id	sid	tid	token	lemma	pos
eurjchem-942	1	1	untitled	untitle	VERB
eurjchem-942	1	2	european	european	PROPN
eurjchem-942	1	3	journal	journal	PROPN
eurjchem-942	1	4	of	of	ADP
eurjchem-942	1	5	chemistry	chemistry	NOUN
eurjchem-942	1	6	5	5	NUM
eurjchem-942	1	7	(	(	PUNCT
eurjchem-942	1	8	1	1	NUM
eurjchem-942	1	9	)	)	PUNCT
eurjchem-942	1	10	(	(	PUNCT
eurjchem-942	1	11	2014	2014	NUM
eurjchem-942	1	12	)	)	PUNCT
eurjchem-942	1	13	181‐185	181‐185	NUM
eurjchem-942	1	14	european	european	PROPN
eurjchem-942	1	15	journal	journal	PROPN
eurjchem-942	1	16	of	of	ADP
eurjchem-942	1	17	chemistry	chemistry	NOUN
eurjchem-942	1	18	issn	issn	PROPN
eurjchem-942	1	19	2153‐2249	2153‐2249	PROPN
eurjchem-942	1	20	(	(	PUNCT
eurjchem-942	1	21	print	print	NOUN
eurjchem-942	1	22	)	)	PUNCT
eurjchem-942	1	23	/	/	SYM
eurjchem-942	1	24	issn	issn	PROPN
eurjchem-942	1	25	2153‐2257	2153‐2257	NUM
eurjchem-942	1	26	(	(	PUNCT
eurjchem-942	1	27	online	online	ADJ
eurjchem-942	1	28	)	)	PUNCT
eurjchem-942	1	29			NOUN
eurjchem-942	1	30	2014	2014	NUM
eurjchem-942	2	1	eurjchem	eurjchem	PROPN
eurjchem-942	2	2	publishing	publish	VERB
eurjchem-942	2	3	‐	‐	NOUN
eurjchem-942	2	4	printed	print	VERB
eurjchem-942	2	5	in	in	ADP
eurjchem-942	2	6	the	the	DET
eurjchem-942	2	7	usa	usa	PROPN
eurjchem-942	2	8	http://dx.doi.org/10.5155/eurjchem.5.1.181‐185.942	http://dx.doi.org/10.5155/eurjchem.5.1.181‐185.942	NUM
eurjchem-942	2	9	european	european	PROPN
eurjchem-942	2	10	journal	journal	PROPN
eurjchem-942	2	11	of	of	ADP
eurjchem-942	2	12	chemistry	chemistry	PROPN
eurjchem-942	2	13	journal	journal	PROPN
eurjchem-942	2	14	homepage	homepage	NOUN
eurjchem-942	2	15	:	:	PUNCT
eurjchem-942	2	16	www.eurjchem.com	www.eurjchem.com	X
eurjchem-942	2	17	simultaneous	simultaneous	ADJ
eurjchem-942	2	18	quantitative	quantitative	ADJ
eurjchem-942	2	19	analysis	analysis	NOUN
eurjchem-942	2	20	of	of	ADP
eurjchem-942	2	21	tamsulosin	tamsulosin	NOUN
eurjchem-942	2	22	and	and	CCONJ
eurjchem-942	2	23	finasteride	finasteride	ADJ
eurjchem-942	2	24	in	in	ADP
eurjchem-942	2	25	pharmaceutical	pharmaceutical	ADJ
eurjchem-942	2	26	dosage	dosage	NOUN
eurjchem-942	2	27	form	form	NOUN
eurjchem-942	2	28	by	by	ADP
eurjchem-942	2	29	u‐hplc	u‐hplc	PUNCT
eurjchem-942	2	30	tandem	tandem	PROPN
eurjchem-942	2	31	mass	mass	PROPN
eurjchem-942	2	32	spectrometry	spectrometry	PROPN
eurjchem-942	2	33	dalia	dalia	PROPN
eurjchem-942	2	34	mohamed	mohame	VERB
eurjchem-942	2	35	a	a	PROPN
eurjchem-942	2	36	,	,	PUNCT
eurjchem-942	2	37	b	b	PROPN
eurjchem-942	2	38	,	,	PUNCT
eurjchem-942	2	39	*	*	PROPN
eurjchem-942	2	40	,	,	PUNCT
eurjchem-942	2	41	shereen	shereen	PROPN
eurjchem-942	2	42	mowaka	mowaka	PROPN
eurjchem-942	2	43	a	a	PRON
eurjchem-942	2	44	,	,	PUNCT
eurjchem-942	2	45	c	c	NOUN
eurjchem-942	2	46	,	,	PUNCT
eurjchem-942	2	47	and	and	CCONJ
eurjchem-942	2	48	ahmed	ahmed	PROPN
eurjchem-942	2	49	mostafa	mostafa	PROPN
eurjchem-942	3	1	d	d	PROPN
eurjchem-942	3	2	a	a	DET
eurjchem-942	3	3	analytical	analytical	ADJ
eurjchem-942	3	4	chemistry	chemistry	NOUN
eurjchem-942	3	5	department	department	NOUN
eurjchem-942	3	6	,	,	PUNCT
eurjchem-942	3	7	faculty	faculty	NOUN
eurjchem-942	3	8	of	of	ADP
eurjchem-942	3	9	pharmacy	pharmacy	NOUN
eurjchem-942	3	10	,	,	PUNCT
eurjchem-942	3	11	helwan	helwan	PROPN
eurjchem-942	3	12	university	university	PROPN
eurjchem-942	3	13	,	,	PUNCT
eurjchem-942	3	14	ein	ein	PROPN
eurjchem-942	3	15	helwan	helwan	PROPN
eurjchem-942	3	16	,	,	PUNCT
eurjchem-942	3	17	11795	11795	NUM
eurjchem-942	3	18	,	,	PUNCT
eurjchem-942	3	19	cairo	cairo	PROPN
eurjchem-942	3	20	,	,	PUNCT
eurjchem-942	3	21	egypt	egypt	PROPN
eurjchem-942	3	22	b	b	PROPN
eurjchem-942	3	23	pharmaceutical	pharmaceutical	ADJ
eurjchem-942	3	24	analytical	analytical	ADJ
eurjchem-942	3	25	chemistry	chemistry	NOUN
eurjchem-942	3	26	department	department	NOUN
eurjchem-942	3	27	,	,	PUNCT
eurjchem-942	3	28	faculty	faculty	NOUN
eurjchem-942	3	29	of	of	ADP
eurjchem-942	3	30	pharmacy	pharmacy	NOUN
eurjchem-942	3	31	,	,	PUNCT
eurjchem-942	3	32	6	6	NUM
eurjchem-942	3	33	october	october	PROPN
eurjchem-942	3	34	university	university	NOUN
eurjchem-942	3	35	for	for	ADP
eurjchem-942	3	36	modern	modern	ADJ
eurjchem-942	3	37	sciences	science	NOUN
eurjchem-942	3	38	and	and	CCONJ
eurjchem-942	3	39	arts	art	NOUN
eurjchem-942	3	40	,	,	PUNCT
eurjchem-942	3	41	11787	11787	NUM
eurjchem-942	3	42	,	,	PUNCT
eurjchem-942	3	43	6	6	NUM
eurjchem-942	3	44	october	october	PROPN
eurjchem-942	3	45	city	city	PROPN
eurjchem-942	3	46	,	,	PUNCT
eurjchem-942	3	47	egypt	egypt	PROPN
eurjchem-942	3	48	c	c	PROPN
eurjchem-942	3	49	analytical	analytical	ADJ
eurjchem-942	3	50	chemistry	chemistry	NOUN
eurjchem-942	3	51	department	department	NOUN
eurjchem-942	3	52	,	,	PUNCT
eurjchem-942	3	53	faculty	faculty	NOUN
eurjchem-942	3	54	of	of	ADP
eurjchem-942	3	55	pharmacy	pharmacy	NOUN
eurjchem-942	3	56	,	,	PUNCT
eurjchem-942	3	57	british	british	ADJ
eurjchem-942	3	58	university	university	PROPN
eurjchem-942	3	59	in	in	ADP
eurjchem-942	3	60	egypt	egypt	PROPN
eurjchem-942	3	61	,	,	PUNCT
eurjchem-942	3	62	11837	11837	NUM
eurjchem-942	3	63	,	,	PUNCT
eurjchem-942	3	64	el‐sherouk	el‐sherouk	PROPN
eurjchem-942	3	65	city	city	NOUN
eurjchem-942	3	66	,	,	PUNCT
eurjchem-942	3	67	egypt	egypt	PROPN
eurjchem-942	3	68	d	d	PROPN
eurjchem-942	3	69	pharmaceutical	pharmaceutical	ADJ
eurjchem-942	3	70	chemistry	chemistry	NOUN
eurjchem-942	3	71	department	department	NOUN
eurjchem-942	3	72	,	,	PUNCT
eurjchem-942	3	73	faculty	faculty	NOUN
eurjchem-942	3	74	of	of	ADP
eurjchem-942	3	75	pharmacy	pharmacy	NOUN
eurjchem-942	3	76	,	,	PUNCT
eurjchem-942	3	77	helwan	helwan	PROPN
eurjchem-942	3	78	university	university	PROPN
eurjchem-942	3	79	,	,	PUNCT
eurjchem-942	3	80	ein	ein	PROPN
eurjchem-942	3	81	helwan	helwan	PROPN
eurjchem-942	3	82	,	,	PUNCT
eurjchem-942	3	83	11795	11795	NUM
eurjchem-942	3	84	,	,	PUNCT
eurjchem-942	3	85	cairo	cairo	PROPN
eurjchem-942	3	86	,	,	PUNCT
eurjchem-942	3	87	egypt	egypt	PROPN
eurjchem-942	3	88	*	*	PUNCT
eurjchem-942	3	89	corresponding	correspond	VERB
eurjchem-942	3	90	author	author	NOUN
eurjchem-942	3	91	at	at	ADP
eurjchem-942	3	92	:	:	PUNCT
eurjchem-942	3	93	analytical	analytical	ADJ
eurjchem-942	3	94	chemistry	chemistry	NOUN
eurjchem-942	3	95	department	department	NOUN
eurjchem-942	3	96	,	,	PUNCT
eurjchem-942	3	97	faculty	faculty	NOUN
eurjchem-942	3	98	of	of	ADP
eurjchem-942	3	99	pharmacy	pharmacy	NOUN
eurjchem-942	3	100	,	,	PUNCT
eurjchem-942	3	101	helwan	helwan	PROPN
eurjchem-942	3	102	university	university	PROPN
eurjchem-942	3	103	,	,	PUNCT
eurjchem-942	3	104	ein	ein	PROPN
eurjchem-942	3	105	helwan	helwan	PROPN
eurjchem-942	3	106	,	,	PUNCT
eurjchem-942	3	107	11795	11795	NUM
eurjchem-942	3	108	,	,	PUNCT
eurjchem-942	3	109	cairo	cairo	PROPN
eurjchem-942	3	110	,	,	PUNCT
eurjchem-942	3	111	egypt	egypt	PROPN
eurjchem-942	3	112	.	.	PUNCT
eurjchem-942	4	1	tel	tel	PROPN
eurjchem-942	4	2	.	.	PROPN
eurjchem-942	4	3	:	:	PUNCT
eurjchem-942	5	1	+2.02.25541601	+2.02.25541601	PROPN
eurjchem-942	5	2	.	.	PUNCT
eurjchem-942	5	3	fax	fax	NOUN
eurjchem-942	5	4	:	:	PUNCT
eurjchem-942	5	5	+2.02.25541601	+2.02.25541601	PROPN
eurjchem-942	5	6	.	.	PUNCT
eurjchem-942	5	7	e‐mail	e‐mail	PUNCT
eurjchem-942	6	1	address	address	NOUN
eurjchem-942	6	2	:	:	PUNCT
eurjchem-942	6	3	daliammamdouh@gmail.com	daliammamdouh@gmail.com	PROPN
eurjchem-942	6	4	(	(	PUNCT
eurjchem-942	6	5	d.	d.	PROPN
eurjchem-942	6	6	mohamed	mohamed	PROPN
eurjchem-942	6	7	)	)	PUNCT
eurjchem-942	6	8	.	.	PUNCT
eurjchem-942	7	1	article	article	NOUN
eurjchem-942	7	2	information	information	PROPN
eurjchem-942	7	3	abstract	abstract	ADJ
eurjchem-942	7	4	doi	doi	NOUN
eurjchem-942	7	5	:	:	PUNCT
eurjchem-942	7	6	10.5155	10.5155	NUM
eurjchem-942	7	7	/	/	SYM
eurjchem-942	7	8	eurjchem.5.1.181‐185.942	eurjchem.5.1.181‐185.942	NOUN
eurjchem-942	7	9	received	receive	VERB
eurjchem-942	7	10	:	:	PUNCT
eurjchem-942	7	11	04	04	NUM
eurjchem-942	7	12	october	october	PROPN
eurjchem-942	7	13	2013	2013	NUM
eurjchem-942	7	14	received	receive	VERB
eurjchem-942	7	15	in	in	ADP
eurjchem-942	7	16	revised	revise	VERB
eurjchem-942	7	17	form	form	NOUN
eurjchem-942	7	18	:	:	PUNCT
eurjchem-942	7	19	02	02	NUM
eurjchem-942	7	20	november	november	PROPN
eurjchem-942	7	21	2013	2013	NUM
eurjchem-942	7	22	accepted	accept	VERB
eurjchem-942	7	23	:	:	PUNCT
eurjchem-942	7	24	02	02	NUM
eurjchem-942	7	25	november	november	PROPN
eurjchem-942	7	26	2013	2013	NUM
eurjchem-942	7	27	online	online	NOUN
eurjchem-942	7	28	:	:	PUNCT
eurjchem-942	7	29	31	31	NUM
eurjchem-942	7	30	march	march	NOUN
eurjchem-942	7	31	2014	2014	NUM
eurjchem-942	7	32	keywords	keyword	VERB
eurjchem-942	7	33	a	a	DET
eurjchem-942	7	34	sensitive	sensitive	ADJ
eurjchem-942	7	35	,	,	PUNCT
eurjchem-942	7	36	rapid	rapid	ADJ
eurjchem-942	7	37	,	,	PUNCT
eurjchem-942	7	38	selective	selective	ADJ
eurjchem-942	7	39	and	and	CCONJ
eurjchem-942	7	40	accurate	accurate	ADJ
eurjchem-942	7	41	liquid	liquid	ADJ
eurjchem-942	7	42	chromatography	chromatography	NOUN
eurjchem-942	7	43	coupled	couple	VERB
eurjchem-942	7	44	to	to	ADP
eurjchem-942	7	45	quadrupole	quadrupole	PROPN
eurjchem-942	7	46	tandem	tandem	PROPN
eurjchem-942	7	47	mass	mass	PROPN
eurjchem-942	7	48	spectrometry	spectrometry	NOUN
eurjchem-942	7	49	(	(	PUNCT
eurjchem-942	7	50	lc‐ms	lc‐ms	NUM
eurjchem-942	7	51	/	/	SYM
eurjchem-942	7	52	ms	ms	PROPN
eurjchem-942	7	53	)	)	PUNCT
eurjchem-942	7	54	method	method	NOUN
eurjchem-942	7	55	was	be	AUX
eurjchem-942	7	56	developed	develop	VERB
eurjchem-942	7	57	for	for	ADP
eurjchem-942	7	58	simultaneous	simultaneous	ADJ
eurjchem-942	7	59	identification	identification	NOUN
eurjchem-942	7	60	and	and	CCONJ
eurjchem-942	7	61	quantification	quantification	NOUN
eurjchem-942	7	62	of	of	ADP
eurjchem-942	7	63	tamsulosin	tamsulosin	NOUN
eurjchem-942	7	64	and	and	CCONJ
eurjchem-942	7	65	finasteride	finasteride	ADV
eurjchem-942	7	66	in	in	ADP
eurjchem-942	7	67	bulk	bulk	NOUN
eurjchem-942	7	68	and	and	CCONJ
eurjchem-942	7	69	in	in	ADP
eurjchem-942	7	70	their	their	PRON
eurjchem-942	7	71	combined	combine	VERB
eurjchem-942	7	72	dosage	dosage	NOUN
eurjchem-942	7	73	form	form	NOUN
eurjchem-942	7	74	.	.	PUNCT
eurjchem-942	8	1	chromatography	chromatography	NOUN
eurjchem-942	8	2	was	be	AUX
eurjchem-942	8	3	performed	perform	VERB
eurjchem-942	8	4	on	on	ADP
eurjchem-942	8	5	a	a	DET
eurjchem-942	8	6	hypersil	hypersil	NOUN
eurjchem-942	8	7	gold	gold	NOUN
eurjchem-942	8	8	50	50	NUM
eurjchem-942	8	9	mm	mm	NOUN
eurjchem-942	8	10	×	×	NOUN
eurjchem-942	8	11	2	2	NUM
eurjchem-942	8	12	mm	mm	NOUN
eurjchem-942	8	13	(	(	PUNCT
eurjchem-942	8	14	1.9	1.9	NUM
eurjchem-942	8	15	μm	μm	NUM
eurjchem-942	8	16	)	)	PUNCT
eurjchem-942	8	17	column	column	NOUN
eurjchem-942	8	18	,	,	PUNCT
eurjchem-942	8	19	using	use	VERB
eurjchem-942	8	20	acetonitrile	acetonitrile	NOUN
eurjchem-942	8	21	:	:	PUNCT
eurjchem-942	8	22	ammonium	ammonium	NOUN
eurjchem-942	8	23	acetate	acetate	NOUN
eurjchem-942	8	24	(	(	PUNCT
eurjchem-942	8	25	90:10	90:10	NUM
eurjchem-942	8	26	,	,	PUNCT
eurjchem-942	8	27	v	v	NOUN
eurjchem-942	8	28	:	:	SYM
eurjchem-942	8	29	v	v	NOUN
eurjchem-942	8	30	)	)	PUNCT
eurjchem-942	8	31	ph	ph	NOUN
eurjchem-942	8	32	=	=	NOUN
eurjchem-942	8	33	3.5	3.5	NUM
eurjchem-942	8	34	as	as	ADP
eurjchem-942	8	35	the	the	DET
eurjchem-942	8	36	mobile	mobile	ADJ
eurjchem-942	8	37	phase	phase	NOUN
eurjchem-942	8	38	.	.	PUNCT
eurjchem-942	9	1	protonated	protonate	VERB
eurjchem-942	9	2	ions	ion	NOUN
eurjchem-942	9	3	formed	form	VERB
eurjchem-942	9	4	by	by	ADP
eurjchem-942	9	5	a	a	DET
eurjchem-942	9	6	turbo	turbo	NOUN
eurjchem-942	9	7	ion‐spray	ion‐spray	NOUN
eurjchem-942	9	8	in	in	ADP
eurjchem-942	9	9	positive	positive	ADJ
eurjchem-942	9	10	mode	mode	NOUN
eurjchem-942	9	11	were	be	AUX
eurjchem-942	9	12	used	use	VERB
eurjchem-942	9	13	to	to	PART
eurjchem-942	9	14	detect	detect	VERB
eurjchem-942	9	15	the	the	DET
eurjchem-942	9	16	analytes	analyte	NOUN
eurjchem-942	9	17	as	as	ADV
eurjchem-942	9	18	well	well	ADV
eurjchem-942	9	19	as	as	ADP
eurjchem-942	9	20	the	the	DET
eurjchem-942	9	21	internal	internal	ADJ
eurjchem-942	9	22	standard	standard	NOUN
eurjchem-942	9	23	(	(	PUNCT
eurjchem-942	9	24	is	be	AUX
eurjchem-942	9	25	)	)	PUNCT
eurjchem-942	9	26	.	.	PUNCT
eurjchem-942	10	1	ms	ms	PROPN
eurjchem-942	10	2	/	/	SYM
eurjchem-942	10	3	ms	ms	PROPN
eurjchem-942	10	4	detection	detection	NOUN
eurjchem-942	10	5	was	be	AUX
eurjchem-942	10	6	carried	carry	VERB
eurjchem-942	10	7	out	out	ADP
eurjchem-942	10	8	by	by	ADP
eurjchem-942	10	9	monitoring	monitor	VERB
eurjchem-942	10	10	the	the	DET
eurjchem-942	10	11	fragmentation	fragmentation	NOUN
eurjchem-942	10	12	of	of	ADP
eurjchem-942	10	13	408.74	408.74	NUM
eurjchem-942	10	14	→	→	SYM
eurjchem-942	10	15	227.29	227.29	NUM
eurjchem-942	10	16	(	(	PUNCT
eurjchem-942	10	17	m	m	NOUN
eurjchem-942	10	18	/	/	SYM
eurjchem-942	10	19	z	z	NOUN
eurjchem-942	10	20	)	)	PUNCT
eurjchem-942	10	21	,	,	PUNCT
eurjchem-942	10	22	373.11	373.11	NUM
eurjchem-942	10	23	→	→	SYM
eurjchem-942	10	24	304.96	304.96	NUM
eurjchem-942	10	25	(	(	PUNCT
eurjchem-942	10	26	m	m	PROPN
eurjchem-942	10	27	/	/	SYM
eurjchem-942	10	28	z	z	NOUN
eurjchem-942	10	29	)	)	PUNCT
eurjchem-942	10	30	and	and	CCONJ
eurjchem-942	10	31	255.75	255.75	NUM
eurjchem-942	10	32	→	→	SYM
eurjchem-942	10	33	166.15	166.15	NUM
eurjchem-942	10	34	(	(	PUNCT
eurjchem-942	10	35	m	m	PROPN
eurjchem-942	10	36	/	/	SYM
eurjchem-942	10	37	z	z	NOUN
eurjchem-942	10	38	)	)	PUNCT
eurjchem-942	10	39	for	for	ADP
eurjchem-942	10	40	tamsulosin	tamsulosin	NOUN
eurjchem-942	10	41	,	,	PUNCT
eurjchem-942	10	42	finasteride	finasteride	ADJ
eurjchem-942	10	43	and	and	CCONJ
eurjchem-942	10	44	diphenhydramine	diphenhydramine	ADJ
eurjchem-942	10	45	(	(	PUNCT
eurjchem-942	10	46	is	be	AUX
eurjchem-942	10	47	)	)	PUNCT
eurjchem-942	10	48	,	,	PUNCT
eurjchem-942	10	49	respectively	respectively	ADV
eurjchem-942	10	50	,	,	PUNCT
eurjchem-942	10	51	on	on	ADP
eurjchem-942	10	52	a	a	DET
eurjchem-942	10	53	triple	triple	ADJ
eurjchem-942	10	54	quadrupole	quadrupole	NOUN
eurjchem-942	10	55	mass	mass	NOUN
eurjchem-942	10	56	spectrometer	spectrometer	NOUN
eurjchem-942	10	57	.	.	PUNCT
eurjchem-942	11	1	the	the	DET
eurjchem-942	11	2	linearity	linearity	NOUN
eurjchem-942	11	3	was	be	AUX
eurjchem-942	11	4	obtained	obtain	VERB
eurjchem-942	11	5	over	over	ADP
eurjchem-942	11	6	the	the	DET
eurjchem-942	11	7	concentration	concentration	NOUN
eurjchem-942	11	8	range	range	NOUN
eurjchem-942	11	9	of	of	ADP
eurjchem-942	11	10	1.6‐40.0	1.6‐40.0	PROPN
eurjchem-942	11	11	ng	ng	PROPN
eurjchem-942	11	12	/	/	SYM
eurjchem-942	11	13	ml	ml	X
eurjchem-942	11	14	for	for	ADP
eurjchem-942	11	15	tamsulosin	tamsulosin	NOUN
eurjchem-942	11	16	and	and	CCONJ
eurjchem-942	11	17	20.0‐500.0	20.0‐500.0	PROPN
eurjchem-942	11	18	ng	ng	PROPN
eurjchem-942	11	19	/	/	SYM
eurjchem-942	11	20	ml	ml	X
eurjchem-942	11	21	for	for	ADP
eurjchem-942	11	22	finasteride	finasteride	ADJ
eurjchem-942	11	23	with	with	ADP
eurjchem-942	11	24	a	a	DET
eurjchem-942	11	25	lower	low	ADJ
eurjchem-942	11	26	limit	limit	NOUN
eurjchem-942	11	27	of	of	ADP
eurjchem-942	11	28	detection	detection	NOUN
eurjchem-942	11	29	of	of	ADP
eurjchem-942	11	30	0.5	0.5	NUM
eurjchem-942	11	31	ng	ng	NOUN
eurjchem-942	11	32	/	/	SYM
eurjchem-942	11	33	ml	ml	PROPN
eurjchem-942	11	34	and	and	CCONJ
eurjchem-942	11	35	5.0	5.0	NUM
eurjchem-942	11	36	ng	ng	NOUN
eurjchem-942	11	37	/	/	SYM
eurjchem-942	11	38	ml	ml	X
eurjchem-942	11	39	for	for	ADP
eurjchem-942	11	40	the	the	DET
eurjchem-942	11	41	two	two	NUM
eurjchem-942	11	42	drugs	drug	NOUN
eurjchem-942	11	43	,	,	PUNCT
eurjchem-942	11	44	respectively	respectively	ADV
eurjchem-942	11	45	.	.	PUNCT
eurjchem-942	12	1	the	the	DET
eurjchem-942	12	2	proposed	propose	VERB
eurjchem-942	12	3	method	method	NOUN
eurjchem-942	12	4	was	be	AUX
eurjchem-942	12	5	successfully	successfully	ADV
eurjchem-942	12	6	applied	apply	VERB
eurjchem-942	12	7	to	to	ADP
eurjchem-942	12	8	tamsulosin	tamsulosin	NOUN
eurjchem-942	12	9	and	and	CCONJ
eurjchem-942	12	10	finasteride	finasteride	ADJ
eurjchem-942	12	11	determination	determination	NOUN
eurjchem-942	12	12	in	in	ADP
eurjchem-942	12	13	pharmaceutical	pharmaceutical	ADJ
eurjchem-942	12	14	dosage	dosage	NOUN
eurjchem-942	12	15	form	form	NOUN
eurjchem-942	12	16	.	.	PUNCT
eurjchem-942	13	1	the	the	DET
eurjchem-942	13	2	results	result	NOUN
eurjchem-942	13	3	obtained	obtain	VERB
eurjchem-942	13	4	were	be	AUX
eurjchem-942	13	5	statistically	statistically	ADV
eurjchem-942	13	6	analyzed	analyze	VERB
eurjchem-942	13	7	and	and	CCONJ
eurjchem-942	13	8	compared	compare	VERB
eurjchem-942	13	9	with	with	ADP
eurjchem-942	13	10	those	those	PRON
eurjchem-942	13	11	of	of	ADP
eurjchem-942	13	12	reference	reference	NOUN
eurjchem-942	13	13	ones	one	NOUN
eurjchem-942	13	14	;	;	PUNCT
eurjchem-942	13	15	in	in	ADP
eurjchem-942	13	16	addition	addition	NOUN
eurjchem-942	13	17	,	,	PUNCT
eurjchem-942	13	18	the	the	DET
eurjchem-942	13	19	method	method	NOUN
eurjchem-942	13	20	was	be	AUX
eurjchem-942	13	21	validated	validate	VERB
eurjchem-942	13	22	according	accord	VERB
eurjchem-942	13	23	to	to	ADP
eurjchem-942	13	24	usp	usp	NOUN
eurjchem-942	13	25	34	34	NUM
eurjchem-942	13	26	recommendations	recommendation	NOUN
eurjchem-942	13	27	.	.	PUNCT
eurjchem-942	14	1	the	the	DET
eurjchem-942	14	2	simplicity	simplicity	NOUN
eurjchem-942	14	3	and	and	CCONJ
eurjchem-942	14	4	sensitivity	sensitivity	NOUN
eurjchem-942	14	5	of	of	ADP
eurjchem-942	14	6	this	this	DET
eurjchem-942	14	7	method	method	NOUN
eurjchem-942	14	8	allows	allow	VERB
eurjchem-942	14	9	its	its	PRON
eurjchem-942	14	10	use	use	NOUN
eurjchem-942	14	11	in	in	ADP
eurjchem-942	14	12	the	the	DET
eurjchem-942	14	13	quality	quality	NOUN
eurjchem-942	14	14	control	control	NOUN
eurjchem-942	14	15	of	of	ADP
eurjchem-942	14	16	the	the	DET
eurjchem-942	14	17	cited	cite	VERB
eurjchem-942	14	18	drugs	drug	NOUN
eurjchem-942	14	19	and	and	CCONJ
eurjchem-942	14	20	can	can	AUX
eurjchem-942	14	21	be	be	AUX
eurjchem-942	14	22	extended	extend	VERB
eurjchem-942	14	23	for	for	ADP
eurjchem-942	14	24	routine	routine	ADJ
eurjchem-942	14	25	analysis	analysis	NOUN
eurjchem-942	14	26	of	of	ADP
eurjchem-942	14	27	the	the	DET
eurjchem-942	14	28	drugs	drug	NOUN
eurjchem-942	14	29	in	in	ADP
eurjchem-942	14	30	their	their	PRON
eurjchem-942	14	31	pharmaceutical	pharmaceutical	ADJ
eurjchem-942	14	32	preparations	preparation	NOUN
eurjchem-942	14	33	.	.	PUNCT
eurjchem-942	15	1	validation	validation	NOUN
eurjchem-942	15	2	tamsulosin	tamsulosin	VERB
eurjchem-942	15	3	finasteride	finasteride	ADJ
eurjchem-942	15	4	diphenhydramine	diphenhydramine	NOUN
eurjchem-942	15	5	pharmaceutical	pharmaceutical	ADJ
eurjchem-942	15	6	dosage	dosage	NOUN
eurjchem-942	15	7	form	form	NOUN
eurjchem-942	15	8	liquid	liquid	ADJ
eurjchem-942	15	9	chromatography	chromatography	NOUN
eurjchem-942	15	10	tandem	tandem	NOUN
eurjchem-942	15	11	mass	mass	PROPN
eurjchem-942	15	12	spectrometry	spectrometry	NOUN
eurjchem-942	15	13	1	1	NUM
eurjchem-942	15	14	.	.	PUNCT
eurjchem-942	15	15	introduction	introduction	NOUN
eurjchem-942	15	16	tamsulosin	tamsulosin	NOUN
eurjchem-942	15	17	(	(	PUNCT
eurjchem-942	15	18	tam	tam	NOUN
eurjchem-942	15	19	)	)	PUNCT
eurjchem-942	15	20	is	be	AUX
eurjchem-942	15	21	a	a	DET
eurjchem-942	15	22	sulfamoylphenethylamine	sulfamoylphenethylamine	ADJ
eurjchem-942	15	23	derivative	derivative	NOUN
eurjchem-942	15	24	(	(	PUNCT
eurjchem-942	15	25	figure	figure	NOUN
eurjchem-942	15	26	1	1	NUM
