id	sid	tid	token	lemma	pos
eurjchem-976	1	1	untitled	untitle	VERB
eurjchem-976	1	2	european	european	PROPN
eurjchem-976	1	3	journal	journal	PROPN
eurjchem-976	1	4	of	of	ADP
eurjchem-976	1	5	chemistry	chemistry	NOUN
eurjchem-976	1	6	5	5	NUM
eurjchem-976	1	7	(	(	PUNCT
eurjchem-976	1	8	2	2	NUM
eurjchem-976	1	9	)	)	PUNCT
eurjchem-976	1	10	(	(	PUNCT
eurjchem-976	1	11	2014	2014	NUM
eurjchem-976	1	12	)	)	PUNCT
eurjchem-976	1	13	277‐286	277‐286	NUM
eurjchem-976	1	14	european	european	ADJ
eurjchem-976	1	15	journal	journal	NOUN
eurjchem-976	1	16	of	of	ADP
eurjchem-976	1	17	chemistry	chemistry	NOUN
eurjchem-976	1	18	issn	issn	PROPN
eurjchem-976	1	19	2153‐2249	2153‐2249	PROPN
eurjchem-976	1	20	(	(	PUNCT
eurjchem-976	1	21	print	print	NOUN
eurjchem-976	1	22	)	)	PUNCT
eurjchem-976	1	23	/	/	SYM
eurjchem-976	1	24	issn	issn	PROPN
eurjchem-976	1	25	2153‐2257	2153‐2257	NUM
eurjchem-976	1	26	(	(	PUNCT
eurjchem-976	1	27	online	online	ADJ
eurjchem-976	1	28	)	)	PUNCT
eurjchem-976	1	29			NOUN
eurjchem-976	1	30	2014	2014	NUM
eurjchem-976	2	1	eurjchem	eurjchem	PROPN
eurjchem-976	2	2	publishing	publish	VERB
eurjchem-976	2	3	‐	‐	NOUN
eurjchem-976	2	4	printed	print	VERB
eurjchem-976	2	5	in	in	ADP
eurjchem-976	2	6	the	the	DET
eurjchem-976	2	7	usa	usa	PROPN
eurjchem-976	2	8	http://dx.doi.org/10.5155/eurjchem.5.2.277‐286.976	http://dx.doi.org/10.5155/eurjchem.5.2.277‐286.976	PROPN
eurjchem-976	2	9	european	european	PROPN
eurjchem-976	2	10	journal	journal	PROPN
eurjchem-976	2	11	of	of	ADP
eurjchem-976	2	12	chemistry	chemistry	PROPN
eurjchem-976	2	13	journal	journal	PROPN
eurjchem-976	2	14	homepage	homepage	NOUN
eurjchem-976	2	15	:	:	PUNCT
eurjchem-976	2	16	www.eurjchem.com	www.eurjchem.com	X
eurjchem-976	2	17	friedel‐crafts	friedel‐craft	VERB
eurjchem-976	2	18	chemistry	chemistry	NOUN
eurjchem-976	2	19	:	:	PUNCT
eurjchem-976	2	20	part	part	NOUN
eurjchem-976	2	21	41	41	NUM
eurjchem-976	2	22	.	.	PUNCT
eurjchem-976	3	1	a	a	DET
eurjchem-976	3	2	new	new	ADJ
eurjchem-976	3	3	facile	facile	ADJ
eurjchem-976	3	4	synthesis	synthesis	NOUN
eurjchem-976	3	5	of	of	ADP
eurjchem-976	3	6	indeno[1,2‐c	indeno[1,2‐c	NOUN
eurjchem-976	3	7	]	]	PUNCT
eurjchem-976	3	8	pyrazoles	pyrazole	NOUN
eurjchem-976	3	9	,	,	PUNCT
eurjchem-976	3	10	2h‐benzo[g]indazoles	2h‐benzo[g]indazole	NOUN
eurjchem-976	3	11	and	and	CCONJ
eurjchem-976	3	12	benzo[6,7]cyclohepta[1,2‐c]pyrazoles	benzo[6,7]cyclohepta[1,2‐c]pyrazole	NOUN
eurjchem-976	3	13	via	via	ADP
eurjchem-976	3	14	friedel‐crafts	friedel‐craft	NOUN
eurjchem-976	3	15	ring	ring	NOUN
eurjchem-976	3	16	closures	closure	NOUN
eurjchem-976	3	17	hassan	hassan	PROPN
eurjchem-976	3	18	abdou	abdou	PROPN
eurjchem-976	3	19	kotb	kotb	PROPN
eurjchem-976	3	20	abd	abd	PROPN
eurjchem-976	3	21	el‐aal	el‐aal	PROPN
eurjchem-976	3	22	*	*	PUNCT
eurjchem-976	3	23	,	,	PUNCT
eurjchem-976	3	24	ahmed	ahmed	PROPN
eurjchem-976	3	25	mahmoud	mahmoud	PROPN
eurjchem-976	3	26	abdel	abdel	PROPN
eurjchem-976	3	27	mageed	mageed	PROPN
eurjchem-976	3	28	el‐khawaga	el‐khawaga	PROPN
eurjchem-976	3	29	and	and	CCONJ
eurjchem-976	3	30	ali	ali	PROPN
eurjchem-976	3	31	ali	ali	PROPN
eurjchem-976	3	32	khalaf	khalaf	PROPN
eurjchem-976	3	33	chemistry	chemistry	PROPN
eurjchem-976	3	34	department	department	PROPN
eurjchem-976	3	35	,	,	PUNCT
eurjchem-976	3	36	faculty	faculty	NOUN
eurjchem-976	3	37	of	of	ADP
eurjchem-976	3	38	science	science	NOUN
eurjchem-976	3	39	,	,	PUNCT
eurjchem-976	3	40	assiut	assiut	PROPN
eurjchem-976	3	41	university	university	PROPN
eurjchem-976	3	42	,	,	PUNCT
eurjchem-976	3	43	assiut	assiut	NOUN
eurjchem-976	3	44	,	,	PUNCT
eurjchem-976	3	45	71516	71516	NUM
eurjchem-976	3	46	,	,	PUNCT
eurjchem-976	3	47	egypt	egypt	PROPN
eurjchem-976	3	48	*	*	PUNCT
eurjchem-976	3	49	corresponding	correspond	VERB
eurjchem-976	3	50	author	author	NOUN
eurjchem-976	3	51	at	at	ADP
eurjchem-976	3	52	:	:	PUNCT
eurjchem-976	3	53	chemistry	chemistry	NOUN
eurjchem-976	3	54	department	department	NOUN
eurjchem-976	3	55	,	,	PUNCT
eurjchem-976	3	56	faculty	faculty	NOUN
eurjchem-976	3	57	of	of	ADP
eurjchem-976	3	58	science	science	NOUN
eurjchem-976	3	59	,	,	PUNCT
eurjchem-976	3	60	assiut	assiut	PROPN
eurjchem-976	3	61	university	university	PROPN
eurjchem-976	3	62	,	,	PUNCT
eurjchem-976	3	63	assiut	assiut	NOUN
eurjchem-976	3	64	,	,	PUNCT
eurjchem-976	3	65	71516	71516	NUM
eurjchem-976	3	66	,	,	PUNCT
eurjchem-976	3	67	egypt	egypt	PROPN
eurjchem-976	3	68	.	.	PUNCT
eurjchem-976	4	1	tel	tel	PROPN
eurjchem-976	4	2	.	.	PUNCT
eurjchem-976	4	3	:	:	PUNCT
eurjchem-976	5	1	+2.088.2411485	+2.088.2411485	PROPN
eurjchem-976	5	2	.	.	PUNCT
eurjchem-976	6	1	fax	fax	NOUN
eurjchem-976	6	2	:	:	PUNCT
eurjchem-976	6	3	+2.088.2342708	+2.088.2342708	NUM
eurjchem-976	6	4	.	.	PUNCT
eurjchem-976	6	5	e‐mail	e‐mail	PUNCT
eurjchem-976	7	1	address	address	NOUN
eurjchem-976	7	2	:	:	PUNCT
eurjchem-976	7	3	hassankotb33@yahoo.com	hassankotb33@yahoo.com	X
eurjchem-976	7	4	(	(	PUNCT
eurjchem-976	7	5	h.a.k.a	h.a.k.a	PROPN
eurjchem-976	7	6	.	.	PROPN
eurjchem-976	7	7	el‐aal	el‐aal	PROPN
eurjchem-976	7	8	)	)	PUNCT
eurjchem-976	7	9	.	.	PUNCT
eurjchem-976	8	1	article	article	NOUN
eurjchem-976	8	2	information	information	PROPN
eurjchem-976	8	3	abstract	abstract	ADJ
eurjchem-976	8	4	doi	doi	NOUN
eurjchem-976	8	5	:	:	PUNCT
eurjchem-976	8	6	10.5155	10.5155	NUM
eurjchem-976	8	7	/	/	SYM
eurjchem-976	8	8	eurjchem.5.2.277‐286.976	eurjchem.5.2.277‐286.976	NOUN
eurjchem-976	8	9	received	receive	VERB
eurjchem-976	8	10	:	:	PUNCT
eurjchem-976	8	11	17	17	NUM
eurjchem-976	8	12	november	november	PROPN
eurjchem-976	8	13	2013	2013	NUM
eurjchem-976	8	14	received	receive	VERB
eurjchem-976	8	15	in	in	ADP
eurjchem-976	8	16	revised	revise	VERB
eurjchem-976	8	17	form	form	NOUN
eurjchem-976	8	18	:	:	PUNCT
eurjchem-976	8	19	25	25	NUM
eurjchem-976	8	20	december	december	PROPN
eurjchem-976	8	21	2013	2013	NUM
eurjchem-976	8	22	accepted	accept	VERB
eurjchem-976	8	23	:	:	PUNCT
eurjchem-976	8	24	25	25	NUM
eurjchem-976	8	25	december	december	PROPN
eurjchem-976	8	26	2013	2013	NUM
eurjchem-976	8	27	online	online	NOUN
eurjchem-976	8	28	:	:	PUNCT
eurjchem-976	8	29	30	30	NUM
eurjchem-976	8	30	june	june	PROPN
eurjchem-976	8	31	2014	2014	NUM
eurjchem-976	8	32	keywords	keyword	NOUN
eurjchem-976	8	33	expedient	expedient	VERB
eurjchem-976	8	34	and	and	CCONJ
eurjchem-976	8	35	novel	novel	ADJ
eurjchem-976	8	36	alternative	alternative	ADJ
eurjchem-976	8	37	synthesis	synthesis	NOUN
eurjchem-976	8	38	of	of	ADP
eurjchem-976	8	39	some	some	DET
eurjchem-976	8	40	fused	fuse	VERB
eurjchem-976	8	41	heteropolycycles	heteropolycycle	NOUN
eurjchem-976	8	42	containing	contain	VERB
eurjchem-976	8	43	pyrazole	pyrazole	NOUN
eurjchem-976	8	44	moiety	moiety	NOUN
eurjchem-976	8	45	is	be	AUX
eurjchem-976	8	46	described	describe	VERB
eurjchem-976	8	47	.	.	PUNCT
eurjchem-976	9	1	a	a	DET
eurjchem-976	9	2	series	series	NOUN
eurjchem-976	9	3	of	of	ADP
eurjchem-976	9	4	indeno[1,2‐c]pyrazoles	indeno[1,2‐c]pyrazole	NOUN
eurjchem-976	9	5	,	,	PUNCT
eurjchem-976	9	6	2h‐benzo[g]indazoles	2h‐benzo[g]indazole	NOUN
eurjchem-976	9	7	and	and	CCONJ
eurjchem-976	9	8	benzo[6,7	benzo[6,7	PROPN
eurjchem-976	9	9	]	]	X
eurjchem-976	10	1	cyclohepta[1,2‐c]pyrazoles	cyclohepta[1,2‐c]pyrazole	NOUN
eurjchem-976	10	2	were	be	AUX
eurjchem-976	10	3	prepared	prepare	VERB
eurjchem-976	10	4	by	by	ADP
eurjchem-976	10	5	friedel‐crafts	friedel‐craft	NOUN
eurjchem-976	10	6	ring	ring	NOUN
eurjchem-976	10	7	closure	closure	NOUN
eurjchem-976	10	8	of	of	ADP
eurjchem-976	10	9	suitable	suitable	ADJ
eurjchem-976	10	10	synthesized	synthesize	VERB
eurjchem-976	10	11	carboxylic	carboxylic	ADJ
eurjchem-976	10	12	acids	acid	NOUN
eurjchem-976	10	13	and	and	CCONJ
eurjchem-976	10	14	alkanols	alkanol	NOUN
eurjchem-976	10	15	in	in	ADP
eurjchem-976	10	16	the	the	DET
eurjchem-976	10	17	presence	presence	NOUN
eurjchem-976	10	18	of	of	ADP
eurjchem-976	10	19	alcl3	alcl3	PROPN
eurjchem-976	10	20	/	/	SYM
eurjchem-976	10	21	ch3no2	ch3no2	NOUN
eurjchem-976	10	22	or	or	CCONJ
eurjchem-976	10	23	p2o5	p2o5	X
eurjchem-976	10	24	or	or	CCONJ
eurjchem-976	10	25	ppa	ppa	PROPN
eurjchem-976	10	26	(	(	PUNCT
eurjchem-976	10	27	polyphosphoric	polyphosphoric	ADJ
eurjchem-976	10	28	acid	acid	NOUN
eurjchem-976	10	29	)	)	PUNCT
eurjchem-976	10	30	catalysts	catalyst	NOUN
eurjchem-976	10	31	.	.	PUNCT
eurjchem-976	11	1	the	the	DET
eurjchem-976	11	2	precursor	precursor	NOUN
eurjchem-976	11	3	acids	acid	NOUN
eurjchem-976	11	4	were	be	AUX
eurjchem-976	11	5	obtained	obtain	VERB
eurjchem-976	11	6	by	by	ADP
eurjchem-976	11	7	utilizing	utilize	VERB
eurjchem-976	11	8	kmno4	kmno4	NOUN
eurjchem-976	11	9	oxidation	oxidation	NOUN
eurjchem-976	11	10	of	of	ADP
eurjchem-976	11	11	the	the	DET
eurjchem-976	11	12	corresponding	corresponding	ADJ
eurjchem-976	11	13	aldehyde	aldehyde	NOUN
eurjchem-976	11	14	,	,	PUNCT
eurjchem-976	11	15	alkylations	alkylation	NOUN
eurjchem-976	11	16	of	of	ADP
eurjchem-976	11	17	diethyl	diethyl	NOUN
eurjchem-976	11	18	malonates	malonate	NOUN
eurjchem-976	11	19	and	and	CCONJ
eurjchem-976	11	20	perkin	perkin	PROPN
eurjchem-976	11	21	type	type	NOUN
eurjchem-976	11	22	approaches	approach	NOUN
eurjchem-976	11	23	,	,	PUNCT
eurjchem-976	11	24	whereas	whereas	SCONJ
eurjchem-976	11	25	starting	start	VERB
eurjchem-976	11	26	alkanols	alkanol	NOUN
eurjchem-976	11	27	were	be	AUX
eurjchem-976	11	28	smoothly	smoothly	ADV
eurjchem-976	11	29	obtained	obtain	VERB
eurjchem-976	11	30	by	by	ADP
eurjchem-976	11	31	reaction	reaction	NOUN
eurjchem-976	11	32	of	of	ADP
eurjchem-976	11	33	carboxylic	carboxylic	ADJ
eurjchem-976	11	34	acid	acid	NOUN
eurjchem-976	11	35	ester	ester	NOUN
eurjchem-976	11	36	with	with	ADP
eurjchem-976	11	37	grignard	grignard	ADJ
eurjchem-976	11	38	reagent	reagent	NOUN
eurjchem-976	11	39	.	.	PUNCT
eurjchem-976	12	1	to	to	PART
eurjchem-976	12	2	exemplify	exemplify	VERB
eurjchem-976	12	3	,	,	PUNCT
eurjchem-976	12	4	cyclizations	cyclization	NOUN
eurjchem-976	12	5	of	of	ADP
eurjchem-976	12	6	5‐chloro‐1,3‐diphenyl‐1h‐pyrazole‐	5‐chloro‐1,3‐diphenyl‐1h‐pyrazole‐	NUM
eurjchem-976	12	7	4‐carboxylic	4‐carboxylic	ADJ
eurjchem-976	12	8	acid	acid	NOUN
eurjchem-976	12	9	(	(	PUNCT
eurjchem-976	12	10	6	6	NUM
eurjchem-976	12	11	)	)	PUNCT
eurjchem-976	12	12	were	be	AUX
eurjchem-976	12	13	accomplished	accomplish	VERB
eurjchem-976	12	14	using	use	VERB
eurjchem-976	12	15	the	the	DET
eurjchem-976	12	16	above	above	ADJ
eurjchem-976	12	17	catalysts	catalyst	NOUN
eurjchem-976	12	18	afforded	afford	VERB
eurjchem-976	12	19	3‐chloro‐2‐	3‐chloro‐2‐	NUM
eurjchem-976	12	20	phenylindeno[1,2‐c]pyrazol‐4(2h)‐one	phenylindeno[1,2‐c]pyrazol‐4(2h)‐one	NOUN
eurjchem-976	12	21	(	(	PUNCT
eurjchem-976	12	22	1b	1b	NUM
eurjchem-976	12	23	)	)	PUNCT
eurjchem-976	12	24	.	.	PUNCT
eurjchem-976	13	1	similarly	similarly	ADV
eurjchem-976	13	2	,	,	PUNCT
eurjchem-976	13	3	cyclization	cyclization	NOUN
eurjchem-976	13	4	of	of	ADP
eurjchem-976	13	5	the	the	DET
eurjchem-976	13	6	2‐(5‐chloro‐1,3‐	2‐(5‐chloro‐1,3‐	NUM
eurjchem-976	13	7	diphenyl‐1h‐pyrazol‐4‐yl)propan‐2‐ol	diphenyl‐1h‐pyrazol‐4‐yl)propan‐2‐ol	PROPN
eurjchem-976	13	8	(	(	PUNCT
eurjchem-976	13	9	8)	8)	NUM
eurjchem-976	13	10	by	by	ADP
eurjchem-976	13	11	a	a	DET
eurjchem-976	13	12	friedel	friedel	PROPN
eurjchem-976	13	13	–	–	PUNCT
eurjchem-976	13	14	crafts‐type	crafts‐type	NOUN
eurjchem-976	13	15	ring	ring	NOUN
eurjchem-976	13	16	closure	closure	NOUN
eurjchem-976	13	17	afforded	afford	VERB
eurjchem-976	13	18	the	the	DET
eurjchem-976	13	19	3‐chloro‐2,4‐dihydro‐4,4‐dimethyl‐2‐phenylindeno[1,2‐c]pyrazole	3‐chloro‐2,4‐dihydro‐4,4‐dimethyl‐2‐phenylindeno[1,2‐c]pyrazole	PROPN
eurjchem-976	13	20	(	(	PUNCT
eurjchem-976	13	21	1a	1a	NUM
eurjchem-976	13	22	)	)	PUNCT
eurjchem-976	13	23	.	.	PUNCT
eurjchem-976	14	1	benzo[g]indazole	benzo[g]indazole	PROPN
eurjchem-976	14	2	heteropolycycles	heteropolycycle	NOUN
eurjchem-976	14	3	heteroarylalkanols	heteroarylalkanol	VERB
eurjchem-976	14	4	indeno[1,2‐c]pyrazole	indeno[1,2‐c]pyrazole	PROPN
eurjchem-976	14	5	friedel‐crafts	friedel‐craft	NOUN
eurjchem-976	14	6	ring	ring	NOUN
eurjchem-976	14	7	closures	closure	NOUN
eurjchem-976	14	8	benzo[6,7]cyclohepta[1,2‐c]pyrazole	benzo[6,7]cyclohepta[1,2‐c]pyrazole	VERB
eurjchem-976	14	9	1	1	NUM
eurjchem-976	14	10	.	.	PUNCT
eurjchem-976	15	1	introduction	introduction	VERB
eurjchem-976	15	2	the	the	DET
eurjchem-976	15	3	synthesis	synthesis	NOUN
eurjchem-976	15	4	of	of	ADP
eurjchem-976	15	5	pyrazoles	pyrazole	NOUN
eurjchem-976	15	6	and	and	CCONJ
eurjchem-976	15	7	their	their	PRON
eurjchem-976	15	8	condensed	condense	VERB
eurjchem-976	15	9	scaffolds	scaffold	NOUN
eurjchem-976	15	10	have	have	AUX
eurjchem-976	15	11	been	be	AUX
eurjchem-976	15	12	a	a	DET
eurjchem-976	15	13	subject	subject	NOUN
eurjchem-976	15	14	of	of	ADP
eurjchem-976	15	15	consistent	consistent	ADJ
eurjchem-976	15	16	interest	interest	NOUN
eurjchem-976	15	17	because	because	SCONJ
eurjchem-976	15	18	of	of	ADP
eurjchem-976	15	19	their	their	PRON
eurjchem-976	15	20	long	long	ADJ
eurjchem-976	15	21	history	history	NOUN
eurjchem-976	15	22	of	of	ADP
eurjchem-976	15	23	application	application	NOUN
eurjchem-976	15	24	in	in	ADP
eurjchem-976	15	25	pharmaceutical	pharmaceutical	NOUN
eurjchem-976	15	26	[	[	X
eurjchem-976	15	27	1‐3	1‐3	X
eurjchem-976	15	28	]	]	PUNCT
eurjchem-976	15	29	and	and	CCONJ
eurjchem-976	15	30	agrochemical	agrochemical	NOUN
eurjchem-976	15	31	[	[	X
eurjchem-976	15	32	4‐6	4‐6	X
eurjchem-976	15	33	]	]	X
eurjchem-976	15	34	industries	industry	NOUN
eurjchem-976	15	35	.	.	PUNCT
eurjchem-976	16	1	over	over	ADP
eurjchem-976	16	2	the	the	DET
eurjchem-976	16	3	past	past	ADJ
eurjchem-976	16	4	two	two	NUM
eurjchem-976	16	5	decades	decade	NOUN
eurjchem-976	16	6	,	,	PUNCT
eurjchem-976	16	7	pyrazole‐containing	pyrazole‐containing	NOUN
eurjchem-976	16	8	compounds	compound	NOUN
eurjchem-976	16	9	have	have	AUX
eurjchem-976	16	10	received	receive	VERB
eurjchem-976	16	11	considerable	considerable	ADJ
eurjchem-976	16	12	attention	attention	NOUN
eurjchem-976	16	13	owing	owe	VERB
eurjchem-976	16	14	to	to	ADP
eurjchem-976	16	15	their	their	PRON
eurjchem-976	16	16	diverse	diverse	ADJ
eurjchem-976	16	17	chemotherapeutic	chemotherapeutic	ADJ
eurjchem-976	16	18	potentials	potential	NOUN
eurjchem-976	16	19	.	.	PUNCT
eurjchem-976	17	1	they	they	PRON
eurjchem-976	17	2	display	display	VERB
eurjchem-976	17	3	a	a	DET
eurjchem-976	17	4	broad	broad	ADJ
eurjchem-976	17	5	spectrum	spectrum	NOUN
eurjchem-976	17	6	of	of	ADP
eurjchem-976	17	7	biological	biological	ADJ
eurjchem-976	17	8	activities	activity	NOUN
eurjchem-976	17	9	such	such	ADJ
eurjchem-976	17	10	as	as	ADP
eurjchem-976	17	11	antimicrobial	antimicrobial	ADJ
eurjchem-976	17	12	[	[	X
eurjchem-976	17	13	7	7	NUM
eurjchem-976	17	14	]	]	PUNCT
eurjchem-976	17	15	,	,	PUNCT
eurjchem-976	17	16	antifungal	antifungal	PROPN
eurjchem-976	18	1	[	[	X
eurjchem-976	18	2	8	8	NUM
eurjchem-976	18	3	]	]	PUNCT
eurjchem-976	18	4	,	,	PUNCT
eurjchem-976	18	5	anti‐inflammatory	anti‐inflammatory	NOUN
eurjchem-976	19	1	[	[	X
eurjchem-976	19	2	9	9	NUM
eurjchem-976	19	3	]	]	PUNCT
eurjchem-976	19	4	,	,	PUNCT
eurjchem-976	19	5	antitumor	antitumor	PROPN
eurjchem-976	20	1	[	[	X
eurjchem-976	20	2	10	10	NUM
eurjchem-976	20	3	]	]	PUNCT
eurjchem-976	20	4	,	,	PUNCT
eurjchem-976	20	5	antihyperglycemic	antihyperglycemic	PROPN
eurjchem-976	20	6	[	[	X
eurjchem-976	20	7	11	11	NUM
eurjchem-976	20	8	]	]	PUNCT
eurjchem-976	20	9	,	,	PUNCT
eurjchem-976	20	10	analgesic	analgesic	ADJ
eurjchem-976	20	11	[	[	X
eurjchem-976	20	12	12	12	NUM
eurjchem-976	20	13	]	]	PUNCT
eurjchem-976	20	14	,	,	PUNCT
eurjchem-976	20	15	antipyretic	antipyretic	ADJ
eurjchem-976	20	16	[	[	X
eurjchem-976	20	17	13	13	NUM
eurjchem-976	20	18	]	]	PUNCT
eurjchem-976	20	19	,	,	PUNCT
eurjchem-976	20	20	antibacterial	antibacterial	ADJ
eurjchem-976	20	21	[	[	X
eurjchem-976	20	22	14	14	NUM
eurjchem-976	20	23	]	]	X
eurjchem-976	20	24	,	,	PUNCT
eurjchem-976	20	25	sedative‐	sedative‐	PROPN
eurjchem-976	20	26	hypnotic	hypnotic	ADJ
eurjchem-976	21	1	[	[	X
eurjchem-976	21	2	15	15	NUM
eurjchem-976	21	3	]	]	PUNCT
eurjchem-976	21	4	,	,	PUNCT
eurjchem-976	21	5	antidepressant	antidepressant	ADJ
eurjchem-976	21	6	[	[	X
eurjchem-976	21	7	16	16	NUM
eurjchem-976	21	8	]	]	PUNCT
eurjchem-976	21	9	,	,	PUNCT
eurjchem-976	21	10	anti‐rheumatoid	anti‐rheumatoid	ADJ
eurjchem-976	21	11	arthritis	arthritis	NOUN
eurjchem-976	21	12	[	[	X
eurjchem-976	21	13	17	17	NUM
eurjchem-976	21	14	]	]	PUNCT
eurjchem-976	21	15	,	,	PUNCT
eurjchem-976	21	16	anticonvulsant	anticonvulsant	PROPN
eurjchem-976	21	17	[	[	X
eurjchem-976	21	18	18	18	NUM
eurjchem-976	21	19	]	]	PUNCT
eurjchem-976	21	20	,	,	PUNCT
eurjchem-976	21	21	antipsychotic	antipsychotic	ADJ
eurjchem-976	21	22	[	[	X
eurjchem-976	21	23	19	19	NUM
eurjchem-976	21	24	]	]	PUNCT
eurjchem-976	21	25	,	,	PUNCT
eurjchem-976	21	26	antileukemic	antileukemic	ADJ
eurjchem-976	21	27	[	[	X
eurjchem-976	21	28	20	20	NUM
eurjchem-976	21	29	]	]	PUNCT
eurjchem-976	21	30	and	and	CCONJ
eurjchem-976	21	31	as	as	SCONJ
eurjchem-976	21	32	hiv	hiv	PROPN
eurjchem-976	21	33	integrase	integrase	VERB
eurjchem-976	21	34	inhibitor	inhibitor	NOUN
eurjchem-976	21	35	[	[	X
eurjchem-976	21	36	21	21	NUM
eurjchem-976	21	37	]	]	PUNCT
eurjchem-976	21	38	agents	agent	NOUN
eurjchem-976	21	39	.	.	PUNCT
eurjchem-976	22	1	also	also	ADV
eurjchem-976	22	2	pyrazole	pyrazole	VERB
eurjchem-976	22	3	derivatives	derivative	NOUN
eurjchem-976	22	4	were	be	AUX
eurjchem-976	22	5	present	present	ADJ
eurjchem-976	22	6	in	in	ADP
eurjchem-976	22	7	numerous	numerous	ADJ
eurjchem-976	22	8	herbicides	herbicide	NOUN
eurjchem-976	22	9	[	[	X
eurjchem-976	22	10	22	22	NUM
eurjchem-976	22	11	]	]	PUNCT
eurjchem-976	22	12	,	,	PUNCT
eurjchem-976	22	13	fungicides	fungicide	NOUN
eurjchem-976	22	14	[	[	X
eurjchem-976	22	15	23	23	NUM
eurjchem-976	22	16	]	]	PUNCT
eurjchem-976	22	17	,	,	PUNCT
eurjchem-976	22	18	insecticides	insecticide	NOUN
eurjchem-976	22	19	[	[	X
eurjchem-976	22	20	24	24	NUM
eurjchem-976	22	21	]	]	PUNCT
eurjchem-976	22	22	,	,	PUNCT
eurjchem-976	22	23	pesticides	pesticide	VERB
eurjchem-976	22	24	[	[	X
eurjchem-976	22	25	25	25	NUM
eurjchem-976	22	26	]	]	PUNCT
eurjchem-976	22	27	and	and	CCONJ
eurjchem-976	22	28	dyestuffs	dyestuff	NOUN
eurjchem-976	22	29	[	[	X
eurjchem-976	22	30	26	26	NUM
eurjchem-976	22	31	]	]	PUNCT
eurjchem-976	22	32	.	.	PUNCT
eurjchem-976	23	1	in	in	ADP
eurjchem-976	23	2	spite	spite	NOUN
eurjchem-976	23	3	of	of	ADP
eurjchem-976	23	4	they	they	PRON
eurjchem-976	23	5	are	be	AUX
eurjchem-976	23	6	rare	rare	ADJ
eurjchem-976	23	7	in	in	ADP
eurjchem-976	23	8	nature	nature	NOUN
eurjchem-976	23	9	,	,	PUNCT
eurjchem-976	23	10	the	the	DET
eurjchem-976	23	11	only	only	ADJ
eurjchem-976	23	12	natural	natural	ADJ
eurjchem-976	23	13	pyrazole	pyrazole	NOUN
eurjchem-976	23	14	(	(	PUNCT
eurjchem-976	23	15	1‐pyrazolyl‐alanine	1‐pyrazolyl‐alanine	NUM
eurjchem-976	23	16	)	)	PUNCT
eurjchem-976	23	17	was	be	AUX
eurjchem-976	23	18	isolated	isolate	VERB
eurjchem-976	23	19	from	from	ADP
eurjchem-976	23	20	seeds	seed	NOUN
eurjchem-976	23	21	of	of	ADP
eurjchem-976	23	22	watermelons	watermelon	NOUN
eurjchem-976	23	23	[	[	X
eurjchem-976	23	24	27	27	NUM
eurjchem-976	23	25	]	]	PUNCT
eurjchem-976	23	26	.	.	PUNCT
eurjchem-976	24	1	although	although	SCONJ
eurjchem-976	24	2	the	the	DET
eurjchem-976	24	3	discovery	discovery	NOUN
eurjchem-976	24	4	[	[	X
eurjchem-976	24	5	28	28	NUM
eurjchem-976	24	6	]	]	PUNCT
eurjchem-976	24	7	of	of	ADP
eurjchem-976	24	8	pyrazoles	pyrazole	NOUN
eurjchem-976	24	9	as	as	ADP
eurjchem-976	24	10	antipyretic	antipyretic	ADJ
eurjchem-976	24	11	agents	agent	NOUN
eurjchem-976	24	12	dated	date	VERB
eurjchem-976	24	13	back	back	ADV
eurjchem-976	24	14	to	to	ADP
eurjchem-976	24	15	1884	1884	NUM
eurjchem-976	24	16	,	,	PUNCT
eurjchem-976	24	17	synthesis	synthesis	NOUN
eurjchem-976	24	18	of	of	ADP
eurjchem-976	24	19	pyrazole	pyrazole	NOUN
eurjchem-976	24	20	systems	system	NOUN
eurjchem-976	24	21	have	have	AUX
eurjchem-976	24	22	been	be	AUX
eurjchem-976	24	23	a	a	DET
eurjchem-976	24	24	prominent	prominent	ADJ
eurjchem-976	24	25	research	research	NOUN
eurjchem-976	24	26	objective	objective	NOUN
eurjchem-976	24	27	for	for	ADP
eurjchem-976	24	28	over	over	ADP
eurjchem-976	24	29	a	a	PRON
eurjchem-976	24	30	century	century	NOUN
eurjchem-976	24	31	and	and	CCONJ
eurjchem-976	24	32	a	a	DET
eurjchem-976	24	33	variety	variety	NOUN
eurjchem-976	24	34	of	of	ADP
eurjchem-976	24	35	well‐established	well‐establishe	VERB
eurjchem-976	24	36	synthetic	synthetic	ADJ
eurjchem-976	24	37	methodologies	methodology	NOUN
eurjchem-976	24	38	are	be	AUX
eurjchem-976	24	39	available	available	ADJ
eurjchem-976	24	40	in	in	ADP
eurjchem-976	24	41	the	the	DET
eurjchem-976	24	42	literature	literature	NOUN
eurjchem-976	24	43	.	.	PUNCT
eurjchem-976	25	1	of	of	ADP
eurjchem-976	25	2	the	the	DET
eurjchem-976	25	3	methods	method	NOUN
eurjchem-976	25	4	developed	develop	VERB
eurjchem-976	25	5	,	,	PUNCT
eurjchem-976	25	6	1,3‐	1,3‐	NUM
eurjchem-976	25	7	dipolar	dipolar	ADJ
eurjchem-976	25	8	cycloadditions	cycloaddition	NOUN
eurjchem-976	25	9	of	of	ADP
eurjchem-976	25	10	diazocompounds	diazocompound	NOUN
eurjchem-976	25	11	[	[	X
eurjchem-976	25	12	29	29	NUM
eurjchem-976	25	13	]	]	PUNCT
eurjchem-976	25	14	or	or	CCONJ
eurjchem-976	25	15	nitrilimines	nitrilimine	NOUN
eurjchem-976	25	16	with	with	ADP
eurjchem-976	25	17	alkynes	alkyne	NOUN
eurjchem-976	25	18	[	[	X
eurjchem-976	25	19	30	30	NUM
eurjchem-976	25	20	]	]	PUNCT
eurjchem-976	25	21	or	or	CCONJ
eurjchem-976	25	22	alkenes	alkene	NOUN
eurjchem-976	25	23	[	[	X
eurjchem-976	25	24	31,32	31,32	NUM
eurjchem-976	25	25	]	]	PUNCT
eurjchem-976	25	26	,	,	PUNCT
eurjchem-976	25	27	reaction	reaction	NOUN
eurjchem-976	25	28	of	of	ADP
eurjchem-976	25	29	chalcones	chalcone	NOUN
eurjchem-976	25	30	and	and	CCONJ
eurjchem-976	25	31	hydrazines	hydrazine	NOUN
eurjchem-976	25	32	[	[	X
eurjchem-976	25	33	33	33	NUM
eurjchem-976	25	34	]	]	PUNCT
eurjchem-976	25	35	,	,	PUNCT
eurjchem-976	25	36	reaction	reaction	NOUN
eurjchem-976	25	37	of	of	ADP
eurjchem-976	25	38	enaminones	enaminone	NOUN
eurjchem-976	25	39	with	with	ADP
eurjchem-976	25	40	different	different	ADJ
eurjchem-976	25	41	aminoheterocycles	aminoheterocycle	NOUN
eurjchem-976	25	42	[	[	X
eurjchem-976	25	43	34	34	NUM
eurjchem-976	25	44	]	]	PUNCT
eurjchem-976	25	45	,	,	PUNCT
eurjchem-976	25	46	condensation	condensation	NOUN
eurjchem-976	25	47	of	of	ADP
eurjchem-976	25	48	1,3‐diketones	1,3‐diketone	NOUN
eurjchem-976	25	49	and	and	CCONJ
eurjchem-976	25	50	hydrazines	hydrazine	NOUN
eurjchem-976	25	51	in	in	ADP
eurjchem-976	25	52	the	the	DET
eurjchem-976	25	53	presence	presence	NOUN
eurjchem-976	25	54	of	of	ADP
eurjchem-976	25	55	an	an	DET
eurjchem-976	25	56	acidic	acidic	ADJ
eurjchem-976	25	57	catalyst	catalyst	NOUN
eurjchem-976	25	58	[	[	X
eurjchem-976	25	59	35	35	NUM
eurjchem-976	25	60	]	]	PUNCT
eurjchem-976	25	61	and	and	CCONJ
eurjchem-976	25	62	coupling	coupling	NOUN
eurjchem-976	25	63	of	of	ADP
eurjchem-976	25	64	terminal	terminal	ADJ
eurjchem-976	25	65	alkynes	alkyne	NOUN
eurjchem-976	25	66	with	with	ADP
eurjchem-976	25	67	hydrazine	hydrazine	NOUN
eurjchem-976	25	68	and	and	CCONJ
eurjchem-976	25	69	carbon	carbon	NOUN
eurjchem-976	25	70	monoxide	monoxide	NOUN
eurjchem-976	25	71	[	[	X
eurjchem-976	25	72	36	36	NUM
eurjchem-976	25	73	]	]	PUNCT
eurjchem-976	25	74	.	.	PUNCT
eurjchem-976	26	1	among	among	ADP
eurjchem-976	26	2	different	different	ADJ
eurjchem-976	26	3	condensed	condense	VERB
eurjchem-976	26	4	pyrazoles	pyrazole	NOUN
eurjchem-976	26	5	polycycles	polycycle	NOUN
eurjchem-976	26	6	,	,	PUNCT
eurjchem-976	26	7	indeno[1,2‐c]pyrazole	indeno[1,2‐c]pyrazole	PROPN
eurjchem-976	26	8	(	(	PUNCT
eurjchem-976	26	9	1	1	NUM
eurjchem-976	26	10	)	)	PUNCT
eurjchem-976	26	11	[	[	X
eurjchem-976	26	12	37,38	37,38	NOUN
eurjchem-976	26	13	]	]	PUNCT
eurjchem-976	26	14	,	,	PUNCT
eurjchem-976	26	15	2h‐benzo[g]indazole	2h‐benzo[g]indazole	NUM
eurjchem-976	26	16	(	(	PUNCT
eurjchem-976	26	17	2	2	NUM
eurjchem-976	26	18	)	)	PUNCT
eurjchem-976	27	1	[	[	X
eurjchem-976	27	2	39‐41	39‐41	NUM
eurjchem-976	27	3	]	]	PUNCT
eurjchem-976	27	4	and	and	CCONJ
eurjchem-976	27	5	benzo[6,7]cyclohepta[1,2‐c]pyrazole	benzo[6,7]cyclohepta[1,2‐c]pyrazole	NOUN
eurjchem-976	27	6	(	(	PUNCT
eurjchem-976	27	7	3	3	NUM
eurjchem-976	27	8	)	)	PUNCT
eurjchem-976	27	9	[	[	X
eurjchem-976	27	10	42	42	NUM
eurjchem-976	27	11	]	]	X
eurjchem-976	27	12	derivatives	derivative	NOUN
eurjchem-976	27	13	(	(	PUNCT
eurjchem-976	27	14	figure	figure	NOUN
eurjchem-976	27	15	1	1	NUM
eurjchem-976	27	16	)	)	PUNCT
eurjchem-976	27	17	are	be	AUX
eurjchem-976	27	18	such	such	ADJ
eurjchem-976	27	19	molecules	molecule	NOUN
eurjchem-976	27	20	which	which	PRON
eurjchem-976	27	21	have	have	VERB
eurjchem-976	27	22	unique	unique	ADJ
eurjchem-976	27	23	nitrogen‐containing	nitrogen‐containing	NOUN
eurjchem-976	27	24	tricyclic	tricyclic	ADJ
eurjchem-976	27	25	structures	structure	NOUN
