id	sid	tid	token	lemma	pos
eurjchem-966	1	1	untitled	untitle	VERB
eurjchem-966	1	2	european	european	PROPN
eurjchem-966	1	3	journal	journal	PROPN
eurjchem-966	1	4	of	of	ADP
eurjchem-966	1	5	chemistry	chemistry	NOUN
eurjchem-966	1	6	5	5	NUM
eurjchem-966	1	7	(	(	PUNCT
eurjchem-966	1	8	2	2	NUM
eurjchem-966	1	9	)	)	PUNCT
eurjchem-966	1	10	(	(	PUNCT
eurjchem-966	1	11	2014	2014	NUM
eurjchem-966	1	12	)	)	PUNCT
eurjchem-966	1	13	219‐226	219‐226	NUM
eurjchem-966	1	14	european	european	PROPN
eurjchem-966	1	15	journal	journal	PROPN
eurjchem-966	1	16	of	of	ADP
eurjchem-966	1	17	chemistry	chemistry	NOUN
eurjchem-966	1	18	issn	issn	PROPN
eurjchem-966	1	19	2153‐2249	2153‐2249	PROPN
eurjchem-966	1	20	(	(	PUNCT
eurjchem-966	1	21	print	print	NOUN
eurjchem-966	1	22	)	)	PUNCT
eurjchem-966	1	23	/	/	SYM
eurjchem-966	1	24	issn	issn	PROPN
eurjchem-966	1	25	2153‐2257	2153‐2257	NUM
eurjchem-966	1	26	(	(	PUNCT
eurjchem-966	1	27	online	online	ADJ
eurjchem-966	1	28	)	)	PUNCT
eurjchem-966	1	29			NOUN
eurjchem-966	1	30	2014	2014	NUM
eurjchem-966	2	1	eurjchem	eurjchem	PROPN
eurjchem-966	2	2	publishing	publish	VERB
eurjchem-966	2	3	‐	‐	NOUN
eurjchem-966	2	4	printed	print	VERB
eurjchem-966	2	5	in	in	ADP
eurjchem-966	2	6	the	the	DET
eurjchem-966	2	7	usa	usa	PROPN
eurjchem-966	2	8	http://dx.doi.org/10.5155/eurjchem.5.2.219‐226.966	http://dx.doi.org/10.5155/eurjchem.5.2.219‐226.966	PROPN
eurjchem-966	2	9	european	european	PROPN
eurjchem-966	2	10	journal	journal	PROPN
eurjchem-966	2	11	of	of	ADP
eurjchem-966	2	12	chemistry	chemistry	PROPN
eurjchem-966	2	13	journal	journal	PROPN
eurjchem-966	2	14	homepage	homepage	NOUN
eurjchem-966	2	15	:	:	PUNCT
eurjchem-966	2	16	www.eurjchem.com	www.eurjchem.com	X
eurjchem-966	2	17	development	development	NOUN
eurjchem-966	2	18	and	and	CCONJ
eurjchem-966	2	19	validation	validation	NOUN
eurjchem-966	2	20	of	of	ADP
eurjchem-966	2	21	stability	stability	NOUN
eurjchem-966	2	22	indicating	indicate	VERB
eurjchem-966	2	23	spectrophotometric	spectrophotometric	ADJ
eurjchem-966	2	24	and	and	CCONJ
eurjchem-966	2	25	hptlc	hptlc	NOUN
eurjchem-966	2	26	methods	method	NOUN
eurjchem-966	2	27	for	for	ADP
eurjchem-966	2	28	determination	determination	NOUN
eurjchem-966	2	29	of	of	ADP
eurjchem-966	2	30	acemetacin	acemetacin	PROPN
eurjchem-966	2	31	ibrahim	ibrahim	PROPN
eurjchem-966	2	32	ahmed	ahme	VERB
eurjchem-966	2	33	naguib	naguib	PROPN
eurjchem-966	2	34	a	a	PROPN
eurjchem-966	2	35	,	,	PUNCT
eurjchem-966	2	36	eglal	eglal	VERB
eurjchem-966	2	37	abdelhamid	abdelhamid	INTJ
eurjchem-966	2	38	abdelaleem	abdelaleem	ADV
eurjchem-966	2	39	a	a	PRON
eurjchem-966	2	40	,	,	PUNCT
eurjchem-966	2	41	hala	hala	PROPN
eurjchem-966	2	42	elsayed	elsaye	VERB
eurjchem-966	2	43	zaazaa	zaazaa	PROPN
eurjchem-966	2	44	b	b	PROPN
eurjchem-966	2	45	and	and	CCONJ
eurjchem-966	2	46	essraa	essraa	VERB
eurjchem-966	2	47	abd	abd	PROPN
eurjchem-966	2	48	elwahab	elwahab	PROPN
eurjchem-966	2	49	hussein	hussein	PROPN
eurjchem-966	2	50	a	a	DET
eurjchem-966	2	51	,	,	PUNCT
eurjchem-966	2	52	*	*	PUNCT
eurjchem-966	2	53	a	a	DET
eurjchem-966	2	54	pharmaceutical	pharmaceutical	ADJ
eurjchem-966	2	55	analytical	analytical	ADJ
eurjchem-966	2	56	chemistry	chemistry	NOUN
eurjchem-966	2	57	department	department	NOUN
eurjchem-966	2	58	,	,	PUNCT
eurjchem-966	2	59	faculty	faculty	NOUN
eurjchem-966	2	60	of	of	ADP
eurjchem-966	2	61	pharmacy	pharmacy	NOUN
eurjchem-966	2	62	,	,	PUNCT
eurjchem-966	2	63	beni‐suef	beni‐suef	ADJ
eurjchem-966	2	64	university	university	NOUN
eurjchem-966	2	65	,	,	PUNCT
eurjchem-966	2	66	62514	62514	NUM
eurjchem-966	2	67	,	,	PUNCT
eurjchem-966	2	68	beni‐suef	beni‐suef	PROPN
eurjchem-966	2	69	,	,	PUNCT
eurjchem-966	2	70	egypt	egypt	PROPN
eurjchem-966	2	71	b	b	PROPN
eurjchem-966	2	72	analytical	analytical	ADJ
eurjchem-966	2	73	chemistry	chemistry	NOUN
eurjchem-966	2	74	department	department	NOUN
eurjchem-966	2	75	,	,	PUNCT
eurjchem-966	2	76	faculty	faculty	NOUN
eurjchem-966	2	77	of	of	ADP
eurjchem-966	2	78	pharmacy	pharmacy	NOUN
eurjchem-966	2	79	,	,	PUNCT
eurjchem-966	2	80	cairo	cairo	PROPN
eurjchem-966	2	81	university	university	PROPN
eurjchem-966	2	82	,	,	PUNCT
eurjchem-966	2	83	kasr	kasr	PROPN
eurjchem-966	2	84	el‐aini	el‐aini	PROPN
eurjchem-966	2	85	,	,	PUNCT
eurjchem-966	2	86	11562	11562	NUM
eurjchem-966	2	87	cairo	cairo	PROPN
eurjchem-966	2	88	,	,	PUNCT
eurjchem-966	2	89	egypt	egypt	PROPN
eurjchem-966	2	90	*	*	PUNCT
eurjchem-966	2	91	corresponding	correspond	VERB
eurjchem-966	2	92	author	author	NOUN
eurjchem-966	2	93	at	at	ADP
eurjchem-966	2	94	:	:	PUNCT
eurjchem-966	2	95	pharmaceutical	pharmaceutical	ADJ
eurjchem-966	2	96	analytical	analytical	ADJ
eurjchem-966	2	97	chemistry	chemistry	NOUN
eurjchem-966	2	98	department	department	NOUN
eurjchem-966	2	99	,	,	PUNCT
eurjchem-966	2	100	faculty	faculty	NOUN
eurjchem-966	2	101	of	of	ADP
eurjchem-966	2	102	pharmacy	pharmacy	NOUN
eurjchem-966	2	103	,	,	PUNCT
eurjchem-966	2	104	beni‐suef	beni‐suef	ADJ
eurjchem-966	2	105	university	university	NOUN
eurjchem-966	2	106	,	,	PUNCT
eurjchem-966	2	107	62514	62514	NUM
eurjchem-966	2	108	,	,	PUNCT
eurjchem-966	2	109	beni‐suef	beni‐suef	PROPN
eurjchem-966	2	110	,	,	PUNCT
eurjchem-966	2	111	egypt	egypt	PROPN
eurjchem-966	2	112	.	.	PUNCT
eurjchem-966	3	1	tel	tel	PROPN
eurjchem-966	3	2	.	.	PUNCT
eurjchem-966	3	3	:	:	PUNCT
eurjchem-966	4	1	+2.010.08025080	+2.010.08025080	ADJ
eurjchem-966	4	2	.	.	PUNCT
eurjchem-966	5	1	fax	fax	NOUN
eurjchem-966	5	2	:	:	PUNCT
eurjchem-966	5	3	+2.082.2317950	+2.082.2317950	PROPN
eurjchem-966	5	4	.	.	PUNCT
eurjchem-966	5	5	e‐mail	e‐mail	PUNCT
eurjchem-966	6	1	address	address	NOUN
eurjchem-966	6	2	:	:	PUNCT
eurjchem-966	6	3	essraa_88@yahoo.com	essraa_88@yahoo.com	X
eurjchem-966	6	4	(	(	PUNCT
eurjchem-966	6	5	e.a.e	e.a.e	ADJ
eurjchem-966	6	6	.	.	PUNCT
eurjchem-966	6	7	hussein	hussein	PROPN
eurjchem-966	6	8	)	)	PUNCT
eurjchem-966	6	9	.	.	PUNCT
eurjchem-966	7	1	article	article	NOUN
eurjchem-966	7	2	information	information	PROPN
eurjchem-966	7	3	abstract	abstract	ADJ
eurjchem-966	7	4	doi	doi	NOUN
eurjchem-966	7	5	:	:	PUNCT
eurjchem-966	7	6	10.5155	10.5155	NUM
eurjchem-966	7	7	/	/	SYM
eurjchem-966	7	8	eurjchem.5.2.219‐226.966	eurjchem.5.2.219‐226.966	ADJ
eurjchem-966	7	9	received	receive	VERB
eurjchem-966	7	10	:	:	PUNCT
eurjchem-966	7	11	09	09	NUM
eurjchem-966	7	12	november	november	PROPN
eurjchem-966	7	13	2013	2013	NUM
eurjchem-966	7	14	received	receive	VERB
eurjchem-966	7	15	in	in	ADP
eurjchem-966	7	16	revised	revise	VERB
eurjchem-966	7	17	form	form	NOUN
eurjchem-966	7	18	:	:	PUNCT
eurjchem-966	7	19	01	01	NUM
eurjchem-966	7	20	december	december	PROPN
eurjchem-966	7	21	2013	2013	NUM
eurjchem-966	7	22	accepted	accept	VERB
eurjchem-966	7	23	:	:	PUNCT
eurjchem-966	7	24	05	05	NUM
eurjchem-966	7	25	december	december	PROPN
eurjchem-966	7	26	2013	2013	NUM
eurjchem-966	7	27	online	online	NOUN
eurjchem-966	7	28	:	:	PUNCT
eurjchem-966	7	29	30	30	NUM
eurjchem-966	7	30	june	june	PROPN
eurjchem-966	7	31	2014	2014	NUM
eurjchem-966	7	32	keywords	keyword	VERB
eurjchem-966	7	33	three	three	NUM
eurjchem-966	7	34	simple	simple	ADJ
eurjchem-966	7	35	and	and	CCONJ
eurjchem-966	7	36	sensitive	sensitive	ADJ
eurjchem-966	7	37	methods	method	NOUN
eurjchem-966	7	38	were	be	AUX
eurjchem-966	7	39	developed	develop	VERB
eurjchem-966	7	40	for	for	ADP
eurjchem-966	7	41	the	the	DET
eurjchem-966	7	42	determination	determination	NOUN
eurjchem-966	7	43	of	of	ADP
eurjchem-966	7	44	acemetacin	acemetacin	PROPN
eurjchem-966	7	45	(	(	PUNCT
eurjchem-966	7	46	acm	acm	PROPN
eurjchem-966	7	47	)	)	PUNCT
eurjchem-966	7	48	in	in	ADP
eurjchem-966	7	49	presence	presence	NOUN
eurjchem-966	7	50	of	of	ADP
eurjchem-966	7	51	its	its	PRON
eurjchem-966	7	52	degradation	degradation	NOUN
eurjchem-966	7	53	product	product	NOUN
eurjchem-966	7	54	,	,	PUNCT
eurjchem-966	7	55	indomethacin	indomethacin	PROPN
eurjchem-966	7	56	(	(	PUNCT
eurjchem-966	7	57	deg	deg	PROPN
eurjchem-966	7	58	)	)	PUNCT
eurjchem-966	7	59	.	.	PUNCT
eurjchem-966	8	1	several	several	ADJ
eurjchem-966	8	2	methods	method	NOUN
eurjchem-966	8	3	were	be	AUX
eurjchem-966	8	4	evaluated	evaluate	VERB
eurjchem-966	8	5	and	and	CCONJ
eurjchem-966	8	6	are	be	AUX
eurjchem-966	8	7	presented	present	VERB
eurjchem-966	8	8	.	.	PUNCT
eurjchem-966	9	1	method	method	PROPN
eurjchem-966	9	2	a	a	PRON
eurjchem-966	9	3	was	be	AUX
eurjchem-966	9	4	based	base	VERB
eurjchem-966	9	5	on	on	ADP
eurjchem-966	9	6	measuring	measure	VERB
eurjchem-966	9	7	the	the	DET
eurjchem-966	9	8	peak	peak	NOUN
eurjchem-966	9	9	amplitude	amplitude	NOUN
eurjchem-966	9	10	of	of	ADP
eurjchem-966	9	11	the	the	DET
eurjchem-966	9	12	first	first	ADJ
eurjchem-966	9	13	derivative	derivative	NOUN
eurjchem-966	9	14	of	of	ADP
eurjchem-966	9	15	the	the	DET
eurjchem-966	9	16	ratio	ratio	NOUN
eurjchem-966	9	17	spectra	spectra	PROPN
eurjchem-966	9	18	1dd	1dd	NOUN
eurjchem-966	9	19	at	at	ADP
eurjchem-966	9	20	244	244	NUM
eurjchem-966	9	21	nm	nm	NOUN
eurjchem-966	9	22	.	.	PUNCT
eurjchem-966	10	1	in	in	ADP
eurjchem-966	10	2	method	method	PROPN
eurjchem-966	10	3	b	b	PROPN
eurjchem-966	10	4	,	,	PUNCT
eurjchem-966	10	5	mean	mean	INTJ
eurjchem-966	10	6	centering	centering	NOUN
eurjchem-966	10	7	of	of	ADP
eurjchem-966	10	8	ratio	ratio	NOUN
eurjchem-966	10	9	spectra	spectra	PROPN
eurjchem-966	10	10	method	method	NOUN
eurjchem-966	10	11	(	(	PUNCT
eurjchem-966	10	12	mcr	mcr	PROPN
eurjchem-966	10	13	)	)	PUNCT
eurjchem-966	10	14	was	be	AUX
eurjchem-966	10	15	applied	apply	VERB
eurjchem-966	10	16	,	,	PUNCT
eurjchem-966	10	17	which	which	PRON
eurjchem-966	10	18	depends	depend	VERB
eurjchem-966	10	19	on	on	ADP
eurjchem-966	10	20	measuring	measure	VERB
eurjchem-966	10	21	the	the	DET
eurjchem-966	10	22	mean	mean	ADJ
eurjchem-966	10	23	centered	center	VERB
eurjchem-966	10	24	values	value	NOUN
eurjchem-966	10	25	of	of	ADP
eurjchem-966	10	26	ratio	ratio	NOUN
eurjchem-966	10	27	spectra	spectra	NOUN
eurjchem-966	10	28	of	of	ADP
eurjchem-966	10	29	acm	acm	PROPN
eurjchem-966	10	30	at	at	ADP
eurjchem-966	10	31	234	234	NUM
eurjchem-966	10	32	nm	nm	NOUN
eurjchem-966	10	33	.	.	PUNCT
eurjchem-966	11	1	method	method	PROPN
eurjchem-966	11	2	c	c	PROPN
eurjchem-966	11	3	provided	provide	VERB
eurjchem-966	11	4	separation	separation	NOUN
eurjchem-966	11	5	of	of	ADP
eurjchem-966	11	6	acm	acm	PROPN
eurjchem-966	11	7	from	from	ADP
eurjchem-966	11	8	its	its	PRON
eurjchem-966	11	9	deg	deg	NOUN
eurjchem-966	11	10	on	on	ADP
eurjchem-966	11	11	pre‐	pre‐	NOUN
eurjchem-966	11	12	activated	activate	VERB
eurjchem-966	11	13	silica	silica	NOUN
eurjchem-966	11	14	gel	gel	NOUN
eurjchem-966	11	15	60f254	60f254	NOUN
eurjchem-966	11	16	hptlc	hptlc	NOUN
eurjchem-966	11	17	plates	plate	NOUN
eurjchem-966	11	18	using	use	VERB
eurjchem-966	11	19	hexane	hexane	NOUN
eurjchem-966	11	20	:	:	PUNCT
eurjchem-966	11	21	ethyl	ethyl	PROPN
eurjchem-966	11	22	acetate	acetate	NOUN
eurjchem-966	11	23	:	:	PUNCT
eurjchem-966	11	24	glacial	glacial	ADJ
eurjchem-966	11	25	acetic	acetic	ADJ
eurjchem-966	11	26	acid	acid	NOUN
eurjchem-966	11	27	(	(	PUNCT
eurjchem-966	11	28	6:4:0.3	6:4:0.3	PROPN
eurjchem-966	11	29	,	,	PUNCT
eurjchem-966	11	30	v	v	NOUN
eurjchem-966	11	31	:	:	PUNCT
eurjchem-966	11	32	v	v	ADJ
eurjchem-966	11	33	:	:	PUNCT
eurjchem-966	11	34	v	v	NOUN
eurjchem-966	11	35	)	)	PUNCT
eurjchem-966	11	36	as	as	SCONJ
eurjchem-966	11	37	developing	develop	VERB
eurjchem-966	11	38	system	system	NOUN
eurjchem-966	11	39	followed	follow	VERB
eurjchem-966	11	40	by	by	ADP
eurjchem-966	11	41	scanning	scan	VERB
eurjchem-966	11	42	at	at	ADP
eurjchem-966	11	43	254	254	NUM
eurjchem-966	11	44	nm	nm	NOUN
eurjchem-966	11	45	.	.	PUNCT
eurjchem-966	12	1	the	the	DET
eurjchem-966	12	2	suggested	suggest	VERB
eurjchem-966	12	3	methods	method	NOUN
eurjchem-966	12	4	were	be	AUX
eurjchem-966	12	5	validated	validate	VERB
eurjchem-966	12	6	in	in	ADP
eurjchem-966	12	7	compliance	compliance	NOUN
eurjchem-966	12	8	with	with	ADP
eurjchem-966	12	9	the	the	DET
eurjchem-966	12	10	international	international	ADJ
eurjchem-966	12	11	conference	conference	NOUN
eurjchem-966	12	12	on	on	ADP
eurjchem-966	12	13	harmonisation	harmonisation	NOUN
eurjchem-966	12	14	(	(	PUNCT
eurjchem-966	12	15	ich	ich	NOUN
eurjchem-966	12	16	)	)	PUNCT
eurjchem-966	12	17	guidelines	guideline	NOUN
eurjchem-966	12	18	and	and	CCONJ
eurjchem-966	12	19	were	be	AUX
eurjchem-966	12	20	successfully	successfully	ADV
eurjchem-966	12	21	applied	apply	VERB
eurjchem-966	12	22	for	for	ADP
eurjchem-966	12	23	quantification	quantification	NOUN
eurjchem-966	12	24	of	of	ADP
eurjchem-966	12	25	acm	acm	NOUN
eurjchem-966	12	26	in	in	ADP
eurjchem-966	12	27	its	its	PRON
eurjchem-966	12	28	commercial	commercial	ADJ
eurjchem-966	12	29	capsule	capsule	NOUN
eurjchem-966	12	30	.	.	PUNCT
eurjchem-966	13	1	the	the	DET
eurjchem-966	13	2	proposed	propose	VERB
eurjchem-966	13	3	methods	method	NOUN
eurjchem-966	13	4	were	be	AUX
eurjchem-966	13	5	also	also	ADV
eurjchem-966	13	6	statistically	statistically	ADV
eurjchem-966	13	7	compared	compare	VERB
eurjchem-966	13	8	to	to	ADP
eurjchem-966	13	9	a	a	DET
eurjchem-966	13	10	reported	report	VERB
eurjchem-966	13	11	hplc	hplc	NOUN
eurjchem-966	13	12	method	method	NOUN
eurjchem-966	13	13	with	with	ADP
eurjchem-966	13	14	no	no	DET
eurjchem-966	13	15	significant	significant	ADJ
eurjchem-966	13	16	difference	difference	NOUN
eurjchem-966	13	17	in	in	ADP
eurjchem-966	13	18	performance	performance	NOUN
eurjchem-966	13	19	;	;	PUNCT
eurjchem-966	13	20	indicating	indicate	VERB
eurjchem-966	13	21	the	the	DET
eurjchem-966	13	22	ability	ability	NOUN
eurjchem-966	13	23	of	of	ADP
eurjchem-966	13	24	the	the	DET
eurjchem-966	13	25	proposed	propose	VERB
eurjchem-966	13	26	method	method	NOUN
eurjchem-966	13	27	to	to	PART
eurjchem-966	13	28	be	be	AUX
eurjchem-966	13	29	reliable	reliable	ADJ
eurjchem-966	13	30	and	and	CCONJ
eurjchem-966	13	31	suitable	suitable	ADJ
eurjchem-966	13	32	for	for	ADP
eurjchem-966	13	33	routine	routine	ADJ
eurjchem-966	13	34	analysis	analysis	NOUN
eurjchem-966	13	35	of	of	ADP
eurjchem-966	13	36	drug	drug	NOUN
eurjchem-966	13	37	product	product	NOUN
eurjchem-966	13	38	.	.	PUNCT
eurjchem-966	14	1	hptlc	hptlc	NOUN
eurjchem-966	14	2	validation	validation	NOUN
eurjchem-966	14	3	acemetacin	acemetacin	VERB
eurjchem-966	14	4	degradation	degradation	NOUN
eurjchem-966	14	5	first	first	ADJ
eurjchem-966	14	6	derivative	derivative	NOUN
eurjchem-966	14	7	of	of	ADP
eurjchem-966	14	8	ratio	ratio	NOUN
eurjchem-966	14	9	spectra	spectra	NOUN
eurjchem-966	14	10	mean	mean	NOUN
eurjchem-966	14	11	centering	centering	NOUN
eurjchem-966	14	12	of	of	ADP
eurjchem-966	14	13	ratio	ratio	NOUN
eurjchem-966	14	14	spectra	spectra	NOUN
eurjchem-966	14	15	1	1	X
eurjchem-966	14	16	.	.	PUNCT
eurjchem-966	14	17	introduction	introduction	NOUN
eurjchem-966	14	18	acemetacin	acemetacin	ADV
eurjchem-966	14	19	(	(	PUNCT
eurjchem-966	14	20	acm	acm	PROPN
eurjchem-966	14	21	)	)	PUNCT
eurjchem-966	14	22	,	,	PUNCT
eurjchem-966	15	1	[	[	X
eurjchem-966	15	2	1‐(4‐chlorobenzoyl)‐5‐methoxy‐2‐	1‐(4‐chlorobenzoyl)‐5‐methoxy‐2‐	NUM
eurjchem-966	15	3	methylindol‐3‐yl	methylindol‐3‐yl	NOUN
eurjchem-966	15	4	]	]	PUNCT
eurjchem-966	15	5	acetyloxy	acetyloxy	ADJ
eurjchem-966	15	6	acetic	acetic	ADJ
eurjchem-966	15	7	acid	acid	NOUN
eurjchem-966	16	1	[	[	X
eurjchem-966	16	2	1	1	NUM
eurjchem-966	16	3	]	]	PUNCT
eurjchem-966	16	4	,	,	PUNCT
eurjchem-966	16	5	is	be	AUX
eurjchem-966	16	6	a	a	DET
eurjchem-966	16	7	non‐steroidal	non‐steroidal	ADJ
eurjchem-966	16	8	anti‐inflammatory	anti‐inflammatory	NOUN
eurjchem-966	16	9	drug	drug	NOUN
eurjchem-966	16	10	(	(	PUNCT
eurjchem-966	16	11	nsaid	nsaid	PROPN
eurjchem-966	16	12	)	)	PUNCT
eurjchem-966	16	13	used	use	VERB
eurjchem-966	16	14	in	in	ADP
eurjchem-966	16	15	musculoskeletal	musculoskeletal	ADJ
eurjchem-966	16	16	,	,	PUNCT
eurjchem-966	16	17	joint	joint	ADJ
eurjchem-966	16	18	disorder	disorder	NOUN
eurjchem-966	16	19	,	,	PUNCT
eurjchem-966	16	20	rheumatoid	rheumatoid	VERB
eurjchem-966	16	21	arthritis	arthritis	NOUN
eurjchem-966	16	22	and	and	CCONJ
eurjchem-966	16	23	for	for	ADP
eurjchem-966	16	24	treatment	treatment	NOUN
eurjchem-966	16	25	of	of	ADP
eurjchem-966	16	26	post‐	post‐	NOUN
eurjchem-966	16	27	operative	operative	ADJ
eurjchem-966	16	28	pain	pain	NOUN
eurjchem-966	16	29	and	and	CCONJ
eurjchem-966	16	30	inflammation	inflammation	NOUN
eurjchem-966	16	31	[	[	X
eurjchem-966	16	32	2	2	NUM
eurjchem-966	16	33	]	]	PUNCT
eurjchem-966	16	34	.	.	PUNCT
eurjchem-966	17	1	being	be	AUX
eurjchem-966	17	2	a	a	DET
eurjchem-966	17	3	glycolic	glycolic	NOUN
eurjchem-966	17	4	acid	acid	NOUN
eurjchem-966	17	5	ester	ester	NOUN
eurjchem-966	17	6	of	of	ADP
eurjchem-966	17	7	indometacin	indometacin	PROPN
eurjchem-966	17	8	(	(	PUNCT
eurjchem-966	17	9	nsaid	nsaid	PROPN
eurjchem-966	17	10	)	)	PUNCT
eurjchem-966	17	11	;	;	PUNCT
eurjchem-966	17	12	50‐90	50‐90	NUM
eurjchem-966	17	13	%	%	NOUN
eurjchem-966	17	14	of	of	ADP
eurjchem-966	17	15	absorbed	absorb	VERB
eurjchem-966	17	16	acemetacin	acemetacin	ADV
eurjchem-966	17	17	is	be	AUX
eurjchem-966	17	18	converted	convert	VERB
eurjchem-966	17	19	inside	inside	ADP
eurjchem-966	17	20	the	the	DET
eurjchem-966	17	21	body	body	NOUN
eurjchem-966	17	22	into	into	ADP
eurjchem-966	17	23	indomethacin	indomethacin	NOUN
eurjchem-966	17	24	where	where	SCONJ
eurjchem-966	17	25	both	both	PRON
eurjchem-966	17	26	exert	exert	VERB
eurjchem-966	17	27	their	their	PRON
eurjchem-966	17	28	anti‐inflammatory	anti‐inflammatory	NOUN
eurjchem-966	17	29	action	action	NOUN
eurjchem-966	17	30	by	by	ADP
eurjchem-966	17	31	the	the	DET
eurjchem-966	17	32	same	same	ADJ
eurjchem-966	17	33	mechanism	mechanism	NOUN
eurjchem-966	17	34	[	[	X
eurjchem-966	17	35	3	3	NUM
eurjchem-966	17	36	]	]	PUNCT
eurjchem-966	17	37	.	.	PUNCT
eurjchem-966	18	1	the	the	DET
eurjchem-966	18	2	literature	literature	NOUN
eurjchem-966	18	3	survey	survey	NOUN
eurjchem-966	18	4	reveals	reveal	VERB
eurjchem-966	18	5	several	several	ADJ
eurjchem-966	18	6	methods	method	NOUN
eurjchem-966	18	7	for	for	ADP
eurjchem-966	18	8	determination	determination	NOUN
eurjchem-966	18	9	of	of	ADP
eurjchem-966	18	10	acemetacin	acemetacin	NOUN
eurjchem-966	18	11	in	in	ADP
eurjchem-966	18	12	its	its	PRON
eurjchem-966	18	13	pharmaceutical	pharmaceutical	ADJ
eurjchem-966	18	14	preparation	preparation	NOUN
eurjchem-966	18	15	including	include	VERB
eurjchem-966	18	16	direct	direct	ADJ
eurjchem-966	18	17	uv	uv	NOUN
eurjchem-966	18	18	,	,	PUNCT
eurjchem-966	18	19	derivative	derivative	ADJ
eurjchem-966	18	20	uv	uv	NOUN
eurjchem-966	18	21	spectrophotometry	spectrophotometry	NOUN
eurjchem-966	18	22	and	and	CCONJ
eurjchem-966	18	23	hplc	hplc	PROPN
eurjchem-966	18	24	[	[	X
eurjchem-966	18	25	4	4	NUM
eurjchem-966	18	26	]	]	PUNCT
eurjchem-966	18	27	and	and	CCONJ
eurjchem-966	18	28	micellar	micellar	NOUN
eurjchem-966	18	29	liquid	liquid	NOUN
eurjchem-966	18	30	chromatograpgy	chromatograpgy	NOUN
eurjchem-966	19	1	[	[	X
eurjchem-966	19	2	5	5	NUM
eurjchem-966	19	3	]	]	PUNCT
eurjchem-966	19	4	.	.	PUNCT
eurjchem-966	20	1	the	the	DET
eurjchem-966	20	2	effect	effect	NOUN
eurjchem-966	20	3	of	of	ADP
eurjchem-966	20	4	micelles	micelle	NOUN
eurjchem-966	20	5	on	on	ADP
eurjchem-966	20	6	the	the	DET
eurjchem-966	20	7	spectroscopic	spectroscopic	ADJ
eurjchem-966	20	8	and	and	CCONJ
eurjchem-966	20	9	solubility	solubility	NOUN
eurjchem-966	20	10	properties	property	NOUN
eurjchem-966	20	11	of	of	ADP
eurjchem-966	20	12	the	the	DET
eurjchem-966	20	13	two	two	NUM
eurjchem-966	20	14	non‐steroidal	non‐steroidal	ADJ
eurjchem-966	20	15	anti‐inflammatory	anti‐inflammatory	NOUN
eurjchem-966	20	16	drugs	drug	NOUN
eurjchem-966	20	17	,	,	PUNCT
eurjchem-966	20	18	indomethacin	indomethacin	NOUN
eurjchem-966	20	19	and	and	CCONJ
eurjchem-966	20	20	acemetacin	acemetacin	ADV
eurjchem-966	20	21	,	,	PUNCT
eurjchem-966	20	22	was	be	AUX
eurjchem-966	20	23	studied	study	VERB
eurjchem-966	20	24	at	at	ADP
eurjchem-966	20	25	different	different	ADJ
eurjchem-966	20	26	ph	ph	ADJ
eurjchem-966	20	27	values	value	NOUN
eurjchem-966	20	28	[	[	X
eurjchem-966	20	29	6	6	NUM
eurjchem-966	20	30	]	]	PUNCT
eurjchem-966	20	31	.	.	PUNCT
eurjchem-966	21	1	application	application	NOUN
eurjchem-966	21	2	of	of	ADP
eurjchem-966	21	3	partial	partial	ADJ
eurjchem-966	21	4	least	least	ADV
eurjchem-966	21	5	square	square	ADJ
eurjchem-966	21	6	(	(	PUNCT
eurjchem-966	21	7	pls	pls	INTJ
eurjchem-966	21	8	)	)	PUNCT
eurjchem-966	21	9	chemometric	chemometric	ADJ
eurjchem-966	21	10	method	method	NOUN
eurjchem-966	21	11	for	for	ADP
eurjchem-966	21	12	resolving	resolve	VERB
eurjchem-966	21	13	a	a	DET
eurjchem-966	21	14	mixture	mixture	NOUN
eurjchem-966	21	15	of	of	ADP
eurjchem-966	21	16	acemetacin	acemetacin	ADV
eurjchem-966	21	17	and	and	CCONJ
eurjchem-966	21	18	indomethacin	indomethacin	NOUN
eurjchem-966	21	19	mixture	mixture	NOUN
eurjchem-966	21	20	was	be	AUX
eurjchem-966	21	21	reported	report	VERB
eurjchem-966	21	22	[	[	X
eurjchem-966	21	23	7	7	NUM
eurjchem-966	21	24	]	]	PUNCT
eurjchem-966	21	25	.	.	PUNCT
eurjchem-966	22	1	additionally	additionally	ADV
eurjchem-966	22	2	,	,	PUNCT
eurjchem-966	22	3	it	it	PRON
eurjchem-966	22	4	was	be	AUX
eurjchem-966	22	5	determined	determine	VERB
eurjchem-966	22	6	in	in	ADP
eurjchem-966	22	7	plasma	plasma	NOUN
eurjchem-966	22	8	as	as	ADV
eurjchem-966	22	9	well	well	ADV
eurjchem-966	22	10	by	by	ADP
eurjchem-966	22	11	and	and	CCONJ
eurjchem-966	22	12	hplc	hplc	X
eurjchem-966	23	1	[	[	X
eurjchem-966	23	2	8‐10	8‐10	NUM
eurjchem-966	23	3	]	]	X
eurjchem-966	23	4	and	and	CCONJ
eurjchem-966	23	5	voltammetry	voltammetry	NOUN
eurjchem-966	24	1	[	[	X
eurjchem-966	24	2	11	11	NUM
eurjchem-966	24	3	]	]	PUNCT
eurjchem-966	24	4	.	.	PUNCT
eurjchem-966	25	1	none	none	NOUN
eurjchem-966	25	2	of	of	ADP
eurjchem-966	25	3	the	the	DET
eurjchem-966	25	4	reported	report	VERB
eurjchem-966	25	5	methods	method	NOUN
eurjchem-966	25	6	have	have	AUX
eurjchem-966	25	7	described	describe	VERB
eurjchem-966	25	8	a	a	DET
eurjchem-966	25	9	stability‐	stability‐	NOUN
eurjchem-966	25	10	indicating	indicate	VERB
eurjchem-966	25	11	method	method	NOUN
eurjchem-966	25	12	for	for	ADP
eurjchem-966	25	13	the	the	DET
eurjchem-966	25	14	determination	determination	NOUN
eurjchem-966	25	15	of	of	ADP
eurjchem-966	25	16	acm	acm	NOUN
eurjchem-966	25	17	in	in	ADP
eurjchem-966	25	18	capsule	capsule	ADJ
eurjchem-966	25	19	dosage	dosage	NOUN
eurjchem-966	25	20	form	form	NOUN
eurjchem-966	25	21	.	.	PUNCT
eurjchem-966	26	1	therefore	therefore	ADV
eurjchem-966	26	2	,	,	PUNCT
eurjchem-966	26	3	the	the	DET
eurjchem-966	26	4	aim	aim	NOUN
eurjchem-966	26	5	of	of	ADP
eurjchem-966	26	6	this	this	DET
eurjchem-966	26	7	manuscript	manuscript	NOUN
eurjchem-966	26	8	is	be	AUX
eurjchem-966	26	9	to	to	PART
eurjchem-966	26	10	establish	establish	VERB
eurjchem-966	26	11	and	and	CCONJ
eurjchem-966	26	12	validate	validate	VERB
eurjchem-966	26	13	stability‐indicating	stability‐indicate	VERB
eurjchem-966	26	14	methods	method	NOUN
eurjchem-966	26	15	for	for	ADP
eurjchem-966	26	16	the	the	DET
eurjchem-966	26	17	determination	determination	NOUN
eurjchem-966	26	18	of	of	ADP
eurjchem-966	26	19	active	active	ADJ
eurjchem-966	26	20	compound	compound	NOUN
eurjchem-966	26	21	in	in	ADP
eurjchem-966	26	22	the	the	DET
eurjchem-966	26	23	presence	presence	NOUN
eurjchem-966	26	24	of	of	ADP
eurjchem-966	26	25	its	its	PRON
eurjchem-966	26	26	degradation	degradation	NOUN
eurjchem-966	26	27	product	product	NOUN
eurjchem-966	26	28	.	.	PUNCT
eurjchem-966	27	1	to	to	PART
eurjchem-966	27	2	establish	establish	VERB
eurjchem-966	27	3	the	the	DET
eurjchem-966	27	4	stability‐indicating	stability‐indicate	VERB
eurjchem-966	27	5	nature	nature	NOUN
eurjchem-966	27	6	of	of	ADP
eurjchem-966	27	7	the	the	DET
eurjchem-966	27	8	methods	method	NOUN
eurjchem-966	27	9	,	,	PUNCT
eurjchem-966	27	10	forced	force	VERB
eurjchem-966	27	11	degradation	degradation	NOUN
eurjchem-966	27	12	of	of	ADP
eurjchem-966	27	13	acm	acm	NOUN
eurjchem-966	27	14	was	be	AUX
eurjchem-966	27	15	performed	perform	VERB
eurjchem-966	27	16	under	under	ADP
eurjchem-966	27	17	stress	stress	NOUN
eurjchem-966	27	18	conditions	condition	NOUN
eurjchem-966	27	19	,	,	PUNCT
eurjchem-966	27	20	and	and	CCONJ
eurjchem-966	27	21	stressed	stress	VERB
eurjchem-966	27	22	samples	sample	NOUN
eurjchem-966	27	23	were	be	AUX
eurjchem-966	27	24	analyzed	analyze	VERB
eurjchem-966	27	25	by	by	ADP
eurjchem-966	27	26	use	use	NOUN
eurjchem-966	27	27	of	of	ADP
eurjchem-966	27	28	the	the	DET
eurjchem-966	27	29	proposed	propose	VERB
eurjchem-966	27	30	spectrophotometric	spectrophotometric	ADJ
eurjchem-966	27	31	and	and	CCONJ
eurjchem-966	27	32	hptlc	hptlc	NOUN
eurjchem-966	27	33	methods	method	NOUN
eurjchem-966	27	34	,	,	PUNCT
eurjchem-966	27	35	which	which	PRON
eurjchem-966	27	36	were	be	AUX
eurjchem-966	27	37	able	able	ADJ
eurjchem-966	27	38	to	to	PART
eurjchem-966	27	39	separate	separate	VERB
eurjchem-966	27	40	the	the	DET
eurjchem-966	27	41	drugs	drug	NOUN
eurjchem-966	27	42	from	from	ADP
eurjchem-966	27	43	compound	compound	NOUN
eurjchem-966	27	44	produced	produce	VERB
eurjchem-966	27	45	during	during	ADP
eurjchem-966	27	46	forced	force	VERB
eurjchem-966	27	47	degradation	degradation	NOUN
eurjchem-966	27	48	studies	study	NOUN
eurjchem-966	27	49	.	.	PUNCT
eurjchem-966	28	1	2	2	X
eurjchem-966	28	2	.	.	X
eurjchem-966	28	3	experimental	experimental	ADJ
eurjchem-966	28	4	2.1	2.1	NUM
eurjchem-966	28	5	.	.	PUNCT
eurjchem-966	28	6	instruments	instrument	NOUN
eurjchem-966	28	7	a	a	DET
eurjchem-966	28	8	double	double	ADJ
eurjchem-966	28	9	beam	beam	NOUN
eurjchem-966	28	10	uv‐vis	uv‐vis	PROPN
eurjchem-966	28	11	spectrophotometer	spectrophotometer	X
eurjchem-966	28	12	(	(	PUNCT
eurjchem-966	28	13	shimadzu	shimadzu	PROPN
eurjchem-966	28	14	,	,	PUNCT
eurjchem-966	28	15	japan	japan	PROPN
eurjchem-966	28	16	)	)	PUNCT
eurjchem-966	28	17	model	model	NOUN
eurjchem-966	28	18	uv‐1601	uv‐1601	PROPN
eurjchem-966	28	19	pc	pc	NOUN
eurjchem-966	28	20	with	with	ADP
eurjchem-966	28	21	quartz	quartz	NOUN
eurjchem-966	28	22	cell	cell	NOUN
eurjchem-966	28	23	of	of	ADP
eurjchem-966	28	24	1	1	NUM
eurjchem-966	28	25	cm	cm	NOUN
eurjchem-966	28	26	pathlength	pathlength	NOUN
eurjchem-966	28	27	,	,	PUNCT
eurjchem-966	28	28	connected	connect	VERB
eurjchem-966	28	29	to	to	ADP
eurjchem-966	28	30	ibm	ibm	PROPN
eurjchem-966	28	31	compatible	compatible	ADJ
eurjchem-966	28	32	computer	computer	NOUN
eurjchem-966	28	33	.	.	PUNCT
eurjchem-966	29	1	the	the	DET
eurjchem-966	29	2	software	software	NOUN
eurjchem-966	29	3	was	be	AUX
eurjchem-966	29	4	uvpc	uvpc	ADJ
eurjchem-966	29	5	personal	personal	ADJ
eurjchem-966	29	6	spectroscopy	spectroscopy	NOUN
eurjchem-966	29	7	software	software	NOUN
eurjchem-966	29	8	version	version	NOUN
eurjchem-966	29	9	3.7	3.7	NUM
eurjchem-966	29	10	.	.	PUNCT
eurjchem-966	30	1	data	datum	NOUN
eurjchem-966	30	2	concerning	concern	VERB
eurjchem-966	30	3	mcr	mcr	PROPN
eurjchem-966	30	4	was	be	AUX
eurjchem-966	30	5	performed	perform	VERB
eurjchem-966	30	6	using	use	VERB
eurjchem-966	30	7	pls‐toolbox	pls‐toolbox	ADP
eurjchem-966	30	8	2.0	2.0	NUM
eurjchem-966	30	9	running	run	VERB
eurjchem-966	30	10	under	under	ADP
eurjchem-966	30	11	matlab	matlab	PROPN
eurjchem-966	30	12	®	®	PROPN
eurjchem-966	30	13	,	,	PUNCT
eurjchem-966	30	14	version	version	NOUN
eurjchem-966	30	15	(	(	PUNCT
eurjchem-966	30	16	r2007b	r2007b	NOUN
eurjchem-966	30	17	)	)	PUNCT
eurjchem-966	30	18	.	.	PUNCT
eurjchem-966	31	1	camag	camag	VERB
eurjchem-966	31	2	tlc	tlc	NOUN
eurjchem-966	31	3	scanner	scanner	NOUN
eurjchem-966	31	4	3	3	NUM
eurjchem-966	31	5	s	s	NOUN
eurjchem-966	31	6	/	/	SYM
eurjchem-966	31	7	n	n	PRON
eurjchem-966	31	8	130319	130319	NUM
eurjchem-966	31	9	operated	operate	VERB
eurjchem-966	31	10	with	with	ADP
eurjchem-966	31	11	wincats	wincat	NOUN
eurjchem-966	31	12	software	software	PROPN
eurjchem-966	31	13	.	.	PUNCT
eurjchem-966	32	1	the	the	DET
eurjchem-966	32	2	following	follow	VERB
eurjchem-966	32	3	requirements	requirement	NOUN
eurjchem-966	32	4	are	be	AUX
eurjchem-966	32	5	taken	take	VERB
eurjchem-966	32	6	into	into	ADP
eurjchem-966	32	7	consideration	consideration	NOUN