eurjchem-942	15	27	)	)	PUNCT
eurjchem-942	15	28	commonly	commonly	ADV
eurjchem-942	15	29	used	use	VERB
eurjchem-942	15	30	to	to	PART
eurjchem-942	15	31	treat	treat	VERB
eurjchem-942	15	32	signs	sign	NOUN
eurjchem-942	15	33	and	and	CCONJ
eurjchem-942	15	34	symptoms	symptom	NOUN
eurjchem-942	15	35	of	of	ADP
eurjchem-942	15	36	benign	benign	ADJ
eurjchem-942	15	37	prostatic	prostatic	ADJ
eurjchem-942	15	38	hyperplasia	hyperplasia	NOUN
eurjchem-942	15	39	(	(	PUNCT
eurjchem-942	15	40	bph	bph	NOUN
eurjchem-942	15	41	)	)	PUNCT
eurjchem-942	16	1	[	[	X
eurjchem-942	16	2	1,2	1,2	NUM
eurjchem-942	16	3	]	]	PUNCT
eurjchem-942	16	4	.	.	PUNCT
eurjchem-942	17	1	tam	tam	PROPN
eurjchem-942	17	2	is	be	AUX
eurjchem-942	17	3	a	a	DET
eurjchem-942	17	4	selective	selective	ADJ
eurjchem-942	17	5	,	,	PUNCT
eurjchem-942	17	6	potent	potent	ADJ
eurjchem-942	17	7	and	and	CCONJ
eurjchem-942	17	8	competitive	competitive	ADJ
eurjchem-942	17	9	α1‐adrenoceptor	α1‐adrenoceptor	NOUN
eurjchem-942	17	10	antagonist	antagonist	NOUN
eurjchem-942	17	11	[	[	PUNCT
eurjchem-942	17	12	3,4	3,4	NUM
eurjchem-942	17	13	]	]	PUNCT
eurjchem-942	17	14	.	.	PUNCT
eurjchem-942	18	1	the	the	DET
eurjchem-942	18	2	usp	usp	PROPN
eurjchem-942	18	3	has	have	AUX
eurjchem-942	18	4	described	describe	VERB
eurjchem-942	18	5	a	a	DET
eurjchem-942	18	6	potentiometric	potentiometric	ADJ
eurjchem-942	18	7	method	method	NOUN
eurjchem-942	18	8	for	for	ADP
eurjchem-942	18	9	the	the	DET
eurjchem-942	18	10	analysis	analysis	NOUN
eurjchem-942	18	11	of	of	ADP
eurjchem-942	18	12	tam	tam	NOUN
eurjchem-942	18	13	[	[	X
eurjchem-942	18	14	5	5	NUM
eurjchem-942	18	15	]	]	PUNCT
eurjchem-942	18	16	,	,	PUNCT
eurjchem-942	18	17	besides	besides	ADV
eurjchem-942	18	18	;	;	PUNCT
eurjchem-942	18	19	various	various	ADJ
eurjchem-942	18	20	analytical	analytical	ADJ
eurjchem-942	18	21	techniques	technique	NOUN
eurjchem-942	18	22	have	have	AUX
eurjchem-942	18	23	been	be	AUX
eurjchem-942	18	24	reported	report	VERB
eurjchem-942	18	25	for	for	ADP
eurjchem-942	18	26	the	the	DET
eurjchem-942	18	27	determination	determination	NOUN
eurjchem-942	18	28	of	of	ADP
eurjchem-942	18	29	tam	tam	NOUN
eurjchem-942	18	30	in	in	ADP
eurjchem-942	18	31	bulk	bulk	NOUN
eurjchem-942	18	32	,	,	PUNCT
eurjchem-942	18	33	pharma‐	pharma‐	NOUN
eurjchem-942	18	34	ceutical	ceutical	ADJ
eurjchem-942	18	35	formulations	formulation	NOUN
eurjchem-942	18	36	and	and	CCONJ
eurjchem-942	18	37	biological	biological	ADJ
eurjchem-942	18	38	samples	sample	NOUN
eurjchem-942	18	39	.	.	PUNCT
eurjchem-942	19	1	these	these	DET
eurjchem-942	19	2	techniques	technique	NOUN
eurjchem-942	19	3	include	include	VERB
eurjchem-942	19	4	hplc	hplc	NOUN
eurjchem-942	19	5	[	[	X
eurjchem-942	19	6	6‐9	6‐9	NOUN
eurjchem-942	19	7	]	]	PUNCT
eurjchem-942	19	8	,	,	PUNCT
eurjchem-942	19	9	stability	stability	NOUN
eurjchem-942	19	10	indicating	indicate	VERB
eurjchem-942	19	11	hplc	hplc	NOUN
eurjchem-942	19	12	[	[	X
eurjchem-942	19	13	10	10	NUM
eurjchem-942	19	14	]	]	PUNCT
eurjchem-942	19	15	,	,	PUNCT
eurjchem-942	19	16	stability	stability	NOUN
eurjchem-942	19	17	indicating	indicate	VERB
eurjchem-942	19	18	hptlc	hptlc	NOUN
eurjchem-942	19	19	[	[	X
eurjchem-942	19	20	11	11	NUM
eurjchem-942	19	21	]	]	PUNCT
eurjchem-942	19	22	,	,	PUNCT
eurjchem-942	19	23	lc‐ms	lc‐ms	AUX
eurjchem-942	19	24	/	/	SYM
eurjchem-942	19	25	ms	ms	NOUN
eurjchem-942	20	1	[	[	X
eurjchem-942	20	2	12‐14	12‐14	X
eurjchem-942	20	3	]	]	PUNCT
eurjchem-942	20	4	,	,	PUNCT
eurjchem-942	20	5	potentiometry	potentiometry	NOUN
eurjchem-942	20	6	[	[	X
eurjchem-942	20	7	15	15	NUM
eurjchem-942	20	8	]	]	PUNCT
eurjchem-942	20	9	,	,	PUNCT
eurjchem-942	20	10	voltametry	voltametry	NOUN
eurjchem-942	21	1	[	[	X
eurjchem-942	21	2	16	16	NUM
eurjchem-942	21	3	]	]	PUNCT
eurjchem-942	21	4	,	,	PUNCT
eurjchem-942	21	5	capillary	capillary	ADJ
eurjchem-942	21	6	electrophoresis	electrophoresis	NOUN
eurjchem-942	21	7	[	[	X
eurjchem-942	21	8	17	17	NUM
eurjchem-942	21	9	]	]	PUNCT
eurjchem-942	21	10	,	,	PUNCT
eurjchem-942	21	11	spectrofluori‐	spectrofluori‐	SCONJ
eurjchem-942	21	12	metry	metry	NOUN
eurjchem-942	22	1	[	[	X
eurjchem-942	22	2	18	18	NUM
eurjchem-942	22	3	]	]	PUNCT
eurjchem-942	22	4	,	,	PUNCT
eurjchem-942	22	5	uv	uv	NOUN
eurjchem-942	22	6	[	[	X
eurjchem-942	22	7	19	19	NUM
eurjchem-942	22	8	]	]	PUNCT
eurjchem-942	22	9	and	and	CCONJ
eurjchem-942	22	10	visible	visible	ADJ
eurjchem-942	22	11	spectrophotometry	spectrophotometry	NOUN
eurjchem-942	22	12	[	[	X
eurjchem-942	22	13	20	20	NUM
eurjchem-942	22	14	]	]	PUNCT
eurjchem-942	22	15	.	.	PUNCT
eurjchem-942	23	1	finasteride	finasteride	ADJ
eurjchem-942	23	2	(	(	PUNCT
eurjchem-942	23	3	fin	fin	NOUN
eurjchem-942	23	4	)	)	PUNCT
eurjchem-942	23	5	,	,	PUNCT
eurjchem-942	23	6	n‐(1,1‐dimethylethyl)‐3‐oxo‐(5α,17β)‐4‐	n‐(1,1‐dimethylethyl)‐3‐oxo‐(5α,17β)‐4‐	NOUN
eurjchem-942	23	7	azaandrost‐1‐ene‐17‐carboxamide	azaandrost‐1‐ene‐17‐carboxamide	ADJ
eurjchem-942	23	8	(	(	PUNCT
eurjchem-942	23	9	figure	figure	NOUN
eurjchem-942	23	10	1	1	NUM
eurjchem-942	23	11	)	)	PUNCT
eurjchem-942	23	12	,	,	PUNCT
eurjchem-942	23	13	is	be	AUX
eurjchem-942	23	14	a	a	DET
eurjchem-942	23	15	synthetic	synthetic	ADJ
eurjchem-942	23	16	antiandrogen	antiandrogen	NOUN
eurjchem-942	23	17	which	which	PRON
eurjchem-942	23	18	acts	act	VERB
eurjchem-942	23	19	by	by	ADP
eurjchem-942	23	20	inhibiting	inhibit	VERB
eurjchem-942	23	21	type	type	NOUN
eurjchem-942	23	22	ii	ii	PROPN
eurjchem-942	23	23	5‐α	5‐α	NUM
eurjchem-942	23	24	reductase	reductase	NOUN
eurjchem-942	23	25	,	,	PUNCT
eurjchem-942	23	26	the	the	DET
eurjchem-942	23	27	enzyme	enzyme	NOUN
eurjchem-942	23	28	that	that	PRON
eurjchem-942	23	29	converts	convert	VERB
eurjchem-942	23	30	testosterone	testosterone	NOUN
eurjchem-942	23	31	to	to	ADP
eurjchem-942	23	32	dihydrotestosterone	dihydrotestosterone	NOUN
eurjchem-942	23	33	(	(	PUNCT
eurjchem-942	23	34	dht	dht	NOUN
eurjchem-942	23	35	)	)	PUNCT
eurjchem-942	23	36	.	.	PUNCT
eurjchem-942	24	1	it	it	PRON
eurjchem-942	24	2	is	be	AUX
eurjchem-942	24	3	used	use	VERB
eurjchem-942	24	4	as	as	ADP
eurjchem-942	24	5	a	a	DET
eurjchem-942	24	6	treatment	treatment	NOUN
eurjchem-942	24	7	in	in	ADP
eurjchem-942	24	8	benign	benign	ADJ
eurjchem-942	24	9	prostatic	prostatic	ADJ
eurjchem-942	24	10	hyperplasia	hyperplasia	NOUN
eurjchem-942	24	11	in	in	ADP
eurjchem-942	24	12	low	low	ADJ
eurjchem-942	24	13	doses	dose	NOUN
eurjchem-942	24	14	,	,	PUNCT
eurjchem-942	24	15	and	and	CCONJ
eurjchem-942	24	16	prostate	prostate	NOUN
eurjchem-942	24	17	cancer	cancer	NOUN
eurjchem-942	24	18	in	in	ADP
eurjchem-942	24	19	higher	high	ADJ
eurjchem-942	24	20	doses	dose	NOUN
eurjchem-942	24	21	.	.	PUNCT
eurjchem-942	25	1	it	it	PRON
eurjchem-942	25	2	is	be	AUX
eurjchem-942	25	3	also	also	ADV
eurjchem-942	25	4	used	use	VERB
eurjchem-942	25	5	for	for	ADP
eurjchem-942	25	6	treatment	treatment	NOUN
eurjchem-942	25	7	of	of	ADP
eurjchem-942	25	8	male‐pattern	male‐pattern	ADJ
eurjchem-942	25	9	baldness	baldness	NOUN
eurjchem-942	25	10	in	in	ADP
eurjchem-942	25	11	men	man	NOUN
eurjchem-942	25	12	at	at	ADP
eurjchem-942	25	13	a	a	DET
eurjchem-942	25	14	dose	dose	NOUN
eurjchem-942	25	15	of	of	ADP
eurjchem-942	25	16	1	1	NUM
eurjchem-942	25	17	mg	mg	NOUN
eurjchem-942	25	18	daily	daily	ADV
eurjchem-942	25	19	[	[	X
eurjchem-942	25	20	21	21	NUM
eurjchem-942	25	21	]	]	PUNCT
eurjchem-942	25	22	.	.	PUNCT
eurjchem-942	26	1	in	in	ADP
eurjchem-942	26	2	addition	addition	NOUN
eurjchem-942	26	3	to	to	ADP
eurjchem-942	26	4	the	the	DET
eurjchem-942	26	5	hplc	hplc	NOUN
eurjchem-942	26	6	method	method	NOUN
eurjchem-942	26	7	described	describe	VERB
eurjchem-942	26	8	by	by	ADP
eurjchem-942	26	9	the	the	DET
eurjchem-942	26	10	usp	usp	PROPN
eurjchem-942	26	11	[	[	X
eurjchem-942	26	12	5	5	NUM
eurjchem-942	26	13	]	]	PUNCT
eurjchem-942	26	14	,	,	PUNCT
eurjchem-942	26	15	several	several	ADJ
eurjchem-942	26	16	methods	method	NOUN
eurjchem-942	26	17	for	for	ADP
eurjchem-942	26	18	determination	determination	NOUN
eurjchem-942	26	19	of	of	ADP
eurjchem-942	26	20	fin	fin	NOUN
eurjchem-942	26	21	in	in	ADP
eurjchem-942	26	22	bulk	bulk	NOUN
eurjchem-942	26	23	,	,	PUNCT
eurjchem-942	26	24	pharmaceutical	pharmaceutical	NOUN
eurjchem-942	26	25	formulations	formulation	NOUN
eurjchem-942	26	26	and	and	CCONJ
eurjchem-942	26	27	biological	biological	ADJ
eurjchem-942	26	28	samples	sample	NOUN
eurjchem-942	26	29	have	have	AUX
eurjchem-942	26	30	been	be	AUX
eurjchem-942	26	31	developed	develop	VERB
eurjchem-942	26	32	.	.	PUNCT
eurjchem-942	27	1	these	these	DET
eurjchem-942	27	2	methods	method	NOUN
eurjchem-942	27	3	include	include	VERB
eurjchem-942	27	4	hplc	hplc	NOUN
eurjchem-942	27	5	[	[	X
eurjchem-942	27	6	22	22	NUM
eurjchem-942	27	7	]	]	PUNCT
eurjchem-942	27	8	,	,	PUNCT
eurjchem-942	27	9	polarography	polarography	NOUN
eurjchem-942	27	10	[	[	X
eurjchem-942	27	11	23	23	NUM
eurjchem-942	27	12	]	]	PUNCT
eurjchem-942	27	13	and	and	CCONJ
eurjchem-942	27	14	lc‐ms	lc‐ms	X
eurjchem-942	28	1	[	[	X
eurjchem-942	28	2	24,25	24,25	NUM
eurjchem-942	28	3	]	]	PUNCT
eurjchem-942	28	4	.	.	PUNCT
eurjchem-942	29	1	there	there	PRON
eurjchem-942	29	2	are	be	VERB
eurjchem-942	29	3	few	few	ADJ
eurjchem-942	29	4	published	publish	VERB
eurjchem-942	29	5	methods	method	NOUN
eurjchem-942	29	6	for	for	ADP
eurjchem-942	29	7	the	the	DET
eurjchem-942	29	8	high	high	ADJ
eurjchem-942	29	9	throughput	throughput	NOUN
eurjchem-942	29	10	determination	determination	NOUN
eurjchem-942	29	11	of	of	ADP
eurjchem-942	29	12	tam	tam	NOUN
eurjchem-942	29	13	and	and	CCONJ
eurjchem-942	29	14	fin	fin	NOUN
eurjchem-942	29	15	in	in	ADP
eurjchem-942	29	16	bulk	bulk	NOUN
eurjchem-942	29	17	and	and	CCONJ
eurjchem-942	29	18	combined	combine	VERB
eurjchem-942	29	19	dosage	dosage	NOUN
eurjchem-942	29	20	forms	form	NOUN
eurjchem-942	29	21	previously	previously	ADV
eurjchem-942	29	22	reported	report	VERB
eurjchem-942	29	23	using	use	VERB
eurjchem-942	29	24	hplc	hplc	NOUN
eurjchem-942	29	25	and	and	CCONJ
eurjchem-942	29	26	tlc	tlc	NOUN
eurjchem-942	29	27	methods	method	NOUN
eurjchem-942	29	28	[	[	X
eurjchem-942	29	29	26,27	26,27	NUM
eurjchem-942	29	30	]	]	PUNCT
eurjchem-942	29	31	.	.	PUNCT
eurjchem-942	30	1	the	the	DET
eurjchem-942	30	2	lack	lack	NOUN
eurjchem-942	30	3	of	of	ADP
eurjchem-942	30	4	lc‐ms	lc‐ms	AUX
eurjchem-942	30	5	/	/	SYM
eurjchem-942	30	6	ms	ms	NOUN
eurjchem-942	30	7	methods	method	NOUN
eurjchem-942	30	8	for	for	ADP
eurjchem-942	30	9	the	the	DET
eurjchem-942	30	10	simultaneous	simultaneous	ADJ
eurjchem-942	30	11	analysis	analysis	NOUN
eurjchem-942	30	12	of	of	ADP
eurjchem-942	30	13	both	both	DET
eurjchem-942	30	14	tam	tam	NOUN
eurjchem-942	30	15	and	and	CCONJ
eurjchem-942	30	16	fin	fin	NOUN
eurjchem-942	30	17	has	have	AUX
eurjchem-942	30	18	motivated	motivate	VERB
eurjchem-942	30	19	us	we	PRON
eurjchem-942	30	20	to	to	PART
eurjchem-942	30	21	develop	develop	VERB
eurjchem-942	30	22	a	a	DET
eurjchem-942	30	23	simple	simple	ADJ
eurjchem-942	30	24	,	,	PUNCT
eurjchem-942	30	25	sensitive	sensitive	ADJ
eurjchem-942	30	26	and	and	CCONJ
eurjchem-942	30	27	validated	validated	ADJ
eurjchem-942	30	28	lc‐ms	lc‐ms	AUX
eurjchem-942	30	29	/	/	SYM
eurjchem-942	30	30	ms	ms	PROPN
eurjchem-942	30	31	method	method	NOUN
eurjchem-942	30	32	for	for	ADP
eurjchem-942	30	33	their	their	PRON
eurjchem-942	30	34	determination	determination	NOUN
eurjchem-942	30	35	.	.	PUNCT
eurjchem-942	31	1	for	for	ADP
eurjchem-942	31	2	best	good	ADJ
eurjchem-942	31	3	detection	detection	NOUN
eurjchem-942	31	4	up	up	ADP
eurjchem-942	31	5	to	to	ADP
eurjchem-942	31	6	nano‐gram	nano‐gram	NOUN
eurjchem-942	31	7	level	level	NOUN
eurjchem-942	31	8	of	of	ADP
eurjchem-942	31	9	tam	tam	NOUN
eurjchem-942	31	10	and	and	CCONJ
eurjchem-942	31	11	fin	fin	NOUN
eurjchem-942	31	12	;	;	PUNCT
eurjchem-942	31	13	the	the	DET
eurjchem-942	31	14	chromatographic	chromatographic	ADJ
eurjchem-942	31	15	conditions	condition	NOUN
eurjchem-942	31	16	and	and	CCONJ
eurjchem-942	31	17	the	the	DET
eurjchem-942	31	18	mass	mass	ADJ
eurjchem-942	31	19	spectrometric	spectrometric	ADJ
eurjchem-942	31	20	parameters	parameter	NOUN
eurjchem-942	31	21	were	be	AUX
eurjchem-942	31	22	thoroughly	thoroughly	ADV
eurjchem-942	31	23	studied	study	VERB
eurjchem-942	31	24	and	and	CCONJ
eurjchem-942	31	25	adjusted	adjust	VERB
eurjchem-942	31	26	.	.	PUNCT
eurjchem-942	32	1	the	the	DET
eurjchem-942	32	2	method	method	NOUN
eurjchem-942	32	3	was	be	AUX
eurjchem-942	32	4	subsequently	subsequently	ADV
eurjchem-942	32	5	used	use	VERB
eurjchem-942	32	6	to	to	PART
eurjchem-942	32	7	determine	determine	VERB
eurjchem-942	32	8	the	the	DET
eurjchem-942	32	9	concentration	concentration	NOUN
eurjchem-942	32	10	of	of	ADP
eurjchem-942	32	11	the	the	DET
eurjchem-942	32	12	drugs	drug	NOUN
eurjchem-942	32	13	in	in	ADP
eurjchem-942	32	14	laboratory	laboratory	NOUN
eurjchem-942	32	15	prepared	prepare	VERB
eurjchem-942	32	16	mixtures	mixture	NOUN
eurjchem-942	32	17	as	as	ADV
eurjchem-942	32	18	well	well	ADV
eurjchem-942	32	19	as	as	ADP
eurjchem-942	32	20	in	in	ADP
eurjchem-942	32	21	combined	combined	ADJ
eurjchem-942	32	22	dosage	dosage	NOUN
eurjchem-942	32	23	forms	form	NOUN
eurjchem-942	32	24	.	.	PUNCT
eurjchem-942	33	1	our	our	PRON
eurjchem-942	33	2	experimental	experimental	ADJ
eurjchem-942	33	3	results	result	NOUN
eurjchem-942	33	4	were	be	AUX
eurjchem-942	33	5	statistically	statistically	ADV
eurjchem-942	33	6	analyzed	analyze	VERB
eurjchem-942	33	7	and	and	CCONJ
eurjchem-942	33	8	compared	compare	VERB
eurjchem-942	33	9	with	with	ADP
eurjchem-942	33	10	those	those	PRON
eurjchem-942	33	11	of	of	ADP
eurjchem-942	33	12	reference	reference	NOUN
eurjchem-942	33	13	ones	one	NOUN
eurjchem-942	33	14	.	.	PUNCT
eurjchem-942	34	1	2	2	X
eurjchem-942	34	2	.	.	X
eurjchem-942	34	3	experimental	experimental	ADJ
eurjchem-942	34	4	2.1	2.1	NUM
eurjchem-942	34	5	.	.	PUNCT
eurjchem-942	35	1	materials	material	NOUN
eurjchem-942	35	2	and	and	CCONJ
eurjchem-942	35	3	reagents	reagent	NOUN
eurjchem-942	35	4	tamsulosin	tamsulosin	NOUN
eurjchem-942	35	5	hcl	hcl	PROPN
eurjchem-942	35	6	was	be	AUX
eurjchem-942	35	7	kindly	kindly	ADV
eurjchem-942	35	8	supplied	supply	VERB
eurjchem-942	35	9	from	from	ADP
eurjchem-942	35	10	osmopharm	osmopharm	PROPN
eurjchem-942	35	11	s.	s.	PROPN
eurjchem-942	35	12	a.	a.	PROPN
eurjchem-942	35	13	,	,	PUNCT
eurjchem-942	35	14	bedano	bedano	PROPN
eurjchem-942	35	15	,	,	PUNCT
eurjchem-942	35	16	switzerland	switzerland	PROPN
eurjchem-942	35	17	,	,	PUNCT
eurjchem-942	35	18	while	while	SCONJ
eurjchem-942	35	19	,	,	PUNCT
eurjchem-942	35	20	finasteride	finasteride	ADJ
eurjchem-942	35	21	and	and	CCONJ
eurjchem-942	35	22	diphenhydramine	diphenhydramine	PROPN
eurjchem-942	35	23	182	182	NUM
eurjchem-942	35	24	mohamed	mohamed	PROPN
eurjchem-942	35	25	et	et	PROPN
eurjchem-942	35	26	al	al	PROPN
eurjchem-942	35	27	.	.	PUNCT
eurjchem-942	35	28	/	/	SYM
eurjchem-942	35	29	european	european	PROPN
eurjchem-942	35	30	journal	journal	PROPN
eurjchem-942	35	31	of	of	ADP
eurjchem-942	35	32	chemistry	chemistry	NOUN
eurjchem-942	35	33	5	5	NUM
eurjchem-942	35	34	(	(	PUNCT
eurjchem-942	35	35	1	1	NUM
eurjchem-942	35	36	)	)	PUNCT
eurjchem-942	35	37	(	(	PUNCT
eurjchem-942	35	38	2014	2014	NUM
eurjchem-942	35	39	)	)	PUNCT
eurjchem-942	35	40	181‐185	181‐185	NUM
eurjchem-942	35	41	table	table	NOUN
eurjchem-942	35	42	1	1	NUM
eurjchem-942	35	43	.	.	PUNCT
eurjchem-942	36	1	tandem	tandem	PROPN
eurjchem-942	36	2	mass	mass	PROPN
eurjchem-942	36	3	spectrometric	spectrometric	ADJ
eurjchem-942	36	4	parameters	parameter	NOUN
eurjchem-942	36	5	of	of	ADP
eurjchem-942	36	6	tamsulosin	tamsulosin	NOUN
eurjchem-942	36	7	,	,	PUNCT
eurjchem-942	36	8	finasteride	finasteride	ADJ
eurjchem-942	36	9	and	and	CCONJ
eurjchem-942	36	10	diphenhydramine	diphenhydramine	PROPN
eurjchem-942	36	11	.	.	PUNCT
eurjchem-942	37	1	parameter	parameter	PROPN
eurjchem-942	37	2	value	value	NOUN
eurjchem-942	37	3	turbo	turbo	NOUN
eurjchem-942	37	4	ion	ion	NOUN
eurjchem-942	37	5	spray	spray	NOUN
eurjchem-942	37	6	temperature	temperature	NOUN
eurjchem-942	37	7	(	(	PUNCT
eurjchem-942	37	8	°	°	ADP
eurjchem-942	37	9	c	c	NOUN
eurjchem-942	37	10	)	)	PUNCT
eurjchem-942	37	11	400	400	NUM
eurjchem-942	37	12	capillary	capillary	ADJ
eurjchem-942	37	13	temperature	temperature	NOUN
eurjchem-942	37	14	(	(	PUNCT
eurjchem-942	37	15	°	°	ADP
eurjchem-942	37	16	c	c	NOUN
eurjchem-942	37	17	)	)	PUNCT
eurjchem-942	37	18	270	270	NUM
eurjchem-942	37	19	sheath	sheath	NOUN
eurjchem-942	37	20	gas	gas	NOUN
eurjchem-942	37	21	(	(	PUNCT
eurjchem-942	37	22	psi	psi	NOUN
eurjchem-942	37	23	)	)	PUNCT
eurjchem-942	37	24	20	20	NUM
eurjchem-942	37	25	auxillary	auxillary	PROPN
eurjchem-942	37	26	gas	gas	NOUN
eurjchem-942	37	27	(	(	PUNCT
eurjchem-942	37	28	psi	psi	NOUN
eurjchem-942	37	29	)	)	PUNCT
eurjchem-942	37	30	2	2	NUM
eurjchem-942	37	31	ion	ion	NOUN
eurjchem-942	37	32	spray	spray	NOUN
eurjchem-942	37	33	voltage	voltage	NOUN
eurjchem-942	37	34	(	(	PUNCT
eurjchem-942	37	35	v	v	NOUN
eurjchem-942	37	36	)	)	PUNCT
eurjchem-942	37	37	3600	3600	NUM
eurjchem-942	37	38	capillary	capillary	ADJ
eurjchem-942	37	39	offset	offset	NOUN
eurjchem-942	37	40	35	35	NUM
eurjchem-942	37	41	tamsulosin	tamsulosin	NOUN
eurjchem-942	37	42	finasteride	finasteride	ADJ
eurjchem-942	37	43	diphenhydramine	diphenhydramine	NOUN
eurjchem-942	37	44	(	(	PUNCT
eurjchem-942	37	45	is	be	AUX
eurjchem-942	37	46	)	)	PUNCT
eurjchem-942	37	47	collision	collision	NOUN
eurjchem-942	37	48	energy	energy	NOUN
eurjchem-942	37	49	(	(	PUNCT
eurjchem-942	37	50	v	v	NOUN
eurjchem-942	37	51	)	)	PUNCT
eurjchem-942	37	52	23	23	NUM
eurjchem-942	37	53	27	27	NUM
eurjchem-942	37	54	25	25	NUM
eurjchem-942	37	55	srm	srm	NOUN
eurjchem-942	37	56	transition	transition	NOUN
eurjchem-942	37	57	(	(	PUNCT
eurjchem-942	37	58	m	m	NOUN
eurjchem-942	37	59	/	/	SYM
eurjchem-942	37	60	z	z	NOUN
eurjchem-942	37	61	)	)	PUNCT
eurjchem-942	37	62	408.74	408.74	NUM
eurjchem-942	37	63	/	/	SYM
eurjchem-942	37	64	227.29	227.29	NUM
eurjchem-942	37	65	373.11	373.11	NUM
eurjchem-942	37	66	/	/	SYM
eurjchem-942	37	67	304.96	304.96	NUM
eurjchem-942	37	68	255.75	255.75	NUM
eurjchem-942	37	69	/	/	SYM
eurjchem-942	37	70	166.15	166.15	NUM
eurjchem-942	37	71	(	(	PUNCT
eurjchem-942	37	72	a	a	NOUN
eurjchem-942	37	73	)	)	PUNCT
eurjchem-942	38	1	n	n	NOUN
eurjchem-942	38	2	h	h	NOUN
eurjchem-942	39	1	o	o	X
eurjchem-942	39	2	nh	nh	INTJ
eurjchem-942	39	3	o	o	NOUN
eurjchem-942	40	1	h	h	NOUN
eurjchem-942	40	2	h	h	NOUN
eurjchem-942	40	3	h	h	NOUN
eurjchem-942	40	4	h	h	NOUN
eurjchem-942	40	5	(	(	PUNCT
eurjchem-942	40	6	b	b	NOUN
eurjchem-942	40	7	)	)	PUNCT
eurjchem-942	40	8	(	(	PUNCT
eurjchem-942	40	9	c	c	X
eurjchem-942	40	10	)	)	PUNCT
eurjchem-942	40	11	figure	figure	NOUN
eurjchem-942	40	12	1	1	NUM
eurjchem-942	40	13	.	.	PUNCT
eurjchem-942	41	1	chemical	chemical	NOUN
eurjchem-942	41	2	structures	structure	NOUN
eurjchem-942	41	3	of	of	ADP
eurjchem-942	41	4	tamsulosin	tamsulosin	NOUN
eurjchem-942	41	5	(	(	PUNCT
eurjchem-942	41	6	a	a	NOUN
eurjchem-942	41	7	)	)	PUNCT
eurjchem-942	41	8	,	,	PUNCT
eurjchem-942	41	9	finasteride	finasteride	ADJ
eurjchem-942	41	10	(	(	PUNCT
eurjchem-942	41	11	b	b	NOUN
eurjchem-942	41	12	)	)	PUNCT
eurjchem-942	41	13	and	and	CCONJ
eurjchem-942	41	14	diphenhydramine	diphenhydramine	NOUN
eurjchem-942	41	15	as	as	SCONJ
eurjchem-942	41	16	is	be	AUX
eurjchem-942	41	17	(	(	PUNCT
eurjchem-942	41	18	c	c	NOUN
eurjchem-942	41	19	)	)	PUNCT
eurjchem-942	41	20	.	.	PUNCT
eurjchem-942	42	1	(	(	PUNCT
eurjchem-942	42	2	is	be	AUX