eurjchem-976	27	26	are	be	AUX
eurjchem-976	27	27	known	know	VERB
eurjchem-976	27	28	to	to	PART
eurjchem-976	27	29	exert	exert	VERB
eurjchem-976	27	30	biological	biological	ADJ
eurjchem-976	27	31	activities	activity	NOUN
eurjchem-976	27	32	in	in	ADP
eurjchem-976	27	33	many	many	ADJ
eurjchem-976	27	34	active	active	ADJ
eurjchem-976	27	35	pharmaceutical	pharmaceutical	ADJ
eurjchem-976	27	36	ingredients	ingredient	NOUN
eurjchem-976	28	1	[	[	X
eurjchem-976	28	2	43,44	43,44	X
eurjchem-976	28	3	]	]	PUNCT
eurjchem-976	28	4	.	.	PUNCT
eurjchem-976	29	1	literature	literature	NOUN
eurjchem-976	29	2	survey	survey	NOUN
eurjchem-976	29	3	revealed	reveal	VERB
eurjchem-976	29	4	that	that	SCONJ
eurjchem-976	29	5	limited	limited	ADJ
eurjchem-976	29	6	numbers	number	NOUN
eurjchem-976	29	7	of	of	ADP
eurjchem-976	29	8	strategies	strategy	NOUN
eurjchem-976	29	9	have	have	AUX
eurjchem-976	29	10	been	be	AUX
eurjchem-976	29	11	successfully	successfully	ADV
eurjchem-976	29	12	applied	apply	VERB
eurjchem-976	29	13	in	in	ADP
eurjchem-976	29	14	the	the	DET
eurjchem-976	29	15	synthesis	synthesis	NOUN
eurjchem-976	29	16	of	of	ADP
eurjchem-976	29	17	such	such	ADJ
eurjchem-976	29	18	1‐3	1‐3	PROPN
eurjchem-976	29	19	skeletons	skeleton	NOUN
eurjchem-976	29	20	derivatives	derivative	NOUN
eurjchem-976	29	21	.	.	PUNCT
eurjchem-976	30	1	however	however	ADV
eurjchem-976	30	2	,	,	PUNCT
eurjchem-976	30	3	all	all	DET
eurjchem-976	30	4	such	such	ADJ
eurjchem-976	30	5	reported	report	VERB
eurjchem-976	30	6	methods	method	NOUN
eurjchem-976	30	7	were	be	AUX
eurjchem-976	30	8	based	base	VERB
eurjchem-976	30	9	on	on	ADP
eurjchem-976	30	10	the	the	DET
eurjchem-976	30	11	addition	addition	NOUN
eurjchem-976	30	12	of	of	ADP
eurjchem-976	30	13	substituted	substitute	VERB
eurjchem-976	30	14	hydrazines	hydrazine	NOUN
eurjchem-976	30	15	to	to	ADP
eurjchem-976	30	16	suitable	suitable	ADJ
eurjchem-976	30	17	chalcones	chalcone	NOUN
eurjchem-976	30	18	,	,	PUNCT
eurjchem-976	30	19	β‐diketones	β‐diketones	PUNCT
eurjchem-976	30	20	and	and	CCONJ
eurjchem-976	30	21	α‐keto‐β‐hydroxyesters	α‐keto‐β‐hydroxyester	NOUN
eurjchem-976	30	22	.	.	PUNCT
eurjchem-976	31	1	in	in	ADP
eurjchem-976	31	2	an	an	DET
eurjchem-976	31	3	alternative	alternative	ADJ
eurjchem-976	31	4	pioneering	pioneering	ADJ
eurjchem-976	31	5	strategy	strategy	NOUN
eurjchem-976	31	6	,	,	PUNCT
eurjchem-976	31	7	li	li	PROPN
eurjchem-976	31	8	et	et	PROPN
eurjchem-976	31	9	al	al	PROPN
eurjchem-976	31	10	.	.	PUNCT
eurjchem-976	32	1	[	[	X
eurjchem-976	32	2	45	45	NUM
eurjchem-976	32	3	]	]	PUNCT
eurjchem-976	32	4	achieved	achieve	VERB
eurjchem-976	32	5	the	the	DET
eurjchem-976	32	6	synthesis	synthesis	NOUN
eurjchem-976	32	7	of	of	ADP
eurjchem-976	32	8	scaffold	scaffold	NOUN
eurjchem-976	32	9	2	2	NUM
eurjchem-976	32	10	and	and	CCONJ
eurjchem-976	32	11	variety	variety	NOUN
eurjchem-976	32	12	of	of	ADP
eurjchem-976	32	13	aza‐polycyclic	aza‐polycyclic	ADJ
eurjchem-976	32	14	aromatic	aromatic	ADJ
eurjchem-976	32	15	compounds	compound	NOUN
eurjchem-976	32	16	via	via	ADP
eurjchem-976	32	17	superelectrophilic	superelectrophilic	ADJ
eurjchem-976	32	18	cyclizations	cyclization	NOUN
eurjchem-976	32	19	of	of	ADP
eurjchem-976	32	20	alkenyl‐substituted	alkenyl‐substitute	VERB
eurjchem-976	32	21	n‐heterocycles	n‐heterocycle	NOUN
eurjchem-976	32	22	with	with	ADP
eurjchem-976	32	23	triflic	triflic	ADJ
eurjchem-976	32	24	acid	acid	NOUN
eurjchem-976	32	25	(	(	PUNCT
eurjchem-976	32	26	cf3so3h	cf3so3h	NOUN
eurjchem-976	32	27	)	)	PUNCT
eurjchem-976	32	28	.	.	PUNCT
eurjchem-976	33	1	278	278	NUM
eurjchem-976	33	2	el‐aal	el‐aal	PROPN
eurjchem-976	33	3	et	et	NOUN
eurjchem-976	33	4	al	al	PROPN
eurjchem-976	33	5	.	.	PUNCT
eurjchem-976	33	6	/	/	SYM
eurjchem-976	33	7	european	european	PROPN
eurjchem-976	33	8	journal	journal	PROPN
eurjchem-976	33	9	of	of	ADP
eurjchem-976	33	10	chemistry	chemistry	NOUN
eurjchem-976	33	11	5	5	NUM
eurjchem-976	33	12	(	(	PUNCT
eurjchem-976	33	13	2	2	NUM
eurjchem-976	33	14	)	)	PUNCT
eurjchem-976	33	15	(	(	PUNCT
eurjchem-976	33	16	2014	2014	NUM
eurjchem-976	33	17	)	)	PUNCT
eurjchem-976	33	18	277‐286	277‐286	NUM
eurjchem-976	33	19	figure	figure	NOUN
eurjchem-976	33	20	1	1	NUM
eurjchem-976	33	21	.	.	PUNCT
eurjchem-976	34	1	pyrazole	pyrazole	NOUN
eurjchem-976	34	2	heteropolycycles	heteropolycycle	NOUN
eurjchem-976	34	3	containing	contain	VERB
eurjchem-976	34	4	pharmaceuticals	pharmaceutical	NOUN
eurjchem-976	34	5	.	.	PUNCT
eurjchem-976	35	1	the	the	DET
eurjchem-976	35	2	search	search	NOUN
eurjchem-976	35	3	for	for	ADP
eurjchem-976	35	4	new	new	ADJ
eurjchem-976	35	5	methods	method	NOUN
eurjchem-976	35	6	for	for	ADP
eurjchem-976	35	7	the	the	DET
eurjchem-976	35	8	simple	simple	ADJ
eurjchem-976	35	9	,	,	PUNCT
eurjchem-976	35	10	direct	direct	ADJ
eurjchem-976	35	11	,	,	PUNCT
eurjchem-976	35	12	concise	concise	ADJ
eurjchem-976	35	13	,	,	PUNCT
eurjchem-976	35	14	atom‐economical	atom‐economical	ADJ
eurjchem-976	35	15	synthetic	synthetic	ADJ
eurjchem-976	35	16	route	route	NOUN
eurjchem-976	35	17	and	and	CCONJ
eurjchem-976	35	18	efficient	efficient	ADJ
eurjchem-976	35	19	construction	construction	NOUN
eurjchem-976	35	20	of	of	ADP
eurjchem-976	35	21	this	this	DET
eurjchem-976	35	22	class	class	NOUN
eurjchem-976	35	23	of	of	ADP
eurjchem-976	35	24	pyrazole	pyrazole	NOUN
eurjchem-976	35	25	compounds	compound	NOUN
eurjchem-976	35	26	still	still	ADV
eurjchem-976	35	27	constitutes	constitute	VERB
eurjchem-976	35	28	a	a	DET
eurjchem-976	35	29	major	major	ADJ
eurjchem-976	35	30	challenge	challenge	NOUN
eurjchem-976	35	31	in	in	ADP
eurjchem-976	35	32	organic	organic	ADJ
eurjchem-976	35	33	synthesis	synthesis	NOUN
eurjchem-976	35	34	.	.	PUNCT
eurjchem-976	36	1	in	in	ADP
eurjchem-976	36	2	recent	recent	ADJ
eurjchem-976	36	3	communications	communication	NOUN
eurjchem-976	36	4	[	[	X
eurjchem-976	36	5	46‐50	46‐50	NUM
eurjchem-976	36	6	]	]	PUNCT
eurjchem-976	36	7	,	,	PUNCT
eurjchem-976	36	8	we	we	PRON
eurjchem-976	36	9	have	have	AUX
eurjchem-976	36	10	demonstrated	demonstrate	VERB
eurjchem-976	36	11	simple	simple	ADJ
eurjchem-976	36	12	alternative	alternative	ADJ
eurjchem-976	36	13	procedures	procedure	NOUN
eurjchem-976	36	14	in	in	ADP
eurjchem-976	36	15	the	the	DET
eurjchem-976	36	16	construction	construction	NOUN
eurjchem-976	36	17	of	of	ADP
eurjchem-976	36	18	novel	novel	NOUN
eurjchem-976	36	19	and	and	CCONJ
eurjchem-976	36	20	known	know	VERB
eurjchem-976	36	21	heterocyclic	heterocyclic	NOUN
eurjchem-976	36	22	systems	system	NOUN
eurjchem-976	36	23	proving	prove	VERB
eurjchem-976	36	24	the	the	DET
eurjchem-976	36	25	synthetic	synthetic	ADJ
eurjchem-976	36	26	utility	utility	NOUN
eurjchem-976	36	27	of	of	ADP
eurjchem-976	36	28	friedel‐crafts	friedel‐craft	NOUN
eurjchem-976	36	29	[	[	X
eurjchem-976	36	30	51‐54	51‐54	NOUN
eurjchem-976	36	31	]	]	PUNCT
eurjchem-976	36	32	cyclialkylation	cyclialkylation	NOUN
eurjchem-976	36	33	approach	approach	NOUN
eurjchem-976	36	34	.	.	PUNCT
eurjchem-976	37	1	the	the	DET
eurjchem-976	37	2	results	result	NOUN
eurjchem-976	37	3	manifested	manifest	VERB
eurjchem-976	37	4	that	that	SCONJ
eurjchem-976	37	5	a	a	DET
eurjchem-976	37	6	number	number	NOUN
eurjchem-976	37	7	of	of	ADP
eurjchem-976	37	8	difficult	difficult	ADJ
eurjchem-976	37	9	heterocyclic	heterocyclic	ADJ
eurjchem-976	37	10	skeletons	skeleton	NOUN
eurjchem-976	37	11	can	can	AUX
eurjchem-976	37	12	be	be	AUX
eurjchem-976	37	13	easily	easily	ADV
eurjchem-976	37	14	prepared	prepare	VERB
eurjchem-976	37	15	with	with	ADP
eurjchem-976	37	16	the	the	DET
eurjchem-976	37	17	advantages	advantage	NOUN
eurjchem-976	37	18	of	of	ADP
eurjchem-976	37	19	short	short	ADJ
eurjchem-976	37	20	reaction	reaction	NOUN
eurjchem-976	37	21	time	time	NOUN
eurjchem-976	37	22	and	and	CCONJ
eurjchem-976	37	23	high	high	ADJ
eurjchem-976	37	24	yield	yield	NOUN
eurjchem-976	37	25	.	.	PUNCT
eurjchem-976	38	1	in	in	ADP
eurjchem-976	38	2	view	view	NOUN
eurjchem-976	38	3	of	of	ADP
eurjchem-976	38	4	the	the	DET
eurjchem-976	38	5	above	above	ADJ
eurjchem-976	38	6	reports	report	NOUN
eurjchem-976	38	7	and	and	CCONJ
eurjchem-976	38	8	in	in	ADP
eurjchem-976	38	9	continuation	continuation	NOUN
eurjchem-976	38	10	of	of	ADP
eurjchem-976	38	11	our	our	PRON
eurjchem-976	38	12	research	research	NOUN
eurjchem-976	38	13	in	in	ADP
eurjchem-976	38	14	friedel‐crafts	friedel‐craft	NOUN
eurjchem-976	38	15	ring	ring	NOUN
eurjchem-976	38	16	closures	closure	NOUN
eurjchem-976	38	17	,	,	PUNCT
eurjchem-976	38	18	herein	herein	NOUN
eurjchem-976	38	19	,	,	PUNCT
eurjchem-976	38	20	we	we	PRON
eurjchem-976	38	21	wish	wish	VERB
eurjchem-976	38	22	to	to	PART
eurjchem-976	38	23	report	report	VERB
eurjchem-976	38	24	facile	facile	ADJ
eurjchem-976	38	25	and	and	CCONJ
eurjchem-976	38	26	efficient	efficient	ADJ
eurjchem-976	38	27	synthesis	synthesis	NOUN
eurjchem-976	38	28	of	of	ADP
eurjchem-976	38	29	substituted	substitute	VERB
eurjchem-976	38	30	indeno[1,2‐c]pyrazoles	indeno[1,2‐c]pyrazole	NOUN
eurjchem-976	38	31	,	,	PUNCT
eurjchem-976	38	32	2h‐benzo[g]indazoles	2h‐benzo[g]indazole	NOUN
eurjchem-976	38	33	and	and	CCONJ
eurjchem-976	38	34	benzo[6,7	benzo[6,7	NOUN
eurjchem-976	38	35	]	]	X
eurjchem-976	38	36	cyclohepta[1,2‐c]pyrazole	cyclohepta[1,2‐c]pyrazole	NOUN
eurjchem-976	38	37	via	via	ADP
eurjchem-976	38	38	friedel‐crafts	friedel‐craft	NOUN
eurjchem-976	38	39	ring	ring	NOUN
eurjchem-976	38	40	closures	closure	NOUN
eurjchem-976	38	41	of	of	ADP
eurjchem-976	38	42	heteoraryl	heteoraryl	ADJ
eurjchem-976	38	43	acids	acid	NOUN
eurjchem-976	38	44	and	and	CCONJ
eurjchem-976	38	45	alkanols	alkanol	NOUN
eurjchem-976	38	46	in	in	ADP
eurjchem-976	38	47	the	the	DET
eurjchem-976	38	48	presence	presence	NOUN
eurjchem-976	38	49	of	of	ADP
eurjchem-976	38	50	both	both	CCONJ
eurjchem-976	38	51	brönsted	brönste	VERB
eurjchem-976	38	52	and	and	CCONJ
eurjchem-976	38	53	lewis	lewis	PROPN
eurjchem-976	38	54	acid	acid	NOUN
eurjchem-976	38	55	catalysts	catalyst	NOUN
eurjchem-976	38	56	.	.	PUNCT
eurjchem-976	39	1	2	2	X
eurjchem-976	39	2	.	.	X
eurjchem-976	39	3	experimental	experimental	ADJ
eurjchem-976	39	4	2.1	2.1	NUM
eurjchem-976	39	5	.	.	PUNCT
eurjchem-976	39	6	instrumentation	instrumentation	NOUN
eurjchem-976	39	7	all	all	DET
eurjchem-976	39	8	reagents	reagent	NOUN
eurjchem-976	39	9	were	be	AUX
eurjchem-976	39	10	purchased	purchase	VERB
eurjchem-976	39	11	from	from	ADP
eurjchem-976	39	12	merck	merck	PROPN
eurjchem-976	39	13	,	,	PUNCT
eurjchem-976	39	14	sigma	sigma	NOUN
eurjchem-976	39	15	or	or	CCONJ
eurjchem-976	39	16	aldrich	aldrich	PROPN
eurjchem-976	39	17	chemical	chemical	PROPN
eurjchem-976	39	18	co.	co.	PROPN
eurjchem-976	39	19	and	and	CCONJ
eurjchem-976	39	20	were	be	AUX
eurjchem-976	39	21	used	use	VERB
eurjchem-976	39	22	without	without	ADP
eurjchem-976	39	23	further	further	ADJ
eurjchem-976	39	24	purification	purification	NOUN
eurjchem-976	39	25	.	.	PUNCT
eurjchem-976	40	1	melting	melting	NOUN
eurjchem-976	40	2	points	point	NOUN
eurjchem-976	40	3	were	be	AUX
eurjchem-976	40	4	measured	measure	VERB
eurjchem-976	40	5	on	on	ADP
eurjchem-976	40	6	a	a	DET
eurjchem-976	40	7	digital	digital	ADJ
eurjchem-976	40	8	gallenkamp	gallenkamp	ADJ
eurjchem-976	40	9	capillary	capillary	ADJ
eurjchem-976	40	10	melting	melting	NOUN
eurjchem-976	40	11	point	point	NOUN
eurjchem-976	40	12	apparatus	apparatus	NOUN
eurjchem-976	40	13	and	and	CCONJ
eurjchem-976	40	14	are	be	AUX
eurjchem-976	40	15	uncorrected	uncorrecte	VERB
eurjchem-976	40	16	.	.	PUNCT
eurjchem-976	41	1	the	the	DET
eurjchem-976	41	2	ir	ir	PROPN
eurjchem-976	41	3	spectra	spectra	PROPN
eurjchem-976	41	4	were	be	AUX
eurjchem-976	41	5	determined	determine	VERB
eurjchem-976	41	6	with	with	ADP
eurjchem-976	41	7	a	a	DET
eurjchem-976	41	8	shimadzu	shimadzu	ADJ
eurjchem-976	41	9	470	470	NUM
eurjchem-976	41	10	infrared	infrared	ADJ
eurjchem-976	41	11	spectrophotometer	spectrophotometer	NOUN
eurjchem-976	41	12	using	use	VERB
eurjchem-976	41	13	kbr	kbr	PROPN
eurjchem-976	41	14	wafer	wafer	NOUN
eurjchem-976	41	15	and	and	CCONJ
eurjchem-976	41	16	thin	thin	ADJ
eurjchem-976	41	17	film	film	NOUN
eurjchem-976	41	18	techniques	technique	NOUN
eurjchem-976	41	19	.	.	PUNCT
eurjchem-976	42	1	the	the	DET
eurjchem-976	42	2	1h	1h	NUM
eurjchem-976	42	3	and	and	CCONJ
eurjchem-976	42	4	13c	13c	NOUN
eurjchem-976	42	5	nmr	nmr	NOUN
eurjchem-976	42	6	spectra	spectra	NOUN
eurjchem-976	42	7	were	be	AUX
eurjchem-976	42	8	recorded	record	VERB
eurjchem-976	42	9	on	on	ADP
eurjchem-976	42	10	jeol	jeol	PROPN
eurjchem-976	42	11	la	la	PROPN
eurjchem-976	42	12	400	400	NUM
eurjchem-976	42	13	mhz	mhz	ADJ
eurjchem-976	42	14	ft‐nmr	ft‐nmr	NOUN
eurjchem-976	42	15	(	(	PUNCT
eurjchem-976	42	16	400	400	NUM
eurjchem-976	42	17	mhz	mhz	NOUN
eurjchem-976	42	18	for	for	ADP
eurjchem-976	42	19	1h	1h	NUM
eurjchem-976	42	20	,	,	PUNCT
eurjchem-976	42	21	100	100	NUM
eurjchem-976	42	22	mhz	mhz	NOUN
eurjchem-976	42	23	for	for	ADP
eurjchem-976	42	24	13c	13c	NOUN
eurjchem-976	42	25	)	)	PUNCT
eurjchem-976	42	26	and	and	CCONJ
eurjchem-976	42	27	on	on	ADP
eurjchem-976	42	28	varian	varian	PROPN
eurjchem-976	42	29	nmr	nmr	NOUN
eurjchem-976	42	30	(	(	PUNCT
eurjchem-976	42	31	90	90	NUM
eurjchem-976	42	32	mhz	mhz	NOUN
eurjchem-976	42	33	)	)	PUNCT
eurjchem-976	42	34	spectrometers	spectrometer	NOUN
eurjchem-976	42	35	using	use	VERB
eurjchem-976	42	36	cdcl3	cdcl3	PROPN
eurjchem-976	42	37	or	or	CCONJ
eurjchem-976	42	38	dmso‐d6	dmso‐d6	NOUN
eurjchem-976	42	39	solvents	solvent	NOUN
eurjchem-976	42	40	with	with	ADP
eurjchem-976	42	41	tms	tms	PROPN
eurjchem-976	42	42	as	as	ADP
eurjchem-976	42	43	internal	internal	ADJ
eurjchem-976	42	44	standard	standard	NOUN
eurjchem-976	42	45	.	.	PUNCT
eurjchem-976	43	1	chemical	chemical	ADJ
eurjchem-976	43	2	shifts	shift	NOUN
eurjchem-976	43	3	(	(	PUNCT
eurjchem-976	43	4	δ	δ	NOUN
eurjchem-976	43	5	)	)	PUNCT
eurjchem-976	43	6	and	and	CCONJ
eurjchem-976	43	7	j	j	PROPN
eurjchem-976	43	8	values	value	NOUN
eurjchem-976	43	9	are	be	AUX
eurjchem-976	43	10	reported	report	VERB
eurjchem-976	43	11	in	in	ADP
eurjchem-976	43	12	ppm	ppm	NOUN
eurjchem-976	43	13	and	and	CCONJ
eurjchem-976	43	14	hz	hz	NOUN
eurjchem-976	43	15	,	,	PUNCT
eurjchem-976	43	16	respectively	respectively	ADV
eurjchem-976	43	17	.	.	PUNCT
eurjchem-976	44	1	elemental	elemental	ADJ
eurjchem-976	44	2	analyses	analysis	NOUN
eurjchem-976	44	3	were	be	AUX
eurjchem-976	44	4	performed	perform	VERB
eurjchem-976	44	5	on	on	ADP
eurjchem-976	44	6	a	a	DET
eurjchem-976	44	7	perkin‐elmer	perkin‐elmer	PROPN
eurjchem-976	44	8	2400	2400	NUM
eurjchem-976	44	9	series	series	NOUN
eurjchem-976	44	10	ii	ii	PROPN
eurjchem-976	44	11	analyser	analyser	NOUN
eurjchem-976	44	12	.	.	PUNCT
eurjchem-976	45	1	the	the	DET
eurjchem-976	45	2	mass	mass	PROPN
eurjchem-976	45	3	spectra	spectra	NOUN
eurjchem-976	45	4	were	be	AUX
eurjchem-976	45	5	recorded	record	VERB
eurjchem-976	45	6	on	on	ADP
eurjchem-976	45	7	a	a	DET
eurjchem-976	45	8	jeol	jeol	PROPN
eurjchem-976	45	9	jms	jms	PROPN
eurjchem-976	45	10	600	600	NUM
eurjchem-976	45	11	spectrometer	spectrometer	NOUN
eurjchem-976	45	12	at	at	ADP
eurjchem-976	45	13	an	an	DET
eurjchem-976	45	14	ionizing	ionize	VERB
eurjchem-976	45	15	potential	potential	NOUN
eurjchem-976	45	16	of	of	ADP
eurjchem-976	45	17	70	70	NUM
eurjchem-976	45	18	ev	ev	NOUN
eurjchem-976	45	19	(	(	PUNCT
eurjchem-976	45	20	ei	ei	NOUN
eurjchem-976	45	21	)	)	PUNCT
eurjchem-976	45	22	electron	electron	NOUN
eurjchem-976	45	23	impact	impact	NOUN
eurjchem-976	45	24	ionization	ionization	NOUN
eurjchem-976	45	25	mode	mode	NOUN
eurjchem-976	45	26	using	use	VERB
eurjchem-976	45	27	the	the	DET
eurjchem-976	45	28	direct	direct	ADJ
eurjchem-976	45	29	inlet	inlet	NOUN
eurjchem-976	45	30	system	system	NOUN
eurjchem-976	45	31	.	.	PUNCT
eurjchem-976	46	1	reactions	reaction	NOUN
eurjchem-976	46	2	were	be	AUX
eurjchem-976	46	3	monitored	monitor	VERB
eurjchem-976	46	4	by	by	ADP
eurjchem-976	46	5	thin‐layer	thin‐layer	NOUN
eurjchem-976	46	6	chromatography	chromatography	NOUN
eurjchem-976	46	7	(	(	PUNCT
eurjchem-976	46	8	tlc	tlc	NOUN
eurjchem-976	46	9	)	)	PUNCT
eurjchem-976	46	10	using	use	VERB
eurjchem-976	46	11	pre‐coated	pre‐coate	VERB
eurjchem-976	46	12	silica	silica	NOUN
eurjchem-976	46	13	plates	plate	NOUN
eurjchem-976	46	14	and	and	CCONJ
eurjchem-976	46	15	visualized	visualize	VERB
eurjchem-976	46	16	with	with	ADP
eurjchem-976	46	17	uv	uv	NOUN
eurjchem-976	46	18	light	light	NOUN
eurjchem-976	46	19	.	.	PUNCT
eurjchem-976	47	1	flash	flash	NOUN
eurjchem-976	47	2	column	column	NOUN
eurjchem-976	47	3	chromatography	chromatography	NOUN
eurjchem-976	47	4	was	be	AUX
eurjchem-976	47	5	performed	perform	VERB
eurjchem-976	47	6	on	on	ADP
eurjchem-976	47	7	silica	silica	NOUN
eurjchem-976	47	8	gel	gel	NOUN
eurjchem-976	47	9	and	and	CCONJ
eurjchem-976	47	10	basic	basic	ADJ
eurjchem-976	47	11	alumina	alumina	NOUN
eurjchem-976	47	12	.	.	PUNCT
eurjchem-976	48	1	2.2	2.2	NUM
eurjchem-976	48	2	.	.	PUNCT
eurjchem-976	48	3	synthesis	synthesis	NOUN
eurjchem-976	48	4	2.2.1	2.2.1	NUM
eurjchem-976	48	5	.	.	PUNCT
eurjchem-976	49	1	5‐chloro‐1,3‐diphenyl‐1h‐pyrazole‐4‐carbaldehyde	5‐chloro‐1,3‐diphenyl‐1h‐pyrazole‐4‐carbaldehyde	NUM
eurjchem-976	49	2	(	(	PUNCT
eurjchem-976	49	3	5	5	X
eurjchem-976	49	4	)	)	PUNCT
eurjchem-976	49	5	pyrazolone	pyrazolone	NOUN
eurjchem-976	49	6	4	4	NUM
eurjchem-976	49	7	(	(	PUNCT
eurjchem-976	49	8	4.7	4.7	NUM
eurjchem-976	49	9	g	g	NOUN
eurjchem-976	49	10	,	,	PUNCT
eurjchem-976	49	11	0.02	0.02	NUM
eurjchem-976	49	12	mol	mol	NOUN
eurjchem-976	49	13	)	)	PUNCT
eurjchem-976	49	14	was	be	AUX
eurjchem-976	49	15	added	add	VERB
eurjchem-976	49	16	in	in	ADP
eurjchem-976	49	17	small	small	ADJ
eurjchem-976	49	18	portions	portion	NOUN
eurjchem-976	49	19	over	over	ADP
eurjchem-976	49	20	5	5	NUM
eurjchem-976	49	21	min	min	NOUN
eurjchem-976	49	22	to	to	ADP
eurjchem-976	49	23	an	an	DET
eurjchem-976	49	24	ice‐cold	ice‐cold	VERB
eurjchem-976	49	25	vilsmeier	vilsmeier	NOUN
eurjchem-976	49	26	reagent	reagent	NOUN
eurjchem-976	49	27	prepared	prepare	VERB
eurjchem-976	49	28	by	by	ADP
eurjchem-976	49	29	slowly	slowly	ADV
eurjchem-976	49	30	addition	addition	NOUN
eurjchem-976	49	31	of	of	ADP
eurjchem-976	49	32	pocl3	pocl3	NOUN
eurjchem-976	49	33	(	(	PUNCT
eurjchem-976	49	34	9.8	9.8	NUM
eurjchem-976	49	35	ml	ml	NOUN
eurjchem-976	49	36	,	,	PUNCT
eurjchem-976	49	37	16.12	16.12	NUM
eurjchem-976	49	38	g	g	NOUN
eurjchem-976	49	39	,	,	PUNCT
eurjchem-976	49	40	0.1	0.1	NUM
eurjchem-976	49	41	mol	mol	NOUN
eurjchem-976	49	42	)	)	PUNCT
eurjchem-976	49	43	to	to	ADP
eurjchem-976	49	44	dmf	dmf	PROPN
eurjchem-976	49	45	(	(	PUNCT
eurjchem-976	49	46	17.8	17.8	NUM
eurjchem-976	49	47	ml	ml	NOUN
eurjchem-976	49	48	,	,	PUNCT
eurjchem-976	49	49	16.8	16.8	NUM
eurjchem-976	49	50	g	g	NOUN
eurjchem-976	49	51	,	,	PUNCT
eurjchem-976	49	52	0.23	0.23	NUM
eurjchem-976	49	53	mol	mol	NOUN
eurjchem-976	49	54	)	)	PUNCT
eurjchem-976	49	55	at	at	ADP
eurjchem-976	49	56	0	0	NUM
eurjchem-976	49	57	°	°	ADP
eurjchem-976	49	58	c	c	NOUN
eurjchem-976	49	59	over	over	ADP
eurjchem-976	49	60	30	30	NUM
eurjchem-976	49	61	min	min	NOUN
eurjchem-976	49	62	.	.	PUNCT
eurjchem-976	50	1	the	the	DET
eurjchem-976	50	2	reaction	reaction	NOUN
eurjchem-976	50	3	mixture	mixture	NOUN
eurjchem-976	50	4	was	be	AUX
eurjchem-976	50	5	heated	heat	VERB
eurjchem-976	50	6	for	for	ADP
eurjchem-976	50	7	3	3	NUM
eurjchem-976	50	8	h	h	NOUN
eurjchem-976	50	9	at	at	ADP
eurjchem-976	50	10	90	90	NUM
eurjchem-976	50	11	°	°	NOUN
eurjchem-976	50	12	c	c	NOUN
eurjchem-976	50	13	then	then	ADV
eurjchem-976	50	14	cooled	cool	VERB
eurjchem-976	50	15	to	to	ADP
eurjchem-976	50	16	0	0	NUM
eurjchem-976	50	17	°	°	NOUN
eurjchem-976	50	18	c	c	NOUN
eurjchem-976	50	19	,	,	PUNCT
eurjchem-976	50	20	poured	pour	VERB
eurjchem-976	50	21	into	into	ADP
eurjchem-976	50	22	ice‐cold	ice‐cold	VERB
eurjchem-976	50	23	water	water	NOUN
eurjchem-976	50	24	(	(	PUNCT
eurjchem-976	50	25	100	100	NUM
eurjchem-976	50	26	ml	ml	NOUN
eurjchem-976	50	27	)	)	PUNCT
eurjchem-976	50	28	and	and	CCONJ
eurjchem-976	50	29	finally	finally	ADV
eurjchem-976	50	30	treated	treat	VERB
eurjchem-976	50	31	with	with	ADP
eurjchem-976	50	32	potassium	potassium	NOUN
eurjchem-976	50	33	carbonate	carbonate	NOUN
eurjchem-976	50	34	till	till	SCONJ
eurjchem-976	50	35	ph	ph	NOUN
eurjchem-976	51	1	=	=	SYM
eurjchem-976	51	2	9	9	NUM
eurjchem-976	51	3	.	.	PUNCT
eurjchem-976	52	1	the	the	DET
eurjchem-976	52	2	separated	separate	VERB
eurjchem-976	52	3	yellow	yellow	ADJ
eurjchem-976	52	4	solid	solid	ADJ
eurjchem-976	52	5	was	be	AUX
eurjchem-976	52	6	filtered	filter	VERB
eurjchem-976	52	7	,	,	PUNCT
eurjchem-976	52	8	dried	dry	VERB
eurjchem-976	52	9	and	and	CCONJ
eurjchem-976	52	10	recrystallized	recrystallize	VERB
eurjchem-976	52	11	from	from	ADP
eurjchem-976	52	12	benzene	benzene	NOUN
eurjchem-976	52	13	to	to	PART
eurjchem-976	52	14	afford	afford	VERB
eurjchem-976	52	15	(	(	PUNCT
eurjchem-976	52	16	4.4	4.4	NUM
eurjchem-976	52	17	g	g	NOUN
eurjchem-976	52	18	,	,	PUNCT
eurjchem-976	52	19	79	79	NUM
eurjchem-976	52	20	%	%	NOUN
eurjchem-976	52	21	)	)	PUNCT
eurjchem-976	52	22	of	of	ADP
eurjchem-976	52	23	pure	pure	ADJ
eurjchem-976	52	24	aldehyde	aldehyde	NOUN
eurjchem-976	52	25	5	5	NUM
eurjchem-976	52	26	(	(	PUNCT
eurjchem-976	52	27	scheme	scheme	NOUN
eurjchem-976	52	28	1	1	NUM
eurjchem-976	52	29	)	)	PUNCT
eurjchem-976	52	30	.	.	PUNCT
eurjchem-976	53	1	color	color	NOUN
eurjchem-976	53	2	:	:	PUNCT
eurjchem-976	53	3	white	white	ADJ
eurjchem-976	53	4	crystals	crystal	NOUN
eurjchem-976	53	5	.	.	PUNCT
eurjchem-976	54	1	m.p	m.p	PROPN
eurjchem-976	54	2	.	.	PROPN
eurjchem-976	54	3	:	:	PUNCT
eurjchem-976	55	1	107	107	NUM
eurjchem-976	55	2	°	°	PRON
eurjchem-976	55	3	c	c	X
eurjchem-976	55	4	(	(	PUNCT
eurjchem-976	55	5	lit	lit	ADJ
eurjchem-976	55	6	.	.	PUNCT
eurjchem-976	56	1	[	[	X
eurjchem-976	56	2	55	55	NUM
eurjchem-976	56	3	]	]	PUNCT
eurjchem-976	56	4	,	,	PUNCT
eurjchem-976	56	5	m.p	m.p	PROPN
eurjchem-976	56	6	.	.	PROPN
eurjchem-976	56	7	:	:	PUNCT
eurjchem-976	56	8	109‐111	109‐111	PROPN
eurjchem-976	56	9	c	c	NUM
eurjchem-976	56	10	)	)	PUNCT
eurjchem-976	56	11	.	.	PUNCT
eurjchem-976	57	1	ir	ir	PROPN
eurjchem-976	57	2	(	(	PUNCT
eurjchem-976	57	3	kbr	kbr	PROPN
eurjchem-976	57	4	,	,	PUNCT
eurjchem-976	57	5	ν	ν	PROPN
eurjchem-976	57	6	,	,	PUNCT
eurjchem-976	57	7	cm‐1	cm‐1	PROPN
eurjchem-976	57	8	):	):	PUNCT
eurjchem-976	57	9	3110	3110	NUM
eurjchem-976	57	10	,	,	PUNCT
eurjchem-976	57	11	3065	3065	NUM
eurjchem-976	57	12	(	(	PUNCT
eurjchem-976	57	13	ch	ch	NOUN
eurjchem-976	57	14	)	)	PUNCT
eurjchem-976	57	15	(	(	PUNCT
eurjchem-976	57	16	aromatic	aromatic	NOUN
eurjchem-976	57	17	)	)	PUNCT
eurjchem-976	57	18	,	,	PUNCT
eurjchem-976	57	19	2830	2830	NUM
eurjchem-976	57	20	,	,	PUNCT
eurjchem-976	57	21	2745	2745	NUM
eurjchem-976	57	22	(	(	PUNCT
eurjchem-976	57	23	ch	ch	NOUN
eurjchem-976	57	24	)	)	PUNCT
eurjchem-976	57	25	(	(	PUNCT
eurjchem-976	57	26	aldehyde	aldehyde	NOUN
eurjchem-976	57	27	)	)	PUNCT
eurjchem-976	57	28	,	,	PUNCT
eurjchem-976	57	29	1695	1695	NUM
eurjchem-976	57	30	(	(	PUNCT
eurjchem-976	57	31	c	c	NOUN
eurjchem-976	57	32	=	=	NOUN
eurjchem-976	57	33	o	o	NOUN
eurjchem-976	57	34	)	)	PUNCT
eurjchem-976	57	35	(	(	PUNCT
eurjchem-976	57	36	aldehyde	aldehyde	NOUN
eurjchem-976	57	37	)	)	PUNCT
eurjchem-976	57	38	,	,	PUNCT
eurjchem-976	57	39	1605	1605	NUM
eurjchem-976	57	40	,	,	PUNCT
eurjchem-976	57	41	1590	1590	NUM
eurjchem-976	57	42	,	,	PUNCT
eurjchem-976	57	43	1489	1489	NUM
eurjchem-976	57	44	,	,	PUNCT
eurjchem-976	57	45	1440	1440	NUM
eurjchem-976	57	46	(	(	PUNCT
eurjchem-976	57	47	c	c	NOUN
eurjchem-976	57	48	=	=	SYM
eurjchem-976	57	49	c	c	NOUN
eurjchem-976	57	50	)	)	PUNCT
eurjchem-976	57	51	(	(	PUNCT
eurjchem-976	57	52	aromatic	aromatic	NOUN
eurjchem-976	57	53	)	)	PUNCT
eurjchem-976	57	54	,	,	PUNCT
eurjchem-976	57	55	1360	1360	NUM
eurjchem-976	57	56	,	,	PUNCT
eurjchem-976	57	57	1189	1189	NUM
eurjchem-976	57	58	,	,	PUNCT
eurjchem-976	57	59	716	716	NUM
eurjchem-976	57	60	,	,	PUNCT
eurjchem-976	57	61	658	658	NUM
eurjchem-976	57	62	.	.	PUNCT
eurjchem-976	58	1	1h	1h	NUM
eurjchem-976	58	2	nmr	nmr	NOUN
eurjchem-976	58	3	(	(	PUNCT
eurjchem-976	58	4	90	90	NUM
eurjchem-976	58	5	mhz	mhz	NOUN
eurjchem-976	58	6	,	,	PUNCT
eurjchem-976	58	7	cdcl3	cdcl3	PROPN
eurjchem-976	58	8	,	,	PUNCT
eurjchem-976	58	9	δ	δ	PROPN
eurjchem-976	58	10	,	,	PUNCT
eurjchem-976	58	11	ppm	ppm	NUM
eurjchem-976	58	12	):	):	PUNCT
eurjchem-976	58	13	7.20‐8.90	7.20‐8.90	NUM
eurjchem-976	58	14	(	(	PUNCT
eurjchem-976	58	15	m	m	PROPN
eurjchem-976	58	16	,	,	PUNCT
eurjchem-976	58	17	10	10	NUM
eurjchem-976	58	18	h	h	NOUN
eurjchem-976	58	19	,	,	PUNCT
eurjchem-976	58	20	ar‐h	ar‐h	NOUN
eurjchem-976	58	21	)	)	PUNCT
eurjchem-976	58	22	,	,	PUNCT
eurjchem-976	58	23	10.30	10.30	NUM
eurjchem-976	58	24	(	(	PUNCT
eurjchem-976	58	25	s	s	PROPN
eurjchem-976	58	26	,	,	PUNCT
eurjchem-976	58	27	1h	1h	NUM
eurjchem-976	58	28	,	,	PUNCT
eurjchem-976	58	29	cho	cho	NOUN
eurjchem-976	58	30	)	)	PUNCT
