id	sid	tid	token	lemma	pos
eurjchem-845	1	1	untitled	untitle	VERB
eurjchem-845	1	2	european	european	PROPN
eurjchem-845	1	3	journal	journal	PROPN
eurjchem-845	1	4	of	of	ADP
eurjchem-845	1	5	chemistry	chemistry	NOUN
eurjchem-845	1	6	5	5	NUM
eurjchem-845	1	7	(	(	PUNCT
eurjchem-845	1	8	2	2	NUM
eurjchem-845	1	9	)	)	PUNCT
eurjchem-845	1	10	(	(	PUNCT
eurjchem-845	1	11	2014	2014	NUM
eurjchem-845	1	12	)	)	PUNCT
eurjchem-845	1	13	380‐382	380‐382	PROPN
eurjchem-845	1	14	european	european	ADJ
eurjchem-845	1	15	journal	journal	PROPN
eurjchem-845	1	16	of	of	ADP
eurjchem-845	1	17	chemistry	chemistry	NOUN
eurjchem-845	1	18	issn	issn	PROPN
eurjchem-845	1	19	2153‐2249	2153‐2249	PROPN
eurjchem-845	1	20	(	(	PUNCT
eurjchem-845	1	21	print	print	NOUN
eurjchem-845	1	22	)	)	PUNCT
eurjchem-845	1	23	/	/	SYM
eurjchem-845	1	24	issn	issn	PROPN
eurjchem-845	1	25	2153‐2257	2153‐2257	NUM
eurjchem-845	1	26	(	(	PUNCT
eurjchem-845	1	27	online	online	ADJ
eurjchem-845	1	28	)	)	PUNCT
eurjchem-845	1	29			NOUN
eurjchem-845	1	30	2014	2014	NUM
eurjchem-845	2	1	eurjchem	eurjchem	PROPN
eurjchem-845	2	2	publishing	publish	VERB
eurjchem-845	2	3	‐	‐	NOUN
eurjchem-845	2	4	printed	print	VERB
eurjchem-845	2	5	in	in	ADP
eurjchem-845	2	6	the	the	DET
eurjchem-845	2	7	usa	usa	PROPN
eurjchem-845	2	8	http://dx.doi.org/10.5155/eurjchem.5.2.380‐382.845	http://dx.doi.org/10.5155/eurjchem.5.2.380‐382.845	PROPN
eurjchem-845	2	9	european	european	PROPN
eurjchem-845	2	10	journal	journal	PROPN
eurjchem-845	2	11	of	of	ADP
eurjchem-845	2	12	chemistry	chemistry	PROPN
eurjchem-845	2	13	journal	journal	PROPN
eurjchem-845	2	14	homepage	homepage	NOUN
eurjchem-845	2	15	:	:	PUNCT
eurjchem-845	2	16	www.eurjchem.com	www.eurjchem.com	X
eurjchem-845	2	17	spectrofluorometric	spectrofluorometric	ADJ
eurjchem-845	2	18	determination	determination	NOUN
eurjchem-845	2	19	of	of	ADP
eurjchem-845	2	20	linagliptin	linagliptin	NOUN
eurjchem-845	2	21	in	in	ADP
eurjchem-845	2	22	bulk	bulk	NOUN
eurjchem-845	2	23	and	and	CCONJ
eurjchem-845	2	24	in	in	ADP
eurjchem-845	2	25	pharmaceutical	pharmaceutical	ADJ
eurjchem-845	2	26	dosage	dosage	NOUN
eurjchem-845	2	27	form	form	NOUN
eurjchem-845	2	28	ramzia	ramzia	PROPN
eurjchem-845	2	29	ismail	ismail	PROPN
eurjchem-845	2	30	el‐bagary	el‐bagary	PROPN
eurjchem-845	2	31	a	a	PROPN
eurjchem-845	2	32	,	,	PUNCT
eurjchem-845	2	33	ehab	ehab	PROPN
eurjchem-845	2	34	farouk	farouk	PROPN
eurjchem-845	2	35	elkady	elkady	PROPN
eurjchem-845	2	36	a	a	PROPN
eurjchem-845	2	37	,	,	PUNCT
eurjchem-845	2	38	and	and	CCONJ
eurjchem-845	2	39	bassam	bassam	PROPN
eurjchem-845	2	40	mahfouz	mahfouz	PROPN
eurjchem-845	2	41	ayoub	ayoub	PROPN
eurjchem-845	2	42	b	b	PROPN
eurjchem-845	2	43	,	,	PUNCT
eurjchem-845	2	44	*	*	PUNCT
eurjchem-845	2	45	a	a	DET
eurjchem-845	2	46	pharmaceutical	pharmaceutical	ADJ
eurjchem-845	2	47	chemistry	chemistry	NOUN
eurjchem-845	2	48	department	department	NOUN
eurjchem-845	2	49	,	,	PUNCT
eurjchem-845	2	50	faculty	faculty	NOUN
eurjchem-845	2	51	of	of	ADP
eurjchem-845	2	52	pharmacy	pharmacy	NOUN
eurjchem-845	2	53	,	,	PUNCT
eurjchem-845	2	54	cairo	cairo	PROPN
eurjchem-845	2	55	university	university	PROPN
eurjchem-845	2	56	,	,	PUNCT
eurjchem-845	2	57	cairo	cairo	PROPN
eurjchem-845	2	58	11562	11562	NUM
eurjchem-845	2	59	,	,	PUNCT
eurjchem-845	2	60	egypt	egypt	PROPN
eurjchem-845	2	61	b	b	PROPN
eurjchem-845	2	62	pharmaceutical	pharmaceutical	ADJ
eurjchem-845	2	63	chemistry	chemistry	NOUN
eurjchem-845	2	64	department	department	NOUN
eurjchem-845	2	65	,	,	PUNCT
eurjchem-845	2	66	faculty	faculty	NOUN
eurjchem-845	2	67	of	of	ADP
eurjchem-845	2	68	pharmacy	pharmacy	NOUN
eurjchem-845	2	69	,	,	PUNCT
eurjchem-845	2	70	british	british	ADJ
eurjchem-845	2	71	university	university	PROPN
eurjchem-845	2	72	in	in	ADP
eurjchem-845	2	73	egypt	egypt	PROPN
eurjchem-845	2	74	,	,	PUNCT
eurjchem-845	2	75	el‐sherouk	el‐sherouk	PROPN
eurjchem-845	2	76	city	city	NOUN
eurjchem-845	2	77	,	,	PUNCT
eurjchem-845	2	78	cairo	cairo	PROPN
eurjchem-845	2	79	11837	11837	NUM
eurjchem-845	2	80	,	,	PUNCT
eurjchem-845	2	81	egypt	egypt	PROPN
eurjchem-845	2	82	*	*	PUNCT
eurjchem-845	2	83	corresponding	correspond	VERB
eurjchem-845	2	84	author	author	NOUN
eurjchem-845	2	85	at	at	ADP
eurjchem-845	2	86	:	:	PUNCT
eurjchem-845	2	87	pharmaceutical	pharmaceutical	ADJ
eurjchem-845	2	88	chemistry	chemistry	NOUN
eurjchem-845	2	89	department	department	NOUN
eurjchem-845	2	90	,	,	PUNCT
eurjchem-845	2	91	faculty	faculty	NOUN
eurjchem-845	2	92	of	of	ADP
eurjchem-845	2	93	pharmacy	pharmacy	NOUN
eurjchem-845	2	94	,	,	PUNCT
eurjchem-845	2	95	british	british	ADJ
eurjchem-845	2	96	university	university	PROPN
eurjchem-845	2	97	in	in	ADP
eurjchem-845	2	98	egypt	egypt	PROPN
eurjchem-845	2	99	,	,	PUNCT
eurjchem-845	2	100	el‐sherouk	el‐sherouk	PROPN
eurjchem-845	2	101	city	city	NOUN
eurjchem-845	2	102	,	,	PUNCT
eurjchem-845	2	103	cairo	cairo	PROPN
eurjchem-845	2	104	11837	11837	NUM
eurjchem-845	2	105	,	,	PUNCT
eurjchem-845	2	106	egypt	egypt	PROPN
eurjchem-845	2	107	.	.	PUNCT
eurjchem-845	3	1	tel	tel	PROPN
eurjchem-845	3	2	.	.	PUNCT
eurjchem-845	3	3	:	:	PUNCT
eurjchem-845	4	1	+2.01.225104337	+2.01.225104337	ADJ
eurjchem-845	4	2	.	.	PUNCT
eurjchem-845	5	1	fax	fax	NOUN
eurjchem-845	5	2	:	:	PUNCT
eurjchem-845	5	3	+2.02.24148452	+2.02.24148452	PROPN
eurjchem-845	5	4	.	.	PUNCT
eurjchem-845	5	5	e‐mail	e‐mail	PUNCT
eurjchem-845	6	1	address	address	NOUN
eurjchem-845	6	2	:	:	PUNCT
eurjchem-845	6	3	bassam.ayoub@bue.edu.eg	bassam.ayoub@bue.edu.eg	PROPN
eurjchem-845	6	4	(	(	PUNCT
eurjchem-845	6	5	b.m	b.m	PROPN
eurjchem-845	6	6	.	.	PROPN
eurjchem-845	6	7	ayoub	ayoub	PROPN
eurjchem-845	6	8	)	)	PUNCT
eurjchem-845	6	9	.	.	PUNCT
eurjchem-845	7	1	communication	communication	NOUN
eurjchem-845	7	2	information	information	NOUN
eurjchem-845	7	3	abstract	abstract	ADJ
eurjchem-845	7	4	doi	doi	NOUN
eurjchem-845	7	5	:	:	PUNCT
eurjchem-845	7	6	10.5155	10.5155	NUM
eurjchem-845	7	7	/	/	SYM
eurjchem-845	7	8	eurjchem.5.2.380‐382.845	eurjchem.5.2.380‐382.845	NOUN
eurjchem-845	7	9	received	receive	VERB
eurjchem-845	7	10	:	:	PUNCT
eurjchem-845	7	11	04	04	NUM
eurjchem-845	7	12	june	june	PROPN
eurjchem-845	7	13	2013	2013	NUM
eurjchem-845	7	14	received	receive	VERB
eurjchem-845	7	15	in	in	ADP
eurjchem-845	7	16	revised	revise	VERB
eurjchem-845	7	17	form	form	NOUN
eurjchem-845	7	18	:	:	PUNCT
eurjchem-845	7	19	26	26	NUM
eurjchem-845	7	20	july	july	PROPN
eurjchem-845	7	21	2013	2013	NUM
eurjchem-845	7	22	accepted	accept	VERB
eurjchem-845	7	23	:	:	PUNCT
eurjchem-845	7	24	18	18	NUM
eurjchem-845	7	25	august	august	PROPN
eurjchem-845	7	26	2013	2013	NUM
eurjchem-845	7	27	online	online	NOUN
eurjchem-845	7	28	:	:	PUNCT
eurjchem-845	7	29	30	30	NUM
eurjchem-845	7	30	june	june	PROPN
eurjchem-845	7	31	2014	2014	NUM
eurjchem-845	7	32	keywords	keyword	NOUN
eurjchem-845	7	33	simple	simple	ADJ
eurjchem-845	7	34	and	and	CCONJ
eurjchem-845	7	35	precise	precise	ADJ
eurjchem-845	7	36	spectrofluorometric	spectrofluorometric	ADJ
eurjchem-845	7	37	method	method	NOUN
eurjchem-845	7	38	has	have	AUX
eurjchem-845	7	39	been	be	AUX
eurjchem-845	7	40	developed	develop	VERB
eurjchem-845	7	41	and	and	CCONJ
eurjchem-845	7	42	validated	validate	VERB
eurjchem-845	7	43	for	for	ADP
eurjchem-845	7	44	the	the	DET
eurjchem-845	7	45	determination	determination	NOUN
eurjchem-845	7	46	of	of	ADP
eurjchem-845	7	47	linagliptin	linagliptin	ADJ