eurjchem-966	32	8	:	:	PUNCT
eurjchem-966	32	9	slit	slit	ADJ
eurjchem-966	32	10	dimensions	dimension	NOUN
eurjchem-966	32	11	:	:	PUNCT
eurjchem-966	32	12	6	6	NUM
eurjchem-966	32	13	×	×	NOUN
eurjchem-966	32	14	0.3	0.3	NUM
eurjchem-966	32	15	mm	mm	NOUN
eurjchem-966	32	16	,	,	PUNCT
eurjchem-966	32	17	scanning	scan	VERB
eurjchem-966	32	18	speed	speed	NOUN
eurjchem-966	32	19	:	:	PUNCT
eurjchem-966	32	20	20	20	NUM
eurjchem-966	32	21	mm	mm	NOUN
eurjchem-966	32	22	/	/	SYM
eurjchem-966	32	23	s	s	PROPN
eurjchem-966	32	24	,	,	PUNCT
eurjchem-966	32	25	spraying	spray	VERB
eurjchem-966	32	26	rate	rate	NOUN
eurjchem-966	32	27	:	:	PUNCT
eurjchem-966	32	28	10	10	NUM
eurjchem-966	32	29	s/µl	s/µl	PROPN
eurjchem-966	32	30	,	,	PUNCT
eurjchem-966	32	31	data	datum	NOUN
eurjchem-966	32	32	resolution	resolution	NOUN
eurjchem-966	32	33	:	:	PUNCT
eurjchem-966	32	34	100	100	NUM
eurjchem-966	32	35	µm	µm	NOUN
eurjchem-966	32	36	/	/	SYM
eurjchem-966	32	37	step	step	NOUN
eurjchem-966	32	38	,	,	PUNCT
eurjchem-966	32	39	band	band	NOUN
eurjchem-966	32	40	width	width	NOUN
eurjchem-966	32	41	:	:	PUNCT
eurjchem-966	32	42	6	6	NUM
eurjchem-966	32	43	mm	mm	NOUN
eurjchem-966	32	44	,	,	PUNCT
eurjchem-966	32	45	result	result	NOUN
eurjchem-966	32	46	output	output	NOUN
eurjchem-966	32	47	:	:	PUNCT
eurjchem-966	32	48	chromatogram	chromatogram	PROPN
eurjchem-966	32	49	and	and	CCONJ
eurjchem-966	32	50	integrated	integrate	VERB
eurjchem-966	32	51	peak	peak	NOUN
eurjchem-966	32	52	area	area	NOUN
eurjchem-966	32	53	,	,	PUNCT
eurjchem-966	32	54	linomat	linomat	NOUN
eurjchem-966	32	55	iv	iv	NUM
eurjchem-966	32	56	with	with	ADP
eurjchem-966	32	57	100	100	NUM
eurjchem-966	32	58	220	220	NUM
eurjchem-966	32	59	naguib	naguib	NOUN
eurjchem-966	32	60	et	et	PROPN
eurjchem-966	32	61	al	al	PROPN
eurjchem-966	32	62	.	.	PUNCT
eurjchem-966	32	63	/	/	SYM
eurjchem-966	32	64	european	european	PROPN
eurjchem-966	32	65	journal	journal	PROPN
eurjchem-966	32	66	of	of	ADP
eurjchem-966	32	67	chemistry	chemistry	NOUN
eurjchem-966	32	68	5	5	NUM
eurjchem-966	32	69	(	(	PUNCT
eurjchem-966	32	70	2	2	NUM
eurjchem-966	32	71	)	)	PUNCT
eurjchem-966	32	72	(	(	PUNCT
eurjchem-966	32	73	2014	2014	NUM
eurjchem-966	32	74	)	)	PUNCT
eurjchem-966	32	75	219‐226	219‐226	NUM
eurjchem-966	32	76	μl	μl	ADP
eurjchem-966	32	77	syringe	syringe	NOUN
eurjchem-966	32	78	(	(	PUNCT
eurjchem-966	32	79	camag	camag	NOUN
eurjchem-966	32	80	,	,	PUNCT
eurjchem-966	32	81	muttenz	muttenz	NOUN
eurjchem-966	32	82	,	,	PUNCT
eurjchem-966	32	83	switzerland	switzerland	PROPN
eurjchem-966	32	84	)	)	PUNCT
eurjchem-966	32	85	,	,	PUNCT
eurjchem-966	32	86	hptlc	hptlc	NOUN
eurjchem-966	32	87	aluminum	aluminum	NOUN
eurjchem-966	32	88	plates	plate	NOUN
eurjchem-966	32	89	(	(	PUNCT
eurjchem-966	32	90	20	20	NUM
eurjchem-966	32	91	x	x	SYM
eurjchem-966	32	92	20	20	NUM
eurjchem-966	32	93	cm	cm	NOUN
eurjchem-966	32	94	)	)	PUNCT
eurjchem-966	32	95	coated	coat	VERB
eurjchem-966	32	96	with	with	ADP
eurjchem-966	32	97	0.25	0.25	NUM
eurjchem-966	32	98	mm	mm	NOUN
eurjchem-966	32	99	silica	silica	NOUN
eurjchem-966	32	100	gel	gel	NOUN
eurjchem-966	32	101	60f254	60f254	NOUN
eurjchem-966	32	102	(	(	PUNCT
eurjchem-966	32	103	merck	merck	PROPN
eurjchem-966	32	104	,	,	PUNCT
eurjchem-966	32	105	germany	germany	PROPN
eurjchem-966	32	106	)	)	PUNCT
eurjchem-966	32	107	.	.	PUNCT
eurjchem-966	33	1	sonix	sonix	NOUN
eurjchem-966	33	2	tv	tv	PROPN
eurjchem-966	33	3	ss‐series	ss‐serie	NOUN
eurjchem-966	33	4	ultrasonicator	ultrasonicator	NOUN
eurjchem-966	33	5	(	(	PUNCT
eurjchem-966	33	6	usa	usa	PROPN
eurjchem-966	33	7	)	)	PUNCT
eurjchem-966	33	8	.	.	PUNCT
eurjchem-966	34	1	2.2	2.2	NUM
eurjchem-966	34	2	.	.	PUNCT
eurjchem-966	34	3	material	material	NOUN
eurjchem-966	34	4	and	and	CCONJ
eurjchem-966	34	5	reagents	reagent	NOUN
eurjchem-966	34	6	2.2.1	2.2.1	NUM
eurjchem-966	34	7	pure	pure	ADJ
eurjchem-966	34	8	standard	standard	ADJ
eurjchem-966	34	9	acm	acm	PROPN
eurjchem-966	34	10	was	be	AUX
eurjchem-966	34	11	purchased	purchase	VERB
eurjchem-966	34	12	from	from	ADP
eurjchem-966	34	13	sigma‐aldrich	sigma‐aldrich	NOUN
eurjchem-966	34	14	through	through	ADP
eurjchem-966	34	15	the	the	DET
eurjchem-966	34	16	egyptian	egyptian	ADJ
eurjchem-966	34	17	international	international	ADJ
eurjchem-966	34	18	center	center	NOUN
eurjchem-966	34	19	for	for	ADP
eurjchem-966	34	20	import	import	NOUN
eurjchem-966	34	21	and	and	CCONJ
eurjchem-966	34	22	export	export	NOUN
eurjchem-966	34	23	(	(	PUNCT
eurjchem-966	34	24	eic	eic	PROPN
eurjchem-966	34	25	,	,	PUNCT
eurjchem-966	34	26	egypt	egypt	PROPN
eurjchem-966	34	27	)	)	PUNCT
eurjchem-966	34	28	.	.	PUNCT
eurjchem-966	35	1	its	its	PRON
eurjchem-966	35	2	purity	purity	NOUN
eurjchem-966	35	3	was	be	AUX
eurjchem-966	35	4	certified	certify	VERB
eurjchem-966	35	5	to	to	PART
eurjchem-966	35	6	be	be	AUX
eurjchem-966	35	7	98.00	98.00	NUM
eurjchem-966	35	8	%	%	NOUN
eurjchem-966	35	9	according	accord	VERB
eurjchem-966	35	10	to	to	ADP
eurjchem-966	35	11	the	the	DET
eurjchem-966	35	12	company	company	NOUN
eurjchem-966	35	13	’s	’s	PART
eurjchem-966	35	14	certificate	certificate	NOUN
eurjchem-966	35	15	of	of	ADP
eurjchem-966	35	16	analysis	analysis	NOUN
eurjchem-966	35	17	.	.	PUNCT
eurjchem-966	36	1	indomethacin	indomethacin	PROPN
eurjchem-966	36	2	was	be	AUX
eurjchem-966	36	3	kindly	kindly	ADV
eurjchem-966	36	4	supplied	supply	VERB
eurjchem-966	36	5	by	by	ADP
eurjchem-966	36	6	pharco	pharco	PROPN
eurjchem-966	36	7	pharmaceuticals	pharmaceuticals	PROPN
eurjchem-966	36	8	co.	co.	PROPN
eurjchem-966	36	9	,	,	PUNCT
eurjchem-966	36	10	egypt	egypt	PROPN
eurjchem-966	36	11	.	.	PUNCT
eurjchem-966	37	1	2.2.2	2.2.2	X
eurjchem-966	37	2	.	.	PUNCT
eurjchem-966	37	3	pharmaceutical	pharmaceutical	ADJ
eurjchem-966	37	4	preparation	preparation	NOUN
eurjchem-966	37	5	ostmap	ostmap	NOUN
eurjchem-966	37	6	®	®	NOUN
eurjchem-966	37	7	capsules	capsule	NOUN
eurjchem-966	37	8	batch	batch	VERB
eurjchem-966	37	9	no	no	PRON
eurjchem-966	37	10	(	(	PUNCT
eurjchem-966	37	11	mt	mt	PROPN
eurjchem-966	37	12	3710911	3710911	NUM
eurjchem-966	37	13	)	)	PUNCT
eurjchem-966	37	14	were	be	AUX
eurjchem-966	37	15	manufactured	manufacture	VERB
eurjchem-966	37	16	by	by	ADP
eurjchem-966	37	17	multi‐apex	multi‐apex	PROPN
eurjchem-966	37	18	pharmaceutical	pharmaceutical	PROPN
eurjchem-966	37	19	industries	industry	NOUN
eurjchem-966	37	20	co.	co.	PROPN
eurjchem-966	37	21	(	(	PUNCT
eurjchem-966	37	22	maisons‐alfort	maisons‐alfort	PROPN
eurjchem-966	37	23	,	,	PUNCT
eurjchem-966	37	24	france	france	PROPN
eurjchem-966	37	25	)	)	PUNCT
eurjchem-966	37	26	,	,	PUNCT
eurjchem-966	37	27	each	each	DET
eurjchem-966	37	28	capsule	capsule	NOUN
eurjchem-966	37	29	is	be	AUX
eurjchem-966	37	30	claimed	claim	VERB
eurjchem-966	37	31	to	to	PART
eurjchem-966	37	32	contain	contain	VERB
eurjchem-966	37	33	60	60	NUM
eurjchem-966	37	34	mg	mg	NOUN
eurjchem-966	37	35	of	of	ADP
eurjchem-966	37	36	acm	acm	PROPN
eurjchem-966	37	37	.	.	PUNCT
eurjchem-966	38	1	2.2.3	2.2.3	NUM
eurjchem-966	38	2	.	.	PUNCT
eurjchem-966	38	3	chemicals	chemical	NOUN
eurjchem-966	38	4	and	and	CCONJ
eurjchem-966	38	5	reagents	reagent	NOUN
eurjchem-966	38	6	all	all	DET
eurjchem-966	38	7	chemicals	chemical	NOUN
eurjchem-966	38	8	and	and	CCONJ
eurjchem-966	38	9	solvents	solvent	NOUN
eurjchem-966	38	10	used	use	VERB
eurjchem-966	38	11	were	be	AUX
eurjchem-966	38	12	of	of	ADP
eurjchem-966	38	13	analytical	analytical	ADJ
eurjchem-966	38	14	grade	grade	NOUN
eurjchem-966	38	15	,	,	PUNCT
eurjchem-966	38	16	methanol	methanol	NOUN
eurjchem-966	38	17	(	(	PUNCT
eurjchem-966	38	18	e.	e.	PROPN
eurjchem-966	38	19	merck	merck	PROPN
eurjchem-966	38	20	,	,	PUNCT
eurjchem-966	38	21	germany	germany	PROPN
eurjchem-966	38	22	)	)	PUNCT
eurjchem-966	38	23	.	.	PUNCT
eurjchem-966	39	1	purified	purified	ADJ
eurjchem-966	39	2	water	water	NOUN
eurjchem-966	39	3	(	(	PUNCT
eurjchem-966	39	4	3a	3a	PROPN
eurjchem-966	39	5	international	international	PROPN
eurjchem-966	39	6	co.	co.	PROPN
eurjchem-966	39	7	,	,	PUNCT
eurjchem-966	39	8	kalubia	kalubia	PROPN
eurjchem-966	39	9	,	,	PUNCT
eurjchem-966	39	10	egypt	egypt	PROPN
eurjchem-966	39	11	)	)	PUNCT
eurjchem-966	39	12	.	.	PUNCT
eurjchem-966	40	1	sodium	sodium	NOUN
eurjchem-966	40	2	hydroxide	hydroxide	PROPN
eurjchem-966	40	3	,	,	PUNCT
eurjchem-966	40	4	hydrochloric	hydrochloric	ADJ
eurjchem-966	40	5	acid	acid	NOUN
eurjchem-966	40	6	,	,	PUNCT
eurjchem-966	40	7	30	30	NUM
eurjchem-966	40	8	%	%	NOUN
eurjchem-966	40	9	hydrogen	hydrogen	NOUN
eurjchem-966	40	10	peroxide	peroxide	NOUN
eurjchem-966	40	11	solution	solution	NOUN
eurjchem-966	40	12	,	,	PUNCT
eurjchem-966	40	13	hexane	hexane	NOUN
eurjchem-966	40	14	,	,	PUNCT
eurjchem-966	40	15	ethyl	ethyl	PROPN
eurjchem-966	40	16	acetate	acetate	PROPN
eurjchem-966	40	17	and	and	CCONJ
eurjchem-966	40	18	glacial	glacial	ADJ
eurjchem-966	40	19	acetic	acetic	ADJ
eurjchem-966	40	20	acid	acid	NOUN
eurjchem-966	40	21	(	(	PUNCT
eurjchem-966	40	22	el‐nasr	el‐nasr	NOUN
eurjchem-966	40	23	pharmaceutical	pharmaceutical	PROPN
eurjchem-966	40	24	chemicals	chemicals	PROPN
eurjchem-966	40	25	co.	co.	PROPN
eurjchem-966	40	26	,	,	PUNCT
eurjchem-966	40	27	abu‐zabaal	abu‐zabaal	PROPN
eurjchem-966	40	28	,	,	PUNCT
eurjchem-966	40	29	cairo	cairo	PROPN
eurjchem-966	40	30	,	,	PUNCT
eurjchem-966	40	31	egypt	egypt	PROPN
eurjchem-966	40	32	)	)	PUNCT
eurjchem-966	40	33	.	.	PUNCT
eurjchem-966	41	1	2.2.4	2.2.4	NUM
eurjchem-966	41	2	.	.	PUNCT
eurjchem-966	41	3	degraded	degraded	ADJ
eurjchem-966	41	4	sample	sample	NOUN
eurjchem-966	41	5	a	a	DET
eurjchem-966	41	6	stock	stock	NOUN
eurjchem-966	41	7	solution	solution	NOUN
eurjchem-966	41	8	containing	contain	VERB
eurjchem-966	41	9	0.1	0.1	NUM
eurjchem-966	41	10	g	g	NOUN
eurjchem-966	41	11	of	of	ADP
eurjchem-966	41	12	acm	acm	NOUN
eurjchem-966	41	13	in	in	ADP
eurjchem-966	41	14	100	100	NUM
eurjchem-966	41	15	ml	ml	NOUN
eurjchem-966	41	16	methanol	methanol	NOUN
eurjchem-966	41	17	was	be	AUX
eurjchem-966	41	18	prepared	prepare	VERB
eurjchem-966	41	19	.	.	PUNCT
eurjchem-966	42	1	this	this	DET
eurjchem-966	42	2	solution	solution	NOUN
eurjchem-966	42	3	was	be	AUX
eurjchem-966	42	4	used	use	VERB
eurjchem-966	42	5	for	for	ADP
eurjchem-966	42	6	forced	force	VERB
eurjchem-966	42	7	degradation	degradation	NOUN
eurjchem-966	42	8	under	under	ADP
eurjchem-966	42	9	variety	variety	NOUN
eurjchem-966	42	10	of	of	ADP
eurjchem-966	42	11	conditions	condition	NOUN
eurjchem-966	42	12	such	such	ADJ
eurjchem-966	42	13	as	as	ADP
eurjchem-966	42	14	:	:	PUNCT
eurjchem-966	42	15	acid	acid	ADJ
eurjchem-966	42	16	and	and	CCONJ
eurjchem-966	42	17	alkaline	alkaline	NOUN
eurjchem-966	42	18	hydrolysis	hydrolysis	NOUN
eurjchem-966	42	19	,	,	PUNCT
eurjchem-966	42	20	oxidation	oxidation	NOUN
eurjchem-966	42	21	and	and	CCONJ
eurjchem-966	42	22	photodegradation	photodegradation	NOUN
eurjchem-966	42	23	.	.	PUNCT
eurjchem-966	43	1	alkaline	alkaline	NOUN
eurjchem-966	43	2	hydrolysis	hydrolysis	NOUN
eurjchem-966	43	3	was	be	AUX
eurjchem-966	43	4	performed	perform	VERB
eurjchem-966	43	5	by	by	ADP
eurjchem-966	43	6	adding	add	VERB
eurjchem-966	43	7	5	5	NUM
eurjchem-966	43	8	ml	ml	NOUN
eurjchem-966	43	9	of	of	ADP
eurjchem-966	43	10	0.1	0.1	NUM
eurjchem-966	43	11	m	m	NOUN
eurjchem-966	43	12	naoh	naoh	NOUN
eurjchem-966	43	13	solution	solution	NOUN
eurjchem-966	43	14	to	to	ADP
eurjchem-966	43	15	5	5	NUM
eurjchem-966	43	16	ml	ml	NOUN
eurjchem-966	43	17	of	of	ADP
eurjchem-966	43	18	acm	acm	NOUN
eurjchem-966	43	19	stock	stock	NOUN
eurjchem-966	43	20	solution	solution	NOUN
eurjchem-966	43	21	and	and	CCONJ
eurjchem-966	43	22	standing	stand	VERB
eurjchem-966	43	23	for	for	ADP
eurjchem-966	43	24	about	about	ADV
eurjchem-966	43	25	30	30	NUM
eurjchem-966	43	26	minutes	minute	NOUN
eurjchem-966	43	27	at	at	ADP
eurjchem-966	43	28	room	room	NOUN
eurjchem-966	43	29	temperature	temperature	NOUN
eurjchem-966	43	30	.	.	PUNCT
eurjchem-966	44	1	acid	acid	NOUN
eurjchem-966	44	2	hydrolysis	hydrolysis	NOUN
eurjchem-966	44	3	was	be	AUX
eurjchem-966	44	4	carried	carry	VERB
eurjchem-966	44	5	out	out	ADP
eurjchem-966	44	6	by	by	ADP
eurjchem-966	44	7	refluxing	refluxe	VERB
eurjchem-966	44	8	with	with	ADP
eurjchem-966	44	9	0.1	0.1	NUM
eurjchem-966	44	10	m	m	NOUN
eurjchem-966	44	11	hcl	hcl	PROPN
eurjchem-966	44	12	at	at	ADP
eurjchem-966	44	13	80	80	NUM
eurjchem-966	44	14	°	°	NOUN
eurjchem-966	44	15	c	c	NOUN
eurjchem-966	44	16	for	for	ADP
eurjchem-966	44	17	about	about	ADV
eurjchem-966	44	18	4	4	NUM
eurjchem-966	44	19	h.	h.	NOUN
eurjchem-966	44	20	oxidation	oxidation	NOUN
eurjchem-966	44	21	studies	study	NOUN
eurjchem-966	44	22	were	be	AUX
eurjchem-966	44	23	implemented	implement	VERB
eurjchem-966	44	24	using	use	VERB
eurjchem-966	44	25	30	30	NUM
eurjchem-966	44	26	%	%	NOUN
eurjchem-966	44	27	hydrogen	hydrogen	NOUN
eurjchem-966	44	28	peroxide	peroxide	NOUN
eurjchem-966	44	29	solution	solution	NOUN
eurjchem-966	44	30	.	.	PUNCT
eurjchem-966	45	1	finally	finally	ADV
eurjchem-966	45	2	,	,	PUNCT
eurjchem-966	45	3	photochemical	photochemical	ADJ
eurjchem-966	45	4	stability	stability	NOUN
eurjchem-966	45	5	was	be	AUX
eurjchem-966	45	6	studied	study	VERB
eurjchem-966	45	7	by	by	ADP
eurjchem-966	45	8	exposing	expose	VERB
eurjchem-966	45	9	the	the	DET
eurjchem-966	45	10	drug	drug	NOUN
eurjchem-966	45	11	sample	sample	NOUN
eurjchem-966	45	12	to	to	PART
eurjchem-966	45	13	daylight	daylight	VERB
eurjchem-966	45	14	for	for	ADP
eurjchem-966	45	15	24	24	NUM
eurjchem-966	45	16	hours	hour	NOUN
eurjchem-966	45	17	.	.	PUNCT
eurjchem-966	46	1	appropriate	appropriate	ADJ
eurjchem-966	46	2	volume	volume	NOUN
eurjchem-966	46	3	of	of	ADP
eurjchem-966	46	4	the	the	DET
eurjchem-966	46	5	resultant	resultant	NOUN
eurjchem-966	46	6	solution	solution	NOUN
eurjchem-966	46	7	was	be	AUX
eurjchem-966	46	8	applied	apply	VERB
eurjchem-966	46	9	on	on	ADP
eurjchem-966	46	10	tlc	tlc	NOUN
eurjchem-966	46	11	plate	plate	NOUN
eurjchem-966	46	12	where	where	SCONJ
eurjchem-966	46	13	complete	complete	ADJ
eurjchem-966	46	14	degradation	degradation	NOUN
eurjchem-966	46	15	was	be	AUX
eurjchem-966	46	16	followed	follow	VERB
eurjchem-966	46	17	up	up	ADP
eurjchem-966	46	18	via	via	ADP
eurjchem-966	46	19	tlc	tlc	NOUN
eurjchem-966	46	20	using	use	VERB
eurjchem-966	46	21	hexane	hexane	NOUN
eurjchem-966	46	22	:	:	PUNCT
eurjchem-966	46	23	ethyl	ethyl	PROPN
eurjchem-966	46	24	acetate	acetate	PROPN
eurjchem-966	46	25	:	:	PUNCT
eurjchem-966	46	26	glacial	glacial	ADJ
eurjchem-966	46	27	acetic	acetic	ADJ
eurjchem-966	46	28	acid	acid	NOUN
eurjchem-966	46	29	(	(	PUNCT
eurjchem-966	46	30	6:4:0.3	6:4:0.3	PROPN
eurjchem-966	46	31	,	,	PUNCT
eurjchem-966	46	32	v	v	NOUN
eurjchem-966	46	33	:	:	PUNCT
eurjchem-966	46	34	v	v	ADJ
eurjchem-966	46	35	:	:	PUNCT
eurjchem-966	46	36	v	v	NOUN
eurjchem-966	46	37	)	)	PUNCT
eurjchem-966	46	38	as	as	ADP
eurjchem-966	46	39	developing	develop	VERB
eurjchem-966	46	40	system	system	NOUN
eurjchem-966	46	41	till	till	SCONJ
eurjchem-966	46	42	complete	complete	ADJ
eurjchem-966	46	43	disappearance	disappearance	NOUN
eurjchem-966	46	44	of	of	ADP
eurjchem-966	46	45	acm	acm	NOUN
eurjchem-966	46	46	spot	spot	NOUN
eurjchem-966	46	47	.	.	PUNCT
eurjchem-966	47	1	pure	pure	ADJ
eurjchem-966	47	2	standard	standard	NOUN
eurjchem-966	47	3	of	of	ADP
eurjchem-966	47	4	indomethacin	indomethacin	ADJ
eurjchem-966	47	5	solution	solution	NOUN
eurjchem-966	47	6	was	be	AUX
eurjchem-966	47	7	used	use	VERB
eurjchem-966	47	8	for	for	ADP
eurjchem-966	47	9	comparison	comparison	NOUN
eurjchem-966	47	10	and	and	CCONJ
eurjchem-966	47	11	its	its	PRON
eurjchem-966	47	12	rf	rf	NOUN
eurjchem-966	47	13	was	be	AUX
eurjchem-966	47	14	coinciding	coincide	VERB
eurjchem-966	47	15	with	with	ADP
eurjchem-966	47	16	the	the	DET
eurjchem-966	47	17	resultant	resultant	NOUN
eurjchem-966	47	18	degradation	degradation	NOUN
eurjchem-966	47	19	product	product	NOUN
eurjchem-966	47	20	(	(	PUNCT
eurjchem-966	47	21	deg	deg	PROPN
eurjchem-966	47	22	)	)	PUNCT
eurjchem-966	47	23	.	.	PUNCT
eurjchem-966	48	1	furthermore	furthermore	ADV
eurjchem-966	48	2	,	,	PUNCT
eurjchem-966	48	3	the	the	DET
eurjchem-966	48	4	degradation	degradation	NOUN
eurjchem-966	48	5	product	product	NOUN
eurjchem-966	48	6	was	be	AUX
eurjchem-966	48	7	elucidated	elucidate	VERB
eurjchem-966	48	8	by	by	ADP
eurjchem-966	48	9	ir	ir	PROPN
eurjchem-966	48	10	and	and	CCONJ
eurjchem-966	48	11	mass	mass	ADJ
eurjchem-966	48	12	spectrometry	spectrometry	NOUN
eurjchem-966	48	13	.	.	PUNCT
eurjchem-966	49	1	2.3	2.3	NUM
eurjchem-966	49	2	.	.	PUNCT
eurjchem-966	50	1	standard	standard	ADJ
eurjchem-966	50	2	solutions	solution	NOUN
eurjchem-966	50	3	stock	stock	NOUN
eurjchem-966	50	4	standard	standard	ADJ
eurjchem-966	50	5	solutions	solution	NOUN
eurjchem-966	50	6	of	of	ADP
eurjchem-966	50	7	acm	acm	PROPN
eurjchem-966	50	8	and	and	CCONJ
eurjchem-966	50	9	deg	deg	NOUN
eurjchem-966	50	10	1	1	NUM
eurjchem-966	50	11	mg	mg	PROPN
eurjchem-966	50	12	/	/	SYM
eurjchem-966	50	13	ml	ml	PROPN
eurjchem-966	50	14	of	of	ADP
eurjchem-966	50	15	each	each	PRON
eurjchem-966	50	16	in	in	ADP
eurjchem-966	50	17	methanol	methanol	NOUN
eurjchem-966	50	18	.	.	PUNCT
eurjchem-966	51	1	working	work	VERB
eurjchem-966	51	2	standard	standard	ADJ
eurjchem-966	51	3	solutions	solution	NOUN
eurjchem-966	51	4	of	of	ADP
eurjchem-966	51	5	acm	acm	PROPN
eurjchem-966	51	6	and	and	CCONJ
eurjchem-966	51	7	deg	deg	VERB
eurjchem-966	51	8	100	100	NUM
eurjchem-966	51	9	µg	µg	NOUN
eurjchem-966	51	10	/	/	SYM
eurjchem-966	51	11	ml	ml	NOUN
eurjchem-966	51	12	of	of	ADP
eurjchem-966	51	13	each	each	PRON
eurjchem-966	51	14	in	in	ADP
eurjchem-966	51	15	methanol	methanol	NOUN
eurjchem-966	51	16	.	.	PUNCT
eurjchem-966	52	1	all	all	DET
eurjchem-966	52	2	stock	stock	NOUN
eurjchem-966	52	3	standard	standard	ADJ
eurjchem-966	52	4	solutions	solution	NOUN
eurjchem-966	52	5	were	be	AUX
eurjchem-966	52	6	freshly	freshly	ADV
eurjchem-966	52	7	prepared	prepared	ADJ
eurjchem-966	52	8	on	on	ADP
eurjchem-966	52	9	the	the	DET
eurjchem-966	52	10	day	day	NOUN
eurjchem-966	52	11	of	of	ADP
eurjchem-966	52	12	analysis	analysis	NOUN
eurjchem-966	52	13	and	and	CCONJ
eurjchem-966	52	14	stored	store	VERB
eurjchem-966	52	15	in	in	ADP
eurjchem-966	52	16	refrigerator	refrigerator	NOUN
eurjchem-966	52	17	to	to	PART
eurjchem-966	52	18	be	be	AUX
eurjchem-966	52	19	used	use	VERB
eurjchem-966	52	20	within	within	ADP
eurjchem-966	52	21	24	24	NUM
eurjchem-966	52	22	h.	h.	PROPN
eurjchem-966	52	23	2.4	2.4	NUM
eurjchem-966	52	24	.	.	PUNCT
eurjchem-966	53	1	methods	method	NOUN
eurjchem-966	53	2	2.4.1	2.4.1	NUM
eurjchem-966	53	3	.	.	PUNCT
eurjchem-966	53	4	spectrophotometric	spectrophotometric	ADJ
eurjchem-966	53	5	methods	method	NOUN
eurjchem-966	53	6	2.4.1.1	2.4.1.1	NUM
eurjchem-966	53	7	.	.	PUNCT
eurjchem-966	54	1	construction	construction	NOUN
eurjchem-966	54	2	of	of	ADP
eurjchem-966	54	3	calibration	calibration	NOUN
eurjchem-966	54	4	curve	curve	NOUN
eurjchem-966	54	5	for	for	ADP
eurjchem-966	54	6	1dd	1dd	ADJ
eurjchem-966	54	7	spectrophotometric	spectrophotometric	ADJ
eurjchem-966	54	8	method	method	NOUN
eurjchem-966	54	9	accurately	accurately	ADV
eurjchem-966	54	10	measured	measure	VERB
eurjchem-966	54	11	aliquots	aliquot	NOUN
eurjchem-966	54	12	equivalent	equivalent	ADJ
eurjchem-966	54	13	to	to	ADP
eurjchem-966	54	14	20‐220	20‐220	NUM
eurjchem-966	54	15	µg	µg	ADV
eurjchem-966	54	16	of	of	ADP
eurjchem-966	54	17	acm	acm	NOUN
eurjchem-966	54	18	were	be	AUX
eurjchem-966	54	19	transferred	transfer	VERB
eurjchem-966	54	20	from	from	ADP
eurjchem-966	54	21	its	its	PRON
eurjchem-966	54	22	working	work	VERB
eurjchem-966	54	23	solution	solution	NOUN
eurjchem-966	54	24	(	(	PUNCT
eurjchem-966	54	25	100	100	NUM
eurjchem-966	54	26	µg	µg	ADJ
eurjchem-966	54	27	/	/	SYM
eurjchem-966	54	28	ml	ml	NOUN
eurjchem-966	54	29	)	)	PUNCT
eurjchem-966	54	30	into	into	ADP
eurjchem-966	54	31	a	a	DET
eurjchem-966	54	32	series	series	NOUN
eurjchem-966	54	33	of	of	ADP
eurjchem-966	54	34	10	10	NUM
eurjchem-966	54	35	ml	ml	NOUN
eurjchem-966	54	36	volumetric	volumetric	ADJ
eurjchem-966	54	37	flasks	flask	NOUN
eurjchem-966	54	38	.	.	PUNCT
eurjchem-966	55	1	the	the	DET
eurjchem-966	55	2	volume	volume	NOUN
eurjchem-966	55	3	was	be	AUX
eurjchem-966	55	4	completed	complete	VERB
eurjchem-966	55	5	with	with	ADP
eurjchem-966	55	6	purified	purified	ADJ
eurjchem-966	55	7	water	water	NOUN
eurjchem-966	55	8	to	to	PART
eurjchem-966	55	9	obtain	obtain	VERB
eurjchem-966	55	10	a	a	DET
eurjchem-966	55	11	final	final	ADJ
eurjchem-966	55	12	concentration	concentration	NOUN
eurjchem-966	55	13	range	range	NOUN
eurjchem-966	55	14	(	(	PUNCT
eurjchem-966	55	15	2‐22	2‐22	NUM
eurjchem-966	55	16	µg	µg	NOUN
eurjchem-966	55	17	/	/	SYM
eurjchem-966	55	18	ml	ml	NOUN
eurjchem-966	55	19	)	)	PUNCT
eurjchem-966	55	20	.	.	PUNCT
eurjchem-966	56	1	1dd	1dd	ADJ
eurjchem-966	56	2	curves	curve	NOUN
eurjchem-966	56	3	were	be	AUX
eurjchem-966	56	4	recorded	record	VERB
eurjchem-966	56	5	at	at	ADP
eurjchem-966	56	6	δλ	δλ	NOUN
eurjchem-966	56	7	=	=	SYM
eurjchem-966	56	8	4	4	NUM
eurjchem-966	56	9	nm	nm	NOUN
eurjchem-966	56	10	and	and	CCONJ
eurjchem-966	56	11	scaling	scale	VERB
eurjchem-966	56	12	factor	factor	NOUN
eurjchem-966	56	13	=	=	NOUN
eurjchem-966	56	14	10	10	NUM
eurjchem-966	56	15	.	.	PUNCT
eurjchem-966	57	1	the	the	DET
eurjchem-966	57	2	absorption	absorption	NOUN
eurjchem-966	57	3	spectra	spectra	NOUN
eurjchem-966	57	4	of	of	ADP
eurjchem-966	57	5	this	this	DET
eurjchem-966	57	6	solution	solution	NOUN
eurjchem-966	57	7	were	be	AUX
eurjchem-966	57	8	divided	divide	VERB
eurjchem-966	57	9	by	by	ADP
eurjchem-966	57	10	the	the	DET
eurjchem-966	57	11	absorption	absorption	NOUN
eurjchem-966	57	12	spectrum	spectrum	NOUN
eurjchem-966	57	13	of	of	ADP
eurjchem-966	57	14	20	20	NUM
eurjchem-966	57	15	µg	µg	NOUN
eurjchem-966	57	16	/	/	SYM
eurjchem-966	57	17	ml	ml	NOUN
eurjchem-966	57	18	of	of	ADP
eurjchem-966	57	19	deg	deg	PROPN
eurjchem-966	57	20	(	(	PUNCT
eurjchem-966	57	21	as	as	ADP
eurjchem-966	57	22	a	a	DET
eurjchem-966	57	23	divisor	divisor	NOUN
eurjchem-966	57	24	)	)	PUNCT
eurjchem-966	57	25	,	,	PUNCT
eurjchem-966	57	26	and	and	CCONJ
eurjchem-966	57	27	then	then	ADV
eurjchem-966	57	28	the	the	DET
eurjchem-966	57	29	obtained	obtain	VERB
eurjchem-966	57	30	ratio	ratio	NOUN
eurjchem-966	57	31	spectra	spectra	NOUN
eurjchem-966	57	32	were	be	AUX
eurjchem-966	57	33	differentiated	differentiate	VERB
eurjchem-966	57	34	with	with	ADP
eurjchem-966	57	35	respect	respect	NOUN
eurjchem-966	57	36	to	to	ADP
eurjchem-966	57	37	wavelength	wavelength	NOUN
eurjchem-966	57	38	.	.	PUNCT
eurjchem-966	58	1	the	the	DET
eurjchem-966	58	2	peak	peak	NOUN
eurjchem-966	58	3	amplitudes	amplitude	NOUN
eurjchem-966	58	4	at	at	ADP
eurjchem-966	58	5	244	244	NUM
eurjchem-966	58	6	nm	nm	NOUN
eurjchem-966	58	7	were	be	AUX
eurjchem-966	58	8	recorded	record	VERB
eurjchem-966	58	9	then	then	ADV
eurjchem-966	58	10	calibration	calibration	NOUN
eurjchem-966	58	11	graph	graph	NOUN
eurjchem-966	58	12	was	be	AUX
eurjchem-966	58	13	constructed	construct	VERB
eurjchem-966	58	14	relating	relate	VERB
eurjchem-966	58	15	the	the	DET
eurjchem-966	58	16	peak	peak	NOUN
eurjchem-966	58	17	amplitudes	amplitude	NOUN
eurjchem-966	58	18	of	of	ADP
eurjchem-966	58	19	(	(	PUNCT
eurjchem-966	58	20	1dd	1dd	ADJ
eurjchem-966	58	21	)	)	PUNCT
eurjchem-966	58	22	to	to	ADP
eurjchem-966	58	23	the	the	DET
eurjchem-966	58	24	corresponding	corresponding	ADJ
eurjchem-966	58	25	concentrations	concentration	NOUN
eurjchem-966	58	26	.	.	PUNCT
eurjchem-966	59	1	the	the	DET
eurjchem-966	59	2	regression	regression	NOUN
eurjchem-966	59	3	equation	equation	NOUN
eurjchem-966	59	4	was	be	AUX
eurjchem-966	59	5	then	then	ADV
eurjchem-966	59	6	computed	compute	VERB
eurjchem-966	59	7	for	for	ADP
eurjchem-966	59	8	the	the	DET
eurjchem-966	59	9	studied	study	VERB
eurjchem-966	59	10	drug	drug	NOUN
eurjchem-966	59	11	at	at	ADP
eurjchem-966	59	12	the	the	DET
eurjchem-966	59	13	specified	specified	ADJ
eurjchem-966	59	14	wavelength	wavelength	NOUN
eurjchem-966	59	15	and	and	CCONJ
eurjchem-966	59	16	used	use	VERB
eurjchem-966	59	17	for	for	ADP
eurjchem-966	59	18	determination	determination	NOUN
eurjchem-966	59	19	of	of	ADP
eurjchem-966	59	20	unknown	unknown	ADJ
eurjchem-966	59	21	samples	sample	NOUN
eurjchem-966	59	22	containing	contain	VERB
eurjchem-966	59	23	acm	acm	NOUN
eurjchem-966	59	24	.	.	PUNCT
eurjchem-966	60	1	2.4.1.2	2.4.1.2	X
eurjchem-966	60	2	.	.	PUNCT
eurjchem-966	60	3	construction	construction	NOUN
eurjchem-966	60	4	of	of	ADP
eurjchem-966	60	5	calibration	calibration	NOUN
eurjchem-966	60	6	curves	curve	NOUN
eurjchem-966	60	7	for	for	ADP
eurjchem-966	60	8	mean	mean	ADJ
eurjchem-966	60	9	centering	centering	NOUN
eurjchem-966	60	10	of	of	ADP
eurjchem-966	60	11	ratio	ratio	NOUN
eurjchem-966	60	12	spectra	spectra	PROPN
eurjchem-966	60	13	spectrophotometric	spectrophotometric	ADJ
eurjchem-966	60	14	method	method	NOUN
eurjchem-966	60	15	(	(	PUNCT
eurjchem-966	60	16	mcr	mcr	PROPN
eurjchem-966	60	17	)	)	PUNCT
eurjchem-966	60	18	accurately	accurately	ADV
eurjchem-966	60	19	measured	measure	VERB
eurjchem-966	60	20	aliquots	aliquot	NOUN
eurjchem-966	60	21	equivalent	equivalent	ADJ
eurjchem-966	60	22	to	to	ADP
eurjchem-966	60	23	20‐220	20‐220	NUM
eurjchem-966	60	24	µg	µg	ADV
eurjchem-966	60	25	of	of	ADP
eurjchem-966	60	26	acm	acm	NOUN
eurjchem-966	60	27	were	be	AUX
eurjchem-966	60	28	transferred	transfer	VERB
eurjchem-966	60	29	from	from	ADP
eurjchem-966	60	30	its	its	PRON
eurjchem-966	60	31	working	work	VERB
eurjchem-966	60	32	solution	solution	NOUN
eurjchem-966	60	33	(	(	PUNCT
eurjchem-966	60	34	100	100	NUM
eurjchem-966	60	35	µg	µg	ADJ
eurjchem-966	60	36	/	/	SYM
eurjchem-966	60	37	ml	ml	NOUN
eurjchem-966	60	38	)	)	PUNCT
eurjchem-966	60	39	into	into	ADP
eurjchem-966	60	40	a	a	DET
eurjchem-966	60	41	series	series	NOUN
eurjchem-966	60	42	of	of	ADP
eurjchem-966	60	43	10	10	NUM
eurjchem-966	60	44	ml	ml	NOUN
eurjchem-966	60	45	volumetric	volumetric	ADJ
eurjchem-966	60	46	flasks	flask	NOUN
eurjchem-966	60	47	and	and	CCONJ
eurjchem-966	60	48	the	the	DET
eurjchem-966	60	49	volume	volume	NOUN
eurjchem-966	60	50	was	be	AUX
eurjchem-966	60	51	completed	complete	VERB
eurjchem-966	60	52	with	with	ADP
eurjchem-966	60	53	purified	purified	ADJ
eurjchem-966	60	54	water	water	NOUN
eurjchem-966	60	55	to	to	ADP
eurjchem-966	60	56	final	final	ADJ
eurjchem-966	60	57	concentration	concentration	NOUN
eurjchem-966	60	58	range	range	NOUN
eurjchem-966	60	59	(	(	PUNCT
eurjchem-966	60	60	2‐	2‐	NUM
eurjchem-966	60	61	22	22	NUM
eurjchem-966	60	62	µg	µg	NOUN
eurjchem-966	60	63	/	/	SYM
eurjchem-966	60	64	ml	ml	NOUN
eurjchem-966	60	65	)	)	PUNCT
eurjchem-966	60	66	.	.	PUNCT
eurjchem-966	61	1	the	the	DET
eurjchem-966	61	2	recorded	record	VERB
eurjchem-966	61	3	absorption	absorption	NOUN
eurjchem-966	61	4	spectra	spectra	NOUN
eurjchem-966	61	5	of	of	ADP
eurjchem-966	61	6	acm	acm	PROPN
eurjchem-966	61	7	from	from	ADP
eurjchem-966	61	8	220‐320	220‐320	NUM
eurjchem-966	61	9	nm	nm	NOUN
eurjchem-966	61	10	were	be	AUX
eurjchem-966	61	11	divided	divide	VERB
eurjchem-966	61	12	by	by	ADP
eurjchem-966	61	13	the	the	DET
eurjchem-966	61	14	absorption	absorption	NOUN
eurjchem-966	61	15	spectrum	spectrum	NOUN
eurjchem-966	61	16	of	of	ADP
eurjchem-966	61	17	deg	deg	PROPN
eurjchem-966	61	18	(	(	PUNCT
eurjchem-966	61	19	20	20	NUM
eurjchem-966	61	20	µg	µg	NOUN
eurjchem-966	61	21	/	/	SYM
eurjchem-966	61	22	ml	ml	NOUN
eurjchem-966	61	23	)	)	PUNCT
eurjchem-966	61	24	to	to	PART
eurjchem-966	61	25	obtain	obtain	VERB
eurjchem-966	61	26	the	the	DET
eurjchem-966	61	27	ratio	ratio	NOUN
eurjchem-966	61	28	spectra	spectra	NOUN
eurjchem-966	61	29	,	,	PUNCT
eurjchem-966	61	30	which	which	PRON
eurjchem-966	61	31	were	be	AUX
eurjchem-966	61	32	then	then	ADV
eurjchem-966	61	33	mean	mean	VERB
eurjchem-966	61	34	centered	center	VERB
eurjchem-966	61	35	.	.	PUNCT
eurjchem-966	62	1	these	these	DET
eurjchem-966	62	2	mean	mean	VERB
eurjchem-966	62	3	centered	center	VERB
eurjchem-966	62	4	values	value	NOUN
eurjchem-966	62	5	of	of	ADP
eurjchem-966	62	6	the	the	DET
eurjchem-966	62	7	ratio	ratio	NOUN
eurjchem-966	62	8	spectra	spectra	NOUN
