id	sid	tid	token	lemma	pos
eurjchem-864	1	1	untitled	untitle	VERB
eurjchem-864	1	2	european	european	PROPN
eurjchem-864	1	3	journal	journal	PROPN
eurjchem-864	1	4	of	of	ADP
eurjchem-864	1	5	chemistry	chemistry	NOUN
eurjchem-864	1	6	4	4	NUM
eurjchem-864	1	7	(	(	PUNCT
eurjchem-864	1	8	4	4	NUM
eurjchem-864	1	9	)	)	PUNCT
eurjchem-864	1	10	(	(	PUNCT
eurjchem-864	1	11	2013	2013	NUM
eurjchem-864	1	12	)	)	PUNCT
eurjchem-864	1	13	402‐407	402‐407	PROPN
eurjchem-864	1	14	european	european	PROPN
eurjchem-864	1	15	journal	journal	PROPN
eurjchem-864	1	16	of	of	ADP
eurjchem-864	1	17	chemistry	chemistry	NOUN
eurjchem-864	1	18	issn	issn	PROPN
eurjchem-864	1	19	2153‐2249	2153‐2249	PROPN
eurjchem-864	1	20	(	(	PUNCT
eurjchem-864	1	21	print	print	NOUN
eurjchem-864	1	22	)	)	PUNCT
eurjchem-864	1	23	/	/	SYM
eurjchem-864	1	24	issn	issn	PROPN
eurjchem-864	1	25	2153‐2257	2153‐2257	NUM
eurjchem-864	1	26	(	(	PUNCT
eurjchem-864	1	27	online	online	ADJ
eurjchem-864	1	28	)	)	PUNCT
eurjchem-864	1	29			NOUN
eurjchem-864	1	30	2013	2013	NUM
eurjchem-864	1	31	eurjchem	eurjchem	PROPN
eurjchem-864	1	32	doi:10.5155	doi:10.5155	PROPN
eurjchem-864	1	33	/	/	SYM
eurjchem-864	1	34	eurjchem.4.4.402‐407.864	eurjchem.4.4.402‐407.864	ADJ
eurjchem-864	1	35	european	european	ADJ
eurjchem-864	1	36	journal	journal	PROPN
eurjchem-864	1	37	of	of	ADP
eurjchem-864	1	38	chemistry	chemistry	PROPN
eurjchem-864	1	39	journal	journal	PROPN
eurjchem-864	1	40	homepage	homepage	NOUN
eurjchem-864	1	41	:	:	PUNCT
eurjchem-864	1	42	www.eurjchem.com	www.eurjchem.com	X
eurjchem-864	1	43	new	new	ADJ
eurjchem-864	1	44	synthetic	synthetic	ADJ
eurjchem-864	1	45	benzisoxazole	benzisoxazole	NOUN
eurjchem-864	1	46	derivatives	derivative	NOUN
eurjchem-864	1	47	as	as	ADP
eurjchem-864	1	48	antimicrobial	antimicrobial	ADJ
eurjchem-864	1	49	,	,	PUNCT
eurjchem-864	1	50	antioxidant	antioxidant	ADJ
eurjchem-864	1	51	and	and	CCONJ
eurjchem-864	1	52	anti‐inflammatory	anti‐inflammatory	NOUN
eurjchem-864	1	53	agents	agent	NOUN
eurjchem-864	1	54	chalya	chalya	PROPN
eurjchem-864	1	55	mallappaji	mallappaji	PROPN
eurjchem-864	1	56	shivaprasad	shivaprasad	PROPN
eurjchem-864	1	57	,	,	PUNCT
eurjchem-864	1	58	swamy	swamy	PROPN
eurjchem-864	1	59	jagadish	jagadish	PROPN
eurjchem-864	1	60	,	,	PUNCT
eurjchem-864	1	61	toreshettahally	toreshettahally	PROPN
eurjchem-864	1	62	ramesh	ramesh	PROPN
eurjchem-864	1	63	swaroop	swaroop	PROPN
eurjchem-864	1	64	,	,	PUNCT
eurjchem-864	1	65	chakrabhavi	chakrabhavi	PROPN
eurjchem-864	1	66	dhananjaya	dhananjaya	PROPN
eurjchem-864	1	67	mohan	mohan	PROPN
eurjchem-864	1	68	,	,	PUNCT
eurjchem-864	1	69	rangaswamy	rangaswamy	NOUN
eurjchem-864	1	70	roopashree	roopashree	NOUN
eurjchem-864	1	71	,	,	PUNCT
eurjchem-864	1	72	kothanahally	kothanahally	ADV
eurjchem-864	1	73	shivaramu	shivaramu	VERB
eurjchem-864	1	74	sharath	sharath	PROPN
eurjchem-864	1	75	kumar	kumar	PROPN
eurjchem-864	1	76	and	and	CCONJ
eurjchem-864	1	77	kanchugarakoppal	kanchugarakoppal	PROPN
eurjchem-864	1	78	subbegowda	subbegowda	PROPN
eurjchem-864	1	79	rangappa	rangappa	PROPN
eurjchem-864	1	80	*	*	PROPN
eurjchem-864	1	81	department	department	PROPN
eurjchem-864	1	82	of	of	ADP
eurjchem-864	1	83	studies	study	NOUN
eurjchem-864	1	84	in	in	ADP
eurjchem-864	1	85	chemistry	chemistry	NOUN
eurjchem-864	1	86	,	,	PUNCT
eurjchem-864	1	87	university	university	NOUN
eurjchem-864	1	88	of	of	ADP
eurjchem-864	1	89	mysore	mysore	PROPN
eurjchem-864	1	90	,	,	PUNCT
eurjchem-864	1	91	manasagangotri	manasagangotri	NOUN
eurjchem-864	1	92	,	,	PUNCT
eurjchem-864	1	93	mysore	mysore	VERB
eurjchem-864	1	94	570	570	NUM
eurjchem-864	1	95	006	006	NUM
eurjchem-864	1	96	,	,	PUNCT
eurjchem-864	1	97	india	india	PROPN
eurjchem-864	1	98	*	*	PUNCT
eurjchem-864	1	99	corresponding	correspond	VERB
eurjchem-864	1	100	author	author	NOUN
eurjchem-864	1	101	at	at	ADP
eurjchem-864	1	102	:	:	PUNCT
eurjchem-864	1	103	department	department	NOUN
eurjchem-864	1	104	of	of	ADP
eurjchem-864	1	105	studies	study	NOUN
eurjchem-864	1	106	in	in	ADP
eurjchem-864	1	107	chemistry	chemistry	NOUN
eurjchem-864	1	108	,	,	PUNCT
eurjchem-864	1	109	university	university	NOUN
eurjchem-864	1	110	of	of	ADP
eurjchem-864	1	111	mysore	mysore	PROPN
eurjchem-864	1	112	,	,	PUNCT
eurjchem-864	1	113	manasagangotri	manasagangotri	NOUN
eurjchem-864	1	114	,	,	PUNCT
eurjchem-864	1	115	mysore	mysore	VERB
eurjchem-864	1	116	570	570	NUM
eurjchem-864	1	117	006	006	NUM
eurjchem-864	1	118	,	,	PUNCT
eurjchem-864	1	119	india	india	PROPN
eurjchem-864	1	120	.	.	PUNCT
eurjchem-864	2	1	tel	tel	PROPN
eurjchem-864	2	2	.	.	PROPN
eurjchem-864	2	3	:	:	PUNCT
eurjchem-864	3	1	+91.0821.2419661	+91.0821.2419661	ADJ
eurjchem-864	3	2	;	;	PUNCT
eurjchem-864	3	3	fax	fax	NOUN
eurjchem-864	3	4	:	:	PUNCT
eurjchem-864	3	5	+91.0821.2500846	+91.0821.2500846	PROPN
eurjchem-864	3	6	.	.	PUNCT
eurjchem-864	3	7	e‐mail	e‐mail	PUNCT
eurjchem-864	3	8	address	address	NOUN
eurjchem-864	3	9	:	:	PUNCT
eurjchem-864	3	10	rangappaks@gmail.com	rangappaks@gmail.com	X
eurjchem-864	3	11	(	(	PUNCT
eurjchem-864	3	12	k.s	k.s	PROPN
eurjchem-864	3	13	.	.	PROPN
eurjchem-864	3	14	rangappa	rangappa	PROPN
eurjchem-864	3	15	)	)	PUNCT
eurjchem-864	3	16	.	.	PUNCT
eurjchem-864	4	1	article	article	NOUN
eurjchem-864	4	2	information	information	PROPN
eurjchem-864	4	3	abstract	abstract	ADV
eurjchem-864	4	4	received	receive	VERB
eurjchem-864	4	5	:	:	PUNCT
eurjchem-864	4	6	28	28	NUM
eurjchem-864	4	7	june	june	PROPN
eurjchem-864	4	8	2013	2013	NUM
eurjchem-864	4	9	received	receive	VERB
eurjchem-864	4	10	in	in	ADP
eurjchem-864	4	11	revised	revise	VERB
eurjchem-864	4	12	form	form	NOUN
eurjchem-864	4	13	:	:	PUNCT
eurjchem-864	4	14	19	19	NUM
eurjchem-864	4	15	july	july	PROPN
eurjchem-864	4	16	2013	2013	NUM
eurjchem-864	4	17	accepted	accept	VERB
eurjchem-864	4	18	:	:	PUNCT
eurjchem-864	4	19	22	22	NUM
eurjchem-864	4	20	july	july	PROPN
eurjchem-864	4	21	2013	2013	NUM
eurjchem-864	4	22	online	online	NOUN
eurjchem-864	4	23	:	:	PUNCT
eurjchem-864	4	24	31	31	NUM
eurjchem-864	4	25	december	december	PROPN
eurjchem-864	4	26	2013	2013	NUM
eurjchem-864	4	27	keywords	keyword	VERB
eurjchem-864	4	28	a	a	DET
eurjchem-864	4	29	series	series	NOUN
eurjchem-864	4	30	of	of	ADP
eurjchem-864	4	31	piperidine	piperidine	NOUN
eurjchem-864	4	32	conjugated	conjugate	VERB
eurjchem-864	4	33	benzisoxazole	benzisoxazole	NOUN
eurjchem-864	4	34	derivatives	derivative	NOUN
eurjchem-864	4	35	were	be	AUX
eurjchem-864	4	36	synthesized	synthesize	VERB
eurjchem-864	4	37	and	and	CCONJ
eurjchem-864	4	38	evaluated	evaluate	VERB
eurjchem-864	4	39	for	for	ADP
eurjchem-864	4	40	their	their	PRON
eurjchem-864	4	41	antibacterial	antibacterial	ADJ
eurjchem-864	4	42	,	,	PUNCT
eurjchem-864	4	43	anti‐oxidant	anti‐oxidant	NOUN
eurjchem-864	4	44	and	and	CCONJ
eurjchem-864	4	45	anti‐inflammatory	anti‐inflammatory	NOUN
eurjchem-864	4	46	activities	activity	NOUN
eurjchem-864	4	47	.	.	PUNCT
eurjchem-864	5	1	the	the	DET
eurjchem-864	5	2	results	result	NOUN
eurjchem-864	5	3	showed	show	VERB
eurjchem-864	5	4	that	that	SCONJ
eurjchem-864	5	5	most	most	ADJ
eurjchem-864	5	6	of	of	ADP
eurjchem-864	5	7	the	the	DET
eurjchem-864	5	8	tested	test	VERB
eurjchem-864	5	9	compounds	compound	NOUN
eurjchem-864	5	10	exhibit	exhibit	VERB
eurjchem-864	5	11	good	good	ADJ
eurjchem-864	5	12	to	to	ADP
eurjchem-864	5	13	moderate	moderate	ADJ
eurjchem-864	5	14	antimicrobial	antimicrobial	ADJ
eurjchem-864	5	15	activity	activity	NOUN
eurjchem-864	5	16	against	against	ADP
eurjchem-864	5	17	some	some	DET
eurjchem-864	5	18	strains	strain	NOUN
eurjchem-864	5	19	of	of	ADP
eurjchem-864	5	20	gram	gram	NOUN
eurjchem-864	5	21	negative	negative	ADJ
eurjchem-864	5	22	bacteria	bacteria	NOUN
eurjchem-864	5	23	(	(	PUNCT
eurjchem-864	5	24	escherichia	escherichia	NOUN
eurjchem-864	5	25	coli	coli	NOUN
eurjchem-864	5	26	,	,	PUNCT
eurjchem-864	5	27	klebsiella	klebsiella	NOUN
eurjchem-864	5	28	pneumoniae	pneumoniae	NOUN
eurjchem-864	5	29	,	,	PUNCT
eurjchem-864	5	30	salmonella	salmonella	NOUN
eurjchem-864	5	31	typhi	typhi	ADV
eurjchem-864	5	32	,	,	PUNCT
eurjchem-864	5	33	shigella	shigella	PROPN
eurjchem-864	5	34	flexineri	flexineri	PROPN
eurjchem-864	5	35	)	)	PUNCT
eurjchem-864	5	36	and	and	CCONJ
eurjchem-864	5	37	gram	gram	NOUN
eurjchem-864	5	38	positive	positive	ADJ
eurjchem-864	5	39	bacteria	bacteria	NOUN
eurjchem-864	5	40	(	(	PUNCT
eurjchem-864	5	41	bacillus	bacillus	NOUN
eurjchem-864	5	42	subtilis	subtili	NOUN
eurjchem-864	5	43	)	)	PUNCT
eurjchem-864	5	44	.	.	PUNCT
eurjchem-864	6	1	further	far	ADV
eurjchem-864	6	2	,	,	PUNCT
eurjchem-864	6	3	the	the	DET
eurjchem-864	6	4	molecules	molecule	NOUN
eurjchem-864	6	5	were	be	AUX
eurjchem-864	6	6	evaluated	evaluate	VERB
eurjchem-864	6	7	for	for	ADP
eurjchem-864	6	8	anti‐oxidant	anti‐oxidant	ADJ
eurjchem-864	6	9	assays	assay	NOUN
eurjchem-864	6	10	such	such	ADJ
eurjchem-864	6	11	as	as	ADP
eurjchem-864	6	12	dpph	dpph	NOUN
eurjchem-864	6	13	scavenging	scavenging	NOUN
eurjchem-864	6	14	,	,	PUNCT
eurjchem-864	6	15	super	super	ADJ
eurjchem-864	6	16	oxide	oxide	NOUN
eurjchem-864	6	17	radical	radical	ADJ
eurjchem-864	6	18	scavenging	scavenging	NOUN
eurjchem-864	6	19	and	and	CCONJ
eurjchem-864	6	20	hydroxyl	hydroxyl	NOUN
eurjchem-864	6	21	radical	radical	ADJ
eurjchem-864	6	22	scavenging	scavenging	ADJ
eurjchem-864	6	23	assays	assay	NOUN
eurjchem-864	6	24	.	.	PUNCT
eurjchem-864	7	1	most	most	ADJ
eurjchem-864	7	2	of	of	ADP
eurjchem-864	7	3	the	the	DET
eurjchem-864	7	4	compounds	compound	NOUN
eurjchem-864	7	5	showed	show	VERB
eurjchem-864	7	6	potent	potent	ADJ
eurjchem-864	7	7	antioxidant	antioxidant	ADJ
eurjchem-864	7	8	activities	activity	NOUN
eurjchem-864	7	9	.	.	PUNCT
eurjchem-864	8	1	also	also	ADV
eurjchem-864	8	2	,	,	PUNCT
eurjchem-864	8	3	the	the	DET
eurjchem-864	8	4	synthesized	synthesize	VERB
eurjchem-864	8	5	compounds	compound	NOUN
eurjchem-864	8	6	were	be	AUX
eurjchem-864	8	7	screened	screen	VERB
eurjchem-864	8	8	for	for	ADP
eurjchem-864	8	9	anti‐inflammatory	anti‐inflammatory	NOUN
eurjchem-864	8	10	activities	activity	NOUN
eurjchem-864	8	11	such	such	ADJ
eurjchem-864	8	12	as	as	ADP
eurjchem-864	8	13	lipoxygenase	lipoxygenase	NOUN
eurjchem-864	8	14	inhibition	inhibition	NOUN
eurjchem-864	8	15	and	and	CCONJ
eurjchem-864	8	16	indirect	indirect	ADJ
eurjchem-864	8	17	haemolytic	haemolytic	ADJ
eurjchem-864	8	18	assays	assay	NOUN
eurjchem-864	8	19	,	,	PUNCT
eurjchem-864	8	20	where	where	SCONJ
eurjchem-864	8	21	compounds	compound	NOUN
eurjchem-864	8	22	revealed	reveal	VERB
eurjchem-864	8	23	good	good	ADJ
eurjchem-864	8	24	activity	activity	NOUN
eurjchem-864	8	25	.	.	PUNCT
eurjchem-864	9	1	piperidine	piperidine	NOUN
eurjchem-864	9	2	antioxidant	antioxidant	NOUN
eurjchem-864	9	3	spirolactone	spirolactone	NOUN
eurjchem-864	9	4	antimicrobial	antimicrobial	ADJ
eurjchem-864	9	5	benzisoxazole	benzisoxazole	NOUN
eurjchem-864	9	6	anti‐inflammatory	anti‐inflammatory	NOUN
eurjchem-864	9	7	1	1	NUM
eurjchem-864	9	8	.	.	PUNCT
eurjchem-864	10	1	introduction	introduction	NOUN
eurjchem-864	10	2	benzisoxazole	benzisoxazole	PROPN
eurjchem-864	10	3	scaffold	scaffold	NOUN
eurjchem-864	10	4	present	present	NOUN
eurjchem-864	10	5	in	in	ADP
eurjchem-864	10	6	large	large	ADJ
eurjchem-864	10	7	number	number	NOUN
eurjchem-864	10	8	of	of	ADP
eurjchem-864	10	9	pharmaceutical	pharmaceutical	ADJ
eurjchem-864	10	10	products	product	NOUN
eurjchem-864	10	11	with	with	ADP
eurjchem-864	10	12	antimicrobial	antimicrobial	ADJ
eurjchem-864	10	13	[	[	X
eurjchem-864	10	14	1	1	NUM
eurjchem-864	10	15	]	]	PUNCT
eurjchem-864	10	16	,	,	PUNCT
eurjchem-864	10	17	anticonvulsant	anticonvulsant	NOUN
eurjchem-864	10	18	[	[	X
eurjchem-864	10	19	2,3	2,3	NUM
eurjchem-864	10	20	]	]	PUNCT
eurjchem-864	10	21	,	,	PUNCT
eurjchem-864	10	22	antitumor	antitumor	PROPN
eurjchem-864	11	1	[	[	X
eurjchem-864	11	2	4,5	4,5	NUM
eurjchem-864	11	3	]	]	PUNCT
eurjchem-864	11	4	,	,	PUNCT
eurjchem-864	11	5	antipsychotic	antipsychotic	ADJ
eurjchem-864	11	6	[	[	X
eurjchem-864	11	7	6‐8	6‐8	NOUN
eurjchem-864	11	8	]	]	PUNCT
eurjchem-864	11	9	,	,	PUNCT
eurjchem-864	11	10	antithrombotic	antithrombotic	ADJ
eurjchem-864	11	11	[	[	PUNCT
eurjchem-864	11	12	9	9	NUM
eurjchem-864	11	13	]	]	PUNCT
eurjchem-864	11	14	,	,	PUNCT
eurjchem-864	11	15	analgesic	analgesic	ADJ
eurjchem-864	11	16	activities	activity	NOUN
eurjchem-864	11	17	[	[	X
eurjchem-864	11	18	10	10	NUM
eurjchem-864	11	19	]	]	PUNCT
eurjchem-864	11	20	.	.	PUNCT
eurjchem-864	12	1	they	they	PRON
eurjchem-864	12	2	have	have	AUX
eurjchem-864	12	3	also	also	ADV
eurjchem-864	12	4	exhibited	exhibit	VERB
eurjchem-864	12	5	antiglycating	antiglycate	VERB
eurjchem-864	12	6	[	[	X
eurjchem-864	12	7	11	11	NUM
eurjchem-864	12	8	]	]	PUNCT
eurjchem-864	12	9	and	and	CCONJ
eurjchem-864	12	10	cholinesterase‐inhibiting	cholinesterase‐inhibite	VERB
eurjchem-864	12	11	properties	property	NOUN
eurjchem-864	12	12	[	[	X
eurjchem-864	12	13	12,13	12,13	NUM
eurjchem-864	12	14	]	]	PUNCT
eurjchem-864	12	15	.	.	PUNCT
eurjchem-864	13	1	previously	previously	ADV
eurjchem-864	13	2	we	we	PRON
eurjchem-864	13	3	have	have	AUX
eurjchem-864	13	4	investigated	investigate	VERB
eurjchem-864	13	5	various	various	ADJ
eurjchem-864	13	6	biological	biological	ADJ
eurjchem-864	13	7	activities	activity	NOUN
eurjchem-864	13	8	of	of	ADP
eurjchem-864	13	9	these	these	DET
eurjchem-864	13	10	benzisoxazole	benzisoxazole	NOUN
eurjchem-864	13	11	derivatives	derivative	NOUN
eurjchem-864	13	12	as	as	ADP
eurjchem-864	13	13	antimicrobial	antimicrobial	ADJ
eurjchem-864	13	14	[	[	X
eurjchem-864	13	15	1	1	NUM
eurjchem-864	13	16	]	]	PUNCT
eurjchem-864	13	17	and	and	CCONJ
eurjchem-864	13	18	cholinesterase‐inhibiting	cholinesterase‐inhibite	VERB
eurjchem-864	13	19	agents	agent	NOUN
eurjchem-864	13	20	[	[	X
eurjchem-864	13	21	13	13	NUM
eurjchem-864	13	22	]	]	PUNCT
eurjchem-864	13	23	.	.	PUNCT
eurjchem-864	14	1	in	in	ADP
eurjchem-864	14	2	continuation	continuation	NOUN
eurjchem-864	14	3	of	of	ADP
eurjchem-864	14	4	this	this	DET
eurjchem-864	14	5	work	work	NOUN
eurjchem-864	14	6	,	,	PUNCT
eurjchem-864	14	7	we	we	PRON
eurjchem-864	14	8	report	report	VERB
eurjchem-864	14	9	herein	herein	ADJ
eurjchem-864	14	10	antibacterial	antibacterial	ADJ
eurjchem-864	14	11	,	,	PUNCT
eurjchem-864	14	12	antioxidant	antioxidant	NOUN
eurjchem-864	14	13	and	and	CCONJ
eurjchem-864	14	14	anti‐	anti‐	NOUN
eurjchem-864	14	15	inflammatory	inflammatory	ADJ
eurjchem-864	14	16	activities	activity	NOUN
eurjchem-864	14	17	of	of	ADP
eurjchem-864	14	18	piperidyl	piperidyl	ADJ
eurjchem-864	14	19	spirolactone	spirolactone	NOUN
eurjchem-864	14	20	linked	link	VERB
eurjchem-864	14	21	benzisoxazole	benzisoxazole	NOUN
eurjchem-864	14	22	derivatives	derivative	NOUN
eurjchem-864	14	23	.	.	PUNCT
eurjchem-864	15	1	2	2	X
eurjchem-864	15	2	.	.	X
eurjchem-864	15	3	experimental	experimental	ADJ
eurjchem-864	15	4	2.1	2.1	NUM
eurjchem-864	15	5	.	.	PUNCT
eurjchem-864	16	1	instrumentation	instrumentation	NOUN
eurjchem-864	16	2	the	the	DET
eurjchem-864	16	3	melting	melting	NOUN
eurjchem-864	16	4	points	point	NOUN
eurjchem-864	16	5	were	be	AUX
eurjchem-864	16	6	determined	determine	VERB
eurjchem-864	16	7	on	on	ADP
eurjchem-864	16	8	selaco	selaco	NOUN
eurjchem-864	16	9	melting	melting	NOUN
eurjchem-864	16	10	point	point	NOUN
eurjchem-864	16	11	apparatus	apparatus	NOUN
eurjchem-864	16	12	and	and	CCONJ
eurjchem-864	16	13	are	be	AUX
eurjchem-864	16	14	uncorrected	uncorrecte	VERB
eurjchem-864	16	15	.	.	PUNCT
eurjchem-864	17	1	infrared	infrared	PROPN
eurjchem-864	17	2	spectra	spectra	PROPN
eurjchem-864	17	3	were	be	AUX
eurjchem-864	17	4	recorded	record	VERB
eurjchem-864	17	5	on	on	ADP
eurjchem-864	17	6	shimadzu	shimadzu	PROPN
eurjchem-864	17	7	ft‐ir	ft‐ir	ADJ
eurjchem-864	17	8	model	model	NOUN
eurjchem-864	17	9	8300	8300	NUM
eurjchem-864	17	10	spectrometer	spectrometer	NOUN
eurjchem-864	17	11	.	.	PUNCT
eurjchem-864	18	1	1h	1h	NUM
eurjchem-864	18	2	nmr	nmr	PROPN
eurjchem-864	18	3	spectra	spectra	NOUN
eurjchem-864	18	4	were	be	AUX
eurjchem-864	18	5	recorded	record	VERB
eurjchem-864	18	6	on	on	ADP
eurjchem-864	18	7	an	an	DET
eurjchem-864	18	8	nmr	nmr	NOUN
eurjchem-864	18	9	spectrometer	spectrometer	NOUN
eurjchem-864	18	10	operating	operate	VERB
eurjchem-864	18	11	at	at	ADP
eurjchem-864	18	12	400	400	NUM
eurjchem-864	18	13	mhz	mhz	NOUN
eurjchem-864	18	14	using	use	VERB
eurjchem-864	18	15	tms	tms	PROPN
eurjchem-864	18	16	as	as	ADP
eurjchem-864	18	17	internal	internal	ADJ
eurjchem-864	18	18	standard	standard	NOUN
eurjchem-864	18	19	.	.	PUNCT
eurjchem-864	19	1	mass	mass	PROPN
eurjchem-864	19	2	spectra	spectra	PROPN
eurjchem-864	19	3	were	be	AUX
eurjchem-864	19	4	recorded	record	VERB
eurjchem-864	19	5	using	use	VERB
eurjchem-864	19	6	electrospray	electrospray	ADJ
eurjchem-864	19	7	ionization	ionization	NOUN
eurjchem-864	19	8	mass	mass	NOUN
eurjchem-864	19	9	spectrometry	spectrometry	NOUN
eurjchem-864	19	10	.	.	PUNCT
eurjchem-864	20	1	the	the	DET
eurjchem-864	20	2	c	c	PROPN
eurjchem-864	20	3	,	,	PUNCT
eurjchem-864	20	4	h	h	NOUN
eurjchem-864	20	5	and	and	CCONJ
eurjchem-864	20	6	n	n	PRON
eurjchem-864	20	7	analysis	analysis	NOUN
eurjchem-864	20	8	were	be	AUX
eurjchem-864	20	9	performed	perform	VERB
eurjchem-864	20	10	using	use	VERB
eurjchem-864	20	11	ce‐400	ce‐400	PROPN
eurjchem-864	20	12	chn	chn	PROPN
eurjchem-864	20	13	analyzer	analyzer	NOUN
eurjchem-864	20	14	.	.	PUNCT
eurjchem-864	21	1	reactions	reaction	NOUN
eurjchem-864	21	2	were	be	AUX
eurjchem-864	21	3	monitored	monitor	VERB
eurjchem-864	21	4	by	by	ADP
eurjchem-864	21	5	tlc	tlc	NOUN
eurjchem-864	21	6	using	use	VERB
eurjchem-864	21	7	precoated	precoate	VERB
eurjchem-864	21	8	sheets	sheet	NOUN
eurjchem-864	21	9	of	of	ADP
eurjchem-864	21	10	silica	silica	NOUN
eurjchem-864	21	11	gel	gel	NOUN
eurjchem-864	21	12	g	g	PROPN
eurjchem-864	21	13	/	/	SYM
eurjchem-864	21	14	uv‐254	uv‐254	PROPN
eurjchem-864	21	15	of	of	ADP
eurjchem-864	21	16	0.25	0.25	NUM
eurjchem-864	21	17	mm	mm	NOUN
eurjchem-864	21	18	thickness	thickness	NOUN
eurjchem-864	21	19	(	(	PUNCT
eurjchem-864	21	20	merck	merck	PROPN
eurjchem-864	21	21	60f254	60f254	PROPN
eurjchem-864	21	22	)	)	PUNCT
eurjchem-864	21	23	using	use	VERB
eurjchem-864	21	24	uv	uv	NOUN
eurjchem-864	21	25	light	light	NOUN
eurjchem-864	21	26	for	for	ADP
eurjchem-864	21	27	visualization	visualization	NOUN
eurjchem-864	21	28	.	.	PUNCT
eurjchem-864	22	1	all	all	DET
eurjchem-864	22	2	chemicals	chemical	NOUN
eurjchem-864	22	3	were	be	AUX
eurjchem-864	22	4	obtained	obtain	VERB
eurjchem-864	22	5	from	from	ADP
eurjchem-864	22	6	aldrich	aldrich	PROPN
eurjchem-864	22	7	,	,	PUNCT
eurjchem-864	22	8	fluka	fluka	NOUN
eurjchem-864	22	9	and	and	CCONJ
eurjchem-864	22	10	merck	merck	PROPN
eurjchem-864	22	11	chemicals	chemical	NOUN
eurjchem-864	22	12	.	.	PUNCT
eurjchem-864	23	1	2.2	2.2	NUM
eurjchem-864	23	2	.	.	PUNCT
eurjchem-864	24	1	synthesis	synthesis	NOUN
eurjchem-864	24	2	2.2.1	2.2.1	NUM
eurjchem-864	24	3	.	.	PUNCT
eurjchem-864	24	4	general	general	ADJ
eurjchem-864	24	5	procedure	procedure	NOUN
eurjchem-864	24	6	for	for	ADP
eurjchem-864	24	7	the	the	DET
eurjchem-864	24	8	synthesis	synthesis	NOUN
eurjchem-864	24	9	of	of	ADP
eurjchem-864	24	10	8‐tert‐butyl	8‐tert‐butyl	NUM
eurjchem-864	24	11	4‐	4‐	NUM
eurjchem-864	24	12	methyl	methyl	NOUN
eurjchem-864	24	13	3‐methyl‐2‐oxo‐1‐oxa‐8‐azaspiro[4.5]dec‐3‐ene‐4,8‐	3‐methyl‐2‐oxo‐1‐oxa‐8‐azaspiro[4.5]dec‐3‐ene‐4,8‐	NUM
eurjchem-864	24	14	dicarboxylate	dicarboxylate	ADJ
eurjchem-864	24	15	(	(	PUNCT
eurjchem-864	24	16	3	3	NUM
eurjchem-864	24	17	)	)	PUNCT
eurjchem-864	24	18	to	to	ADP
eurjchem-864	24	19	a	a	DET
eurjchem-864	24	20	solution	solution	NOUN
eurjchem-864	24	21	of	of	ADP
eurjchem-864	24	22	tert‐butyl	tert‐butyl	ADP
eurjchem-864	24	23	4‐oxopiperidine‐1‐carboxylate	4‐oxopiperidine‐1‐carboxylate	PROPN
eurjchem-864	24	24	(	(	PUNCT
eurjchem-864	24	25	20	20	NUM
eurjchem-864	24	26	mmol	mmol	NOUN
eurjchem-864	24	27	)	)	PUNCT
eurjchem-864	24	28	and	and	CCONJ
eurjchem-864	24	29	dimethyl	dimethyl	PROPN
eurjchem-864	24	30	2‐methylenesuccinate	2‐methylenesuccinate	NOUN
eurjchem-864	24	31	(	(	PUNCT
eurjchem-864	24	32	20	20	NUM
eurjchem-864	24	33	mmol	mmol	NOUN
eurjchem-864	24	34	)	)	PUNCT
eurjchem-864	24	35	in	in	ADP
eurjchem-864	24	36	thf	thf	NOUN
eurjchem-864	24	37	(	(	PUNCT
eurjchem-864	24	38	50	50	NUM
eurjchem-864	24	39	ml	ml	NOUN
eurjchem-864	24	40	)	)	PUNCT
eurjchem-864	24	41	,	,	PUNCT
eurjchem-864	24	42	a	a	DET
eurjchem-864	24	43	solution	solution	NOUN
eurjchem-864	24	44	of	of	ADP
eurjchem-864	24	45	sodium	sodium	NOUN
eurjchem-864	24	46	methoxide	methoxide	NOUN
eurjchem-864	24	47	(	(	PUNCT
eurjchem-864	24	48	40	40	NUM
eurjchem-864	24	49	mmol	mmol	NOUN
eurjchem-864	24	50	)	)	PUNCT
eurjchem-864	24	51	was	be	AUX
eurjchem-864	24	52	added	add	VERB
eurjchem-864	24	53	at	at	ADP
eurjchem-864	24	54	0	0	NUM
eurjchem-864	24	55	°	°	NUM
eurjchem-864	24	56	c	c	NOUN
eurjchem-864	24	57	.	.	PUNCT
eurjchem-864	25	1	the	the	DET
eurjchem-864	25	2	reaction	reaction	NOUN
eurjchem-864	25	3	mixture	mixture	NOUN
eurjchem-864	25	4	was	be	AUX
eurjchem-864	25	5	stirred	stir	VERB
eurjchem-864	25	6	at	at	ADP
eurjchem-864	25	7	room	room	NOUN
eurjchem-864	25	8	temperature	temperature	NOUN
eurjchem-864	25	9	for	for	ADP
eurjchem-864	25	10	8	8	NUM
eurjchem-864	25	11	h.	h.	NOUN
eurjchem-864	25	12	after	after	ADP
eurjchem-864	25	13	completion	completion	NOUN
eurjchem-864	25	14	of	of	ADP
eurjchem-864	25	15	the	the	DET
eurjchem-864	25	16	reaction	reaction	NOUN
eurjchem-864	25	17	,	,	PUNCT
eurjchem-864	25	18	10	10	NUM
eurjchem-864	25	19	ml	ml	NOUN
eurjchem-864	25	20	of	of	ADP
eurjchem-864	25	21	water	water	NOUN
eurjchem-864	25	22	was	be	AUX
eurjchem-864	25	23	added	add	VERB
eurjchem-864	25	24	;	;	PUNCT
eurjchem-864	25	25	the	the	DET
eurjchem-864	25	26	organic	organic	ADJ
eurjchem-864	25	27	layer	layer	NOUN
eurjchem-864	25	28	was	be	AUX
eurjchem-864	25	29	extracted	extract	VERB
eurjchem-864	25	30	with	with	ADP
eurjchem-864	25	31	ethyl	ethyl	PROPN
eurjchem-864	25	32	acetate	acetate	NOUN
eurjchem-864	25	33	distilled	distil	VERB
eurjchem-864	25	34	under	under	ADP
eurjchem-864	25	35	reduced	reduce	VERB
eurjchem-864	25	36	pressure	pressure	NOUN
eurjchem-864	25	37	to	to	PART
eurjchem-864	25	38	get	get	VERB
eurjchem-864	25	39	product	product	NOUN
eurjchem-864	25	40	3	3	NUM
eurjchem-864	25	41	in	in	ADP
eurjchem-864	25	42	good	good	ADJ
eurjchem-864	25	43	yield	yield	NOUN
eurjchem-864	25	44	(	(	PUNCT
eurjchem-864	25	45	scheme	scheme	NOUN
eurjchem-864	25	46	1	1	NUM
eurjchem-864	25	47	)	)	PUNCT
eurjchem-864	25	48	.	.	PUNCT
eurjchem-864	26	1	colour	colour	NOUN
eurjchem-864	26	2	:	:	PUNCT
eurjchem-864	27	1	white	white	ADJ
eurjchem-864	27	2	.	.	PUNCT
eurjchem-864	27	3	yield	yield	NOUN
eurjchem-864	27	4	:	:	PUNCT
eurjchem-864	27	5	70	70	NUM
eurjchem-864	27	6	%	%	NOUN
eurjchem-864	27	7	(	(	PUNCT
eurjchem-864	27	8	4.55	4.55	NUM
eurjchem-864	27	9	g	g	NOUN
eurjchem-864	27	10	)	)	PUNCT
eurjchem-864	27	11	.	.	PUNCT
eurjchem-864	28	1	viscous	viscous	ADJ
eurjchem-864	28	2	liquid	liquid	NOUN
eurjchem-864	28	3	.	.	PUNCT
eurjchem-864	29	1	ft‐ir	ft‐ir	NOUN
eurjchem-864	29	2	(	(	PUNCT
eurjchem-864	29	3	kbr	kbr	PROPN
eurjchem-864	29	4	,	,	PUNCT
eurjchem-864	29	5	cm‐1	cm‐1	PROPN
eurjchem-864	29	6	):	):	PUNCT
eurjchem-864	29	7	1555	1555	NUM
eurjchem-864	29	8	(	(	PUNCT
eurjchem-864	29	9	olefin	olefin	PROPN
eurjchem-864	29	10	c	c	NOUN
eurjchem-864	29	11	=	=	SYM
eurjchem-864	29	12	c	c	NOUN
eurjchem-864	29	13	str	str	NOUN
eurjchem-864	29	14	.	.	PUNCT
eurjchem-864	29	15	)	)	PUNCT
eurjchem-864	29	16	,	,	PUNCT
eurjchem-864	29	17	1740	1740	NUM
eurjchem-864	29	18	(	(	PUNCT
eurjchem-864	29	19	ester	ester	NOUN
eurjchem-864	29	20	co	co	NOUN
eurjchem-864	29	21	str	str	PROPN
eurjchem-864	29	22	.	.	PUNCT
eurjchem-864	29	23	)	)	PUNCT
eurjchem-864	29	24	,	,	PUNCT
eurjchem-864	29	25	3045	3045	NUM
eurjchem-864	29	26	(	(	PUNCT
eurjchem-864	29	27	aromatic	aromatic	ADJ
eurjchem-864	29	28	ch	ch	NOUN
eurjchem-864	29	29	str	str	NOUN
eurjchem-864	29	30	.	.	PUNCT
eurjchem-864	29	31	)	)	PUNCT
eurjchem-864	29	32	.	.	PUNCT
eurjchem-864	30	1	1h	1h	NUM
eurjchem-864	30	2	nmr	nmr	NOUN
eurjchem-864	30	3	(	(	PUNCT
eurjchem-864	30	4	400	400	NUM
eurjchem-864	30	5	mhz	mhz	NOUN
eurjchem-864	30	6	,	,	PUNCT
eurjchem-864	30	7	cdcl3	cdcl3	PROPN
eurjchem-864	30	8	,	,	PUNCT
eurjchem-864	30	9	δ	δ	PROPN
eurjchem-864	30	10	,	,	PUNCT
eurjchem-864	30	11	ppm	ppm	NUM
eurjchem-864	30	12	):	):	PUNCT
eurjchem-864	30	13	3.77	3.77	NUM
eurjchem-864	30	14	(	(	PUNCT
eurjchem-864	30	15	s	s	PROPN
eurjchem-864	30	16	,	,	PUNCT
eurjchem-864	30	17	3h	3h	NUM
eurjchem-864	30	18	,	,	PUNCT
eurjchem-864	30	19	ome	ome	PROPN
eurjchem-864	30	20	)	)	PUNCT
eurjchem-864	30	21	,	,	PUNCT
eurjchem-864	30	22	3.30‐3.41	3.30‐3.41	NUM
eurjchem-864	30	23	(	(	PUNCT
eurjchem-864	30	24	m	m	PROPN
eurjchem-864	30	25	,	,	PUNCT
eurjchem-864	30	26	4h	4h	NOUN
eurjchem-864	30	27	,	,	PUNCT
eurjchem-864	30	28	ch2	ch2	PROPN
eurjchem-864	30	29	)	)	PUNCT
eurjchem-864	30	30	,	,	PUNCT
eurjchem-864	30	31	2.43	2.43	NUM
eurjchem-864	30	32	(	(	PUNCT
eurjchem-864	30	33	s	s	PROPN
eurjchem-864	30	34	,	,	PUNCT
eurjchem-864	30	35	3h	3h	NUM
eurjchem-864	30	36	,	,	PUNCT
eurjchem-864	30	37	ch3	ch3	PROPN
eurjchem-864	30	38	)	)	PUNCT
eurjchem-864	30	39	,	,	PUNCT
eurjchem-864	30	40	1.65‐1.80	1.65‐1.80	NUM
eurjchem-864	30	41	(	(	PUNCT
eurjchem-864	30	42	m	m	PROPN
eurjchem-864	30	43	,	,	PUNCT
eurjchem-864	30	44	4h	4h	NOUN
eurjchem-864	30	45	,	,	PUNCT
eurjchem-864	30	46	ch2	ch2	PROPN
eurjchem-864	30	47	)	)	PUNCT
eurjchem-864	30	48	,	,	PUNCT
eurjchem-864	30	49	1.38	1.38	NUM
eurjchem-864	30	50	(	(	PUNCT
eurjchem-864	30	51	s	s	PROPN
eurjchem-864	30	52	,	,	PUNCT
eurjchem-864	30	53	9h	9h	NUM
eurjchem-864	30	54	,	,	PUNCT
eurjchem-864	30	55	(	(	PUNCT
eurjchem-864	30	56	ch3)3	ch3)3	NOUN
eurjchem-864	30	57	)	)	PUNCT
eurjchem-864	30	58	.	.	PUNCT
eurjchem-864	31	1	anal	anal	PROPN
eurjchem-864	31	2	.	.	PUNCT
eurjchem-864	31	3	calcd	calcd	NOUN
eurjchem-864	31	4	.	.	PUNCT
eurjchem-864	32	1	for	for	SCONJ
eurjchem-864	32	2	c16h23no6	c16h23no6	PROPN
eurjchem-864	32	3	:	:	PUNCT
eurjchem-864	32	4	c	c	X
eurjchem-864	32	5	,	,	PUNCT
eurjchem-864	32	6	59.06	59.06	NUM
eurjchem-864	32	7	;	;	PUNCT
eurjchem-864	32	8	h	h	X
eurjchem-864	32	9	,	,	PUNCT
eurjchem-864	32	10	7.13	7.13	NUM
eurjchem-864	32	11	;	;	PUNCT
eurjchem-864	32	12	n	n	CCONJ
eurjchem-864	32	13	,	,	PUNCT
eurjchem-864	32	14	4.31	4.31	NUM
eurjchem-864	32	15	.	.	PUNCT
eurjchem-864	32	16	found	find	VERB
eurjchem-864	32	17	:	:	PUNCT
eurjchem-864	33	1	c	c	X
eurjchem-864	33	2	,	,	PUNCT
eurjchem-864	33	3	59.15	59.15	NUM
eurjchem-864	33	4	;	;	PUNCT
eurjchem-864	33	5	h	h	NOUN
eurjchem-864	33	6	,	,	PUNCT
eurjchem-864	33	7	7.21	7.21	NUM
eurjchem-864	33	8	;	;	PUNCT
eurjchem-864	33	9	n	n	CCONJ
eurjchem-864	33	10	,	,	PUNCT
eurjchem-864	33	11	4.36	4.36	NUM
eurjchem-864	33	12	%	%	NOUN
eurjchem-864	33	13	.	.	PUNCT
eurjchem-864	34	1	ms	ms	NOUN
eurjchem-864	34	2	(	(	PUNCT
eurjchem-864	34	3	m	m	PROPN
eurjchem-864	34	4	/	/	SYM
eurjchem-864	34	5	z	z	NOUN
eurjchem-864	34	6	):	):	PUNCT
eurjchem-864	34	7	326	326	NUM
eurjchem-864	34	8	(	(	PUNCT
eurjchem-864	34	9	m+1	m+1	NUM
eurjchem-864	34	10	)	)	PUNCT
eurjchem-864	34	11	.	.	PUNCT
eurjchem-864	35	1	2.2.2	2.2.2	X
eurjchem-864	35	2	.	.	PUNCT
eurjchem-864	35	3	general	general	ADJ
eurjchem-864	35	4	procedure	procedure	NOUN
eurjchem-864	35	5	for	for	ADP
eurjchem-864	35	6	the	the	DET
eurjchem-864	35	7	synthesis	synthesis	NOUN
eurjchem-864	35	8	of	of	ADP
eurjchem-864	35	9	8‐(tert‐butoxy	8‐(tert‐butoxy	NUM
eurjchem-864	35	10	carbonyl)‐3‐methyl‐2‐oxo‐1‐oxa‐8‐azaspiro[4.5]dec‐3‐ene‐4‐	carbonyl)‐3‐methyl‐2‐oxo‐1‐oxa‐8‐azaspiro[4.5]dec‐3‐ene‐4‐	NOUN
eurjchem-864	35	11	carboxylic	carboxylic	ADJ
eurjchem-864	35	12	acid	acid	NOUN
eurjchem-864	35	13	(	(	PUNCT
eurjchem-864	35	14	4	4	NUM
eurjchem-864	35	15	)	)	PUNCT
eurjchem-864	35	16	to	to	ADP