eurjchem-976	58	31	.	.	PUNCT
eurjchem-976	59	1	ms	ms	NOUN
eurjchem-976	59	2	(	(	PUNCT
eurjchem-976	59	3	ei	ei	PROPN
eurjchem-976	59	4	,	,	PUNCT
eurjchem-976	59	5	m	m	PROPN
eurjchem-976	59	6	/	/	SYM
eurjchem-976	59	7	z	z	PROPN
eurjchem-976	59	8	(	(	PUNCT
eurjchem-976	59	9	%	%	NOUN
eurjchem-976	59	10	)	)	PUNCT
eurjchem-976	59	11	):	):	PUNCT
eurjchem-976	59	12	283	283	NUM
eurjchem-976	59	13	(	(	PUNCT
eurjchem-976	59	14	m++1	m++1	NOUN
eurjchem-976	59	15	,	,	PUNCT
eurjchem-976	59	16	45	45	NUM
eurjchem-976	59	17	)	)	PUNCT
eurjchem-976	59	18	,	,	PUNCT
eurjchem-976	59	19	284	284	NUM
eurjchem-976	59	20	(	(	PUNCT
eurjchem-976	59	21	m++2	m++2	PROPN
eurjchem-976	59	22	,	,	PUNCT
eurjchem-976	59	23	28	28	NUM
eurjchem-976	59	24	)	)	PUNCT
eurjchem-976	59	25	,	,	PUNCT
eurjchem-976	59	26	282	282	NUM
eurjchem-976	59	27	(	(	PUNCT
eurjchem-976	59	28	m+	m+	NUM
eurjchem-976	59	29	,	,	PUNCT
eurjchem-976	59	30	100	100	NUM
eurjchem-976	59	31	)	)	PUNCT
eurjchem-976	59	32	,	,	PUNCT
eurjchem-976	59	33	254	254	NUM
eurjchem-976	59	34	(	(	PUNCT
eurjchem-976	59	35	16	16	NUM
eurjchem-976	59	36	)	)	PUNCT
eurjchem-976	59	37	,	,	PUNCT
eurjchem-976	59	38	253	253	NUM
eurjchem-976	59	39	(	(	PUNCT
eurjchem-976	59	40	25	25	NUM
eurjchem-976	59	41	)	)	PUNCT
eurjchem-976	59	42	,	,	PUNCT
eurjchem-976	59	43	248	248	NUM
eurjchem-976	59	44	(	(	PUNCT
eurjchem-976	59	45	15	15	NUM
eurjchem-976	59	46	)	)	PUNCT
eurjchem-976	59	47	,	,	PUNCT
eurjchem-976	59	48	220	220	NUM
eurjchem-976	59	49	(	(	PUNCT
eurjchem-976	59	50	18	18	NUM
eurjchem-976	59	51	)	)	PUNCT
eurjchem-976	59	52	,	,	PUNCT
eurjchem-976	59	53	77	77	NUM
eurjchem-976	59	54	(	(	PUNCT
eurjchem-976	59	55	86	86	NUM
eurjchem-976	59	56	)	)	PUNCT
eurjchem-976	59	57	,	,	PUNCT
eurjchem-976	59	58	51	51	NUM
eurjchem-976	59	59	(	(	PUNCT
eurjchem-976	59	60	92	92	NUM
eurjchem-976	59	61	)	)	PUNCT
eurjchem-976	59	62	.	.	PUNCT
eurjchem-976	60	1	anal	anal	PROPN
eurjchem-976	60	2	.	.	PUNCT
eurjchem-976	60	3	calcd	calcd	NOUN
eurjchem-976	60	4	.	.	PUNCT
eurjchem-976	61	1	for	for	ADP
eurjchem-976	61	2	c16h11cln2o	c16h11cln2o	ADJ
eurjchem-976	61	3	:	:	PUNCT
eurjchem-976	61	4	c	c	NOUN
eurjchem-976	61	5	,	,	PUNCT
eurjchem-976	61	6	67.96	67.96	NUM
eurjchem-976	61	7	;	;	PUNCT
eurjchem-976	61	8	h	h	NOUN
eurjchem-976	61	9	,	,	PUNCT
eurjchem-976	61	10	3.92	3.92	NUM
eurjchem-976	61	11	;	;	PUNCT
eurjchem-976	61	12	n	n	CCONJ
eurjchem-976	61	13	,	,	PUNCT
eurjchem-976	61	14	9.91	9.91	NUM
eurjchem-976	61	15	.	.	PUNCT
eurjchem-976	61	16	found	find	VERB
eurjchem-976	61	17	:	:	PUNCT
eurjchem-976	62	1	c	c	X
eurjchem-976	62	2	,	,	PUNCT
eurjchem-976	62	3	68.25	68.25	NUM
eurjchem-976	62	4	;	;	PUNCT
eurjchem-976	62	5	h	h	NOUN
eurjchem-976	62	6	,	,	PUNCT
eurjchem-976	62	7	3.77	3.77	NUM
eurjchem-976	62	8	;	;	PUNCT
eurjchem-976	62	9	n	n	CCONJ
eurjchem-976	62	10	,	,	PUNCT
eurjchem-976	62	11	9.90	9.90	NUM
eurjchem-976	62	12	%	%	NOUN
eurjchem-976	62	13	.	.	PUNCT
eurjchem-976	63	1	2.2.2	2.2.2	NUM
eurjchem-976	63	2	.	.	X
eurjchem-976	63	3	5‐chloro‐1,3‐diphenyl‐1h‐pyrazole‐4‐carboxylic	5‐chloro‐1,3‐diphenyl‐1h‐pyrazole‐4‐carboxylic	NUM
eurjchem-976	63	4	acid	acid	NOUN
eurjchem-976	63	5	(	(	PUNCT
eurjchem-976	63	6	6	6	NUM
eurjchem-976	63	7	)	)	PUNCT
eurjchem-976	63	8	to	to	ADP
eurjchem-976	63	9	a	a	DET
eurjchem-976	63	10	solution	solution	NOUN
eurjchem-976	63	11	of	of	ADP
eurjchem-976	63	12	compound	compound	NOUN
eurjchem-976	63	13	5	5	NUM
eurjchem-976	63	14	(	(	PUNCT
eurjchem-976	63	15	4.2	4.2	NUM
eurjchem-976	63	16	g	g	NOUN
eurjchem-976	63	17	,	,	PUNCT
eurjchem-976	63	18	15	15	NUM
eurjchem-976	63	19	mmol	mmol	NOUN
eurjchem-976	63	20	)	)	PUNCT
eurjchem-976	63	21	in	in	ADP
eurjchem-976	63	22	a	a	DET
eurjchem-976	63	23	mixture	mixture	NOUN
eurjchem-976	63	24	of	of	ADP
eurjchem-976	63	25	h2o	h2o	PROPN
eurjchem-976	63	26	/	/	SYM
eurjchem-976	63	27	t‐butanol	t‐butanol	PROPN
eurjchem-976	63	28	(	(	PUNCT
eurjchem-976	63	29	1:1	1:1	NUM
eurjchem-976	63	30	,	,	PUNCT
eurjchem-976	63	31	30	30	NUM
eurjchem-976	63	32	ml	ml	NOUN
eurjchem-976	63	33	)	)	PUNCT
eurjchem-976	63	34	was	be	AUX
eurjchem-976	63	35	added	add	VERB
eurjchem-976	63	36	a	a	DET
eurjchem-976	63	37	solution	solution	NOUN
eurjchem-976	63	38	of	of	ADP
eurjchem-976	63	39	kmno4	kmno4	NOUN
eurjchem-976	63	40	(	(	PUNCT
eurjchem-976	63	41	3.3	3.3	NUM
eurjchem-976	63	42	g	g	NOUN
eurjchem-976	63	43	,	,	PUNCT
eurjchem-976	63	44	21	21	NUM
eurjchem-976	63	45	mmol	mmol	NOUN
eurjchem-976	63	46	)	)	PUNCT
eurjchem-976	63	47	in	in	ADP
eurjchem-976	63	48	h2o	h2o	PROPN
eurjchem-976	63	49	(	(	PUNCT
eurjchem-976	63	50	30	30	NUM
eurjchem-976	63	51	ml	ml	NOUN
eurjchem-976	63	52	)	)	PUNCT
eurjchem-976	63	53	at	at	ADP
eurjchem-976	63	54	70‐80	70‐80	NUM
eurjchem-976	63	55	°	°	ADP
eurjchem-976	63	56	c	c	NOUN
eurjchem-976	63	57	over	over	ADP
eurjchem-976	63	58	2	2	NUM
eurjchem-976	63	59	h.	h.	NOUN
eurjchem-976	63	60	then	then	ADV
eurjchem-976	63	61	an	an	DET
eurjchem-976	63	62	aqueous	aqueous	ADJ
eurjchem-976	63	63	solution	solution	NOUN
eurjchem-976	63	64	of	of	ADP
eurjchem-976	63	65	koh	koh	PROPN
eurjchem-976	63	66	(	(	PUNCT
eurjchem-976	63	67	10	10	NUM
eurjchem-976	63	68	%	%	NOUN
eurjchem-976	63	69	,	,	PUNCT
eurjchem-976	63	70	30	30	NUM
eurjchem-976	63	71	ml	ml	NOUN
eurjchem-976	63	72	)	)	PUNCT
eurjchem-976	63	73	was	be	AUX
eurjchem-976	63	74	added	add	VERB
eurjchem-976	63	75	while	while	SCONJ
eurjchem-976	63	76	stirring	stir	VERB
eurjchem-976	63	77	until	until	SCONJ
eurjchem-976	63	78	the	the	DET
eurjchem-976	63	79	solution	solution	NOUN
eurjchem-976	63	80	turned	turn	VERB
eurjchem-976	63	81	alkaline	alkaline	NOUN
eurjchem-976	63	82	.	.	PUNCT
eurjchem-976	64	1	the	the	DET
eurjchem-976	64	2	mixture	mixture	NOUN
eurjchem-976	64	3	was	be	AUX
eurjchem-976	64	4	filtered	filter	VERB
eurjchem-976	64	5	and	and	CCONJ
eurjchem-976	64	6	the	the	DET
eurjchem-976	64	7	clear	clear	ADJ
eurjchem-976	64	8	filtrate	filtrate	NOUN
eurjchem-976	64	9	was	be	AUX
eurjchem-976	64	10	acidified	acidify	VERB
eurjchem-976	64	11	with	with	ADP
eurjchem-976	64	12	concentrated	concentrated	ADJ
eurjchem-976	64	13	hydrochloric	hydrochloric	ADJ
eurjchem-976	64	14	acid	acid	NOUN
eurjchem-976	64	15	(	(	PUNCT
eurjchem-976	64	16	20	20	NUM
eurjchem-976	64	17	ml	ml	NOUN
eurjchem-976	64	18	,	,	PUNCT
eurjchem-976	64	19	30	30	NUM
eurjchem-976	64	20	%	%	NOUN
eurjchem-976	64	21	)	)	PUNCT
eurjchem-976	64	22	to	to	ADP
eurjchem-976	64	23	ph	ph	ADJ
eurjchem-976	64	24	=	=	SYM
eurjchem-976	64	25	2	2	NUM
eurjchem-976	64	26	.	.	X
eurjchem-976	65	1	the	the	DET
eurjchem-976	65	2	resulting	result	VERB
eurjchem-976	65	3	precipitate	precipitate	NOUN
eurjchem-976	65	4	was	be	AUX
eurjchem-976	65	5	filtered	filter	VERB
eurjchem-976	65	6	,	,	PUNCT
eurjchem-976	65	7	washed	wash	VERB
eurjchem-976	65	8	with	with	ADP
eurjchem-976	65	9	water	water	NOUN
eurjchem-976	65	10	,	,	PUNCT
eurjchem-976	65	11	dried	dry	VERB
eurjchem-976	65	12	and	and	CCONJ
eurjchem-976	65	13	crystallized	crystallize	VERB
eurjchem-976	65	14	from	from	ADP
eurjchem-976	65	15	ethanol	ethanol	NOUN
eurjchem-976	65	16	to	to	PART
eurjchem-976	65	17	give	give	VERB
eurjchem-976	65	18	(	(	PUNCT
eurjchem-976	65	19	3.8	3.8	NUM
eurjchem-976	65	20	g	g	NOUN
eurjchem-976	65	21	,	,	PUNCT
eurjchem-976	65	22	85	85	NUM
eurjchem-976	65	23	%	%	NOUN
eurjchem-976	65	24	)	)	PUNCT
eurjchem-976	65	25	of	of	ADP
eurjchem-976	65	26	pure	pure	ADJ
eurjchem-976	65	27	acid	acid	NOUN
eurjchem-976	65	28	6	6	NUM
eurjchem-976	65	29	(	(	PUNCT
eurjchem-976	65	30	scheme	scheme	NOUN
eurjchem-976	65	31	1	1	NUM
eurjchem-976	65	32	)	)	PUNCT
eurjchem-976	65	33	.	.	PUNCT
eurjchem-976	66	1	color	color	NOUN
eurjchem-976	66	2	:	:	PUNCT
eurjchem-976	66	3	white	white	ADJ
eurjchem-976	66	4	crystals	crystal	NOUN
eurjchem-976	66	5	.	.	PUNCT
eurjchem-976	67	1	m.p	m.p	PROPN
eurjchem-976	67	2	.	.	PROPN
eurjchem-976	67	3	:	:	PUNCT
eurjchem-976	67	4	183	183	NUM
eurjchem-976	67	5	°	°	SYM
eurjchem-976	67	6	c	c	X
eurjchem-976	67	7	.	.	PUNCT
eurjchem-976	68	1	ir	ir	PROPN
eurjchem-976	68	2	(	(	PUNCT
eurjchem-976	68	3	kbr	kbr	PROPN
eurjchem-976	68	4	,	,	PUNCT
eurjchem-976	68	5	ν	ν	PROPN
eurjchem-976	68	6	,	,	PUNCT
eurjchem-976	68	7	cm‐1	cm‐1	PROPN
eurjchem-976	68	8	):	):	PUNCT
eurjchem-976	68	9	3440	3440	NUM
eurjchem-976	68	10	(	(	PUNCT
eurjchem-976	68	11	oh	oh	INTJ
eurjchem-976	68	12	)	)	PUNCT
eurjchem-976	68	13	(	(	PUNCT
eurjchem-976	68	14	acid	acid	NOUN
eurjchem-976	68	15	)	)	PUNCT
eurjchem-976	68	16	,	,	PUNCT
eurjchem-976	68	17	3105	3105	NUM
eurjchem-976	68	18	(	(	PUNCT
eurjchem-976	68	19	ch	ch	NOUN
eurjchem-976	68	20	)	)	PUNCT
eurjchem-976	68	21	(	(	PUNCT
eurjchem-976	68	22	aromatic	aromatic	NOUN
eurjchem-976	68	23	)	)	PUNCT
eurjchem-976	68	24	,	,	PUNCT
eurjchem-976	68	25	1690(c	1690(c	NOUN
eurjchem-976	68	26	=	=	SYM
eurjchem-976	68	27	o	o	NOUN
eurjchem-976	68	28	)	)	PUNCT
eurjchem-976	68	29	(	(	PUNCT
eurjchem-976	68	30	acid	acid	NOUN
eurjchem-976	68	31	)	)	PUNCT
eurjchem-976	68	32	,	,	PUNCT
eurjchem-976	68	33	1610	1610	NUM
eurjchem-976	68	34	,	,	PUNCT
eurjchem-976	68	35	1585	1585	NUM
eurjchem-976	68	36	,	,	PUNCT
eurjchem-976	68	37	1473	1473	NUM
eurjchem-976	68	38	,	,	PUNCT
eurjchem-976	68	39	1440	1440	NUM
eurjchem-976	68	40	(	(	PUNCT
eurjchem-976	68	41	c	c	NOUN
eurjchem-976	68	42	=	=	SYM
eurjchem-976	68	43	c	c	NOUN
eurjchem-976	68	44	)	)	PUNCT
eurjchem-976	68	45	(	(	PUNCT
eurjchem-976	68	46	aromatic	aromatic	NOUN
eurjchem-976	68	47	)	)	PUNCT
eurjchem-976	68	48	,	,	PUNCT
eurjchem-976	68	49	1360	1360	NUM
eurjchem-976	68	50	,	,	PUNCT
eurjchem-976	68	51	1140	1140	NUM
eurjchem-976	68	52	,	,	PUNCT
eurjchem-976	68	53	755	755	NUM
eurjchem-976	68	54	.	.	NOUN
eurjchem-976	68	55	1h	1h	NUM
eurjchem-976	68	56	nmr	nmr	NOUN
eurjchem-976	68	57	(	(	PUNCT
eurjchem-976	68	58	90	90	NUM
eurjchem-976	68	59	mhz	mhz	NOUN
eurjchem-976	68	60	,	,	PUNCT
eurjchem-976	68	61	dmso‐d6	dmso‐d6	PROPN
eurjchem-976	68	62	,	,	PUNCT
eurjchem-976	68	63	δ	δ	PROPN
eurjchem-976	68	64	,	,	PUNCT
eurjchem-976	68	65	ppm	ppm	NOUN
eurjchem-976	68	66	):	):	PUNCT
eurjchem-976	68	67	7.60‐8.70	7.60‐8.70	NUM
eurjchem-976	68	68	(	(	PUNCT
eurjchem-976	68	69	m	m	PROPN
eurjchem-976	68	70	,	,	PUNCT
eurjchem-976	68	71	10h	10h	NUM
eurjchem-976	68	72	,	,	PUNCT
eurjchem-976	68	73	ar‐h	ar‐h	PROPN
eurjchem-976	68	74	)	)	PUNCT
eurjchem-976	68	75	,	,	PUNCT
eurjchem-976	68	76	11.20	11.20	NUM
eurjchem-976	68	77	(	(	PUNCT
eurjchem-976	68	78	s	s	PROPN
eurjchem-976	68	79	,	,	PUNCT
eurjchem-976	68	80	1h	1h	NUM
eurjchem-976	68	81	,	,	PUNCT
eurjchem-976	68	82	cooh	cooh	NOUN
eurjchem-976	68	83	)	)	PUNCT
eurjchem-976	68	84	.	.	PUNCT
eurjchem-976	69	1	anal	anal	PROPN
eurjchem-976	69	2	.	.	PUNCT
eurjchem-976	69	3	calcd	calcd	NOUN
eurjchem-976	69	4	.	.	PUNCT
eurjchem-976	70	1	for	for	ADP
eurjchem-976	70	2	c16h11cln2o2	c16h11cln2o2	NOUN
eurjchem-976	70	3	:	:	PUNCT
eurjchem-976	70	4	c	c	X
eurjchem-976	70	5	,	,	PUNCT
eurjchem-976	70	6	64.33	64.33	NUM
eurjchem-976	70	7	;	;	PUNCT
eurjchem-976	70	8	h	h	NOUN
eurjchem-976	70	9	,	,	PUNCT
eurjchem-976	70	10	3.71	3.71	NUM
eurjchem-976	70	11	;	;	PUNCT
eurjchem-976	70	12	n	n	CCONJ
eurjchem-976	70	13	,	,	PUNCT
eurjchem-976	70	14	9.38	9.38	NUM
eurjchem-976	70	15	.	.	PUNCT
eurjchem-976	70	16	found	find	VERB
eurjchem-976	70	17	;	;	PUNCT
eurjchem-976	70	18	c	c	X
eurjchem-976	70	19	,	,	PUNCT
eurjchem-976	70	20	64.52	64.52	NUM
eurjchem-976	70	21	;	;	PUNCT
eurjchem-976	71	1	h	h	NOUN
eurjchem-976	71	2	,	,	PUNCT
eurjchem-976	71	3	3.72	3.72	NUM
eurjchem-976	71	4	;	;	PUNCT
eurjchem-976	71	5	n	n	CCONJ
eurjchem-976	71	6	,	,	PUNCT
eurjchem-976	71	7	9.33	9.33	NUM
eurjchem-976	71	8	%	%	NOUN
eurjchem-976	71	9	.	.	PUNCT
eurjchem-976	72	1	2.2.3	2.2.3	X
eurjchem-976	72	2	.	.	X
eurjchem-976	73	1	4‐bromo‐1,3‐diphenyl‐1h‐pyrazol‐5(4h)‐one	4‐bromo‐1,3‐diphenyl‐1h‐pyrazol‐5(4h)‐one	NUM
eurjchem-976	73	2	(	(	PUNCT
eurjchem-976	73	3	9	9	NUM
eurjchem-976	73	4	)	)	PUNCT
eurjchem-976	73	5	to	to	ADP
eurjchem-976	73	6	a	a	DET
eurjchem-976	73	7	an	an	DET
eurjchem-976	73	8	ice‐cold	ice‐cold	VERB
eurjchem-976	73	9	solution	solution	NOUN
eurjchem-976	73	10	of	of	ADP
eurjchem-976	73	11	pyrazolone	pyrazolone	NOUN
eurjchem-976	73	12	4	4	NUM
eurjchem-976	73	13	(	(	PUNCT
eurjchem-976	73	14	4.7	4.7	NUM
eurjchem-976	73	15	g	g	NOUN
eurjchem-976	73	16	,	,	PUNCT
eurjchem-976	73	17	20	20	NUM
eurjchem-976	73	18	mmol	mmol	NOUN
eurjchem-976	73	19	)	)	PUNCT
eurjchem-976	73	20	in	in	ADP
eurjchem-976	73	21	acoh	acoh	ADJ
eurjchem-976	73	22	(	(	PUNCT
eurjchem-976	73	23	30	30	NUM
eurjchem-976	73	24	ml	ml	NOUN
eurjchem-976	73	25	)	)	PUNCT
eurjchem-976	73	26	was	be	AUX
eurjchem-976	73	27	added	add	VERB
eurjchem-976	73	28	a	a	DET
eurjchem-976	73	29	solution	solution	NOUN
eurjchem-976	73	30	of	of	ADP
eurjchem-976	73	31	bromine	bromine	NOUN
eurjchem-976	73	32	(	(	PUNCT
eurjchem-976	73	33	4.3	4.3	NUM
eurjchem-976	73	34	g	g	NOUN
eurjchem-976	73	35	,	,	PUNCT
eurjchem-976	73	36	27	27	NUM
eurjchem-976	73	37	mmol	mmol	NOUN
eurjchem-976	73	38	)	)	PUNCT
eurjchem-976	73	39	in	in	ADP
eurjchem-976	73	40	acoh	acoh	ADJ
eurjchem-976	73	41	(	(	PUNCT
eurjchem-976	73	42	10	10	NUM
eurjchem-976	73	43	ml	ml	NOUN
eurjchem-976	73	44	)	)	PUNCT
eurjchem-976	73	45	over	over	ADP
eurjchem-976	73	46	a	a	DET
eurjchem-976	73	47	period	period	NOUN
eurjchem-976	73	48	of	of	ADP
eurjchem-976	73	49	10	10	NUM
eurjchem-976	73	50	min	min	NOUN
eurjchem-976	73	51	at	at	ADP
eurjchem-976	73	52	5‐10	5‐10	NUM
eurjchem-976	73	53	°	°	NOUN
eurjchem-976	73	54	c	c	NOUN
eurjchem-976	73	55	.	.	PUNCT
eurjchem-976	74	1	the	the	DET
eurjchem-976	74	2	reaction	reaction	NOUN
eurjchem-976	74	3	mixture	mixture	NOUN
eurjchem-976	74	4	was	be	AUX
eurjchem-976	74	5	stirred	stir	VERB
eurjchem-976	74	6	for	for	ADP
eurjchem-976	74	7	10	10	NUM
eurjchem-976	74	8	min	min	NOUN
eurjchem-976	74	9	,	,	PUNCT
eurjchem-976	74	10	diluted	dilute	VERB
eurjchem-976	74	11	with	with	ADP
eurjchem-976	74	12	water	water	NOUN
eurjchem-976	74	13	(	(	PUNCT
eurjchem-976	74	14	100	100	NUM
eurjchem-976	74	15	ml	ml	NOUN
eurjchem-976	74	16	)	)	PUNCT
eurjchem-976	74	17	over	over	ADP
eurjchem-976	74	18	5‐10	5‐10	NUM
eurjchem-976	74	19	min	min	NOUN
eurjchem-976	74	20	and	and	CCONJ
eurjchem-976	74	21	left	leave	VERB
eurjchem-976	74	22	to	to	PART
eurjchem-976	74	23	stand	stand	VERB
eurjchem-976	74	24	in	in	ADP
eurjchem-976	74	25	refrigerator	refrigerator	NOUN
eurjchem-976	74	26	for	for	ADP
eurjchem-976	74	27	overnight	overnight	ADV
eurjchem-976	74	28	.	.	PUNCT
eurjchem-976	75	1	the	the	DET
eurjchem-976	75	2	solid	solid	ADJ
eurjchem-976	75	3	was	be	AUX
eurjchem-976	75	4	filtered	filter	VERB
eurjchem-976	75	5	,	,	PUNCT
eurjchem-976	75	6	washed	wash	VERB
eurjchem-976	75	7	with	with	ADP
eurjchem-976	75	8	acoh	acoh	ADJ
eurjchem-976	75	9	(	(	PUNCT
eurjchem-976	75	10	20	20	NUM
eurjchem-976	75	11	%	%	NOUN
eurjchem-976	75	12	)	)	PUNCT
eurjchem-976	75	13	and	and	CCONJ
eurjchem-976	75	14	dried	dry	VERB
eurjchem-976	75	15	.	.	PUNCT
eurjchem-976	76	1	crystallization	crystallization	NOUN
eurjchem-976	76	2	from	from	ADP
eurjchem-976	76	3	ethanol	ethanol	NOUN
eurjchem-976	76	4	gave	give	VERB
eurjchem-976	76	5	(	(	PUNCT
eurjchem-976	76	6	4.6	4.6	NUM
eurjchem-976	76	7	g	g	NOUN
eurjchem-976	76	8	,	,	PUNCT
eurjchem-976	76	9	74	74	NUM
eurjchem-976	76	10	%	%	NOUN
eurjchem-976	76	11	)	)	PUNCT
eurjchem-976	76	12	of	of	ADP
eurjchem-976	76	13	pure	pure	ADJ
eurjchem-976	76	14	bromopyrazolone	bromopyrazolone	NOUN
eurjchem-976	76	15	9	9	NUM
eurjchem-976	76	16	(	(	PUNCT
eurjchem-976	76	17	scheme	scheme	NOUN
eurjchem-976	76	18	1	1	NUM
eurjchem-976	76	19	)	)	PUNCT
eurjchem-976	76	20	.	.	PUNCT
eurjchem-976	77	1	color	color	NOUN
eurjchem-976	77	2	:	:	PUNCT
eurjchem-976	77	3	pale	pale	ADJ
eurjchem-976	77	4	yellow	yellow	ADJ
eurjchem-976	77	5	needless	needless	NOUN
eurjchem-976	77	6	.	.	PUNCT
eurjchem-976	78	1	m.p	m.p	PROPN
eurjchem-976	78	2	.	.	PROPN
eurjchem-976	78	3	:	:	PUNCT
eurjchem-976	79	1	117	117	NUM
eurjchem-976	79	2	°	°	SYM
eurjchem-976	79	3	c	c	X
eurjchem-976	79	4	.	.	PUNCT
eurjchem-976	80	1	ir	ir	PROPN
eurjchem-976	80	2	(	(	PUNCT
eurjchem-976	80	3	kbr	kbr	PROPN
eurjchem-976	80	4	,	,	PUNCT
eurjchem-976	80	5	ν	ν	PROPN
eurjchem-976	80	6	,	,	PUNCT
eurjchem-976	80	7	cm‐1	cm‐1	PROPN
eurjchem-976	80	8	):	):	PUNCT
eurjchem-976	80	9	3090	3090	NUM
eurjchem-976	80	10	(	(	PUNCT
eurjchem-976	80	11	ch	ch	NOUN
eurjchem-976	80	12	)	)	PUNCT
eurjchem-976	80	13	(	(	PUNCT
eurjchem-976	80	14	aromatic	aromatic	NOUN
eurjchem-976	80	15	)	)	PUNCT
eurjchem-976	80	16	,	,	PUNCT
eurjchem-976	80	17	2970	2970	NUM
eurjchem-976	80	18	(	(	PUNCT
eurjchem-976	80	19	ch	ch	NOUN
eurjchem-976	80	20	)	)	PUNCT
eurjchem-976	80	21	(	(	PUNCT
eurjchem-976	80	22	pyrazole	pyrazole	NOUN
eurjchem-976	80	23	)	)	PUNCT
eurjchem-976	80	24	,	,	PUNCT
eurjchem-976	80	25	1678	1678	NUM
eurjchem-976	80	26	(	(	PUNCT
eurjchem-976	80	27	c	c	NOUN
eurjchem-976	80	28	=	=	NOUN
eurjchem-976	80	29	o	o	NOUN
eurjchem-976	80	30	)	)	PUNCT
eurjchem-976	80	31	(	(	PUNCT
eurjchem-976	80	32	amide	amide	NOUN
eurjchem-976	80	33	)	)	PUNCT
eurjchem-976	80	34	,	,	PUNCT
eurjchem-976	80	35	1593	1593	NUM
eurjchem-976	80	36	,	,	PUNCT
eurjchem-976	80	37	1560	1560	NUM
eurjchem-976	80	38	,	,	PUNCT
eurjchem-976	80	39	1490	1490	NUM
eurjchem-976	80	40	,	,	PUNCT
eurjchem-976	80	41	1455	1455	NUM
eurjchem-976	80	42	(	(	PUNCT
eurjchem-976	80	43	c	c	NOUN
eurjchem-976	80	44	=	=	SYM
eurjchem-976	80	45	c	c	NOUN
eurjchem-976	80	46	)	)	PUNCT
eurjchem-976	80	47	(	(	PUNCT
eurjchem-976	80	48	aromatic	aromatic	NOUN
eurjchem-976	80	49	)	)	PUNCT
eurjchem-976	80	50	,	,	PUNCT
eurjchem-976	80	51	1340	1340	NUM
eurjchem-976	80	52	,	,	PUNCT
eurjchem-976	80	53	1170	1170	NUM
eurjchem-976	80	54	,	,	PUNCT
eurjchem-976	80	55	745	745	NUM
eurjchem-976	80	56	,	,	PUNCT
eurjchem-976	80	57	670	670	NUM
eurjchem-976	80	58	.	.	PUNCT
eurjchem-976	81	1	1h	1h	NUM
eurjchem-976	81	2	nmr	nmr	NOUN
eurjchem-976	81	3	(	(	PUNCT
eurjchem-976	81	4	90	90	NUM
eurjchem-976	81	5	mhz	mhz	NOUN
eurjchem-976	81	6	,	,	PUNCT
eurjchem-976	81	7	cdcl3	cdcl3	PROPN
eurjchem-976	81	8	,	,	PUNCT
eurjchem-976	81	9	δ	δ	PROPN
eurjchem-976	81	10	,	,	PUNCT
eurjchem-976	81	11	ppm	ppm	NUM
eurjchem-976	81	12	):	):	PUNCT
eurjchem-976	81	13	4.6	4.6	NUM
eurjchem-976	81	14	(	(	PUNCT
eurjchem-976	81	15	s	s	PROPN
eurjchem-976	81	16	,	,	PUNCT
eurjchem-976	81	17	1h	1h	NUM
eurjchem-976	81	18	,	,	PUNCT
eurjchem-976	81	19	ch	ch	NOUN
eurjchem-976	81	20	)	)	PUNCT
eurjchem-976	81	21	,	,	PUNCT
eurjchem-976	81	22	7.45‐8.50	7.45‐8.50	NUM
eurjchem-976	81	23	(	(	PUNCT
eurjchem-976	81	24	m	m	PROPN
eurjchem-976	81	25	,	,	PUNCT
eurjchem-976	81	26	10h	10h	NUM
eurjchem-976	81	27	,	,	PUNCT
eurjchem-976	81	28	ar‐h	ar‐h	NOUN
eurjchem-976	81	29	)	)	PUNCT
eurjchem-976	81	30	.	.	PUNCT
eurjchem-976	82	1	anal	anal	PROPN
eurjchem-976	82	2	.	.	PUNCT
eurjchem-976	82	3	calcd	calcd	NOUN
eurjchem-976	82	4	.	.	PUNCT
eurjchem-976	83	1	for	for	ADP
eurjchem-976	83	2	c15h11brn2o	c15h11brn2o	VERB
eurjchem-976	83	3	:	:	PUNCT
eurjchem-976	83	4	c	c	X
eurjchem-976	83	5	,	,	PUNCT
eurjchem-976	83	6	57.16	57.16	NUM
eurjchem-976	83	7	;	;	PUNCT
eurjchem-976	83	8	h	h	NOUN
eurjchem-976	83	9	,	,	PUNCT
eurjchem-976	83	10	3.52	3.52	NUM
eurjchem-976	83	11	;	;	PUNCT
eurjchem-976	83	12	n	n	CCONJ
eurjchem-976	83	13	,	,	PUNCT
eurjchem-976	83	14	8.89	8.89	NUM
eurjchem-976	83	15	.	.	PUNCT
eurjchem-976	83	16	found	find	VERB
eurjchem-976	83	17	;	;	PUNCT
eurjchem-976	83	18	c	c	X
eurjchem-976	83	19	,	,	PUNCT
eurjchem-976	83	20	57.05	57.05	NUM
eurjchem-976	83	21	;	;	PUNCT
eurjchem-976	84	1	h	h	NOUN
eurjchem-976	84	2	,	,	PUNCT
eurjchem-976	84	3	3.55	3.55	NUM
eurjchem-976	84	4	;	;	PUNCT
eurjchem-976	84	5	n	n	CCONJ
eurjchem-976	84	6	,	,	PUNCT
eurjchem-976	84	7	8.84	8.84	NUM
eurjchem-976	84	8	%	%	NOUN
eurjchem-976	84	9	.	.	PUNCT
eurjchem-976	85	1	2.2.4	2.2.4	X
eurjchem-976	85	2	.	.	PUNCT
eurjchem-976	85	3	general	general	ADJ
eurjchem-976	85	4	procedure	procedure	NOUN
eurjchem-976	85	5	for	for	ADP
eurjchem-976	85	6	the	the	DET
eurjchem-976	85	7	synthesis	synthesis	NOUN
eurjchem-976	85	8	of	of	ADP
eurjchem-976	85	9	substituted	substitute	VERB
eurjchem-976	85	10	acids	acid	NOUN
eurjchem-976	85	11	10a	10a	NOUN
eurjchem-976	85	12	,	,	PUNCT
eurjchem-976	85	13	b	b	NOUN
eurjchem-976	85	14	a	a	DET
eurjchem-976	85	15	solution	solution	NOUN
eurjchem-976	85	16	of	of	ADP
eurjchem-976	85	17	4‐bromo‐1,3‐diphenyl‐1h‐pyrazol‐5(4h)‐one	4‐bromo‐1,3‐diphenyl‐1h‐pyrazol‐5(4h)‐one	NUM
eurjchem-976	85	18	(	(	PUNCT
eurjchem-976	85	19	9	9	NUM
eurjchem-976	85	20	)	)	PUNCT
eurjchem-976	85	21	(	(	PUNCT
eurjchem-976	85	22	4.7	4.7	NUM
eurjchem-976	85	23	g	g	NOUN
eurjchem-976	85	24	,	,	PUNCT
eurjchem-976	85	25	15	15	NUM
eurjchem-976	85	26	mmol	mmol	NOUN
eurjchem-976	85	27	)	)	PUNCT
eurjchem-976	85	28	in	in	ADP
eurjchem-976	85	29	30	30	NUM
eurjchem-976	85	30	ml	ml	NOUN
eurjchem-976	85	31	of	of	ADP
eurjchem-976	85	32	dry	dry	ADJ
eurjchem-976	85	33	benzene	benzene	NOUN
eurjchem-976	85	34	was	be	AUX
eurjchem-976	85	35	added	add	VERB
eurjchem-976	85	36	dropwise	dropwise	NOUN
eurjchem-976	85	37	over	over	ADP
eurjchem-976	85	38	40	40	NUM
eurjchem-976	85	39	minutes	minute	NOUN
eurjchem-976	85	40	to	to	ADP
eurjchem-976	85	41	an	an	DET
eurjchem-976	85	42	ice‐cold	ice‐cold	ADJ
eurjchem-976	85	43	suspension	suspension	NOUN
eurjchem-976	85	44	of	of	ADP
eurjchem-976	85	45	sodio‐	sodio‐	NOUN
eurjchem-976	85	46	malonic	malonic	ADJ
eurjchem-976	85	47	ester	ester	NOUN
eurjchem-976	85	48	prepared	prepare	VERB
eurjchem-976	85	49	from	from	ADP
eurjchem-976	85	50	sodium	sodium	NOUN
eurjchem-976	85	51	(	(	PUNCT
eurjchem-976	85	52	1.0	1.0	NUM
eurjchem-976	85	53	g	g	NOUN
eurjchem-976	85	54	,	,	PUNCT
eurjchem-976	85	55	45	45	NUM
eurjchem-976	85	56	mmol	mmol	NOUN
eurjchem-976	85	57	)	)	PUNCT
eurjchem-976	85	58	and	and	CCONJ
eurjchem-976	85	59	substituted	substitute	VERB
eurjchem-976	85	60	diethyl	diethyl	NOUN
eurjchem-976	85	61	malonate	malonate	NOUN
eurjchem-976	85	62	(	(	PUNCT
eurjchem-976	85	63	5.3	5.3	NUM
eurjchem-976	85	64	g	g	NOUN
eurjchem-976	85	65	,	,	PUNCT
eurjchem-976	85	66	33	33	NUM
eurjchem-976	85	67	mmol	mmol	NOUN
eurjchem-976	85	68	)	)	PUNCT
eurjchem-976	85	69	in	in	ADP
eurjchem-976	85	70	30	30	NUM
eurjchem-976	85	71	ml	ml	NOUN
eurjchem-976	85	72	of	of	ADP
eurjchem-976	85	73	absolute	absolute	ADJ
eurjchem-976	85	74	ethanol	ethanol	NOUN
eurjchem-976	85	75	.	.	PUNCT
eurjchem-976	86	1	after	after	ADP
eurjchem-976	86	2	complete	complete	ADJ
eurjchem-976	86	3	addition	addition	NOUN
eurjchem-976	86	4	,	,	PUNCT
eurjchem-976	86	5	the	the	DET
eurjchem-976	86	6	reaction	reaction	NOUN
eurjchem-976	86	7	mixture	mixture	NOUN
eurjchem-976	86	8	was	be	AUX
eurjchem-976	86	9	kept	keep	VERB
eurjchem-976	86	10	in	in	ADP
eurjchem-976	86	11	a	a	DET
eurjchem-976	86	12	refrigerator	refrigerator	NOUN
eurjchem-976	86	13	for	for	ADP
eurjchem-976	86	14	24	24	NUM
eurjchem-976	86	15	h	h	NOUN
eurjchem-976	86	16	and	and	CCONJ
eurjchem-976	86	17	then	then	ADV
eurjchem-976	86	18	refluxed	refluxe	VERB
eurjchem-976	86	19	for	for	ADP
eurjchem-976	86	20	4	4	NUM
eurjchem-976	86	21	h.	h.	NOUN
eurjchem-976	86	22	the	the	DET
eurjchem-976	86	23	solvents	solvent	NOUN
eurjchem-976	86	24	were	be	AUX
eurjchem-976	86	25	evaporated	evaporate	VERB
eurjchem-976	86	26	and	and	CCONJ
eurjchem-976	86	27	the	the	DET
eurjchem-976	86	28	resulting	result	VERB
eurjchem-976	86	29	ester	ester	NOUN
eurjchem-976	86	30	was	be	AUX
eurjchem-976	86	31	refluxed	refluxe	VERB
eurjchem-976	86	32	for	for	ADP
eurjchem-976	86	33	2h	2h	NUM
eurjchem-976	86	34	with	with	ADP
eurjchem-976	86	35	koh	koh	PROPN
eurjchem-976	86	36	solution	solution	NOUN
eurjchem-976	86	37	(	(	PUNCT
eurjchem-976	86	38	25	25	NUM
eurjchem-976	86	39	ml	ml	NOUN
eurjchem-976	86	40	,	,	PUNCT
eurjchem-976	86	41	30	30	NUM
eurjchem-976	86	42	%	%	NOUN
eurjchem-976	86	43	)	)	PUNCT
eurjchem-976	86	44	.	.	PUNCT
eurjchem-976	87	1	the	the	DET
eurjchem-976	87	2	mixture	mixture	NOUN
eurjchem-976	87	3	was	be	AUX
eurjchem-976	87	4	diluted	dilute	VERB
eurjchem-976	87	5	with	with	ADP
eurjchem-976	87	6	water	water	NOUN
eurjchem-976	87	7	(	(	PUNCT
eurjchem-976	87	8	30	30	NUM
eurjchem-976	87	9	ml	ml	NOUN
eurjchem-976	87	10	)	)	PUNCT
eurjchem-976	87	11	,	,	PUNCT
eurjchem-976	87	12	refluxed	refluxe	VERB
eurjchem-976	87	13	for	for	ADP
eurjchem-976	87	14	an	an	DET
eurjchem-976	87	15	additional	additional	ADJ
eurjchem-976	87	16	1	1	NUM
eurjchem-976	87	17	h	h	NOUN
eurjchem-976	87	18	,	,	PUNCT
eurjchem-976	87	19	cooled	cool	VERB
eurjchem-976	87	20	and	and	CCONJ
eurjchem-976	87	21	acidified	acidify	VERB
eurjchem-976	87	22	with	with	ADP
eurjchem-976	87	23	hcl	hcl	PROPN
eurjchem-976	87	24	solution	solution	NOUN
eurjchem-976	87	25	(	(	PUNCT
eurjchem-976	87	26	40	40	NUM
eurjchem-976	87	27	ml	ml	NOUN
eurjchem-976	87	28	,	,	PUNCT
eurjchem-976	87	29	30	30	NUM
eurjchem-976	87	30	%	%	NOUN
eurjchem-976	87	31	)	)	PUNCT
eurjchem-976	87	32	.	.	PUNCT
eurjchem-976	88	1	the	the	DET
eurjchem-976	88	2	crude	crude	ADJ
eurjchem-976	88	3	substituted	substitute	VERB
eurjchem-976	88	4	malonic	malonic	ADJ
eurjchem-976	88	5	acid	acid	NOUN
