	16	determination	determination	NOUN
eurjchem-844	157	17	of	of	ADP
eurjchem-844	157	18	sitagliptin	sitagliptin	NOUN
eurjchem-844	157	19	,	,	PUNCT
eurjchem-844	157	20	vildagliptin	vildagliptin	NOUN
eurjchem-844	157	21	and	and	CCONJ
eurjchem-844	157	22	saxagliptin	saxagliptin	NOUN
eurjchem-844	157	23	.	.	PUNCT
eurjchem-844	158	1	statistical	statistical	ADJ
eurjchem-844	158	2	term	term	NOUN
eurjchem-844	158	3	reference	reference	NOUN
eurjchem-844	158	4	method	method	NOUN
eurjchem-844	158	5	for	for	ADP
eurjchem-844	158	6	sitagliptin	sitagliptin	NOUN
eurjchem-844	158	7	b	b	PROPN
eurjchem-844	158	8	hplc	hplc	NOUN
eurjchem-844	158	9	method	method	NOUN
eurjchem-844	158	10	reference	reference	NOUN
eurjchem-844	158	11	method	method	NOUN
eurjchem-844	158	12	for	for	ADP
eurjchem-844	158	13	vildagliptin	vildagliptin	NOUN
eurjchem-844	158	14	c	c	PROPN
eurjchem-844	158	15	hplc	hplc	NOUN
eurjchem-844	158	16	method	method	NOUN
eurjchem-844	158	17	reference	reference	NOUN
eurjchem-844	158	18	method	method	NOUN
eurjchem-844	158	19	for	for	ADP
eurjchem-844	158	20	saxagliptin	saxagliptin	NOUN
eurjchem-844	158	21	d	d	PROPN
eurjchem-844	158	22	hplc	hplc	NOUN
eurjchem-844	158	23	method	method	NOUN
eurjchem-844	158	24	mean	mean	VERB
eurjchem-844	158	25	100.50	100.50	NUM
eurjchem-844	158	26	100.32	100.32	NUM
eurjchem-844	158	27	100.01	100.01	NUM
eurjchem-844	158	28	100.17	100.17	NUM
eurjchem-844	158	29	100.20	100.20	NUM
eurjchem-844	158	30	100.01	100.01	NUM
eurjchem-844	158	31	s.d	s.d	PROPN
eurjchem-844	158	32	.	.	PROPN
eurjchem-844	158	33	1.39	1.39	NUM
eurjchem-844	158	34	1.44	1.44	NUM
eurjchem-844	158	35	0.99	0.99	NUM
eurjchem-844	158	36	1.41	1.41	NUM
eurjchem-844	158	37	1.10	1.10	NUM
eurjchem-844	158	38	1.51	1.51	NUM
eurjchem-844	158	39	s.e	s.e	PROPN
eurjchem-844	158	40	.	.	PROPN
eurjchem-844	158	41	0.62	0.62	NUM
eurjchem-844	158	42	0.64	0.64	NUM
eurjchem-844	158	43	0.44	0.44	NUM
eurjchem-844	158	44	0.63	0.63	NUM
eurjchem-844	158	45	0.49	0.49	NUM
eurjchem-844	158	46	0.68	0.68	NUM
eurjchem-844	158	47	%	%	NOUN
eurjchem-844	158	48	r.s.d	r.s.d	NOUN
eurjchem-844	158	49	.	.	PUNCT
eurjchem-844	159	1	1.38	1.38	NUM
eurjchem-844	159	2	1.44	1.44	NUM
eurjchem-844	159	3	0.99	0.99	NUM
eurjchem-844	159	4	1.41	1.41	NUM
eurjchem-844	159	5	1.1	1.1	NUM
eurjchem-844	159	6	1.51	1.51	NUM
eurjchem-844	159	7	n	n	NUM
eurjchem-844	159	8	5	5	NUM
eurjchem-844	159	9	5	5	NUM
eurjchem-844	159	10	5	5	NUM
eurjchem-844	159	11	5	5	NUM
eurjchem-844	159	12	5	5	NUM
eurjchem-844	159	13	5	5	NUM
eurjchem-844	159	14	v	v	ADP
eurjchem-844	159	15	1.93	1.93	NUM
eurjchem-844	159	16	2.1	2.1	NUM
eurjchem-844	159	17	0.98	0.98	NUM
eurjchem-844	159	18	1.98	1.98	NUM
eurjchem-844	159	19	1.21	1.21	NUM
eurjchem-844	159	20	2.28	2.28	NUM
eurjchem-844	159	21	t	t	NOUN
eurjchem-844	159	22	(	(	PUNCT
eurjchem-844	159	23	2.306	2.306	NUM
eurjchem-844	159	24	)	)	PUNCT
eurjchem-844	159	25	a	a	DET
eurjchem-844	159	26	0.20	0.20	NUM
eurjchem-844	159	27	0.21	0.21	NUM
eurjchem-844	159	28	0.23	0.23	NUM
eurjchem-844	159	29	a	a	DET
eurjchem-844	159	30	figure	figure	NOUN
eurjchem-844	159	31	in	in	ADP
eurjchem-844	159	32	parentheses	parenthesis	NOUN
eurjchem-844	159	33	are	be	AUX
eurjchem-844	159	34	the	the	DET
eurjchem-844	159	35	theoretical	theoretical	ADJ
eurjchem-844	159	36	t	t	NOUN
eurjchem-844	159	37	value	value	NOUN
eurjchem-844	159	38	at	at	ADP
eurjchem-844	159	39	(	(	PUNCT
eurjchem-844	159	40	p	p	X
eurjchem-844	159	41	=	=	NOUN
eurjchem-844	159	42	0.05	0.05	NUM
eurjchem-844	159	43	)	)	PUNCT
eurjchem-844	159	44	.	.	PUNCT
eurjchem-844	160	1	b	b	X
eurjchem-844	160	2	reference	reference	NOUN
eurjchem-844	160	3	method	method	NOUN
eurjchem-844	160	4	:	:	PUNCT
eurjchem-844	160	5	aliquots	aliquot	NOUN
eurjchem-844	160	6	of	of	ADP
eurjchem-844	160	7	standard	standard	ADJ
eurjchem-844	160	8	solutions	solution	NOUN
eurjchem-844	160	9	in	in	ADP
eurjchem-844	160	10	distilled	distil	VERB
eurjchem-844	160	11	water	water	NOUN
eurjchem-844	160	12	containing	contain	VERB
eurjchem-844	160	13	2‐10	2‐10	NUM
eurjchem-844	160	14	μg	μg	PROPN
eurjchem-844	160	15	/	/	SYM
eurjchem-844	160	16	ml	ml	PROPN
eurjchem-844	160	17	stg	stg	PROPN
eurjchem-844	160	18	were	be	AUX
eurjchem-844	160	19	measured	measure	VERB
eurjchem-844	160	20	using	use	VERB
eurjchem-844	160	21	methanol	methanol	NOUN
eurjchem-844	160	22	as	as	ADP
eurjchem-844	160	23	a	a	DET
eurjchem-844	160	24	blank	blank	NOUN
eurjchem-844	161	1	[	[	X
eurjchem-844	161	2	5	5	NUM
eurjchem-844	161	3	]	]	PUNCT
eurjchem-844	161	4	.	.	PUNCT
eurjchem-844	162	1	no	no	DET
eurjchem-844	162	2	significant	significant	ADJ
eurjchem-844	162	3	difference	difference	NOUN
eurjchem-844	162	4	between	between	ADP
eurjchem-844	162	5	groups	group	NOUN
eurjchem-844	162	6	of	of	ADP
eurjchem-844	162	7	sitagliptin	sitagliptin	NOUN
eurjchem-844	162	8	by	by	ADP
eurjchem-844	162	9	using	use	VERB
eurjchem-844	162	10	one	one	NUM
eurjchem-844	162	11	way	way	NOUN
eurjchem-844	162	12	anova	anova	X
eurjchem-844	162	13	with	with	ADP
eurjchem-844	162	14	f	f	PROPN
eurjchem-844	162	15	=	=	PROPN
eurjchem-844	162	16	0.04	0.04	NUM
eurjchem-844	162	17	and	and	CCONJ
eurjchem-844	162	18	p	p	NOUN
eurjchem-844	162	19	=	=	NOUN
eurjchem-844	162	20	0.85	0.85	NUM
eurjchem-844	162	21	.	.	PUNCT
eurjchem-844	163	1	c	c	PROPN
eurjchem-844	163	2	reference	reference	NOUN
eurjchem-844	163	3	method	method	NOUN
eurjchem-844	163	4	:	:	PUNCT
eurjchem-844	163	5	aliquots	aliquot	NOUN
eurjchem-844	163	6	of	of	ADP
eurjchem-844	163	7	standard	standard	ADJ
eurjchem-844	163	8	solutions	solution	NOUN
eurjchem-844	163	9	in	in	ADP
eurjchem-844	163	10	distilled	distil	VERB
eurjchem-844	163	11	water	water	NOUN
eurjchem-844	163	12	containing	contain	VERB
eurjchem-844	163	13	5‐25	5‐25	NUM
eurjchem-844	163	14	μg	μg	NOUN
eurjchem-844	163	15	/	/	SYM
eurjchem-844	163	16	ml	ml	ADP
eurjchem-844	163	17	vdg	vdg	NOUN
eurjchem-844	163	18	were	be	AUX
eurjchem-844	163	19	measured	measure	VERB
eurjchem-844	163	20	using	use	VERB
eurjchem-844	163	21	water	water	NOUN
eurjchem-844	163	22	as	as	ADP
eurjchem-844	163	23	a	a	DET
eurjchem-844	163	24	blank	blank	NOUN
eurjchem-844	164	1	[	[	X
eurjchem-844	164	2	5	5	NUM
eurjchem-844	164	3	]	]	PUNCT
eurjchem-844	164	4	.	.	PUNCT
eurjchem-844	165	1	no	no	DET
eurjchem-844	165	2	significant	significant	ADJ
eurjchem-844	165	3	difference	difference	NOUN
eurjchem-844	165	4	between	between	ADP
eurjchem-844	165	5	groups	group	NOUN
eurjchem-844	165	6	of	of	ADP
eurjchem-844	165	7	vildagliptin	vildagliptin	NOUN
eurjchem-844	165	8	by	by	ADP
eurjchem-844	165	9	using	use	VERB
eurjchem-844	165	10	one	one	NUM
eurjchem-844	165	11	way	way	NOUN
eurjchem-844	165	12	anova	anova	X
eurjchem-844	165	13	with	with	ADP
eurjchem-844	165	14	f	f	PROPN
eurjchem-844	165	15	=	=	PROPN
eurjchem-844	165	16	0.04	0.04	NUM
eurjchem-844	165	17	and	and	CCONJ
eurjchem-844	165	18	p	p	NOUN
eurjchem-844	165	19	=	=	PROPN
eurjchem-844	165	20	0.84	0.84	NUM
eurjchem-844	165	21	.	.	PUNCT
eurjchem-844	166	1	d	d	PRON
eurjchem-844	166	2	reference	reference	NOUN
eurjchem-844	166	3	method	method	NOUN
eurjchem-844	166	4	:	:	PUNCT