eurjchem-864	35	17	a	a	DET
eurjchem-864	35	18	solution	solution	NOUN
eurjchem-864	35	19	of	of	ADP
eurjchem-864	35	20	compound	compound	NOUN
eurjchem-864	35	21	3	3	NUM
eurjchem-864	35	22	(	(	PUNCT
eurjchem-864	35	23	20	20	NUM
eurjchem-864	35	24	mmol	mmol	NOUN
eurjchem-864	35	25	)	)	PUNCT
eurjchem-864	35	26	in	in	ADP
eurjchem-864	35	27	methanol	methanol	NOUN
eurjchem-864	35	28	30	30	NUM
eurjchem-864	35	29	ml	ml	NOUN
eurjchem-864	35	30	and	and	CCONJ
eurjchem-864	35	31	lioh	lioh	ADV
eurjchem-864	35	32	(	(	PUNCT
eurjchem-864	35	33	20	20	NUM
eurjchem-864	35	34	mmol	mmol	NOUN
eurjchem-864	35	35	)	)	PUNCT
eurjchem-864	35	36	in	in	ADP
eurjchem-864	35	37	water	water	NOUN
eurjchem-864	35	38	(	(	PUNCT
eurjchem-864	35	39	30	30	NUM
eurjchem-864	35	40	ml	ml	NOUN
eurjchem-864	35	41	)	)	PUNCT
eurjchem-864	35	42	was	be	AUX
eurjchem-864	35	43	added	add	VERB
eurjchem-864	35	44	at	at	ADP
eurjchem-864	35	45	0	0	NUM
eurjchem-864	35	46	°	°	ADP
eurjchem-864	35	47	c	c	NOUN
eurjchem-864	35	48	and	and	CCONJ
eurjchem-864	35	49	stirred	stir	VERB
eurjchem-864	35	50	for	for	ADP
eurjchem-864	35	51	3	3	NUM
eurjchem-864	35	52	h	h	NOUN
eurjchem-864	35	53	at	at	ADP
eurjchem-864	35	54	room	room	NOUN
eurjchem-864	35	55	temperature	temperature	NOUN
eurjchem-864	35	56	.	.	PUNCT
eurjchem-864	36	1	after	after	ADP
eurjchem-864	36	2	completion	completion	NOUN
eurjchem-864	36	3	of	of	ADP
eurjchem-864	36	4	the	the	DET
eurjchem-864	36	5	reaction	reaction	NOUN
eurjchem-864	36	6	,	,	PUNCT
eurjchem-864	36	7	reaction	reaction	NOUN
eurjchem-864	36	8	mass	mass	NOUN
eurjchem-864	36	9	was	be	AUX
eurjchem-864	36	10	concentrated	concentrate	VERB
eurjchem-864	36	11	under	under	ADP
eurjchem-864	36	12	reduced	reduce	VERB
eurjchem-864	36	13	pressure	pressure	NOUN
eurjchem-864	36	14	and	and	CCONJ
eurjchem-864	36	15	the	the	DET
eurjchem-864	36	16	residue	residue	NOUN
eurjchem-864	36	17	was	be	AUX
eurjchem-864	36	18	extracted	extract	VERB
eurjchem-864	36	19	with	with	ADP
eurjchem-864	36	20	ethyl	ethyl	PROPN
eurjchem-864	36	21	acetate	acetate	NOUN
eurjchem-864	36	22	(	(	PUNCT
eurjchem-864	36	23	3	3	NUM
eurjchem-864	36	24	x	x	SYM
eurjchem-864	36	25	50	50	NUM
eurjchem-864	36	26	ml	ml	NOUN
eurjchem-864	36	27	)	)	PUNCT
eurjchem-864	36	28	,	,	PUNCT
eurjchem-864	36	29	the	the	DET
eurjchem-864	36	30	solvent	solvent	NOUN
eurjchem-864	36	31	was	be	AUX
eurjchem-864	36	32	removed	remove	VERB
eurjchem-864	36	33	under	under	ADP
eurjchem-864	36	34	reduced	reduce	VERB
eurjchem-864	36	35	pressure	pressure	NOUN
eurjchem-864	36	36	to	to	PART
eurjchem-864	36	37	get	get	VERB
eurjchem-864	36	38	product	product	NOUN
eurjchem-864	36	39	4	4	NUM
eurjchem-864	36	40	(	(	PUNCT
eurjchem-864	36	41	scheme	scheme	NOUN
eurjchem-864	36	42	1	1	NUM
eurjchem-864	36	43	)	)	PUNCT
eurjchem-864	36	44	.	.	PUNCT
eurjchem-864	37	1	colour	colour	NOUN
eurjchem-864	37	2	:	:	PUNCT
eurjchem-864	38	1	white	white	ADJ
eurjchem-864	38	2	.	.	PUNCT
eurjchem-864	38	3	yield	yield	NOUN
eurjchem-864	38	4	:	:	PUNCT
eurjchem-864	38	5	89	89	NUM
eurjchem-864	38	6	%	%	NOUN
eurjchem-864	38	7	(	(	PUNCT
eurjchem-864	38	8	5.53	5.53	NUM
eurjchem-864	38	9	g	g	NOUN
eurjchem-864	38	10	)	)	PUNCT
eurjchem-864	38	11	.	.	PUNCT
eurjchem-864	39	1	m.p	m.p	PROPN
eurjchem-864	39	2	.	.	PROPN
eurjchem-864	39	3	:	:	PUNCT
eurjchem-864	40	1	126‐128	126‐128	PROPN
eurjchem-864	40	2	°	°	SYM
eurjchem-864	40	3	c	c	X
eurjchem-864	40	4	.	.	PUNCT
eurjchem-864	41	1	ft‐ir	ft‐ir	NOUN
eurjchem-864	41	2	(	(	PUNCT
eurjchem-864	41	3	kbr	kbr	PROPN
eurjchem-864	41	4	,	,	PUNCT
eurjchem-864	41	5	cm‐1	cm‐1	PROPN
eurjchem-864	41	6	):	):	PUNCT
eurjchem-864	41	7	1715	1715	NUM
eurjchem-864	41	8	(	(	PUNCT
eurjchem-864	41	9	acid	acid	PROPN
eurjchem-864	41	10	co	co	NOUN
eurjchem-864	41	11	str	str	PROPN
eurjchem-864	41	12	.	.	PUNCT
eurjchem-864	41	13	)	)	PUNCT
eurjchem-864	41	14	,	,	PUNCT
eurjchem-864	41	15	1742	1742	NUM
eurjchem-864	41	16	(	(	PUNCT
eurjchem-864	41	17	ester	ester	NOUN
eurjchem-864	41	18	co	co	NOUN
eurjchem-864	41	19	str	str	PROPN
eurjchem-864	41	20	.	.	PUNCT
eurjchem-864	41	21	)	)	PUNCT
eurjchem-864	41	22	,	,	PUNCT
eurjchem-864	41	23	3042	3042	NUM
eurjchem-864	41	24	(	(	PUNCT
eurjchem-864	41	25	aromatic	aromatic	ADJ
eurjchem-864	41	26	ch	ch	NOUN
eurjchem-864	41	27	str	str	NOUN
eurjchem-864	41	28	.	.	PUNCT
eurjchem-864	41	29	)	)	PUNCT
eurjchem-864	41	30	,	,	PUNCT
eurjchem-864	41	31	3215	3215	NUM
eurjchem-864	41	32	(	(	PUNCT
eurjchem-864	41	33	acid	acid	PROPN
eurjchem-864	41	34	oh	oh	INTJ
eurjchem-864	41	35	str	str	NOUN
eurjchem-864	41	36	.	.	PUNCT
eurjchem-864	41	37	)	)	PUNCT
eurjchem-864	41	38	.	.	PUNCT
eurjchem-864	42	1	shivaprasad	shivaprasad	PROPN
eurjchem-864	42	2	et	et	PROPN
eurjchem-864	42	3	al	al	PROPN
eurjchem-864	42	4	.	.	PUNCT
eurjchem-864	42	5	/	/	SYM
eurjchem-864	42	6	european	european	PROPN
eurjchem-864	42	7	journal	journal	PROPN
eurjchem-864	42	8	of	of	ADP
eurjchem-864	42	9	chemistry	chemistry	NOUN
eurjchem-864	42	10	4	4	NUM
eurjchem-864	42	11	(	(	PUNCT
eurjchem-864	42	12	4	4	NUM
eurjchem-864	42	13	)	)	PUNCT
eurjchem-864	42	14	(	(	PUNCT
eurjchem-864	42	15	2013	2013	NUM
eurjchem-864	42	16	)	)	PUNCT
eurjchem-864	42	17	402‐407	402‐407	PROPN
eurjchem-864	43	1	403	403	NUM
eurjchem-864	43	2	reagents	reagent	NOUN
eurjchem-864	43	3	and	and	CCONJ
eurjchem-864	43	4	reaction	reaction	NOUN
eurjchem-864	43	5	conditions	condition	NOUN
eurjchem-864	43	6	:	:	PUNCT
eurjchem-864	43	7	(	(	PUNCT
eurjchem-864	43	8	a	a	X
eurjchem-864	43	9	)	)	PUNCT
eurjchem-864	43	10	meona	meona	NOUN
eurjchem-864	43	11	/	/	SYM
eurjchem-864	43	12	thf	thf	NOUN
eurjchem-864	43	13	,	,	PUNCT
eurjchem-864	43	14	0	0	NUM
eurjchem-864	43	15	°	°	NUM
eurjchem-864	43	16	c‐rt	c‐rt	PROPN
eurjchem-864	43	17	,	,	PUNCT
eurjchem-864	43	18	8	8	NUM
eurjchem-864	43	19	h.	h.	NOUN
eurjchem-864	43	20	(	(	PUNCT
eurjchem-864	43	21	b	b	NOUN
eurjchem-864	43	22	)	)	PUNCT
eurjchem-864	43	23	lioh	lioh	ADV
eurjchem-864	43	24	/	/	SYM
eurjchem-864	43	25	meoh	meoh	PROPN
eurjchem-864	43	26	/	/	SYM
eurjchem-864	43	27	h2o	h2o	PROPN
eurjchem-864	43	28	,	,	PUNCT
eurjchem-864	43	29	0	0	NUM
eurjchem-864	43	30	°	°	NUM
eurjchem-864	43	31	c‐rt	c‐rt	PROPN
eurjchem-864	43	32	,	,	PUNCT
eurjchem-864	43	33	3	3	NUM
eurjchem-864	43	34	h.	h.	NOUN
eurjchem-864	43	35	(	(	PUNCT
eurjchem-864	43	36	c	c	NOUN
eurjchem-864	43	37	)	)	PUNCT
eurjchem-864	43	38	6‐fluoro‐3‐(piperidin‐4‐yl)benzo[d]isoxazole	6‐fluoro‐3‐(piperidin‐4‐yl)benzo[d]isoxazole	NUM
eurjchem-864	43	39	hydrochloride	hydrochloride	NOUN
eurjchem-864	43	40	5	5	NUM
eurjchem-864	43	41	,	,	PUNCT
eurjchem-864	43	42	edc.hcl/hobt/dipea/ch2cl2	edc.hcl/hobt/dipea/ch2cl2	NOUN
eurjchem-864	43	43	,	,	PUNCT
eurjchem-864	43	44	0	0	NUM
eurjchem-864	43	45	°	°	NUM
eurjchem-864	43	46	c‐rt	c‐rt	PROPN
eurjchem-864	43	47	,	,	PUNCT
eurjchem-864	43	48	8h	8h	NUM
eurjchem-864	43	49	.	.	PUNCT
eurjchem-864	44	1	(	(	PUNCT
eurjchem-864	44	2	d	d	X
eurjchem-864	44	3	)	)	PUNCT
eurjchem-864	44	4	hcl	hcl	PROPN
eurjchem-864	44	5	/	/	SYM
eurjchem-864	44	6	ether	ether	NOUN
eurjchem-864	44	7	,	,	PUNCT
eurjchem-864	44	8	0	0	NUM
eurjchem-864	44	9	°	°	NUM
eurjchem-864	44	10	c‐rt	c‐rt	PROPN
eurjchem-864	44	11	,	,	PUNCT
eurjchem-864	44	12	1h	1h	NUM
eurjchem-864	44	13	.	.	PUNCT
eurjchem-864	45	1	(	(	PUNCT
eurjchem-864	45	2	e	e	NOUN
eurjchem-864	45	3	)	)	PUNCT
eurjchem-864	45	4	rcocl	rcocl	NOUN
eurjchem-864	45	5	8	8	NUM
eurjchem-864	45	6	,	,	PUNCT
eurjchem-864	45	7	tea	tea	NOUN
eurjchem-864	45	8	/	/	SYM
eurjchem-864	45	9	edc	edc	PROPN
eurjchem-864	45	10	,	,	PUNCT
eurjchem-864	45	11	0	0	NUM
eurjchem-864	45	12	°	°	NUM
eurjchem-864	45	13	c‐rt	c‐rt	PROPN
eurjchem-864	45	14	,	,	PUNCT
eurjchem-864	45	15	3‐4	3‐4	PROPN
eurjchem-864	45	16	h.	h.	PROPN
eurjchem-864	45	17	scheme	scheme	NOUN
eurjchem-864	45	18	1	1	NUM
eurjchem-864	45	19	1h	1h	NUM
eurjchem-864	45	20	nmr	nmr	NOUN
eurjchem-864	45	21	(	(	PUNCT
eurjchem-864	45	22	400	400	NUM
eurjchem-864	45	23	mhz	mhz	NOUN
eurjchem-864	45	24	,	,	PUNCT
eurjchem-864	45	25	cdcl3	cdcl3	PROPN
eurjchem-864	45	26	,	,	PUNCT
eurjchem-864	45	27	δ	δ	PROPN
eurjchem-864	45	28	,	,	PUNCT
eurjchem-864	45	29	ppm	ppm	NUM
eurjchem-864	45	30	):	):	PUNCT
eurjchem-864	45	31	10.5	10.5	NUM
eurjchem-864	45	32	(	(	PUNCT
eurjchem-864	45	33	s	s	PROPN
eurjchem-864	45	34	,	,	PUNCT
eurjchem-864	45	35	1h	1h	NUM
eurjchem-864	45	36	,	,	PUNCT
eurjchem-864	45	37	cooh	cooh	NOUN
eurjchem-864	45	38	)	)	PUNCT
eurjchem-864	45	39	,	,	PUNCT
eurjchem-864	45	40	3.30‐	3.30‐	NUM
eurjchem-864	45	41	3.40	3.40	NUM
eurjchem-864	45	42	(	(	PUNCT
eurjchem-864	45	43	m	m	PROPN
eurjchem-864	45	44	,	,	PUNCT
eurjchem-864	45	45	4h	4h	NOUN
eurjchem-864	45	46	,	,	PUNCT
eurjchem-864	45	47	ch2	ch2	PROPN
eurjchem-864	45	48	)	)	PUNCT
eurjchem-864	45	49	,	,	PUNCT
eurjchem-864	45	50	2.43	2.43	NUM
eurjchem-864	45	51	(	(	PUNCT
eurjchem-864	45	52	s	s	PROPN
eurjchem-864	45	53	,	,	PUNCT
eurjchem-864	45	54	3h	3h	NUM
eurjchem-864	45	55	,	,	PUNCT
eurjchem-864	45	56	ch3	ch3	PROPN
eurjchem-864	45	57	)	)	PUNCT
eurjchem-864	45	58	,	,	PUNCT
eurjchem-864	45	59	1.65‐1.80	1.65‐1.80	NUM
eurjchem-864	45	60	(	(	PUNCT
eurjchem-864	45	61	m	m	PROPN
eurjchem-864	45	62	,	,	PUNCT
eurjchem-864	45	63	4h	4h	NOUN
eurjchem-864	45	64	,	,	PUNCT
eurjchem-864	45	65	ch2	ch2	PROPN
eurjchem-864	45	66	)	)	PUNCT
eurjchem-864	45	67	,	,	PUNCT
eurjchem-864	45	68	1.38	1.38	NUM
eurjchem-864	45	69	(	(	PUNCT
eurjchem-864	45	70	s	s	PROPN
eurjchem-864	45	71	,	,	PUNCT
eurjchem-864	45	72	9h	9h	NUM
eurjchem-864	45	73	,	,	PUNCT
eurjchem-864	45	74	(	(	PUNCT
eurjchem-864	45	75	ch3)3	ch3)3	NOUN
eurjchem-864	45	76	)	)	PUNCT
eurjchem-864	45	77	.	.	PUNCT
eurjchem-864	46	1	anal	anal	PROPN
eurjchem-864	46	2	.	.	PUNCT
eurjchem-864	46	3	calcd	calcd	NOUN
eurjchem-864	46	4	.	.	PUNCT
eurjchem-864	47	1	for	for	ADP
eurjchem-864	47	2	c15h21no6	c15h21no6	NOUN
eurjchem-864	47	3	:	:	PUNCT
eurjchem-864	47	4	c	c	X
eurjchem-864	47	5	,	,	PUNCT
eurjchem-864	47	6	57.87	57.87	NUM
eurjchem-864	47	7	;	;	PUNCT
eurjchem-864	47	8	h	h	NOUN
eurjchem-864	47	9	,	,	PUNCT
eurjchem-864	47	10	6.80	6.80	NUM
eurjchem-864	47	11	;	;	PUNCT
eurjchem-864	47	12	n	n	CCONJ
eurjchem-864	47	13	,	,	PUNCT
eurjchem-864	47	14	4.50	4.50	NUM
eurjchem-864	47	15	.	.	PUNCT
eurjchem-864	47	16	found	find	VERB
eurjchem-864	47	17	:	:	PUNCT
eurjchem-864	48	1	c	c	X
eurjchem-864	48	2	,	,	PUNCT
eurjchem-864	48	3	57.96	57.96	NUM
eurjchem-864	48	4	;	;	PUNCT
eurjchem-864	48	5	h	h	NOUN
eurjchem-864	48	6	,	,	PUNCT
eurjchem-864	48	7	6.88	6.88	NUM
eurjchem-864	48	8	;	;	PUNCT
eurjchem-864	48	9	n	n	CCONJ
eurjchem-864	48	10	,	,	PUNCT
eurjchem-864	48	11	4.58	4.58	NUM
eurjchem-864	48	12	.	.	PUNCT
eurjchem-864	49	1	ms	ms	NOUN
eurjchem-864	49	2	(	(	PUNCT
eurjchem-864	49	3	m	m	PROPN
eurjchem-864	49	4	/	/	SYM
eurjchem-864	49	5	z	z	NOUN
eurjchem-864	49	6	):	):	PUNCT
eurjchem-864	49	7	311	311	NUM
eurjchem-864	49	8	(	(	PUNCT
eurjchem-864	49	9	m+1	m+1	NUM
eurjchem-864	49	10	)	)	PUNCT
eurjchem-864	49	11	.	.	PUNCT
eurjchem-864	50	1	2.2.3	2.2.3	X
eurjchem-864	50	2	.	.	PUNCT
eurjchem-864	50	3	general	general	ADJ
eurjchem-864	50	4	procedure	procedure	NOUN
eurjchem-864	50	5	for	for	ADP
eurjchem-864	50	6	the	the	DET
eurjchem-864	50	7	synthesis	synthesis	NOUN
eurjchem-864	50	8	of	of	ADP
eurjchem-864	50	9	tert‐butyl	tert‐butyl	X
eurjchem-864	50	10	4‐(4‐	4‐(4‐	NOUN
eurjchem-864	50	11	(	(	PUNCT
eurjchem-864	50	12	6‐fluorobenzo[d]isoxazol‐3‐yl)piperidine‐1‐carbonyl)‐3‐	6‐fluorobenzo[d]isoxazol‐3‐yl)piperidine‐1‐carbonyl)‐3‐	NUM
eurjchem-864	50	13	methyl‐2‐oxo‐1‐oxa‐8‐azaspiro[4.5]dec‐3‐ene‐8‐carboxylate	methyl‐2‐oxo‐1‐oxa‐8‐azaspiro[4.5]dec‐3‐ene‐8‐carboxylate	PROPN
eurjchem-864	50	14	(	(	PUNCT
eurjchem-864	50	15	6	6	NUM
eurjchem-864	50	16	)	)	PUNCT
eurjchem-864	50	17	to	to	ADP
eurjchem-864	50	18	a	a	DET
eurjchem-864	50	19	solution	solution	NOUN
eurjchem-864	50	20	of	of	ADP
eurjchem-864	50	21	compound	compound	NOUN
eurjchem-864	50	22	4	4	NUM
eurjchem-864	50	23	(	(	PUNCT
eurjchem-864	50	24	20	20	NUM
eurjchem-864	50	25	mmol	mmol	NOUN
eurjchem-864	50	26	)	)	PUNCT
eurjchem-864	50	27	and	and	CCONJ
eurjchem-864	50	28	6‐fluoro‐3‐	6‐fluoro‐3‐	NUM
eurjchem-864	50	29	(	(	PUNCT
eurjchem-864	50	30	piperidin‐4‐yl)benzo[d]isoxazole	piperidin‐4‐yl)benzo[d]isoxazole	PROPN
eurjchem-864	50	31	hydrochloride	hydrochloride	NOUN
eurjchem-864	51	1	[	[	X
eurjchem-864	51	2	14	14	NUM
eurjchem-864	51	3	]	]	SYM
eurjchem-864	51	4	5	5	NUM
eurjchem-864	51	5	(	(	PUNCT
eurjchem-864	51	6	20	20	NUM
eurjchem-864	51	7	mmol	mmol	NOUN
eurjchem-864	51	8	)	)	PUNCT
eurjchem-864	51	9	in	in	ADP
eurjchem-864	51	10	dichloromethane	dichloromethane	NOUN
eurjchem-864	51	11	(	(	PUNCT
eurjchem-864	51	12	40	40	NUM
eurjchem-864	51	13	ml	ml	NOUN
eurjchem-864	51	14	)	)	PUNCT
eurjchem-864	51	15	;	;	PUNCT
eurjchem-864	51	16	1‐ethyl‐3‐(3‐dimethyl	1‐ethyl‐3‐(3‐dimethyl	PROPN
eurjchem-864	51	17	aminopropyl)carbodiimide	aminopropyl)carbodiimide	PROPN
eurjchem-864	51	18	hydrochloride	hydrochloride	NOUN
eurjchem-864	51	19	(	(	PUNCT
eurjchem-864	51	20	edc.hcl	edc.hcl	X
eurjchem-864	51	21	)	)	PUNCT
eurjchem-864	51	22	(	(	PUNCT
eurjchem-864	51	23	20	20	NUM
eurjchem-864	51	24	mmol	mmol	NOUN
eurjchem-864	51	25	)	)	PUNCT
eurjchem-864	51	26	and	and	CCONJ
eurjchem-864	51	27	hydroxybenzotriazole	hydroxybenzotriazole	PROPN
eurjchem-864	51	28	(	(	PUNCT
eurjchem-864	51	29	hobt	hobt	NOUN
eurjchem-864	51	30	)	)	PUNCT
eurjchem-864	51	31	(	(	PUNCT
eurjchem-864	51	32	2	2	NUM
eurjchem-864	51	33	mmol	mmol	NOUN
eurjchem-864	51	34	)	)	PUNCT
eurjchem-864	51	35	was	be	AUX
eurjchem-864	51	36	added	add	VERB
eurjchem-864	51	37	at	at	ADP
eurjchem-864	51	38	0	0	NUM
eurjchem-864	51	39	°	°	ADP
eurjchem-864	51	40	c	c	NOUN
eurjchem-864	51	41	and	and	CCONJ
eurjchem-864	51	42	the	the	DET
eurjchem-864	51	43	reaction	reaction	NOUN
eurjchem-864	51	44	mixture	mixture	NOUN
eurjchem-864	51	45	was	be	AUX
eurjchem-864	51	46	stirred	stir	VERB
eurjchem-864	51	47	at	at	ADP
eurjchem-864	51	48	room	room	NOUN
eurjchem-864	51	49	temperature	temperature	NOUN
eurjchem-864	51	50	for	for	ADP
eurjchem-864	51	51	8	8	NUM
eurjchem-864	51	52	h.	h.	NOUN
eurjchem-864	51	53	after	after	ADP
eurjchem-864	51	54	completion	completion	NOUN
eurjchem-864	51	55	of	of	ADP
eurjchem-864	51	56	the	the	DET
eurjchem-864	51	57	reaction	reaction	NOUN
eurjchem-864	51	58	,	,	PUNCT
eurjchem-864	51	59	20	20	NUM
eurjchem-864	51	60	ml	ml	NOUN
eurjchem-864	51	61	of	of	ADP
eurjchem-864	51	62	water	water	NOUN
eurjchem-864	51	63	was	be	AUX
eurjchem-864	51	64	added	add	VERB
eurjchem-864	51	65	;	;	PUNCT
eurjchem-864	51	66	the	the	DET
eurjchem-864	51	67	organic	organic	ADJ
eurjchem-864	51	68	layer	layer	NOUN
eurjchem-864	51	69	was	be	AUX
eurjchem-864	51	70	extracted	extract	VERB
eurjchem-864	51	71	with	with	ADP
eurjchem-864	51	72	ethyl	ethyl	PROPN
eurjchem-864	51	73	acetate	acetate	NOUN
eurjchem-864	51	74	and	and	CCONJ
eurjchem-864	51	75	distilled	distil	VERB
eurjchem-864	51	76	under	under	ADP
eurjchem-864	51	77	reduced	reduce	VERB
eurjchem-864	51	78	pressure	pressure	NOUN
eurjchem-864	51	79	to	to	PART
eurjchem-864	51	80	get	get	VERB
eurjchem-864	51	81	product	product	NOUN
eurjchem-864	51	82	6	6	NUM
eurjchem-864	51	83	in	in	ADP
eurjchem-864	51	84	good	good	ADJ
eurjchem-864	51	85	yield	yield	NOUN
eurjchem-864	51	86	(	(	PUNCT
eurjchem-864	51	87	scheme	scheme	NOUN
eurjchem-864	51	88	1	1	NUM
eurjchem-864	51	89	)	)	PUNCT
eurjchem-864	51	90	.	.	PUNCT
eurjchem-864	52	1	colour	colour	NOUN
eurjchem-864	52	2	:	:	PUNCT
eurjchem-864	52	3	white	white	ADJ
eurjchem-864	52	4	.	.	PUNCT
eurjchem-864	53	1	yield	yield	NOUN
eurjchem-864	53	2	:	:	PUNCT
eurjchem-864	53	3	78	78	NUM
eurjchem-864	53	4	%	%	NOUN
eurjchem-864	53	5	(	(	PUNCT
eurjchem-864	53	6	8.00	8.00	NUM
eurjchem-864	53	7	g	g	NOUN
eurjchem-864	53	8	)	)	PUNCT
eurjchem-864	53	9	.	.	PUNCT
eurjchem-864	54	1	m.p	m.p	PROPN
eurjchem-864	54	2	.	.	PROPN
eurjchem-864	54	3	:	:	PUNCT
eurjchem-864	55	1	130‐132	130‐132	NUM
eurjchem-864	55	2	°	°	SYM
eurjchem-864	55	3	c	c	X
eurjchem-864	55	4	.	.	PUNCT
eurjchem-864	56	1	ft‐ir	ft‐ir	NOUN
eurjchem-864	56	2	(	(	PUNCT
eurjchem-864	56	3	kbr	kbr	PROPN
eurjchem-864	56	4	,	,	PUNCT
eurjchem-864	56	5	cm‐1	cm‐1	PROPN
eurjchem-864	56	6	):	):	PUNCT
eurjchem-864	56	7	1660	1660	NUM
eurjchem-864	56	8	(	(	PUNCT
eurjchem-864	56	9	amide	amide	PROPN
eurjchem-864	56	10	co	co	NOUN
eurjchem-864	56	11	str	str	PROPN
eurjchem-864	56	12	.	.	PUNCT
eurjchem-864	56	13	)	)	PUNCT
eurjchem-864	56	14	,	,	PUNCT
eurjchem-864	56	15	1742	1742	NUM
eurjchem-864	56	16	(	(	PUNCT
eurjchem-864	56	17	ester	ester	NOUN
eurjchem-864	56	18	co	co	NOUN
eurjchem-864	56	19	str	str	PROPN
eurjchem-864	56	20	.	.	PUNCT
eurjchem-864	56	21	)	)	PUNCT
eurjchem-864	56	22	,	,	PUNCT
eurjchem-864	56	23	3039	3039	NUM
eurjchem-864	56	24	(	(	PUNCT
eurjchem-864	56	25	aromatic	aromatic	ADJ
eurjchem-864	56	26	ch	ch	NOUN
eurjchem-864	56	27	str	str	NOUN
eurjchem-864	56	28	.	.	PUNCT
eurjchem-864	56	29	)	)	PUNCT
eurjchem-864	56	30	.	.	PUNCT
eurjchem-864	57	1	1h	1h	NUM
eurjchem-864	57	2	nmr	nmr	NOUN
eurjchem-864	57	3	(	(	PUNCT
eurjchem-864	57	4	400	400	NUM
eurjchem-864	57	5	mhz	mhz	NOUN
eurjchem-864	57	6	,	,	PUNCT
eurjchem-864	57	7	cdcl3	cdcl3	PROPN
eurjchem-864	57	8	,	,	PUNCT
eurjchem-864	57	9	δ	δ	PROPN
eurjchem-864	57	10	,	,	PUNCT
eurjchem-864	57	11	ppm	ppm	NOUN
eurjchem-864	57	12	):	):	PUNCT
eurjchem-864	57	13	7.54	7.54	NUM
eurjchem-864	57	14	(	(	PUNCT
eurjchem-864	57	15	d	d	PROPN
eurjchem-864	57	16	,	,	PUNCT
eurjchem-864	57	17	j=7.8	j=7.8	NOUN
eurjchem-864	57	18	hz	hz	NOUN
eurjchem-864	57	19	,	,	PUNCT
eurjchem-864	57	20	1h	1h	NUM
eurjchem-864	57	21	,	,	PUNCT
eurjchem-864	57	22	ar‐h	ar‐h	NOUN
eurjchem-864	57	23	)	)	PUNCT
eurjchem-864	57	24	,	,	PUNCT
eurjchem-864	57	25	7.24	7.24	NUM
eurjchem-864	57	26	(	(	PUNCT
eurjchem-864	57	27	d	d	PROPN
eurjchem-864	57	28	,	,	PUNCT
eurjchem-864	57	29	j=7.8	j=7.8	NOUN
eurjchem-864	57	30	hz	hz	NOUN
eurjchem-864	57	31	,	,	PUNCT
eurjchem-864	57	32	1h	1h	NUM
eurjchem-864	57	33	,	,	PUNCT
eurjchem-864	57	34	ar‐h	ar‐h	NOUN
eurjchem-864	57	35	)	)	PUNCT
eurjchem-864	57	36	,	,	PUNCT
eurjchem-864	57	37	6.97	6.97	NUM
eurjchem-864	57	38	(	(	PUNCT
eurjchem-864	57	39	s	s	PROPN
eurjchem-864	57	40	,	,	PUNCT
eurjchem-864	57	41	1h	1h	NUM
eurjchem-864	57	42	,	,	PUNCT
eurjchem-864	57	43	ar‐	ar‐	PROPN
eurjchem-864	57	44	h	h	NOUN
eurjchem-864	57	45	)	)	PUNCT
eurjchem-864	57	46	,	,	PUNCT
eurjchem-864	57	47	3.30‐3.41	3.30‐3.41	NUM
eurjchem-864	57	48	(	(	PUNCT
eurjchem-864	57	49	m	m	PROPN
eurjchem-864	57	50	,	,	PUNCT
eurjchem-864	57	51	8h	8h	NUM
eurjchem-864	57	52	,	,	PUNCT
eurjchem-864	57	53	ch2	ch2	PROPN
eurjchem-864	57	54	)	)	PUNCT
eurjchem-864	57	55	,	,	PUNCT
eurjchem-864	57	56	2.78	2.78	NUM
eurjchem-864	57	57	(	(	PUNCT
eurjchem-864	57	58	m	m	PROPN
eurjchem-864	57	59	,	,	PUNCT
eurjchem-864	57	60	1h	1h	NUM
eurjchem-864	57	61	,	,	PUNCT
eurjchem-864	57	62	ch	ch	NOUN
eurjchem-864	57	63	)	)	PUNCT
eurjchem-864	57	64	,	,	PUNCT
eurjchem-864	57	65	2.42	2.42	NUM
eurjchem-864	57	66	(	(	PUNCT
eurjchem-864	57	67	s	s	PROPN
eurjchem-864	57	68	,	,	PUNCT
eurjchem-864	57	69	3h	3h	NUM
eurjchem-864	57	70	,	,	PUNCT
eurjchem-864	57	71	ch3	ch3	PROPN
eurjchem-864	57	72	)	)	PUNCT
eurjchem-864	57	73	,	,	PUNCT
eurjchem-864	57	74	1.70‐1.86	1.70‐1.86	NUM
eurjchem-864	57	75	(	(	PUNCT
eurjchem-864	57	76	m	m	PROPN
eurjchem-864	57	77	,	,	PUNCT
eurjchem-864	57	78	8h	8h	NUM
eurjchem-864	57	79	,	,	PUNCT
eurjchem-864	57	80	ch2	ch2	PROPN
eurjchem-864	57	81	)	)	PUNCT
eurjchem-864	57	82	,	,	PUNCT
eurjchem-864	57	83	1.38	1.38	NUM
eurjchem-864	57	84	(	(	PUNCT
eurjchem-864	57	85	s	s	PROPN
eurjchem-864	57	86	,	,	PUNCT
eurjchem-864	57	87	9h	9h	NUM
eurjchem-864	57	88	,	,	PUNCT
eurjchem-864	57	89	(	(	PUNCT
eurjchem-864	57	90	ch3)3	ch3)3	NOUN
eurjchem-864	57	91	)	)	PUNCT
eurjchem-864	57	92	.	.	PUNCT
eurjchem-864	58	1	anal	anal	PROPN
eurjchem-864	58	2	.	.	PUNCT
eurjchem-864	58	3	calcd	calcd	NOUN
eurjchem-864	58	4	.	.	PUNCT
eurjchem-864	59	1	for	for	SCONJ
eurjchem-864	59	2	c27h32fn3o6	c27h32fn3o6	PROPN
eurjchem-864	59	3	:	:	PUNCT
eurjchem-864	59	4	c	c	X
eurjchem-864	59	5	,	,	PUNCT
eurjchem-864	59	6	63.15	63.15	NUM
eurjchem-864	59	7	;	;	PUNCT
eurjchem-864	59	8	h	h	NOUN
eurjchem-864	59	9	,	,	PUNCT
eurjchem-864	59	10	6.28	6.28	NUM
eurjchem-864	59	11	;	;	PUNCT
eurjchem-864	59	12	n	n	CCONJ
eurjchem-864	59	13	,	,	PUNCT
eurjchem-864	59	14	8.18	8.18	NUM
eurjchem-864	59	15	.	.	PUNCT
eurjchem-864	59	16	found	find	VERB
eurjchem-864	59	17	:	:	PUNCT
eurjchem-864	60	1	c	c	X
eurjchem-864	60	2	,	,	PUNCT
eurjchem-864	60	3	63.19	63.19	NUM
eurjchem-864	60	4	;	;	PUNCT
eurjchem-864	61	1	h	h	NOUN
eurjchem-864	61	2	,	,	PUNCT
eurjchem-864	61	3	6.35	6.35	NUM
eurjchem-864	61	4	;	;	PUNCT
eurjchem-864	61	5	n	n	CCONJ
eurjchem-864	61	6	,	,	PUNCT
eurjchem-864	61	7	8.26	8.26	NUM
eurjchem-864	61	8	.	.	PUNCT
eurjchem-864	62	1	ms	ms	NOUN
eurjchem-864	62	2	(	(	PUNCT
eurjchem-864	62	3	m	m	PROPN
eurjchem-864	62	4	/	/	SYM
eurjchem-864	62	5	z	z	NOUN
eurjchem-864	62	6	):	):	PUNCT
eurjchem-864	62	7	513	513	NUM
eurjchem-864	62	8	(	(	PUNCT
eurjchem-864	62	9	m+1	m+1	NUM
eurjchem-864	62	10	)	)	PUNCT
eurjchem-864	62	11	.	.	PUNCT
eurjchem-864	63	1	2.2.4	2.2.4	NUM
eurjchem-864	63	2	.	.	PUNCT
eurjchem-864	63	3	general	general	ADJ
eurjchem-864	63	4	procedure	procedure	NOUN
eurjchem-864	63	5	for	for	ADP
eurjchem-864	63	6	the	the	DET
eurjchem-864	63	7	synthesis	synthesis	NOUN
eurjchem-864	63	8	of	of	ADP
eurjchem-864	63	9	4‐(4‐(6‐fluoro	4‐(4‐(6‐fluoro	NUM
eurjchem-864	63	10	benzo[d]isoxazol‐3‐yl)piperidine‐1‐carbonyl)‐3‐methyl‐1‐	benzo[d]isoxazol‐3‐yl)piperidine‐1‐carbonyl)‐3‐methyl‐1‐	ADJ
eurjchem-864	63	11	oxa‐8‐azaspiro[4.5]dec‐3‐en‐2‐one	oxa‐8‐azaspiro[4.5]dec‐3‐en‐2‐one	NOUN
eurjchem-864	63	12	hydrochloride	hydrochloride	NOUN
eurjchem-864	63	13	(	(	PUNCT
eurjchem-864	63	14	7	7	NUM
eurjchem-864	63	15	)	)	PUNCT
eurjchem-864	63	16	to	to	ADP
eurjchem-864	63	17	a	a	DET
eurjchem-864	63	18	solution	solution	NOUN
eurjchem-864	63	19	of	of	ADP
eurjchem-864	63	20	compound	compound	NOUN
eurjchem-864	63	21	6	6	NUM
eurjchem-864	63	22	(	(	PUNCT
eurjchem-864	63	23	20	20	NUM
eurjchem-864	63	24	mmol)in	mmol)in	PROPN
eurjchem-864	63	25	diethyl	diethyl	NOUN
eurjchem-864	63	26	ether	ether	NOUN
eurjchem-864	63	27	(	(	PUNCT
eurjchem-864	63	28	40	40	NUM
eurjchem-864	63	29	ml	ml	NOUN
eurjchem-864	63	30	)	)	PUNCT
eurjchem-864	63	31	,	,	PUNCT
eurjchem-864	63	32	a	a	DET
eurjchem-864	63	33	saturated	saturate	VERB
eurjchem-864	63	34	solution	solution	NOUN
eurjchem-864	63	35	of	of	ADP
eurjchem-864	63	36	hcl	hcl	PROPN
eurjchem-864	63	37	in	in	ADP
eurjchem-864	63	38	ether	ether	NOUN
eurjchem-864	63	39	was	be	AUX
eurjchem-864	63	40	added	add	VERB
eurjchem-864	63	41	at	at	ADP
eurjchem-864	63	42	0	0	NUM
eurjchem-864	63	43	°	°	ADP
eurjchem-864	63	44	c	c	NOUN
eurjchem-864	63	45	for	for	ADP
eurjchem-864	63	46	1	1	NUM
eurjchem-864	63	47	h.	h.	NOUN
eurjchem-864	63	48	the	the	DET
eurjchem-864	63	49	reaction	reaction	NOUN
eurjchem-864	63	50	mixture	mixture	NOUN
eurjchem-864	63	51	was	be	AUX
eurjchem-864	63	52	concentrated	concentrate	VERB
eurjchem-864	63	53	under	under	ADP
eurjchem-864	63	54	reduced	reduce	VERB
eurjchem-864	63	55	pressure	pressure	NOUN
eurjchem-864	63	56	to	to	PART
eurjchem-864	63	57	get	get	VERB
eurjchem-864	63	58	compound	compound	NOUN
eurjchem-864	63	59	7	7	NUM
eurjchem-864	63	60	in	in	ADP
eurjchem-864	63	61	high	high	ADJ
eurjchem-864	63	62	yield	yield	NOUN
eurjchem-864	63	63	(	(	PUNCT
eurjchem-864	63	64	scheme	scheme	NOUN
eurjchem-864	63	65	1	1	NUM
eurjchem-864	63	66	)	)	PUNCT
eurjchem-864	63	67	.	.	PUNCT
eurjchem-864	64	1	colour	colour	NOUN
eurjchem-864	64	2	:	:	PUNCT
eurjchem-864	64	3	white	white	ADJ
eurjchem-864	64	4	.	.	PUNCT
eurjchem-864	65	1	yield	yield	NOUN
eurjchem-864	65	2	:	:	PUNCT
eurjchem-864	65	3	92	92	NUM
eurjchem-864	65	4	%	%	NOUN
eurjchem-864	65	5	(	(	PUNCT
eurjchem-864	65	6	8.26	8.26	NUM
eurjchem-864	65	7	g	g	NOUN
eurjchem-864	65	8	)	)	PUNCT
eurjchem-864	65	9	.	.	PUNCT
eurjchem-864	66	1	m.p	m.p	PROPN
eurjchem-864	66	2	.	.	PROPN
eurjchem-864	66	3	:	:	PUNCT
eurjchem-864	67	1	180‐182	180‐182	NUM
eurjchem-864	67	2	°	°	PROPN
eurjchem-864	67	3	c	c	X
eurjchem-864	67	4	.	.	PUNCT
eurjchem-864	68	1	ft‐ir	ft‐ir	NOUN
eurjchem-864	68	2	(	(	PUNCT
eurjchem-864	68	3	kbr	kbr	PROPN
eurjchem-864	68	4	,	,	PUNCT
eurjchem-864	68	5	cm‐1	cm‐1	PROPN
eurjchem-864	68	6	):	):	PUNCT
eurjchem-864	68	7	1664	1664	NUM
eurjchem-864	68	8	(	(	PUNCT
eurjchem-864	68	9	amide	amide	PROPN
eurjchem-864	68	10	co	co	NOUN
eurjchem-864	68	11	str	str	PROPN
eurjchem-864	68	12	.	.	PUNCT
eurjchem-864	68	13	)	)	PUNCT
eurjchem-864	68	14	,	,	PUNCT
eurjchem-864	68	15	1744	1744	NUM
eurjchem-864	68	16	(	(	PUNCT
eurjchem-864	68	17	ester	ester	NOUN
eurjchem-864	68	18	co	co	NOUN
eurjchem-864	68	19	str	str	PROPN
eurjchem-864	68	20	.	.	PUNCT
eurjchem-864	68	21	)	)	PUNCT
eurjchem-864	68	22	,	,	PUNCT
eurjchem-864	68	23	3035	3035	NUM
eurjchem-864	68	24	(	(	PUNCT
eurjchem-864	68	25	aromatic	aromatic	ADJ
eurjchem-864	68	26	ch	ch	NOUN
eurjchem-864	68	27	str	str	NOUN
eurjchem-864	68	28	.	.	PUNCT
eurjchem-864	68	29	)	)	PUNCT
eurjchem-864	68	30	,	,	PUNCT
eurjchem-864	68	31	3320	3320	NUM
eurjchem-864	68	32	(	(	PUNCT
eurjchem-864	68	33	amine	amine	PROPN
eurjchem-864	68	34	nh	nh	PROPN
eurjchem-864	68	35	str	str	NOUN
eurjchem-864	68	36	.	.	PUNCT
eurjchem-864	68	37	)	)	PUNCT
eurjchem-864	68	38	.	.	PUNCT
eurjchem-864	69	1	1h	1h	NUM
eurjchem-864	69	2	nmr	nmr	NOUN
eurjchem-864	69	3	(	(	PUNCT
eurjchem-864	69	4	400	400	NUM
eurjchem-864	69	5	mhz	mhz	NOUN
eurjchem-864	69	6	,	,	PUNCT
eurjchem-864	69	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-864	69	8	,	,	PUNCT
eurjchem-864	69	9	δ	δ	PROPN
eurjchem-864	69	10	,	,	PUNCT
eurjchem-864	69	11	ppm	ppm	NOUN
eurjchem-864	69	12	):	):	PUNCT
eurjchem-864	69	13	7.56	7.56	NUM
eurjchem-864	69	14	(	(	PUNCT
eurjchem-864	69	15	d	d	PROPN
eurjchem-864	69	16	,	,	PUNCT
eurjchem-864	69	17	j=7.8	j=7.8	NOUN
eurjchem-864	69	18	hz	hz	NOUN
eurjchem-864	69	19	,	,	PUNCT
eurjchem-864	69	20	1h	1h	NUM
eurjchem-864	69	21	,	,	PUNCT
eurjchem-864	69	22	ar‐h	ar‐h	NOUN
eurjchem-864	69	23	)	)	PUNCT
eurjchem-864	69	24	,	,	PUNCT
eurjchem-864	69	25	7.24	7.24	NUM
eurjchem-864	69	26	(	(	PUNCT
eurjchem-864	69	27	d	d	PROPN
eurjchem-864	69	28	,	,	PUNCT
eurjchem-864	69	29	j=7.8	j=7.8	NOUN
eurjchem-864	69	30	hz	hz	NOUN
eurjchem-864	69	31	,	,	PUNCT
eurjchem-864	69	32	1h	1h	NUM
eurjchem-864	69	33	,	,	PUNCT
eurjchem-864	69	34	ar‐h	ar‐h	NOUN
eurjchem-864	69	35	)	)	PUNCT
eurjchem-864	69	36	,	,	PUNCT
eurjchem-864	69	37	6.97	6.97	NUM
eurjchem-864	69	38	(	(	PUNCT
eurjchem-864	69	39	s	s	PROPN
eurjchem-864	69	40	,	,	PUNCT
eurjchem-864	69	41	1h	1h	NUM
eurjchem-864	69	42	,	,	PUNCT
eurjchem-864	69	43	ar‐h	ar‐h	NOUN
eurjchem-864	69	44	)	)	PUNCT
eurjchem-864	69	45	,	,	PUNCT
eurjchem-864	69	46	6.51	6.51	NUM
eurjchem-864	69	47	(	(	PUNCT
eurjchem-864	69	48	s	s	PROPN
eurjchem-864	69	49	,	,	PUNCT
eurjchem-864	69	50	1h	1h	NUM
eurjchem-864	69	51	,	,	PUNCT
eurjchem-864	69	52	nh	nh	PROPN
eurjchem-864	69	53	)	)	PUNCT
eurjchem-864	69	54	,	,	PUNCT
eurjchem-864	69	55	3.3‐3.42	3.3‐3.42	NUM
eurjchem-864	69	56	(	(	PUNCT
eurjchem-864	69	57	m	m	PROPN
eurjchem-864	69	58	,	,	PUNCT
eurjchem-864	69	59	8h	8h	NUM
eurjchem-864	69	60	,	,	PUNCT
eurjchem-864	69	61	ch2	ch2	PROPN
eurjchem-864	69	62	)	)	PUNCT
eurjchem-864	69	63	,	,	PUNCT
eurjchem-864	69	64	2.78	2.78	NUM
eurjchem-864	69	65	(	(	PUNCT
eurjchem-864	69	66	m	m	PROPN
eurjchem-864	69	67	,	,	PUNCT
eurjchem-864	69	68	1h	1h	NUM
eurjchem-864	69	69	,	,	PUNCT
eurjchem-864	69	70	ch	ch	NOUN
eurjchem-864	69	71	)	)	PUNCT
eurjchem-864	69	72	,	,	PUNCT
eurjchem-864	69	73	2.51	2.51	NUM
eurjchem-864	69	74	(	(	PUNCT
eurjchem-864	69	75	s	s	PROPN
eurjchem-864	69	76	,	,	PUNCT
eurjchem-864	69	77	3h	3h	NUM
eurjchem-864	69	78	,	,	PUNCT
eurjchem-864	69	79	ch3	ch3	PROPN
eurjchem-864	69	80	)	)	PUNCT
eurjchem-864	69	81	,	,	PUNCT
eurjchem-864	69	82	2.15‐2.30	2.15‐2.30	NUM
eurjchem-864	69	83	(	(	PUNCT