eurjchem-942	42	3	)	)	PUNCT
eurjchem-942	42	4	were	be	AUX
eurjchem-942	42	5	purchased	purchase	VERB
eurjchem-942	42	6	from	from	ADP
eurjchem-942	42	7	sigma	sigma	PROPN
eurjchem-942	42	8	pharmaceutical	pharmaceutical	NOUN
eurjchem-942	42	9	industries	industry	NOUN
eurjchem-942	42	10	,	,	PUNCT
eurjchem-942	42	11	steinheim	steinheim	PROPN
eurjchem-942	42	12	,	,	PUNCT
eurjchem-942	42	13	germany	germany	PROPN
eurjchem-942	42	14	.	.	PUNCT
eurjchem-942	43	1	their	their	PRON
eurjchem-942	43	2	purities	purity	NOUN
eurjchem-942	43	3	were	be	AUX
eurjchem-942	43	4	certified	certify	VERB
eurjchem-942	43	5	and	and	CCONJ
eurjchem-942	43	6	analyzed	analyze	VERB
eurjchem-942	43	7	by	by	ADP
eurjchem-942	43	8	reference	reference	NOUN
eurjchem-942	43	9	methods	method	NOUN
eurjchem-942	43	10	and	and	CCONJ
eurjchem-942	43	11	were	be	AUX
eurjchem-942	43	12	found	find	VERB
eurjchem-942	43	13	to	to	PART
eurjchem-942	43	14	be	be	AUX
eurjchem-942	43	15	99.54	99.54	NUM
eurjchem-942	43	16	%	%	NOUN
eurjchem-942	43	17	for	for	ADP
eurjchem-942	43	18	tam	tam	NOUN
eurjchem-942	44	1	[	[	X
eurjchem-942	44	2	26	26	NUM
eurjchem-942	44	3	]	]	PUNCT
eurjchem-942	44	4	and	and	CCONJ
eurjchem-942	44	5	99.86	99.86	NUM
eurjchem-942	44	6	%	%	NOUN
eurjchem-942	44	7	for	for	ADP
eurjchem-942	44	8	fin	fin	NOUN
eurjchem-942	45	1	[	[	X
eurjchem-942	45	2	5	5	NUM
eurjchem-942	45	3	]	]	PUNCT
eurjchem-942	45	4	.	.	PUNCT
eurjchem-942	46	1	they	they	PRON
eurjchem-942	46	2	were	be	AUX
eurjchem-942	46	3	used	use	VERB
eurjchem-942	46	4	as	as	ADP
eurjchem-942	46	5	provided	provide	VERB
eurjchem-942	46	6	.	.	PUNCT
eurjchem-942	47	1	urimax	urimax	PROPN
eurjchem-942	47	2	f	f	PROPN
eurjchem-942	47	3	tablets	tablet	NOUN
eurjchem-942	47	4	(	(	PUNCT
eurjchem-942	47	5	0.4	0.4	NUM
eurjchem-942	47	6	mg	mg	PROPN
eurjchem-942	47	7	tam	tam	PROPN
eurjchem-942	47	8	+	+	CCONJ
eurjchem-942	47	9	5	5	NUM
eurjchem-942	47	10	mg	mg	PROPN
eurjchem-942	47	11	fin	fin	NOUN
eurjchem-942	47	12	)	)	PUNCT
eurjchem-942	47	13	cipla	cipla	PROPN
eurjchem-942	47	14	pharmaceutical	pharmaceutical	PROPN
eurjchem-942	47	15	ltd	ltd	PROPN
eurjchem-942	47	16	.	.	PROPN
eurjchem-942	47	17	,	,	PUNCT
eurjchem-942	47	18	mumbai	mumbai	PROPN
eurjchem-942	47	19	,	,	PUNCT
eurjchem-942	47	20	india	india	PROPN
eurjchem-942	47	21	.	.	PUNCT
eurjchem-942	48	1	all	all	DET
eurjchem-942	48	2	solvents	solvent	NOUN
eurjchem-942	48	3	and	and	CCONJ
eurjchem-942	48	4	materials	material	NOUN
eurjchem-942	48	5	were	be	AUX
eurjchem-942	48	6	of	of	ADP
eurjchem-942	48	7	hplc	hplc	NOUN
eurjchem-942	48	8	grade	grade	NOUN
eurjchem-942	48	9	.	.	PUNCT
eurjchem-942	49	1	methanol	methanol	NOUN
eurjchem-942	49	2	was	be	AUX
eurjchem-942	49	3	purchased	purchase	VERB
eurjchem-942	49	4	from	from	ADP
eurjchem-942	49	5	fischer	fischer	PROPN
eurjchem-942	49	6	scientific	scientific	PROPN
eurjchem-942	49	7	uk	uk	PROPN
eurjchem-942	49	8	ltd	ltd	PROPN
eurjchem-942	49	9	,	,	PUNCT
eurjchem-942	49	10	loughborough	loughborough	PROPN
eurjchem-942	49	11	,	,	PUNCT
eurjchem-942	49	12	uk	uk	PROPN
eurjchem-942	49	13	.	.	PROPN
eurjchem-942	49	14	acetonitrile	acetonitrile	NOUN
eurjchem-942	49	15	and	and	CCONJ
eurjchem-942	49	16	ammonium	ammonium	NOUN
eurjchem-942	49	17	acetate	acetate	NOUN
eurjchem-942	49	18	were	be	AUX
eurjchem-942	49	19	purchased	purchase	VERB
eurjchem-942	49	20	from	from	ADP
eurjchem-942	49	21	merck	merck	PROPN
eurjchem-942	49	22	,	,	PUNCT
eurjchem-942	49	23	darmstadt	darmstadt	PROPN
eurjchem-942	49	24	,	,	PUNCT
eurjchem-942	49	25	germany	germany	PROPN
eurjchem-942	49	26	.	.	PROPN
eurjchem-942	50	1	deionized	deionize	VERB
eurjchem-942	50	2	water	water	NOUN
eurjchem-942	50	3	(	(	PUNCT
eurjchem-942	50	4	purelab	purelab	VERB
eurjchem-942	50	5	flex	flex	ADJ
eurjchem-942	50	6	,	,	PUNCT
eurjchem-942	50	7	elga	elga	NOUN
eurjchem-942	50	8	)	)	PUNCT
eurjchem-942	50	9	was	be	AUX
eurjchem-942	50	10	used	use	VERB
eurjchem-942	50	11	.	.	PUNCT
eurjchem-942	51	1	2.2	2.2	NUM
eurjchem-942	51	2	.	.	PUNCT
eurjchem-942	52	1	instrumentation	instrumentation	NOUN
eurjchem-942	52	2	the	the	DET
eurjchem-942	52	3	analysis	analysis	NOUN
eurjchem-942	52	4	was	be	AUX
eurjchem-942	52	5	performed	perform	VERB
eurjchem-942	52	6	using	use	VERB
eurjchem-942	52	7	a	a	DET
eurjchem-942	52	8	tsq	tsq	NOUN
eurjchem-942	52	9	quantum	quantum	NOUN
eurjchem-942	52	10	access	access	NOUN
eurjchem-942	52	11	max	max	PROPN
eurjchem-942	52	12	triple	triple	ADJ
eurjchem-942	52	13	stage	stage	NOUN
eurjchem-942	52	14	quadrupole	quadrupole	NOUN
eurjchem-942	52	15	mass	mass	PROPN
eurjchem-942	52	16	spectrometer	spectrometer	NOUN
eurjchem-942	52	17	,	,	PUNCT
eurjchem-942	52	18	thermoscientific	thermoscientific	NOUN
eurjchem-942	52	19	,	,	PUNCT
eurjchem-942	52	20	new	new	PROPN
eurjchem-942	52	21	york	york	PROPN
eurjchem-942	52	22	,	,	PUNCT
eurjchem-942	52	23	usa	usa	PROPN
eurjchem-942	52	24	,	,	PUNCT
eurjchem-942	52	25	equipped	equip	VERB
eurjchem-942	52	26	with	with	ADP
eurjchem-942	52	27	an	an	DET
eurjchem-942	52	28	electrospray	electrospray	ADJ
eurjchem-942	52	29	ionization	ionization	NOUN
eurjchem-942	52	30	(	(	PUNCT
eurjchem-942	52	31	esi	esi	NOUN
eurjchem-942	52	32	)	)	PUNCT
eurjchem-942	52	33	source	source	NOUN
eurjchem-942	52	34	.	.	PUNCT
eurjchem-942	53	1	xcalibur	xcalibur	PROPN
eurjchem-942	53	2	software	software	PROPN
eurjchem-942	53	3	version	version	PROPN
eurjchem-942	53	4	2.2	2.2	NUM
eurjchem-942	53	5	was	be	AUX
eurjchem-942	53	6	used	use	VERB
eurjchem-942	53	7	to	to	PART
eurjchem-942	53	8	control	control	VERB
eurjchem-942	53	9	the	the	DET
eurjchem-942	53	10	lc‐ms	lc‐ms	NOUN
eurjchem-942	53	11	/	/	SYM
eurjchem-942	53	12	ms	ms	NOUN
eurjchem-942	53	13	system	system	NOUN
eurjchem-942	53	14	,	,	PUNCT
eurjchem-942	53	15	collect	collect	VERB
eurjchem-942	53	16	and	and	CCONJ
eurjchem-942	53	17	analyse	analyse	VERB
eurjchem-942	53	18	the	the	DET
eurjchem-942	53	19	data	datum	NOUN
eurjchem-942	53	20	.	.	PUNCT
eurjchem-942	54	1	the	the	DET
eurjchem-942	54	2	hplc	hplc	NOUN
eurjchem-942	54	3	system	system	NOUN
eurjchem-942	54	4	consisted	consist	VERB
eurjchem-942	54	5	of	of	ADP
eurjchem-942	54	6	an	an	DET
eurjchem-942	54	7	accela	accela	NOUN
eurjchem-942	54	8	u‐	u‐	ADP
eurjchem-942	54	9	hplc	hplc	NOUN
eurjchem-942	54	10	with	with	ADP
eurjchem-942	54	11	accela	accela	NOUN
eurjchem-942	54	12	1250	1250	NUM
eurjchem-942	54	13	quaternary	quaternary	ADJ
eurjchem-942	54	14	pump	pump	NOUN
eurjchem-942	54	15	and	and	CCONJ
eurjchem-942	54	16	accela	accela	NOUN
eurjchem-942	54	17	open	open	ADJ
eurjchem-942	54	18	autosampler	autosampler	NOUN
eurjchem-942	54	19	,	,	PUNCT
eurjchem-942	54	20	new	new	PROPN
eurjchem-942	54	21	york	york	PROPN
eurjchem-942	54	22	,	,	PUNCT
eurjchem-942	54	23	usa	usa	PROPN
eurjchem-942	54	24	operated	operate	VERB
eurjchem-942	54	25	at	at	ADP
eurjchem-942	54	26	15	15	NUM
eurjchem-942	54	27	°	°	NOUN
eurjchem-942	54	28	c	c	NOUN
eurjchem-942	54	29	.	.	PUNCT
eurjchem-942	55	1	2.3	2.3	NUM
eurjchem-942	55	2	.	.	PUNCT
eurjchem-942	55	3	mass	mass	ADJ
eurjchem-942	55	4	spectrometric	spectrometric	ADJ
eurjchem-942	55	5	conditions	condition	NOUN
eurjchem-942	55	6	the	the	DET
eurjchem-942	55	7	positive‐ion	positive‐ion	NOUN
eurjchem-942	55	8	mass	mass	NOUN
eurjchem-942	55	9	spectrometric	spectrometric	ADJ
eurjchem-942	55	10	detection	detection	NOUN
eurjchem-942	55	11	method	method	NOUN
eurjchem-942	55	12	utilised	utilise	VERB
eurjchem-942	55	13	electrospray	electrospray	VERB
eurjchem-942	55	14	ionization	ionization	NOUN
eurjchem-942	55	15	and	and	CCONJ
eurjchem-942	55	16	single	single	ADJ
eurjchem-942	55	17	reaction	reaction	NOUN
eurjchem-942	55	18	monitoring	monitoring	NOUN
eurjchem-942	55	19	(	(	PUNCT
eurjchem-942	55	20	srm	srm	NOUN
eurjchem-942	55	21	)	)	PUNCT
eurjchem-942	55	22	mode	mode	NOUN
eurjchem-942	55	23	.	.	PUNCT
eurjchem-942	56	1	the	the	DET
eurjchem-942	56	2	optimized	optimize	VERB
eurjchem-942	56	3	parameters	parameter	NOUN
eurjchem-942	56	4	are	be	AUX
eurjchem-942	56	5	summarized	summarize	VERB
eurjchem-942	56	6	in	in	ADP
eurjchem-942	56	7	table	table	NOUN
eurjchem-942	56	8	1	1	NUM
eurjchem-942	56	9	.	.	X
eurjchem-942	56	10	2.4	2.4	NUM
eurjchem-942	56	11	.	.	PUNCT
eurjchem-942	56	12	chromatographic	chromatographic	ADJ
eurjchem-942	56	13	conditions	condition	NOUN
eurjchem-942	56	14	chromatographic	chromatographic	ADJ
eurjchem-942	56	15	separation	separation	NOUN
eurjchem-942	56	16	was	be	AUX
eurjchem-942	56	17	performed	perform	VERB
eurjchem-942	56	18	on	on	ADP
eurjchem-942	56	19	hypersil‐	hypersil‐	X
eurjchem-942	56	20	gold	gold	NOUN
eurjchem-942	56	21	column	column	NOUN
eurjchem-942	56	22	(	(	PUNCT
eurjchem-942	56	23	c18‐bonded	c18‐bonde	VERB
eurjchem-942	56	24	ultrapure	ultrapure	NOUN
eurjchem-942	56	25	silica	silica	NOUN
eurjchem-942	56	26	based	base	VERB
eurjchem-942	56	27	column	column	NOUN
eurjchem-942	56	28	)	)	PUNCT
eurjchem-942	56	29	50	50	NUM
eurjchem-942	56	30	mm	mm	NOUN
eurjchem-942	56	31	×	×	NOUN
eurjchem-942	56	32	2.0	2.0	NUM
eurjchem-942	56	33	mm	mm	NOUN
eurjchem-942	56	34	(	(	PUNCT
eurjchem-942	56	35	1.9	1.9	NUM
eurjchem-942	56	36	μm	μm	NUM
eurjchem-942	56	37	)	)	PUNCT
eurjchem-942	56	38	from	from	ADP
eurjchem-942	56	39	thermoscientific	thermoscientific	NOUN
eurjchem-942	56	40	,	,	PUNCT
eurjchem-942	56	41	new	new	PROPN
eurjchem-942	56	42	york	york	PROPN
eurjchem-942	56	43	,	,	PUNCT
eurjchem-942	56	44	usa	usa	PROPN
eurjchem-942	56	45	.	.	PROPN
eurjchem-942	56	46	elution	elution	NOUN
eurjchem-942	56	47	was	be	AUX
eurjchem-942	56	48	performed	perform	VERB
eurjchem-942	56	49	at	at	ADP
eurjchem-942	56	50	room	room	NOUN
eurjchem-942	56	51	temperature	temperature	NOUN
eurjchem-942	56	52	using	use	VERB
eurjchem-942	56	53	the	the	DET
eurjchem-942	56	54	mobile	mobile	ADJ
eurjchem-942	56	55	phase	phase	NOUN
eurjchem-942	56	56	10	10	NUM
eurjchem-942	56	57	mm	mm	NOUN
eurjchem-942	56	58	ammonium	ammonium	NOUN
eurjchem-942	56	59	acetate	acetate	NOUN
eurjchem-942	56	60	:	:	PUNCT
eurjchem-942	56	61	acetonitrile	acetonitrile	NOUN
eurjchem-942	56	62	(	(	PUNCT
eurjchem-942	56	63	10:90	10:90	NUM
eurjchem-942	56	64	,	,	PUNCT
eurjchem-942	56	65	v	v	NOUN
eurjchem-942	56	66	:	:	SYM
eurjchem-942	56	67	v	v	NOUN
eurjchem-942	56	68	)	)	PUNCT
eurjchem-942	56	69	(	(	PUNCT
eurjchem-942	56	70	ph	ph	NOUN
eurjchem-942	56	71	=	=	NOUN
eurjchem-942	56	72	3.5	3.5	NUM
eurjchem-942	56	73	)	)	PUNCT
eurjchem-942	56	74	.	.	PUNCT
eurjchem-942	57	1	the	the	DET
eurjchem-942	57	2	lc	lc	PROPN
eurjchem-942	57	3	system	system	NOUN
eurjchem-942	57	4	was	be	AUX
eurjchem-942	57	5	operated	operate	VERB
eurjchem-942	57	6	isocratically	isocratically	ADV
eurjchem-942	57	7	at	at	ADP
eurjchem-942	57	8	250	250	NUM
eurjchem-942	57	9	μl	μl	PRON
eurjchem-942	57	10	/	/	SYM
eurjchem-942	57	11	min	min	NOUN
eurjchem-942	57	12	.	.	PUNCT
eurjchem-942	58	1	the	the	DET
eurjchem-942	58	2	injection	injection	NOUN
eurjchem-942	58	3	volume	volume	NOUN
eurjchem-942	58	4	was	be	AUX
eurjchem-942	58	5	10	10	NUM
eurjchem-942	58	6	µl	µl	NOUN
eurjchem-942	58	7	.	.	PUNCT
eurjchem-942	59	1	the	the	DET
eurjchem-942	59	2	total	total	ADJ
eurjchem-942	59	3	run	run	NOUN
eurjchem-942	59	4	time	time	NOUN
eurjchem-942	59	5	for	for	ADP
eurjchem-942	59	6	each	each	DET
eurjchem-942	59	7	sample	sample	NOUN
eurjchem-942	59	8	was	be	AUX
eurjchem-942	59	9	3	3	NUM
eurjchem-942	59	10	min	min	NOUN
eurjchem-942	59	11	.	.	PROPN
eurjchem-942	59	12	2.5	2.5	NUM
eurjchem-942	59	13	.	.	PUNCT
eurjchem-942	60	1	standard	standard	ADJ
eurjchem-942	60	2	solutions	solution	NOUN
eurjchem-942	60	3	stock	stock	NOUN
eurjchem-942	60	4	solutions	solution	NOUN
eurjchem-942	60	5	(	(	PUNCT
eurjchem-942	60	6	0.1	0.1	NUM
eurjchem-942	60	7	mg	mg	PROPN
eurjchem-942	60	8	/	/	SYM
eurjchem-942	60	9	ml	ml	NOUN
eurjchem-942	60	10	)	)	PUNCT
eurjchem-942	60	11	of	of	ADP
eurjchem-942	60	12	tam	tam	PROPN
eurjchem-942	60	13	,	,	PUNCT
eurjchem-942	60	14	fin	fin	NOUN
eurjchem-942	60	15	and	and	CCONJ
eurjchem-942	60	16	is	be	AUX
eurjchem-942	60	17	were	be	AUX
eurjchem-942	60	18	separately	separately	ADV
eurjchem-942	60	19	prepared	prepare	VERB
eurjchem-942	60	20	in	in	ADP
eurjchem-942	60	21	100	100	NUM
eurjchem-942	60	22	ml	ml	NOUN
eurjchem-942	60	23	volumetric	volumetric	ADJ
eurjchem-942	60	24	flasks	flask	NOUN
eurjchem-942	60	25	in	in	ADP
eurjchem-942	60	26	methanol	methanol	NOUN
eurjchem-942	60	27	while	while	SCONJ
eurjchem-942	60	28	the	the	DET
eurjchem-942	60	29	working	work	VERB
eurjchem-942	60	30	standard	standard	ADJ
eurjchem-942	60	31	solutions	solution	NOUN
eurjchem-942	60	32	were	be	AUX
eurjchem-942	60	33	prepared	prepare	VERB
eurjchem-942	60	34	by	by	ADP
eurjchem-942	60	35	further	further	ADJ
eurjchem-942	60	36	dilution	dilution	NOUN
eurjchem-942	60	37	of	of	ADP
eurjchem-942	60	38	the	the	DET
eurjchem-942	60	39	corresponding	correspond	VERB
eurjchem-942	60	40	stock	stock	NOUN
eurjchem-942	60	41	solutions	solution	NOUN
eurjchem-942	60	42	with	with	ADP
eurjchem-942	60	43	methanol	methanol	NOUN
eurjchem-942	60	44	.	.	PUNCT
eurjchem-942	61	1	all	all	DET
eurjchem-942	61	2	stock	stock	NOUN
eurjchem-942	61	3	solutions	solution	NOUN
eurjchem-942	61	4	were	be	AUX
eurjchem-942	61	5	kept	keep	VERB
eurjchem-942	61	6	at	at	ADP
eurjchem-942	61	7	‐20	‐20	PROPN
eurjchem-942	61	8	°	°	ADP
eurjchem-942	61	9	c	c	NOUN
eurjchem-942	61	10	until	until	ADP
eurjchem-942	61	11	use	use	NOUN
eurjchem-942	61	12	,	,	PUNCT
eurjchem-942	61	13	whilst	whilst	SCONJ
eurjchem-942	61	14	the	the	DET
eurjchem-942	61	15	working	work	VERB
eurjchem-942	61	16	solutions	solution	NOUN
eurjchem-942	61	17	were	be	AUX
eurjchem-942	61	18	kept	keep	VERB
eurjchem-942	61	19	at	at	ADP
eurjchem-942	61	20	4	4	NUM
eurjchem-942	61	21	°	°	NOUN
eurjchem-942	61	22	c	c	NOUN
eurjchem-942	61	23	and	and	CCONJ
eurjchem-942	61	24	discarded	discard	VERB
eurjchem-942	61	25	within	within	ADP
eurjchem-942	61	26	30	30	NUM
eurjchem-942	61	27	days	day	NOUN
eurjchem-942	61	28	.	.	PUNCT
eurjchem-942	62	1	2.6	2.6	NUM
eurjchem-942	62	2	.	.	PUNCT
eurjchem-942	62	3	procedures	procedure	NOUN
eurjchem-942	62	4	2.6.1	2.6.1	NUM
eurjchem-942	62	5	.	.	PUNCT
eurjchem-942	63	1	calibration	calibration	NOUN
eurjchem-942	63	2	curves	curve	VERB
eurjchem-942	63	3	six	six	NUM
eurjchem-942	63	4	standard	standard	ADJ
eurjchem-942	63	5	solutions	solution	NOUN
eurjchem-942	63	6	of	of	ADP
eurjchem-942	63	7	each	each	DET
eurjchem-942	63	8	drug	drug	NOUN
eurjchem-942	63	9	were	be	AUX
eurjchem-942	63	10	prepared	prepare	VERB
eurjchem-942	63	11	in	in	ADP
eurjchem-942	63	12	concentration	concentration	NOUN
eurjchem-942	63	13	ranges	range	NOUN
eurjchem-942	63	14	1.6‐40.0	1.6‐40.0	PROPN
eurjchem-942	63	15	ng	ng	PROPN
eurjchem-942	63	16	/	/	SYM
eurjchem-942	63	17	ml	ml	X
eurjchem-942	63	18	for	for	ADP
eurjchem-942	63	19	tam	tam	NOUN
eurjchem-942	63	20	and	and	CCONJ
eurjchem-942	63	21	20.0‐500.0	20.0‐500.0	PROPN
eurjchem-942	63	22	ng	ng	PROPN
eurjchem-942	63	23	/	/	SYM
eurjchem-942	63	24	ml	ml	X
eurjchem-942	63	25	for	for	ADP
eurjchem-942	63	26	fin	fin	NOUN
eurjchem-942	63	27	with	with	ADP
eurjchem-942	63	28	the	the	DET
eurjchem-942	63	29	addition	addition	NOUN
eurjchem-942	63	30	of	of	ADP
eurjchem-942	63	31	40	40	NUM
eurjchem-942	63	32	ng	ng	NOUN
eurjchem-942	63	33	/	/	SYM
eurjchem-942	63	34	ml	ml	X
eurjchem-942	63	35	of	of	ADP
eurjchem-942	63	36	is	be	AUX
eurjchem-942	63	37	on	on	ADP
eurjchem-942	63	38	every	every	DET
eurjchem-942	63	39	standard	standard	ADJ
eurjchem-942	63	40	solution	solution	NOUN
eurjchem-942	63	41	.	.	PUNCT
eurjchem-942	64	1	a	a	DET
eurjchem-942	64	2	10	10	NUM
eurjchem-942	64	3	μl	μl	ADP
eurjchem-942	64	4	aliquot	aliquot	NOUN
eurjchem-942	64	5	of	of	ADP
eurjchem-942	64	6	each	each	DET
eurjchem-942	64	7	solution	solution	NOUN
eurjchem-942	64	8	was	be	AUX
eurjchem-942	64	9	injected	inject	VERB
eurjchem-942	64	10	onto	onto	ADP
eurjchem-942	64	11	the	the	DET
eurjchem-942	64	12	lc‐ms	lc‐ms	NOUN
eurjchem-942	64	13	system	system	NOUN
eurjchem-942	64	14	.	.	PUNCT
eurjchem-942	65	1	two	two	NUM
eurjchem-942	65	2	calibration	calibration	NOUN
eurjchem-942	65	3	curves	curve	NOUN
eurjchem-942	65	4	were	be	AUX
eurjchem-942	65	5	established	establish	VERB
eurjchem-942	65	6	separately	separately	ADV
eurjchem-942	65	7	for	for	ADP
eurjchem-942	65	8	each	each	DET
eurjchem-942	65	9	drug	drug	NOUN
eurjchem-942	65	10	.	.	PUNCT
eurjchem-942	66	1	the	the	DET
eurjchem-942	66	2	calibration	calibration	NOUN
eurjchem-942	66	3	curve	curve	NOUN
eurjchem-942	66	4	was	be	AUX
eurjchem-942	66	5	constructed	construct	VERB
eurjchem-942	66	6	by	by	ADP
eurjchem-942	66	7	plotting	plot	VERB
eurjchem-942	66	8	of	of	ADP
eurjchem-942	66	9	the	the	DET
eurjchem-942	66	10	peak	peak	NOUN
eurjchem-942	66	11	area	area	NOUN
eurjchem-942	66	12	ratios	ratio	NOUN
eurjchem-942	66	13	of	of	ADP
eurjchem-942	66	14	each	each	DET
eurjchem-942	66	15	analyte	analyte	NOUN
eurjchem-942	66	16	to	to	PART
eurjchem-942	66	17	is	be	AUX
eurjchem-942	66	18	obtained	obtain	VERB
eurjchem-942	66	19	against	against	ADP
eurjchem-942	66	20	the	the	DET
eurjchem-942	66	21	corresponding	corresponding	ADJ
eurjchem-942	66	22	concentrations	concentration	NOUN
eurjchem-942	66	23	.	.	PUNCT
eurjchem-942	67	1	2.6.2	2.6.2	X
eurjchem-942	67	2	.	.	X
eurjchem-942	67	3	laboratory	laboratory	NOUN
eurjchem-942	67	4	prepared	prepare	VERB
eurjchem-942	67	5	mixtures	mixture	NOUN
eurjchem-942	67	6	binary	binary	PROPN
eurjchem-942	67	7	laboratory	laboratory	NOUN
eurjchem-942	67	8	prepared	prepare	VERB
eurjchem-942	67	9	mixtures	mixture	NOUN
eurjchem-942	67	10	of	of	ADP
eurjchem-942	67	11	tam	tam	PROPN
eurjchem-942	67	12	and	and	CCONJ
eurjchem-942	67	13	fin	fin	NOUN
eurjchem-942	67	14	were	be	AUX
eurjchem-942	67	15	prepared	prepare	VERB
eurjchem-942	67	16	by	by	ADP
eurjchem-942	67	17	mixing	mix	VERB
eurjchem-942	67	18	their	their	PRON
eurjchem-942	67	19	working	work	VERB
eurjchem-942	67	20	solutions	solution	NOUN
eurjchem-942	67	21	in	in	ADP
eurjchem-942	67	22	different	different	ADJ
eurjchem-942	67	23	ratios	ratio	NOUN
eurjchem-942	67	24	,	,	PUNCT
eurjchem-942	67	25	then	then	ADV
eurjchem-942	67	26	40.0	40.0	NUM
eurjchem-942	67	27	ng	ng	NOUN
eurjchem-942	67	28	/	/	SYM
eurjchem-942	67	29	ml	ml	X
eurjchem-942	67	30	of	of	ADP
eurjchem-942	67	31	is	be	AUX
eurjchem-942	67	32	was	be	AUX
eurjchem-942	67	33	added	add	VERB
eurjchem-942	67	34	.	.	PUNCT
eurjchem-942	68	1	a	a	DET
eurjchem-942	68	2	10	10	NUM
eurjchem-942	68	3	μl	μl	ADP
eurjchem-942	68	4	aliquot	aliquot	NOUN
eurjchem-942	68	5	of	of	ADP
eurjchem-942	68	6	each	each	DET
eurjchem-942	68	7	solution	solution	NOUN
eurjchem-942	68	8	was	be	AUX
eurjchem-942	68	9	injected	inject	VERB
eurjchem-942	68	10	onto	onto	ADP
eurjchem-942	68	11	the	the	DET
eurjchem-942	68	12	lc‐ms	lc‐ms	NOUN
eurjchem-942	68	13	system	system	NOUN
eurjchem-942	68	14	,	,	PUNCT
eurjchem-942	68	15	and	and	CCONJ
eurjchem-942	68	16	the	the	DET
eurjchem-942	68	17	procedure	procedure	NOUN
eurjchem-942	68	18	was	be	AUX
eurjchem-942	68	19	continued	continue	VERB
eurjchem-942	68	20	as	as	SCONJ
eurjchem-942	68	21	stated	state	VERB
eurjchem-942	68	22	under	under	ADP
eurjchem-942	68	23	calibration	calibration	NOUN
eurjchem-942	68	24	curves	curve	NOUN
eurjchem-942	68	25	.	.	PUNCT
eurjchem-942	69	1	2.6.3	2.6.3	NUM
eurjchem-942	69	2	.	.	PUNCT
eurjchem-942	70	1	dosage	dosage	NOUN
eurjchem-942	70	2	form	form	NOUN
eurjchem-942	70	3	for	for	ADP
eurjchem-942	70	4	analysis	analysis	NOUN
eurjchem-942	70	5	of	of	ADP
eurjchem-942	70	6	the	the	DET
eurjchem-942	70	7	pharmaceutical	pharmaceutical	ADJ