eurjchem-844	166	5	aliquots	aliquot	NOUN
eurjchem-844	166	6	of	of	ADP
eurjchem-844	166	7	standard	standard	ADJ
eurjchem-844	166	8	solutions	solution	NOUN
eurjchem-844	166	9	in	in	ADP
eurjchem-844	166	10	distilled	distil	VERB
eurjchem-844	166	11	water	water	NOUN
eurjchem-844	166	12	containing	contain	VERB
eurjchem-844	166	13	5‐40	5‐40	NUM
eurjchem-844	166	14	μg	μg	NOUN
eurjchem-844	166	15	/	/	SYM
eurjchem-844	166	16	ml	ml	NOUN
eurjchem-844	166	17	sxg	sxg	NOUN
eurjchem-844	166	18	were	be	AUX
eurjchem-844	166	19	measured	measure	VERB
eurjchem-844	166	20	using	use	VERB
eurjchem-844	166	21	methanol	methanol	NOUN
eurjchem-844	166	22	as	as	ADP
eurjchem-844	166	23	a	a	DET
eurjchem-844	166	24	blank	blank	NOUN
eurjchem-844	167	1	[	[	X
eurjchem-844	167	2	9	9	NUM
eurjchem-844	167	3	]	]	PUNCT
eurjchem-844	167	4	.	.	PUNCT
eurjchem-844	168	1	no	no	DET
eurjchem-844	168	2	significant	significant	ADJ
eurjchem-844	168	3	difference	difference	NOUN
eurjchem-844	168	4	between	between	ADP
eurjchem-844	168	5	groups	group	NOUN
eurjchem-844	168	6	of	of	ADP
eurjchem-844	168	7	saxagliptin	saxagliptin	NOUN
eurjchem-844	168	8	by	by	ADP
eurjchem-844	168	9	using	use	VERB
eurjchem-844	168	10	one	one	NUM
eurjchem-844	168	11	way	way	NOUN
eurjchem-844	168	12	anova	anova	X
eurjchem-844	168	13	with	with	ADP
eurjchem-844	168	14	f	f	PROPN
eurjchem-844	168	15	=	=	PROPN
eurjchem-844	168	16	0.05	0.05	NUM
eurjchem-844	168	17	and	and	CCONJ
eurjchem-844	168	18	p	p	NOUN
eurjchem-844	168	19	=	=	NOUN
eurjchem-844	168	20	0.83	0.83	NUM
eurjchem-844	168	21	.	.	PUNCT
eurjchem-844	168	22	figure	figure	NOUN
eurjchem-844	168	23	7	7	NUM
eurjchem-844	168	24	.	.	PUNCT
eurjchem-844	169	1	a	a	DET
eurjchem-844	169	2	typical	typical	ADJ
eurjchem-844	169	3	lc	lc	NOUN
eurjchem-844	169	4	chromatogram	chromatogram	NOUN
eurjchem-844	169	5	of	of	ADP
eurjchem-844	169	6	25	25	NUM
eurjchem-844	169	7	µl	µl	ADP
eurjchem-844	169	8	injector	injector	NOUN
eurjchem-844	169	9	of	of	ADP
eurjchem-844	169	10	kombiglyze	kombiglyze	NOUN
eurjchem-844	169	11	®	®	NOUN
eurjchem-844	169	12	sample	sample	NOUN
eurjchem-844	169	13	solution	solution	NOUN
eurjchem-844	169	14	,	,	PUNCT
eurjchem-844	169	15	(	(	PUNCT
eurjchem-844	169	16	a	a	X
eurjchem-844	169	17	)	)	PUNCT
eurjchem-844	169	18	metformin	metformin	NOUN
eurjchem-844	169	19	hydrochloride	hydrochloride	NOUN
eurjchem-844	169	20	(	(	PUNCT
eurjchem-844	169	21	500	500	NUM
eurjchem-844	169	22	μg	μg	NOUN
eurjchem-844	169	23	/	/	SYM
eurjchem-844	169	24	ml	ml	NOUN
eurjchem-844	169	25	)	)	PUNCT
eurjchem-844	169	26	and	and	CCONJ
eurjchem-844	169	27	(	(	PUNCT
eurjchem-844	169	28	b	b	NOUN
eurjchem-844	169	29	)	)	PUNCT
eurjchem-844	169	30	saxagliptin	saxagliptin	NOUN
eurjchem-844	169	31	hydrochloride	hydrochloride	NOUN
eurjchem-844	169	32	(	(	PUNCT
eurjchem-844	169	33	5.6	5.6	NUM
eurjchem-844	169	34	μg	μg	NOUN
eurjchem-844	169	35	/	/	SYM
eurjchem-844	169	36	ml	ml	NOUN
eurjchem-844	169	37	)	)	PUNCT
eurjchem-844	169	38	.	.	PUNCT
eurjchem-844	170	1	in	in	ADP
eurjchem-844	170	2	the	the	DET
eurjchem-844	170	3	present	present	ADJ
eurjchem-844	170	4	work	work	NOUN
eurjchem-844	170	5	,	,	PUNCT
eurjchem-844	170	6	specificity	specificity	NOUN
eurjchem-844	170	7	was	be	AUX
eurjchem-844	170	8	checked	check	VERB
eurjchem-844	170	9	by	by	ADP
eurjchem-844	170	10	analyzing	analyze	VERB
eurjchem-844	170	11	stg	stg	PROPN
eurjchem-844	170	12	with	with	ADP
eurjchem-844	170	13	met	meet	VERB
eurjchem-844	170	14	,	,	PUNCT
eurjchem-844	170	15	vdg	vdg	NOUN
eurjchem-844	170	16	with	with	ADP
eurjchem-844	170	17	met	meet	VERB
eurjchem-844	170	18	and	and	CCONJ
eurjchem-844	170	19	sxg	sxg	ADJ
eurjchem-844	170	20	with	with	ADP
eurjchem-844	170	21	met	meet	VERB
eurjchem-844	170	22	in	in	ADP
eurjchem-844	170	23	laboratory	laboratory	NOUN
eurjchem-844	170	24	prepared	prepare	VERB
eurjchem-844	170	25	mixtures	mixture	NOUN
eurjchem-844	170	26	with	with	ADP
eurjchem-844	170	27	cgn	cgn	PROPN
eurjchem-844	170	28	.	.	PUNCT
eurjchem-844	171	1	good	good	ADJ
eurjchem-844	171	2	resolution	resolution	NOUN
eurjchem-844	171	3	and	and	CCONJ
eurjchem-844	171	4	absence	absence	NOUN
eurjchem-844	171	5	of	of	ADP
eurjchem-844	171	6	interference	interference	NOUN
eurjchem-844	171	7	between	between	ADP
eurjchem-844	171	8	drugs	drug	NOUN
eurjchem-844	171	9	being	be	AUX
eurjchem-844	171	10	analyzed	analyze	VERB
eurjchem-844	171	11	are	be	AUX
eurjchem-844	171	12	shown	show	VERB
eurjchem-844	171	13	in	in	ADP
eurjchem-844	171	14	figure	figure	NOUN
eurjchem-844	171	15	2‐7	2‐7	NUM
eurjchem-844	171	16	.	.	PUNCT
eurjchem-844	172	1	besides	besides	SCONJ
eurjchem-844	172	2	,	,	PUNCT
eurjchem-844	172	3	the	the	DET
eurjchem-844	172	4	chromatograms	chromatogram	NOUN
eurjchem-844	172	5	of	of	ADP
eurjchem-844	172	6	the	the	DET
eurjchem-844	172	7	pharmaceutical	pharmaceutical	ADJ
eurjchem-844	172	8	formulation	formulation	NOUN
eurjchem-844	172	9	samples	sample	NOUN
eurjchem-844	172	10	were	be	AUX
eurjchem-844	172	11	checked	check	VERB
eurjchem-844	172	12	for	for	ADP
eurjchem-844	172	13	the	the	DET
eurjchem-844	172	14	appearance	appearance	NOUN
eurjchem-844	172	15	of	of	ADP
eurjchem-844	172	16	any	any	DET
eurjchem-844	172	17	extra	extra	ADJ
eurjchem-844	172	18	peaks	peak	NOUN
eurjchem-844	172	19	.	.	PUNCT
eurjchem-844	173	1	no	no	DET
eurjchem-844	173	2	chromatographic	chromatographic	ADJ
eurjchem-844	173	3	interference	interference	NOUN
eurjchem-844	173	4	from	from	ADP
eurjchem-844	173	5	any	any	PRON
eurjchem-844	173	6	of	of	ADP
eurjchem-844	173	7	the	the	DET
eurjchem-844	173	8	excipients	excipient	NOUN
eurjchem-844	173	9	was	be	AUX
eurjchem-844	173	10	found	find	VERB
eurjchem-844	173	11	at	at	ADP
eurjchem-844	173	12	the	the	DET
eurjchem-844	173	13	retention	retention	NOUN
eurjchem-844	173	14	times	time	NOUN
eurjchem-844	173	15	of	of	ADP
eurjchem-844	173	16	the	the	DET
eurjchem-844	173	17	examined	examine	VERB
eurjchem-844	173	18	drugs	drug	NOUN
eurjchem-844	173	19	(	(	PUNCT
eurjchem-844	173	20	figure	figure	NOUN
eurjchem-844	173	21	5‐7	5‐7	NUM
eurjchem-844	173	22	)	)	PUNCT
eurjchem-844	173	23	.	.	PUNCT
eurjchem-844	174	1	in	in	ADP
eurjchem-844	174	2	addition	addition	NOUN
eurjchem-844	174	3	,	,	PUNCT
eurjchem-844	174	4	the	the	DET
eurjchem-844	174	5	chromatograms	chromatogram	NOUN
eurjchem-844	174	6	of	of	ADP
eurjchem-844	174	7	the	the	DET
eurjchem-844	174	8	drugs	drug	NOUN
eurjchem-844	174	9	in	in	ADP
eurjchem-844	174	10	the	the	DET
eurjchem-844	174	11	samples	sample	NOUN
eurjchem-844	174	12	’	'	PUNCT
eurjchem-844	174	13	solutions	solution	NOUN
eurjchem-844	174	14	were	be	AUX
eurjchem-844	174	15	found	find	VERB
eurjchem-844	174	16	identical	identical	ADJ
eurjchem-844	174	17	to	to	ADP
eurjchem-844	174	18	the	the	DET
eurjchem-844	174	19	chromatograms	chromatogram	NOUN
eurjchem-844	174	20	received	receive	VERB
eurjchem-844	174	21	by	by	ADP
eurjchem-844	174	22	the	the	DET
eurjchem-844	174	23	standard	standard	ADJ
eurjchem-844	174	24	solutions	solution	NOUN
eurjchem-844	174	25	at	at	ADP
eurjchem-844	174	26	the	the	DET
eurjchem-844	174	27	wavelengths	wavelength	NOUN