eurjchem-845	7	48	(	(	PUNCT
eurjchem-845	7	49	lng	lng	NOUN
eurjchem-845	7	50	)	)	PUNCT
eurjchem-845	7	51	in	in	ADP
eurjchem-845	7	52	the	the	DET
eurjchem-845	7	53	range	range	NOUN
eurjchem-845	7	54	of	of	ADP
eurjchem-845	7	55	10‐110	10‐110	NUM
eurjchem-845	7	56	μg	μg	PROPN
eurjchem-845	7	57	/	/	SYM
eurjchem-845	7	58	ml	ml	PROPN
eurjchem-845	7	59	.	.	PUNCT
eurjchem-845	8	1	the	the	DET
eurjchem-845	8	2	results	result	NOUN
eurjchem-845	8	3	obtained	obtain	VERB
eurjchem-845	8	4	were	be	AUX
eurjchem-845	8	5	of	of	ADP
eurjchem-845	8	6	good	good	ADJ
eurjchem-845	8	7	precision	precision	NOUN
eurjchem-845	8	8	and	and	CCONJ
eurjchem-845	8	9	statistically	statistically	ADV
eurjchem-845	8	10	compared	compare	VERB
eurjchem-845	8	11	to	to	ADP
eurjchem-845	8	12	the	the	DET
eurjchem-845	8	13	reference	reference	NOUN
eurjchem-845	8	14	method	method	NOUN
eurjchem-845	8	15	using	use	VERB
eurjchem-845	8	16	one‐way	one‐way	NUM
eurjchem-845	8	17	analysis	analysis	NOUN
eurjchem-845	8	18	of	of	ADP
eurjchem-845	8	19	variance	variance	NOUN
eurjchem-845	8	20	(	(	PUNCT
eurjchem-845	8	21	anova	anova	PROPN
eurjchem-845	8	22	)	)	PUNCT
eurjchem-845	8	23	.	.	PUNCT
eurjchem-845	9	1	the	the	DET
eurjchem-845	9	2	method	method	NOUN
eurjchem-845	9	3	developed	develop	VERB
eurjchem-845	9	4	was	be	AUX
eurjchem-845	9	5	satisfactorily	satisfactorily	ADV
eurjchem-845	9	6	applied	apply	VERB
eurjchem-845	9	7	to	to	ADP
eurjchem-845	9	8	the	the	DET
eurjchem-845	9	9	analysis	analysis	NOUN
eurjchem-845	9	10	of	of	ADP
eurjchem-845	9	11	the	the	DET
eurjchem-845	9	12	pharmaceutical	pharmaceutical	ADJ
eurjchem-845	9	13	formulation	formulation	NOUN
eurjchem-845	9	14	and	and	CCONJ
eurjchem-845	9	15	proved	prove	VERB
eurjchem-845	9	16	to	to	PART
eurjchem-845	9	17	be	be	AUX
eurjchem-845	9	18	specific	specific	ADJ
eurjchem-845	9	19	and	and	CCONJ
eurjchem-845	9	20	accurate	accurate	ADJ
eurjchem-845	9	21	for	for	ADP
eurjchem-845	9	22	the	the	DET
eurjchem-845	9	23	quality	quality	NOUN
eurjchem-845	9	24	control	control	NOUN
eurjchem-845	9	25	of	of	ADP
eurjchem-845	9	26	linagliptin	linagliptin	NOUN
eurjchem-845	9	27	in	in	ADP
eurjchem-845	9	28	its	its	PRON
eurjchem-845	9	29	pharmaceutical	pharmaceutical	ADJ
eurjchem-845	9	30	dosage	dosage	NOUN
eurjchem-845	9	31	form	form	NOUN
eurjchem-845	9	32	.	.	PUNCT
eurjchem-845	10	1	the	the	DET
eurjchem-845	10	2	development	development	NOUN
eurjchem-845	10	3	of	of	ADP
eurjchem-845	10	4	spectrofluorometric	spectrofluorometric	ADJ
eurjchem-845	10	5	method	method	NOUN
eurjchem-845	10	6	for	for	ADP
eurjchem-845	10	7	the	the	DET
eurjchem-845	10	8	determination	determination	NOUN
eurjchem-845	10	9	of	of	ADP
eurjchem-845	10	10	lng	lng	PROPN
eurjchem-845	10	11	was	be	AUX
eurjchem-845	10	12	of	of	ADP
eurjchem-845	10	13	interest	interest	NOUN
eurjchem-845	10	14	as	as	ADP
eurjchem-845	10	15	no	no	DET
eurjchem-845	10	16	such	such	ADJ
eurjchem-845	10	17	methods	method	NOUN
eurjchem-845	10	18	have	have	AUX
eurjchem-845	10	19	been	be	AUX
eurjchem-845	10	20	reported	report	VERB
eurjchem-845	10	21	.	.	PUNCT
eurjchem-845	11	1	tradjenta	tradjenta	PROPN
eurjchem-845	11	2	linagliptin	linagliptin	PROPN
eurjchem-845	11	3	fluorometry	fluorometry	NOUN
eurjchem-845	11	4	dpp‐4	dpp‐4	NOUN
eurjchem-845	11	5	inhibitors	inhibitor	NOUN
eurjchem-845	11	6	statistical	statistical	ADJ
eurjchem-845	11	7	analysis	analysis	NOUN
eurjchem-845	11	8	pharmaceutical	pharmaceutical	ADJ
eurjchem-845	11	9	preparation	preparation	NOUN
eurjchem-845	11	10	1	1	NUM
eurjchem-845	11	11	.	.	PUNCT
eurjchem-845	11	12	introduction	introduction	NOUN
eurjchem-845	11	13	linagliptin	linagliptin	ADJ
eurjchem-845	11	14	,	,	PUNCT
eurjchem-845	11	15	8‐[(3r)‐3‐aminopiperidin‐1‐yl]‐7‐(but‐2‐yn‐1‐	8‐[(3r)‐3‐aminopiperidin‐1‐yl]‐7‐(but‐2‐yn‐1‐	NUM
eurjchem-845	11	16	yl)‐3‐methyl‐1‐[(4‐methylquinazolin‐2‐yl)methyl]‐3,7‐dihydro‐	yl)‐3‐methyl‐1‐[(4‐methylquinazolin‐2‐yl)methyl]‐3,7‐dihydro‐	NOUN
eurjchem-845	11	17	1h‐purine‐2,6‐dione	1h‐purine‐2,6‐dione	NUM
eurjchem-845	11	18	]	]	PUNCT
eurjchem-845	11	19	(	(	PUNCT
eurjchem-845	11	20	figure	figure	NOUN
eurjchem-845	11	21	1	1	NUM
eurjchem-845	11	22	)	)	PUNCT
eurjchem-845	11	23	is	be	AUX
eurjchem-845	11	24	a	a	DET
eurjchem-845	11	25	new	new	ADJ
eurjchem-845	11	26	hypoglycemic	hypoglycemic	ADJ
eurjchem-845	11	27	drug	drug	NOUN
eurjchem-845	11	28	that	that	PRON
eurjchem-845	11	29	belongs	belong	VERB
eurjchem-845	11	30	to	to	ADP
eurjchem-845	11	31	dipeptidyl‐peptidase‐4	dipeptidyl‐peptidase‐4	VERB
eurjchem-845	11	32	inhibitor	inhibitor	NOUN
eurjchem-845	11	33	class	class	NOUN
eurjchem-845	11	34	which	which	PRON
eurjchem-845	11	35	stimulates	stimulate	VERB
eurjchem-845	11	36	glucose‐dependent	glucose‐dependent	ADJ
eurjchem-845	11	37	insulin	insulin	NOUN
eurjchem-845	11	38	release	release	NOUN
eurjchem-845	11	39	[	[	X
eurjchem-845	11	40	1,2	1,2	NUM
eurjchem-845	11	41	]	]	PUNCT
eurjchem-845	11	42	.	.	PUNCT
eurjchem-845	12	1	dpp‐4	dpp‐4	NOUN
eurjchem-845	12	2	inhibitors	inhibitor	NOUN
eurjchem-845	12	3	represent	represent	VERB
eurjchem-845	12	4	a	a	DET
eurjchem-845	12	5	new	new	ADJ
eurjchem-845	12	6	therapeutic	therapeutic	ADJ
eurjchem-845	12	7	approach	approach	NOUN
eurjchem-845	12	8	to	to	ADP
eurjchem-845	12	9	the	the	DET
eurjchem-845	12	10	treatment	treatment	NOUN
eurjchem-845	12	11	of	of	ADP
eurjchem-845	12	12	type	type	NOUN
eurjchem-845	12	13	2	2	NUM
eurjchem-845	12	14	diabetes	diabetes	NOUN
eurjchem-845	12	15	that	that	PRON
eurjchem-845	12	16	functions	function	NOUN
eurjchem-845	12	17	to	to	PART
eurjchem-845	12	18	stimulate	stimulate	VERB
eurjchem-845	12	19	glucose‐dependent	glucose‐dependent	NOUN
eurjchem-845	12	20	insulin	insulin	NOUN
eurjchem-845	12	21	release	release	NOUN
eurjchem-845	12	22	and	and	CCONJ
eurjchem-845	12	23	reduce	reduce	VERB
eurjchem-845	12	24	glucagons	glucagon	NOUN
eurjchem-845	12	25	levels	level	NOUN
eurjchem-845	12	26	.	.	PUNCT
eurjchem-845	13	1	this	this	PRON
eurjchem-845	13	2	is	be	AUX
eurjchem-845	13	3	done	do	VERB
eurjchem-845	13	4	through	through	ADP
eurjchem-845	13	5	inhibition	inhibition	NOUN
eurjchem-845	13	6	of	of	ADP
eurjchem-845	13	7	the	the	DET
eurjchem-845	13	8	inactivation	inactivation	NOUN
eurjchem-845	13	9	of	of	ADP
eurjchem-845	13	10	incretins	incretin	NOUN
eurjchem-845	13	11	,	,	PUNCT
eurjchem-845	13	12	particularly	particularly	ADV
eurjchem-845	13	13	glucagon‐like	glucagon‐like	ADP
eurjchem-845	13	14	peptide‐1	peptide‐1	PROPN
eurjchem-845	13	15	(	(	PUNCT
eurjchem-845	13	16	glp‐1	glp‐1	NOUN
eurjchem-845	13	17	)	)	PUNCT
eurjchem-845	13	18	and	and	CCONJ
eurjchem-845	13	19	gastric	gastric	ADJ
eurjchem-845	13	20	inhibitory	inhibitory	ADJ
eurjchem-845	13	21	polypeptide	polypeptide	ADJ
eurjchem-845	13	22	(	(	PUNCT
eurjchem-845	13	23	gip	gip	NOUN
eurjchem-845	13	24	)	)	PUNCT
eurjchem-845	14	1	[	[	X
eurjchem-845	14	2	1,2	1,2	NUM
eurjchem-845	14	3	]	]	PUNCT
eurjchem-845	14	4	.	.	PUNCT
eurjchem-845	15	1	only	only	ADV
eurjchem-845	15	2	one	one	NUM
eurjchem-845	15	3	method	method	NOUN
eurjchem-845	15	4	has	have	AUX
eurjchem-845	15	5	been	be	AUX
eurjchem-845	15	6	described	describe	VERB
eurjchem-845	15	7	for	for	ADP
eurjchem-845	15	8	the	the	DET
eurjchem-845	15	9	determination	determination	NOUN
eurjchem-845	15	10	of	of	ADP
eurjchem-845	15	11	lng	lng	PROPN
eurjchem-845	15	12	in	in	ADP
eurjchem-845	15	13	its	its	PRON
eurjchem-845	15	14	pharmaceutical	pharmaceutical	ADJ