eurjchem-942	70	8	dosage	dosage	NOUN
eurjchem-942	70	9	form	form	NOUN
eurjchem-942	70	10	,	,	PUNCT
eurjchem-942	70	11	10	10	NUM
eurjchem-942	70	12	tablets	tablet	NOUN
eurjchem-942	70	13	were	be	AUX
eurjchem-942	70	14	pulverized	pulverize	VERB
eurjchem-942	70	15	well	well	ADV
eurjchem-942	70	16	;	;	PUNCT
eurjchem-942	70	17	an	an	DET
eurjchem-942	70	18	accurate	accurate	ADJ
eurjchem-942	70	19	amount	amount	NOUN
eurjchem-942	70	20	of	of	ADP
eurjchem-942	70	21	the	the	DET
eurjchem-942	70	22	powdered	powdered	ADJ
eurjchem-942	70	23	mohamed	mohamed	PROPN
eurjchem-942	70	24	et	et	PROPN
eurjchem-942	70	25	al	al	PROPN
eurjchem-942	70	26	.	.	PUNCT
eurjchem-942	70	27	/	/	SYM
eurjchem-942	70	28	european	european	PROPN
eurjchem-942	70	29	journal	journal	PROPN
eurjchem-942	70	30	of	of	ADP
eurjchem-942	70	31	chemistry	chemistry	NOUN
eurjchem-942	70	32	5	5	NUM
eurjchem-942	70	33	(	(	PUNCT
eurjchem-942	70	34	1	1	NUM
eurjchem-942	70	35	)	)	PUNCT
eurjchem-942	70	36	(	(	PUNCT
eurjchem-942	70	37	2014	2014	NUM
eurjchem-942	70	38	)	)	PUNCT
eurjchem-942	70	39	181‐185	181‐185	NUM
eurjchem-942	70	40	183	183	NUM
eurjchem-942	70	41	tablets	tablet	NOUN
eurjchem-942	70	42	equivalent	equivalent	ADJ
eurjchem-942	70	43	to	to	ADP
eurjchem-942	70	44	12.5	12.5	NUM
eurjchem-942	70	45	mg	mg	NOUN
eurjchem-942	70	46	of	of	ADP
eurjchem-942	70	47	fin	fin	NOUN
eurjchem-942	70	48	and	and	CCONJ
eurjchem-942	70	49	1.0	1.0	NUM
eurjchem-942	70	50	mg	mg	NOUN
eurjchem-942	70	51	of	of	ADP
eurjchem-942	70	52	tam	tam	PROPN
eurjchem-942	70	53	,	,	PUNCT
eurjchem-942	70	54	was	be	AUX
eurjchem-942	70	55	weighed	weigh	VERB
eurjchem-942	70	56	and	and	CCONJ
eurjchem-942	70	57	transferred	transfer	VERB
eurjchem-942	70	58	into	into	ADP
eurjchem-942	70	59	100	100	NUM
eurjchem-942	70	60	ml	ml	NOUN
eurjchem-942	70	61	volumetric	volumetric	ADJ
eurjchem-942	70	62	flask	flask	NOUN
eurjchem-942	70	63	and	and	CCONJ
eurjchem-942	70	64	dissolved	dissolve	VERB
eurjchem-942	70	65	in	in	ADP
eurjchem-942	70	66	methanol	methanol	NOUN
eurjchem-942	70	67	,	,	PUNCT
eurjchem-942	70	68	then	then	ADV
eurjchem-942	70	69	the	the	DET
eurjchem-942	70	70	procedure	procedure	NOUN
eurjchem-942	70	71	was	be	AUX
eurjchem-942	70	72	continued	continue	VERB
eurjchem-942	70	73	as	as	SCONJ
eurjchem-942	70	74	stated	state	VERB
eurjchem-942	70	75	under	under	ADP
eurjchem-942	70	76	calibration	calibration	NOUN
eurjchem-942	70	77	curves	curve	NOUN
eurjchem-942	70	78	.	.	PUNCT
eurjchem-942	71	1	3	3	X
eurjchem-942	71	2	.	.	NOUN
eurjchem-942	71	3	results	result	NOUN
eurjchem-942	71	4	and	and	CCONJ
eurjchem-942	71	5	discussion	discussion	NOUN
eurjchem-942	71	6	for	for	ADP
eurjchem-942	71	7	optimum	optimum	ADJ
eurjchem-942	71	8	detection	detection	NOUN
eurjchem-942	71	9	up	up	ADP
eurjchem-942	71	10	to	to	ADP
eurjchem-942	71	11	nano‐gram	nano‐gram	NOUN
eurjchem-942	71	12	level	level	NOUN
eurjchem-942	71	13	of	of	ADP
eurjchem-942	71	14	tam	tam	PROPN
eurjchem-942	71	15	,	,	PUNCT
eurjchem-942	71	16	fin	fin	NOUN
eurjchem-942	71	17	and	and	CCONJ
eurjchem-942	71	18	the	the	PRON
eurjchem-942	71	19	is	be	AUX
eurjchem-942	71	20	it	it	PRON
eurjchem-942	71	21	was	be	AUX
eurjchem-942	71	22	necessary	necessary	ADJ
eurjchem-942	71	23	to	to	PART
eurjchem-942	71	24	adjust	adjust	VERB
eurjchem-942	71	25	both	both	CCONJ
eurjchem-942	71	26	the	the	DET
eurjchem-942	71	27	chromatographic	chromatographic	ADJ
eurjchem-942	71	28	conditions	condition	NOUN
eurjchem-942	71	29	and	and	CCONJ
eurjchem-942	71	30	the	the	DET
eurjchem-942	71	31	mass	mass	ADJ
eurjchem-942	71	32	spectrometric	spectrometric	ADJ
eurjchem-942	71	33	parameters	parameter	NOUN
eurjchem-942	71	34	.	.	PUNCT
eurjchem-942	72	1	precursor	precursor	NOUN
eurjchem-942	72	2	ions	ion	NOUN
eurjchem-942	72	3	and	and	CCONJ
eurjchem-942	72	4	product	product	NOUN
eurjchem-942	72	5	ions	ion	NOUN
eurjchem-942	72	6	were	be	AUX
eurjchem-942	72	7	optimized	optimize	VERB
eurjchem-942	72	8	by	by	ADP
eurjchem-942	72	9	infusing	infuse	VERB
eurjchem-942	72	10	1.00	1.00	NUM
eurjchem-942	72	11	µg	µg	NOUN
eurjchem-942	72	12	/	/	SYM
eurjchem-942	72	13	ml	ml	ADV
eurjchem-942	72	14	neat	neat	ADJ
eurjchem-942	72	15	solutions	solution	NOUN
eurjchem-942	72	16	into	into	ADP
eurjchem-942	72	17	mass	mass	ADJ
eurjchem-942	72	18	spectrometer	spectrometer	NOUN
eurjchem-942	72	19	in	in	ADP
eurjchem-942	72	20	about	about	ADP
eurjchem-942	72	21	a	a	DET
eurjchem-942	72	22	100‐500	100‐500	NUM
eurjchem-942	72	23	m	m	NOUN
eurjchem-942	72	24	/	/	SYM
eurjchem-942	72	25	z	z	NOUN
eurjchem-942	72	26	range	range	NOUN
eurjchem-942	72	27	,	,	PUNCT
eurjchem-942	72	28	in	in	ADP
eurjchem-942	72	29	positive	positive	ADJ
eurjchem-942	72	30	polarity	polarity	NOUN
eurjchem-942	72	31	mode	mode	NOUN
eurjchem-942	72	32	using	use	VERB
eurjchem-942	72	33	electrospray	electrospray	ADJ
eurjchem-942	72	34	ionization	ionization	NOUN
eurjchem-942	72	35	technique	technique	NOUN
eurjchem-942	72	36	.	.	PUNCT
eurjchem-942	73	1	best	good	ADJ
eurjchem-942	73	2	intensity	intensity	NOUN
eurjchem-942	73	3	for	for	ADP
eurjchem-942	73	4	precursor	precursor	NOUN
eurjchem-942	73	5	ions	ion	NOUN
eurjchem-942	73	6	and	and	CCONJ
eurjchem-942	73	7	product	product	NOUN
eurjchem-942	73	8	ions	ion	NOUN
eurjchem-942	73	9	was	be	AUX
eurjchem-942	73	10	found	find	VERB
eurjchem-942	73	11	in	in	ADP
eurjchem-942	73	12	the	the	DET
eurjchem-942	73	13	positive	positive	ADJ
eurjchem-942	73	14	mode	mode	NOUN
eurjchem-942	73	15	for	for	ADP
eurjchem-942	73	16	both	both	DET
eurjchem-942	73	17	drugs	drug	NOUN
eurjchem-942	73	18	as	as	SCONJ
eurjchem-942	73	19	they	they	PRON
eurjchem-942	73	20	have	have	VERB
eurjchem-942	73	21	the	the	DET
eurjchem-942	73	22	ability	ability	NOUN
eurjchem-942	73	23	to	to	PART
eurjchem-942	73	24	accept	accept	VERB
eurjchem-942	73	25	protons	proton	NOUN
eurjchem-942	73	26	.	.	PUNCT
eurjchem-942	74	1	the	the	DET
eurjchem-942	74	2	protonated	protonate	VERB
eurjchem-942	74	3	molecular	molecular	ADJ
eurjchem-942	74	4	ions	ion	NOUN
eurjchem-942	74	5	[	[	X
eurjchem-942	74	6	m	m	VERB
eurjchem-942	74	7	+	+	X
eurjchem-942	74	8	h]+	h]+	X
eurjchem-942	74	9	of	of	ADP
eurjchem-942	74	10	tam	tam	PROPN
eurjchem-942	74	11	,	,	PUNCT
eurjchem-942	74	12	fin	fin	NOUN
eurjchem-942	74	13	and	and	CCONJ
eurjchem-942	74	14	is	be	AUX
eurjchem-942	74	15	,	,	PUNCT
eurjchem-942	74	16	observed	observe	VERB
eurjchem-942	74	17	on	on	ADP
eurjchem-942	74	18	the	the	DET
eurjchem-942	74	19	full	full	ADJ
eurjchem-942	74	20	scan	scan	PROPN
eurjchem-942	74	21	mass	mass	PROPN
eurjchem-942	74	22	spectra	spectra	PROPN
eurjchem-942	74	23	,	,	PUNCT
eurjchem-942	74	24	were	be	AUX
eurjchem-942	74	25	408.74	408.74	NUM
eurjchem-942	74	26	,	,	PUNCT
eurjchem-942	74	27	373.11	373.11	NUM
eurjchem-942	74	28	and	and	CCONJ
eurjchem-942	74	29	255.75	255.75	NUM
eurjchem-942	74	30	m	m	PROPN
eurjchem-942	74	31	/	/	SYM
eurjchem-942	74	32	z	z	NOUN
eurjchem-942	74	33	,	,	PUNCT
eurjchem-942	74	34	respectively	respectively	ADV
eurjchem-942	74	35	.	.	PUNCT
eurjchem-942	75	1	moreover	moreover	ADV
eurjchem-942	75	2	,	,	PUNCT
eurjchem-942	75	3	the	the	DET
eurjchem-942	75	4	collision	collision	NOUN
eurjchem-942	75	5	energy	energy	NOUN
eurjchem-942	75	6	in	in	ADP
eurjchem-942	75	7	q2	q2	PROPN
eurjchem-942	75	8	produced	produce	VERB
eurjchem-942	75	9	significant	significant	ADJ
eurjchem-942	75	10	fragments	fragment	NOUN
eurjchem-942	75	11	.	.	PUNCT
eurjchem-942	76	1	the	the	DET
eurjchem-942	76	2	ms	ms	PROPN
eurjchem-942	76	3	/	/	SYM
eurjchem-942	76	4	ms	ms	PROPN
eurjchem-942	76	5	transition	transition	NOUN
eurjchem-942	76	6	408.74	408.74	NUM
eurjchem-942	76	7	→	→	SYM
eurjchem-942	76	8	227.29	227.29	NUM
eurjchem-942	76	9	,	,	PUNCT
eurjchem-942	76	10	373.11	373.11	NUM
eurjchem-942	76	11	→	→	SYM
eurjchem-942	76	12	304.96	304.96	NUM
eurjchem-942	76	13	and	and	CCONJ
eurjchem-942	76	14	255.75	255.75	NUM
eurjchem-942	76	15	→	→	SYM
eurjchem-942	76	16	166.15	166.15	NUM
eurjchem-942	76	17	for	for	ADP
eurjchem-942	76	18	tam	tam	PROPN
eurjchem-942	76	19	,	,	PUNCT
eurjchem-942	76	20	fin	fin	NOUN
eurjchem-942	76	21	and	and	CCONJ
eurjchem-942	76	22	is	be	AUX
eurjchem-942	76	23	,	,	PUNCT
eurjchem-942	76	24	respectively	respectively	ADV
eurjchem-942	76	25	,	,	PUNCT
eurjchem-942	76	26	were	be	AUX
eurjchem-942	76	27	selected	select	VERB
eurjchem-942	76	28	since	since	SCONJ
eurjchem-942	76	29	these	these	DET
eurjchem-942	76	30	products	product	NOUN
eurjchem-942	76	31	ions	ion	NOUN
eurjchem-942	76	32	represented	represent	VERB
eurjchem-942	76	33	the	the	DET
eurjchem-942	76	34	most	most	ADV
eurjchem-942	76	35	abundant	abundant	ADJ
eurjchem-942	76	36	ions	ion	NOUN
eurjchem-942	76	37	by	by	ADP
eurjchem-942	76	38	applying	apply	VERB
eurjchem-942	76	39	sufficient	sufficient	ADJ
eurjchem-942	76	40	collision	collision	NOUN
eurjchem-942	76	41	activated	activate	VERB
eurjchem-942	76	42	dissociation	dissociation	NOUN
eurjchem-942	76	43	gas	gas	NOUN
eurjchem-942	76	44	and	and	CCONJ
eurjchem-942	76	45	collision	collision	NOUN
eurjchem-942	76	46	energy	energy	NOUN
eurjchem-942	76	47	(	(	PUNCT
eurjchem-942	76	48	figure	figure	NOUN
eurjchem-942	76	49	2	2	NUM
eurjchem-942	76	50	)	)	PUNCT
eurjchem-942	76	51	.	.	PUNCT
eurjchem-942	77	1	optimization	optimization	NOUN
eurjchem-942	77	2	of	of	ADP
eurjchem-942	77	3	capillary	capillary	ADJ
eurjchem-942	77	4	temperature	temperature	NOUN
eurjchem-942	77	5	and	and	CCONJ
eurjchem-942	77	6	sheath	sheath	NOUN
eurjchem-942	77	7	gas	gas	NOUN
eurjchem-942	77	8	flow	flow	NOUN
eurjchem-942	77	9	is	be	AUX
eurjchem-942	77	10	important	important	ADJ
eurjchem-942	77	11	as	as	SCONJ
eurjchem-942	77	12	they	they	PRON
eurjchem-942	77	13	play	play	VERB
eurjchem-942	77	14	a	a	DET
eurjchem-942	77	15	great	great	ADJ
eurjchem-942	77	16	role	role	NOUN
eurjchem-942	77	17	in	in	ADP
eurjchem-942	77	18	minimizing	minimize	VERB
eurjchem-942	77	19	ion	ion	NOUN
eurjchem-942	77	20	suppression	suppression	NOUN
eurjchem-942	77	21	and	and	CCONJ
eurjchem-942	77	22	altering	alter	VERB
eurjchem-942	77	23	the	the	DET
eurjchem-942	77	24	sensitivity	sensitivity	NOUN
eurjchem-942	77	25	.	.	PUNCT
eurjchem-942	78	1	adjustment	adjustment	NOUN
eurjchem-942	78	2	of	of	ADP
eurjchem-942	78	3	capillary	capillary	ADJ
eurjchem-942	78	4	temperature	temperature	NOUN
eurjchem-942	78	5	at	at	ADP
eurjchem-942	78	6	270	270	NUM
eurjchem-942	78	7	°	°	NOUN
eurjchem-942	78	8	c	c	NOUN
eurjchem-942	78	9	and	and	CCONJ
eurjchem-942	78	10	sheath	sheath	NOUN
eurjchem-942	78	11	gas	gas	NOUN
eurjchem-942	78	12	at	at	ADP
eurjchem-942	78	13	20	20	NUM
eurjchem-942	78	14	psi	psi	NOUN
eurjchem-942	78	15	,	,	PUNCT
eurjchem-942	78	16	augmented	augment	VERB
eurjchem-942	78	17	the	the	DET
eurjchem-942	78	18	intensity	intensity	NOUN
eurjchem-942	78	19	of	of	ADP
eurjchem-942	78	20	the	the	DET
eurjchem-942	78	21	analytes	analyte	NOUN
eurjchem-942	78	22	.	.	PUNCT
eurjchem-942	79	1	minor	minor	ADJ
eurjchem-942	79	2	changes	change	NOUN
eurjchem-942	79	3	in	in	ADP
eurjchem-942	79	4	ion	ion	NOUN
eurjchem-942	79	5	spray	spray	NOUN
eurjchem-942	79	6	voltage	voltage	NOUN
eurjchem-942	79	7	did	do	AUX
eurjchem-942	79	8	not	not	PART
eurjchem-942	79	9	have	have	VERB
eurjchem-942	79	10	a	a	DET
eurjchem-942	79	11	marked	mark	VERB
eurjchem-942	79	12	effect	effect	NOUN
eurjchem-942	79	13	on	on	ADP
eurjchem-942	79	14	the	the	DET
eurjchem-942	79	15	signal	signal	ADJ
eurjchem-942	79	16	intensity	intensity	NOUN
eurjchem-942	79	17	and	and	CCONJ
eurjchem-942	79	18	was	be	AUX
eurjchem-942	79	19	maintained	maintain	VERB
eurjchem-942	79	20	at	at	ADP
eurjchem-942	79	21	3600	3600	NUM
eurjchem-942	79	22	v.	v.	CCONJ
eurjchem-942	79	23	(	(	PUNCT
eurjchem-942	79	24	a	a	X
eurjchem-942	79	25	)	)	PUNCT
eurjchem-942	79	26	(	(	PUNCT
eurjchem-942	79	27	b	b	X
eurjchem-942	79	28	)	)	PUNCT
eurjchem-942	79	29	(	(	PUNCT
eurjchem-942	79	30	c	c	X
eurjchem-942	79	31	)	)	PUNCT
eurjchem-942	79	32	figure	figure	NOUN
eurjchem-942	79	33	2	2	NUM
eurjchem-942	79	34	.	.	PUNCT
eurjchem-942	79	35	product	product	NOUN
eurjchem-942	79	36	ion	ion	NOUN
eurjchem-942	79	37	spectra	spectra	NOUN
eurjchem-942	79	38	of	of	ADP
eurjchem-942	79	39	[	[	X
eurjchem-942	79	40	m	m	X
eurjchem-942	79	41	+	+	X
eurjchem-942	79	42	h]+	h]+	X
eurjchem-942	79	43	of	of	ADP
eurjchem-942	79	44	tam	tam	X
eurjchem-942	79	45	(	(	PUNCT
eurjchem-942	79	46	a	a	NOUN
eurjchem-942	79	47	)	)	PUNCT
eurjchem-942	79	48	,	,	PUNCT
eurjchem-942	79	49	fin	fin	NOUN
eurjchem-942	79	50	(	(	PUNCT
eurjchem-942	79	51	b	b	NOUN
eurjchem-942	79	52	)	)	PUNCT
eurjchem-942	79	53	and	and	CCONJ
eurjchem-942	79	54	is	be	AUX
eurjchem-942	79	55	(	(	PUNCT
eurjchem-942	79	56	c	c	NOUN
eurjchem-942	79	57	)	)	PUNCT
eurjchem-942	79	58	.	.	PUNCT
eurjchem-942	80	1	to	to	PART
eurjchem-942	80	2	obtain	obtain	VERB
eurjchem-942	80	3	the	the	DET
eurjchem-942	80	4	best	good	ADJ
eurjchem-942	80	5	chromatographic	chromatographic	ADJ
eurjchem-942	80	6	separation	separation	NOUN
eurjchem-942	80	7	with	with	ADP
eurjchem-942	80	8	the	the	DET
eurjchem-942	80	9	desired	desire	VERB
eurjchem-942	80	10	response	response	NOUN
eurjchem-942	80	11	it	it	PRON
eurjchem-942	80	12	was	be	AUX
eurjchem-942	80	13	observed	observe	VERB
eurjchem-942	80	14	that	that	SCONJ
eurjchem-942	80	15	,	,	PUNCT
eurjchem-942	80	16	mobile	mobile	ADJ
eurjchem-942	80	17	phase	phase	NOUN
eurjchem-942	80	18	as	as	ADV
eurjchem-942	80	19	well	well	ADV
eurjchem-942	80	20	as	as	ADP
eurjchem-942	80	21	selection	selection	NOUN
eurjchem-942	80	22	of	of	ADP
eurjchem-942	80	23	column	column	NOUN
eurjchem-942	80	24	is	be	AUX
eurjchem-942	80	25	an	an	DET
eurjchem-942	80	26	important	important	ADJ
eurjchem-942	80	27	criterion	criterion	NOUN
eurjchem-942	80	28	.	.	PUNCT
eurjchem-942	81	1	chromatographic	chromatographic	ADJ
eurjchem-942	81	2	analysis	analysis	NOUN
eurjchem-942	81	3	of	of	ADP
eurjchem-942	81	4	the	the	DET
eurjchem-942	81	5	drugs	drug	NOUN
eurjchem-942	81	6	and	and	CCONJ
eurjchem-942	81	7	is	be	AUX
eurjchem-942	81	8	was	be	AUX
eurjchem-942	81	9	initiated	initiate	VERB
eurjchem-942	81	10	under	under	ADP
eurjchem-942	81	11	isocratic	isocratic	ADJ
eurjchem-942	81	12	conditions	condition	NOUN
eurjchem-942	81	13	with	with	ADP
eurjchem-942	81	14	the	the	DET
eurjchem-942	81	15	aim	aim	NOUN
eurjchem-942	81	16	to	to	PART
eurjchem-942	81	17	develop	develop	VERB
eurjchem-942	81	18	a	a	DET
eurjchem-942	81	19	simple	simple	ADJ
eurjchem-942	81	20	separation	separation	NOUN
eurjchem-942	81	21	process	process	NOUN
eurjchem-942	81	22	with	with	ADP
eurjchem-942	81	23	a	a	DET
eurjchem-942	81	24	short	short	ADJ
eurjchem-942	81	25	run	run	NOUN
eurjchem-942	81	26	time	time	NOUN
eurjchem-942	81	27	.	.	PUNCT
eurjchem-942	82	1	separation	separation	NOUN
eurjchem-942	82	2	was	be	AUX
eurjchem-942	82	3	tried	try	VERB
eurjchem-942	82	4	using	use	VERB
eurjchem-942	82	5	various	various	ADJ
eurjchem-942	82	6	combination	combination	NOUN
eurjchem-942	82	7	of	of	ADP
eurjchem-942	82	8	acetonitrile	acetonitrile	NOUN
eurjchem-942	82	9	and	and	CCONJ
eurjchem-942	82	10	buffer	buffer	VERB
eurjchem-942	82	11	solution	solution	NOUN
eurjchem-942	82	12	with	with	ADP
eurjchem-942	82	13	varying	vary	VERB
eurjchem-942	82	14	contents	content	NOUN
eurjchem-942	82	15	of	of	ADP
eurjchem-942	82	16	each	each	DET
eurjchem-942	82	17	component	component	NOUN
eurjchem-942	82	18	on	on	ADP
eurjchem-942	82	19	different	different	ADJ
eurjchem-942	82	20	columns	column	NOUN
eurjchem-942	82	21	like	like	ADP
eurjchem-942	82	22	hypersil‐	hypersil‐	NOUN
eurjchem-942	82	23	gold	gold	NOUN
eurjchem-942	82	24	(	(	PUNCT
eurjchem-942	82	25	c18‐bonded	c18‐bonde	VERB
eurjchem-942	82	26	ultrapure	ultrapure	NOUN
eurjchem-942	82	27	silica	silica	NOUN
eurjchem-942	82	28	based	base	VERB
eurjchem-942	82	29	column	column	NOUN
eurjchem-942	82	30	)	)	PUNCT
eurjchem-942	82	31	and	and	CCONJ
eurjchem-942	82	32	bio	bio	INTJ
eurjchem-942	82	33	basic‐8	basic‐8	PROPN
eurjchem-942	82	34	to	to	PART
eurjchem-942	82	35	identify	identify	VERB
eurjchem-942	82	36	the	the	DET
eurjchem-942	82	37	optimal	optimal	ADJ
eurjchem-942	82	38	conditions	condition	NOUN
eurjchem-942	82	39	that	that	PRON
eurjchem-942	82	40	produce	produce	VERB
eurjchem-942	82	41	the	the	DET
eurjchem-942	82	42	best	good	ADJ
eurjchem-942	82	43	sensitivity	sensitivity	NOUN
eurjchem-942	82	44	,	,	PUNCT
eurjchem-942	82	45	efficiency	efficiency	NOUN
eurjchem-942	82	46	and	and	CCONJ
eurjchem-942	82	47	peak	peak	NOUN
eurjchem-942	82	48	shape	shape	NOUN
eurjchem-942	82	49	.	.	PUNCT
eurjchem-942	83	1	the	the	DET
eurjchem-942	83	2	use	use	NOUN
eurjchem-942	83	3	of	of	ADP
eurjchem-942	83	4	buffer	buffer	NOUN
eurjchem-942	83	5	solution	solution	NOUN
eurjchem-942	83	6	helped	help	VERB
eurjchem-942	83	7	in	in	ADP
eurjchem-942	83	8	achieving	achieve	VERB
eurjchem-942	83	9	good	good	ADJ
eurjchem-942	83	10	response	response	NOUN
eurjchem-942	83	11	for	for	ADP
eurjchem-942	83	12	ms	ms	NOUN
eurjchem-942	83	13	detection	detection	NOUN
eurjchem-942	83	14	operating	operate	VERB
eurjchem-942	83	15	in	in	ADP
eurjchem-942	83	16	the	the	DET
eurjchem-942	83	17	positive	positive	ADJ
eurjchem-942	83	18	mode	mode	NOUN
eurjchem-942	83	19	.	.	PUNCT
eurjchem-942	84	1	thus	thus	ADV
eurjchem-942	84	2	,	,	PUNCT
eurjchem-942	84	3	a	a	DET
eurjchem-942	84	4	mobile	mobile	ADJ
eurjchem-942	84	5	phase	phase	NOUN
eurjchem-942	84	6	consisting	consist	VERB
eurjchem-942	84	7	of	of	ADP
eurjchem-942	84	8	10	10	NUM
eurjchem-942	84	9	mm	mm	NOUN
eurjchem-942	84	10	ammonium	ammonium	NOUN
eurjchem-942	84	11	acetate	acetate	NOUN
eurjchem-942	84	12	buffer	buffer	NOUN
eurjchem-942	84	13	ph	ph	NOUN
eurjchem-942	84	14	adjusted	adjust	VERB
eurjchem-942	84	15	to	to	ADP
eurjchem-942	84	16	3.5	3.5	NUM
eurjchem-942	84	17	with	with	ADP
eurjchem-942	84	18	acetic	acetic	ADJ
eurjchem-942	84	19	acid	acid	NOUN
eurjchem-942	84	20	:	:	PUNCT
eurjchem-942	84	21	acetonitrile	acetonitrile	NOUN
eurjchem-942	84	22	(	(	PUNCT
eurjchem-942	84	23	10:90	10:90	NUM
eurjchem-942	84	24	,	,	PUNCT
eurjchem-942	84	25	v	v	NOUN
eurjchem-942	84	26	:	:	PUNCT
eurjchem-942	84	27	v	v	NOUN
eurjchem-942	84	28	)	)	PUNCT
eurjchem-942	84	29	was	be	AUX
eurjchem-942	84	30	found	find	VERB
eurjchem-942	84	31	suitable	suitable	ADJ
eurjchem-942	84	32	as	as	SCONJ
eurjchem-942	84	33	the	the	DET
eurjchem-942	84	34	drugs	drug	NOUN
eurjchem-942	84	35	were	be	AUX
eurjchem-942	84	36	protonated	protonate	VERB
eurjchem-942	84	37	and	and	CCONJ
eurjchem-942	84	38	well	well	ADV
eurjchem-942	84	39	separated	separate	VERB
eurjchem-942	84	40	by	by	ADP
eurjchem-942	84	41	this	this	DET
eurjchem-942	84	42	phase	phase	NOUN
eurjchem-942	84	43	(	(	PUNCT
eurjchem-942	84	44	figure	figure	NOUN
eurjchem-942	84	45	3	3	NUM
eurjchem-942	84	46	)	)	PUNCT
eurjchem-942	84	47	.	.	PUNCT
eurjchem-942	85	1	high	high	ADJ
eurjchem-942	85	2	content	content	NOUN
eurjchem-942	85	3	of	of	ADP
eurjchem-942	85	4	acetonitrile	acetonitrile	NOUN
eurjchem-942	85	5	(	(	PUNCT
eurjchem-942	85	6	90	90	NUM
eurjchem-942	85	7	%	%	NOUN
eurjchem-942	85	8	)	)	PUNCT
eurjchem-942	85	9	in	in	ADP
eurjchem-942	85	10	the	the	DET
eurjchem-942	85	11	mobile	mobile	ADJ
eurjchem-942	85	12	phase	phase	NOUN
eurjchem-942	85	13	helped	help	VERB
eurjchem-942	85	14	in	in	ADP
eurjchem-942	85	15	eluting	elute	VERB
eurjchem-942	85	16	the	the	DET
eurjchem-942	85	17	drugs	drug	NOUN
eurjchem-942	85	18	along	along	ADP
eurjchem-942	85	19	with	with	ADP
eurjchem-942	85	20	their	their	PRON
eurjchem-942	85	21	is	be	AUX
eurjchem-942	85	22	within	within	ADP
eurjchem-942	85	23	3	3	NUM
eurjchem-942	85	24	min	min	NOUN