eurjchem-864	69	84	m	m	PROPN
eurjchem-864	69	85	,	,	PUNCT
eurjchem-864	69	86	4h	4h	NOUN
eurjchem-864	69	87	,	,	PUNCT
eurjchem-864	69	88	ch2	ch2	PROPN
eurjchem-864	69	89	)	)	PUNCT
eurjchem-864	69	90	,	,	PUNCT
eurjchem-864	69	91	1.70‐1.90	1.70‐1.90	NUM
eurjchem-864	69	92	(	(	PUNCT
eurjchem-864	69	93	m	m	PROPN
eurjchem-864	69	94	,	,	PUNCT
eurjchem-864	69	95	4h	4h	NOUN
eurjchem-864	69	96	,	,	PUNCT
eurjchem-864	69	97	ch2	ch2	PROPN
eurjchem-864	69	98	)	)	PUNCT
eurjchem-864	69	99	.	.	PUNCT
eurjchem-864	70	1	anal	anal	PROPN
eurjchem-864	70	2	.	.	PUNCT
eurjchem-864	70	3	calcd	calcd	NOUN
eurjchem-864	70	4	.	.	PUNCT
eurjchem-864	71	1	for	for	ADP
eurjchem-864	71	2	c22h25clfn3o4	c22h25clfn3o4	NOUN
eurjchem-864	71	3	:	:	PUNCT
eurjchem-864	71	4	c	c	X
eurjchem-864	71	5	,	,	PUNCT
eurjchem-864	71	6	58.73	58.73	NUM
eurjchem-864	71	7	;	;	PUNCT
eurjchem-864	71	8	h	h	NOUN
eurjchem-864	71	9	,	,	PUNCT
eurjchem-864	71	10	5.60	5.60	NUM
eurjchem-864	71	11	;	;	PUNCT
eurjchem-864	71	12	n	n	CCONJ
eurjchem-864	71	13	,	,	PUNCT
eurjchem-864	71	14	9.34	9.34	NUM
eurjchem-864	71	15	.	.	PUNCT
eurjchem-864	71	16	found	find	VERB
eurjchem-864	71	17	:	:	PUNCT
eurjchem-864	72	1	c	c	X
eurjchem-864	72	2	,	,	PUNCT
eurjchem-864	72	3	58.79	58.79	NUM
eurjchem-864	72	4	;	;	PUNCT
eurjchem-864	72	5	h	h	NOUN
eurjchem-864	72	6	,	,	PUNCT
eurjchem-864	72	7	5.68	5.68	NUM
eurjchem-864	72	8	;	;	PUNCT
eurjchem-864	72	9	n	n	CCONJ
eurjchem-864	72	10	,	,	PUNCT
eurjchem-864	72	11	9.42	9.42	NUM
eurjchem-864	72	12	.	.	PUNCT
eurjchem-864	73	1	ms	ms	NOUN
eurjchem-864	73	2	(	(	PUNCT
eurjchem-864	73	3	m	m	PROPN
eurjchem-864	73	4	/	/	SYM
eurjchem-864	73	5	z	z	NOUN
eurjchem-864	73	6	):	):	PUNCT
eurjchem-864	73	7	450	450	NUM
eurjchem-864	73	8	(	(	PUNCT
eurjchem-864	73	9	m+1	m+1	NUM
eurjchem-864	73	10	)	)	PUNCT
eurjchem-864	73	11	.	.	PUNCT
eurjchem-864	74	1	2.2.5	2.2.5	X
eurjchem-864	74	2	.	.	PUNCT
eurjchem-864	74	3	general	general	ADJ
eurjchem-864	74	4	procedure	procedure	NOUN
eurjchem-864	74	5	for	for	ADP
eurjchem-864	74	6	the	the	DET
eurjchem-864	74	7	synthesis	synthesis	NOUN
eurjchem-864	74	8	of	of	ADP
eurjchem-864	74	9	8‐acyl‐4‐(4‐(6‐	8‐acyl‐4‐(4‐(6‐	NUM
eurjchem-864	74	10	fluorobenzo[d]isoxazol‐3‐yl)piperidine‐1‐carbonyl)‐3‐	fluorobenzo[d]isoxazol‐3‐yl)piperidine‐1‐carbonyl)‐3‐	NUM
eurjchem-864	74	11	methyl‐1‐oxa‐8‐azaspiro[4.5]dec‐3‐en‐2‐one	methyl‐1‐oxa‐8‐azaspiro[4.5]dec‐3‐en‐2‐one	PROPN
eurjchem-864	74	12	(	(	PUNCT
eurjchem-864	74	13	9	9	NUM
eurjchem-864	74	14	)	)	PUNCT
eurjchem-864	74	15	to	to	ADP
eurjchem-864	74	16	a	a	DET
eurjchem-864	74	17	solution	solution	NOUN
eurjchem-864	74	18	of	of	ADP
eurjchem-864	74	19	compound	compound	NOUN
eurjchem-864	74	20	7	7	NUM
eurjchem-864	74	21	(	(	PUNCT
eurjchem-864	74	22	5	5	NUM
eurjchem-864	74	23	mmol	mmol	NOUN
eurjchem-864	74	24	)	)	PUNCT
eurjchem-864	74	25	and	and	CCONJ
eurjchem-864	74	26	triethyl	triethyl	PROPN
eurjchem-864	74	27	amine	amine	PROPN
eurjchem-864	74	28	(	(	PUNCT
eurjchem-864	74	29	5	5	NUM
eurjchem-864	74	30	mmol	mmol	NOUN
eurjchem-864	74	31	)	)	PUNCT
eurjchem-864	74	32	in	in	ADP
eurjchem-864	74	33	dichloromethane	dichloromethane	NOUN
eurjchem-864	74	34	(	(	PUNCT
eurjchem-864	74	35	20	20	NUM
eurjchem-864	74	36	ml	ml	NOUN
eurjchem-864	74	37	)	)	PUNCT
eurjchem-864	74	38	;	;	PUNCT
eurjchem-864	74	39	acyl	acyl	X
eurjchem-864	74	40	chloride	chloride	NOUN
eurjchem-864	74	41	(	(	PUNCT
eurjchem-864	74	42	8)	8)	NUM
eurjchem-864	74	43	(	(	PUNCT
eurjchem-864	74	44	5	5	NUM
eurjchem-864	74	45	mmol	mmol	NOUN
eurjchem-864	74	46	)	)	PUNCT
eurjchem-864	74	47	was	be	AUX
eurjchem-864	74	48	added	add	VERB
eurjchem-864	74	49	at	at	ADP
eurjchem-864	74	50	0	0	NUM
eurjchem-864	74	51	°	°	ADP
eurjchem-864	74	52	c	c	NOUN
eurjchem-864	74	53	and	and	CCONJ
eurjchem-864	74	54	stirred	stir	VERB
eurjchem-864	74	55	at	at	ADP
eurjchem-864	74	56	room	room	NOUN
eurjchem-864	74	57	temperature	temperature	NOUN
eurjchem-864	74	58	for	for	ADP
eurjchem-864	74	59	3‐4	3‐4	PROPN
eurjchem-864	74	60	h.	h.	PROPN
eurjchem-864	74	61	after	after	ADP
eurjchem-864	74	62	the	the	DET
eurjchem-864	74	63	completion	completion	NOUN
eurjchem-864	74	64	of	of	ADP
eurjchem-864	74	65	the	the	DET
eurjchem-864	74	66	reaction	reaction	NOUN
eurjchem-864	74	67	,	,	PUNCT
eurjchem-864	74	68	20	20	NUM
eurjchem-864	74	69	ml	ml	NOUN
eurjchem-864	74	70	of	of	ADP
eurjchem-864	74	71	water	water	NOUN
eurjchem-864	74	72	was	be	AUX
eurjchem-864	74	73	added	add	VERB
eurjchem-864	74	74	and	and	CCONJ
eurjchem-864	74	75	extracted	extract	VERB
eurjchem-864	74	76	the	the	DET
eurjchem-864	74	77	reaction	reaction	NOUN
eurjchem-864	74	78	mixture	mixture	NOUN
eurjchem-864	74	79	with	with	ADP
eurjchem-864	74	80	dichloro‐	dichloro‐	PROPN
eurjchem-864	74	81	methane	methane	NOUN
eurjchem-864	74	82	(	(	PUNCT
eurjchem-864	74	83	2	2	NUM
eurjchem-864	74	84	x	x	SYM
eurjchem-864	74	85	20	20	NUM
eurjchem-864	74	86	ml	ml	NOUN
eurjchem-864	74	87	)	)	PUNCT
eurjchem-864	74	88	.	.	PUNCT
eurjchem-864	75	1	the	the	DET
eurjchem-864	75	2	organic	organic	ADJ
eurjchem-864	75	3	layer	layer	NOUN
eurjchem-864	75	4	was	be	AUX
eurjchem-864	75	5	concentrated	concentrate	VERB
eurjchem-864	75	6	under	under	ADP
eurjchem-864	75	7	reduced	reduce	VERB
eurjchem-864	75	8	pressure	pressure	NOUN
eurjchem-864	75	9	to	to	PART
eurjchem-864	75	10	get	get	VERB
eurjchem-864	75	11	products	product	NOUN
eurjchem-864	75	12	9	9	NUM
eurjchem-864	75	13	(	(	PUNCT
eurjchem-864	75	14	table	table	NOUN
eurjchem-864	75	15	1	1	NUM
eurjchem-864	75	16	)	)	PUNCT
eurjchem-864	75	17	which	which	PRON
eurjchem-864	75	18	were	be	AUX
eurjchem-864	75	19	purified	purify	VERB
eurjchem-864	75	20	by	by	ADP
eurjchem-864	75	21	column	column	NOUN
eurjchem-864	75	22	chromatography	chromatography	NOUN
eurjchem-864	75	23	using	use	VERB
eurjchem-864	75	24	chcl3	chcl3	PROPN
eurjchem-864	75	25	:	:	PUNCT
eurjchem-864	75	26	meoh	meoh	PROPN
eurjchem-864	75	27	(	(	PUNCT
eurjchem-864	75	28	9:1	9:1	NUM
eurjchem-864	75	29	,	,	PUNCT
eurjchem-864	75	30	v	v	NOUN
eurjchem-864	75	31	:	:	PUNCT
eurjchem-864	75	32	v	v	NOUN
eurjchem-864	75	33	)	)	PUNCT
eurjchem-864	75	34	as	as	ADP
eurjchem-864	75	35	eluent	eluent	NOUN
eurjchem-864	75	36	(	(	PUNCT
eurjchem-864	75	37	scheme	scheme	NOUN
eurjchem-864	75	38	1	1	NUM
eurjchem-864	75	39	)	)	PUNCT
eurjchem-864	75	40	.	.	PUNCT
eurjchem-864	76	1	8‐(4‐chlorobenzoyl)‐4‐(4‐(6‐fluorobenzo[d]isoxazol‐3‐yl	8‐(4‐chlorobenzoyl)‐4‐(4‐(6‐fluorobenzo[d]isoxazol‐3‐yl	NUM
eurjchem-864	76	2	)	)	PUNCT
eurjchem-864	76	3	piperidine‐1‐carbonyl)‐3‐methyl‐1‐oxa‐8‐azaspiro[4.5]dec‐3‐en‐	piperidine‐1‐carbonyl)‐3‐methyl‐1‐oxa‐8‐azaspiro[4.5]dec‐3‐en‐	NUM
eurjchem-864	76	4	2‐one	2‐one	NUM
eurjchem-864	76	5	(	(	PUNCT
eurjchem-864	76	6	9a	9a	NOUN
eurjchem-864	76	7	):	):	PUNCT
eurjchem-864	76	8	colour	colour	NOUN
eurjchem-864	76	9	:	:	PUNCT
eurjchem-864	76	10	white	white	ADJ
eurjchem-864	76	11	.	.	PUNCT
eurjchem-864	77	1	yield	yield	NOUN
eurjchem-864	77	2	:	:	PUNCT
eurjchem-864	77	3	81	81	NUM
eurjchem-864	77	4	%	%	NOUN
eurjchem-864	77	5	(	(	PUNCT
eurjchem-864	77	6	2.23	2.23	NUM
eurjchem-864	77	7	g	g	NOUN
eurjchem-864	77	8	)	)	PUNCT
eurjchem-864	77	9	.	.	PUNCT
eurjchem-864	78	1	m.p	m.p	PROPN
eurjchem-864	78	2	.	.	PROPN
eurjchem-864	78	3	:	:	PUNCT
eurjchem-864	79	1	108‐110	108‐110	NUM
eurjchem-864	79	2	°	°	SYM
eurjchem-864	79	3	c	c	NOUN
eurjchem-864	79	4	.	.	PUNCT
eurjchem-864	80	1	ft‐ir	ft‐ir	NOUN
eurjchem-864	80	2	(	(	PUNCT
eurjchem-864	80	3	kbr	kbr	PROPN
eurjchem-864	80	4	,	,	PUNCT
eurjchem-864	80	5	cm‐1	cm‐1	PROPN
eurjchem-864	80	6	):	):	PUNCT
eurjchem-864	80	7	1660	1660	NUM
eurjchem-864	80	8	(	(	PUNCT
eurjchem-864	80	9	amide	amide	PROPN
eurjchem-864	80	10	co	co	NOUN
eurjchem-864	80	11	str	str	PROPN
eurjchem-864	80	12	.	.	PUNCT
eurjchem-864	80	13	)	)	PUNCT
eurjchem-864	80	14	,	,	PUNCT
eurjchem-864	80	15	1740	1740	NUM
eurjchem-864	80	16	(	(	PUNCT
eurjchem-864	80	17	ester	ester	NOUN
eurjchem-864	80	18	co	co	NOUN
eurjchem-864	80	19	str	str	PROPN
eurjchem-864	80	20	.	.	PUNCT
eurjchem-864	80	21	)	)	PUNCT
eurjchem-864	80	22	,	,	PUNCT
eurjchem-864	80	23	3045	3045	NUM
eurjchem-864	80	24	(	(	PUNCT
eurjchem-864	80	25	aromatic	aromatic	ADJ
eurjchem-864	80	26	ch	ch	NOUN
eurjchem-864	80	27	str	str	NOUN
eurjchem-864	80	28	.	.	PUNCT
eurjchem-864	80	29	)	)	PUNCT
eurjchem-864	80	30	.	.	PUNCT
eurjchem-864	81	1	1h	1h	NUM
eurjchem-864	81	2	nmr	nmr	NOUN
eurjchem-864	81	3	(	(	PUNCT
eurjchem-864	81	4	400	400	NUM
eurjchem-864	81	5	mhz	mhz	NOUN
eurjchem-864	81	6	,	,	PUNCT
eurjchem-864	81	7	cdcl3	cdcl3	PROPN
eurjchem-864	81	8	,	,	PUNCT
eurjchem-864	81	9	δ	δ	PROPN
eurjchem-864	81	10	,	,	PUNCT
eurjchem-864	81	11	ppm	ppm	NUM
eurjchem-864	81	12	):	):	PUNCT
eurjchem-864	81	13	8.08	8.08	NUM
eurjchem-864	81	14	(	(	PUNCT
eurjchem-864	81	15	d	d	PROPN
eurjchem-864	81	16	,	,	PUNCT
eurjchem-864	81	17	j	j	PROPN
eurjchem-864	81	18	=	=	SYM
eurjchem-864	81	19	7.8	7.8	NUM
eurjchem-864	81	20	hz	hz	NOUN
eurjchem-864	81	21	,	,	PUNCT
eurjchem-864	81	22	2h	2h	NUM
eurjchem-864	81	23	,	,	PUNCT
eurjchem-864	81	24	ar‐h	ar‐h	NOUN
eurjchem-864	81	25	)	)	PUNCT
eurjchem-864	81	26	,	,	PUNCT
eurjchem-864	81	27	7.75	7.75	NUM
eurjchem-864	81	28	(	(	PUNCT
eurjchem-864	81	29	d	d	PROPN
eurjchem-864	81	30	,	,	PUNCT
eurjchem-864	81	31	j	j	PROPN
eurjchem-864	81	32	=	=	PROPN
eurjchem-864	81	33	8.2	8.2	NUM
eurjchem-864	81	34	hz	hz	NOUN
eurjchem-864	81	35	,	,	PUNCT
eurjchem-864	81	36	2h	2h	NUM
eurjchem-864	81	37	,	,	PUNCT
eurjchem-864	81	38	ar‐	ar‐	PROPN
eurjchem-864	81	39	h	h	NOUN
eurjchem-864	81	40	)	)	PUNCT
eurjchem-864	81	41	,	,	PUNCT
eurjchem-864	81	42	7.61	7.61	NUM
eurjchem-864	81	43	(	(	PUNCT
eurjchem-864	81	44	d	d	PROPN
eurjchem-864	81	45	,	,	PUNCT
eurjchem-864	81	46	j	j	PROPN
eurjchem-864	81	47	=	=	SYM
eurjchem-864	81	48	7.2	7.2	NUM
eurjchem-864	81	49	hz	hz	NOUN
eurjchem-864	81	50	,	,	PUNCT
eurjchem-864	81	51	1h	1h	NUM
eurjchem-864	81	52	,	,	PUNCT
eurjchem-864	81	53	ar‐h	ar‐h	NOUN
eurjchem-864	81	54	)	)	PUNCT
eurjchem-864	81	55	,	,	PUNCT
eurjchem-864	81	56	7.29	7.29	NUM
eurjchem-864	81	57	(	(	PUNCT
eurjchem-864	81	58	d	d	PROPN
eurjchem-864	81	59	,	,	PUNCT
eurjchem-864	81	60	j	j	PROPN
eurjchem-864	82	1	=	=	SYM
eurjchem-864	82	2	7.2	7.2	NUM
eurjchem-864	82	3	hz	hz	NOUN
eurjchem-864	82	4	,	,	PUNCT
eurjchem-864	82	5	1h	1h	NUM
eurjchem-864	82	6	,	,	PUNCT
eurjchem-864	82	7	ar‐h	ar‐h	NOUN
eurjchem-864	82	8	)	)	PUNCT
eurjchem-864	82	9	,	,	PUNCT
eurjchem-864	82	10	7.03	7.03	NUM
eurjchem-864	82	11	(	(	PUNCT
eurjchem-864	82	12	s	s	PROPN
eurjchem-864	82	13	,	,	PUNCT
eurjchem-864	82	14	1h	1h	NUM
eurjchem-864	82	15	,	,	PUNCT
eurjchem-864	82	16	ar‐h	ar‐h	NOUN
eurjchem-864	82	17	)	)	PUNCT
eurjchem-864	82	18	,	,	PUNCT
eurjchem-864	82	19	3.29‐3.39	3.29‐3.39	NUM
eurjchem-864	82	20	(	(	PUNCT
eurjchem-864	82	21	m	m	PROPN
eurjchem-864	82	22	,	,	PUNCT
eurjchem-864	82	23	8h	8h	NUM
eurjchem-864	82	24	,	,	PUNCT
eurjchem-864	82	25	ch2	ch2	PROPN
eurjchem-864	82	26	)	)	PUNCT
eurjchem-864	82	27	,	,	PUNCT
eurjchem-864	82	28	2.72	2.72	NUM
eurjchem-864	82	29	(	(	PUNCT
eurjchem-864	82	30	m	m	PROPN
eurjchem-864	82	31	,	,	PUNCT
eurjchem-864	82	32	1h	1h	NUM
eurjchem-864	82	33	,	,	PUNCT
eurjchem-864	82	34	ch	ch	NOUN
eurjchem-864	82	35	)	)	PUNCT
eurjchem-864	82	36	,	,	PUNCT
eurjchem-864	82	37	2.52	2.52	NUM
eurjchem-864	82	38	(	(	PUNCT
eurjchem-864	82	39	s	s	PROPN
eurjchem-864	82	40	,	,	PUNCT
eurjchem-864	82	41	3h	3h	NUM
eurjchem-864	82	42	,	,	PUNCT
eurjchem-864	82	43	ch3	ch3	PROPN
eurjchem-864	82	44	)	)	PUNCT
eurjchem-864	82	45	,	,	PUNCT
eurjchem-864	82	46	1.60‐1.90	1.60‐1.90	NUM
eurjchem-864	82	47	(	(	PUNCT
eurjchem-864	82	48	m	m	PROPN
eurjchem-864	82	49	,	,	PUNCT
eurjchem-864	82	50	8h	8h	NUM
eurjchem-864	82	51	,	,	PUNCT
eurjchem-864	82	52	ch2	ch2	PROPN
eurjchem-864	82	53	)	)	PUNCT
eurjchem-864	82	54	.	.	PUNCT
eurjchem-864	83	1	anal	anal	PROPN
eurjchem-864	83	2	.	.	PUNCT
eurjchem-864	83	3	calcd	calcd	NOUN
eurjchem-864	83	4	.	.	PUNCT
eurjchem-864	84	1	for	for	ADP
eurjchem-864	84	2	c29h27clfn3o5	c29h27clfn3o5	ADV
eurjchem-864	84	3	:	:	PUNCT
eurjchem-864	84	4	c	c	X
eurjchem-864	84	5	,	,	PUNCT
eurjchem-864	84	6	63.10	63.10	NUM
eurjchem-864	84	7	;	;	PUNCT
eurjchem-864	84	8	h	h	X
eurjchem-864	84	9	,	,	PUNCT
eurjchem-864	84	10	4.93	4.93	NUM
eurjchem-864	84	11	;	;	PUNCT
eurjchem-864	84	12	n	n	CCONJ
eurjchem-864	84	13	,	,	PUNCT
eurjchem-864	84	14	7.61	7.61	NUM
eurjchem-864	84	15	.	.	PUNCT
eurjchem-864	84	16	found	find	VERB
eurjchem-864	84	17	:	:	PUNCT
eurjchem-864	85	1	c	c	X
eurjchem-864	85	2	,	,	PUNCT
eurjchem-864	85	3	63.15	63.15	NUM
eurjchem-864	85	4	;	;	PUNCT
eurjchem-864	86	1	h	h	NOUN
eurjchem-864	86	2	,	,	PUNCT
eurjchem-864	86	3	4.96	4.96	NUM
eurjchem-864	86	4	;	;	PUNCT
eurjchem-864	86	5	n	n	CCONJ
eurjchem-864	86	6	,	,	PUNCT
eurjchem-864	86	7	7.63	7.63	NUM
eurjchem-864	86	8	%	%	NOUN
eurjchem-864	86	9	.	.	PUNCT
eurjchem-864	87	1	ms	ms	NOUN
eurjchem-864	87	2	(	(	PUNCT
eurjchem-864	87	3	m	m	PROPN
eurjchem-864	87	4	/	/	SYM
eurjchem-864	87	5	z	z	NOUN
eurjchem-864	87	6	):	):	PUNCT
eurjchem-864	87	7	553	553	NUM
eurjchem-864	87	8	(	(	PUNCT
eurjchem-864	87	9	m+1	m+1	NUM
eurjchem-864	87	10	)	)	PUNCT
eurjchem-864	87	11	.	.	PUNCT
eurjchem-864	88	1	8‐(4‐(tert‐butyl)benzoyl)‐4‐(4‐(6‐fluorobenzo[d]isoxazol‐3‐	8‐(4‐(tert‐butyl)benzoyl)‐4‐(4‐(6‐fluorobenzo[d]isoxazol‐3‐	VERB
eurjchem-864	88	2	yl)piperidine‐1‐carbonyl)‐3‐methyl‐1‐oxa‐8‐azaspiro[4.5]dec‐3‐	yl)piperidine‐1‐carbonyl)‐3‐methyl‐1‐oxa‐8‐azaspiro[4.5]dec‐3‐	PRON
eurjchem-864	88	3	en‐2‐one	en‐2‐one	NOUN
eurjchem-864	88	4	(	(	PUNCT
eurjchem-864	88	5	9b	9b	NUM
eurjchem-864	88	6	):	):	PUNCT
eurjchem-864	88	7	colour	colour	NOUN
eurjchem-864	88	8	:	:	PUNCT
eurjchem-864	88	9	white	white	ADJ
eurjchem-864	88	10	.	.	PUNCT
eurjchem-864	89	1	yield	yield	NOUN
eurjchem-864	89	2	:	:	PUNCT
eurjchem-864	89	3	76	76	NUM
eurjchem-864	89	4	%	%	NOUN
eurjchem-864	89	5	(	(	PUNCT
eurjchem-864	89	6	2.17	2.17	NUM
eurjchem-864	89	7	g	g	NOUN
eurjchem-864	89	8	)	)	PUNCT
eurjchem-864	89	9	.	.	PUNCT
eurjchem-864	90	1	m.p	m.p	PROPN
eurjchem-864	90	2	.	.	PROPN
eurjchem-864	90	3	:	:	PUNCT
eurjchem-864	91	1	108‐	108‐	NUM
eurjchem-864	91	2	110	110	NUM
eurjchem-864	91	3	°	°	SYM
eurjchem-864	91	4	c	c	X
eurjchem-864	91	5	.	.	PUNCT
eurjchem-864	92	1	ft‐ir	ft‐ir	NOUN
eurjchem-864	92	2	(	(	PUNCT
eurjchem-864	92	3	kbr	kbr	PROPN
eurjchem-864	92	4	,	,	PUNCT
eurjchem-864	92	5	cm‐1	cm‐1	PROPN
eurjchem-864	92	6	):	):	PUNCT
eurjchem-864	92	7	1671	1671	NUM
eurjchem-864	92	8	(	(	PUNCT
eurjchem-864	92	9	amide	amide	PROPN
eurjchem-864	92	10	co	co	NOUN
eurjchem-864	92	11	str	str	PROPN
eurjchem-864	92	12	.	.	PUNCT
eurjchem-864	92	13	)	)	PUNCT
eurjchem-864	92	14	,	,	PUNCT
eurjchem-864	92	15	1749	1749	NUM
eurjchem-864	92	16	(	(	PUNCT
eurjchem-864	92	17	ester	ester	NOUN
eurjchem-864	92	18	co	co	NOUN
eurjchem-864	92	19	str	str	PROPN
eurjchem-864	92	20	.	.	PUNCT
eurjchem-864	92	21	)	)	PUNCT
eurjchem-864	92	22	,	,	PUNCT
eurjchem-864	92	23	3039	3039	NUM
eurjchem-864	92	24	(	(	PUNCT
eurjchem-864	92	25	aromatic	aromatic	ADJ
eurjchem-864	92	26	ch	ch	NOUN
eurjchem-864	92	27	str	str	NOUN
eurjchem-864	92	28	.	.	PUNCT
eurjchem-864	92	29	)	)	PUNCT
eurjchem-864	92	30	.	.	PUNCT
eurjchem-864	93	1	1h	1h	NUM
eurjchem-864	93	2	nmr	nmr	NOUN
eurjchem-864	93	3	(	(	PUNCT
eurjchem-864	93	4	400	400	NUM
eurjchem-864	93	5	mhz	mhz	NOUN
eurjchem-864	93	6	,	,	PUNCT
eurjchem-864	93	7	cdcl3	cdcl3	PROPN
eurjchem-864	93	8	,	,	PUNCT
eurjchem-864	93	9	δ	δ	PROPN
eurjchem-864	93	10	,	,	PUNCT
eurjchem-864	93	11	404	404	NOUN
eurjchem-864	93	12	shivaprasad	shivaprasad	ADJ
eurjchem-864	93	13	et	et	PROPN
eurjchem-864	93	14	al	al	PROPN
eurjchem-864	93	15	.	.	PUNCT
eurjchem-864	93	16	/	/	SYM
eurjchem-864	93	17	european	european	PROPN
eurjchem-864	93	18	journal	journal	PROPN
eurjchem-864	93	19	of	of	ADP
eurjchem-864	93	20	chemistry	chemistry	NOUN
eurjchem-864	93	21	4	4	NUM
eurjchem-864	93	22	(	(	PUNCT
eurjchem-864	93	23	4	4	NUM
eurjchem-864	93	24	)	)	PUNCT
eurjchem-864	93	25	(	(	PUNCT
eurjchem-864	93	26	2013	2013	NUM
eurjchem-864	93	27	)	)	PUNCT
eurjchem-864	93	28	402‐407	402‐407	PROPN
eurjchem-864	93	29	ppm	ppm	NOUN
eurjchem-864	93	30	):	):	PUNCT
eurjchem-864	93	31	7.95	7.95	NUM
eurjchem-864	93	32	(	(	PUNCT
eurjchem-864	93	33	d	d	NOUN
eurjchem-864	93	34	,	,	PUNCT
eurjchem-864	93	35	j	j	PROPN
eurjchem-864	93	36	=	=	SYM
eurjchem-864	93	37	7.8	7.8	NUM
eurjchem-864	93	38	hz	hz	NOUN
eurjchem-864	93	39	,	,	PUNCT
eurjchem-864	93	40	2h	2h	NUM
eurjchem-864	93	41	,	,	PUNCT
eurjchem-864	93	42	ar‐h	ar‐h	NOUN
eurjchem-864	93	43	)	)	PUNCT
eurjchem-864	93	44	,	,	PUNCT
eurjchem-864	93	45	7.55	7.55	NUM
eurjchem-864	93	46	(	(	PUNCT
eurjchem-864	93	47	d	d	PROPN
eurjchem-864	93	48	,	,	PUNCT
eurjchem-864	93	49	j	j	PROPN
eurjchem-864	93	50	=	=	SYM
eurjchem-864	93	51	7.2	7.2	NUM
eurjchem-864	93	52	hz	hz	NOUN
eurjchem-864	93	53	,	,	PUNCT
eurjchem-864	93	54	1h	1h	NUM
eurjchem-864	93	55	,	,	PUNCT
eurjchem-864	93	56	ar‐	ar‐	PROPN
eurjchem-864	93	57	h	h	NOUN
eurjchem-864	93	58	)	)	PUNCT
eurjchem-864	93	59	,	,	PUNCT
eurjchem-864	93	60	7.47	7.47	NUM
eurjchem-864	93	61	(	(	PUNCT
eurjchem-864	93	62	d	d	PROPN
eurjchem-864	93	63	,	,	PUNCT
eurjchem-864	93	64	j	j	PROPN
eurjchem-864	93	65	=	=	SYM
eurjchem-864	93	66	7.8	7.8	NUM
eurjchem-864	93	67	hz	hz	NOUN
eurjchem-864	93	68	,	,	PUNCT
eurjchem-864	93	69	2h	2h	NUM
eurjchem-864	93	70	,	,	PUNCT
eurjchem-864	93	71	ar‐h	ar‐h	NOUN
eurjchem-864	93	72	)	)	PUNCT
eurjchem-864	93	73	,	,	PUNCT
eurjchem-864	93	74	7.24	7.24	NUM
eurjchem-864	93	75	(	(	PUNCT
eurjchem-864	93	76	d	d	PROPN
eurjchem-864	93	77	,	,	PUNCT
eurjchem-864	93	78	j	j	PROPN
eurjchem-864	93	79	=	=	SYM
eurjchem-864	93	80	7.2	7.2	NUM
eurjchem-864	93	81	hz	hz	NOUN
eurjchem-864	93	82	,	,	PUNCT
eurjchem-864	93	83	1h	1h	NUM
eurjchem-864	93	84	,	,	PUNCT
eurjchem-864	93	85	ar‐h	ar‐h	NOUN
eurjchem-864	93	86	)	)	PUNCT
eurjchem-864	93	87	,	,	PUNCT
eurjchem-864	93	88	6.97	6.97	NUM
eurjchem-864	93	89	(	(	PUNCT
eurjchem-864	93	90	s	s	PROPN
eurjchem-864	93	91	,	,	PUNCT
eurjchem-864	93	92	1h	1h	NUM
eurjchem-864	93	93	,	,	PUNCT
eurjchem-864	93	94	ar‐h	ar‐h	NOUN
eurjchem-864	93	95	)	)	PUNCT
eurjchem-864	93	96	,	,	PUNCT
eurjchem-864	93	97	3.28‐3.36	3.28‐3.36	NUM
eurjchem-864	93	98	(	(	PUNCT
eurjchem-864	93	99	m	m	PROPN
eurjchem-864	93	100	,	,	PUNCT
eurjchem-864	93	101	8h	8h	NUM
eurjchem-864	93	102	,	,	PUNCT
eurjchem-864	93	103	ch2	ch2	PROPN
eurjchem-864	93	104	)	)	PUNCT
eurjchem-864	93	105	,	,	PUNCT
eurjchem-864	93	106	2.71	2.71	NUM
eurjchem-864	93	107	(	(	PUNCT
eurjchem-864	93	108	m	m	PROPN
eurjchem-864	93	109	,	,	PUNCT
eurjchem-864	93	110	1h	1h	NUM
eurjchem-864	93	111	,	,	PUNCT
eurjchem-864	93	112	ch	ch	NOUN
eurjchem-864	93	113	)	)	PUNCT
eurjchem-864	93	114	,	,	PUNCT
eurjchem-864	93	115	2.53	2.53	NUM
eurjchem-864	93	116	(	(	PUNCT
eurjchem-864	93	117	s	s	PROPN
eurjchem-864	93	118	,	,	PUNCT
eurjchem-864	93	119	3h	3h	NUM
eurjchem-864	93	120	,	,	PUNCT
eurjchem-864	93	121	ch3	ch3	PROPN
eurjchem-864	93	122	)	)	PUNCT
eurjchem-864	93	123	,	,	PUNCT
eurjchem-864	93	124	1.60‐1.91	1.60‐1.91	NUM
eurjchem-864	93	125	(	(	PUNCT
eurjchem-864	93	126	m	m	PROPN
eurjchem-864	93	127	,	,	PUNCT
eurjchem-864	93	128	8h	8h	NUM
eurjchem-864	93	129	,	,	PUNCT
eurjchem-864	93	130	ch2	ch2	PROPN
eurjchem-864	93	131	)	)	PUNCT
eurjchem-864	93	132	,	,	PUNCT
eurjchem-864	93	133	1.35	1.35	NUM
eurjchem-864	93	134	(	(	PUNCT
eurjchem-864	93	135	s	s	PROPN
eurjchem-864	93	136	,	,	PUNCT
eurjchem-864	93	137	9h	9h	NUM
eurjchem-864	93	138	,	,	PUNCT
eurjchem-864	93	139	cme3	cme3	PROPN
eurjchem-864	93	140	)	)	PUNCT
eurjchem-864	93	141	.	.	PUNCT
eurjchem-864	94	1	anal	anal	PROPN
eurjchem-864	94	2	.	.	PUNCT
eurjchem-864	94	3	calcd	calcd	NOUN
eurjchem-864	94	4	.	.	PUNCT
eurjchem-864	95	1	for	for	ADP
eurjchem-864	95	2	c33h36fn3o5	c33h36fn3o5	NOUN
eurjchem-864	95	3	:	:	PUNCT
eurjchem-864	95	4	c	c	X
eurjchem-864	95	5	,	,	PUNCT
eurjchem-864	95	6	69.09	69.09	NUM
eurjchem-864	95	7	;	;	PUNCT
eurjchem-864	95	8	h	h	NOUN
eurjchem-864	95	9	,	,	PUNCT
eurjchem-864	95	10	6.33	6.33	NUM
eurjchem-864	95	11	;	;	PUNCT
eurjchem-864	95	12	n	n	CCONJ
eurjchem-864	95	13	,	,	PUNCT
eurjchem-864	95	14	7.32	7.32	NUM
eurjchem-864	95	15	.	.	PUNCT
eurjchem-864	95	16	found	find	VERB
eurjchem-864	95	17	:	:	PUNCT
eurjchem-864	96	1	c	c	X
eurjchem-864	96	2	,	,	PUNCT
eurjchem-864	96	3	69.12	69.12	NUM
eurjchem-864	96	4	;	;	PUNCT
eurjchem-864	96	5	h	h	NOUN
eurjchem-864	96	6	,	,	PUNCT
eurjchem-864	96	7	6.39	6.39	NUM
eurjchem-864	96	8	;	;	PUNCT
eurjchem-864	96	9	n	n	CCONJ
eurjchem-864	96	10	,	,	PUNCT
eurjchem-864	96	11	7.36	7.36	NUM
eurjchem-864	96	12	%	%	NOUN
eurjchem-864	96	13	.	.	PUNCT
eurjchem-864	97	1	ms	ms	NOUN
eurjchem-864	97	2	(	(	PUNCT
eurjchem-864	97	3	m	m	PROPN
eurjchem-864	97	4	/	/	SYM
eurjchem-864	97	5	z	z	NOUN
eurjchem-864	97	6	):	):	PUNCT
eurjchem-864	97	7	574	574	NUM
eurjchem-864	97	8	(	(	PUNCT
eurjchem-864	97	9	m+1	m+1	NUM
eurjchem-864	97	10	)	)	PUNCT
eurjchem-864	97	11	.	.	PUNCT
eurjchem-864	98	1	8‐(2,4‐dichlorobenzoyl)‐4‐(4‐(6‐fluorobenzo[d]isoxazol‐3‐yl	8‐(2,4‐dichlorobenzoyl)‐4‐(4‐(6‐fluorobenzo[d]isoxazol‐3‐yl	NUM
eurjchem-864	98	2	)	)	PUNCT
eurjchem-864	98	3	piperidine‐1‐carbonyl)‐3‐methyl‐1‐oxa‐8‐azaspiro[4.5]dec‐3‐en‐	piperidine‐1‐carbonyl)‐3‐methyl‐1‐oxa‐8‐azaspiro[4.5]dec‐3‐en‐	PART
eurjchem-864	98	4	2‐one	2‐one	NUM
eurjchem-864	98	5	(	(	PUNCT
eurjchem-864	98	6	9c	9c	NUM
eurjchem-864	98	7	):	):	PUNCT
eurjchem-864	98	8	colour	colour	NOUN
eurjchem-864	98	9	:	:	PUNCT
eurjchem-864	98	10	white	white	ADJ
eurjchem-864	98	11	.	.	PUNCT
eurjchem-864	98	12	yield	yield	NOUN
eurjchem-864	98	13	:	:	PUNCT
eurjchem-864	98	14	72	72	NUM
eurjchem-864	98	15	%	%	NOUN
eurjchem-864	98	16	(	(	PUNCT
eurjchem-864	98	17	2.10	2.10	NUM
eurjchem-864	98	18	g	g	NOUN
eurjchem-864	98	19	)	)	PUNCT
eurjchem-864	98	20	.	.	PUNCT
eurjchem-864	99	1	m.p	m.p	PROPN
eurjchem-864	99	2	.	.	PROPN
eurjchem-864	99	3	:	:	PUNCT
eurjchem-864	100	1	114‐116	114‐116	PROPN
eurjchem-864	100	2	°	°	NOUN
eurjchem-864	100	3	c	c	X
eurjchem-864	100	4	.	.	PUNCT
eurjchem-864	101	1	ft‐ir	ft‐ir	NOUN
eurjchem-864	101	2	(	(	PUNCT
eurjchem-864	101	3	kbr	kbr	PROPN
eurjchem-864	101	4	,	,	PUNCT
eurjchem-864	101	5	cm‐1	cm‐1	PROPN
eurjchem-864	101	6	):	):	PUNCT
eurjchem-864	101	7	1655	1655	NUM
eurjchem-864	101	8	(	(	PUNCT
eurjchem-864	101	9	amide	amide	PROPN
eurjchem-864	101	10	co	co	NOUN
eurjchem-864	101	11	str	str	PROPN
eurjchem-864	101	12	.	.	PUNCT
eurjchem-864	101	13	)	)	PUNCT
eurjchem-864	101	14	,	,	PUNCT
eurjchem-864	101	15	1756	1756	NUM
eurjchem-864	101	16	(	(	PUNCT
eurjchem-864	101	17	ester	ester	NOUN
eurjchem-864	101	18	co	co	NOUN
eurjchem-864	101	19	str	str	PROPN
eurjchem-864	101	20	.	.	PUNCT
eurjchem-864	101	21	)	)	PUNCT
eurjchem-864	101	22	,	,	PUNCT
eurjchem-864	101	23	3049	3049	NUM
eurjchem-864	101	24	(	(	PUNCT
eurjchem-864	101	25	aromatic	aromatic	ADJ
eurjchem-864	101	26	ch	ch	NOUN
eurjchem-864	101	27	str	str	NOUN
eurjchem-864	101	28	.	.	PUNCT
eurjchem-864	101	29	)	)	PUNCT
eurjchem-864	101	30	.	.	PUNCT
eurjchem-864	102	1	1h	1h	NUM
eurjchem-864	102	2	nmr	nmr	NOUN
eurjchem-864	102	3	(	(	PUNCT
eurjchem-864	102	4	400	400	NUM
eurjchem-864	102	5	mhz	mhz	NOUN
eurjchem-864	102	6	,	,	PUNCT
eurjchem-864	102	7	cdcl3	cdcl3	PROPN
eurjchem-864	102	8	,	,	PUNCT
eurjchem-864	102	9	δ	δ	PROPN
eurjchem-864	102	10	,	,	PUNCT
eurjchem-864	102	11	ppm	ppm	NOUN
eurjchem-864	102	12	):	):	PUNCT
eurjchem-864	102	13	7.75	7.75	NUM
eurjchem-864	102	14	(	(	PUNCT
eurjchem-864	102	15	s	s	PROPN
eurjchem-864	102	16	,	,	PUNCT
eurjchem-864	102	17	1h	1h	NUM
eurjchem-864	102	18	,	,	PUNCT
eurjchem-864	102	19	ar‐h	ar‐h	NOUN
eurjchem-864	102	20	)	)	PUNCT
eurjchem-864	102	21	,	,	PUNCT
eurjchem-864	102	22	7.49‐7.55	7.49‐7.55	NUM
eurjchem-864	102	23	(	(	PUNCT
eurjchem-864	102	24	m	m	PROPN
eurjchem-864	102	25	,	,	PUNCT
eurjchem-864	102	26	3h	3h	NUM
eurjchem-864	102	27	,	,	PUNCT
eurjchem-864	102	28	ar‐h	ar‐h	NOUN
eurjchem-864	102	29	)	)	PUNCT
eurjchem-864	102	30	,	,	PUNCT
eurjchem-864	102	31	7.26	7.26	NUM
eurjchem-864	102	32	(	(	PUNCT
eurjchem-864	102	33	d	d	PROPN
eurjchem-864	102	34	,	,	PUNCT
eurjchem-864	102	35	j	j	PROPN
eurjchem-864	102	36	=	=	SYM
eurjchem-864	102	37	7.8	7.8	NUM
eurjchem-864	102	38	hz	hz	NOUN
eurjchem-864	102	39	,	,	PUNCT
eurjchem-864	102	40	1h	1h	NUM
eurjchem-864	102	41	,	,	PUNCT
eurjchem-864	102	42	ar‐h	ar‐h	NOUN
eurjchem-864	102	43	)	)	PUNCT
eurjchem-864	102	44	,	,	PUNCT
eurjchem-864	102	45	7.02	7.02	NUM
eurjchem-864	102	46	(	(	PUNCT
eurjchem-864	102	47	s	s	PROPN
eurjchem-864	102	48	,	,	PUNCT
eurjchem-864	102	49	1h	1h	NUM
eurjchem-864	102	50	,	,	PUNCT
eurjchem-864	102	51	ar‐h	ar‐h	NOUN
eurjchem-864	102	52	)	)	PUNCT
eurjchem-864	102	53	,	,	PUNCT
eurjchem-864	102	54	3.27‐3.35	3.27‐3.35	NUM
eurjchem-864	102	55	(	(	PUNCT
eurjchem-864	102	56	m	m	PROPN
eurjchem-864	102	57	,	,	PUNCT
eurjchem-864	102	58	8h	8h	NUM
eurjchem-864	102	59	,	,	PUNCT
eurjchem-864	102	60	ch2	ch2	PROPN
eurjchem-864	102	61	)	)	PUNCT
eurjchem-864	102	62	,	,	PUNCT
eurjchem-864	102	63	2.72	2.72	NUM
eurjchem-864	102	64	(	(	PUNCT
eurjchem-864	102	65	m	m	PROPN
eurjchem-864	102	66	,	,	PUNCT
eurjchem-864	102	67	1h	1h	NUM
eurjchem-864	102	68	,	,	PUNCT
eurjchem-864	102	69	ch	ch	NOUN
eurjchem-864	102	70	)	)	PUNCT
eurjchem-864	102	71	,	,	PUNCT
eurjchem-864	102	72	2.50	2.50	NUM
eurjchem-864	102	73	(	(	PUNCT
eurjchem-864	102	74	s	s	PROPN
eurjchem-864	102	75	,	,	PUNCT
eurjchem-864	102	76	3h	3h	NUM
eurjchem-864	102	77	,	,	PUNCT
eurjchem-864	102	78	ch3	ch3	PROPN
eurjchem-864	102	79	)	)	PUNCT
eurjchem-864	102	80	,	,	PUNCT
eurjchem-864	102	81	1.62‐1.88	1.62‐1.88	NUM
eurjchem-864	102	82	(	(	PUNCT
eurjchem-864	102	83	m	m	PROPN
eurjchem-864	102	84	,	,	PUNCT
eurjchem-864	102	85	8h	8h	NUM
eurjchem-864	102	86	,	,	PUNCT
eurjchem-864	102	87	ch2	ch2	PROPN
eurjchem-864	102	88	)	)	PUNCT
eurjchem-864	102	89	.	.	PUNCT
eurjchem-864	103	1	anal	anal	PROPN
eurjchem-864	103	2	.	.	PUNCT
eurjchem-864	103	3	calcd	calcd	NOUN
eurjchem-864	103	4	.	.	PUNCT
eurjchem-864	104	1	for	for	ADP
eurjchem-864	104	2	c29h26cl2fn3o5	c29h26cl2fn3o5	ADV
eurjchem-864	104	3	:	:	PUNCT
eurjchem-864	104	4	c	c	X
eurjchem-864	104	5	,	,	PUNCT
eurjchem-864	104	6	59.39	59.39	NUM
eurjchem-864	104	7	;	;	PUNCT
eurjchem-864	104	8	h	h	X
eurjchem-864	104	9	,	,	PUNCT
eurjchem-864	104	10	4.47	4.47	NUM
eurjchem-864	104	11	;	;	PUNCT
eurjchem-864	104	12	n	n	CCONJ
eurjchem-864	104	13	,	,	PUNCT
eurjchem-864	104	14	7.17	7.17	NUM
eurjchem-864	104	15	.	.	PUNCT
eurjchem-864	104	16	found	find	VERB
eurjchem-864	104	17	:	:	PUNCT
eurjchem-864	105	1	c	c	X
eurjchem-864	105	2	,	,	PUNCT
eurjchem-864	105	3	59.45	59.45	NUM
eurjchem-864	105	4	;	;	PUNCT
eurjchem-864	105	5	h	h	X
eurjchem-864	105	6	,	,	PUNCT
eurjchem-864	105	7	4.52	4.52	NUM
eurjchem-864	105	8	;	;	PUNCT
eurjchem-864	105	9	n	n	CCONJ
eurjchem-864	105	10	,	,	PUNCT
eurjchem-864	105	11	7.25	7.25	NUM
eurjchem-864	105	12	%	%	NOUN
eurjchem-864	105	13	.	.	PUNCT
eurjchem-864	106	1	ms	ms	NOUN
eurjchem-864	106	2	(	(	PUNCT
eurjchem-864	106	3	m	m	PROPN
eurjchem-864	106	4	/	/	SYM
eurjchem-864	106	5	z	z	NOUN
eurjchem-864	106	6	):	):	PUNCT
eurjchem-864	106	7	587	587	NUM
eurjchem-864	106	8	(	(	PUNCT
eurjchem-864	106	9	m+1	m+1	NUM
eurjchem-864	106	10	)	)	PUNCT
eurjchem-864	106	11	.	.	PUNCT
eurjchem-864	107	1	8‐(3‐bromobenzoyl)‐4‐(4‐(6‐fluorobenzo[d]isoxazol‐3‐yl	8‐(3‐bromobenzoyl)‐4‐(4‐(6‐fluorobenzo[d]isoxazol‐3‐yl	NUM
eurjchem-864	107	2	)	)	PUNCT
eurjchem-864	107	3	piperidine‐1‐carbonyl)‐3‐methyl‐1‐oxa‐8‐azaspiro[4.5]dec‐3‐en‐	piperidine‐1‐carbonyl)‐3‐methyl‐1‐oxa‐8‐azaspiro[4.5]dec‐3‐en‐	PART
eurjchem-864	107	4	2‐one	2‐one	NUM
eurjchem-864	107	5	(	(	PUNCT
eurjchem-864	107	6	9d	9d	NUM
eurjchem-864	107	7	):	):	PUNCT
eurjchem-864	107	8	colour	colour	NOUN
eurjchem-864	107	9	:	:	PUNCT
eurjchem-864	107	10	white	white	ADJ
eurjchem-864	107	11	.	.	PUNCT
eurjchem-864	108	1	yield	yield	NOUN
eurjchem-864	108	2	:	:	PUNCT
eurjchem-864	108	3	83	83	NUM
eurjchem-864	108	4	%	%	NOUN
eurjchem-864	108	5	(	(	PUNCT