eurjchem-845	15	15	preparation	preparation	NOUN
eurjchem-845	15	16	[	[	X
eurjchem-845	15	17	3	3	NUM
eurjchem-845	15	18	]	]	PUNCT
eurjchem-845	15	19	.	.	PUNCT
eurjchem-845	16	1	figure	figure	NOUN
eurjchem-845	16	2	1	1	NUM
eurjchem-845	16	3	.	.	PUNCT
eurjchem-845	16	4	chemical	chemical	ADJ
eurjchem-845	16	5	structure	structure	NOUN
eurjchem-845	16	6	of	of	ADP
eurjchem-845	16	7	linagliptin	linagliptin	PROPN
eurjchem-845	16	8	.	.	PUNCT
eurjchem-845	17	1	the	the	DET
eurjchem-845	17	2	aim	aim	NOUN
eurjchem-845	17	3	of	of	ADP
eurjchem-845	17	4	the	the	DET
eurjchem-845	17	5	present	present	ADJ
eurjchem-845	17	6	work	work	NOUN
eurjchem-845	17	7	was	be	AUX
eurjchem-845	17	8	to	to	PART
eurjchem-845	17	9	develop	develop	VERB
eurjchem-845	17	10	a	a	DET
eurjchem-845	17	11	spectrofluorometric	spectrofluorometric	ADJ
eurjchem-845	17	12	method	method	NOUN
eurjchem-845	17	13	for	for	ADP
eurjchem-845	17	14	the	the	DET
eurjchem-845	17	15	determination	determination	NOUN
eurjchem-845	17	16	of	of	ADP
eurjchem-845	17	17	lng	lng	PROPN
eurjchem-845	17	18	based	base	VERB
eurjchem-845	17	19	on	on	ADP
eurjchem-845	17	20	the	the	DET
eurjchem-845	17	21	native	native	ADJ
eurjchem-845	17	22	fluorescence	fluorescence	NOUN
eurjchem-845	17	23	of	of	ADP
eurjchem-845	17	24	the	the	DET
eurjchem-845	17	25	drug	drug	NOUN
eurjchem-845	17	26	.	.	PUNCT
eurjchem-845	18	1	spectro‐	spectro‐	PROPN
eurjchem-845	18	2	fluorometry	fluorometry	NOUN
eurjchem-845	18	3	has	have	AUX
eurjchem-845	18	4	long	long	ADV
eurjchem-845	18	5	been	be	AUX
eurjchem-845	18	6	applied	apply	VERB
eurjchem-845	18	7	in	in	ADP
eurjchem-845	18	8	the	the	DET
eurjchem-845	18	9	field	field	NOUN
eurjchem-845	18	10	of	of	ADP
eurjchem-845	18	11	pharmaceutical	pharmaceutical	ADJ
eurjchem-845	18	12	analysis	analysis	NOUN
eurjchem-845	18	13	of	of	ADP
eurjchem-845	18	14	many	many	ADJ
eurjchem-845	18	15	drugs	drug	NOUN
eurjchem-845	18	16	[	[	X
eurjchem-845	18	17	4‐7	4‐7	NOUN
eurjchem-845	18	18	]	]	PUNCT
eurjchem-845	18	19	because	because	SCONJ
eurjchem-845	18	20	of	of	ADP
eurjchem-845	18	21	the	the	DET
eurjchem-845	18	22	higher	high	ADJ
eurjchem-845	18	23	sensitivity	sensitivity	NOUN
eurjchem-845	18	24	than	than	SCONJ
eurjchem-845	18	25	is	be	AUX
eurjchem-845	18	26	attainable	attainable	ADJ
eurjchem-845	18	27	in	in	ADP
eurjchem-845	18	28	absorption	absorption	NOUN
eurjchem-845	18	29	spectro‐	spectro‐	NOUN
eurjchem-845	18	30	photometry	photometry	NOUN
eurjchem-845	18	31	.	.	PUNCT
eurjchem-845	19	1	a	a	DET
eurjchem-845	19	2	necessary	necessary	ADJ
eurjchem-845	19	3	condition	condition	NOUN
eurjchem-845	19	4	for	for	ADP
eurjchem-845	19	5	a	a	DET
eurjchem-845	19	6	compound	compound	NOUN
eurjchem-845	19	7	to	to	PART
eurjchem-845	19	8	fluoresce	fluoresce	VERB
eurjchem-845	19	9	is	be	AUX
eurjchem-845	19	10	that	that	SCONJ
eurjchem-845	19	11	it	it	PRON
eurjchem-845	19	12	absorbs	absorb	VERB
eurjchem-845	19	13	light	light	NOUN
eurjchem-845	19	14	in	in	ADP
eurjchem-845	19	15	the	the	DET
eurjchem-845	19	16	uv	uv	NOUN
eurjchem-845	19	17	or	or	CCONJ
eurjchem-845	19	18	visible	visible	ADJ
eurjchem-845	19	19	region	region	NOUN
eurjchem-845	19	20	of	of	ADP
eurjchem-845	19	21	the	the	DET
eurjchem-845	19	22	spectrum	spectrum	NOUN
eurjchem-845	19	23	.	.	PUNCT
eurjchem-845	20	1	accordingly	accordingly	ADV
eurjchem-845	20	2	,	,	PUNCT
eurjchem-845	20	3	compounds	compound	VERB
eurjchem-845	20	4	that	that	PRON
eurjchem-845	20	5	have	have	VERB
eurjchem-845	20	6	a	a	DET
eurjchem-845	20	7	conjugated	conjugate	VERB
eurjchem-845	20	8	π‐	π‐	ADJ
eurjchem-845	20	9	electron	electron	NOUN
eurjchem-845	20	10	system	system	NOUN
eurjchem-845	20	11	may	may	AUX
eurjchem-845	20	12	give	give	VERB
eurjchem-845	20	13	efficient	efficient	ADJ
eurjchem-845	20	14	re‐emission	re‐emission	NOUN
eurjchem-845	20	15	of	of	ADP
eurjchem-845	20	16	the	the	DET
eurjchem-845	20	17	absorbed	absorb	VERB
eurjchem-845	20	18	energy	energy	NOUN
eurjchem-845	20	19	as	as	ADP
eurjchem-845	20	20	a	a	DET
eurjchem-845	20	21	direct	direct	ADJ
eurjchem-845	20	22	method	method	NOUN
eurjchem-845	20	23	for	for	ADP
eurjchem-845	20	24	the	the	DET
eurjchem-845	20	25	determination	determination	NOUN
eurjchem-845	20	26	in	in	ADP
eurjchem-845	20	27	which	which	PRON
eurjchem-845	20	28	the	the	DET
eurjchem-845	20	29	native	native	ADJ
eurjchem-845	20	30	fluorescence	fluorescence	NOUN
eurjchem-845	20	31	of	of	ADP
eurjchem-845	20	32	the	the	DET
eurjchem-845	20	33	molecule	molecule	NOUN
eurjchem-845	20	34	is	be	AUX
eurjchem-845	20	35	measured	measure	VERB
eurjchem-845	20	36	[	[	X
eurjchem-845	20	37	4‐7	4‐7	X
eurjchem-845	20	38	]	]	X
eurjchem-845	20	39	.	.	PUNCT
eurjchem-845	21	1	2	2	X
eurjchem-845	21	2	.	.	X
eurjchem-845	21	3	experimental	experimental	ADJ
eurjchem-845	21	4	2.1	2.1	NUM
eurjchem-845	21	5	.	.	PUNCT
eurjchem-845	21	6	instrumentation	instrumentation	NOUN
eurjchem-845	21	7	a	a	DET
eurjchem-845	21	8	shimadzu	shimadzu	ADJ
eurjchem-845	21	9	rf‐1501	rf‐1501	ADJ
eurjchem-845	21	10	spectrofluorimeter	spectrofluorimeter	NOUN
eurjchem-845	21	11	(	(	PUNCT
eurjchem-845	21	12	japan	japan	PROPN
eurjchem-845	21	13	)	)	PUNCT
eurjchem-845	21	14	was	be	AUX
eurjchem-845	21	15	used	use	VERB
eurjchem-845	21	16	.	.	PUNCT
eurjchem-845	22	1	2.2	2.2	NUM
eurjchem-845	22	2	.	.	PUNCT
eurjchem-845	22	3	reagents	reagent	NOUN
eurjchem-845	22	4	and	and	CCONJ
eurjchem-845	22	5	reference	reference	NOUN
eurjchem-845	22	6	samples	sample	VERB
eurjchem-845	22	7	pharmaceutical	pharmaceutical	ADJ
eurjchem-845	22	8	grade	grade	NOUN
eurjchem-845	22	9	lng	lng	PROPN
eurjchem-845	22	10	,	,	PUNCT
eurjchem-845	22	11	certified	certify	VERB
eurjchem-845	22	12	to	to	PART
eurjchem-845	22	13	contain	contain	VERB
eurjchem-845	22	14	99.80	99.80	NUM
eurjchem-845	22	15	%	%	NOUN
eurjchem-845	22	16	,	,	PUNCT
eurjchem-845	22	17	tradjenta	tradjenta	ADJ
eurjchem-845	22	18	®	®	NOUN
eurjchem-845	22	19	tablets	tablet	NOUN
eurjchem-845	22	20	nominally	nominally	ADV
eurjchem-845	22	21	containing	contain	VERB
eurjchem-845	22	22	5	5	NUM
eurjchem-845	22	23	mg	mg	NOUN
eurjchem-845	22	24	of	of	ADP
eurjchem-845	22	25	lng	lng	PROPN
eurjchem-845	22	26	per	per	ADP
eurjchem-845	22	27	tablet	tablet	NOUN
eurjchem-845	22	28	were	be	AUX
eurjchem-845	22	29	supplied	supply	VERB
eurjchem-845	22	30	from	from	ADP
eurjchem-845	22	31	eli	eli	PROPN
eurjchem-845	22	32	lilly	lilly	PROPN
eurjchem-845	22	33	and	and	CCONJ
eurjchem-845	22	34	company	company	PROPN
eurjchem-845	22	35	(	(	PUNCT
eurjchem-845	22	36	usa	usa	PROPN
eurjchem-845	22	37	)	)	PUNCT
eurjchem-845	22	38	.	.	PUNCT
eurjchem-845	23	1	el‐bagary	el‐bagary	PROPN
eurjchem-845	23	2	et	et	PROPN
eurjchem-845	23	3	al	al	PROPN
eurjchem-845	23	4	.	.	PUNCT
eurjchem-845	23	5	/	/	SYM
eurjchem-845	23	6	european	european	PROPN
eurjchem-845	23	7	journal	journal	PROPN
eurjchem-845	23	8	of	of	ADP
eurjchem-845	23	9	chemistry	chemistry	NOUN
eurjchem-845	23	10	5	5	NUM
eurjchem-845	23	11	(	(	PUNCT
eurjchem-845	23	12	2	2	NUM
eurjchem-845	23	13	)	)	PUNCT
eurjchem-845	23	14	(	(	PUNCT
eurjchem-845	23	15	2014	2014	NUM
eurjchem-845	23	16	)	)	PUNCT
eurjchem-845	24	1	380‐382	380‐382	NOUN
eurjchem-845	24	2	381	381	NUM
eurjchem-845	24	3	table	table	NOUN
eurjchem-845	24	4	1	1	NUM
eurjchem-845	24	5	.	.	PUNCT
eurjchem-845	25	1	results	result	NOUN
eurjchem-845	25	2	obtained	obtain	VERB
eurjchem-845	25	3	by	by	ADP
eurjchem-845	25	4	the	the	DET
eurjchem-845	25	5	proposed	propose	VERB