eurjchem-844	174	28	applied	apply	VERB
eurjchem-844	174	29	.	.	PUNCT
eurjchem-844	175	1	moreover	moreover	ADV
eurjchem-844	175	2	,	,	PUNCT
eurjchem-844	175	3	good	good	ADJ
eurjchem-844	175	4	results	result	NOUN
eurjchem-844	175	5	were	be	AUX
eurjchem-844	175	6	obtained	obtain	VERB
eurjchem-844	175	7	for	for	ADP
eurjchem-844	175	8	the	the	DET
eurjchem-844	175	9	determination	determination	NOUN
eurjchem-844	175	10	of	of	ADP
eurjchem-844	175	11	the	the	DET
eurjchem-844	175	12	cited	cite	VERB
eurjchem-844	175	13	drugs	drug	NOUN
eurjchem-844	175	14	in	in	ADP
eurjchem-844	175	15	the	the	DET
eurjchem-844	175	16	two	two	NUM
eurjchem-844	175	17	dosage	dosage	NOUN
eurjchem-844	175	18	forms	form	NOUN
eurjchem-844	175	19	,	,	PUNCT
eurjchem-844	175	20	tables	table	NOUN
eurjchem-844	175	21	4	4	NUM
eurjchem-844	175	22	and	and	CCONJ
eurjchem-844	175	23	5	5	NUM
eurjchem-844	175	24	.	.	PUNCT
eurjchem-844	176	1	these	these	DET
eurjchem-844	176	2	results	result	NOUN
eurjchem-844	176	3	confirm	confirm	VERB
eurjchem-844	176	4	the	the	DET
eurjchem-844	176	5	absence	absence	NOUN
eurjchem-844	176	6	of	of	ADP
eurjchem-844	176	7	interference	interference	NOUN
eurjchem-844	176	8	from	from	ADP
eurjchem-844	176	9	other	other	ADJ
eurjchem-844	176	10	materials	material	NOUN
eurjchem-844	176	11	in	in	ADP
eurjchem-844	176	12	the	the	DET
eurjchem-844	176	13	pharmaceutical	pharmaceutical	NOUN
eurjchem-844	176	14	formulations	formulation	NOUN
eurjchem-844	176	15	and	and	CCONJ
eurjchem-844	176	16	therefore	therefore	ADV
eurjchem-844	176	17	confirm	confirm	VERB
eurjchem-844	176	18	the	the	DET
eurjchem-844	176	19	specificity	specificity	NOUN
eurjchem-844	176	20	of	of	ADP
eurjchem-844	176	21	the	the	DET
eurjchem-844	176	22	two	two	NUM
eurjchem-844	176	23	proposed	propose	VERB
eurjchem-844	176	24	methods	method	NOUN
eurjchem-844	176	25	.	.	PUNCT
eurjchem-844	177	1	3.3.5	3.3.5	X
eurjchem-844	177	2	.	.	PUNCT
eurjchem-844	178	1	robustness	robustness	VERB
eurjchem-844	178	2	the	the	DET
eurjchem-844	178	3	most	most	ADV
eurjchem-844	178	4	important	important	ADJ
eurjchem-844	178	5	parameter	parameter	NOUN
eurjchem-844	178	6	to	to	PART
eurjchem-844	178	7	be	be	AUX
eurjchem-844	178	8	studied	study	VERB
eurjchem-844	178	9	was	be	AUX
eurjchem-844	178	10	the	the	DET
eurjchem-844	178	11	resolution	resolution	NOUN
eurjchem-844	178	12	factor	factor	NOUN
eurjchem-844	178	13	between	between	ADP
eurjchem-844	178	14	the	the	DET
eurjchem-844	178	15	two	two	NUM
eurjchem-844	178	16	peaks	peak	NOUN
eurjchem-844	178	17	of	of	ADP
eurjchem-844	178	18	stg	stg	PROPN
eurjchem-844	178	19	and	and	CCONJ
eurjchem-844	178	20	met	meet	VERB
eurjchem-844	178	21	,	,	PUNCT
eurjchem-844	178	22	vlg	vlg	PROPN
eurjchem-844	178	23	and	and	CCONJ
eurjchem-844	178	24	met	meet	VERB
eurjchem-844	178	25	and	and	CCONJ
eurjchem-844	178	26	also	also	ADV
eurjchem-844	178	27	between	between	ADP
eurjchem-844	178	28	the	the	DET
eurjchem-844	178	29	two	two	NUM
eurjchem-844	178	30	peaks	peak	NOUN
eurjchem-844	178	31	of	of	ADP
eurjchem-844	178	32	sxg	sxg	NOUN
eurjchem-844	178	33	and	and	CCONJ
eurjchem-844	178	34	met	meet	VERB
eurjchem-844	178	35	.	.	PUNCT
eurjchem-844	179	1	besides	besides	SCONJ
eurjchem-844	179	2	,	,	PUNCT
eurjchem-844	179	3	any	any	DET
eurjchem-844	179	4	interference	interference	NOUN
eurjchem-844	179	5	from	from	ADP
eurjchem-844	179	6	the	the	DET
eurjchem-844	179	7	peak	peak	NOUN
eurjchem-844	179	8	of	of	ADP
eurjchem-844	179	9	cgn	cgn	PROPN
eurjchem-844	179	10	was	be	AUX
eurjchem-844	179	11	checked	check	VERB
eurjchem-844	179	12	visually	visually	ADV
eurjchem-844	179	13	.	.	PUNCT
eurjchem-844	180	1	the	the	DET
eurjchem-844	180	2	flow	flow	NOUN
eurjchem-844	180	3	rate	rate	NOUN
eurjchem-844	180	4	of	of	ADP
eurjchem-844	180	5	the	the	DET
eurjchem-844	180	6	mobile	mobile	ADJ
eurjchem-844	180	7	phase	phase	NOUN
eurjchem-844	180	8	was	be	AUX
eurjchem-844	180	9	changed	change	VERB
eurjchem-844	180	10	from	from	ADP
eurjchem-844	180	11	1	1	NUM
eurjchem-844	180	12	ml	ml	NOUN
eurjchem-844	180	13	/	/	SYM
eurjchem-844	180	14	min	min	NOUN
eurjchem-844	180	15	to	to	PART
eurjchem-844	180	16	0.8	0.8	NUM
eurjchem-844	180	17	ml	ml	NOUN
eurjchem-844	180	18	/	/	SYM
eurjchem-844	180	19	min	min	NOUN
eurjchem-844	180	20	and	and	CCONJ
eurjchem-844	180	21	1.2	1.2	NUM
eurjchem-844	180	22	ml	ml	NOUN
eurjchem-844	180	23	/	/	SYM
eurjchem-844	180	24	min	min	NOUN
eurjchem-844	180	25	,	,	PUNCT
eurjchem-844	180	26	where	where	SCONJ
eurjchem-844	180	27	resolution	resolution	NOUN
eurjchem-844	180	28	factors	factor	NOUN
eurjchem-844	180	29	obtained	obtain	VERB
eurjchem-844	180	30	were	be	AUX
eurjchem-844	180	31	(	(	PUNCT
eurjchem-844	180	32	4.1	4.1	NUM
eurjchem-844	180	33	,	,	PUNCT
eurjchem-844	180	34	2.5	2.5	NUM
eurjchem-844	180	35	,	,	PUNCT
eurjchem-844	180	36	and	and	CCONJ
eurjchem-844	180	37	3.2	3.2	NUM
eurjchem-844	180	38	)	)	PUNCT
eurjchem-844	180	39	,	,	PUNCT
eurjchem-844	180	40	(	(	PUNCT
eurjchem-844	180	41	4.2	4.2	NUM
eurjchem-844	180	42	,	,	PUNCT
eurjchem-844	180	43	2.45	2.45	NUM
eurjchem-844	180	44	,	,	PUNCT
eurjchem-844	180	45	and	and	CCONJ
eurjchem-844	180	46	3.11	3.11	NUM
eurjchem-844	180	47	)	)	PUNCT
eurjchem-844	180	48	and	and	CCONJ
eurjchem-844	180	49	(	(	PUNCT
eurjchem-844	180	50	4.15	4.15	NUM
eurjchem-844	180	51	,	,	PUNCT
eurjchem-844	180	52	2.6	2.6	NUM
eurjchem-844	180	53	,	,	PUNCT
eurjchem-844	180	54	and	and	CCONJ
eurjchem-844	180	55	3.2	3.2	NUM
eurjchem-844	180	56	)	)	PUNCT
eurjchem-844	180	57	,	,	PUNCT
eurjchem-844	180	58	respectively	respectively	ADV
eurjchem-844	180	59	.	.	PUNCT
eurjchem-844	181	1	the	the	DET
eurjchem-844	181	2	organic	organic	ADJ
eurjchem-844	181	3	strength	strength	NOUN
eurjchem-844	181	4	was	be	AUX
eurjchem-844	181	5	changed	change	VERB
eurjchem-844	181	6	by	by	ADP
eurjchem-844	181	7	%	%	INTJ
eurjchem-844	181	8	±2	±2	NOUN
eurjchem-844	181	9	where	where	SCONJ
eurjchem-844	181	10	resolution	resolution	NOUN
eurjchem-844	181	11	factors	factor	NOUN
eurjchem-844	181	12	obtained	obtain	VERB
eurjchem-844	181	13	were	be	AUX
eurjchem-844	181	14	(	(	PUNCT
eurjchem-844	181	15	4.1	4.1	NUM
eurjchem-844	181	16	,	,	PUNCT
eurjchem-844	181	17	2.5	2.5	NUM
eurjchem-844	181	18	,	,	PUNCT
eurjchem-844	181	19	and	and	CCONJ
eurjchem-844	181	20	3.2	3.2	NUM
eurjchem-844	181	21	)	)	PUNCT
eurjchem-844	181	22	,	,	PUNCT
eurjchem-844	181	23	(	(	PUNCT
eurjchem-844	181	24	4.25	4.25	NUM
eurjchem-844	181	25	,	,	PUNCT
eurjchem-844	181	26	2.5	2.5	NUM
eurjchem-844	181	27	,	,	PUNCT
eurjchem-844	181	28	and	and	CCONJ
eurjchem-844	181	29	3.28	3.28	NUM
eurjchem-844	181	30	)	)	PUNCT
eurjchem-844	181	31	and	and	CCONJ
eurjchem-844	181	32	(	(	PUNCT
eurjchem-844	181	33	4.12	4.12	NUM
eurjchem-844	181	34	,	,	PUNCT
eurjchem-844	181	35	2.6	2.6	NUM
eurjchem-844	181	36	,	,	PUNCT
eurjchem-844	181	37	and	and	CCONJ
eurjchem-844	181	38	3.35	3.35	NUM
eurjchem-844	181	39	)	)	PUNCT
eurjchem-844	181	40	,	,	PUNCT
eurjchem-844	181	41	respectively	respectively	ADV
eurjchem-844	181	42	.	.	PUNCT
eurjchem-844	182	1	finally	finally	ADV
eurjchem-844	182	2	,	,	PUNCT
eurjchem-844	182	3	a	a	DET
eurjchem-844	182	4	value	value	NOUN