eurjchem-966	62	9	at	at	ADP
eurjchem-966	62	10	234	234	NUM
eurjchem-966	62	11	nm	nm	NOUN
eurjchem-966	62	12	were	be	AUX
eurjchem-966	62	13	recorded	record	VERB
eurjchem-966	62	14	and	and	CCONJ
eurjchem-966	62	15	plotted	plot	VERB
eurjchem-966	62	16	versus	versus	ADP
eurjchem-966	62	17	the	the	DET
eurjchem-966	62	18	corresponding	corresponding	ADJ
eurjchem-966	62	19	concentrations	concentration	NOUN
eurjchem-966	62	20	.	.	PUNCT
eurjchem-966	63	1	calibration	calibration	NOUN
eurjchem-966	63	2	curve	curve	NOUN
eurjchem-966	63	3	was	be	AUX
eurjchem-966	63	4	constructed	construct	VERB
eurjchem-966	63	5	and	and	CCONJ
eurjchem-966	63	6	regression	regression	NOUN
eurjchem-966	63	7	equation	equation	NOUN
eurjchem-966	63	8	was	be	AUX
eurjchem-966	63	9	computed	compute	VERB
eurjchem-966	63	10	.	.	PUNCT
eurjchem-966	64	1	2.4.1.3	2.4.1.3	NUM
eurjchem-966	64	2	.	.	PUNCT
eurjchem-966	64	3	analysis	analysis	NOUN
eurjchem-966	64	4	of	of	ADP
eurjchem-966	64	5	laboratory	laboratory	NOUN
eurjchem-966	64	6	prepared	prepare	VERB
eurjchem-966	64	7	mixtures	mixture	NOUN
eurjchem-966	64	8	containing	contain	VERB
eurjchem-966	64	9	different	different	ADJ
eurjchem-966	64	10	ratios	ratio	NOUN
eurjchem-966	64	11	of	of	ADP
eurjchem-966	64	12	acemetacin	acemetacin	NOUN
eurjchem-966	64	13	and	and	CCONJ
eurjchem-966	64	14	its	its	PRON
eurjchem-966	64	15	degradation	degradation	NOUN
eurjchem-966	64	16	product	product	NOUN
eurjchem-966	64	17	using	use	VERB
eurjchem-966	64	18	the	the	DET
eurjchem-966	64	19	suggested	suggest	VERB
eurjchem-966	64	20	methods	method	NOUN
eurjchem-966	64	21	aliquots	aliquot	NOUN
eurjchem-966	64	22	of	of	ADP
eurjchem-966	64	23	intact	intact	ADJ
eurjchem-966	64	24	drug	drug	NOUN
eurjchem-966	64	25	and	and	CCONJ
eurjchem-966	64	26	the	the	DET
eurjchem-966	64	27	deg	deg	NOUN
eurjchem-966	64	28	were	be	AUX
eurjchem-966	64	29	mixed	mixed	ADJ
eurjchem-966	64	30	to	to	PART
eurjchem-966	64	31	prepare	prepare	VERB
eurjchem-966	64	32	different	different	ADJ
eurjchem-966	64	33	mixtures	mixture	NOUN
eurjchem-966	64	34	containing	contain	VERB
eurjchem-966	64	35	10‐90	10‐90	NUM
eurjchem-966	64	36	%	%	NOUN
eurjchem-966	64	37	of	of	ADP
eurjchem-966	64	38	the	the	DET
eurjchem-966	64	39	degradation	degradation	NOUN
eurjchem-966	64	40	product	product	NOUN
eurjchem-966	64	41	,	,	PUNCT
eurjchem-966	64	42	and	and	CCONJ
eurjchem-966	64	43	proceed	proceed	VERB
eurjchem-966	64	44	as	as	SCONJ
eurjchem-966	64	45	mentioned	mention	VERB
eurjchem-966	64	46	under	under	ADP
eurjchem-966	64	47	each	each	DET
eurjchem-966	64	48	method	method	NOUN
eurjchem-966	64	49	.	.	PUNCT
eurjchem-966	65	1	the	the	DET
eurjchem-966	65	2	concentrations	concentration	NOUN
eurjchem-966	65	3	were	be	AUX
eurjchem-966	65	4	calculated	calculate	VERB
eurjchem-966	65	5	from	from	ADP
eurjchem-966	65	6	the	the	DET
eurjchem-966	65	7	corresponding	corresponding	ADJ
eurjchem-966	65	8	regression	regression	NOUN
eurjchem-966	65	9	equations	equation	NOUN
eurjchem-966	65	10	.	.	PUNCT
eurjchem-966	66	1	2.4.2	2.4.2	NUM
eurjchem-966	66	2	.	.	PUNCT
eurjchem-966	66	3	hptlc	hptlc	NOUN
eurjchem-966	66	4	chromatographic	chromatographic	ADJ
eurjchem-966	66	5	method	method	NOUN
eurjchem-966	66	6	2.4.2.1	2.4.2.1	NUM
eurjchem-966	66	7	.	.	PUNCT
eurjchem-966	67	1	construction	construction	NOUN
eurjchem-966	67	2	of	of	ADP
eurjchem-966	67	3	calibration	calibration	NOUN
eurjchem-966	67	4	curve	curve	NOUN
eurjchem-966	67	5	for	for	ADP
eurjchem-966	67	6	hptlc‐	hptlc‐	X
eurjchem-966	67	7	densitometric	densitometric	ADJ
eurjchem-966	67	8	method	method	NOUN
eurjchem-966	67	9	aliquots	aliquot	NOUN
eurjchem-966	67	10	equivalent	equivalent	ADJ
eurjchem-966	67	11	to	to	ADP
eurjchem-966	67	12	0.4‐1.4	0.4‐1.4	PRON
eurjchem-966	67	13	mg	mg	ADP
eurjchem-966	67	14	of	of	ADP
eurjchem-966	67	15	acm	acm	PROPN
eurjchem-966	67	16	were	be	AUX
eurjchem-966	67	17	transferred	transfer	VERB
eurjchem-966	67	18	from	from	ADP
eurjchem-966	67	19	its	its	PRON
eurjchem-966	67	20	standard	standard	ADJ
eurjchem-966	67	21	solution	solution	NOUN
eurjchem-966	67	22	(	(	PUNCT
eurjchem-966	67	23	1	1	NUM
eurjchem-966	67	24	mg	mg	NUM
eurjchem-966	67	25	/	/	SYM
eurjchem-966	67	26	ml	ml	NOUN
eurjchem-966	67	27	in	in	ADP
eurjchem-966	67	28	methanol	methanol	NOUN
eurjchem-966	67	29	)	)	PUNCT
eurjchem-966	67	30	into	into	ADP
eurjchem-966	67	31	a	a	DET
eurjchem-966	67	32	series	series	NOUN
eurjchem-966	67	33	of	of	ADP
eurjchem-966	67	34	10	10	NUM
eurjchem-966	67	35	ml	ml	NOUN
eurjchem-966	67	36	measuring	measure	VERB
eurjchem-966	67	37	flasks	flask	NOUN
eurjchem-966	67	38	,	,	PUNCT
eurjchem-966	67	39	then	then	ADV
eurjchem-966	67	40	the	the	DET
eurjchem-966	67	41	volume	volume	NOUN
eurjchem-966	67	42	of	of	ADP
eurjchem-966	67	43	each	each	DET
eurjchem-966	67	44	flask	flask	NOUN
eurjchem-966	67	45	were	be	AUX
eurjchem-966	67	46	completed	complete	VERB
eurjchem-966	67	47	to	to	PART
eurjchem-966	67	48	volume	volume	VERB
eurjchem-966	67	49	with	with	ADP
eurjchem-966	67	50	methanol	methanol	NOUN
eurjchem-966	67	51	.	.	PUNCT
eurjchem-966	68	1	10	10	NUM
eurjchem-966	68	2	µl	µl	NOUN
eurjchem-966	68	3	of	of	ADP
eurjchem-966	68	4	each	each	DET
eurjchem-966	68	5	solution	solution	NOUN
eurjchem-966	68	6	were	be	AUX
eurjchem-966	68	7	applied	apply	VERB
eurjchem-966	68	8	in	in	ADP
eurjchem-966	68	9	triplicate	triplicate	NOUN
eurjchem-966	68	10	to	to	ADP
eurjchem-966	68	11	hptlc	hptlc	NOUN
eurjchem-966	68	12	plates	plate	NOUN
eurjchem-966	68	13	(	(	PUNCT
eurjchem-966	68	14	20	20	NUM
eurjchem-966	68	15	×	×	NOUN
eurjchem-966	68	16	11	11	NUM
eurjchem-966	68	17	cm	cm	NOUN
eurjchem-966	68	18	)	)	PUNCT
eurjchem-966	68	19	as	as	ADP
eurjchem-966	68	20	bands	band	NOUN
eurjchem-966	68	21	with	with	ADP
eurjchem-966	68	22	6	6	NUM
eurjchem-966	68	23	mm	mm	NOUN
eurjchem-966	68	24	width	width	NOUN
eurjchem-966	68	25	using	use	VERB
eurjchem-966	68	26	a	a	DET
eurjchem-966	68	27	camag	camag	NOUN
eurjchem-966	68	28	linomat	linomat	NOUN
eurjchem-966	68	29	iv	iv	NUM
eurjchem-966	68	30	applicator	applicator	NOUN
eurjchem-966	68	31	.	.	PUNCT
eurjchem-966	69	1	the	the	DET
eurjchem-966	69	2	bands	band	NOUN
eurjchem-966	69	3	were	be	AUX
eurjchem-966	69	4	spaced	space	VERB
eurjchem-966	69	5	5	5	NUM
eurjchem-966	69	6	mm	mm	NOUN
eurjchem-966	69	7	from	from	ADP
eurjchem-966	69	8	each	each	DET
eurjchem-966	69	9	other	other	ADJ
eurjchem-966	69	10	and	and	CCONJ
eurjchem-966	69	11	10	10	NUM
eurjchem-966	69	12	mm	mm	NOUN
eurjchem-966	69	13	apart	apart	ADV
eurjchem-966	69	14	from	from	ADP
eurjchem-966	69	15	the	the	DET
eurjchem-966	69	16	bottom	bottom	ADJ
eurjchem-966	69	17	edge	edge	NOUN
eurjchem-966	69	18	of	of	ADP
eurjchem-966	69	19	the	the	DET
eurjchem-966	69	20	plate	plate	NOUN
eurjchem-966	69	21	.	.	PUNCT
eurjchem-966	70	1	linear	linear	ADJ
eurjchem-966	70	2	ascending	ascend	VERB
eurjchem-966	70	3	development	development	NOUN
eurjchem-966	70	4	was	be	AUX
eurjchem-966	70	5	performed	perform	VERB
eurjchem-966	70	6	in	in	ADP
eurjchem-966	70	7	a	a	DET
eurjchem-966	70	8	chromatographic	chromatographic	ADJ
eurjchem-966	70	9	chamber	chamber	NOUN
eurjchem-966	70	10	previously	previously	ADV
eurjchem-966	70	11	saturated	saturate	VERB
eurjchem-966	70	12	with	with	ADP
eurjchem-966	70	13	hexane	hexane	NOUN
eurjchem-966	70	14	:	:	PUNCT
eurjchem-966	70	15	ethyl	ethyl	PROPN
eurjchem-966	70	16	acetate	acetate	NOUN
eurjchem-966	70	17	:	:	PUNCT
eurjchem-966	70	18	glacial	glacial	ADJ
eurjchem-966	70	19	acetic	acetic	ADJ
eurjchem-966	70	20	acid	acid	NOUN
eurjchem-966	70	21	(	(	PUNCT
eurjchem-966	70	22	6:4:0.3	6:4:0.3	PROPN
eurjchem-966	70	23	,	,	PUNCT
eurjchem-966	70	24	v	v	NOUN
eurjchem-966	70	25	:	:	PUNCT
eurjchem-966	70	26	v	v	ADJ
eurjchem-966	70	27	:	:	PUNCT
eurjchem-966	70	28	v	v	NOUN
eurjchem-966	70	29	)	)	PUNCT
eurjchem-966	70	30	as	as	ADP
eurjchem-966	70	31	a	a	DET
eurjchem-966	70	32	developing	develop	VERB
eurjchem-966	70	33	system	system	NOUN
eurjchem-966	70	34	for	for	ADP
eurjchem-966	70	35	one	one	NUM
eurjchem-966	70	36	hour	hour	NOUN
eurjchem-966	70	37	at	at	ADP
eurjchem-966	70	38	room	room	NOUN
eurjchem-966	70	39	temperature	temperature	NOUN
eurjchem-966	70	40	to	to	ADP
eurjchem-966	70	41	a	a	DET
eurjchem-966	70	42	distance	distance	NOUN
eurjchem-966	70	43	of	of	ADP
eurjchem-966	70	44	9	9	NUM
eurjchem-966	70	45	cm	cm	NOUN
eurjchem-966	70	46	.	.	PUNCT
eurjchem-966	71	1	the	the	DET
eurjchem-966	71	2	integrated	integrate	VERB
eurjchem-966	71	3	peak	peak	NOUN
eurjchem-966	71	4	areas	area	NOUN
eurjchem-966	71	5	were	be	AUX
eurjchem-966	71	6	recorded	record	VERB
eurjchem-966	71	7	using	use	VERB
eurjchem-966	71	8	scanning	scan	VERB
eurjchem-966	71	9	wavelength	wavelength	NOUN
eurjchem-966	71	10	at	at	ADP
eurjchem-966	71	11	254	254	NUM
eurjchem-966	71	12	nm	nm	NOUN
eurjchem-966	71	13	under	under	ADP
eurjchem-966	71	14	the	the	DET
eurjchem-966	71	15	specified	specify	VERB
eurjchem-966	71	16	instrumental	instrumental	ADJ
eurjchem-966	71	17	conditions	condition	NOUN
eurjchem-966	71	18	.	.	PUNCT
eurjchem-966	72	1	the	the	DET
eurjchem-966	72	2	calibration	calibration	NOUN
eurjchem-966	72	3	curve	curve	NOUN
eurjchem-966	72	4	constructed	construct	VERB
eurjchem-966	72	5	by	by	ADP
eurjchem-966	72	6	plotting	plot	VERB
eurjchem-966	72	7	the	the	DET
eurjchem-966	72	8	mean	mean	ADJ
eurjchem-966	72	9	integrated	integrate	VERB
eurjchem-966	72	10	peak	peak	NOUN
eurjchem-966	72	11	area/103	area/103	VERB
eurjchem-966	72	12	versus	versus	ADP
eurjchem-966	72	13	the	the	DET
eurjchem-966	72	14	corresponding	corresponding	ADJ
eurjchem-966	72	15	concentration	concentration	NOUN
eurjchem-966	72	16	of	of	ADP
eurjchem-966	72	17	acm	acm	PROPN
eurjchem-966	72	18	and	and	CCONJ
eurjchem-966	72	19	then	then	ADV
eurjchem-966	72	20	the	the	DET
eurjchem-966	72	21	regression	regression	NOUN
eurjchem-966	72	22	equation	equation	NOUN
eurjchem-966	72	23	was	be	AUX
eurjchem-966	72	24	computed	compute	VERB
eurjchem-966	72	25	.	.	PUNCT
eurjchem-966	73	1	2.4.3	2.4.3	NUM
eurjchem-966	73	2	assay	assay	NOUN
eurjchem-966	73	3	of	of	ADP
eurjchem-966	73	4	pharmaceutical	pharmaceutical	ADJ
eurjchem-966	73	5	formulation	formulation	NOUN
eurjchem-966	73	6	(	(	PUNCT
eurjchem-966	73	7	ostmap	ostmap	VERB
eurjchem-966	73	8	®	®	NOUN
eurjchem-966	73	9	capsules	capsule	NOUN
eurjchem-966	73	10	)	)	PUNCT
eurjchem-966	73	11	the	the	DET
eurjchem-966	73	12	contents	content	NOUN
eurjchem-966	73	13	of	of	ADP
eurjchem-966	73	14	twenty	twenty	NUM
eurjchem-966	73	15	capsules	capsule	NOUN
eurjchem-966	73	16	of	of	ADP
eurjchem-966	73	17	ostmap	ostmap	NOUN
eurjchem-966	73	18	®	®	NOUN
eurjchem-966	73	19	were	be	AUX
eurjchem-966	73	20	weighed	weigh	VERB
eurjchem-966	73	21	and	and	CCONJ
eurjchem-966	73	22	mixed	mix	VERB
eurjchem-966	73	23	well	well	ADV
eurjchem-966	73	24	.	.	PUNCT
eurjchem-966	74	1	an	an	DET
eurjchem-966	74	2	accurately	accurately	ADV
eurjchem-966	74	3	weighed	weigh	VERB
eurjchem-966	74	4	portion	portion	NOUN
eurjchem-966	74	5	equivalent	equivalent	ADJ
eurjchem-966	74	6	to	to	ADP
eurjchem-966	74	7	100	100	NUM
eurjchem-966	74	8	mg	mg	NUM
eurjchem-966	74	9	of	of	ADP
eurjchem-966	74	10	acm	acm	PROPN
eurjchem-966	74	11	was	be	AUX
eurjchem-966	74	12	transferred	transfer	VERB
eurjchem-966	74	13	into	into	ADP
eurjchem-966	74	14	100	100	NUM
eurjchem-966	74	15	ml	ml	NOUN
eurjchem-966	74	16	volumetric	volumetric	ADJ
eurjchem-966	74	17	flask	flask	NOUN
eurjchem-966	74	18	and	and	CCONJ
eurjchem-966	74	19	then	then	ADV
eurjchem-966	74	20	75	75	NUM
eurjchem-966	74	21	ml	ml	NOUN
eurjchem-966	74	22	methanol	methanol	NOUN
eurjchem-966	74	23	was	be	AUX
eurjchem-966	74	24	added	add	VERB
eurjchem-966	74	25	.	.	PUNCT
eurjchem-966	75	1	the	the	DET
eurjchem-966	75	2	prepared	prepare	VERB
eurjchem-966	75	3	solution	solution	NOUN
eurjchem-966	75	4	was	be	AUX
eurjchem-966	75	5	sonicated	sonicate	VERB
eurjchem-966	75	6	for	for	ADP
eurjchem-966	75	7	30	30	NUM
eurjchem-966	75	8	min	min	NOUN
eurjchem-966	75	9	,	,	PUNCT
eurjchem-966	75	10	cooled	cool	VERB
eurjchem-966	75	11	and	and	CCONJ
eurjchem-966	75	12	completed	complete	VERB
eurjchem-966	75	13	to	to	PART
eurjchem-966	75	14	volume	volume	VERB
eurjchem-966	75	15	with	with	ADP
eurjchem-966	75	16	methanol	methanol	NOUN
eurjchem-966	75	17	.	.	PUNCT
eurjchem-966	76	1	the	the	DET
eurjchem-966	76	2	solution	solution	NOUN
eurjchem-966	76	3	was	be	AUX
eurjchem-966	76	4	filtered	filter	VERB
eurjchem-966	76	5	and	and	CCONJ
eurjchem-966	76	6	diluted	dilute	VERB
eurjchem-966	76	7	to	to	PART
eurjchem-966	76	8	obtain	obtain	VERB
eurjchem-966	76	9	100	100	NUM
eurjchem-966	76	10	µg	µg	NOUN
eurjchem-966	76	11	/	/	SYM
eurjchem-966	76	12	ml	ml	X
eurjchem-966	76	13	working	working	NOUN
eurjchem-966	76	14	solution	solution	NOUN
eurjchem-966	76	15	for	for	ADP
eurjchem-966	76	16	each	each	DET
eurjchem-966	76	17	method	method	NOUN
eurjchem-966	76	18	.	.	PUNCT
eurjchem-966	77	1	naguib	naguib	NOUN
eurjchem-966	77	2	et	et	PROPN
eurjchem-966	77	3	al	al	PROPN
eurjchem-966	77	4	.	.	PUNCT
eurjchem-966	77	5	/	/	SYM
eurjchem-966	77	6	european	european	PROPN
eurjchem-966	77	7	journal	journal	PROPN
eurjchem-966	77	8	of	of	ADP
eurjchem-966	77	9	chemistry	chemistry	NOUN
eurjchem-966	77	10	5	5	NUM
eurjchem-966	77	11	(	(	PUNCT
eurjchem-966	77	12	2	2	NUM
eurjchem-966	77	13	)	)	PUNCT
eurjchem-966	77	14	(	(	PUNCT
eurjchem-966	77	15	2014	2014	NUM
eurjchem-966	77	16	)	)	PUNCT
eurjchem-966	77	17	219‐226	219‐226	NUM
eurjchem-966	77	18	221	221	NUM
eurjchem-966	77	19	figure	figure	NOUN
eurjchem-966	77	20	1	1	NUM
eurjchem-966	77	21	.	.	PUNCT
eurjchem-966	77	22	chemical	chemical	ADJ
eurjchem-966	77	23	structure	structure	NOUN
eurjchem-966	77	24	of	of	ADP
eurjchem-966	77	25	acemetacin	acemetacin	PROPN
eurjchem-966	77	26	(	(	PUNCT
eurjchem-966	77	27	acm	acm	PROPN
eurjchem-966	77	28	)	)	PUNCT
eurjchem-966	77	29	.	.	PUNCT
eurjchem-966	78	1	figure	figure	NOUN
eurjchem-966	78	2	2	2	NUM
eurjchem-966	78	3	.	.	PUNCT
eurjchem-966	78	4	pathway	pathway	NOUN
eurjchem-966	78	5	of	of	ADP
eurjchem-966	78	6	acm	acm	PROPN
eurjchem-966	78	7	hydrolytic	hydrolytic	ADJ
eurjchem-966	78	8	degradation	degradation	NOUN
eurjchem-966	78	9	.	.	PUNCT
eurjchem-966	79	1	the	the	DET
eurjchem-966	79	2	procedure	procedure	NOUN
eurjchem-966	79	3	detailed	detail	VERB
eurjchem-966	79	4	under	under	ADP
eurjchem-966	79	5	linearity	linearity	NOUN
eurjchem-966	79	6	and	and	CCONJ
eurjchem-966	79	7	construction	construction	NOUN
eurjchem-966	79	8	of	of	ADP
eurjchem-966	79	9	calibration	calibration	NOUN
eurjchem-966	79	10	curve	curve	NOUN
eurjchem-966	79	11	for	for	ADP
eurjchem-966	79	12	each	each	DET
eurjchem-966	79	13	method	method	NOUN
eurjchem-966	79	14	was	be	AUX
eurjchem-966	79	15	followed	follow	VERB
eurjchem-966	79	16	.	.	PUNCT
eurjchem-966	80	1	when	when	SCONJ
eurjchem-966	80	2	carrying	carry	VERB
eurjchem-966	80	3	out	out	ADP
eurjchem-966	80	4	the	the	DET
eurjchem-966	80	5	standard	standard	ADJ
eurjchem-966	80	6	addition	addition	NOUN
eurjchem-966	80	7	technique	technique	NOUN
eurjchem-966	80	8	,	,	PUNCT
eurjchem-966	80	9	the	the	DET
eurjchem-966	80	10	powder	powder	NOUN
eurjchem-966	80	11	content	content	NOUN
eurjchem-966	80	12	of	of	ADP
eurjchem-966	80	13	the	the	DET
eurjchem-966	80	14	capsules	capsule	NOUN
eurjchem-966	80	15	and	and	CCONJ
eurjchem-966	80	16	that	that	PRON
eurjchem-966	80	17	of	of	ADP
eurjchem-966	80	18	pure	pure	ADJ
eurjchem-966	80	19	acm	acm	NOUN
eurjchem-966	80	20	were	be	AUX
eurjchem-966	80	21	mixed	mix	VERB
eurjchem-966	80	22	well	well	ADV
eurjchem-966	80	23	together	together	ADV
eurjchem-966	80	24	before	before	ADP
eurjchem-966	80	25	proceeding	proceed	VERB
eurjchem-966	80	26	in	in	ADP
eurjchem-966	80	27	the	the	DET
eurjchem-966	80	28	above‐mentioned	above‐mentione	VERB
eurjchem-966	80	29	procedures	procedure	NOUN
eurjchem-966	80	30	.	.	PUNCT
eurjchem-966	81	1	3	3	X
eurjchem-966	81	2	.	.	NOUN
eurjchem-966	81	3	results	result	NOUN
eurjchem-966	81	4	and	and	CCONJ
eurjchem-966	81	5	discussion	discussion	NOUN
eurjchem-966	81	6	acemetacin	acemetacin	ADV
eurjchem-966	81	7	is	be	AUX
eurjchem-966	81	8	regarded	regard	VERB
eurjchem-966	81	9	as	as	ADP
eurjchem-966	81	10	a	a	DET
eurjchem-966	81	11	pro‐drug	pro‐drug	NOUN
eurjchem-966	81	12	of	of	ADP
eurjchem-966	81	13	indomethacin	indomethacin	NOUN
eurjchem-966	81	14	[	[	X
eurjchem-966	81	15	12	12	NUM
eurjchem-966	81	16	]	]	PUNCT
eurjchem-966	81	17	,	,	PUNCT
eurjchem-966	81	18	both	both	DET
eurjchem-966	81	19	drugs	drug	NOUN
eurjchem-966	81	20	have	have	VERB
eurjchem-966	81	21	the	the	DET
eurjchem-966	81	22	same	same	ADJ
eurjchem-966	81	23	efficiency	efficiency	NOUN
eurjchem-966	81	24	,	,	PUNCT
eurjchem-966	81	25	but	but	CCONJ
eurjchem-966	81	26	with	with	ADP
eurjchem-966	81	27	regard	regard	NOUN
eurjchem-966	81	28	to	to	ADP
eurjchem-966	81	29	tolerability	tolerability	NOUN
eurjchem-966	81	30	,	,	PUNCT
eurjchem-966	81	31	the	the	DET
eurjchem-966	81	32	incidence	incidence	NOUN
eurjchem-966	81	33	and	and	CCONJ
eurjchem-966	81	34	severity	severity	NOUN
eurjchem-966	81	35	of	of	ADP
eurjchem-966	81	36	gastro‐intestinal	gastro‐intestinal	ADJ
eurjchem-966	81	37	adverse	adverse	ADJ
eurjchem-966	81	38	effects	effect	NOUN
eurjchem-966	81	39	was	be	AUX
eurjchem-966	81	40	significantly	significantly	ADV
eurjchem-966	81	41	less	less	ADJ
eurjchem-966	81	42	with	with	ADP
eurjchem-966	81	43	acemetacin	acemetacin	ADV
eurjchem-966	81	44	than	than	ADP
eurjchem-966	81	45	with	with	ADP
eurjchem-966	81	46	indomethacin	indomethacin	NOUN
eurjchem-966	81	47	as	as	SCONJ
eurjchem-966	81	48	it	it	PRON
eurjchem-966	81	49	induced	induce	VERB
eurjchem-966	81	50	more	more	ADJ
eurjchem-966	81	51	gastric	gastric	ADJ
eurjchem-966	81	52	damage	damage	NOUN
eurjchem-966	81	53	,	,	PUNCT
eurjchem-966	81	54	and	and	CCONJ
eurjchem-966	81	55	central	central	ADJ
eurjchem-966	81	56	nervous	nervous	ADJ
eurjchem-966	81	57	system	system	NOUN
eurjchem-966	81	58	adverse	adverse	ADJ
eurjchem-966	81	59	effects	effect	NOUN
eurjchem-966	81	60	were	be	AUX
eurjchem-966	81	61	also	also	ADV
eurjchem-966	81	62	markedly	markedly	ADV
eurjchem-966	81	63	fewer	few	ADJ
eurjchem-966	81	64	.	.	PUNCT
eurjchem-966	82	1	so	so	ADV
eurjchem-966	82	2	acemetacin	acemetacin	ADV
eurjchem-966	82	3	is	be	AUX
eurjchem-966	82	4	as	as	ADV
eurjchem-966	82	5	effective	effective	ADJ
eurjchem-966	82	6	as	as	ADP
eurjchem-966	82	7	indomethacin	indomethacin	NOUN
eurjchem-966	82	8	in	in	ADP
eurjchem-966	82	9	the	the	DET
eurjchem-966	82	10	treatment	treatment	NOUN
eurjchem-966	82	11	of	of	ADP
eurjchem-966	82	12	rheumatoid	rheumatoid	NOUN
eurjchem-966	82	13	arthritis	arthritis	NOUN
eurjchem-966	82	14	,	,	PUNCT
eurjchem-966	82	15	but	but	CCONJ
eurjchem-966	82	16	has	have	VERB
eurjchem-966	82	17	significant	significant	ADJ
eurjchem-966	82	18	advantages	advantage	NOUN
eurjchem-966	82	19	in	in	ADP
eurjchem-966	82	20	terms	term	NOUN
eurjchem-966	82	21	of	of	ADP
eurjchem-966	82	22	tolerability	tolerability	NOUN
eurjchem-966	82	23	and	and	CCONJ
eurjchem-966	82	24	safety	safety	NOUN
eurjchem-966	82	25	[	[	X
eurjchem-966	82	26	13	13	NUM
eurjchem-966	82	27	]	]	PUNCT
eurjchem-966	82	28	.	.	PUNCT
eurjchem-966	83	1	thus	thus	ADV
eurjchem-966	83	2	the	the	DET
eurjchem-966	83	3	main	main	ADJ
eurjchem-966	83	4	task	task	NOUN
eurjchem-966	83	5	of	of	ADP
eurjchem-966	83	6	this	this	DET
eurjchem-966	83	7	work	work	NOUN
eurjchem-966	83	8	was	be	AUX
eurjchem-966	83	9	to	to	PART
eurjchem-966	83	10	study	study	VERB
eurjchem-966	83	11	the	the	DET
eurjchem-966	83	12	stability	stability	NOUN
eurjchem-966	83	13	of	of	ADP
eurjchem-966	83	14	acm	acm	PROPN
eurjchem-966	83	15	according	accord	VERB
eurjchem-966	83	16	to	to	ADP
eurjchem-966	83	17	ich	ich	NOUN
eurjchem-966	83	18	guidelines	guideline	NOUN
eurjchem-966	83	19	[	[	X
eurjchem-966	83	20	14	14	NUM
eurjchem-966	83	21	]	]	PUNCT
eurjchem-966	83	22	for	for	ADP
eurjchem-966	83	23	:	:	PUNCT
eurjchem-966	83	24	(	(	PUNCT
eurjchem-966	83	25	a	a	X
eurjchem-966	83	26	)	)	PUNCT
eurjchem-966	83	27	stress	stress	NOUN
eurjchem-966	83	28	alkaline	alkaline	NOUN
eurjchem-966	83	29	hydrolysis	hydrolysis	NOUN
eurjchem-966	83	30	:	:	PUNCT
eurjchem-966	83	31	0.1	0.1	NUM
eurjchem-966	83	32	m	m	PROPN
eurjchem-966	83	33	naoh	naoh	NOUN
eurjchem-966	83	34	at	at	ADP
eurjchem-966	83	35	room	room	NOUN
eurjchem-966	83	36	temperature	temperature	NOUN
eurjchem-966	83	37	for	for	ADP
eurjchem-966	83	38	30	30	NUM
eurjchem-966	83	39	min	min	NOUN
eurjchem-966	83	40	.	.	PUNCT
eurjchem-966	83	41	(	(	PUNCT
eurjchem-966	83	42	b	b	X
eurjchem-966	83	43	)	)	PUNCT
eurjchem-966	83	44	stress	stress	NOUN
eurjchem-966	83	45	acid	acid	NOUN
eurjchem-966	83	46	hydrolysis	hydrolysis	NOUN
eurjchem-966	83	47	:	:	PUNCT
eurjchem-966	83	48	0.1	0.1	NUM
eurjchem-966	83	49	m	m	NOUN
eurjchem-966	83	50	hcl	hcl	PROPN
eurjchem-966	83	51	at	at	ADP
eurjchem-966	83	52	80	80	NUM
eurjchem-966	83	53	°	°	NUM
eurjchem-966	83	54	c	c	NOUN
eurjchem-966	83	55	for	for	ADP
eurjchem-966	83	56	4	4	NUM
eurjchem-966	83	57	h.	h.	NOUN
eurjchem-966	83	58	(	(	PUNCT
eurjchem-966	83	59	c	c	NOUN
eurjchem-966	83	60	)	)	PUNCT
eurjchem-966	83	61	oxidative	oxidative	ADJ
eurjchem-966	83	62	condition	condition	NOUN
eurjchem-966	83	63	:	:	PUNCT
eurjchem-966	83	64	30	30	NUM
eurjchem-966	83	65	%	%	NOUN
eurjchem-966	83	66	h2o2	h2o2	NOUN
eurjchem-966	83	67	for	for	ADP
eurjchem-966	83	68	24	24	NUM
eurjchem-966	83	69	h.	h.	NOUN
eurjchem-966	83	70	(	(	PUNCT
eurjchem-966	83	71	d	d	X
eurjchem-966	83	72	)	)	PUNCT
eurjchem-966	83	73	photochemical	photochemical	ADJ
eurjchem-966	83	74	stability	stability	NOUN
eurjchem-966	83	75	was	be	AUX
eurjchem-966	83	76	studied	study	VERB
eurjchem-966	83	77	by	by	ADP
eurjchem-966	83	78	exposing	expose	VERB
eurjchem-966	83	79	the	the	DET
eurjchem-966	83	80	drug	drug	NOUN
eurjchem-966	83	81	sample	sample	NOUN
eurjchem-966	83	82	to	to	PART
eurjchem-966	83	83	daylight	daylight	VERB
eurjchem-966	83	84	for	for	ADP
eurjchem-966	83	85	24	24	NUM
eurjchem-966	83	86	h.	h.	PROPN
eurjchem-966	83	87	being	be	AUX
eurjchem-966	83	88	an	an	DET
eurjchem-966	83	89	ester	ester	NOUN
eurjchem-966	83	90	;	;	PUNCT
eurjchem-966	83	91	acm	acm	NOUN
eurjchem-966	83	92	(	(	PUNCT
eurjchem-966	83	93	figure	figure	NOUN
eurjchem-966	83	94	1	1	NUM
eurjchem-966	83	95	)	)	PUNCT
eurjchem-966	83	96	was	be	AUX
eurjchem-966	83	97	easily	easily	ADV
eurjchem-966	83	98	hydrolyzed	hydrolyze	VERB
eurjchem-966	83	99	in	in	ADP
eurjchem-966	83	100	alkaline	alkaline	NOUN
eurjchem-966	83	101	medium	medium	NOUN
eurjchem-966	83	102	using	use	VERB
eurjchem-966	83	103	0.1	0.1	NUM
eurjchem-966	83	104	m	m	PROPN
eurjchem-966	83	105	naoh	naoh	ADJ
eurjchem-966	83	106	into	into	ADP
eurjchem-966	83	107	corresponding	correspond	VERB
eurjchem-966	83	108	acid	acid	NOUN
eurjchem-966	83	109	;	;	PUNCT
eurjchem-966	83	110	indomethacin	indomethacin	NOUN
eurjchem-966	83	111	.	.	PUNCT
eurjchem-966	84	1	it	it	PRON
eurjchem-966	84	2	was	be	AUX
eurjchem-966	84	3	also	also	ADV
eurjchem-966	84	4	hydrolyzed	hydrolyze	VERB
eurjchem-966	84	5	to	to	ADP
eurjchem-966	84	6	the	the	DET
eurjchem-966	84	7	same	same	ADJ
eurjchem-966	84	8	degradation	degradation	NOUN
eurjchem-966	84	9	product	product	NOUN
eurjchem-966	84	10	by	by	ADP
eurjchem-966	84	11	refluxing	refluxe	VERB
eurjchem-966	84	12	with	with	ADP
eurjchem-966	84	13	0.1	0.1	NUM
eurjchem-966	84	14	m	m	NOUN
eurjchem-966	84	15	hcl	hcl	PROPN
eurjchem-966	84	16	for	for	ADP
eurjchem-966	84	17	about	about	ADV
eurjchem-966	84	18	4	4	NUM
eurjchem-966	84	19	h.	h.	NOUN
eurjchem-966	84	20	the	the	DET
eurjchem-966	84	21	resultant	resultant	NOUN
eurjchem-966	84	22	solution	solution	NOUN
eurjchem-966	84	23	after	after	ADP
eurjchem-966	84	24	both	both	CCONJ
eurjchem-966	84	25	alkaline	alkaline	NOUN
eurjchem-966	84	26	and	and	CCONJ
eurjchem-966	84	27	acid	acid	NOUN
eurjchem-966	84	28	hydrolysis	hydrolysis	NOUN
eurjchem-966	84	29	was	be	AUX
eurjchem-966	84	30	compared	compare	VERB
eurjchem-966	84	31	to	to	ADP
eurjchem-966	84	32	the	the	DET
eurjchem-966	84	33	pure	pure	ADJ
eurjchem-966	84	34	standard	standard	NOUN
eurjchem-966	84	35	indomethacin	indomethacin	VERB
eurjchem-966	84	36	via	via	ADP
eurjchem-966	84	37	tlc	tlc	NOUN
eurjchem-966	84	38	using	use	VERB
eurjchem-966	84	39	hexane	hexane	NOUN
eurjchem-966	84	40	:	:	PUNCT
eurjchem-966	84	41	ethyl	ethyl	PROPN
eurjchem-966	84	42	acetate	acetate	PROPN
eurjchem-966	84	43	:	:	PUNCT
eurjchem-966	84	44	glacial	glacial	ADJ
eurjchem-966	84	45	acetic	acetic	ADJ
eurjchem-966	84	46	acid	acid	NOUN
eurjchem-966	84	47	(	(	PUNCT
eurjchem-966	84	48	6:4:0.3	6:4:0.3	PROPN
eurjchem-966	84	49	,	,	PUNCT
eurjchem-966	84	50	v	v	NOUN
eurjchem-966	84	51	:	:	PUNCT
eurjchem-966	84	52	v	v	ADJ
eurjchem-966	84	53	:	:	PUNCT
eurjchem-966	84	54	v	v	NOUN
eurjchem-966	84	55	)	)	PUNCT
eurjchem-966	84	56	as	as	ADP
eurjchem-966	84	57	developing	develop	VERB
eurjchem-966	84	58	system	system	NOUN
eurjchem-966	84	59	.	.	PUNCT
eurjchem-966	85	1	the	the	DET
eurjchem-966	85	2	resultant	resultant	NOUN
eurjchem-966	85	3	degradation	degradation	NOUN
eurjchem-966	85	4	product	product	NOUN
eurjchem-966	85	5	was	be	AUX
eurjchem-966	85	6	compared	compare	VERB
eurjchem-966	85	7	with	with	ADP
eurjchem-966	85	8	the	the	DET
eurjchem-966	85	9	authentic	authentic	ADJ
eurjchem-966	85	10	indomethacin	indomethacin	NOUN
eurjchem-966	85	11	on	on	ADP
eurjchem-966	85	12	tlc	tlc	NOUN
eurjchem-966	85	13	plate	plate	NOUN
eurjchem-966	85	14	and	and	CCONJ
eurjchem-966	85	15	both	both	PRON
eurjchem-966	85	16	shows	show	VERB
eurjchem-966	85	17	the	the	DET
eurjchem-966	85	18	same	same	ADJ
eurjchem-966	85	19	rf	rf	ADJ
eurjchem-966	85	20	values	value	NOUN
eurjchem-966	85	21	.	.	PUNCT
eurjchem-966	86	1	degradation	degradation	NOUN
eurjchem-966	86	2	pathway	pathway	NOUN
eurjchem-966	86	3	of	of	ADP
eurjchem-966	86	4	acm	acm	PROPN
eurjchem-966	86	5	is	be	AUX
eurjchem-966	86	6	shown	show	VERB
eurjchem-966	86	7	in	in	ADP
eurjchem-966	86	8	figure	figure	NOUN
eurjchem-966	86	9	2	2	NUM
eurjchem-966	86	10	.	.	X
eurjchem-966	86	11	acm	acm	PROPN
eurjchem-966	86	12	showed	show	VERB
eurjchem-966	86	13	stability	stability	NOUN
eurjchem-966	86	14	regarding	regard	VERB
eurjchem-966	86	15	both	both	PRON
eurjchem-966	86	16	oxidation	oxidation	NOUN
eurjchem-966	86	17	and	and	CCONJ
eurjchem-966	86	18	photo‐	photo‐	NOUN
eurjchem-966	86	19	stability	stability	NOUN
eurjchem-966	86	20	studies	study	NOUN
eurjchem-966	86	21	.	.	PUNCT
eurjchem-966	87	1	moreover	moreover	ADV
eurjchem-966	87	2	,	,	PUNCT
eurjchem-966	87	3	both	both	DET
eurjchem-966	87	4	acm	acm	PROPN
eurjchem-966	87	5	and	and	CCONJ
eurjchem-966	87	6	deg	deg	PROPN
eurjchem-966	87	7	were	be	AUX
eurjchem-966	87	8	characterized	characterize	VERB
eurjchem-966	87	9	by	by	ADP
eurjchem-966	87	10	ir‐	ir‐	NOUN
eurjchem-966	87	11	and	and	CCONJ
eurjchem-966	87	12	ms‐spectrometry	ms‐spectrometry	NOUN
eurjchem-966	87	13	;	;	PUNCT
eurjchem-966	87	14	figures	figure	NOUN
eurjchem-966	87	15	3	3	NUM
eurjchem-966	87	16	and	and	CCONJ
eurjchem-966	87	17	4	4	NUM
eurjchem-966	87	18	.	.	X
eurjchem-966	87	19	ir	ir	PROPN
eurjchem-966	87	20	spectrum	spectrum	PROPN
eurjchem-966	87	21	of	of	ADP
eurjchem-966	87	22	acm	acm	PROPN
eurjchem-966	87	23	shows	show	VERB
eurjchem-966	87	24	four	four	NUM
eurjchem-966	87	25	characteristic	characteristic	ADJ
eurjchem-966	87	26	bands	band	NOUN
eurjchem-966	87	27	at	at	ADP
eurjchem-966	87	28	about	about	ADP
eurjchem-966	87	29	1605.5	1605.5	NUM
eurjchem-966	87	30	,	,	PUNCT
eurjchem-966	87	31	1667.2	1667.2	NUM
eurjchem-966	87	32	,	,	PUNCT
eurjchem-966	87	33	1723.1	1723.1	NUM
eurjchem-966	87	34	cm‐1	cm‐1	NOUN
eurjchem-966	87	35	indicating	indicate	VERB
eurjchem-966	87	36	three	three	NUM
eurjchem-966	87	37	carbonyl	carbonyl	NOUN
eurjchem-966	87	38	groups	group	NOUN
eurjchem-966	87	39	of	of	ADP
eurjchem-966	87	40	amide	amide	NOUN
eurjchem-966	87	41	,	,	PUNCT
eurjchem-966	87	42	carboxylic	carboxylic	ADJ
eurjchem-966	87	43	acid	acid	NOUN
eurjchem-966	87	44	and	and	CCONJ
eurjchem-966	87	45	ester	ester	NOUN
eurjchem-966	87	46	respectively	respectively	ADV
eurjchem-966	87	47	[	[	X
eurjchem-966	87	48	15	15	NUM
eurjchem-966	87	49	]	]	PUNCT
eurjchem-966	87	50	.	.	PUNCT
eurjchem-966	88	1	a	a	DET
eurjchem-966	88	2	broad	broad	ADJ