eurjchem-845	25	6	fluorometric	fluorometric	ADJ
eurjchem-845	25	7	method	method	NOUN
eurjchem-845	25	8	for	for	ADP
eurjchem-845	25	9	the	the	DET
eurjchem-845	25	10	determination	determination	NOUN
eurjchem-845	25	11	of	of	ADP
eurjchem-845	25	12	linagliptin	linagliptin	PROPN
eurjchem-845	25	13	.	.	PUNCT
eurjchem-845	25	14	λmax	λmax	NOUN
eurjchem-845	25	15	excitation	excitation	NOUN
eurjchem-845	25	16	of	of	ADP
eurjchem-845	25	17	measurements	measurement	NOUN
eurjchem-845	25	18	,	,	PUNCT
eurjchem-845	25	19	nm	nm	PRON
eurjchem-845	25	20	339	339	NUM
eurjchem-845	25	21	λmax	λmax	NOUN
eurjchem-845	25	22	emission	emission	NOUN
eurjchem-845	25	23	of	of	ADP
eurjchem-845	25	24	measurements	measurement	NOUN
eurjchem-845	25	25	,	,	PUNCT
eurjchem-845	25	26	nm	nm	ADP
eurjchem-845	25	27	435	435	NUM
eurjchem-845	25	28	linearity	linearity	NOUN
eurjchem-845	25	29	,	,	PUNCT
eurjchem-845	25	30	μg	μg	PROPN
eurjchem-845	25	31	/	/	SYM
eurjchem-845	25	32	ml	ml	PROPN
eurjchem-845	25	33	10‐110	10‐110	NUM
eurjchem-845	25	34	regression	regression	NOUN
eurjchem-845	25	35	equation	equation	NOUN
eurjchem-845	25	36	f*435	f*435	PROPN
eurjchem-845	26	1	=	=	PUNCT
eurjchem-845	26	2	1.0534	1.0534	NUM
eurjchem-845	26	3	cμg	cμg	NOUN
eurjchem-845	26	4	/	/	SYM
eurjchem-845	26	5	ml	ml	NOUN
eurjchem-845	26	6	‐	‐	ADP
eurjchem-845	26	7	0.183	0.183	NUM
eurjchem-845	26	8	regression	regression	NOUN
eurjchem-845	26	9	coefficient	coefficient	NOUN
eurjchem-845	26	10	(	(	PUNCT
eurjchem-845	26	11	r2	r2	PROPN
eurjchem-845	26	12	)	)	PUNCT
eurjchem-845	26	13	0.9999	0.9999	NUM
eurjchem-845	26	14	lod	lod	NOUN
eurjchem-845	26	15	,	,	PUNCT
eurjchem-845	26	16	μg	μg	PROPN
eurjchem-845	26	17	/	/	SYM
eurjchem-845	26	18	ml	ml	PROPN
eurjchem-845	26	19	0.84	0.84	NUM
eurjchem-845	26	20	loq	loq	PROPN
eurjchem-845	26	21	,	,	PUNCT
eurjchem-845	26	22	μg	μg	PROPN
eurjchem-845	26	23	/	/	SYM
eurjchem-845	26	24	ml	ml	PROPN
eurjchem-845	26	25	8.01	8.01	NUM
eurjchem-845	26	26	sb	sb	PROPN
eurjchem-845	26	27	3.8×10‐3	3.8×10‐3	NUM
eurjchem-845	26	28	sa	sa	NOUN
eurjchem-845	26	29	0.32	0.32	NUM
eurjchem-845	26	30	confidence	confidence	NOUN
eurjchem-845	26	31	limit	limit	NOUN
eurjchem-845	26	32	of	of	ADP
eurjchem-845	26	33	the	the	DET
eurjchem-845	26	34	slope	slope	NOUN
eurjchem-845	26	35	1.0534±0.34	1.0534±0.34	NOUN
eurjchem-845	26	36	confidence	confidence	NOUN
eurjchem-845	26	37	limit	limit	NOUN
eurjchem-845	26	38	of	of	ADP
eurjchem-845	26	39	the	the	DET
eurjchem-845	26	40	intercept	intercept	NOUN
eurjchem-845	26	41	‐0.183±7.03×10‐4	‐0.183±7.03×10‐4	NOUN
eurjchem-845	26	42	standard	standard	ADJ
eurjchem-845	26	43	error	error	NOUN
eurjchem-845	26	44	of	of	ADP
eurjchem-845	26	45	the	the	DET
eurjchem-845	26	46	estimation	estimation	NOUN
eurjchem-845	26	47	0.32	0.32	NUM
eurjchem-845	26	48	drug	drug	NOUN
eurjchem-845	26	49	in	in	ADP
eurjchem-845	26	50	bulk	bulk	ADJ
eurjchem-845	26	51	100.30±0.93	100.30±0.93	NUM
eurjchem-845	26	52	drug	drug	NOUN
eurjchem-845	26	53	in	in	ADP
eurjchem-845	26	54	dosage	dosage	NOUN
eurjchem-845	26	55	form	form	NOUN
eurjchem-845	26	56	(	(	PUNCT
eurjchem-845	26	57	tradjenta	tradjenta	NOUN
eurjchem-845	26	58	®	®	NOUN
eurjchem-845	26	59	)	)	PUNCT
eurjchem-845	26	60	99.83±0.56	99.83±0.56	NUM
eurjchem-845	26	61	drug	drug	NOUN
eurjchem-845	26	62	added	add	VERB
eurjchem-845	26	63	100.05±0.92	100.05±0.92	NUM
eurjchem-845	26	64	f	f	X
eurjchem-845	26	65	*	*	NOUN
eurjchem-845	26	66	:	:	PUNCT
eurjchem-845	26	67	relative	relative	ADJ
eurjchem-845	26	68	fluorescence	fluorescence	NOUN
eurjchem-845	26	69	.	.	PUNCT
eurjchem-845	27	1	lod	lod	PROPN
eurjchem-845	27	2	:	:	PUNCT
eurjchem-845	27	3	limit	limit	NOUN
eurjchem-845	27	4	of	of	ADP
eurjchem-845	27	5	detection	detection	NOUN
eurjchem-845	27	6	,	,	PUNCT
eurjchem-845	27	7	loq	loq	PROPN
eurjchem-845	27	8	:	:	PUNCT
eurjchem-845	27	9	limit	limit	NOUN
eurjchem-845	27	10	of	of	ADP
eurjchem-845	27	11	quantification	quantification	NOUN
eurjchem-845	27	12	.	.	PUNCT
eurjchem-845	28	1	table	table	NOUN
eurjchem-845	28	2	2	2	NUM
eurjchem-845	28	3	.	.	PUNCT
eurjchem-845	29	1	statistical	statistical	ADJ
eurjchem-845	29	2	comparison	comparison	NOUN
eurjchem-845	29	3	between	between	ADP
eurjchem-845	29	4	the	the	DET
eurjchem-845	29	5	results	result	NOUN
eurjchem-845	29	6	of	of	ADP
eurjchem-845	29	7	the	the	DET
eurjchem-845	29	8	fluorometric	fluorometric	ADJ
eurjchem-845	29	9	method	method	NOUN
eurjchem-845	29	10	and	and	CCONJ
eurjchem-845	29	11	the	the	DET
eurjchem-845	29	12	reference	reference	NOUN
eurjchem-845	29	13	method	method	NOUN
eurjchem-845	29	14	for	for	ADP
eurjchem-845	29	15	the	the	DET
eurjchem-845	29	16	determination	determination	NOUN
eurjchem-845	29	17	of	of	ADP
eurjchem-845	29	18	linagliptin	linagliptin	ADJ
eurjchem-845	29	19	.	.	PUNCT
eurjchem-845	30	1	statistical	statistical	ADJ
eurjchem-845	30	2	term	term	NOUN
eurjchem-845	30	3	*	*	PUNCT
eurjchem-845	30	4	reference	reference	NOUN
eurjchem-845	30	5	method	method	NOUN
eurjchem-845	30	6	*	*	PUNCT
eurjchem-845	30	7	*	*	PUNCT
eurjchem-845	30	8	drug	drug	NOUN
eurjchem-845	30	9	in	in	ADP
eurjchem-845	30	10	bulk	bulk	ADJ
eurjchem-845	30	11	mean	mean	NOUN
eurjchem-845	30	12	99.45	99.45	NUM
eurjchem-845	30	13	100.30	100.30	NUM
eurjchem-845	30	14	s.d	s.d	PROPN
eurjchem-845	30	15	.	.	PROPN
eurjchem-845	30	16	1.34	1.34	NUM
eurjchem-845	30	17	0.93	0.93	NUM
eurjchem-845	30	18	s.e	s.e	PROPN
eurjchem-845	30	19	.	.	PROPN
eurjchem-845	30	20	0.60	0.60	NUM
eurjchem-845	30	21	0.42	0.42	NUM
eurjchem-845	30	22	%	%	NOUN
eurjchem-845	30	23	r.s.d	r.s.d	NOUN
eurjchem-845	30	24	.	.	PUNCT
eurjchem-845	31	1	1.35	1.35	NUM
eurjchem-845	31	2	0.93	0.93	NUM
eurjchem-845	31	3	n	n	NUM
eurjchem-845	31	4	5	5	NUM
eurjchem-845	31	5	5	5	NUM
eurjchem-845	31	6	v	v	ADP
eurjchem-845	31	7	1.80	1.80	NUM
eurjchem-845	31	8	0.86	0.86	NUM
eurjchem-845	31	9	t	t	NOUN
eurjchem-845	31	10	(	(	PUNCT
eurjchem-845	31	11	2.306	2.306	NUM
eurjchem-845	31	12	)	)	PUNCT
eurjchem-845	31	13	*	*	PUNCT
eurjchem-845	32	1	*	*	PUNCT
eurjchem-845	32	2	*	*	PUNCT
eurjchem-845	32	3	1.20	1.20	NUM
eurjchem-845	32	4	*	*	PUNCT
eurjchem-845	32	5	s.d	s.d	PROPN
eurjchem-845	32	6	.	.	PROPN
eurjchem-845	32	7	:	:	PUNCT
eurjchem-845	32	8	standard	standard	ADJ
eurjchem-845	32	9	deviation	deviation	NOUN
eurjchem-845	32	10	,	,	PUNCT
eurjchem-845	32	11	s.e	s.e	PROPN
eurjchem-845	32	12	.	.	PROPN
eurjchem-845	32	13	:	:	PUNCT
eurjchem-845	32	14	standard	standard	ADJ
eurjchem-845	32	15	error	error	NOUN
eurjchem-845	32	16	,	,	PUNCT
eurjchem-845	32	17	%	%	INTJ
eurjchem-845	32	18	r.s.d	r.s.d	NOUN
eurjchem-845	32	19	.	.	PUNCT
eurjchem-845	32	20	:	:	PUNCT
eurjchem-845	33	1	relative	relative	ADJ
eurjchem-845	33	2	standard	standard	ADJ
eurjchem-845	33	3	deviation	deviation	NOUN
eurjchem-845	33	4	,	,	PUNCT
eurjchem-845	33	5	n	n	CCONJ
eurjchem-845	33	6	:	:	PUNCT
eurjchem-845	33	7	number	number	NOUN
eurjchem-845	33	8	of	of	ADP
eurjchem-845	33	9	samples	sample	NOUN
eurjchem-845	33	10	,	,	PUNCT
eurjchem-845	33	11	v	v	NOUN
eurjchem-845	33	12	:	:	PUNCT
eurjchem-845	33	13	variance	variance	NOUN
eurjchem-845	33	14	.	.	PUNCT
eurjchem-845	34	1	*	*	PUNCT
eurjchem-845	34	2	*	*	PUNCT
eurjchem-845	34	3	reference	reference	NOUN
eurjchem-845	34	4	method	method	NOUN
eurjchem-845	34	5	:	:	PUNCT
eurjchem-845	34	6	aliquots	aliquot	NOUN
eurjchem-845	34	7	of	of	ADP
eurjchem-845	34	8	standard	standard	ADJ
eurjchem-845	34	9	solutions	solution	NOUN