eurjchem-942	85	25	at	at	ADP
eurjchem-942	85	26	a	a	DET
eurjchem-942	85	27	flow	flow	NOUN
eurjchem-942	85	28	rate	rate	NOUN
eurjchem-942	85	29	of	of	ADP
eurjchem-942	85	30	250	250	NUM
eurjchem-942	85	31	µl	µl	NOUN
eurjchem-942	85	32	/	/	SYM
eurjchem-942	85	33	min	min	NOUN
eurjchem-942	85	34	.	.	PROPN
eurjchem-942	86	1	hypersil‐gold	hypersil‐gold	NOUN
eurjchem-942	86	2	(	(	PUNCT
eurjchem-942	86	3	50.0	50.0	NUM
eurjchem-942	86	4	mm	mm	NOUN
eurjchem-942	86	5	×	×	NOUN
eurjchem-942	86	6	2.0	2.0	NUM
eurjchem-942	86	7	mm	mm	NOUN
eurjchem-942	86	8	,	,	PUNCT
eurjchem-942	86	9	1.9	1.9	NUM
eurjchem-942	86	10	µm	µm	ADP
eurjchem-942	86	11	particle	particle	NOUN
eurjchem-942	86	12	size	size	NOUN
eurjchem-942	86	13	)	)	PUNCT
eurjchem-942	86	14	column	column	NOUN
eurjchem-942	86	15	gave	give	VERB
eurjchem-942	86	16	good	good	ADJ
eurjchem-942	86	17	peak	peak	NOUN
eurjchem-942	86	18	shape	shape	NOUN
eurjchem-942	86	19	and	and	CCONJ
eurjchem-942	86	20	response	response	NOUN
eurjchem-942	86	21	even	even	ADV
eurjchem-942	86	22	at	at	ADP
eurjchem-942	86	23	loq	loq	PROPN
eurjchem-942	86	24	levels	level	NOUN
eurjchem-942	86	25	for	for	ADP
eurjchem-942	86	26	both	both	DET
eurjchem-942	86	27	drugs	drug	NOUN
eurjchem-942	86	28	.	.	PUNCT
eurjchem-942	87	1	figure	figure	VERB
eurjchem-942	87	2	3	3	NUM
eurjchem-942	87	3	.	.	PUNCT
eurjchem-942	87	4	representative	representative	ADJ
eurjchem-942	87	5	srm	srm	PROPN
eurjchem-942	87	6	chromatograms	chromatogram	NOUN
eurjchem-942	87	7	of	of	ADP
eurjchem-942	87	8	is	be	AUX
eurjchem-942	87	9	(	(	PUNCT
eurjchem-942	87	10	40	40	NUM
eurjchem-942	87	11	ng	ng	NOUN
eurjchem-942	87	12	/	/	SYM
eurjchem-942	87	13	ml	ml	PROPN
eurjchem-942	87	14	)	)	PUNCT
eurjchem-942	87	15	(	(	PUNCT
eurjchem-942	87	16	a	a	X
eurjchem-942	87	17	)	)	PUNCT
eurjchem-942	87	18	,	,	PUNCT
eurjchem-942	87	19	fin	fin	NOUN
eurjchem-942	87	20	(	(	PUNCT
eurjchem-942	87	21	300	300	NUM
eurjchem-942	87	22	ng	ng	NOUN
eurjchem-942	87	23	/	/	SYM
eurjchem-942	87	24	ml	ml	NOUN
eurjchem-942	87	25	)	)	PUNCT
eurjchem-942	87	26	(	(	PUNCT
eurjchem-942	87	27	b	b	X
eurjchem-942	87	28	)	)	PUNCT
eurjchem-942	87	29	and	and	CCONJ
eurjchem-942	87	30	tam	tam	X
eurjchem-942	87	31	(	(	PUNCT
eurjchem-942	87	32	25	25	NUM
eurjchem-942	87	33	ng	ng	PROPN
eurjchem-942	87	34	/	/	SYM
eurjchem-942	87	35	ml	ml	NOUN
eurjchem-942	87	36	)	)	PUNCT
eurjchem-942	87	37	(	(	PUNCT
eurjchem-942	87	38	c	c	NOUN
eurjchem-942	87	39	)	)	PUNCT
eurjchem-942	87	40	.	.	PUNCT
eurjchem-942	88	1	3.1	3.1	NUM
eurjchem-942	88	2	.	.	PUNCT
eurjchem-942	88	3	method	method	NOUN
eurjchem-942	88	4	validation	validation	NOUN
eurjchem-942	88	5	3.1.1	3.1.1	NUM
eurjchem-942	88	6	.	.	PUNCT
eurjchem-942	89	1	linearity	linearity	NOUN
eurjchem-942	89	2	and	and	CCONJ
eurjchem-942	89	3	range	range	VERB
eurjchem-942	89	4	under	under	ADP
eurjchem-942	89	5	the	the	DET
eurjchem-942	89	6	optimum	optimum	ADJ
eurjchem-942	89	7	chromatographic	chromatographic	ADJ
eurjchem-942	89	8	and	and	CCONJ
eurjchem-942	89	9	mass	mass	ADJ
eurjchem-942	89	10	spectrometric	spectrometric	ADJ
eurjchem-942	89	11	conditions	condition	NOUN
eurjchem-942	89	12	a	a	DET
eurjchem-942	89	13	linear	linear	ADJ
eurjchem-942	89	14	relationship	relationship	NOUN
eurjchem-942	89	15	was	be	AUX
eurjchem-942	89	16	established	establish	VERB
eurjchem-942	89	17	.	.	PUNCT
eurjchem-942	90	1	the	the	DET
eurjchem-942	90	2	calibration	calibration	NOUN
eurjchem-942	90	3	graphs	graph	NOUN
eurjchem-942	90	4	were	be	AUX
eurjchem-942	90	5	found	find	VERB
eurjchem-942	90	6	to	to	PART
eurjchem-942	90	7	be	be	AUX
eurjchem-942	90	8	rectilinear	rectilinear	ADJ
eurjchem-942	90	9	within	within	ADP
eurjchem-942	90	10	the	the	DET
eurjchem-942	90	11	concentration	concentration	NOUN
eurjchem-942	90	12	range	range	NOUN
eurjchem-942	90	13	of	of	ADP
eurjchem-942	90	14	1.6‐40.0	1.6‐40.0	PROPN
eurjchem-942	90	15	ng	ng	PROPN
eurjchem-942	90	16	/	/	SYM
eurjchem-942	90	17	ml	ml	X
eurjchem-942	90	18	for	for	ADP
eurjchem-942	90	19	tam	tam	NOUN
eurjchem-942	90	20	and	and	CCONJ
eurjchem-942	90	21	20.0‐500.0	20.0‐500.0	PROPN
eurjchem-942	90	22	ng	ng	PROPN
eurjchem-942	90	23	/	/	SYM
eurjchem-942	90	24	ml	ml	NOUN
eurjchem-942	90	25	for	for	ADP
eurjchem-942	90	26	fin	fin	NOUN
eurjchem-942	90	27	.	.	PUNCT
eurjchem-942	91	1	the	the	DET
eurjchem-942	91	2	linearity	linearity	NOUN
eurjchem-942	91	3	of	of	ADP
eurjchem-942	91	4	standard	standard	ADJ
eurjchem-942	91	5	curves	curve	NOUN
eurjchem-942	91	6	(	(	PUNCT
eurjchem-942	91	7	r2	r2	PROPN
eurjchem-942	91	8	)	)	PUNCT
eurjchem-942	91	9	for	for	ADP
eurjchem-942	91	10	all	all	DET
eurjchem-942	91	11	analytes	analyte	NOUN
eurjchem-942	91	12	were	be	AUX
eurjchem-942	91	13	greater	great	ADJ
eurjchem-942	91	14	than	than	ADP
eurjchem-942	91	15	0.99	0.99	NUM
eurjchem-942	91	16	.	.	PUNCT
eurjchem-942	92	1	the	the	DET
eurjchem-942	92	2	calibration	calibration	NOUN
eurjchem-942	92	3	curve	curve	NOUN
eurjchem-942	92	4	had	have	VERB
eurjchem-942	92	5	a	a	DET
eurjchem-942	92	6	reliable	reliable	ADJ
eurjchem-942	92	7	reproducibility	reproducibility	NOUN
eurjchem-942	92	8	across	across	ADP
eurjchem-942	92	9	the	the	DET
eurjchem-942	92	10	calibration	calibration	NOUN
eurjchem-942	92	11	range	range	NOUN
eurjchem-942	92	12	.	.	PUNCT
eurjchem-942	93	1	the	the	DET
eurjchem-942	93	2	corresponding	correspond	VERB
eurjchem-942	93	3	regression	regression	NOUN
eurjchem-942	93	4	equations	equation	NOUN
eurjchem-942	93	5	are	be	AUX
eurjchem-942	93	6	cited	cite	VERB
eurjchem-942	93	7	in	in	ADP
eurjchem-942	93	8	table	table	NOUN
eurjchem-942	93	9	2	2	NUM
eurjchem-942	93	10	,	,	PUNCT
eurjchem-942	93	11	where	where	SCONJ
eurjchem-942	93	12	the	the	DET
eurjchem-942	93	13	slopes	slope	NOUN
eurjchem-942	93	14	are	be	AUX
eurjchem-942	93	15	consistent	consistent	ADJ
eurjchem-942	93	16	with	with	ADP
eurjchem-942	93	17	the	the	DET
eurjchem-942	93	18	relative	relative	ADJ
eurjchem-942	93	19	peak	peak	NOUN
eurjchem-942	93	20	areas	area	NOUN
eurjchem-942	93	21	.	.	PUNCT
eurjchem-942	94	1	3.1.2	3.1.2	X
eurjchem-942	94	2	.	.	PUNCT
eurjchem-942	94	3	accuracy	accuracy	NOUN
eurjchem-942	94	4	and	and	CCONJ
eurjchem-942	94	5	precision	precision	NOUN
eurjchem-942	94	6	the	the	DET
eurjchem-942	94	7	accuracy	accuracy	NOUN
eurjchem-942	94	8	of	of	ADP
eurjchem-942	94	9	the	the	DET
eurjchem-942	94	10	proposed	propose	VERB
eurjchem-942	94	11	method	method	NOUN
eurjchem-942	94	12	was	be	AUX
eurjchem-942	94	13	evaluated	evaluate	VERB
eurjchem-942	94	14	by	by	ADP
eurjchem-942	94	15	analyzing	analyze	VERB
eurjchem-942	94	16	six	six	NUM
eurjchem-942	94	17	levels	level	NOUN
eurjchem-942	94	18	of	of	ADP
eurjchem-942	94	19	standard	standard	ADJ
eurjchem-942	94	20	solutions	solution	NOUN
eurjchem-942	94	21	of	of	ADP
eurjchem-942	94	22	the	the	DET
eurjchem-942	94	23	studied	study	VERB
eurjchem-942	94	24	drugs	drug	NOUN
eurjchem-942	94	25	,	,	PUNCT
eurjchem-942	94	26	each	each	DET
eurjchem-942	94	27	three	three	NUM
eurjchem-942	94	28	times	time	NOUN
eurjchem-942	94	29	.	.	PUNCT
eurjchem-942	95	1	the	the	DET
eurjchem-942	95	2	results	result	NOUN
eurjchem-942	95	3	obtained	obtain	VERB
eurjchem-942	95	4	by	by	ADP
eurjchem-942	95	5	the	the	DET
eurjchem-942	95	6	proposed	propose	VERB
eurjchem-942	95	7	method	method	NOUN
eurjchem-942	95	8	were	be	AUX
eurjchem-942	95	9	favorably	favorably	ADV
eurjchem-942	95	10	compared	compare	VERB
eurjchem-942	95	11	with	with	ADP
eurjchem-942	95	12	those	those	PRON
eurjchem-942	95	13	of	of	ADP
eurjchem-942	95	14	reference	reference	NOUN
eurjchem-942	95	15	ones	one	NOUN
eurjchem-942	95	16	[	[	X
eurjchem-942	95	17	26	26	NUM
eurjchem-942	95	18	]	]	PUNCT
eurjchem-942	95	19	for	for	ADP
eurjchem-942	95	20	tam	tam	NOUN
eurjchem-942	95	21	and	and	CCONJ
eurjchem-942	95	22	[	[	X
eurjchem-942	95	23	5	5	NUM
eurjchem-942	95	24	]	]	PUNCT
eurjchem-942	95	25	for	for	ADP
eurjchem-942	95	26	fin	fin	NOUN
eurjchem-942	95	27	.	.	PUNCT
eurjchem-942	96	1	184	184	NUM
eurjchem-942	96	2	mohamed	mohame	VERB
eurjchem-942	96	3	et	et	PROPN
eurjchem-942	96	4	al	al	PROPN
eurjchem-942	96	5	.	.	PUNCT
eurjchem-942	96	6	/	/	SYM
eurjchem-942	96	7	european	european	PROPN
eurjchem-942	96	8	journal	journal	PROPN
eurjchem-942	96	9	of	of	ADP
eurjchem-942	96	10	chemistry	chemistry	NOUN
eurjchem-942	96	11	5	5	NUM
eurjchem-942	96	12	(	(	PUNCT
eurjchem-942	96	13	1	1	NUM
eurjchem-942	96	14	)	)	PUNCT
eurjchem-942	96	15	(	(	PUNCT
eurjchem-942	96	16	2014	2014	NUM
eurjchem-942	96	17	)	)	PUNCT
eurjchem-942	96	18	181‐185	181‐185	NUM
eurjchem-942	96	19	table	table	NOUN
eurjchem-942	96	20	2	2	NUM
eurjchem-942	96	21	.	.	PUNCT
eurjchem-942	96	22	performance	performance	NOUN
eurjchem-942	96	23	data	datum	NOUN
eurjchem-942	96	24	for	for	ADP
eurjchem-942	96	25	tamsulosin	tamsulosin	NOUN
eurjchem-942	96	26	and	and	CCONJ
eurjchem-942	96	27	finasteride	finasteride	ADV
eurjchem-942	96	28	by	by	ADP
eurjchem-942	96	29	the	the	DET
eurjchem-942	96	30	proposed	propose	VERB
eurjchem-942	96	31	lc‐ms	lc‐ms	AUX
eurjchem-942	96	32	/	/	SYM
eurjchem-942	96	33	ms	ms	PROPN
eurjchem-942	96	34	method	method	PROPN
eurjchem-942	96	35	*	*	PUNCT
eurjchem-942	96	36	.	.	PUNCT
eurjchem-942	97	1	parameter	parameter	PROPN
eurjchem-942	97	2	tamsulosin	tamsulosin	VERB
eurjchem-942	97	3	finasteride	finasteride	ADJ
eurjchem-942	97	4	linearity	linearity	NOUN
eurjchem-942	97	5	range	range	VERB
eurjchem-942	97	6	1.60	1.60	NUM
eurjchem-942	97	7	‐	‐	ADP
eurjchem-942	97	8	40.00	40.00	NUM
eurjchem-942	97	9	ng	ng	PROPN
eurjchem-942	97	10	/	/	SYM
eurjchem-942	97	11	ml	ml	PROPN
eurjchem-942	97	12	20.00	20.00	NUM
eurjchem-942	97	13	‐	‐	NOUN
eurjchem-942	97	14	500.00	500.00	NUM
eurjchem-942	97	15	ng	ng	NOUN
eurjchem-942	97	16	/	/	SYM
eurjchem-942	97	17	ml	ml	ADP
eurjchem-942	97	18	regression	regression	NOUN
eurjchem-942	97	19	equation	equation	NOUN
eurjchem-942	97	20	7.21×10‐3	7.21×10‐3	NUM
eurjchem-942	97	21	c	c	NOUN
eurjchem-942	97	22	‐	‐	VERB
eurjchem-942	97	23	1.82×10‐3	1.82×10‐3	NUM
eurjchem-942	97	24	1.85×10‐4	1.85×10‐4	NUM
eurjchem-942	97	25	c	c	NOUN
eurjchem-942	97	26	‐	‐	NOUN
eurjchem-942	97	27	6.56×10‐3	6.56×10‐3	NUM
eurjchem-942	97	28	slope	slope	NOUN
eurjchem-942	97	29	(	(	PUNCT
eurjchem-942	97	30	b	b	NOUN
eurjchem-942	97	31	)	)	PUNCT
eurjchem-942	97	32	7.21×10‐3	7.21×10‐3	NUM
eurjchem-942	97	33	1.85×10‐4	1.85×10‐4	NUM
eurjchem-942	97	34	intercept	intercept	NOUN
eurjchem-942	97	35	(	(	PUNCT
eurjchem-942	97	36	a	a	NOUN
eurjchem-942	97	37	)	)	PUNCT
eurjchem-942	97	38	1.82×10‐3	1.82×10‐3	NUM
eurjchem-942	97	39	6.56×10‐3	6.56×10‐3	NUM
eurjchem-942	97	40	correlation	correlation	NOUN
eurjchem-942	97	41	coefficient	coefficient	NOUN
eurjchem-942	97	42	(	(	PUNCT
eurjchem-942	97	43	r	r	NOUN
eurjchem-942	97	44	)	)	PUNCT
eurjchem-942	97	45	0.9998	0.9998	NUM
eurjchem-942	97	46	0.9997	0.9997	NUM
eurjchem-942	97	47	r2	r2	PROPN
eurjchem-942	97	48	0.9997	0.9997	NUM
eurjchem-942	97	49	0.9995	0.9995	NUM
eurjchem-942	97	50	se	se	X
eurjchem-942	97	51	of	of	ADP
eurjchem-942	97	52	slope	slope	NOUN
eurjchem-942	97	53	6.45×10‐5	6.45×10‐5	NUM
eurjchem-942	97	54	2.12×10‐6	2.12×10‐6	NUM
eurjchem-942	97	55	se	se	X
eurjchem-942	97	56	of	of	ADP
eurjchem-942	97	57	intercept	intercept	NOUN
eurjchem-942	97	58	1.42×10‐3	1.42×10‐3	NUM
eurjchem-942	97	59	5.84×10‐4	5.84×10‐4	NUM
eurjchem-942	97	60	sy	sy	NOUN
eurjchem-942	97	61	/	/	SYM
eurjchem-942	97	62	x	x	SYM
eurjchem-942	97	63	2.11×10‐3	2.11×10‐3	NUM
eurjchem-942	97	64	8.67×10‐4	8.67×10‐4	NUM
eurjchem-942	97	65	lod	lod	PROPN
eurjchem-942	97	66	0.50	0.50	NUM
eurjchem-942	97	67	ng	ng	PROPN
eurjchem-942	97	68	/	/	SYM
eurjchem-942	97	69	ml	ml	PROPN
eurjchem-942	97	70	5.00	5.00	NUM
eurjchem-942	97	71	ng	ng	NOUN
eurjchem-942	97	72	/	/	SYM
eurjchem-942	97	73	ml	ml	PROPN
eurjchem-942	97	74	loq	loq	PROPN
eurjchem-942	97	75	1.60	1.60	NUM
eurjchem-942	97	76	ng	ng	PROPN
eurjchem-942	97	77	/	/	SYM
eurjchem-942	97	78	ml	ml	PROPN
eurjchem-942	97	79	20.00	20.00	NUM
eurjchem-942	97	80	ng	ng	NOUN
eurjchem-942	97	81	/	/	SYM
eurjchem-942	97	82	ml	ml	PROPN
eurjchem-942	97	83	*	*	ADJ
eurjchem-942	97	84	c	c	NOUN
eurjchem-942	97	85	:	:	PUNCT
eurjchem-942	97	86	concentration	concentration	NOUN
eurjchem-942	97	87	,	,	PUNCT
eurjchem-942	97	88	sy	sy	PROPN
eurjchem-942	97	89	/	/	SYM
eurjchem-942	97	90	x	x	NOUN
eurjchem-942	97	91	:	:	PUNCT
eurjchem-942	97	92	standard	standard	ADJ
eurjchem-942	97	93	deviation	deviation	NOUN
eurjchem-942	97	94	of	of	ADP
eurjchem-942	97	95	residuals	residual	NOUN
eurjchem-942	97	96	,	,	PUNCT
eurjchem-942	97	97	lod	lod	PROPN
eurjchem-942	97	98	:	:	PUNCT
eurjchem-942	97	99	limit	limit	NOUN
eurjchem-942	97	100	of	of	ADP
eurjchem-942	97	101	detection	detection	NOUN
eurjchem-942	97	102	,	,	PUNCT
eurjchem-942	97	103	loq	loq	PROPN
eurjchem-942	97	104	:	:	PUNCT
eurjchem-942	97	105	limit	limit	NOUN
eurjchem-942	97	106	of	of	ADP
eurjchem-942	97	107	quantification	quantification	NOUN
eurjchem-942	97	108	.	.	PUNCT
eurjchem-942	98	1	table	table	NOUN
eurjchem-942	98	2	3	3	NUM
eurjchem-942	98	3	.	.	PUNCT
eurjchem-942	98	4	accuracy	accuracy	NOUN
eurjchem-942	98	5	and	and	CCONJ
eurjchem-942	98	6	precision	precision	NOUN
eurjchem-942	98	7	data	datum	NOUN
eurjchem-942	98	8	obtained	obtain	VERB
eurjchem-942	98	9	by	by	ADP
eurjchem-942	98	10	the	the	DET
eurjchem-942	98	11	proposed	propose	VERB
eurjchem-942	98	12	lc‐ms	lc‐ms	AUX
eurjchem-942	98	13	/	/	SYM
eurjchem-942	98	14	ms	ms	PROPN
eurjchem-942	98	15	method	method	NOUN
eurjchem-942	98	16	and	and	CCONJ
eurjchem-942	98	17	the	the	DET
eurjchem-942	98	18	reference	reference	NOUN
eurjchem-942	98	19	ones	one	NOUN
eurjchem-942	98	20	for	for	ADP
eurjchem-942	98	21	the	the	DET
eurjchem-942	98	22	analysis	analysis	NOUN
eurjchem-942	98	23	of	of	ADP
eurjchem-942	98	24	tamsulosin	tamsulosin	NOUN
eurjchem-942	98	25	and	and	CCONJ
eurjchem-942	98	26	finasteride	finasteride	ADV
eurjchem-942	98	27	in	in	ADP
eurjchem-942	98	28	pure	pure	ADJ
eurjchem-942	98	29	form	form	NOUN
eurjchem-942	98	30	a.	a.	NOUN
eurjchem-942	98	31	item	item	NOUN
eurjchem-942	98	32	tamsulosin	tamsulosin	NOUN
eurjchem-942	98	33	finasteride	finasteride	ADV
eurjchem-942	98	34	proposed	propose	VERB
eurjchem-942	98	35	reported	report	VERB
eurjchem-942	98	36	[	[	X
eurjchem-942	98	37	26	26	NUM
eurjchem-942	98	38	]	]	X
eurjchem-942	98	39	c	c	PROPN
eurjchem-942	98	40	proposed	propose	VERB
eurjchem-942	98	41	reported	report	VERB
eurjchem-942	98	42	[	[	X
eurjchem-942	98	43	5	5	NUM
eurjchem-942	98	44	]	]	PUNCT
eurjchem-942	99	1	d	d	NOUN
eurjchem-942	99	2	mean	mean	NOUN
eurjchem-942	99	3	b	b	X
eurjchem-942	99	4	±	±	NUM
eurjchem-942	99	5	sd	sd	ADP
eurjchem-942	99	6	100.11±0.78	100.11±0.78	NOUN
eurjchem-942	99	7	99.54±0.88	99.54±0.88	NUM
eurjchem-942	99	8	100.01±0.61	100.01±0.61	NOUN
eurjchem-942	99	9	99.86±0.81	99.86±0.81	NUM
eurjchem-942	99	10	%	%	NOUN
eurjchem-942	99	11	rsd	rsd	NOUN
eurjchem-942	99	12	0.78	0.78	NUM
eurjchem-942	99	13	0.88	0.88	NUM
eurjchem-942	99	14	0.69	0.69	NUM
eurjchem-942	99	15	0.81	0.81	NUM
eurjchem-942	99	16	%	%	NOUN
eurjchem-942	99	17	rer	rer	X
eurjchem-942	99	18	0.32	0.32	NUM
eurjchem-942	99	19	0.44	0.44	NUM
eurjchem-942	99	20	0.28	0.28	NUM
eurjchem-942	99	21	0.40	0.40	NUM
eurjchem-942	99	22	n	n	NUM
eurjchem-942	99	23	6	6	NUM
eurjchem-942	99	24	4	4	NUM
eurjchem-942	99	25	6	6	NUM
eurjchem-942	99	26	4	4	NUM
eurjchem-942	99	27	variance	variance	NOUN
eurjchem-942	99	28	0.61	0.61	NUM
eurjchem-942	99	29	0.77	0.77	NUM
eurjchem-942	99	30	0.47	0.47	NUM
eurjchem-942	99	31	0.65	0.65	NUM
eurjchem-942	99	32	t‐	t‐	ADJ
eurjchem-942	99	33	test	test	NOUN
eurjchem-942	99	34	(	(	PUNCT
eurjchem-942	99	35	2.31	2.31	NUM
eurjchem-942	99	36	)	)	PUNCT
eurjchem-942	99	37	1.08	1.08	NUM
eurjchem-942	99	38	0.32	0.32	NUM
eurjchem-942	99	39	f‐	f‐	NOUN
eurjchem-942	99	40	test	test	NOUN
eurjchem-942	99	41	(	(	PUNCT
eurjchem-942	99	42	5.409	5.409	NUM
eurjchem-942	99	43	)	)	PUNCT
eurjchem-942	99	44	1.26	1.26	NUM
eurjchem-942	99	45	1.37	1.37	NUM
eurjchem-942	99	46	intraday	intraday	NOUN
eurjchem-942	99	47	precision	precision	NOUN
eurjchem-942	99	48	b	b	PROPN
eurjchem-942	99	49	99.83±0.77	99.83±0.77	NUM
eurjchem-942	99	50	99.75±0.63	99.75±0.63	NUM
eurjchem-942	99	51	inter‐day	inter‐day	PROPN
eurjchem-942	99	52	precision	precision	PROPN
eurjchem-942	99	53	b	b	PROPN
eurjchem-942	100	1	99.16±0.83	99.16±0.83	NUM
eurjchem-942	100	2	99.06±1.01	99.06±1.01	NUM
eurjchem-942	100	3	a	a	DET
eurjchem-942	100	4	sd	sd	NOUN
eurjchem-942	100	5	:	:	PUNCT
eurjchem-942	100	6	standard	standard	ADJ
eurjchem-942	100	7	deviation	deviation	NOUN
eurjchem-942	100	8	,	,	PUNCT
eurjchem-942	100	9	%	%	PUNCT
eurjchem-942	100	10	rsd	rsd	NOUN
eurjchem-942	100	11	:	:	PUNCT
eurjchem-942	100	12	percent	percent	NOUN
eurjchem-942	100	13	relative	relative	ADJ
eurjchem-942	100	14	standard	standard	ADJ
eurjchem-942	100	15	deviation	deviation	NOUN
eurjchem-942	100	16	,	,	PUNCT
eurjchem-942	100	17	%	%	INTJ
eurjchem-942	100	18	rer	rer	X
eurjchem-942	100	19	:	:	PUNCT
eurjchem-942	100	20	percent	percent	NOUN
eurjchem-942	100	21	relative	relative	ADJ
eurjchem-942	100	22	standard	standard	PROPN
eurjchem-942	100	23	error	error	NOUN
eurjchem-942	100	24	,	,	PUNCT
eurjchem-942	100	25	values	value	NOUN
eurjchem-942	100	26	in	in	ADP
eurjchem-942	100	27	parenthesis	parenthesis	NOUN
eurjchem-942	100	28	are	be	AUX
eurjchem-942	100	29	the	the	DET
eurjchem-942	100	30	theoretical	theoretical	ADJ
eurjchem-942	100	31	values	value	NOUN
eurjchem-942	100	32	of	of	ADP
eurjchem-942	100	33	t	t	PROPN
eurjchem-942	100	34	and	and	CCONJ
eurjchem-942	100	35	f	f	PROPN
eurjchem-942	100	36	at	at	ADP
eurjchem-942	100	37	p	p	NOUN
eurjchem-942	100	38	=	=	NOUN
eurjchem-942	100	39	0.05	0.05	NUM
eurjchem-942	100	40	[	[	X
eurjchem-942	100	41	28	28	NUM
eurjchem-942	100	42	]	]	PUNCT
eurjchem-942	100	43	.	.	PUNCT
eurjchem-942	101	1	b	b	X
eurjchem-942	101	2	average	average	NOUN
eurjchem-942	101	3	of	of	ADP
eurjchem-942	101	4	three	three	NUM
eurjchem-942	101	5	different	different	ADJ
eurjchem-942	101	6	determinations	determination	NOUN
eurjchem-942	101	7	.	.	PUNCT
eurjchem-942	102	1	c	c	PROPN
eurjchem-942	102	2	the	the	DET
eurjchem-942	102	3	reported	report	VERB
eurjchem-942	102	4	method	method	NOUN
eurjchem-942	102	5	for	for	ADP
eurjchem-942	102	6	tamsulosin	tamsulosin	NOUN
eurjchem-942	102	7	[	[	X
eurjchem-942	102	8	26	26	NUM
eurjchem-942	102	9	]	]	PUNCT
eurjchem-942	102	10	is	be	AUX
eurjchem-942	102	11	an	an	DET
eurjchem-942	102	12	hplc	hplc	NOUN
eurjchem-942	102	13	method	method	NOUN
eurjchem-942	102	14	and	and	CCONJ
eurjchem-942	102	15	was	be	AUX
eurjchem-942	102	16	performed	perform	VERB
eurjchem-942	102	17	using	use	VERB
eurjchem-942	102	18	c18	c18	NOUN
eurjchem-942	102	19	column	column	NOUN
eurjchem-942	102	20	250	250	NUM
eurjchem-942	102	21	×	×	NOUN
eurjchem-942	102	22	4.6	4.6	NUM
eurjchem-942	102	23	mm	mm	NOUN
eurjchem-942	102	24	(	(	PUNCT
eurjchem-942	102	25	particle	particle	NOUN
eurjchem-942	102	26	size	size	NOUN
eurjchem-942	102	27	of	of	ADP
eurjchem-942	102	28	5	5	NUM
eurjchem-942	102	29	µm	µm	NOUN
eurjchem-942	102	30	)	)	PUNCT
eurjchem-942	102	31	.	.	PUNCT
eurjchem-942	103	1	mobile	mobile	ADJ
eurjchem-942	103	2	phase	phase	NOUN
eurjchem-942	103	3	:	:	PUNCT
eurjchem-942	103	4	acetonitrile	acetonitrile	NOUN
eurjchem-942	103	5	:	:	PUNCT
eurjchem-942	103	6	(	(	PUNCT
eurjchem-942	103	7	0.05	0.05	NUM
eurjchem-942	103	8	m	m	NOUN
eurjchem-942	103	9	)	)	PUNCT
eurjchem-942	103	10	kh2po4	kh2po4	NOUN
eurjchem-942	103	11	buffer	buffer	NOUN
eurjchem-942	103	12	(	(	PUNCT
eurjchem-942	103	13	45:55	45:55	NUM