eurjchem-966	88	3	peak	peak	NOUN
eurjchem-966	88	4	appeared	appear	VERB
eurjchem-966	88	5	at	at	ADP
eurjchem-966	88	6	2937.1	2937.1	NUM
eurjchem-966	88	7	cm‐1	cm‐1	NOUN
eurjchem-966	88	8	indicating	indicate	VERB
eurjchem-966	88	9	the	the	DET
eurjchem-966	88	10	peripheral	peripheral	ADJ
eurjchem-966	88	11	hydroxyl	hydroxyl	NOUN
eurjchem-966	88	12	group	group	NOUN
eurjchem-966	88	13	[	[	X
eurjchem-966	88	14	15	15	NUM
eurjchem-966	88	15	]	]	PUNCT
eurjchem-966	88	16	.	.	PUNCT
eurjchem-966	89	1	the	the	DET
eurjchem-966	89	2	ir	ir	PROPN
eurjchem-966	89	3	spectrum	spectrum	NOUN
eurjchem-966	89	4	of	of	ADP
eurjchem-966	89	5	deg	deg	PROPN
eurjchem-966	89	6	indicates	indicate	VERB
eurjchem-966	89	7	the	the	DET
eurjchem-966	89	8	disappearance	disappearance	NOUN
eurjchem-966	89	9	of	of	ADP
eurjchem-966	89	10	the	the	DET
eurjchem-966	89	11	1723.1	1723.1	NUM
eurjchem-966	89	12	cm‐1	cm‐1	NOUN
eurjchem-966	89	13	ester	ester	NOUN
eurjchem-966	89	14	carbonyl	carbonyl	NOUN
eurjchem-966	89	15	group	group	NOUN
eurjchem-966	89	16	peak	peak	NOUN
eurjchem-966	89	17	.	.	PUNCT
eurjchem-966	90	1	this	this	DET
eurjchem-966	90	2	result	result	NOUN
eurjchem-966	90	3	was	be	AUX
eurjchem-966	90	4	confirmed	confirm	VERB
eurjchem-966	90	5	by	by	ADP
eurjchem-966	90	6	mass	mass	PROPN
eurjchem-966	90	7	spectra	spectra	PROPN
eurjchem-966	90	8	,	,	PUNCT
eurjchem-966	90	9	where	where	SCONJ
eurjchem-966	90	10	the	the	DET
eurjchem-966	90	11	ms	ms	PROPN
eurjchem-966	90	12	chart	chart	NOUN
eurjchem-966	90	13	of	of	ADP
eurjchem-966	90	14	acm	acm	PROPN
eurjchem-966	90	15	shows	show	VERB
eurjchem-966	90	16	parent	parent	NOUN
eurjchem-966	90	17	peak	peak	NOUN
eurjchem-966	90	18	identified	identify	VERB
eurjchem-966	90	19	at	at	ADP
eurjchem-966	90	20	m	m	PROPN
eurjchem-966	90	21	/	/	SYM
eurjchem-966	90	22	z	z	PROPN
eurjchem-966	90	23	415	415	NUM
eurjchem-966	90	24	(	(	PUNCT
eurjchem-966	90	25	corresponding	correspond	VERB
eurjchem-966	90	26	to	to	ADP
eurjchem-966	90	27	the	the	DET
eurjchem-966	90	28	molecular	molecular	ADJ
eurjchem-966	90	29	weight	weight	NOUN
eurjchem-966	90	30	of	of	ADP
eurjchem-966	90	31	acm	acm	NOUN
eurjchem-966	90	32	)	)	PUNCT
eurjchem-966	90	33	while	while	SCONJ
eurjchem-966	90	34	ms	ms	PROPN
eurjchem-966	90	35	chart	chart	NOUN
eurjchem-966	90	36	of	of	ADP
eurjchem-966	90	37	deg	deg	PROPN
eurjchem-966	90	38	shows	show	VERB
eurjchem-966	90	39	parent	parent	NOUN
eurjchem-966	90	40	peak	peak	NOUN
eurjchem-966	90	41	at	at	ADP
eurjchem-966	90	42	m	m	PROPN
eurjchem-966	90	43	/	/	SYM
eurjchem-966	90	44	z	z	PROPN
eurjchem-966	90	45	357	357	NUM
eurjchem-966	90	46	(	(	PUNCT
eurjchem-966	90	47	corresponding	correspond	VERB
eurjchem-966	90	48	to	to	ADP
eurjchem-966	90	49	the	the	DET
eurjchem-966	90	50	molecular	molecular	ADJ
eurjchem-966	90	51	weight	weight	NOUN
eurjchem-966	90	52	of	of	ADP
eurjchem-966	90	53	deg	deg	PROPN
eurjchem-966	90	54	)	)	PUNCT
eurjchem-966	90	55	.	.	PUNCT
eurjchem-966	91	1	(	(	PUNCT
eurjchem-966	91	2	a	a	X
eurjchem-966	91	3	)	)	PUNCT
eurjchem-966	91	4	(	(	PUNCT
eurjchem-966	91	5	b	b	X
eurjchem-966	91	6	)	)	PUNCT
eurjchem-966	91	7	figure	figure	NOUN
eurjchem-966	91	8	3	3	NUM
eurjchem-966	91	9	.	.	PUNCT
eurjchem-966	91	10	ir	ir	PROPN
eurjchem-966	91	11	spectra	spectra	PROPN
eurjchem-966	91	12	of	of	ADP
eurjchem-966	91	13	(	(	PUNCT
eurjchem-966	91	14	a	a	PRON
eurjchem-966	91	15	)	)	PUNCT
eurjchem-966	91	16	acm	acm	NOUN
eurjchem-966	91	17	and	and	CCONJ
eurjchem-966	91	18	(	(	PUNCT
eurjchem-966	91	19	b	b	NOUN
eurjchem-966	91	20	)	)	PUNCT
eurjchem-966	91	21	deg	deg	NOUN
eurjchem-966	91	22	.	.	PUNCT
eurjchem-966	92	1	222	222	NUM
eurjchem-966	92	2	naguib	naguib	NOUN
eurjchem-966	92	3	et	et	PROPN
eurjchem-966	92	4	al	al	PROPN
eurjchem-966	92	5	.	.	PUNCT
eurjchem-966	92	6	/	/	SYM
eurjchem-966	92	7	european	european	PROPN
eurjchem-966	92	8	journal	journal	PROPN
eurjchem-966	92	9	of	of	ADP
eurjchem-966	92	10	chemistry	chemistry	NOUN
eurjchem-966	92	11	5	5	NUM
eurjchem-966	92	12	(	(	PUNCT
eurjchem-966	92	13	2	2	NUM
eurjchem-966	92	14	)	)	PUNCT
eurjchem-966	92	15	(	(	PUNCT
eurjchem-966	92	16	2014	2014	NUM
eurjchem-966	92	17	)	)	PUNCT
eurjchem-966	92	18	219‐226	219‐226	NUM
eurjchem-966	92	19	(	(	PUNCT
eurjchem-966	92	20	a	a	NOUN
eurjchem-966	92	21	)	)	PUNCT
eurjchem-966	92	22	(	(	PUNCT
eurjchem-966	92	23	b	b	X
eurjchem-966	92	24	)	)	PUNCT
eurjchem-966	92	25	figure	figure	NOUN
eurjchem-966	92	26	4	4	NUM
eurjchem-966	92	27	.	.	PUNCT
eurjchem-966	92	28	mass	mass	ADJ
eurjchem-966	92	29	spectra	spectra	NOUN
eurjchem-966	92	30	of	of	ADP
eurjchem-966	92	31	(	(	PUNCT
eurjchem-966	92	32	a	a	PRON
eurjchem-966	92	33	)	)	PUNCT
eurjchem-966	92	34	acm	acm	NOUN
eurjchem-966	92	35	and	and	CCONJ
eurjchem-966	92	36	(	(	PUNCT
eurjchem-966	92	37	b	b	NOUN
eurjchem-966	92	38	)	)	PUNCT
eurjchem-966	92	39	deg	deg	NOUN
eurjchem-966	92	40	.	.	PROPN
eurjchem-966	93	1	3.1	3.1	NUM
eurjchem-966	93	2	.	.	PUNCT
eurjchem-966	93	3	spectrophotometric	spectrophotometric	ADJ
eurjchem-966	93	4	methods	method	NOUN
eurjchem-966	93	5	3.1.1	3.1.1	NUM
eurjchem-966	93	6	.	.	PUNCT
eurjchem-966	94	1	1dd	1dd	ADJ
eurjchem-966	94	2	spectrophotometric	spectrophotometric	ADJ
eurjchem-966	94	3	method	method	NOUN
eurjchem-966	94	4	the	the	DET
eurjchem-966	94	5	zero‐order	zero‐order	NOUN
eurjchem-966	94	6	absorption	absorption	NOUN
eurjchem-966	94	7	spectra	spectra	NOUN
eurjchem-966	94	8	of	of	ADP
eurjchem-966	94	9	acm	acm	PROPN
eurjchem-966	94	10	and	and	CCONJ
eurjchem-966	94	11	its	its	PRON
eurjchem-966	94	12	deg	deg	NOUN
eurjchem-966	94	13	show	show	NOUN
eurjchem-966	94	14	sever	sever	ADJ
eurjchem-966	94	15	or	or	CCONJ
eurjchem-966	94	16	even	even	ADV
eurjchem-966	94	17	complete	complete	ADJ
eurjchem-966	94	18	overlapping	overlap	VERB
eurjchem-966	94	19	(	(	PUNCT
eurjchem-966	94	20	figure	figure	NOUN
eurjchem-966	94	21	5	5	NUM
eurjchem-966	94	22	)	)	PUNCT
eurjchem-966	94	23	,	,	PUNCT
eurjchem-966	94	24	which	which	PRON
eurjchem-966	94	25	interferes	interfere	VERB
eurjchem-966	94	26	with	with	ADP
eurjchem-966	94	27	the	the	DET
eurjchem-966	94	28	direct	direct	ADJ
eurjchem-966	94	29	spectrophotometric	spectrophotometric	ADJ
eurjchem-966	94	30	determination	determination	NOUN
eurjchem-966	94	31	of	of	ADP
eurjchem-966	94	32	acm	acm	NOUN
eurjchem-966	94	33	in	in	ADP
eurjchem-966	94	34	presence	presence	NOUN
eurjchem-966	94	35	of	of	ADP
eurjchem-966	94	36	its	its	PRON
eurjchem-966	94	37	deg	deg	NOUN
eurjchem-966	94	38	.	.	PUNCT
eurjchem-966	95	1	derivative	derivative	ADJ
eurjchem-966	95	2	ratio	ratio	NOUN
eurjchem-966	95	3	spectroscopy	spectroscopy	NOUN
eurjchem-966	95	4	is	be	AUX
eurjchem-966	95	5	an	an	DET
eurjchem-966	95	6	analytical	analytical	ADJ
eurjchem-966	95	7	technique	technique	NOUN
eurjchem-966	95	8	of	of	ADP
eurjchem-966	95	9	great	great	ADJ
eurjchem-966	95	10	utility	utility	NOUN
eurjchem-966	95	11	for	for	ADP
eurjchem-966	95	12	resolving	resolve	VERB
eurjchem-966	95	13	overlapped	overlapped	ADJ
eurjchem-966	95	14	spectra	spectra	NOUN
eurjchem-966	95	15	,	,	PUNCT
eurjchem-966	95	16	by	by	ADP
eurjchem-966	95	17	applying	apply	VERB
eurjchem-966	95	18	this	this	DET
eurjchem-966	95	19	technique	technique	NOUN
eurjchem-966	95	20	selective	selective	ADJ
eurjchem-966	95	21	determination	determination	NOUN
eurjchem-966	95	22	of	of	ADP
eurjchem-966	95	23	acm	acm	NOUN
eurjchem-966	95	24	in	in	ADP
eurjchem-966	95	25	presence	presence	NOUN
eurjchem-966	95	26	of	of	ADP
eurjchem-966	95	27	deg	deg	PROPN
eurjchem-966	95	28	was	be	AUX
eurjchem-966	95	29	achieved	achieve	VERB
eurjchem-966	95	30	by	by	ADP
eurjchem-966	95	31	measuring	measure	VERB
eurjchem-966	95	32	the	the	DET
eurjchem-966	95	33	peak	peak	NOUN
eurjchem-966	95	34	amplitude	amplitude	NOUN
eurjchem-966	95	35	at	at	ADP
eurjchem-966	95	36	244	244	NUM
eurjchem-966	95	37	nm	nm	NOUN
eurjchem-966	95	38	as	as	SCONJ
eurjchem-966	95	39	shown	show	VERB
eurjchem-966	95	40	in	in	ADP
eurjchem-966	95	41	figure	figure	NOUN
eurjchem-966	95	42	6	6	NUM
eurjchem-966	95	43	.	.	PUNCT
eurjchem-966	95	44	figure	figure	NOUN
eurjchem-966	95	45	5	5	NUM
eurjchem-966	95	46	.	.	NOUN
eurjchem-966	95	47	zero	zero	NUM
eurjchem-966	95	48	order	order	NOUN
eurjchem-966	95	49	absorption	absorption	NOUN
eurjchem-966	95	50	spectra	spectra	NOUN
eurjchem-966	95	51	of	of	ADP
eurjchem-966	95	52	8	8	NUM
eurjchem-966	95	53	µg	µg	NOUN
eurjchem-966	95	54	/	/	SYM
eurjchem-966	95	55	ml	ml	NOUN
eurjchem-966	95	56	of	of	ADP
eurjchem-966	95	57	acm	acm	NOUN
eurjchem-966	95	58	(	(	PUNCT
eurjchem-966	95	59	ــــــ	ــــــ	PROPN
eurjchem-966	95	60	)	)	PUNCT
eurjchem-966	95	61	and	and	CCONJ
eurjchem-966	95	62	8	8	NUM
eurjchem-966	95	63	µg	µg	NOUN
eurjchem-966	95	64	/	/	SYM
eurjchem-966	95	65	ml	ml	NOUN
eurjchem-966	95	66	of	of	ADP
eurjchem-966	95	67	deg	deg	PROPN
eurjchem-966	95	68	(	(	PUNCT
eurjchem-966	95	69	ــ	ــ	NOUN
eurjchem-966	95	70	ــ	ــ	X
eurjchem-966	95	71	ــ	ــ	NOUN
eurjchem-966	95	72	)	)	PUNCT
eurjchem-966	95	73	using	use	VERB
eurjchem-966	95	74	purified	purified	ADJ
eurjchem-966	95	75	water	water	NOUN
eurjchem-966	95	76	as	as	ADP
eurjchem-966	95	77	a	a	DET
eurjchem-966	95	78	blank	blank	NOUN
eurjchem-966	95	79	.	.	PUNCT
eurjchem-966	96	1	figure	figure	NOUN
eurjchem-966	96	2	6	6	NUM
eurjchem-966	96	3	.	.	PUNCT
eurjchem-966	97	1	first	first	ADJ
eurjchem-966	97	2	derivative	derivative	NOUN
eurjchem-966	97	3	of	of	ADP
eurjchem-966	97	4	the	the	DET
eurjchem-966	97	5	ratio	ratio	NOUN
eurjchem-966	97	6	spectra	spectra	NOUN
eurjchem-966	97	7	of	of	ADP
eurjchem-966	97	8	16	16	NUM
eurjchem-966	97	9	µg	µg	NOUN
eurjchem-966	97	10	/	/	SYM
eurjchem-966	97	11	ml	ml	NOUN
eurjchem-966	97	12	of	of	ADP
eurjchem-966	97	13	acm	acm	NOUN
eurjchem-966	97	14	(	(	PUNCT
eurjchem-966	97	15	ــــــ	ــــــ	PROPN
eurjchem-966	97	16	)	)	PUNCT
eurjchem-966	97	17	and	and	CCONJ
eurjchem-966	97	18	16	16	NUM
eurjchem-966	97	19	µg	µg	NOUN
eurjchem-966	97	20	/	/	SYM
eurjchem-966	97	21	ml	ml	PROPN
eurjchem-966	97	22	of	of	ADP
eurjchem-966	97	23	deg	deg	PROPN
eurjchem-966	97	24	(	(	PUNCT
eurjchem-966	97	25	ــ	ــ	NOUN
eurjchem-966	97	26	ــ	ــ	X
eurjchem-966	97	27	ــ	ــ	NOUN
eurjchem-966	97	28	)	)	PUNCT
eurjchem-966	97	29	using	use	VERB
eurjchem-966	97	30	20	20	NUM
eurjchem-966	97	31	µg	µg	NOUN
eurjchem-966	97	32	/	/	SYM
eurjchem-966	97	33	ml	ml	NOUN
eurjchem-966	97	34	of	of	ADP
eurjchem-966	97	35	deg	deg	PROPN
eurjchem-966	97	36	as	as	ADP
eurjchem-966	97	37	divisor	divisor	NOUN
eurjchem-966	97	38	and	and	CCONJ
eurjchem-966	97	39	purified	purified	ADJ
eurjchem-966	97	40	water	water	NOUN
eurjchem-966	97	41	as	as	ADP
eurjchem-966	97	42	a	a	DET
eurjchem-966	97	43	blank	blank	NOUN
eurjchem-966	97	44	.	.	PUNCT
eurjchem-966	98	1	3.1.2	3.1.2	X
eurjchem-966	98	2	.	.	PUNCT
eurjchem-966	98	3	mean	mean	ADJ
eurjchem-966	98	4	centering	centering	NOUN
eurjchem-966	98	5	of	of	ADP
eurjchem-966	98	6	ratio	ratio	NOUN
eurjchem-966	98	7	spectra	spectra	PROPN
eurjchem-966	98	8	spectrophotometric	spectrophotometric	ADJ
eurjchem-966	98	9	method	method	NOUN
eurjchem-966	98	10	(	(	PUNCT
eurjchem-966	98	11	mcr	mcr	PROPN
eurjchem-966	98	12	)	)	PUNCT
eurjchem-966	98	13	the	the	DET
eurjchem-966	98	14	developed	develop	VERB
eurjchem-966	98	15	mcr	mcr	PROPN
eurjchem-966	98	16	method	method	NOUN
eurjchem-966	98	17	depends	depend	VERB
eurjchem-966	98	18	on	on	ADP
eurjchem-966	98	19	the	the	DET
eurjchem-966	98	20	mean	mean	ADJ
eurjchem-966	98	21	centering	centering	NOUN
eurjchem-966	98	22	of	of	ADP
eurjchem-966	98	23	the	the	DET
eurjchem-966	98	24	ratio	ratio	NOUN
eurjchem-966	98	25	spectra	spectra	NOUN
eurjchem-966	98	26	,	,	PUNCT
eurjchem-966	98	27	it	it	PRON
eurjchem-966	98	28	eliminates	eliminate	VERB
eurjchem-966	98	29	the	the	DET
eurjchem-966	98	30	derivative	derivative	ADJ
eurjchem-966	98	31	steps	step	NOUN
eurjchem-966	98	32	and	and	CCONJ
eurjchem-966	98	33	so	so	ADV
eurjchem-966	98	34	signal‐to‐noise	signal‐to‐noise	PROPN
eurjchem-966	98	35	ratio	ratio	NOUN
eurjchem-966	98	36	is	be	AUX
eurjchem-966	98	37	enhanced	enhance	VERB
eurjchem-966	98	38	[	[	PUNCT
eurjchem-966	98	39	16	16	NUM
eurjchem-966	98	40	]	]	PUNCT
eurjchem-966	98	41	.	.	PUNCT
eurjchem-966	99	1	it	it	PRON
eurjchem-966	99	2	has	have	AUX
eurjchem-966	99	3	been	be	AUX
eurjchem-966	99	4	applied	apply	VERB
eurjchem-966	99	5	for	for	ADP
eurjchem-966	99	6	resolving	resolve	VERB
eurjchem-966	99	7	binary	binary	ADJ
eurjchem-966	99	8	and	and	CCONJ
eurjchem-966	99	9	ternary	ternary	ADJ
eurjchem-966	99	10	mixtures	mixture	NOUN
eurjchem-966	99	11	in	in	ADP
eurjchem-966	99	12	complex	complex	ADJ
eurjchem-966	99	13	samples	sample	NOUN
eurjchem-966	99	14	with	with	ADP
eurjchem-966	99	15	unknown	unknown	ADJ
eurjchem-966	99	16	matrices	matrix	NOUN
eurjchem-966	99	17	[	[	X
eurjchem-966	99	18	17	17	NUM
eurjchem-966	99	19	]	]	PUNCT
eurjchem-966	99	20	.	.	PUNCT
eurjchem-966	100	1	the	the	DET
eurjchem-966	100	2	mathematical	mathematical	ADJ
eurjchem-966	100	3	explanation	explanation	NOUN
eurjchem-966	100	4	of	of	ADP
eurjchem-966	100	5	the	the	DET
eurjchem-966	100	6	method	method	NOUN
eurjchem-966	100	7	was	be	AUX
eurjchem-966	100	8	obtained	obtain	VERB
eurjchem-966	100	9	and	and	CCONJ
eurjchem-966	100	10	illustrated	illustrate	VERB
eurjchem-966	100	11	by	by	ADP
eurjchem-966	100	12	afkhami	afkhami	NOUN
eurjchem-966	100	13	and	and	CCONJ
eurjchem-966	100	14	bahram	bahram	PROPN
eurjchem-966	101	1	[	[	X
eurjchem-966	101	2	18	18	NUM
eurjchem-966	101	3	]	]	PUNCT
eurjchem-966	101	4	.	.	PUNCT
eurjchem-966	102	1	the	the	DET
eurjchem-966	102	2	main	main	ADJ
eurjchem-966	102	3	step	step	NOUN
eurjchem-966	102	4	in	in	ADP
eurjchem-966	102	5	the	the	DET
eurjchem-966	102	6	development	development	NOUN
eurjchem-966	102	7	of	of	ADP
eurjchem-966	102	8	an	an	DET
eurjchem-966	102	9	analytical	analytical	ADJ
eurjchem-966	102	10	method	method	NOUN
eurjchem-966	102	11	is	be	AUX
eurjchem-966	102	12	to	to	PART
eurjchem-966	102	13	optimize	optimize	VERB
eurjchem-966	102	14	the	the	DET
eurjchem-966	102	15	conditions	condition	NOUN
eurjchem-966	102	16	and	and	CCONJ
eurjchem-966	102	17	parameters	parameter	NOUN
eurjchem-966	102	18	,	,	PUNCT
eurjchem-966	102	19	which	which	PRON
eurjchem-966	102	20	will	will	AUX
eurjchem-966	102	21	be	be	AUX
eurjchem-966	102	22	followed	follow	VERB
eurjchem-966	102	23	in	in	ADP
eurjchem-966	102	24	development	development	NOUN
eurjchem-966	102	25	and	and	CCONJ
eurjchem-966	102	26	validation	validation	NOUN
eurjchem-966	102	27	to	to	PART
eurjchem-966	102	28	obtain	obtain	VERB
eurjchem-966	102	29	the	the	DET
eurjchem-966	102	30	best	good	ADJ
eurjchem-966	102	31	results	result	NOUN
eurjchem-966	102	32	.	.	PUNCT
eurjchem-966	103	1	to	to	PART
eurjchem-966	103	2	optimize	optimize	VERB
eurjchem-966	103	3	the	the	DET
eurjchem-966	103	4	1dd	1dd	ADJ
eurjchem-966	103	5	and	and	CCONJ
eurjchem-966	103	6	mean	mean	ADJ
eurjchem-966	103	7	centering	center	VERB
eurjchem-966	103	8	spectrophotometric	spectrophotometric	ADJ
eurjchem-966	103	9	methods	method	NOUN
eurjchem-966	103	10	,	,	PUNCT
eurjchem-966	103	11	it	it	PRON
eurjchem-966	103	12	was	be	AUX
eurjchem-966	103	13	necessary	necessary	ADJ
eurjchem-966	103	14	to	to	PART
eurjchem-966	103	15	test	test	VERB
eurjchem-966	103	16	the	the	DET
eurjchem-966	103	17	influence	influence	NOUN
eurjchem-966	103	18	of	of	ADP
eurjchem-966	103	19	the	the	DET
eurjchem-966	103	20	following	following	ADJ
eurjchem-966	103	21	variables	variable	NOUN
eurjchem-966	103	22	:	:	PUNCT
eurjchem-966	103	23	3.1.2.1	3.1.2.1	NUM
eurjchem-966	103	24	.	.	PUNCT
eurjchem-966	104	1	solvents	solvent	NOUN
eurjchem-966	104	2	different	different	ADJ
eurjchem-966	104	3	solvents	solvent	NOUN
eurjchem-966	104	4	were	be	AUX
eurjchem-966	104	5	studied	study	VERB
eurjchem-966	104	6	(	(	PUNCT
eurjchem-966	104	7	methanol	methanol	NOUN
eurjchem-966	104	8	,	,	PUNCT
eurjchem-966	104	9	ethanol	ethanol	NOUN
eurjchem-966	104	10	,	,	PUNCT
eurjchem-966	104	11	isopropanol	isopropanol	NOUN
eurjchem-966	104	12	,	,	PUNCT
eurjchem-966	104	13	acetonitrile	acetonitrile	NOUN
eurjchem-966	104	14	,	,	PUNCT
eurjchem-966	104	15	purified	purified	ADJ
eurjchem-966	104	16	water	water	NOUN
eurjchem-966	104	17	,	,	PUNCT
eurjchem-966	105	1	0.1	0.1	NUM
eurjchem-966	105	2	m	m	NOUN
eurjchem-966	105	3	hcl	hcl	PROPN
eurjchem-966	105	4	and	and	CCONJ
eurjchem-966	105	5	0.1	0.1	NUM
eurjchem-966	105	6	m	m	NOUN
eurjchem-966	105	7	naoh	naoh	NOUN
eurjchem-966	105	8	)	)	PUNCT
eurjchem-966	105	9	.	.	PUNCT
eurjchem-966	106	1	it	it	PRON
eurjchem-966	106	2	was	be	AUX
eurjchem-966	106	3	found	find	VERB
eurjchem-966	106	4	that	that	SCONJ
eurjchem-966	106	5	purified	purified	ADJ
eurjchem-966	106	6	water	water	NOUN
eurjchem-966	106	7	was	be	AUX
eurjchem-966	106	8	the	the	DET
eurjchem-966	106	9	best	good	ADJ
eurjchem-966	106	10	solvent	solvent	NOUN
eurjchem-966	106	11	regarding	regard	VERB
eurjchem-966	106	12	selectivity	selectivity	NOUN
eurjchem-966	106	13	and	and	CCONJ
eurjchem-966	106	14	sensitivity	sensitivity	NOUN
eurjchem-966	106	15	.	.	PUNCT
eurjchem-966	107	1	3.1.2.2	3.1.2.2	X
eurjchem-966	107	2	.	.	PUNCT
eurjchem-966	108	1	the	the	DET
eurjchem-966	108	2	divisor	divisor	NOUN
eurjchem-966	108	3	and	and	CCONJ
eurjchem-966	108	4	its	its	PRON
eurjchem-966	108	5	concentration	concentration	NOUN
eurjchem-966	108	6	the	the	DET
eurjchem-966	108	7	effect	effect	NOUN
eurjchem-966	108	8	of	of	ADP
eurjchem-966	108	9	divisor	divisor	NOUN
eurjchem-966	108	10	concentration	concentration	NOUN
eurjchem-966	108	11	on	on	ADP
eurjchem-966	108	12	the	the	DET
eurjchem-966	108	13	method	method	NOUN
eurjchem-966	108	14	selectivity	selectivity	NOUN
eurjchem-966	108	15	and	and	CCONJ
eurjchem-966	108	16	analytical	analytical	ADJ
eurjchem-966	108	17	parameters	parameter	NOUN
eurjchem-966	108	18	such	such	ADJ
eurjchem-966	108	19	as	as	ADP
eurjchem-966	108	20	slope	slope	NOUN
eurjchem-966	108	21	,	,	PUNCT
eurjchem-966	108	22	intercept	intercept	NOUN
eurjchem-966	108	23	and	and	CCONJ
eurjchem-966	108	24	correlation	correlation	NOUN
eurjchem-966	108	25	coefficient	coefficient	NOUN
eurjchem-966	108	26	of	of	ADP
eurjchem-966	108	27	calibration	calibration	NOUN
eurjchem-966	108	28	equations	equation	NOUN
eurjchem-966	108	29	was	be	AUX
eurjchem-966	108	30	tested	test	VERB
eurjchem-966	108	31	.	.	PUNCT
eurjchem-966	109	1	different	different	ADJ
eurjchem-966	109	2	concentrations	concentration	NOUN
eurjchem-966	109	3	of	of	ADP
eurjchem-966	109	4	deg	deg	PROPN
eurjchem-966	109	5	were	be	AUX
eurjchem-966	109	6	tested	test	VERB
eurjchem-966	109	7	as	as	ADP
eurjchem-966	109	8	a	a	DET
eurjchem-966	109	9	divisor	divisor	NOUN
eurjchem-966	109	10	(	(	PUNCT
eurjchem-966	109	11	2	2	NUM
eurjchem-966	109	12	,	,	PUNCT
eurjchem-966	109	13	4	4	NUM
eurjchem-966	109	14	,	,	PUNCT
eurjchem-966	109	15	6	6	NUM
eurjchem-966	109	16	,	,	PUNCT
eurjchem-966	109	17	8	8	NUM
eurjchem-966	109	18	,	,	PUNCT
eurjchem-966	109	19	16	16	NUM
eurjchem-966	109	20	,	,	PUNCT
eurjchem-966	109	21	20	20	NUM
eurjchem-966	109	22	µg	µg	NOUN
eurjchem-966	109	23	/	/	SYM
eurjchem-966	109	24	ml	ml	NOUN
eurjchem-966	109	25	)	)	PUNCT
eurjchem-966	109	26	.	.	PUNCT
eurjchem-966	110	1	it	it	PRON
eurjchem-966	110	2	was	be	AUX
eurjchem-966	110	3	found	find	VERB
eurjchem-966	110	4	that	that	SCONJ
eurjchem-966	110	5	20	20	NUM
eurjchem-966	110	6	µg	µg	NOUN
eurjchem-966	110	7	/	/	SYM
eurjchem-966	110	8	ml	ml	NOUN
eurjchem-966	110	9	of	of	ADP
eurjchem-966	110	10	deg	deg	PROPN
eurjchem-966	110	11	was	be	AUX
eurjchem-966	110	12	the	the	DET
eurjchem-966	110	13	best	good	ADJ
eurjchem-966	110	14	regarding	regard	VERB
eurjchem-966	110	15	selectivity	selectivity	NOUN
eurjchem-966	110	16	and	and	CCONJ
eurjchem-966	110	17	sensitivity	sensitivity	NOUN
eurjchem-966	110	18	.	.	PUNCT
eurjchem-966	111	1	3.1.2.3	3.1.2.3	NUM
eurjchem-966	111	2	.	.	NOUN
eurjchem-966	111	3	smoothing	smooth	VERB
eurjchem-966	111	4	and	and	CCONJ
eurjchem-966	111	5	scaling	scale	VERB
eurjchem-966	111	6	factors	factor	NOUN
eurjchem-966	111	7	different	different	ADJ
eurjchem-966	111	8	smoothing	smoothing	NOUN
eurjchem-966	111	9	factor	factor	NOUN
eurjchem-966	111	10	(	(	PUNCT
eurjchem-966	111	11	δλ	δλ	NOUN
eurjchem-966	111	12	)	)	PUNCT
eurjchem-966	111	13	values	value	NOUN
eurjchem-966	111	14	were	be	AUX
eurjchem-966	111	15	tried	try	VERB
eurjchem-966	111	16	,	,	PUNCT
eurjchem-966	111	17	where	where	SCONJ
eurjchem-966	111	18	smoothing	smoothing	NOUN
eurjchem-966	111	19	factor	factor	NOUN
eurjchem-966	111	20	=	=	SYM
eurjchem-966	111	21	4	4	NUM
eurjchem-966	111	22	showed	show	VERB
eurjchem-966	111	23	a	a	DET
eurjchem-966	111	24	suitable	suitable	ADJ
eurjchem-966	111	25	signal	signal	NOUN
eurjchem-966	111	26	to	to	PART
eurjchem-966	111	27	noise	noise	VERB
eurjchem-966	111	28	ratio	ratio	NOUN
eurjchem-966	111	29	with	with	ADP
eurjchem-966	111	30	good	good	ADJ
eurjchem-966	111	31	resolution	resolution	NOUN
eurjchem-966	111	32	.	.	PUNCT
eurjchem-966	112	1	different	different	ADJ
eurjchem-966	112	2	scaling	scale	VERB
eurjchem-966	112	3	factor	factor	NOUN
eurjchem-966	112	4	values	value	NOUN
eurjchem-966	112	5	were	be	AUX
eurjchem-966	112	6	tried	try	VERB
eurjchem-966	112	7	where	where	SCONJ
eurjchem-966	112	8	scaling	scaling	NOUN
eurjchem-966	112	9	factor	factor	NOUN
eurjchem-966	112	10	=	=	SYM
eurjchem-966	112	11	10	10	NUM
eurjchem-966	112	12	was	be	AUX
eurjchem-966	112	13	the	the	DET
eurjchem-966	112	14	best	good	ADJ
eurjchem-966	112	15	to	to	PART
eurjchem-966	112	16	measure	measure	VERB
eurjchem-966	112	17	the	the	DET
eurjchem-966	112	18	signal	signal	NOUN
eurjchem-966	112	19	of	of	ADP
eurjchem-966	112	20	acm	acm	PROPN
eurjchem-966	112	21	and	and	CCONJ
eurjchem-966	112	22	to	to	PART
eurjchem-966	112	23	decrease	decrease	VERB
eurjchem-966	112	24	the	the	DET
eurjchem-966	112	25	reading	reading	NOUN
eurjchem-966	112	26	error	error	NOUN
eurjchem-966	112	27	.	.	PUNCT
eurjchem-966	113	1	the	the	DET
eurjchem-966	113	2	peak	peak	NOUN
eurjchem-966	113	3	amplitude	amplitude	NOUN
eurjchem-966	113	4	of	of	ADP
eurjchem-966	113	5	the	the	DET
eurjchem-966	113	6	first	first	ADJ
eurjchem-966	113	7	derivative	derivative	NOUN
eurjchem-966	113	8	of	of	ADP
eurjchem-966	113	9	ratio	ratio	NOUN
eurjchem-966	113	10	spectra	spectra	NOUN
eurjchem-966	113	11	at	at	ADP
eurjchem-966	113	12	λ	λ	X
eurjchem-966	113	13	=	=	SYM
eurjchem-966	113	14	244	244	NUM
eurjchem-966	113	15	nm	nm	NOUN
eurjchem-966	113	16	(	(	PUNCT
eurjchem-966	113	17	as	as	SCONJ
eurjchem-966	113	18	shown	show	VERB
eurjchem-966	113	19	in	in	ADP
eurjchem-966	113	20	figure	figure	NOUN
eurjchem-966	113	21	7	7	NUM
eurjchem-966	113	22	)	)	PUNCT
eurjchem-966	113	23	was	be	AUX
eurjchem-966	113	24	plotted	plot	VERB
eurjchem-966	113	25	versus	versus	ADP
eurjchem-966	113	26	the	the	DET
eurjchem-966	113	27	concentration	concentration	NOUN
eurjchem-966	113	28	of	of	ADP
eurjchem-966	113	29	acm	acm	NOUN
eurjchem-966	113	30	in	in	ADP
eurjchem-966	113	31	the	the	DET
eurjchem-966	113	32	range	range	NOUN
eurjchem-966	113	33	of	of	ADP
eurjchem-966	113	34	2‐22	2‐22	NUM
eurjchem-966	113	35	µg	µg	NOUN
eurjchem-966	113	36	/	/	SYM
eurjchem-966	113	37	ml	ml	NOUN
eurjchem-966	113	38	.	.	PUNCT
eurjchem-966	114	1	the	the	DET
eurjchem-966	114	2	calibration	calibration	NOUN
eurjchem-966	114	3	curve	curve	NOUN
eurjchem-966	114	4	was	be	AUX
eurjchem-966	114	5	constructed	construct	VERB
eurjchem-966	114	6	with	with	ADP
eurjchem-966	114	7	mean	mean	ADJ
eurjchem-966	114	8	percentage	percentage	NOUN
eurjchem-966	114	9	recovery	recovery	NOUN
eurjchem-966	114	10	99.65%±0.797	99.65%±0.797	NOUN
eurjchem-966	114	11	.	.	PUNCT
eurjchem-966	115	1	the	the	DET
eurjchem-966	115	2	following	follow	VERB
eurjchem-966	115	3	linear	linear	PROPN
eurjchem-966	115	4	regression	regression	NOUN
eurjchem-966	115	5	equation	equation	NOUN
eurjchem-966	115	6	was	be	AUX
eurjchem-966	115	7	obtained	obtain	VERB
eurjchem-966	115	8	:	:	PUNCT
eurjchem-966	116	1	y	y	PROPN
eurjchem-966	116	2	=	=	PUNCT
eurjchem-966	116	3	0.0039c	0.0039c	PROPN
eurjchem-966	116	4	+	+	NOUN
eurjchem-966	116	5	0.0024	0.0024	NUM
eurjchem-966	116	6	,	,	PUNCT
eurjchem-966	116	7	r	r	NOUN
eurjchem-966	116	8	=	=	SYM
eurjchem-966	116	9	0.9999	0.9999	NUM
eurjchem-966	116	10	(	(	PUNCT
eurjchem-966	116	11	1	1	NUM
eurjchem-966	116	12	)	)	PUNCT
eurjchem-966	116	13	where	where	SCONJ
eurjchem-966	116	14	y	y	PROPN
eurjchem-966	116	15	is	be	AUX
eurjchem-966	116	16	the	the	DET
eurjchem-966	116	17	peak	peak	NOUN
eurjchem-966	116	18	amplitude	amplitude	NOUN
eurjchem-966	116	19	at	at	ADP
eurjchem-966	116	20	244	244	NUM
eurjchem-966	116	21	nm	nm	NOUN
eurjchem-966	116	22	,	,	PUNCT
eurjchem-966	116	23	c	c	PROPN
eurjchem-966	116	24	is	be	AUX
eurjchem-966	116	25	the	the	DET
eurjchem-966	116	26	concentration	concentration	NOUN
eurjchem-966	116	27	in	in	ADP
eurjchem-966	116	28	µg	µg	ADV
eurjchem-966	116	29	/	/	SYM
eurjchem-966	116	30	ml	ml	NOUN
eurjchem-966	116	31	and	and	CCONJ
eurjchem-966	116	32	r	r	NOUN
eurjchem-966	116	33	is	be	AUX
eurjchem-966	116	34	the	the	DET
eurjchem-966	116	35	correlation	correlation	NOUN
eurjchem-966	116	36	coefficient	coefficient	NOUN
eurjchem-966	116	37	.	.	PUNCT
eurjchem-966	117	1	figure	figure	VERB
eurjchem-966	117	2	7	7	NUM
eurjchem-966	117	3	.	.	PUNCT
eurjchem-966	118	1	first	first	ADJ
eurjchem-966	118	2	derivative	derivative	NOUN
eurjchem-966	118	3	of	of	ADP
eurjchem-966	118	4	ratio	ratio	NOUN
eurjchem-966	118	5	spectra	spectra	NOUN
eurjchem-966	118	6	of	of	ADP
eurjchem-966	118	7	of	of	ADP
eurjchem-966	118	8	acm	acm	NOUN
eurjchem-966	118	9	in	in	ADP
eurjchem-966	118	10	the	the	DET
eurjchem-966	118	11	range	range	NOUN
eurjchem-966	118	12	of	of	ADP
eurjchem-966	118	13	2‐22	2‐22	NUM
eurjchem-966	118	14	µg	µg	NOUN
eurjchem-966	118	15	/	/	SYM
eurjchem-966	118	16	ml	ml	NOUN
eurjchem-966	118	17	using	use	VERB
eurjchem-966	118	18	20	20	NUM
eurjchem-966	118	19	µg	µg	NOUN
eurjchem-966	118	20	/	/	SYM
eurjchem-966	118	21	ml	ml	NOUN
eurjchem-966	118	22	deg	deg	NOUN
eurjchem-966	118	23	as	as	ADP
eurjchem-966	118	24	a	a	DET
eurjchem-966	118	25	divisor	divisor	NOUN
eurjchem-966	118	26	purified	purify	VERB
eurjchem-966	118	27	water	water	NOUN
eurjchem-966	118	28	as	as	ADP
eurjchem-966	118	29	blank	blank	ADJ
eurjchem-966	118	30	.	.	PUNCT
eurjchem-966	119	1	while	while	SCONJ
eurjchem-966	119	2	the	the	DET
eurjchem-966	119	3	absorption	absorption	NOUN
eurjchem-966	119	4	spectra	spectra	NOUN
eurjchem-966	119	5	of	of	ADP
eurjchem-966	119	6	acm	acm	PROPN
eurjchem-966	119	7	were	be	AUX
eurjchem-966	119	8	recorded	record	VERB
eurjchem-966	119	9	in	in	ADP
eurjchem-966	119	10	the	the	DET
eurjchem-966	119	11	wavelength	wavelength	NOUN
eurjchem-966	119	12	range	range	NOUN
eurjchem-966	119	13	of	of	ADP
eurjchem-966	119	14	220‐320	220‐320	NUM
eurjchem-966	119	15	nm	nm	NOUN
eurjchem-966	119	16	and	and	CCONJ
eurjchem-966	119	17	divided	divide	VERB
eurjchem-966	119	18	by	by	ADP
eurjchem-966	119	19	the	the	DET
eurjchem-966	119	20	absorption	absorption	NOUN
eurjchem-966	119	21	spectrum	spectrum	NOUN
eurjchem-966	119	22	deg	deg	NOUN
eurjchem-966	119	23	(	(	PUNCT
eurjchem-966	119	24	20	20	NUM
eurjchem-966	119	25	µg	µg	NOUN
eurjchem-966	119	26	/	/	SYM
eurjchem-966	119	27	ml	ml	NOUN
eurjchem-966	119	28	)	)	PUNCT
eurjchem-966	119	29	to	to	PART
eurjchem-966	119	30	obtain	obtain	VERB
eurjchem-966	119	31	the	the	DET
eurjchem-966	119	32	ratio	ratio	NOUN
eurjchem-966	119	33	spectra	spectra	NOUN
eurjchem-966	119	34	which	which	PRON
eurjchem-966	119	35	were	be	AUX
eurjchem-966	119	36	then	then	ADV
eurjchem-966	119	37	mean	mean	VERB
eurjchem-966	119	38	centered	center	VERB
eurjchem-966	119	39	.	.	PUNCT
eurjchem-966	120	1	acm	acm	PROPN
eurjchem-966	120	2	was	be	AUX
eurjchem-966	120	3	determined	determine	VERB
eurjchem-966	120	4	by	by	ADP
eurjchem-966	120	5	measuring	measure	VERB
eurjchem-966	120	6	the	the	DET
eurjchem-966	120	7	peak	peak	NOUN
eurjchem-966	120	8	amplitude	amplitude	NOUN
eurjchem-966	120	9	at	at	ADP
eurjchem-966	120	10	234	234	NUM
eurjchem-966	120	11	nm	nm	NOUN
eurjchem-966	120	12	which	which	PRON
eurjchem-966	120	13	corresponds	correspond	VERB
eurjchem-966	120	14	to	to	ADP
eurjchem-966	120	15	maximum	maximum	ADJ
eurjchem-966	120	16	wavelength	wavelength	NOUN