eurjchem-976	88	6	was	be	AUX
eurjchem-976	88	7	filtered	filter	VERB
eurjchem-976	88	8	,	,	PUNCT
eurjchem-976	88	9	washed	wash	VERB
eurjchem-976	88	10	with	with	ADP
eurjchem-976	88	11	water	water	NOUN
eurjchem-976	88	12	and	and	CCONJ
eurjchem-976	88	13	dried	dry	VERB
eurjchem-976	88	14	.	.	PUNCT
eurjchem-976	89	1	el‐aal	el‐aal	PROPN
eurjchem-976	89	2	et	et	NOUN
eurjchem-976	89	3	al	al	PROPN
eurjchem-976	89	4	.	.	PUNCT
eurjchem-976	89	5	/	/	SYM
eurjchem-976	89	6	european	european	PROPN
eurjchem-976	89	7	journal	journal	PROPN
eurjchem-976	89	8	of	of	ADP
eurjchem-976	89	9	chemistry	chemistry	NOUN
eurjchem-976	89	10	5	5	NUM
eurjchem-976	89	11	(	(	PUNCT
eurjchem-976	89	12	2	2	NUM
eurjchem-976	89	13	)	)	PUNCT
eurjchem-976	89	14	(	(	PUNCT
eurjchem-976	89	15	2014	2014	NUM
eurjchem-976	89	16	)	)	PUNCT
eurjchem-976	90	1	277‐286	277‐286	NUM
eurjchem-976	90	2	279	279	NUM
eurjchem-976	90	3	reagents	reagent	NOUN
eurjchem-976	90	4	and	and	CCONJ
eurjchem-976	90	5	conditions	condition	NOUN
eurjchem-976	90	6	:	:	PUNCT
eurjchem-976	90	7	(	(	PUNCT
eurjchem-976	90	8	i	i	NOUN
eurjchem-976	90	9	)	)	PUNCT
eurjchem-976	90	10	pocl3	pocl3	PROPN
eurjchem-976	90	11	/	/	SYM
eurjchem-976	90	12	dmf	dmf	PROPN
eurjchem-976	90	13	,	,	PUNCT
eurjchem-976	90	14	90	90	NUM
eurjchem-976	90	15	°	°	NOUN
eurjchem-976	90	16	c	c	NOUN
eurjchem-976	90	17	,	,	PUNCT
eurjchem-976	90	18	3	3	NUM
eurjchem-976	90	19	h	h	NOUN
eurjchem-976	90	20	,	,	PUNCT
eurjchem-976	90	21	k2co3	k2co3	ADJ
eurjchem-976	90	22	,	,	PUNCT
eurjchem-976	90	23	(	(	PUNCT
eurjchem-976	90	24	ii	ii	NOUN
eurjchem-976	90	25	)	)	PUNCT
eurjchem-976	90	26	kmno4	kmno4	PROPN
eurjchem-976	90	27	,	,	PUNCT
eurjchem-976	90	28	h2o	h2o	PROPN
eurjchem-976	90	29	/	/	SYM
eurjchem-976	90	30	t‐butanol	t‐butanol	NUM
eurjchem-976	90	31	,	,	PUNCT
eurjchem-976	90	32	70‐80	70‐80	NUM
eurjchem-976	90	33	°	°	NOUN
eurjchem-976	90	34	c	c	NOUN
eurjchem-976	90	35	,	,	PUNCT
eurjchem-976	90	36	2	2	NUM
eurjchem-976	90	37	h	h	NOUN
eurjchem-976	90	38	,	,	PUNCT
eurjchem-976	90	39	(	(	PUNCT
eurjchem-976	90	40	iii	iii	NOUN
eurjchem-976	90	41	)	)	PUNCT
eurjchem-976	90	42	etoh	etoh	PROPN
eurjchem-976	90	43	/	/	SYM
eurjchem-976	90	44	h2so4	h2so4	PROPN
eurjchem-976	90	45	,	,	PUNCT
eurjchem-976	90	46	8h	8h	PROPN
eurjchem-976	90	47	,	,	PUNCT
eurjchem-976	90	48	reflux	reflux	NOUN
eurjchem-976	90	49	,	,	PUNCT
eurjchem-976	90	50	na2co3	na2co3	PROPN
eurjchem-976	90	51	,	,	PUNCT
eurjchem-976	90	52	(	(	PUNCT
eurjchem-976	90	53	iv	iv	X
eurjchem-976	90	54	)	)	PUNCT
eurjchem-976	90	55	memgi	memgi	NOUN
eurjchem-976	90	56	,	,	PUNCT
eurjchem-976	90	57	thf	thf	NOUN
eurjchem-976	90	58	/	/	SYM
eurjchem-976	90	59	et2o	et2o	PROPN
eurjchem-976	90	60	,	,	PUNCT
eurjchem-976	90	61	rt	rt	PROPN
eurjchem-976	90	62	,	,	PUNCT
eurjchem-976	90	63	nh4cl	nh4cl	PROPN
eurjchem-976	90	64	soln	soln	NOUN
eurjchem-976	90	65	(	(	PUNCT
eurjchem-976	90	66	table	table	NOUN
eurjchem-976	90	67	1	1	NUM
eurjchem-976	90	68	)	)	PUNCT
eurjchem-976	90	69	,	,	PUNCT
eurjchem-976	90	70	(	(	PUNCT
eurjchem-976	90	71	v	v	NOUN
eurjchem-976	90	72	)	)	PUNCT
eurjchem-976	90	73	br2	br2	PROPN
eurjchem-976	90	74	/	/	SYM
eurjchem-976	90	75	acoh	acoh	ADJ
eurjchem-976	90	76	,	,	PUNCT
eurjchem-976	90	77	5‐10	5‐10	NUM
eurjchem-976	90	78	°	°	NOUN
eurjchem-976	90	79	c	c	NOUN
eurjchem-976	90	80	,	,	PUNCT
eurjchem-976	90	81	20	20	NUM
eurjchem-976	90	82	min	min	NOUN
eurjchem-976	90	83	,	,	PUNCT
eurjchem-976	90	84	(	(	PUNCT
eurjchem-976	90	85	vi	vi	NOUN
eurjchem-976	90	86	)	)	PUNCT
eurjchem-976	90	87	(	(	PUNCT
eurjchem-976	90	88	a	a	X
eurjchem-976	90	89	)	)	PUNCT
eurjchem-976	90	90	nach(cooet)2	nach(cooet)2	PROPN
eurjchem-976	90	91	,	,	PUNCT
eurjchem-976	90	92	koh	koh	PROPN
eurjchem-976	90	93	,	,	PUNCT
eurjchem-976	90	94	24	24	NUM
eurjchem-976	90	95	h	h	NOUN
eurjchem-976	90	96	,	,	PUNCT
eurjchem-976	90	97	(	(	PUNCT
eurjchem-976	90	98	b	b	NOUN
eurjchem-976	90	99	)	)	PUNCT
eurjchem-976	90	100	heated	heat	VERB
eurjchem-976	90	101	at	at	ADP
eurjchem-976	90	102	190‐200	190‐200	NUM
eurjchem-976	90	103	°	°	SYM
eurjchem-976	90	104	c	c	NOUN
eurjchem-976	90	105	.	.	PUNCT
eurjchem-976	91	1	scheme	scheme	NOUN
eurjchem-976	91	2	1	1	NUM
eurjchem-976	91	3	the	the	DET
eurjchem-976	91	4	acid	acid	NOUN
eurjchem-976	91	5	was	be	AUX
eurjchem-976	91	6	then	then	ADV
eurjchem-976	91	7	heated	heated	ADJ
eurjchem-976	91	8	at	at	ADP
eurjchem-976	91	9	190‐200	190‐200	NUM
eurjchem-976	91	10	°	°	ADP
eurjchem-976	91	11	c	c	NOUN
eurjchem-976	91	12	in	in	ADP
eurjchem-976	91	13	an	an	DET
eurjchem-976	91	14	oil	oil	NOUN
eurjchem-976	91	15	bath	bath	NOUN
eurjchem-976	91	16	with	with	ADP
eurjchem-976	91	17	stirring	stir	VERB
eurjchem-976	91	18	for	for	ADP
eurjchem-976	91	19	20	20	NUM
eurjchem-976	91	20	minutes	minute	NOUN
eurjchem-976	91	21	and	and	CCONJ
eurjchem-976	91	22	the	the	DET
eurjchem-976	91	23	melt	melt	NOUN
eurjchem-976	91	24	was	be	AUX
eurjchem-976	91	25	poured	pour	VERB
eurjchem-976	91	26	into	into	ADP
eurjchem-976	91	27	20	20	NUM
eurjchem-976	91	28	ml	ml	NOUN
eurjchem-976	91	29	of	of	ADP
eurjchem-976	91	30	acetone	acetone	NOUN
eurjchem-976	91	31	.	.	PUNCT
eurjchem-976	92	1	the	the	DET
eurjchem-976	92	2	acetone	acetone	NOUN
eurjchem-976	92	3	solution	solution	NOUN
eurjchem-976	92	4	was	be	AUX
eurjchem-976	92	5	treated	treat	VERB
eurjchem-976	92	6	with	with	ADP
eurjchem-976	92	7	charcoal	charcoal	NOUN
eurjchem-976	92	8	,	,	PUNCT
eurjchem-976	92	9	warmed	warm	VERB
eurjchem-976	92	10	,	,	PUNCT
eurjchem-976	92	11	filtered	filter	VERB
eurjchem-976	92	12	and	and	CCONJ
eurjchem-976	92	13	the	the	DET
eurjchem-976	92	14	solvent	solvent	NOUN
eurjchem-976	92	15	was	be	AUX
eurjchem-976	92	16	evaporated	evaporate	VERB
eurjchem-976	92	17	to	to	PART
eurjchem-976	92	18	afford	afford	VERB
eurjchem-976	92	19	crude	crude	ADJ
eurjchem-976	92	20	acids	acid	NOUN
eurjchem-976	92	21	.	.	PUNCT
eurjchem-976	93	1	crystallization	crystallization	NOUN
eurjchem-976	93	2	from	from	ADP
eurjchem-976	93	3	suitable	suitable	ADJ
eurjchem-976	93	4	solvents	solvent	NOUN
eurjchem-976	93	5	gave	give	VERB
eurjchem-976	93	6	pure	pure	ADJ
eurjchem-976	93	7	acids	acid	NOUN
eurjchem-976	93	8	10a	10a	NOUN
eurjchem-976	93	9	,	,	PUNCT
eurjchem-976	93	10	b	b	PROPN
eurjchem-976	93	11	(	(	PUNCT
eurjchem-976	93	12	scheme	scheme	NOUN
eurjchem-976	93	13	1	1	NUM
eurjchem-976	93	14	)	)	PUNCT
eurjchem-976	93	15	.	.	PUNCT
eurjchem-976	94	1	analytical	analytical	ADJ
eurjchem-976	94	2	,	,	PUNCT
eurjchem-976	94	3	physical	physical	ADJ
eurjchem-976	94	4	and	and	CCONJ
eurjchem-976	94	5	spectroscopic	spectroscopic	ADJ
eurjchem-976	94	6	data	datum	NOUN
eurjchem-976	94	7	are	be	AUX
eurjchem-976	94	8	given	give	VERB
eurjchem-976	94	9	in	in	ADP
eurjchem-976	94	10	the	the	DET
eurjchem-976	94	11	following	following	NOUN
eurjchem-976	94	12	:	:	PUNCT
eurjchem-976	94	13	2‐(4,5‐dihydro‐5‐oxo‐1,3‐diphenyl‐1h‐pyrazol‐4‐yl)acetic	2‐(4,5‐dihydro‐5‐oxo‐1,3‐diphenyl‐1h‐pyrazol‐4‐yl)acetic	ADJ
eurjchem-976	94	14	acid	acid	NOUN
eurjchem-976	94	15	(	(	PUNCT
eurjchem-976	94	16	10a	10a	NUM
eurjchem-976	94	17	):	):	PUNCT
eurjchem-976	94	18	color	color	NOUN
eurjchem-976	94	19	:	:	PUNCT
eurjchem-976	94	20	pale	pale	ADJ
eurjchem-976	94	21	yellow	yellow	ADJ
eurjchem-976	94	22	crystals	crystal	NOUN
eurjchem-976	94	23	.	.	PUNCT
eurjchem-976	95	1	yield	yield	NOUN
eurjchem-976	95	2	:	:	PUNCT
eurjchem-976	95	3	82	82	NUM
eurjchem-976	95	4	%	%	NOUN
eurjchem-976	95	5	.	.	PUNCT
eurjchem-976	96	1	m.p	m.p	PROPN
eurjchem-976	96	2	.	.	PROPN
eurjchem-976	96	3	:	:	PUNCT
eurjchem-976	97	1	124	124	NUM
eurjchem-976	97	2	°	°	NUM
eurjchem-976	97	3	c	c	NOUN
eurjchem-976	97	4	(	(	PUNCT
eurjchem-976	97	5	benzene	benzene	NOUN
eurjchem-976	97	6	)	)	PUNCT
eurjchem-976	97	7	.	.	PUNCT
eurjchem-976	98	1	ir	ir	PROPN
eurjchem-976	98	2	(	(	PUNCT
eurjchem-976	98	3	kbr	kbr	PROPN
eurjchem-976	98	4	,	,	PUNCT
eurjchem-976	98	5	ν	ν	PROPN
eurjchem-976	98	6	,	,	PUNCT
eurjchem-976	98	7	cm‐1	cm‐1	PROPN
eurjchem-976	98	8	):	):	PUNCT
eurjchem-976	98	9	3370	3370	NUM
eurjchem-976	98	10	(	(	PUNCT
eurjchem-976	98	11	oh	oh	INTJ
eurjchem-976	98	12	)	)	PUNCT
eurjchem-976	98	13	(	(	PUNCT
eurjchem-976	98	14	acid	acid	NOUN
eurjchem-976	98	15	)	)	PUNCT
eurjchem-976	98	16	,	,	PUNCT
eurjchem-976	98	17	3085	3085	NUM
eurjchem-976	98	18	(	(	PUNCT
eurjchem-976	98	19	ch	ch	NOUN
eurjchem-976	98	20	)	)	PUNCT
eurjchem-976	98	21	(	(	PUNCT
eurjchem-976	98	22	aromatic	aromatic	NOUN
eurjchem-976	98	23	)	)	PUNCT
eurjchem-976	98	24	,	,	PUNCT
eurjchem-976	98	25	2950	2950	NUM
eurjchem-976	98	26	(	(	PUNCT
eurjchem-976	98	27	ch	ch	NOUN
eurjchem-976	98	28	)	)	PUNCT
eurjchem-976	98	29	(	(	PUNCT
eurjchem-976	98	30	alkyl	alkyl	NOUN
eurjchem-976	98	31	)	)	PUNCT
eurjchem-976	98	32	,	,	PUNCT
eurjchem-976	98	33	1720	1720	NUM
eurjchem-976	98	34	(	(	PUNCT
eurjchem-976	98	35	c	c	NOUN
eurjchem-976	98	36	=	=	NOUN
eurjchem-976	98	37	o	o	NOUN
eurjchem-976	98	38	)	)	PUNCT
eurjchem-976	98	39	(	(	PUNCT
eurjchem-976	98	40	acid	acid	NOUN
eurjchem-976	98	41	)	)	PUNCT
eurjchem-976	98	42	,	,	PUNCT
eurjchem-976	98	43	1674	1674	NUM
eurjchem-976	98	44	(	(	PUNCT
eurjchem-976	98	45	c	c	NOUN
eurjchem-976	98	46	=	=	NOUN
eurjchem-976	98	47	o	o	NOUN
eurjchem-976	98	48	)	)	PUNCT
eurjchem-976	98	49	(	(	PUNCT
eurjchem-976	98	50	amide	amide	NOUN
eurjchem-976	98	51	)	)	PUNCT
eurjchem-976	98	52	,	,	PUNCT
eurjchem-976	98	53	1610	1610	NUM
eurjchem-976	98	54	,	,	PUNCT
eurjchem-976	98	55	1590	1590	NUM
eurjchem-976	98	56	,	,	PUNCT
eurjchem-976	98	57	1460	1460	NUM
eurjchem-976	98	58	,	,	PUNCT
eurjchem-976	98	59	1445	1445	NUM
eurjchem-976	98	60	(	(	PUNCT
eurjchem-976	98	61	c	c	NOUN
eurjchem-976	98	62	=	=	SYM
eurjchem-976	98	63	c	c	NOUN
eurjchem-976	98	64	)	)	PUNCT
eurjchem-976	98	65	(	(	PUNCT
eurjchem-976	98	66	aromatic	aromatic	NOUN
eurjchem-976	98	67	)	)	PUNCT
eurjchem-976	98	68	,	,	PUNCT
eurjchem-976	98	69	1335	1335	NUM
eurjchem-976	98	70	,	,	PUNCT
eurjchem-976	98	71	1180	1180	NUM
eurjchem-976	98	72	,	,	PUNCT
eurjchem-976	98	73	745	745	NUM
eurjchem-976	98	74	.	.	PUNCT
eurjchem-976	99	1	1h	1h	NUM
eurjchem-976	99	2	nmr	nmr	NOUN
eurjchem-976	99	3	(	(	PUNCT
eurjchem-976	99	4	90	90	NUM
eurjchem-976	99	5	mhz	mhz	NOUN
eurjchem-976	99	6	,	,	PUNCT
eurjchem-976	99	7	cdcl3	cdcl3	PROPN
eurjchem-976	99	8	,	,	PUNCT
eurjchem-976	99	9	δ	δ	PROPN
eurjchem-976	99	10	,	,	PUNCT
eurjchem-976	99	11	ppm	ppm	NOUN
eurjchem-976	99	12	):	):	PUNCT
eurjchem-976	99	13	2.61	2.61	NUM
eurjchem-976	99	14	(	(	PUNCT
eurjchem-976	99	15	t	t	PROPN
eurjchem-976	99	16	,	,	PUNCT
eurjchem-976	99	17	1	1	NUM
eurjchem-976	99	18	ha	ha	INTJ
eurjchem-976	99	19	,	,	PUNCT
eurjchem-976	99	20	j	j	PROPN
eurjchem-976	99	21	=	=	PROPN
eurjchem-976	99	22	14.2	14.2	NUM
eurjchem-976	99	23	hz	hz	NOUN
eurjchem-976	99	24	,	,	PUNCT
eurjchem-976	99	25	ch2	ch2	PROPN
eurjchem-976	99	26	)	)	PUNCT
eurjchem-976	99	27	,	,	PUNCT
eurjchem-976	99	28	2.75	2.75	NUM
eurjchem-976	99	29	(	(	PUNCT
eurjchem-976	99	30	t	t	PROPN
eurjchem-976	99	31	,	,	PUNCT
eurjchem-976	99	32	1hb	1hb	NOUN
eurjchem-976	99	33	,	,	PUNCT
eurjchem-976	99	34	j	j	PROPN
eurjchem-976	99	35	=	=	PROPN
eurjchem-976	99	36	14.2	14.2	NUM
eurjchem-976	99	37	hz	hz	NOUN
eurjchem-976	99	38	,	,	PUNCT
eurjchem-976	99	39	ch2	ch2	PROPN
eurjchem-976	99	40	)	)	PUNCT
eurjchem-976	99	41	,	,	PUNCT
eurjchem-976	99	42	2.82	2.82	NUM
eurjchem-976	99	43	(	(	PUNCT
eurjchem-976	99	44	app	app	PROPN
eurjchem-976	99	45	.	.	PROPN
eurjchem-976	99	46	t	t	PROPN
eurjchem-976	99	47	,	,	PUNCT
eurjchem-976	99	48	1h	1h	NUM
eurjchem-976	99	49	,	,	PUNCT
eurjchem-976	99	50	j	j	PROPN
eurjchem-976	99	51	=	=	PROPN
eurjchem-976	99	52	10.4	10.4	NUM
eurjchem-976	99	53	hz	hz	NOUN
eurjchem-976	99	54	,	,	PUNCT
eurjchem-976	99	55	ch	ch	NOUN
eurjchem-976	99	56	)	)	PUNCT
eurjchem-976	99	57	,	,	PUNCT
eurjchem-976	99	58	7.30‐8.55	7.30‐8.55	ADP
eurjchem-976	99	59	(	(	PUNCT
eurjchem-976	99	60	m	m	PROPN
eurjchem-976	99	61	,	,	PUNCT
eurjchem-976	99	62	10h	10h	NUM
eurjchem-976	99	63	,	,	PUNCT
eurjchem-976	99	64	ar‐h	ar‐h	PROPN
eurjchem-976	99	65	)	)	PUNCT
eurjchem-976	99	66	,	,	PUNCT
eurjchem-976	99	67	10.9	10.9	NUM
eurjchem-976	99	68	(	(	PUNCT
eurjchem-976	99	69	s	s	PROPN
eurjchem-976	99	70	,	,	PUNCT
eurjchem-976	99	71	1h	1h	NUM
eurjchem-976	99	72	,	,	PUNCT
eurjchem-976	99	73	cooh	cooh	NOUN
eurjchem-976	99	74	)	)	PUNCT
eurjchem-976	99	75	.	.	PUNCT
eurjchem-976	100	1	anal	anal	PROPN
eurjchem-976	100	2	.	.	PUNCT
eurjchem-976	100	3	calcd	calcd	NOUN
eurjchem-976	100	4	.	.	PUNCT
eurjchem-976	101	1	for	for	ADP
eurjchem-976	101	2	c17h14n2o3	c17h14n2o3	PROPN
eurjchem-976	101	3	:	:	PUNCT
eurjchem-976	101	4	c	c	X
eurjchem-976	101	5	,	,	PUNCT
eurjchem-976	101	6	69.38	69.38	NUM
eurjchem-976	101	7	;	;	PUNCT
eurjchem-976	101	8	h	h	NOUN
eurjchem-976	101	9	,	,	PUNCT
eurjchem-976	101	10	4.79	4.79	NUM
eurjchem-976	101	11	;	;	PUNCT
eurjchem-976	101	12	n	n	CCONJ
eurjchem-976	101	13	,	,	PUNCT
eurjchem-976	101	14	9.52	9.52	NUM
eurjchem-976	101	15	.	.	PUNCT
eurjchem-976	101	16	found	find	VERB
eurjchem-976	101	17	;	;	PUNCT
eurjchem-976	101	18	c	c	X
eurjchem-976	101	19	,	,	PUNCT
eurjchem-976	101	20	69.25	69.25	NUM
eurjchem-976	101	21	;	;	PUNCT
eurjchem-976	102	1	h	h	NOUN
eurjchem-976	102	2	,	,	PUNCT
eurjchem-976	102	3	4.56	4.56	NUM
eurjchem-976	102	4	;	;	PUNCT
eurjchem-976	102	5	n	n	CCONJ
eurjchem-976	102	6	,	,	PUNCT
eurjchem-976	102	7	9.50	9.50	NUM
eurjchem-976	102	8	%	%	NOUN
eurjchem-976	102	9	.	.	PUNCT
eurjchem-976	103	1	2‐(4,5‐dihydro‐5‐oxo‐1,3‐diphenyl‐1h‐pyrazol‐4‐yl	2‐(4,5‐dihydro‐5‐oxo‐1,3‐diphenyl‐1h‐pyrazol‐4‐yl	NUM
eurjchem-976	103	2	)	)	PUNCT
eurjchem-976	103	3	propanoic	propanoic	ADJ
eurjchem-976	103	4	acid	acid	NOUN
eurjchem-976	103	5	(	(	PUNCT
eurjchem-976	103	6	10b	10b	NOUN
eurjchem-976	103	7	):	):	PUNCT
eurjchem-976	103	8	color	color	NOUN
eurjchem-976	103	9	:	:	PUNCT
eurjchem-976	103	10	white	white	ADJ
eurjchem-976	103	11	crystals	crystal	NOUN
eurjchem-976	103	12	.	.	PUNCT
eurjchem-976	104	1	yield	yield	NOUN
eurjchem-976	104	2	:	:	PUNCT
eurjchem-976	104	3	75	75	NUM
eurjchem-976	104	4	%	%	NOUN
eurjchem-976	104	5	.	.	PUNCT
eurjchem-976	105	1	m.p	m.p	PROPN
eurjchem-976	105	2	.	.	PROPN
eurjchem-976	105	3	:	:	PUNCT
eurjchem-976	106	1	95	95	NUM
eurjchem-976	106	2	°	°	NUM
eurjchem-976	106	3	c	c	NOUN
eurjchem-976	106	4	(	(	PUNCT
eurjchem-976	106	5	ethanol	ethanol	NOUN
eurjchem-976	106	6	)	)	PUNCT
eurjchem-976	106	7	.	.	PUNCT
eurjchem-976	107	1	ir	ir	PROPN
eurjchem-976	107	2	(	(	PUNCT
eurjchem-976	107	3	kbr	kbr	PROPN
eurjchem-976	107	4	,	,	PUNCT
eurjchem-976	107	5	ν	ν	PROPN
eurjchem-976	107	6	,	,	PUNCT
eurjchem-976	107	7	cm‐1	cm‐1	PROPN
eurjchem-976	107	8	):	):	PUNCT
eurjchem-976	107	9	3355	3355	NUM
eurjchem-976	107	10	(	(	PUNCT
eurjchem-976	107	11	oh	oh	INTJ
eurjchem-976	107	12	)	)	PUNCT
eurjchem-976	107	13	(	(	PUNCT
eurjchem-976	107	14	acid	acid	NOUN
eurjchem-976	107	15	)	)	PUNCT
eurjchem-976	107	16	,	,	PUNCT
eurjchem-976	107	17	3075	3075	NUM
eurjchem-976	107	18	(	(	PUNCT
eurjchem-976	107	19	ch	ch	NOUN
eurjchem-976	107	20	)	)	PUNCT
eurjchem-976	107	21	(	(	PUNCT
eurjchem-976	107	22	aromatic	aromatic	NOUN
eurjchem-976	107	23	)	)	PUNCT
eurjchem-976	107	24	,	,	PUNCT
eurjchem-976	107	25	2977(ch	2977(ch	NUM
eurjchem-976	107	26	)	)	PUNCT
eurjchem-976	107	27	(	(	PUNCT
eurjchem-976	107	28	alkyl	alkyl	NOUN
eurjchem-976	107	29	)	)	PUNCT
eurjchem-976	107	30	,	,	PUNCT
eurjchem-976	107	31	1715	1715	NUM
eurjchem-976	107	32	(	(	PUNCT
eurjchem-976	107	33	c	c	NOUN
eurjchem-976	107	34	=	=	NOUN
eurjchem-976	107	35	o	o	NOUN
eurjchem-976	107	36	)	)	PUNCT
eurjchem-976	107	37	(	(	PUNCT
eurjchem-976	107	38	acid	acid	NOUN
eurjchem-976	107	39	)	)	PUNCT
eurjchem-976	107	40	,	,	PUNCT
eurjchem-976	107	41	1664	1664	NUM
eurjchem-976	107	42	(	(	PUNCT
eurjchem-976	107	43	c	c	NOUN
eurjchem-976	107	44	=	=	NOUN
eurjchem-976	107	45	o	o	NOUN
eurjchem-976	107	46	)	)	PUNCT
eurjchem-976	107	47	(	(	PUNCT
eurjchem-976	107	48	amide	amide	NOUN
eurjchem-976	107	49	)	)	PUNCT
eurjchem-976	107	50	,	,	PUNCT
eurjchem-976	107	51	1600	1600	NUM
eurjchem-976	107	52	,	,	PUNCT
eurjchem-976	107	53	1585	1585	NUM
eurjchem-976	107	54	,	,	PUNCT
eurjchem-976	107	55	1450	1450	NUM
eurjchem-976	107	56	,	,	PUNCT
eurjchem-976	107	57	1440	1440	NUM
eurjchem-976	107	58	,	,	PUNCT
eurjchem-976	107	59	1380	1380	NUM
eurjchem-976	107	60	,	,	PUNCT
eurjchem-976	107	61	1130	1130	NUM
eurjchem-976	107	62	,	,	PUNCT
eurjchem-976	107	63	749	749	NUM
eurjchem-976	107	64	.	.	PUNCT
eurjchem-976	108	1	1h	1h	NUM
eurjchem-976	108	2	nmr	nmr	NOUN
eurjchem-976	108	3	(	(	PUNCT
eurjchem-976	108	4	90	90	NUM
eurjchem-976	108	5	mhz	mhz	NOUN
eurjchem-976	108	6	,	,	PUNCT
eurjchem-976	108	7	cdcl3	cdcl3	PROPN
eurjchem-976	108	8	,	,	PUNCT
eurjchem-976	108	9	δ	δ	PROPN
eurjchem-976	108	10	,	,	PUNCT
eurjchem-976	108	11	ppm	ppm	NOUN
eurjchem-976	108	12	):	):	PUNCT
eurjchem-976	108	13	1.24	1.24	NUM
eurjchem-976	108	14	(	(	PUNCT
eurjchem-976	108	15	d	d	PROPN
eurjchem-976	108	16	,	,	PUNCT
eurjchem-976	108	17	3h	3h	NUM
eurjchem-976	108	18	,	,	PUNCT
eurjchem-976	108	19	j	j	PROPN
eurjchem-976	108	20	=	=	SYM
eurjchem-976	108	21	9.4	9.4	NUM
eurjchem-976	108	22	hz	hz	NOUN
eurjchem-976	108	23	,	,	PUNCT
eurjchem-976	108	24	ch3	ch3	PROPN
eurjchem-976	108	25	)	)	PUNCT
eurjchem-976	108	26	,	,	PUNCT
eurjchem-976	108	27	2.92	2.92	NUM
eurjchem-976	108	28	(	(	PUNCT
eurjchem-976	108	29	p	p	X
eurjchem-976	108	30	,	,	PUNCT
eurjchem-976	108	31	1h	1h	NUM
eurjchem-976	108	32	,	,	PUNCT
eurjchem-976	108	33	j	j	PROPN
eurjchem-976	108	34	=	=	PROPN
eurjchem-976	108	35	12.4	12.4	NUM
eurjchem-976	108	36	hz	hz	NOUN
eurjchem-976	108	37	,	,	PUNCT
eurjchem-976	108	38	ch	ch	NOUN
eurjchem-976	108	39	)	)	PUNCT
eurjchem-976	108	40	,	,	PUNCT
eurjchem-976	108	41	3.04	3.04	NUM
eurjchem-976	108	42	(	(	PUNCT
eurjchem-976	108	43	app	app	X
eurjchem-976	108	44	.	.	PROPN
eurjchem-976	109	1	q	q	X
eurjchem-976	109	2	,	,	PUNCT
eurjchem-976	109	3	1h	1h	NUM
eurjchem-976	109	4	,	,	PUNCT
eurjchem-976	109	5	j	j	PROPN
eurjchem-976	109	6	=	=	PROPN
eurjchem-976	109	7	12.4	12.4	NUM
eurjchem-976	109	8	hz	hz	NOUN
eurjchem-976	109	9	,	,	PUNCT
eurjchem-976	109	10	ch	ch	NOUN
eurjchem-976	109	11	)	)	PUNCT
eurjchem-976	109	12	,	,	PUNCT
eurjchem-976	109	13	7.35‐8.23	7.35‐8.23	NUM
eurjchem-976	109	14	(	(	PUNCT
eurjchem-976	109	15	m	m	PROPN
eurjchem-976	109	16	,	,	PUNCT
eurjchem-976	109	17	10	10	NUM
eurjchem-976	109	18	h	h	NOUN
eurjchem-976	109	19	,	,	PUNCT
eurjchem-976	109	20	ar‐h	ar‐h	NOUN
eurjchem-976	109	21	)	)	PUNCT
eurjchem-976	109	22	,	,	PUNCT
eurjchem-976	109	23	11.6	11.6	NUM
eurjchem-976	109	24	(	(	PUNCT
eurjchem-976	109	25	s	s	PROPN
eurjchem-976	109	26	,	,	PUNCT
eurjchem-976	109	27	1h	1h	NUM
eurjchem-976	109	28	,	,	PUNCT
eurjchem-976	109	29	cooh	cooh	NOUN
eurjchem-976	109	30	)	)	PUNCT
eurjchem-976	109	31	.	.	PUNCT
eurjchem-976	110	1	anal	anal	PROPN
eurjchem-976	110	2	.	.	PUNCT
eurjchem-976	110	3	calcd	calcd	NOUN
eurjchem-976	110	4	.	.	PUNCT
eurjchem-976	111	1	for	for	ADP
eurjchem-976	111	2	c18h16n2o3	c18h16n2o3	PROPN
eurjchem-976	111	3	:	:	PUNCT
eurjchem-976	111	4	c	c	X
eurjchem-976	111	5	,	,	PUNCT
eurjchem-976	111	6	70.12	70.12	NUM
eurjchem-976	111	7	;	;	PUNCT
eurjchem-976	111	8	h	h	NOUN
eurjchem-976	111	9	,	,	PUNCT
eurjchem-976	111	10	5.23	5.23	NUM
eurjchem-976	111	11	;	;	PUNCT
eurjchem-976	111	12	n	n	CCONJ
eurjchem-976	111	13	,	,	PUNCT
eurjchem-976	111	14	9.09	9.09	NUM
eurjchem-976	111	15	.	.	PUNCT
eurjchem-976	111	16	found	find	VERB
eurjchem-976	111	17	;	;	PUNCT
eurjchem-976	111	18	c	c	X
eurjchem-976	111	19	,	,	PUNCT
eurjchem-976	111	20	70.05	70.05	NUM
eurjchem-976	111	21	;	;	PUNCT
eurjchem-976	112	1	h	h	NOUN
eurjchem-976	112	2	,	,	PUNCT
eurjchem-976	112	3	5.22	5.22	NUM
eurjchem-976	112	4	;	;	PUNCT
eurjchem-976	112	5	n	n	CCONJ
eurjchem-976	112	6	,	,	PUNCT
eurjchem-976	112	7	9.26	9.26	NUM
eurjchem-976	112	8	%	%	NOUN
eurjchem-976	112	9	.	.	PUNCT
eurjchem-976	113	1	2.2.5	2.2.5	X
eurjchem-976	113	2	.	.	PUNCT
eurjchem-976	113	3	general	general	ADJ
eurjchem-976	113	4	procedure	procedure	NOUN
eurjchem-976	113	5	for	for	ADP
eurjchem-976	113	6	the	the	DET
eurjchem-976	113	7	synthesis	synthesis	NOUN
eurjchem-976	113	8	of	of	ADP
eurjchem-976	113	9	acids	acid	NOUN
eurjchem-976	113	10	13a	13a	NOUN
eurjchem-976	113	11	,	,	PUNCT
eurjchem-976	113	12	b	b	PROPN
eurjchem-976	113	13	a	a	DET
eurjchem-976	113	14	mixture	mixture	NOUN
eurjchem-976	113	15	of	of	ADP
eurjchem-976	113	16	aldehyde	aldehyde	NOUN
eurjchem-976	113	17	5	5	NUM
eurjchem-976	113	18	(	(	PUNCT
eurjchem-976	113	19	4.2	4.2	NUM
eurjchem-976	113	20	g	g	NOUN
eurjchem-976	113	21	,	,	PUNCT
eurjchem-976	113	22	15	15	NUM
eurjchem-976	113	23	mmol	mmol	NOUN
eurjchem-976	113	24	)	)	PUNCT
eurjchem-976	113	25	,	,	PUNCT
eurjchem-976	113	26	acid	acid	NOUN
eurjchem-976	113	27	anhydride	anhydride	NOUN
eurjchem-976	113	28	(	(	PUNCT
eurjchem-976	113	29	18	18	NUM
eurjchem-976	113	30	mmol	mmol	NOUN
eurjchem-976	113	31	)	)	PUNCT
eurjchem-976	113	32	and	and	CCONJ
eurjchem-976	113	33	sodium	sodium	NOUN
eurjchem-976	113	34	salt	salt	NOUN
eurjchem-976	113	35	of	of	ADP
eurjchem-976	113	36	the	the	DET
eurjchem-976	113	37	corresponding	correspond	VERB
eurjchem-976	113	38	acid	acid	NOUN
eurjchem-976	113	39	(	(	PUNCT
eurjchem-976	113	40	18	18	NUM
eurjchem-976	113	41	mmol	mmol	NOUN
eurjchem-976	113	42	)	)	PUNCT
eurjchem-976	113	43	was	be	AUX
eurjchem-976	113	44	heated	heat	VERB
eurjchem-976	113	45	in	in	ADP
eurjchem-976	113	46	an	an	DET
eurjchem-976	113	47	oil	oil	NOUN
eurjchem-976	113	48	bath	bath	NOUN
eurjchem-976	113	49	at	at	ADP
eurjchem-976	113	50	140‐150	140‐150	NUM
eurjchem-976	113	51	°	°	ADP
eurjchem-976	113	52	c	c	NOUN
eurjchem-976	113	53	with	with	ADP
eurjchem-976	113	54	occasionally	occasionally	ADV
eurjchem-976	113	55	stirring	stir	VERB
eurjchem-976	113	56	for	for	ADP
eurjchem-976	113	57	10‐12	10‐12	NUM
eurjchem-976	113	58	h.	h.	NOUN
eurjchem-976	113	59	the	the	DET
eurjchem-976	113	60	warm	warm	ADJ
eurjchem-976	113	61	mixture	mixture	NOUN
eurjchem-976	113	62	was	be	AUX
eurjchem-976	113	63	poured	pour	VERB
eurjchem-976	113	64	with	with	ADP
eurjchem-976	113	65	stirring	stir	VERB
eurjchem-976	113	66	into	into	ADP
eurjchem-976	113	67	water	water	NOUN
eurjchem-976	113	68	(	(	PUNCT
eurjchem-976	113	69	50	50	NUM
eurjchem-976	113	70	ml	ml	NOUN
eurjchem-976	113	71	)	)	PUNCT
eurjchem-976	113	72	,	,	PUNCT
eurjchem-976	113	73	basified	basify	VERB
eurjchem-976	113	74	with	with	ADP
eurjchem-976	113	75	na2co3	na2co3	ADJ
eurjchem-976	113	76	solution	solution	NOUN
eurjchem-976	113	77	(	(	PUNCT
eurjchem-976	113	78	20	20	NUM
eurjchem-976	113	79	ml	ml	NOUN
eurjchem-976	113	80	,	,	PUNCT
eurjchem-976	113	81	30	30	NUM
eurjchem-976	113	82	%	%	NOUN
eurjchem-976	113	83	)	)	PUNCT
eurjchem-976	113	84	and	and	CCONJ
eurjchem-976	113	85	extracted	extract	VERB
eurjchem-976	113	86	with	with	ADP
eurjchem-976	113	87	ether	ether	NOUN
eurjchem-976	113	88	(	(	PUNCT
eurjchem-976	113	89	2	2	NUM
eurjchem-976	113	90	×	×	NOUN
eurjchem-976	113	91	20	20	NUM
eurjchem-976	113	92	ml	ml	NOUN
eurjchem-976	113	93	)	)	PUNCT
eurjchem-976	113	94	.	.	PUNCT
eurjchem-976	114	1	the	the	DET
eurjchem-976	114	2	ether	ether	ADJ
eurjchem-976	114	3	extracts	extract	NOUN
eurjchem-976	114	4	was	be	AUX
eurjchem-976	114	5	discarded	discard	VERB
eurjchem-976	114	6	and	and	CCONJ
eurjchem-976	114	7	the	the	DET
eurjchem-976	114	8	resulting	result	VERB
eurjchem-976	114	9	solution	solution	NOUN
eurjchem-976	114	10	was	be	AUX
eurjchem-976	114	11	heated	heat	VERB
eurjchem-976	114	12	with	with	ADP
eurjchem-976	114	13	decolorizing	decolorize	VERB
eurjchem-976	114	14	carbon	carbon	NOUN
eurjchem-976	114	15	(	(	PUNCT
eurjchem-976	114	16	1	1	NUM
eurjchem-976	114	17	g	g	NOUN
eurjchem-976	114	18	)	)	PUNCT
eurjchem-976	114	19	,	,	PUNCT
eurjchem-976	114	20	filtered	filter	VERB
eurjchem-976	114	21	while	while	SCONJ
eurjchem-976	114	22	hot	hot	ADJ
eurjchem-976	114	23	then	then	ADV
eurjchem-976	114	24	it	it	PRON
eurjchem-976	114	25	was	be	AUX
eurjchem-976	114	26	poured	pour	VERB
eurjchem-976	114	27	with	with	ADP
eurjchem-976	114	28	stirring	stir	VERB
eurjchem-976	114	29	into	into	ADP
eurjchem-976	114	30	ice‐cold	ice‐cold	VERB
eurjchem-976	114	31	concentrated	concentrated	ADJ
eurjchem-976	114	32	hydrochloric	hydrochloric	ADJ
eurjchem-976	114	33	acid	acid	NOUN
eurjchem-976	114	34	chopped	chop	VERB
eurjchem-976	114	35	with	with	ADP
eurjchem-976	114	36	ice	ice	NOUN
eurjchem-976	114	37	(	(	PUNCT
eurjchem-976	114	38	50	50	NUM
eurjchem-976	114	39	ml	ml	NOUN
eurjchem-976	114	40	)	)	PUNCT
eurjchem-976	114	41	.	.	PUNCT
eurjchem-976	115	1	after	after	ADP
eurjchem-976	115	2	standing	stand	VERB
eurjchem-976	115	3	for	for	ADP
eurjchem-976	115	4	overnight	overnight	ADV
eurjchem-976	115	5	,	,	PUNCT
eurjchem-976	115	6	the	the	DET
eurjchem-976	115	7	precipitated	precipitate	VERB
eurjchem-976	115	8	acids	acid	NOUN
eurjchem-976	115	9	13a	13a	NOUN
eurjchem-976	115	10	or	or	CCONJ
eurjchem-976	115	11	b	b	NOUN
eurjchem-976	115	12	was	be	AUX
eurjchem-976	115	13	filtered	filter	VERB
eurjchem-976	115	14	,	,	PUNCT
eurjchem-976	115	15	washed	wash	VERB