eurjchem-845	34	10	in	in	ADP
eurjchem-845	34	11	methanol	methanol	NOUN
eurjchem-845	34	12	containing	contain	VERB
eurjchem-845	34	13	2‐10	2‐10	NUM
eurjchem-845	34	14	μg	μg	NOUN
eurjchem-845	34	15	/	/	SYM
eurjchem-845	34	16	ml	ml	PROPN
eurjchem-845	34	17	lng	lng	PROPN
eurjchem-845	34	18	were	be	AUX
eurjchem-845	34	19	measured	measure	VERB
eurjchem-845	34	20	at	at	ADP
eurjchem-845	34	21	299	299	NUM
eurjchem-845	34	22	nm	nm	NOUN
eurjchem-845	34	23	using	use	VERB
eurjchem-845	34	24	methanol	methanol	NOUN
eurjchem-845	34	25	as	as	ADP
eurjchem-845	34	26	a	a	DET
eurjchem-845	34	27	blank	blank	NOUN
eurjchem-845	35	1	[	[	X
eurjchem-845	35	2	2	2	NUM
eurjchem-845	35	3	]	]	PUNCT
eurjchem-845	35	4	.	.	PUNCT
eurjchem-845	36	1	no	no	DET
eurjchem-845	36	2	significant	significant	ADJ
eurjchem-845	36	3	difference	difference	NOUN
eurjchem-845	36	4	between	between	ADP
eurjchem-845	36	5	groups	group	NOUN
eurjchem-845	36	6	by	by	ADP
eurjchem-845	36	7	using	use	VERB
eurjchem-845	36	8	one	one	NUM
eurjchem-845	36	9	way	way	NOUN
eurjchem-845	36	10	anova	anova	X
eurjchem-845	36	11	with	with	ADP
eurjchem-845	36	12	f	f	PROPN
eurjchem-845	36	13	=	=	PROPN
eurjchem-845	36	14	1.40	1.40	NUM
eurjchem-845	36	15	and	and	CCONJ
eurjchem-845	36	16	p	p	NOUN
eurjchem-845	36	17	=	=	PROPN
eurjchem-845	36	18	0.27	0.27	NUM
eurjchem-845	36	19	.	.	PUNCT
eurjchem-845	37	1	*	*	PUNCT
eurjchem-845	37	2	*	*	PUNCT
eurjchem-845	37	3	*	*	PUNCT
eurjchem-845	37	4	figure	figure	NOUN
eurjchem-845	37	5	in	in	ADP
eurjchem-845	37	6	parentheses	parenthesis	NOUN
eurjchem-845	37	7	are	be	AUX
eurjchem-845	37	8	the	the	DET
eurjchem-845	37	9	theoretical	theoretical	ADJ
eurjchem-845	37	10	t	t	NOUN
eurjchem-845	37	11	and	and	CCONJ
eurjchem-845	37	12	f	f	PROPN
eurjchem-845	37	13	values	value	NOUN
eurjchem-845	37	14	at	at	ADP
eurjchem-845	37	15	(	(	PUNCT
eurjchem-845	37	16	p	p	X
eurjchem-845	37	17	=	=	NOUN
eurjchem-845	37	18	0.05	0.05	NUM
eurjchem-845	37	19	)	)	PUNCT
eurjchem-845	37	20	.	.	PUNCT
eurjchem-845	38	1	standard	standard	ADJ
eurjchem-845	38	2	stock	stock	NOUN
eurjchem-845	38	3	solutions	solution	NOUN
eurjchem-845	38	4	of	of	ADP
eurjchem-845	38	5	lng	lng	PROPN
eurjchem-845	38	6	(	(	PUNCT
eurjchem-845	38	7	1	1	NUM
eurjchem-845	38	8	mg	mg	NUM
eurjchem-845	38	9	/	/	SYM
eurjchem-845	38	10	ml	ml	NOUN
eurjchem-845	38	11	)	)	PUNCT
eurjchem-845	38	12	were	be	AUX
eurjchem-845	38	13	prepared	prepare	VERB
eurjchem-845	38	14	by	by	ADP
eurjchem-845	38	15	dissolving	dissolve	VERB
eurjchem-845	38	16	100	100	NUM
eurjchem-845	38	17	mg	mg	ADP
eurjchem-845	38	18	of	of	ADP
eurjchem-845	38	19	the	the	DET
eurjchem-845	38	20	drug	drug	NOUN
eurjchem-845	38	21	in	in	ADP
eurjchem-845	38	22	acetonitrile	acetonitrile	NOUN
eurjchem-845	38	23	:	:	PUNCT
eurjchem-845	38	24	methanol	methanol	NOUN
eurjchem-845	38	25	,	,	PUNCT
eurjchem-845	38	26	(	(	PUNCT
eurjchem-845	38	27	90:10	90:10	NUM
eurjchem-845	38	28	,	,	PUNCT
eurjchem-845	38	29	v	v	NOUN
eurjchem-845	38	30	:	:	PUNCT
eurjchem-845	38	31	v	v	NOUN
eurjchem-845	38	32	)	)	PUNCT
eurjchem-845	38	33	and	and	CCONJ
eurjchem-845	38	34	completing	complete	VERB
eurjchem-845	38	35	the	the	DET
eurjchem-845	38	36	volume	volume	NOUN
eurjchem-845	38	37	to	to	ADP
eurjchem-845	38	38	100	100	NUM
eurjchem-845	38	39	ml	ml	NOUN
eurjchem-845	38	40	in	in	ADP
eurjchem-845	38	41	a	a	DET
eurjchem-845	38	42	volumetric	volumetric	NOUN
eurjchem-845	38	43	flask	flask	NOUN
eurjchem-845	38	44	and	and	CCONJ
eurjchem-845	38	45	then	then	ADV
eurjchem-845	38	46	the	the	DET
eurjchem-845	38	47	required	require	VERB
eurjchem-845	38	48	concentrations	concentration	NOUN
eurjchem-845	38	49	were	be	AUX
eurjchem-845	38	50	prepared	prepare	VERB
eurjchem-845	38	51	by	by	ADP
eurjchem-845	38	52	serial	serial	ADJ
eurjchem-845	38	53	dilution	dilution	NOUN
eurjchem-845	38	54	.	.	PUNCT
eurjchem-845	39	1	all	all	DET
eurjchem-845	39	2	the	the	DET
eurjchem-845	39	3	solvents	solvent	NOUN
eurjchem-845	39	4	used	use	VERB
eurjchem-845	39	5	were	be	AUX
eurjchem-845	39	6	of	of	ADP
eurjchem-845	39	7	analytical	analytical	ADJ
eurjchem-845	39	8	grade	grade	NOUN
eurjchem-845	39	9	.	.	PUNCT
eurjchem-845	40	1	2.3	2.3	NUM
eurjchem-845	40	2	.	.	PUNCT
eurjchem-845	40	3	general	general	ADJ
eurjchem-845	40	4	procedure	procedure	NOUN
eurjchem-845	40	5	and	and	CCONJ
eurjchem-845	40	6	calibration	calibration	NOUN
eurjchem-845	40	7	graph	graph	NOUN
eurjchem-845	40	8	aliquots	aliquot	NOUN
eurjchem-845	40	9	from	from	ADP
eurjchem-845	40	10	lng	lng	PROPN
eurjchem-845	40	11	stock	stock	PROPN
eurjchem-845	40	12	standard	standard	PROPN
eurjchem-845	40	13	solution	solution	NOUN
eurjchem-845	40	14	equivalent	equivalent	ADJ
eurjchem-845	40	15	to	to	ADP
eurjchem-845	40	16	100‐1100	100‐1100	NUM
eurjchem-845	40	17	μg	μg	PROPN
eurjchem-845	40	18	were	be	AUX
eurjchem-845	40	19	accurately	accurately	ADV
eurjchem-845	40	20	measured	measure	VERB
eurjchem-845	40	21	and	and	CCONJ
eurjchem-845	40	22	transferred	transfer	VERB
eurjchem-845	40	23	into	into	ADP
eurjchem-845	40	24	a	a	DET
eurjchem-845	40	25	set	set	NOUN
eurjchem-845	40	26	of	of	ADP
eurjchem-845	40	27	10	10	NUM
eurjchem-845	40	28	ml	ml	NOUN
eurjchem-845	40	29	volumetric	volumetric	ADJ
eurjchem-845	40	30	flasks	flask	NOUN
eurjchem-845	40	31	and	and	CCONJ
eurjchem-845	40	32	the	the	DET
eurjchem-845	40	33	volumes	volume	NOUN
eurjchem-845	40	34	were	be	AUX
eurjchem-845	40	35	completed	complete	VERB
eurjchem-845	40	36	with	with	ADP
eurjchem-845	40	37	acetonitrile	acetonitrile	ADJ
eurjchem-845	40	38	:	:	PUNCT
eurjchem-845	40	39	methanol	methanol	NOUN
eurjchem-845	40	40	,	,	PUNCT
eurjchem-845	40	41	(	(	PUNCT
eurjchem-845	40	42	90:10	90:10	NUM
eurjchem-845	40	43	,	,	PUNCT
eurjchem-845	40	44	v	v	NOUN
eurjchem-845	40	45	:	:	PUNCT
eurjchem-845	40	46	v	v	NOUN
eurjchem-845	40	47	)	)	PUNCT
eurjchem-845	40	48	.	.	PUNCT
eurjchem-845	41	1	the	the	DET
eurjchem-845	41	2	relative	relative	ADJ
eurjchem-845	41	3	fluorescence	fluorescence	NOUN
eurjchem-845	41	4	intensity	intensity	NOUN
eurjchem-845	41	5	was	be	AUX
eurjchem-845	41	6	measured	measure	VERB
eurjchem-845	41	7	at	at	ADP
eurjchem-845	41	8	the	the	DET
eurjchem-845	41	9	specified	specified	ADJ
eurjchem-845	41	10	excitation	excitation	NOUN
eurjchem-845	41	11	and	and	CCONJ
eurjchem-845	41	12	emission	emission	NOUN
eurjchem-845	41	13	wavelengths	wavelength	NOUN
eurjchem-845	41	14	(	(	PUNCT
eurjchem-845	41	15	λem	λem	ADJ
eurjchem-845	41	16	at	at	ADP
eurjchem-845	41	17	435	435	NUM
eurjchem-845	41	18	nm	nm	NOUN
eurjchem-845	41	19	with	with	ADP
eurjchem-845	41	20	λex	λex	PROPN
eurjchem-845	41	21	at	at	ADP
eurjchem-845	41	22	339	339	NUM
eurjchem-845	41	23	nm	nm	NOUN
eurjchem-845	41	24	(	(	PUNCT
eurjchem-845	41	25	figure	figure	NOUN
eurjchem-845	41	26	2	2	NUM
eurjchem-845	41	27	)	)	PUNCT
eurjchem-845	41	28	)	)	PUNCT
eurjchem-845	41	29	,	,	PUNCT
eurjchem-845	41	30	then	then	ADV
eurjchem-845	41	31	plotted	plot	VERB
eurjchem-845	41	32	against	against	ADP
eurjchem-845	41	33	its	its	PRON
eurjchem-845	41	34	corresponding	corresponding	ADJ
eurjchem-845	41	35	concentration	concentration	NOUN
eurjchem-845	41	36	and	and	CCONJ
eurjchem-845	41	37	the	the	DET
eurjchem-845	41	38	regression	regression	NOUN
eurjchem-845	41	39	parameters	parameter	NOUN
eurjchem-845	41	40	were	be	AUX
eurjchem-845	41	41	computed	compute	VERB
eurjchem-845	41	42	.	.	PUNCT
eurjchem-845	42	1	2.4	2.4	NUM