eurjchem-966	120	17	as	as	SCONJ
eurjchem-966	120	18	shown	show	VERB
eurjchem-966	120	19	in	in	ADP
eurjchem-966	120	20	figure	figure	NOUN
eurjchem-966	120	21	8	8	NUM
eurjchem-966	120	22	.	.	PUNCT
eurjchem-966	121	1	the	the	DET
eurjchem-966	121	2	peak	peak	NOUN
eurjchem-966	121	3	amplitude	amplitude	NOUN
eurjchem-966	121	4	was	be	AUX
eurjchem-966	121	5	plotted	plot	VERB
eurjchem-966	121	6	versus	versus	ADP
eurjchem-966	121	7	the	the	DET
eurjchem-966	121	8	corresponding	corresponding	ADJ
eurjchem-966	121	9	concentration	concentration	NOUN
eurjchem-966	121	10	in	in	ADP
eurjchem-966	121	11	the	the	DET
eurjchem-966	121	12	range	range	NOUN
eurjchem-966	121	13	of	of	ADP
eurjchem-966	121	14	2‐22	2‐22	NUM
eurjchem-966	121	15	µg	µg	NOUN
eurjchem-966	121	16	/	/	SYM
eurjchem-966	121	17	ml	ml	NOUN
eurjchem-966	121	18	.	.	PUNCT
eurjchem-966	122	1	the	the	DET
eurjchem-966	122	2	calibration	calibration	NOUN
eurjchem-966	122	3	curve	curve	NOUN
eurjchem-966	122	4	was	be	AUX
eurjchem-966	122	5	constructed	construct	VERB
eurjchem-966	122	6	with	with	ADP
eurjchem-966	122	7	mean	mean	ADJ
eurjchem-966	122	8	percentage	percentage	NOUN
eurjchem-966	122	9	recovery	recovery	NOUN
eurjchem-966	122	10	99.30%±1.146	99.30%±1.146	NOUN
eurjchem-966	122	11	.	.	PUNCT
eurjchem-966	123	1	the	the	DET
eurjchem-966	123	2	following	follow	VERB
eurjchem-966	123	3	linear	linear	PROPN
eurjchem-966	123	4	regression	regression	NOUN
eurjchem-966	123	5	equation	equation	NOUN
eurjchem-966	123	6	was	be	AUX
eurjchem-966	123	7	obtained	obtain	VERB
eurjchem-966	123	8	:	:	PUNCT
eurjchem-966	123	9	y	y	NOUN
eurjchem-966	123	10	=	=	PUNCT
eurjchem-966	123	11	0.003	0.003	NUM
eurjchem-966	123	12	c	c	NOUN
eurjchem-966	123	13	+	+	NOUN
eurjchem-966	123	14	0.003	0.003	NUM
eurjchem-966	123	15	,	,	PUNCT
eurjchem-966	123	16	r	r	NOUN
eurjchem-966	123	17	=	=	SYM
eurjchem-966	123	18	0.9999	0.9999	NUM
eurjchem-966	123	19	(	(	PUNCT
eurjchem-966	123	20	2	2	NUM
eurjchem-966	123	21	)	)	PUNCT
eurjchem-966	123	22	where	where	SCONJ
eurjchem-966	123	23	y	y	PROPN
eurjchem-966	123	24	is	be	AUX
eurjchem-966	123	25	the	the	DET
eurjchem-966	123	26	peak	peak	NOUN
eurjchem-966	123	27	amplitude	amplitude	NOUN
eurjchem-966	123	28	at	at	ADP
eurjchem-966	123	29	234	234	NUM
eurjchem-966	123	30	nm	nm	NOUN
eurjchem-966	123	31	,	,	PUNCT
eurjchem-966	123	32	c	c	PROPN
eurjchem-966	123	33	is	be	AUX
eurjchem-966	123	34	the	the	DET
eurjchem-966	123	35	concentration	concentration	NOUN
eurjchem-966	123	36	in	in	ADP
eurjchem-966	123	37	µg	µg	ADV
eurjchem-966	123	38	/	/	SYM
eurjchem-966	123	39	ml	ml	NOUN
eurjchem-966	123	40	and	and	CCONJ
eurjchem-966	123	41	r	r	NOUN
eurjchem-966	123	42	is	be	AUX
eurjchem-966	123	43	the	the	DET
eurjchem-966	123	44	correlation	correlation	NOUN
eurjchem-966	123	45	coefficient	coefficient	NOUN
eurjchem-966	123	46	.	.	PUNCT
eurjchem-966	124	1	naguib	naguib	PROPN
eurjchem-966	124	2	et	et	PROPN
eurjchem-966	124	3	al	al	PROPN
eurjchem-966	124	4	.	.	PUNCT
eurjchem-966	124	5	/	/	SYM
eurjchem-966	124	6	european	european	PROPN
eurjchem-966	124	7	journal	journal	PROPN
eurjchem-966	124	8	of	of	ADP
eurjchem-966	124	9	chemistry	chemistry	NOUN
eurjchem-966	124	10	5	5	NUM
eurjchem-966	124	11	(	(	PUNCT
eurjchem-966	124	12	2	2	NUM
eurjchem-966	124	13	)	)	PUNCT
eurjchem-966	124	14	(	(	PUNCT
eurjchem-966	124	15	2014	2014	NUM
eurjchem-966	124	16	)	)	PUNCT
eurjchem-966	124	17	219‐226	219‐226	NUM
eurjchem-966	124	18	223	223	NUM
eurjchem-966	124	19	figure	figure	NOUN
eurjchem-966	124	20	8	8	NUM
eurjchem-966	124	21	.	.	PUNCT
eurjchem-966	125	1	the	the	DET
eurjchem-966	125	2	mean	mean	ADJ
eurjchem-966	125	3	centered	center	VERB
eurjchem-966	125	4	ratio	ratio	NOUN
eurjchem-966	125	5	absorption	absorption	NOUN
eurjchem-966	125	6	spectra	spectra	NOUN
eurjchem-966	125	7	of	of	ADP
eurjchem-966	125	8	acm	acm	PROPN
eurjchem-966	125	9	in	in	ADP
eurjchem-966	125	10	the	the	DET
eurjchem-966	125	11	range	range	NOUN
eurjchem-966	125	12	of	of	ADP
eurjchem-966	125	13	2‐22	2‐22	NUM
eurjchem-966	125	14	µg	µg	NOUN
eurjchem-966	125	15	/	/	SYM
eurjchem-966	125	16	ml	ml	VERB
eurjchem-966	125	17	using	use	VERB
eurjchem-966	125	18	purified	purified	ADJ
eurjchem-966	125	19	water	water	NOUN
eurjchem-966	125	20	as	as	ADP
eurjchem-966	125	21	a	a	DET
eurjchem-966	125	22	blank	blank	NOUN
eurjchem-966	125	23	.	.	PUNCT
eurjchem-966	126	1	3.2	3.2	NUM
eurjchem-966	126	2	.	.	PUNCT
eurjchem-966	127	1	hptlc	hptlc	NOUN
eurjchem-966	127	2	method	method	NOUN
eurjchem-966	127	3	thin	thin	ADJ
eurjchem-966	127	4	layer	layer	NOUN
eurjchem-966	127	5	chromatography	chromatography	NOUN
eurjchem-966	127	6	(	(	PUNCT
eurjchem-966	127	7	tlc	tlc	NOUN
eurjchem-966	127	8	)	)	PUNCT
eurjchem-966	127	9	made	make	VERB
eurjchem-966	127	10	a	a	DET
eurjchem-966	127	11	great	great	ADJ
eurjchem-966	127	12	progress	progress	NOUN
eurjchem-966	127	13	and	and	CCONJ
eurjchem-966	127	14	attained	attain	VERB
eurjchem-966	127	15	a	a	DET
eurjchem-966	127	16	wide	wide	ADJ
eurjchem-966	127	17	acceptance	acceptance	NOUN
eurjchem-966	127	18	as	as	ADP
eurjchem-966	127	19	a	a	DET
eurjchem-966	127	20	major	major	ADJ
eurjchem-966	127	21	analytical	analytical	ADJ
eurjchem-966	127	22	tool	tool	NOUN
eurjchem-966	127	23	for	for	ADP
eurjchem-966	127	24	both	both	CCONJ
eurjchem-966	127	25	qualitative	qualitative	ADJ
eurjchem-966	127	26	and	and	CCONJ
eurjchem-966	127	27	quantitative	quantitative	ADJ
eurjchem-966	127	28	methods	method	NOUN
eurjchem-966	127	29	of	of	ADP
eurjchem-966	127	30	analysis	analysis	NOUN
eurjchem-966	127	31	and	and	CCONJ
eurjchem-966	127	32	became	become	VERB
eurjchem-966	127	33	a	a	DET
eurjchem-966	127	34	well	well	ADV
eurjchem-966	127	35	established	establish	VERB
eurjchem-966	127	36	method	method	NOUN
eurjchem-966	127	37	for	for	ADP
eurjchem-966	127	38	the	the	DET
eurjchem-966	127	39	assay	assay	NOUN
eurjchem-966	127	40	of	of	ADP
eurjchem-966	127	41	drugs	drug	NOUN
eurjchem-966	127	42	in	in	ADP
eurjchem-966	127	43	mixtures	mixture	NOUN
eurjchem-966	127	44	.	.	PUNCT
eurjchem-966	128	1	hptlc	hptlc	NOUN
eurjchem-966	128	2	offers	offer	VERB
eurjchem-966	128	3	the	the	DET
eurjchem-966	128	4	advantages	advantage	NOUN
eurjchem-966	128	5	of	of	ADP
eurjchem-966	128	6	automatic	automatic	ADJ
eurjchem-966	128	7	application	application	NOUN
eurjchem-966	128	8	,	,	PUNCT
eurjchem-966	128	9	high	high	ADJ
eurjchem-966	128	10	separation	separation	NOUN
eurjchem-966	128	11	and	and	CCONJ
eurjchem-966	128	12	giving	give	VERB
eurjchem-966	128	13	dense	dense	ADJ
eurjchem-966	128	14	and	and	CCONJ
eurjchem-966	128	15	compact	compact	ADJ
eurjchem-966	128	16	spots	spot	NOUN
eurjchem-966	128	17	with	with	ADP
eurjchem-966	128	18	appropriately	appropriately	ADV
eurjchem-966	128	19	and	and	CCONJ
eurjchem-966	128	20	significantly	significantly	ADV
eurjchem-966	128	21	different	different	ADJ
eurjchem-966	128	22	rf	rf	ADJ
eurjchem-966	128	23	values	value	NOUN
eurjchem-966	128	24	in	in	ADP
eurjchem-966	128	25	addition	addition	NOUN
eurjchem-966	128	26	to	to	ADP
eurjchem-966	128	27	high	high	ADJ
eurjchem-966	128	28	sensitivity	sensitivity	NOUN
eurjchem-966	128	29	[	[	X
eurjchem-966	128	30	19	19	NUM
eurjchem-966	128	31	]	]	PUNCT
eurjchem-966	128	32	.	.	PUNCT
eurjchem-966	129	1	accordingly	accordingly	ADV
eurjchem-966	129	2	,	,	PUNCT
eurjchem-966	129	3	hptlc	hptlc	NOUN
eurjchem-966	129	4	method	method	NOUN
eurjchem-966	129	5	was	be	AUX
eurjchem-966	129	6	successfully	successfully	ADV
eurjchem-966	129	7	applied	apply	VERB
eurjchem-966	129	8	for	for	ADP
eurjchem-966	129	9	separation	separation	NOUN
eurjchem-966	129	10	of	of	ADP
eurjchem-966	129	11	acm	acm	PROPN
eurjchem-966	129	12	and	and	CCONJ
eurjchem-966	129	13	deg	deg	NOUN
eurjchem-966	129	14	mixture	mixture	NOUN
eurjchem-966	129	15	and	and	CCONJ
eurjchem-966	129	16	for	for	ADP
eurjchem-966	129	17	quantification	quantification	NOUN
eurjchem-966	129	18	of	of	ADP
eurjchem-966	129	19	acm	acm	NOUN
eurjchem-966	129	20	in	in	ADP
eurjchem-966	129	21	presence	presence	NOUN
eurjchem-966	129	22	of	of	ADP
eurjchem-966	129	23	its	its	PRON
eurjchem-966	129	24	deg	deg	NOUN
eurjchem-966	129	25	in	in	ADP
eurjchem-966	129	26	pure	pure	ADJ
eurjchem-966	129	27	form	form	NOUN
eurjchem-966	129	28	and	and	CCONJ
eurjchem-966	129	29	in	in	ADP
eurjchem-966	129	30	pharmaceutical	pharmaceutical	ADJ
eurjchem-966	129	31	preparation	preparation	NOUN
eurjchem-966	129	32	.	.	PUNCT
eurjchem-966	130	1	in	in	ADP
eurjchem-966	130	2	order	order	NOUN
eurjchem-966	130	3	to	to	PART
eurjchem-966	130	4	optimize	optimize	VERB
eurjchem-966	130	5	the	the	DET
eurjchem-966	130	6	developed	develop	VERB
eurjchem-966	130	7	hptlc	hptlc	NOUN
eurjchem-966	130	8	method	method	NOUN
eurjchem-966	130	9	,	,	PUNCT
eurjchem-966	130	10	it	it	PRON
eurjchem-966	130	11	was	be	AUX
eurjchem-966	130	12	necessary	necessary	ADJ
eurjchem-966	130	13	to	to	PART
eurjchem-966	130	14	investigate	investigate	VERB
eurjchem-966	130	15	the	the	DET
eurjchem-966	130	16	effect	effect	NOUN
eurjchem-966	130	17	of	of	ADP
eurjchem-966	130	18	different	different	ADJ
eurjchem-966	130	19	factors	factor	NOUN
eurjchem-966	130	20	to	to	PART
eurjchem-966	130	21	get	get	VERB
eurjchem-966	130	22	the	the	DET
eurjchem-966	130	23	desired	desire	VERB
eurjchem-966	130	24	chromatographic	chromatographic	ADJ
eurjchem-966	130	25	resolution	resolution	NOUN
eurjchem-966	130	26	.	.	PUNCT
eurjchem-966	131	1	3.2.1	3.2.1	NUM
eurjchem-966	131	2	.	.	X
eurjchem-966	131	3	developing	develop	VERB
eurjchem-966	131	4	system	system	NOUN
eurjchem-966	131	5	and	and	CCONJ
eurjchem-966	131	6	efficiency	efficiency	NOUN
eurjchem-966	131	7	different	different	ADJ
eurjchem-966	131	8	developing	develop	VERB
eurjchem-966	131	9	systems	system	NOUN
eurjchem-966	131	10	of	of	ADP
eurjchem-966	131	11	different	different	ADJ
eurjchem-966	131	12	composition	composition	NOUN
eurjchem-966	131	13	and	and	CCONJ
eurjchem-966	131	14	ratios	ratio	NOUN
eurjchem-966	131	15	were	be	AUX
eurjchem-966	131	16	tried	try	VERB
eurjchem-966	131	17	such	such	ADJ
eurjchem-966	131	18	as	as	ADP
eurjchem-966	131	19	chloroform	chloroform	NOUN
eurjchem-966	131	20	:	:	PUNCT
eurjchem-966	131	21	methanol	methanol	NOUN
eurjchem-966	131	22	(	(	PUNCT
eurjchem-966	131	23	9:1	9:1	NUM
eurjchem-966	131	24	,	,	PUNCT
eurjchem-966	131	25	v	v	NOUN
eurjchem-966	131	26	:	:	PUNCT
eurjchem-966	131	27	v	v	NOUN
eurjchem-966	131	28	)	)	PUNCT
eurjchem-966	131	29	,	,	PUNCT
eurjchem-966	131	30	chloroform	chloroform	NOUN
eurjchem-966	131	31	:	:	PUNCT
eurjchem-966	131	32	methanol	methanol	NOUN
eurjchem-966	131	33	:	:	PUNCT
eurjchem-966	131	34	ammonia	ammonia	NOUN
eurjchem-966	131	35	solution	solution	NOUN
eurjchem-966	131	36	(	(	PUNCT
eurjchem-966	131	37	9:1:0.1	9:1:0.1	NOUN
eurjchem-966	131	38	,	,	PUNCT
eurjchem-966	131	39	v	v	NOUN
eurjchem-966	131	40	:	:	PUNCT
eurjchem-966	131	41	v	v	ADJ
eurjchem-966	131	42	:	:	PUNCT
eurjchem-966	131	43	v	v	NOUN
eurjchem-966	131	44	)	)	PUNCT
eurjchem-966	131	45	,	,	PUNCT
eurjchem-966	131	46	chloroform	chloroform	NOUN
eurjchem-966	131	47	:	:	PUNCT
eurjchem-966	131	48	methanol	methanol	NOUN
eurjchem-966	131	49	:	:	PUNCT
eurjchem-966	131	50	glacial	glacial	ADJ
eurjchem-966	131	51	acetic	acetic	ADJ
eurjchem-966	131	52	acid	acid	NOUN
eurjchem-966	131	53	(	(	PUNCT
eurjchem-966	131	54	9:1:0.1	9:1:0.1	NOUN
eurjchem-966	131	55	,	,	PUNCT
eurjchem-966	131	56	v	v	NOUN
eurjchem-966	131	57	:	:	PUNCT
eurjchem-966	131	58	v	v	ADJ
eurjchem-966	131	59	:	:	PUNCT
eurjchem-966	131	60	v	v	NOUN
eurjchem-966	131	61	)	)	PUNCT
eurjchem-966	131	62	,	,	PUNCT
eurjchem-966	131	63	and	and	CCONJ
eurjchem-966	131	64	hexane	hexane	NOUN
eurjchem-966	131	65	:	:	PUNCT
eurjchem-966	131	66	ethyl	ethyl	PROPN
eurjchem-966	131	67	acetate	acetate	NOUN
eurjchem-966	131	68	:	:	PUNCT
eurjchem-966	131	69	glacial	glacial	ADJ
eurjchem-966	131	70	acetic	acetic	ADJ
eurjchem-966	131	71	acid	acid	NOUN
eurjchem-966	131	72	(	(	PUNCT
eurjchem-966	131	73	6:4:0.3	6:4:0.3	PROPN
eurjchem-966	131	74	,	,	PUNCT
eurjchem-966	131	75	v	v	NOUN
eurjchem-966	131	76	:	:	PUNCT
eurjchem-966	131	77	v	v	ADJ
eurjchem-966	131	78	:	:	PUNCT
eurjchem-966	131	79	v	v	NOUN
eurjchem-966	131	80	)	)	PUNCT
eurjchem-966	131	81	to	to	PART
eurjchem-966	131	82	obtain	obtain	VERB
eurjchem-966	131	83	optimum	optimum	ADJ
eurjchem-966	131	84	separation	separation	NOUN
eurjchem-966	131	85	between	between	ADP
eurjchem-966	131	86	acm	acm	PROPN
eurjchem-966	131	87	and	and	CCONJ
eurjchem-966	131	88	its	its	PRON
eurjchem-966	131	89	degradation	degradation	NOUN
eurjchem-966	131	90	product	product	NOUN
eurjchem-966	131	91	(	(	PUNCT
eurjchem-966	131	92	deg	deg	PROPN
eurjchem-966	131	93	)	)	PUNCT
eurjchem-966	131	94	.	.	PUNCT
eurjchem-966	132	1	the	the	DET
eurjchem-966	132	2	best	good	ADJ
eurjchem-966	132	3	developing	develop	VERB
eurjchem-966	132	4	system	system	NOUN
eurjchem-966	132	5	was	be	AUX
eurjchem-966	132	6	found	find	VERB
eurjchem-966	132	7	to	to	PART
eurjchem-966	132	8	be	be	AUX
eurjchem-966	132	9	hexane	hexane	NOUN
eurjchem-966	132	10	:	:	PUNCT
eurjchem-966	132	11	ethyl	ethyl	PROPN
eurjchem-966	132	12	acetate	acetate	NOUN
eurjchem-966	132	13	:	:	PUNCT
eurjchem-966	132	14	glacial	glacial	ADJ
eurjchem-966	132	15	acetic	acetic	ADJ
eurjchem-966	132	16	acid	acid	NOUN
eurjchem-966	132	17	(	(	PUNCT
eurjchem-966	132	18	6:4:0.3	6:4:0.3	PROPN
eurjchem-966	132	19	,	,	PUNCT
eurjchem-966	132	20	v	v	NOUN
eurjchem-966	132	21	:	:	PUNCT
eurjchem-966	132	22	v	v	ADJ
eurjchem-966	132	23	:	:	PUNCT
eurjchem-966	132	24	v	v	NOUN
eurjchem-966	132	25	)	)	PUNCT
eurjchem-966	132	26	.	.	PUNCT
eurjchem-966	133	1	this	this	DET
eurjchem-966	133	2	selected	select	VERB
eurjchem-966	133	3	developing	develop	VERB
eurjchem-966	133	4	system	system	NOUN
eurjchem-966	133	5	allowed	allow	VERB
eurjchem-966	133	6	good	good	ADJ
eurjchem-966	133	7	separation	separation	NOUN
eurjchem-966	133	8	between	between	ADP
eurjchem-966	133	9	acm	acm	PROPN
eurjchem-966	133	10	and	and	CCONJ
eurjchem-966	133	11	its	its	PRON
eurjchem-966	133	12	degradation	degradation	NOUN
eurjchem-966	133	13	product	product	NOUN
eurjchem-966	133	14	with	with	ADP
eurjchem-966	133	15	satisfactory	satisfactory	ADJ
eurjchem-966	133	16	rf	rf	ADJ
eurjchem-966	133	17	values	value	NOUN
eurjchem-966	133	18	without	without	ADP
eurjchem-966	133	19	tailing	tail	VERB
eurjchem-966	133	20	of	of	ADP
eurjchem-966	133	21	the	the	DET
eurjchem-966	133	22	separated	separate	VERB
eurjchem-966	133	23	bands	band	NOUN
eurjchem-966	133	24	,	,	PUNCT
eurjchem-966	133	25	as	as	SCONJ
eurjchem-966	133	26	shown	show	VERB
eurjchem-966	133	27	in	in	ADP
eurjchem-966	133	28	figure	figure	NOUN
eurjchem-966	133	29	9	9	NUM
eurjchem-966	133	30	.	.	PUNCT
eurjchem-966	134	1	it	it	PRON
eurjchem-966	134	2	was	be	AUX
eurjchem-966	134	3	found	find	VERB
eurjchem-966	134	4	that	that	DET
eurjchem-966	134	5	presence	presence	NOUN
eurjchem-966	134	6	of	of	ADP
eurjchem-966	134	7	glacial	glacial	ADJ
eurjchem-966	134	8	acetic	acetic	ADJ
eurjchem-966	134	9	acid	acid	NOUN
eurjchem-966	134	10	with	with	ADP
eurjchem-966	134	11	this	this	DET
eurjchem-966	134	12	ratio	ratio	NOUN
eurjchem-966	134	13	in	in	ADP
eurjchem-966	134	14	the	the	DET
eurjchem-966	134	15	developing	develop	VERB
eurjchem-966	134	16	system	system	NOUN
eurjchem-966	134	17	is	be	AUX
eurjchem-966	134	18	essential	essential	ADJ
eurjchem-966	134	19	for	for	ADP
eurjchem-966	134	20	separation	separation	NOUN
eurjchem-966	134	21	.	.	PUNCT
eurjchem-966	135	1	figure	figure	NOUN
eurjchem-966	135	2	9	9	NUM
eurjchem-966	135	3	.	.	PUNCT
eurjchem-966	135	4	2d	2d	NUM
eurjchem-966	135	5	hptlc	hptlc	NOUN
eurjchem-966	135	6	densitogram	densitogram	NOUN
eurjchem-966	135	7	of	of	ADP
eurjchem-966	135	8	resolved	resolve	VERB
eurjchem-966	135	9	mixtures	mixture	NOUN
eurjchem-966	135	10	of	of	ADP
eurjchem-966	135	11	acm	acm	NOUN
eurjchem-966	135	12	(	(	PUNCT
eurjchem-966	135	13	rf	rf	NOUN
eurjchem-966	135	14	=	=	NOUN
eurjchem-966	135	15	0.21	0.21	NUM
eurjchem-966	135	16	)	)	PUNCT
eurjchem-966	135	17	and	and	CCONJ
eurjchem-966	135	18	deg	deg	PROPN
eurjchem-966	135	19	(	(	PUNCT
eurjchem-966	135	20	rf	rf	NOUN
eurjchem-966	135	21	=	=	NOUN
eurjchem-966	135	22	0.51	0.51	NUM
eurjchem-966	135	23	)	)	PUNCT
eurjchem-966	135	24	using	use	VERB
eurjchem-966	135	25	(	(	PUNCT
eurjchem-966	135	26	hexane	hexane	NOUN
eurjchem-966	135	27	:	:	PUNCT
eurjchem-966	135	28	ethyl	ethyl	PROPN
eurjchem-966	135	29	acetate	acetate	NOUN
eurjchem-966	135	30	:	:	PUNCT
eurjchem-966	135	31	glacial	glacial	ADJ
eurjchem-966	135	32	acetic	acetic	ADJ
eurjchem-966	135	33	acid	acid	NOUN
eurjchem-966	135	34	)	)	PUNCT
eurjchem-966	136	1	(	(	PUNCT
eurjchem-966	136	2	6:4:0.3	6:4:0.3	NOUN
eurjchem-966	136	3	,	,	PUNCT
eurjchem-966	136	4	v	v	NOUN
eurjchem-966	136	5	:	:	PUNCT
eurjchem-966	136	6	v	v	ADJ
eurjchem-966	136	7	:	:	PUNCT
eurjchem-966	136	8	v	v	NOUN
eurjchem-966	136	9	)	)	PUNCT
eurjchem-966	136	10	as	as	ADP
eurjchem-966	136	11	a	a	DET
eurjchem-966	136	12	developing	develop	VERB
eurjchem-966	136	13	system	system	NOUN
eurjchem-966	136	14	at	at	ADP
eurjchem-966	136	15	254	254	NUM
eurjchem-966	136	16	nm	nm	NOUN
eurjchem-966	136	17	.	.	PUNCT
eurjchem-966	137	1	3.2.2	3.2.2	NUM
eurjchem-966	137	2	.	.	PUNCT
eurjchem-966	138	1	scanning	scan	VERB
eurjchem-966	138	2	wavelength	wavelength	NOUN
eurjchem-966	138	3	different	different	ADJ
eurjchem-966	138	4	scanning	scanning	NOUN
eurjchem-966	138	5	wavelengths	wavelength	NOUN
eurjchem-966	138	6	were	be	AUX
eurjchem-966	138	7	tried	try	VERB
eurjchem-966	138	8	(	(	PUNCT
eurjchem-966	138	9	254	254	NUM
eurjchem-966	138	10	,	,	PUNCT
eurjchem-966	138	11	265	265	NUM
eurjchem-966	138	12	and	and	CCONJ
eurjchem-966	138	13	318	318	NUM
eurjchem-966	138	14	nm	nm	NOUN
eurjchem-966	138	15	)	)	PUNCT
eurjchem-966	138	16	in	in	ADP
eurjchem-966	138	17	order	order	NOUN
eurjchem-966	138	18	to	to	PART
eurjchem-966	138	19	obtain	obtain	VERB
eurjchem-966	138	20	good	good	ADJ
eurjchem-966	138	21	sensitivity	sensitivity	NOUN
eurjchem-966	138	22	of	of	ADP
eurjchem-966	138	23	acm	acm	NOUN
eurjchem-966	138	24	with	with	ADP
eurjchem-966	138	25	minimum	minimum	NOUN
eurjchem-966	138	26	noise	noise	NOUN
eurjchem-966	138	27	.	.	PUNCT
eurjchem-966	139	1	the	the	DET
eurjchem-966	139	2	wavelength	wavelength	NOUN
eurjchem-966	139	3	254	254	NUM
eurjchem-966	139	4	nm	nm	NOUN
eurjchem-966	139	5	was	be	AUX
eurjchem-966	139	6	found	find	VERB
eurjchem-966	139	7	to	to	PART
eurjchem-966	139	8	be	be	AUX
eurjchem-966	139	9	the	the	DET
eurjchem-966	139	10	best	good	ADJ
eurjchem-966	139	11	wavelength	wavelength	NOUN
eurjchem-966	139	12	regarding	regard	VERB
eurjchem-966	139	13	sensitivity	sensitivity	NOUN
eurjchem-966	139	14	of	of	ADP
eurjchem-966	139	15	acm	acm	PROPN
eurjchem-966	139	16	.	.	PUNCT
eurjchem-966	140	1	peaks	peak	NOUN
eurjchem-966	140	2	were	be	AUX
eurjchem-966	140	3	sharp	sharp	ADJ
eurjchem-966	140	4	and	and	CCONJ
eurjchem-966	140	5	symmetrical	symmetrical	ADJ
eurjchem-966	140	6	with	with	ADP
eurjchem-966	140	7	minimum	minimum	ADJ
eurjchem-966	140	8	noise	noise	NOUN
eurjchem-966	140	9	,	,	PUNCT
eurjchem-966	140	10	as	as	SCONJ
eurjchem-966	140	11	shown	show	VERB
eurjchem-966	140	12	in	in	ADP
eurjchem-966	140	13	figure	figure	NOUN
eurjchem-966	140	14	10	10	NUM
eurjchem-966	140	15	.	.	PUNCT
eurjchem-966	141	1	figure	figure	NOUN
eurjchem-966	141	2	10	10	NUM
eurjchem-966	141	3	.	.	PUNCT
eurjchem-966	142	1	hptlc	hptlc	NOUN
eurjchem-966	142	2	densitogram	densitogram	PROPN
eurjchem-966	142	3	of	of	ADP
eurjchem-966	142	4	acm	acm	NOUN
eurjchem-966	142	5	in	in	ADP
eurjchem-966	142	6	the	the	DET
eurjchem-966	142	7	concentration	concentration	NOUN
eurjchem-966	142	8	range	range	NOUN
eurjchem-966	142	9	(	(	PUNCT
eurjchem-966	142	10	0.4‐1.4	0.4‐1.4	NOUN
eurjchem-966	142	11	µg	µg	ADJ
eurjchem-966	142	12	/	/	SYM
eurjchem-966	142	13	band	band	NOUN
eurjchem-966	142	14	)	)	PUNCT
eurjchem-966	142	15	using	use	VERB
eurjchem-966	142	16	(	(	PUNCT
eurjchem-966	142	17	hexane	hexane	NOUN
eurjchem-966	142	18	:	:	PUNCT
eurjchem-966	142	19	ethyl	ethyl	PROPN
eurjchem-966	142	20	acetate	acetate	NOUN
eurjchem-966	142	21	:	:	PUNCT
eurjchem-966	142	22	glacial	glacial	ADJ
eurjchem-966	142	23	acetic	acetic	ADJ
eurjchem-966	142	24	acid	acid	NOUN
eurjchem-966	142	25	)	)	PUNCT
eurjchem-966	142	26	solution	solution	NOUN
eurjchem-966	142	27	(	(	PUNCT
eurjchem-966	142	28	6:4:0.3	6:4:0.3	NOUN
eurjchem-966	142	29	,	,	PUNCT
eurjchem-966	142	30	v	v	NOUN
eurjchem-966	142	31	:	:	PUNCT
eurjchem-966	142	32	v	v	ADJ
eurjchem-966	142	33	:	:	PUNCT
eurjchem-966	142	34	v	v	NOUN
eurjchem-966	142	35	)	)	PUNCT
eurjchem-966	142	36	as	as	ADP
eurjchem-966	142	37	a	a	DET
eurjchem-966	142	38	developing	develop	VERB
eurjchem-966	142	39	system	system	NOUN
eurjchem-966	142	40	at	at	ADP
eurjchem-966	142	41	254	254	NUM
eurjchem-966	142	42	nm	nm	NOUN
eurjchem-966	142	43	.	.	PUNCT
eurjchem-966	143	1	3.2.3	3.2.3	X
eurjchem-966	143	2	.	.	PUNCT
eurjchem-966	143	3	band	band	NOUN
eurjchem-966	143	4	dimensions	dimension	NOUN
eurjchem-966	143	5	the	the	DET
eurjchem-966	143	6	slight	slight	ADJ
eurjchem-966	143	7	spread	spread	NOUN
eurjchem-966	143	8	of	of	ADP
eurjchem-966	143	9	the	the	DET
eurjchem-966	143	10	developed	develop	VERB
eurjchem-966	143	11	bands	band	NOUN
eurjchem-966	143	12	due	due	ADP
eurjchem-966	143	13	to	to	ADP
eurjchem-966	143	14	ordinary	ordinary	ADJ
eurjchem-966	143	15	diffusion	diffusion	NOUN
eurjchem-966	143	16	should	should	AUX
eurjchem-966	143	17	be	be	AUX
eurjchem-966	143	18	taken	take	VERB
eurjchem-966	143	19	into	into	ADP
eurjchem-966	143	20	consideration	consideration	NOUN
eurjchem-966	143	21	,	,	PUNCT
eurjchem-966	143	22	so	so	CCONJ
eurjchem-966	143	23	the	the	DET
eurjchem-966	143	24	band	band	NOUN
eurjchem-966	143	25	width	width	NOUN
eurjchem-966	143	26	and	and	CCONJ
eurjchem-966	143	27	interspaces	interspace	NOUN
eurjchem-966	143	28	between	between	ADP
eurjchem-966	143	29	bands	band	NOUN
eurjchem-966	143	30	should	should	AUX
eurjchem-966	143	31	be	be	AUX
eurjchem-966	143	32	chosen	choose	VERB
eurjchem-966	143	33	carefully	carefully	ADV
eurjchem-966	143	34	to	to	PART
eurjchem-966	143	35	avoid	avoid	VERB
eurjchem-966	143	36	spread	spread	NOUN
eurjchem-966	143	37	of	of	ADP
eurjchem-966	143	38	bands	band	NOUN
eurjchem-966	143	39	outside	outside	ADP
eurjchem-966	143	40	the	the	DET
eurjchem-966	143	41	scanning	scanning	NOUN
eurjchem-966	143	42	tracks	track	NOUN
eurjchem-966	143	43	and	and	CCONJ
eurjchem-966	143	44	interference	interference	VERB
eurjchem-966	143	45	between	between	ADP
eurjchem-966	143	46	adjacent	adjacent	ADJ
eurjchem-966	143	47	bands	band	NOUN
eurjchem-966	143	48	.	.	PUNCT
eurjchem-966	144	1	different	different	ADJ
eurjchem-966	144	2	band	band	NOUN
eurjchem-966	144	3	dimensions	dimension	NOUN
eurjchem-966	144	4	were	be	AUX
eurjchem-966	144	5	tried	try	VERB
eurjchem-966	144	6	to	to	PART
eurjchem-966	144	7	obtain	obtain	VERB
eurjchem-966	144	8	sharp	sharp	ADJ
eurjchem-966	144	9	and	and	CCONJ
eurjchem-966	144	10	symmetrical	symmetrical	ADJ
eurjchem-966	144	11	peaks	peak	NOUN
eurjchem-966	144	12	.	.	PUNCT
eurjchem-966	145	1	the	the	DET
eurjchem-966	145	2	optimum	optimum	ADJ
eurjchem-966	145	3	bandwidth	bandwidth	NOUN
eurjchem-966	145	4	chosen	choose	VERB
eurjchem-966	145	5	was	be	AUX
eurjchem-966	145	6	6	6	NUM
eurjchem-966	145	7	mm	mm	NOUN
eurjchem-966	145	8	and	and	CCONJ
eurjchem-966	145	9	the	the	DET
eurjchem-966	145	10	inter‐space	inter‐space	NOUN
eurjchem-966	145	11	between	between	ADP
eurjchem-966	145	12	bands	band	NOUN
eurjchem-966	145	13	was	be	AUX
eurjchem-966	145	14	5	5	NUM
eurjchem-966	145	15	mm	mm	NOUN
eurjchem-966	145	16	.	.	PUNCT
eurjchem-966	146	1	3.2.4	3.2.4	NUM
eurjchem-966	146	2	.	.	PUNCT
eurjchem-966	147	1	slit	slit	ADJ
eurjchem-966	147	2	dimensions	dimension	NOUN
eurjchem-966	147	3	of	of	ADP
eurjchem-966	147	4	scanning	scan	VERB
eurjchem-966	147	5	light	light	NOUN
eurjchem-966	147	6	beam	beam	NOUN
eurjchem-966	147	7	the	the	DET
eurjchem-966	147	8	slit	slit	NOUN
eurjchem-966	147	9	dimensions	dimension	NOUN
eurjchem-966	147	10	of	of	ADP
eurjchem-966	147	11	the	the	DET
eurjchem-966	147	12	scanning	scan	VERB
eurjchem-966	147	13	light	light	ADJ
eurjchem-966	147	14	beam	beam	NOUN
eurjchem-966	147	15	should	should	AUX
eurjchem-966	147	16	ensure	ensure	VERB
eurjchem-966	147	17	complete	complete	ADJ
eurjchem-966	147	18	coverage	coverage	NOUN
eurjchem-966	147	19	of	of	ADP
eurjchem-966	147	20	band	band	NOUN
eurjchem-966	147	21	dimensions	dimension	NOUN
eurjchem-966	147	22	on	on	ADP
eurjchem-966	147	23	the	the	DET
eurjchem-966	147	24	scanned	scan	VERB
eurjchem-966	147	25	track	track	NOUN
eurjchem-966	147	26	without	without	ADP
eurjchem-966	147	27	interference	interference	NOUN
eurjchem-966	147	28	of	of	ADP
eurjchem-966	147	29	adjacent	adjacent	ADJ
eurjchem-966	147	30	bands	band	NOUN
eurjchem-966	147	31	.	.	PUNCT
eurjchem-966	148	1	different	different	ADJ
eurjchem-966	148	2	slit	slit	NOUN
eurjchem-966	148	3	dimensions	dimension	NOUN
eurjchem-966	148	4	were	be	AUX
eurjchem-966	148	5	tried	try	VERB
eurjchem-966	148	6	where	where	SCONJ
eurjchem-966	148	7	6	6	NUM
eurjchem-966	148	8	mm	mm	NOUN
eurjchem-966	148	9	×	×	NOUN
eurjchem-966	148	10	0.3	0.3	NUM
eurjchem-966	148	11	mm	mm	NOUN
eurjchem-966	148	12	proved	prove	VERB
eurjchem-966	148	13	to	to	PART
eurjchem-966	148	14	be	be	AUX
eurjchem-966	148	15	the	the	DET
eurjchem-966	148	16	slit	slit	ADJ
eurjchem-966	148	17	dimensions	dimension	NOUN
eurjchem-966	148	18	of	of	ADP
eurjchem-966	148	19	choice	choice	NOUN
eurjchem-966	148	20	which	which	PRON
eurjchem-966	148	21	provided	provide	VERB
eurjchem-966	148	22	highest	high	ADJ
eurjchem-966	148	23	sensitivity	sensitivity	NOUN
eurjchem-966	148	24	.	.	PUNCT
eurjchem-966	149	1	this	this	DET
eurjchem-966	149	2	method	method	NOUN
eurjchem-966	149	3	offers	offer	VERB
eurjchem-966	149	4	high	high	ADJ
eurjchem-966	149	5	sensitivity	sensitivity	NOUN
eurjchem-966	149	6	and	and	CCONJ
eurjchem-966	149	7	selectivity	selectivity	NOUN
eurjchem-966	149	8	for	for	ADP
eurjchem-966	149	9	analysis	analysis	NOUN
eurjchem-966	149	10	of	of	ADP
eurjchem-966	149	11	acm	acm	NOUN
eurjchem-966	149	12	in	in	ADP
eurjchem-966	149	13	presence	presence	NOUN
eurjchem-966	149	14	of	of	ADP
eurjchem-966	149	15	deg	deg	NOUN
eurjchem-966	149	16	using	use	VERB
eurjchem-966	149	17	hexane	hexane	NOUN
eurjchem-966	149	18	:	:	PUNCT
eurjchem-966	149	19	ethyl	ethyl	PROPN
eurjchem-966	149	20	acetate	acetate	PROPN
eurjchem-966	149	21	:	:	PUNCT
eurjchem-966	149	22	glacial	glacial	ADJ
eurjchem-966	149	23	acetic	acetic	ADJ
eurjchem-966	149	24	acid	acid	NOUN
eurjchem-966	149	25	(	(	PUNCT
eurjchem-966	149	26	6:4:0.3	6:4:0.3	PROPN
eurjchem-966	149	27	,	,	PUNCT
eurjchem-966	149	28	v	v	NOUN
eurjchem-966	149	29	:	:	PUNCT
eurjchem-966	149	30	v	v	ADJ
eurjchem-966	149	31	:	:	PUNCT
eurjchem-966	149	32	v	v	NOUN
eurjchem-966	149	33	)	)	PUNCT
eurjchem-966	149	34	as	as	ADP
eurjchem-966	149	35	a	a	DET
eurjchem-966	149	36	developing	develop	VERB
eurjchem-966	149	37	system	system	NOUN
eurjchem-966	149	38	,	,	PUNCT
eurjchem-966	149	39	where	where	SCONJ
eurjchem-966	149	40	good	good	ADJ
eurjchem-966	149	41	separation	separation	NOUN
eurjchem-966	149	42	was	be	AUX
eurjchem-966	149	43	obtained	obtain	VERB
eurjchem-966	149	44	by	by	ADP
eurjchem-966	149	45	the	the	DET
eurjchem-966	149	46	difference	difference	NOUN
eurjchem-966	149	47	in	in	ADP
eurjchem-966	149	48	the	the	DET
eurjchem-966	149	49	retention	retention	NOUN
eurjchem-966	149	50	factor	factor	NOUN
eurjchem-966	149	51	(	(	PUNCT
eurjchem-966	149	52	rf	rf	NOUN
eurjchem-966	149	53	)	)	PUNCT
eurjchem-966	149	54	values	value	NOUN
eurjchem-966	149	55	of	of	ADP
eurjchem-966	149	56	acm	acm	NOUN
eurjchem-966	149	57	(	(	PUNCT
eurjchem-966	149	58	rf	rf	NOUN
eurjchem-966	149	59	=	=	NOUN
eurjchem-966	149	60	0.21	0.21	NUM
eurjchem-966	149	61	)	)	PUNCT
eurjchem-966	149	62	and	and	CCONJ
eurjchem-966	149	63	deg	deg	PROPN
eurjchem-966	149	64	(	(	PUNCT
eurjchem-966	149	65	rf	rf	NOUN
eurjchem-966	149	66	=	=	NOUN
eurjchem-966	149	67	0.51	0.51	NUM
eurjchem-966	149	68	)	)	PUNCT
eurjchem-966	149	69	as	as	SCONJ
eurjchem-966	149	70	shown	show	VERB
eurjchem-966	149	71	in	in	ADP