eurjchem-976	115	16	successively	successively	ADV
eurjchem-976	115	17	with	with	ADP
eurjchem-976	115	18	water	water	NOUN
eurjchem-976	115	19	and	and	CCONJ
eurjchem-976	115	20	left	leave	VERB
eurjchem-976	115	21	to	to	PART
eurjchem-976	115	22	dry	dry	VERB
eurjchem-976	115	23	(	(	PUNCT
eurjchem-976	115	24	scheme	scheme	NOUN
eurjchem-976	115	25	2	2	NUM
eurjchem-976	115	26	)	)	PUNCT
eurjchem-976	115	27	.	.	PUNCT
eurjchem-976	116	1	purifications	purification	NOUN
eurjchem-976	116	2	,	,	PUNCT
eurjchem-976	116	3	yields	yield	NOUN
eurjchem-976	116	4	and	and	CCONJ
eurjchem-976	116	5	spectral	spectral	ADJ
eurjchem-976	116	6	data	datum	NOUN
eurjchem-976	116	7	are	be	AUX
eurjchem-976	116	8	given	give	VERB
eurjchem-976	116	9	in	in	ADP
eurjchem-976	116	10	the	the	DET
eurjchem-976	116	11	following	following	NOUN
eurjchem-976	116	12	:	:	PUNCT
eurjchem-976	116	13	(	(	PUNCT
eurjchem-976	116	14	e)‐3‐(5‐chloro‐1,3‐diphenyl‐1h‐pyrazol‐4‐yl)acrylic	e)‐3‐(5‐chloro‐1,3‐diphenyl‐1h‐pyrazol‐4‐yl)acrylic	PROPN
eurjchem-976	116	15	acid	acid	NOUN
eurjchem-976	116	16	(	(	PUNCT
eurjchem-976	116	17	13a	13a	NOUN
eurjchem-976	116	18	):	):	PUNCT
eurjchem-976	116	19	color	color	NOUN
eurjchem-976	116	20	:	:	PUNCT
eurjchem-976	116	21	white	white	ADJ
eurjchem-976	116	22	crystals	crystal	NOUN
eurjchem-976	116	23	.	.	PUNCT
eurjchem-976	117	1	yield	yield	NOUN
eurjchem-976	117	2	:	:	PUNCT
eurjchem-976	117	3	74	74	NUM
eurjchem-976	117	4	%	%	NOUN
eurjchem-976	117	5	.	.	PUNCT
eurjchem-976	118	1	m.p	m.p	PROPN
eurjchem-976	118	2	.	.	PROPN
eurjchem-976	118	3	:	:	PUNCT
eurjchem-976	119	1	156	156	NUM
eurjchem-976	119	2	°	°	NUM
eurjchem-976	119	3	c	c	X
eurjchem-976	119	4	(	(	PUNCT
eurjchem-976	119	5	acetone	acetone	NOUN
eurjchem-976	119	6	)	)	PUNCT
eurjchem-976	119	7	.	.	PUNCT
eurjchem-976	120	1	ir	ir	PROPN
eurjchem-976	120	2	(	(	PUNCT
eurjchem-976	120	3	kbr	kbr	PROPN
eurjchem-976	120	4	,	,	PUNCT
eurjchem-976	120	5	ν	ν	PROPN
eurjchem-976	120	6	,	,	PUNCT
eurjchem-976	120	7	cm‐1	cm‐1	PROPN
eurjchem-976	120	8	):	):	PUNCT
eurjchem-976	120	9	3410	3410	NUM
eurjchem-976	120	10	(	(	PUNCT
eurjchem-976	120	11	oh	oh	INTJ
eurjchem-976	120	12	)	)	PUNCT
eurjchem-976	120	13	(	(	PUNCT
eurjchem-976	120	14	br	br	INTJ
eurjchem-976	120	15	,	,	PUNCT
eurjchem-976	120	16	acid	acid	NOUN
eurjchem-976	120	17	)	)	PUNCT
eurjchem-976	120	18	,	,	PUNCT
eurjchem-976	120	19	3105	3105	NUM
eurjchem-976	120	20	(=	(=	X
eurjchem-976	120	21	ch	ch	NOUN
eurjchem-976	120	22	)	)	PUNCT
eurjchem-976	120	23	(	(	PUNCT
eurjchem-976	120	24	alkene	alkene	NOUN
eurjchem-976	120	25	)	)	PUNCT
eurjchem-976	120	26	,	,	PUNCT
eurjchem-976	120	27	3060	3060	NUM
eurjchem-976	120	28	(	(	PUNCT
eurjchem-976	120	29	ch	ch	NOUN
eurjchem-976	120	30	)	)	PUNCT
eurjchem-976	120	31	(	(	PUNCT
eurjchem-976	120	32	aromatic	aromatic	NOUN
eurjchem-976	120	33	)	)	PUNCT
eurjchem-976	120	34	,	,	PUNCT
eurjchem-976	120	35	2995	2995	NUM
eurjchem-976	120	36	(	(	PUNCT
eurjchem-976	120	37	ch	ch	NOUN
eurjchem-976	120	38	)	)	PUNCT
eurjchem-976	120	39	(	(	PUNCT
eurjchem-976	120	40	alkyl	alkyl	NOUN
eurjchem-976	120	41	)	)	PUNCT
eurjchem-976	120	42	,	,	PUNCT
eurjchem-976	120	43	1697	1697	NUM
eurjchem-976	120	44	(	(	PUNCT
eurjchem-976	120	45	c	c	NOUN
eurjchem-976	120	46	=	=	NOUN
eurjchem-976	120	47	o	o	NOUN
eurjchem-976	120	48	)	)	PUNCT
eurjchem-976	120	49	(	(	PUNCT
eurjchem-976	120	50	acid	acid	NOUN
eurjchem-976	120	51	)	)	PUNCT
eurjchem-976	120	52	,	,	PUNCT
eurjchem-976	120	53	1600	1600	NUM
eurjchem-976	120	54	(	(	PUNCT
eurjchem-976	120	55	c	c	NOUN
eurjchem-976	120	56	=	=	SYM
eurjchem-976	120	57	c	c	NOUN
eurjchem-976	120	58	)	)	PUNCT
eurjchem-976	120	59	(	(	PUNCT
eurjchem-976	120	60	alkene	alkene	NOUN
eurjchem-976	120	61	)	)	PUNCT
eurjchem-976	120	62	,	,	PUNCT
eurjchem-976	120	63	1580	1580	NUM
eurjchem-976	120	64	,	,	PUNCT
eurjchem-976	120	65	1463	1463	NUM
eurjchem-976	120	66	,	,	PUNCT
eurjchem-976	120	67	1440	1440	NUM
eurjchem-976	120	68	(	(	PUNCT
eurjchem-976	120	69	c	c	NOUN
eurjchem-976	120	70	=	=	SYM
eurjchem-976	120	71	c	c	NOUN
eurjchem-976	120	72	)	)	PUNCT
eurjchem-976	120	73	(	(	PUNCT
eurjchem-976	120	74	aromatic	aromatic	NOUN
eurjchem-976	120	75	)	)	PUNCT
eurjchem-976	120	76	,	,	PUNCT
eurjchem-976	120	77	1360	1360	NUM
eurjchem-976	120	78	,	,	PUNCT
eurjchem-976	120	79	1140	1140	NUM
eurjchem-976	120	80	,	,	PUNCT
eurjchem-976	120	81	745	745	NUM
eurjchem-976	120	82	.	.	PUNCT
eurjchem-976	121	1	1h	1h	NUM
eurjchem-976	121	2	nmr	nmr	NOUN
eurjchem-976	121	3	(	(	PUNCT
eurjchem-976	121	4	90	90	NUM
eurjchem-976	121	5	mhz	mhz	NOUN
eurjchem-976	121	6	,	,	PUNCT
eurjchem-976	121	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-976	121	8	,	,	PUNCT
eurjchem-976	121	9	δ	δ	PROPN
eurjchem-976	121	10	,	,	PUNCT
eurjchem-976	121	11	ppm	ppm	NUM
eurjchem-976	121	12	):	):	PUNCT
eurjchem-976	121	13	6.35	6.35	NUM
eurjchem-976	121	14	(	(	PUNCT
eurjchem-976	121	15	d	d	PROPN
eurjchem-976	121	16	,	,	PUNCT
eurjchem-976	121	17	1h	1h	NUM
eurjchem-976	121	18	,	,	PUNCT
eurjchem-976	121	19	j	j	PROPN
eurjchem-976	121	20	=	=	PROPN
eurjchem-976	121	21	16.4	16.4	NUM
eurjchem-976	121	22	hz	hz	VERB
eurjchem-976	121	23	,	,	PUNCT
eurjchem-976	121	24	=	=	NOUN
eurjchem-976	121	25	ch	ch	NOUN
eurjchem-976	121	26	)	)	PUNCT
eurjchem-976	121	27	,	,	PUNCT
eurjchem-976	121	28	7.20‐8.10	7.20‐8.10	NUM
eurjchem-976	121	29	(	(	PUNCT
eurjchem-976	121	30	m	m	PROPN
eurjchem-976	121	31	,	,	PUNCT
eurjchem-976	121	32	10	10	NUM
eurjchem-976	121	33	h	h	NOUN
eurjchem-976	121	34	,	,	PUNCT
eurjchem-976	121	35	ar‐h	ar‐h	NOUN
eurjchem-976	121	36	)	)	PUNCT
eurjchem-976	121	37	,	,	PUNCT
eurjchem-976	121	38	8.31	8.31	NUM
eurjchem-976	121	39	(	(	PUNCT
eurjchem-976	121	40	d	d	PROPN
eurjchem-976	121	41	,	,	PUNCT
eurjchem-976	121	42	1h	1h	NUM
eurjchem-976	121	43	,	,	PUNCT
eurjchem-976	121	44	j	j	PROPN
eurjchem-976	121	45	=	=	PROPN
eurjchem-976	121	46	16.4	16.4	NUM
eurjchem-976	121	47	hz	hz	VERB
eurjchem-976	121	48	,	,	PUNCT
eurjchem-976	121	49	=	=	NOUN
eurjchem-976	121	50	ch	ch	NOUN
eurjchem-976	121	51	)	)	PUNCT
eurjchem-976	121	52	,	,	PUNCT
eurjchem-976	121	53	11.2	11.2	NUM
eurjchem-976	121	54	(	(	PUNCT
eurjchem-976	121	55	s	s	PROPN
eurjchem-976	121	56	,	,	PUNCT
eurjchem-976	121	57	1h	1h	NUM
eurjchem-976	121	58	,	,	PUNCT
eurjchem-976	121	59	cooh	cooh	NOUN
eurjchem-976	121	60	)	)	PUNCT
eurjchem-976	121	61	.	.	PUNCT
eurjchem-976	122	1	anal	anal	PROPN
eurjchem-976	122	2	.	.	PUNCT
eurjchem-976	122	3	calcd	calcd	NOUN
eurjchem-976	122	4	.	.	PUNCT
eurjchem-976	123	1	for	for	ADP
eurjchem-976	123	2	c18h13cln2o2	c18h13cln2o2	NOUN
eurjchem-976	123	3	:	:	PUNCT
eurjchem-976	123	4	c	c	X
eurjchem-976	123	5	,	,	PUNCT
eurjchem-976	123	6	66.57	66.57	NUM
eurjchem-976	123	7	;	;	PUNCT
eurjchem-976	123	8	h	h	NOUN
eurjchem-976	123	9	,	,	PUNCT
eurjchem-976	123	10	4.03	4.03	NUM
eurjchem-976	123	11	;	;	PUNCT
eurjchem-976	123	12	n	n	CCONJ
eurjchem-976	123	13	,	,	PUNCT
eurjchem-976	123	14	8.62	8.62	NUM
eurjchem-976	123	15	.	.	PUNCT
eurjchem-976	123	16	found	find	VERB
eurjchem-976	123	17	;	;	PUNCT
eurjchem-976	123	18	c	c	X
eurjchem-976	123	19	,	,	PUNCT
eurjchem-976	123	20	66.49	66.49	NUM
eurjchem-976	123	21	;	;	PUNCT
eurjchem-976	124	1	h	h	X
eurjchem-976	124	2	,	,	PUNCT
eurjchem-976	124	3	4.22	4.22	NUM
eurjchem-976	124	4	;	;	PUNCT
eurjchem-976	124	5	n	n	CCONJ
eurjchem-976	124	6	,	,	PUNCT
eurjchem-976	124	7	8.64	8.64	NUM
eurjchem-976	124	8	%	%	NOUN
eurjchem-976	124	9	.	.	PUNCT
eurjchem-976	125	1	(	(	PUNCT
eurjchem-976	125	2	e)‐3‐(5‐chloro‐1,3‐diphenyl‐1h‐pyrazol‐4‐yl)‐2‐methyl	e)‐3‐(5‐chloro‐1,3‐diphenyl‐1h‐pyrazol‐4‐yl)‐2‐methyl	PROPN
eurjchem-976	125	3	acrylic	acrylic	PROPN
eurjchem-976	125	4	acid	acid	PROPN
eurjchem-976	125	5	(	(	PUNCT
eurjchem-976	125	6	13b	13b	NUM
eurjchem-976	125	7	):	):	PUNCT
eurjchem-976	125	8	color	color	NOUN
eurjchem-976	125	9	:	:	PUNCT
eurjchem-976	125	10	pale	pale	ADJ
eurjchem-976	125	11	yellow	yellow	ADJ
eurjchem-976	125	12	solid	solid	ADJ
eurjchem-976	125	13	.	.	PUNCT
eurjchem-976	126	1	yield	yield	NOUN
eurjchem-976	126	2	:	:	PUNCT
eurjchem-976	126	3	82	82	NUM
eurjchem-976	126	4	%	%	NOUN
eurjchem-976	126	5	.	.	PUNCT
eurjchem-976	127	1	m.p	m.p	PROPN
eurjchem-976	127	2	.	.	PROPN
eurjchem-976	127	3	:	:	PUNCT
eurjchem-976	128	1	172	172	NUM
eurjchem-976	128	2	°	°	PRON
eurjchem-976	128	3	c	c	NOUN
eurjchem-976	128	4	(	(	PUNCT
eurjchem-976	128	5	ethanol	ethanol	NOUN
eurjchem-976	128	6	)	)	PUNCT
eurjchem-976	128	7	.	.	PUNCT
eurjchem-976	129	1	ir	ir	PROPN
eurjchem-976	129	2	(	(	PUNCT
eurjchem-976	129	3	kbr	kbr	PROPN
eurjchem-976	129	4	,	,	PUNCT
eurjchem-976	129	5	ν	ν	PROPN
eurjchem-976	129	6	,	,	PUNCT
eurjchem-976	129	7	cm‐1	cm‐1	PROPN
eurjchem-976	129	8	):	):	PUNCT
eurjchem-976	129	9	3410	3410	NUM
eurjchem-976	129	10	(	(	PUNCT
eurjchem-976	129	11	oh	oh	INTJ
eurjchem-976	129	12	)	)	PUNCT
eurjchem-976	129	13	(	(	PUNCT
eurjchem-976	129	14	br	br	INTJ
eurjchem-976	129	15	,	,	PUNCT
eurjchem-976	129	16	acid	acid	NOUN
eurjchem-976	129	17	)	)	PUNCT
eurjchem-976	129	18	,	,	PUNCT
eurjchem-976	129	19	3094	3094	NUM
eurjchem-976	129	20	(=	(=	X
eurjchem-976	129	21	ch	ch	NOUN
eurjchem-976	129	22	)	)	PUNCT
eurjchem-976	129	23	(	(	PUNCT
eurjchem-976	129	24	alkene	alkene	NOUN
eurjchem-976	129	25	)	)	PUNCT
eurjchem-976	129	26	,	,	PUNCT
eurjchem-976	129	27	3024	3024	NUM
eurjchem-976	129	28	(	(	PUNCT
eurjchem-976	129	29	ch	ch	NOUN
eurjchem-976	129	30	)	)	PUNCT
eurjchem-976	129	31	(	(	PUNCT
eurjchem-976	129	32	aromatic	aromatic	NOUN
eurjchem-976	129	33	)	)	PUNCT
eurjchem-976	129	34	,	,	PUNCT
eurjchem-976	129	35	2975	2975	NUM
eurjchem-976	129	36	(	(	PUNCT
eurjchem-976	129	37	ch	ch	NOUN
eurjchem-976	129	38	)	)	PUNCT
eurjchem-976	129	39	(	(	PUNCT
eurjchem-976	129	40	alkyl	alkyl	NOUN
eurjchem-976	129	41	)	)	PUNCT
eurjchem-976	129	42	,	,	PUNCT
eurjchem-976	129	43	1700	1700	NUM
eurjchem-976	129	44	(	(	PUNCT
eurjchem-976	129	45	c	c	NOUN
eurjchem-976	129	46	=	=	NOUN
eurjchem-976	129	47	o	o	NOUN
eurjchem-976	129	48	)	)	PUNCT
eurjchem-976	129	49	(	(	PUNCT
eurjchem-976	129	50	acid	acid	NOUN
eurjchem-976	129	51	)	)	PUNCT
eurjchem-976	129	52	,	,	PUNCT
eurjchem-976	129	53	1622	1622	NUM
eurjchem-976	129	54	(	(	PUNCT
eurjchem-976	129	55	c	c	NOUN
eurjchem-976	129	56	=	=	SYM
eurjchem-976	129	57	c	c	NOUN
eurjchem-976	129	58	)	)	PUNCT
eurjchem-976	129	59	(	(	PUNCT
eurjchem-976	129	60	alkene	alkene	NOUN
eurjchem-976	129	61	)	)	PUNCT
eurjchem-976	129	62	,	,	PUNCT
eurjchem-976	129	63	1588	1588	NUM
eurjchem-976	129	64	,	,	PUNCT
eurjchem-976	129	65	1450	1450	NUM
eurjchem-976	129	66	,	,	PUNCT
eurjchem-976	129	67	1440	1440	NUM
eurjchem-976	129	68	(	(	PUNCT
eurjchem-976	129	69	c	c	NOUN
eurjchem-976	129	70	=	=	SYM
eurjchem-976	129	71	c	c	NOUN
eurjchem-976	129	72	)	)	PUNCT
eurjchem-976	129	73	(	(	PUNCT
eurjchem-976	129	74	aromatic	aromatic	NOUN
eurjchem-976	129	75	)	)	PUNCT
eurjchem-976	129	76	,	,	PUNCT
eurjchem-976	129	77	1385	1385	NUM
eurjchem-976	129	78	,	,	PUNCT
eurjchem-976	129	79	1145	1145	NUM
eurjchem-976	129	80	,	,	PUNCT
eurjchem-976	129	81	749	749	NUM
eurjchem-976	129	82	.	.	PUNCT
eurjchem-976	130	1	1h	1h	NUM
eurjchem-976	130	2	nmr	nmr	NOUN
eurjchem-976	130	3	(	(	PUNCT
eurjchem-976	130	4	90	90	NUM
eurjchem-976	130	5	mhz	mhz	NOUN
eurjchem-976	130	6	,	,	PUNCT
eurjchem-976	130	7	dmso‐d6	dmso‐d6	PROPN
eurjchem-976	130	8	,	,	PUNCT
eurjchem-976	130	9	δ	δ	PROPN
eurjchem-976	130	10	,	,	PUNCT
eurjchem-976	130	11	ppm	ppm	NUM
eurjchem-976	130	12	):	):	PUNCT
eurjchem-976	130	13	1.83	1.83	NUM
eurjchem-976	130	14	(	(	PUNCT
eurjchem-976	130	15	s	s	PROPN
eurjchem-976	130	16	,	,	PUNCT
eurjchem-976	130	17	3h	3h	NUM
eurjchem-976	130	18	,	,	PUNCT
eurjchem-976	130	19	ch3	ch3	PROPN
eurjchem-976	130	20	)	)	PUNCT
eurjchem-976	130	21	,	,	PUNCT
eurjchem-976	130	22	7.20‐8.36	7.20‐8.36	NUM
eurjchem-976	130	23	(	(	PUNCT
eurjchem-976	130	24	11	11	NUM
eurjchem-976	130	25	h	h	NOUN
eurjchem-976	130	26	,	,	PUNCT
eurjchem-976	130	27	m	m	PROPN
eurjchem-976	130	28	,	,	PUNCT
eurjchem-976	130	29	ar‐h	ar‐h	PROPN
eurjchem-976	130	30	,	,	PUNCT
eurjchem-976	130	31	=	=	NOUN
eurjchem-976	130	32	ch	ch	NOUN
eurjchem-976	130	33	)	)	PUNCT
eurjchem-976	130	34	,	,	PUNCT
eurjchem-976	130	35	10.9	10.9	NUM
eurjchem-976	130	36	(	(	PUNCT
eurjchem-976	130	37	1h	1h	NUM
eurjchem-976	130	38	,	,	PUNCT
eurjchem-976	130	39	s	s	X
eurjchem-976	130	40	,	,	PUNCT
eurjchem-976	130	41	cooh	cooh	NOUN
eurjchem-976	130	42	)	)	PUNCT
eurjchem-976	130	43	.	.	PUNCT
eurjchem-976	131	1	anal	anal	PROPN
eurjchem-976	131	2	.	.	PUNCT
eurjchem-976	131	3	calcd	calcd	NOUN
eurjchem-976	131	4	.	.	PUNCT
eurjchem-976	132	1	for	for	ADP
eurjchem-976	132	2	c19h15cln2o2	c19h15cln2o2	NOUN
eurjchem-976	132	3	:	:	PUNCT
eurjchem-976	132	4	c	c	X
eurjchem-976	132	5	,	,	PUNCT
eurjchem-976	132	6	67.36	67.36	NUM
eurjchem-976	132	7	;	;	PUNCT
eurjchem-976	132	8	h	h	NOUN
eurjchem-976	132	9	,	,	PUNCT
eurjchem-976	132	10	4.46	4.46	NUM
eurjchem-976	132	11	;	;	PUNCT
eurjchem-976	132	12	n	n	CCONJ
eurjchem-976	132	13	,	,	PUNCT
eurjchem-976	132	14	8.27	8.27	NUM
eurjchem-976	132	15	.	.	PUNCT
eurjchem-976	132	16	found	find	VERB
eurjchem-976	132	17	;	;	PUNCT
eurjchem-976	132	18	c	c	X
eurjchem-976	132	19	,	,	PUNCT
eurjchem-976	132	20	67.30	67.30	NUM
eurjchem-976	132	21	;	;	PUNCT
eurjchem-976	133	1	h	h	NOUN
eurjchem-976	133	2	,	,	PUNCT
eurjchem-976	133	3	4.55	4.55	NUM
eurjchem-976	133	4	;	;	PUNCT
eurjchem-976	133	5	n	n	CCONJ
eurjchem-976	133	6	,	,	PUNCT
eurjchem-976	133	7	8.40	8.40	NUM
eurjchem-976	133	8	%	%	NOUN
eurjchem-976	133	9	.	.	PUNCT
eurjchem-976	134	1	2.2.6	2.2.6	X
eurjchem-976	134	2	.	.	PUNCT
eurjchem-976	134	3	general	general	ADJ
eurjchem-976	134	4	procedure	procedure	NOUN
eurjchem-976	134	5	for	for	ADP
eurjchem-976	134	6	reduction	reduction	NOUN
eurjchem-976	134	7	of	of	ADP
eurjchem-976	134	8	acids	acid	NOUN
eurjchem-976	134	9	14a	14a	NOUN
eurjchem-976	134	10	,	,	PUNCT
eurjchem-976	134	11	b	b	NOUN
eurjchem-976	134	12	to	to	ADP
eurjchem-976	134	13	a	a	DET
eurjchem-976	134	14	solution	solution	NOUN
eurjchem-976	134	15	of	of	ADP
eurjchem-976	134	16	acid	acid	PROPN
eurjchem-976	134	17	13a	13a	NOUN
eurjchem-976	134	18	or	or	CCONJ
eurjchem-976	134	19	13b	13b	NOUN
eurjchem-976	134	20	(	(	PUNCT
eurjchem-976	134	21	10	10	NUM
eurjchem-976	134	22	mmol	mmol	NOUN
eurjchem-976	134	23	)	)	PUNCT
eurjchem-976	134	24	in	in	ADP
eurjchem-976	134	25	sodium	sodium	NOUN
eurjchem-976	134	26	hydroxide	hydroxide	NOUN
eurjchem-976	134	27	solution	solution	NOUN
eurjchem-976	134	28	(	(	PUNCT
eurjchem-976	134	29	15	15	NUM
eurjchem-976	134	30	ml	ml	NOUN
eurjchem-976	134	31	,	,	PUNCT
eurjchem-976	134	32	1	1	NUM
eurjchem-976	134	33	n	n	CCONJ
eurjchem-976	134	34	)	)	PUNCT
eurjchem-976	134	35	was	be	AUX
eurjchem-976	134	36	treated	treat	VERB
eurjchem-976	134	37	with	with	ADP
eurjchem-976	134	38	sodium	sodium	NOUN
eurjchem-976	134	39	amalgam	amalgam	NOUN
eurjchem-976	134	40	(	(	PUNCT
eurjchem-976	134	41	25	25	NUM
eurjchem-976	134	42	g	g	NOUN
eurjchem-976	134	43	,	,	PUNCT
eurjchem-976	134	44	2.5	2.5	NUM
eurjchem-976	134	45	%	%	NOUN
eurjchem-976	134	46	)	)	PUNCT
eurjchem-976	134	47	in	in	ADP
eurjchem-976	134	48	small	small	ADJ
eurjchem-976	134	49	portions	portion	NOUN
eurjchem-976	134	50	over	over	ADP
eurjchem-976	134	51	a	a	DET
eurjchem-976	134	52	period	period	NOUN
eurjchem-976	134	53	of	of	ADP
eurjchem-976	134	54	20	20	NUM
eurjchem-976	134	55	min	min	NOUN
eurjchem-976	134	56	with	with	ADP
eurjchem-976	134	57	vigorous	vigorous	ADJ
eurjchem-976	134	58	stirring	stirring	NOUN
eurjchem-976	134	59	.	.	PUNCT
eurjchem-976	135	1	280	280	NUM
eurjchem-976	135	2	el‐aal	el‐aal	PROPN
eurjchem-976	135	3	et	et	NOUN
eurjchem-976	135	4	al	al	PROPN
eurjchem-976	135	5	.	.	PUNCT
eurjchem-976	135	6	/	/	SYM
eurjchem-976	135	7	european	european	PROPN
eurjchem-976	135	8	journal	journal	PROPN
eurjchem-976	135	9	of	of	ADP
eurjchem-976	135	10	chemistry	chemistry	NOUN
eurjchem-976	135	11	5	5	NUM
eurjchem-976	135	12	(	(	PUNCT
eurjchem-976	135	13	2	2	NUM
eurjchem-976	135	14	)	)	PUNCT
eurjchem-976	135	15	(	(	PUNCT
eurjchem-976	135	16	2014	2014	NUM
eurjchem-976	135	17	)	)	PUNCT
eurjchem-976	135	18	277‐286	277‐286	NUM
eurjchem-976	135	19	reagents	reagent	NOUN
eurjchem-976	135	20	and	and	CCONJ
eurjchem-976	135	21	conditions	condition	NOUN
eurjchem-976	135	22	:	:	PUNCT
eurjchem-976	135	23	(	(	PUNCT
eurjchem-976	135	24	i	i	NOUN
eurjchem-976	135	25	)	)	PUNCT
eurjchem-976	135	26	(	(	PUNCT
eurjchem-976	135	27	ac2o	ac2o	NOUN
eurjchem-976	135	28	/	/	SYM
eurjchem-976	135	29	acona	acona	NOUN
eurjchem-976	135	30	)	)	PUNCT
eurjchem-976	135	31	or	or	CCONJ
eurjchem-976	135	32	(	(	PUNCT
eurjchem-976	135	33	pr2o	pr2o	NUM
eurjchem-976	135	34	/	/	SYM
eurjchem-976	135	35	prona)/140‐150	prona)/140‐150	NOUN
eurjchem-976	135	36	°	°	NOUN
eurjchem-976	135	37	c	c	X
eurjchem-976	135	38	,	,	PUNCT
eurjchem-976	135	39	na2co3	na2co3	PROPN
eurjchem-976	135	40	,	,	PUNCT
eurjchem-976	135	41	10‐12	10‐12	NUM
eurjchem-976	135	42	h	h	NOUN
eurjchem-976	135	43	,	,	PUNCT
eurjchem-976	135	44	(	(	PUNCT
eurjchem-976	135	45	ii	ii	NOUN
eurjchem-976	135	46	)	)	PUNCT
eurjchem-976	135	47	na	na	NOUN
eurjchem-976	135	48	/	/	SYM
eurjchem-976	135	49	hg	hg	NOUN
eurjchem-976	135	50	(	(	PUNCT
eurjchem-976	135	51	2.5	2.5	NUM
eurjchem-976	135	52	%	%	NOUN
eurjchem-976	135	53	)	)	PUNCT
eurjchem-976	135	54	,	,	PUNCT
eurjchem-976	135	55	naoh	naoh	NOUN
eurjchem-976	135	56	,	,	PUNCT
eurjchem-976	135	57	5	5	NUM
eurjchem-976	135	58	h	h	NOUN
eurjchem-976	135	59	,	,	PUNCT
eurjchem-976	135	60	(	(	PUNCT
eurjchem-976	135	61	iii	iii	NOUN
eurjchem-976	135	62	)	)	PUNCT
eurjchem-976	135	63	etoh	etoh	PROPN
eurjchem-976	135	64	/	/	SYM
eurjchem-976	135	65	h2so4	h2so4	PROPN
eurjchem-976	135	66	,	,	PUNCT
eurjchem-976	135	67	8	8	NUM
eurjchem-976	135	68	h	h	NOUN
eurjchem-976	135	69	,	,	PUNCT
eurjchem-976	135	70	reflux	reflux	NOUN
eurjchem-976	135	71	,	,	PUNCT
eurjchem-976	135	72	na2co3	na2co3	PROPN
eurjchem-976	135	73	,	,	PUNCT
eurjchem-976	135	74	(	(	PUNCT
eurjchem-976	135	75	iv	iv	X
eurjchem-976	135	76	)	)	PUNCT
eurjchem-976	135	77	memgi	memgi	NOUN
eurjchem-976	135	78	,	,	PUNCT
eurjchem-976	135	79	thf	thf	NOUN
eurjchem-976	135	80	/	/	SYM
eurjchem-976	135	81	et2o	et2o	PROPN
eurjchem-976	135	82	,	,	PUNCT
eurjchem-976	135	83	rt	rt	PROPN
eurjchem-976	135	84	,	,	PUNCT
eurjchem-976	135	85	nh4cl	nh4cl	PROPN
eurjchem-976	135	86	solution	solution	NOUN
eurjchem-976	135	87	(	(	PUNCT
eurjchem-976	135	88	table	table	NOUN
eurjchem-976	135	89	1	1	NUM
eurjchem-976	135	90	)	)	PUNCT
eurjchem-976	135	91	.	.	PUNCT
eurjchem-976	136	1	scheme	scheme	NOUN
eurjchem-976	136	2	2	2	NUM
eurjchem-976	136	3	the	the	DET
eurjchem-976	136	4	reaction	reaction	NOUN
eurjchem-976	136	5	mixture	mixture	NOUN
eurjchem-976	136	6	was	be	AUX
eurjchem-976	136	7	stirred	stir	VERB
eurjchem-976	136	8	for	for	ADP
eurjchem-976	136	9	additional	additional	ADJ
eurjchem-976	136	10	5	5	NUM
eurjchem-976	136	11	h	h	NOUN
eurjchem-976	136	12	at	at	ADP
eurjchem-976	136	13	room	room	NOUN
eurjchem-976	136	14	temperature	temperature	NOUN
eurjchem-976	136	15	and	and	CCONJ
eurjchem-976	136	16	then	then	ADV
eurjchem-976	136	17	mercury	mercury	NOUN
eurjchem-976	136	18	was	be	AUX
eurjchem-976	136	19	separated	separate	VERB
eurjchem-976	136	20	,	,	PUNCT
eurjchem-976	136	21	washed	wash	VERB
eurjchem-976	136	22	with	with	ADP
eurjchem-976	136	23	water	water	NOUN
eurjchem-976	136	24	and	and	CCONJ
eurjchem-976	136	25	the	the	DET
eurjchem-976	136	26	washings	washing	NOUN
eurjchem-976	136	27	were	be	AUX
eurjchem-976	136	28	added	add	VERB
eurjchem-976	136	29	to	to	ADP
eurjchem-976	136	30	the	the	DET
eurjchem-976	136	31	main	main	ADJ
eurjchem-976	136	32	solution	solution	NOUN
eurjchem-976	136	33	.	.	PUNCT
eurjchem-976	137	1	the	the	DET
eurjchem-976	137	2	whole	whole	ADJ
eurjchem-976	137	3	solution	solution	NOUN
eurjchem-976	137	4	was	be	AUX
eurjchem-976	137	5	acidified	acidify	VERB
eurjchem-976	137	6	with	with	ADP
eurjchem-976	137	7	concentrated	concentrated	ADJ
eurjchem-976	137	8	hcl	hcl	PROPN
eurjchem-976	137	9	(	(	PUNCT
eurjchem-976	137	10	10	10	NUM
eurjchem-976	137	11	ml	ml	NOUN
eurjchem-976	137	12	)	)	PUNCT
eurjchem-976	137	13	and	and	CCONJ
eurjchem-976	137	14	the	the	DET
eurjchem-976	137	15	crude	crude	ADJ
eurjchem-976	137	16	acid	acid	NOUN
eurjchem-976	137	17	14a	14a	NOUN
eurjchem-976	137	18	or	or	CCONJ
eurjchem-976	137	19	b	b	NOUN
eurjchem-976	137	20	was	be	AUX
eurjchem-976	137	21	filtered	filter	VERB
eurjchem-976	137	22	,	,	PUNCT
eurjchem-976	137	23	washed	wash	VERB
eurjchem-976	137	24	with	with	ADP
eurjchem-976	137	25	water	water	NOUN
eurjchem-976	137	26	and	and	CCONJ
eurjchem-976	137	27	dried	dry	VERB
eurjchem-976	137	28	(	(	PUNCT
eurjchem-976	137	29	scheme	scheme	NOUN
eurjchem-976	137	30	2	2	NUM
eurjchem-976	137	31	)	)	PUNCT
eurjchem-976	137	32	.	.	PUNCT
eurjchem-976	138	1	yields	yield	NOUN
eurjchem-976	138	2	and	and	CCONJ
eurjchem-976	138	3	spectral	spectral	ADJ
eurjchem-976	138	4	data	datum	NOUN
eurjchem-976	138	5	are	be	AUX
eurjchem-976	138	6	given	give	VERB
eurjchem-976	138	7	in	in	ADP
eurjchem-976	138	8	the	the	DET
eurjchem-976	138	9	following	following	NOUN
eurjchem-976	138	10	:	:	PUNCT
eurjchem-976	138	11	3‐(5‐chloro‐1,3‐diphenyl‐1h‐pyrazol‐4‐yl)propanoic	3‐(5‐chloro‐1,3‐diphenyl‐1h‐pyrazol‐4‐yl)propanoic	NUM
eurjchem-976	138	12	acid	acid	NOUN
eurjchem-976	138	13	(	(	PUNCT
eurjchem-976	138	14	14a	14a	NOUN
eurjchem-976	138	15	):	):	PUNCT
eurjchem-976	138	16	color	color	NOUN
eurjchem-976	138	17	:	:	PUNCT
eurjchem-976	138	18	white	white	ADJ
eurjchem-976	138	19	needles	needle	NOUN
eurjchem-976	138	20	.	.	PUNCT
eurjchem-976	139	1	yield	yield	NOUN
eurjchem-976	139	2	:	:	PUNCT
eurjchem-976	139	3	92	92	NUM
eurjchem-976	139	4	%	%	NOUN
eurjchem-976	139	5	.	.	PUNCT
eurjchem-976	140	1	m.p	m.p	PROPN
eurjchem-976	140	2	.	.	PROPN
eurjchem-976	140	3	:	:	PUNCT
eurjchem-976	141	1	135	135	NUM
eurjchem-976	141	2	°	°	NUM
eurjchem-976	141	3	c	c	NOUN
eurjchem-976	141	4	(	(	PUNCT
eurjchem-976	141	5	ethanol	ethanol	NOUN
eurjchem-976	141	6	)	)	PUNCT
eurjchem-976	141	7	.	.	PUNCT
eurjchem-976	142	1	ir	ir	PROPN
eurjchem-976	142	2	(	(	PUNCT
eurjchem-976	142	3	kbr	kbr	PROPN
eurjchem-976	142	4	,	,	PUNCT
eurjchem-976	142	5	ν	ν	PROPN
eurjchem-976	142	6	,	,	PUNCT
eurjchem-976	142	7	cm‐1	cm‐1	PROPN
eurjchem-976	142	8	):	):	PUNCT
eurjchem-976	142	9	3345	3345	NUM
eurjchem-976	142	10	(	(	PUNCT
eurjchem-976	142	11	oh	oh	INTJ
eurjchem-976	142	12	)	)	PUNCT
eurjchem-976	142	13	(	(	PUNCT
eurjchem-976	142	14	br	br	INTJ
eurjchem-976	142	15	,	,	PUNCT
eurjchem-976	142	16	acid	acid	NOUN
eurjchem-976	142	17	)	)	PUNCT
eurjchem-976	142	18	,	,	PUNCT
eurjchem-976	142	19	3090(ch	3090(ch	NUM
eurjchem-976	142	20	)	)	PUNCT
eurjchem-976	142	21	(	(	PUNCT
eurjchem-976	142	22	aromatic	aromatic	NOUN
eurjchem-976	142	23	)	)	PUNCT
eurjchem-976	142	24	,	,	PUNCT
eurjchem-976	142	25	2988(ch	2988(ch	NUM
eurjchem-976	142	26	)	)	PUNCT
eurjchem-976	142	27	(	(	PUNCT
eurjchem-976	142	28	alkyl	alkyl	NOUN
eurjchem-976	142	29	)	)	PUNCT
eurjchem-976	142	30	,	,	PUNCT
eurjchem-976	142	31	2490	2490	NUM
eurjchem-976	142	32	,	,	PUNCT
eurjchem-976	142	33	1720	1720	NUM
eurjchem-976	142	34	(	(	PUNCT
eurjchem-976	142	35	c	c	NOUN
eurjchem-976	142	36	=	=	NOUN
eurjchem-976	142	37	o	o	NOUN
eurjchem-976	142	38	)	)	PUNCT
eurjchem-976	142	39	(	(	PUNCT
eurjchem-976	142	40	acid	acid	NOUN
eurjchem-976	142	41	)	)	PUNCT
eurjchem-976	142	42	,	,	PUNCT
eurjchem-976	142	43	1605	1605	NUM
eurjchem-976	142	44	,	,	PUNCT
eurjchem-976	142	45	1590	1590	NUM
eurjchem-976	142	46	,	,	PUNCT
eurjchem-976	142	47	1465	1465	NUM
eurjchem-976	142	48	,	,	PUNCT
eurjchem-976	142	49	1450(c	1450(c	PROPN
eurjchem-976	142	50	=	=	SYM
eurjchem-976	142	51	c	c	NOUN
eurjchem-976	142	52	)	)	PUNCT
eurjchem-976	142	53	(	(	PUNCT
eurjchem-976	142	54	aromatic	aromatic	NOUN
eurjchem-976	142	55	)	)	PUNCT
eurjchem-976	142	56	,	,	PUNCT
eurjchem-976	142	57	1350	1350	NUM
eurjchem-976	142	58	,	,	PUNCT
eurjchem-976	142	59	1165	1165	NUM
eurjchem-976	142	60	,	,	PUNCT
eurjchem-976	142	61	745	745	NUM
eurjchem-976	142	62	.	.	PUNCT
eurjchem-976	143	1	1h	1h	NUM
eurjchem-976	143	2	nmr	nmr	NOUN
eurjchem-976	143	3	(	(	PUNCT
eurjchem-976	143	4	90	90	NUM
eurjchem-976	143	5	mhz	mhz	NOUN
eurjchem-976	143	6	,	,	PUNCT
eurjchem-976	143	7	cdcl3	cdcl3	PROPN
eurjchem-976	143	8	,	,	PUNCT
eurjchem-976	143	9	δ	δ	PROPN
eurjchem-976	143	10	,	,	PUNCT
eurjchem-976	143	11	ppm	ppm	NOUN
eurjchem-976	143	12	):	):	PUNCT
eurjchem-976	143	13	2.65	2.65	NUM
eurjchem-976	143	14	(	(	PUNCT
eurjchem-976	143	15	t	t	PROPN
eurjchem-976	143	16	,	,	PUNCT
eurjchem-976	143	17	2h	2h	NUM
eurjchem-976	143	18	,	,	PUNCT
eurjchem-976	143	19	j	j	PROPN
eurjchem-976	143	20	=	=	SYM
eurjchem-976	143	21	6.2	6.2	NUM
eurjchem-976	143	22	hz	hz	NOUN
eurjchem-976	143	23	,	,	PUNCT
eurjchem-976	143	24	ch2	ch2	PROPN
eurjchem-976	143	25	)	)	PUNCT
eurjchem-976	143	26	,	,	PUNCT
eurjchem-976	143	27	2.90	2.90	NUM
eurjchem-976	143	28	(	(	PUNCT
eurjchem-976	143	29	t	t	PROPN
eurjchem-976	143	30	,	,	PUNCT
eurjchem-976	143	31	2h	2h	NUM
eurjchem-976	143	32	,	,	PUNCT
eurjchem-976	143	33	j	j	PROPN
eurjchem-976	143	34	=	=	SYM