eurjchem-845	42	2	.	.	PUNCT
eurjchem-845	43	1	assay	assay	PROPN
eurjchem-845	43	2	of	of	ADP
eurjchem-845	43	3	lng	lng	PROPN
eurjchem-845	43	4	in	in	ADP
eurjchem-845	43	5	bulk	bulk	NOUN
eurjchem-845	43	6	the	the	DET
eurjchem-845	43	7	relative	relative	ADJ
eurjchem-845	43	8	fluorescence	fluorescence	NOUN
eurjchem-845	43	9	intensity	intensity	NOUN
eurjchem-845	43	10	of	of	ADP
eurjchem-845	43	11	lng	lng	PROPN
eurjchem-845	43	12	in	in	ADP
eurjchem-845	43	13	bulk	bulk	NOUN
eurjchem-845	43	14	was	be	AUX
eurjchem-845	43	15	measured	measure	VERB
eurjchem-845	43	16	at	at	ADP
eurjchem-845	43	17	the	the	DET
eurjchem-845	43	18	specified	specified	ADJ
eurjchem-845	43	19	excitation	excitation	NOUN
eurjchem-845	43	20	and	and	CCONJ
eurjchem-845	43	21	emission	emission	NOUN
eurjchem-845	43	22	wavelengths	wavelength	NOUN
eurjchem-845	43	23	(	(	PUNCT
eurjchem-845	43	24	λem	λem	ADJ
eurjchem-845	43	25	at	at	ADP
eurjchem-845	43	26	435	435	NUM
eurjchem-845	43	27	nm	nm	NOUN
eurjchem-845	43	28	with	with	ADP
eurjchem-845	43	29	λex	λex	PROPN
eurjchem-845	43	30	at	at	ADP
eurjchem-845	43	31	339	339	NUM
eurjchem-845	43	32	nm	nm	NOUN
eurjchem-845	43	33	)	)	PUNCT
eurjchem-845	43	34	with	with	ADP
eurjchem-845	43	35	the	the	DET
eurjchem-845	43	36	concentration	concentration	NOUN
eurjchem-845	43	37	range	range	NOUN
eurjchem-845	43	38	20‐100	20‐100	PROPN
eurjchem-845	43	39	μg	μg	NOUN
eurjchem-845	43	40	/	/	SYM
eurjchem-845	43	41	ml	ml	NOUN
eurjchem-845	43	42	.	.	PROPN
eurjchem-845	43	43	2.5	2.5	NUM
eurjchem-845	43	44	.	.	PUNCT
eurjchem-845	44	1	assay	assay	PROPN
eurjchem-845	44	2	of	of	ADP
eurjchem-845	44	3	tradjenta	tradjenta	ADJ
eurjchem-845	44	4	®	®	NOUN
eurjchem-845	44	5	tablets	tablet	NOUN
eurjchem-845	44	6	twenty	twenty	NUM
eurjchem-845	44	7	tablets	tablet	NOUN
eurjchem-845	44	8	were	be	AUX
eurjchem-845	44	9	weighed	weigh	VERB
eurjchem-845	44	10	and	and	CCONJ
eurjchem-845	44	11	the	the	DET
eurjchem-845	44	12	coats	coat	NOUN
eurjchem-845	44	13	were	be	AUX
eurjchem-845	44	14	removed	remove	VERB
eurjchem-845	44	15	by	by	ADP
eurjchem-845	44	16	carefully	carefully	ADV
eurjchem-845	44	17	rubbing	rub	VERB
eurjchem-845	44	18	with	with	ADP
eurjchem-845	44	19	a	a	DET
eurjchem-845	44	20	clean	clean	ADJ
eurjchem-845	44	21	tissue	tissue	NOUN
eurjchem-845	44	22	wetted	wet	VERB
eurjchem-845	44	23	with	with	ADP
eurjchem-845	44	24	methanol	methanol	NOUN
eurjchem-845	44	25	.	.	PUNCT
eurjchem-845	45	1	an	an	DET
eurjchem-845	45	2	accurately	accurately	ADV
eurjchem-845	45	3	weighed	weigh	VERB
eurjchem-845	45	4	amount	amount	NOUN
eurjchem-845	45	5	of	of	ADP
eurjchem-845	45	6	the	the	DET
eurjchem-845	45	7	finely	finely	ADV
eurjchem-845	45	8	powdered	powder	VERB
eurjchem-845	45	9	tablets	tablet	NOUN
eurjchem-845	45	10	equivalent	equivalent	ADJ
eurjchem-845	45	11	to	to	ADP
eurjchem-845	45	12	100	100	NUM
eurjchem-845	45	13	mg	mg	PROPN
eurjchem-845	45	14	of	of	ADP
eurjchem-845	45	15	lng	lng	PROPN
eurjchem-845	45	16	were	be	AUX
eurjchem-845	45	17	made	make	VERB
eurjchem-845	45	18	up	up	ADP
eurjchem-845	45	19	to	to	PART
eurjchem-845	45	20	100	100	NUM
eurjchem-845	45	21	ml	ml	NOUN
eurjchem-845	45	22	with	with	ADP
eurjchem-845	45	23	acetonitrile	acetonitrile	NOUN
eurjchem-845	45	24	:	:	PUNCT
eurjchem-845	45	25	methanol	methanol	NOUN
eurjchem-845	45	26	,	,	PUNCT
eurjchem-845	45	27	(	(	PUNCT
eurjchem-845	45	28	90:10	90:10	NUM
eurjchem-845	45	29	,	,	PUNCT
eurjchem-845	45	30	v	v	NOUN
eurjchem-845	45	31	:	:	PUNCT
eurjchem-845	45	32	v	v	NOUN
eurjchem-845	45	33	)	)	PUNCT
eurjchem-845	45	34	,	,	PUNCT
eurjchem-845	45	35	the	the	DET
eurjchem-845	45	36	solution	solution	NOUN
eurjchem-845	45	37	was	be	AUX
eurjchem-845	45	38	filtered	filter	VERB
eurjchem-845	45	39	followed	follow	VERB
eurjchem-845	45	40	by	by	ADP
eurjchem-845	45	41	serial	serial	ADJ
eurjchem-845	45	42	dilution	dilution	NOUN
eurjchem-845	45	43	to	to	ADP
eurjchem-845	45	44	the	the	DET
eurjchem-845	45	45	required	require	VERB
eurjchem-845	45	46	concentration	concentration	NOUN
eurjchem-845	45	47	.	.	PUNCT
eurjchem-845	46	1	the	the	DET
eurjchem-845	46	2	procedure	procedure	NOUN
eurjchem-845	46	3	was	be	AUX
eurjchem-845	46	4	continued	continue	VERB
eurjchem-845	46	5	as	as	SCONJ
eurjchem-845	46	6	mentioned	mention	VERB
eurjchem-845	46	7	under	under	ADP
eurjchem-845	46	8	general	general	ADJ
eurjchem-845	46	9	procedures	procedure	NOUN
eurjchem-845	46	10	and	and	CCONJ
eurjchem-845	46	11	calibration	calibration	NOUN
eurjchem-845	46	12	.	.	PUNCT
eurjchem-845	47	1	3	3	X
eurjchem-845	47	2	.	.	NOUN
eurjchem-845	47	3	results	result	NOUN
eurjchem-845	47	4	and	and	CCONJ
eurjchem-845	47	5	discussion	discussion	NOUN
eurjchem-845	47	6	literature	literature	NOUN
eurjchem-845	47	7	survey	survey	NOUN
eurjchem-845	47	8	reveals	reveal	VERB
eurjchem-845	47	9	that	that	SCONJ
eurjchem-845	47	10	only	only	ADV
eurjchem-845	47	11	one	one	NUM
eurjchem-845	47	12	method	method	NOUN
eurjchem-845	47	13	has	have	AUX
eurjchem-845	47	14	been	be	AUX
eurjchem-845	47	15	described	describe	VERB
eurjchem-845	47	16	for	for	ADP
eurjchem-845	47	17	the	the	DET
eurjchem-845	47	18	determination	determination	NOUN
eurjchem-845	47	19	of	of	ADP
eurjchem-845	47	20	lng	lng	PROPN
eurjchem-845	47	21	in	in	ADP
eurjchem-845	47	22	its	its	PRON
eurjchem-845	47	23	pharmaceutical	pharmaceutical	ADJ
eurjchem-845	47	24	preparation	preparation	NOUN
eurjchem-845	47	25	[	[	X
eurjchem-845	47	26	3	3	NUM
eurjchem-845	47	27	]	]	PUNCT
eurjchem-845	47	28	.	.	PUNCT
eurjchem-845	48	1	the	the	DET
eurjchem-845	48	2	development	development	NOUN
eurjchem-845	48	3	of	of	ADP
eurjchem-845	48	4	spectrofluorometric	spectrofluorometric	ADJ
eurjchem-845	48	5	method	method	NOUN
eurjchem-845	48	6	for	for	ADP
eurjchem-845	48	7	the	the	DET
eurjchem-845	48	8	determination	determination	NOUN
eurjchem-845	48	9	of	of	ADP
eurjchem-845	48	10	lng	lng	PROPN
eurjchem-845	48	11	was	be	AUX
eurjchem-845	48	12	of	of	ADP
eurjchem-845	48	13	interest	interest	NOUN
eurjchem-845	48	14	as	as	SCONJ
eurjchem-845	48	15	no	no	DET
eurjchem-845	48	16	such	such	ADJ
eurjchem-845	48	17	methods	method	NOUN
eurjchem-845	48	18	have	have	AUX
eurjchem-845	48	19	been	be	AUX
eurjchem-845	48	20	reported	report	VERB
eurjchem-845	48	21	.	.	PUNCT
eurjchem-845	49	1	3.1	3.1	NUM
eurjchem-845	49	2	.	.	PUNCT
eurjchem-845	49	3	quantification	quantification	NOUN
eurjchem-845	49	4	,	,	PUNCT
eurjchem-845	49	5	accuracy	accuracy	NOUN
eurjchem-845	49	6	and	and	CCONJ
eurjchem-845	49	7	precision	precision	NOUN
eurjchem-845	49	8	standard	standard	ADJ
eurjchem-845	49	9	calibration	calibration	NOUN
eurjchem-845	49	10	curves	curve	NOUN
eurjchem-845	49	11	were	be	AUX
eurjchem-845	49	12	prepared	prepare	VERB
eurjchem-845	49	13	by	by	ADP
eurjchem-845	49	14	separately	separately	ADV
eurjchem-845	49	15	preparing	prepare	VERB
eurjchem-845	49	16	series	series	NOUN
eurjchem-845	49	17	of	of	ADP
eurjchem-845	49	18	different	different	ADJ
eurjchem-845	49	19	concentrations	concentration	NOUN
eurjchem-845	49	20	and	and	CCONJ
eurjchem-845	49	21	applying	apply	VERB
eurjchem-845	49	22	the	the	DET
eurjchem-845	49	23	suggested	suggest	VERB
eurjchem-845	49	24	procedures	procedure	NOUN
eurjchem-845	49	25	.	.	PUNCT
eurjchem-845	50	1	the	the	DET
eurjchem-845	50	2	linearity	linearity	NOUN
eurjchem-845	50	3	of	of	ADP
eurjchem-845	50	4	the	the	DET
eurjchem-845	50	5	calibration	calibration	NOUN
eurjchem-845	50	6	curve	curve	NOUN