eurjchem-966	149	72	figure	figure	NOUN
eurjchem-966	149	73	9	9	NUM
eurjchem-966	149	74	.	.	PUNCT
eurjchem-966	150	1	the	the	DET
eurjchem-966	150	2	calibration	calibration	NOUN
eurjchem-966	150	3	curve	curve	NOUN
eurjchem-966	150	4	for	for	ADP
eurjchem-966	150	5	acm	acm	PROPN
eurjchem-966	150	6	was	be	AUX
eurjchem-966	150	7	constructed	construct	VERB
eurjchem-966	150	8	by	by	ADP
eurjchem-966	150	9	plotting	plot	VERB
eurjchem-966	150	10	the	the	DET
eurjchem-966	150	11	integrated	integrate	VERB
eurjchem-966	150	12	peak	peak	NOUN
eurjchem-966	150	13	area/103	area/103	VERB
eurjchem-966	150	14	versus	versus	ADP
eurjchem-966	150	15	the	the	DET
eurjchem-966	150	16	corresponding	corresponding	ADJ
eurjchem-966	150	17	concentrations	concentration	NOUN
eurjchem-966	150	18	of	of	ADP
eurjchem-966	150	19	acm	acm	NOUN
eurjchem-966	150	20	in	in	ADP
eurjchem-966	150	21	the	the	DET
eurjchem-966	150	22	range	range	NOUN
eurjchem-966	150	23	of	of	ADP
eurjchem-966	150	24	0.4‐1.4	0.4‐1.4	NUM
eurjchem-966	150	25	μg	μg	PROPN
eurjchem-966	150	26	/	/	SYM
eurjchem-966	150	27	band	band	NOUN
eurjchem-966	150	28	with	with	ADP
eurjchem-966	150	29	mean	mean	ADJ
eurjchem-966	150	30	percentage	percentage	NOUN
eurjchem-966	150	31	recovery	recovery	NOUN
eurjchem-966	150	32	100.00±0.709	100.00±0.709	NOUN
eurjchem-966	150	33	.	.	PUNCT
eurjchem-966	151	1	the	the	DET
eurjchem-966	151	2	concentration	concentration	NOUN
eurjchem-966	151	3	of	of	ADP
eurjchem-966	151	4	acm	acm	PROPN
eurjchem-966	151	5	was	be	AUX
eurjchem-966	151	6	calculated	calculate	VERB
eurjchem-966	151	7	from	from	ADP
eurjchem-966	151	8	the	the	DET
eurjchem-966	151	9	following	follow	VERB
eurjchem-966	151	10	regression	regression	NOUN
eurjchem-966	151	11	equation	equation	NOUN
eurjchem-966	151	12	:	:	PUNCT
eurjchem-966	151	13	a	a	DET
eurjchem-966	151	14	=	=	SYM
eurjchem-966	151	15	0.1944	0.1944	NUM
eurjchem-966	151	16	c	c	NOUN
eurjchem-966	151	17	+	+	NOUN
eurjchem-966	151	18	0.0671	0.0671	NUM
eurjchem-966	151	19	,	,	PUNCT
eurjchem-966	151	20	r	r	NOUN
eurjchem-966	151	21	=	=	SYM
eurjchem-966	151	22	0.9999	0.9999	NUM
eurjchem-966	151	23	(	(	PUNCT
eurjchem-966	151	24	3	3	NUM
eurjchem-966	151	25	)	)	PUNCT
eurjchem-966	151	26	where	where	SCONJ
eurjchem-966	151	27	a	a	PRON
eurjchem-966	151	28	is	be	AUX
eurjchem-966	151	29	integrated	integrate	VERB
eurjchem-966	151	30	peak	peak	NOUN
eurjchem-966	151	31	areas/103	areas/103	NOUN
eurjchem-966	151	32	,	,	PUNCT
eurjchem-966	151	33	c	c	PROPN
eurjchem-966	151	34	is	be	AUX
eurjchem-966	151	35	the	the	DET
eurjchem-966	151	36	concentration	concentration	NOUN
eurjchem-966	151	37	in	in	ADP
eurjchem-966	151	38	µg	µg	ADJ
eurjchem-966	151	39	/	/	SYM
eurjchem-966	151	40	band	band	NOUN
eurjchem-966	151	41	and	and	CCONJ
eurjchem-966	151	42	r	r	NOUN
eurjchem-966	151	43	is	be	AUX
eurjchem-966	151	44	the	the	DET
eurjchem-966	151	45	correlation	correlation	NOUN
eurjchem-966	151	46	coefficient	coefficient	NOUN
eurjchem-966	151	47	.	.	PUNCT
eurjchem-966	152	1	3.3	3.3	NUM
eurjchem-966	152	2	.	.	PUNCT
eurjchem-966	152	3	stability‐indication	stability‐indication	NOUN
eurjchem-966	152	4	to	to	PART
eurjchem-966	152	5	assess	assess	VERB
eurjchem-966	152	6	the	the	DET
eurjchem-966	152	7	stability‐indicating	stability‐indicate	VERB
eurjchem-966	152	8	efficiency	efficiency	NOUN
eurjchem-966	152	9	of	of	ADP
eurjchem-966	152	10	the	the	DET
eurjchem-966	152	11	proposed	propose	VERB
eurjchem-966	152	12	methods	method	NOUN
eurjchem-966	152	13	,	,	PUNCT
eurjchem-966	152	14	they	they	PRON
eurjchem-966	152	15	were	be	AUX
eurjchem-966	152	16	applied	apply	VERB
eurjchem-966	152	17	to	to	ADP
eurjchem-966	152	18	laboratory	laboratory	NOUN
eurjchem-966	152	19	prepared	prepare	VERB
eurjchem-966	152	20	mixtures	mixture	NOUN
eurjchem-966	152	21	containing	contain	VERB
eurjchem-966	152	22	different	different	ADJ
eurjchem-966	152	23	ratios	ratio	NOUN
eurjchem-966	152	24	of	of	ADP
eurjchem-966	152	25	acm	acm	PROPN
eurjchem-966	152	26	and	and	CCONJ
eurjchem-966	152	27	deg	deg	NOUN
eurjchem-966	152	28	.	.	PUNCT
eurjchem-966	153	1	224	224	NUM
eurjchem-966	153	2	naguib	naguib	NOUN
eurjchem-966	153	3	et	et	PROPN
eurjchem-966	153	4	al	al	PROPN
eurjchem-966	153	5	.	.	PUNCT
eurjchem-966	153	6	/	/	SYM
eurjchem-966	153	7	european	european	PROPN
eurjchem-966	153	8	journal	journal	PROPN
eurjchem-966	153	9	of	of	ADP
eurjchem-966	153	10	chemistry	chemistry	NOUN
eurjchem-966	153	11	5	5	NUM
eurjchem-966	153	12	(	(	PUNCT
eurjchem-966	153	13	2	2	NUM
eurjchem-966	153	14	)	)	PUNCT
eurjchem-966	153	15	(	(	PUNCT
eurjchem-966	153	16	2014	2014	NUM
eurjchem-966	153	17	)	)	PUNCT
eurjchem-966	153	18	219‐226	219‐226	NUM
eurjchem-966	153	19	table	table	NOUN
eurjchem-966	153	20	1	1	NUM
eurjchem-966	153	21	.	.	PUNCT
eurjchem-966	153	22	assay	assay	VERB
eurjchem-966	153	23	results	result	NOUN
eurjchem-966	153	24	for	for	ADP
eurjchem-966	153	25	the	the	DET
eurjchem-966	153	26	determination	determination	NOUN
eurjchem-966	153	27	of	of	ADP
eurjchem-966	153	28	acm	acm	NOUN
eurjchem-966	153	29	in	in	ADP
eurjchem-966	153	30	synthetic	synthetic	ADJ
eurjchem-966	153	31	mixtures	mixture	NOUN
eurjchem-966	153	32	with	with	ADP
eurjchem-966	153	33	deg	deg	PROPN
eurjchem-966	153	34	.	.	PUNCT
eurjchem-966	154	1	deg	deg	PROPN
eurjchem-966	154	2	%	%	NOUN
eurjchem-966	154	3	%	%	NOUN
eurjchem-966	154	4	recovery	recovery	NOUN
eurjchem-966	154	5	%	%	NOUN
eurjchem-966	154	6	recovery	recovery	NOUN
eurjchem-966	154	7	1dd	1dd	ADJ
eurjchem-966	154	8	spectrophotometric	spectrophotometric	ADJ
eurjchem-966	154	9	method	method	NOUN
eurjchem-966	154	10	mean	mean	VERB
eurjchem-966	154	11	centering	center	VERB
eurjchem-966	154	12	method	method	NOUN
eurjchem-966	154	13	10	10	NUM
eurjchem-966	154	14	%	%	NOUN
eurjchem-966	154	15	100	100	NUM
eurjchem-966	154	16	99.60	99.60	NUM
eurjchem-966	154	17	20	20	NUM
eurjchem-966	154	18	%	%	NOUN
eurjchem-966	154	19	101.9	101.9	NUM
eurjchem-966	154	20	101.60	101.60	NUM
eurjchem-966	154	21	30	30	NUM
eurjchem-966	154	22	%	%	NOUN
eurjchem-966	154	23	101.1	101.1	NUM
eurjchem-966	154	24	100.30	100.30	NUM
eurjchem-966	154	25	40	40	NUM
eurjchem-966	154	26	%	%	NOUN
eurjchem-966	154	27	98.85	98.85	NUM
eurjchem-966	154	28	99.17	99.17	NUM
eurjchem-966	154	29	50	50	NUM
eurjchem-966	154	30	%	%	NOUN
eurjchem-966	154	31	98.97	98.97	NUM
eurjchem-966	154	32	99.00	99.00	NUM
eurjchem-966	154	33	60	60	NUM
eurjchem-966	154	34	%	%	NOUN
eurjchem-966	154	35	101.9	101.9	NUM
eurjchem-966	154	36	102.50	102.50	NUM
eurjchem-966	154	37	70	70	NUM
eurjchem-966	154	38	%	%	NOUN
eurjchem-966	154	39	100.9	100.9	NUM
eurjchem-966	154	40	97.18	97.18	NUM
eurjchem-966	154	41	80	80	NUM
eurjchem-966	154	42	%	%	NOUN
eurjchem-966	154	43	97.44	97.44	NUM
eurjchem-966	154	44	98.31	98.31	NUM
eurjchem-966	154	45	90	90	NUM
eurjchem-966	154	46	%	%	NOUN
eurjchem-966	154	47	93.59	93.59	NUM
eurjchem-966	154	48	*	*	SYM
eurjchem-966	154	49	101.90	101.90	NUM
eurjchem-966	154	50	mean±sd	mean±sd	ADP
eurjchem-966	154	51	100.13±1.610	100.13±1.610	NUM
eurjchem-966	154	52	99.96±1.780	99.96±1.780	NUM
eurjchem-966	154	53	*	*	PUNCT
eurjchem-966	154	54	rejected	reject	VERB
eurjchem-966	154	55	value	value	NOUN
eurjchem-966	154	56	.	.	PUNCT
eurjchem-966	155	1	table	table	NOUN
eurjchem-966	155	2	2	2	NUM
eurjchem-966	155	3	.	.	PUNCT
eurjchem-966	155	4	determination	determination	NOUN
eurjchem-966	155	5	of	of	ADP
eurjchem-966	155	6	acm	acm	NOUN
eurjchem-966	155	7	in	in	ADP
eurjchem-966	155	8	pharmaceutical	pharmaceutical	ADJ
eurjchem-966	155	9	formulation	formulation	NOUN
eurjchem-966	155	10	by	by	ADP
eurjchem-966	155	11	the	the	DET
eurjchem-966	155	12	proposed	propose	VERB
eurjchem-966	155	13	methods	method	NOUN
eurjchem-966	155	14	and	and	CCONJ
eurjchem-966	155	15	application	application	NOUN
eurjchem-966	155	16	of	of	ADP
eurjchem-966	155	17	standard	standard	ADJ
eurjchem-966	155	18	addition	addition	NOUN
eurjchem-966	155	19	technique	technique	NOUN
eurjchem-966	155	20	.	.	PUNCT
eurjchem-966	156	1	pharmaceutical	pharmaceutical	ADJ
eurjchem-966	156	2	formulation	formulation	NOUN
eurjchem-966	156	3	ostmap	ostmap	NOUN
eurjchem-966	156	4	®	®	NOUN
eurjchem-966	156	5	capsules	capsule	NOUN
eurjchem-966	156	6	b.n	b.n	PROPN
eurjchem-966	156	7	:	:	PUNCT
eurjchem-966	156	8	3710911	3710911	NUM
eurjchem-966	156	9	taken	take	VERB
eurjchem-966	156	10	(	(	PUNCT
eurjchem-966	156	11	µg	µg	NOUN
eurjchem-966	156	12	/	/	SYM
eurjchem-966	156	13	ml	ml	NOUN
eurjchem-966	156	14	)	)	PUNCT
eurjchem-966	156	15	found	find	VERB
eurjchem-966	156	16	%	%	NOUN
eurjchem-966	156	17	*	*	PUNCT
eurjchem-966	156	18	±	±	NOUN
eurjchem-966	156	19	sd	sd	ADP
eurjchem-966	156	20	pure	pure	ADJ
eurjchem-966	156	21	added	add	VERB
eurjchem-966	156	22	(	(	PUNCT
eurjchem-966	156	23	µg	µg	ADJ
eurjchem-966	156	24	/	/	SYM
eurjchem-966	156	25	ml	ml	NOUN
eurjchem-966	156	26	)	)	PUNCT
eurjchem-966	156	27	recovery	recovery	NOUN
eurjchem-966	156	28	%	%	NOUN
eurjchem-966	156	29	1dd	1dd	ADJ
eurjchem-966	156	30	method	method	NOUN
eurjchem-966	156	31	10.00	10.00	NUM
eurjchem-966	156	32	101.23±1.008	101.23±1.008	NOUN
eurjchem-966	156	33	8.00	8.00	NUM
eurjchem-966	156	34	99.04	99.04	NUM
eurjchem-966	156	35	10.00	10.00	NUM
eurjchem-966	156	36	100.3	100.3	NUM
eurjchem-966	156	37	12.00	12.00	NUM
eurjchem-966	156	38	97.22	97.22	NUM
eurjchem-966	156	39	mean±sd	mean±sd	ADP
eurjchem-966	156	40	98.84±1.527	98.84±1.527	NUM
eurjchem-966	156	41	mean	mean	NOUN
eurjchem-966	156	42	centring	centre	VERB
eurjchem-966	156	43	spectrophotometric	spectrophotometric	ADJ
eurjchem-966	156	44	method	method	NOUN
eurjchem-966	156	45	10.00	10.00	NUM
eurjchem-966	156	46	101.28±1.758	101.28±1.758	NOUN
eurjchem-966	156	47	8.00	8.00	NUM
eurjchem-966	156	48	101.48	101.48	NUM
eurjchem-966	156	49	10.00	10.00	NUM
eurjchem-966	156	50	101.55	101.55	NUM
eurjchem-966	156	51	12.00	12.00	NUM
eurjchem-966	156	52	100.89	100.89	NUM
eurjchem-966	156	53	mean±sd	mean±sd	ADP
eurjchem-966	156	54	101.31±0.359	101.31±0.359	NUM
eurjchem-966	156	55	hptlc	hptlc	NOUN
eurjchem-966	156	56	method	method	NOUN
eurjchem-966	156	57	0.60	0.60	NUM
eurjchem-966	156	58	99.88±1.004	99.88±1.004	NUM
eurjchem-966	156	59	0.40	0.40	NUM
eurjchem-966	156	60	101.6	101.6	NUM
eurjchem-966	156	61	0.60	0.60	NUM
eurjchem-966	156	62	98.83	98.83	NUM
eurjchem-966	156	63	0.80	0.80	NUM
eurjchem-966	156	64	97.4	97.4	NUM
eurjchem-966	156	65	mean±sd	mean±sd	ADP
eurjchem-966	156	66	99.28±2.139	99.28±2.139	NUM
eurjchem-966	156	67	*	*	PUNCT
eurjchem-966	156	68	average	average	NOUN
eurjchem-966	156	69	of	of	ADP
eurjchem-966	156	70	6	6	NUM
eurjchem-966	156	71	determinations	determination	NOUN
eurjchem-966	156	72	.	.	PUNCT
eurjchem-966	157	1	table	table	NOUN
eurjchem-966	157	2	3	3	NUM
eurjchem-966	157	3	.	.	PUNCT
eurjchem-966	158	1	regression	regression	NOUN
eurjchem-966	158	2	and	and	CCONJ
eurjchem-966	158	3	validation	validation	NOUN
eurjchem-966	158	4	parameters	parameter	NOUN
eurjchem-966	158	5	of	of	ADP
eurjchem-966	158	6	the	the	DET
eurjchem-966	158	7	proposed	propose	VERB
eurjchem-966	158	8	methods	method	NOUN
eurjchem-966	158	9	for	for	ADP
eurjchem-966	158	10	determination	determination	NOUN
eurjchem-966	158	11	of	of	ADP
eurjchem-966	158	12	acm	acm	NOUN
eurjchem-966	158	13	in	in	ADP
eurjchem-966	158	14	presence	presence	NOUN
eurjchem-966	158	15	of	of	ADP
eurjchem-966	158	16	deg	deg	PROPN
eurjchem-966	158	17	.	.	PUNCT
eurjchem-966	159	1	parameter	parameter	PROPN
eurjchem-966	159	2	1dd	1dd	ADJ
eurjchem-966	159	3	spectrophotometric	spectrophotometric	ADJ
eurjchem-966	159	4	method	method	NOUN
eurjchem-966	159	5	mean	mean	VERB
eurjchem-966	159	6	centering	centering	NOUN
eurjchem-966	159	7	method	method	NOUN
eurjchem-966	159	8	hptlc	hptlc	NOUN
eurjchem-966	159	9	method	method	NOUN
eurjchem-966	159	10	linearity	linearity	NOUN
eurjchem-966	159	11	and	and	CCONJ
eurjchem-966	159	12	range	range	VERB
eurjchem-966	159	13	2‐22	2‐22	NUM
eurjchem-966	159	14	µg	µg	NOUN
eurjchem-966	159	15	/	/	SYM
eurjchem-966	159	16	ml	ml	NOUN
eurjchem-966	159	17	2‐22	2‐22	NUM
eurjchem-966	159	18	µg	µg	NOUN
eurjchem-966	159	19	/	/	SYM
eurjchem-966	159	20	ml	ml	NOUN
eurjchem-966	159	21	0.4‐1.4	0.4‐1.4	NOUN
eurjchem-966	159	22	µg	µg	ADJ
eurjchem-966	159	23	/	/	SYM
eurjchem-966	159	24	band	band	NOUN
eurjchem-966	159	25	slope	slope	NOUN
eurjchem-966	159	26	0.0039	0.0039	NUM
eurjchem-966	159	27	0.0030	0.0030	NUM
eurjchem-966	159	28	0.1944	0.1944	NUM
eurjchem-966	159	29	intercept	intercept	NOUN
eurjchem-966	159	30	0.0024	0.0024	NUM
eurjchem-966	159	31	0.0030	0.0030	NUM
eurjchem-966	159	32	0.0671	0.0671	NUM
eurjchem-966	159	33	correlation	correlation	NOUN
eurjchem-966	159	34	coefficient	coefficient	NOUN
eurjchem-966	159	35	(	(	PUNCT
eurjchem-966	159	36	r	r	NOUN
eurjchem-966	159	37	)	)	PUNCT
eurjchem-966	159	38	0.9999	0.9999	NUM
eurjchem-966	159	39	0.9999	0.9999	NUM
eurjchem-966	159	40	0.9999	0.9999	NUM
eurjchem-966	159	41	accuracy	accuracy	NOUN
eurjchem-966	159	42	99.65%±0.797	99.65%±0.797	NOUN
eurjchem-966	159	43	99.30%±1.146	99.30%±1.146	NOUN
eurjchem-966	160	1	100.00%±0.709	100.00%±0.709	NUM
eurjchem-966	160	2	specificity	specificity	NOUN
eurjchem-966	160	3	and	and	CCONJ
eurjchem-966	160	4	selectivity	selectivity	NOUN
eurjchem-966	160	5	100.13±1.61	100.13±1.61	NUM
eurjchem-966	160	6	99.96±1.780	99.96±1.780	NUM
eurjchem-966	160	7	‐	‐	ADJ
eurjchem-966	160	8	precision	precision	NOUN
eurjchem-966	160	9	repeatability	repeatability	NOUN
eurjchem-966	160	10	(	(	PUNCT
eurjchem-966	160	11	rsd%	rsd%	NOUN
eurjchem-966	160	12	)	)	PUNCT
eurjchem-966	160	13	a	a	DET
eurjchem-966	160	14	0.318‐0.056	0.318‐0.056	NUM
eurjchem-966	160	15	0.037‐0.099	0.037‐0.099	NUM
eurjchem-966	160	16	0.341‐1.358	0.341‐1.358	NUM
eurjchem-966	160	17	intermediadte	intermediadte	VERB
eurjchem-966	160	18	precision	precision	NOUN
eurjchem-966	160	19	(	(	PUNCT
eurjchem-966	160	20	rsd%	rsd%	NOUN
eurjchem-966	160	21	)	)	PUNCT
eurjchem-966	160	22	a	a	DET
eurjchem-966	160	23	0.275‐0.450	0.275‐0.450	NOUN
eurjchem-966	160	24	0.057‐0.910	0.057‐0.910	NUM
eurjchem-966	160	25	2.828‐2.805	2.828‐2.805	NUM
eurjchem-966	161	1	lod	lod	PROPN
eurjchem-966	161	2	b	b	PROPN
eurjchem-966	161	3	0.379	0.379	NUM
eurjchem-966	161	4	µg	µg	ADJ
eurjchem-966	161	5	/	/	SYM
eurjchem-966	161	6	ml	ml	ADP
eurjchem-966	161	7	0.407	0.407	NUM
eurjchem-966	161	8	µg	µg	NOUN
eurjchem-966	161	9	/	/	SYM
eurjchem-966	161	10	ml	ml	NOUN
eurjchem-966	161	11	0.050	0.050	NUM
eurjchem-966	161	12	µg	µg	ADJ
eurjchem-966	161	13	/	/	SYM
eurjchem-966	161	14	band	band	NOUN
eurjchem-966	161	15	loq	loq	PROPN
eurjchem-966	161	16	b	b	PROPN
eurjchem-966	161	17	1.147	1.147	NUM
eurjchem-966	161	18	µg	µg	NOUN
eurjchem-966	161	19	/	/	SYM
eurjchem-966	161	20	ml	ml	NOUN
eurjchem-966	161	21	1.232	1.232	NUM
eurjchem-966	161	22	µg	µg	NOUN
eurjchem-966	161	23	/	/	SYM
eurjchem-966	161	24	ml	ml	NOUN
eurjchem-966	161	25	0.400	0.400	NUM
eurjchem-966	161	26	µg	µg	ADJ
eurjchem-966	161	27	/	/	SYM
eurjchem-966	161	28	band	band	NOUN
eurjchem-966	161	29	robustness	robustness	NOUN
eurjchem-966	161	30	‐	‐	NOUN
eurjchem-966	161	31	‐	‐	ADV
eurjchem-966	161	32	99.50%±0.884	99.50%±0.884	PROPN
eurjchem-966	161	33	a	a	DET
eurjchem-966	161	34	(	(	PUNCT
eurjchem-966	161	35	rsd%	rsd%	NOUN
eurjchem-966	161	36	)	)	PUNCT
eurjchem-966	161	37	and	and	CCONJ
eurjchem-966	161	38	(	(	PUNCT
eurjchem-966	161	39	rsd%	rsd%	NOUN
eurjchem-966	161	40	)	)	PUNCT
eurjchem-966	161	41	;	;	PUNCT
eurjchem-966	161	42	the	the	DET
eurjchem-966	161	43	intra‐	intra‐	PROPN
eurjchem-966	161	44	and	and	CCONJ
eurjchem-966	161	45	inter‐day	inter‐day	PROPN
eurjchem-966	161	46	relative	relative	ADJ
eurjchem-966	161	47	standard	standard	ADJ
eurjchem-966	161	48	deviation	deviation	NOUN
eurjchem-966	161	49	of	of	ADP
eurjchem-966	161	50	concentrations	concentration	NOUN
eurjchem-966	161	51	(	(	PUNCT
eurjchem-966	161	52	6	6	NUM
eurjchem-966	161	53	,	,	PUNCT
eurjchem-966	161	54	20	20	NUM
eurjchem-966	161	55	µg	µg	NOUN
eurjchem-966	161	56	/	/	SYM
eurjchem-966	161	57	ml	ml	NOUN
eurjchem-966	161	58	)	)	PUNCT
eurjchem-966	161	59	for	for	ADP
eurjchem-966	161	60	1dd	1dd	ADJ
eurjchem-966	161	61	method	method	NOUN
eurjchem-966	161	62	,	,	PUNCT
eurjchem-966	161	63	(	(	PUNCT
eurjchem-966	161	64	4	4	NUM
eurjchem-966	161	65	,	,	PUNCT
eurjchem-966	161	66	12	12	NUM
eurjchem-966	161	67	µg	µg	NOUN
eurjchem-966	161	68	/	/	SYM
eurjchem-966	161	69	ml	ml	NOUN
eurjchem-966	161	70	)	)	PUNCT
eurjchem-966	161	71	for	for	ADP
eurjchem-966	161	72	mcr	mcr	PROPN
eurjchem-966	161	73	method	method	NOUN
eurjchem-966	161	74	and	and	CCONJ
eurjchem-966	161	75	(	(	PUNCT
eurjchem-966	161	76	0.6	0.6	NUM
eurjchem-966	161	77	,	,	PUNCT
eurjchem-966	161	78	1.2	1.2	NUM
eurjchem-966	161	79	µg	µg	ADJ
eurjchem-966	161	80	/	/	SYM
eurjchem-966	161	81	band	band	NOUN
eurjchem-966	161	82	)	)	PUNCT
eurjchem-966	161	83	for	for	ADP
eurjchem-966	161	84	hptlc	hptlc	NOUN
eurjchem-966	161	85	method	method	NOUN
eurjchem-966	161	86	.	.	PUNCT
eurjchem-966	162	1	b	b	X
eurjchem-966	162	2	limit	limit	NOUN
eurjchem-966	162	3	of	of	ADP
eurjchem-966	162	4	detection	detection	NOUN
eurjchem-966	162	5	and	and	CCONJ
eurjchem-966	162	6	quantitation	quantitation	NOUN
eurjchem-966	162	7	are	be	AUX
eurjchem-966	162	8	determined	determine	VERB
eurjchem-966	162	9	via	via	ADP
eurjchem-966	162	10	calculations	calculation	NOUN
eurjchem-966	162	11	for	for	ADP
eurjchem-966	162	12	1dd	1dd	ADJ
eurjchem-966	162	13	and	and	CCONJ
eurjchem-966	162	14	mcr	mcr	PROPN
eurjchem-966	162	15	methods	method	NOUN
eurjchem-966	162	16	(	(	PUNCT
eurjchem-966	162	17	lod	lod	PROPN
eurjchem-966	162	18	=	=	SYM
eurjchem-966	162	19	3.3	3.3	NUM
eurjchem-966	162	20	×	×	NOUN
eurjchem-966	162	21	sd	sd	NOUN
eurjchem-966	162	22	/	/	SYM
eurjchem-966	162	23	slope	slope	NOUN
eurjchem-966	162	24	,	,	PUNCT
eurjchem-966	162	25	loq	loq	PROPN
eurjchem-966	162	26	=	=	PROPN
eurjchem-966	162	27	10	10	NUM
eurjchem-966	162	28	×	×	NOUN
eurjchem-966	162	29	sd	sd	NOUN
eurjchem-966	162	30	/	/	SYM
eurjchem-966	162	31	slope	slope	NOUN
eurjchem-966	162	32	)	)	PUNCT
eurjchem-966	162	33	and	and	CCONJ
eurjchem-966	162	34	experimentally	experimentally	ADV
eurjchem-966	162	35	by	by	ADP
eurjchem-966	162	36	signal‐to‐noise	signal‐to‐noise	NOUN
eurjchem-966	162	37	ratio	ratio	NOUN
eurjchem-966	162	38	for	for	ADP
eurjchem-966	162	39	hptlc	hptlc	NOUN
eurjchem-966	162	40	method	method	NOUN
eurjchem-966	162	41	[	[	X
eurjchem-966	162	42	20	20	NUM
eurjchem-966	162	43	]	]	PUNCT
eurjchem-966	162	44	.	.	PUNCT
eurjchem-966	163	1	results	result	NOUN
eurjchem-966	163	2	given	give	VERB
eurjchem-966	163	3	in	in	ADP
eurjchem-966	163	4	table	table	NOUN
eurjchem-966	163	5	1	1	NUM
eurjchem-966	163	6	indicate	indicate	VERB
eurjchem-966	163	7	that	that	SCONJ
eurjchem-966	163	8	the	the	DET
eurjchem-966	163	9	proposed	propose	VERB
eurjchem-966	163	10	1dd	1dd	ADJ
eurjchem-966	163	11	method	method	NOUN
eurjchem-966	163	12	is	be	AUX
eurjchem-966	163	13	valid	valid	ADJ
eurjchem-966	163	14	for	for	ADP
eurjchem-966	163	15	determination	determination	NOUN
eurjchem-966	163	16	of	of	ADP
eurjchem-966	163	17	intact	intact	ADJ
eurjchem-966	163	18	acm	acm	NOUN
eurjchem-966	163	19	in	in	ADP
eurjchem-966	163	20	presence	presence	NOUN
eurjchem-966	163	21	of	of	ADP
eurjchem-966	163	22	up	up	ADP
eurjchem-966	163	23	to	to	PART
eurjchem-966	163	24	80	80	NUM
eurjchem-966	163	25	%	%	NOUN
eurjchem-966	163	26	of	of	ADP
eurjchem-966	163	27	its	its	PRON
eurjchem-966	163	28	deg	deg	NOUN
eurjchem-966	163	29	and	and	CCONJ
eurjchem-966	163	30	mean	mean	VERB
eurjchem-966	163	31	centering	centering	NOUN
eurjchem-966	163	32	method	method	NOUN
eurjchem-966	163	33	is	be	AUX
eurjchem-966	163	34	selective	selective	ADJ
eurjchem-966	163	35	and	and	CCONJ
eurjchem-966	163	36	valid	valid	ADJ
eurjchem-966	163	37	for	for	ADP
eurjchem-966	163	38	determination	determination	NOUN
eurjchem-966	163	39	of	of	ADP
eurjchem-966	163	40	acm	acm	NOUN
eurjchem-966	163	41	in	in	ADP
eurjchem-966	163	42	presence	presence	NOUN
eurjchem-966	163	43	of	of	ADP
eurjchem-966	163	44	up	up	ADP
eurjchem-966	163	45	to	to	PART
eurjchem-966	163	46	90	90	NUM
eurjchem-966	163	47	%	%	NOUN
eurjchem-966	163	48	of	of	ADP
eurjchem-966	163	49	its	its	PRON
eurjchem-966	163	50	deg	deg	NOUN
eurjchem-966	163	51	.	.	PUNCT
eurjchem-966	164	1	as	as	SCONJ
eurjchem-966	164	2	the	the	DET
eurjchem-966	164	3	suggested	suggest	VERB
eurjchem-966	164	4	methods	method	NOUN
eurjchem-966	164	5	could	could	AUX
eurjchem-966	164	6	effectively	effectively	ADV
eurjchem-966	164	7	determine	determine	VERB
eurjchem-966	164	8	the	the	DET
eurjchem-966	164	9	drug	drug	NOUN
eurjchem-966	164	10	in	in	ADP
eurjchem-966	164	11	presence	presence	NOUN
eurjchem-966	164	12	of	of	ADP
eurjchem-966	164	13	its	its	PRON
eurjchem-966	164	14	deg	deg	NOUN
eurjchem-966	164	15	,	,	PUNCT
eurjchem-966	164	16	they	they	PRON
eurjchem-966	164	17	can	can	AUX
eurjchem-966	164	18	be	be	AUX
eurjchem-966	164	19	employed	employ	VERB
eurjchem-966	164	20	as	as	ADP
eurjchem-966	164	21	stability	stability	NOUN
eurjchem-966	164	22	indicating	indicate	VERB
eurjchem-966	164	23	ones	one	NOUN
eurjchem-966	164	24	.	.	PUNCT
eurjchem-966	165	1	3.4	3.4	NUM
eurjchem-966	165	2	.	.	PUNCT
eurjchem-966	165	3	application	application	NOUN
eurjchem-966	165	4	of	of	ADP
eurjchem-966	165	5	the	the	DET
eurjchem-966	165	6	proposed	propose	VERB
eurjchem-966	165	7	methods	method	NOUN
eurjchem-966	165	8	to	to	ADP
eurjchem-966	165	9	the	the	DET
eurjchem-966	165	10	pharmaceutical	pharmaceutical	ADJ
eurjchem-966	165	11	formulation	formulation	NOUN
eurjchem-966	165	12	the	the	DET
eurjchem-966	165	13	suggested	suggest	VERB
eurjchem-966	165	14	methods	method	NOUN
eurjchem-966	165	15	were	be	AUX
eurjchem-966	165	16	successfully	successfully	ADV
eurjchem-966	165	17	applied	apply	VERB
eurjchem-966	165	18	for	for	ADP
eurjchem-966	165	19	the	the	DET
eurjchem-966	165	20	determination	determination	NOUN
eurjchem-966	165	21	of	of	ADP
eurjchem-966	165	22	acm	acm	NOUN
eurjchem-966	165	23	in	in	ADP
eurjchem-966	165	24	its	its	PRON
eurjchem-966	165	25	pharmaceutical	pharmaceutical	ADJ
eurjchem-966	165	26	formulation	formulation	NOUN
eurjchem-966	165	27	(	(	PUNCT
eurjchem-966	165	28	ostmap	ostmap	VERB
eurjchem-966	165	29	®	®	NOUN
eurjchem-966	165	30	capsules	capsule	NOUN
eurjchem-966	165	31	)	)	PUNCT
eurjchem-966	165	32	,	,	PUNCT
eurjchem-966	165	33	showing	show	VERB
eurjchem-966	165	34	good	good	ADJ
eurjchem-966	165	35	percentage	percentage	NOUN
eurjchem-966	165	36	recoveries	recovery	NOUN
eurjchem-966	165	37	.	.	PUNCT
eurjchem-966	166	1	the	the	DET
eurjchem-966	166	2	validity	validity	NOUN
eurjchem-966	166	3	of	of	ADP
eurjchem-966	166	4	the	the	DET
eurjchem-966	166	5	suggested	suggest	VERB
eurjchem-966	166	6	methods	method	NOUN
eurjchem-966	166	7	was	be	AUX
eurjchem-966	166	8	further	far	ADV
eurjchem-966	166	9	assessed	assess	VERB
eurjchem-966	166	10	by	by	ADP
eurjchem-966	166	11	applying	apply	VERB
eurjchem-966	166	12	the	the	DET
eurjchem-966	166	13	standard	standard	ADJ
eurjchem-966	166	14	addition	addition	NOUN
eurjchem-966	166	15	technique	technique	NOUN
eurjchem-966	166	16	as	as	SCONJ
eurjchem-966	166	17	shown	show	VERB
eurjchem-966	166	18	in	in	ADP
eurjchem-966	166	19	table	table	NOUN
eurjchem-966	166	20	2	2	NUM
eurjchem-966	166	21	.	.	NOUN
eurjchem-966	166	22	4	4	NUM
eurjchem-966	166	23	.	.	X
eurjchem-966	166	24	methods	method	NOUN
eurjchem-966	166	25	validation	validation	NOUN
eurjchem-966	166	26	methods	method	NOUN
eurjchem-966	166	27	validation	validation	NOUN
eurjchem-966	166	28	was	be	AUX
eurjchem-966	166	29	performed	perform	VERB
eurjchem-966	166	30	according	accord	VERB
eurjchem-966	166	31	to	to	ADP
eurjchem-966	166	32	the	the	DET
eurjchem-966	166	33	international	international	ADJ
eurjchem-966	166	34	conference	conference	NOUN
eurjchem-966	166	35	on	on	ADP
eurjchem-966	166	36	harmonization	harmonization	NOUN
eurjchem-966	167	1	(	(	PUNCT
eurjchem-966	167	2	ich	ich	NOUN
eurjchem-966	167	3	)	)	PUNCT
eurjchem-966	167	4	guidelines	guideline	NOUN
eurjchem-966	167	5	[	[	X
eurjchem-966	167	6	20	20	NUM
eurjchem-966	167	7	]	]	PUNCT
eurjchem-966	167	8	for	for	ADP
eurjchem-966	167	9	the	the	DET
eurjchem-966	167	10	proposed	propose	VERB
eurjchem-966	167	11	methods	method	NOUN
eurjchem-966	167	12	.	.	PUNCT
eurjchem-966	168	1	4.1	4.1	NUM
eurjchem-966	168	2	.	.	PUNCT
eurjchem-966	168	3	linearity	linearity	NOUN
eurjchem-966	168	4	under	under	ADP
eurjchem-966	168	5	optimum	optimum	ADJ
eurjchem-966	168	6	experimental	experimental	ADJ
eurjchem-966	168	7	conditions	condition	NOUN
eurjchem-966	168	8	,	,	PUNCT
eurjchem-966	168	9	acm	acm	PROPN
eurjchem-966	168	10	was	be	AUX
eurjchem-966	168	11	determined	determine	VERB
eurjchem-966	168	12	in	in	ADP
eurjchem-966	168	13	triplicates	triplicate	NOUN
eurjchem-966	168	14	in	in	ADP
eurjchem-966	168	15	the	the	DET
eurjchem-966	168	16	range	range	NOUN
eurjchem-966	168	17	of	of	ADP
eurjchem-966	168	18	2‐22	2‐22	NUM
eurjchem-966	168	19	µg	µg	NOUN
eurjchem-966	168	20	/	/	SYM
eurjchem-966	168	21	ml	ml	NOUN
eurjchem-966	168	22	for	for	ADP
eurjchem-966	168	23	1dd	1dd	ADJ
eurjchem-966	168	24	and	and	CCONJ
eurjchem-966	168	25	mcr	mcr	ADJ
eurjchem-966	168	26	methods	method	NOUN
eurjchem-966	168	27	and	and	CCONJ
eurjchem-966	168	28	in	in	ADP
eurjchem-966	168	29	the	the	DET
eurjchem-966	168	30	range	range	NOUN
eurjchem-966	168	31	of	of	ADP
eurjchem-966	168	32	0.4‐1.4	0.4‐1.4	NUM
eurjchem-966	168	33	μg	μg	PROPN
eurjchem-966	168	34	/	/	SYM
eurjchem-966	168	35	band	band	NOUN
eurjchem-966	168	36	for	for	ADP
eurjchem-966	168	37	hptlc	hptlc	NOUN
eurjchem-966	168	38	method	method	NOUN
eurjchem-966	168	39	,	,	PUNCT
eurjchem-966	168	40	table	table	NOUN
eurjchem-966	168	41	3	3	NUM
eurjchem-966	168	42	.	.	NOUN
eurjchem-966	168	43	4.2	4.2	NUM
eurjchem-966	168	44	.	.	PUNCT
eurjchem-966	169	1	range	range	VERB
eurjchem-966	169	2	the	the	DET
eurjchem-966	169	3	specified	specified	ADJ
eurjchem-966	169	4	range	range	NOUN
eurjchem-966	169	5	is	be	AUX
eurjchem-966	169	6	derived	derive	VERB
eurjchem-966	169	7	from	from	ADP
eurjchem-966	169	8	linearity	linearity	NOUN
eurjchem-966	169	9	studies	study	NOUN
eurjchem-966	169	10	and	and	CCONJ
eurjchem-966	169	11	depends	depend	VERB
eurjchem-966	169	12	on	on	ADP
eurjchem-966	169	13	the	the	DET
eurjchem-966	169	14	application	application	NOUN
eurjchem-966	169	15	of	of	ADP
eurjchem-966	169	16	analytical	analytical	ADJ
eurjchem-966	169	17	procedure	procedure	NOUN
eurjchem-966	169	18	.	.	PUNCT
eurjchem-966	170	1	the	the	DET
eurjchem-966	170	2	concentration	concentration	NOUN
eurjchem-966	170	3	of	of	ADP
eurjchem-966	170	4	acm	acm	PROPN
eurjchem-966	170	5	present	present	NOUN
eurjchem-966	170	6	in	in	ADP
eurjchem-966	170	7	pharmaceutical	pharmaceutical	ADJ
eurjchem-966	170	8	preparation	preparation	NOUN
eurjchem-966	170	9	gave	give	VERB
eurjchem-966	170	10	accurate	accurate	ADJ
eurjchem-966	170	11	and	and	CCONJ
eurjchem-966	170	12	precise	precise	ADJ
eurjchem-966	170	13	results	result	NOUN
eurjchem-966	170	14	with	with	ADP
eurjchem-966	170	15	the	the	DET
eurjchem-966	170	16	suggested	suggest	VERB
eurjchem-966	170	17	methods	method	NOUN
eurjchem-966	170	18	as	as	SCONJ
eurjchem-966	170	19	shown	show	VERB
eurjchem-966	170	20	in	in	ADP
eurjchem-966	170	21	table	table	NOUN
eurjchem-966	170	22	3	3	NUM
eurjchem-966	170	23	.	.	X
eurjchem-966	170	24	4.3	4.3	NUM
eurjchem-966	170	25	.	.	PUNCT
eurjchem-966	171	1	accuracy	accuracy	NOUN
eurjchem-966	171	2	accuracy	accuracy	NOUN
eurjchem-966	171	3	was	be	AUX
eurjchem-966	171	4	assessed	assess	VERB
eurjchem-966	171	5	by	by	ADP
eurjchem-966	171	6	the	the	DET
eurjchem-966	171	7	standard	standard	ADJ
eurjchem-966	171	8	addition	addition	NOUN
eurjchem-966	171	9	technique	technique	NOUN
eurjchem-966	171	10	and	and	CCONJ
eurjchem-966	171	11	through	through	ADP
eurjchem-966	171	12	analysis	analysis	NOUN
eurjchem-966	171	13	of	of	ADP
eurjchem-966	171	14	market	market	NOUN
eurjchem-966	171	15	pharmaceutical	pharmaceutical	NOUN
eurjchem-966	171	16	preparation	preparation	NOUN
eurjchem-966	171	17	by	by	ADP
eurjchem-966	171	18	the	the	DET
eurjchem-966	171	19	proposed	propose	VERB
eurjchem-966	171	20	methods	method	NOUN