eurjchem-942	103	14	)	)	PUNCT
eurjchem-942	103	15	at	at	ADP
eurjchem-942	103	16	flow	flow	NOUN
eurjchem-942	103	17	rate	rate	NOUN
eurjchem-942	103	18	1.8	1.8	NUM
eurjchem-942	103	19	ml	ml	NOUN
eurjchem-942	103	20	/	/	SYM
eurjchem-942	103	21	min	min	NOUN
eurjchem-942	103	22	.	.	PUNCT
eurjchem-942	104	1	the	the	DET
eurjchem-942	104	2	detection	detection	NOUN
eurjchem-942	104	3	was	be	AUX
eurjchem-942	104	4	monitored	monitor	VERB
eurjchem-942	104	5	at	at	ADP
eurjchem-942	104	6	240	240	NUM
eurjchem-942	104	7	nm	nm	NOUN
eurjchem-942	104	8	.	.	PUNCT
eurjchem-942	105	1	d	d	X
eurjchem-942	105	2	the	the	DET
eurjchem-942	105	3	official	official	ADJ
eurjchem-942	105	4	method	method	NOUN
eurjchem-942	105	5	for	for	ADP
eurjchem-942	105	6	finasteride	finasteride	ADJ
eurjchem-942	105	7	[	[	X
eurjchem-942	105	8	5	5	NUM
eurjchem-942	105	9	]	]	PUNCT
eurjchem-942	105	10	is	be	AUX
eurjchem-942	105	11	an	an	DET
eurjchem-942	105	12	hplc	hplc	NOUN
eurjchem-942	105	13	method	method	NOUN
eurjchem-942	105	14	and	and	CCONJ
eurjchem-942	105	15	was	be	AUX
eurjchem-942	105	16	performed	perform	VERB
eurjchem-942	105	17	using	use	VERB
eurjchem-942	105	18	,	,	PUNCT
eurjchem-942	105	19	c18	c18	NOUN
eurjchem-942	105	20	column	column	PROPN
eurjchem-942	105	21	.	.	PUNCT
eurjchem-942	106	1	mobile	mobile	ADJ
eurjchem-942	106	2	phase	phase	NOUN
eurjchem-942	106	3	,	,	PUNCT
eurjchem-942	106	4	water	water	NOUN
eurjchem-942	106	5	:	:	PUNCT
eurjchem-942	106	6	tetrahydrofuran	tetrahydrofuran	NOUN
eurjchem-942	106	7	(	(	PUNCT
eurjchem-942	106	8	4:1	4:1	NUM
eurjchem-942	106	9	,	,	PUNCT
eurjchem-942	106	10	v	v	NOUN
eurjchem-942	106	11	:	:	PUNCT
eurjchem-942	106	12	v	v	NOUN
eurjchem-942	106	13	)	)	PUNCT
eurjchem-942	106	14	.	.	PUNCT
eurjchem-942	107	1	the	the	DET
eurjchem-942	107	2	detection	detection	NOUN
eurjchem-942	107	3	was	be	AUX
eurjchem-942	107	4	monitored	monitor	VERB
eurjchem-942	107	5	at	at	ADP
eurjchem-942	107	6	215	215	NUM
eurjchem-942	107	7	nm	nm	NOUN
eurjchem-942	107	8	.	.	PUNCT
eurjchem-942	107	9	table	table	NOUN
eurjchem-942	107	10	4	4	NUM
eurjchem-942	107	11	.	.	PUNCT
eurjchem-942	108	1	determination	determination	NOUN
eurjchem-942	108	2	of	of	ADP
eurjchem-942	108	3	tamsulosin	tamsulosin	NOUN
eurjchem-942	108	4	and	and	CCONJ
eurjchem-942	108	5	finasteride	finasteride	ADV
eurjchem-942	108	6	in	in	ADP
eurjchem-942	108	7	laboratory	laboratory	NOUN
eurjchem-942	108	8	prepared	prepare	VERB
eurjchem-942	108	9	mixtures	mixture	NOUN
eurjchem-942	108	10	by	by	ADP
eurjchem-942	108	11	the	the	DET
eurjchem-942	108	12	proposed	propose	VERB
eurjchem-942	108	13	lc‐ms\ms	lc‐ms\ms	NOUN
eurjchem-942	108	14	method	method	NOUN
eurjchem-942	108	15	.	.	PUNCT
eurjchem-942	109	1	concentration	concentration	NOUN
eurjchem-942	109	2	(	(	PUNCT
eurjchem-942	109	3	ng	ng	NOUN
eurjchem-942	109	4	/	/	SYM
eurjchem-942	109	5	ml	ml	NOUN
eurjchem-942	109	6	)	)	PUNCT
eurjchem-942	109	7	%	%	NOUN
eurjchem-942	109	8	recovery	recovery	NOUN
eurjchem-942	109	9	*	*	PUNCT
eurjchem-942	109	10	tamsulosin	tamsulosin	VERB
eurjchem-942	109	11	finasteride	finasteride	ADJ
eurjchem-942	109	12	tamsulosin	tamsulosin	NOUN
eurjchem-942	109	13	finasteride	finasteride	ADV
eurjchem-942	109	14	30.00	30.00	NUM
eurjchem-942	109	15	30.00	30.00	NUM
eurjchem-942	109	16	101.04	101.04	NUM
eurjchem-942	109	17	97.95	97.95	NUM
eurjchem-942	109	18	30.00	30.00	NUM
eurjchem-942	109	19	60.00	60.00	NUM
eurjchem-942	109	20	100.45	100.45	NUM
eurjchem-942	109	21	98.06	98.06	NUM
eurjchem-942	109	22	40.00	40.00	NUM
eurjchem-942	109	23	20.00	20.00	NUM
eurjchem-942	109	24	99.76	99.76	NUM
eurjchem-942	109	25	99.95	99.95	NUM
eurjchem-942	109	26	10.00	10.00	NUM
eurjchem-942	109	27	125.00	125.00	NUM
eurjchem-942	109	28	100.35	100.35	NUM
eurjchem-942	109	29	99.55	99.55	NUM
eurjchem-942	109	30	30.00	30.00	NUM
eurjchem-942	109	31	375.00	375.00	NUM
eurjchem-942	109	32	98.76	98.76	NUM
eurjchem-942	109	33	100.09	100.09	NUM
eurjchem-942	109	34	20.00	20.00	NUM
eurjchem-942	109	35	200.00	200.00	NUM
eurjchem-942	109	36	100.59	100.59	NUM
eurjchem-942	109	37	98.50	98.50	NUM
eurjchem-942	109	38	mean	mean	NOUN
eurjchem-942	109	39	±	±	NUM
eurjchem-942	109	40	sd	sd	ADP
eurjchem-942	109	41	100.16±0.80	100.16±0.80	NUM
eurjchem-942	109	42	99.02±0.96	99.02±0.96	NUM
eurjchem-942	109	43	%	%	NOUN
eurjchem-942	109	44	rsd	rsd	PROPN
eurjchem-942	109	45	0.80	0.80	NUM
eurjchem-942	109	46	0.97	0.97	NUM
eurjchem-942	109	47	%	%	NOUN
eurjchem-942	109	48	rer	rer	PROPN
eurjchem-942	109	49	0.33	0.33	NUM
eurjchem-942	109	50	0.40	0.40	NUM
eurjchem-942	109	51	variance	variance	NOUN
eurjchem-942	109	52	0.64	0.64	NUM
eurjchem-942	109	53	0.93	0.93	NUM
eurjchem-942	109	54	*	*	PUNCT
eurjchem-942	109	55	average	average	NOUN
eurjchem-942	109	56	of	of	ADP
eurjchem-942	109	57	three	three	NUM
eurjchem-942	109	58	different	different	ADJ
eurjchem-942	109	59	determinations	determination	NOUN
eurjchem-942	109	60	.	.	PUNCT
eurjchem-942	110	1	statistical	statistical	ADJ
eurjchem-942	110	2	analysis	analysis	NOUN
eurjchem-942	110	3	[	[	X
eurjchem-942	110	4	28	28	NUM
eurjchem-942	110	5	]	]	PUNCT
eurjchem-942	110	6	obtained	obtain	VERB
eurjchem-942	110	7	by	by	ADP
eurjchem-942	110	8	the	the	DET
eurjchem-942	110	9	proposed	propose	VERB
eurjchem-942	110	10	and	and	CCONJ
eurjchem-942	110	11	reported	report	VERB
eurjchem-942	110	12	methods	method	NOUN
eurjchem-942	110	13	using	use	VERB
eurjchem-942	110	14	student´s	student´s	NOUN
eurjchem-942	110	15	t‐test	t‐test	PUNCT
eurjchem-942	110	16	and	and	CCONJ
eurjchem-942	110	17	variance	variance	NOUN
eurjchem-942	110	18	ratio	ratio	NOUN
eurjchem-942	110	19	f‐	f‐	PROPN
eurjchem-942	110	20	test	test	NOUN
eurjchem-942	110	21	,	,	PUNCT
eurjchem-942	110	22	showed	show	VERB
eurjchem-942	110	23	no	no	DET
eurjchem-942	110	24	significant	significant	ADJ
eurjchem-942	110	25	difference	difference	NOUN
eurjchem-942	110	26	between	between	ADP
eurjchem-942	110	27	the	the	DET
eurjchem-942	110	28	performance	performance	NOUN
eurjchem-942	110	29	of	of	ADP
eurjchem-942	110	30	the	the	DET
eurjchem-942	110	31	two	two	NUM
eurjchem-942	110	32	methods	method	NOUN
eurjchem-942	110	33	regarding	regard	VERB
eurjchem-942	110	34	the	the	DET
eurjchem-942	110	35	accuracy	accuracy	NOUN
eurjchem-942	110	36	and	and	CCONJ
eurjchem-942	110	37	precision	precision	NOUN
eurjchem-942	110	38	,	,	PUNCT
eurjchem-942	110	39	respectively	respectively	ADV
eurjchem-942	110	40	,	,	PUNCT
eurjchem-942	110	41	(	(	PUNCT
eurjchem-942	110	42	table	table	NOUN
eurjchem-942	110	43	3	3	NUM
eurjchem-942	110	44	)	)	PUNCT
eurjchem-942	110	45	.	.	PUNCT
eurjchem-942	111	1	in	in	ADP
eurjchem-942	111	2	addition	addition	NOUN
eurjchem-942	111	3	,	,	PUNCT
eurjchem-942	111	4	the	the	DET
eurjchem-942	111	5	intraday	intraday	NOUN
eurjchem-942	111	6	precision	precision	NOUN
eurjchem-942	111	7	was	be	AUX
eurjchem-942	111	8	evaluated	evaluate	VERB
eurjchem-942	111	9	through	through	ADP
eurjchem-942	111	10	replicate	replicate	VERB
eurjchem-942	111	11	analysis	analysis	NOUN
eurjchem-942	111	12	of	of	ADP
eurjchem-942	111	13	the	the	DET
eurjchem-942	111	14	standard	standard	ADJ
eurjchem-942	111	15	solutions	solution	NOUN
eurjchem-942	111	16	of	of	ADP
eurjchem-942	111	17	the	the	DET
eurjchem-942	111	18	drugs	drug	NOUN
eurjchem-942	111	19	.	.	PUNCT
eurjchem-942	112	1	however	however	ADV
eurjchem-942	112	2	,	,	PUNCT
eurjchem-942	112	3	the	the	DET
eurjchem-942	112	4	interday	interday	PROPN
eurjchem-942	112	5	precision	precision	NOUN
eurjchem-942	112	6	was	be	AUX
eurjchem-942	112	7	performed	perform	VERB
eurjchem-942	112	8	through	through	ADP
eurjchem-942	112	9	replicate	replicate	VERB
eurjchem-942	112	10	analysis	analysis	NOUN
eurjchem-942	112	11	of	of	ADP
eurjchem-942	112	12	the	the	DET
eurjchem-942	112	13	standard	standard	ADJ
eurjchem-942	112	14	solutions	solution	NOUN
eurjchem-942	112	15	of	of	ADP
eurjchem-942	112	16	the	the	DET
eurjchem-942	112	17	drugs	drug	NOUN
eurjchem-942	112	18	on	on	ADP
eurjchem-942	112	19	three	three	NUM
eurjchem-942	112	20	successive	successive	ADJ
eurjchem-942	112	21	days	day	NOUN
eurjchem-942	112	22	.	.	PUNCT
eurjchem-942	113	1	the	the	DET
eurjchem-942	113	2	percentage	percentage	NOUN
eurjchem-942	113	3	recoveries	recovery	NOUN
eurjchem-942	113	4	as	as	ADV
eurjchem-942	113	5	well	well	ADV
eurjchem-942	113	6	as	as	ADP
eurjchem-942	113	7	the	the	DET
eurjchem-942	113	8	percentage	percentage	NOUN
eurjchem-942	113	9	relative	relative	ADJ
eurjchem-942	113	10	standard	standard	ADJ
eurjchem-942	113	11	deviations	deviation	NOUN
eurjchem-942	113	12	were	be	AUX
eurjchem-942	113	13	calculated	calculate	VERB
eurjchem-942	113	14	as	as	SCONJ
eurjchem-942	113	15	abridged	abridge	VERB
eurjchem-942	113	16	in	in	ADP
eurjchem-942	113	17	table	table	NOUN
eurjchem-942	113	18	3	3	NUM
eurjchem-942	113	19	.	.	PUNCT
eurjchem-942	114	1	the	the	DET
eurjchem-942	114	2	repeatability	repeatability	NOUN
eurjchem-942	114	3	of	of	ADP
eurjchem-942	114	4	the	the	DET
eurjchem-942	114	5	proposed	propose	VERB
eurjchem-942	114	6	method	method	NOUN
eurjchem-942	114	7	is	be	AUX
eurjchem-942	114	8	good	good	ADJ
eurjchem-942	114	9	as	as	SCONJ
eurjchem-942	114	10	indicated	indicate	VERB
eurjchem-942	114	11	by	by	ADP
eurjchem-942	114	12	small	small	ADJ
eurjchem-942	114	13	value	value	NOUN
eurjchem-942	114	14	of	of	ADP
eurjchem-942	114	15	standard	standard	ADJ
eurjchem-942	114	16	deviation	deviation	NOUN
eurjchem-942	114	17	(	(	PUNCT
eurjchem-942	114	18	sd	sd	NOUN
eurjchem-942	114	19	)	)	PUNCT
eurjchem-942	114	20	.	.	PUNCT
eurjchem-942	115	1	3.1.3	3.1.3	X
eurjchem-942	115	2	.	.	PUNCT
eurjchem-942	115	3	limit	limit	NOUN
eurjchem-942	115	4	of	of	ADP
eurjchem-942	115	5	detection	detection	NOUN
eurjchem-942	115	6	(	(	PUNCT
eurjchem-942	115	7	lod	lod	PROPN
eurjchem-942	115	8	)	)	PUNCT
eurjchem-942	115	9	and	and	CCONJ
eurjchem-942	115	10	limit	limit	NOUN
eurjchem-942	115	11	of	of	ADP
eurjchem-942	115	12	quantification	quantification	NOUN
eurjchem-942	115	13	(	(	PUNCT
eurjchem-942	115	14	loq	loq	PROPN
eurjchem-942	115	15	)	)	PUNCT
eurjchem-942	115	16	the	the	DET
eurjchem-942	115	17	limit	limit	NOUN
eurjchem-942	115	18	of	of	ADP
eurjchem-942	115	19	quantification	quantification	NOUN
eurjchem-942	115	20	(	(	PUNCT
eurjchem-942	115	21	loq	loq	PROPN
eurjchem-942	115	22	)	)	PUNCT
eurjchem-942	115	23	was	be	AUX
eurjchem-942	115	24	determined	determine	VERB
eurjchem-942	115	25	by	by	ADP
eurjchem-942	115	26	establishing	establish	VERB
eurjchem-942	115	27	the	the	DET
eurjchem-942	115	28	lowest	low	ADJ
eurjchem-942	115	29	concentration	concentration	NOUN
eurjchem-942	115	30	that	that	PRON
eurjchem-942	115	31	can	can	AUX
eurjchem-942	115	32	be	be	AUX
eurjchem-942	115	33	measured	measure	VERB
eurjchem-942	115	34	according	accord	VERB
eurjchem-942	115	35	to	to	ADP
eurjchem-942	115	36	usp	usp	NOUN
eurjchem-942	115	37	34	34	NUM
eurjchem-942	115	38	recommendations	recommendation	NOUN
eurjchem-942	115	39	,	,	PUNCT
eurjchem-942	115	40	below	below	ADP
eurjchem-942	115	41	which	which	PRON
eurjchem-942	115	42	the	the	DET
eurjchem-942	115	43	calibration	calibration	NOUN
eurjchem-942	115	44	graph	graph	NOUN
eurjchem-942	115	45	is	be	AUX
eurjchem-942	115	46	nonlinear	nonlinear	ADJ
eurjchem-942	115	47	and	and	CCONJ
eurjchem-942	115	48	was	be	AUX
eurjchem-942	115	49	found	find	VERB
eurjchem-942	115	50	to	to	PART
eurjchem-942	115	51	be	be	AUX
eurjchem-942	115	52	1.6	1.6	NUM
eurjchem-942	115	53	ng	ng	NOUN
eurjchem-942	115	54	/	/	SYM
eurjchem-942	115	55	ml	ml	X
eurjchem-942	115	56	for	for	ADP
eurjchem-942	115	57	tam	tam	NOUN
eurjchem-942	115	58	and	and	CCONJ
eurjchem-942	115	59	20.0	20.0	NUM
eurjchem-942	115	60	ng	ng	NOUN
eurjchem-942	115	61	/	/	SYM
eurjchem-942	115	62	ml	ml	X
eurjchem-942	115	63	for	for	ADP
eurjchem-942	115	64	fin	fin	NOUN
eurjchem-942	115	65	.	.	PUNCT
eurjchem-942	116	1	the	the	DET
eurjchem-942	116	2	limit	limit	NOUN
eurjchem-942	116	3	of	of	ADP
eurjchem-942	116	4	detection	detection	NOUN
eurjchem-942	116	5	(	(	PUNCT
eurjchem-942	116	6	lod	lod	PROPN
eurjchem-942	116	7	)	)	PUNCT
eurjchem-942	116	8	was	be	AUX
eurjchem-942	116	9	determined	determine	VERB
eurjchem-942	116	10	by	by	ADP
eurjchem-942	116	11	evaluating	evaluate	VERB
eurjchem-942	116	12	the	the	DET
eurjchem-942	116	13	lowest	low	ADJ
eurjchem-942	116	14	concentration	concentration	NOUN
eurjchem-942	116	15	of	of	ADP
eurjchem-942	116	16	the	the	DET
eurjchem-942	116	17	analyte	analyte	NOUN
eurjchem-942	116	18	that	that	PRON
eurjchem-942	116	19	can	can	AUX
eurjchem-942	116	20	be	be	AUX
eurjchem-942	116	21	readily	readily	ADV
eurjchem-942	116	22	detected	detect	VERB
eurjchem-942	116	23	and	and	CCONJ
eurjchem-942	116	24	was	be	AUX
eurjchem-942	116	25	found	find	VERB
eurjchem-942	116	26	to	to	PART
eurjchem-942	116	27	be	be	AUX
eurjchem-942	116	28	0.5	0.5	NUM
eurjchem-942	116	29	ng	ng	NOUN
eurjchem-942	116	30	/	/	SYM
eurjchem-942	116	31	ml	ml	X
eurjchem-942	116	32	for	for	ADP
eurjchem-942	116	33	tam	tam	NOUN
eurjchem-942	116	34	and	and	CCONJ
eurjchem-942	116	35	5.0	5.0	NUM
eurjchem-942	116	36	ng	ng	NOUN
eurjchem-942	116	37	/	/	SYM
eurjchem-942	116	38	ml	ml	X
eurjchem-942	116	39	for	for	ADP
eurjchem-942	116	40	fin	fin	NOUN
eurjchem-942	116	41	.	.	PUNCT
eurjchem-942	117	1	3.1.4	3.1.4	NUM
eurjchem-942	117	2	.	.	PUNCT
eurjchem-942	118	1	robustness	robustness	NOUN
eurjchem-942	118	2	of	of	ADP
eurjchem-942	118	3	the	the	DET
eurjchem-942	118	4	method	method	NOUN
eurjchem-942	118	5	the	the	DET
eurjchem-942	118	6	robustness	robustness	NOUN
eurjchem-942	118	7	of	of	ADP
eurjchem-942	118	8	the	the	DET
eurjchem-942	118	9	method	method	NOUN
eurjchem-942	118	10	adopted	adopt	VERB
eurjchem-942	118	11	was	be	AUX
eurjchem-942	118	12	demonstrated	demonstrate	VERB
eurjchem-942	118	13	by	by	ADP
eurjchem-942	118	14	the	the	DET
eurjchem-942	118	15	consistency	consistency	NOUN
eurjchem-942	118	16	of	of	ADP
eurjchem-942	118	17	the	the	DET
eurjchem-942	118	18	relative	relative	ADJ
eurjchem-942	118	19	peak	peak	NOUN
eurjchem-942	118	20	area	area	NOUN
eurjchem-942	118	21	values	value	NOUN
eurjchem-942	118	22	with	with	ADP
eurjchem-942	118	23	the	the	DET
eurjchem-942	118	24	deliberately	deliberately	ADV
eurjchem-942	118	25	minor	minor	ADJ
eurjchem-942	118	26	changes	change	NOUN
eurjchem-942	118	27	in	in	ADP
eurjchem-942	118	28	the	the	DET
eurjchem-942	118	29	chromatographic	chromatographic	ADJ
eurjchem-942	118	30	and	and	CCONJ
eurjchem-942	118	31	mass	mass	ADJ
eurjchem-942	118	32	spectrometric	spectrometric	ADJ
eurjchem-942	118	33	parameters	parameter	NOUN
eurjchem-942	118	34	,	,	PUNCT
eurjchem-942	118	35	e.g.	e.g.	ADV
eurjchem-942	118	36	the	the	DET
eurjchem-942	118	37	ph	ph	NOUN
eurjchem-942	118	38	of	of	ADP
eurjchem-942	118	39	the	the	DET
eurjchem-942	118	40	buffer	buffer	NOUN
eurjchem-942	118	41	(	(	PUNCT
eurjchem-942	118	42	±0.5	±0.5	PROPN
eurjchem-942	118	43	)	)	PUNCT
eurjchem-942	118	44	,	,	PUNCT
eurjchem-942	118	45	the	the	DET
eurjchem-942	118	46	turbo	turbo	NOUN
eurjchem-942	118	47	ion	ion	NOUN
eurjchem-942	118	48	spray	spray	NOUN
eurjchem-942	118	49	temperature	temperature	NOUN
eurjchem-942	118	50	or	or	CCONJ
eurjchem-942	118	51	capillary	capillary	ADJ
eurjchem-942	118	52	temperature	temperature	NOUN
eurjchem-942	118	53	(	(	PUNCT
eurjchem-942	118	54	±5	±5	VERB
eurjchem-942	118	55	°	°	NOUN
eurjchem-942	118	56	c	c	NOUN
eurjchem-942	118	57	)	)	PUNCT
eurjchem-942	118	58	,	,	PUNCT
eurjchem-942	118	59	sheath	sheath	NOUN
eurjchem-942	118	60	gas	gas	NOUN
eurjchem-942	118	61	flow	flow	NOUN
eurjchem-942	118	62	(	(	PUNCT
eurjchem-942	118	63	±5	±5	NOUN
eurjchem-942	118	64	psi	psi	NOUN
eurjchem-942	118	65	)	)	PUNCT
eurjchem-942	118	66	and	and	CCONJ
eurjchem-942	118	67	collision	collision	VERB
eurjchem-942	118	68	energy	energy	NOUN
eurjchem-942	118	69	(	(	PUNCT
eurjchem-942	118	70	±5	±5	NOUN
eurjchem-942	118	71	v	v	NOUN
eurjchem-942	118	72	)	)	PUNCT
eurjchem-942	118	73	.	.	PUNCT
eurjchem-942	119	1	3.2	3.2	NUM
eurjchem-942	119	2	.	.	PUNCT
eurjchem-942	119	3	application	application	NOUN
eurjchem-942	119	4	of	of	ADP
eurjchem-942	119	5	the	the	DET
eurjchem-942	119	6	proposed	propose	VERB
eurjchem-942	119	7	method	method	NOUN
eurjchem-942	119	8	the	the	DET
eurjchem-942	119	9	proposed	propose	VERB
eurjchem-942	119	10	method	method	NOUN
eurjchem-942	119	11	was	be	AUX
eurjchem-942	119	12	successfully	successfully	ADV
eurjchem-942	119	13	applied	apply	VERB
eurjchem-942	119	14	to	to	ADP
eurjchem-942	119	15	the	the	DET
eurjchem-942	119	16	analysis	analysis	NOUN
eurjchem-942	119	17	of	of	ADP
eurjchem-942	119	18	tam	tam	NOUN
eurjchem-942	119	19	and	and	CCONJ
eurjchem-942	119	20	fin	fin	NOUN
eurjchem-942	119	21	in	in	ADP
eurjchem-942	119	22	laboratory	laboratory	NOUN
eurjchem-942	119	23	prepared	prepare	VERB
eurjchem-942	119	24	mixtures	mixture	NOUN
eurjchem-942	119	25	containing	contain	VERB
eurjchem-942	119	26	both	both	DET
eurjchem-942	119	27	drugs	drug	NOUN
eurjchem-942	119	28	in	in	ADP
eurjchem-942	119	29	different	different	ADJ
eurjchem-942	119	30	ratios	ratio	NOUN
eurjchem-942	119	31	.	.	PUNCT
eurjchem-942	120	1	the	the	DET
eurjchem-942	120	2	average	average	ADJ
eurjchem-942	120	3	percent	percent	NOUN
eurjchem-942	120	4	recoveries	recovery	NOUN
eurjchem-942	120	5	were	be	AUX
eurjchem-942	120	6	based	base	VERB
eurjchem-942	120	7	on	on	ADP
eurjchem-942	120	8	the	the	DET
eurjchem-942	120	9	average	average	NOUN
eurjchem-942	120	10	of	of	ADP
eurjchem-942	120	11	three	three	NUM
eurjchem-942	120	12	replicate	replicate	ADJ
eurjchem-942	120	13	determinations	determination	NOUN
eurjchem-942	120	14	(	(	PUNCT
eurjchem-942	120	15	table	table	NOUN
eurjchem-942	120	16	4	4	NUM
eurjchem-942	120	17	)	)	PUNCT
eurjchem-942	120	18	.	.	PUNCT
eurjchem-942	121	1	to	to	PART
eurjchem-942	121	2	indicate	indicate	VERB
eurjchem-942	121	3	the	the	DET
eurjchem-942	121	4	potential	potential	NOUN
eurjchem-942	121	5	of	of	ADP
eurjchem-942	121	6	lc‐ms	lc‐ms	NOUN
eurjchem-942	121	7	for	for	ADP
eurjchem-942	121	8	quality	quality	NOUN
eurjchem-942	121	9	control	control	NOUN
eurjchem-942	121	10	and	and	CCONJ
eurjchem-942	121	11	routine	routine	ADJ
eurjchem-942	121	12	analysis	analysis	NOUN
eurjchem-942	121	13	of	of	ADP
eurjchem-942	121	14	tam	tam	NOUN
eurjchem-942	121	15	and	and	CCONJ
eurjchem-942	121	16	fin	fin	NOUN
eurjchem-942	121	17	in	in	ADP
eurjchem-942	121	18	pharmaceutical	pharmaceutical	ADJ
eurjchem-942	121	19	formulation	formulation	NOUN
eurjchem-942	121	20	;	;	PUNCT
eurjchem-942	121	21	urimax	urimax	PROPN
eurjchem-942	121	22	f	f	PROPN
eurjchem-942	121	23	tablets	tablet	NOUN
eurjchem-942	121	24	were	be	AUX
eurjchem-942	121	25	analyzed	analyze	VERB
eurjchem-942	121	26	.	.	PUNCT
eurjchem-942	122	1	mohamed	mohamed	PROPN
eurjchem-942	122	2	et	et	PROPN
eurjchem-942	122	3	al	al	PROPN
eurjchem-942	122	4	.	.	PUNCT
eurjchem-942	122	5	/	/	SYM
eurjchem-942	122	6	european	european	PROPN
eurjchem-942	122	7	journal	journal	PROPN
eurjchem-942	122	8	of	of	ADP
eurjchem-942	122	9	chemistry	chemistry	NOUN
eurjchem-942	122	10	5	5	NUM
eurjchem-942	122	11	(	(	PUNCT
eurjchem-942	122	12	1	1	NUM
eurjchem-942	122	13	)	)	PUNCT
eurjchem-942	122	14	(	(	PUNCT
eurjchem-942	122	15	2014	2014	NUM
eurjchem-942	122	16	)	)	PUNCT
eurjchem-942	122	17	181‐185	181‐185	NUM
eurjchem-942	122	18	185	185	NUM
eurjchem-942	122	19	table	table	NOUN
eurjchem-942	122	20	5	5	NUM
eurjchem-942	122	21	.	.	PUNCT
eurjchem-942	122	22	application	application	NOUN
eurjchem-942	122	23	of	of	ADP
eurjchem-942	122	24	standard	standard	ADJ