eurjchem-864	108	6	2.47	2.47	NUM
eurjchem-864	108	7	g	g	NOUN
eurjchem-864	108	8	)	)	PUNCT
eurjchem-864	108	9	.	.	PUNCT
eurjchem-864	109	1	m.p	m.p	PROPN
eurjchem-864	109	2	.	.	PROPN
eurjchem-864	109	3	:	:	PUNCT
eurjchem-864	110	1	128‐130	128‐130	PROPN
eurjchem-864	110	2	°	°	PROPN
eurjchem-864	110	3	c	c	PROPN
eurjchem-864	110	4	.	.	PUNCT
eurjchem-864	111	1	ft‐ir	ft‐ir	NOUN
eurjchem-864	111	2	(	(	PUNCT
eurjchem-864	111	3	kbr	kbr	PROPN
eurjchem-864	111	4	,	,	PUNCT
eurjchem-864	111	5	cm‐1	cm‐1	PROPN
eurjchem-864	111	6	):	):	PUNCT
eurjchem-864	111	7	1659	1659	NUM
eurjchem-864	111	8	(	(	PUNCT
eurjchem-864	111	9	amide	amide	PROPN
eurjchem-864	111	10	co	co	NOUN
eurjchem-864	111	11	str	str	PROPN
eurjchem-864	111	12	.	.	PUNCT
eurjchem-864	111	13	)	)	PUNCT
eurjchem-864	111	14	,	,	PUNCT
eurjchem-864	111	15	1765	1765	NUM
eurjchem-864	111	16	(	(	PUNCT
eurjchem-864	111	17	ester	ester	NOUN
eurjchem-864	111	18	co	co	NOUN
eurjchem-864	111	19	str	str	PROPN
eurjchem-864	111	20	.	.	PUNCT
eurjchem-864	111	21	)	)	PUNCT
eurjchem-864	111	22	,	,	PUNCT
eurjchem-864	111	23	3055	3055	NUM
eurjchem-864	111	24	(	(	PUNCT
eurjchem-864	111	25	aromatic	aromatic	ADJ
eurjchem-864	111	26	ch	ch	NOUN
eurjchem-864	111	27	str	str	NOUN
eurjchem-864	111	28	.	.	PUNCT
eurjchem-864	111	29	)	)	PUNCT
eurjchem-864	111	30	.	.	PUNCT
eurjchem-864	112	1	1h	1h	NUM
eurjchem-864	112	2	nmr	nmr	NOUN
eurjchem-864	112	3	(	(	PUNCT
eurjchem-864	112	4	400	400	NUM
eurjchem-864	112	5	mhz	mhz	NOUN
eurjchem-864	112	6	,	,	PUNCT
eurjchem-864	112	7	cdcl3	cdcl3	PROPN
eurjchem-864	112	8	,	,	PUNCT
eurjchem-864	112	9	δ	δ	PROPN
eurjchem-864	112	10	,	,	PUNCT
eurjchem-864	112	11	ppm	ppm	NOUN
eurjchem-864	112	12	):	):	PUNCT
eurjchem-864	112	13	8.25	8.25	NUM
eurjchem-864	112	14	(	(	PUNCT
eurjchem-864	112	15	s	s	PROPN
eurjchem-864	112	16	,	,	PUNCT
eurjchem-864	112	17	1h	1h	NUM
eurjchem-864	112	18	,	,	PUNCT
eurjchem-864	112	19	ar‐h	ar‐h	NOUN
eurjchem-864	112	20	)	)	PUNCT
eurjchem-864	112	21	,	,	PUNCT
eurjchem-864	112	22	8.05	8.05	NUM
eurjchem-864	112	23	(	(	PUNCT
eurjchem-864	112	24	d	d	PROPN
eurjchem-864	112	25	,	,	PUNCT
eurjchem-864	112	26	j	j	PROPN
eurjchem-864	112	27	=	=	SYM
eurjchem-864	112	28	7.8	7.8	NUM
eurjchem-864	112	29	hz	hz	NOUN
eurjchem-864	112	30	,	,	PUNCT
eurjchem-864	112	31	1h	1h	NUM
eurjchem-864	112	32	,	,	PUNCT
eurjchem-864	112	33	ar‐h	ar‐h	NOUN
eurjchem-864	112	34	)	)	PUNCT
eurjchem-864	112	35	,	,	PUNCT
eurjchem-864	112	36	7.98	7.98	NUM
eurjchem-864	112	37	(	(	PUNCT
eurjchem-864	112	38	d	d	NOUN
eurjchem-864	112	39	,	,	PUNCT
eurjchem-864	112	40	j	j	PROPN
eurjchem-864	112	41	=	=	SYM
eurjchem-864	112	42	7.6	7.6	NUM
eurjchem-864	112	43	hz	hz	NOUN
eurjchem-864	112	44	,	,	PUNCT
eurjchem-864	112	45	1h	1h	NUM
eurjchem-864	112	46	,	,	PUNCT
eurjchem-864	112	47	ar‐h	ar‐h	NOUN
eurjchem-864	112	48	)	)	PUNCT
eurjchem-864	112	49	,	,	PUNCT
eurjchem-864	112	50	7.55	7.55	NUM
eurjchem-864	112	51	(	(	PUNCT
eurjchem-864	112	52	m	m	PROPN
eurjchem-864	112	53	,	,	PUNCT
eurjchem-864	112	54	2h	2h	NUM
eurjchem-864	112	55	,	,	PUNCT
eurjchem-864	112	56	ar‐h	ar‐h	NOUN
eurjchem-864	112	57	)	)	PUNCT
eurjchem-864	112	58	,	,	PUNCT
eurjchem-864	112	59	7.26	7.26	NUM
eurjchem-864	112	60	(	(	PUNCT
eurjchem-864	112	61	m	m	PROPN
eurjchem-864	112	62	,	,	PUNCT
eurjchem-864	112	63	1h	1h	NUM
eurjchem-864	112	64	,	,	PUNCT
eurjchem-864	112	65	ar‐h	ar‐h	NOUN
eurjchem-864	112	66	)	)	PUNCT
eurjchem-864	112	67	,	,	PUNCT
eurjchem-864	112	68	7.05	7.05	NUM
eurjchem-864	112	69	(	(	PUNCT
eurjchem-864	112	70	s	s	PROPN
eurjchem-864	112	71	,	,	PUNCT
eurjchem-864	112	72	1h	1h	NUM
eurjchem-864	112	73	,	,	PUNCT
eurjchem-864	112	74	ar‐h	ar‐h	NOUN
eurjchem-864	112	75	)	)	PUNCT
eurjchem-864	112	76	,	,	PUNCT
eurjchem-864	112	77	3.25‐3.35	3.25‐3.35	NUM
eurjchem-864	112	78	(	(	PUNCT
eurjchem-864	112	79	m	m	PROPN
eurjchem-864	112	80	,	,	PUNCT
eurjchem-864	112	81	8h	8h	NUM
eurjchem-864	112	82	,	,	PUNCT
eurjchem-864	112	83	ch2	ch2	PROPN
eurjchem-864	112	84	)	)	PUNCT
eurjchem-864	112	85	,	,	PUNCT
eurjchem-864	112	86	2.70	2.70	NUM
eurjchem-864	112	87	(	(	PUNCT
eurjchem-864	112	88	m	m	PROPN
eurjchem-864	112	89	,	,	PUNCT
eurjchem-864	112	90	1h	1h	NUM
eurjchem-864	112	91	,	,	PUNCT
eurjchem-864	112	92	ch	ch	NOUN
eurjchem-864	112	93	)	)	PUNCT
eurjchem-864	112	94	,	,	PUNCT
eurjchem-864	112	95	2.52	2.52	NUM
eurjchem-864	112	96	(	(	PUNCT
eurjchem-864	112	97	s	s	PROPN
eurjchem-864	112	98	,	,	PUNCT
eurjchem-864	112	99	3h	3h	NUM
eurjchem-864	112	100	,	,	PUNCT
eurjchem-864	112	101	ch3	ch3	PROPN
eurjchem-864	112	102	)	)	PUNCT
eurjchem-864	112	103	,	,	PUNCT
eurjchem-864	112	104	1.60‐1.84	1.60‐1.84	PROPN
eurjchem-864	112	105	(	(	PUNCT
eurjchem-864	112	106	m	m	PROPN
eurjchem-864	112	107	,	,	PUNCT
eurjchem-864	112	108	8h	8h	NUM
eurjchem-864	112	109	,	,	PUNCT
eurjchem-864	112	110	ch2	ch2	PROPN
eurjchem-864	112	111	)	)	PUNCT
eurjchem-864	112	112	.	.	PUNCT
eurjchem-864	113	1	anal	anal	PROPN
eurjchem-864	113	2	.	.	PUNCT
eurjchem-864	113	3	calcd	calcd	NOUN
eurjchem-864	113	4	.	.	PUNCT
eurjchem-864	114	1	for	for	ADP
eurjchem-864	114	2	c29h27brfn3o5	c29h27brfn3o5	NOUN
eurjchem-864	114	3	:	:	PUNCT
eurjchem-864	114	4	c	c	X
eurjchem-864	114	5	,	,	PUNCT
eurjchem-864	114	6	58.40	58.40	NUM
eurjchem-864	114	7	;	;	PUNCT
eurjchem-864	114	8	h	h	X
eurjchem-864	114	9	,	,	PUNCT
eurjchem-864	114	10	4.56	4.56	NUM
eurjchem-864	114	11	;	;	PUNCT
eurjchem-864	114	12	n	n	CCONJ
eurjchem-864	114	13	,	,	PUNCT
eurjchem-864	114	14	7.05	7.05	NUM
eurjchem-864	114	15	.	.	PUNCT
eurjchem-864	114	16	found	find	VERB
eurjchem-864	114	17	:	:	PUNCT
eurjchem-864	115	1	c	c	X
eurjchem-864	115	2	,	,	PUNCT
eurjchem-864	115	3	58.46	58.46	NUM
eurjchem-864	115	4	;	;	PUNCT
eurjchem-864	116	1	h	h	NOUN
eurjchem-864	116	2	,	,	PUNCT
eurjchem-864	116	3	4.60	4.60	NUM
eurjchem-864	116	4	;	;	PUNCT
eurjchem-864	116	5	n	n	CCONJ
eurjchem-864	116	6	,	,	PUNCT
eurjchem-864	116	7	7.11	7.11	NUM
eurjchem-864	116	8	.	.	PUNCT
eurjchem-864	117	1	ms	ms	NOUN
eurjchem-864	117	2	(	(	PUNCT
eurjchem-864	117	3	m	m	PROPN
eurjchem-864	117	4	/	/	SYM
eurjchem-864	117	5	z	z	NOUN
eurjchem-864	117	6	):	):	PUNCT
eurjchem-864	117	7	597	597	NUM
eurjchem-864	117	8	(	(	PUNCT
eurjchem-864	117	9	m+1	m+1	NUM
eurjchem-864	117	10	)	)	PUNCT
eurjchem-864	117	11	.	.	PUNCT
eurjchem-864	117	12	8‐(3,5‐dinitrobenzoyl)‐4‐(4‐(6‐fluorobenzo[d]isoxazol‐3‐yl	8‐(3,5‐dinitrobenzoyl)‐4‐(4‐(6‐fluorobenzo[d]isoxazol‐3‐yl	NUM
eurjchem-864	117	13	)	)	PUNCT
eurjchem-864	117	14	piperidine‐1‐carbonyl)‐3‐methyl‐1‐oxa‐8‐azaspiro[4.5]dec‐3‐en‐	piperidine‐1‐carbonyl)‐3‐methyl‐1‐oxa‐8‐azaspiro[4.5]dec‐3‐en‐	PART
eurjchem-864	117	15	2‐one	2‐one	NUM
eurjchem-864	117	16	(	(	PUNCT
eurjchem-864	117	17	9e	9e	NOUN
eurjchem-864	117	18	):	):	PUNCT
eurjchem-864	117	19	colour	colour	NOUN
eurjchem-864	117	20	:	:	PUNCT
eurjchem-864	117	21	white	white	ADJ
eurjchem-864	117	22	.	.	PUNCT
eurjchem-864	117	23	yield	yield	NOUN
eurjchem-864	117	24	:	:	PUNCT
eurjchem-864	117	25	65	65	NUM
eurjchem-864	117	26	%	%	NOUN
eurjchem-864	117	27	(	(	PUNCT
eurjchem-864	117	28	1.97	1.97	NUM
eurjchem-864	117	29	g	g	NOUN
eurjchem-864	117	30	)	)	PUNCT
eurjchem-864	117	31	.	.	PUNCT
eurjchem-864	118	1	m.p	m.p	PROPN
eurjchem-864	118	2	.	.	PROPN
eurjchem-864	118	3	:	:	PUNCT
eurjchem-864	119	1	184‐186	184‐186	NUM
eurjchem-864	119	2	°	°	SYM
eurjchem-864	119	3	c	c	NOUN
eurjchem-864	119	4	.	.	PUNCT
eurjchem-864	120	1	ft‐ir	ft‐ir	NOUN
eurjchem-864	120	2	(	(	PUNCT
eurjchem-864	120	3	kbr	kbr	PROPN
eurjchem-864	120	4	,	,	PUNCT
eurjchem-864	120	5	cm‐1	cm‐1	PROPN
eurjchem-864	120	6	):	):	PUNCT
eurjchem-864	120	7	1665	1665	NUM
eurjchem-864	120	8	(	(	PUNCT
eurjchem-864	120	9	amide	amide	PROPN
eurjchem-864	120	10	co	co	NOUN
eurjchem-864	120	11	str	str	PROPN
eurjchem-864	120	12	.	.	PUNCT
eurjchem-864	120	13	)	)	PUNCT
eurjchem-864	120	14	,	,	PUNCT
eurjchem-864	120	15	1771	1771	NUM
eurjchem-864	120	16	(	(	PUNCT
eurjchem-864	120	17	ester	ester	NOUN
eurjchem-864	120	18	co	co	NOUN
eurjchem-864	120	19	str	str	PROPN
eurjchem-864	120	20	.	.	PUNCT
eurjchem-864	120	21	)	)	PUNCT
eurjchem-864	120	22	,	,	PUNCT
eurjchem-864	120	23	3032	3032	NUM
eurjchem-864	120	24	(	(	PUNCT
eurjchem-864	120	25	aromatic	aromatic	ADJ
eurjchem-864	120	26	ch	ch	NOUN
eurjchem-864	120	27	str	str	NOUN
eurjchem-864	120	28	.	.	PUNCT
eurjchem-864	120	29	)	)	PUNCT
eurjchem-864	120	30	.	.	PUNCT
eurjchem-864	121	1	1h	1h	NUM
eurjchem-864	121	2	nmr	nmr	NOUN
eurjchem-864	121	3	(	(	PUNCT
eurjchem-864	121	4	400	400	NUM
eurjchem-864	121	5	mhz	mhz	NOUN
eurjchem-864	121	6	,	,	PUNCT
eurjchem-864	121	7	cdcl3	cdcl3	PROPN
eurjchem-864	121	8	,	,	PUNCT
eurjchem-864	121	9	δ	δ	PROPN
eurjchem-864	121	10	,	,	PUNCT
eurjchem-864	121	11	ppm	ppm	NUM
eurjchem-864	121	12	):	):	PUNCT
eurjchem-864	121	13	9.01	9.01	NUM
eurjchem-864	121	14	(	(	PUNCT
eurjchem-864	121	15	d	d	NOUN
eurjchem-864	121	16	,	,	PUNCT
eurjchem-864	121	17	j	j	PROPN
eurjchem-864	121	18	=	=	SYM
eurjchem-864	121	19	2.8	2.8	NUM
eurjchem-864	121	20	hz	hz	VERB
eurjchem-864	121	21	,	,	PUNCT
eurjchem-864	121	22	2h	2h	NUM
eurjchem-864	121	23	,	,	PUNCT
eurjchem-864	121	24	ar‐h	ar‐h	NOUN
eurjchem-864	121	25	)	)	PUNCT
eurjchem-864	121	26	,	,	PUNCT
eurjchem-864	121	27	8.93	8.93	NUM
eurjchem-864	121	28	(	(	PUNCT
eurjchem-864	121	29	s	s	PROPN
eurjchem-864	121	30	,	,	PUNCT
eurjchem-864	121	31	1h	1h	NUM
eurjchem-864	121	32	,	,	PUNCT
eurjchem-864	121	33	ar‐h	ar‐h	NOUN
eurjchem-864	121	34	)	)	PUNCT
eurjchem-864	121	35	,	,	PUNCT
eurjchem-864	121	36	7.59	7.59	NUM
eurjchem-864	121	37	(	(	PUNCT
eurjchem-864	121	38	d	d	PROPN
eurjchem-864	121	39	,	,	PUNCT
eurjchem-864	121	40	j	j	PROPN
eurjchem-864	121	41	=	=	SYM
eurjchem-864	121	42	7.2	7.2	NUM
eurjchem-864	121	43	hz	hz	NOUN
eurjchem-864	121	44	,	,	PUNCT
eurjchem-864	121	45	1h	1h	NUM
eurjchem-864	121	46	,	,	PUNCT
eurjchem-864	121	47	ar‐h	ar‐h	NOUN
eurjchem-864	121	48	)	)	PUNCT
eurjchem-864	121	49	,	,	PUNCT
eurjchem-864	121	50	7.32	7.32	NUM
eurjchem-864	121	51	(	(	PUNCT
eurjchem-864	121	52	d	d	PROPN
eurjchem-864	121	53	,	,	PUNCT
eurjchem-864	121	54	j	j	PROPN
eurjchem-864	122	1	=	=	SYM
eurjchem-864	122	2	7.2	7.2	NUM
eurjchem-864	122	3	hz	hz	NOUN
eurjchem-864	122	4	,	,	PUNCT
eurjchem-864	122	5	1h	1h	NUM
eurjchem-864	122	6	,	,	PUNCT
eurjchem-864	122	7	ar‐h	ar‐h	NOUN
eurjchem-864	122	8	)	)	PUNCT
eurjchem-864	122	9	,	,	PUNCT
eurjchem-864	122	10	7.01	7.01	NUM
eurjchem-864	122	11	(	(	PUNCT
eurjchem-864	122	12	s	s	PROPN
eurjchem-864	122	13	,	,	PUNCT
eurjchem-864	122	14	1h	1h	NUM
eurjchem-864	122	15	,	,	PUNCT
eurjchem-864	122	16	ar‐	ar‐	PROPN
eurjchem-864	122	17	h	h	NOUN
eurjchem-864	122	18	)	)	PUNCT
eurjchem-864	122	19	,	,	PUNCT
eurjchem-864	122	20	3.28‐3.39	3.28‐3.39	NUM
eurjchem-864	122	21	(	(	PUNCT
eurjchem-864	122	22	m	m	PROPN
eurjchem-864	122	23	,	,	PUNCT
eurjchem-864	122	24	8h	8h	NUM
eurjchem-864	122	25	,	,	PUNCT
eurjchem-864	122	26	ch2	ch2	PROPN
eurjchem-864	122	27	)	)	PUNCT
eurjchem-864	122	28	,	,	PUNCT
eurjchem-864	122	29	2.73	2.73	NUM
eurjchem-864	122	30	(	(	PUNCT
eurjchem-864	122	31	m	m	PROPN
eurjchem-864	122	32	,	,	PUNCT
eurjchem-864	122	33	1h	1h	NUM
eurjchem-864	122	34	,	,	PUNCT
eurjchem-864	122	35	ch	ch	NOUN
eurjchem-864	122	36	)	)	PUNCT
eurjchem-864	122	37	,	,	PUNCT
eurjchem-864	122	38	2.49	2.49	NUM
eurjchem-864	122	39	(	(	PUNCT
eurjchem-864	122	40	s	s	PROPN
eurjchem-864	122	41	,	,	PUNCT
eurjchem-864	122	42	3h	3h	NUM
eurjchem-864	122	43	,	,	PUNCT
eurjchem-864	122	44	ch3	ch3	PROPN
eurjchem-864	122	45	)	)	PUNCT
eurjchem-864	122	46	,	,	PUNCT
eurjchem-864	122	47	1.62‐1.81	1.62‐1.81	NUM
eurjchem-864	122	48	(	(	PUNCT
eurjchem-864	122	49	m	m	PROPN
eurjchem-864	122	50	,	,	PUNCT
eurjchem-864	122	51	8h	8h	NUM
eurjchem-864	122	52	,	,	PUNCT
eurjchem-864	122	53	ch2	ch2	PROPN
eurjchem-864	122	54	)	)	PUNCT
eurjchem-864	122	55	.	.	PUNCT
eurjchem-864	123	1	anal	anal	PROPN
eurjchem-864	123	2	.	.	PUNCT
eurjchem-864	123	3	calcd	calcd	NOUN
eurjchem-864	123	4	.	.	PUNCT
eurjchem-864	124	1	for	for	SCONJ
eurjchem-864	124	2	c29h26fn5o9	c29h26fn5o9	PROPN
eurjchem-864	124	3	:	:	PUNCT
eurjchem-864	124	4	c	c	NOUN
eurjchem-864	124	5	,	,	PUNCT
eurjchem-864	124	6	57.33	57.33	NUM
eurjchem-864	124	7	;	;	PUNCT
eurjchem-864	124	8	h	h	NOUN
eurjchem-864	124	9	,	,	PUNCT
eurjchem-864	124	10	4.31	4.31	NUM
eurjchem-864	124	11	;	;	PUNCT
eurjchem-864	124	12	n	n	CCONJ
eurjchem-864	124	13	,	,	PUNCT
eurjchem-864	124	14	11.53	11.53	NUM
eurjchem-864	124	15	.	.	PUNCT
eurjchem-864	124	16	found	find	VERB
eurjchem-864	124	17	:	:	PUNCT
eurjchem-864	125	1	c	c	X
eurjchem-864	125	2	,	,	PUNCT
eurjchem-864	125	3	57.39	57.39	NUM
eurjchem-864	125	4	;	;	PUNCT
eurjchem-864	125	5	h	h	NOUN
eurjchem-864	125	6	,	,	PUNCT
eurjchem-864	125	7	4.36	4.36	NUM
eurjchem-864	125	8	;	;	PUNCT
eurjchem-864	125	9	n	n	CCONJ
eurjchem-864	125	10	,	,	PUNCT
eurjchem-864	125	11	11.59	11.59	NUM
eurjchem-864	125	12	.	.	PUNCT
eurjchem-864	126	1	ms	ms	NOUN
eurjchem-864	126	2	(	(	PUNCT
eurjchem-864	126	3	m	m	PROPN
eurjchem-864	126	4	/	/	SYM
eurjchem-864	126	5	z	z	NOUN
eurjchem-864	126	6	):	):	PUNCT
eurjchem-864	126	7	608	608	NUM
eurjchem-864	126	8	(	(	PUNCT
eurjchem-864	126	9	m+1	m+1	NUM
eurjchem-864	126	10	)	)	PUNCT
eurjchem-864	126	11	.	.	PUNCT
eurjchem-864	127	1	4‐(4‐(6‐fluorobenzo[d]isoxazol‐3‐yl)piperidine‐1‐carbonyl)‐	4‐(4‐(6‐fluorobenzo[d]isoxazol‐3‐yl)piperidine‐1‐carbonyl)‐	NOUN
eurjchem-864	128	1	3‐methyl‐8‐(3,4,5‐trimethoxy	3‐methyl‐8‐(3,4,5‐trimethoxy	NUM
eurjchem-864	128	2	benzoyl)‐1‐oxa‐8‐azaspiro[4.5]dec‐	benzoyl)‐1‐oxa‐8‐azaspiro[4.5]dec‐	NOUN
eurjchem-864	128	3	3‐en‐2‐one	3‐en‐2‐one	NUM
eurjchem-864	128	4	(	(	PUNCT
eurjchem-864	128	5	9f	9f	NUM
eurjchem-864	128	6	):	):	PUNCT
eurjchem-864	128	7	colour	colour	NOUN
eurjchem-864	128	8	:	:	PUNCT
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eurjchem-864	128	10	.	.	PUNCT
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eurjchem-864	129	2	:	:	PUNCT
eurjchem-864	129	3	70	70	NUM
eurjchem-864	129	4	%	%	NOUN
eurjchem-864	129	5	(	(	PUNCT
eurjchem-864	129	6	2.12	2.12	NUM
eurjchem-864	129	7	g	g	NOUN
eurjchem-864	129	8	)	)	PUNCT
eurjchem-864	129	9	.	.	PUNCT
eurjchem-864	130	1	m.p	m.p	PROPN
eurjchem-864	130	2	.	.	PROPN
eurjchem-864	130	3	:	:	PUNCT
eurjchem-864	131	1	188‐	188‐	NUM
eurjchem-864	132	1	190	190	NUM
eurjchem-864	132	2	°	°	PROPN
eurjchem-864	132	3	c	c	X
eurjchem-864	132	4	.	.	PUNCT
eurjchem-864	133	1	ft‐ir	ft‐ir	NOUN
eurjchem-864	133	2	(	(	PUNCT
eurjchem-864	133	3	kbr	kbr	PROPN
eurjchem-864	133	4	,	,	PUNCT
eurjchem-864	133	5	cm‐1	cm‐1	PROPN
eurjchem-864	133	6	):	):	PUNCT
eurjchem-864	133	7	1660	1660	NUM
eurjchem-864	133	8	(	(	PUNCT
eurjchem-864	133	9	amide	amide	PROPN
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eurjchem-864	133	11	str	str	PROPN
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eurjchem-864	133	13	)	)	PUNCT
eurjchem-864	133	14	,	,	PUNCT
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eurjchem-864	133	16	(	(	PUNCT
eurjchem-864	133	17	ester	ester	NOUN
eurjchem-864	133	18	co	co	NOUN
eurjchem-864	133	19	str	str	PROPN
eurjchem-864	133	20	.	.	PUNCT
eurjchem-864	133	21	)	)	PUNCT
eurjchem-864	133	22	,	,	PUNCT
eurjchem-864	133	23	3073	3073	NUM
eurjchem-864	133	24	(	(	PUNCT
eurjchem-864	133	25	aromatic	aromatic	ADJ
eurjchem-864	133	26	ch	ch	NOUN
eurjchem-864	133	27	str	str	NOUN
eurjchem-864	133	28	.	.	PUNCT
eurjchem-864	133	29	)	)	PUNCT
eurjchem-864	133	30	.	.	PUNCT
eurjchem-864	134	1	1h	1h	NUM
eurjchem-864	134	2	nmr	nmr	NOUN
eurjchem-864	134	3	(	(	PUNCT
eurjchem-864	134	4	400	400	NUM
eurjchem-864	134	5	mhz	mhz	NOUN
eurjchem-864	134	6	,	,	PUNCT
eurjchem-864	134	7	cdcl3	cdcl3	PROPN
eurjchem-864	134	8	,	,	PUNCT
eurjchem-864	134	9	δ	δ	PROPN
eurjchem-864	134	10	,	,	PUNCT
eurjchem-864	134	11	ppm	ppm	NOUN
eurjchem-864	134	12	):	):	PUNCT
eurjchem-864	134	13	7.55	7.55	NUM
eurjchem-864	134	14	(	(	PUNCT
eurjchem-864	134	15	d	d	PROPN
eurjchem-864	134	16	,	,	PUNCT
eurjchem-864	134	17	j	j	PROPN
eurjchem-864	134	18	=	=	SYM
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eurjchem-864	134	22	1h	1h	NUM
eurjchem-864	134	23	,	,	PUNCT
eurjchem-864	134	24	ar‐h	ar‐h	NOUN
eurjchem-864	134	25	)	)	PUNCT
eurjchem-864	134	26	,	,	PUNCT
eurjchem-864	134	27	7.24	7.24	NUM
eurjchem-864	134	28	(	(	PUNCT
eurjchem-864	134	29	d	d	PROPN
eurjchem-864	134	30	,	,	PUNCT
eurjchem-864	134	31	j	j	PROPN
eurjchem-864	134	32	=	=	SYM
eurjchem-864	134	33	7.4	7.4	NUM
eurjchem-864	134	34	hz	hz	NOUN
eurjchem-864	134	35	,	,	PUNCT
eurjchem-864	134	36	1h	1h	NUM
eurjchem-864	134	37	,	,	PUNCT
eurjchem-864	134	38	ar‐	ar‐	PROPN
eurjchem-864	134	39	h	h	NOUN
eurjchem-864	134	40	)	)	PUNCT
eurjchem-864	134	41	,	,	PUNCT
eurjchem-864	134	42	7.17	7.17	NUM
eurjchem-864	134	43	(	(	PUNCT
eurjchem-864	134	44	s	s	PROPN
eurjchem-864	134	45	,	,	PUNCT
eurjchem-864	134	46	2h	2h	NUM
eurjchem-864	134	47	,	,	PUNCT
eurjchem-864	134	48	ar‐h	ar‐h	NOUN
eurjchem-864	134	49	)	)	PUNCT
eurjchem-864	134	50	,	,	PUNCT
eurjchem-864	134	51	6.97	6.97	NUM
eurjchem-864	134	52	(	(	PUNCT
eurjchem-864	134	53	s	s	PROPN
eurjchem-864	134	54	,	,	PUNCT
eurjchem-864	134	55	1h	1h	NUM
eurjchem-864	134	56	,	,	PUNCT
eurjchem-864	134	57	ar‐h	ar‐h	NOUN
eurjchem-864	134	58	)	)	PUNCT
eurjchem-864	134	59	,	,	PUNCT
eurjchem-864	134	60	3.83	3.83	NUM
eurjchem-864	134	61	(	(	PUNCT
eurjchem-864	134	62	s	s	PROPN
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eurjchem-864	134	65	,	,	PUNCT
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eurjchem-864	134	67	)	)	PUNCT
eurjchem-864	134	68	,	,	PUNCT
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eurjchem-864	134	70	(	(	PUNCT
eurjchem-864	134	71	s	s	PROPN
eurjchem-864	134	72	,	,	PUNCT
eurjchem-864	134	73	3h	3h	NUM
eurjchem-864	134	74	,	,	PUNCT
eurjchem-864	134	75	ome	ome	PROPN
eurjchem-864	134	76	)	)	PUNCT
eurjchem-864	134	77	,	,	PUNCT
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eurjchem-864	134	79	(	(	PUNCT
eurjchem-864	134	80	m	m	PROPN
eurjchem-864	134	81	,	,	PUNCT
eurjchem-864	134	82	8h	8h	NUM
eurjchem-864	134	83	,	,	PUNCT
eurjchem-864	134	84	ch2	ch2	PROPN
eurjchem-864	134	85	)	)	PUNCT
eurjchem-864	134	86	,	,	PUNCT
eurjchem-864	134	87	2.72	2.72	NUM
eurjchem-864	134	88	(	(	PUNCT
eurjchem-864	134	89	m	m	PROPN
eurjchem-864	134	90	,	,	PUNCT
eurjchem-864	134	91	1h	1h	NUM
eurjchem-864	134	92	,	,	PUNCT
eurjchem-864	134	93	ch	ch	NOUN
eurjchem-864	134	94	)	)	PUNCT
eurjchem-864	134	95	,	,	PUNCT
eurjchem-864	134	96	2.50	2.50	NUM
eurjchem-864	134	97	(	(	PUNCT
eurjchem-864	134	98	s	s	PROPN
eurjchem-864	134	99	,	,	PUNCT
eurjchem-864	134	100	3h	3h	NUM
eurjchem-864	134	101	,	,	PUNCT
eurjchem-864	134	102	ch3	ch3	PROPN
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eurjchem-864	134	104	,	,	PUNCT
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eurjchem-864	134	108	,	,	PUNCT
eurjchem-864	134	109	8h	8h	NUM
eurjchem-864	134	110	,	,	PUNCT
eurjchem-864	134	111	ch2	ch2	PROPN
eurjchem-864	134	112	)	)	PUNCT
eurjchem-864	134	113	.	.	PUNCT
eurjchem-864	135	1	anal	anal	PROPN
eurjchem-864	135	2	.	.	PUNCT
eurjchem-864	135	3	calcd	calcd	NOUN
eurjchem-864	135	4	.	.	PUNCT
eurjchem-864	136	1	for	for	ADP
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eurjchem-864	136	3	:	:	PUNCT
eurjchem-864	136	4	c	c	NOUN
eurjchem-864	136	5	,	,	PUNCT
eurjchem-864	136	6	63.25	63.25	NUM
eurjchem-864	136	7	;	;	PUNCT
eurjchem-864	136	8	h	h	NOUN
eurjchem-864	136	9	,	,	PUNCT
eurjchem-864	136	10	5.64	5.64	NUM
eurjchem-864	136	11	;	;	PUNCT
eurjchem-864	136	12	n	n	CCONJ
eurjchem-864	136	13	,	,	PUNCT
eurjchem-864	136	14	6.92	6.92	NUM
eurjchem-864	136	15	.	.	PUNCT
eurjchem-864	136	16	found	find	VERB
eurjchem-864	136	17	:	:	PUNCT
eurjchem-864	137	1	c	c	X
eurjchem-864	137	2	,	,	PUNCT
eurjchem-864	137	3	63.30	63.30	NUM
eurjchem-864	137	4	;	;	PUNCT
eurjchem-864	137	5	h	h	NOUN
eurjchem-864	137	6	,	,	PUNCT
eurjchem-864	137	7	5.71	5.71	NUM
eurjchem-864	137	8	;	;	PUNCT
eurjchem-864	137	9	n	n	CCONJ
eurjchem-864	137	10	,	,	PUNCT
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eurjchem-864	137	12	.	.	PUNCT
eurjchem-864	138	1	ms	ms	NOUN
eurjchem-864	138	2	(	(	PUNCT
eurjchem-864	138	3	m	m	PROPN
eurjchem-864	138	4	/	/	SYM
eurjchem-864	138	5	z	z	NOUN
eurjchem-864	138	6	):	):	PUNCT
eurjchem-864	138	7	608	608	NUM
eurjchem-864	138	8	(	(	PUNCT
eurjchem-864	138	9	m+1	m+1	NUM
eurjchem-864	138	10	)	)	PUNCT
eurjchem-864	138	11	.	.	PUNCT
eurjchem-864	139	1	4‐(4‐(6‐fluorobenzo[d]isoxazol‐3‐yl)piperidine‐1‐carbonyl)‐	4‐(4‐(6‐fluorobenzo[d]isoxazol‐3‐yl)piperidine‐1‐carbonyl)‐	NOUN
eurjchem-864	139	2	3‐methyl‐8‐(3‐nitrobenzoyl)‐1‐oxa‐8‐azaspiro[4.5]dec‐3‐en‐2‐	3‐methyl‐8‐(3‐nitrobenzoyl)‐1‐oxa‐8‐azaspiro[4.5]dec‐3‐en‐2‐	NUM
eurjchem-864	139	3	one	one	NUM
eurjchem-864	139	4	(	(	PUNCT
eurjchem-864	139	5	9	9	NUM
eurjchem-864	139	6	g	g	NOUN
eurjchem-864	139	7	):	):	PUNCT
eurjchem-864	139	8	colour	colour	NOUN
eurjchem-864	139	9	:	:	PUNCT
eurjchem-864	139	10	white	white	ADJ
eurjchem-864	139	11	.	.	PUNCT
eurjchem-864	140	1	yield	yield	NOUN
eurjchem-864	140	2	:	:	PUNCT
eurjchem-864	140	3	68	68	NUM
eurjchem-864	140	4	%	%	NOUN
eurjchem-864	140	5	(	(	PUNCT
eurjchem-864	140	6	1.91	1.91	NUM
eurjchem-864	140	7	g	g	NOUN
eurjchem-864	140	8	)	)	PUNCT
eurjchem-864	140	9	.	.	PUNCT
eurjchem-864	141	1	m.p	m.p	PROPN
eurjchem-864	141	2	.	.	PROPN
eurjchem-864	141	3	:	:	PUNCT
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eurjchem-864	142	2	°	°	SYM
eurjchem-864	142	3	c	c	X
eurjchem-864	142	4	.	.	PUNCT
eurjchem-864	143	1	ft‐ir	ft‐ir	NOUN
eurjchem-864	143	2	(	(	PUNCT
eurjchem-864	143	3	kbr	kbr	PROPN
eurjchem-864	143	4	,	,	PUNCT
eurjchem-864	143	5	cm‐1	cm‐1	PROPN
eurjchem-864	143	6	):	):	PUNCT
eurjchem-864	143	7	1669	1669	NUM
eurjchem-864	143	8	(	(	PUNCT
eurjchem-864	143	9	amide	amide	PROPN
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eurjchem-864	143	11	str	str	PROPN
eurjchem-864	143	12	.	.	PUNCT
eurjchem-864	143	13	)	)	PUNCT
eurjchem-864	143	14	,	,	PUNCT
eurjchem-864	143	15	1771	1771	NUM
eurjchem-864	143	16	(	(	PUNCT
eurjchem-864	143	17	ester	ester	NOUN
eurjchem-864	143	18	co	co	NOUN
eurjchem-864	143	19	str	str	PROPN
eurjchem-864	143	20	.	.	PUNCT
eurjchem-864	143	21	)	)	PUNCT
eurjchem-864	143	22	,	,	PUNCT
eurjchem-864	143	23	3061	3061	NUM
eurjchem-864	143	24	(	(	PUNCT
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eurjchem-864	143	26	ch	ch	NOUN
eurjchem-864	143	27	str	str	NOUN
eurjchem-864	143	28	.	.	PUNCT
eurjchem-864	143	29	)	)	PUNCT
eurjchem-864	143	30	.	.	PUNCT
eurjchem-864	144	1	1h	1h	NUM
eurjchem-864	144	2	nmr	nmr	NOUN
eurjchem-864	144	3	(	(	PUNCT
eurjchem-864	144	4	400	400	NUM
eurjchem-864	144	5	mhz	mhz	NOUN
eurjchem-864	144	6	,	,	PUNCT
eurjchem-864	144	7	cdcl3	cdcl3	PROPN
eurjchem-864	144	8	,	,	PUNCT
eurjchem-864	144	9	δ	δ	PROPN
eurjchem-864	144	10	,	,	PUNCT
eurjchem-864	144	11	ppm	ppm	NUM
eurjchem-864	144	12	):	):	PUNCT
eurjchem-864	144	13	8.72	8.72	NUM
eurjchem-864	144	14	(	(	PUNCT
eurjchem-864	144	15	s	s	PROPN
eurjchem-864	144	16	,	,	PUNCT
eurjchem-864	144	17	1h	1h	NUM
eurjchem-864	144	18	,	,	PUNCT
eurjchem-864	144	19	ar‐h	ar‐h	NOUN
eurjchem-864	144	20	)	)	PUNCT
eurjchem-864	144	21	,	,	PUNCT
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eurjchem-864	144	24	d	d	PROPN
eurjchem-864	144	25	,	,	PUNCT
eurjchem-864	144	26	j	j	PROPN
eurjchem-864	144	27	=	=	SYM
eurjchem-864	144	28	8.0	8.0	NUM
eurjchem-864	144	29	hz	hz	NOUN
eurjchem-864	144	30	,	,	PUNCT
eurjchem-864	144	31	1h	1h	NUM
eurjchem-864	144	32	,	,	PUNCT
eurjchem-864	144	33	ar‐h	ar‐h	NOUN
eurjchem-864	144	34	)	)	PUNCT
eurjchem-864	144	35	,	,	PUNCT
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eurjchem-864	144	37	(	(	PUNCT
eurjchem-864	144	38	d	d	PROPN
eurjchem-864	144	39	,	,	PUNCT
eurjchem-864	144	40	j	j	PROPN
eurjchem-864	145	1	=	=	SYM
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eurjchem-864	145	3	hz	hz	NOUN
eurjchem-864	145	4	,	,	PUNCT
eurjchem-864	145	5	1h	1h	NUM
eurjchem-864	145	6	,	,	PUNCT
eurjchem-864	145	7	ar‐h	ar‐h	NOUN
eurjchem-864	145	8	)	)	PUNCT
eurjchem-864	145	9	,	,	PUNCT
eurjchem-864	145	10	7.89	7.89	NUM
eurjchem-864	145	11	(	(	PUNCT
eurjchem-864	145	12	t	t	PROPN
eurjchem-864	145	13	,	,	PUNCT
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eurjchem-864	146	1	=	=	SYM
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eurjchem-864	146	3	hz	hz	NOUN
eurjchem-864	146	4	,	,	PUNCT
eurjchem-864	146	5	1h	1h	NUM
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eurjchem-864	146	7	ar‐h	ar‐h	NOUN
eurjchem-864	146	8	)	)	PUNCT
eurjchem-864	146	9	,	,	PUNCT
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eurjchem-864	146	12	d	d	PROPN
eurjchem-864	146	13	,	,	PUNCT
eurjchem-864	146	14	j	j	PROPN
eurjchem-864	146	15	=	=	SYM
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eurjchem-864	146	17	hz	hz	NOUN
eurjchem-864	146	18	,	,	PUNCT
eurjchem-864	146	19	1h	1h	NUM
eurjchem-864	146	20	,	,	PUNCT
eurjchem-864	146	21	ar‐h	ar‐h	NOUN
eurjchem-864	146	22	)	)	PUNCT
eurjchem-864	146	23	,	,	PUNCT
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eurjchem-864	146	25	(	(	PUNCT
eurjchem-864	146	26	d	d	PROPN
eurjchem-864	146	27	,	,	PUNCT
eurjchem-864	146	28	j	j	PROPN
eurjchem-864	147	1	=	=	SYM
eurjchem-864	147	2	7.3	7.3	NUM
eurjchem-864	147	3	hz	hz	NOUN
eurjchem-864	147	4	,	,	PUNCT
eurjchem-864	147	5	1h	1h	NUM
eurjchem-864	147	6	,	,	PUNCT
eurjchem-864	147	7	ar‐h	ar‐h	NOUN
eurjchem-864	147	8	)	)	PUNCT
eurjchem-864	147	9	,	,	PUNCT
eurjchem-864	147	10	6.97	6.97	NUM
eurjchem-864	147	11	(	(	PUNCT
eurjchem-864	147	12	s	s	PROPN
eurjchem-864	147	13	,	,	PUNCT
eurjchem-864	147	14	1h	1h	NUM
eurjchem-864	147	15	,	,	PUNCT
eurjchem-864	147	16	ar‐h	ar‐h	NOUN
eurjchem-864	147	17	)	)	PUNCT
eurjchem-864	147	18	,	,	PUNCT
eurjchem-864	147	19	3.29‐	3.29‐	NUM
eurjchem-864	147	20	3.42	3.42	NUM
eurjchem-864	147	21	(	(	PUNCT
eurjchem-864	147	22	m	m	PROPN
eurjchem-864	147	23	,	,	PUNCT
eurjchem-864	147	24	8h	8h	NUM
eurjchem-864	147	25	,	,	PUNCT
eurjchem-864	147	26	ch2	ch2	PROPN
eurjchem-864	147	27	)	)	PUNCT
eurjchem-864	147	28	,	,	PUNCT
eurjchem-864	147	29	2.68	2.68	NUM
eurjchem-864	147	30	(	(	PUNCT
eurjchem-864	147	31	m	m	PROPN
eurjchem-864	147	32	,	,	PUNCT
eurjchem-864	147	33	1h	1h	NUM
eurjchem-864	147	34	,	,	PUNCT
eurjchem-864	147	35	ch	ch	NOUN
eurjchem-864	147	36	)	)	PUNCT
eurjchem-864	147	37	,	,	PUNCT
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eurjchem-864	147	39	(	(	PUNCT
eurjchem-864	147	40	s	s	PROPN
eurjchem-864	147	41	,	,	PUNCT
eurjchem-864	147	42	3h	3h	NUM
eurjchem-864	147	43	,	,	PUNCT
eurjchem-864	147	44	ch3	ch3	PROPN
eurjchem-864	147	45	)	)	PUNCT
eurjchem-864	147	46	,	,	PUNCT
eurjchem-864	147	47	1.65‐1.82	1.65‐1.82	NUM
eurjchem-864	147	48	(	(	PUNCT
eurjchem-864	147	49	m	m	PROPN
eurjchem-864	147	50	,	,	PUNCT
eurjchem-864	147	51	8h	8h	NUM
eurjchem-864	147	52	,	,	PUNCT
eurjchem-864	147	53	ch2	ch2	PROPN
eurjchem-864	147	54	)	)	PUNCT
eurjchem-864	147	55	.	.	PUNCT
eurjchem-864	148	1	anal	anal	PROPN
eurjchem-864	148	2	.	.	PUNCT
eurjchem-864	148	3	calcd	calcd	NOUN
eurjchem-864	148	4	.	.	PUNCT
eurjchem-864	149	1	for	for	SCONJ
eurjchem-864	149	2	c29h27fn4o7	c29h27fn4o7	NOUN
eurjchem-864	149	3	:	:	PUNCT
eurjchem-864	149	4	c	c	X
eurjchem-864	149	5	,	,	PUNCT
eurjchem-864	149	6	61.92	61.92	NUM
eurjchem-864	149	7	;	;	PUNCT
eurjchem-864	149	8	h	h	X
eurjchem-864	149	9	,	,	PUNCT
eurjchem-864	149	10	4.84	4.84	NUM
eurjchem-864	149	11	;	;	PUNCT
eurjchem-864	149	12	n	n	CCONJ
eurjchem-864	149	13	,	,	PUNCT
eurjchem-864	149	14	9.96	9.96	NUM
eurjchem-864	149	15	.	.	PUNCT
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eurjchem-864	149	17	:	:	PUNCT
eurjchem-864	150	1	c	c	X
eurjchem-864	150	2	,	,	PUNCT
eurjchem-864	150	3	61.98	61.98	NUM
eurjchem-864	150	4	;	;	PUNCT
eurjchem-864	150	5	h	h	NOUN
eurjchem-864	150	6	,	,	PUNCT
eurjchem-864	150	7	4.89	4.89	NUM
eurjchem-864	150	8	;	;	PUNCT
eurjchem-864	150	9	n	n	CCONJ
eurjchem-864	150	10	,	,	PUNCT
eurjchem-864	150	11	9.98	9.98	NUM
eurjchem-864	150	12	.	.	PUNCT
eurjchem-864	151	1	ms	ms	NOUN