eurjchem-966	171	21	.	.	PUNCT
eurjchem-966	172	1	the	the	DET
eurjchem-966	172	2	resulting	result	VERB
eurjchem-966	172	3	synthetic	synthetic	ADJ
eurjchem-966	172	4	mixtures	mixture	NOUN
eurjchem-966	172	5	(	(	PUNCT
eurjchem-966	172	6	of	of	ADP
eurjchem-966	172	7	pure	pure	ADJ
eurjchem-966	172	8	drug	drug	NOUN
eurjchem-966	172	9	portions	portion	NOUN
eurjchem-966	172	10	added	add	VERB
eurjchem-966	172	11	to	to	PART
eurjchem-966	172	12	dosage	dosage	NOUN
eurjchem-966	172	13	form	form	NOUN
eurjchem-966	172	14	)	)	PUNCT
eurjchem-966	172	15	were	be	AUX
eurjchem-966	172	16	assayed	assayed	ADJ
eurjchem-966	172	17	and	and	CCONJ
eurjchem-966	172	18	the	the	DET
eurjchem-966	172	19	found	find	VERB
eurjchem-966	172	20	concentration	concentration	NOUN
eurjchem-966	172	21	of	of	ADP
eurjchem-966	172	22	pure	pure	ADJ
eurjchem-966	172	23	drug	drug	NOUN
eurjchem-966	172	24	portions	portion	NOUN
eurjchem-966	172	25	were	be	AUX
eurjchem-966	172	26	compared	compare	VERB
eurjchem-966	172	27	to	to	ADP
eurjchem-966	172	28	those	those	PRON
eurjchem-966	172	29	expected	expect	VERB
eurjchem-966	172	30	.	.	PUNCT
eurjchem-966	173	1	the	the	DET
eurjchem-966	173	2	good	good	ADJ
eurjchem-966	173	3	recoveries	recovery	NOUN
eurjchem-966	173	4	of	of	ADP
eurjchem-966	173	5	pure	pure	ADJ
eurjchem-966	173	6	drug	drug	NOUN
eurjchem-966	173	7	samples	sample	NOUN
eurjchem-966	173	8	suggest	suggest	VERB
eurjchem-966	173	9	good	good	ADJ
eurjchem-966	173	10	accuracy	accuracy	NOUN
eurjchem-966	173	11	of	of	ADP
eurjchem-966	173	12	the	the	DET
eurjchem-966	173	13	proposed	propose	VERB
eurjchem-966	173	14	methods	method	NOUN
eurjchem-966	173	15	,	,	PUNCT
eurjchem-966	173	16	table	table	NOUN
eurjchem-966	173	17	2	2	NUM
eurjchem-966	173	18	.	.	PUNCT
eurjchem-966	173	19	naguib	naguib	PROPN
eurjchem-966	173	20	et	et	PROPN
eurjchem-966	173	21	al	al	PROPN
eurjchem-966	173	22	.	.	PUNCT
eurjchem-966	173	23	/	/	SYM
eurjchem-966	173	24	european	european	PROPN
eurjchem-966	173	25	journal	journal	PROPN
eurjchem-966	173	26	of	of	ADP
eurjchem-966	173	27	chemistry	chemistry	NOUN
eurjchem-966	173	28	5	5	NUM
eurjchem-966	173	29	(	(	PUNCT
eurjchem-966	173	30	2	2	NUM
eurjchem-966	173	31	)	)	PUNCT
eurjchem-966	173	32	(	(	PUNCT
eurjchem-966	173	33	2014	2014	NUM
eurjchem-966	173	34	)	)	PUNCT
eurjchem-966	173	35	219‐226	219‐226	NUM
eurjchem-966	173	36	225	225	NUM
eurjchem-966	173	37	table	table	NOUN
eurjchem-966	173	38	4	4	NUM
eurjchem-966	173	39	.	.	PUNCT
eurjchem-966	174	1	parameters	parameter	NOUN
eurjchem-966	174	2	of	of	ADP
eurjchem-966	174	3	system	system	NOUN
eurjchem-966	174	4	suitability	suitability	NOUN
eurjchem-966	174	5	of	of	ADP
eurjchem-966	174	6	the	the	DET
eurjchem-966	174	7	developed	develop	VERB
eurjchem-966	174	8	hptlc	hptlc	NOUN
eurjchem-966	174	9	method	method	NOUN
eurjchem-966	174	10	for	for	ADP
eurjchem-966	174	11	the	the	DET
eurjchem-966	174	12	determination	determination	NOUN
eurjchem-966	174	13	of	of	ADP
eurjchem-966	174	14	acm	acm	NOUN
eurjchem-966	174	15	in	in	ADP
eurjchem-966	174	16	presence	presence	NOUN
eurjchem-966	174	17	of	of	ADP
eurjchem-966	174	18	deg	deg	PROPN
eurjchem-966	174	19	.	.	PUNCT
eurjchem-966	175	1	parameters	parameter	NOUN
eurjchem-966	175	2	acm	acm	PROPN
eurjchem-966	175	3	deg	deg	PROPN
eurjchem-966	175	4	capacity	capacity	NOUN
eurjchem-966	175	5	factor	factor	NOUN
eurjchem-966	175	6	(	(	PUNCT
eurjchem-966	175	7	k	k	NOUN
eurjchem-966	175	8	'	'	PUNCT
eurjchem-966	175	9	)	)	PUNCT
eurjchem-966	175	10	2	2	NUM
eurjchem-966	175	11	6	6	NUM
eurjchem-966	175	12	symmetry	symmetry	NOUN
eurjchem-966	175	13	factor	factor	NOUN
eurjchem-966	175	14	1.03	1.03	NUM
eurjchem-966	175	15	0.83	0.83	NUM
eurjchem-966	175	16	resolution	resolution	NOUN
eurjchem-966	175	17	(	(	PUNCT
eurjchem-966	175	18	rs	rs	NOUN
eurjchem-966	175	19	)	)	PUNCT
eurjchem-966	175	20	6.62	6.62	NUM
eurjchem-966	175	21	selectivity	selectivity	NOUN
eurjchem-966	175	22	(	(	PUNCT
eurjchem-966	175	23	α	α	NOUN
eurjchem-966	175	24	)	)	PUNCT
eurjchem-966	175	25	2.43	2.43	NUM
eurjchem-966	175	26	table	table	NOUN
eurjchem-966	175	27	5	5	NUM
eurjchem-966	175	28	.	.	PUNCT
eurjchem-966	175	29	statistical	statistical	ADJ
eurjchem-966	175	30	analysis	analysis	NOUN
eurjchem-966	175	31	of	of	ADP
eurjchem-966	175	32	the	the	DET
eurjchem-966	175	33	three	three	NUM
eurjchem-966	175	34	proposed	propose	VERB
eurjchem-966	175	35	methods	method	NOUN
eurjchem-966	175	36	(	(	PUNCT
eurjchem-966	175	37	1dd	1dd	ADJ
eurjchem-966	175	38	spectrophotometric	spectrophotometric	ADJ
eurjchem-966	175	39	method	method	NOUN
eurjchem-966	175	40	,	,	PUNCT
eurjchem-966	175	41	mean	mean	VERB
eurjchem-966	175	42	centering	centering	NOUN
eurjchem-966	175	43	method	method	NOUN
eurjchem-966	175	44	and	and	CCONJ
eurjchem-966	175	45	hptlc	hptlc	NOUN
eurjchem-966	175	46	method	method	NOUN
eurjchem-966	175	47	)	)	PUNCT
eurjchem-966	175	48	and	and	CCONJ
eurjchem-966	175	49	the	the	DET
eurjchem-966	175	50	reported	report	VERB
eurjchem-966	175	51	hplc	hplc	NOUN
eurjchem-966	175	52	method	method	NOUN
eurjchem-966	175	53	for	for	ADP
eurjchem-966	175	54	determination	determination	NOUN
eurjchem-966	175	55	of	of	ADP
eurjchem-966	175	56	acm	acm	NOUN
eurjchem-966	175	57	in	in	ADP
eurjchem-966	175	58	ostmap	ostmap	NOUN
eurjchem-966	175	59	®	®	NOUN
eurjchem-966	175	60	capsules	capsule	NOUN
eurjchem-966	175	61	.	.	PUNCT
eurjchem-966	176	1	parameters	parameter	NOUN
eurjchem-966	176	2	1dd	1dd	ADJ
eurjchem-966	176	3	spectrophotometric	spectrophotometric	ADJ
eurjchem-966	176	4	method	method	NOUN
eurjchem-966	176	5	mean	mean	VERB
eurjchem-966	176	6	centering	centering	NOUN
eurjchem-966	176	7	method	method	NOUN
eurjchem-966	176	8	hptlc	hptlc	NOUN
eurjchem-966	176	9	method	method	NOUN
eurjchem-966	176	10	reported	report	VERB
eurjchem-966	176	11	hplc	hplc	NOUN
eurjchem-966	176	12	method	method	NOUN
eurjchem-966	176	13	a	a	DET
eurjchem-966	176	14	mean	mean	NOUN
eurjchem-966	176	15	101.23	101.23	NUM
eurjchem-966	176	16	101.28	101.28	NUM
eurjchem-966	176	17	99.88	99.88	NUM
eurjchem-966	176	18	102.86	102.86	NUM
eurjchem-966	176	19	sd	sd	ADP
eurjchem-966	176	20	1.008	1.008	NUM
eurjchem-966	176	21	1.758	1.758	NUM
eurjchem-966	176	22	1.004	1.004	NUM
eurjchem-966	176	23	1.682	1.682	NUM
eurjchem-966	176	24	variance	variance	NOUN
eurjchem-966	176	25	1.0151	1.0151	NUM
eurjchem-966	176	26	3.091	3.091	NUM
eurjchem-966	176	27	1.008	1.008	NUM
eurjchem-966	176	28	2.830	2.830	NUM
eurjchem-966	176	29	n	n	ADP
eurjchem-966	176	30	6	6	NUM
eurjchem-966	176	31	6	6	NUM
eurjchem-966	176	32	6	6	NUM
eurjchem-966	176	33	6	6	NUM
eurjchem-966	176	34	student	student	NOUN
eurjchem-966	176	35	’s	’s	PART
eurjchem-966	176	36	t‐test	t‐test	X
eurjchem-966	176	37	b	b	X
eurjchem-966	176	38	(	(	PUNCT
eurjchem-966	176	39	2.228	2.228	NUM
eurjchem-966	176	40	)	)	PUNCT
eurjchem-966	176	41	0.075	0.075	NUM
eurjchem-966	176	42	0.142	0.142	NUM
eurjchem-966	176	43	0.006	0.006	NUM
eurjchem-966	176	44	f‐	f‐	PROPN
eurjchem-966	176	45	test	test	NOUN
eurjchem-966	176	46	b	b	PROPN
eurjchem-966	176	47	(	(	PUNCT
eurjchem-966	176	48	5.050	5.050	NUM
eurjchem-966	176	49	)	)	PUNCT
eurjchem-966	176	50	2.788	2.788	NUM
eurjchem-966	176	51	1.092	1.092	NUM
eurjchem-966	176	52	2.807	2.807	NUM
eurjchem-966	176	53	a	a	DET
eurjchem-966	176	54	hplc	hplc	NOUN
eurjchem-966	176	55	determination	determination	NOUN
eurjchem-966	176	56	of	of	ADP
eurjchem-966	176	57	acm	acm	NOUN
eurjchem-966	176	58	using	use	VERB
eurjchem-966	176	59	acetonitrile	acetonitrile	NOUN
eurjchem-966	176	60	:	:	PUNCT
eurjchem-966	176	61	water	water	NOUN
eurjchem-966	176	62	(	(	PUNCT
eurjchem-966	176	63	80:20	80:20	NUM
eurjchem-966	176	64	,	,	PUNCT
eurjchem-966	176	65	v	v	NOUN
eurjchem-966	176	66	:	:	PUNCT
eurjchem-966	176	67	v	v	NOUN
eurjchem-966	176	68	)	)	PUNCT
eurjchem-966	176	69	as	as	ADP
eurjchem-966	176	70	mobile	mobile	ADJ
eurjchem-966	176	71	phase	phase	NOUN
eurjchem-966	176	72	and	and	CCONJ
eurjchem-966	176	73	uv	uv	NOUN
eurjchem-966	176	74	detection	detection	NOUN
eurjchem-966	176	75	at	at	ADP
eurjchem-966	176	76	280	280	NUM
eurjchem-966	176	77	nm	nm	NOUN
eurjchem-966	176	78	[	[	X
eurjchem-966	176	79	4	4	NUM
eurjchem-966	176	80	]	]	PUNCT
eurjchem-966	176	81	.	.	PUNCT
eurjchem-966	177	1	b	b	X
eurjchem-966	177	2	the	the	DET
eurjchem-966	177	3	values	value	NOUN
eurjchem-966	177	4	between	between	ADP
eurjchem-966	177	5	parenthesis	parenthesis	NOUN
eurjchem-966	177	6	are	be	AUX
eurjchem-966	177	7	corresponding	correspond	VERB
eurjchem-966	177	8	to	to	ADP
eurjchem-966	177	9	the	the	DET
eurjchem-966	177	10	theoretical	theoretical	ADJ
eurjchem-966	177	11	values	value	NOUN
eurjchem-966	177	12	of	of	ADP
eurjchem-966	177	13	t	t	PROPN
eurjchem-966	177	14	and	and	CCONJ
eurjchem-966	177	15	f	f	PROPN
eurjchem-966	177	16	(	(	PUNCT
eurjchem-966	177	17	p	p	X
eurjchem-966	177	18	=	=	NOUN
eurjchem-966	177	19	0.05	0.05	NUM
eurjchem-966	177	20	)	)	PUNCT
eurjchem-966	177	21	.	.	PUNCT
eurjchem-966	178	1	4.4	4.4	NUM
eurjchem-966	178	2	.	.	PUNCT
eurjchem-966	179	1	precision	precision	PROPN
eurjchem-966	179	2	4.4.1	4.4.1	NUM
eurjchem-966	179	3	.	.	PUNCT
eurjchem-966	180	1	repeatability	repeatability	NOUN
eurjchem-966	180	2	two	two	NUM
eurjchem-966	180	3	concentrations	concentration	NOUN
eurjchem-966	180	4	of	of	ADP
eurjchem-966	180	5	acm	acm	NOUN
eurjchem-966	180	6	(	(	PUNCT
eurjchem-966	180	7	6	6	NUM
eurjchem-966	180	8	,	,	PUNCT
eurjchem-966	180	9	20	20	NUM
eurjchem-966	180	10	µg	µg	NOUN
eurjchem-966	180	11	/	/	SYM
eurjchem-966	180	12	ml	ml	NOUN
eurjchem-966	180	13	)	)	PUNCT
eurjchem-966	180	14	for	for	ADP
eurjchem-966	180	15	1dd	1dd	ADJ
eurjchem-966	180	16	method	method	NOUN
eurjchem-966	180	17	,	,	PUNCT
eurjchem-966	180	18	(	(	PUNCT
eurjchem-966	180	19	4	4	NUM
eurjchem-966	180	20	,	,	PUNCT
eurjchem-966	180	21	12	12	NUM
eurjchem-966	180	22	µg	µg	NOUN
eurjchem-966	180	23	/	/	SYM
eurjchem-966	180	24	ml	ml	NOUN
eurjchem-966	180	25	)	)	PUNCT
eurjchem-966	180	26	for	for	ADP
eurjchem-966	180	27	mcr	mcr	PROPN
eurjchem-966	180	28	method	method	NOUN
eurjchem-966	180	29	and	and	CCONJ
eurjchem-966	180	30	(	(	PUNCT
eurjchem-966	180	31	0.6	0.6	NUM
eurjchem-966	180	32	,	,	PUNCT
eurjchem-966	180	33	1.2	1.2	NUM
eurjchem-966	180	34	µg	µg	ADJ
eurjchem-966	180	35	/	/	SYM
eurjchem-966	180	36	band	band	NOUN
eurjchem-966	180	37	)	)	PUNCT
eurjchem-966	180	38	for	for	ADP
eurjchem-966	180	39	hptlc	hptlc	NOUN
eurjchem-966	180	40	method	method	NOUN
eurjchem-966	180	41	were	be	AUX
eurjchem-966	180	42	determined	determine	VERB
eurjchem-966	180	43	in	in	ADP
eurjchem-966	180	44	triplicates	triplicate	NOUN
eurjchem-966	180	45	in	in	ADP
eurjchem-966	180	46	the	the	DET
eurjchem-966	180	47	same	same	ADJ
eurjchem-966	180	48	day	day	NOUN
eurjchem-966	180	49	to	to	PART
eurjchem-966	180	50	estimate	estimate	VERB
eurjchem-966	180	51	intraday	intraday	NOUN
eurjchem-966	180	52	variation	variation	NOUN
eurjchem-966	180	53	.	.	PUNCT
eurjchem-966	181	1	good	good	ADJ
eurjchem-966	181	2	results	result	NOUN
eurjchem-966	181	3	and	and	CCONJ
eurjchem-966	181	4	acceptable	acceptable	ADJ
eurjchem-966	181	5	relative	relative	ADJ
eurjchem-966	181	6	standard	standard	ADJ
eurjchem-966	181	7	deviation	deviation	NOUN
eurjchem-966	181	8	(	(	PUNCT
eurjchem-966	181	9	rsd%	rsd%	NOUN
eurjchem-966	181	10	)	)	PUNCT
eurjchem-966	181	11	are	be	AUX
eurjchem-966	181	12	shown	show	VERB
eurjchem-966	181	13	in	in	ADP
eurjchem-966	181	14	table	table	NOUN
eurjchem-966	181	15	3	3	NUM
eurjchem-966	181	16	.	.	X
eurjchem-966	181	17	4.4.2	4.4.2	NUM
eurjchem-966	181	18	.	.	PUNCT
eurjchem-966	182	1	intermediate	intermediate	ADJ
eurjchem-966	182	2	precision	precision	NOUN
eurjchem-966	182	3	the	the	DET
eurjchem-966	182	4	previous	previous	ADJ
eurjchem-966	182	5	procedures	procedure	NOUN
eurjchem-966	182	6	were	be	AUX
eurjchem-966	182	7	repeated	repeat	VERB
eurjchem-966	182	8	on	on	ADP
eurjchem-966	182	9	the	the	DET
eurjchem-966	182	10	same	same	ADJ
eurjchem-966	182	11	concentrations	concentration	NOUN
eurjchem-966	182	12	seven	seven	NUM
eurjchem-966	182	13	times	time	NOUN
eurjchem-966	182	14	on	on	ADP
eurjchem-966	182	15	different	different	ADJ
eurjchem-966	182	16	four	four	NUM
eurjchem-966	182	17	days	day	NOUN
eurjchem-966	182	18	to	to	PART
eurjchem-966	182	19	determine	determine	VERB
eurjchem-966	182	20	the	the	DET
eurjchem-966	182	21	intermediate	intermediate	ADJ
eurjchem-966	182	22	precision	precision	NOUN
eurjchem-966	182	23	.	.	PUNCT
eurjchem-966	183	1	good	good	ADJ
eurjchem-966	183	2	results	result	NOUN
eurjchem-966	183	3	and	and	CCONJ
eurjchem-966	183	4	acceptable	acceptable	ADJ
eurjchem-966	183	5	relative	relative	ADJ
eurjchem-966	183	6	standard	standard	ADJ
eurjchem-966	183	7	deviation	deviation	NOUN
eurjchem-966	183	8	(	(	PUNCT
eurjchem-966	183	9	rsd%	rsd%	NOUN
eurjchem-966	183	10	)	)	PUNCT
eurjchem-966	183	11	shown	show	VERB
eurjchem-966	183	12	in	in	ADP
eurjchem-966	183	13	table	table	NOUN
eurjchem-966	183	14	3	3	NUM
eurjchem-966	183	15	.	.	NOUN
eurjchem-966	183	16	4.5	4.5	NUM
eurjchem-966	183	17	.	.	PUNCT
eurjchem-966	184	1	specificity	specificity	NOUN
eurjchem-966	184	2	it	it	PRON
eurjchem-966	184	3	was	be	AUX
eurjchem-966	184	4	evaluated	evaluate	VERB
eurjchem-966	184	5	by	by	ADP
eurjchem-966	184	6	analysis	analysis	NOUN
eurjchem-966	184	7	of	of	ADP
eurjchem-966	184	8	different	different	ADJ
eurjchem-966	184	9	synthetic	synthetic	ADJ
eurjchem-966	184	10	laboratory	laboratory	NOUN
eurjchem-966	184	11	prepared	prepare	VERB
eurjchem-966	184	12	mixtures	mixture	NOUN
eurjchem-966	184	13	containing	contain	VERB
eurjchem-966	184	14	different	different	ADJ
eurjchem-966	184	15	ratios	ratio	NOUN
eurjchem-966	184	16	of	of	ADP
eurjchem-966	184	17	acm	acm	NOUN
eurjchem-966	184	18	spiked	spike	VERB
eurjchem-966	184	19	with	with	ADP
eurjchem-966	184	20	appropriate	appropriate	ADJ
eurjchem-966	184	21	levels	level	NOUN
eurjchem-966	184	22	of	of	ADP
eurjchem-966	184	23	deg	deg	PROPN
eurjchem-966	184	24	.	.	PUNCT
eurjchem-966	185	1	demonstrating	demonstrate	VERB
eurjchem-966	185	2	that	that	SCONJ
eurjchem-966	185	3	the	the	DET
eurjchem-966	185	4	assay	assay	NOUN
eurjchem-966	185	5	results	result	NOUN
eurjchem-966	185	6	are	be	AUX
eurjchem-966	185	7	unaffected	unaffected	ADJ
eurjchem-966	185	8	by	by	ADP
eurjchem-966	185	9	the	the	DET
eurjchem-966	185	10	presence	presence	NOUN
eurjchem-966	185	11	of	of	ADP
eurjchem-966	185	12	deg	deg	PROPN
eurjchem-966	185	13	prove	prove	VERB
eurjchem-966	185	14	specificity	specificity	NOUN
eurjchem-966	185	15	of	of	ADP
eurjchem-966	185	16	the	the	DET
eurjchem-966	185	17	methods	method	NOUN
eurjchem-966	185	18	as	as	SCONJ
eurjchem-966	185	19	shown	show	VERB
eurjchem-966	185	20	in	in	ADP
eurjchem-966	185	21	table	table	NOUN
eurjchem-966	185	22	1	1	NUM
eurjchem-966	185	23	.	.	X
eurjchem-966	185	24	4.6	4.6	NUM
eurjchem-966	185	25	.	.	PUNCT
eurjchem-966	186	1	detection	detection	NOUN
eurjchem-966	186	2	and	and	CCONJ
eurjchem-966	186	3	quantitation	quantitation	NOUN
eurjchem-966	186	4	limits	limit	NOUN
eurjchem-966	186	5	for	for	ADP
eurjchem-966	186	6	spectrophotometric	spectrophotometric	ADJ
eurjchem-966	186	7	methods	method	NOUN
eurjchem-966	186	8	(	(	PUNCT
eurjchem-966	186	9	1dd	1dd	ADJ
eurjchem-966	186	10	and	and	CCONJ
eurjchem-966	186	11	mcr	mcr	PROPN
eurjchem-966	186	12	)	)	PUNCT
eurjchem-966	186	13	,	,	PUNCT
eurjchem-966	186	14	the	the	DET
eurjchem-966	186	15	approach	approach	NOUN
eurjchem-966	186	16	based	base	VERB
eurjchem-966	186	17	on	on	ADP
eurjchem-966	186	18	the	the	DET
eurjchem-966	186	19	standard	standard	ADJ
eurjchem-966	186	20	deviation	deviation	NOUN
eurjchem-966	186	21	of	of	ADP
eurjchem-966	186	22	the	the	DET
eurjchem-966	186	23	response	response	NOUN
eurjchem-966	186	24	and	and	CCONJ
eurjchem-966	186	25	the	the	DET
eurjchem-966	186	26	slope	slope	NOUN
eurjchem-966	186	27	was	be	AUX
eurjchem-966	186	28	used	use	VERB
eurjchem-966	186	29	for	for	ADP
eurjchem-966	186	30	determining	determine	VERB
eurjchem-966	186	31	the	the	DET
eurjchem-966	186	32	detection	detection	NOUN
eurjchem-966	186	33	and	and	CCONJ
eurjchem-966	186	34	quantitation	quantitation	NOUN
eurjchem-966	186	35	limits	limit	NOUN
eurjchem-966	186	36	,	,	PUNCT
eurjchem-966	186	37	table	table	NOUN
eurjchem-966	186	38	3	3	NUM
eurjchem-966	186	39	.	.	PUNCT
eurjchem-966	187	1	lod	lod	PROPN
eurjchem-966	187	2	=	=	PUNCT
eurjchem-966	187	3	3.3	3.3	NUM
eurjchem-966	187	4	x	x	SYM
eurjchem-966	187	5	sd	sd	NOUN
eurjchem-966	187	6	/	/	SYM
eurjchem-966	187	7	slope	slope	NOUN
eurjchem-966	187	8	[	[	X
eurjchem-966	187	9	20	20	NUM
eurjchem-966	187	10	]	]	PUNCT
eurjchem-966	187	11	(	(	PUNCT
eurjchem-966	187	12	4	4	X
eurjchem-966	187	13	)	)	PUNCT
eurjchem-966	187	14	loq	loq	NOUN
eurjchem-966	187	15	=	=	PUNCT
eurjchem-966	187	16	10	10	NUM
eurjchem-966	187	17	x	x	SYM
eurjchem-966	187	18	sd	sd	NOUN
eurjchem-966	187	19	/	/	SYM
eurjchem-966	187	20	slope	slope	NOUN
eurjchem-966	187	21	[	[	X
eurjchem-966	187	22	20	20	NUM
eurjchem-966	187	23	]	]	PUNCT
eurjchem-966	187	24	(	(	PUNCT
eurjchem-966	187	25	5	5	NUM
eurjchem-966	187	26	)	)	PUNCT
eurjchem-966	187	27	for	for	ADP
eurjchem-966	187	28	hptlc	hptlc	NOUN
eurjchem-966	187	29	method	method	NOUN
eurjchem-966	187	30	,	,	PUNCT
eurjchem-966	187	31	as	as	SCONJ
eurjchem-966	187	32	it	it	PRON
eurjchem-966	187	33	exhibits	exhibit	VERB
eurjchem-966	187	34	baseline	baseline	NOUN
eurjchem-966	187	35	noise	noise	NOUN
eurjchem-966	187	36	,	,	PUNCT
eurjchem-966	187	37	the	the	DET
eurjchem-966	187	38	detection	detection	NOUN
eurjchem-966	187	39	limit	limit	NOUN
eurjchem-966	187	40	is	be	AUX
eurjchem-966	187	41	determined	determine	VERB
eurjchem-966	187	42	by	by	ADP
eurjchem-966	187	43	signal‐to‐noise	signal‐to‐noise	NOUN
eurjchem-966	187	44	ratio	ratio	NOUN
eurjchem-966	187	45	.	.	PUNCT
eurjchem-966	188	1	determination	determination	NOUN
eurjchem-966	188	2	of	of	ADP
eurjchem-966	188	3	signal‐	signal‐	PROPN
eurjchem-966	188	4	to‐noise	to‐noise	PROPN
eurjchem-966	188	5	ratio	ratio	NOUN
eurjchem-966	188	6	is	be	AUX
eurjchem-966	188	7	made	make	VERB
eurjchem-966	188	8	by	by	ADP
eurjchem-966	188	9	comparing	compare	VERB
eurjchem-966	188	10	the	the	DET
eurjchem-966	188	11	measured	measure	VERB
eurjchem-966	188	12	signals	signal	NOUN
eurjchem-966	188	13	of	of	ADP
eurjchem-966	188	14	samples	sample	NOUN
eurjchem-966	188	15	with	with	ADP
eurjchem-966	188	16	known	know	VERB
eurjchem-966	188	17	low	low	ADJ
eurjchem-966	188	18	concentrations	concentration	NOUN
eurjchem-966	188	19	of	of	ADP
eurjchem-966	188	20	analyte	analyte	NOUN
eurjchem-966	188	21	with	with	ADP
eurjchem-966	188	22	those	those	PRON
eurjchem-966	188	23	of	of	ADP
eurjchem-966	188	24	blank	blank	ADJ
eurjchem-966	188	25	samples	sample	NOUN
eurjchem-966	188	26	.	.	PUNCT
eurjchem-966	189	1	for	for	ADP
eurjchem-966	189	2	detection	detection	NOUN
eurjchem-966	189	3	limit	limit	NOUN
eurjchem-966	189	4	,	,	PUNCT
eurjchem-966	189	5	determine	determine	VERB
eurjchem-966	189	6	the	the	DET
eurjchem-966	189	7	minimum	minimum	ADJ
eurjchem-966	189	8	concentration	concentration	NOUN
eurjchem-966	189	9	at	at	ADP
eurjchem-966	189	10	which	which	PRON
eurjchem-966	189	11	the	the	DET
eurjchem-966	189	12	analyte	analyte	NOUN
eurjchem-966	189	13	can	can	AUX
eurjchem-966	189	14	be	be	AUX
eurjchem-966	189	15	detected	detect	VERB
eurjchem-966	189	16	.	.	PUNCT
eurjchem-966	190	1	for	for	ADP
eurjchem-966	190	2	quantitation	quantitation	NOUN
eurjchem-966	190	3	limit	limit	NOUN
eurjchem-966	190	4	,	,	PUNCT
eurjchem-966	190	5	determine	determine	VERB
eurjchem-966	190	6	the	the	DET
eurjchem-966	190	7	minimum	minimum	ADJ
eurjchem-966	190	8	concentration	concentration	NOUN
eurjchem-966	190	9	at	at	ADP
eurjchem-966	190	10	which	which	PRON
eurjchem-966	190	11	the	the	DET
eurjchem-966	190	12	analyte	analyte	NOUN
eurjchem-966	190	13	can	can	AUX
eurjchem-966	190	14	be	be	AUX
eurjchem-966	190	15	quantified	quantify	VERB
eurjchem-966	190	16	[	[	PUNCT
eurjchem-966	190	17	20	20	NUM
eurjchem-966	190	18	]	]	PUNCT
eurjchem-966	190	19	.	.	PUNCT
eurjchem-966	191	1	acceptable	acceptable	ADJ
eurjchem-966	191	2	detection	detection	NOUN
eurjchem-966	191	3	and	and	CCONJ
eurjchem-966	191	4	quantitation	quantitation	NOUN
eurjchem-966	191	5	limits	limit	NOUN
eurjchem-966	191	6	are	be	AUX
eurjchem-966	191	7	shown	show	VERB
eurjchem-966	191	8	in	in	ADP
eurjchem-966	191	9	table	table	NOUN
eurjchem-966	191	10	3	3	NUM
eurjchem-966	191	11	.	.	PUNCT
eurjchem-966	191	12	4.7	4.7	NUM
eurjchem-966	191	13	.	.	PUNCT
eurjchem-966	192	1	robustness	robustness	VERB
eurjchem-966	192	2	the	the	DET
eurjchem-966	192	3	robustness	robustness	NOUN
eurjchem-966	192	4	of	of	ADP
eurjchem-966	192	5	an	an	DET
eurjchem-966	192	6	analytical	analytical	ADJ
eurjchem-966	192	7	procedure	procedure	NOUN
eurjchem-966	192	8	is	be	AUX
eurjchem-966	192	9	a	a	DET
eurjchem-966	192	10	measure	measure	NOUN
eurjchem-966	192	11	of	of	ADP
eurjchem-966	192	12	its	its	PRON
eurjchem-966	192	13	capacity	capacity	NOUN
eurjchem-966	192	14	to	to	PART
eurjchem-966	192	15	remain	remain	VERB
eurjchem-966	192	16	unaffected	unaffected	ADJ
eurjchem-966	192	17	by	by	ADP
eurjchem-966	192	18	small	small	ADJ
eurjchem-966	192	19	deliberate	deliberate	ADJ
eurjchem-966	192	20	variations	variation	NOUN
eurjchem-966	192	21	in	in	ADP
eurjchem-966	192	22	method	method	NOUN
eurjchem-966	192	23	parameters	parameter	NOUN
eurjchem-966	192	24	and	and	CCONJ
eurjchem-966	192	25	provides	provide	VERB
eurjchem-966	192	26	an	an	DET
eurjchem-966	192	27	indication	indication	NOUN
eurjchem-966	192	28	of	of	ADP
eurjchem-966	192	29	its	its	PRON
eurjchem-966	192	30	reliability	reliability	NOUN
eurjchem-966	192	31	during	during	ADP
eurjchem-966	192	32	normal	normal	ADJ
eurjchem-966	192	33	usage	usage	NOUN
eurjchem-966	192	34	.	.	PUNCT
eurjchem-966	193	1	for	for	ADP
eurjchem-966	193	2	hptlc	hptlc	NOUN
eurjchem-966	193	3	method	method	NOUN
eurjchem-966	193	4	,	,	PUNCT
eurjchem-966	193	5	the	the	DET
eurjchem-966	193	6	organic	organic	ADJ
eurjchem-966	193	7	strength	strength	NOUN
eurjchem-966	193	8	of	of	ADP
eurjchem-966	193	9	the	the	DET
eurjchem-966	193	10	developing	develop	VERB
eurjchem-966	193	11	system	system	NOUN
eurjchem-966	193	12	was	be	AUX
eurjchem-966	193	13	deliberately	deliberately	ADV
eurjchem-966	193	14	changed	change	VERB
eurjchem-966	193	15	by	by	ADP
eurjchem-966	193	16	±0.5	±0.5	PROPN
eurjchem-966	193	17	ml	ml	ADV
eurjchem-966	194	1	and	and	CCONJ
eurjchem-966	194	2	it	it	PRON
eurjchem-966	194	3	has	have	VERB
eurjchem-966	194	4	no	no	DET
eurjchem-966	194	5	significant	significant	ADJ
eurjchem-966	194	6	effect	effect	NOUN
eurjchem-966	194	7	on	on	ADP
eurjchem-966	194	8	rf	rf	NOUN
eurjchem-966	194	9	values	value	NOUN
eurjchem-966	194	10	or	or	CCONJ
eurjchem-966	194	11	symmetry	symmetry	NOUN
eurjchem-966	194	12	of	of	ADP
eurjchem-966	194	13	the	the	DET
eurjchem-966	194	14	peaks	peak	NOUN
eurjchem-966	194	15	as	as	SCONJ
eurjchem-966	194	16	shown	show	VERB
eurjchem-966	194	17	in	in	ADP
eurjchem-966	194	18	table	table	NOUN
eurjchem-966	194	19	3	3	NUM
eurjchem-966	194	20	.	.	PUNCT
eurjchem-966	195	1	however	however	ADV
eurjchem-966	195	2	,	,	PUNCT
eurjchem-966	195	3	small	small	ADJ
eurjchem-966	195	4	changes	change	NOUN
eurjchem-966	195	5	in	in	ADP
eurjchem-966	195	6	the	the	DET
eurjchem-966	195	7	volume	volume	NOUN
eurjchem-966	195	8	of	of	ADP
eurjchem-966	195	9	glacial	glacial	ADJ
eurjchem-966	195	10	acetic	acetic	ADJ
eurjchem-966	195	11	acid	acid	NOUN
eurjchem-966	195	12	greatly	greatly	ADV
eurjchem-966	195	13	affect	affect	VERB
eurjchem-966	195	14	separation	separation	NOUN
eurjchem-966	195	15	of	of	ADP
eurjchem-966	195	16	deg	deg	PROPN
eurjchem-966	195	17	.	.	PROPN
eurjchem-966	196	1	4.8	4.8	NUM
eurjchem-966	196	2	.	.	PUNCT
eurjchem-966	197	1	system	system	NOUN
eurjchem-966	197	2	suitability	suitability	NOUN
eurjchem-966	197	3	ich	ich	NOUN
eurjchem-966	197	4	states	state	VERB
eurjchem-966	197	5	that	that	SCONJ
eurjchem-966	197	6	system	system	NOUN
eurjchem-966	197	7	suitability	suitability	NOUN
eurjchem-966	197	8	tests	test	NOUN
eurjchem-966	197	9	are	be	AUX
eurjchem-966	197	10	an	an	DET
eurjchem-966	197	11	integral	integral	ADJ
eurjchem-966	197	12	part	part	NOUN
eurjchem-966	197	13	of	of	ADP
eurjchem-966	197	14	many	many	ADJ
eurjchem-966	197	15	analytical	analytical	ADJ
eurjchem-966	197	16	methods	method	NOUN
eurjchem-966	197	17	,	,	PUNCT
eurjchem-966	197	18	especially	especially	ADV
eurjchem-966	197	19	liquid	liquid	ADJ
eurjchem-966	197	20	chromatographic	chromatographic	ADJ
eurjchem-966	197	21	methods	method	NOUN
eurjchem-966	197	22	.	.	PUNCT
eurjchem-966	198	1	they	they	PRON
eurjchem-966	198	2	are	be	AUX
eurjchem-966	198	3	used	use	VERB
eurjchem-966	198	4	to	to	PART
eurjchem-966	198	5	verify	verify	VERB
eurjchem-966	198	6	that	that	SCONJ
eurjchem-966	198	7	the	the	DET
eurjchem-966	198	8	resolution	resolution	NOUN
eurjchem-966	198	9	and	and	CCONJ
eurjchem-966	198	10	reproducibility	reproducibility	NOUN
eurjchem-966	198	11	of	of	ADP
eurjchem-966	198	12	the	the	DET
eurjchem-966	198	13	chromatographic	chromatographic	ADJ
eurjchem-966	198	14	system	system	NOUN
eurjchem-966	198	15	are	be	AUX
eurjchem-966	198	16	adequate	adequate	ADJ
eurjchem-966	198	17	for	for	SCONJ
eurjchem-966	198	18	the	the	DET
eurjchem-966	198	19	analysis	analysis	NOUN
eurjchem-966	198	20	to	to	PART
eurjchem-966	198	21	be	be	AUX
eurjchem-966	198	22	done	do	VERB
eurjchem-966	198	23	.	.	PUNCT
eurjchem-966	199	1	parameters	parameter	NOUN
eurjchem-966	199	2	including	include	VERB
eurjchem-966	199	3	resolution	resolution	NOUN
eurjchem-966	199	4	(	(	PUNCT
eurjchem-966	199	5	rs	rs	NOUN
eurjchem-966	199	6	)	)	PUNCT
eurjchem-966	199	7	,	,	PUNCT
eurjchem-966	199	8	capacity	capacity	NOUN
eurjchem-966	199	9	factor	factor	NOUN
eurjchem-966	199	10	(	(	PUNCT
eurjchem-966	199	11	k	k	NOUN
eurjchem-966	199	12	'	'	PUNCT
eurjchem-966	199	13	)	)	PUNCT
eurjchem-966	199	14	,	,	PUNCT
eurjchem-966	199	15	peak	peak	NOUN
eurjchem-966	199	16	symmetry	symmetry	NOUN
eurjchem-966	199	17	and	and	CCONJ
eurjchem-966	199	18	selectivity	selectivity	NOUN
eurjchem-966	199	19	factor	factor	NOUN
eurjchem-966	199	20	(	(	PUNCT
eurjchem-966	199	21	α	α	NOUN
eurjchem-966	199	22	)	)	PUNCT
eurjchem-966	199	23	were	be	AUX
eurjchem-966	199	24	calculated	calculate	VERB
eurjchem-966	199	25	as	as	SCONJ
eurjchem-966	199	26	shown	show	VERB
eurjchem-966	199	27	in	in	ADP
eurjchem-966	199	28	table	table	NOUN
eurjchem-966	199	29	4	4	NUM
eurjchem-966	199	30	.	.	PUNCT
eurjchem-966	200	1	the	the	DET
eurjchem-966	200	2	results	result	NOUN
eurjchem-966	200	3	obtained	obtain	VERB
eurjchem-966	200	4	by	by	ADP
eurjchem-966	200	5	the	the	DET
eurjchem-966	200	6	proposed	propose	VERB
eurjchem-966	200	7	methods	method	NOUN
eurjchem-966	200	8	were	be	AUX
eurjchem-966	200	9	statistically	statistically	ADV
eurjchem-966	200	10	compared	compare	VERB
eurjchem-966	200	11	with	with	ADP
eurjchem-966	200	12	those	those	PRON
eurjchem-966	200	13	obtained	obtain	VERB
eurjchem-966	200	14	by	by	ADP
eurjchem-966	200	15	the	the	DET
eurjchem-966	200	16	reported	report	VERB
eurjchem-966	200	17	hplc	hplc	NOUN
eurjchem-966	200	18	method	method	NOUN
eurjchem-966	200	19	using	use	VERB
eurjchem-966	200	20	t‐	t‐	ADJ
eurjchem-966	200	21	and	and	CCONJ
eurjchem-966	200	22	f‐	f‐	NOUN
eurjchem-966	200	23	tests	test	NOUN
eurjchem-966	200	24	.	.	PUNCT
eurjchem-966	201	1	the	the	DET
eurjchem-966	201	2	values	value	NOUN
eurjchem-966	201	3	obtained	obtain	VERB
eurjchem-966	201	4	are	be	AUX
eurjchem-966	201	5	less	less	ADJ
eurjchem-966	201	6	than	than	ADP
eurjchem-966	201	7	the	the	DET
eurjchem-966	201	8	theoretical	theoretical	ADJ
eurjchem-966	201	9	ones	one	NOUN
eurjchem-966	201	10	indicating	indicate	VERB
eurjchem-966	201	11	that	that	SCONJ
eurjchem-966	201	12	there	there	PRON
eurjchem-966	201	13	is	be	VERB
eurjchem-966	201	14	no	no	DET
eurjchem-966	201	15	significant	significant	ADJ
eurjchem-966	201	16	difference	difference	NOUN
eurjchem-966	201	17	between	between	ADP
eurjchem-966	201	18	the	the	DET
eurjchem-966	201	19	proposed	propose	VERB
eurjchem-966	201	20	methods	method	NOUN
eurjchem-966	201	21	and	and	CCONJ