eurjchem-942	122	25	addition	addition	NOUN
eurjchem-942	122	26	technique	technique	NOUN
eurjchem-942	122	27	for	for	ADP
eurjchem-942	122	28	the	the	DET
eurjchem-942	122	29	determination	determination	NOUN
eurjchem-942	122	30	of	of	ADP
eurjchem-942	122	31	tamsulosin	tamsulosin	NOUN
eurjchem-942	122	32	and	and	CCONJ
eurjchem-942	122	33	finasteride	finasteride	ADJ
eurjchem-942	122	34	in	in	ADP
eurjchem-942	122	35	pharmaceutical	pharmaceutical	ADJ
eurjchem-942	122	36	formulation	formulation	NOUN
eurjchem-942	122	37	a.	a.	NOUN
eurjchem-942	122	38	item	item	NOUN
eurjchem-942	122	39	taken	take	VERB
eurjchem-942	122	40	concentration	concentration	NOUN
eurjchem-942	122	41	(	(	PUNCT
eurjchem-942	122	42	ng	ng	NOUN
eurjchem-942	122	43	/	/	SYM
eurjchem-942	122	44	ml	ml	PROPN
eurjchem-942	122	45	)	)	PUNCT
eurjchem-942	122	46	added	add	VERB
eurjchem-942	122	47	concentration	concentration	NOUN
eurjchem-942	122	48	(	(	PUNCT
eurjchem-942	122	49	ng	ng	NOUN
eurjchem-942	122	50	/	/	SYM
eurjchem-942	122	51	ml	ml	NOUN
eurjchem-942	122	52	)	)	PUNCT
eurjchem-942	122	53	%	%	NOUN
eurjchem-942	123	1	recovery	recovery	NOUN
eurjchem-942	123	2	b	b	PROPN
eurjchem-942	123	3	tamsulosin	tamsulosin	VERB
eurjchem-942	123	4	finasteride	finasteride	ADJ
eurjchem-942	123	5	tamsulosin	tamsulosin	NOUN
eurjchem-942	123	6	finasteride	finasteride	ADJ
eurjchem-942	123	7	tamsulosin	tamsulosin	NOUN
eurjchem-942	123	8	finasteride	finasteride	ADV
eurjchem-942	123	9	5.00	5.00	NUM
eurjchem-942	123	10	62.50	62.50	NUM
eurjchem-942	123	11	5.00	5.00	NUM
eurjchem-942	123	12	62.50	62.50	NUM
eurjchem-942	123	13	99.95	99.95	NUM
eurjchem-942	123	14	98.89	98.89	NUM
eurjchem-942	123	15	5.00	5.00	NUM
eurjchem-942	123	16	62.50	62.50	NUM
eurjchem-942	123	17	10.00	10.00	NUM
eurjchem-942	123	18	125.00	125.00	NUM
eurjchem-942	123	19	99.99	99.99	NUM
eurjchem-942	123	20	98.54	98.54	NUM
eurjchem-942	123	21	5.00	5.00	NUM
eurjchem-942	123	22	62.50	62.50	NUM
eurjchem-942	123	23	15.00	15.00	NUM
eurjchem-942	123	24	187.50	187.50	NUM
eurjchem-942	123	25	98.16	98.16	NUM
eurjchem-942	123	26	98.24	98.24	NUM
eurjchem-942	123	27	5.00	5.00	NUM
eurjchem-942	123	28	62.50	62.50	NUM
eurjchem-942	123	29	20.00	20.00	NUM
eurjchem-942	123	30	250.00	250.00	NUM
eurjchem-942	123	31	99.00	99.00	NUM
eurjchem-942	123	32	97.98	97.98	NUM
eurjchem-942	123	33	5.00	5.00	NUM
eurjchem-942	123	34	62.50	62.50	NUM
eurjchem-942	123	35	25.00	25.00	NUM
eurjchem-942	123	36	312.50	312.50	NUM
eurjchem-942	123	37	98.85	98.85	NUM
eurjchem-942	123	38	99.69	99.69	NUM
eurjchem-942	123	39	5.00	5.00	NUM
eurjchem-942	123	40	62.50	62.50	NUM
eurjchem-942	123	41	30.00	30.00	NUM
eurjchem-942	123	42	375.00	375.00	NUM
eurjchem-942	123	43	98.05	98.05	NUM
eurjchem-942	123	44	97.00	97.00	NUM
eurjchem-942	123	45	mean	mean	NOUN
eurjchem-942	123	46	±	±	NUM
eurjchem-942	123	47	sd	sd	ADP
eurjchem-942	123	48	98.76±0.78	98.76±0.78	NUM
eurjchem-942	123	49	98.12±0.89	98.12±0.89	NUM
eurjchem-942	123	50	99.00±0.84	99.00±0.84	NUM
eurjchem-942	123	51	98.39±0.90	98.39±0.90	NUM
eurjchem-942	123	52	%	%	NOUN
eurjchem-942	123	53	rsd	rsd	NOUN
eurjchem-942	123	54	0.79	0.79	NUM
eurjchem-942	123	55	0.91	0.91	NUM
eurjchem-942	123	56	0.85	0.85	NUM
eurjchem-942	123	57	0.92	0.92	NUM
eurjchem-942	123	58	%	%	NOUN
eurjchem-942	123	59	rer	rer	X
eurjchem-942	123	60	0.32	0.32	NUM
eurjchem-942	123	61	0.37	0.37	NUM
eurjchem-942	123	62	0.35	0.35	NUM
eurjchem-942	123	63	0.37	0.37	NUM
eurjchem-942	123	64	variance	variance	NOUN
eurjchem-942	123	65	0.61	0.61	NUM
eurjchem-942	123	66	0.79	0.79	NUM
eurjchem-942	123	67	0.70	0.70	NUM
eurjchem-942	123	68	0.82	0.82	NUM
eurjchem-942	123	69	a	a	DET
eurjchem-942	123	70	sd	sd	NOUN
eurjchem-942	123	71	:	:	PUNCT
eurjchem-942	123	72	standard	standard	ADJ
eurjchem-942	123	73	deviation	deviation	NOUN
eurjchem-942	123	74	,	,	PUNCT
eurjchem-942	123	75	%	%	PUNCT
eurjchem-942	123	76	rsd	rsd	NOUN
eurjchem-942	123	77	:	:	PUNCT
eurjchem-942	123	78	percent	percent	NOUN
eurjchem-942	123	79	relative	relative	ADJ
eurjchem-942	123	80	standard	standard	ADJ
eurjchem-942	123	81	deviation	deviation	NOUN
eurjchem-942	123	82	,	,	PUNCT
eurjchem-942	123	83	%	%	INTJ
eurjchem-942	123	84	rer	rer	X
eurjchem-942	123	85	:	:	PUNCT
eurjchem-942	123	86	percent	percent	NOUN
eurjchem-942	123	87	relative	relative	ADJ
eurjchem-942	123	88	standard	standard	ADJ
eurjchem-942	123	89	error	error	NOUN
eurjchem-942	123	90	.	.	PUNCT
eurjchem-942	124	1	b	b	NOUN
eurjchem-942	124	2	average	average	NOUN
eurjchem-942	124	3	of	of	ADP
eurjchem-942	124	4	three	three	NUM
eurjchem-942	124	5	different	different	ADJ
eurjchem-942	124	6	determinations	determination	NOUN
eurjchem-942	124	7	.	.	PUNCT
eurjchem-942	125	1	the	the	DET
eurjchem-942	125	2	concentrations	concentration	NOUN
eurjchem-942	125	3	of	of	ADP
eurjchem-942	125	4	the	the	DET
eurjchem-942	125	5	drugs	drug	NOUN
eurjchem-942	125	6	were	be	AUX
eurjchem-942	125	7	calculated	calculate	VERB
eurjchem-942	125	8	referring	refer	VERB
eurjchem-942	125	9	to	to	ADP
eurjchem-942	125	10	the	the	DET
eurjchem-942	125	11	corresponding	corresponding	ADJ
eurjchem-942	125	12	regression	regression	NOUN
eurjchem-942	125	13	equation	equation	NOUN
eurjchem-942	125	14	.	.	PUNCT
eurjchem-942	126	1	the	the	DET
eurjchem-942	126	2	coupling	coupling	NOUN
eurjchem-942	126	3	of	of	ADP
eurjchem-942	126	4	lc	lc	PROPN
eurjchem-942	126	5	with	with	ADP
eurjchem-942	126	6	ms	ms	PROPN
eurjchem-942	126	7	/	/	SYM
eurjchem-942	126	8	ms	ms	PROPN
eurjchem-942	126	9	detection	detection	NOUN
eurjchem-942	126	10	in	in	ADP
eurjchem-942	126	11	the	the	DET
eurjchem-942	126	12	srm	srm	PROPN
eurjchem-942	126	13	mode	mode	NOUN
eurjchem-942	126	14	showed	show	VERB
eurjchem-942	126	15	high	high	ADJ
eurjchem-942	126	16	specificity	specificity	NOUN
eurjchem-942	126	17	,	,	PUNCT
eurjchem-942	126	18	because	because	SCONJ
eurjchem-942	126	19	only	only	ADV
eurjchem-942	126	20	the	the	DET
eurjchem-942	126	21	ions	ion	NOUN
eurjchem-942	126	22	derived	derive	VERB
eurjchem-942	126	23	from	from	ADP
eurjchem-942	126	24	the	the	DET
eurjchem-942	126	25	analytes	analyte	NOUN
eurjchem-942	126	26	of	of	ADP
eurjchem-942	126	27	interest	interest	NOUN
eurjchem-942	126	28	were	be	AUX
eurjchem-942	126	29	monitored	monitor	VERB
eurjchem-942	126	30	,	,	PUNCT
eurjchem-942	126	31	thus	thus	ADV
eurjchem-942	126	32	,	,	PUNCT
eurjchem-942	126	33	commonly	commonly	ADV
eurjchem-942	126	34	used	use	VERB
eurjchem-942	126	35	tablet	tablet	NOUN
eurjchem-942	126	36	excipients	excipient	NOUN
eurjchem-942	126	37	did	do	AUX
eurjchem-942	126	38	not	not	PART
eurjchem-942	126	39	interfere	interfere	VERB
eurjchem-942	126	40	in	in	ADP
eurjchem-942	126	41	the	the	DET
eurjchem-942	126	42	analysis	analysis	NOUN
eurjchem-942	126	43	as	as	SCONJ
eurjchem-942	126	44	indicated	indicate	VERB
eurjchem-942	126	45	by	by	ADP
eurjchem-942	126	46	the	the	DET
eurjchem-942	126	47	percentages	percentage	NOUN
eurjchem-942	126	48	found	find	VERB
eurjchem-942	126	49	.	.	PUNCT
eurjchem-942	127	1	the	the	DET
eurjchem-942	127	2	results	result	NOUN
eurjchem-942	127	3	obtained	obtain	VERB
eurjchem-942	127	4	by	by	ADP
eurjchem-942	127	5	applying	apply	VERB
eurjchem-942	127	6	the	the	DET
eurjchem-942	127	7	standard	standard	ADJ
eurjchem-942	127	8	addition	addition	NOUN
eurjchem-942	127	9	technique	technique	NOUN
eurjchem-942	127	10	are	be	AUX
eurjchem-942	127	11	abridged	abridge	VERB
eurjchem-942	127	12	in	in	ADP
eurjchem-942	127	13	table	table	NOUN
eurjchem-942	127	14	5	5	NUM
eurjchem-942	127	15	.	.	NOUN
eurjchem-942	128	1	4	4	NUM
eurjchem-942	128	2	.	.	X
eurjchem-942	128	3	conclusion	conclusion	NOUN
eurjchem-942	128	4	a	a	DET
eurjchem-942	128	5	rapid	rapid	ADJ
eurjchem-942	128	6	and	and	CCONJ
eurjchem-942	128	7	precise	precise	ADJ
eurjchem-942	128	8	liquid	liquid	ADJ
eurjchem-942	128	9	chromatography	chromatography	NOUN
eurjchem-942	128	10	with	with	ADP
eurjchem-942	128	11	electrospray	electrospray	ADJ
eurjchem-942	128	12	ionization	ionization	NOUN
eurjchem-942	128	13	tandem	tandem	NOUN
eurjchem-942	128	14	mass	mass	ADJ
eurjchem-942	128	15	spectrometry	spectrometry	NOUN
eurjchem-942	128	16	method	method	NOUN
eurjchem-942	128	17	for	for	ADP
eurjchem-942	128	18	the	the	DET
eurjchem-942	128	19	determination	determination	NOUN
eurjchem-942	128	20	of	of	ADP
eurjchem-942	128	21	tamsulosin	tamsulosin	NOUN
eurjchem-942	128	22	and	and	CCONJ
eurjchem-942	128	23	finasteride	finasteride	ADJ
eurjchem-942	128	24	in	in	ADP
eurjchem-942	128	25	bulk	bulk	ADJ
eurjchem-942	128	26	powders	powder	NOUN
eurjchem-942	128	27	and	and	CCONJ
eurjchem-942	128	28	in	in	ADP
eurjchem-942	128	29	pharmaceutical	pharmaceutical	ADJ
eurjchem-942	128	30	formulation	formulation	NOUN
eurjchem-942	128	31	was	be	AUX
eurjchem-942	128	32	developed	develop	VERB
eurjchem-942	128	33	and	and	CCONJ
eurjchem-942	128	34	validated	validate	VERB
eurjchem-942	128	35	.	.	PUNCT
eurjchem-942	129	1	the	the	DET
eurjchem-942	129	2	method	method	NOUN
eurjchem-942	129	3	offers	offer	VERB
eurjchem-942	129	4	several	several	ADJ
eurjchem-942	129	5	advantages	advantage	NOUN
eurjchem-942	129	6	such	such	ADJ
eurjchem-942	129	7	as	as	ADP
eurjchem-942	129	8	unnecessary	unnecessary	ADJ
eurjchem-942	129	9	complete	complete	ADJ
eurjchem-942	129	10	separation	separation	NOUN
eurjchem-942	129	11	of	of	ADP
eurjchem-942	129	12	analytes	analyte	NOUN
eurjchem-942	129	13	,	,	PUNCT
eurjchem-942	129	14	non‐tedious	non‐tedious	ADJ
eurjchem-942	129	15	sample	sample	NOUN
eurjchem-942	129	16	preparation	preparation	NOUN
eurjchem-942	129	17	.	.	PUNCT
eurjchem-942	130	1	in	in	ADP
eurjchem-942	130	2	addition	addition	NOUN
eurjchem-942	130	3	,	,	PUNCT
eurjchem-942	130	4	the	the	DET
eurjchem-942	130	5	short	short	ADJ
eurjchem-942	130	6	run	run	NOUN
eurjchem-942	130	7	time	time	NOUN
eurjchem-942	130	8	and	and	CCONJ
eurjchem-942	130	9	the	the	DET
eurjchem-942	130	10	relatively	relatively	ADV
eurjchem-942	130	11	low	low	ADJ
eurjchem-942	130	12	flow	flow	NOUN
eurjchem-942	130	13	rate	rate	NOUN
eurjchem-942	130	14	allows	allow	VERB
eurjchem-942	130	15	the	the	DET
eurjchem-942	130	16	analysis	analysis	NOUN
eurjchem-942	130	17	of	of	ADP
eurjchem-942	130	18	a	a	DET
eurjchem-942	130	19	large	large	ADJ
eurjchem-942	130	20	number	number	NOUN
eurjchem-942	130	21	of	of	ADP
eurjchem-942	130	22	samples	sample	NOUN
eurjchem-942	130	23	with	with	ADP
eurjchem-942	130	24	less	less	ADJ
eurjchem-942	130	25	mobile	mobile	ADJ
eurjchem-942	130	26	phase	phase	NOUN
eurjchem-942	130	27	that	that	PRON
eurjchem-942	130	28	proves	prove	VERB
eurjchem-942	130	29	to	to	PART
eurjchem-942	130	30	be	be	AUX
eurjchem-942	130	31	cost	cost	NOUN
eurjchem-942	130	32	effective	effective	ADJ
eurjchem-942	130	33	.	.	PUNCT
eurjchem-942	131	1	the	the	DET
eurjchem-942	131	2	data	data	PROPN
eurjchem-942	131	3	validation	validation	NOUN
eurjchem-942	131	4	shows	show	VERB
eurjchem-942	131	5	that	that	SCONJ
eurjchem-942	131	6	the	the	DET
eurjchem-942	131	7	optimized	optimize	VERB
eurjchem-942	131	8	lc‐ms	lc‐ms	AUX
eurjchem-942	131	9	/	/	SYM
eurjchem-942	131	10	ms	ms	PROPN
eurjchem-942	131	11	possess	possess	NOUN
eurjchem-942	131	12	specificity	specificity	NOUN
eurjchem-942	131	13	,	,	PUNCT
eurjchem-942	131	14	sensitivity	sensitivity	NOUN
eurjchem-942	131	15	,	,	PUNCT
eurjchem-942	131	16	linearity	linearity	NOUN
eurjchem-942	131	17	,	,	PUNCT
eurjchem-942	131	18	precision	precision	NOUN
eurjchem-942	131	19	and	and	CCONJ
eurjchem-942	131	20	accuracy	accuracy	NOUN
eurjchem-942	131	21	,	,	PUNCT
eurjchem-942	131	22	thus	thus	ADV
eurjchem-942	131	23	,	,	PUNCT
eurjchem-942	131	24	the	the	DET
eurjchem-942	131	25	proposed	propose	VERB
eurjchem-942	131	26	method	method	NOUN
eurjchem-942	131	27	can	can	AUX
eurjchem-942	131	28	be	be	AUX
eurjchem-942	131	29	used	use	VERB
eurjchem-942	131	30	for	for	ADP
eurjchem-942	131	31	the	the	DET
eurjchem-942	131	32	routine	routine	ADJ
eurjchem-942	131	33	analysis	analysis	NOUN
eurjchem-942	131	34	of	of	ADP
eurjchem-942	131	35	tamsulosin	tamsulosin	NOUN
eurjchem-942	131	36	and	and	CCONJ
eurjchem-942	131	37	finasteride	finasteride	ADJ
eurjchem-942	131	38	in	in	ADP
eurjchem-942	131	39	pharmaceutical	pharmaceutical	ADJ
eurjchem-942	131	40	dosage	dosage	NOUN
eurjchem-942	131	41	forms	form	NOUN
eurjchem-942	131	42	.	.	PUNCT
eurjchem-942	132	1	references	reference	NOUN
eurjchem-942	132	2	[	[	X
eurjchem-942	132	3	1	1	NUM
eurjchem-942	132	4	]	]	PUNCT
eurjchem-942	132	5	.	.	PUNCT
eurjchem-942	133	1	dunn	dunn	PROPN
eurjchem-942	133	2	,	,	PUNCT
eurjchem-942	133	3	c.	c.	PROPN
eurjchem-942	133	4	j.	j.	PROPN
eurjchem-942	133	5	;	;	PUNCT
eurjchem-942	133	6	matheson	matheson	PROPN
eurjchem-942	133	7	,	,	PUNCT
eurjchem-942	133	8	a.	a.	NOUN
eurjchem-942	133	9	;	;	PUNCT
eurjchem-942	133	10	faulds	fauld	NOUN
eurjchem-942	133	11	,	,	PUNCT
eurjchem-942	133	12	d.	d.	PROPN
eurjchem-942	133	13	m.	m.	NOUN
eurjchem-942	133	14	drugs	drug	NOUN
eurjchem-942	133	15	aging	age	VERB
eurjchem-942	133	16	2002	2002	NUM
eurjchem-942	133	17	,	,	PUNCT
eurjchem-942	133	18	19	19	NUM
eurjchem-942	133	19	,	,	PUNCT
eurjchem-942	133	20	135‐161	135‐161	NUM
eurjchem-942	133	21	.	.	PUNCT
eurjchem-942	134	1	[	[	X
eurjchem-942	134	2	2	2	NUM
eurjchem-942	134	3	]	]	PUNCT
eurjchem-942	134	4	.	.	PUNCT
eurjchem-942	134	5	narayan	narayan	PROPN
eurjchem-942	134	6	,	,	PUNCT
eurjchem-942	134	7	p.	p.	NOUN
eurjchem-942	134	8	;	;	PUNCT
eurjchem-942	134	9	rao	rao	PROPN
eurjchem-942	134	10	,	,	PUNCT
eurjchem-942	134	11	t.	t.	PROPN
eurjchem-942	134	12	h.	h.	PROPN
eurjchem-942	134	13	s.	s.	PROPN
eurjchem-942	134	14	g.	g.	PROPN
eurjchem-942	134	15	rev	rev	PROPN
eurjchem-942	134	16	.	.	PROPN
eurjchem-942	134	17	urol	urol	PROPN
eurjchem-942	134	18	.	.	PROPN
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eurjchem-942	135	2	,	,	PUNCT
eurjchem-942	135	3	7	7	NUM
eurjchem-942	135	4	,	,	PUNCT
eurjchem-942	135	5	42‐48	42‐48	NUM
eurjchem-942	135	6	.	.	PUNCT
eurjchem-942	136	1	[	[	X
eurjchem-942	136	2	3	3	NUM
eurjchem-942	136	3	]	]	PUNCT
eurjchem-942	136	4	.	.	PUNCT
eurjchem-942	136	5	honda	honda	PROPN
eurjchem-942	136	6	,	,	PUNCT
eurjchem-942	136	7	k.	k.	PROPN
eurjchem-942	136	8	;	;	PUNCT
eurjchem-942	136	9	nakagawa	nakagawa	PROPN
eurjchem-942	136	10	,	,	PUNCT
eurjchem-942	136	11	c.	c.	PROPN
eurjchem-942	136	12	j.	j.	PROPN
eurjchem-942	136	13	pharmacol	pharmacol	PROPN
eurjchem-942	136	14	.	.	PUNCT
eurjchem-942	137	1	exp	exp	PROPN
eurjchem-942	137	2	.	.	PUNCT
eurjchem-942	138	1	ther	ther	PROPN
eurjchem-942	138	2	.	.	PUNCT
eurjchem-942	139	1	1986	1986	NUM
eurjchem-942	139	2	,	,	PUNCT
eurjchem-942	139	3	239	239	NUM
eurjchem-942	139	4	,	,	PUNCT
eurjchem-942	139	5	512‐516	512‐516	NUM
eurjchem-942	139	6	.	.	PUNCT
eurjchem-942	140	1	[	[	X
eurjchem-942	140	2	4	4	NUM
eurjchem-942	140	3	]	]	PUNCT
eurjchem-942	140	4	.	.	PUNCT
eurjchem-942	140	5	honda	honda	PROPN
eurjchem-942	140	6	,	,	PUNCT
eurjchem-942	140	7	k.	k.	PROPN
eurjchem-942	140	8	;	;	PUNCT
eurjchem-942	140	9	nakagawa	nakagawa	PROPN
eurjchem-942	140	10	,	,	PUNCT
eurjchem-942	140	11	c.	c.	PROPN
eurjchem-942	140	12	;	;	PUNCT
eurjchem-942	140	13	terai	terai	PROPN
eurjchem-942	140	14	,	,	PUNCT
eurjchem-942	140	15	m.	m.	NOUN
eurjchem-942	140	16	;	;	PUNCT
eurjchem-942	140	17	naunyn	naunyn	PROPN
eurjchem-942	140	18	,	,	PUNCT
eurjchem-942	140	19	s.	s.	PROPN
eurjchem-942	140	20	arch	arch	PROPN
eurjchem-942	140	21	.	.	PUNCT
eurjchem-942	141	1	pharmacol	pharmacol	PROPN
eurjchem-942	141	2	.	.	PUNCT
eurjchem-942	142	1	1987	1987	NUM
eurjchem-942	142	2	,	,	PUNCT
eurjchem-942	142	3	336	336	NUM
eurjchem-942	142	4	,	,	PUNCT
eurjchem-942	142	5	295‐302	295‐302	PROPN
eurjchem-942	142	6	.	.	PUNCT
eurjchem-942	143	1	[	[	X
eurjchem-942	143	2	5	5	NUM
eurjchem-942	143	3	]	]	PUNCT
eurjchem-942	143	4	.	.	PUNCT
eurjchem-942	144	1	the	the	DET
eurjchem-942	144	2	united	united	PROPN
eurjchem-942	144	3	states	states	PROPN
eurjchem-942	144	4	pharmacopeia	pharmacopeia	PROPN
eurjchem-942	144	5	34	34	NUM
eurjchem-942	144	6	,	,	PUNCT
eurjchem-942	144	7	nf	nf	NOUN
eurjchem-942	144	8	29	29	NUM
eurjchem-942	144	9	,	,	PUNCT
eurjchem-942	144	10	usp	usp	PROPN
eurjchem-942	144	11	convention	convention	PROPN
eurjchem-942	144	12	,	,	PUNCT
eurjchem-942	144	13	rockville	rockville	PROPN
eurjchem-942	144	14	,	,	PUNCT
eurjchem-942	144	15	md	md	PROPN
eurjchem-942	144	16	,	,	PUNCT
eurjchem-942	144	17	usa	usa	PROPN
eurjchem-942	144	18	,	,	PUNCT
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eurjchem-942	144	20	.	.	PUNCT
eurjchem-942	145	1	[	[	X
eurjchem-942	145	2	6	6	NUM
eurjchem-942	145	3	]	]	PUNCT
eurjchem-942	145	4	.	.	PUNCT
eurjchem-942	146	1	kumari	kumari	PROPN
eurjchem-942	146	2	,	,	PUNCT
eurjchem-942	146	3	r.	r.	PROPN
eurjchem-942	146	4	;	;	PUNCT
eurjchem-942	146	5	dash	dash	NOUN
eurjchem-942	146	6	,	,	PUNCT
eurjchem-942	146	7	p.	p.	NOUN
eurjchem-942	146	8	p.	p.	NOUN
eurjchem-942	146	9	;	;	PUNCT
eurjchem-942	146	10	lal	lal	PROPN
eurjchem-942	146	11	,	,	PUNCT
eurjchem-942	146	12	v.	v.	PROPN
eurjchem-942	146	13	k.	k.	PROPN
eurjchem-942	146	14	;	;	PUNCT
eurjchem-942	146	15	mishra	mishra	PROPN
eurjchem-942	146	16	,	,	PUNCT
eurjchem-942	146	17	a.	a.	NOUN
eurjchem-942	146	18	;	;	PUNCT
eurjchem-942	146	19	murthy	murthy	PROPN
eurjchem-942	146	20	,	,	PUNCT
eurjchem-942	146	21	p.	p.	PROPN
eurjchem-942	146	22	n.	n.	PROPN
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eurjchem-942	146	24	j.	j.	PROPN
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eurjchem-942	146	26	.	.	PUNCT
eurjchem-942	147	1	sci	sci	PROPN
eurjchem-942	147	2	.	.	PROPN
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eurjchem-942	147	4	,	,	PUNCT
eurjchem-942	147	5	72	72	NUM
eurjchem-942	147	6	,	,	PUNCT
eurjchem-942	147	7	785‐787	785‐787	NUM
eurjchem-942	147	8	.	.	PUNCT
eurjchem-942	148	1	[	[	X
eurjchem-942	148	2	7	7	NUM
eurjchem-942	148	3	]	]	PUNCT
eurjchem-942	148	4	.	.	PUNCT
eurjchem-942	148	5	sudha	sudha	PROPN
eurjchem-942	148	6	,	,	PUNCT
eurjchem-942	148	7	t.	t.	PROPN
eurjchem-942	148	8	;	;	PUNCT
eurjchem-942	148	9	jitendra	jitendra	PROPN
eurjchem-942	148	10	,	,	PUNCT
eurjchem-942	148	11	d.	d.	PROPN
eurjchem-942	148	12	int	int	PROPN
eurjchem-942	148	13	.	.	PUNCT
eurjchem-942	149	1	j.	j.	PROPN
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eurjchem-942	149	3	.	.	PUNCT
eurjchem-942	150	1	res	re	NOUN
eurjchem-942	150	2	.	.	PROPN
eurjchem-942	151	1	2011	2011	NUM
eurjchem-942	151	2	,	,	PUNCT
eurjchem-942	151	3	2	2	NUM
eurjchem-942	151	4	,	,	PUNCT
eurjchem-942	151	5	29‐33	29‐33	NUM
eurjchem-942	151	6	.	.	PUNCT
eurjchem-942	152	1	[	[	X
eurjchem-942	152	2	8	8	NUM
eurjchem-942	152	3	]	]	PUNCT
eurjchem-942	152	4	.	.	PUNCT
eurjchem-942	153	1	chandorkar	chandorkar	PROPN
eurjchem-942	153	2	,	,	PUNCT
eurjchem-942	153	3	j.	j.	PROPN
eurjchem-942	153	4	g.	g.	PROPN
eurjchem-942	153	5	;	;	PUNCT
eurjchem-942	153	6	kotwal	kotwal	PROPN
eurjchem-942	153	7	,	,	PUNCT
eurjchem-942	153	8	v.	v.	PROPN
eurjchem-942	153	9	b.	b.	PROPN
eurjchem-942	153	10	;	;	PUNCT
eurjchem-942	153	11	dhande	dhande	PROPN
eurjchem-942	153	12	,	,	PUNCT
eurjchem-942	153	13	n.	n.	PROPN
eurjchem-942	153	14	s.	s.	PROPN
eurjchem-942	153	15	;	;	PUNCT
eurjchem-942	153	16	gurav	gurav	PROPN
eurjchem-942	153	17	,	,	PUNCT
eurjchem-942	153	18	s.	s.	PROPN
eurjchem-942	153	19	g.	g.	PROPN
eurjchem-942	153	20	;	;	PUNCT
eurjchem-942	153	21	pande	pande	NOUN
eurjchem-942	153	22	,	,	PUNCT
eurjchem-942	153	23	v.	v.	PROPN
eurjchem-942	153	24	v.	v.	ADP
eurjchem-942	153	25	;	;	PUNCT
eurjchem-942	153	26	yadav	yadav	PROPN
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eurjchem-942	153	29	v.	v.	PROPN