eurjchem-864	151	2	(	(	PUNCT
eurjchem-864	151	3	m	m	PROPN
eurjchem-864	151	4	/	/	SYM
eurjchem-864	151	5	z	z	NOUN
eurjchem-864	151	6	):	):	PUNCT
eurjchem-864	151	7	563	563	NUM
eurjchem-864	151	8	(	(	PUNCT
eurjchem-864	151	9	m+1	m+1	NUM
eurjchem-864	151	10	)	)	PUNCT
eurjchem-864	151	11	.	.	PUNCT
eurjchem-864	152	1	4‐(4‐(6‐fluorobenzo[d]isoxazol‐3‐yl)piperidine‐1‐carbonyl)‐	4‐(4‐(6‐fluorobenzo[d]isoxazol‐3‐yl)piperidine‐1‐carbonyl)‐	NOUN
eurjchem-864	152	2	8‐(4‐methoxybenzoyl)‐3‐methyl‐1‐oxa‐8‐azaspiro[4.5]dec‐3‐en‐	8‐(4‐methoxybenzoyl)‐3‐methyl‐1‐oxa‐8‐azaspiro[4.5]dec‐3‐en‐	NUM
eurjchem-864	152	3	2‐one	2‐one	NUM
eurjchem-864	152	4	(	(	PUNCT
eurjchem-864	152	5	9h	9h	NUM
eurjchem-864	152	6	):	):	PUNCT
eurjchem-864	152	7	colour	colour	NOUN
eurjchem-864	152	8	:	:	PUNCT
eurjchem-864	152	9	white	white	ADJ
eurjchem-864	152	10	.	.	PUNCT
eurjchem-864	153	1	yield	yield	NOUN
eurjchem-864	153	2	:	:	PUNCT
eurjchem-864	153	3	72	72	NUM
eurjchem-864	153	4	%	%	NOUN
eurjchem-864	153	5	(	(	PUNCT
eurjchem-864	153	6	1.96	1.96	NUM
eurjchem-864	153	7	g	g	NOUN
eurjchem-864	153	8	)	)	PUNCT
eurjchem-864	153	9	.	.	PUNCT
eurjchem-864	154	1	m.p	m.p	PROPN
eurjchem-864	154	2	.	.	PROPN
eurjchem-864	154	3	:	:	PUNCT
eurjchem-864	155	1	108‐110	108‐110	NUM
eurjchem-864	155	2	°	°	SYM
eurjchem-864	155	3	c	c	NOUN
eurjchem-864	155	4	.	.	PUNCT
eurjchem-864	156	1	ft‐ir	ft‐ir	NOUN
eurjchem-864	156	2	(	(	PUNCT
eurjchem-864	156	3	kbr	kbr	PROPN
eurjchem-864	156	4	,	,	PUNCT
eurjchem-864	156	5	cm‐1	cm‐1	PROPN
eurjchem-864	156	6	):	):	PUNCT
eurjchem-864	156	7	1659	1659	NUM
eurjchem-864	156	8	(	(	PUNCT
eurjchem-864	156	9	amide	amide	PROPN
eurjchem-864	156	10	co	co	NOUN
eurjchem-864	156	11	str	str	PROPN
eurjchem-864	156	12	.	.	PUNCT
eurjchem-864	156	13	)	)	PUNCT
eurjchem-864	156	14	,	,	PUNCT
eurjchem-864	156	15	1782	1782	NUM
eurjchem-864	156	16	(	(	PUNCT
eurjchem-864	156	17	ester	ester	NOUN
eurjchem-864	156	18	co	co	NOUN
eurjchem-864	156	19	str	str	PROPN
eurjchem-864	156	20	.	.	PUNCT
eurjchem-864	156	21	)	)	PUNCT
eurjchem-864	156	22	,	,	PUNCT
eurjchem-864	156	23	3047	3047	NUM
eurjchem-864	156	24	(	(	PUNCT
eurjchem-864	156	25	aromatic	aromatic	ADJ
eurjchem-864	156	26	ch	ch	NOUN
eurjchem-864	156	27	str	str	NOUN
eurjchem-864	156	28	.	.	PUNCT
eurjchem-864	156	29	)	)	PUNCT
eurjchem-864	156	30	.	.	PUNCT
eurjchem-864	157	1	1h	1h	NUM
eurjchem-864	157	2	nmr	nmr	NOUN
eurjchem-864	157	3	(	(	PUNCT
eurjchem-864	157	4	400	400	NUM
eurjchem-864	157	5	mhz	mhz	NOUN
eurjchem-864	157	6	,	,	PUNCT
eurjchem-864	157	7	cdcl3	cdcl3	PROPN
eurjchem-864	157	8	,	,	PUNCT
eurjchem-864	157	9	δ	δ	PROPN
eurjchem-864	157	10	,	,	PUNCT
eurjchem-864	157	11	ppm	ppm	NOUN
eurjchem-864	157	12	):	):	PUNCT
eurjchem-864	157	13	7.92	7.92	NUM
eurjchem-864	157	14	(	(	PUNCT
eurjchem-864	157	15	d	d	PROPN
eurjchem-864	157	16	,	,	PUNCT
eurjchem-864	157	17	j	j	PROPN
eurjchem-864	157	18	=	=	SYM
eurjchem-864	157	19	8.0	8.0	NUM
eurjchem-864	157	20	hz	hz	NOUN
eurjchem-864	157	21	,	,	PUNCT
eurjchem-864	157	22	2h	2h	NUM
eurjchem-864	157	23	,	,	PUNCT
eurjchem-864	157	24	ar‐h	ar‐h	NOUN
eurjchem-864	157	25	)	)	PUNCT
eurjchem-864	157	26	,	,	PUNCT
eurjchem-864	157	27	7.55	7.55	NUM
eurjchem-864	157	28	(	(	PUNCT
eurjchem-864	157	29	d	d	PROPN
eurjchem-864	157	30	,	,	PUNCT
eurjchem-864	157	31	j	j	PROPN
eurjchem-864	158	1	=	=	SYM
eurjchem-864	158	2	7.6	7.6	NUM
eurjchem-864	158	3	hz	hz	NOUN
eurjchem-864	158	4	,	,	PUNCT
eurjchem-864	158	5	1h	1h	NUM
eurjchem-864	158	6	,	,	PUNCT
eurjchem-864	158	7	ar‐	ar‐	PROPN
eurjchem-864	158	8	h	h	NOUN
eurjchem-864	158	9	)	)	PUNCT
eurjchem-864	158	10	,	,	PUNCT
eurjchem-864	158	11	7.26	7.26	NUM
eurjchem-864	158	12	(	(	PUNCT
eurjchem-864	158	13	d	d	NOUN
eurjchem-864	158	14	,	,	PUNCT
eurjchem-864	158	15	j=7.6	j=7.6	PROPN
eurjchem-864	158	16	hz	hz	NOUN
eurjchem-864	158	17	,	,	PUNCT
eurjchem-864	158	18	1h	1h	NUM
eurjchem-864	158	19	,	,	PUNCT
eurjchem-864	158	20	ar‐h	ar‐h	NOUN
eurjchem-864	158	21	)	)	PUNCT
eurjchem-864	158	22	,	,	PUNCT
eurjchem-864	158	23	7.16	7.16	NUM
eurjchem-864	158	24	(	(	PUNCT
eurjchem-864	158	25	d	d	PROPN
eurjchem-864	158	26	,	,	PUNCT
eurjchem-864	158	27	j=8.0	j=8.0	PROPN
eurjchem-864	158	28	hz	hz	PROPN
eurjchem-864	158	29	,	,	PUNCT
eurjchem-864	158	30	2h	2h	NUM
eurjchem-864	158	31	,	,	PUNCT
eurjchem-864	158	32	ar‐h	ar‐h	NOUN
eurjchem-864	158	33	)	)	PUNCT
eurjchem-864	158	34	,	,	PUNCT
eurjchem-864	158	35	6.97	6.97	NUM
eurjchem-864	158	36	(	(	PUNCT
eurjchem-864	158	37	s	s	PROPN
eurjchem-864	158	38	,	,	PUNCT
eurjchem-864	158	39	1h	1h	NUM
eurjchem-864	158	40	,	,	PUNCT
eurjchem-864	158	41	ar‐h	ar‐h	NOUN
eurjchem-864	158	42	)	)	PUNCT
eurjchem-864	158	43	,	,	PUNCT
eurjchem-864	158	44	3.82	3.82	NUM
eurjchem-864	158	45	(	(	PUNCT
eurjchem-864	158	46	s	s	PROPN
eurjchem-864	158	47	,	,	PUNCT
eurjchem-864	158	48	3h	3h	NUM
eurjchem-864	158	49	,	,	PUNCT
eurjchem-864	158	50	ome	ome	PROPN
eurjchem-864	158	51	)	)	PUNCT
eurjchem-864	158	52	,	,	PUNCT
eurjchem-864	158	53	3.32‐3.45	3.32‐3.45	PROPN
eurjchem-864	158	54	(	(	PUNCT
eurjchem-864	158	55	m	m	PROPN
eurjchem-864	158	56	,	,	PUNCT
eurjchem-864	158	57	8h	8h	NUM
eurjchem-864	158	58	,	,	PUNCT
eurjchem-864	158	59	ch2	ch2	PROPN
eurjchem-864	158	60	)	)	PUNCT
eurjchem-864	158	61	,	,	PUNCT
eurjchem-864	158	62	2.70	2.70	NUM
eurjchem-864	158	63	(	(	PUNCT
eurjchem-864	158	64	m	m	PROPN
eurjchem-864	158	65	,	,	PUNCT
eurjchem-864	158	66	1h	1h	NUM
eurjchem-864	158	67	,	,	PUNCT
eurjchem-864	158	68	ch	ch	NOUN
eurjchem-864	158	69	)	)	PUNCT
eurjchem-864	158	70	,	,	PUNCT
eurjchem-864	158	71	2.49	2.49	NUM
eurjchem-864	158	72	(	(	PUNCT
eurjchem-864	158	73	s	s	PROPN
eurjchem-864	158	74	,	,	PUNCT
eurjchem-864	158	75	3h	3h	NUM
eurjchem-864	158	76	,	,	PUNCT
eurjchem-864	158	77	ch3	ch3	PROPN
eurjchem-864	158	78	)	)	PUNCT
eurjchem-864	158	79	,	,	PUNCT
eurjchem-864	158	80	1.62‐1.85	1.62‐1.85	NUM
eurjchem-864	158	81	(	(	PUNCT
eurjchem-864	158	82	m	m	PROPN
eurjchem-864	158	83	,	,	PUNCT
eurjchem-864	158	84	8h	8h	NUM
eurjchem-864	158	85	,	,	PUNCT
eurjchem-864	158	86	ch2	ch2	PROPN
eurjchem-864	158	87	)	)	PUNCT
eurjchem-864	158	88	.	.	PUNCT
eurjchem-864	159	1	anal	anal	PROPN
eurjchem-864	159	2	.	.	PUNCT
eurjchem-864	159	3	calcd	calcd	NOUN
eurjchem-864	159	4	.	.	PUNCT
eurjchem-864	160	1	for	for	SCONJ
eurjchem-864	160	2	c30h30fn3o6	c30h30fn3o6	ADJ
eurjchem-864	160	3	:	:	PUNCT
eurjchem-864	160	4	c	c	X
eurjchem-864	160	5	,	,	PUNCT
eurjchem-864	160	6	65.80	65.80	NUM
eurjchem-864	160	7	;	;	PUNCT
eurjchem-864	160	8	h	h	NOUN
eurjchem-864	160	9	,	,	PUNCT
eurjchem-864	160	10	5.52	5.52	NUM
eurjchem-864	160	11	;	;	PUNCT
eurjchem-864	160	12	n	n	CCONJ
eurjchem-864	160	13	,	,	PUNCT
eurjchem-864	160	14	7.67	7.67	NUM
eurjchem-864	160	15	.	.	PUNCT
eurjchem-864	160	16	found	find	VERB
eurjchem-864	160	17	:	:	PUNCT
eurjchem-864	161	1	c	c	X
eurjchem-864	161	2	,	,	PUNCT
eurjchem-864	161	3	65.85	65.85	NUM
eurjchem-864	161	4	;	;	PUNCT
eurjchem-864	161	5	h	h	NOUN
eurjchem-864	161	6	,	,	PUNCT
eurjchem-864	161	7	5.59	5.59	NUM
eurjchem-864	161	8	;	;	PUNCT
eurjchem-864	161	9	n	n	CCONJ
eurjchem-864	161	10	,	,	PUNCT
eurjchem-864	161	11	7.73	7.73	NUM
eurjchem-864	161	12	.	.	PUNCT
eurjchem-864	162	1	ms	ms	NOUN
eurjchem-864	162	2	(	(	PUNCT
eurjchem-864	162	3	m	m	PROPN
eurjchem-864	162	4	/	/	SYM
eurjchem-864	162	5	z	z	NOUN
eurjchem-864	162	6	):	):	PUNCT
eurjchem-864	162	7	548	548	NUM
eurjchem-864	162	8	(	(	PUNCT
eurjchem-864	162	9	m+1	m+1	NUM
eurjchem-864	162	10	)	)	PUNCT
eurjchem-864	162	11	.	.	PUNCT
eurjchem-864	163	1	8‐(2,6‐difluorobenzoyl)‐4‐(4‐(6‐fluorobenzo[d]isoxazol‐3‐yl	8‐(2,6‐difluorobenzoyl)‐4‐(4‐(6‐fluorobenzo[d]isoxazol‐3‐yl	PROPN
eurjchem-864	163	2	)	)	PUNCT
eurjchem-864	163	3	piperidine‐1‐carbonyl)‐3‐methyl	piperidine‐1‐carbonyl)‐3‐methyl	PROPN
eurjchem-864	163	4	‐1‐oxa‐8‐azaspiro[4.5]dec‐3‐en‐	‐1‐oxa‐8‐azaspiro[4.5]dec‐3‐en‐	NUM
eurjchem-864	163	5	2‐one	2‐one	NUM
eurjchem-864	163	6	(	(	PUNCT
eurjchem-864	163	7	9i	9i	NOUN
eurjchem-864	163	8	):	):	PUNCT
eurjchem-864	163	9	colour	colour	NOUN
eurjchem-864	163	10	:	:	PUNCT
eurjchem-864	163	11	white	white	ADJ
eurjchem-864	163	12	.	.	PUNCT
eurjchem-864	164	1	yield	yield	NOUN
eurjchem-864	164	2	:	:	PUNCT
eurjchem-864	164	3	60	60	NUM
eurjchem-864	164	4	%	%	NOUN
eurjchem-864	164	5	(	(	PUNCT
eurjchem-864	164	6	1.65	1.65	NUM
eurjchem-864	164	7	g	g	NOUN
eurjchem-864	164	8	)	)	PUNCT
eurjchem-864	164	9	.	.	PUNCT
eurjchem-864	165	1	m.p	m.p	PROPN
eurjchem-864	165	2	.	.	PROPN
eurjchem-864	165	3	:	:	PUNCT
eurjchem-864	166	1	128‐130	128‐130	PROPN
eurjchem-864	166	2	°	°	PROPN
eurjchem-864	166	3	c	c	PROPN
eurjchem-864	166	4	.	.	PUNCT
eurjchem-864	167	1	ft‐ir	ft‐ir	NOUN
eurjchem-864	167	2	(	(	PUNCT
eurjchem-864	167	3	kbr	kbr	PROPN
eurjchem-864	167	4	,	,	PUNCT
eurjchem-864	167	5	cm‐1	cm‐1	PROPN
eurjchem-864	167	6	):	):	PUNCT
eurjchem-864	167	7	1667	1667	NUM
eurjchem-864	167	8	(	(	PUNCT
eurjchem-864	167	9	amide	amide	PROPN
eurjchem-864	167	10	co	co	NOUN
eurjchem-864	167	11	str	str	PROPN
eurjchem-864	167	12	.	.	PUNCT
eurjchem-864	167	13	)	)	PUNCT
eurjchem-864	167	14	,	,	PUNCT
eurjchem-864	167	15	1774	1774	NUM
eurjchem-864	167	16	(	(	PUNCT
eurjchem-864	167	17	ester	ester	NOUN
eurjchem-864	167	18	co	co	NOUN
eurjchem-864	167	19	str	str	PROPN
eurjchem-864	167	20	.	.	PUNCT
eurjchem-864	167	21	)	)	PUNCT
eurjchem-864	167	22	,	,	PUNCT
eurjchem-864	167	23	3059	3059	NUM
eurjchem-864	167	24	(	(	PUNCT
eurjchem-864	167	25	aromatic	aromatic	ADJ
eurjchem-864	167	26	ch	ch	NOUN
eurjchem-864	167	27	str	str	NOUN
eurjchem-864	167	28	.	.	PUNCT
eurjchem-864	167	29	)	)	PUNCT
eurjchem-864	167	30	.	.	PUNCT
eurjchem-864	168	1	1h	1h	NUM
eurjchem-864	168	2	nmr	nmr	NOUN
eurjchem-864	168	3	(	(	PUNCT
eurjchem-864	168	4	400	400	NUM
eurjchem-864	168	5	mhz	mhz	NOUN
eurjchem-864	168	6	,	,	PUNCT
eurjchem-864	168	7	cdcl3	cdcl3	PROPN
eurjchem-864	168	8	,	,	PUNCT
eurjchem-864	168	9	δ	δ	PROPN
eurjchem-864	168	10	,	,	PUNCT
eurjchem-864	168	11	ppm	ppm	NOUN
eurjchem-864	168	12	):	):	PUNCT
eurjchem-864	168	13	7.53‐7.56	7.53‐7.56	NUM
eurjchem-864	168	14	(	(	PUNCT
eurjchem-864	168	15	m	m	PROPN
eurjchem-864	168	16	,	,	PUNCT
eurjchem-864	168	17	2h	2h	NUM
eurjchem-864	168	18	,	,	PUNCT
eurjchem-864	168	19	ar‐h	ar‐h	NOUN
eurjchem-864	168	20	)	)	PUNCT
eurjchem-864	168	21	,	,	PUNCT
eurjchem-864	168	22	7.19‐7.24	7.19‐7.24	NUM
eurjchem-864	168	23	(	(	PUNCT
eurjchem-864	168	24	m	m	PROPN
eurjchem-864	168	25	,	,	PUNCT
eurjchem-864	168	26	3h	3h	NUM
eurjchem-864	168	27	,	,	PUNCT
eurjchem-864	168	28	ar‐h	ar‐h	NOUN
eurjchem-864	168	29	)	)	PUNCT
eurjchem-864	168	30	,	,	PUNCT
eurjchem-864	168	31	6.97	6.97	NUM
eurjchem-864	168	32	(	(	PUNCT
eurjchem-864	168	33	s	s	PROPN
eurjchem-864	168	34	,	,	PUNCT
eurjchem-864	168	35	1h	1h	NUM
eurjchem-864	168	36	,	,	PUNCT
eurjchem-864	168	37	ar‐h	ar‐h	NOUN
eurjchem-864	168	38	)	)	PUNCT
eurjchem-864	168	39	,	,	PUNCT
eurjchem-864	168	40	3.30‐3.44	3.30‐3.44	NUM
eurjchem-864	168	41	(	(	PUNCT
eurjchem-864	168	42	m	m	PROPN
eurjchem-864	168	43	,	,	PUNCT
eurjchem-864	168	44	8h	8h	NUM
eurjchem-864	168	45	,	,	PUNCT
eurjchem-864	168	46	ch2	ch2	PROPN
eurjchem-864	168	47	)	)	PUNCT
eurjchem-864	168	48	,	,	PUNCT
eurjchem-864	168	49	2.71	2.71	NUM
eurjchem-864	168	50	(	(	PUNCT
eurjchem-864	168	51	m	m	PROPN
eurjchem-864	168	52	,	,	PUNCT
eurjchem-864	168	53	1h	1h	NUM
eurjchem-864	168	54	,	,	PUNCT
eurjchem-864	168	55	ch	ch	NOUN
eurjchem-864	168	56	)	)	PUNCT
eurjchem-864	168	57	,	,	PUNCT
eurjchem-864	168	58	2.54	2.54	NUM
eurjchem-864	168	59	(	(	PUNCT
eurjchem-864	168	60	s	s	PROPN
eurjchem-864	168	61	,	,	PUNCT
eurjchem-864	168	62	3h	3h	NUM
eurjchem-864	168	63	,	,	PUNCT
eurjchem-864	168	64	ch3	ch3	PROPN
eurjchem-864	168	65	)	)	PUNCT
eurjchem-864	168	66	,	,	PUNCT
eurjchem-864	168	67	1.60‐1.85	1.60‐1.85	NUM
eurjchem-864	168	68	(	(	PUNCT
eurjchem-864	168	69	m	m	PROPN
eurjchem-864	168	70	,	,	PUNCT
eurjchem-864	168	71	8h	8h	NUM
eurjchem-864	168	72	,	,	PUNCT
eurjchem-864	168	73	ch2	ch2	PROPN
eurjchem-864	168	74	)	)	PUNCT
eurjchem-864	168	75	.	.	PUNCT
eurjchem-864	169	1	anal	anal	PROPN
eurjchem-864	169	2	.	.	PUNCT
eurjchem-864	169	3	calcd	calcd	NOUN
eurjchem-864	169	4	.	.	PUNCT
eurjchem-864	170	1	for	for	ADP
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eurjchem-864	170	3	:	:	PUNCT
eurjchem-864	170	4	c	c	X
eurjchem-864	170	5	,	,	PUNCT
eurjchem-864	170	6	62.93	62.93	NUM
eurjchem-864	170	7	;	;	PUNCT
eurjchem-864	170	8	h	h	NOUN
eurjchem-864	170	9	,	,	PUNCT
eurjchem-864	170	10	4.73	4.73	NUM
eurjchem-864	170	11	;	;	PUNCT
eurjchem-864	170	12	n	n	CCONJ
eurjchem-864	170	13	,	,	PUNCT
eurjchem-864	170	14	7.59	7.59	NUM
eurjchem-864	170	15	.	.	PUNCT
eurjchem-864	170	16	found	find	VERB
eurjchem-864	170	17	:	:	PUNCT
eurjchem-864	171	1	c	c	X
eurjchem-864	171	2	,	,	PUNCT
eurjchem-864	171	3	62.96	62.96	NUM
eurjchem-864	171	4	;	;	PUNCT
eurjchem-864	171	5	h	h	X
eurjchem-864	171	6	,	,	PUNCT
eurjchem-864	171	7	4.79	4.79	NUM
eurjchem-864	171	8	;	;	PUNCT
eurjchem-864	171	9	n	n	CCONJ
eurjchem-864	171	10	,	,	PUNCT
eurjchem-864	171	11	7.64	7.64	NUM
eurjchem-864	171	12	.	.	PUNCT
eurjchem-864	172	1	ms	ms	NOUN
eurjchem-864	172	2	(	(	PUNCT
eurjchem-864	172	3	m	m	PROPN
eurjchem-864	172	4	/	/	SYM
eurjchem-864	172	5	z	z	NOUN
eurjchem-864	172	6	):	):	PUNCT
eurjchem-864	172	7	554	554	NUM
eurjchem-864	172	8	(	(	PUNCT
eurjchem-864	172	9	m+1	m+1	NUM
eurjchem-864	172	10	)	)	PUNCT
eurjchem-864	172	11	.	.	PUNCT
eurjchem-864	173	1	8‐(3‐chlorobenzoyl)‐4‐(4‐(6‐fluorobenzo[d]isoxazol‐3‐yl	8‐(3‐chlorobenzoyl)‐4‐(4‐(6‐fluorobenzo[d]isoxazol‐3‐yl	NUM
eurjchem-864	173	2	)	)	PUNCT
eurjchem-864	173	3	piperidine‐1‐carbonyl)‐3‐methyl‐1‐oxa‐8‐azaspiro[4.5]dec‐3‐en‐	piperidine‐1‐carbonyl)‐3‐methyl‐1‐oxa‐8‐azaspiro[4.5]dec‐3‐en‐	NUM
eurjchem-864	173	4	2‐one	2‐one	NUM
eurjchem-864	173	5	(	(	PUNCT
eurjchem-864	173	6	9j	9j	NUM
eurjchem-864	173	7	):	):	PUNCT
eurjchem-864	173	8	colour	colour	NOUN
eurjchem-864	173	9	:	:	PUNCT
eurjchem-864	173	10	white	white	ADJ
eurjchem-864	173	11	.	.	PUNCT
eurjchem-864	174	1	yield	yield	NOUN
eurjchem-864	174	2	:	:	PUNCT
eurjchem-864	174	3	73	73	NUM
eurjchem-864	174	4	%	%	NOUN
eurjchem-864	174	5	(	(	PUNCT
eurjchem-864	174	6	2.01	2.01	NUM
eurjchem-864	174	7	g	g	NOUN
eurjchem-864	174	8	)	)	PUNCT
eurjchem-864	174	9	.	.	PUNCT
eurjchem-864	175	1	m.p	m.p	PROPN
eurjchem-864	175	2	.	.	PROPN
eurjchem-864	175	3	:	:	PUNCT
eurjchem-864	176	1	110‐112	110‐112	NUM
eurjchem-864	176	2	°	°	PRON
eurjchem-864	176	3	c	c	X
eurjchem-864	176	4	.	.	PUNCT
eurjchem-864	177	1	ft‐ir	ft‐ir	NOUN
eurjchem-864	177	2	(	(	PUNCT
eurjchem-864	177	3	kbr	kbr	PROPN
eurjchem-864	177	4	,	,	PUNCT
eurjchem-864	177	5	cm‐1	cm‐1	PROPN
eurjchem-864	177	6	):	):	PUNCT
eurjchem-864	177	7	1665	1665	NUM
eurjchem-864	177	8	(	(	PUNCT
eurjchem-864	177	9	amide	amide	PROPN
eurjchem-864	177	10	co	co	NOUN
eurjchem-864	177	11	str	str	PROPN
eurjchem-864	177	12	.	.	PUNCT
eurjchem-864	177	13	)	)	PUNCT
eurjchem-864	177	14	,	,	PUNCT
eurjchem-864	177	15	1755	1755	NUM
eurjchem-864	177	16	(	(	PUNCT
eurjchem-864	177	17	ester	ester	NOUN
eurjchem-864	177	18	co	co	NOUN
eurjchem-864	177	19	str	str	PROPN
eurjchem-864	177	20	.	.	PUNCT
eurjchem-864	177	21	)	)	PUNCT
eurjchem-864	177	22	,	,	PUNCT
eurjchem-864	177	23	3068	3068	NUM
eurjchem-864	177	24	(	(	PUNCT
eurjchem-864	177	25	aromatic	aromatic	ADJ
eurjchem-864	177	26	ch	ch	NOUN
eurjchem-864	177	27	str	str	NOUN
eurjchem-864	177	28	.	.	PUNCT
eurjchem-864	177	29	)	)	PUNCT
eurjchem-864	177	30	.	.	PUNCT
eurjchem-864	178	1	1h	1h	NUM
eurjchem-864	178	2	nmr	nmr	NOUN
eurjchem-864	178	3	(	(	PUNCT
eurjchem-864	178	4	400	400	NUM
eurjchem-864	178	5	mhz	mhz	NOUN
eurjchem-864	178	6	,	,	PUNCT
eurjchem-864	178	7	cdcl3	cdcl3	PROPN
eurjchem-864	178	8	,	,	PUNCT
eurjchem-864	178	9	δ	δ	PROPN
eurjchem-864	178	10	,	,	PUNCT
eurjchem-864	178	11	ppm	ppm	NUM
eurjchem-864	178	12	):	):	PUNCT
eurjchem-864	178	13	8.22	8.22	NUM
eurjchem-864	178	14	(	(	PUNCT
eurjchem-864	178	15	s	s	PROPN
eurjchem-864	178	16	,	,	PUNCT
eurjchem-864	178	17	1h	1h	NUM
eurjchem-864	178	18	,	,	PUNCT
eurjchem-864	178	19	ar‐h	ar‐h	NOUN
eurjchem-864	178	20	)	)	PUNCT
eurjchem-864	178	21	,	,	PUNCT
eurjchem-864	178	22	8.03	8.03	NUM
eurjchem-864	178	23	(	(	PUNCT
eurjchem-864	178	24	d	d	NOUN
eurjchem-864	178	25	,	,	PUNCT
eurjchem-864	178	26	j	j	PROPN
eurjchem-864	178	27	=	=	SYM
eurjchem-864	178	28	7.8	7.8	NUM
eurjchem-864	178	29	hz	hz	NOUN
eurjchem-864	178	30	,	,	PUNCT
eurjchem-864	178	31	1h	1h	NUM
eurjchem-864	178	32	,	,	PUNCT
eurjchem-864	178	33	ar‐h	ar‐h	NOUN
eurjchem-864	178	34	)	)	PUNCT
eurjchem-864	178	35	,	,	PUNCT
eurjchem-864	178	36	7.96	7.96	NUM
eurjchem-864	178	37	(	(	PUNCT
eurjchem-864	178	38	d	d	NOUN
eurjchem-864	178	39	,	,	PUNCT
eurjchem-864	178	40	j	j	PROPN
eurjchem-864	178	41	=	=	SYM
eurjchem-864	178	42	7.6	7.6	NUM
eurjchem-864	178	43	hz	hz	NOUN
eurjchem-864	178	44	,	,	PUNCT
eurjchem-864	178	45	1h	1h	NUM
eurjchem-864	178	46	,	,	PUNCT
eurjchem-864	178	47	ar‐h	ar‐h	NOUN
eurjchem-864	178	48	)	)	PUNCT
eurjchem-864	178	49	,	,	PUNCT
eurjchem-864	178	50	7.52	7.52	NUM
eurjchem-864	178	51	(	(	PUNCT
eurjchem-864	178	52	m	m	PROPN
eurjchem-864	178	53	,	,	PUNCT
eurjchem-864	178	54	2h	2h	NUM
eurjchem-864	178	55	,	,	PUNCT
eurjchem-864	178	56	ar‐h	ar‐h	NOUN
eurjchem-864	178	57	)	)	PUNCT
eurjchem-864	178	58	,	,	PUNCT
eurjchem-864	178	59	7.23	7.23	NUM
eurjchem-864	178	60	(	(	PUNCT
eurjchem-864	178	61	m	m	PROPN
eurjchem-864	178	62	,	,	PUNCT
eurjchem-864	178	63	1h	1h	NUM
eurjchem-864	178	64	,	,	PUNCT
eurjchem-864	178	65	ar‐h	ar‐h	NOUN
eurjchem-864	178	66	)	)	PUNCT
eurjchem-864	178	67	,	,	PUNCT
eurjchem-864	178	68	7.02	7.02	NUM
eurjchem-864	178	69	(	(	PUNCT
eurjchem-864	178	70	s	s	PROPN
eurjchem-864	178	71	,	,	PUNCT
eurjchem-864	178	72	1h	1h	NUM
eurjchem-864	178	73	,	,	PUNCT
eurjchem-864	178	74	ar‐h	ar‐h	NOUN
eurjchem-864	178	75	)	)	PUNCT
eurjchem-864	178	76	,	,	PUNCT
eurjchem-864	178	77	3.26‐3.36	3.26‐3.36	NUM
eurjchem-864	178	78	(	(	PUNCT
eurjchem-864	178	79	m	m	PROPN
eurjchem-864	178	80	,	,	PUNCT
eurjchem-864	178	81	8h	8h	NUM
eurjchem-864	178	82	,	,	PUNCT
eurjchem-864	178	83	ch2	ch2	PROPN
eurjchem-864	178	84	)	)	PUNCT
eurjchem-864	178	85	,	,	PUNCT
eurjchem-864	178	86	2.71	2.71	NUM
eurjchem-864	178	87	(	(	PUNCT
eurjchem-864	178	88	m	m	PROPN
eurjchem-864	178	89	,	,	PUNCT
eurjchem-864	178	90	1h	1h	NUM
eurjchem-864	178	91	,	,	PUNCT
eurjchem-864	178	92	ch	ch	NOUN
eurjchem-864	178	93	)	)	PUNCT
eurjchem-864	178	94	,	,	PUNCT
eurjchem-864	178	95	2.53	2.53	NUM
eurjchem-864	178	96	(	(	PUNCT
eurjchem-864	178	97	s	s	PROPN
eurjchem-864	178	98	,	,	PUNCT
eurjchem-864	178	99	3h	3h	NUM
eurjchem-864	178	100	,	,	PUNCT
eurjchem-864	178	101	ch3	ch3	PROPN
eurjchem-864	178	102	)	)	PUNCT
eurjchem-864	178	103	,	,	PUNCT
eurjchem-864	178	104	1.61‐1.83	1.61‐1.83	NUM
eurjchem-864	178	105	(	(	PUNCT
eurjchem-864	178	106	m	m	PROPN
eurjchem-864	178	107	,	,	PUNCT
eurjchem-864	178	108	8h	8h	NUM
eurjchem-864	178	109	,	,	PUNCT
eurjchem-864	178	110	ch2	ch2	PROPN
eurjchem-864	178	111	)	)	PUNCT
eurjchem-864	178	112	.	.	PUNCT
eurjchem-864	179	1	anal	anal	PROPN
eurjchem-864	179	2	.	.	PUNCT
eurjchem-864	179	3	calcd	calcd	NOUN
eurjchem-864	179	4	.	.	PUNCT
eurjchem-864	180	1	for	for	ADP
eurjchem-864	180	2	c29h27clfn3o5	c29h27clfn3o5	ADV
eurjchem-864	180	3	:	:	PUNCT
eurjchem-864	180	4	c	c	X
eurjchem-864	180	5	,	,	PUNCT
eurjchem-864	180	6	63.10	63.10	NUM
eurjchem-864	180	7	;	;	PUNCT
eurjchem-864	180	8	h	h	X
eurjchem-864	180	9	,	,	PUNCT
eurjchem-864	180	10	4.93	4.93	NUM
eurjchem-864	180	11	;	;	PUNCT
eurjchem-864	180	12	n	n	CCONJ
eurjchem-864	180	13	,	,	PUNCT
eurjchem-864	180	14	7.61	7.61	NUM
eurjchem-864	180	15	.	.	PUNCT
eurjchem-864	180	16	found	find	VERB
eurjchem-864	180	17	:	:	PUNCT
eurjchem-864	181	1	c	c	X
eurjchem-864	181	2	,	,	PUNCT
eurjchem-864	181	3	63.10	63.10	NUM
eurjchem-864	181	4	;	;	PUNCT
eurjchem-864	181	5	h	h	X
eurjchem-864	181	6	,	,	PUNCT
eurjchem-864	181	7	4.93	4.93	NUM
eurjchem-864	181	8	;	;	PUNCT
eurjchem-864	181	9	n	n	CCONJ
eurjchem-864	181	10	,	,	PUNCT
eurjchem-864	181	11	7.61	7.61	NUM
eurjchem-864	181	12	.	.	PUNCT
eurjchem-864	182	1	ms	ms	NOUN
eurjchem-864	182	2	(	(	PUNCT
eurjchem-864	182	3	m	m	PROPN
eurjchem-864	182	4	/	/	SYM
eurjchem-864	182	5	z	z	NOUN
eurjchem-864	182	6	):	):	PUNCT
eurjchem-864	182	7	553	553	NUM
eurjchem-864	182	8	(	(	PUNCT
eurjchem-864	182	9	m+1	m+1	NUM
eurjchem-864	182	10	)	)	PUNCT
eurjchem-864	182	11	.	.	PUNCT
eurjchem-864	183	1	table	table	NOUN
eurjchem-864	183	2	1	1	NUM
eurjchem-864	183	3	.	.	PUNCT
eurjchem-864	184	1	derivatives	derivative	NOUN
eurjchem-864	184	2	of	of	ADP
eurjchem-864	184	3	benzisoxazole	benzisoxazole	NOUN
eurjchem-864	184	4	.	.	PUNCT
eurjchem-864	185	1	entry	entry	NOUN
eurjchem-864	185	2	r	r	NOUN
eurjchem-864	185	3	(	(	PUNCT
eurjchem-864	185	4	8,9	8,9	NUM
eurjchem-864	185	5	)	)	PUNCT
eurjchem-864	185	6	compound	compound	NOUN
eurjchem-864	185	7	9	9	NUM
eurjchem-864	185	8	yield	yield	NOUN
eurjchem-864	185	9	,	,	PUNCT
eurjchem-864	185	10	%	%	NOUN
eurjchem-864	185	11	1	1	NUM
eurjchem-864	185	12	4‐clc6h4	4‐clc6h4	NUM
eurjchem-864	185	13	9a	9a	NOUN
eurjchem-864	185	14	81	81	NUM
eurjchem-864	185	15	2	2	NUM
eurjchem-864	185	16	4‐cme3c6h4	4‐cme3c6h4	NUM
eurjchem-864	185	17	9b	9b	NOUN
eurjchem-864	185	18	76	76	NUM
eurjchem-864	186	1	3	3	NUM
eurjchem-864	186	2	2,4‐cl2c6h3	2,4‐cl2c6h3	NUM
eurjchem-864	186	3	9c	9c	NUM
eurjchem-864	186	4	72	72	NUM
eurjchem-864	186	5	4	4	NUM
eurjchem-864	186	6	3‐brc6h4	3‐brc6h4	NUM
eurjchem-864	186	7	9d	9d	NOUN
eurjchem-864	186	8	83	83	NUM
eurjchem-864	186	9	5	5	NUM
eurjchem-864	186	10	3,5‐(no2)2c6h3	3,5‐(no2)2c6h3	NOUN
eurjchem-864	186	11	9e	9e	NUM
eurjchem-864	186	12	65	65	NUM
eurjchem-864	186	13	6	6	NUM
eurjchem-864	186	14	3,4,5‐(meo)3c6h2	3,4,5‐(meo)3c6h2	PROPN
eurjchem-864	186	15	9f	9f	NOUN
eurjchem-864	186	16	70	70	NUM
eurjchem-864	186	17	7	7	NUM
eurjchem-864	186	18	3‐no2c6h4	3‐no2c6h4	NUM
eurjchem-864	186	19	9	9	NUM
eurjchem-864	186	20	g	g	NOUN
eurjchem-864	186	21	68	68	NUM
eurjchem-864	186	22	8	8	NUM
eurjchem-864	186	23	4‐meoc6h4	4‐meoc6h4	NUM
eurjchem-864	186	24	9h	9h	NOUN
eurjchem-864	186	25	72	72	NUM
eurjchem-864	186	26	9	9	NUM
eurjchem-864	186	27	2,6‐f2c6h3	2,6‐f2c6h3	NUM
eurjchem-864	186	28	9i	9i	NOUN
eurjchem-864	186	29	60	60	NUM
eurjchem-864	186	30	10	10	NUM
eurjchem-864	186	31	3‐clc6h4	3‐clc6h4	NUM
eurjchem-864	186	32	9j	9j	NUM
eurjchem-864	186	33	73	73	NUM
eurjchem-864	186	34	2.3	2.3	NUM
eurjchem-864	186	35	.	.	PUNCT
eurjchem-864	187	1	biological	biological	ADJ
eurjchem-864	187	2	evaluation‐antibacterial	evaluation‐antibacterial	ADJ
eurjchem-864	187	3	,	,	PUNCT
eurjchem-864	187	4	antioxidant	antioxidant	ADJ
eurjchem-864	187	5	and	and	CCONJ
eurjchem-864	187	6	anti‐inflammatory	anti‐inflammatory	NOUN
eurjchem-864	187	7	activities	activity	NOUN
eurjchem-864	187	8	2.3.1	2.3.1	NUM
eurjchem-864	187	9	.	.	PUNCT
eurjchem-864	187	10	antibacterial	antibacterial	ADJ
eurjchem-864	187	11	activity	activity	NOUN
eurjchem-864	187	12	antibacterial	antibacterial	ADJ
eurjchem-864	187	13	tests	test	NOUN
eurjchem-864	187	14	were	be	AUX
eurjchem-864	187	15	carried	carry	VERB
eurjchem-864	187	16	out	out	ADP
eurjchem-864	187	17	by	by	ADP
eurjchem-864	187	18	disc	disc	NOUN
eurjchem-864	187	19	diffusion	diffusion	NOUN
eurjchem-864	187	20	method	method	NOUN
eurjchem-864	187	21	using	use	VERB
eurjchem-864	187	22	100	100	NUM
eurjchem-864	187	23	μl	μl	ADP
eurjchem-864	187	24	of	of	ADP
eurjchem-864	187	25	suspension	suspension	NOUN
eurjchem-864	187	26	containing	contain	VERB
eurjchem-864	187	27	106	106	NUM
eurjchem-864	187	28	cells	cell	NOUN
eurjchem-864	187	29	/	/	SYM
eurjchem-864	187	30	ml	ml	PROPN
eurjchem-864	187	31	of	of	ADP
eurjchem-864	187	32	bacteria	bacteria	NOUN
eurjchem-864	187	33	.	.	PUNCT
eurjchem-864	188	1	the	the	DET
eurjchem-864	188	2	discs	disc	NOUN
eurjchem-864	188	3	(	(	PUNCT
eurjchem-864	188	4	6	6	NUM
eurjchem-864	188	5	mm	mm	PROPN
eurjchem-864	188	6	diameter	diameter	NOUN
eurjchem-864	188	7	)	)	PUNCT
eurjchem-864	188	8	were	be	AUX
eurjchem-864	188	9	impregnated	impregnate	VERB
eurjchem-864	188	10	with	with	ADP
eurjchem-864	188	11	5	5	NUM
eurjchem-864	188	12	mg	mg	NOUN
eurjchem-864	188	13	and	and	CCONJ
eurjchem-864	188	14	10	10	NUM
eurjchem-864	188	15	mg	mg	NUM
eurjchem-864	188	16	/	/	SYM
eurjchem-864	188	17	ml	ml	NOUN
eurjchem-864	188	18	of	of	ADP
eurjchem-864	188	19	each	each	DET
eurjchem-864	188	20	compound	compound	NOUN
eurjchem-864	188	21	and	and	CCONJ
eurjchem-864	188	22	placed	place	VERB
eurjchem-864	188	23	on	on	ADP
eurjchem-864	188	24	the	the	DET
eurjchem-864	188	25	inoculated	inoculate	VERB
eurjchem-864	188	26	nutrient	nutrient	NOUN
eurjchem-864	188	27	agar	agar	NOUN
eurjchem-864	188	28	.	.	PUNCT
eurjchem-864	189	1	then	then	ADV
eurjchem-864	189	2	,	,	PUNCT
eurjchem-864	189	3	the	the	DET
eurjchem-864	189	4	inoculated	inoculate	VERB
eurjchem-864	189	5	plates	plate	NOUN
eurjchem-864	189	6	were	be	AUX
eurjchem-864	189	7	incubated	incubate	VERB
eurjchem-864	189	8	at	at	ADP
eurjchem-864	189	9	37±0.1	37±0.1	NUM
eurjchem-864	189	10	°	°	ADP
eurjchem-864	189	11	c	c	PROPN
eurjchem-864	189	12	at	at	ADP
eurjchem-864	189	13	24	24	NUM
eurjchem-864	189	14	h.	h.	NOUN
eurjchem-864	189	15	one	one	NUM
eurjchem-864	189	16	antibacterial	antibacterial	ADJ
eurjchem-864	189	17	drug	drug	NOUN
eurjchem-864	189	18	,	,	PUNCT
eurjchem-864	189	19	chloramphenicol	chloramphenicol	NOUN
eurjchem-864	189	20	was	be	AUX
eurjchem-864	189	21	used	use	VERB
eurjchem-864	189	22	as	as	ADP
eurjchem-864	189	23	positive	positive	ADJ
eurjchem-864	189	24	control	control	NOUN
eurjchem-864	189	25	.	.	PUNCT
eurjchem-864	190	1	antibacterial	antibacterial	ADJ
eurjchem-864	190	2	activity	activity	NOUN
eurjchem-864	190	3	was	be	AUX
eurjchem-864	190	4	evaluated	evaluate	VERB
eurjchem-864	190	5	by	by	ADP
eurjchem-864	190	6	measuring	measure	VERB
eurjchem-864	190	7	the	the	DET
eurjchem-864	190	8	zone	zone	NOUN
eurjchem-864	190	9	of	of	ADP
eurjchem-864	190	10	inhibition	inhibition	NOUN
eurjchem-864	190	11	against	against	ADP
eurjchem-864	190	12	the	the	DET
eurjchem-864	190	13	test	test	NOUN
eurjchem-864	190	14	organisms	organism	NOUN
eurjchem-864	190	15	and	and	CCONJ
eurjchem-864	190	16	the	the	DET
eurjchem-864	190	17	results	result	NOUN
eurjchem-864	190	18	are	be	AUX
eurjchem-864	190	19	summarised	summarise	VERB
eurjchem-864	190	20	in	in	ADP
eurjchem-864	190	21	table	table	NOUN
eurjchem-864	190	22	2	2	NUM
eurjchem-864	190	23	.	.	NOUN
eurjchem-864	190	24	2.3.2	2.3.2	NUM
eurjchem-864	190	25	.	.	PUNCT
eurjchem-864	191	1	antioxidant	antioxidant	ADJ
eurjchem-864	191	2	activity	activity	NOUN
eurjchem-864	191	3	2.3.2.1	2.3.2.1	PROPN
eurjchem-864	191	4	.	.	PUNCT
eurjchem-864	192	1	dpph	dpph	PROPN
eurjchem-864	192	2	radical	radical	ADJ
eurjchem-864	192	3	scavenging	scavenging	NOUN
eurjchem-864	192	4	assay	assay	PROPN
eurjchem-864	192	5	dpph	dpph	PROPN
eurjchem-864	192	6	radical	radical	ADJ
eurjchem-864	192	7	scavenging	scavenge	VERB
eurjchem-864	192	8	assays	assay	NOUN
eurjchem-864	192	9	[	[	X
eurjchem-864	192	10	15	15	NUM
eurjchem-864	192	11	]	]	PUNCT
eurjchem-864	192	12	were	be	AUX
eurjchem-864	192	13	performed	perform	VERB
eurjchem-864	192	14	in	in	ADP
eurjchem-864	192	15	300	300	NUM
eurjchem-864	192	16	µl	µl	ADP
eurjchem-864	192	17	reaction	reaction	NOUN
eurjchem-864	192	18	mixtures	mixture	NOUN
eurjchem-864	192	19	containing	contain	VERB
eurjchem-864	192	20	200	200	NUM
eurjchem-864	192	21	µl	µl	NOUN
eurjchem-864	192	22	of	of	ADP
eurjchem-864	192	23	0.1	0.1	NUM
eurjchem-864	192	24	mm	mm	NOUN
eurjchem-864	192	25	dpph‐	dpph‐	NOUN
eurjchem-864	192	26	ethanol	ethanol	NOUN
eurjchem-864	192	27	solution	solution	NOUN
eurjchem-864	192	28	,	,	PUNCT
eurjchem-864	192	29	90	90	NUM
eurjchem-864	192	30	µl	µl	NOUN
eurjchem-864	192	31	of	of	ADP
eurjchem-864	192	32	50	50	NUM
eurjchem-864	192	33	mm	mm	NOUN
eurjchem-864	192	34	tris‐hcl	tris‐hcl	NOUN
eurjchem-864	192	35	buffer	buffer	NOUN
eurjchem-864	192	36	(	(	PUNCT
eurjchem-864	192	37	ph	ph	NOUN