eurjchem-844	182	5	of	of	ADP
eurjchem-844	182	6	ph	ph	NOUN
eurjchem-844	182	7	of	of	ADP
eurjchem-844	182	8	the	the	DET
eurjchem-844	182	9	phosphate	phosphate	ADJ
eurjchem-844	182	10	buffer	buffer	NOUN
eurjchem-844	182	11	was	be	AUX
eurjchem-844	182	12	varied	varied	ADJ
eurjchem-844	182	13	from	from	ADP
eurjchem-844	182	14	4.6	4.6	NUM
eurjchem-844	182	15	to	to	ADP
eurjchem-844	182	16	4.5	4.5	NUM
eurjchem-844	182	17	and	and	CCONJ
eurjchem-844	182	18	4.7	4.7	NUM
eurjchem-844	182	19	,	,	PUNCT
eurjchem-844	182	20	where	where	SCONJ
eurjchem-844	182	21	resolution	resolution	NOUN
eurjchem-844	182	22	factors	factor	NOUN
eurjchem-844	182	23	obtained	obtain	VERB
eurjchem-844	182	24	were	be	AUX
eurjchem-844	182	25	(	(	PUNCT
eurjchem-844	182	26	4.1	4.1	NUM
eurjchem-844	182	27	,	,	PUNCT
eurjchem-844	182	28	2.5	2.5	NUM
eurjchem-844	182	29	,	,	PUNCT
eurjchem-844	182	30	and	and	CCONJ
eurjchem-844	182	31	3.2	3.2	NUM
eurjchem-844	182	32	)	)	PUNCT
eurjchem-844	182	33	,	,	PUNCT
eurjchem-844	182	34	(	(	PUNCT
eurjchem-844	182	35	3.95	3.95	NUM
eurjchem-844	182	36	,	,	PUNCT
eurjchem-844	182	37	2.62	2.62	NUM
eurjchem-844	182	38	,	,	PUNCT
eurjchem-844	182	39	and	and	CCONJ
eurjchem-844	182	40	3.21	3.21	NUM
eurjchem-844	182	41	)	)	PUNCT
eurjchem-844	182	42	and	and	CCONJ
eurjchem-844	182	43	(	(	PUNCT
eurjchem-844	182	44	3.9	3.9	NUM
eurjchem-844	182	45	,	,	PUNCT
eurjchem-844	182	46	2.65	2.65	NUM
eurjchem-844	182	47	,	,	PUNCT
eurjchem-844	182	48	and	and	CCONJ
eurjchem-844	182	49	3.31	3.31	NUM
eurjchem-844	182	50	)	)	PUNCT
eurjchem-844	182	51	,	,	PUNCT
eurjchem-844	182	52	respectively	respectively	ADV
eurjchem-844	182	53	.	.	PUNCT
eurjchem-844	183	1	as	as	SCONJ
eurjchem-844	183	2	can	can	AUX
eurjchem-844	183	3	also	also	ADV
eurjchem-844	183	4	be	be	AUX
eurjchem-844	183	5	seen	see	VERB
eurjchem-844	183	6	from	from	ADP
eurjchem-844	183	7	these	these	DET
eurjchem-844	183	8	results	result	NOUN
eurjchem-844	183	9	,	,	PUNCT
eurjchem-844	183	10	good	good	ADJ
eurjchem-844	183	11	values	value	NOUN
eurjchem-844	183	12	of	of	ADP
eurjchem-844	183	13	the	the	DET
eurjchem-844	183	14	resolution	resolution	NOUN
eurjchem-844	183	15	factor	factor	NOUN
eurjchem-844	183	16	were	be	AUX
eurjchem-844	183	17	obtained	obtain	VERB
eurjchem-844	183	18	for	for	ADP
eurjchem-844	183	19	all	all	DET
eurjchem-844	183	20	these	these	DET
eurjchem-844	183	21	variations	variation	NOUN
eurjchem-844	183	22	,	,	PUNCT
eurjchem-844	183	23	indicating	indicate	VERB
eurjchem-844	183	24	good	good	ADJ
eurjchem-844	183	25	robustness	robustness	NOUN
eurjchem-844	183	26	of	of	ADP
eurjchem-844	183	27	the	the	DET
eurjchem-844	183	28	proposed	propose	VERB
eurjchem-844	183	29	lc	lc	NOUN
eurjchem-844	183	30	method	method	NOUN
eurjchem-844	183	31	.	.	PUNCT
eurjchem-844	184	1	no	no	DET
eurjchem-844	184	2	interference	interference	NOUN
eurjchem-844	184	3	was	be	AUX
eurjchem-844	184	4	observed	observe	VERB
eurjchem-844	184	5	from	from	ADP
eurjchem-844	184	6	the	the	DET
eurjchem-844	184	7	peak	peak	NOUN
eurjchem-844	184	8	of	of	ADP
eurjchem-844	184	9	cgn	cgn	PROPN
eurjchem-844	184	10	in	in	ADP
eurjchem-844	184	11	all	all	DET
eurjchem-844	184	12	the	the	DET
eurjchem-844	184	13	previously	previously	ADV
eurjchem-844	184	14	mentioned	mention	VERB
eurjchem-844	184	15	conditions	condition	NOUN
eurjchem-844	184	16	.	.	PUNCT
eurjchem-844	185	1	3.3.6	3.3.6	X
eurjchem-844	185	2	.	.	PUNCT
eurjchem-844	185	3	limit	limit	NOUN
eurjchem-844	185	4	of	of	ADP
eurjchem-844	185	5	detection	detection	NOUN
eurjchem-844	185	6	and	and	CCONJ
eurjchem-844	185	7	limit	limit	NOUN
eurjchem-844	185	8	of	of	ADP
eurjchem-844	185	9	quantification	quantification	NOUN
eurjchem-844	185	10	limit	limit	NOUN
eurjchem-844	185	11	of	of	ADP
eurjchem-844	185	12	detection	detection	NOUN
eurjchem-844	185	13	(	(	PUNCT
eurjchem-844	185	14	lod	lod	PROPN
eurjchem-844	185	15	)	)	PUNCT
eurjchem-844	185	16	which	which	PRON
eurjchem-844	185	17	represents	represent	VERB
eurjchem-844	185	18	the	the	DET
eurjchem-844	185	19	concentration	concentration	NOUN
eurjchem-844	185	20	of	of	ADP
eurjchem-844	185	21	analyte	analyte	NOUN
eurjchem-844	185	22	at	at	ADP
eurjchem-844	185	23	s	s	PROPN
eurjchem-844	185	24	/	/	SYM
eurjchem-844	185	25	n	n	PRON
eurjchem-844	185	26	ratio	ratio	NOUN
eurjchem-844	185	27	of	of	ADP
eurjchem-844	185	28	3	3	NUM
eurjchem-844	185	29	and	and	CCONJ
eurjchem-844	185	30	limit	limit	NOUN
eurjchem-844	185	31	of	of	ADP
eurjchem-844	185	32	quantification	quantification	NOUN
eurjchem-844	185	33	(	(	PUNCT
eurjchem-844	185	34	loq	loq	PROPN
eurjchem-844	185	35	)	)	PUNCT
eurjchem-844	185	36	at	at	ADP
eurjchem-844	185	37	which	which	PRON
eurjchem-844	185	38	s	s	PROPN
eurjchem-844	185	39	/	/	SYM
eurjchem-844	185	40	n	n	PRON
eurjchem-844	185	41	is	be	AUX
eurjchem-844	185	42	10	10	NUM
eurjchem-844	185	43	were	be	AUX
eurjchem-844	185	44	determined	determine	VERB
eurjchem-844	185	45	experimentally	experimentally	ADV
eurjchem-844	185	46	for	for	ADP
eurjchem-844	185	47	the	the	DET
eurjchem-844	185	48	proposed	propose	VERB
eurjchem-844	185	49	methods	method	NOUN
eurjchem-844	185	50	and	and	CCONJ
eurjchem-844	185	51	results	result	NOUN
eurjchem-844	185	52	are	be	AUX
eurjchem-844	185	53	given	give	VERB
eurjchem-844	185	54	in	in	ADP
eurjchem-844	185	55	tables	table	NOUN
eurjchem-844	185	56	4	4	NUM
eurjchem-844	185	57	and	and	CCONJ
eurjchem-844	185	58	5	5	NUM
eurjchem-844	185	59	.	.	X
eurjchem-844	186	1	3.3.7	3.3.7	NUM
eurjchem-844	186	2	.	.	PUNCT
eurjchem-844	187	1	statistical	statistical	ADJ
eurjchem-844	187	2	analysis	analysis	NOUN
eurjchem-844	187	3	statistical	statistical	ADJ
eurjchem-844	187	4	analysis	analysis	NOUN
eurjchem-844	187	5	of	of	ADP
eurjchem-844	187	6	the	the	DET
eurjchem-844	187	7	results	result	NOUN
eurjchem-844	187	8	obtained	obtain	VERB
eurjchem-844	187	9	by	by	ADP
eurjchem-844	187	10	the	the	DET
eurjchem-844	187	11	proposed	propose	VERB
eurjchem-844	187	12	methods	method	NOUN
eurjchem-844	187	13	and	and	CCONJ
eurjchem-844	187	14	the	the	DET
eurjchem-844	187	15	reference	reference	NOUN
eurjchem-844	187	16	methods	method	NOUN
eurjchem-844	187	17	for	for	ADP
eurjchem-844	187	18	each	each	DET
eurjchem-844	187	19	drug	drug	NOUN
eurjchem-844	187	20	were	be	AUX
eurjchem-844	187	21	carried	carry	VERB
eurjchem-844	187	22	out	out	ADP
eurjchem-844	187	23	by	by	ADP
eurjchem-844	187	24	“	"	PUNCT
eurjchem-844	187	25	spss	spss	ADJ
eurjchem-844	187	26	statistical	statistical	ADJ
eurjchem-844	187	27	package	package	NOUN
eurjchem-844	187	28	version	version	NOUN
eurjchem-844	187	29	11	11	NUM
eurjchem-844	187	30	”	"	PUNCT
eurjchem-844	187	31	.	.	PUNCT
eurjchem-844	188	1	the	the	DET
eurjchem-844	188	2	significant	significant	ADJ
eurjchem-844	188	3	difference	difference	NOUN
eurjchem-844	188	4	between	between	ADP
eurjchem-844	188	5	the	the	DET
eurjchem-844	188	6	reference	reference	NOUN
eurjchem-844	188	7	methods	method	NOUN
eurjchem-844	188	8	and	and	CCONJ
eurjchem-844	188	9	the	the	DET
eurjchem-844	188	10	described	describe	VERB
eurjchem-844	188	11	methods	method	NOUN
eurjchem-844	188	12	was	be	AUX