eurjchem-976	143	35	6.2	6.2	NUM
eurjchem-976	143	36	hz	hz	NOUN
eurjchem-976	143	37	,	,	PUNCT
eurjchem-976	143	38	ch2	ch2	PROPN
eurjchem-976	143	39	)	)	PUNCT
eurjchem-976	143	40	,	,	PUNCT
eurjchem-976	143	41	6.83‐8.15	6.83‐8.15	NUM
eurjchem-976	143	42	(	(	PUNCT
eurjchem-976	143	43	10	10	NUM
eurjchem-976	143	44	h	h	NOUN
eurjchem-976	143	45	,	,	PUNCT
eurjchem-976	143	46	m	m	PROPN
eurjchem-976	143	47	,	,	PUNCT
eurjchem-976	143	48	ar‐h	ar‐h	PROPN
eurjchem-976	143	49	)	)	PUNCT
eurjchem-976	143	50	,	,	PUNCT
eurjchem-976	143	51	10.5	10.5	NUM
eurjchem-976	143	52	(	(	PUNCT
eurjchem-976	143	53	1h	1h	NUM
eurjchem-976	143	54	,	,	PUNCT
eurjchem-976	143	55	s	s	X
eurjchem-976	143	56	,	,	PUNCT
eurjchem-976	143	57	cooh	cooh	NOUN
eurjchem-976	143	58	)	)	PUNCT
eurjchem-976	143	59	.	.	PUNCT
eurjchem-976	144	1	anal	anal	PROPN
eurjchem-976	144	2	.	.	PUNCT
eurjchem-976	144	3	calcd	calcd	NOUN
eurjchem-976	144	4	.	.	PUNCT
eurjchem-976	145	1	for	for	SCONJ
eurjchem-976	145	2	c18h15cln2o2	c18h15cln2o2	NOUN
eurjchem-976	145	3	:	:	PUNCT
eurjchem-976	145	4	c	c	NOUN
eurjchem-976	145	5	,	,	PUNCT
eurjchem-976	145	6	66.16	66.16	NUM
eurjchem-976	145	7	;	;	PUNCT
eurjchem-976	145	8	h	h	NOUN
eurjchem-976	145	9	,	,	PUNCT
eurjchem-976	145	10	4.63	4.63	NUM
eurjchem-976	145	11	;	;	PUNCT
eurjchem-976	145	12	n	n	CCONJ
eurjchem-976	145	13	,	,	PUNCT
eurjchem-976	145	14	8.57	8.57	NUM
eurjchem-976	145	15	.	.	PUNCT
eurjchem-976	145	16	found	find	VERB
eurjchem-976	145	17	;	;	PUNCT
eurjchem-976	146	1	c	c	X
eurjchem-976	146	2	,	,	PUNCT
eurjchem-976	146	3	66.24	66.24	NUM
eurjchem-976	146	4	;	;	PUNCT
eurjchem-976	146	5	h	h	NOUN
eurjchem-976	146	6	,	,	PUNCT
eurjchem-976	146	7	4.64	4.64	NUM
eurjchem-976	146	8	;	;	PUNCT
eurjchem-976	146	9	n	n	CCONJ
eurjchem-976	146	10	,	,	PUNCT
eurjchem-976	146	11	8.53	8.53	NUM
eurjchem-976	146	12	%	%	NOUN
eurjchem-976	146	13	.	.	PUNCT
eurjchem-976	147	1	2‐((5‐chloro‐1,3‐diphenyl‐1h‐pyrazol‐4‐yl)methyl)propanoic	2‐((5‐chloro‐1,3‐diphenyl‐1h‐pyrazol‐4‐yl)methyl)propanoic	NUM
eurjchem-976	147	2	acid	acid	NOUN
eurjchem-976	147	3	(	(	PUNCT
eurjchem-976	147	4	14b	14b	NUM
eurjchem-976	147	5	):	):	PUNCT
eurjchem-976	147	6	color	color	NOUN
eurjchem-976	147	7	:	:	PUNCT
eurjchem-976	147	8	pale	pale	ADJ
eurjchem-976	147	9	yellow	yellow	ADJ
eurjchem-976	147	10	solid	solid	ADJ
eurjchem-976	147	11	.	.	PUNCT
eurjchem-976	148	1	yield	yield	NOUN
eurjchem-976	148	2	:	:	PUNCT
eurjchem-976	148	3	86	86	NUM
eurjchem-976	148	4	%	%	NOUN
eurjchem-976	148	5	.	.	PUNCT
eurjchem-976	149	1	m.p	m.p	PROPN
eurjchem-976	149	2	.	.	PROPN
eurjchem-976	149	3	:	:	PUNCT
eurjchem-976	150	1	94	94	NUM
eurjchem-976	150	2	°	°	NUM
eurjchem-976	150	3	c	c	NOUN
eurjchem-976	150	4	(	(	PUNCT
eurjchem-976	150	5	ethanol	ethanol	NOUN
eurjchem-976	150	6	)	)	PUNCT
eurjchem-976	150	7	.	.	PUNCT
eurjchem-976	151	1	ir	ir	PROPN
eurjchem-976	151	2	(	(	PUNCT
eurjchem-976	151	3	kbr	kbr	PROPN
eurjchem-976	151	4	,	,	PUNCT
eurjchem-976	151	5	ν	ν	PROPN
eurjchem-976	151	6	,	,	PUNCT
eurjchem-976	151	7	cm‐1	cm‐1	PROPN
eurjchem-976	151	8	):	):	PUNCT
eurjchem-976	151	9	3320	3320	NUM
eurjchem-976	151	10	(	(	PUNCT
eurjchem-976	151	11	oh	oh	INTJ
eurjchem-976	151	12	)	)	PUNCT
eurjchem-976	151	13	(	(	PUNCT
eurjchem-976	151	14	br	br	INTJ
eurjchem-976	151	15	,	,	PUNCT
eurjchem-976	151	16	acid	acid	NOUN
eurjchem-976	151	17	)	)	PUNCT
eurjchem-976	151	18	,	,	PUNCT
eurjchem-976	151	19	3030	3030	NUM
eurjchem-976	151	20	(	(	PUNCT
eurjchem-976	151	21	ch	ch	NOUN
eurjchem-976	151	22	)	)	PUNCT
eurjchem-976	151	23	(	(	PUNCT
eurjchem-976	151	24	aromatic	aromatic	NOUN
eurjchem-976	151	25	)	)	PUNCT
eurjchem-976	151	26	,	,	PUNCT
eurjchem-976	151	27	2975	2975	NUM
eurjchem-976	151	28	(	(	PUNCT
eurjchem-976	151	29	ch	ch	NOUN
eurjchem-976	151	30	)	)	PUNCT
eurjchem-976	151	31	(	(	PUNCT
eurjchem-976	151	32	alkyl	alkyl	NOUN
eurjchem-976	151	33	)	)	PUNCT
eurjchem-976	151	34	,	,	PUNCT
eurjchem-976	151	35	1715	1715	NUM
eurjchem-976	151	36	(	(	PUNCT
eurjchem-976	151	37	c	c	NOUN
eurjchem-976	151	38	=	=	NOUN
eurjchem-976	151	39	o	o	NOUN
eurjchem-976	151	40	)	)	PUNCT
eurjchem-976	151	41	(	(	PUNCT
eurjchem-976	151	42	acid	acid	NOUN
eurjchem-976	151	43	)	)	PUNCT
eurjchem-976	151	44	,	,	PUNCT
eurjchem-976	151	45	1600	1600	NUM
eurjchem-976	151	46	,	,	PUNCT
eurjchem-976	151	47	1580	1580	NUM
eurjchem-976	151	48	,	,	PUNCT
eurjchem-976	151	49	1450	1450	NUM
eurjchem-976	151	50	(	(	PUNCT
eurjchem-976	151	51	c	c	X
eurjchem-976	151	52	=	=	SYM
eurjchem-976	151	53	c	c	NOUN
eurjchem-976	151	54	)	)	PUNCT
eurjchem-976	151	55	(	(	PUNCT
eurjchem-976	151	56	aromatic	aromatic	NOUN
eurjchem-976	151	57	)	)	PUNCT
eurjchem-976	151	58	,	,	PUNCT
eurjchem-976	151	59	1350	1350	NUM
eurjchem-976	151	60	,	,	PUNCT
eurjchem-976	151	61	1140	1140	NUM
eurjchem-976	151	62	,	,	PUNCT
eurjchem-976	151	63	755	755	NUM
eurjchem-976	151	64	.	.	NOUN
eurjchem-976	151	65	1h	1h	NUM
eurjchem-976	151	66	nmr	nmr	NOUN
eurjchem-976	151	67	(	(	PUNCT
eurjchem-976	151	68	90	90	NUM
eurjchem-976	151	69	mhz	mhz	NOUN
eurjchem-976	151	70	,	,	PUNCT
eurjchem-976	151	71	cdcl3	cdcl3	PROPN
eurjchem-976	151	72	,	,	PUNCT
eurjchem-976	151	73	δ	δ	PROPN
eurjchem-976	151	74	,	,	PUNCT
eurjchem-976	151	75	ppm	ppm	NUM
eurjchem-976	151	76	):	):	PUNCT
eurjchem-976	151	77	1.10	1.10	NUM
eurjchem-976	151	78	(	(	PUNCT
eurjchem-976	151	79	d	d	PROPN
eurjchem-976	151	80	,	,	PUNCT
eurjchem-976	151	81	3h	3h	NUM
eurjchem-976	151	82	,	,	PUNCT
eurjchem-976	151	83	j	j	PROPN
eurjchem-976	151	84	=	=	PROPN
eurjchem-976	151	85	10.4	10.4	NUM
eurjchem-976	151	86	hz	hz	NOUN
eurjchem-976	151	87	,	,	PUNCT
eurjchem-976	151	88	ch3	ch3	PROPN
eurjchem-976	151	89	)	)	PUNCT
eurjchem-976	151	90	,	,	PUNCT
eurjchem-976	151	91	2.63	2.63	NUM
eurjchem-976	151	92	(	(	PUNCT
eurjchem-976	151	93	t	t	PROPN
eurjchem-976	151	94	,	,	PUNCT
eurjchem-976	151	95	ha	ha	INTJ
eurjchem-976	151	96	,	,	PUNCT
eurjchem-976	151	97	j	j	PROPN
eurjchem-976	151	98	=	=	PROPN
eurjchem-976	151	99	16.3	16.3	NUM
eurjchem-976	151	100	hz	hz	NOUN
eurjchem-976	151	101	,	,	PUNCT
eurjchem-976	151	102	ch2	ch2	PROPN
eurjchem-976	151	103	)	)	PUNCT
eurjchem-976	151	104	,	,	PUNCT
eurjchem-976	151	105	2.73	2.73	NUM
eurjchem-976	151	106	(	(	PUNCT
eurjchem-976	151	107	ddq	ddq	PROPN
eurjchem-976	151	108	,	,	PUNCT
eurjchem-976	151	109	1h	1h	NUM
eurjchem-976	151	110	,	,	PUNCT
eurjchem-976	151	111	j	j	PROPN
eurjchem-976	151	112	=	=	SYM
eurjchem-976	151	113	9.3	9.3	NUM
eurjchem-976	151	114	hz	hz	VERB
eurjchem-976	151	115	,	,	PUNCT
eurjchem-976	151	116	‐ch	‐ch	NOUN
eurjchem-976	151	117	)	)	PUNCT
eurjchem-976	151	118	,	,	PUNCT
eurjchem-976	151	119	2.86	2.86	NUM
eurjchem-976	151	120	(	(	PUNCT
eurjchem-976	151	121	dd	dd	PROPN
eurjchem-976	151	122	,	,	PUNCT
eurjchem-976	151	123	hb	hb	PROPN
eurjchem-976	151	124	,	,	PUNCT
eurjchem-976	151	125	j	j	PROPN
eurjchem-976	151	126	=	=	PROPN
eurjchem-976	151	127	16.3	16.3	NUM
eurjchem-976	151	128	hz	hz	NOUN
eurjchem-976	151	129	,	,	PUNCT
eurjchem-976	151	130	ch2	ch2	PROPN
eurjchem-976	151	131	)	)	PUNCT
eurjchem-976	151	132	,	,	PUNCT
eurjchem-976	152	1	6.90‐8.25	6.90‐8.25	NUM
eurjchem-976	152	2	(	(	PUNCT
eurjchem-976	152	3	m	m	PROPN
eurjchem-976	152	4	,	,	PUNCT
eurjchem-976	152	5	10	10	NUM
eurjchem-976	152	6	h	h	NOUN
eurjchem-976	152	7	,	,	PUNCT
eurjchem-976	152	8	ar‐h	ar‐h	NOUN
eurjchem-976	152	9	)	)	PUNCT
eurjchem-976	152	10	,	,	PUNCT
eurjchem-976	152	11	10.8	10.8	NUM
eurjchem-976	152	12	(	(	PUNCT
eurjchem-976	152	13	s	s	PROPN
eurjchem-976	152	14	,	,	PUNCT
eurjchem-976	152	15	1h	1h	NUM
eurjchem-976	152	16	,	,	PUNCT
eurjchem-976	152	17	cooh	cooh	NOUN
eurjchem-976	152	18	)	)	PUNCT
eurjchem-976	152	19	.	.	PUNCT
eurjchem-976	153	1	anal	anal	PROPN
eurjchem-976	153	2	.	.	PUNCT
eurjchem-976	153	3	calcd	calcd	NOUN
eurjchem-976	153	4	.	.	PUNCT
eurjchem-976	154	1	for	for	ADP
eurjchem-976	154	2	c19h17cln2o2	c19h17cln2o2	NOUN
eurjchem-976	154	3	:	:	PUNCT
eurjchem-976	154	4	c	c	NOUN
eurjchem-976	154	5	,	,	PUNCT
eurjchem-976	154	6	66.96	66.96	NUM
eurjchem-976	154	7	;	;	PUNCT
eurjchem-976	154	8	h	h	NOUN
eurjchem-976	154	9	,	,	PUNCT
eurjchem-976	154	10	5.03	5.03	NUM
eurjchem-976	154	11	;	;	PUNCT
eurjchem-976	154	12	n	n	CCONJ
eurjchem-976	154	13	,	,	PUNCT
eurjchem-976	154	14	8.22	8.22	NUM
eurjchem-976	154	15	.	.	PUNCT
eurjchem-976	154	16	found	find	VERB
eurjchem-976	154	17	;	;	PUNCT
eurjchem-976	154	18	c	c	X
eurjchem-976	154	19	,	,	PUNCT
eurjchem-976	154	20	66.95	66.95	NUM
eurjchem-976	154	21	;	;	PUNCT
eurjchem-976	155	1	h	h	NOUN
eurjchem-976	155	2	,	,	PUNCT
eurjchem-976	155	3	4.85	4.85	NUM
eurjchem-976	155	4	;	;	PUNCT
eurjchem-976	155	5	n	n	CCONJ
eurjchem-976	155	6	,	,	PUNCT
eurjchem-976	155	7	8.37	8.37	NUM
eurjchem-976	155	8	%	%	NOUN
eurjchem-976	155	9	.	.	PUNCT
eurjchem-976	156	1	2.2.7	2.2.7	X
eurjchem-976	156	2	.	.	PUNCT
eurjchem-976	156	3	general	general	ADJ
eurjchem-976	156	4	procedure	procedure	NOUN
eurjchem-976	156	5	for	for	ADP
eurjchem-976	156	6	the	the	DET
eurjchem-976	156	7	synthesis	synthesis	NOUN
eurjchem-976	156	8	of	of	ADP
eurjchem-976	156	9	ester	ester	NOUN
eurjchem-976	156	10	7	7	NUM
eurjchem-976	156	11	or	or	CCONJ
eurjchem-976	156	12	11a	11a	NUM
eurjchem-976	156	13	,	,	PUNCT
eurjchem-976	156	14	b	b	NOUN
eurjchem-976	156	15	or	or	CCONJ
eurjchem-976	156	16	15a	15a	NOUN
eurjchem-976	156	17	,	,	PUNCT
eurjchem-976	156	18	b	b	PROPN
eurjchem-976	156	19	a	a	DET
eurjchem-976	156	20	mixture	mixture	NOUN
eurjchem-976	156	21	of	of	ADP
eurjchem-976	156	22	acid	acid	PROPN
eurjchem-976	156	23	6	6	NUM
eurjchem-976	156	24	or	or	CCONJ
eurjchem-976	156	25	10a	10a	NOUN
eurjchem-976	156	26	,	,	PUNCT
eurjchem-976	156	27	b	b	NOUN
eurjchem-976	156	28	or	or	CCONJ
eurjchem-976	156	29	14a	14a	NOUN
eurjchem-976	156	30	,	,	PUNCT
eurjchem-976	156	31	b	b	PROPN
eurjchem-976	156	32	(	(	PUNCT
eurjchem-976	156	33	15	15	NUM
eurjchem-976	156	34	mmol	mmol	NOUN
eurjchem-976	156	35	)	)	PUNCT
eurjchem-976	156	36	,	,	PUNCT
eurjchem-976	156	37	absolute	absolute	ADJ
eurjchem-976	156	38	ethanol	ethanol	NOUN
eurjchem-976	156	39	(	(	PUNCT
eurjchem-976	156	40	30	30	NUM
eurjchem-976	156	41	ml	ml	NOUN
eurjchem-976	156	42	)	)	PUNCT
eurjchem-976	156	43	and	and	CCONJ
eurjchem-976	156	44	concentrated	concentrated	ADJ
eurjchem-976	156	45	sulfuric	sulfuric	NOUN
eurjchem-976	156	46	acid	acid	NOUN
eurjchem-976	156	47	(	(	PUNCT
eurjchem-976	156	48	4	4	NUM
eurjchem-976	156	49	ml	ml	NOUN
eurjchem-976	156	50	)	)	PUNCT
eurjchem-976	156	51	was	be	AUX
eurjchem-976	156	52	refluxed	refluxe	VERB
eurjchem-976	156	53	for	for	ADP
eurjchem-976	156	54	8	8	NUM
eurjchem-976	156	55	h.	h.	NOUN
eurjchem-976	156	56	the	the	DET
eurjchem-976	156	57	excess	excess	ADJ
eurjchem-976	156	58	alcohol	alcohol	NOUN
eurjchem-976	156	59	was	be	AUX
eurjchem-976	156	60	removed	remove	VERB
eurjchem-976	156	61	in	in	ADP
eurjchem-976	156	62	vacuo	vacuo	PROPN
eurjchem-976	156	63	and	and	CCONJ
eurjchem-976	156	64	the	the	DET
eurjchem-976	156	65	resulting	result	VERB
eurjchem-976	156	66	residue	residue	NOUN
eurjchem-976	156	67	was	be	AUX
eurjchem-976	156	68	poured	pour	VERB
eurjchem-976	156	69	into	into	ADP
eurjchem-976	156	70	water	water	NOUN
eurjchem-976	156	71	(	(	PUNCT
eurjchem-976	156	72	100	100	NUM
eurjchem-976	156	73	ml	ml	NOUN
eurjchem-976	156	74	)	)	PUNCT
eurjchem-976	156	75	,	,	PUNCT
eurjchem-976	156	76	basified	basify	VERB
eurjchem-976	156	77	by	by	ADP
eurjchem-976	156	78	addition	addition	NOUN
eurjchem-976	156	79	of	of	ADP
eurjchem-976	156	80	solid	solid	ADJ
eurjchem-976	156	81	na2co3	na2co3	NOUN
eurjchem-976	156	82	and	and	CCONJ
eurjchem-976	156	83	left	leave	VERB
eurjchem-976	156	84	to	to	PART
eurjchem-976	156	85	stand	stand	VERB
eurjchem-976	156	86	for	for	ADP
eurjchem-976	156	87	3	3	NUM
eurjchem-976	156	88	h	h	NOUN
eurjchem-976	156	89	at	at	ADP
eurjchem-976	156	90	refrigerator	refrigerator	NOUN
eurjchem-976	156	91	.	.	PUNCT
eurjchem-976	157	1	the	the	DET
eurjchem-976	157	2	product	product	NOUN
eurjchem-976	157	3	was	be	AUX
eurjchem-976	157	4	filtered	filter	VERB
eurjchem-976	157	5	,	,	PUNCT
eurjchem-976	157	6	washed	wash	VERB
eurjchem-976	157	7	with	with	ADP
eurjchem-976	157	8	water	water	NOUN
eurjchem-976	157	9	and	and	CCONJ
eurjchem-976	157	10	dried	dry	VERB
eurjchem-976	157	11	to	to	PART
eurjchem-976	157	12	yield	yield	VERB
eurjchem-976	157	13	the	the	DET
eurjchem-976	157	14	crude	crude	ADJ
eurjchem-976	157	15	esters	ester	NOUN
eurjchem-976	157	16	.	.	PUNCT
eurjchem-976	158	1	these	these	DET
eurjchem-976	158	2	products	product	NOUN
eurjchem-976	158	3	were	be	AUX
eurjchem-976	158	4	subjected	subject	VERB
eurjchem-976	158	5	to	to	PART
eurjchem-976	158	6	flash	flash	VERB
eurjchem-976	158	7	column	column	NOUN
eurjchem-976	158	8	chromatography	chromatography	NOUN
eurjchem-976	158	9	(	(	PUNCT
eurjchem-976	158	10	basic	basic	ADJ
eurjchem-976	158	11	alumina	alumina	NOUN
eurjchem-976	158	12	,	,	PUNCT
eurjchem-976	158	13	etoac	etoac	ADJ
eurjchem-976	158	14	/	/	SYM
eurjchem-976	158	15	n‐	n‐	NOUN
eurjchem-976	158	16	hexane	hexane	NOUN
eurjchem-976	158	17	,	,	PUNCT
eurjchem-976	158	18	2/1	2/1	NUM
eurjchem-976	158	19	)	)	PUNCT
eurjchem-976	158	20	to	to	PART
eurjchem-976	158	21	give	give	VERB
eurjchem-976	158	22	the	the	DET
eurjchem-976	158	23	pure	pure	ADJ
eurjchem-976	158	24	esters	ester	NOUN
eurjchem-976	158	25	7	7	NUM
eurjchem-976	158	26	or	or	CCONJ
eurjchem-976	158	27	11a	11a	NUM
eurjchem-976	158	28	,	,	PUNCT
eurjchem-976	158	29	b	b	NOUN
eurjchem-976	158	30	or	or	CCONJ
eurjchem-976	158	31	15a	15a	NOUN
eurjchem-976	158	32	,	,	PUNCT
eurjchem-976	158	33	b	b	PROPN
eurjchem-976	158	34	(	(	PUNCT
eurjchem-976	158	35	scheme	scheme	NOUN
eurjchem-976	158	36	2	2	NUM
eurjchem-976	158	37	)	)	PUNCT
eurjchem-976	158	38	.	.	PUNCT
eurjchem-976	159	1	yields	yield	NOUN
eurjchem-976	159	2	,	,	PUNCT
eurjchem-976	159	3	further	further	ADJ
eurjchem-976	159	4	purifications	purification	NOUN
eurjchem-976	159	5	and	and	CCONJ
eurjchem-976	159	6	spectral	spectral	ADJ
eurjchem-976	159	7	data	datum	NOUN
eurjchem-976	159	8	are	be	AUX
eurjchem-976	159	9	given	give	VERB
eurjchem-976	159	10	in	in	ADP
eurjchem-976	159	11	the	the	DET
eurjchem-976	159	12	following	following	NOUN
eurjchem-976	159	13	:	:	PUNCT
eurjchem-976	159	14	ethyl	ethyl	PROPN
eurjchem-976	159	15	5‐chloro‐1,3‐diphenyl‐1h‐pyrazole‐4‐carboxylate	5‐chloro‐1,3‐diphenyl‐1h‐pyrazole‐4‐carboxylate	NUM
eurjchem-976	159	16	(	(	PUNCT
eurjchem-976	159	17	7	7	NUM
eurjchem-976	159	18	):	):	PUNCT
eurjchem-976	159	19	color	color	NOUN
eurjchem-976	159	20	:	:	PUNCT
eurjchem-976	159	21	pale	pale	ADJ
eurjchem-976	159	22	yellow	yellow	ADJ
eurjchem-976	159	23	crystals	crystal	NOUN
eurjchem-976	159	24	.	.	PUNCT
eurjchem-976	160	1	yield	yield	NOUN
eurjchem-976	160	2	:	:	PUNCT
eurjchem-976	160	3	90	90	NUM
eurjchem-976	160	4	%	%	NOUN
eurjchem-976	160	5	.	.	PUNCT
eurjchem-976	161	1	m.p	m.p	PROPN
eurjchem-976	161	2	.	.	PROPN
eurjchem-976	161	3	:	:	PUNCT
eurjchem-976	162	1	105	105	NUM
eurjchem-976	162	2	°	°	PRON
eurjchem-976	162	3	c	c	X
eurjchem-976	162	4	(	(	PUNCT
eurjchem-976	162	5	benzene	benzene	NOUN
eurjchem-976	162	6	)	)	PUNCT
eurjchem-976	162	7	.	.	PUNCT
eurjchem-976	163	1	ir	ir	PROPN
eurjchem-976	163	2	(	(	PUNCT
eurjchem-976	163	3	kbr	kbr	PROPN
eurjchem-976	163	4	,	,	PUNCT
eurjchem-976	163	5	ν	ν	PROPN
eurjchem-976	163	6	,	,	PUNCT
eurjchem-976	163	7	cm‐1	cm‐1	PROPN
eurjchem-976	163	8	):	):	PUNCT
eurjchem-976	163	9	3070	3070	NUM
eurjchem-976	163	10	(	(	PUNCT
eurjchem-976	163	11	ch	ch	NOUN
eurjchem-976	163	12	)	)	PUNCT
eurjchem-976	163	13	(	(	PUNCT
eurjchem-976	163	14	aromatic	aromatic	NOUN
eurjchem-976	163	15	)	)	PUNCT
eurjchem-976	163	16	,	,	PUNCT
eurjchem-976	163	17	2965	2965	NUM
eurjchem-976	163	18	(	(	PUNCT
eurjchem-976	163	19	ch	ch	NOUN
eurjchem-976	163	20	)	)	PUNCT
eurjchem-976	163	21	(	(	PUNCT
eurjchem-976	163	22	alkyl	alkyl	NOUN
eurjchem-976	163	23	)	)	PUNCT
eurjchem-976	163	24	,	,	PUNCT
eurjchem-976	163	25	1715	1715	NUM
eurjchem-976	163	26	(	(	PUNCT
eurjchem-976	163	27	c	c	NOUN
eurjchem-976	163	28	=	=	NOUN
eurjchem-976	163	29	o	o	NOUN
eurjchem-976	163	30	)	)	PUNCT
eurjchem-976	163	31	(	(	PUNCT
eurjchem-976	163	32	ester	ester	NOUN
eurjchem-976	163	33	)	)	PUNCT
eurjchem-976	163	34	,	,	PUNCT
eurjchem-976	163	35	1600	1600	NUM
eurjchem-976	163	36	,	,	PUNCT
eurjchem-976	163	37	1585	1585	NUM
eurjchem-976	163	38	,	,	PUNCT
eurjchem-976	163	39	1490	1490	NUM
eurjchem-976	163	40	,	,	PUNCT
eurjchem-976	163	41	1440	1440	NUM
eurjchem-976	163	42	(	(	PUNCT
eurjchem-976	163	43	c	c	NOUN
eurjchem-976	163	44	=	=	SYM
eurjchem-976	163	45	c	c	NOUN
eurjchem-976	163	46	)	)	PUNCT
eurjchem-976	163	47	(	(	PUNCT
eurjchem-976	163	48	aromatic	aromatic	NOUN
eurjchem-976	163	49	)	)	PUNCT
eurjchem-976	163	50	,	,	PUNCT
eurjchem-976	163	51	1340	1340	NUM
eurjchem-976	163	52	,	,	PUNCT
eurjchem-976	163	53	1230	1230	NUM
eurjchem-976	163	54	,	,	PUNCT
eurjchem-976	163	55	750	750	NUM
eurjchem-976	163	56	.	.	PUNCT
eurjchem-976	164	1	1h	1h	NUM
eurjchem-976	164	2	nmr	nmr	NOUN
eurjchem-976	164	3	(	(	PUNCT
eurjchem-976	164	4	90	90	NUM
eurjchem-976	164	5	mhz	mhz	NOUN
eurjchem-976	164	6	,	,	PUNCT
eurjchem-976	164	7	cdcl3	cdcl3	PROPN
eurjchem-976	164	8	,	,	PUNCT
eurjchem-976	164	9	δ	δ	PROPN
eurjchem-976	164	10	,	,	PUNCT
eurjchem-976	164	11	ppm	ppm	NOUN
eurjchem-976	164	12	):	):	PUNCT
eurjchem-976	164	13	1.27	1.27	NUM
eurjchem-976	164	14	(	(	PUNCT
eurjchem-976	164	15	t	t	PROPN
eurjchem-976	164	16	,	,	PUNCT
eurjchem-976	164	17	3h	3h	NUM
eurjchem-976	164	18	,	,	PUNCT
eurjchem-976	164	19	j	j	PROPN
eurjchem-976	164	20	=	=	SYM
eurjchem-976	164	21	7.5	7.5	NUM
eurjchem-976	164	22	hz	hz	ADJ
eurjchem-976	164	23	,	,	PUNCT
eurjchem-976	164	24	ch3	ch3	PROPN
eurjchem-976	164	25	)	)	PUNCT
eurjchem-976	164	26	,	,	PUNCT
eurjchem-976	164	27	4.40	4.40	NUM
eurjchem-976	164	28	(	(	PUNCT
eurjchem-976	164	29	q	q	NOUN
eurjchem-976	164	30	,	,	PUNCT
eurjchem-976	164	31	2h	2h	NUM
eurjchem-976	164	32	,	,	PUNCT
eurjchem-976	164	33	j	j	PROPN
eurjchem-976	164	34	=	=	SYM
eurjchem-976	164	35	7.5	7.5	NUM
eurjchem-976	164	36	hz	hz	NOUN
eurjchem-976	164	37	,	,	PUNCT
eurjchem-976	164	38	ch2	ch2	PROPN
eurjchem-976	164	39	)	)	PUNCT
eurjchem-976	164	40	,	,	PUNCT
eurjchem-976	164	41	7.40‐8.60	7.40‐8.60	NUM
eurjchem-976	164	42	(	(	PUNCT
eurjchem-976	164	43	m	m	PROPN
eurjchem-976	164	44	,	,	PUNCT
eurjchem-976	164	45	10h	10h	NUM
eurjchem-976	164	46	,	,	PUNCT
eurjchem-976	164	47	ar‐h	ar‐h	NOUN
eurjchem-976	164	48	)	)	PUNCT
eurjchem-976	164	49	.	.	PUNCT
eurjchem-976	165	1	anal	anal	PROPN
eurjchem-976	165	2	.	.	PUNCT
eurjchem-976	165	3	calcd	calcd	NOUN
eurjchem-976	165	4	.	.	PUNCT
eurjchem-976	166	1	for	for	SCONJ
eurjchem-976	166	2	c18h15cln2o2	c18h15cln2o2	NOUN
eurjchem-976	166	3	:	:	PUNCT
eurjchem-976	166	4	c	c	NOUN
eurjchem-976	166	5	,	,	PUNCT
eurjchem-976	166	6	66.16	66.16	NUM
eurjchem-976	166	7	;	;	PUNCT
eurjchem-976	166	8	h	h	NOUN
eurjchem-976	166	9	,	,	PUNCT
eurjchem-976	166	10	4.63	4.63	NUM
eurjchem-976	166	11	;	;	PUNCT
eurjchem-976	166	12	n	n	CCONJ
eurjchem-976	166	13	,	,	PUNCT
eurjchem-976	166	14	8.57	8.57	NUM
eurjchem-976	166	15	.	.	PUNCT
eurjchem-976	166	16	found	find	VERB
eurjchem-976	166	17	;	;	PUNCT
eurjchem-976	166	18	c	c	X
eurjchem-976	166	19	,	,	PUNCT
eurjchem-976	166	20	66.27	66.27	NUM
eurjchem-976	166	21	;	;	PUNCT
eurjchem-976	167	1	h	h	NOUN
eurjchem-976	167	2	,	,	PUNCT
eurjchem-976	167	3	4.36	4.36	NUM
eurjchem-976	167	4	;	;	PUNCT
eurjchem-976	167	5	n	n	CCONJ
eurjchem-976	167	6	,	,	PUNCT
eurjchem-976	167	7	8.56	8.56	NUM
eurjchem-976	167	8	%	%	NOUN
eurjchem-976	167	9	.	.	PUNCT
eurjchem-976	168	1	ethyl	ethyl	PROPN
eurjchem-976	168	2	2‐(4,5‐dihydro‐5‐oxo‐1,3‐diphenyl‐1h‐pyrazol‐4‐yl	2‐(4,5‐dihydro‐5‐oxo‐1,3‐diphenyl‐1h‐pyrazol‐4‐yl	NUM
eurjchem-976	168	3	)	)	PUNCT
eurjchem-976	168	4	acetate	acetate	NOUN
eurjchem-976	168	5	(	(	PUNCT
eurjchem-976	168	6	11a	11a	NUM
eurjchem-976	168	7	):	):	PUNCT
eurjchem-976	168	8	color	color	NOUN
eurjchem-976	168	9	:	:	PUNCT
eurjchem-976	168	10	white	white	ADJ
eurjchem-976	168	11	plates	plate	NOUN
eurjchem-976	168	12	.	.	PUNCT
eurjchem-976	169	1	yield	yield	NOUN
eurjchem-976	169	2	:	:	PUNCT
eurjchem-976	169	3	88	88	NUM
eurjchem-976	169	4	%	%	NOUN
eurjchem-976	169	5	.	.	PUNCT
eurjchem-976	170	1	m.p	m.p	PROPN
eurjchem-976	170	2	.	.	PROPN
eurjchem-976	170	3	:	:	PUNCT
eurjchem-976	171	1	142	142	NUM
eurjchem-976	171	2	°	°	PRON
eurjchem-976	171	3	c	c	NOUN
eurjchem-976	171	4	(	(	PUNCT
eurjchem-976	171	5	ethanol	ethanol	NOUN
eurjchem-976	171	6	)	)	PUNCT
eurjchem-976	171	7	.	.	PUNCT
eurjchem-976	172	1	ir	ir	PROPN
eurjchem-976	172	2	(	(	PUNCT
eurjchem-976	172	3	kbr	kbr	PROPN
eurjchem-976	172	4	,	,	PUNCT
eurjchem-976	172	5	ν	ν	PROPN
eurjchem-976	172	6	,	,	PUNCT
eurjchem-976	172	7	cm‐1	cm‐1	PROPN
eurjchem-976	172	8	):	):	PUNCT
eurjchem-976	172	9	3083	3083	NUM
eurjchem-976	172	10	(	(	PUNCT
eurjchem-976	172	11	ch	ch	NOUN
eurjchem-976	172	12	)	)	PUNCT
eurjchem-976	172	13	(	(	PUNCT
eurjchem-976	172	14	aromatic	aromatic	NOUN
eurjchem-976	172	15	)	)	PUNCT
eurjchem-976	172	16	,	,	PUNCT
eurjchem-976	172	17	2980	2980	NUM
eurjchem-976	172	18	(	(	PUNCT
eurjchem-976	172	19	ch	ch	NOUN
eurjchem-976	172	20	)	)	PUNCT
eurjchem-976	172	21	(	(	PUNCT
eurjchem-976	172	22	alkyl	alkyl	NOUN
eurjchem-976	172	23	)	)	PUNCT
eurjchem-976	172	24	,	,	PUNCT
eurjchem-976	172	25	1745	1745	NUM
eurjchem-976	172	26	(	(	PUNCT
eurjchem-976	172	27	c	c	NOUN
eurjchem-976	172	28	=	=	NOUN
eurjchem-976	172	29	o	o	NOUN
eurjchem-976	172	30	)	)	PUNCT
eurjchem-976	172	31	(	(	PUNCT
eurjchem-976	172	32	ester	ester	NOUN
eurjchem-976	172	33	)	)	PUNCT
eurjchem-976	172	34	,	,	PUNCT
eurjchem-976	172	35	1682	1682	NUM
eurjchem-976	172	36	(	(	PUNCT
eurjchem-976	172	37	c	c	NOUN
eurjchem-976	172	38	=	=	NOUN
eurjchem-976	172	39	o	o	NOUN
eurjchem-976	172	40	)	)	PUNCT
eurjchem-976	172	41	(	(	PUNCT
eurjchem-976	172	42	amide	amide	NOUN
eurjchem-976	172	43	)	)	PUNCT
eurjchem-976	172	44	,	,	PUNCT
eurjchem-976	172	45	1605	1605	NUM
eurjchem-976	172	46	,	,	PUNCT
eurjchem-976	172	47	1585	1585	NUM
eurjchem-976	172	48	,	,	PUNCT
eurjchem-976	172	49	1460	1460	NUM
eurjchem-976	172	50	,	,	PUNCT
eurjchem-976	172	51	1455	1455	NUM
eurjchem-976	172	52	(	(	PUNCT
eurjchem-976	172	53	c	c	NOUN
eurjchem-976	172	54	=	=	SYM
eurjchem-976	172	55	c	c	NOUN
eurjchem-976	172	56	)	)	PUNCT
eurjchem-976	172	57	(	(	PUNCT
eurjchem-976	172	58	aromatic	aromatic	NOUN
eurjchem-976	172	59	)	)	PUNCT
eurjchem-976	172	60	,	,	PUNCT
eurjchem-976	172	61	1330	1330	NUM
eurjchem-976	172	62	,	,	PUNCT
eurjchem-976	172	63	1275	1275	NUM
eurjchem-976	172	64	,	,	PUNCT
eurjchem-976	172	65	745	745	NUM
eurjchem-976	172	66	.	.	PUNCT
eurjchem-976	173	1	1h	1h	NUM
eurjchem-976	173	2	nmr	nmr	NOUN
eurjchem-976	173	3	(	(	PUNCT
eurjchem-976	173	4	90	90	NUM
eurjchem-976	173	5	mhz	mhz	NOUN
eurjchem-976	173	6	,	,	PUNCT
eurjchem-976	173	7	cdcl3	cdcl3	PROPN
eurjchem-976	173	8	,	,	PUNCT
eurjchem-976	173	9	δ	δ	PROPN
eurjchem-976	173	10	,	,	PUNCT
eurjchem-976	173	11	ppm	ppm	NUM
eurjchem-976	173	12	):	):	PUNCT
eurjchem-976	173	13	1.32	1.32	NUM
eurjchem-976	173	14	(	(	PUNCT
eurjchem-976	173	15	t	t	PROPN
eurjchem-976	173	16	,	,	PUNCT
eurjchem-976	173	17	3h	3h	NUM
eurjchem-976	173	18	,	,	PUNCT
eurjchem-976	173	19	j	j	PROPN
eurjchem-976	173	20	=	=	SYM
eurjchem-976	173	21	7.5	7.5	NUM
eurjchem-976	173	22	hz	hz	ADJ
eurjchem-976	173	23	,	,	PUNCT
eurjchem-976	173	24	ch3	ch3	PROPN
eurjchem-976	173	25	)	)	PUNCT
eurjchem-976	173	26	,	,	PUNCT
eurjchem-976	173	27	2.62	2.62	NUM
eurjchem-976	173	28	(	(	PUNCT
eurjchem-976	173	29	dd	dd	NOUN
eurjchem-976	173	30	,	,	PUNCT
eurjchem-976	173	31	1	1	NUM
eurjchem-976	173	32	ha	ha	INTJ
eurjchem-976	173	33	,	,	PUNCT
eurjchem-976	173	34	j	j	PROPN
eurjchem-976	173	35	=	=	PROPN
eurjchem-976	173	36	14.2	14.2	NUM
eurjchem-976	173	37	hz	hz	NOUN
eurjchem-976	173	38	,	,	PUNCT
eurjchem-976	173	39	ch2	ch2	PROPN
eurjchem-976	173	40	)	)	PUNCT
eurjchem-976	173	41	,	,	PUNCT
eurjchem-976	173	42	2.74	2.74	NUM
eurjchem-976	173	43	(	(	PUNCT
eurjchem-976	173	44	t	t	PROPN
eurjchem-976	173	45	,	,	PUNCT
eurjchem-976	173	46	1hb	1hb	NOUN
eurjchem-976	173	47	,	,	PUNCT
eurjchem-976	173	48	j	j	PROPN
eurjchem-976	173	49	=	=	PROPN
eurjchem-976	173	50	14.2	14.2	NUM
eurjchem-976	173	51	hz	hz	NOUN
eurjchem-976	173	52	,	,	PUNCT
eurjchem-976	173	53	ch2	ch2	PROPN
eurjchem-976	173	54	)	)	PUNCT
eurjchem-976	173	55	,	,	PUNCT
eurjchem-976	173	56	3.27	3.27	NUM
eurjchem-976	173	57	(	(	PUNCT
eurjchem-976	173	58	t	t	PROPN
eurjchem-976	173	59	,	,	PUNCT
eurjchem-976	173	60	1h	1h	NUM
eurjchem-976	173	61	,	,	PUNCT
eurjchem-976	173	62	j	j	PROPN
eurjchem-976	173	63	=	=	PROPN
eurjchem-976	173	64	10.4	10.4	NUM
eurjchem-976	173	65	hz	hz	NOUN
eurjchem-976	173	66	,	,	PUNCT
eurjchem-976	173	67	ch	ch	NOUN
eurjchem-976	173	68	)	)	PUNCT
eurjchem-976	173	69	,	,	PUNCT
eurjchem-976	173	70	4.22	4.22	NUM
eurjchem-976	173	71	(	(	PUNCT
eurjchem-976	173	72	q	q	NOUN
eurjchem-976	173	73	,	,	PUNCT
eurjchem-976	173	74	2h	2h	NUM
eurjchem-976	173	75	,	,	PUNCT
eurjchem-976	173	76	j	j	PROPN
eurjchem-976	173	77	=	=	SYM
eurjchem-976	173	78	7.5	7.5	NUM
eurjchem-976	173	79	hz	hz	NOUN