eurjchem-864	192	38	=	=	NOUN
eurjchem-864	192	39	7.4	7.4	NUM
eurjchem-864	192	40	)	)	PUNCT
eurjchem-864	192	41	,	,	PUNCT
eurjchem-864	192	42	and	and	CCONJ
eurjchem-864	192	43	10	10	NUM
eurjchem-864	192	44	µl	µl	NOUN
eurjchem-864	192	45	of	of	ADP
eurjchem-864	192	46	deionised	deionise	VERB
eurjchem-864	192	47	water	water	NOUN
eurjchem-864	192	48	(	(	PUNCT
eurjchem-864	192	49	as	as	ADP
eurjchem-864	192	50	control	control	NOUN
eurjchem-864	192	51	)	)	PUNCT
eurjchem-864	192	52	and	and	CCONJ
eurjchem-864	192	53	various	various	ADJ
eurjchem-864	192	54	concentrations	concentration	NOUN
eurjchem-864	192	55	of	of	ADP
eurjchem-864	192	56	compounds	compound	NOUN
eurjchem-864	192	57	9a‐j	9a‐j	NOUN
eurjchem-864	192	58	(	(	PUNCT
eurjchem-864	192	59	1.8‐9.0	1.8‐9.0	NUM
eurjchem-864	192	60	µm	µm	NOUN
eurjchem-864	192	61	)	)	PUNCT
eurjchem-864	192	62	.	.	PUNCT
eurjchem-864	193	1	ascorbic	ascorbic	NOUN
eurjchem-864	193	2	acid	acid	NOUN
eurjchem-864	193	3	was	be	AUX
eurjchem-864	193	4	used	use	VERB
eurjchem-864	193	5	as	as	ADP
eurjchem-864	193	6	a	a	DET
eurjchem-864	193	7	standard	standard	NOUN
eurjchem-864	193	8	.	.	PUNCT
eurjchem-864	194	1	after	after	ADP
eurjchem-864	194	2	30	30	NUM
eurjchem-864	194	3	min	min	NOUN
eurjchem-864	194	4	of	of	ADP
eurjchem-864	194	5	incubation	incubation	NOUN
eurjchem-864	194	6	at	at	ADP
eurjchem-864	194	7	room	room	NOUN
eurjchem-864	194	8	temperature	temperature	NOUN
eurjchem-864	194	9	,	,	PUNCT
eurjchem-864	194	10	absorbance	absorbance	NOUN
eurjchem-864	194	11	(	(	PUNCT
eurjchem-864	194	12	540	540	NUM
eurjchem-864	194	13	nm	nm	NOUN
eurjchem-864	194	14	)	)	PUNCT
eurjchem-864	194	15	of	of	ADP
eurjchem-864	194	16	the	the	DET
eurjchem-864	194	17	reaction	reaction	NOUN
eurjchem-864	194	18	mixtures	mixture	NOUN
eurjchem-864	194	19	was	be	AUX
eurjchem-864	194	20	taken	take	VERB
eurjchem-864	194	21	by	by	ADP
eurjchem-864	194	22	a	a	DET
eurjchem-864	194	23	plate	plate	NOUN
eurjchem-864	194	24	reader	reader	NOUN
eurjchem-864	194	25	(	(	PUNCT
eurjchem-864	194	26	lab	lab	NOUN
eurjchem-864	194	27	systems	system	NOUN
eurjchem-864	194	28	mullikan	mullikan	PROPN
eurjchem-864	194	29	ms	ms	PROPN
eurjchem-864	194	30	)	)	PUNCT
eurjchem-864	194	31	.	.	PUNCT
eurjchem-864	195	1	the	the	DET
eurjchem-864	195	2	percentage	percentage	NOUN
eurjchem-864	195	3	radical	radical	ADJ
eurjchem-864	195	4	scavenging	scavenge	VERB
eurjchem-864	195	5	activity	activity	NOUN
eurjchem-864	195	6	was	be	AUX
eurjchem-864	195	7	calculated	calculate	VERB
eurjchem-864	195	8	according	accord	VERB
eurjchem-864	195	9	to	to	ADP
eurjchem-864	195	10	equation	equation	NOUN
eurjchem-864	195	11	(	(	PUNCT
eurjchem-864	195	12	1	1	NUM
eurjchem-864	195	13	)	)	PUNCT
eurjchem-864	195	14	.	.	PUNCT
eurjchem-864	196	1	inhibition	inhibition	NOUN
eurjchem-864	196	2	(	(	PUNCT
eurjchem-864	196	3	%	%	INTJ
eurjchem-864	196	4	)	)	PUNCT
eurjchem-864	196	5	=	=	SYM
eurjchem-864	196	6	(	(	PUNCT
eurjchem-864	196	7	absorbance	absorbance	NOUN
eurjchem-864	196	8	control‐absorbance	control‐absorbance	NOUN
eurjchem-864	196	9	sample	sample	NOUN
eurjchem-864	196	10	/	/	SYM
eurjchem-864	196	11	absorbance	absorbance	NOUN
eurjchem-864	196	12	control	control	NOUN
eurjchem-864	196	13	)	)	PUNCT
eurjchem-864	196	14	×	×	NOUN
eurjchem-864	196	15	100	100	NUM
eurjchem-864	196	16	(	(	PUNCT
eurjchem-864	196	17	1	1	NUM
eurjchem-864	196	18	)	)	PUNCT
eurjchem-864	196	19	the	the	DET
eurjchem-864	196	20	dpph	dpph	PROPN
eurjchem-864	196	21	radical	radical	ADJ
eurjchem-864	196	22	scavenging	scavenge	VERB
eurjchem-864	196	23	activity	activity	NOUN
eurjchem-864	196	24	is	be	AUX
eurjchem-864	196	25	demonstrated	demonstrate	VERB
eurjchem-864	196	26	in	in	ADP
eurjchem-864	196	27	figure	figure	NOUN
eurjchem-864	196	28	1	1	NUM
eurjchem-864	196	29	and	and	CCONJ
eurjchem-864	196	30	table	table	NOUN
eurjchem-864	196	31	3	3	NUM
eurjchem-864	196	32	.	.	PUNCT
eurjchem-864	196	33	shivaprasad	shivaprasad	PROPN
eurjchem-864	196	34	et	et	PROPN
eurjchem-864	196	35	al	al	PROPN
eurjchem-864	196	36	.	.	PUNCT
eurjchem-864	196	37	/	/	SYM
eurjchem-864	196	38	european	european	PROPN
eurjchem-864	196	39	journal	journal	PROPN
eurjchem-864	196	40	of	of	ADP
eurjchem-864	196	41	chemistry	chemistry	NOUN
eurjchem-864	196	42	4	4	NUM
eurjchem-864	196	43	(	(	PUNCT
eurjchem-864	196	44	4	4	NUM
eurjchem-864	196	45	)	)	PUNCT
eurjchem-864	196	46	(	(	PUNCT
eurjchem-864	196	47	2013	2013	NUM
eurjchem-864	196	48	)	)	PUNCT
eurjchem-864	196	49	402‐407	402‐407	PROPN
eurjchem-864	196	50	405	405	NUM
eurjchem-864	196	51	table	table	NOUN
eurjchem-864	196	52	2	2	NUM
eurjchem-864	196	53	.	.	PUNCT
eurjchem-864	196	54	antibacterial	antibacterial	ADJ
eurjchem-864	196	55	activity	activity	NOUN
eurjchem-864	196	56	of	of	ADP
eurjchem-864	196	57	benzisoxazoles	benzisoxazole	NOUN
eurjchem-864	196	58	9a‐j	9a‐j	ADJ
eurjchem-864	196	59	.	.	PUNCT
eurjchem-864	197	1	compound	compound	NOUN
eurjchem-864	197	2	zone	zone	NOUN
eurjchem-864	197	3	of	of	ADP
eurjchem-864	197	4	inhibition	inhibition	NOUN
eurjchem-864	197	5	in	in	ADP
eurjchem-864	197	6	millimetre	millimetre	PROPN
eurjchem-864	197	7	*	*	PUNCT
eurjchem-864	197	8	escherichia	escherichia	NOUN
eurjchem-864	197	9	coli	coli	NOUN
eurjchem-864	197	10	bacillus	bacillus	NOUN
eurjchem-864	197	11	subtilis	subtili	NOUN
eurjchem-864	197	12	klebsiella	klebsiella	NOUN
eurjchem-864	197	13	pneumoniae	pneumoniae	ADJ
eurjchem-864	197	14	salmonella	salmonella	NOUN
eurjchem-864	197	15	typhi	typhi	VERB
eurjchem-864	197	16	shigella	shigella	PROPN
eurjchem-864	197	17	flexneri	flexneri	ADJ
eurjchem-864	197	18	9a	9a	NOUN
eurjchem-864	197	19	12	12	NUM
eurjchem-864	197	20	11	11	NUM
eurjchem-864	197	21	11	11	NUM
eurjchem-864	197	22	10	10	NUM
eurjchem-864	197	23	11	11	NUM
eurjchem-864	197	24	9b	9b	NOUN
eurjchem-864	197	25	13	13	NUM
eurjchem-864	197	26	12	12	NUM
eurjchem-864	197	27	9	9	NUM
eurjchem-864	197	28	12	12	NUM
eurjchem-864	197	29	9	9	NUM
eurjchem-864	197	30	9c	9c	NUM
eurjchem-864	197	31	14	14	NUM
eurjchem-864	197	32	‐	‐	ADV
eurjchem-864	197	33	10	10	NUM
eurjchem-864	197	34	‐	‐	NOUN
eurjchem-864	197	35	‐	‐	ADJ
eurjchem-864	197	36	9d	9d	NOUN
eurjchem-864	197	37	10	10	NUM
eurjchem-864	197	38	13	13	NUM
eurjchem-864	197	39	9	9	NUM
eurjchem-864	197	40	12	12	NUM
eurjchem-864	197	41	10	10	NUM
eurjchem-864	197	42	9e	9e	NOUN
eurjchem-864	197	43	16	16	NUM
eurjchem-864	197	44	15	15	NUM
eurjchem-864	197	45	16	16	NUM
eurjchem-864	197	46	22	22	NUM
eurjchem-864	197	47	26	26	NUM
eurjchem-864	197	48	9f	9f	NUM
eurjchem-864	197	49	10	10	NUM
eurjchem-864	197	50	15	15	NUM
eurjchem-864	197	51	11	11	NUM
eurjchem-864	197	52	11	11	NUM
eurjchem-864	197	53	9	9	NUM
eurjchem-864	197	54	9	9	NUM
eurjchem-864	197	55	g	g	NOUN
eurjchem-864	197	56	11	11	NUM
eurjchem-864	197	57	12	12	NUM
eurjchem-864	197	58	10	10	NUM
eurjchem-864	197	59	9	9	NUM
eurjchem-864	197	60	10	10	NUM
eurjchem-864	197	61	9h	9h	NOUN
eurjchem-864	197	62	12	12	NUM
eurjchem-864	197	63	‐	‐	NOUN
eurjchem-864	197	64	‐	‐	ADV
eurjchem-864	197	65	‐	‐	ADV
eurjchem-864	197	66	‐	‐	ADP
eurjchem-864	197	67	9i	9i	NOUN
eurjchem-864	197	68	‐	‐	NOUN
eurjchem-864	197	69	‐	‐	ADV
eurjchem-864	197	70	10	10	NUM
eurjchem-864	197	71	‐	‐	NOUN
eurjchem-864	197	72	‐	‐	NOUN
eurjchem-864	197	73	9j	9j	NOUN
eurjchem-864	197	74	17	17	NUM
eurjchem-864	197	75	‐	‐	NOUN
eurjchem-864	197	76	‐	‐	ADV
eurjchem-864	197	77	11	11	NUM
eurjchem-864	197	78	11	11	NUM
eurjchem-864	197	79	*	*	PUNCT
eurjchem-864	197	80	inhibition	inhibition	NOUN
eurjchem-864	197	81	zones	zone	NOUN
eurjchem-864	197	82	including	include	VERB
eurjchem-864	197	83	disc	disc	NOUN
eurjchem-864	197	84	(	(	PUNCT
eurjchem-864	197	85	6	6	NUM
eurjchem-864	197	86	mm	mm	NOUN
eurjchem-864	197	87	)	)	PUNCT
eurjchem-864	197	88	diameter	diameter	NOUN
eurjchem-864	197	89	,	,	PUNCT
eurjchem-864	197	90	positive	positive	ADJ
eurjchem-864	197	91	control	control	NOUN
eurjchem-864	197	92	zone	zone	NOUN
eurjchem-864	197	93	is	be	AUX
eurjchem-864	197	94	35	35	NUM
eurjchem-864	197	95	to	to	PART
eurjchem-864	197	96	40	40	NUM
eurjchem-864	197	97	mm	mm	NOUN
eurjchem-864	197	98	,	,	PUNCT
eurjchem-864	197	99	“	"	PUNCT
eurjchem-864	197	100	‐	‐	ADJ
eurjchem-864	197	101	“	"	PUNCT
eurjchem-864	197	102	=	=	NOUN
eurjchem-864	197	103	not	not	PART
eurjchem-864	197	104	active	active	ADJ
eurjchem-864	197	105	.	.	PUNCT
eurjchem-864	198	1	table	table	NOUN
eurjchem-864	198	2	3	3	NUM
eurjchem-864	198	3	.	.	PUNCT
eurjchem-864	198	4	antioxidant	antioxidant	ADJ
eurjchem-864	198	5	activity	activity	NOUN
eurjchem-864	198	6	of	of	ADP
eurjchem-864	198	7	benzisoxazoles	benzisoxazole	NOUN
eurjchem-864	198	8	9a‐j	9a‐j	ADJ
eurjchem-864	198	9	.	.	PUNCT
eurjchem-864	199	1	compound	compound	NOUN
eurjchem-864	199	2	ic50	ic50	PROPN
eurjchem-864	199	3	values	value	NOUN
eurjchem-864	199	4	in	in	ADP
eurjchem-864	199	5	µm	µm	ADP
eurjchem-864	199	6	dpph	dpph	NOUN
eurjchem-864	199	7	scavenging	scavenge	VERB
eurjchem-864	199	8	assay	assay	ADV
eurjchem-864	199	9	hydroxy	hydroxy	PROPN
eurjchem-864	199	10	radical	radical	ADJ
eurjchem-864	199	11	scavenging	scavenging	NOUN
eurjchem-864	199	12	assay	assay	NOUN
eurjchem-864	199	13	superoxide	superoxide	NOUN
eurjchem-864	199	14	radical	radical	ADJ
eurjchem-864	199	15	scavenging	scavenging	NOUN
eurjchem-864	199	16	assay	assay	NOUN
eurjchem-864	199	17	9a	9a	NOUN
eurjchem-864	199	18	7.0	7.0	NUM
eurjchem-864	199	19	7.5	7.5	NUM
eurjchem-864	199	20	7.3	7.3	NUM
eurjchem-864	199	21	9b	9b	NOUN
eurjchem-864	199	22	4.1	4.1	NUM
eurjchem-864	199	23	3.9	3.9	NUM
eurjchem-864	199	24	3.8	3.8	NUM
eurjchem-864	199	25	9c	9c	NUM
eurjchem-864	199	26	6.2	6.2	NUM
eurjchem-864	199	27	6.4	6.4	NUM
eurjchem-864	199	28	6.5	6.5	NUM
eurjchem-864	199	29	9d	9d	NOUN
eurjchem-864	199	30	7.9	7.9	NUM
eurjchem-864	199	31	8.2	8.2	NUM
eurjchem-864	199	32	8.2	8.2	NUM
eurjchem-864	199	33	9e	9e	NOUN
eurjchem-864	199	34	6.5	6.5	NUM
eurjchem-864	199	35	6.2	6.2	NUM
eurjchem-864	199	36	6.2	6.2	NUM
eurjchem-864	199	37	9f	9f	NOUN
eurjchem-864	199	38	4.9	4.9	NUM
eurjchem-864	199	39	4.6	4.6	NUM
eurjchem-864	199	40	4.1	4.1	NUM
eurjchem-864	199	41	9	9	NUM
eurjchem-864	199	42	g	g	ADP
eurjchem-864	199	43	6.8	6.8	NUM
eurjchem-864	199	44	6.8	6.8	NUM
eurjchem-864	199	45	6.8	6.8	NUM
eurjchem-864	199	46	9h	9h	NOUN
eurjchem-864	199	47	5.2	5.2	NUM
eurjchem-864	199	48	5.1	5.1	NUM
eurjchem-864	199	49	4.7	4.7	NUM
eurjchem-864	199	50	9i	9i	NOUN
eurjchem-864	199	51	8.5	8.5	NUM
eurjchem-864	199	52	8.5	8.5	NUM
eurjchem-864	199	53	8.5	8.5	NUM
eurjchem-864	199	54	9j	9j	NUM
eurjchem-864	199	55	7.4	7.4	NUM
eurjchem-864	199	56	8.0	8.0	NUM
eurjchem-864	199	57	7.8	7.8	NUM
eurjchem-864	199	58	ascorbic	ascorbic	NOUN
eurjchem-864	199	59	acid	acid	NOUN
eurjchem-864	199	60	3.5	3.5	NUM
eurjchem-864	199	61	3.4	3.4	NUM
eurjchem-864	199	62	‐	‐	NOUN
eurjchem-864	199	63	quercetin	quercetin	NOUN
eurjchem-864	199	64	‐	‐	NOUN
eurjchem-864	199	65	‐	‐	ADP
eurjchem-864	199	66	2.8	2.8	NUM
eurjchem-864	199	67	“	"	PUNCT
eurjchem-864	199	68	‐	‐	PROPN
eurjchem-864	199	69	“	"	PUNCT
eurjchem-864	199	70	=	=	NOUN
eurjchem-864	199	71	not	not	PART
eurjchem-864	199	72	active	active	ADJ
eurjchem-864	199	73	.	.	PUNCT
eurjchem-864	200	1	figure	figure	NOUN
eurjchem-864	200	2	1	1	NUM
eurjchem-864	200	3	.	.	PUNCT
eurjchem-864	201	1	dpph	dpph	PROPN
eurjchem-864	201	2	radical	radical	ADJ
eurjchem-864	201	3	scavenging	scavenging	NOUN
eurjchem-864	201	4	assay	assay	NOUN
eurjchem-864	201	5	.	.	PUNCT
eurjchem-864	202	1	2.3.2.2	2.3.2.2	X
eurjchem-864	202	2	.	.	PUNCT
eurjchem-864	202	3	hydroxyl	hydroxyl	PROPN
eurjchem-864	202	4	radical	radical	ADJ
eurjchem-864	202	5	scavenging	scavenging	NOUN
eurjchem-864	202	6	assay	assay	VERB
eurjchem-864	202	7	the	the	DET
eurjchem-864	202	8	reaction	reaction	NOUN
eurjchem-864	202	9	mixture	mixture	NOUN
eurjchem-864	202	10	in	in	ADP
eurjchem-864	202	11	final	final	ADJ
eurjchem-864	202	12	volume	volume	NOUN
eurjchem-864	202	13	of	of	ADP
eurjchem-864	202	14	2	2	NUM
eurjchem-864	202	15	ml	ml	NOUN
eurjchem-864	202	16	containing	contain	VERB
eurjchem-864	202	17	0.1	0.1	NUM
eurjchem-864	202	18	ml	ml	NOUN
eurjchem-864	202	19	of	of	ADP
eurjchem-864	202	20	edta	edta	NOUN
eurjchem-864	202	21	(	(	PUNCT
eurjchem-864	202	22	1	1	NUM
eurjchem-864	202	23	mm	mm	NOUN
eurjchem-864	202	24	)	)	PUNCT
eurjchem-864	202	25	,	,	PUNCT
eurjchem-864	202	26	0.01	0.01	NUM
eurjchem-864	202	27	ml	ml	NOUN
eurjchem-864	202	28	of	of	ADP
eurjchem-864	202	29	fecl3	fecl3	PROPN
eurjchem-864	202	30	(	(	PUNCT
eurjchem-864	202	31	10	10	NUM
eurjchem-864	202	32	mm	mm	NOUN
eurjchem-864	202	33	)	)	PUNCT
eurjchem-864	202	34	,	,	PUNCT
eurjchem-864	202	35	0.1	0.1	NUM
eurjchem-864	202	36	ml	ml	NOUN
eurjchem-864	202	37	of	of	ADP
eurjchem-864	202	38	h2o2	h2o2	PROPN
eurjchem-864	202	39	(	(	PUNCT
eurjchem-864	202	40	10	10	NUM
eurjchem-864	202	41	mm	mm	NOUN
eurjchem-864	202	42	)	)	PUNCT
eurjchem-864	202	43	,	,	PUNCT
eurjchem-864	202	44	0.36	0.36	NUM
eurjchem-864	202	45	ml	ml	NOUN
eurjchem-864	202	46	of	of	ADP
eurjchem-864	202	47	deoxyribose	deoxyribose	NOUN
eurjchem-864	202	48	(	(	PUNCT
eurjchem-864	202	49	10	10	NUM
eurjchem-864	202	50	mm	mm	NOUN
eurjchem-864	202	51	)	)	PUNCT
eurjchem-864	202	52	,	,	PUNCT
eurjchem-864	202	53	1	1	NUM
eurjchem-864	202	54	ml	ml	NOUN
eurjchem-864	202	55	of	of	ADP
eurjchem-864	202	56	the	the	DET
eurjchem-864	202	57	compounds	compound	NOUN
eurjchem-864	202	58	9a‐j	9a‐j	NOUN
eurjchem-864	202	59	(	(	PUNCT
eurjchem-864	202	60	concentrations	concentration	NOUN
eurjchem-864	202	61	from	from	ADP
eurjchem-864	202	62	1.8‐9.0	1.8‐9.0	NUM
eurjchem-864	202	63	µm	µm	NOUN
eurjchem-864	202	64	)	)	PUNCT
eurjchem-864	202	65	,	,	PUNCT
eurjchem-864	202	66	0.33	0.33	NUM
eurjchem-864	202	67	ml	ml	NOUN
eurjchem-864	202	68	of	of	ADP
eurjchem-864	202	69	phosphate	phosphate	ADJ
eurjchem-864	202	70	buffer	buffer	NOUN
eurjchem-864	202	71	(	(	PUNCT
eurjchem-864	202	72	50	50	NUM
eurjchem-864	202	73	mm	mm	NOUN
eurjchem-864	202	74	,	,	PUNCT
eurjchem-864	202	75	ph	ph	NOUN
eurjchem-864	202	76	=	=	NOUN
eurjchem-864	202	77	7.4	7.4	NUM
eurjchem-864	202	78	)	)	PUNCT
eurjchem-864	202	79	and	and	CCONJ
eurjchem-864	202	80	0.1	0.1	NUM
eurjchem-864	202	81	ml	ml	ADP
eurjchem-864	202	82	ascorbic	ascorbic	NOUN
eurjchem-864	202	83	acid	acid	NOUN
eurjchem-864	202	84	(	(	PUNCT
eurjchem-864	202	85	1	1	NUM
eurjchem-864	202	86	mm	mm	NOUN
eurjchem-864	202	87	)	)	PUNCT
eurjchem-864	202	88	added	add	VERB
eurjchem-864	202	89	in	in	ADP
eurjchem-864	202	90	sequence	sequence	NOUN
eurjchem-864	202	91	.	.	PUNCT
eurjchem-864	203	1	the	the	DET
eurjchem-864	203	2	mixture	mixture	NOUN
eurjchem-864	203	3	was	be	AUX
eurjchem-864	203	4	incubated	incubate	VERB
eurjchem-864	203	5	at	at	ADP
eurjchem-864	203	6	37	37	NUM
eurjchem-864	203	7	°	°	NOUN
eurjchem-864	203	8	c	c	NOUN
eurjchem-864	203	9	for	for	SCONJ
eurjchem-864	203	10	1	1	NUM
eurjchem-864	203	11	h.	h.	NOUN
eurjchem-864	203	12	1	1	NUM
eurjchem-864	203	13	ml	ml	NOUN
eurjchem-864	203	14	of	of	ADP
eurjchem-864	203	15	the	the	DET
eurjchem-864	203	16	incubated	incubate	VERB
eurjchem-864	203	17	mixture	mixture	NOUN
eurjchem-864	203	18	was	be	AUX
eurjchem-864	203	19	mixed	mix	VERB
eurjchem-864	203	20	with	with	ADP
eurjchem-864	203	21	1	1	NUM
eurjchem-864	203	22	ml	ml	NOUN
eurjchem-864	203	23	of	of	ADP
eurjchem-864	203	24	10	10	NUM
eurjchem-864	203	25	%	%	NOUN
eurjchem-864	203	26	trichloro	trichloro	NOUN
eurjchem-864	203	27	acetic	acetic	ADJ
eurjchem-864	203	28	acid	acid	NOUN
eurjchem-864	203	29	and	and	CCONJ
eurjchem-864	203	30	1	1	NUM
eurjchem-864	203	31	ml	ml	NOUN
eurjchem-864	203	32	of	of	ADP
eurjchem-864	203	33	tba	tba	NOUN
eurjchem-864	203	34	(	(	PUNCT
eurjchem-864	203	35	1	1	NUM
eurjchem-864	203	36	%	%	NOUN
eurjchem-864	203	37	in	in	ADP
eurjchem-864	203	38	0.025	0.025	NUM
eurjchem-864	203	39	m	m	NOUN
eurjchem-864	203	40	naoh	naoh	NOUN
eurjchem-864	203	41	)	)	PUNCT
eurjchem-864	203	42	,	,	PUNCT
eurjchem-864	203	43	the	the	DET
eurjchem-864	203	44	resulting	result	VERB
eurjchem-864	203	45	mixture	mixture	NOUN
eurjchem-864	203	46	was	be	AUX
eurjchem-864	203	47	incubated	incubate	VERB
eurjchem-864	203	48	in	in	ADP
eurjchem-864	203	49	water	water	NOUN
eurjchem-864	203	50	bath	bath	NOUN
eurjchem-864	203	51	at	at	ADP
eurjchem-864	203	52	90	90	NUM
eurjchem-864	203	53	°	°	NOUN
eurjchem-864	203	54	c	c	NOUN
eurjchem-864	203	55	for	for	SCONJ
eurjchem-864	203	56	20	20	NUM
eurjchem-864	203	57	min	min	NOUN
eurjchem-864	203	58	to	to	PART
eurjchem-864	203	59	develop	develop	VERB
eurjchem-864	203	60	a	a	DET
eurjchem-864	203	61	pink	pink	ADJ
eurjchem-864	203	62	chromogen	chromogen	NOUN
eurjchem-864	203	63	which	which	PRON
eurjchem-864	203	64	was	be	AUX
eurjchem-864	203	65	measured	measure	VERB
eurjchem-864	203	66	at	at	ADP
eurjchem-864	203	67	532	532	NUM
eurjchem-864	203	68	nm	nm	NOUN
eurjchem-864	204	1	[	[	X
eurjchem-864	204	2	16	16	NUM
eurjchem-864	204	3	]	]	PUNCT
eurjchem-864	204	4	.	.	PUNCT
eurjchem-864	205	1	ascorbic	ascorbic	NOUN
eurjchem-864	205	2	acid	acid	NOUN
eurjchem-864	205	3	was	be	AUX
eurjchem-864	205	4	used	use	VERB
eurjchem-864	205	5	as	as	ADP
eurjchem-864	205	6	a	a	DET
eurjchem-864	205	7	positive	positive	ADJ
eurjchem-864	205	8	control	control	NOUN
eurjchem-864	205	9	.	.	PUNCT
eurjchem-864	206	1	percentage	percentage	NOUN
eurjchem-864	206	2	inhibition	inhibition	NOUN
eurjchem-864	206	3	was	be	AUX
eurjchem-864	206	4	evaluated	evaluate	VERB
eurjchem-864	206	5	by	by	ADP
eurjchem-864	206	6	using	use	VERB
eurjchem-864	206	7	equation	equation	NOUN
eurjchem-864	206	8	(	(	PUNCT
eurjchem-864	206	9	2	2	NUM
eurjchem-864	206	10	)	)	PUNCT
eurjchem-864	206	11	.	.	PUNCT
eurjchem-864	207	1	inhibition	inhibition	NOUN
eurjchem-864	207	2	(	(	PUNCT
eurjchem-864	207	3	%	%	INTJ
eurjchem-864	207	4	)	)	PUNCT
eurjchem-864	207	5	=	=	SYM
eurjchem-864	207	6	(	(	PUNCT
eurjchem-864	207	7	absorbance	absorbance	NOUN
eurjchem-864	207	8	control‐absorbance	control‐absorbance	NOUN
eurjchem-864	207	9	sample	sample	NOUN
eurjchem-864	207	10	/	/	SYM
eurjchem-864	207	11	absorbance	absorbance	NOUN
eurjchem-864	207	12	control	control	NOUN
eurjchem-864	207	13	)	)	PUNCT
eurjchem-864	207	14	×	×	NOUN
eurjchem-864	207	15	100	100	NUM
eurjchem-864	207	16	(	(	PUNCT
eurjchem-864	207	17	2	2	NUM
eurjchem-864	207	18	)	)	PUNCT
eurjchem-864	207	19	the	the	DET
eurjchem-864	207	20	potency	potency	NOUN
eurjchem-864	207	21	of	of	ADP
eurjchem-864	207	22	benzisoxazoles	benzisoxazole	NOUN
eurjchem-864	207	23	for	for	ADP
eurjchem-864	207	24	hydroxyl	hydroxyl	NOUN
eurjchem-864	207	25	radical	radical	ADJ
eurjchem-864	207	26	scavenging	scavenge	VERB
eurjchem-864	207	27	activity	activity	NOUN
eurjchem-864	207	28	is	be	AUX
eurjchem-864	207	29	illustrated	illustrate	VERB
eurjchem-864	207	30	in	in	ADP
eurjchem-864	207	31	figure	figure	NOUN
eurjchem-864	207	32	2	2	NUM
eurjchem-864	207	33	and	and	CCONJ
eurjchem-864	207	34	table	table	NOUN
eurjchem-864	207	35	3	3	NUM
eurjchem-864	207	36	.	.	X
eurjchem-864	208	1	2.3.2.3	2.3.2.3	NUM
eurjchem-864	208	2	.	.	NOUN
eurjchem-864	208	3	superoxide	superoxide	NOUN
eurjchem-864	208	4	anion	anion	NOUN
eurjchem-864	208	5	radical	radical	ADJ
eurjchem-864	208	6	scavenging	scavenging	NOUN
eurjchem-864	208	7	assay	assay	NOUN
eurjchem-864	208	8	1	1	NUM
eurjchem-864	208	9	ml	ml	NOUN
eurjchem-864	208	10	of	of	ADP
eurjchem-864	208	11	nbt	nbt	NOUN
eurjchem-864	208	12	(	(	PUNCT
eurjchem-864	208	13	156	156	NUM
eurjchem-864	208	14	µm	µm	NOUN
eurjchem-864	208	15	nbt	nbt	VERB
eurjchem-864	208	16	in	in	ADP
eurjchem-864	208	17	100	100	NUM
eurjchem-864	208	18	mm	mm	NOUN
eurjchem-864	208	19	phosphate	phosphate	NOUN
eurjchem-864	208	20	buffer	buffer	NOUN
eurjchem-864	208	21	of	of	ADP
eurjchem-864	208	22	ph	ph	NOUN
eurjchem-864	208	23	=	=	NOUN
eurjchem-864	208	24	7.4	7.4	NUM
eurjchem-864	208	25	)	)	PUNCT
eurjchem-864	208	26	,	,	PUNCT
eurjchem-864	208	27	1	1	NUM
eurjchem-864	208	28	ml	ml	NOUN
eurjchem-864	208	29	of	of	ADP
eurjchem-864	208	30	nadh	nadh	NOUN
eurjchem-864	208	31	(	(	PUNCT
eurjchem-864	208	32	468	468	NUM
eurjchem-864	208	33	µm	µm	NOUN
eurjchem-864	208	34	in	in	ADP
eurjchem-864	208	35	100	100	NUM
eurjchem-864	208	36	mm	mm	NOUN
eurjchem-864	208	37	phosphate	phosphate	NOUN
eurjchem-864	208	38	buffer	buffer	NOUN
eurjchem-864	208	39	of	of	ADP
eurjchem-864	208	40	ph	ph	NOUN
eurjchem-864	208	41	=	=	NOUN
eurjchem-864	208	42	7.4	7.4	NUM
eurjchem-864	208	43	)	)	PUNCT
eurjchem-864	208	44	and	and	CCONJ
eurjchem-864	208	45	varying	vary	VERB
eurjchem-864	208	46	concentration	concentration	NOUN
eurjchem-864	208	47	of	of	ADP
eurjchem-864	208	48	compounds	compound	NOUN
eurjchem-864	208	49	9a‐j	9a‐j	NOUN
eurjchem-864	208	50	(	(	PUNCT
eurjchem-864	208	51	1.8‐	1.8‐	NUM
eurjchem-864	208	52	9.0	9.0	NUM
eurjchem-864	208	53	µm	µm	NOUN
eurjchem-864	208	54	)	)	PUNCT
eurjchem-864	208	55	were	be	AUX
eurjchem-864	208	56	mixed	mix	VERB
eurjchem-864	208	57	to	to	PART
eurjchem-864	208	58	give	give	VERB
eurjchem-864	208	59	a	a	DET
eurjchem-864	208	60	final	final	ADJ
eurjchem-864	208	61	volume	volume	NOUN
eurjchem-864	208	62	of	of	ADP
eurjchem-864	208	63	3	3	NUM
eurjchem-864	208	64	ml	ml	NOUN
eurjchem-864	208	65	.	.	PUNCT
eurjchem-864	209	1	the	the	DET
eurjchem-864	209	2	reaction	reaction	NOUN
eurjchem-864	209	3	was	be	AUX
eurjchem-864	209	4	started	start	VERB
eurjchem-864	209	5	by	by	ADP
eurjchem-864	209	6	the	the	DET
eurjchem-864	209	7	addition	addition	NOUN
eurjchem-864	209	8	of	of	ADP
eurjchem-864	209	9	100	100	NUM
eurjchem-864	209	10	µl	µl	NOUN
eurjchem-864	209	11	of	of	ADP
eurjchem-864	209	12	pms	pm	NOUN
eurjchem-864	209	13	(	(	PUNCT
eurjchem-864	209	14	60	60	NUM
eurjchem-864	209	15	µm	µm	NOUN
eurjchem-864	209	16	in	in	ADP
eurjchem-864	209	17	100	100	NUM
eurjchem-864	209	18	mm	mm	NOUN
eurjchem-864	209	19	phosphate	phosphate	NOUN
eurjchem-864	209	20	buffer	buffer	NOUN
eurjchem-864	209	21	of	of	ADP
eurjchem-864	209	22	ph	ph	NOUN
eurjchem-864	209	23	=	=	NOUN
eurjchem-864	209	24	7.4	7.4	NUM
eurjchem-864	209	25	)	)	PUNCT
eurjchem-864	209	26	.	.	PUNCT
eurjchem-864	210	1	the	the	DET
eurjchem-864	210	2	reaction	reaction	NOUN
eurjchem-864	210	3	mixture	mixture	NOUN
eurjchem-864	210	4	was	be	AUX
eurjchem-864	210	5	incubated	incubate	VERB
eurjchem-864	210	6	at	at	ADP
eurjchem-864	210	7	25	25	NUM
eurjchem-864	210	8	°	°	NOUN
eurjchem-864	210	9	c	c	NOUN
eurjchem-864	210	10	for	for	ADP
eurjchem-864	210	11	5	5	NUM
eurjchem-864	210	12	min	min	NOUN
eurjchem-864	210	13	and	and	CCONJ
eurjchem-864	210	14	the	the	DET
eurjchem-864	210	15	absorbance	absorbance	NOUN
eurjchem-864	210	16	was	be	AUX
eurjchem-864	210	17	measured	measure	VERB
eurjchem-864	210	18	at	at	ADP
eurjchem-864	210	19	560	560	NUM
eurjchem-864	210	20	nm	nm	NOUN
eurjchem-864	210	21	.	.	PUNCT
eurjchem-864	211	1	quercetin	quercetin	NOUN
eurjchem-864	211	2	was	be	AUX
eurjchem-864	211	3	used	use	VERB
eurjchem-864	211	4	as	as	ADP
eurjchem-864	211	5	a	a	DET
eurjchem-864	211	6	standard	standard	NOUN
eurjchem-864	211	7	[	[	X
eurjchem-864	211	8	17	17	NUM
eurjchem-864	211	9	]	]	PUNCT
eurjchem-864	211	10	.	.	PUNCT
eurjchem-864	212	1	decreased	decrease	VERB
eurjchem-864	212	2	absorbance	absorbance	NOUN
eurjchem-864	212	3	of	of	ADP
eurjchem-864	212	4	the	the	DET
eurjchem-864	212	5	reaction	reaction	NOUN
eurjchem-864	212	6	mixture	mixture	NOUN
eurjchem-864	212	7	indicated	indicate	VERB
eurjchem-864	212	8	increased	increase	VERB
eurjchem-864	212	9	superoxide	superoxide	NOUN
eurjchem-864	212	10	anion	anion	NOUN
eurjchem-864	212	11	scavenging	scavenge	VERB
eurjchem-864	212	12	activity	activity	NOUN
eurjchem-864	212	13	and	and	CCONJ
eurjchem-864	212	14	it	it	PRON
eurjchem-864	212	15	is	be	AUX
eurjchem-864	212	16	illustrated	illustrate	VERB
eurjchem-864	212	17	in	in	ADP
eurjchem-864	212	18	figure	figure	NOUN
eurjchem-864	212	19	3	3	NUM
eurjchem-864	212	20	and	and	CCONJ
eurjchem-864	212	21	table	table	NOUN
eurjchem-864	213	1	3	3	NUM
eurjchem-864	213	2	.	.	PUNCT
eurjchem-864	213	3	figure	figure	NOUN
eurjchem-864	213	4	2	2	NUM
eurjchem-864	213	5	.	.	PUNCT
eurjchem-864	213	6	hydroxyl	hydroxyl	PROPN
eurjchem-864	213	7	radical	radical	ADJ
eurjchem-864	213	8	scavenging	scavenging	NOUN
eurjchem-864	213	9	assay	assay	NOUN
eurjchem-864	213	10	.	.	PUNCT
eurjchem-864	214	1	figure	figure	VERB
eurjchem-864	214	2	3	3	NUM
eurjchem-864	214	3	.	.	PUNCT
eurjchem-864	214	4	super	super	ADJ
eurjchem-864	214	5	oxide	oxide	NOUN
eurjchem-864	214	6	radical	radical	ADJ
eurjchem-864	214	7	scavenging	scavenging	NOUN
eurjchem-864	214	8	assay	assay	NOUN
eurjchem-864	214	9	.	.	PUNCT
eurjchem-864	215	1	2.3.3	2.3.3	X
eurjchem-864	215	2	.	.	PUNCT
eurjchem-864	215	3	anti‐inflammatory	anti‐inflammatory	NOUN
eurjchem-864	215	4	activity	activity	NOUN
eurjchem-864	215	5	2.3.3.1	2.3.3.1	NUM
eurjchem-864	215	6	.	.	PUNCT
eurjchem-864	215	7	lipoxygenase	lipoxygenase	NOUN
eurjchem-864	215	8	inhibition	inhibition	NOUN
eurjchem-864	215	9	assay	assay	NOUN
eurjchem-864	215	10	lipoxygenase	lipoxygenase	NOUN
eurjchem-864	215	11	inhibition	inhibition	NOUN
eurjchem-864	215	12	assay	assay	VERB
eurjchem-864	215	13	[	[	X
eurjchem-864	215	14	18	18	NUM
eurjchem-864	215	15	]	]	PUNCT
eurjchem-864	215	16	was	be	AUX
eurjchem-864	215	17	carried	carry	VERB
eurjchem-864	215	18	out	out	ADP
eurjchem-864	215	19	using	use	VERB
eurjchem-864	215	20	linoleic	linoleic	ADJ
eurjchem-864	215	21	acid	acid	NOUN
eurjchem-864	215	22	as	as	ADP
eurjchem-864	215	23	substrate	substrate	NOUN
eurjchem-864	215	24	and	and	CCONJ
eurjchem-864	215	25	lipoxgenase	lipoxgenase	NOUN
eurjchem-864	215	26	enzyme	enzyme	NOUN
eurjchem-864	215	27	.	.	PUNCT
eurjchem-864	216	1	to	to	ADP
eurjchem-864	216	2	a	a	DET
eurjchem-864	216	3	solution	solution	NOUN
eurjchem-864	216	4	of	of	ADP
eurjchem-864	216	5	0.1	0.1	NUM
eurjchem-864	216	6	ml	ml	NOUN
eurjchem-864	216	7	of	of	ADP
eurjchem-864	216	8	0.2	0.2	NUM
eurjchem-864	216	9	m	m	NOUN
eurjchem-864	216	10	borate	borate	NOUN
eurjchem-864	216	11	buffer	buffer	NOUN
eurjchem-864	216	12	(	(	PUNCT
eurjchem-864	216	13	ph	ph	NOUN
eurjchem-864	216	14	=	=	NOUN
eurjchem-864	216	15	9.0	9.0	NUM
eurjchem-864	216	16	)	)	PUNCT
eurjchem-864	216	17	,	,	PUNCT
eurjchem-864	216	18	containing	contain	VERB
eurjchem-864	216	19	0.1	0.1	NUM
eurjchem-864	216	20	ml	ml	NOUN
eurjchem-864	216	21	of	of	ADP
eurjchem-864	216	22	1000	1000	NUM
eurjchem-864	216	23	units	unit	NOUN
eurjchem-864	216	24	lipoxidase	lipoxidase	NOUN
eurjchem-864	216	25	enzyme	enzyme	NOUN
eurjchem-864	216	26	,	,	PUNCT
eurjchem-864	216	27	solution	solution	NOUN
eurjchem-864	216	28	of	of	ADP
eurjchem-864	216	29	compounds	compound	NOUN
eurjchem-864	216	30	9a‐j	9a‐j	ADJ
eurjchem-864	216	31	in	in	ADP
eurjchem-864	216	32	dmso	dmso	NOUN
eurjchem-864	216	33	(	(	PUNCT
eurjchem-864	216	34	1	1	NUM
eurjchem-864	216	35	mg	mg	NUM
eurjchem-864	216	36	/	/	SYM
eurjchem-864	216	37	ml	ml	NOUN
eurjchem-864	216	38	)	)	PUNCT
eurjchem-864	216	39	was	be	AUX
eurjchem-864	216	40	added	add	VERB
eurjchem-864	216	41	and	and	CCONJ
eurjchem-864	216	42	incubated	incubate	VERB
eurjchem-864	216	43	with	with	ADP
eurjchem-864	216	44	the	the	DET
eurjchem-864	216	45	enzyme	enzyme	NOUN
eurjchem-864	216	46	with	with	ADP
eurjchem-864	216	47	various	various	ADJ
eurjchem-864	216	48	concentrations	concentration	NOUN
eurjchem-864	216	49	(	(	PUNCT
eurjchem-864	216	50	1.8‐9.0	1.8‐9.0	NUM
eurjchem-864	216	51	µm	µm	NOUN
eurjchem-864	216	52	)	)	PUNCT
eurjchem-864	216	53	.	.	PUNCT
eurjchem-864	217	1	406	406	NUM
eurjchem-864	217	2	shivaprasad	shivaprasad	PROPN
eurjchem-864	217	3	et	et	PROPN
eurjchem-864	217	4	al	al	PROPN
eurjchem-864	217	5	.	.	PUNCT
eurjchem-864	217	6	/	/	SYM
eurjchem-864	217	7	european	european	PROPN
eurjchem-864	217	8	journal	journal	PROPN
eurjchem-864	217	9	of	of	ADP
eurjchem-864	217	10	chemistry	chemistry	NOUN
eurjchem-864	217	11	4	4	NUM
eurjchem-864	217	12	(	(	PUNCT
eurjchem-864	217	13	4	4	NUM
eurjchem-864	217	14	)	)	PUNCT
eurjchem-864	217	15	(	(	PUNCT
eurjchem-864	217	16	2013	2013	NUM