eurjchem-844	188	13	tested	test	VERB
eurjchem-844	188	14	by	by	ADP
eurjchem-844	188	15	one	one	NUM
eurjchem-844	188	16	way	way	NOUN
eurjchem-844	188	17	anova	anova	X
eurjchem-844	188	18	(	(	PUNCT
eurjchem-844	188	19	f‐test	f‐test	X
eurjchem-844	188	20	)	)	PUNCT
eurjchem-844	188	21	at	at	ADP
eurjchem-844	188	22	p	p	NOUN
eurjchem-844	188	23	=	=	NOUN
eurjchem-844	188	24	0.05	0.05	NUM
eurjchem-844	188	25	as	as	SCONJ
eurjchem-844	188	26	shown	show	VERB
eurjchem-844	188	27	in	in	ADP
eurjchem-844	188	28	tables	table	NOUN
eurjchem-844	188	29	6	6	NUM
eurjchem-844	188	30	and	and	CCONJ
eurjchem-844	188	31	7	7	NUM
eurjchem-844	188	32	.	.	PUNCT
eurjchem-844	189	1	the	the	DET
eurjchem-844	189	2	test	test	NOUN
eurjchem-844	189	3	ascertained	ascertain	VERB
eurjchem-844	189	4	that	that	SCONJ
eurjchem-844	189	5	there	there	PRON
eurjchem-844	189	6	was	be	VERB
eurjchem-844	189	7	no	no	DET
eurjchem-844	189	8	significant	significant	ADJ
eurjchem-844	189	9	difference	difference	NOUN
eurjchem-844	189	10	among	among	ADP
eurjchem-844	189	11	the	the	DET
eurjchem-844	189	12	methods	method	NOUN
eurjchem-844	189	13	.	.	PUNCT
eurjchem-844	190	1	4	4	X
eurjchem-844	190	2	.	.	X
eurjchem-844	190	3	conclusion	conclusion	NOUN
eurjchem-844	190	4	the	the	DET
eurjchem-844	190	5	proposed	propose	VERB
eurjchem-844	190	6	lc	lc	NOUN
eurjchem-844	190	7	method	method	NOUN
eurjchem-844	190	8	has	have	VERB
eurjchem-844	190	9	the	the	DET
eurjchem-844	190	10	advantages	advantage	NOUN
eurjchem-844	190	11	of	of	ADP
eurjchem-844	190	12	simplicity	simplicity	NOUN
eurjchem-844	190	13	,	,	PUNCT
eurjchem-844	190	14	precision	precision	NOUN
eurjchem-844	190	15	,	,	PUNCT
eurjchem-844	190	16	accuracy	accuracy	NOUN
eurjchem-844	190	17	and	and	CCONJ
eurjchem-844	190	18	convenience	convenience	NOUN
eurjchem-844	190	19	for	for	ADP
eurjchem-844	190	20	the	the	DET
eurjchem-844	190	21	separation	separation	NOUN
eurjchem-844	190	22	and	and	CCONJ
eurjchem-844	190	23	quantization	quantization	NOUN
eurjchem-844	190	24	of	of	ADP
eurjchem-844	190	25	stg	stg	PROPN
eurjchem-844	190	26	,	,	PUNCT
eurjchem-844	190	27	vdg	vdg	NOUN
eurjchem-844	190	28	or	or	CCONJ
eurjchem-844	190	29	sxg	sxg	NOUN
eurjchem-844	190	30	in	in	ADP
eurjchem-844	190	31	combination	combination	NOUN
eurjchem-844	190	32	with	with	ADP
eurjchem-844	190	33	met	meet	VERB
eurjchem-844	190	34	in	in	ADP
eurjchem-844	190	35	the	the	DET
eurjchem-844	190	36	presence	presence	NOUN
eurjchem-844	190	37	of	of	ADP
eurjchem-844	190	38	cgn	cgn	PROPN
eurjchem-844	190	39	.	.	PUNCT
eurjchem-844	191	1	the	the	DET
eurjchem-844	191	2	method	method	NOUN
eurjchem-844	191	3	can	can	AUX
eurjchem-844	191	4	be	be	AUX
eurjchem-844	191	5	applied	apply	VERB
eurjchem-844	191	6	for	for	ADP
eurjchem-844	191	7	the	the	DET
eurjchem-844	191	8	determination	determination	NOUN
eurjchem-844	191	9	of	of	ADP
eurjchem-844	191	10	the	the	DET
eurjchem-844	191	11	cited	cite	VERB
eurjchem-844	191	12	drugs	drug	NOUN
eurjchem-844	191	13	in	in	ADP
eurjchem-844	191	14	pharmaceutical	pharmaceutical	ADJ
eurjchem-844	191	15	dosage	dosage	NOUN
eurjchem-844	191	16	forms	form	NOUN
eurjchem-844	191	17	.	.	PUNCT
eurjchem-844	192	1	the	the	DET
eurjchem-844	192	2	method	method	NOUN
eurjchem-844	192	3	was	be	AUX
eurjchem-844	192	4	validated	validate	VERB
eurjchem-844	192	5	showing	show	VERB
eurjchem-844	192	6	satisfactory	satisfactory	ADJ
eurjchem-844	192	7	data	datum	NOUN
eurjchem-844	192	8	for	for	ADP
eurjchem-844	192	9	el‐bagary	el‐bagary	PROPN
eurjchem-844	192	10	et	et	PROPN
eurjchem-844	192	11	al	al	PROPN
eurjchem-844	192	12	.	.	PUNCT
eurjchem-844	192	13	/	/	SYM
eurjchem-844	192	14	european	european	PROPN
eurjchem-844	192	15	journal	journal	PROPN
eurjchem-844	192	16	of	of	ADP
eurjchem-844	192	17	chemistry	chemistry	NOUN
eurjchem-844	192	18	4	4	NUM
eurjchem-844	192	19	(	(	PUNCT
eurjchem-844	192	20	4	4	NUM
eurjchem-844	192	21	)	)	PUNCT
eurjchem-844	192	22	(	(	PUNCT
eurjchem-844	192	23	2013	2013	NUM
eurjchem-844	192	24	)	)	PUNCT
eurjchem-844	192	25	444‐449	444‐449	NOUN
eurjchem-844	193	1	449	449	NUM
eurjchem-844	193	2	all	all	DET
eurjchem-844	193	3	the	the	DET
eurjchem-844	193	4	method	method	NOUN
eurjchem-844	193	5	validation	validation	NOUN
eurjchem-844	193	6	parameters	parameter	NOUN
eurjchem-844	193	7	tested	test	VERB
eurjchem-844	193	8	.	.	PUNCT
eurjchem-844	194	1	the	the	DET
eurjchem-844	194	2	developed	develop	VERB
eurjchem-844	194	3	method	method	NOUN
eurjchem-844	194	4	can	can	AUX
eurjchem-844	194	5	be	be	AUX
eurjchem-844	194	6	conveniently	conveniently	ADV
eurjchem-844	194	7	used	use	VERB
eurjchem-844	194	8	by	by	ADP
eurjchem-844	194	9	quality	quality	NOUN
eurjchem-844	194	10	control	control	NOUN
eurjchem-844	194	11	laboratories	laboratory	NOUN
eurjchem-844	194	12	.	.	PUNCT
eurjchem-844	195	1	references	reference	NOUN
eurjchem-844	195	2	[	[	X
eurjchem-844	195	3	1	1	NUM
eurjchem-844	195	4	]	]	PUNCT
eurjchem-844	195	5	.	.	PUNCT
eurjchem-844	196	1	nirogi	nirogi	PROPN
eurjchem-844	196	2	,	,	PUNCT
eurjchem-844	196	3	r.	r.	PROPN
eurjchem-844	196	4	;	;	PUNCT
eurjchem-844	196	5	kandikere	kandikere	PROPN
eurjchem-844	196	6	,	,	PUNCT
eurjchem-844	196	7	v.	v.	PROPN
eurjchem-844	196	8	;	;	PUNCT
eurjchem-844	196	9	mudigonda	mudigonda	NOUN
eurjchem-844	196	10	,	,	PUNCT
eurjchem-844	196	11	k.	k.	PROPN
eurjchem-844	196	12	;	;	PUNCT
eurjchem-844	196	13	komarneni	komarneni	PROPN
eurjchem-844	196	14	,	,	PUNCT
eurjchem-844	196	15	p.	p.	NOUN
eurjchem-844	196	16	;	;	PUNCT
eurjchem-844	196	17	aleti	aleti	PROPN
eurjchem-844	196	18	,	,	PUNCT
eurjchem-844	196	19	r.	r.	PROPN
eurjchem-844	196	20	;	;	PUNCT
eurjchem-844	196	21	boggavarapu	boggavarapu	PROPN
eurjchem-844	196	22	,	,	PUNCT
eurjchem-844	196	23	r.	r.	PROPN
eurjchem-844	196	24	biomed	biome	VERB
eurjchem-844	196	25	chromatogr	chromatogr	PROPN
eurjchem-844	196	26	.	.	PUNCT
eurjchem-844	197	1	2008	2008	NUM
eurjchem-844	197	2	,	,	PUNCT
eurjchem-844	197	3	22	22	NUM
eurjchem-844	197	4	,	,	PUNCT
eurjchem-844	197	5	214‐222	214‐222	NUM
eurjchem-844	197	6	.	.	PUNCT
eurjchem-844	198	1	[	[	X
eurjchem-844	198	2	2	2	NUM
eurjchem-844	198	3	]	]	PUNCT
eurjchem-844	198	4	.	.	PUNCT
eurjchem-844	199	1	sekaran	sekaran	PROPN
eurjchem-844	199	2	,	,	PUNCT
eurjchem-844	199	3	b.	b.	PROPN
eurjchem-844	199	4	;	;	PUNCT
eurjchem-844	199	5	rani	rani	PROPN
eurjchem-844	199	6	,	,	PUNCT
eurjchem-844	199	7	p.	p.	NOUN
eurjchem-844	199	8	int	int	NOUN
eurjchem-844	199	9	.	.	PUNCT
eurjchem-844	200	1	j.	j.	PROPN
eurjchem-844	200	2	pharm	pharm	PROPN
eurjchem-844	200	3	.	.	PUNCT
eurjchem-844	201	1	pharm	pharm	PROPN
eurjchem-844	201	2	.	.	PUNCT
eurjchem-844	202	1	sci	sci	PROPN
eurjchem-844	202	2	.	.	PROPN
eurjchem-844	202	3	2010	2010	NUM
eurjchem-844	202	4	,	,	PUNCT
eurjchem-844	202	5	2	2	NUM
eurjchem-844	202	6	,	,	PUNCT
eurjchem-844	202	7	138‐142	138‐142	NUM
eurjchem-844	202	8	.	.	PUNCT
eurjchem-844	203	1	[	[	X
eurjchem-844	203	2	3	3	NUM
eurjchem-844	203	3	]	]	PUNCT
eurjchem-844	203	4	.	.	PUNCT
eurjchem-844	204	1	zeng	zeng	PROPN
eurjchem-844	204	2	,	,	PUNCT
eurjchem-844	204	3	w.	w.	PROPN
eurjchem-844	204	4	;	;	PUNCT