eurjchem-976	173	80	,	,	PUNCT
eurjchem-976	173	81	ch2	ch2	PROPN
eurjchem-976	173	82	)	)	PUNCT
eurjchem-976	173	83	,	,	PUNCT
eurjchem-976	173	84	7.50‐8.30	7.50‐8.30	NUM
eurjchem-976	173	85	(	(	PUNCT
eurjchem-976	173	86	m	m	PROPN
eurjchem-976	173	87	,	,	PUNCT
eurjchem-976	173	88	10	10	NUM
eurjchem-976	173	89	h	h	NOUN
eurjchem-976	173	90	,	,	PUNCT
eurjchem-976	173	91	ar‐h	ar‐h	NOUN
eurjchem-976	173	92	)	)	PUNCT
eurjchem-976	173	93	.	.	PUNCT
eurjchem-976	174	1	anal	anal	PROPN
eurjchem-976	174	2	.	.	PUNCT
eurjchem-976	174	3	calcd	calcd	NOUN
eurjchem-976	174	4	.	.	PUNCT
eurjchem-976	175	1	for	for	ADP
eurjchem-976	175	2	c19h18n2o3	c19h18n2o3	NOUN
eurjchem-976	175	3	:	:	PUNCT
eurjchem-976	175	4	c	c	X
eurjchem-976	175	5	,	,	PUNCT
eurjchem-976	175	6	70.79	70.79	NUM
eurjchem-976	175	7	;	;	PUNCT
eurjchem-976	175	8	h	h	NOUN
eurjchem-976	175	9	,	,	PUNCT
eurjchem-976	175	10	5.63	5.63	NUM
eurjchem-976	175	11	;	;	PUNCT
eurjchem-976	175	12	n	n	CCONJ
eurjchem-976	175	13	,	,	PUNCT
eurjchem-976	175	14	8.69	8.69	NUM
eurjchem-976	175	15	.	.	PUNCT
eurjchem-976	175	16	found	find	VERB
eurjchem-976	175	17	;	;	PUNCT
eurjchem-976	175	18	c	c	X
eurjchem-976	175	19	,	,	PUNCT
eurjchem-976	175	20	70.83	70.83	NUM
eurjchem-976	175	21	;	;	PUNCT
eurjchem-976	176	1	h	h	NOUN
eurjchem-976	176	2	,	,	PUNCT
eurjchem-976	176	3	5.74	5.74	NUM
eurjchem-976	176	4	;	;	PUNCT
eurjchem-976	176	5	n	n	CCONJ
eurjchem-976	176	6	,	,	PUNCT
eurjchem-976	176	7	8.49	8.49	NUM
eurjchem-976	176	8	%	%	NOUN
eurjchem-976	176	9	.	.	PUNCT
eurjchem-976	177	1	ethyl	ethyl	PROPN
eurjchem-976	177	2	2‐(4,5‐dihydro‐5‐oxo‐1,3‐diphenyl‐1h‐pyrazol‐4‐yl	2‐(4,5‐dihydro‐5‐oxo‐1,3‐diphenyl‐1h‐pyrazol‐4‐yl	NUM
eurjchem-976	177	3	)	)	PUNCT
eurjchem-976	177	4	propanoate	propanoate	NOUN
eurjchem-976	177	5	(	(	PUNCT
eurjchem-976	177	6	11b	11b	NOUN
eurjchem-976	177	7	):	):	PUNCT
eurjchem-976	177	8	color	color	NOUN
eurjchem-976	177	9	:	:	PUNCT
eurjchem-976	177	10	reddish	reddish	ADJ
eurjchem-976	177	11	viscous	viscous	ADJ
eurjchem-976	177	12	oil	oil	NOUN
eurjchem-976	177	13	.	.	PUNCT
eurjchem-976	178	1	yield	yield	NOUN
eurjchem-976	178	2	:	:	PUNCT
eurjchem-976	178	3	89	89	NUM
eurjchem-976	178	4	%	%	NOUN
eurjchem-976	178	5	.	.	PUNCT
eurjchem-976	179	1	nd25	nd25	PROPN
eurjchem-976	179	2	=	=	PUNCT
eurjchem-976	179	3	1.644	1.644	NUM
eurjchem-976	179	4	.	.	PUNCT
eurjchem-976	180	1	ir	ir	PROPN
eurjchem-976	180	2	(	(	PUNCT
eurjchem-976	180	3	film	film	NOUN
eurjchem-976	180	4	,	,	PUNCT
eurjchem-976	180	5	ν	ν	NOUN
eurjchem-976	180	6	,	,	PUNCT
eurjchem-976	180	7	cm‐1	cm‐1	PROPN
eurjchem-976	180	8	):	):	PUNCT
eurjchem-976	180	9	3075	3075	NUM
eurjchem-976	180	10	(	(	PUNCT
eurjchem-976	180	11	ch	ch	NOUN
eurjchem-976	180	12	)	)	PUNCT
eurjchem-976	180	13	(	(	PUNCT
eurjchem-976	180	14	aromatic	aromatic	NOUN
eurjchem-976	180	15	)	)	PUNCT
eurjchem-976	180	16	,	,	PUNCT
eurjchem-976	180	17	2977	2977	NUM
eurjchem-976	180	18	(	(	PUNCT
eurjchem-976	180	19	ch	ch	NOUN
eurjchem-976	180	20	)	)	PUNCT
eurjchem-976	180	21	(	(	PUNCT
eurjchem-976	180	22	alkyl	alkyl	NOUN
eurjchem-976	180	23	)	)	PUNCT
eurjchem-976	180	24	,	,	PUNCT
eurjchem-976	180	25	1740	1740	NUM
eurjchem-976	180	26	(	(	PUNCT
eurjchem-976	180	27	c	c	NOUN
eurjchem-976	180	28	=	=	NOUN
eurjchem-976	180	29	o	o	NOUN
eurjchem-976	180	30	)	)	PUNCT
eurjchem-976	180	31	(	(	PUNCT
eurjchem-976	180	32	ester	ester	NOUN
eurjchem-976	180	33	)	)	PUNCT
eurjchem-976	180	34	,	,	PUNCT
eurjchem-976	180	35	1673	1673	NUM
eurjchem-976	180	36	(	(	PUNCT
eurjchem-976	180	37	c	c	NOUN
eurjchem-976	180	38	=	=	NOUN
eurjchem-976	180	39	o	o	NOUN
eurjchem-976	180	40	)	)	PUNCT
eurjchem-976	180	41	(	(	PUNCT
eurjchem-976	180	42	amide	amide	NOUN
eurjchem-976	180	43	)	)	PUNCT
eurjchem-976	180	44	,	,	PUNCT
eurjchem-976	180	45	1600	1600	NUM
eurjchem-976	180	46	,	,	PUNCT
eurjchem-976	180	47	1585	1585	NUM
eurjchem-976	180	48	,	,	PUNCT
eurjchem-976	180	49	1495	1495	NUM
eurjchem-976	180	50	,	,	PUNCT
eurjchem-976	180	51	1455	1455	NUM
eurjchem-976	180	52	(	(	PUNCT
eurjchem-976	180	53	c	c	NOUN
eurjchem-976	180	54	=	=	SYM
eurjchem-976	180	55	c	c	NOUN
eurjchem-976	180	56	)	)	PUNCT
eurjchem-976	180	57	(	(	PUNCT
eurjchem-976	180	58	aromatic	aromatic	NOUN
eurjchem-976	180	59	)	)	PUNCT
eurjchem-976	180	60	,	,	PUNCT
eurjchem-976	180	61	1340	1340	NUM
eurjchem-976	180	62	,	,	PUNCT
eurjchem-976	180	63	1245	1245	NUM
eurjchem-976	180	64	,	,	PUNCT
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eurjchem-976	180	66	.	.	PUNCT
eurjchem-976	181	1	1h	1h	NUM
eurjchem-976	181	2	nmr	nmr	NOUN
eurjchem-976	181	3	(	(	PUNCT
eurjchem-976	181	4	90	90	NUM
eurjchem-976	181	5	mhz	mhz	NOUN
eurjchem-976	181	6	,	,	PUNCT
eurjchem-976	181	7	cdcl3	cdcl3	PROPN
eurjchem-976	181	8	,	,	PUNCT
eurjchem-976	181	9	δ	δ	PROPN
eurjchem-976	181	10	,	,	PUNCT
eurjchem-976	181	11	ppm	ppm	NUM
eurjchem-976	181	12	):	):	PUNCT
eurjchem-976	181	13	1.15	1.15	NUM
eurjchem-976	181	14	(	(	PUNCT
eurjchem-976	181	15	d	d	PROPN
eurjchem-976	181	16	,	,	PUNCT
eurjchem-976	181	17	3h	3h	NUM
eurjchem-976	181	18	,	,	PUNCT
eurjchem-976	181	19	j	j	PROPN
eurjchem-976	181	20	=	=	SYM
eurjchem-976	181	21	9.4	9.4	NUM
eurjchem-976	181	22	hz	hz	NOUN
eurjchem-976	181	23	,	,	PUNCT
eurjchem-976	181	24	ch3	ch3	PROPN
eurjchem-976	181	25	)	)	PUNCT
eurjchem-976	181	26	,	,	PUNCT
eurjchem-976	181	27	1.35	1.35	NUM
eurjchem-976	181	28	(	(	PUNCT
eurjchem-976	181	29	t	t	PROPN
eurjchem-976	181	30	,	,	PUNCT
eurjchem-976	181	31	3h	3h	NUM
eurjchem-976	181	32	,	,	PUNCT
eurjchem-976	181	33	j	j	PROPN
eurjchem-976	182	1	=	=	SYM
eurjchem-976	182	2	7.5	7.5	NUM
eurjchem-976	182	3	hz	hz	ADJ
eurjchem-976	182	4	,	,	PUNCT
eurjchem-976	182	5	ch3	ch3	PROPN
eurjchem-976	182	6	)	)	PUNCT
eurjchem-976	182	7	,	,	PUNCT
eurjchem-976	182	8	2.82	2.82	NUM
eurjchem-976	182	9	(	(	PUNCT
eurjchem-976	182	10	p	p	X
eurjchem-976	182	11	,	,	PUNCT
eurjchem-976	182	12	1h	1h	NUM
eurjchem-976	182	13	,	,	PUNCT
eurjchem-976	182	14	j	j	PROPN
eurjchem-976	182	15	=	=	PROPN
eurjchem-976	182	16	12.5	12.5	NUM
eurjchem-976	182	17	hz	hz	NOUN
eurjchem-976	182	18	,	,	PUNCT
eurjchem-976	182	19	ch	ch	NOUN
eurjchem-976	182	20	)	)	PUNCT
eurjchem-976	182	21	,	,	PUNCT
eurjchem-976	182	22	3.24	3.24	NUM
eurjchem-976	183	1	(	(	PUNCT
eurjchem-976	183	2	app	app	PROPN
eurjchem-976	183	3	.	.	PROPN
eurjchem-976	183	4	t	t	PROPN
eurjchem-976	183	5	,	,	PUNCT
eurjchem-976	183	6	1h	1h	NUM
eurjchem-976	183	7	,	,	PUNCT
eurjchem-976	183	8	j	j	PROPN
eurjchem-976	183	9	=	=	PROPN
eurjchem-976	183	10	12.5	12.5	NUM
eurjchem-976	183	11	hz	hz	NOUN
eurjchem-976	183	12	,	,	PUNCT
eurjchem-976	183	13	ch	ch	NOUN
eurjchem-976	183	14	)	)	PUNCT
eurjchem-976	183	15	,	,	PUNCT
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eurjchem-976	183	17	(	(	PUNCT
eurjchem-976	183	18	q	q	NOUN
eurjchem-976	183	19	,	,	PUNCT
eurjchem-976	183	20	2h	2h	NUM
eurjchem-976	183	21	,	,	PUNCT
eurjchem-976	183	22	j	j	PROPN
eurjchem-976	183	23	=	=	SYM
eurjchem-976	183	24	7.5	7.5	NUM
eurjchem-976	183	25	hz	hz	NOUN
eurjchem-976	183	26	,	,	PUNCT
eurjchem-976	183	27	ch2	ch2	PROPN
eurjchem-976	183	28	)	)	PUNCT
eurjchem-976	183	29	,	,	PUNCT
eurjchem-976	183	30	7.45‐8.50	7.45‐8.50	NUM
eurjchem-976	183	31	(	(	PUNCT
eurjchem-976	183	32	m	m	PROPN
eurjchem-976	183	33	,	,	PUNCT
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eurjchem-976	183	35	h	h	NOUN
eurjchem-976	183	36	,	,	PUNCT
eurjchem-976	183	37	ar‐h	ar‐h	NOUN
eurjchem-976	183	38	)	)	PUNCT
eurjchem-976	183	39	.	.	PUNCT
eurjchem-976	184	1	anal	anal	PROPN
eurjchem-976	184	2	.	.	PUNCT
eurjchem-976	184	3	calcd	calcd	NOUN
eurjchem-976	184	4	.	.	PUNCT
eurjchem-976	185	1	for	for	SCONJ
eurjchem-976	185	2	c20h20n2o3	c20h20n2o3	PROPN
eurjchem-976	185	3	:	:	PUNCT
eurjchem-976	185	4	c	c	X
eurjchem-976	185	5	,	,	PUNCT
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eurjchem-976	185	7	;	;	PUNCT
eurjchem-976	185	8	h	h	NOUN
eurjchem-976	185	9	,	,	PUNCT
eurjchem-976	185	10	5.99	5.99	NUM
eurjchem-976	185	11	;	;	PUNCT
eurjchem-976	185	12	n	n	CCONJ
eurjchem-976	185	13	,	,	PUNCT
eurjchem-976	185	14	8.33	8.33	NUM
eurjchem-976	185	15	.	.	PUNCT
eurjchem-976	185	16	found	find	VERB
eurjchem-976	185	17	;	;	PUNCT
eurjchem-976	185	18	c	c	X
eurjchem-976	185	19	,	,	PUNCT
eurjchem-976	185	20	71.44	71.44	NUM
eurjchem-976	185	21	;	;	PUNCT
eurjchem-976	186	1	h	h	NOUN
eurjchem-976	186	2	,	,	PUNCT
eurjchem-976	186	3	6.14	6.14	NUM
eurjchem-976	186	4	;	;	PUNCT
eurjchem-976	186	5	n	n	CCONJ
eurjchem-976	186	6	,	,	PUNCT
eurjchem-976	186	7	8.09	8.09	NUM
eurjchem-976	186	8	%	%	NOUN
eurjchem-976	186	9	.	.	PUNCT
eurjchem-976	187	1	ethyl	ethyl	PROPN
eurjchem-976	187	2	3‐(5‐chloro‐1,3‐diphenyl‐1h‐pyrazol‐4‐yl)propanoate	3‐(5‐chloro‐1,3‐diphenyl‐1h‐pyrazol‐4‐yl)propanoate	PROPN
eurjchem-976	187	3	(	(	PUNCT
eurjchem-976	187	4	15a	15a	NOUN
eurjchem-976	187	5	):	):	PUNCT
eurjchem-976	187	6	color	color	NOUN
eurjchem-976	187	7	:	:	PUNCT
eurjchem-976	187	8	yellowish	yellowish	VERB
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eurjchem-976	187	10	oil	oil	NOUN
eurjchem-976	187	11	.	.	PUNCT
eurjchem-976	188	1	yield	yield	NOUN
eurjchem-976	188	2	:	:	PUNCT
eurjchem-976	188	3	85	85	NUM
eurjchem-976	188	4	%	%	NOUN
eurjchem-976	188	5	.	.	PUNCT
eurjchem-976	189	1	nd25	nd25	PROPN
eurjchem-976	189	2	=	=	PUNCT
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eurjchem-976	190	2	.	.	PUNCT
eurjchem-976	191	1	ir	ir	PROPN
eurjchem-976	191	2	(	(	PUNCT
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eurjchem-976	191	4	,	,	PUNCT
eurjchem-976	191	5	ν	ν	NOUN
eurjchem-976	191	6	,	,	PUNCT
eurjchem-976	191	7	cm‐1	cm‐1	PROPN
eurjchem-976	191	8	):	):	PUNCT
eurjchem-976	191	9	3055	3055	NUM
eurjchem-976	191	10	(	(	PUNCT
eurjchem-976	191	11	ch	ch	NOUN
eurjchem-976	191	12	)	)	PUNCT
eurjchem-976	191	13	(	(	PUNCT
eurjchem-976	191	14	aromatic	aromatic	NOUN
eurjchem-976	191	15	)	)	PUNCT
eurjchem-976	191	16	,	,	PUNCT
eurjchem-976	191	17	2964	2964	NUM
eurjchem-976	191	18	(	(	PUNCT
eurjchem-976	191	19	ch	ch	NOUN
eurjchem-976	191	20	)	)	PUNCT
eurjchem-976	191	21	(	(	PUNCT
eurjchem-976	191	22	alkyl	alkyl	NOUN
eurjchem-976	191	23	)	)	PUNCT
eurjchem-976	191	24	,	,	PUNCT
eurjchem-976	191	25	1738	1738	NUM
eurjchem-976	191	26	(	(	PUNCT
eurjchem-976	191	27	c	c	NOUN
eurjchem-976	191	28	=	=	NOUN
eurjchem-976	191	29	o	o	NOUN
eurjchem-976	191	30	)	)	PUNCT
eurjchem-976	191	31	(	(	PUNCT
eurjchem-976	191	32	ester	ester	NOUN
eurjchem-976	191	33	)	)	PUNCT
eurjchem-976	191	34	,	,	PUNCT
eurjchem-976	191	35	1590	1590	NUM
eurjchem-976	191	36	,	,	PUNCT
eurjchem-976	191	37	1550	1550	NUM
eurjchem-976	191	38	,	,	PUNCT
eurjchem-976	191	39	1460	1460	NUM
eurjchem-976	191	40	,	,	PUNCT
eurjchem-976	191	41	1430	1430	NUM
eurjchem-976	191	42	(	(	PUNCT
eurjchem-976	191	43	c	c	X
eurjchem-976	191	44	=	=	SYM
eurjchem-976	191	45	c	c	NOUN
eurjchem-976	191	46	)	)	PUNCT
eurjchem-976	191	47	(	(	PUNCT
eurjchem-976	191	48	aromatic	aromatic	NOUN
eurjchem-976	191	49	)	)	PUNCT
eurjchem-976	191	50	,	,	PUNCT
eurjchem-976	191	51	1335	1335	NUM
eurjchem-976	191	52	,	,	PUNCT
eurjchem-976	191	53	1265	1265	NUM
eurjchem-976	191	54	,	,	PUNCT
eurjchem-976	191	55	750	750	NUM
eurjchem-976	191	56	.	.	PUNCT
eurjchem-976	191	57	1h	1h	NUM
eurjchem-976	191	58	nmr	nmr	NOUN
eurjchem-976	191	59	(	(	PUNCT
eurjchem-976	191	60	90	90	NUM
eurjchem-976	191	61	mhz	mhz	NOUN
eurjchem-976	191	62	,	,	PUNCT
eurjchem-976	191	63	cdcl3	cdcl3	PROPN
eurjchem-976	191	64	,	,	PUNCT
eurjchem-976	191	65	δ	δ	PROPN
eurjchem-976	191	66	,	,	PUNCT
eurjchem-976	191	67	ppm	ppm	NOUN
eurjchem-976	191	68	):	):	PUNCT
eurjchem-976	191	69	1.30	1.30	NUM
eurjchem-976	191	70	(	(	PUNCT
eurjchem-976	191	71	t	t	PROPN
eurjchem-976	191	72	,	,	PUNCT
eurjchem-976	191	73	3h	3h	NUM
eurjchem-976	191	74	,	,	PUNCT
eurjchem-976	191	75	j	j	PROPN
eurjchem-976	191	76	=	=	SYM
eurjchem-976	191	77	7.5	7.5	NUM
eurjchem-976	191	78	hz	hz	ADJ
eurjchem-976	191	79	,	,	PUNCT
eurjchem-976	191	80	ch3	ch3	PROPN
eurjchem-976	191	81	)	)	PUNCT
eurjchem-976	191	82	,	,	PUNCT
eurjchem-976	191	83	2.52	2.52	NUM
eurjchem-976	191	84	(	(	PUNCT
eurjchem-976	191	85	t	t	PROPN
eurjchem-976	191	86	,	,	PUNCT
eurjchem-976	191	87	2h	2h	NUM
eurjchem-976	191	88	,	,	PUNCT
eurjchem-976	191	89	j	j	PROPN
eurjchem-976	191	90	=	=	SYM
eurjchem-976	191	91	6.2	6.2	NUM
eurjchem-976	191	92	hz	hz	NOUN
eurjchem-976	191	93	,	,	PUNCT
eurjchem-976	191	94	ch2	ch2	PROPN
eurjchem-976	191	95	)	)	PUNCT
eurjchem-976	191	96	,	,	PUNCT
eurjchem-976	191	97	2.95	2.95	NUM
eurjchem-976	191	98	(	(	PUNCT
eurjchem-976	191	99	t	t	PROPN
eurjchem-976	191	100	,	,	PUNCT
eurjchem-976	191	101	2h	2h	NUM
eurjchem-976	191	102	,	,	PUNCT
eurjchem-976	191	103	j	j	PROPN
eurjchem-976	191	104	=	=	SYM
eurjchem-976	191	105	6.2	6.2	NUM
eurjchem-976	191	106	hz	hz	NOUN
eurjchem-976	191	107	,	,	PUNCT
eurjchem-976	191	108	ch2	ch2	PROPN
eurjchem-976	191	109	)	)	PUNCT
eurjchem-976	191	110	,	,	PUNCT
eurjchem-976	191	111	4.10	4.10	NUM
eurjchem-976	191	112	(	(	PUNCT
eurjchem-976	191	113	q	q	NOUN
eurjchem-976	191	114	,	,	PUNCT
eurjchem-976	191	115	2h	2h	NUM
eurjchem-976	191	116	,	,	PUNCT
eurjchem-976	191	117	j	j	PROPN
eurjchem-976	191	118	=	=	SYM
eurjchem-976	191	119	7.5	7.5	NUM
eurjchem-976	191	120	hz	hz	NOUN
eurjchem-976	191	121	,	,	PUNCT
eurjchem-976	191	122	ch2	ch2	PROPN
eurjchem-976	191	123	)	)	PUNCT
eurjchem-976	191	124	,	,	PUNCT
eurjchem-976	191	125	7.22‐8.45	7.22‐8.45	NUM
eurjchem-976	191	126	(	(	PUNCT
eurjchem-976	191	127	m	m	PROPN
eurjchem-976	191	128	,	,	PUNCT
eurjchem-976	191	129	10	10	NUM
eurjchem-976	191	130	h	h	NOUN
eurjchem-976	191	131	,	,	PUNCT
eurjchem-976	191	132	ar‐h	ar‐h	NOUN
eurjchem-976	191	133	)	)	PUNCT
eurjchem-976	191	134	.	.	PUNCT
eurjchem-976	192	1	anal	anal	PROPN
eurjchem-976	192	2	.	.	PUNCT
eurjchem-976	192	3	calcd	calcd	NOUN
eurjchem-976	192	4	.	.	PUNCT
eurjchem-976	193	1	for	for	ADP
eurjchem-976	193	2	c20h19cln2o2	c20h19cln2o2	NOUN
eurjchem-976	193	3	:	:	PUNCT
eurjchem-976	193	4	c	c	NOUN
eurjchem-976	193	5	,	,	PUNCT
eurjchem-976	193	6	67.70	67.70	NUM
eurjchem-976	193	7	;	;	PUNCT
eurjchem-976	193	8	h	h	NOUN
eurjchem-976	193	9	,	,	PUNCT
eurjchem-976	193	10	5.40	5.40	NUM
eurjchem-976	193	11	;	;	PUNCT
eurjchem-976	193	12	n	n	CCONJ
eurjchem-976	193	13	,	,	PUNCT
eurjchem-976	193	14	7.89	7.89	NUM
eurjchem-976	193	15	.	.	PUNCT
eurjchem-976	193	16	found	find	VERB
eurjchem-976	193	17	;	;	PUNCT
eurjchem-976	193	18	c	c	X
eurjchem-976	193	19	,	,	PUNCT
eurjchem-976	193	20	67.91	67.91	NUM
eurjchem-976	193	21	;	;	PUNCT
eurjchem-976	194	1	h	h	NOUN
eurjchem-976	194	2	,	,	PUNCT
eurjchem-976	194	3	5.37	5.37	NUM
eurjchem-976	194	4	;	;	PUNCT
eurjchem-976	194	5	n	n	CCONJ
eurjchem-976	194	6	,	,	PUNCT
eurjchem-976	194	7	7.90	7.90	NUM
eurjchem-976	194	8	%	%	NOUN
eurjchem-976	194	9	.	.	PUNCT
eurjchem-976	195	1	ethyl	ethyl	PROPN
eurjchem-976	195	2	2‐((5‐chloro‐1,3‐diphenyl‐1h‐pyrazol‐4‐yl)methyl	2‐((5‐chloro‐1,3‐diphenyl‐1h‐pyrazol‐4‐yl)methyl	PROPN
eurjchem-976	195	3	)	)	PUNCT
eurjchem-976	195	4	propanoate	propanoate	NOUN
eurjchem-976	195	5	(	(	PUNCT
eurjchem-976	195	6	15b	15b	NUM
eurjchem-976	195	7	):	):	PUNCT
eurjchem-976	195	8	color	color	NOUN
eurjchem-976	195	9	:	:	PUNCT
eurjchem-976	195	10	pale	pale	ADJ
eurjchem-976	195	11	yellow	yellow	ADJ
eurjchem-976	195	12	crystals	crystal	NOUN
eurjchem-976	195	13	.	.	PUNCT
eurjchem-976	196	1	yield	yield	NOUN
eurjchem-976	196	2	:	:	PUNCT
eurjchem-976	196	3	86	86	NUM
eurjchem-976	196	4	%	%	NOUN
eurjchem-976	196	5	.	.	PUNCT
eurjchem-976	197	1	m.p	m.p	PROPN
eurjchem-976	197	2	.	.	PROPN
eurjchem-976	197	3	:	:	PUNCT
eurjchem-976	198	1	74	74	NUM
eurjchem-976	198	2	°	°	NUM
eurjchem-976	198	3	c	c	NOUN
eurjchem-976	198	4	(	(	PUNCT
eurjchem-976	198	5	ethanol	ethanol	NOUN
eurjchem-976	198	6	)	)	PUNCT
eurjchem-976	198	7	.	.	PUNCT
eurjchem-976	199	1	ir	ir	PROPN
eurjchem-976	199	2	(	(	PUNCT
eurjchem-976	199	3	kbr	kbr	PROPN
eurjchem-976	199	4	,	,	PUNCT
eurjchem-976	199	5	ν	ν	PROPN
eurjchem-976	199	6	,	,	PUNCT
eurjchem-976	199	7	cm‐1	cm‐1	PROPN
eurjchem-976	199	8	):	):	PUNCT
eurjchem-976	199	9	3105	3105	NUM
eurjchem-976	199	10	(	(	PUNCT
eurjchem-976	199	11	ch	ch	NOUN
eurjchem-976	199	12	)	)	PUNCT
eurjchem-976	199	13	(	(	PUNCT
eurjchem-976	199	14	aromatic	aromatic	NOUN
eurjchem-976	199	15	)	)	PUNCT
eurjchem-976	199	16	,	,	PUNCT
eurjchem-976	199	17	2985	2985	NUM
eurjchem-976	199	18	(	(	PUNCT
eurjchem-976	199	19	ch	ch	NOUN
eurjchem-976	199	20	)	)	PUNCT
eurjchem-976	199	21	(	(	PUNCT
eurjchem-976	199	22	alkyl	alkyl	NOUN
eurjchem-976	199	23	)	)	PUNCT
eurjchem-976	199	24	,	,	PUNCT
eurjchem-976	199	25	1742	1742	NUM
eurjchem-976	199	26	(	(	PUNCT
eurjchem-976	199	27	c	c	NOUN
eurjchem-976	199	28	=	=	NOUN
eurjchem-976	199	29	o	o	NOUN
eurjchem-976	199	30	)	)	PUNCT
eurjchem-976	199	31	(	(	PUNCT
eurjchem-976	199	32	ester	ester	NOUN
eurjchem-976	199	33	)	)	PUNCT
eurjchem-976	199	34	,	,	PUNCT
eurjchem-976	199	35	1600	1600	NUM
eurjchem-976	199	36	,	,	PUNCT
eurjchem-976	199	37	1560	1560	NUM
eurjchem-976	199	38	,	,	PUNCT
eurjchem-976	199	39	1485	1485	NUM
eurjchem-976	199	40	,	,	PUNCT
eurjchem-976	199	41	1440	1440	NUM
eurjchem-976	199	42	(	(	PUNCT
eurjchem-976	199	43	c	c	NOUN
eurjchem-976	199	44	=	=	SYM
eurjchem-976	199	45	c	c	NOUN
eurjchem-976	199	46	)	)	PUNCT
eurjchem-976	199	47	(	(	PUNCT
eurjchem-976	199	48	aromatic	aromatic	NOUN
eurjchem-976	199	49	)	)	PUNCT
eurjchem-976	199	50	,	,	PUNCT
eurjchem-976	199	51	1370	1370	NUM
eurjchem-976	199	52	,	,	PUNCT
eurjchem-976	199	53	1220	1220	NUM
eurjchem-976	199	54	,	,	PUNCT
eurjchem-976	199	55	747	747	NUM
eurjchem-976	199	56	.	.	NOUN
eurjchem-976	199	57	1h	1h	NUM
eurjchem-976	199	58	nmr	nmr	NOUN
eurjchem-976	199	59	(	(	PUNCT
eurjchem-976	199	60	90	90	NUM
eurjchem-976	199	61	mhz	mhz	NOUN
eurjchem-976	199	62	,	,	PUNCT
eurjchem-976	199	63	cdcl3	cdcl3	PROPN
eurjchem-976	199	64	,	,	PUNCT
eurjchem-976	199	65	δ	δ	PROPN
eurjchem-976	199	66	,	,	PUNCT
eurjchem-976	199	67	ppm	ppm	NUM
eurjchem-976	199	68	):	):	PUNCT
eurjchem-976	199	69	1.12	1.12	NUM
eurjchem-976	199	70	(	(	PUNCT
eurjchem-976	199	71	d	d	PROPN
eurjchem-976	199	72	,	,	PUNCT
eurjchem-976	199	73	3h	3h	NUM
eurjchem-976	199	74	,	,	PUNCT
eurjchem-976	199	75	j	j	PROPN
eurjchem-976	199	76	=	=	PROPN
eurjchem-976	199	77	10.4	10.4	NUM
eurjchem-976	199	78	hz	hz	NOUN
eurjchem-976	199	79	,	,	PUNCT
eurjchem-976	199	80	ch3	ch3	PROPN
eurjchem-976	199	81	)	)	PUNCT
eurjchem-976	199	82	,	,	PUNCT
eurjchem-976	199	83	1.25	1.25	NUM
eurjchem-976	199	84	(	(	PUNCT
eurjchem-976	199	85	t	t	PROPN
eurjchem-976	199	86	,	,	PUNCT
eurjchem-976	199	87	3h	3h	NUM
eurjchem-976	199	88	,	,	PUNCT
eurjchem-976	199	89	j	j	PROPN
eurjchem-976	199	90	=	=	SYM
eurjchem-976	199	91	7.5	7.5	NUM
eurjchem-976	199	92	hz	hz	ADJ
eurjchem-976	199	93	,	,	PUNCT
eurjchem-976	199	94	ch3	ch3	PROPN
eurjchem-976	199	95	)	)	PUNCT
eurjchem-976	199	96	,	,	PUNCT
eurjchem-976	199	97	2.66	2.66	NUM
eurjchem-976	199	98	(	(	PUNCT
eurjchem-976	199	99	q	q	NOUN
eurjchem-976	199	100	,	,	PUNCT
eurjchem-976	199	101	ha	ha	INTJ
eurjchem-976	199	102	,	,	PUNCT
eurjchem-976	199	103	j	j	PROPN
eurjchem-976	199	104	=	=	PROPN
eurjchem-976	199	105	16.3	16.3	NUM
eurjchem-976	199	106	hz	hz	NOUN
eurjchem-976	199	107	,	,	PUNCT
eurjchem-976	199	108	ch2	ch2	PROPN
eurjchem-976	199	109	)	)	PUNCT
eurjchem-976	199	110	,	,	PUNCT
eurjchem-976	199	111	2.71	2.71	NUM
eurjchem-976	199	112	(	(	PUNCT
eurjchem-976	199	113	ddq	ddq	PROPN
eurjchem-976	199	114	,	,	PUNCT
eurjchem-976	199	115	1h	1h	NUM
eurjchem-976	199	116	,	,	PUNCT
eurjchem-976	199	117	j	j	PROPN
eurjchem-976	199	118	=	=	SYM
eurjchem-976	199	119	9.3	9.3	NUM
eurjchem-976	199	120	hz	hz	VERB
eurjchem-976	199	121	,	,	PUNCT
eurjchem-976	199	122	‐ch	‐ch	NOUN
eurjchem-976	199	123	)	)	PUNCT
eurjchem-976	199	124	,	,	PUNCT
eurjchem-976	199	125	2.94	2.94	NUM
eurjchem-976	199	126	(	(	PUNCT
eurjchem-976	199	127	dd	dd	PROPN
eurjchem-976	199	128	,	,	PUNCT
eurjchem-976	199	129	hb	hb	PROPN
eurjchem-976	199	130	,	,	PUNCT
eurjchem-976	199	131	j	j	PROPN
eurjchem-976	199	132	=	=	PROPN
eurjchem-976	199	133	16.3	16.3	NUM
eurjchem-976	199	134	hz	hz	NOUN
eurjchem-976	199	135	,	,	PUNCT
eurjchem-976	199	136	ch2	ch2	PROPN
eurjchem-976	199	137	)	)	PUNCT
eurjchem-976	199	138	,	,	PUNCT
eurjchem-976	199	139	4.25	4.25	NUM
eurjchem-976	199	140	(	(	PUNCT
eurjchem-976	199	141	q	q	NOUN
eurjchem-976	199	142	,	,	PUNCT
eurjchem-976	199	143	2h	2h	NUM
eurjchem-976	199	144	,	,	PUNCT
eurjchem-976	199	145	j	j	PROPN
eurjchem-976	199	146	=	=	SYM
eurjchem-976	199	147	7.5	7.5	NUM
eurjchem-976	199	148	hz	hz	NOUN
eurjchem-976	199	149	,	,	PUNCT
eurjchem-976	199	150	ch2	ch2	PROPN
eurjchem-976	199	151	)	)	PUNCT
eurjchem-976	199	152	,	,	PUNCT
eurjchem-976	199	153	6.95‐8.25	6.95‐8.25	PROPN
eurjchem-976	199	154	(	(	PUNCT
eurjchem-976	199	155	m	m	PROPN
eurjchem-976	199	156	,	,	PUNCT
eurjchem-976	199	157	10h	10h	NUM
eurjchem-976	199	158	,	,	PUNCT
eurjchem-976	199	159	ar‐h	ar‐h	NOUN
eurjchem-976	199	160	)	)	PUNCT
eurjchem-976	199	161	.	.	PUNCT
eurjchem-976	200	1	anal	anal	PROPN
eurjchem-976	200	2	.	.	PUNCT
eurjchem-976	200	3	calcd	calcd	NOUN
eurjchem-976	200	4	.	.	PUNCT
eurjchem-976	201	1	for	for	ADP
eurjchem-976	201	2	c21h21cln2o2	c21h21cln2o2	ADJ
eurjchem-976	201	3	:	:	PUNCT
eurjchem-976	201	4	c	c	X
eurjchem-976	201	5	,	,	PUNCT
eurjchem-976	201	6	68.38	68.38	NUM
eurjchem-976	201	7	;	;	PUNCT
eurjchem-976	201	8	h	h	NOUN
eurjchem-976	201	9	,	,	PUNCT
eurjchem-976	201	10	5.74	5.74	NUM
eurjchem-976	201	11	;	;	PUNCT
eurjchem-976	201	12	n	n	CCONJ
eurjchem-976	201	13	,	,	PUNCT
eurjchem-976	201	14	7.59	7.59	NUM
eurjchem-976	201	15	.	.	PUNCT
eurjchem-976	201	16	found	find	VERB
eurjchem-976	201	17	;	;	PUNCT
eurjchem-976	202	1	c	c	X
eurjchem-976	202	2	,	,	PUNCT
eurjchem-976	202	3	68.36	68.36	NUM
eurjchem-976	202	4	;	;	PUNCT
eurjchem-976	202	5	h	h	NOUN
eurjchem-976	202	6	,	,	PUNCT
eurjchem-976	202	7	5.69	5.69	NUM
eurjchem-976	202	8	;	;	PUNCT
eurjchem-976	202	9	n	n	CCONJ
eurjchem-976	202	10	,	,	PUNCT
eurjchem-976	202	11	7.65	7.65	NUM
eurjchem-976	202	12	%	%	NOUN
eurjchem-976	202	13	.	.	PUNCT
eurjchem-976	203	1	el‐aal	el‐aal	PROPN
eurjchem-976	203	2	et	et	NOUN
eurjchem-976	203	3	al	al	PROPN
eurjchem-976	203	4	.	.	PUNCT
eurjchem-976	203	5	/	/	SYM
eurjchem-976	203	6	european	european	PROPN
eurjchem-976	203	7	journal	journal	PROPN
eurjchem-976	203	8	of	of	ADP
eurjchem-976	203	9	chemistry	chemistry	NOUN
eurjchem-976	203	10	5	5	NUM
eurjchem-976	203	11	(	(	PUNCT
eurjchem-976	203	12	2	2	NUM
eurjchem-976	203	13	)	)	PUNCT
eurjchem-976	203	14	(	(	PUNCT
eurjchem-976	203	15	2014	2014	NUM
eurjchem-976	203	16	)	)	PUNCT
eurjchem-976	203	17	277‐286	277‐286	NUM
eurjchem-976	203	18	281	281	NUM
eurjchem-976	203	19	table	table	NOUN
eurjchem-976	203	20	1	1	NUM
eurjchem-976	203	21	.	.	PUNCT
eurjchem-976	203	22	optimum	optimum	ADJ
eurjchem-976	203	23	conditions	condition	NOUN
eurjchem-976	203	24	for	for	ADP
eurjchem-976	203	25	the	the	DET
eurjchem-976	203	26	synthesis	synthesis	NOUN
eurjchem-976	203	27	of	of	ADP
eurjchem-976	203	28	heteroarylalkanols	heteroarylalkanol	NOUN
eurjchem-976	203	29	8	8	NUM
eurjchem-976	203	30	,	,	PUNCT
eurjchem-976	203	31	12a	12a	NUM
eurjchem-976	203	32	,	,	PUNCT
eurjchem-976	203	33	b	b	NOUN
eurjchem-976	203	34	and	and	CCONJ
eurjchem-976	203	35	16a	16a	NOUN
eurjchem-976	203	36	,	,	PUNCT
eurjchem-976	203	37	b.	b.	NOUN
eurjchem-976	203	38	entry	entry	NOUN
eurjchem-976	203	39	substrate	substrate	NOUN
eurjchem-976	203	40	product	product	NOUN
eurjchem-976	203	41	conditions	condition	NOUN
eurjchem-976	203	42	a	a	DET
eurjchem-976	203	43	mp	mp	NOUN
eurjchem-976	203	44	°	°	ADP
eurjchem-976	203	45	c	c	X
eurjchem-976	203	46	(	(	PUNCT
eurjchem-976	203	47	nd25	nd25	PROPN
eurjchem-976	203	48	)	)	PUNCT
eurjchem-976	203	49	yield	yield	NOUN
eurjchem-976	203	50	(	(	PUNCT
eurjchem-976	203	51	%	%	INTJ
eurjchem-976	203	52	)	)	PUNCT
eurjchem-976	203	53	b	b	NOUN
eurjchem-976	203	54	1	1	NUM
eurjchem-976	203	55	7	7	NUM
eurjchem-976	203	56	et2o	et2o	ADJ
eurjchem-976	203	57	/	/	SYM
eurjchem-976	203	58	thf	thf	NOUN
eurjchem-976	203	59	,	,	PUNCT
eurjchem-976	203	60	rt	rt	PROPN
eurjchem-976	203	61	,	,	PUNCT
eurjchem-976	203	62	8	8	NUM
eurjchem-976	203	63	h	h	NOUN
eurjchem-976	203	64	92	92	NUM
eurjchem-976	203	65	8	8	NUM
eurjchem-976	203	66	(	(	PUNCT
eurjchem-976	203	67	89	89	NUM
eurjchem-976	203	68	)	)	SYM
eurjchem-976	203	69	2	2	NUM
eurjchem-976	203	70	11a	11a	NOUN
eurjchem-976	203	71	et2o	et2o	ADJ
eurjchem-976	203	72	/	/	SYM
eurjchem-976	203	73	thf	thf	NOUN
eurjchem-976	203	74	,	,	PUNCT
eurjchem-976	203	75	rt	rt	PROPN
eurjchem-976	203	76	,	,	PUNCT
eurjchem-976	203	77	6	6	NUM
eurjchem-976	203	78	h	h	NOUN
eurjchem-976	203	79	(	(	PUNCT
eurjchem-976	203	80	1.597	1.597	NUM
eurjchem-976	203	81	)	)	PUNCT
eurjchem-976	203	82	12a	12a	NOUN
eurjchem-976	203	83	(	(	PUNCT
eurjchem-976	203	84	85	85	NUM
eurjchem-976	203	85	)	)	PUNCT
eurjchem-976	203	86	3	3	NUM
eurjchem-976	203	87	11b	11b	NOUN
eurjchem-976	203	88	n	n	CCONJ
eurjchem-976	203	89	n	n	PRON
eurjchem-976	203	90	ph	ph	NOUN
eurjchem-976	203	91	ph	ph	NOUN
eurjchem-976	203	92	o	o	NOUN
eurjchem-976	204	1	oh	oh	INTJ