eurjchem-966	201	22	the	the	DET
eurjchem-966	201	23	reported	report	VERB
eurjchem-966	201	24	hplc	hplc	NOUN
eurjchem-966	201	25	method	method	NOUN
eurjchem-966	201	26	with	with	ADP
eurjchem-966	201	27	respect	respect	NOUN
eurjchem-966	201	28	to	to	ADP
eurjchem-966	201	29	accuracy	accuracy	NOUN
eurjchem-966	201	30	and	and	CCONJ
eurjchem-966	201	31	precision	precision	NOUN
eurjchem-966	201	32	,	,	PUNCT
eurjchem-966	201	33	table	table	NOUN
eurjchem-966	201	34	5	5	NUM
eurjchem-966	201	35	.	.	NOUN
eurjchem-966	201	36	5	5	NUM
eurjchem-966	201	37	.	.	X
eurjchem-966	201	38	conclusion	conclusion	NOUN
eurjchem-966	201	39	the	the	DET
eurjchem-966	201	40	present	present	ADJ
eurjchem-966	201	41	work	work	NOUN
eurjchem-966	201	42	introduces	introduce	VERB
eurjchem-966	201	43	simple	simple	ADJ
eurjchem-966	201	44	,	,	PUNCT
eurjchem-966	201	45	sensitive	sensitive	ADJ
eurjchem-966	201	46	and	and	CCONJ
eurjchem-966	201	47	rapid	rapid	ADJ
eurjchem-966	201	48	methods	method	NOUN
eurjchem-966	201	49	that	that	PRON
eurjchem-966	201	50	are	be	AUX
eurjchem-966	201	51	performed	perform	VERB
eurjchem-966	201	52	to	to	PART
eurjchem-966	201	53	determine	determine	VERB
eurjchem-966	201	54	acm	acm	NOUN
eurjchem-966	201	55	in	in	ADP
eurjchem-966	201	56	pure	pure	ADJ
eurjchem-966	201	57	form	form	NOUN
eurjchem-966	201	58	and	and	CCONJ
eurjchem-966	201	59	in	in	ADP
eurjchem-966	201	60	pharmaceutical	pharmaceutical	ADJ
eurjchem-966	201	61	preparation	preparation	NOUN
eurjchem-966	201	62	.	.	PUNCT
eurjchem-966	202	1	the	the	DET
eurjchem-966	202	2	spectrophotometric	spectrophotometric	ADJ
eurjchem-966	202	3	methods	method	NOUN
eurjchem-966	202	4	are	be	AUX
eurjchem-966	202	5	simple	simple	ADJ
eurjchem-966	202	6	,	,	PUNCT
eurjchem-966	202	7	less	less	ADJ
eurjchem-966	202	8	time	time	NOUN
eurjchem-966	202	9	consuming	consume	VERB
eurjchem-966	202	10	and	and	CCONJ
eurjchem-966	202	11	economic	economic	ADJ
eurjchem-966	202	12	stability	stability	NOUN
eurjchem-966	202	13	indicating	indicate	VERB
eurjchem-966	202	14	method	method	NOUN
eurjchem-966	202	15	compared	compare	VERB
eurjchem-966	202	16	to	to	ADP
eurjchem-966	202	17	published	publish	VERB
eurjchem-966	202	18	lc	lc	NOUN
eurjchem-966	202	19	methods	method	NOUN
eurjchem-966	202	20	.	.	PUNCT
eurjchem-966	203	1	compared	compare	VERB
eurjchem-966	203	2	to	to	ADP
eurjchem-966	203	3	the	the	DET
eurjchem-966	203	4	derivative	derivative	ADJ
eurjchem-966	203	5	method	method	NOUN
eurjchem-966	203	6	,	,	PUNCT
eurjchem-966	203	7	mcr	mcr	PROPN
eurjchem-966	203	8	eliminates	eliminate	VERB
eurjchem-966	203	9	the	the	DET
eurjchem-966	203	10	derivative	derivative	ADJ
eurjchem-966	203	11	step	step	NOUN
eurjchem-966	203	12	and	and	CCONJ
eurjchem-966	203	13	so	so	ADV
eurjchem-966	203	14	the	the	DET
eurjchem-966	203	15	signal‐to‐noise	signal‐to‐noise	NOUN
eurjchem-966	203	16	ratio	ratio	NOUN
eurjchem-966	203	17	is	be	AUX
eurjchem-966	203	18	enhanced	enhance	VERB
eurjchem-966	203	19	.	.	PUNCT
eurjchem-966	204	1	moreover	moreover	ADV
eurjchem-966	204	2	,	,	PUNCT
eurjchem-966	204	3	it	it	PRON
eurjchem-966	204	4	was	be	AUX
eurjchem-966	204	5	more	more	ADV
eurjchem-966	204	6	selective	selective	ADJ
eurjchem-966	204	7	than	than	ADP
eurjchem-966	204	8	the	the	DET
eurjchem-966	204	9	1dd	1dd	ADJ
eurjchem-966	204	10	spectrophoto‐	spectrophoto‐	NOUN
eurjchem-966	204	11	metric	metric	ADJ
eurjchem-966	204	12	method	method	NOUN
eurjchem-966	204	13	.	.	PUNCT
eurjchem-966	205	1	the	the	DET
eurjchem-966	205	2	hptlc	hptlc	NOUN
eurjchem-966	205	3	method	method	NOUN
eurjchem-966	205	4	has	have	VERB
eurjchem-966	205	5	the	the	DET
eurjchem-966	205	6	advantage	advantage	NOUN
eurjchem-966	205	7	that	that	SCONJ
eurjchem-966	205	8	several	several	ADJ
eurjchem-966	205	9	samples	sample	NOUN
eurjchem-966	205	10	can	can	AUX
eurjchem-966	205	11	be	be	AUX
eurjchem-966	205	12	run	run	VERB
eurjchem-966	205	13	simultaneously	simultaneously	ADV
eurjchem-966	205	14	using	use	VERB
eurjchem-966	205	15	a	a	DET
eurjchem-966	205	16	small	small	ADJ
eurjchem-966	205	17	quantity	quantity	NOUN
eurjchem-966	205	18	of	of	ADP
eurjchem-966	205	19	developing	develop	VERB
eurjchem-966	205	20	system	system	NOUN
eurjchem-966	205	21	.	.	PUNCT
eurjchem-966	206	1	it	it	PRON
eurjchem-966	206	2	can	can	AUX
eurjchem-966	206	3	provide	provide	VERB
eurjchem-966	206	4	high	high	ADJ
eurjchem-966	206	5	sensitivity	sensitivity	NOUN
eurjchem-966	206	6	and	and	CCONJ
eurjchem-966	206	7	selectivity	selectivity	NOUN
eurjchem-966	206	8	,	,	PUNCT
eurjchem-966	206	9	in	in	ADP
eurjchem-966	206	10	addition	addition	NOUN
eurjchem-966	206	11	to	to	ADP
eurjchem-966	206	12	separation	separation	NOUN
eurjchem-966	206	13	of	of	ADP
eurjchem-966	206	14	acm	acm	PROPN
eurjchem-966	206	15	from	from	ADP
eurjchem-966	206	16	deg	deg	PROPN
eurjchem-966	206	17	.	.	PUNCT
eurjchem-966	207	1	the	the	DET
eurjchem-966	207	2	proposed	propose	VERB
eurjchem-966	207	3	methods	method	NOUN
eurjchem-966	207	4	showed	show	VERB
eurjchem-966	207	5	high	high	ADJ
eurjchem-966	207	6	sensitivity	sensitivity	NOUN
eurjchem-966	207	7	,	,	PUNCT
eurjchem-966	207	8	accuracy	accuracy	NOUN
eurjchem-966	207	9	,	,	PUNCT
eurjchem-966	207	10	reproducibility	reproducibility	NOUN
eurjchem-966	207	11	and	and	CCONJ
eurjchem-966	207	12	selectivity	selectivity	NOUN
eurjchem-966	207	13	.	.	PUNCT
eurjchem-966	208	1	moreover	moreover	ADV
eurjchem-966	208	2	,	,	PUNCT
eurjchem-966	208	3	these	these	DET
eurjchem-966	208	4	methods	method	NOUN
eurjchem-966	208	5	can	can	AUX
eurjchem-966	208	6	be	be	AUX
eurjchem-966	208	7	used	use	VERB
eurjchem-966	208	8	as	as	ADP
eurjchem-966	208	9	stability	stability	NOUN
eurjchem-966	208	10	indicating	indicate	VERB
eurjchem-966	208	11	methods	method	NOUN
eurjchem-966	208	12	.	.	PUNCT
eurjchem-966	209	1	these	these	DET
eurjchem-966	209	2	merits	merit	NOUN
eurjchem-966	209	3	suggest	suggest	VERB
eurjchem-966	209	4	the	the	DET
eurjchem-966	209	5	use	use	NOUN
eurjchem-966	209	6	of	of	ADP
eurjchem-966	209	7	the	the	DET
eurjchem-966	209	8	proposed	propose	VERB
eurjchem-966	209	9	methods	method	NOUN
eurjchem-966	209	10	in	in	ADP
eurjchem-966	209	11	routine	routine	ADJ
eurjchem-966	209	12	and	and	CCONJ
eurjchem-966	209	13	quality	quality	NOUN
eurjchem-966	209	14	control	control	NOUN
eurjchem-966	209	15	analysis	analysis	NOUN
eurjchem-966	209	16	without	without	ADP
eurjchem-966	209	17	interference	interference	NOUN
eurjchem-966	209	18	of	of	ADP
eurjchem-966	209	19	commonly	commonly	ADV
eurjchem-966	209	20	encountered	encounter	VERB
eurjchem-966	209	21	pharmaceutical	pharmaceutical	ADJ
eurjchem-966	209	22	preparation	preparation	NOUN
eurjchem-966	209	23	additives	additive	NOUN
eurjchem-966	209	24	.	.	PUNCT
eurjchem-966	210	1	references	reference	NOUN
eurjchem-966	210	2	[	[	X
eurjchem-966	210	3	1	1	NUM
eurjchem-966	210	4	]	]	PUNCT
eurjchem-966	210	5	.	.	PUNCT
eurjchem-966	211	1	maryedele	maryedele	PROPN
eurjchem-966	211	2	,	,	PUNCT
eurjchem-966	211	3	j.	j.	PROPN
eurjchem-966	211	4	o’neil	o’neil	PROPN
eurjchem-966	211	5	,	,	PUNCT
eurjchem-966	211	6	the	the	DET
eurjchem-966	211	7	merck	merck	PROPN
eurjchem-966	211	8	index	index	PROPN
eurjchem-966	211	9	,	,	PUNCT
eurjchem-966	211	10	an	an	DET
eurjchem-966	211	11	encyclopedia	encyclopedia	NOUN
eurjchem-966	211	12	of	of	ADP
eurjchem-966	211	13	chemicals	chemical	NOUN
eurjchem-966	211	14	,	,	PUNCT
eurjchem-966	211	15	drugs	drug	NOUN
eurjchem-966	211	16	and	and	CCONJ
eurjchem-966	211	17	biologicals	biological	NOUN
eurjchem-966	211	18	,	,	PUNCT
eurjchem-966	211	19	14th	14th	ADJ
eurjchem-966	211	20	ed	ed	NOUN
eurjchem-966	211	21	.	.	PROPN
eurjchem-966	211	22	,	,	PUNCT
eurjchem-966	211	23	merck	merck	PROPN
eurjchem-966	211	24	and	and	CCONJ
eurjchem-966	211	25	co.	co.	PROPN
eurjchem-966	211	26	inc	inc	PROPN
eurjchem-966	211	27	.	.	PROPN
eurjchem-966	211	28	,	,	PUNCT
eurjchem-966	211	29	whitehouse	whitehouse	NOUN
eurjchem-966	211	30	station	station	NOUN
eurjchem-966	211	31	,	,	PUNCT
eurjchem-966	211	32	nj	nj	PROPN
eurjchem-966	211	33	,	,	PUNCT
eurjchem-966	211	34	usa	usa	PROPN
eurjchem-966	211	35	.	.	PUNCT
eurjchem-966	212	1	[	[	X
eurjchem-966	212	2	2	2	NUM
eurjchem-966	212	3	]	]	PUNCT
eurjchem-966	212	4	.	.	PUNCT
eurjchem-966	213	1	reynolds	reynolds	PROPN
eurjchem-966	213	2	,	,	PUNCT
eurjchem-966	213	3	j.	j.	PROPN
eurjchem-966	213	4	e.	e.	PROPN
eurjchem-966	213	5	f.	f.	PROPN
eurjchem-966	213	6	,	,	PUNCT
eurjchem-966	213	7	martindale	martindale	PROPN
eurjchem-966	213	8	,	,	PUNCT
eurjchem-966	213	9	the	the	DET
eurjchem-966	213	10	extra	extra	ADJ
eurjchem-966	213	11	pharmacopoeia	pharmacopoeia	NOUN
eurjchem-966	213	12	.	.	PUNCT
eurjchem-966	214	1	thirsty‐first	thirsty‐first	PROPN
eurjchem-966	215	1	ed	ed	NOUN
eurjchem-966	215	2	.	.	PUNCT
eurjchem-966	215	3	;	;	PUNCT
eurjchem-966	215	4	royal	royal	PROPN
eurjchem-966	215	5	pharmaceutica	pharmaceutica	PROPN
eurjchem-966	215	6	society	society	NOUN
eurjchem-966	215	7	:	:	PUNCT
eurjchem-966	215	8	london	london	PROPN
eurjchem-966	215	9	,	,	PUNCT
eurjchem-966	215	10	1996	1996	NUM
eurjchem-966	215	11	.	.	PUNCT
eurjchem-966	216	1	226	226	NUM
eurjchem-966	216	2	naguib	naguib	NOUN
eurjchem-966	216	3	et	et	PROPN
eurjchem-966	216	4	al	al	PROPN
eurjchem-966	216	5	.	.	PUNCT
eurjchem-966	216	6	/	/	SYM
eurjchem-966	216	7	european	european	PROPN
eurjchem-966	216	8	journal	journal	PROPN
eurjchem-966	216	9	of	of	ADP
eurjchem-966	216	10	chemistry	chemistry	NOUN
eurjchem-966	216	11	5	5	NUM
eurjchem-966	216	12	(	(	PUNCT
eurjchem-966	216	13	2	2	NUM
eurjchem-966	216	14	)	)	PUNCT
eurjchem-966	216	15	(	(	PUNCT
eurjchem-966	216	16	2014	2014	NUM
eurjchem-966	216	17	)	)	PUNCT
eurjchem-966	216	18	219‐226	219‐226	NUM
eurjchem-966	217	1	[	[	X
eurjchem-966	217	2	3	3	NUM
eurjchem-966	217	3	]	]	PUNCT
eurjchem-966	217	4	.	.	PUNCT
eurjchem-966	218	1	li	li	PROPN
eurjchem-966	218	2	,	,	PUNCT
eurjchem-966	218	3	d.	d.	PROPN
eurjchem-966	218	4	m.	m.	PROPN
eurjchem-966	218	5	;	;	PUNCT
eurjchem-966	218	6	lu	lu	PROPN
eurjchem-966	218	7	,	,	PUNCT
eurjchem-966	218	8	w.	w.	PROPN
eurjchem-966	218	9	l.	l.	PROPN
eurjchem-966	218	10	;	;	PUNCT
eurjchem-966	218	11	wang	wang	PROPN
eurjchem-966	218	12	,	,	PUNCT
eurjchem-966	218	13	x.	x.	PROPN
eurjchem-966	218	14	q.	q.	PROPN
eurjchem-966	218	15	;	;	PUNCT
eurjchem-966	218	16	wang	wang	PROPN
eurjchem-966	218	17	,	,	PUNCT
eurjchem-966	218	18	j.	j.	PROPN
eurjchem-966	218	19	c.	c.	PROPN
eurjchem-966	218	20	;	;	PUNCT
eurjchem-966	218	21	zhang	zhang	PROPN
eurjchem-966	218	22	,	,	PUNCT
eurjchem-966	218	23	h.	h.	PROPN
eurjchem-966	218	24	;	;	PUNCT
eurjchem-966	218	25	zhang	zhang	PROPN
eurjchem-966	218	26	,	,	PUNCT
eurjchem-966	218	27	r.	r.	PROPN
eurjchem-966	218	28	j.	j.	PROPN
eurjchem-966	218	29	;	;	PUNCT
eurjchem-966	218	30	wang	wang	PROPN
eurjchem-966	218	31	,	,	PUNCT
eurjchem-966	218	32	g.l	g.l	PROPN
eurjchem-966	218	33	.	.	PROPN
eurjchem-966	218	34	;	;	PUNCT
eurjchem-966	218	35	zhang	zhang	PROPN
eurjchem-966	218	36	,	,	PUNCT
eurjchem-966	218	37	x.	x.	PROPN
eurjchem-966	218	38	;	;	PUNCT
eurjchem-966	218	39	zhang	zhang	PROPN
eurjchem-966	218	40	,	,	PUNCT
eurjchem-966	218	41	q.	q.	PROPN
eurjchem-966	218	42	j.	j.	PROPN
eurjchem-966	218	43	health	health	PROPN
eurjchem-966	218	44	sci	sci	PROPN
eurjchem-966	218	45	.	.	PROPN
eurjchem-966	218	46	2005	2005	NUM
eurjchem-966	218	47	,	,	PUNCT
eurjchem-966	218	48	51(3	51(3	NUM
eurjchem-966	218	49	)	)	PUNCT
eurjchem-966	218	50	,	,	PUNCT
eurjchem-966	218	51	308‐316	308‐316	NUM
eurjchem-966	218	52	.	.	PUNCT
eurjchem-966	219	1	[	[	X
eurjchem-966	219	2	4	4	NUM
eurjchem-966	219	3	]	]	PUNCT
eurjchem-966	219	4	.	.	PUNCT
eurjchem-966	220	1	ozbakan	ozbakan	PROPN
eurjchem-966	220	2	,	,	PUNCT
eurjchem-966	220	3	h.	h.	PROPN
eurjchem-966	220	4	;	;	PUNCT
eurjchem-966	220	5	palabiyik	palabiyik	NOUN
eurjchem-966	220	6	,	,	PUNCT
eurjchem-966	220	7	i.	i.	NOUN
eurjchem-966	220	8	m.	m.	NOUN
eurjchem-966	220	9	;	;	PUNCT
eurjchem-966	220	10	caglayan	caglayan	NOUN
eurjchem-966	220	11	,	,	PUNCT
eurjchem-966	220	12	m.	m.	NOUN
eurjchem-966	220	13	g.	g.	PROPN
eurjchem-966	220	14	;	;	PUNCT
eurjchem-966	220	15	feyyaz	feyyaz	ADJ
eurjchem-966	220	16	,	,	PUNCT
eurjchem-966	220	17	o.	o.	PROPN
eurjchem-966	220	18	turk	turk	PROPN
eurjchem-966	220	19	j.	j.	PROPN
eurjchem-966	220	20	pharm	pharm	PROPN
eurjchem-966	220	21	.	.	PUNCT
eurjchem-966	221	1	sci	sci	PROPN
eurjchem-966	221	2	.	.	PROPN
eurjchem-966	221	3	2009	2009	NUM
eurjchem-966	221	4	,	,	PUNCT
eurjchem-966	221	5	6(3	6(3	NUM
eurjchem-966	221	6	)	)	PUNCT
eurjchem-966	221	7	,	,	PUNCT
eurjchem-966	221	8	163‐176	163‐176	PROPN
eurjchem-966	221	9	.	.	PUNCT
eurjchem-966	222	1	[	[	X
eurjchem-966	222	2	5	5	NUM
eurjchem-966	222	3	]	]	PUNCT
eurjchem-966	222	4	.	.	PUNCT
eurjchem-966	223	1	escuder‐gilabert	escuder‐gilabert	PROPN
eurjchem-966	223	2	,	,	PUNCT
eurjchem-966	223	3	l.	l.	PROPN
eurjchem-966	223	4	;	;	PUNCT
eurjchem-966	223	5	martin‐biosca	martin‐biosca	PROPN
eurjchem-966	223	6	,	,	PUNCT
eurjchem-966	223	7	y.	y.	PROPN
eurjchem-966	223	8	;	;	PUNCT
eurjchem-966	223	9	sagrado	sagrado	PROPN
eurjchem-966	223	10	,	,	PUNCT
eurjchem-966	223	11	s.	s.	PROPN
eurjchem-966	223	12	;	;	PUNCT
eurjchem-966	223	13	villanueva‐	villanueva‐	NUM
eurjchem-966	223	14	camanas	camana	NOUN
eurjchem-966	223	15	,	,	PUNCT
eurjchem-966	223	16	r.	r.	PROPN
eurjchem-966	223	17	;	;	PUNCT
eurjchem-966	223	18	medina‐hernandez	medina‐hernandez	NOUN
eurjchem-966	223	19	,	,	PUNCT
eurjchem-966	223	20	m.	m.	NOUN
eurjchem-966	223	21	chromatographia	chromatographia	PROPN
eurjchem-966	223	22	2002	2002	NUM
eurjchem-966	223	23	,	,	PUNCT
eurjchem-966	223	24	55(5‐6	55(5‐6	NUM
eurjchem-966	223	25	)	)	PUNCT
eurjchem-966	223	26	,	,	PUNCT
eurjchem-966	223	27	283‐288	283‐288	NUM
eurjchem-966	223	28	.	.	PUNCT
eurjchem-966	224	1	[	[	X
eurjchem-966	224	2	6	6	NUM
eurjchem-966	224	3	]	]	PUNCT
eurjchem-966	224	4	.	.	PUNCT
eurjchem-966	225	1	castro	castro	PROPN
eurjchem-966	225	2	,	,	PUNCT
eurjchem-966	225	3	b.	b.	PROPN
eurjchem-966	225	4	;	;	PUNCT
eurjchem-966	225	5	gameiro	gameiro	PROPN
eurjchem-966	225	6	,	,	PUNCT
eurjchem-966	225	7	p.	p.	PROPN
eurjchem-966	225	8	;	;	PUNCT
eurjchem-966	225	9	lima	lima	PROPN
eurjchem-966	225	10	,	,	PUNCT
eurjchem-966	225	11	j.	j.	PROPN
eurjchem-966	225	12	l.	l.	PROPN
eurjchem-966	225	13	;	;	PUNCT
eurjchem-966	225	14	matos	matos	PROPN
eurjchem-966	225	15	,	,	PUNCT
eurjchem-966	225	16	c.	c.	NOUN
eurjchem-966	225	17	;	;	PUNCT
eurjchem-966	225	18	reis	reis	NOUN
eurjchem-966	225	19	,	,	PUNCT
eurjchem-966	225	20	s.	s.	PROPN
eurjchem-966	225	21	mater	mater	PROPN
eurjchem-966	225	22	.	.	PUNCT
eurjchem-966	226	1	sci	sci	PROPN
eurjchem-966	226	2	.	.	PUNCT
eurjchem-966	227	1	eng	eng	PROPN
eurjchem-966	227	2	.	.	PROPN
eurjchem-966	228	1	c	c	PROPN
eurjchem-966	228	2	2001	2001	NUM
eurjchem-966	228	3	,	,	PUNCT
eurjchem-966	228	4	18(1	18(1	NUM
eurjchem-966	228	5	)	)	PUNCT
eurjchem-966	228	6	,	,	PUNCT
eurjchem-966	228	7	71‐78	71‐78	X
eurjchem-966	228	8	.	.	PUNCT
eurjchem-966	229	1	[	[	X
eurjchem-966	229	2	7	7	NUM
eurjchem-966	229	3	]	]	PUNCT
eurjchem-966	229	4	.	.	PUNCT
eurjchem-966	229	5	arcos	arcos	PROPN
eurjchem-966	229	6	,	,	PUNCT
eurjchem-966	229	7	m.	m.	PROPN
eurjchem-966	229	8	j.	j.	PROPN
eurjchem-966	229	9	;	;	PUNCT
eurjchem-966	229	10	ortiz	ortiz	PROPN
eurjchem-966	229	11	,	,	PUNCT
eurjchem-966	229	12	m.	m.	PROPN
eurjchem-966	229	13	c.	c.	PROPN
eurjchem-966	229	14	;	;	PUNCT
eurjchem-966	229	15	villahoz	villahoz	PROPN
eurjchem-966	229	16	,	,	PUNCT
eurjchem-966	229	17	b.	b.	PROPN
eurjchem-966	229	18	n.	n.	PROPN
eurjchem-966	229	19	;	;	PUNCT
eurjchem-966	229	20	sarabia	sarabia	PROPN
eurjchem-966	229	21	,	,	PUNCT
eurjchem-966	229	22	l.	l.	PROPN
eurjchem-966	229	23	a.	a.	PROPN
eurjchem-966	229	24	anal	anal	PROPN
eurjchem-966	229	25	.	.	PUNCT
eurjchem-966	230	1	chim	chim	PROPN
eurjchem-966	230	2	.	.	PUNCT
eurjchem-966	231	1	acta	acta	PROPN
eurjchem-966	231	2	1997	1997	NUM
eurjchem-966	231	3	,	,	PUNCT
eurjchem-966	231	4	339(1	339(1	NUM
eurjchem-966	231	5	)	)	PUNCT
eurjchem-966	231	6	,	,	PUNCT
eurjchem-966	231	7	63‐77	63‐77	NUM
eurjchem-966	231	8	.	.	PUNCT
eurjchem-966	232	1	[	[	X
eurjchem-966	232	2	8	8	NUM
eurjchem-966	232	3	]	]	PUNCT
eurjchem-966	232	4	.	.	PUNCT
eurjchem-966	233	1	pang	pang	NOUN
eurjchem-966	233	2	,	,	PUNCT
eurjchem-966	233	3	j.	j.	PROPN
eurjchem-966	233	4	;	;	PUNCT
eurjchem-966	233	5	hengshan	hengshan	PROPN
eurjchem-966	233	6	,	,	PUNCT
eurjchem-966	233	7	t.	t.	PROPN
eurjchem-966	233	8	zhongguo	zhongguo	PROPN
eurjchem-966	233	9	yiyuan	yiyuan	PROPN
eurjchem-966	233	10	yaoxue	yaoxue	PROPN
eurjchem-966	233	11	zazhi	zazhi	PROPN
eurjchem-966	233	12	2004	2004	NUM
eurjchem-966	233	13	,	,	PUNCT
eurjchem-966	233	14	24(4	24(4	NUM
eurjchem-966	233	15	)	)	PUNCT
eurjchem-966	233	16	,	,	PUNCT
eurjchem-966	233	17	246‐247	246‐247	PROPN
eurjchem-966	233	18	.	.	PUNCT
eurjchem-966	234	1	[	[	X
eurjchem-966	234	2	9	9	NUM
eurjchem-966	234	3	]	]	PUNCT
eurjchem-966	234	4	.	.	PUNCT
eurjchem-966	235	1	shi	shi	PROPN
eurjchem-966	235	2	,	,	PUNCT
eurjchem-966	235	3	x.	x.	PROPN
eurjchem-966	235	4	;	;	PUNCT
eurjchem-966	235	5	chen	chen	PROPN
eurjchem-966	235	6	,	,	PUNCT
eurjchem-966	235	7	m.	m.	NOUN
eurjchem-966	235	8	;	;	PUNCT
eurjchem-966	235	9	zhang	zhang	PROPN
eurjchem-966	235	10	,	,	PUNCT
eurjchem-966	235	11	j.	j.	PROPN
eurjchem-966	235	12	;	;	PUNCT
eurjchem-966	235	13	zhang	zhang	PROPN
eurjchem-966	235	14	,	,	PUNCT
eurjchem-966	235	15	l.	l.	PROPN
eurjchem-966	235	16	;	;	PUNCT
eurjchem-966	235	17	wang	wang	PROPN
eurjchem-966	235	18	,	,	PUNCT
eurjchem-966	235	19	h.	h.	PROPN
eurjchem-966	235	20	zhongguo	zhongguo	PROPN
eurjchem-966	235	21	yiyao	yiyao	PROPN
eurjchem-966	235	22	zazhi	zazhi	PROPN
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eurjchem-966	235	24	,	,	PUNCT
eurjchem-966	235	25	32(10	32(10	NUM
eurjchem-966	235	26	)	)	PUNCT
eurjchem-966	235	27	,	,	PUNCT
eurjchem-966	235	28	454‐456	454‐456	PROPN
eurjchem-966	235	29	.	.	PUNCT
eurjchem-966	236	1	[	[	X
eurjchem-966	236	2	10	10	NUM
eurjchem-966	236	3	]	]	PUNCT
eurjchem-966	236	4	.	.	PUNCT
eurjchem-966	237	1	hu	hu	PROPN
eurjchem-966	237	2	,	,	PUNCT
eurjchem-966	237	3	y.	y.	PROPN
eurjchem-966	237	4	q.	q.	PROPN
eurjchem-966	237	5	;	;	PUNCT
eurjchem-966	237	6	liu	liu	PROPN
eurjchem-966	237	7	,	,	PUNCT
eurjchem-966	237	8	h.	h.	PROPN
eurjchem-966	237	9	c.	c.	PROPN
eurjchem-966	237	10	;	;	PUNCT
eurjchem-966	237	11	ma	ma	PROPN
eurjchem-966	237	12	,	,	PUNCT
eurjchem-966	237	13	r.	r.	PROPN
eurjchem-966	237	14	;	;	PUNCT
eurjchem-966	237	15	wang	wang	PROPN
eurjchem-966	237	16	,	,	PUNCT
eurjchem-966	237	17	j.	j.	PROPN
eurjchem-966	237	18	;	;	PUNCT
eurjchem-966	237	19	hou	hou	PROPN
eurjchem-966	237	20	,	,	PUNCT
eurjchem-966	237	21	y.	y.	PROPN
eurjchem-966	237	22	n.	n.	PROPN
eurjchem-966	237	23	se	se	PROPN
eurjchem-966	237	24	pu	pu	PROPN
eurjchem-966	237	25	1999	1999	NUM
eurjchem-966	237	26	,	,	PUNCT
eurjchem-966	237	27	17(6	17(6	NUM
eurjchem-966	237	28	)	)	PUNCT
eurjchem-966	237	29	,	,	PUNCT
eurjchem-966	237	30	586‐	586‐	NUM
eurjchem-966	237	31	587	587	NUM
eurjchem-966	237	32	.	.	PUNCT
eurjchem-966	238	1	[	[	X
eurjchem-966	238	2	11	11	NUM
eurjchem-966	238	3	]	]	PUNCT
eurjchem-966	238	4	.	.	PUNCT
eurjchem-966	239	1	reguera	reguera	NOUN
eurjchem-966	239	2	,	,	PUNCT
eurjchem-966	239	3	c.	c.	PROPN
eurjchem-966	239	4	;	;	PUNCT
eurjchem-966	239	5	julia	julia	PROPN
eurjchem-966	239	6	arcos	arcos	PROPN
eurjchem-966	239	7	,	,	PUNCT
eurjchem-966	239	8	m.	m.	NOUN
eurjchem-966	239	9	;	;	PUNCT
eurjchem-966	239	10	cruz	cruz	PROPN
eurjchem-966	239	11	ortiz	ortiz	PROPN
eurjchem-966	239	12	,	,	PUNCT
eurjchem-966	239	13	m.	m.	NOUN
eurjchem-966	239	14	talanta	talanta	PROPN
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eurjchem-966	239	16	,	,	PUNCT
eurjchem-966	239	17	46(6	46(6	NOUN
eurjchem-966	239	18	)	)	PUNCT
eurjchem-966	239	19	,	,	PUNCT
eurjchem-966	239	20	1493‐	1493‐	NUM
eurjchem-966	239	21	1505	1505	NUM
eurjchem-966	239	22	.	.	PUNCT
eurjchem-966	240	1	[	[	X
eurjchem-966	240	2	12	12	NUM
eurjchem-966	240	3	]	]	PUNCT
eurjchem-966	240	4	.	.	PUNCT
eurjchem-966	241	1	chavez‐pina	chavez‐pina	PROPN
eurjchem-966	241	2	,	,	PUNCT
eurjchem-966	241	3	w.	w.	PROPN
eurjchem-966	241	4	m.	m.	PROPN
eurjchem-966	241	5	;	;	PUNCT
eurjchem-966	241	6	dicay	dicay	PROPN
eurjchem-966	241	7	,	,	PUNCT
eurjchem-966	241	8	m.	m.	NOUN
eurjchem-966	241	9	;	;	PUNCT
eurjchem-966	241	10	castaneda‐hernandez	castaneda‐hernandez	PROPN
eurjchem-966	241	11	,	,	PUNCT
eurjchem-966	241	12	g.	g.	PROPN
eurjchem-966	241	13	;	;	PUNCT
eurjchem-966	241	14	wallace	wallace	PROPN
eurjchem-966	241	15	,	,	PUNCT
eurjchem-966	241	16	j.l	j.l	PROPN
eurjchem-966	241	17	.	.	PROPN
eurjchem-966	241	18	brit	brit	PROPN
eurjchem-966	241	19	.	.	PUNCT
eurjchem-966	242	1	j.	j.	PROPN
eurjchem-966	242	2	pharmacol	pharmacol	PROPN
eurjchem-966	242	3	.	.	PROPN
eurjchem-966	242	4	2007	2007	NUM
eurjchem-966	242	5	,	,	PUNCT
eurjchem-966	242	6	152(6	152(6	NUM
eurjchem-966	242	7	)	)	PUNCT
eurjchem-966	242	8	,	,	PUNCT
eurjchem-966	242	9	930‐938	930‐938	NUM
eurjchem-966	242	10	.	.	PUNCT
eurjchem-966	243	1	[	[	X
eurjchem-966	243	2	13	13	NUM
eurjchem-966	243	3	]	]	PUNCT
eurjchem-966	243	4	.	.	PUNCT
eurjchem-966	244	1	saul	saul	PROPN
eurjchem-966	244	2	pa	pa	PROPN
eurjchem-966	244	3	,	,	PUNCT
eurjchem-966	244	4	k.	k.	PROPN
eurjchem-966	244	5	k.	k.	PROPN
eurjchem-966	244	6	curr	curr	PROPN
eurjchem-966	244	7	.	.	PUNCT
eurjchem-966	245	1	med	med	PROPN
eurjchem-966	245	2	.	.	PUNCT
eurjchem-966	246	1	res	re	NOUN
eurjchem-966	246	2	.	.	PUNCT
eurjchem-966	247	1	opin	opin	NOUN
eurjchem-966	247	2	.	.	PUNCT
eurjchem-966	248	1	1991	1991	NUM
eurjchem-966	248	2	,	,	PUNCT
eurjchem-966	248	3	12(5	12(5	NUM
eurjchem-966	248	4	)	)	PUNCT
eurjchem-966	248	5	,	,	PUNCT
eurjchem-966	248	6	332‐341	332‐341	NUM
eurjchem-966	248	7	.	.	PUNCT
eurjchem-966	249	1	[	[	X
eurjchem-966	249	2	14	14	NUM
eurjchem-966	249	3	]	]	SYM
eurjchem-966	249	4	.	.	PUNCT
eurjchem-966	250	1	bakshi	bakshi	PROPN
eurjchem-966	250	2	,	,	PUNCT
eurjchem-966	250	3	m.	m.	NOUN
eurjchem-966	250	4	;	;	PUNCT
eurjchem-966	250	5	singh	singh	PROPN
eurjchem-966	250	6	,	,	PUNCT
eurjchem-966	250	7	s.	s.	PROPN
eurjchem-966	250	8	j.	j.	PROPN
eurjchem-966	250	9	pharmaceut	pharmaceut	PROPN
eurjchem-966	250	10	.	.	PROPN
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eurjchem-966	250	12	.	.	PUNCT
eurjchem-966	251	1	2002	2002	NUM
eurjchem-966	251	2	,	,	PUNCT
eurjchem-966	251	3	28(6	28(6	NUM
eurjchem-966	251	4	)	)	PUNCT
eurjchem-966	251	5	,	,	PUNCT
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eurjchem-966	251	7	.	.	PUNCT
eurjchem-966	252	1	[	[	X
eurjchem-966	252	2	15	15	NUM
eurjchem-966	252	3	]	]	PUNCT
eurjchem-966	252	4	.	.	PUNCT
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eurjchem-966	253	2	,	,	PUNCT
eurjchem-966	253	3	l.	l.	PROPN
eurjchem-966	253	4	p.	p.	PROPN
eurjchem-966	253	5	;	;	PUNCT
eurjchem-966	253	6	george	george	PROPN
eurjchem-966	253	7	s.	s.	PROPN
eurjchem-966	253	8	k.	k.	PROPN
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eurjchem-966	253	12	.	.	PUNCT
eurjchem-966	254	1	western	western	ADJ
eurjchem-966	254	2	washington	washington	PROPN
eurjchem-966	254	3	university	university	PROPN
eurjchem-966	254	4	:	:	PUNCT
eurjchem-966	254	5	bellingham	bellingham	PROPN
eurjchem-966	254	6	,	,	PUNCT
eurjchem-966	254	7	washington	washington	PROPN
eurjchem-966	254	8	,	,	PUNCT
eurjchem-966	254	9	usa	usa	PROPN
eurjchem-966	254	10	,	,	PUNCT
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eurjchem-966	254	12	.	.	PUNCT
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eurjchem-966	255	2	16	16	NUM
eurjchem-966	255	3	]	]	PUNCT
eurjchem-966	255	4	.	.	PUNCT
eurjchem-966	256	1	afkhami	afkhami	PROPN
eurjchem-966	256	2	,	,	PUNCT
eurjchem-966	256	3	a.	a.	NOUN
eurjchem-966	256	4	;	;	PUNCT
eurjchem-966	256	5	bahram	bahram	PROPN
eurjchem-966	256	6	,	,	PUNCT
eurjchem-966	256	7	m.	m.	NOUN
eurjchem-966	256	8	anal	anal	PROPN
eurjchem-966	256	9	.	.	PUNCT
eurjchem-966	257	1	chim	chim	PROPN
eurjchem-966	257	2	.	.	PUNCT
eurjchem-966	258	1	acta	acta	PROPN
eurjchem-966	258	2	2004	2004	NUM
eurjchem-966	258	3	,	,	PUNCT
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eurjchem-966	258	5	)	)	PUNCT
eurjchem-966	258	6	,	,	PUNCT
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eurjchem-966	258	8	.	.	PUNCT
eurjchem-966	259	1	[	[	X
eurjchem-966	259	2	17	17	NUM
eurjchem-966	259	3	]	]	PUNCT
eurjchem-966	259	4	.	.	PUNCT
eurjchem-966	260	1	afkhami	afkhami	PROPN
eurjchem-966	260	2	,	,	PUNCT
eurjchem-966	260	3	a.	a.	NOUN
eurjchem-966	260	4	;	;	PUNCT
eurjchem-966	260	5	bahram	bahram	PROPN
eurjchem-966	260	6	,	,	PUNCT
eurjchem-966	260	7	m.	m.	NOUN
eurjchem-966	260	8	talanta	talanta	PROPN
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eurjchem-966	260	10	,	,	PUNCT
eurjchem-966	260	11	66(3	66(3	NOUN
eurjchem-966	260	12	)	)	PUNCT
eurjchem-966	260	13	,	,	PUNCT
eurjchem-966	260	14	712‐720	712‐720	NUM
eurjchem-966	260	15	.	.	PUNCT
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eurjchem-966	261	2	18	18	NUM
eurjchem-966	261	3	]	]	PUNCT
eurjchem-966	261	4	.	.	PUNCT
eurjchem-966	261	5	afkhami	afkhami	PROPN
eurjchem-966	261	6	,	,	PUNCT
eurjchem-966	261	7	a.	a.	NOUN
eurjchem-966	261	8	;	;	PUNCT
eurjchem-966	261	9	bahram	bahram	PROPN
eurjchem-966	261	10	,	,	PUNCT
eurjchem-966	261	11	m.	m.	NOUN
eurjchem-966	261	12	talanta	talanta	PROPN
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eurjchem-966	261	14	,	,	PUNCT
eurjchem-966	261	15	68(4	68(4	NUM
eurjchem-966	261	16	)	)	PUNCT
eurjchem-966	261	17	,	,	PUNCT
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eurjchem-966	261	19	.	.	PUNCT
eurjchem-966	262	1	[	[	X
eurjchem-966	262	2	19	19	NUM
eurjchem-966	262	3	]	]	PUNCT
eurjchem-966	262	4	.	.	PUNCT
eurjchem-966	263	1	desai	desai	PROPN
eurjchem-966	263	2	,	,	PUNCT
eurjchem-966	263	3	n.	n.	PROPN
eurjchem-966	263	4	;	;	PUNCT
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eurjchem-966	263	6	,	,	PUNCT
eurjchem-966	263	7	p.	p.	PROPN
eurjchem-966	263	8	i.	i.	PROPN
eurjchem-966	263	9	j.	j.	PROPN
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eurjchem-966	263	11	.	.	PUNCT
eurjchem-966	264	1	sci	sci	PROPN
eurjchem-966	264	2	.	.	PROPN
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eurjchem-966	264	4	,	,	PUNCT
eurjchem-966	264	5	70(5	70(5	NUM
eurjchem-966	264	6	)	)	PUNCT
eurjchem-966	264	7	,	,	PUNCT
eurjchem-966	264	8	644‐647	644‐647	NUM
eurjchem-966	264	9	.	.	PUNCT
eurjchem-966	265	1	[	[	X
eurjchem-966	265	2	20	20	NUM
eurjchem-966	265	3	]	]	PUNCT
eurjchem-966	265	4	.	.	PUNCT
eurjchem-966	266	1	ich	ich	PROPN
eurjchem-966	266	2	,	,	PUNCT
eurjchem-966	266	3	q2	q2	PROPN
eurjchem-966	266	4	(	(	PUNCT
eurjchem-966	266	5	r1	r1	PROPN
eurjchem-966	266	6	)	)	PUNCT
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eurjchem-966	266	10	procedures	procedure	NOUN
eurjchem-966	266	11	:	:	PUNCT
eurjchem-966	266	12	text	text	NOUN
eurjchem-966	266	13	and	and	CCONJ
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eurjchem-966	266	15	,	,	PUNCT
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eurjchem-966	266	17	harmonized	harmonize	VERB
eurjchem-966	266	18	tripartite	tripartite	ADJ
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eurjchem-966	266	20	,	,	PUNCT
eurjchem-966	266	21	2005	2005	NUM
eurjchem-966	266	22	.	.	PUNCT
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eurjchem-966	267	2	,	,	PUNCT
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eurjchem-966	267	4	.	.	PROPN
eurjchem-966	267	5	,	,	PUNCT
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eurjchem-966	267	7	of	of	ADP
eurjchem-966	267	8	analytical	analytical	ADJ
eurjchem-966	267	9	procedures	procedure	NOUN
eurjchem-966	267	10	:	:	PUNCT
eurjchem-966	267	11	text	text	NOUN
eurjchem-966	267	12	and	and	CCONJ
eurjchem-966	267	13	methodology	methodology	NOUN
eurjchem-966	267	14	,	,	PUNCT
eurjchem-966	267	15	q2	q2	PROPN
eurjchem-966	267	16	(	(	PUNCT
eurjchem-966	267	17	r1	r1	PROPN
eurjchem-966	267	18	)	)	PUNCT
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eurjchem-966	267	20	,	,	PUNCT
eurjchem-966	267	21	2005	2005	NUM
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