eurjchem-844	204	5	musson	musson	PROPN
eurjchem-844	204	6	,	,	PUNCT
eurjchem-844	204	7	d.	d.	PROPN
eurjchem-844	204	8	;	;	PUNCT
eurjchem-844	204	9	fisher	fisher	PROPN
eurjchem-844	204	10	,	,	PUNCT
eurjchem-844	204	11	a.	a.	NOUN
eurjchem-844	204	12	;	;	PUNCT
eurjchem-844	204	13	chen	chen	PROPN
eurjchem-844	204	14	,	,	PUNCT
eurjchem-844	204	15	l.	l.	PROPN
eurjchem-844	204	16	;	;	PUNCT
eurjchem-844	204	17	schwartz	schwartz	PROPN
eurjchem-844	204	18	,	,	PUNCT
eurjchem-844	204	19	m.	m.	NOUN
eurjchem-844	204	20	;	;	PUNCT
eurjchem-844	204	21	woolf	woolf	PROPN
eurjchem-844	204	22	,	,	PUNCT
eurjchem-844	204	23	e.	e.	PROPN
eurjchem-844	204	24	;	;	PUNCT
eurjchem-844	204	25	wang	wang	PROPN
eurjchem-844	204	26	,	,	PUNCT
eurjchem-844	204	27	a.	a.	PROPN
eurjchem-844	204	28	j.	j.	PROPN
eurjchem-844	204	29	pharm	pharm	PROPN
eurjchem-844	204	30	.	.	PUNCT
eurjchem-844	204	31	biomed	biome	VERB
eurjchem-844	204	32	.	.	PUNCT
eurjchem-844	205	1	anal	anal	PROPN
eurjchem-844	205	2	.	.	PUNCT
eurjchem-844	206	1	2008	2008	NUM
eurjchem-844	206	2	,	,	PUNCT
eurjchem-844	206	3	46	46	NUM
eurjchem-844	206	4	,	,	PUNCT
eurjchem-844	206	5	534‐542	534‐542	NUM
eurjchem-844	206	6	.	.	PUNCT
eurjchem-844	207	1	[	[	X
eurjchem-844	207	2	4	4	NUM
eurjchem-844	207	3	]	]	PUNCT
eurjchem-844	207	4	.	.	PUNCT
eurjchem-844	208	1	el‐bagary	el‐bagary	PROPN
eurjchem-844	208	2	,	,	PUNCT
eurjchem-844	208	3	r.	r.	PROPN
eurjchem-844	208	4	;	;	PUNCT
eurjchem-844	208	5	elkady	elkady	PROPN
eurjchem-844	208	6	,	,	PUNCT
eurjchem-844	208	7	e.	e.	PROPN
eurjchem-844	208	8	;	;	PUNCT
eurjchem-844	208	9	ayoub	ayoub	PROPN
eurjchem-844	208	10	,	,	PUNCT
eurjchem-844	208	11	b.	b.	PROPN
eurjchem-844	208	12	talanta	talanta	PROPN
eurjchem-844	208	13	2011	2011	NUM
eurjchem-844	208	14	,	,	PUNCT
eurjchem-844	208	15	85	85	NUM
eurjchem-844	208	16	,	,	PUNCT
eurjchem-844	208	17	673‐680	673‐680	NUM
eurjchem-844	208	18	.	.	PUNCT
eurjchem-844	209	1	[	[	X
eurjchem-844	209	2	5	5	NUM
eurjchem-844	209	3	]	]	PUNCT
eurjchem-844	209	4	.	.	PUNCT
eurjchem-844	210	1	el‐bagary	el‐bagary	PROPN
eurjchem-844	210	2	,	,	PUNCT
eurjchem-844	210	3	r.	r.	PROPN
eurjchem-844	210	4	;	;	PUNCT
eurjchem-844	210	5	elkady	elkady	PROPN
eurjchem-844	210	6	,	,	PUNCT
eurjchem-844	210	7	e.	e.	PROPN
eurjchem-844	210	8	;	;	PUNCT
eurjchem-844	210	9	ayoub	ayoub	PROPN
eurjchem-844	210	10	,	,	PUNCT
eurjchem-844	210	11	b.	b.	PROPN
eurjchem-844	210	12	int	int	PROPN
eurjchem-844	210	13	.	.	PUNCT
eurjchem-844	211	1	j.	j.	PROPN
eurjchem-844	211	2	biomed	biome	VERB
eurjchem-844	211	3	.	.	PUNCT
eurjchem-844	212	1	sci	sci	PROPN
eurjchem-844	212	2	.	.	PROPN
eurjchem-844	212	3	2011	2011	NUM
eurjchem-844	212	4	,	,	PUNCT
eurjchem-844	212	5	7	7	NUM
eurjchem-844	212	6	,	,	PUNCT
eurjchem-844	212	7	55‐61	55‐61	NUM
eurjchem-844	212	8	.	.	PUNCT
eurjchem-844	213	1	[	[	X
eurjchem-844	213	2	6	6	NUM
eurjchem-844	213	3	]	]	PUNCT
eurjchem-844	213	4	.	.	PUNCT
eurjchem-844	214	1	el‐bagary	el‐bagary	PROPN
eurjchem-844	214	2	,	,	PUNCT
eurjchem-844	214	3	r.	r.	PROPN
eurjchem-844	214	4	;	;	PUNCT
eurjchem-844	214	5	elkady	elkady	PROPN
eurjchem-844	214	6	,	,	PUNCT
eurjchem-844	214	7	e.	e.	PROPN
eurjchem-844	214	8	;	;	PUNCT
eurjchem-844	214	9	ayoub	ayoub	PROPN
eurjchem-844	214	10	,	,	PUNCT
eurjchem-844	214	11	b.	b.	PROPN
eurjchem-844	214	12	int	int	PROPN
eurjchem-844	214	13	.	.	PUNCT
eurjchem-844	215	1	j.	j.	PROPN
eurjchem-844	215	2	biomed	biome	VERB
eurjchem-844	215	3	.	.	PUNCT
eurjchem-844	216	1	sci	sci	PROPN
eurjchem-844	216	2	.	.	PROPN
eurjchem-844	216	3	2011	2011	NUM
eurjchem-844	216	4	,	,	PUNCT
eurjchem-844	216	5	7	7	NUM
eurjchem-844	216	6	,	,	PUNCT
eurjchem-844	216	7	201‐205	201‐205	NUM
eurjchem-844	216	8	.	.	PUNCT
eurjchem-844	217	1	[	[	X
eurjchem-844	217	2	7	7	NUM
eurjchem-844	217	3	]	]	PUNCT
eurjchem-844	217	4	.	.	PUNCT
eurjchem-844	218	1	kulasa	kulasa	PROPN
eurjchem-844	218	2	,	,	PUNCT
eurjchem-844	218	3	k.	k.	PROPN
eurjchem-844	218	4	;	;	PUNCT
eurjchem-844	218	5	edelman	edelman	PROPN
eurjchem-844	218	6	,	,	PUNCT
eurjchem-844	218	7	s.	s.	PROPN
eurjchem-844	218	8	core	core	PROPN
eurjchem-844	218	9	evid	evid	PROPN
eurjchem-844	218	10	.	.	PUNCT
eurjchem-844	219	1	2010	2010	NUM
eurjchem-844	219	2	,	,	PUNCT
eurjchem-844	219	3	5	5	NUM
eurjchem-844	219	4	,	,	PUNCT
eurjchem-844	219	5	23‐37	23‐37	NOUN
eurjchem-844	219	6	.	.	PUNCT
eurjchem-844	220	1	[	[	X
eurjchem-844	220	2	8	8	NUM
eurjchem-844	220	3	]	]	SYM
eurjchem-844	220	4	.	.	PUNCT
eurjchem-844	221	1	fura	fura	PROPN
eurjchem-844	221	2	,	,	PUNCT
eurjchem-844	221	3	a.	a.	NOUN
eurjchem-844	221	4	;	;	PUNCT
eurjchem-844	221	5	khanna	khanna	PROPN
eurjchem-844	221	6	,	,	PUNCT
eurjchem-844	221	7	a.	a.	PROPN
eurjchem-844	221	8	;	;	PUNCT
eurjchem-844	221	9	vyas	vyas	PROPN
eurjchem-844	221	10	,	,	PUNCT
eurjchem-844	221	11	v.	v.	PROPN
eurjchem-844	221	12	;	;	PUNCT
eurjchem-844	221	13	koplowitz	koplowitz	PROPN
eurjchem-844	221	14	,	,	PUNCT
eurjchem-844	221	15	b.	b.	PROPN
eurjchem-844	221	16	;	;	PUNCT
eurjchem-844	221	17	chang	chang	PROPN
eurjchem-844	221	18	,	,	PUNCT
eurjchem-844	221	19	s.	s.	PROPN
eurjchem-844	221	20	;	;	PUNCT
eurjchem-844	221	21	caporuscio	caporuscio	PROPN
eurjchem-844	221	22	,	,	PUNCT
eurjchem-844	221	23	c.	c.	PROPN
eurjchem-844	221	24	drug	drug	PROPN
eurjchem-844	221	25	metab	metab	PROPN
eurjchem-844	221	26	.	.	PUNCT
eurjchem-844	222	1	dispos	dispos	PROPN
eurjchem-844	222	2	.	.	PUNCT
eurjchem-844	223	1	2009	2009	NUM
eurjchem-844	223	2	,	,	PUNCT
eurjchem-844	223	3	37	37	NUM
eurjchem-844	223	4	,	,	PUNCT
eurjchem-844	223	5	1164‐1171	1164‐1171	NUM
eurjchem-844	223	6	.	.	PUNCT
eurjchem-844	224	1	[	[	X
eurjchem-844	224	2	9	9	NUM
eurjchem-844	224	3	]	]	PUNCT
eurjchem-844	224	4	.	.	PUNCT
eurjchem-844	225	1	kalaichelvi	kalaichelvi	PROPN
eurjchem-844	225	2	,	,	PUNCT
eurjchem-844	225	3	r.	r.	PROPN
eurjchem-844	225	4	;	;	PUNCT
eurjchem-844	225	5	jayachandran	jayachandran	PROPN
eurjchem-844	225	6	,	,	PUNCT
eurjchem-844	225	7	e.	e.	PROPN
eurjchem-844	225	8	int	int	PROPN
eurjchem-844	225	9	.	.	PUNCT
eurjchem-844	226	1	j.	j.	PROPN
eurjchem-844	226	2	pharm	pharm	PROPN
eurjchem-844	226	3	.	.	PUNCT
eurjchem-844	227	1	pharm	pharm	PROPN
eurjchem-844	227	2	.	.	PUNCT
eurjchem-844	228	1	sci	sci	PROPN
eurjchem-844	228	2	.	.	PROPN
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eurjchem-844	228	4	,	,	PUNCT
eurjchem-844	228	5	3	3	NUM
eurjchem-844	228	6	,	,	PUNCT
eurjchem-844	228	7	180‐	180‐	NUM
eurjchem-844	228	8	184	184	NUM
eurjchem-844	228	9	.	.	PUNCT
eurjchem-844	229	1	[	[	X
eurjchem-844	229	2	10	10	NUM
eurjchem-844	229	3	]	]	PUNCT
eurjchem-844	229	4	.	.	PUNCT
eurjchem-844	230	1	sengupta	sengupta	NOUN
eurjchem-844	230	2	,	,	PUNCT
eurjchem-844	230	3	p.	p.	NOUN
eurjchem-844	230	4	;	;	PUNCT
eurjchem-844	230	5	bhaumik	bhaumik	ADJ
eurjchem-844	230	6	,	,	PUNCT
eurjchem-844	230	7	u.	u.	PROPN
eurjchem-844	230	8	;	;	PUNCT
eurjchem-844	230	9	ghosh	ghosh	PROPN
eurjchem-844	230	10	,	,	PUNCT
eurjchem-844	230	11	a.	a.	PROPN
eurjchem-844	230	12	;	;	PUNCT
eurjchem-844	230	13	chatterjee	chatterjee	PROPN
eurjchem-844	230	14	,	,	PUNCT
eurjchem-844	230	15	b.	b.	PROPN
eurjchem-844	230	16	;	;	PUNCT