eurjchem-845	50	7	was	be	AUX
eurjchem-845	50	8	validated	validate	VERB
eurjchem-845	50	9	by	by	ADP
eurjchem-845	50	10	the	the	DET
eurjchem-845	50	11	high	high	ADJ
eurjchem-845	50	12	value	value	NOUN
eurjchem-845	50	13	of	of	ADP
eurjchem-845	50	14	correlation	correlation	NOUN
eurjchem-845	50	15	coefficient	coefficient	NOUN
eurjchem-845	50	16	.	.	PUNCT
eurjchem-845	51	1	the	the	DET
eurjchem-845	51	2	analytical	analytical	ADJ
eurjchem-845	51	3	data	datum	NOUN
eurjchem-845	51	4	of	of	ADP
eurjchem-845	51	5	the	the	DET
eurjchem-845	51	6	calibration	calibration	NOUN
eurjchem-845	51	7	curve	curve	NOUN
eurjchem-845	51	8	including	include	VERB
eurjchem-845	51	9	standard	standard	ADJ
eurjchem-845	51	10	deviations	deviation	NOUN
eurjchem-845	51	11	for	for	ADP
eurjchem-845	51	12	the	the	DET
eurjchem-845	51	13	slope	slope	NOUN
eurjchem-845	51	14	and	and	CCONJ
eurjchem-845	51	15	intercept	intercept	PROPN
eurjchem-845	51	16	(	(	PUNCT
eurjchem-845	51	17	sb	sb	PROPN
eurjchem-845	51	18	,	,	PUNCT
eurjchem-845	51	19	sa	sa	PROPN
eurjchem-845	51	20	)	)	PUNCT
eurjchem-845	51	21	are	be	AUX
eurjchem-845	51	22	summarized	summarize	VERB
eurjchem-845	51	23	in	in	ADP
eurjchem-845	51	24	table	table	NOUN
eurjchem-845	51	25	1	1	NUM
eurjchem-845	51	26	.	.	PUNCT
eurjchem-845	52	1	the	the	DET
eurjchem-845	52	2	regression	regression	NOUN
eurjchem-845	52	3	equation	equation	NOUN
eurjchem-845	52	4	of	of	ADP
eurjchem-845	52	5	the	the	DET
eurjchem-845	52	6	calibration	calibration	NOUN
eurjchem-845	52	7	graph	graph	NOUN
eurjchem-845	52	8	was	be	AUX
eurjchem-845	52	9	utilized	utilize	VERB
eurjchem-845	52	10	for	for	ADP
eurjchem-845	52	11	the	the	DET
eurjchem-845	52	12	determination	determination	NOUN
eurjchem-845	52	13	of	of	ADP
eurjchem-845	52	14	concentrations	concentration	NOUN
eurjchem-845	52	15	of	of	ADP
eurjchem-845	52	16	lng	lng	PROPN
eurjchem-845	52	17	in	in	ADP
eurjchem-845	52	18	bulk	bulk	NOUN
eurjchem-845	52	19	and	and	CCONJ
eurjchem-845	52	20	tablets	tablet	NOUN
eurjchem-845	52	21	.	.	PUNCT
eurjchem-845	53	1	the	the	DET
eurjchem-845	53	2	reproducibility	reproducibility	NOUN
eurjchem-845	53	3	and	and	CCONJ
eurjchem-845	53	4	accuracy	accuracy	NOUN
eurjchem-845	53	5	of	of	ADP
eurjchem-845	53	6	the	the	DET
eurjchem-845	53	7	suggested	suggest	VERB
eurjchem-845	53	8	method	method	NOUN
eurjchem-845	53	9	were	be	AUX
eurjchem-845	53	10	assessed	assess	VERB
eurjchem-845	53	11	using	use	VERB
eurjchem-845	53	12	different	different	ADJ
eurjchem-845	53	13	concentrations	concentration	NOUN
eurjchem-845	53	14	of	of	ADP
eurjchem-845	53	15	lng	lng	PROPN
eurjchem-845	53	16	in	in	ADP
eurjchem-845	53	17	bulk	bulk	NOUN
eurjchem-845	53	18	and	and	CCONJ
eurjchem-845	53	19	determination	determination	NOUN
eurjchem-845	53	20	of	of	ADP
eurjchem-845	53	21	the	the	DET
eurjchem-845	53	22	concentrations	concentration	NOUN
eurjchem-845	53	23	in	in	ADP
eurjchem-845	53	24	tablets	tablet	NOUN
eurjchem-845	53	25	.	.	PUNCT
eurjchem-845	54	1	the	the	DET
eurjchem-845	54	2	results	result	NOUN
eurjchem-845	54	3	obtained	obtain	VERB
eurjchem-845	54	4	were	be	AUX
eurjchem-845	54	5	of	of	ADP
eurjchem-845	54	6	good	good	ADJ
eurjchem-845	54	7	accuracy	accuracy	NOUN
eurjchem-845	54	8	and	and	CCONJ
eurjchem-845	54	9	precision	precision	NOUN
eurjchem-845	54	10	.	.	PUNCT
eurjchem-845	55	1	the	the	DET
eurjchem-845	55	2	applicability	applicability	NOUN
eurjchem-845	55	3	of	of	ADP
eurjchem-845	55	4	the	the	DET
eurjchem-845	55	5	procedure	procedure	NOUN
eurjchem-845	55	6	for	for	ADP
eurjchem-845	55	7	estimation	estimation	NOUN
eurjchem-845	55	8	of	of	ADP
eurjchem-845	55	9	tablets	tablet	NOUN
eurjchem-845	55	10	was	be	AUX
eurjchem-845	55	11	validated	validate	VERB
eurjchem-845	55	12	using	use	VERB
eurjchem-845	55	13	standard	standard	ADJ
eurjchem-845	55	14	addition	addition	NOUN
eurjchem-845	55	15	technique	technique	NOUN
eurjchem-845	55	16	as	as	ADP
eurjchem-845	55	17	a	a	DET
eurjchem-845	55	18	check	check	NOUN
eurjchem-845	55	19	for	for	ADP
eurjchem-845	55	20	accuracy	accuracy	NOUN
eurjchem-845	55	21	(	(	PUNCT
eurjchem-845	55	22	table	table	NOUN
eurjchem-845	55	23	1	1	NUM
eurjchem-845	55	24	)	)	PUNCT
eurjchem-845	55	25	.	.	PUNCT
eurjchem-845	56	1	figure	figure	NOUN
eurjchem-845	56	2	2	2	NUM
eurjchem-845	56	3	.	.	PUNCT
eurjchem-845	56	4	excitation	excitation	NOUN
eurjchem-845	56	5	and	and	CCONJ
eurjchem-845	56	6	emission	emission	NOUN
eurjchem-845	56	7	spectra	spectra	NOUN
eurjchem-845	56	8	of	of	ADP
eurjchem-845	56	9	linagliptin	linagliptin	PROPN
eurjchem-845	56	10	(	(	PUNCT
eurjchem-845	56	11	100	100	NUM
eurjchem-845	56	12	μg	μg	NOUN
eurjchem-845	56	13	/	/	SYM
eurjchem-845	56	14	ml	ml	NOUN
eurjchem-845	56	15	)	)	PUNCT
eurjchem-845	56	16	.	.	PUNCT
eurjchem-845	57	1	a	a	DET
eurjchem-845	57	2	statistical	statistical	ADJ
eurjchem-845	57	3	analysis	analysis	NOUN
eurjchem-845	57	4	of	of	ADP
eurjchem-845	57	5	the	the	DET
eurjchem-845	57	6	results	result	NOUN
eurjchem-845	57	7	obtained	obtain	VERB
eurjchem-845	57	8	by	by	ADP
eurjchem-845	57	9	the	the	DET
eurjchem-845	57	10	proposed	propose	VERB
eurjchem-845	57	11	method	method	NOUN
eurjchem-845	57	12	for	for	ADP
eurjchem-845	57	13	the	the	DET
eurjchem-845	57	14	determination	determination	NOUN
eurjchem-845	57	15	of	of	ADP
eurjchem-845	57	16	lng	lng	PROPN
eurjchem-845	57	17	was	be	AUX
eurjchem-845	57	18	carried	carry	VERB
eurjchem-845	57	19	out	out	ADP
eurjchem-845	57	20	by	by	ADP
eurjchem-845	57	21	“	"	PUNCT
eurjchem-845	57	22	spss	spss	ADJ
eurjchem-845	57	23	statistical	statistical	ADJ
eurjchem-845	57	24	package	package	NOUN
eurjchem-845	57	25	version	version	NOUN
eurjchem-845	57	26	11	11	NUM
eurjchem-845	57	27	”	"	PUNCT
eurjchem-845	57	28	.	.	PUNCT
eurjchem-845	58	1	the	the	DET
eurjchem-845	58	2	significant	significant	ADJ
eurjchem-845	58	3	difference	difference	NOUN
eurjchem-845	58	4	between	between	ADP
eurjchem-845	58	5	groups	group	NOUN
eurjchem-845	58	6	was	be	AUX
eurjchem-845	58	7	tested	test	VERB
eurjchem-845	58	8	by	by	ADP
eurjchem-845	58	9	one	one	NUM
eurjchem-845	58	10	way	way	NOUN
eurjchem-845	58	11	anova	anova	X
eurjchem-845	58	12	(	(	PUNCT
eurjchem-845	58	13	f‐	f‐	NOUN
eurjchem-845	58	14	test	test	NOUN
eurjchem-845	58	15	)	)	PUNCT
eurjchem-845	58	16	at	at	ADP
eurjchem-845	58	17	p	p	NOUN
eurjchem-845	58	18	=	=	NOUN
eurjchem-845	58	19	0.05	0.05	NUM
eurjchem-845	58	20	as	as	SCONJ
eurjchem-845	58	21	shown	show	VERB
eurjchem-845	58	22	in	in	ADP
eurjchem-845	58	23	table	table	NOUN
eurjchem-845	58	24	2	2	NUM
eurjchem-845	58	25	.	.	PUNCT
eurjchem-845	59	1	the	the	DET
eurjchem-845	59	2	test	test	NOUN
eurjchem-845	59	3	ascertained	ascertain	VERB
eurjchem-845	59	4	that	that	SCONJ
eurjchem-845	59	5	there	there	PRON
eurjchem-845	59	6	was	be	VERB
eurjchem-845	59	7	no	no	DET
eurjchem-845	59	8	significant	significant	ADJ
eurjchem-845	59	9	difference	difference	NOUN
eurjchem-845	59	10	among	among	ADP
eurjchem-845	59	11	the	the	DET
eurjchem-845	59	12	methods	method	NOUN
eurjchem-845	59	13	.	.	PUNCT
eurjchem-845	60	1	382	382	NUM
eurjchem-845	60	2	el‐bagary	el‐bagary	ADJ
eurjchem-845	60	3	et	et	PROPN
eurjchem-845	60	4	al	al	PROPN
eurjchem-845	60	5	.	.	PUNCT
eurjchem-845	60	6	/	/	SYM
eurjchem-845	60	7	european	european	PROPN
eurjchem-845	60	8	journal	journal	PROPN
eurjchem-845	60	9	of	of	ADP
eurjchem-845	60	10	chemistry	chemistry	NOUN
eurjchem-845	60	11	5	5	NUM
eurjchem-845	60	12	(	(	PUNCT