eurjchem-864	217	17	)	)	PUNCT
eurjchem-864	217	18	402‐407	402‐407	PROPN
eurjchem-864	217	19	table	table	NOUN
eurjchem-864	217	20	4	4	NUM
eurjchem-864	217	21	.	.	PUNCT
eurjchem-864	217	22	anti‐inflammatory	anti‐inflammatory	NOUN
eurjchem-864	217	23	activity	activity	NOUN
eurjchem-864	217	24	of	of	ADP
eurjchem-864	217	25	benzisoxazoles	benzisoxazole	NOUN
eurjchem-864	217	26	9a‐j	9a‐j	ADJ
eurjchem-864	217	27	.	.	PUNCT
eurjchem-864	218	1	compound	compound	NOUN
eurjchem-864	218	2	ic50	ic50	PROPN
eurjchem-864	218	3	values	value	NOUN
eurjchem-864	218	4	in	in	ADP
eurjchem-864	218	5	µm	µm	ADP
eurjchem-864	218	6	lipoxygenase	lipoxygenase	NOUN
eurjchem-864	218	7	inhibition	inhibition	NOUN
eurjchem-864	218	8	assay	assay	VERB
eurjchem-864	218	9	pla2	pla2	NOUN
eurjchem-864	218	10	inhibition	inhibition	VERB
eurjchem-864	218	11	assay	assay	ADV
eurjchem-864	218	12	9a	9a	NOUN
eurjchem-864	218	13	8.6	8.6	NUM
eurjchem-864	218	14	79.0	79.0	NUM
eurjchem-864	218	15	9b	9b	NOUN
eurjchem-864	218	16	4.1	4.1	NUM
eurjchem-864	218	17	37.4	37.4	NUM
eurjchem-864	218	18	9c	9c	NUM
eurjchem-864	218	19	6.2	6.2	NUM
eurjchem-864	218	20	62.7	62.7	NUM
eurjchem-864	218	21	9d	9d	NOUN
eurjchem-864	218	22	7.9	7.9	NUM
eurjchem-864	218	23	76.9	76.9	NUM
eurjchem-864	218	24	9e	9e	NOUN
eurjchem-864	218	25	3.9	3.9	NUM
eurjchem-864	218	26	40.3	40.3	NUM
eurjchem-864	218	27	9f	9f	NOUN
eurjchem-864	218	28	5.0	5.0	NUM
eurjchem-864	218	29	49.8	49.8	NUM
eurjchem-864	218	30	9	9	NUM
eurjchem-864	218	31	g	g	ADP
eurjchem-864	218	32	3.9	3.9	NUM
eurjchem-864	218	33	40.5	40.5	NUM
eurjchem-864	218	34	9h	9h	NOUN
eurjchem-864	218	35	5.2	5.2	NUM
eurjchem-864	218	36	53.0	53.0	NUM
eurjchem-864	218	37	9i	9i	NOUN
eurjchem-864	218	38	8.5	8.5	NUM
eurjchem-864	218	39	81.1	81.1	NUM
eurjchem-864	218	40	9j	9j	NUM
eurjchem-864	218	41	7.4	7.4	NUM
eurjchem-864	218	42	75.3	75.3	NUM
eurjchem-864	218	43	indomethacin	indomethacin	VERB
eurjchem-864	218	44	3.0	3.0	NUM
eurjchem-864	218	45	‐	‐	NOUN
eurjchem-864	218	46	aristolochic	aristolochic	ADJ
eurjchem-864	218	47	acid	acid	NOUN
eurjchem-864	218	48	‐	‐	ADV
eurjchem-864	218	49	30.0	30.0	NUM
eurjchem-864	218	50	“	"	PUNCT
eurjchem-864	218	51	‐	‐	PROPN
eurjchem-864	218	52	“	"	PUNCT
eurjchem-864	218	53	=	=	PRON
eurjchem-864	218	54	not	not	PART
eurjchem-864	218	55	determined	determine	VERB
eurjchem-864	218	56	.	.	PUNCT
eurjchem-864	219	1	the	the	DET
eurjchem-864	219	2	tubes	tube	NOUN
eurjchem-864	219	3	were	be	AUX
eurjchem-864	219	4	agitated	agitate	VERB
eurjchem-864	219	5	and	and	CCONJ
eurjchem-864	219	6	incubated	incubate	VERB
eurjchem-864	219	7	at	at	ADP
eurjchem-864	219	8	room	room	NOUN
eurjchem-864	219	9	temperature	temperature	NOUN
eurjchem-864	219	10	for	for	ADP
eurjchem-864	219	11	5	5	NUM
eurjchem-864	219	12	min	min	NOUN
eurjchem-864	219	13	,	,	PUNCT
eurjchem-864	219	14	after	after	ADP
eurjchem-864	219	15	which	which	PRON
eurjchem-864	219	16	2.0	2.0	NUM
eurjchem-864	219	17	ml	ml	NOUN
eurjchem-864	219	18	of	of	ADP
eurjchem-864	219	19	substrate	substrate	NOUN
eurjchem-864	219	20	solution	solution	NOUN
eurjchem-864	219	21	,	,	PUNCT
eurjchem-864	219	22	0.6	0.6	NUM
eurjchem-864	219	23	mm	mm	PROPN
eurjchem-864	219	24	linoleum	linoleum	NOUN
eurjchem-864	219	25	acid	acid	NOUN
eurjchem-864	219	26	were	be	AUX
eurjchem-864	219	27	added	add	VERB
eurjchem-864	219	28	,	,	PUNCT
eurjchem-864	219	29	mixed	mix	VERB
eurjchem-864	219	30	well	well	ADV
eurjchem-864	219	31	and	and	CCONJ
eurjchem-864	219	32	the	the	DET
eurjchem-864	219	33	absorbance	absorbance	NOUN
eurjchem-864	219	34	was	be	AUX
eurjchem-864	219	35	measured	measure	VERB
eurjchem-864	219	36	spectrophotometrically	spectrophotometrically	ADV
eurjchem-864	219	37	for	for	ADP
eurjchem-864	219	38	4	4	NUM
eurjchem-864	219	39	min	min	NOUN
eurjchem-864	219	40	at	at	ADP
eurjchem-864	219	41	234	234	NUM
eurjchem-864	219	42	nm	nm	NOUN
eurjchem-864	219	43	(	(	PUNCT
eurjchem-864	219	44	shimadzu‐2401	shimadzu‐2401	PROPN
eurjchem-864	219	45	pc	pc	PROPN
eurjchem-864	219	46	)	)	PUNCT
eurjchem-864	219	47	.	.	PUNCT
eurjchem-864	220	1	indomethacin	indomethacin	PROPN
eurjchem-864	220	2	was	be	AUX
eurjchem-864	220	3	used	use	VERB
eurjchem-864	220	4	as	as	ADP
eurjchem-864	220	5	a	a	DET
eurjchem-864	220	6	reference	reference	NOUN
eurjchem-864	220	7	standard	standard	ADJ
eurjchem-864	220	8	drug	drug	NOUN
eurjchem-864	220	9	.	.	PUNCT
eurjchem-864	221	1	percentage	percentage	NOUN
eurjchem-864	221	2	(	(	PUNCT
eurjchem-864	221	3	%	%	NOUN
eurjchem-864	221	4	)	)	PUNCT
eurjchem-864	221	5	inhibition	inhibition	NOUN
eurjchem-864	221	6	was	be	AUX
eurjchem-864	221	7	calculated	calculate	VERB
eurjchem-864	221	8	by	by	ADP
eurjchem-864	221	9	equation	equation	NOUN
eurjchem-864	221	10	(	(	PUNCT
eurjchem-864	221	11	3	3	NUM
eurjchem-864	221	12	)	)	PUNCT
eurjchem-864	221	13	.	.	PUNCT
eurjchem-864	222	1	inhibition	inhibition	NOUN
eurjchem-864	222	2	(	(	PUNCT
eurjchem-864	222	3	%	%	INTJ
eurjchem-864	222	4	)	)	PUNCT
eurjchem-864	222	5	=	=	SYM
eurjchem-864	222	6	(	(	PUNCT
eurjchem-864	222	7	absorbance	absorbance	NOUN
eurjchem-864	222	8	control‐absorbance	control‐absorbance	NOUN
eurjchem-864	222	9	sample	sample	NOUN
eurjchem-864	222	10	/	/	SYM
eurjchem-864	222	11	absorbance	absorbance	NOUN
eurjchem-864	222	12	control	control	NOUN
eurjchem-864	222	13	)	)	PUNCT
eurjchem-864	222	14	×	×	NOUN
eurjchem-864	222	15	100	100	NUM
eurjchem-864	222	16	(	(	PUNCT
eurjchem-864	222	17	3	3	NUM
eurjchem-864	222	18	)	)	PUNCT
eurjchem-864	222	19	lipoxygenase	lipoxygenase	NOUN
eurjchem-864	222	20	inhibition	inhibition	NOUN
eurjchem-864	222	21	activity	activity	NOUN
eurjchem-864	222	22	of	of	ADP
eurjchem-864	222	23	benzisoxazoles	benzisoxazole	NOUN
eurjchem-864	222	24	is	be	AUX
eurjchem-864	222	25	summarised	summarise	VERB
eurjchem-864	222	26	in	in	ADP
eurjchem-864	222	27	figure	figure	NOUN
eurjchem-864	222	28	4	4	NUM
eurjchem-864	222	29	and	and	CCONJ
eurjchem-864	222	30	table	table	NOUN
eurjchem-864	222	31	4	4	NUM
eurjchem-864	222	32	.	.	PUNCT
eurjchem-864	222	33	figure	figure	VERB
eurjchem-864	222	34	4	4	NUM
eurjchem-864	222	35	.	.	PUNCT
eurjchem-864	222	36	lipoxygenase	lipoxygenase	NOUN
eurjchem-864	222	37	inhibition	inhibition	NOUN
eurjchem-864	222	38	assay	assay	VERB
eurjchem-864	222	39	.	.	PUNCT
eurjchem-864	223	1	2.3.3.2	2.3.3.2	X
eurjchem-864	223	2	.	.	X
eurjchem-864	223	3	inhibition	inhibition	NOUN
eurjchem-864	223	4	of	of	ADP
eurjchem-864	223	5	pla2	pla2	NOUN
eurjchem-864	223	6	induced	induce	VERB
eurjchem-864	223	7	haemolysis	haemolysis	NOUN
eurjchem-864	223	8	in	in	ADP
eurjchem-864	223	9	human	human	ADJ
eurjchem-864	223	10	erythrocytes	erythrocyte	NOUN
eurjchem-864	223	11	the	the	DET
eurjchem-864	223	12	substrate	substrate	NOUN
eurjchem-864	223	13	for	for	ADP
eurjchem-864	223	14	indirect	indirect	ADJ
eurjchem-864	223	15	hemolytic	hemolytic	ADJ
eurjchem-864	223	16	activity	activity	NOUN
eurjchem-864	223	17	was	be	AUX
eurjchem-864	223	18	prepared	prepare	VERB
eurjchem-864	223	19	by	by	ADP
eurjchem-864	223	20	suspending	suspend	VERB
eurjchem-864	223	21	1	1	NUM
eurjchem-864	223	22	ml	ml	NOUN
eurjchem-864	223	23	of	of	ADP
eurjchem-864	223	24	fresh	fresh	ADJ
eurjchem-864	223	25	human	human	ADJ
eurjchem-864	223	26	red	red	ADJ
eurjchem-864	223	27	blood	blood	NOUN
eurjchem-864	223	28	cells	cell	NOUN
eurjchem-864	223	29	and	and	CCONJ
eurjchem-864	223	30	1	1	NUM
eurjchem-864	223	31	ml	ml	NOUN
eurjchem-864	223	32	of	of	ADP
eurjchem-864	223	33	fresh	fresh	ADJ
eurjchem-864	223	34	hen	hen	NOUN
eurjchem-864	223	35	’s	’s	PART
eurjchem-864	223	36	egg	egg	NOUN
eurjchem-864	223	37	yolk	yolk	NOUN
eurjchem-864	223	38	in	in	ADP
eurjchem-864	223	39	8	8	NUM
eurjchem-864	223	40	ml	ml	NOUN
eurjchem-864	223	41	of	of	ADP
eurjchem-864	223	42	phosphate	phosphate	ADJ
eurjchem-864	223	43	buffered	buffer	VERB
eurjchem-864	223	44	saline	saline	NOUN
eurjchem-864	223	45	.	.	PUNCT
eurjchem-864	224	1	1	1	NUM
eurjchem-864	224	2	ml	ml	NOUN
eurjchem-864	224	3	of	of	ADP
eurjchem-864	224	4	suspension	suspension	NOUN
eurjchem-864	224	5	was	be	AUX
eurjchem-864	224	6	incubated	incubate	VERB
eurjchem-864	224	7	with	with	ADP
eurjchem-864	224	8	4‐28	4‐28	NUM
eurjchem-864	224	9	μg	μg	NOUN
eurjchem-864	224	10	of	of	ADP
eurjchem-864	224	11	partially	partially	ADV
eurjchem-864	224	12	purified	purify	VERB
eurjchem-864	224	13	venom	venom	NOUN
eurjchem-864	224	14	for	for	ADP
eurjchem-864	224	15	45	45	NUM
eurjchem-864	224	16	min	min	NOUN
eurjchem-864	224	17	at	at	ADP
eurjchem-864	224	18	37	37	NUM
eurjchem-864	224	19	°	°	ADP
eurjchem-864	224	20	c	c	NOUN
eurjchem-864	224	21	and	and	CCONJ
eurjchem-864	224	22	the	the	DET
eurjchem-864	224	23	reaction	reaction	NOUN
eurjchem-864	224	24	was	be	AUX
eurjchem-864	224	25	stopped	stop	VERB
eurjchem-864	224	26	by	by	ADP
eurjchem-864	224	27	the	the	DET
eurjchem-864	224	28	addition	addition	NOUN
eurjchem-864	224	29	of	of	ADP
eurjchem-864	224	30	9	9	NUM
eurjchem-864	224	31	ml	ml	NOUN
eurjchem-864	224	32	of	of	ADP
eurjchem-864	224	33	ice	ice	NOUN
eurjchem-864	224	34	cold	cold	PROPN
eurjchem-864	224	35	pbs	pbs	PROPN
eurjchem-864	224	36	.	.	PUNCT
eurjchem-864	225	1	the	the	DET
eurjchem-864	225	2	suspension	suspension	NOUN
eurjchem-864	225	3	was	be	AUX
eurjchem-864	225	4	centrifuged	centrifuge	VERB
eurjchem-864	225	5	at	at	ADP
eurjchem-864	225	6	2000	2000	NUM
eurjchem-864	225	7	rpm	rpm	NOUN
eurjchem-864	225	8	for	for	ADP
eurjchem-864	225	9	20	20	NUM
eurjchem-864	225	10	min	min	NOUN
eurjchem-864	225	11	and	and	CCONJ
eurjchem-864	225	12	then	then	ADV
eurjchem-864	225	13	the	the	DET
eurjchem-864	225	14	released	release	VERB
eurjchem-864	225	15	haemoglobin	haemoglobin	NOUN
eurjchem-864	225	16	was	be	AUX
eurjchem-864	225	17	read	read	VERB
eurjchem-864	225	18	at	at	ADP
eurjchem-864	225	19	540	540	NUM
eurjchem-864	225	20	nm	nm	NOUN
eurjchem-864	225	21	.	.	PUNCT
eurjchem-864	226	1	10	10	NUM
eurjchem-864	226	2	μg	μg	PROPN
eurjchem-864	226	3	of	of	ADP
eurjchem-864	226	4	venom	venom	NOUN
eurjchem-864	226	5	sample	sample	NOUN
eurjchem-864	226	6	(	(	PUNCT
eurjchem-864	226	7	secretory‐pla2	secretory‐pla2	PROPN
eurjchem-864	226	8	purchased	purchase	VERB
eurjchem-864	226	9	from	from	ADP
eurjchem-864	226	10	sigma	sigma	PROPN
eurjchem-864	226	11	)	)	PUNCT
eurjchem-864	226	12	was	be	AUX
eurjchem-864	226	13	incubated	incubate	VERB
eurjchem-864	226	14	with	with	ADP
eurjchem-864	226	15	various	various	ADJ
eurjchem-864	226	16	concentration	concentration	NOUN
eurjchem-864	226	17	of	of	ADP
eurjchem-864	226	18	compounds	compound	NOUN
eurjchem-864	226	19	9a‐j	9a‐j	NOUN
eurjchem-864	226	20	(	(	PUNCT
eurjchem-864	226	21	1	1	NUM
eurjchem-864	226	22	mg	mg	NUM
eurjchem-864	226	23	/	/	SYM
eurjchem-864	226	24	ml	ml	X
eurjchem-864	226	25	in	in	ADP
eurjchem-864	226	26	dmso	dmso	NOUN
eurjchem-864	226	27	)	)	PUNCT
eurjchem-864	226	28	for	for	ADP
eurjchem-864	226	29	30	30	NUM
eurjchem-864	226	30	min	min	NOUN
eurjchem-864	226	31	at	at	ADP
eurjchem-864	226	32	room	room	NOUN
eurjchem-864	226	33	temperature	temperature	NOUN
eurjchem-864	226	34	and	and	CCONJ
eurjchem-864	226	35	1	1	NUM
eurjchem-864	226	36	ml	ml	NOUN
eurjchem-864	226	37	of	of	ADP
eurjchem-864	226	38	substrate	substrate	NOUN
eurjchem-864	226	39	was	be	AUX
eurjchem-864	226	40	added	add	VERB
eurjchem-864	226	41	,	,	PUNCT
eurjchem-864	226	42	again	again	ADV
eurjchem-864	226	43	incubated	incubate	VERB
eurjchem-864	226	44	for	for	ADP
eurjchem-864	226	45	30	30	NUM
eurjchem-864	226	46	min	min	NOUN
eurjchem-864	226	47	at	at	ADP
eurjchem-864	226	48	room	room	NOUN
eurjchem-864	226	49	temperature	temperature	NOUN
eurjchem-864	226	50	and	and	CCONJ
eurjchem-864	226	51	the	the	DET
eurjchem-864	226	52	reaction	reaction	NOUN
eurjchem-864	226	53	was	be	AUX
eurjchem-864	226	54	stopped	stop	VERB
eurjchem-864	226	55	by	by	ADP
eurjchem-864	226	56	adding	add	VERB
eurjchem-864	226	57	9	9	NUM
eurjchem-864	226	58	ml	ml	NOUN
eurjchem-864	226	59	of	of	ADP
eurjchem-864	226	60	ice	ice	NOUN
eurjchem-864	226	61	cold	cold	ADJ
eurjchem-864	226	62	pbs	pbs	PROPN
eurjchem-864	226	63	to	to	ADP
eurjchem-864	226	64	all	all	DET
eurjchem-864	226	65	test	test	NOUN
eurjchem-864	226	66	tubes	tube	NOUN
eurjchem-864	226	67	and	and	CCONJ
eurjchem-864	226	68	centrifuged	centrifuge	VERB
eurjchem-864	226	69	at	at	ADP
eurjchem-864	226	70	2000	2000	NUM
eurjchem-864	226	71	rpm	rpm	NOUN
eurjchem-864	226	72	for	for	ADP
eurjchem-864	226	73	10	10	NUM
eurjchem-864	226	74	min	min	NOUN
eurjchem-864	226	75	.	.	PROPN
eurjchem-864	226	76	finally	finally	ADV
eurjchem-864	226	77	absorbance	absorbance	NOUN
eurjchem-864	226	78	was	be	AUX
eurjchem-864	226	79	measured	measure	VERB
eurjchem-864	226	80	at	at	ADP
eurjchem-864	226	81	540	540	NUM
eurjchem-864	226	82	nm	nm	NOUN
eurjchem-864	227	1	[	[	X
eurjchem-864	227	2	19	19	NUM
eurjchem-864	227	3	]	]	PUNCT
eurjchem-864	227	4	and	and	CCONJ
eurjchem-864	227	5	inhibitory	inhibitory	ADJ
eurjchem-864	227	6	activities	activity	NOUN
eurjchem-864	227	7	are	be	AUX
eurjchem-864	227	8	summarised	summarise	VERB
eurjchem-864	227	9	in	in	ADP
eurjchem-864	227	10	figure	figure	NOUN
eurjchem-864	227	11	5	5	NUM
eurjchem-864	227	12	and	and	CCONJ
eurjchem-864	227	13	table	table	NOUN
eurjchem-864	227	14	4	4	NUM
eurjchem-864	227	15	.	.	NOUN
eurjchem-864	227	16	3	3	NUM
eurjchem-864	227	17	.	.	NOUN
eurjchem-864	227	18	results	result	NOUN
eurjchem-864	227	19	and	and	CCONJ
eurjchem-864	227	20	discussion	discussion	NOUN
eurjchem-864	227	21	sodium	sodium	NOUN
eurjchem-864	227	22	methoxide	methoxide	NOUN
eurjchem-864	227	23	induced	induce	VERB
eurjchem-864	227	24	cyclocondensation	cyclocondensation	NOUN
eurjchem-864	227	25	of	of	ADP
eurjchem-864	227	26	tert‐butyl	tert‐butyl	ADP
eurjchem-864	227	27	4‐oxopiperidine‐1‐carboxylate	4‐oxopiperidine‐1‐carboxylate	PROPN
eurjchem-864	227	28	(	(	PUNCT
eurjchem-864	227	29	1	1	NUM
eurjchem-864	227	30	)	)	PUNCT
eurjchem-864	227	31	and	and	CCONJ
eurjchem-864	227	32	dimethyl	dimethyl	NOUN
eurjchem-864	227	33	2‐methylene	2‐methylene	NUM
eurjchem-864	227	34	succinate	succinate	NOUN
eurjchem-864	227	35	(	(	PUNCT
eurjchem-864	227	36	2	2	NUM
eurjchem-864	227	37	)	)	PUNCT
eurjchem-864	227	38	in	in	ADP
eurjchem-864	227	39	thf	thf	NOUN
eurjchem-864	227	40	to	to	PART
eurjchem-864	227	41	afford	afford	VERB
eurjchem-864	227	42	8‐tert‐butyl	8‐tert‐butyl	NUM
eurjchem-864	227	43	4‐methyl	4‐methyl	PROPN
eurjchem-864	227	44	3‐methyl‐	3‐methyl‐	NUM
eurjchem-864	227	45	2‐oxo‐1‐oxa‐8‐azaspiro[4.5]dec‐3‐ene‐4,8‐dicarboxylate	2‐oxo‐1‐oxa‐8‐azaspiro[4.5]dec‐3‐ene‐4,8‐dicarboxylate	NUM
eurjchem-864	227	46	(	(	PUNCT
eurjchem-864	227	47	3	3	NUM
eurjchem-864	227	48	)	)	PUNCT
eurjchem-864	227	49	in	in	ADP
eurjchem-864	227	50	70	70	NUM
eurjchem-864	227	51	%	%	NOUN
eurjchem-864	227	52	yield	yield	NOUN
eurjchem-864	227	53	(	(	PUNCT
eurjchem-864	227	54	via	via	ADP
eurjchem-864	227	55	formation	formation	NOUN
eurjchem-864	227	56	of	of	ADP
eurjchem-864	227	57	β‐hydroxy	β‐hydroxy	PUNCT
eurjchem-864	227	58	ester	ester	NOUN
eurjchem-864	227	59	which	which	PRON
eurjchem-864	227	60	subse‐	subse‐	PRON
eurjchem-864	227	61	quently	quently	ADV
eurjchem-864	227	62	undergo	undergo	VERB
eurjchem-864	227	63	intramolecular	intramolecular	ADJ
eurjchem-864	227	64	cyclication	cyclication	NOUN
eurjchem-864	227	65	to	to	PART
eurjchem-864	227	66	form	form	VERB
eurjchem-864	227	67	lactone	lactone	NOUN
eurjchem-864	227	68	with	with	ADP
eurjchem-864	227	69	exocyclic	exocyclic	ADJ
eurjchem-864	227	70	double	double	ADJ
eurjchem-864	227	71	bond	bond	NOUN
eurjchem-864	227	72	.	.	PUNCT
eurjchem-864	228	1	later	later	ADV
eurjchem-864	228	2	,	,	PUNCT
eurjchem-864	228	3	base	base	NOUN
eurjchem-864	228	4	induced	induce	VERB
eurjchem-864	228	5	migration	migration	NOUN
eurjchem-864	228	6	of	of	ADP
eurjchem-864	228	7	double	double	ADJ
eurjchem-864	228	8	bond	bond	NOUN
eurjchem-864	228	9	in	in	ADP
eurjchem-864	228	10	to	to	ADP
eurjchem-864	228	11	the	the	DET
eurjchem-864	228	12	ring	ring	NOUN
eurjchem-864	228	13	gives	give	VERB
eurjchem-864	228	14	compound	compound	NOUN
eurjchem-864	228	15	3	3	NUM
eurjchem-864	228	16	)	)	PUNCT
eurjchem-864	228	17	.	.	PUNCT
eurjchem-864	229	1	selective	selective	ADJ
eurjchem-864	229	2	hydrolysis	hydrolysis	NOUN
eurjchem-864	229	3	of	of	ADP
eurjchem-864	229	4	methyl	methyl	NOUN
eurjchem-864	229	5	ester	ester	NOUN
eurjchem-864	229	6	group	group	NOUN
eurjchem-864	229	7	in	in	ADP
eurjchem-864	229	8	compound	compound	NOUN
eurjchem-864	229	9	3	3	NUM
eurjchem-864	229	10	by	by	ADP
eurjchem-864	229	11	lithium	lithium	NOUN
eurjchem-864	229	12	hydroxide	hydroxide	NOUN
eurjchem-864	229	13	in	in	ADP
eurjchem-864	229	14	methonolic	methonolic	ADJ
eurjchem-864	229	15	water	water	NOUN
eurjchem-864	229	16	to	to	PART
eurjchem-864	229	17	get	get	VERB
eurjchem-864	229	18	8‐(tert‐butoxycarbonyl)‐	8‐(tert‐butoxycarbonyl)‐	NUM
eurjchem-864	229	19	3‐methyl‐2‐oxo‐1‐oxa‐8‐azaspiro[4.5]dec‐3‐ene‐4‐carboxylic	3‐methyl‐2‐oxo‐1‐oxa‐8‐azaspiro[4.5]dec‐3‐ene‐4‐carboxylic	ADJ
eurjchem-864	229	20	acid	acid	NOUN
eurjchem-864	229	21	(	(	PUNCT
eurjchem-864	229	22	4	4	NUM
eurjchem-864	229	23	)	)	PUNCT
eurjchem-864	229	24	in	in	ADP
eurjchem-864	229	25	89	89	NUM
eurjchem-864	229	26	%	%	NOUN
eurjchem-864	229	27	yield	yield	NOUN
eurjchem-864	229	28	.	.	PUNCT
eurjchem-864	230	1	coupling	coupling	NOUN
eurjchem-864	230	2	of	of	ADP
eurjchem-864	230	3	compound	compound	NOUN
eurjchem-864	230	4	4	4	NUM
eurjchem-864	230	5	with	with	ADP
eurjchem-864	230	6	6‐fluoro‐3‐	6‐fluoro‐3‐	PROPN
eurjchem-864	230	7	(	(	PUNCT
eurjchem-864	230	8	piperidin‐4‐yl)benzo[d]isoxazole	piperidin‐4‐yl)benzo[d]isoxazole	PROPN
eurjchem-864	230	9	hydrochloride	hydrochloride	NOUN
eurjchem-864	230	10	(	(	PUNCT
eurjchem-864	230	11	5	5	NUM
eurjchem-864	230	12	)	)	PUNCT
eurjchem-864	230	13	in	in	ADP
eurjchem-864	230	14	presence	presence	NOUN
eurjchem-864	230	15	of	of	ADP
eurjchem-864	230	16	edc.hcl/hobt	edc.hcl/hobt	NOUN
eurjchem-864	230	17	in	in	ADP
eurjchem-864	230	18	dichloromethane	dichloromethane	NOUN
eurjchem-864	230	19	to	to	PART
eurjchem-864	230	20	furnish	furnish	VERB
eurjchem-864	230	21	tert‐	tert‐	PROPN
eurjchem-864	230	22	butyl	butyl	PROPN
eurjchem-864	230	23	4‐(4‐(6‐fluorobenzo[d]isoxazol‐3‐yl)piperidine‐1‐car‐	4‐(4‐(6‐fluorobenzo[d]isoxazol‐3‐yl)piperidine‐1‐car‐	NUM
eurjchem-864	230	24	bonyl)‐3‐methyl‐2‐oxo‐1‐oxa‐8‐azaspiro[4.5	bonyl)‐3‐methyl‐2‐oxo‐1‐oxa‐8‐azaspiro[4.5	NOUN
eurjchem-864	230	25	]	]	X
eurjchem-864	230	26	dec‐3‐ene‐8‐	dec‐3‐ene‐8‐	NOUN
eurjchem-864	230	27	carboxylate	carboxylate	NOUN
eurjchem-864	230	28	(	(	PUNCT
eurjchem-864	230	29	6	6	NUM
eurjchem-864	230	30	)	)	PUNCT
eurjchem-864	230	31	.	.	PUNCT
eurjchem-864	231	1	cleavage	cleavage	NOUN
eurjchem-864	231	2	of	of	ADP
eurjchem-864	231	3	tert‐butyl	tert‐butyl	PROPN
eurjchem-864	231	4	oxy	oxy	ADJ
eurjchem-864	231	5	group	group	NOUN
eurjchem-864	231	6	in	in	ADP
eurjchem-864	231	7	compound	compound	NOUN
eurjchem-864	231	8	6	6	NUM
eurjchem-864	231	9	by	by	ADP
eurjchem-864	231	10	hydrochloric	hydrochloric	ADJ
eurjchem-864	231	11	acid	acid	NOUN
eurjchem-864	231	12	in	in	ADP
eurjchem-864	231	13	ether	ether	NOUN
eurjchem-864	231	14	to	to	PART
eurjchem-864	231	15	give	give	VERB
eurjchem-864	231	16	4‐(4‐(6‐	4‐(4‐(6‐	NUM
eurjchem-864	231	17	fluorobenzo[d]isoxazol‐3‐yl)piperidine‐1‐carbonyl)‐3‐methyl‐	fluorobenzo[d]isoxazol‐3‐yl)piperidine‐1‐carbonyl)‐3‐methyl‐	NOUN
eurjchem-864	231	18	1‐oxa‐8‐azaspiro[4.5]dec‐3‐en‐2‐one	1‐oxa‐8‐azaspiro[4.5]dec‐3‐en‐2‐one	NUM
eurjchem-864	231	19	hydrochloride	hydrochloride	NOUN
eurjchem-864	231	20	(	(	PUNCT
eurjchem-864	231	21	7	7	NUM
eurjchem-864	231	22	)	)	PUNCT
eurjchem-864	231	23	.	.	PUNCT
eurjchem-864	232	1	acylation	acylation	NOUN
eurjchem-864	232	2	of	of	ADP
eurjchem-864	232	3	compound	compound	NOUN
eurjchem-864	232	4	7	7	NUM
eurjchem-864	232	5	with	with	ADP
eurjchem-864	232	6	various	various	ADJ
eurjchem-864	232	7	benzoyl	benzoyl	ADJ
eurjchem-864	232	8	chloride	chloride	NOUN
eurjchem-864	232	9	derivatives	derivative	NOUN
eurjchem-864	232	10	8	8	NUM
eurjchem-864	232	11	to	to	PART
eurjchem-864	232	12	afford	afford	VERB
eurjchem-864	232	13	final	final	ADJ
eurjchem-864	232	14	products	product	NOUN
eurjchem-864	232	15	8‐acyl‐4‐(4‐(6‐fluoro	8‐acyl‐4‐(4‐(6‐fluoro	NUM
eurjchem-864	232	16	benzo[d]isoxazol‐3‐yl)piperidine‐1‐carbonyl)‐3‐methyl‐1‐oxa‐	benzo[d]isoxazol‐3‐yl)piperidine‐1‐carbonyl)‐3‐methyl‐1‐oxa‐	VERB
eurjchem-864	232	17	8‐azaspiro[4.5]dec‐3‐en‐2‐one	8‐azaspiro[4.5]dec‐3‐en‐2‐one	NUM
eurjchem-864	232	18	(	(	PUNCT
eurjchem-864	232	19	9	9	NUM
eurjchem-864	232	20	)	)	PUNCT
eurjchem-864	232	21	as	as	SCONJ
eurjchem-864	232	22	shown	show	VERB
eurjchem-864	232	23	in	in	ADP
eurjchem-864	232	24	scheme	scheme	NOUN
eurjchem-864	232	25	1	1	NUM
eurjchem-864	232	26	,	,	PUNCT
eurjchem-864	232	27	table	table	NOUN
eurjchem-864	232	28	1	1	NUM
eurjchem-864	232	29	.	.	PUNCT
eurjchem-864	233	1	the	the	DET
eurjchem-864	233	2	structures	structure	NOUN
eurjchem-864	233	3	of	of	ADP
eurjchem-864	233	4	the	the	DET
eurjchem-864	233	5	synthesized	synthesize	VERB
eurjchem-864	233	6	compounds	compound	NOUN
eurjchem-864	233	7	are	be	AUX
eurjchem-864	233	8	established	establish	VERB
eurjchem-864	233	9	with	with	ADP
eurjchem-864	233	10	the	the	DET
eurjchem-864	233	11	help	help	NOUN
eurjchem-864	233	12	of	of	ADP
eurjchem-864	233	13	spectral	spectral	ADJ
eurjchem-864	233	14	data	datum	NOUN
eurjchem-864	233	15	.	.	PUNCT
eurjchem-864	234	1	figure	figure	NOUN
eurjchem-864	234	2	5	5	NUM
eurjchem-864	234	3	.	.	PUNCT
eurjchem-864	235	1	inhibition	inhibition	NOUN
eurjchem-864	235	2	of	of	ADP
eurjchem-864	235	3	pla2	pla2	NOUN
eurjchem-864	235	4	induced	induce	VERB
eurjchem-864	235	5	haemolysis	haemolysis	NOUN
eurjchem-864	235	6	.	.	PUNCT
eurjchem-864	236	1	compounds	compound	VERB
eurjchem-864	236	2	9a‐b	9a‐b	PROPN
eurjchem-864	236	3	and	and	CCONJ
eurjchem-864	236	4	9d‐g	9d‐g	NOUN
eurjchem-864	236	5	showed	show	VERB
eurjchem-864	236	6	good	good	ADJ
eurjchem-864	236	7	antibacterial	antibacterial	ADJ
eurjchem-864	236	8	activity	activity	NOUN
eurjchem-864	236	9	against	against	ADP
eurjchem-864	236	10	escherichia	escherichia	NOUN
eurjchem-864	236	11	coli	coli	NOUN
eurjchem-864	236	12	,	,	PUNCT
eurjchem-864	236	13	klebsiella	klebsiella	NOUN
eurjchem-864	236	14	pneumonia	pneumonia	NOUN
eurjchem-864	236	15	,	,	PUNCT
eurjchem-864	236	16	salmonella	salmonella	NOUN
eurjchem-864	236	17	typhi	typhi	ADV
eurjchem-864	236	18	,	,	PUNCT
eurjchem-864	236	19	shigella	shigella	PROPN
eurjchem-864	236	20	flexneri	flexneri	ADJ
eurjchem-864	236	21	and	and	CCONJ
eurjchem-864	236	22	bacillus	bacillus	NOUN
eurjchem-864	236	23	subtilis	subtili	NOUN
eurjchem-864	236	24	.	.	PUNCT
eurjchem-864	237	1	while	while	SCONJ
eurjchem-864	237	2	the	the	DET
eurjchem-864	237	3	compounds	compound	NOUN
eurjchem-864	237	4	9c	9c	NUM
eurjchem-864	237	5	,	,	PUNCT
eurjchem-864	237	6	9h	9h	NUM
eurjchem-864	237	7	,	,	PUNCT
eurjchem-864	237	8	9i	9i	NOUN
eurjchem-864	237	9	and	and	CCONJ
eurjchem-864	237	10	9j	9j	PROPN
eurjchem-864	237	11	showed	show	VERB
eurjchem-864	237	12	moderate	moderate	ADJ
eurjchem-864	237	13	antibacterial	antibacterial	ADJ
eurjchem-864	237	14	activity	activity	NOUN
eurjchem-864	237	15	.	.	PUNCT
eurjchem-864	238	1	compound	compound	NOUN
eurjchem-864	238	2	with	with	ADP
eurjchem-864	238	3	dinitro	dinitro	ADJ
eurjchem-864	238	4	substituent	substituent	NOUN
eurjchem-864	238	5	showed	show	VERB
eurjchem-864	238	6	highest	high	ADJ
eurjchem-864	238	7	antibacterial	antibacterial	ADJ
eurjchem-864	238	8	activity	activity	NOUN
eurjchem-864	238	9	.	.	PUNCT
eurjchem-864	239	1	most	most	ADJ
eurjchem-864	239	2	of	of	ADP
eurjchem-864	239	3	the	the	DET
eurjchem-864	239	4	compounds	compound	NOUN
eurjchem-864	239	5	exhibited	exhibit	VERB
eurjchem-864	239	6	antibacterial	antibacterial	ADJ
eurjchem-864	239	7	activity	activity	NOUN
eurjchem-864	239	8	probably	probably	ADV
eurjchem-864	239	9	due	due	ADJ
eurjchem-864	239	10	to	to	ADP
eurjchem-864	239	11	the	the	DET
eurjchem-864	239	12	presence	presence	NOUN
eurjchem-864	239	13	of	of	ADP
eurjchem-864	239	14	bioactive	bioactive	PROPN
eurjchem-864	239	15	benzisoxazole	benzisoxazole	PROPN
eurjchem-864	239	16	moiety	moiety	PROPN
eurjchem-864	239	17	.	.	PUNCT
eurjchem-864	240	1	in	in	ADP
eurjchem-864	240	2	all	all	DET
eurjchem-864	240	3	the	the	DET
eurjchem-864	240	4	anti‐oxidant	anti‐oxidant	NOUN
eurjchem-864	240	5	assays	assay	NOUN
eurjchem-864	240	6	compounds	compound	VERB
eurjchem-864	240	7	9b	9b	NUM
eurjchem-864	240	8	,	,	PUNCT
eurjchem-864	240	9	9f	9f	NOUN
eurjchem-864	240	10	and	and	CCONJ
eurjchem-864	240	11	9h	9h	NUM
eurjchem-864	240	12	containing	contain	VERB
eurjchem-864	240	13	electron	electron	NOUN
eurjchem-864	240	14	donating	donate	VERB
eurjchem-864	240	15	groups	group	NOUN
eurjchem-864	240	16	exhibited	exhibit	VERB
eurjchem-864	240	17	good	good	ADJ
eurjchem-864	240	18	inhibitory	inhibitory	ADJ
eurjchem-864	240	19	activity	activity	NOUN
eurjchem-864	240	20	.	.	PUNCT
eurjchem-864	241	1	the	the	DET
eurjchem-864	241	2	remaining	remain	VERB
eurjchem-864	241	3	compounds	compound	NOUN
eurjchem-864	241	4	showed	show	VERB
eurjchem-864	241	5	moderate	moderate	ADJ
eurjchem-864	241	6	anti‐oxidant	anti‐oxidant	NOUN
eurjchem-864	241	7	activity	activity	NOUN
eurjchem-864	241	8	.	.	PUNCT
eurjchem-864	242	1	at	at	ADP
eurjchem-864	242	2	this	this	DET
eurjchem-864	242	3	stage	stage	NOUN
eurjchem-864	242	4	,	,	PUNCT
eurjchem-864	242	5	it	it	PRON
eurjchem-864	242	6	is	be	AUX
eurjchem-864	242	7	not	not	PART
eurjchem-864	242	8	possible	possible	ADJ
eurjchem-864	242	9	to	to	PART
eurjchem-864	242	10	give	give	VERB
eurjchem-864	242	11	any	any	DET
eurjchem-864	242	12	rational	rational	ADJ
eurjchem-864	242	13	explanation	explanation	NOUN
eurjchem-864	242	14	for	for	ADP
eurjchem-864	242	15	the	the	DET
eurjchem-864	242	16	anti‐oxidant	anti‐oxidant	ADJ
eurjchem-864	242	17	activities	activity	NOUN
eurjchem-864	242	18	of	of	ADP
eurjchem-864	242	19	benzisoxazole	benzisoxazole	NOUN
eurjchem-864	242	20	derivatives	derivative	NOUN
eurjchem-864	242	21	even	even	ADV
eurjchem-864	242	22	in	in	ADP
eurjchem-864	242	23	the	the	DET
eurjchem-864	242	24	absence	absence	NOUN
eurjchem-864	242	25	of	of	ADP
eurjchem-864	242	26	essential	essential	ADJ
eurjchem-864	242	27	phenolic	phenolic	ADJ
eurjchem-864	242	28	group	group	NOUN
eurjchem-864	242	29	.	.	PUNCT
eurjchem-864	243	1	in	in	ADP
eurjchem-864	243	2	both	both	DET
eurjchem-864	243	3	lipoxygenase	lipoxygenase	NOUN
eurjchem-864	243	4	inhibition	inhibition	NOUN
eurjchem-864	243	5	and	and	CCONJ
eurjchem-864	243	6	phospholipase	phospholipase	NOUN
eurjchem-864	243	7	a2	a2	NOUN
eurjchem-864	243	8	inhibition	inhibition	VERB
eurjchem-864	243	9	assays	assay	NOUN
eurjchem-864	243	10	compounds	compound	NOUN
eurjchem-864	243	11	bearing	bear	VERB
eurjchem-864	243	12	electron	electron	NOUN
eurjchem-864	243	13	withdrawing	withdraw	VERB
eurjchem-864	243	14	groups	group	NOUN
eurjchem-864	243	15	9e	9e	NOUN
eurjchem-864	243	16	and	and	CCONJ
eurjchem-864	243	17	9	9	NUM
eurjchem-864	243	18	g	g	NOUN
eurjchem-864	243	19	exhibited	exhibit	VERB
eurjchem-864	243	20	good	good	ADJ
eurjchem-864	243	21	anti‐	anti‐	PROPN
eurjchem-864	243	22	inflammatory	inflammatory	ADJ
eurjchem-864	243	23	activity	activity	NOUN
eurjchem-864	243	24	,	,	PUNCT
eurjchem-864	243	25	the	the	DET
eurjchem-864	243	26	remaining	remain	VERB
eurjchem-864	243	27	compounds	compound	NOUN
eurjchem-864	243	28	showed	show	VERB
eurjchem-864	243	29	moderate	moderate	ADJ
eurjchem-864	243	30	activity	activity	NOUN
eurjchem-864	243	31	probably	probably	ADV
eurjchem-864	243	32	due	due	ADJ
eurjchem-864	243	33	to	to	ADP
eurjchem-864	243	34	the	the	DET
eurjchem-864	243	35	absence	absence	NOUN
eurjchem-864	243	36	of	of	ADP
eurjchem-864	243	37	deactivating	deactivate	VERB
eurjchem-864	243	38	groups	group	NOUN
eurjchem-864	243	39	on	on	ADP
eurjchem-864	243	40	phenyl	phenyl	NOUN