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eurjchem-942	154	1	j.	j.	PROPN
eurjchem-942	154	2	pharm	pharm	PROPN
eurjchem-942	154	3	.	.	PUNCT
eurjchem-942	155	1	sci	sci	PROPN
eurjchem-942	155	2	.	.	PROPN
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eurjchem-942	155	4	,	,	PUNCT
eurjchem-942	155	5	21	21	NUM
eurjchem-942	155	6	,	,	PUNCT
eurjchem-942	155	7	307‐310	307‐310	NUM
eurjchem-942	155	8	.	.	PUNCT
eurjchem-942	156	1	[	[	X
eurjchem-942	156	2	9	9	NUM
eurjchem-942	156	3	]	]	PUNCT
eurjchem-942	156	4	.	.	PUNCT
eurjchem-942	156	5	supriya	supriya	PROPN
eurjchem-942	156	6	,	,	PUNCT
eurjchem-942	156	7	m.	m.	NOUN
eurjchem-942	156	8	m.	m.	NOUN
eurjchem-942	156	9	;	;	PUNCT
eurjchem-942	156	10	roshani	roshani	PROPN
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eurjchem-942	156	12	y.	y.	PROPN
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eurjchem-942	156	14	;	;	PUNCT
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eurjchem-942	156	16	,	,	PUNCT
eurjchem-942	156	17	i.	i.	PROPN
eurjchem-942	156	18	b.	b.	PROPN
eurjchem-942	156	19	int	int	PROPN
eurjchem-942	156	20	.	.	PUNCT
eurjchem-942	157	1	j.	j.	PROPN
eurjchem-942	157	2	pharm	pharm	PROPN
eurjchem-942	157	3	.	.	PUNCT
eurjchem-942	158	1	pharm	pharm	PROPN
eurjchem-942	158	2	.	.	PUNCT
eurjchem-942	159	1	sci	sci	PROPN
eurjchem-942	159	2	.	.	PROPN
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eurjchem-942	159	4	,	,	PUNCT
eurjchem-942	159	5	4	4	NUM
eurjchem-942	159	6	,	,	PUNCT
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eurjchem-942	159	8	.	.	PUNCT
eurjchem-942	160	1	[	[	X
eurjchem-942	160	2	10	10	NUM
eurjchem-942	160	3	]	]	PUNCT
eurjchem-942	160	4	.	.	PUNCT
eurjchem-942	161	1	rao	rao	PROPN
eurjchem-942	161	2	,	,	PUNCT
eurjchem-942	161	3	b.	b.	PROPN
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eurjchem-942	161	5	;	;	PUNCT
eurjchem-942	161	6	srinivasu	srinivasu	PROPN
eurjchem-942	161	7	,	,	PUNCT
eurjchem-942	161	8	m.	m.	PROPN
eurjchem-942	161	9	k.	k.	PROPN
eurjchem-942	161	10	;	;	PUNCT
eurjchem-942	161	11	sridhar	sridhar	PROPN
eurjchem-942	161	12	,	,	PUNCT
eurjchem-942	161	13	g.	g.	PROPN
eurjchem-942	161	14	;	;	PUNCT
eurjchem-942	161	15	reddy	reddy	PROPN
eurjchem-942	161	16	,	,	PUNCT
eurjchem-942	161	17	b.	b.	PROPN
eurjchem-942	161	18	s.	s.	PROPN
eurjchem-942	161	19	;	;	PUNCT
eurjchem-942	161	20	vittal	vittal	ADJ
eurjchem-942	161	21	,	,	PUNCT
eurjchem-942	161	22	t.	t.	PROPN
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eurjchem-942	161	24	;	;	PUNCT
eurjchem-942	161	25	kumar	kumar	PROPN
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eurjchem-942	161	32	,	,	PUNCT
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eurjchem-942	161	34	,	,	PUNCT
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eurjchem-942	161	36	.	.	PUNCT
eurjchem-942	162	1	[	[	X
eurjchem-942	162	2	11	11	NUM
eurjchem-942	162	3	]	]	PUNCT
eurjchem-942	162	4	.	.	PUNCT
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eurjchem-942	162	7	s.	s.	PROPN
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eurjchem-942	162	9	;	;	PUNCT
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eurjchem-942	162	12	a.	a.	PROPN
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eurjchem-942	162	14	;	;	PUNCT
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eurjchem-942	162	17	p.	p.	PROPN
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eurjchem-942	162	19	;	;	PUNCT
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eurjchem-942	162	21	,	,	PUNCT
eurjchem-942	162	22	s.	s.	PROPN
eurjchem-942	162	23	j.	j.	PROPN
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eurjchem-942	162	25	.	.	PUNCT
eurjchem-942	163	1	res	re	NOUN
eurjchem-942	163	2	.	.	PUNCT
eurjchem-942	164	1	int	int	NOUN
eurjchem-942	164	2	.	.	PUNCT
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eurjchem-942	165	2	,	,	PUNCT
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eurjchem-942	165	4	,	,	PUNCT
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eurjchem-942	166	1	[	[	X
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eurjchem-942	166	3	]	]	PUNCT
eurjchem-942	166	4	.	.	PUNCT
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eurjchem-942	167	2	,	,	PUNCT
eurjchem-942	167	3	r.	r.	PROPN
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eurjchem-942	167	5	;	;	PUNCT
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eurjchem-942	167	7	,	,	PUNCT
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eurjchem-942	167	11	;	;	PUNCT
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eurjchem-942	167	13	,	,	PUNCT
eurjchem-942	167	14	r.	r.	PROPN
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eurjchem-942	167	16	;	;	PUNCT
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eurjchem-942	167	19	d.	d.	PROPN
eurjchem-942	167	20	d.	d.	PROPN
eurjchem-942	167	21	;	;	PUNCT
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eurjchem-942	167	25	s.	s.	PROPN
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eurjchem-942	168	2	.	.	PUNCT
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eurjchem-942	169	2	.	.	PUNCT
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eurjchem-942	170	2	,	,	PUNCT
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eurjchem-942	170	4	,	,	PUNCT
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eurjchem-942	170	6	.	.	PUNCT
eurjchem-942	171	1	[	[	X
eurjchem-942	171	2	13	13	NUM
eurjchem-942	171	3	]	]	PUNCT
eurjchem-942	171	4	.	.	PUNCT
eurjchem-942	172	1	ramakrishna	ramakrishna	PROPN
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eurjchem-942	172	3	n.	n.	PROPN
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eurjchem-942	172	6	;	;	PUNCT
eurjchem-942	172	7	vishwottan	vishwottan	PROPN
eurjchem-942	172	8	,	,	PUNCT
eurjchem-942	172	9	k.	k.	PROPN
eurjchem-942	172	10	n.	n.	PROPN
eurjchem-942	172	11	;	;	PUNCT
eurjchem-942	172	12	manoj	manoj	PROPN
eurjchem-942	172	13	,	,	PUNCT
eurjchem-942	172	14	s.	s.	PROPN
eurjchem-942	172	15	;	;	PUNCT
eurjchem-942	172	16	koteshwara	koteshwara	PROPN
eurjchem-942	172	17	,	,	PUNCT
eurjchem-942	172	18	m.	m.	NOUN
eurjchem-942	172	19	;	;	PUNCT
eurjchem-942	172	20	wishu	wishu	PROPN
eurjchem-942	172	21	,	,	PUNCT
eurjchem-942	172	22	s.	s.	PROPN
eurjchem-942	172	23	;	;	PUNCT
eurjchem-942	172	24	varma	varma	PROPN
eurjchem-942	172	25	,	,	PUNCT
eurjchem-942	172	26	d.	d.	PROPN
eurjchem-942	172	27	p.	p.	PROPN
eurjchem-942	172	28	biomed	biome	VERB
eurjchem-942	172	29	.	.	PUNCT
eurjchem-942	173	1	chromatogr	chromatogr	PROPN
eurjchem-942	173	2	.	.	PUNCT
eurjchem-942	174	1	2005	2005	NUM
eurjchem-942	174	2	,	,	PUNCT
eurjchem-942	174	3	19	19	NUM
eurjchem-942	174	4	,	,	PUNCT
eurjchem-942	174	5	709‐719	709‐719	PROPN
eurjchem-942	174	6	.	.	PUNCT
eurjchem-942	175	1	[	[	X
eurjchem-942	175	2	14	14	NUM
eurjchem-942	175	3	]	]	PUNCT
eurjchem-942	175	4	.	.	PUNCT
eurjchem-942	176	1	keski‐rahkonen	keski‐rahkonen	PROPN
eurjchem-942	176	2	,	,	PUNCT
eurjchem-942	176	3	p.	p.	NOUN
eurjchem-942	176	4	;	;	PUNCT
eurjchem-942	176	5	parssinen	parssinen	NOUN
eurjchem-942	176	6	,	,	PUNCT
eurjchem-942	176	7	o.	o.	PROPN
eurjchem-942	176	8	;	;	PUNCT
eurjchem-942	176	9	leppanen	leppanen	PROPN
eurjchem-942	176	10	,	,	PUNCT
eurjchem-942	176	11	e.	e.	PROPN
eurjchem-942	176	12	;	;	PUNCT
eurjchem-942	176	13	mauriala	mauriala	PROPN
eurjchem-942	176	14	,	,	PUNCT
eurjchem-942	176	15	t.	t.	PROPN
eurjchem-942	176	16	;	;	PUNCT
eurjchem-942	176	17	lehtonen	lehtonen	NOUN
eurjchem-942	176	18	,	,	PUNCT
eurjchem-942	176	19	m.	m.	NOUN
eurjchem-942	176	20	;	;	PUNCT
eurjchem-942	176	21	auriola	auriola	PROPN
eurjchem-942	176	22	,	,	PUNCT
eurjchem-942	176	23	s.	s.	PROPN
eurjchem-942	176	24	j.	j.	PROPN
eurjchem-942	176	25	pharm	pharm	PROPN
eurjchem-942	176	26	.	.	PUNCT
eurjchem-942	176	27	biomed	biome	VERB
eurjchem-942	176	28	.	.	PUNCT
eurjchem-942	177	1	anal	anal	ADJ
eurjchem-942	177	2	.	.	PUNCT
eurjchem-942	178	1	2007	2007	NUM
eurjchem-942	178	2	,	,	PUNCT
eurjchem-942	178	3	43	43	NUM
eurjchem-942	178	4	,	,	PUNCT
eurjchem-942	178	5	606‐612	606‐612	NUM
eurjchem-942	178	6	.	.	PUNCT
eurjchem-942	179	1	[	[	X
eurjchem-942	179	2	15	15	NUM
eurjchem-942	179	3	]	]	PUNCT
eurjchem-942	179	4	.	.	PUNCT
eurjchem-942	179	5	rao	rao	PROPN
eurjchem-942	179	6	,	,	PUNCT
eurjchem-942	179	7	b.	b.	PROPN
eurjchem-942	179	8	m.	m.	PROPN
eurjchem-942	179	9	;	;	PUNCT
eurjchem-942	179	10	srinivasu	srinivasu	PROPN
eurjchem-942	179	11	,	,	PUNCT
eurjchem-942	179	12	m.	m.	PROPN
eurjchem-942	179	13	k.	k.	PROPN
eurjchem-942	179	14	;	;	PUNCT
eurjchem-942	179	15	thilakumar	thilakumar	PROPN
eurjchem-942	179	16	,	,	PUNCT
eurjchem-942	179	17	t.	t.	PROPN
eurjchem-942	179	18	;	;	PUNCT
eurjchem-942	179	19	more	more	ADJ
eurjchem-942	179	20	,	,	PUNCT
eurjchem-942	179	21	s.	s.	PROPN
eurjchem-942	179	22	;	;	PUNCT
eurjchem-942	179	23	rajendra	rajendra	PROPN
eurjchem-942	179	24	,	,	PUNCT
eurjchem-942	179	25	k.	k.	PROPN
eurjchem-942	180	1	p.	p.	PROPN
eurjchem-942	180	2	indian	indian	ADJ
eurjchem-942	180	3	drugs	drug	NOUN
eurjchem-942	180	4	2005	2005	NUM
eurjchem-942	180	5	,	,	PUNCT
eurjchem-942	180	6	42	42	NUM
eurjchem-942	180	7	,	,	PUNCT
eurjchem-942	180	8	175‐177	175‐177	NUM
eurjchem-942	180	9	.	.	PUNCT
eurjchem-942	181	1	[	[	X
eurjchem-942	181	2	16	16	NUM
eurjchem-942	181	3	]	]	PUNCT
eurjchem-942	181	4	.	.	PUNCT
eurjchem-942	182	1	ozkan	ozkan	PROPN
eurjchem-942	182	2	,	,	PUNCT
eurjchem-942	182	3	s.	s.	PROPN
eurjchem-942	182	4	a.	a.	PROPN
eurjchem-942	182	5	;	;	PUNCT
eurjchem-942	182	6	uslu	uslu	PROPN
eurjchem-942	182	7	,	,	PUNCT
eurjchem-942	182	8	b.	b.	PROPN
eurjchem-942	182	9	;	;	PUNCT
eurjchem-942	182	10	aboul‐enein	aboul‐enein	PROPN
eurjchem-942	182	11	,	,	PUNCT
eurjchem-942	182	12	h.	h.	PROPN
eurjchem-942	182	13	y.	y.	PROPN
eurjchem-942	182	14	talanta	talanta	PROPN
eurjchem-942	182	15	2003	2003	NUM
eurjchem-942	182	16	,	,	PUNCT
eurjchem-942	182	17	61	61	NUM
eurjchem-942	182	18	,	,	PUNCT
eurjchem-942	182	19	147‐156	147‐156	NUM
eurjchem-942	182	20	.	.	PUNCT
eurjchem-942	183	1	[	[	X
eurjchem-942	183	2	17	17	NUM
eurjchem-942	183	3	]	]	PUNCT
eurjchem-942	183	4	.	.	PUNCT
eurjchem-942	184	1	maier	maier	PROPN
eurjchem-942	184	2	,	,	PUNCT
eurjchem-942	184	3	v.	v.	PROPN
eurjchem-942	184	4	;	;	PUNCT
eurjchem-942	184	5	horakova	horakova	PROPN
eurjchem-942	184	6	,	,	PUNCT
eurjchem-942	184	7	j.	j.	PROPN
eurjchem-942	184	8	;	;	PUNCT
eurjchem-942	184	9	petr	petr	PROPN
eurjchem-942	184	10	,	,	PUNCT
eurjchem-942	184	11	j.	j.	PROPN
eurjchem-942	184	12	;	;	PUNCT
eurjchem-942	184	13	tesarova	tesarova	PROPN
eurjchem-942	184	14	,	,	PUNCT
eurjchem-942	184	15	c.	c.	NOUN
eurjchem-942	184	16	;	;	PUNCT
eurjchem-942	184	17	coufal	coufal	NOUN
eurjchem-942	184	18	,	,	PUNCT
eurjchem-942	184	19	p.	p.	NOUN
eurjchem-942	184	20	;	;	PUNCT
eurjchem-942	184	21	sevcik	sevcik	PROPN
eurjchem-942	184	22	,	,	PUNCT
eurjchem-942	184	23	j.	j.	PROPN
eurjchem-942	184	24	j.	j.	PROPN
eurjchem-942	184	25	pharm	pharm	PROPN
eurjchem-942	184	26	.	.	PUNCT
eurjchem-942	184	27	biomed	biome	VERB
eurjchem-942	184	28	.	.	PUNCT
eurjchem-942	185	1	anal	anal	ADJ
eurjchem-942	185	2	.	.	PUNCT
eurjchem-942	186	1	2005	2005	NUM
eurjchem-942	186	2	,	,	PUNCT
eurjchem-942	186	3	39	39	NUM
eurjchem-942	186	4	,	,	PUNCT
eurjchem-942	186	5	691‐696	691‐696	NOUN
eurjchem-942	186	6	.	.	PUNCT
eurjchem-942	187	1	[	[	X
eurjchem-942	187	2	18	18	NUM
eurjchem-942	187	3	]	]	PUNCT
eurjchem-942	187	4	.	.	PUNCT
eurjchem-942	188	1	patel	patel	PROPN
eurjchem-942	188	2	,	,	PUNCT
eurjchem-942	188	3	n.	n.	PROPN
eurjchem-942	188	4	u.	u.	PROPN
eurjchem-942	188	5	;	;	PUNCT
eurjchem-942	188	6	chaudhari	chaudhari	PROPN
eurjchem-942	188	7	,	,	PUNCT
eurjchem-942	188	8	b.	b.	PROPN
eurjchem-942	188	9	g.	g.	PROPN
eurjchem-942	188	10	pharm	pharm	PROPN
eurjchem-942	188	11	.	.	PUNCT
eurjchem-942	189	1	sin	sin	PROPN
eurjchem-942	189	2	.	.	PUNCT
eurjchem-942	190	1	2011	2011	NUM
eurjchem-942	190	2	,	,	PUNCT
eurjchem-942	190	3	2	2	NUM
eurjchem-942	190	4	,	,	PUNCT
eurjchem-942	190	5	172‐175	172‐175	PROPN
eurjchem-942	190	6	.	.	PUNCT
eurjchem-942	191	1	[	[	X
eurjchem-942	191	2	19	19	NUM
eurjchem-942	191	3	]	]	PUNCT
eurjchem-942	191	4	.	.	PUNCT
eurjchem-942	192	1	gadhave	gadhave	PROPN
eurjchem-942	192	2	,	,	PUNCT
eurjchem-942	192	3	n.	n.	PROPN
eurjchem-942	192	4	a.	a.	PROPN
eurjchem-942	192	5	;	;	PUNCT
eurjchem-942	192	6	sawant	sawant	PROPN
eurjchem-942	192	7	,	,	PUNCT
eurjchem-942	192	8	s.	s.	PROPN
eurjchem-942	192	9	d.	d.	PROPN
eurjchem-942	192	10	;	;	PUNCT
eurjchem-942	192	11	ghante	ghante	PROPN
eurjchem-942	192	12	,	,	PUNCT
eurjchem-942	192	13	m.	m.	NOUN
eurjchem-942	192	14	r.	r.	PROPN
eurjchem-942	192	15	;	;	PUNCT
eurjchem-942	192	16	nikam	nikam	NOUN
eurjchem-942	192	17	,	,	PUNCT
eurjchem-942	192	18	a.	a.	PROPN
eurjchem-942	192	19	d.	d.	PROPN
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eurjchem-942	192	21	.	.	PUNCT
eurjchem-942	193	1	j.	j.	PROPN
eurjchem-942	193	2	pharm	pharm	PROPN
eurjchem-942	193	3	.	.	PUNCT
eurjchem-942	194	1	res	re	NOUN
eurjchem-942	194	2	.	.	PUNCT
eurjchem-942	195	1	dev	dev	PROPN
eurjchem-942	195	2	.	.	PROPN
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eurjchem-942	196	2	,	,	PUNCT
eurjchem-942	196	3	3	3	NUM
eurjchem-942	196	4	,	,	PUNCT
eurjchem-942	196	5	87‐92	87‐92	NOUN
eurjchem-942	196	6	.	.	PUNCT
eurjchem-942	197	1	[	[	X
eurjchem-942	197	2	20	20	NUM
eurjchem-942	197	3	]	]	PUNCT
eurjchem-942	197	4	.	.	PUNCT
eurjchem-942	198	1	saradhi	saradhi	PROPN
eurjchem-942	198	2	,	,	PUNCT
eurjchem-942	198	3	s.	s.	PROPN
eurjchem-942	198	4	v.	v.	PROPN
eurjchem-942	198	5	;	;	PUNCT
eurjchem-942	198	6	meherjaha	meherjaha	PROPN
eurjchem-942	198	7	,	,	PUNCT
eurjchem-942	198	8	s.	s.	PROPN
eurjchem-942	198	9	k.	k.	PROPN
eurjchem-942	198	10	;	;	PUNCT
eurjchem-942	198	11	jyothsna	jyothsna	PROPN
eurjchem-942	198	12	,	,	PUNCT
eurjchem-942	198	13	n.	n.	PROPN
eurjchem-942	198	14	;	;	PUNCT
eurjchem-942	198	15	priyanka	priyanka	PROPN
eurjchem-942	198	16	,	,	PUNCT
eurjchem-942	198	17	a.	a.	NOUN
eurjchem-942	198	18	;	;	PUNCT
eurjchem-942	198	19	sirisha	sirisha	PROPN
eurjchem-942	198	20	,	,	PUNCT
eurjchem-942	198	21	p.	p.	PROPN
eurjchem-942	198	22	b.	b.	PROPN
eurjchem-942	198	23	;	;	PUNCT
eurjchem-942	198	24	ramakrishna	ramakrishna	PROPN
eurjchem-942	198	25	,	,	PUNCT
eurjchem-942	198	26	c.	c.	PROPN
eurjchem-942	198	27	h.	h.	PROPN
eurjchem-942	198	28	;	;	PUNCT
eurjchem-942	198	29	sekaran	sekaran	NOUN
eurjchem-942	198	30	,	,	PUNCT
eurjchem-942	198	31	c.	c.	PROPN
eurjchem-942	198	32	b.	b.	PROPN
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eurjchem-942	198	35	.	.	PUNCT
eurjchem-942	199	1	sci	sci	PROPN
eurjchem-942	199	2	.	.	PUNCT
eurjchem-942	199	3	res	res	PROPN
eurjchem-942	199	4	.	.	PROPN
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eurjchem-942	199	6	,	,	PUNCT
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eurjchem-942	199	8	,	,	PUNCT
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eurjchem-942	199	11	.	.	PUNCT
eurjchem-942	200	1	[	[	X
eurjchem-942	200	2	21	21	NUM
eurjchem-942	200	3	]	]	PUNCT
eurjchem-942	200	4	.	.	PUNCT
eurjchem-942	201	1	thompson	thompson	PROPN
eurjchem-942	201	2	,	,	PUNCT
eurjchem-942	201	3	i.	i.	NOUN
eurjchem-942	201	4	m.	m.	PROPN
eurjchem-942	201	5	;	;	PUNCT
eurjchem-942	201	6	klein	klein	PROPN
eurjchem-942	201	7	,	,	PUNCT
eurjchem-942	201	8	e.	e.	PROPN
eurjchem-942	201	9	a.	a.	PROPN
eurjchem-942	201	10	;	;	PUNCT
eurjchem-942	201	11	lippman	lippman	PROPN
eurjchem-942	201	12	,	,	PUNCT
eurjchem-942	201	13	s.	s.	PROPN
eurjchem-942	201	14	m.	m.	PROPN
eurjchem-942	201	15	;	;	PUNCT
eurjchem-942	201	16	coltman	coltman	PROPN
eurjchem-942	201	17	,	,	PUNCT
eurjchem-942	201	18	c.	c.	PROPN
eurjchem-942	201	19	a.	a.	PROPN
eurjchem-942	201	20	;	;	PUNCT
eurjchem-942	201	21	djavan	djavan	PROPN
eurjchem-942	201	22	,	,	PUNCT
eurjchem-942	201	23	b.	b.	PROPN
eurjchem-942	201	24	eur	eur	PROPN
eurjchem-942	201	25	.	.	PUNCT
eurjchem-942	201	26	urol	urol	PROPN
eurjchem-942	201	27	.	.	PROPN
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eurjchem-942	201	29	,	,	PUNCT
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eurjchem-942	201	31	,	,	PUNCT
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eurjchem-942	201	33	.	.	PUNCT
eurjchem-942	202	1	[	[	X
eurjchem-942	202	2	22	22	NUM
eurjchem-942	202	3	]	]	PUNCT
eurjchem-942	202	4	.	.	PUNCT
eurjchem-942	203	1	syed	sye	VERB
eurjchem-942	203	2	,	,	PUNCT
eurjchem-942	203	3	a.	a.	NOUN
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eurjchem-942	203	5	;	;	PUNCT
eurjchem-942	203	6	amshumali	amshumali	PROPN
eurjchem-942	203	7	,	,	PUNCT
eurjchem-942	203	8	m.	m.	PROPN
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eurjchem-942	203	10	j.	j.	PROPN
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eurjchem-942	203	12	.	.	PUNCT
eurjchem-942	203	13	biomed	biome	VERB
eurjchem-942	203	14	.	.	PUNCT
eurjchem-942	204	1	anal	anal	ADJ
eurjchem-942	204	2	.	.	PUNCT
eurjchem-942	205	1	2001	2001	NUM
eurjchem-942	205	2	,	,	PUNCT
eurjchem-942	205	3	25	25	NUM
eurjchem-942	205	4	,	,	PUNCT
eurjchem-942	205	5	1015‐	1015‐	NUM
eurjchem-942	205	6	1019	1019	NUM
eurjchem-942	205	7	.	.	PUNCT
eurjchem-942	206	1	[	[	X
eurjchem-942	206	2	23	23	NUM
eurjchem-942	206	3	]	]	PUNCT
eurjchem-942	206	4	.	.	PUNCT
eurjchem-942	207	1	amer	amer	PROPN
eurjchem-942	207	2	,	,	PUNCT
eurjchem-942	207	3	s.	s.	PROPN
eurjchem-942	207	4	m.	m.	PROPN
eurjchem-942	207	5	farmaco	farmaco	PROPN
eurjchem-942	207	6	2003	2003	NUM
eurjchem-942	207	7	,	,	PUNCT
eurjchem-942	207	8	58	58	NUM
eurjchem-942	207	9	,	,	PUNCT
eurjchem-942	207	10	159‐163	159‐163	NUM
eurjchem-942	207	11	.	.	PUNCT
eurjchem-942	208	1	[	[	X
eurjchem-942	208	2	24	24	NUM
eurjchem-942	208	3	]	]	PUNCT
eurjchem-942	208	4	.	.	PUNCT
eurjchem-942	209	1	matuszewski	matuszewski	PROPN
eurjchem-942	209	2	,	,	PUNCT
eurjchem-942	209	3	b.	b.	PROPN
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eurjchem-942	209	5	;	;	PUNCT
eurjchem-942	209	6	constanzer	constanzer	PROPN
eurjchem-942	209	7	,	,	PUNCT
eurjchem-942	209	8	m.	m.	NOUN
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eurjchem-942	209	10	;	;	PUNCT
eurjchem-942	209	11	chavez‐eng	chavez‐eng	PROPN
eurjchem-942	209	12	,	,	PUNCT
eurjchem-942	209	13	c.	c.	PROPN
eurjchem-942	209	14	m.	m.	PROPN
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eurjchem-942	209	16	.	.	PUNCT
eurjchem-942	210	1	chem	chem	PROPN
eurjchem-942	210	2	.	.	PUNCT
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eurjchem-942	211	2	,	,	PUNCT
eurjchem-942	211	3	70	70	NUM
eurjchem-942	211	4	,	,	PUNCT
eurjchem-942	211	5	882‐889	882‐889	NUM
eurjchem-942	211	6	.	.	PUNCT
eurjchem-942	212	1	[	[	X
eurjchem-942	212	2	25	25	NUM
eurjchem-942	212	3	]	]	PUNCT
eurjchem-942	212	4	.	.	PUNCT
eurjchem-942	213	1	mousavi	mousavi	PROPN
eurjchem-942	213	2	,	,	PUNCT
eurjchem-942	213	3	s.	s.	PROPN
eurjchem-942	213	4	h.	h.	PROPN
eurjchem-942	213	5	h.	h.	PROPN
eurjchem-942	213	6	;	;	PUNCT
eurjchem-942	213	7	kobarfard	kobarfard	PROPN
eurjchem-942	213	8	,	,	PUNCT
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eurjchem-942	213	10	;	;	PUNCT
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eurjchem-942	217	7	,	,	PUNCT
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eurjchem-942	217	9	;	;	PUNCT
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eurjchem-942	220	3	]	]	PUNCT
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eurjchem-942	221	2	,	,	PUNCT
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