eurjchem-844	230	17	bose	bose	PROPN
eurjchem-844	230	18	,	,	PUNCT
eurjchem-844	230	19	a.	a.	NOUN
eurjchem-844	230	20	;	;	PUNCT
eurjchem-844	230	21	pal	pal	NOUN
eurjchem-844	230	22	,	,	PUNCT
eurjchem-844	230	23	t.	t.	PROPN
eurjchem-844	230	24	k.	k.	PROPN
eurjchem-844	230	25	chromatographia	chromatographia	PROPN
eurjchem-844	230	26	2009	2009	NUM
eurjchem-844	230	27	,	,	PUNCT
eurjchem-844	230	28	69	69	NUM
eurjchem-844	230	29	,	,	PUNCT
eurjchem-844	230	30	1243‐1250	1243‐1250	NUM
eurjchem-844	230	31	.	.	PUNCT
eurjchem-844	231	1	[	[	X
eurjchem-844	231	2	11	11	NUM
eurjchem-844	231	3	]	]	PUNCT
eurjchem-844	231	4	.	.	PUNCT
eurjchem-844	232	1	xiong	xiong	PROPN
eurjchem-844	232	2	,	,	PUNCT
eurjchem-844	232	3	y.	y.	PROPN
eurjchem-844	232	4	;	;	PUNCT
eurjchem-844	232	5	zhou	zhou	PROPN
eurjchem-844	232	6	,	,	PUNCT
eurjchem-844	232	7	h.	h.	PROPN
eurjchem-844	232	8	;	;	PUNCT
eurjchem-844	232	9	zhang	zhang	PROPN
eurjchem-844	232	10	,	,	PUNCT
eurjchem-844	232	11	z.	z.	PROPN
eurjchem-844	232	12	fenxi‐shiyanshi	fenxi‐shiyanshi	PROPN
eurjchem-844	232	13	2006	2006	NUM
eurjchem-844	232	14	,	,	PUNCT
eurjchem-844	232	15	25	25	NUM
eurjchem-844	232	16	,	,	PUNCT
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eurjchem-844	232	18	.	.	PUNCT
eurjchem-844	233	1	[	[	X
eurjchem-844	233	2	12	12	NUM
eurjchem-844	233	3	]	]	PUNCT
eurjchem-844	233	4	.	.	PUNCT
eurjchem-844	233	5	ali	ali	PROPN
eurjchem-844	233	6	,	,	PUNCT
eurjchem-844	233	7	a.	a.	PROPN
eurjchem-844	233	8	;	;	PUNCT
eurjchem-844	233	9	duraidi	duraidi	PROPN
eurjchem-844	233	10	,	,	PUNCT
eurjchem-844	233	11	i.	i.	NOUN
eurjchem-844	233	12	;	;	PUNCT
eurjchem-844	233	13	saket	saket	NOUN
eurjchem-844	233	14	,	,	PUNCT
eurjchem-844	233	15	m.	m.	NOUN
eurjchem-844	233	16	;	;	PUNCT
eurjchem-844	233	17	abu‐nameh	abu‐nameh	NOUN
eurjchem-844	233	18	,	,	PUNCT
eurjchem-844	233	19	e.	e.	PROPN
eurjchem-844	233	20	j.	j.	PROPN
eurjchem-844	233	21	aoac	aoac	PROPN
eurjchem-844	233	22	int	int	PROPN
eurjchem-844	233	23	.	.	PUNCT
eurjchem-844	234	1	2009	2009	NUM
eurjchem-844	234	2	,	,	PUNCT
eurjchem-844	234	3	92	92	NUM
eurjchem-844	234	4	,	,	PUNCT
eurjchem-844	234	5	119‐	119‐	NUM
eurjchem-844	234	6	124	124	NUM
eurjchem-844	234	7	.	.	PUNCT
eurjchem-844	235	1	[	[	X
eurjchem-844	235	2	13	13	NUM
eurjchem-844	235	3	]	]	PUNCT
eurjchem-844	235	4	.	.	PUNCT
eurjchem-844	236	1	porta	porta	PROPN
eurjchem-844	236	2	,	,	PUNCT
eurjchem-844	236	3	v.	v.	PROPN
eurjchem-844	236	4	;	;	PUNCT
eurjchem-844	236	5	schramm	schramm	PROPN
eurjchem-844	236	6	,	,	PUNCT
eurjchem-844	236	7	s.	s.	PROPN
eurjchem-844	236	8	;	;	PUNCT
eurjchem-844	236	9	kano	kano	PROPN
eurjchem-844	236	10	,	,	PUNCT
eurjchem-844	236	11	e.	e.	PROPN
eurjchem-844	236	12	;	;	PUNCT
eurjchem-844	236	13	koono	koono	PROPN
eurjchem-844	236	14	,	,	PUNCT
eurjchem-844	236	15	e.	e.	PROPN
eurjchem-844	236	16	;	;	PUNCT
eurjchem-844	236	17	armando	armando	PROPN
eurjchem-844	236	18	,	,	PUNCT
eurjchem-844	236	19	y.	y.	PROPN
eurjchem-844	236	20	;	;	PUNCT
eurjchem-844	236	21	fukuda	fukuda	PROPN
eurjchem-844	236	22	,	,	PUNCT
eurjchem-844	236	23	k.	k.	PROPN
eurjchem-844	236	24	;	;	PUNCT
eurjchem-844	236	25	serra	serra	PROPN
eurjchem-844	236	26	,	,	PUNCT
eurjchem-844	236	27	c.	c.	PROPN
eurjchem-844	236	28	j.	j.	PROPN
eurjchem-844	236	29	pharm	pharm	PROPN
eurjchem-844	236	30	.	.	PUNCT
eurjchem-844	237	1	biomed	biome	VERB
eurjchem-844	237	2	.	.	PUNCT
eurjchem-844	238	1	anal	anal	PROPN
eurjchem-844	238	2	.	.	PUNCT
eurjchem-844	238	3	2008	2008	NUM
eurjchem-844	238	4	,	,	PUNCT
eurjchem-844	238	5	46	46	NUM
eurjchem-844	238	6	,	,	PUNCT
eurjchem-844	238	7	143‐147	143‐147	NUM
eurjchem-844	238	8	.	.	PUNCT
eurjchem-844	239	1	[	[	X
eurjchem-844	239	2	14	14	NUM
eurjchem-844	239	3	]	]	PUNCT
eurjchem-844	239	4	.	.	PUNCT
eurjchem-844	240	1	zhong	zhong	PROPN
eurjchem-844	240	2	,	,	PUNCT
eurjchem-844	240	3	l.	l.	PROPN
eurjchem-844	240	4	;	;	PUNCT
eurjchem-844	240	5	ling	ling	PROPN
eurjchem-844	240	6	,	,	PUNCT
eurjchem-844	240	7	x.	x.	NOUN
eurjchem-844	240	8	;	;	PUNCT
eurjchem-844	240	9	sun	sun	PROPN
eurjchem-844	240	10	,	,	PUNCT
eurjchem-844	240	11	h.	h.	PROPN
eurjchem-844	240	12	yaowu‐fenxi‐zazhi	yaowu‐fenxi‐zazhi	PROPN
eurjchem-844	240	13	2008	2008	NUM
eurjchem-844	240	14	,	,	PUNCT
eurjchem-844	240	15	28	28	NUM
eurjchem-844	240	16	,	,	PUNCT
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eurjchem-844	240	18	.	.	PUNCT
eurjchem-844	241	1	[	[	X
eurjchem-844	241	2	15	15	NUM
eurjchem-844	241	3	]	]	SYM
eurjchem-844	241	4	.	.	PUNCT
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eurjchem-844	241	8	;	;	PUNCT
eurjchem-844	241	9	rafiuddin	rafiuddin	VERB
eurjchem-844	241	10	,	,	PUNCT
eurjchem-844	241	11	s.	s.	PROPN
eurjchem-844	241	12	;	;	PUNCT
eurjchem-844	241	13	ghori	ghori	PROPN
eurjchem-844	241	14	,	,	PUNCT
eurjchem-844	241	15	m.	m.	NOUN
eurjchem-844	241	16	;	;	PUNCT
eurjchem-844	241	17	khatri	khatri	PROPN
eurjchem-844	241	18	,	,	PUNCT
eurjchem-844	241	19	a.	a.	PROPN
eurjchem-844	241	20	chromatographia	chromatographia	NOUN
eurjchem-844	241	21	2008	2008	NUM
eurjchem-844	241	22	,	,	PUNCT
eurjchem-844	241	23	67	67	NUM
eurjchem-844	241	24	,	,	PUNCT
eurjchem-844	241	25	517‐525	517‐525	NOUN
eurjchem-844	241	26	.	.	PUNCT
eurjchem-844	242	1	[	[	X
eurjchem-844	242	2	16	16	NUM
eurjchem-844	242	3	]	]	PUNCT
eurjchem-844	242	4	.	.	PUNCT
eurjchem-844	243	1	al‐rimawi	al‐rimawi	PROPN
eurjchem-844	243	2	,	,	PUNCT
eurjchem-844	243	3	f.	f.	PROPN
eurjchem-844	243	4	talanta	talanta	PROPN
eurjchem-844	243	5	2009	2009	NUM
eurjchem-844	243	6	,	,	PUNCT
eurjchem-844	243	7	79	79	NUM
eurjchem-844	243	8	,	,	PUNCT
eurjchem-844	243	9	1368‐1371	1368‐1371	NUM
eurjchem-844	243	10	.	.	PUNCT
eurjchem-844	244	1	[	[	X
eurjchem-844	244	2	17	17	NUM
eurjchem-844	244	3	]	]	PUNCT
eurjchem-844	244	4	.	.	PUNCT
eurjchem-844	245	1	moffat	moffat	PROPN
eurjchem-844	245	2	,	,	PUNCT
eurjchem-844	245	3	a.	a.	PROPN
eurjchem-844	245	4	;	;	PUNCT
eurjchem-844	245	5	osselton	osselton	PROPN
eurjchem-844	245	6	,	,	PUNCT
eurjchem-844	245	7	m.	m.	NOUN
eurjchem-844	245	8	;	;	PUNCT
eurjchem-844	245	9	widdop	widdop	NOUN
eurjchem-844	245	10	,	,	PUNCT
eurjchem-844	245	11	b.	b.	PROPN
eurjchem-844	245	12	;	;	PUNCT
eurjchem-844	245	13	galichet	galichet	PROPN
eurjchem-844	245	14	,	,	PUNCT
eurjchem-844	245	15	l.	l.	PROPN
eurjchem-844	245	16	clarke	clarke	PROPN
eurjchem-844	245	17	's	's	PART
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eurjchem-844	245	21	and	and	CCONJ
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eurjchem-844	245	23	,	,	PUNCT
eurjchem-844	245	24	3rd	3rd	ADJ
eurjchem-844	245	25	edn	edn	NOUN
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eurjchem-844	245	27	,	,	PUNCT
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eurjchem-844	245	29	press	press	NOUN
eurjchem-844	245	30	,	,	PUNCT
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eurjchem-844	245	32	(	(	PUNCT
eurjchem-844	245	33	2004	2004	NUM
eurjchem-844	245	34	)	)	PUNCT
eurjchem-844	245	35	pp	pp	ADV
eurjchem-844	245	36	.	.	PUNCT
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eurjchem-844	246	2	,	,	PUNCT