eurjchem-864	243	41	ring	ring	NOUN
eurjchem-864	243	42	.	.	PUNCT
eurjchem-864	244	1	it	it	PRON
eurjchem-864	244	2	is	be	AUX
eurjchem-864	244	3	interesting	interesting	ADJ
eurjchem-864	244	4	to	to	PART
eurjchem-864	244	5	note	note	VERB
eurjchem-864	244	6	that	that	SCONJ
eurjchem-864	244	7	the	the	DET
eurjchem-864	244	8	shivaprasad	shivaprasad	PROPN
eurjchem-864	244	9	et	et	PROPN
eurjchem-864	244	10	al	al	PROPN
eurjchem-864	244	11	.	.	PUNCT
eurjchem-864	244	12	/	/	SYM
eurjchem-864	244	13	european	european	PROPN
eurjchem-864	244	14	journal	journal	PROPN
eurjchem-864	244	15	of	of	ADP
eurjchem-864	244	16	chemistry	chemistry	NOUN
eurjchem-864	244	17	4	4	NUM
eurjchem-864	244	18	(	(	PUNCT
eurjchem-864	244	19	4	4	NUM
eurjchem-864	244	20	)	)	PUNCT
eurjchem-864	244	21	(	(	PUNCT
eurjchem-864	244	22	2013	2013	NUM
eurjchem-864	244	23	)	)	PUNCT
eurjchem-864	244	24	402‐407	402‐407	PROPN
eurjchem-864	244	25	407	407	NUM
eurjchem-864	244	26	compounds	compound	NOUN
eurjchem-864	244	27	bearing	bear	VERB
eurjchem-864	244	28	activating	activate	VERB
eurjchem-864	244	29	groups	group	NOUN
eurjchem-864	244	30	on	on	ADP
eurjchem-864	244	31	phenyl	phenyl	NOUN
eurjchem-864	244	32	ring	ring	NOUN
eurjchem-864	244	33	showed	show	VERB
eurjchem-864	244	34	good	good	ADJ
eurjchem-864	244	35	anti‐oxidant	anti‐oxidant	ADJ
eurjchem-864	244	36	activity	activity	NOUN
eurjchem-864	244	37	,	,	PUNCT
eurjchem-864	244	38	whereas	whereas	SCONJ
eurjchem-864	244	39	those	those	PRON
eurjchem-864	244	40	with	with	ADP
eurjchem-864	244	41	deactivating	deactivate	VERB
eurjchem-864	244	42	groups	group	NOUN
eurjchem-864	244	43	exhibited	exhibit	VERB
eurjchem-864	244	44	anti‐inflammatory	anti‐inflammatory	NOUN
eurjchem-864	244	45	activities	activity	NOUN
eurjchem-864	244	46	.	.	PUNCT
eurjchem-864	245	1	4	4	X
eurjchem-864	245	2	.	.	X
eurjchem-864	245	3	conclusion	conclusion	NOUN
eurjchem-864	245	4	in	in	ADP
eurjchem-864	245	5	summary	summary	NOUN
eurjchem-864	245	6	,	,	PUNCT
eurjchem-864	245	7	we	we	PRON
eurjchem-864	245	8	have	have	AUX
eurjchem-864	245	9	synthesized	synthesize	VERB
eurjchem-864	245	10	a	a	DET
eurjchem-864	245	11	series	series	NOUN
eurjchem-864	245	12	of	of	ADP
eurjchem-864	245	13	new	new	ADJ
eurjchem-864	245	14	benzisoxazole	benzisoxazole	NOUN
eurjchem-864	245	15	derivatives	derivative	NOUN
eurjchem-864	245	16	in	in	ADP
eurjchem-864	245	17	good	good	ADJ
eurjchem-864	245	18	yields	yield	NOUN
eurjchem-864	245	19	and	and	CCONJ
eurjchem-864	245	20	screened	screen	VERB
eurjchem-864	245	21	them	they	PRON
eurjchem-864	245	22	for	for	ADP
eurjchem-864	245	23	antibacterial	antibacterial	ADJ
eurjchem-864	245	24	,	,	PUNCT
eurjchem-864	245	25	antioxidant	antioxidant	ADJ
eurjchem-864	245	26	and	and	CCONJ
eurjchem-864	245	27	anti‐inflammatory	anti‐inflammatory	NOUN
eurjchem-864	245	28	activity	activity	NOUN
eurjchem-864	245	29	.	.	PUNCT
eurjchem-864	246	1	compounds	compound	VERB
eurjchem-864	246	2	9a‐b	9a‐b	PROPN
eurjchem-864	246	3	and	and	CCONJ
eurjchem-864	246	4	9d‐g	9d‐g	NOUN
eurjchem-864	246	5	showed	show	VERB
eurjchem-864	246	6	good	good	ADJ
eurjchem-864	246	7	antibacterial	antibacterial	ADJ
eurjchem-864	246	8	activity	activity	NOUN
eurjchem-864	246	9	against	against	ADP
eurjchem-864	246	10	escherichia	escherichia	NOUN
eurjchem-864	246	11	coli	coli	NOUN
eurjchem-864	246	12	,	,	PUNCT
eurjchem-864	246	13	klebsiella	klebsiella	NOUN
eurjchem-864	246	14	pneumonia	pneumonia	NOUN
eurjchem-864	246	15	,	,	PUNCT
eurjchem-864	246	16	salmonella	salmonella	NOUN
eurjchem-864	246	17	typhi	typhi	ADV
eurjchem-864	246	18	,	,	PUNCT
eurjchem-864	246	19	shigella	shigella	PROPN
eurjchem-864	246	20	flexneri	flexneri	ADJ
eurjchem-864	246	21	and	and	CCONJ
eurjchem-864	246	22	bacillus	bacillus	NOUN
eurjchem-864	246	23	subtilis	subtili	NOUN
eurjchem-864	246	24	.	.	PUNCT
eurjchem-864	247	1	benzisoxazoles	benzisoxazole	VERB
eurjchem-864	247	2	9b	9b	NUM
eurjchem-864	247	3	,	,	PUNCT
eurjchem-864	247	4	9f	9f	NOUN
eurjchem-864	247	5	and	and	CCONJ
eurjchem-864	247	6	9h	9h	NUM
eurjchem-864	247	7	bearing	bear	VERB
eurjchem-864	247	8	electron	electron	NOUN
eurjchem-864	247	9	donating	donate	VERB
eurjchem-864	247	10	groups	group	NOUN
eurjchem-864	247	11	exhibited	exhibit	VERB
eurjchem-864	247	12	prominent	prominent	ADJ
eurjchem-864	247	13	antioxidant	antioxidant	ADJ
eurjchem-864	247	14	activity	activity	NOUN
eurjchem-864	247	15	and	and	CCONJ
eurjchem-864	247	16	9e	9e	NOUN
eurjchem-864	247	17	and	and	CCONJ
eurjchem-864	247	18	9	9	NUM
eurjchem-864	247	19	g	g	NOUN
eurjchem-864	247	20	showed	show	VERB
eurjchem-864	247	21	good	good	ADJ
eurjchem-864	247	22	anti‐	anti‐	PROPN
eurjchem-864	247	23	inflammatory	inflammatory	ADJ
eurjchem-864	247	24	activity	activity	NOUN
eurjchem-864	247	25	.	.	PUNCT
eurjchem-864	248	1	acknowledgements	acknowledgement	NOUN
eurjchem-864	248	2	authors	author	NOUN
eurjchem-864	248	3	are	be	AUX
eurjchem-864	248	4	grateful	grateful	ADJ
eurjchem-864	248	5	to	to	ADP
eurjchem-864	248	6	board	board	VERB
eurjchem-864	248	7	of	of	ADP
eurjchem-864	248	8	research	research	NOUN
eurjchem-864	248	9	in	in	ADP
eurjchem-864	248	10	nuclear	nuclear	ADJ
eurjchem-864	248	11	sciences	science	NOUN
eurjchem-864	248	12	(	(	PUNCT
eurjchem-864	248	13	brns	brn	NOUN
eurjchem-864	248	14	)	)	PUNCT
eurjchem-864	248	15	,	,	PUNCT
eurjchem-864	248	16	university	university	NOUN
eurjchem-864	248	17	grants	grant	NOUN
eurjchem-864	248	18	commission	commission	PROPN
eurjchem-864	248	19	(	(	PUNCT
eurjchem-864	248	20	ugc	ugc	PROPN
eurjchem-864	248	21	)	)	PUNCT
eurjchem-864	248	22	and	and	CCONJ
eurjchem-864	248	23	indo‐french	indo‐french	ADJ
eurjchem-864	248	24	centre	centre	NOUN
eurjchem-864	248	25	for	for	ADP
eurjchem-864	248	26	the	the	DET
eurjchem-864	248	27	promotion	promotion	NOUN
eurjchem-864	248	28	of	of	ADP
eurjchem-864	248	29	advance	advance	NOUN
eurjchem-864	248	30	research	research	NOUN
eurjchem-864	248	31	(	(	PUNCT
eurjchem-864	248	32	ifcpar	ifcpar	NOUN
eurjchem-864	248	33	)	)	PUNCT
eurjchem-864	248	34	,	,	PUNCT
eurjchem-864	248	35	government	government	NOUN
eurjchem-864	248	36	of	of	ADP
eurjchem-864	248	37	india	india	PROPN
eurjchem-864	248	38	for	for	ADP
eurjchem-864	248	39	financial	financial	ADJ
eurjchem-864	248	40	support	support	NOUN
eurjchem-864	248	41	to	to	PART
eurjchem-864	248	42	kanchugarakoppal	kanchugarakoppal	VERB
eurjchem-864	248	43	subbegowda	subbegowda	PROPN
eurjchem-864	248	44	rangappa	rangappa	VERB
eurjchem-864	248	45	under	under	ADP
eurjchem-864	248	46	the	the	DET
eurjchem-864	248	47	projects	project	NOUN
eurjchem-864	248	48	vide	vide	ADP
eurjchem-864	248	49	no	no	INTJ
eurjchem-864	248	50	.	.	PUNCT
eurjchem-864	249	1	2009/37/40	2009/37/40	NUM
eurjchem-864	249	2	/	/	SYM
eurjchem-864	249	3	brns/2266	brns/2266	NOUN
eurjchem-864	249	4	dated	date	VERB
eurjchem-864	249	5	23‐11‐2009	23‐11‐2009	NUM
eurjchem-864	249	6	,	,	PUNCT
eurjchem-864	249	7	f‐39‐	f‐39‐	NOUN
eurjchem-864	249	8	106/2010	106/2010	NUM
eurjchem-864	249	9	(	(	PUNCT
eurjchem-864	249	10	sr	sr	PROPN
eurjchem-864	249	11	)	)	PUNCT
eurjchem-864	249	12	dated	date	VERB
eurjchem-864	249	13	24‐12‐2010	24‐12‐2010	NOUN
eurjchem-864	249	14	and	and	CCONJ
eurjchem-864	249	15	no	no	INTJ
eurjchem-864	249	16	.	.	PUNCT
eurjchem-864	250	1	ifc/4303‐1/2010‐	ifc/4303‐1/2010‐	PROPN
eurjchem-864	250	2	11	11	NUM
eurjchem-864	250	3	dated	date	VERB
eurjchem-864	250	4	22‐12‐2010	22‐12‐2010	PROPN
eurjchem-864	250	5	.	.	PROPN
eurjchem-864	250	6	chakrabhavi	chakrabhavi	PROPN
eurjchem-864	250	7	dhananjaya	dhananjaya	PROPN
eurjchem-864	250	8	mohan	mohan	PROPN
eurjchem-864	250	9	thank	thank	PROPN
eurjchem-864	250	10	department	department	PROPN
eurjchem-864	250	11	of	of	ADP
eurjchem-864	250	12	science	science	NOUN
eurjchem-864	250	13	and	and	CCONJ
eurjchem-864	250	14	technology	technology	NOUN
eurjchem-864	250	15	for	for	ADP
eurjchem-864	250	16	innovation	innovation	NOUN
eurjchem-864	250	17	in	in	ADP
eurjchem-864	250	18	science	science	NOUN
eurjchem-864	250	19	pursuit	pursuit	NOUN
eurjchem-864	250	20	for	for	ADP
eurjchem-864	250	21	inspired	inspire	VERB
eurjchem-864	250	22	research	research	NOUN
eurjchem-864	250	23	fellowship	fellowship	NOUN
eurjchem-864	250	24	and	and	CCONJ
eurjchem-864	250	25	toreshettahally	toreshettahally	ADV
eurjchem-864	250	26	ramesh	ramesh	PROPN
eurjchem-864	250	27	swaroop	swaroop	PROPN
eurjchem-864	250	28	thank	thank	PROPN
eurjchem-864	250	29	council	council	PROPN
eurjchem-864	250	30	of	of	ADP
eurjchem-864	250	31	scientific	scientific	ADJ
eurjchem-864	250	32	and	and	CCONJ
eurjchem-864	250	33	industrial	industrial	ADJ
eurjchem-864	250	34	research	research	NOUN
eurjchem-864	250	35	for	for	ADP
eurjchem-864	250	36	junior	junior	ADJ
eurjchem-864	250	37	and	and	CCONJ
eurjchem-864	250	38	senior	senior	ADJ
eurjchem-864	250	39	research	research	NOUN
eurjchem-864	250	40	fellowship	fellowship	NOUN
eurjchem-864	250	41	.	.	PUNCT
eurjchem-864	251	1	references	reference	NOUN
eurjchem-864	251	2	[	[	X
eurjchem-864	251	3	1	1	NUM
eurjchem-864	251	4	]	]	X
eurjchem-864	251	5	priya	priya	PROPN
eurjchem-864	251	6	,	,	PUNCT
eurjchem-864	251	7	b.	b.	PROPN
eurjchem-864	251	8	s.	s.	PROPN
eurjchem-864	251	9	;	;	PUNCT
eurjchem-864	251	10	basappa	basappa	NOUN
eurjchem-864	251	11	;	;	PUNCT
eurjchem-864	251	12	swamy	swamy	PROPN
eurjchem-864	251	13	,	,	PUNCT
eurjchem-864	251	14	s.	s.	PROPN
eurjchem-864	251	15	n.	n.	PROPN
eurjchem-864	251	16	;	;	PUNCT
eurjchem-864	251	17	rangappa	rangappa	PROPN
eurjchem-864	251	18	,	,	PUNCT
eurjchem-864	251	19	k.	k.	PROPN
eurjchem-864	251	20	s.	s.	PROPN
eurjchem-864	251	21	bioorg	bioorg	PROPN
eurjchem-864	251	22	.	.	PUNCT
eurjchem-864	252	1	med	med	PROPN
eurjchem-864	252	2	.	.	PROPN
eurjchem-864	252	3	chem	chem	PROPN
eurjchem-864	252	4	.	.	PUNCT
eurjchem-864	253	1	2005	2005	NUM
eurjchem-864	253	2	,	,	PUNCT
eurjchem-864	253	3	13	13	NUM
eurjchem-864	253	4	,	,	PUNCT
eurjchem-864	253	5	2623‐2628	2623‐2628	NUM
eurjchem-864	253	6	.	.	PUNCT
eurjchem-864	254	1	[	[	X
eurjchem-864	254	2	2	2	NUM
eurjchem-864	254	3	]	]	X
eurjchem-864	254	4	stiff	stiff	ADJ
eurjchem-864	254	5	,	,	PUNCT
eurjchem-864	254	6	d.	d.	PROPN
eurjchem-864	254	7	d.	d.	PROPN
eurjchem-864	254	8	;	;	PUNCT
eurjchem-864	254	9	zemaitis	zemaitis	NOUN
eurjchem-864	254	10	,	,	PUNCT
eurjchem-864	254	11	m.	m.	NOUN
eurjchem-864	254	12	a.	a.	NOUN
eurjchem-864	254	13	drug	drug	PROPN
eurjchem-864	254	14	metab	metab	PROPN
eurjchem-864	254	15	.	.	PUNCT
eurjchem-864	255	1	dispos	dispos	PROPN
eurjchem-864	255	2	.	.	PUNCT
eurjchem-864	256	1	1990	1990	NUM
eurjchem-864	256	2	,	,	PUNCT
eurjchem-864	256	3	18	18	NUM
eurjchem-864	256	4	,	,	PUNCT
eurjchem-864	256	5	888‐894	888‐894	NUM
eurjchem-864	256	6	.	.	PUNCT
eurjchem-864	257	1	[	[	X
eurjchem-864	257	2	3	3	NUM
eurjchem-864	257	3	]	]	X
eurjchem-864	257	4	uno	uno	PROPN
eurjchem-864	257	5	,	,	PUNCT
eurjchem-864	257	6	h.	h.	PROPN
eurjchem-864	257	7	;	;	PUNCT
eurjchem-864	257	8	kurokawa	kurokawa	PROPN
eurjchem-864	257	9	,	,	PUNCT
eurjchem-864	257	10	m.	m.	NOUN
eurjchem-864	257	11	;	;	PUNCT
eurjchem-864	257	12	masuda	masuda	PROPN
eurjchem-864	257	13	,	,	PUNCT
eurjchem-864	257	14	y.	y.	PROPN
eurjchem-864	257	15	;	;	PUNCT
eurjchem-864	257	16	nishimura	nishimura	PROPN
eurjchem-864	257	17	,	,	PUNCT
eurjchem-864	257	18	h.	h.	PROPN
eurjchem-864	257	19	j.	j.	PROPN
eurjchem-864	257	20	med	med	PROPN
eurjchem-864	257	21	.	.	PROPN
eurjchem-864	257	22	chem	chem	PROPN
eurjchem-864	257	23	.	.	PUNCT
eurjchem-864	258	1	1979	1979	NUM
eurjchem-864	258	2	,	,	PUNCT
eurjchem-864	258	3	22	22	NUM
eurjchem-864	258	4	,	,	PUNCT
eurjchem-864	258	5	180‐188	180‐188	NUM
eurjchem-864	258	6	.	.	PUNCT
eurjchem-864	259	1	[	[	X
eurjchem-864	259	2	4	4	NUM
eurjchem-864	259	3	]	]	X
eurjchem-864	259	4	gopalsamy	gopalsamy	NOUN
eurjchem-864	259	5	,	,	PUNCT
eurjchem-864	259	6	a.	a.	NOUN
eurjchem-864	259	7	;	;	PUNCT
eurjchem-864	259	8	shi	shi	PROPN
eurjchem-864	259	9	,	,	PUNCT
eurjchem-864	259	10	m.	m.	NOUN
eurjchem-864	259	11	;	;	PUNCT
eurjchem-864	259	12	golas	gola	NOUN
eurjchem-864	259	13	,	,	PUNCT
eurjchem-864	259	14	j.	j.	PROPN
eurjchem-864	259	15	;	;	PUNCT
eurjchem-864	259	16	vogan	vogan	PROPN
eurjchem-864	259	17	,	,	PUNCT
eurjchem-864	259	18	e.	e.	PROPN
eurjchem-864	259	19	;	;	PUNCT
eurjchem-864	259	20	jacob	jacob	PROPN
eurjchem-864	259	21	,	,	PUNCT
eurjchem-864	259	22	j.	j.	PROPN
eurjchem-864	259	23	;	;	PUNCT
eurjchem-864	259	24	johnson	johnson	PROPN
eurjchem-864	259	25	,	,	PUNCT
eurjchem-864	259	26	m.	m.	NOUN
eurjchem-864	259	27	;	;	PUNCT
eurjchem-864	259	28	lee	lee	PROPN
eurjchem-864	259	29	,	,	PUNCT
eurjchem-864	259	30	f.	f.	PROPN
eurjchem-864	259	31	;	;	PUNCT
eurjchem-864	259	32	nilakantan	nilakantan	PROPN
eurjchem-864	259	33	,	,	PUNCT
eurjchem-864	259	34	r.	r.	PROPN
eurjchem-864	259	35	;	;	PUNCT
eurjchem-864	259	36	petersen	petersen	PROPN
eurjchem-864	259	37	,	,	PUNCT
eurjchem-864	259	38	r.	r.	PROPN
eurjchem-864	259	39	;	;	PUNCT
eurjchem-864	259	40	svenson	svenson	PROPN
eurjchem-864	259	41	,	,	PUNCT
eurjchem-864	259	42	k.	k.	PROPN
eurjchem-864	259	43	;	;	PUNCT
eurjchem-864	259	44	chopra	chopra	PROPN
eurjchem-864	259	45	,	,	PUNCT
eurjchem-864	259	46	r.	r.	PROPN
eurjchem-864	259	47	;	;	PUNCT
eurjchem-864	259	48	tam	tam	PROPN
eurjchem-864	259	49	,	,	PUNCT
eurjchem-864	259	50	m.	m.	NOUN
eurjchem-864	259	51	s.	s.	PROPN
eurjchem-864	259	52	;	;	PUNCT
eurjchem-864	259	53	wen	wen	PROPN
eurjchem-864	259	54	,	,	PUNCT
eurjchem-864	259	55	y.	y.	PROPN
eurjchem-864	259	56	;	;	PUNCT
eurjchem-864	259	57	ellingboe	ellingboe	PROPN
eurjchem-864	259	58	,	,	PUNCT
eurjchem-864	259	59	j.	j.	PROPN
eurjchem-864	259	60	;	;	PUNCT
eurjchem-864	259	61	arndt	arndt	PROPN
eurjchem-864	259	62	,	,	PUNCT
eurjchem-864	259	63	k.	k.	PROPN
eurjchem-864	259	64	;	;	PUNCT
eurjchem-864	259	65	boschelli	boschelli	PROPN
eurjchem-864	259	66	,	,	PUNCT
eurjchem-864	259	67	f.	f.	PROPN
eurjchem-864	259	68	j.	j.	PROPN
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eurjchem-864	259	72	.	.	PUNCT
eurjchem-864	260	1	2008	2008	NUM
eurjchem-864	260	2	,	,	PUNCT
eurjchem-864	260	3	51	51	NUM
eurjchem-864	260	4	,	,	PUNCT
eurjchem-864	260	5	373‐	373‐	NUM
eurjchem-864	260	6	379	379	NUM
eurjchem-864	260	7	.	.	PUNCT
eurjchem-864	261	1	[	[	X
eurjchem-864	261	2	5	5	NUM
eurjchem-864	261	3	]	]	PUNCT
eurjchem-864	261	4	jain	jain	NOUN
eurjchem-864	261	5	,	,	PUNCT
eurjchem-864	261	6	m.	m.	NOUN
eurjchem-864	261	7	;	;	PUNCT
eurjchem-864	261	8	kwon	kwon	PROPN
eurjchem-864	261	9	,	,	PUNCT
eurjchem-864	261	10	c.	c.	PROPN
eurjchem-864	261	11	h.	h.	PROPN
eurjchem-864	261	12	j.	j.	PROPN
eurjchem-864	261	13	med	med	PROPN
eurjchem-864	261	14	.	.	PROPN
eurjchem-864	261	15	chem	chem	PROPN
eurjchem-864	261	16	.	.	PUNCT
eurjchem-864	262	1	2003	2003	NUM
eurjchem-864	262	2	,	,	PUNCT
eurjchem-864	262	3	46	46	NUM
eurjchem-864	262	4	,	,	PUNCT
eurjchem-864	262	5	5428‐5434	5428‐5434	NUM
eurjchem-864	262	6	.	.	PUNCT
eurjchem-864	263	1	[	[	X
eurjchem-864	263	2	6	6	NUM
eurjchem-864	263	3	]	]	X
eurjchem-864	263	4	davis	davis	PROPN
eurjchem-864	263	5	,	,	PUNCT
eurjchem-864	263	6	l.	l.	PROPN
eurjchem-864	263	7	;	;	PUNCT
eurjchem-864	263	8	effland	effland	PROPN
eurjchem-864	263	9	,	,	PUNCT
eurjchem-864	263	10	r.	r.	PROPN
eurjchem-864	263	11	c.	c.	PROPN
eurjchem-864	263	12	;	;	PUNCT
eurjchem-864	263	13	klein	klein	PROPN
eurjchem-864	263	14	,	,	PUNCT
eurjchem-864	263	15	j.	j.	PROPN
eurjchem-864	263	16	t.	t.	PROPN
eurjchem-864	263	17	;	;	PUNCT
eurjchem-864	263	18	dunn	dunn	PROPN
eurjchem-864	263	19	,	,	PUNCT
eurjchem-864	263	20	r.	r.	PROPN
eurjchem-864	263	21	w.	w.	PROPN
eurjchem-864	263	22	;	;	PUNCT
eurjchem-864	263	23	geyer	geyer	PROPN
eurjchem-864	263	24	,	,	PUNCT
eurjchem-864	263	25	h.	h.	PROPN
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eurjchem-864	263	27	;	;	PUNCT
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eurjchem-864	263	29	,	,	PUNCT
eurjchem-864	263	30	w.	w.	PROPN
eurjchem-864	263	31	m.	m.	PROPN
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eurjchem-864	263	34	disc	disc	NOUN
eurjchem-864	263	35	.	.	PUNCT
eurjchem-864	263	36	1992	1992	NUM
eurjchem-864	263	37	,	,	PUNCT
eurjchem-864	263	38	8	8	NUM
eurjchem-864	263	39	,	,	PUNCT
eurjchem-864	263	40	225‐240	225‐240	NUM
eurjchem-864	263	41	.	.	PUNCT
eurjchem-864	264	1	[	[	X
eurjchem-864	264	2	7	7	NUM
eurjchem-864	264	3	]	]	X
eurjchem-864	264	4	strupczewski	strupczewski	NOUN
eurjchem-864	264	5	,	,	PUNCT
eurjchem-864	264	6	j.	j.	PROPN
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eurjchem-864	264	8	;	;	PUNCT
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eurjchem-864	264	10	,	,	PUNCT
eurjchem-864	264	11	r.	r.	PROPN
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eurjchem-864	264	13	;	;	PUNCT
eurjchem-864	264	14	gardner	gardner	PROPN
eurjchem-864	264	15	,	,	PUNCT
eurjchem-864	264	16	b.	b.	PROPN
eurjchem-864	264	17	a.	a.	PROPN
eurjchem-864	264	18	;	;	PUNCT
eurjchem-864	264	19	schmid	schmid	PROPN
eurjchem-864	264	20	,	,	PUNCT
eurjchem-864	264	21	b.	b.	PROPN
eurjchem-864	264	22	l.	l.	PROPN
eurjchem-864	264	23	;	;	PUNCT
eurjchem-864	264	24	stache	stache	NOUN
eurjchem-864	264	25	,	,	PUNCT
eurjchem-864	264	26	u.	u.	PROPN
eurjchem-864	264	27	;	;	PUNCT
eurjchem-864	264	28	glamkowski	glamkowski	PROPN
eurjchem-864	264	29	,	,	PUNCT
eurjchem-864	264	30	e.	e.	PROPN
eurjchem-864	264	31	j.	j.	PROPN
eurjchem-864	264	32	;	;	PUNCT
eurjchem-864	264	33	jones	jones	PROPN
eurjchem-864	264	34	,	,	PUNCT
eurjchem-864	264	35	m.	m.	PROPN
eurjchem-864	264	36	c.	c.	PROPN
eurjchem-864	264	37	;	;	PUNCT
eurjchem-864	264	38	ellis	ellis	PROPN
eurjchem-864	264	39	,	,	PUNCT
eurjchem-864	264	40	d.	d.	PROPN
eurjchem-864	264	41	b.	b.	PROPN
eurjchem-864	264	42	;	;	PUNCT
eurjchem-864	264	43	huger	huger	X
eurjchem-864	264	44	,	,	PUNCT
eurjchem-864	264	45	f.	f.	PROPN
eurjchem-864	264	46	p.	p.	PROPN
eurjchem-864	264	47	;	;	PUNCT
eurjchem-864	264	48	dunn	dunn	PROPN
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eurjchem-864	264	50	r.	r.	PROPN
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eurjchem-864	264	56	.	.	PUNCT
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eurjchem-864	265	2	,	,	PUNCT
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eurjchem-864	265	4	,	,	PUNCT
eurjchem-864	265	5	761‐767	761‐767	PROPN
eurjchem-864	265	6	.	.	PUNCT
eurjchem-864	266	1	[	[	X
eurjchem-864	266	2	8	8	NUM
eurjchem-864	266	3	]	]	X
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eurjchem-864	266	5	,	,	PUNCT
eurjchem-864	266	6	p.	p.	PROPN
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eurjchem-864	266	8	j.	j.	PROPN
eurjchem-864	266	9	;	;	PUNCT
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eurjchem-864	266	11	,	,	PUNCT
eurjchem-864	266	12	c.	c.	PROPN
eurjchem-864	266	13	j.	j.	PROPN
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eurjchem-864	266	15	;	;	PUNCT
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eurjchem-864	266	17	,	,	PUNCT
eurjchem-864	266	18	f.	f.	PROPN
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eurjchem-864	266	22	k.	k.	PROPN
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eurjchem-864	266	25	;	;	PUNCT
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eurjchem-864	266	28	a.	a.	PROPN
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eurjchem-864	266	31	p.	p.	PROPN
eurjchem-864	266	32	;	;	PUNCT
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eurjchem-864	266	35	t.	t.	PROPN
eurjchem-864	266	36	f.	f.	PROPN
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eurjchem-864	266	39	.	.	PUNCT
eurjchem-864	267	1	exp	exp	PROPN
eurjchem-864	267	2	.	.	PUNCT
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eurjchem-864	268	2	.	.	PUNCT
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eurjchem-864	269	2	,	,	PUNCT
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eurjchem-864	269	4	,	,	PUNCT
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eurjchem-864	269	6	.	.	PUNCT
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eurjchem-864	270	3	]	]	PUNCT
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eurjchem-864	270	5	,	,	PUNCT
eurjchem-864	270	6	a.	a.	NOUN
eurjchem-864	270	7	;	;	PUNCT
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eurjchem-864	270	9	,	,	PUNCT
eurjchem-864	270	10	m.	m.	NOUN
eurjchem-864	270	11	;	;	PUNCT
eurjchem-864	270	12	renard	renard	PROPN
eurjchem-864	270	13	,	,	PUNCT
eurjchem-864	270	14	p.	p.	NOUN
eurjchem-864	270	15	;	;	PUNCT
eurjchem-864	270	16	devaux	devaux	PROPN
eurjchem-864	270	17	,	,	PUNCT
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eurjchem-864	270	19	eur	eur	PROPN
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eurjchem-864	271	1	j.	j.	PROPN
eurjchem-864	271	2	med	med	PROPN
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eurjchem-864	271	5	.	.	PUNCT
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eurjchem-864	272	2	,	,	PUNCT
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eurjchem-864	272	4	,	,	PUNCT
eurjchem-864	272	5	75‐82	75‐82	NUM
eurjchem-864	272	6	.	.	PUNCT
eurjchem-864	273	1	[	[	X
eurjchem-864	273	2	10	10	NUM
eurjchem-864	273	3	]	]	X
eurjchem-864	273	4	hasegawa	hasegawa	PROPN
eurjchem-864	273	5	,	,	PUNCT
eurjchem-864	273	6	h.	h.	PROPN
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eurjchem-864	273	8	.	.	PUNCT
eurjchem-864	273	9	med	med	PROPN
eurjchem-864	273	10	.	.	PUNCT
eurjchem-864	274	1	res	re	NOUN
eurjchem-864	274	2	.	.	PUNCT
eurjchem-864	275	1	opin	opin	NOUN
eurjchem-864	275	2	.	.	PUNCT
eurjchem-864	276	1	2004	2004	NUM
eurjchem-864	276	2	,	,	PUNCT
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eurjchem-864	276	4	,	,	PUNCT
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eurjchem-864	276	6	.	.	PUNCT
eurjchem-864	277	1	[	[	X
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eurjchem-864	277	3	]	]	X
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eurjchem-864	277	5	,	,	PUNCT
eurjchem-864	277	6	c.	c.	PROPN
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eurjchem-864	277	8	;	;	PUNCT
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eurjchem-864	277	11	,	,	PUNCT
eurjchem-864	277	12	d.	d.	PROPN
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eurjchem-864	277	14	;	;	PUNCT
eurjchem-864	277	15	suhas	suhas	PROPN
eurjchem-864	277	16	,	,	PUNCT
eurjchem-864	277	17	r.	r.	PROPN
eurjchem-864	277	18	;	;	PUNCT
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eurjchem-864	277	20	,	,	PUNCT
eurjchem-864	277	21	m.	m.	PROPN
eurjchem-864	277	22	b.	b.	PROPN
eurjchem-864	277	23	;	;	PUNCT
eurjchem-864	277	24	channe	channe	PROPN
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eurjchem-864	277	26	,	,	PUNCT
eurjchem-864	277	27	d.	d.	PROPN
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eurjchem-864	278	1	j.	j.	PROPN
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eurjchem-864	278	5	.	.	PUNCT
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eurjchem-864	279	2	,	,	PUNCT
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eurjchem-864	279	4	,	,	PUNCT
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eurjchem-864	279	6	.	.	PUNCT
eurjchem-864	280	1	[	[	X
eurjchem-864	280	2	12	12	NUM
eurjchem-864	280	3	]	]	X
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eurjchem-864	280	5	,	,	PUNCT
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eurjchem-864	280	7	;	;	PUNCT
eurjchem-864	280	8	blake	blake	PROPN
eurjchem-864	280	9	,	,	PUNCT
eurjchem-864	280	10	j.	j.	PROPN
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eurjchem-864	280	17	;	;	PUNCT
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eurjchem-864	280	19	,	,	PUNCT
eurjchem-864	280	20	t.	t.	PROPN
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eurjchem-864	280	22	;	;	PUNCT
eurjchem-864	280	23	chapin	chapin	PROPN
eurjchem-864	280	24	,	,	PUNCT
eurjchem-864	280	25	d.	d.	PROPN
eurjchem-864	280	26	s.	s.	PROPN
eurjchem-864	280	27	;	;	PUNCT
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eurjchem-864	280	29	,	,	PUNCT
eurjchem-864	280	30	y.	y.	PROPN
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eurjchem-864	280	32	;	;	PUNCT
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eurjchem-864	280	35	j.	j.	PROPN
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eurjchem-864	280	40	s.	s.	PROPN
eurjchem-864	280	41	b.	b.	PROPN
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eurjchem-864	280	44	,	,	PUNCT
eurjchem-864	280	45	d.	d.	PROPN
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eurjchem-864	280	55	d.	d.	PROPN
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eurjchem-864	280	60	j.	j.	PROPN
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eurjchem-864	280	62	;	;	PUNCT
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eurjchem-864	280	66	a.	a.	PROPN
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eurjchem-864	280	82	.	.	PUNCT
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eurjchem-864	281	3	]	]	PUNCT
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eurjchem-864	281	5	,	,	PUNCT
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eurjchem-864	281	8	;	;	PUNCT
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eurjchem-864	282	1	j.	j.	PROPN
eurjchem-864	282	2	phys	phys	PROPN
eurjchem-864	282	3	.	.	PUNCT
eurjchem-864	283	1	chem	chem	PROPN
eurjchem-864	283	2	.	.	PUNCT
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eurjchem-864	284	2	,	,	PUNCT
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eurjchem-864	284	4	,	,	PUNCT
eurjchem-864	284	5	773‐779	773‐779	NUM
eurjchem-864	284	6	.	.	PUNCT
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eurjchem-864	285	5	,	,	PUNCT
eurjchem-864	285	6	s.	s.	PROPN
eurjchem-864	285	7	;	;	PUNCT
eurjchem-864	285	8	fitton	fitton	PROPN
eurjchem-864	285	9	,	,	PUNCT
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eurjchem-864	285	13	,	,	PUNCT
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eurjchem-864	285	17	.	.	PUNCT
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eurjchem-864	286	5	,	,	PUNCT
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eurjchem-864	286	9	;	;	PUNCT
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eurjchem-864	286	12	y.	y.	PROPN
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eurjchem-864	286	14	;	;	PUNCT
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eurjchem-864	286	17	y.	y.	PROPN
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eurjchem-864	287	2	,	,	PUNCT
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eurjchem-864	287	4	,	,	PUNCT
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eurjchem-864	288	5	,	,	PUNCT
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eurjchem-864	289	2	.	.	PUNCT
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eurjchem-864	290	2	,	,	PUNCT
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eurjchem-864	291	5	,	,	PUNCT
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eurjchem-864	291	7	;	;	PUNCT
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eurjchem-864	291	16	.	.	PUNCT
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eurjchem-864	292	2	.	.	PUNCT
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eurjchem-864	293	5	,	,	PUNCT
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eurjchem-864	294	8	;	;	PUNCT
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eurjchem-864	295	2	.	.	PUNCT
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eurjchem-864	296	2	,	,	PUNCT
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eurjchem-864	297	5	,	,	PUNCT
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eurjchem-864	298	1	biophys	biophy	NOUN
eurjchem-864	298	2	.	.	PUNCT
eurjchem-864	299	1	acta	acta	PROPN
eurjchem-864	299	2	1957	1957	NUM
eurjchem-864	299	3	,	,	PUNCT
eurjchem-864	299	4	24	24	NUM
eurjchem-864	299	5	,	,	PUNCT
eurjchem-864	299	6	619‐623	619‐623	ADV
eurjchem-864	299	7	.	.	PUNCT