eurjchem-845	60	13	2	2	NUM
eurjchem-845	60	14	)	)	PUNCT
eurjchem-845	60	15	(	(	PUNCT
eurjchem-845	60	16	2014	2014	NUM
eurjchem-845	60	17	)	)	PUNCT
eurjchem-845	60	18	380‐382	380‐382	NOUN
eurjchem-845	60	19	4	4	NUM
eurjchem-845	60	20	.	.	X
eurjchem-845	60	21	conclusion	conclusion	NOUN
eurjchem-845	60	22	the	the	DET
eurjchem-845	60	23	proposed	propose	VERB
eurjchem-845	60	24	method	method	NOUN
eurjchem-845	60	25	has	have	VERB
eurjchem-845	60	26	the	the	DET
eurjchem-845	60	27	advantages	advantage	NOUN
eurjchem-845	60	28	of	of	ADP
eurjchem-845	60	29	simplicity	simplicity	NOUN
eurjchem-845	60	30	,	,	PUNCT
eurjchem-845	60	31	precision	precision	NOUN
eurjchem-845	60	32	,	,	PUNCT
eurjchem-845	60	33	accuracy	accuracy	NOUN
eurjchem-845	60	34	and	and	CCONJ
eurjchem-845	60	35	convenience	convenience	NOUN
eurjchem-845	60	36	for	for	ADP
eurjchem-845	60	37	the	the	DET
eurjchem-845	60	38	quantitation	quantitation	NOUN
eurjchem-845	60	39	of	of	ADP
eurjchem-845	60	40	lng	lng	PROPN
eurjchem-845	60	41	.	.	PUNCT
eurjchem-845	61	1	the	the	DET
eurjchem-845	61	2	proposed	propose	VERB
eurjchem-845	61	3	method	method	NOUN
eurjchem-845	61	4	can	can	AUX
eurjchem-845	61	5	be	be	AUX
eurjchem-845	61	6	used	use	VERB
eurjchem-845	61	7	for	for	ADP
eurjchem-845	61	8	the	the	DET
eurjchem-845	61	9	quality	quality	NOUN
eurjchem-845	61	10	control	control	NOUN
eurjchem-845	61	11	of	of	ADP
eurjchem-845	61	12	lng	lng	PROPN
eurjchem-845	61	13	and	and	CCONJ
eurjchem-845	61	14	can	can	AUX
eurjchem-845	61	15	be	be	AUX
eurjchem-845	61	16	extended	extend	VERB
eurjchem-845	61	17	for	for	ADP
eurjchem-845	61	18	routine	routine	ADJ
eurjchem-845	61	19	analysis	analysis	NOUN
eurjchem-845	61	20	of	of	ADP
eurjchem-845	61	21	lng	lng	PROPN
eurjchem-845	61	22	in	in	ADP
eurjchem-845	61	23	its	its	PRON
eurjchem-845	61	24	pharmaceutical	pharmaceutical	ADJ
eurjchem-845	61	25	preparation	preparation	NOUN
eurjchem-845	61	26	.	.	PUNCT
eurjchem-845	62	1	references	reference	NOUN
eurjchem-845	62	2	[	[	X
eurjchem-845	62	3	1	1	NUM
eurjchem-845	62	4	]	]	X
eurjchem-845	62	5	kirby	kirby	PROPN
eurjchem-845	62	6	,	,	PUNCT
eurjchem-845	62	7	m.	m.	NOUN
eurjchem-845	62	8	;	;	PUNCT
eurjchem-845	62	9	yu	yu	PROPN
eurjchem-845	62	10	,	,	PUNCT
eurjchem-845	62	11	d.	d.	PROPN
eurjchem-845	62	12	;	;	PUNCT
eurjchem-845	62	13	conor	conor	PROPN
eurjchem-845	62	14	,	,	PUNCT
eurjchem-845	62	15	s.	s.	PROPN
eurjchem-845	62	16	clin	clin	PROPN
eurjchem-845	62	17	.	.	PUNCT
eurjchem-845	63	1	sci	sci	PROPN
eurjchem-845	63	2	.	.	PROPN
eurjchem-845	63	3	2010	2010	NUM
eurjchem-845	63	4	,	,	PUNCT
eurjchem-845	63	5	118	118	NUM
eurjchem-845	63	6	,	,	PUNCT
eurjchem-845	63	7	31‐41	31‐41	NUM
eurjchem-845	63	8	.	.	PUNCT
eurjchem-845	64	1	[	[	X
eurjchem-845	64	2	2	2	NUM
eurjchem-845	64	3	]	]	X
eurjchem-845	64	4	sekaran	sekaran	NOUN
eurjchem-845	64	5	,	,	PUNCT
eurjchem-845	64	6	b.	b.	PROPN
eurjchem-845	64	7	;	;	PUNCT
eurjchem-845	64	8	rani	rani	PROPN
eurjchem-845	64	9	,	,	PUNCT
eurjchem-845	64	10	p.	p.	NOUN
eurjchem-845	64	11	int	int	NOUN
eurjchem-845	64	12	.	.	PUNCT
eurjchem-845	65	1	j.	j.	PROPN
eurjchem-845	65	2	pharm	pharm	PROPN
eurjchem-845	65	3	.	.	PUNCT
eurjchem-845	66	1	pharm	pharm	PROPN
eurjchem-845	66	2	.	.	PUNCT
eurjchem-845	67	1	sci	sci	PROPN
eurjchem-845	67	2	.	.	PROPN
eurjchem-845	67	3	2010	2010	NUM
eurjchem-845	67	4	,	,	PUNCT
eurjchem-845	67	5	2	2	NUM
eurjchem-845	67	6	,	,	PUNCT
eurjchem-845	67	7	138‐142	138‐142	NUM
eurjchem-845	67	8	.	.	PUNCT
eurjchem-845	68	1	[	[	X
eurjchem-845	68	2	3	3	NUM
eurjchem-845	68	3	]	]	PUNCT
eurjchem-845	68	4	lakshmi	lakshmi	NOUN
eurjchem-845	68	5	,	,	PUNCT
eurjchem-845	68	6	b.	b.	PROPN
eurjchem-845	68	7	;	;	PUNCT
eurjchem-845	68	8	reddy	reddy	PROPN
eurjchem-845	68	9	,	,	PUNCT
eurjchem-845	68	10	t.	t.	PROPN
eurjchem-845	68	11	j.	j.	PROPN
eurjchem-845	68	12	atom	atom	PROPN
eurjchem-845	68	13	.	.	PUNCT
eurjchem-845	68	14	mol	mol	PROPN
eurjchem-845	68	15	.	.	PROPN
eurjchem-845	68	16	2012	2012	NUM
eurjchem-845	68	17	,	,	PUNCT
eurjchem-845	68	18	2	2	NUM
eurjchem-845	68	19	,	,	PUNCT
eurjchem-845	68	20	155‐164	155‐164	NOUN
eurjchem-845	68	21	.	.	PUNCT
eurjchem-845	69	1	[	[	X
eurjchem-845	69	2	4	4	NUM
eurjchem-845	69	3	]	]	SYM
eurjchem-845	69	4	el‐ashry	el‐ashry	NOUN
eurjchem-845	69	5	,	,	PUNCT
eurjchem-845	69	6	s.	s.	PROPN
eurjchem-845	69	7	;	;	PUNCT
eurjchem-845	69	8	el‐sherbeny	el‐sherbeny	PROPN
eurjchem-845	69	9	,	,	PUNCT
eurjchem-845	69	10	m.	m.	NOUN
eurjchem-845	69	11	;	;	PUNCT
eurjchem-845	69	12	el‐sherbeny	el‐sherbeny	PROPN
eurjchem-845	69	13	,	,	PUNCT
eurjchem-845	69	14	d.	d.	PROPN
eurjchem-845	69	15	j.	j.	PROPN
eurjchem-845	69	16	pharm	pharm	PROPN
eurjchem-845	69	17	.	.	PUNCT
eurjchem-845	69	18	biomed	biome	VERB
eurjchem-845	69	19	.	.	PUNCT
eurjchem-845	70	1	anal	anal	ADJ
eurjchem-845	70	2	.	.	PUNCT
eurjchem-845	71	1	2000	2000	NUM
eurjchem-845	71	2	,	,	PUNCT
eurjchem-845	71	3	22	22	NUM
eurjchem-845	71	4	,	,	PUNCT
eurjchem-845	71	5	729‐737	729‐737	NUM
eurjchem-845	71	6	.	.	PUNCT
eurjchem-845	72	1	[	[	X
eurjchem-845	72	2	5	5	NUM
eurjchem-845	72	3	]	]	X
eurjchem-845	72	4	rizk	rizk	PROPN
eurjchem-845	72	5	,	,	PUNCT
eurjchem-845	72	6	m.	m.	NOUN
eurjchem-845	72	7	;	;	PUNCT
eurjchem-845	72	8	belal	belal	PROPN
eurjchem-845	72	9	,	,	PUNCT
eurjchem-845	72	10	f.	f.	PROPN
eurjchem-845	72	11	;	;	PUNCT
eurjchem-845	72	12	ibrahim	ibrahim	PROPN
eurjchem-845	72	13	,	,	PUNCT
eurjchem-845	72	14	f.	f.	PROPN
eurjchem-845	72	15	pharm	pharm	PROPN
eurjchem-845	72	16	.	.	PUNCT
eurjchem-845	73	1	acta	acta	PROPN
eurjchem-845	73	2	helv	helv	PROPN
eurjchem-845	73	3	.	.	PROPN
eurjchem-845	74	1	2000	2000	NUM
eurjchem-845	74	2	,	,	PUNCT
eurjchem-845	74	3	74	74	NUM
eurjchem-845	74	4	,	,	PUNCT
eurjchem-845	74	5	371‐377	371‐377	NUM
eurjchem-845	74	6	.	.	PUNCT
eurjchem-845	75	1	[	[	X
eurjchem-845	75	2	6	6	NUM
eurjchem-845	75	3	]	]	X
eurjchem-845	75	4	belal	belal	NOUN
eurjchem-845	75	5	,	,	PUNCT
eurjchem-845	75	6	f.	f.	PROPN
eurjchem-845	75	7	;	;	PUNCT
eurjchem-845	75	8	ibrahim	ibrahim	PROPN
eurjchem-845	75	9	,	,	PUNCT
eurjchem-845	75	10	f.	f.	PROPN
eurjchem-845	75	11	;	;	PUNCT
eurjchem-845	75	12	hassan	hassan	PROPN
eurjchem-845	75	13	,	,	PUNCT
eurjchem-845	75	14	s.	s.	PROPN
eurjchem-845	75	15	anal	anal	PROPN
eurjchem-845	75	16	.	.	PUNCT
eurjchem-845	76	1	chim	chim	PROPN
eurjchem-845	76	2	.	.	PUNCT
eurjchem-845	77	1	acta	acta	PROPN
eurjchem-845	77	2	1991	1991	NUM
eurjchem-845	77	3	,	,	PUNCT
eurjchem-845	77	4	255	255	NUM
eurjchem-845	77	5	,	,	PUNCT
eurjchem-845	77	6	103‐106	103‐106	NUM
eurjchem-845	77	7	.	.	PUNCT
eurjchem-845	78	1	[	[	X
eurjchem-845	78	2	7	7	NUM
eurjchem-845	78	3	]	]	X
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eurjchem-845	78	5	,	,	PUNCT
eurjchem-845	78	6	l.	l.	PROPN
eurjchem-845	78	7	;	;	PUNCT
eurjchem-845	78	8	abbas	abbas	PROPN
eurjchem-845	78	9	,	,	PUNCT
eurjchem-845	78	10	s.	s.	PROPN
eurjchem-845	78	11	;	;	PUNCT
eurjchem-845	78	12	fattah	fattah	PROPN
eurjchem-845	78	13	,	,	PUNCT
eurjchem-845	78	14	l.	l.	PROPN
eurjchem-845	78	15	;	;	PUNCT
eurjchem-845	78	16	refaat	refaat	PROPN
eurjchem-845	78	17	,	,	PUNCT
eurjchem-845	78	18	h.	h.	PROPN
eurjchem-845	78	19	il	il	PROPN
eurjchem-845	78	20	farmaco	farmaco	PROPN
eurjchem-845	78	21	2005	2005	NUM
eurjchem-845	78	22	,	,	PUNCT
eurjchem-845	78	23	60	60	NUM
eurjchem-845	78	24	,	,	PUNCT
eurjchem-845	78	25	859‐	859‐	NUM
eurjchem-845	78	26	867	867	NUM
eurjchem-845	78	27	.	.	PUNCT