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eurjchem-844	246	4	.	.	PUNCT
eurjchem-844	247	1	[	[	X
eurjchem-844	247	2	18	18	NUM
eurjchem-844	247	3	]	]	PUNCT
eurjchem-844	247	4	.	.	PUNCT
eurjchem-844	248	1	olmo	olmo	PROPN
eurjchem-844	248	2	,	,	PUNCT
eurjchem-844	248	3	b.	b.	PROPN
eurjchem-844	248	4	;	;	PUNCT
eurjchem-844	248	5	garcia	garcia	PROPN
eurjchem-844	248	6	,	,	PUNCT
eurjchem-844	248	7	a.	a.	NOUN
eurjchem-844	248	8	;	;	PUNCT
eurjchem-844	248	9	marin	marin	NOUN
eurjchem-844	248	10	,	,	PUNCT
eurjchem-844	248	11	a.	a.	NOUN
eurjchem-844	248	12	;	;	PUNCT
eurjchem-844	249	1	barbas	barbas	PROPN
eurjchem-844	249	2	.	.	PUNCT
eurjchem-844	250	1	c.	c.	PROPN
eurjchem-844	250	2	j.	j.	PROPN
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eurjchem-844	250	4	.	.	PUNCT
eurjchem-844	251	1	2005	2005	NUM
eurjchem-844	251	2	,	,	PUNCT
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eurjchem-844	251	4	,	,	PUNCT
eurjchem-844	251	5	159‐165	159‐165	NUM
eurjchem-844	251	6	.	.	PUNCT
eurjchem-844	252	1	[	[	X
eurjchem-844	252	2	19	19	NUM
eurjchem-844	252	3	]	]	SYM
eurjchem-844	252	4	.	.	PUNCT
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eurjchem-844	252	6	,	,	PUNCT
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eurjchem-844	252	8	;	;	PUNCT
eurjchem-844	252	9	shah	shah	PROPN
eurjchem-844	252	10	,	,	PUNCT
eurjchem-844	252	11	s.	s.	PROPN
eurjchem-844	252	12	;	;	PUNCT
eurjchem-844	252	13	karmuse	karmuse	NOUN
eurjchem-844	252	14	,	,	PUNCT
eurjchem-844	252	15	p.	p.	NOUN
eurjchem-844	252	16	;	;	PUNCT
eurjchem-844	252	17	phadke	phadke	ADJ
eurjchem-844	252	18	,	,	PUNCT
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eurjchem-844	252	20	;	;	PUNCT
eurjchem-844	252	21	jadhav	jadhav	PROPN
eurjchem-844	252	22	.	.	PUNCT
eurjchem-844	253	1	v.	v.	PROPN
eurjchem-844	253	2	j.	j.	PROPN
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eurjchem-844	253	4	.	.	PUNCT
eurjchem-844	253	5	biomed	biome	VERB
eurjchem-844	253	6	.	.	PUNCT
eurjchem-844	254	1	anal	anal	PROPN
eurjchem-844	254	2	.	.	PUNCT
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eurjchem-844	254	4	,	,	PUNCT
eurjchem-844	254	5	46	46	NUM
eurjchem-844	254	6	,	,	PUNCT
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eurjchem-844	254	8	.	.	PUNCT
eurjchem-844	255	1	[	[	X
eurjchem-844	255	2	20	20	NUM
eurjchem-844	255	3	]	]	PUNCT
eurjchem-844	255	4	.	.	PUNCT
eurjchem-844	256	1	shaikh	shaikh	PROPN
eurjchem-844	256	2	,	,	PUNCT
eurjchem-844	256	3	s.	s.	PROPN
eurjchem-844	256	4	;	;	PUNCT
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eurjchem-844	256	6	,	,	PUNCT
eurjchem-844	256	7	o.	o.	PROPN
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eurjchem-844	256	12	;	;	PUNCT
eurjchem-844	256	13	akmal	akmal	PROPN
eurjchem-844	256	14	,	,	PUNCT
eurjchem-844	256	15	j.	j.	PROPN
eurjchem-844	256	16	;	;	PUNCT
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eurjchem-844	256	18	,	,	PUNCT
eurjchem-844	256	19	a.	a.	NOUN
eurjchem-844	256	20	;	;	PUNCT
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eurjchem-844	256	22	.	.	PUNCT
eurjchem-844	257	1	k.	k.	PROPN
eurjchem-844	257	2	j.	j.	PROPN
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eurjchem-844	257	4	.	.	PUNCT
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eurjchem-844	257	6	.	.	PUNCT
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eurjchem-844	258	2	.	.	PUNCT
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eurjchem-844	258	4	,	,	PUNCT
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eurjchem-844	258	6	,	,	PUNCT
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eurjchem-844	258	8	.	.	PUNCT
eurjchem-844	259	1	[	[	X
eurjchem-844	259	2	21	21	NUM
eurjchem-844	259	3	]	]	PUNCT
eurjchem-844	259	4	.	.	PUNCT
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eurjchem-844	260	2	,	,	PUNCT
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eurjchem-844	260	4	;	;	PUNCT
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eurjchem-844	260	6	,	,	PUNCT
eurjchem-844	260	7	s.	s.	PROPN
eurjchem-844	260	8	;	;	PUNCT
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eurjchem-844	260	10	,	,	PUNCT
eurjchem-844	260	11	l.	l.	PROPN
eurjchem-844	260	12	;	;	PUNCT
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eurjchem-844	260	14	,	,	PUNCT
eurjchem-844	260	15	c.	c.	PROPN
eurjchem-844	260	16	;	;	PUNCT
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eurjchem-844	261	2	.	.	PUNCT
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eurjchem-844	262	2	,	,	PUNCT
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eurjchem-844	262	4	,	,	PUNCT
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eurjchem-844	262	6	.	.	PUNCT
eurjchem-844	263	1	[	[	X
eurjchem-844	263	2	22	22	NUM
eurjchem-844	263	3	]	]	PUNCT
eurjchem-844	263	4	.	.	PUNCT
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eurjchem-844	264	2	,	,	PUNCT
eurjchem-844	264	3	c.	c.	PROPN
eurjchem-844	264	4	;	;	PUNCT
eurjchem-844	264	5	mok	mok	PROPN
eurjchem-844	264	6	,	,	PUNCT
eurjchem-844	264	7	c.	c.	PROPN
eurjchem-844	264	8	;	;	PUNCT
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eurjchem-844	264	10	,	,	PUNCT
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eurjchem-844	264	13	.	.	PUNCT
eurjchem-844	265	1	chim	chim	PROPN
eurjchem-844	265	2	.	.	PUNCT
eurjchem-844	266	1	acta	acta	PROPN
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eurjchem-844	266	3	,	,	PUNCT
eurjchem-844	266	4	314	314	NUM
eurjchem-844	266	5	,	,	PUNCT
eurjchem-844	266	6	77‐85	77‐85	X
eurjchem-844	266	7	.	.	PUNCT
eurjchem-844	267	1	[	[	X
eurjchem-844	267	2	23	23	NUM
eurjchem-844	267	3	]	]	PUNCT
eurjchem-844	267	4	.	.	PUNCT
eurjchem-844	268	1	united	united	PROPN
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eurjchem-844	268	4	,	,	PUNCT
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eurjchem-844	268	6	.	.	PUNCT
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eurjchem-844	269	3	,	,	PUNCT
eurjchem-844	269	4	nf25	nf25	PROPN
eurjchem-844	269	5	,	,	PUNCT
eurjchem-844	269	6	(	(	PUNCT
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eurjchem-844	269	8	)	)	PUNCT
eurjchem-844	269	9	,	,	PUNCT
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eurjchem-844	269	11	.	.	PUNCT
eurjchem-844	270	1	[	[	X
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eurjchem-844	270	4	.	.	PUNCT
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eurjchem-844	271	4	.	.	PUNCT
eurjchem-844	272	1	4th	4th	ADJ
eurjchem-844	272	2	ed	ed	NOUN
eurjchem-844	272	3	.	.	PUNCT
eurjchem-844	272	4	vol	vol	NOUN
eurjchem-844	272	5	.	.	PUNCT
eurjchem-844	273	1	i.	i.	PROPN
eurjchem-844	273	2	new	new	PROPN
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eurjchem-844	273	4	:	:	PUNCT
eurjchem-844	273	5	the	the	DET
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eurjchem-844	273	8	publications	publication	NOUN
eurjchem-844	273	9	;	;	PUNCT
eurjchem-844	273	10	1996	1996	NUM
eurjchem-844	273	11	.	.	PUNCT
eurjchem-844	274	1	pp	pp	ADV
eurjchem-844	274	2	.	.	PUNCT
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eurjchem-844	275	2	.	.	PUNCT