eurjchem-976	204	2	12b	12b	X
eurjchem-976	204	3	et2o	et2o	ADJ
eurjchem-976	204	4	/	/	SYM
eurjchem-976	204	5	thf	thf	NOUN
eurjchem-976	204	6	,	,	PUNCT
eurjchem-976	204	7	rt	rt	PROPN
eurjchem-976	204	8	,	,	PUNCT
eurjchem-976	204	9	8	8	NUM
eurjchem-976	204	10	h	h	NOUN
eurjchem-976	204	11	84	84	NUM
eurjchem-976	204	12	12b	12b	NOUN
eurjchem-976	204	13	(	(	PUNCT
eurjchem-976	204	14	92	92	NUM
eurjchem-976	204	15	)	)	SYM
eurjchem-976	204	16	4	4	NUM
eurjchem-976	204	17	15a	15a	NOUN
eurjchem-976	204	18	et2o	et2o	PROPN
eurjchem-976	204	19	,	,	PUNCT
eurjchem-976	204	20	rt	rt	PROPN
eurjchem-976	204	21	,	,	PUNCT
eurjchem-976	204	22	4	4	NUM
eurjchem-976	204	23	h	h	NOUN
eurjchem-976	204	24	118	118	NUM
eurjchem-976	204	25	16a	16a	NOUN
eurjchem-976	204	26	(	(	PUNCT
eurjchem-976	204	27	90	90	NUM
eurjchem-976	204	28	)	)	SYM
eurjchem-976	204	29	5	5	NUM
eurjchem-976	204	30	15b	15b	X
eurjchem-976	204	31	et2o	et2o	PROPN
eurjchem-976	204	32	,	,	PUNCT
eurjchem-976	204	33	rt	rt	PROPN
eurjchem-976	204	34	,	,	PUNCT
eurjchem-976	204	35	5	5	NUM
eurjchem-976	204	36	h	h	NOUN
eurjchem-976	204	37	(	(	PUNCT
eurjchem-976	204	38	1.619	1.619	NUM
eurjchem-976	204	39	)	)	PUNCT
eurjchem-976	204	40	16b	16b	NOUN
eurjchem-976	204	41	(	(	PUNCT
eurjchem-976	204	42	86	86	NUM
eurjchem-976	204	43	)	)	PUNCT
eurjchem-976	204	44	a	a	DET
eurjchem-976	204	45	all	all	DET
eurjchem-976	204	46	reactions	reaction	NOUN
eurjchem-976	204	47	were	be	AUX
eurjchem-976	204	48	performed	perform	VERB
eurjchem-976	204	49	using	use	VERB
eurjchem-976	204	50	0.4	0.4	NUM
eurjchem-976	204	51	equiv	equiv	PROPN
eurjchem-976	204	52	.	.	PUNCT
eurjchem-976	205	1	excess	excess	NOUN
eurjchem-976	205	2	of	of	ADP
eurjchem-976	205	3	memgi	memgi	NOUN
eurjchem-976	205	4	.	.	PUNCT
eurjchem-976	206	1	b	b	NOUN
eurjchem-976	206	2	isolated	isolate	VERB
eurjchem-976	206	3	yield	yield	NOUN
eurjchem-976	206	4	refer	refer	VERB
eurjchem-976	206	5	to	to	ADP
eurjchem-976	206	6	substrate	substrate	NOUN
eurjchem-976	206	7	.	.	PUNCT
eurjchem-976	207	1	2.2.8	2.2.8	X
eurjchem-976	207	2	.	.	PUNCT
eurjchem-976	207	3	general	general	ADJ
eurjchem-976	207	4	procedure	procedure	NOUN
eurjchem-976	207	5	for	for	ADP
eurjchem-976	207	6	the	the	DET
eurjchem-976	207	7	synthesis	synthesis	NOUN
eurjchem-976	207	8	of	of	ADP
eurjchem-976	207	9	alcohols	alcohol	NOUN
eurjchem-976	207	10	8	8	NUM
eurjchem-976	207	11	,	,	PUNCT
eurjchem-976	207	12	12a	12a	NUM
eurjchem-976	207	13	,	,	PUNCT
eurjchem-976	207	14	b	b	NOUN
eurjchem-976	207	15	,	,	PUNCT
eurjchem-976	207	16	16a	16a	NOUN
eurjchem-976	207	17	,	,	PUNCT
eurjchem-976	207	18	b	b	NOUN
eurjchem-976	207	19	to	to	ADP
eurjchem-976	207	20	an	an	DET
eurjchem-976	207	21	ice‐cold	ice‐cold	VERB
eurjchem-976	207	22	grignard	grignard	ADJ
eurjchem-976	207	23	reagent	reagent	ADJ
eurjchem-976	207	24	solution	solution	NOUN
eurjchem-976	207	25	obtained	obtain	VERB
eurjchem-976	207	26	as	as	ADP
eurjchem-976	207	27	usual	usual	ADJ
eurjchem-976	207	28	from	from	ADP
eurjchem-976	207	29	mg	mg	PROPN
eurjchem-976	207	30	turnings	turning	NOUN
eurjchem-976	207	31	(	(	PUNCT
eurjchem-976	207	32	0.32	0.32	NUM
eurjchem-976	207	33	g	g	NOUN
eurjchem-976	207	34	,	,	PUNCT
eurjchem-976	207	35	13	13	NUM
eurjchem-976	207	36	mmol	mmol	NOUN
eurjchem-976	207	37	)	)	PUNCT
eurjchem-976	207	38	,	,	PUNCT
eurjchem-976	207	39	alkyl	alkyl	NOUN
eurjchem-976	207	40	or	or	CCONJ
eurjchem-976	207	41	aryl	aryl	NOUN
eurjchem-976	207	42	halide	halide	NOUN
eurjchem-976	207	43	(	(	PUNCT
eurjchem-976	207	44	13	13	NUM
eurjchem-976	207	45	mmol	mmol	NOUN
eurjchem-976	207	46	)	)	PUNCT
eurjchem-976	207	47	in	in	ADP
eurjchem-976	207	48	ether	ether	NOUN
eurjchem-976	207	49	(	(	PUNCT
eurjchem-976	207	50	40	40	NUM
eurjchem-976	207	51	ml	ml	NOUN
eurjchem-976	207	52	)	)	PUNCT
eurjchem-976	207	53	,	,	PUNCT
eurjchem-976	207	54	was	be	AUX
eurjchem-976	207	55	added	add	VERB
eurjchem-976	207	56	a	a	DET
eurjchem-976	207	57	solution	solution	NOUN
eurjchem-976	207	58	of	of	ADP
eurjchem-976	207	59	esters	ester	NOUN
eurjchem-976	207	60	7	7	NUM
eurjchem-976	207	61	or	or	CCONJ
eurjchem-976	207	62	11a	11a	NUM
eurjchem-976	207	63	,	,	PUNCT
eurjchem-976	207	64	b	b	NOUN
eurjchem-976	207	65	or	or	CCONJ
eurjchem-976	207	66	15a	15a	NOUN
eurjchem-976	207	67	,	,	PUNCT
eurjchem-976	207	68	b	b	PROPN
eurjchem-976	207	69	(	(	PUNCT
eurjchem-976	207	70	4.6	4.6	NUM
eurjchem-976	207	71	mmol	mmol	NOUN
eurjchem-976	207	72	)	)	PUNCT
eurjchem-976	207	73	in	in	ADP
eurjchem-976	207	74	ether	ether	NOUN
eurjchem-976	207	75	or	or	CCONJ
eurjchem-976	207	76	thf	thf	NOUN
eurjchem-976	207	77	(	(	PUNCT
eurjchem-976	207	78	30	30	NUM
eurjchem-976	207	79	ml	ml	NOUN
eurjchem-976	207	80	)	)	PUNCT
eurjchem-976	207	81	.	.	PUNCT
eurjchem-976	208	1	the	the	DET
eurjchem-976	208	2	reaction	reaction	NOUN
eurjchem-976	208	3	mixture	mixture	NOUN
eurjchem-976	208	4	was	be	AUX
eurjchem-976	208	5	stirred	stir	VERB
eurjchem-976	208	6	at	at	ADP
eurjchem-976	208	7	required	require	VERB
eurjchem-976	208	8	temperature	temperature	NOUN
eurjchem-976	208	9	for	for	ADP
eurjchem-976	208	10	appointed	appoint	VERB
eurjchem-976	208	11	time	time	NOUN
eurjchem-976	208	12	(	(	PUNCT
eurjchem-976	208	13	table	table	NOUN
eurjchem-976	208	14	1	1	NUM
eurjchem-976	208	15	)	)	PUNCT
eurjchem-976	208	16	followed	follow	VERB
eurjchem-976	208	17	by	by	ADP
eurjchem-976	208	18	decomposition	decomposition	NOUN
eurjchem-976	208	19	with	with	ADP
eurjchem-976	208	20	saturated	saturate	VERB
eurjchem-976	208	21	aqueous	aqueous	ADJ
eurjchem-976	208	22	nh4cl	nh4cl	PROPN
eurjchem-976	208	23	solution	solution	NOUN
eurjchem-976	208	24	.	.	PUNCT
eurjchem-976	209	1	the	the	DET
eurjchem-976	209	2	product	product	NOUN
eurjchem-976	209	3	was	be	AUX
eurjchem-976	209	4	extracted	extract	VERB
eurjchem-976	209	5	with	with	ADP
eurjchem-976	209	6	ether	ether	NOUN
eurjchem-976	209	7	(	(	PUNCT
eurjchem-976	209	8	3×30	3×30	NUM
eurjchem-976	209	9	ml	ml	NOUN
eurjchem-976	209	10	)	)	PUNCT
eurjchem-976	209	11	and	and	CCONJ
eurjchem-976	209	12	the	the	DET
eurjchem-976	209	13	combined	combine	VERB
eurjchem-976	209	14	organic	organic	ADJ
eurjchem-976	209	15	phases	phase	NOUN
eurjchem-976	209	16	were	be	AUX
eurjchem-976	209	17	washed	wash	VERB
eurjchem-976	209	18	with	with	ADP
eurjchem-976	209	19	water	water	NOUN
eurjchem-976	209	20	,	,	PUNCT
eurjchem-976	209	21	dried	dry	VERB
eurjchem-976	209	22	over	over	ADP
eurjchem-976	209	23	anhydrous	anhydrous	ADJ
eurjchem-976	209	24	mgso4	mgso4	NOUN
eurjchem-976	209	25	.	.	PUNCT
eurjchem-976	210	1	the	the	DET
eurjchem-976	210	2	solvent	solvent	NOUN
eurjchem-976	210	3	was	be	AUX
eurjchem-976	210	4	removed	remove	VERB
eurjchem-976	210	5	in	in	ADP
eurjchem-976	210	6	vacuo	vacuo	PROPN
eurjchem-976	210	7	and	and	CCONJ
eurjchem-976	210	8	the	the	DET
eurjchem-976	210	9	residue	residue	NOUN
eurjchem-976	210	10	was	be	AUX
eurjchem-976	210	11	purified	purify	VERB
eurjchem-976	210	12	by	by	ADP
eurjchem-976	210	13	flash	flash	NOUN
eurjchem-976	210	14	column	column	NOUN
eurjchem-976	210	15	chromatography	chromatography	NOUN
eurjchem-976	210	16	(	(	PUNCT
eurjchem-976	210	17	basic	basic	ADJ
eurjchem-976	210	18	alumina	alumina	NOUN
eurjchem-976	210	19	,	,	PUNCT
eurjchem-976	210	20	etoac	etoac	ADJ
eurjchem-976	210	21	:	:	PUNCT
eurjchem-976	210	22	n‐hexane	n‐hexane	ADJ
eurjchem-976	210	23	,	,	PUNCT
eurjchem-976	210	24	3:1	3:1	NUM
eurjchem-976	210	25	,	,	PUNCT
eurjchem-976	210	26	v	v	NOUN
eurjchem-976	210	27	:	:	SYM
eurjchem-976	210	28	v	v	NOUN
eurjchem-976	210	29	)	)	PUNCT
eurjchem-976	210	30	resulting	result	VERB
eurjchem-976	210	31	pure	pure	ADJ
eurjchem-976	210	32	alcohols	alcohol	NOUN
eurjchem-976	210	33	8	8	NUM
eurjchem-976	210	34	or	or	CCONJ
eurjchem-976	210	35	12a	12a	NOUN
eurjchem-976	210	36	,	,	PUNCT
eurjchem-976	210	37	b	b	NOUN
eurjchem-976	210	38	or	or	CCONJ
eurjchem-976	210	39	16a	16a	NOUN
eurjchem-976	210	40	,	,	PUNCT
eurjchem-976	210	41	b	b	NUM
eurjchem-976	210	42	(	(	PUNCT
eurjchem-976	210	43	scheme	scheme	NOUN
eurjchem-976	210	44	2	2	NUM
eurjchem-976	210	45	)	)	PUNCT
eurjchem-976	210	46	.	.	PUNCT
eurjchem-976	211	1	the	the	DET
eurjchem-976	211	2	conditions	condition	NOUN
eurjchem-976	211	3	and	and	CCONJ
eurjchem-976	211	4	isolated	isolated	ADJ
eurjchem-976	211	5	yields	yield	NOUN
eurjchem-976	211	6	are	be	AUX
eurjchem-976	211	7	shown	show	VERB
eurjchem-976	211	8	in	in	ADP
eurjchem-976	211	9	table	table	NOUN
eurjchem-976	211	10	1	1	NUM
eurjchem-976	211	11	and	and	CCONJ
eurjchem-976	211	12	spectral	spectral	ADJ
eurjchem-976	211	13	data	datum	NOUN
eurjchem-976	211	14	are	be	AUX
eurjchem-976	211	15	given	give	VERB
eurjchem-976	211	16	in	in	ADP
eurjchem-976	211	17	the	the	DET
eurjchem-976	211	18	following	following	NOUN
eurjchem-976	211	19	:	:	PUNCT
eurjchem-976	211	20	2‐(5‐chloro‐1,3‐diphenyl‐1h‐pyrazol‐4‐yl)propan‐2‐ol	2‐(5‐chloro‐1,3‐diphenyl‐1h‐pyrazol‐4‐yl)propan‐2‐ol	NUM
eurjchem-976	211	21	(	(	PUNCT
eurjchem-976	211	22	8)	8)	NUM
eurjchem-976	211	23	:	:	PUNCT
eurjchem-976	211	24	color	color	NOUN
eurjchem-976	211	25	:	:	PUNCT
eurjchem-976	211	26	white	white	ADJ
eurjchem-976	211	27	plates	plate	NOUN
eurjchem-976	211	28	.	.	PUNCT
eurjchem-976	212	1	yield	yield	NOUN
eurjchem-976	212	2	:	:	PUNCT
eurjchem-976	212	3	80	80	NUM
eurjchem-976	212	4	%	%	NOUN
eurjchem-976	212	5	.	.	PUNCT
eurjchem-976	213	1	m.p	m.p	PROPN
eurjchem-976	213	2	.	.	PROPN
eurjchem-976	213	3	:	:	PUNCT
eurjchem-976	214	1	92	92	NUM
eurjchem-976	214	2	°	°	NUM
eurjchem-976	214	3	c	c	NOUN
eurjchem-976	214	4	(	(	PUNCT
eurjchem-976	214	5	cyclohexane	cyclohexane	NOUN
eurjchem-976	214	6	)	)	PUNCT
eurjchem-976	214	7	.	.	PUNCT
eurjchem-976	215	1	ir	ir	PROPN
eurjchem-976	215	2	(	(	PUNCT
eurjchem-976	215	3	kbr	kbr	PROPN
eurjchem-976	215	4	,	,	PUNCT
eurjchem-976	215	5	ν	ν	PROPN
eurjchem-976	215	6	,	,	PUNCT
eurjchem-976	215	7	cm‐1	cm‐1	PROPN
eurjchem-976	215	8	):	):	PUNCT
eurjchem-976	215	9	3340	3340	NUM
eurjchem-976	215	10	(	(	PUNCT
eurjchem-976	215	11	oh	oh	INTJ
eurjchem-976	215	12	)	)	PUNCT
eurjchem-976	215	13	(	(	PUNCT
eurjchem-976	215	14	alcohol	alcohol	NOUN
eurjchem-976	215	15	)	)	PUNCT
eurjchem-976	215	16	,	,	PUNCT
eurjchem-976	215	17	3060	3060	NUM
eurjchem-976	215	18	(	(	PUNCT
eurjchem-976	215	19	ch	ch	NOUN
eurjchem-976	215	20	)	)	PUNCT
eurjchem-976	215	21	(	(	PUNCT
eurjchem-976	215	22	aromatic	aromatic	NOUN
eurjchem-976	215	23	)	)	PUNCT
eurjchem-976	215	24	,	,	PUNCT
eurjchem-976	215	25	2975	2975	NUM
eurjchem-976	215	26	(	(	PUNCT
eurjchem-976	215	27	ch	ch	NOUN
eurjchem-976	215	28	)	)	PUNCT
eurjchem-976	215	29	(	(	PUNCT
eurjchem-976	215	30	alkyl	alkyl	NOUN
eurjchem-976	215	31	)	)	PUNCT
eurjchem-976	215	32	,	,	PUNCT
eurjchem-976	215	33	1610	1610	NUM
eurjchem-976	215	34	,	,	PUNCT
eurjchem-976	215	35	1560	1560	NUM
eurjchem-976	215	36	,	,	PUNCT
eurjchem-976	215	37	1450	1450	NUM
eurjchem-976	215	38	,	,	PUNCT
eurjchem-976	215	39	1445	1445	NUM
eurjchem-976	215	40	(	(	PUNCT
eurjchem-976	215	41	c	c	NOUN
eurjchem-976	215	42	=	=	SYM
eurjchem-976	215	43	c	c	NOUN
eurjchem-976	215	44	)	)	PUNCT
eurjchem-976	215	45	(	(	PUNCT
eurjchem-976	215	46	aromatic	aromatic	NOUN
eurjchem-976	215	47	)	)	PUNCT
eurjchem-976	215	48	,	,	PUNCT
eurjchem-976	215	49	1375	1375	NUM
eurjchem-976	215	50	,	,	PUNCT
eurjchem-976	215	51	1330	1330	NUM
eurjchem-976	215	52	,	,	PUNCT
eurjchem-976	215	53	760	760	NUM
eurjchem-976	215	54	.	.	PROPN
eurjchem-976	215	55	1h	1h	NUM
eurjchem-976	215	56	nmr	nmr	NOUN
eurjchem-976	215	57	(	(	PUNCT
eurjchem-976	215	58	400	400	NUM
eurjchem-976	215	59	mhz	mhz	NOUN
eurjchem-976	215	60	,	,	PUNCT
eurjchem-976	215	61	cdcl3	cdcl3	PROPN
eurjchem-976	215	62	,	,	PUNCT
eurjchem-976	215	63	δ	δ	PROPN
eurjchem-976	215	64	,	,	PUNCT
eurjchem-976	215	65	ppm	ppm	NOUN
eurjchem-976	215	66	):	):	PUNCT
eurjchem-976	215	67	1.40	1.40	NUM
eurjchem-976	215	68	(	(	PUNCT
eurjchem-976	215	69	s	s	PROPN
eurjchem-976	215	70	,	,	PUNCT
eurjchem-976	215	71	6h	6h	NUM
eurjchem-976	215	72	,	,	PUNCT
eurjchem-976	215	73	2ch3	2ch3	NUM
eurjchem-976	215	74	)	)	PUNCT
eurjchem-976	215	75	,	,	PUNCT
eurjchem-976	215	76	3.5	3.5	NUM
eurjchem-976	215	77	(	(	PUNCT
eurjchem-976	215	78	s	s	PROPN
eurjchem-976	215	79	,	,	PUNCT
eurjchem-976	215	80	1h	1h	NUM
eurjchem-976	215	81	,	,	PUNCT
eurjchem-976	215	82	oh	oh	INTJ
eurjchem-976	215	83	exchangeable	exchangeable	ADJ
eurjchem-976	215	84	with	with	ADP
eurjchem-976	215	85	d2o	d2o	NOUN
eurjchem-976	215	86	)	)	PUNCT
eurjchem-976	215	87	7.50‐8.60	7.50‐8.60	NUM
eurjchem-976	215	88	(	(	PUNCT
eurjchem-976	215	89	m	m	PROPN
eurjchem-976	215	90	,	,	PUNCT
eurjchem-976	215	91	10h	10h	NUM
eurjchem-976	215	92	,	,	PUNCT
eurjchem-976	215	93	ar‐h	ar‐h	NOUN
eurjchem-976	215	94	)	)	PUNCT
eurjchem-976	215	95	.	.	PUNCT
eurjchem-976	216	1	ms	ms	NOUN
eurjchem-976	216	2	(	(	PUNCT
eurjchem-976	216	3	ei	ei	PROPN
eurjchem-976	216	4	,	,	PUNCT
eurjchem-976	216	5	m	m	PROPN
eurjchem-976	216	6	/	/	SYM
eurjchem-976	216	7	z	z	PROPN
eurjchem-976	216	8	(	(	PUNCT
eurjchem-976	216	9	%	%	NOUN
eurjchem-976	216	10	)	)	PUNCT
eurjchem-976	216	11	):	):	PUNCT
eurjchem-976	216	12	314	314	NUM
eurjchem-976	216	13	(	(	PUNCT
eurjchem-976	216	14	m++2	m++2	PROPN
eurjchem-976	216	15	,	,	PUNCT
eurjchem-976	216	16	6	6	NUM
eurjchem-976	216	17	)	)	PUNCT
eurjchem-976	216	18	,	,	PUNCT
eurjchem-976	216	19	312	312	NUM
eurjchem-976	216	20	(	(	PUNCT
eurjchem-976	216	21	m+	m+	NUM
eurjchem-976	216	22	,	,	PUNCT
eurjchem-976	216	23	17	17	NUM
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eurjchem-976	216	25	,	,	PUNCT
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eurjchem-976	216	27	(	(	PUNCT
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eurjchem-976	216	29	)	)	PUNCT
eurjchem-976	216	30	,	,	PUNCT
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eurjchem-976	216	32	(	(	PUNCT
eurjchem-976	216	33	100	100	NUM
eurjchem-976	216	34	)	)	PUNCT
eurjchem-976	216	35	,	,	PUNCT
eurjchem-976	216	36	277	277	NUM
eurjchem-976	216	37	(	(	PUNCT
eurjchem-976	216	38	61	61	NUM
eurjchem-976	216	39	)	)	PUNCT
eurjchem-976	216	40	,	,	PUNCT
eurjchem-976	216	41	253	253	NUM
eurjchem-976	216	42	(	(	PUNCT
eurjchem-976	216	43	82	82	NUM
eurjchem-976	216	44	)	)	PUNCT
eurjchem-976	216	45	,	,	PUNCT
eurjchem-976	216	46	235	235	NUM
eurjchem-976	216	47	(	(	PUNCT
eurjchem-976	216	48	52	52	NUM
eurjchem-976	216	49	)	)	PUNCT
eurjchem-976	216	50	,	,	PUNCT
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eurjchem-976	216	52	(	(	PUNCT
eurjchem-976	216	53	42	42	NUM
eurjchem-976	216	54	)	)	PUNCT
eurjchem-976	216	55	,	,	PUNCT
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eurjchem-976	216	57	(	(	PUNCT
eurjchem-976	216	58	35	35	NUM
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eurjchem-976	216	60	,	,	PUNCT
eurjchem-976	216	61	177	177	NUM
eurjchem-976	216	62	(	(	PUNCT
eurjchem-976	216	63	18	18	NUM
eurjchem-976	216	64	)	)	PUNCT
eurjchem-976	216	65	,	,	PUNCT
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eurjchem-976	216	67	(	(	PUNCT
eurjchem-976	216	68	14	14	NUM
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eurjchem-976	216	70	,	,	PUNCT
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eurjchem-976	216	72	(	(	PUNCT
eurjchem-976	216	73	37	37	NUM
eurjchem-976	216	74	)	)	PUNCT
eurjchem-976	216	75	,	,	PUNCT
eurjchem-976	216	76	103	103	NUM
eurjchem-976	216	77	(	(	PUNCT
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eurjchem-976	216	80	,	,	PUNCT
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eurjchem-976	216	82	(	(	PUNCT
eurjchem-976	216	83	27	27	NUM
eurjchem-976	216	84	)	)	PUNCT
eurjchem-976	216	85	,	,	PUNCT
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eurjchem-976	216	88	27	27	NUM
eurjchem-976	216	89	)	)	PUNCT
eurjchem-976	216	90	.	.	PUNCT
eurjchem-976	217	1	anal	anal	PROPN
eurjchem-976	217	2	.	.	PUNCT
eurjchem-976	217	3	calcd	calcd	NOUN
eurjchem-976	217	4	.	.	PUNCT
eurjchem-976	218	1	for	for	ADP
eurjchem-976	218	2	c18h17cln2o	c18h17cln2o	NOUN
eurjchem-976	218	3	:	:	PUNCT
eurjchem-976	218	4	c	c	X
eurjchem-976	218	5	,	,	PUNCT
eurjchem-976	218	6	69.12	69.12	NUM
eurjchem-976	218	7	;	;	PUNCT
eurjchem-976	218	8	h	h	X
eurjchem-976	218	9	,	,	PUNCT
eurjchem-976	218	10	5.48	5.48	NUM
eurjchem-976	218	11	;	;	PUNCT
eurjchem-976	218	12	n	n	CCONJ
eurjchem-976	218	13	,	,	PUNCT
eurjchem-976	218	14	8.96	8.96	NUM
eurjchem-976	218	15	.	.	PUNCT
eurjchem-976	218	16	found	find	VERB
eurjchem-976	218	17	;	;	PUNCT
eurjchem-976	218	18	c	c	X
eurjchem-976	218	19	,	,	PUNCT
eurjchem-976	218	20	69.31	69.31	NUM
eurjchem-976	218	21	;	;	PUNCT
eurjchem-976	219	1	h	h	NOUN
eurjchem-976	219	2	,	,	PUNCT
eurjchem-976	219	3	5.26	5.26	NUM
eurjchem-976	219	4	;	;	PUNCT
eurjchem-976	219	5	n	n	CCONJ
eurjchem-976	219	6	,	,	PUNCT
eurjchem-976	219	7	8.82	8.82	NUM
eurjchem-976	219	8	%	%	NOUN
eurjchem-976	219	9	.	.	PUNCT
eurjchem-976	220	1	4‐(2‐hydroxy‐2‐methylpropyl)‐1,3‐diphenyl‐1h‐pyrazol‐5	4‐(2‐hydroxy‐2‐methylpropyl)‐1,3‐diphenyl‐1h‐pyrazol‐5	NUM
eurjchem-976	220	2	(	(	PUNCT
eurjchem-976	220	3	4h)‐one	4h)‐one	NOUN
eurjchem-976	220	4	(	(	PUNCT
eurjchem-976	220	5	12a	12a	NUM
eurjchem-976	220	6	):	):	PUNCT
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eurjchem-976	220	8	:	:	PUNCT
eurjchem-976	220	9	pale	pale	ADJ
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eurjchem-976	220	12	oil	oil	NOUN
eurjchem-976	220	13	.	.	PUNCT
eurjchem-976	221	1	yield	yield	NOUN
eurjchem-976	221	2	:	:	PUNCT
eurjchem-976	221	3	81	81	NUM
eurjchem-976	221	4	%	%	NOUN
eurjchem-976	221	5	.	.	PUNCT
eurjchem-976	222	1	nd25	nd25	PROPN
eurjchem-976	222	2	=	=	PUNCT
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eurjchem-976	222	4	.	.	PUNCT
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eurjchem-976	223	2	(	(	PUNCT
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eurjchem-976	223	4	,	,	PUNCT
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eurjchem-976	223	6	,	,	PUNCT
eurjchem-976	223	7	cm‐1	cm‐1	PROPN
eurjchem-976	223	8	):	):	PUNCT
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eurjchem-976	223	10	(	(	PUNCT
eurjchem-976	223	11	oh	oh	INTJ
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eurjchem-976	223	13	(	(	PUNCT
eurjchem-976	223	14	alcohol	alcohol	NOUN
eurjchem-976	223	15	)	)	PUNCT
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eurjchem-976	223	18	(	(	PUNCT
eurjchem-976	223	19	ch	ch	NOUN
eurjchem-976	223	20	)	)	PUNCT
eurjchem-976	223	21	(	(	PUNCT
eurjchem-976	223	22	aromatic	aromatic	NOUN
eurjchem-976	223	23	)	)	PUNCT
eurjchem-976	223	24	,	,	PUNCT
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eurjchem-976	223	26	(	(	PUNCT
eurjchem-976	223	27	ch	ch	NOUN
eurjchem-976	223	28	)	)	PUNCT
eurjchem-976	223	29	(	(	PUNCT
eurjchem-976	223	30	alkyl	alkyl	NOUN
eurjchem-976	223	31	)	)	PUNCT
eurjchem-976	223	32	,	,	PUNCT
eurjchem-976	223	33	1665	1665	NUM
eurjchem-976	223	34	(	(	PUNCT
eurjchem-976	223	35	c	c	NOUN
eurjchem-976	223	36	=	=	NOUN
eurjchem-976	223	37	o	o	NOUN
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eurjchem-976	223	39	(	(	PUNCT
eurjchem-976	223	40	amide	amide	NOUN
eurjchem-976	223	41	)	)	PUNCT
eurjchem-976	223	42	,	,	PUNCT
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eurjchem-976	223	44	,	,	PUNCT
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eurjchem-976	223	46	,	,	PUNCT
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eurjchem-976	223	48	,	,	PUNCT
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eurjchem-976	223	50	(	(	PUNCT
eurjchem-976	223	51	c	c	NOUN
eurjchem-976	223	52	=	=	SYM
eurjchem-976	223	53	c	c	NOUN
eurjchem-976	223	54	)	)	PUNCT
eurjchem-976	223	55	(	(	PUNCT
eurjchem-976	223	56	aromatic	aromatic	NOUN
eurjchem-976	223	57	)	)	PUNCT
eurjchem-976	223	58	,	,	PUNCT
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eurjchem-976	223	60	,	,	PUNCT
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eurjchem-976	223	62	,	,	PUNCT
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eurjchem-976	223	64	.	.	PUNCT
eurjchem-976	224	1	1h	1h	NUM
eurjchem-976	224	2	nmr	nmr	NOUN
eurjchem-976	224	3	(	(	PUNCT
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eurjchem-976	224	6	,	,	PUNCT
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eurjchem-976	224	8	,	,	PUNCT
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eurjchem-976	224	10	,	,	PUNCT
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eurjchem-976	224	12	):	):	PUNCT
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eurjchem-976	224	14	(	(	PUNCT
eurjchem-976	224	15	s	s	PROPN
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eurjchem-976	224	18	,	,	PUNCT
eurjchem-976	224	19	2ch3	2ch3	NUM
eurjchem-976	224	20	)	)	PUNCT
eurjchem-976	224	21	,	,	PUNCT
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eurjchem-976	224	23	(	(	PUNCT
eurjchem-976	224	24	app	app	PROPN
eurjchem-976	224	25	.	.	PROPN
eurjchem-976	224	26	t	t	PROPN
eurjchem-976	224	27	,	,	PUNCT
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eurjchem-976	224	29	,	,	PUNCT
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eurjchem-976	224	31	=	=	PROPN
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eurjchem-976	224	34	,	,	PUNCT
eurjchem-976	224	35	ch2	ch2	PROPN
eurjchem-976	224	36	)	)	PUNCT
eurjchem-976	224	37	,	,	PUNCT
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eurjchem-976	224	39	(	(	PUNCT
eurjchem-976	224	40	s	s	PROPN
eurjchem-976	224	41	,	,	PUNCT
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eurjchem-976	224	43	,	,	PUNCT
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eurjchem-976	224	45	exchangeable	exchangeable	ADJ
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eurjchem-976	224	47	d2o	d2o	NOUN
eurjchem-976	224	48	)	)	PUNCT
eurjchem-976	224	49	,	,	PUNCT
eurjchem-976	224	50	2.65	2.65	NUM
eurjchem-976	224	51	(	(	PUNCT
eurjchem-976	224	52	t	t	PROPN
eurjchem-976	224	53	,	,	PUNCT
eurjchem-976	224	54	1h	1h	NUM
eurjchem-976	224	55	,	,	PUNCT
eurjchem-976	224	56	j	j	PROPN
eurjchem-976	224	57	=	=	PROPN
eurjchem-976	224	58	14.2	14.2	NUM
eurjchem-976	224	59	hz	hz	NOUN
eurjchem-976	224	60	,	,	PUNCT
eurjchem-976	224	61	ch	ch	NOUN
eurjchem-976	224	62	)	)	PUNCT
eurjchem-976	224	63	,	,	PUNCT
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eurjchem-976	224	65	(	(	PUNCT
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eurjchem-976	224	67	,	,	PUNCT
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eurjchem-976	224	69	,	,	PUNCT
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eurjchem-976	224	71	)	)	PUNCT
eurjchem-976	224	72	.	.	PUNCT
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eurjchem-976	225	2	(	(	PUNCT
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eurjchem-976	225	4	,	,	PUNCT
eurjchem-976	225	5	m	m	PROPN
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eurjchem-976	225	7	z	z	PROPN
eurjchem-976	225	8	(	(	PUNCT
eurjchem-976	225	9	%	%	NOUN
eurjchem-976	225	10	)	)	PUNCT
eurjchem-976	225	11	):	):	PUNCT
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eurjchem-976	225	13	(	(	PUNCT
eurjchem-976	225	14	m+	m+	NUM
eurjchem-976	225	15	,	,	PUNCT
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eurjchem-976	225	17	)	)	PUNCT
eurjchem-976	225	18	,	,	PUNCT
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eurjchem-976	225	20	(	(	PUNCT
eurjchem-976	225	21	100	100	NUM
eurjchem-976	225	22	)	)	PUNCT
eurjchem-976	225	23	,	,	PUNCT
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eurjchem-976	225	25	(	(	PUNCT
eurjchem-976	225	26	55	55	NUM
eurjchem-976	225	27	)	)	PUNCT
eurjchem-976	225	28	,	,	PUNCT
eurjchem-976	225	29	231	231	NUM
eurjchem-976	225	30	(	(	PUNCT
eurjchem-976	225	31	41	41	NUM
eurjchem-976	225	32	)	)	PUNCT
eurjchem-976	225	33	,	,	PUNCT
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eurjchem-976	225	35	(	(	PUNCT
eurjchem-976	225	36	55	55	NUM
eurjchem-976	225	37	)	)	PUNCT
eurjchem-976	225	38	,	,	PUNCT
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eurjchem-976	225	40	(	(	PUNCT
eurjchem-976	225	41	20	20	NUM
eurjchem-976	225	42	)	)	PUNCT
eurjchem-976	225	43	,	,	PUNCT
eurjchem-976	225	44	180	180	NUM
eurjchem-976	225	45	(	(	PUNCT
eurjchem-976	225	46	29	29	NUM
eurjchem-976	225	47	)	)	PUNCT
eurjchem-976	225	48	,	,	PUNCT
eurjchem-976	225	49	178	178	NUM
eurjchem-976	225	50	(	(	PUNCT
eurjchem-976	225	51	15	15	NUM
eurjchem-976	225	52	)	)	PUNCT
eurjchem-976	225	53	,	,	PUNCT
eurjchem-976	225	54	167	167	NUM
eurjchem-976	225	55	(	(	PUNCT
eurjchem-976	225	56	11	11	NUM
eurjchem-976	225	57	)	)	PUNCT
eurjchem-976	225	58	,	,	PUNCT
eurjchem-976	225	59	158	158	NUM
eurjchem-976	225	60	(	(	PUNCT
eurjchem-976	225	61	35	35	NUM
eurjchem-976	225	62	)	)	PUNCT
eurjchem-976	225	63	,	,	PUNCT
eurjchem-976	225	64	103	103	NUM
eurjchem-976	225	65	(	(	PUNCT
eurjchem-976	225	66	24	24	NUM
eurjchem-976	225	67	)	)	PUNCT
eurjchem-976	225	68	,	,	PUNCT
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eurjchem-976	225	70	(	(	PUNCT
eurjchem-976	225	71	22	22	NUM
eurjchem-976	225	72	)	)	PUNCT
eurjchem-976	225	73	,	,	PUNCT
eurjchem-976	225	74	77	77	NUM
eurjchem-976	225	75	(	(	PUNCT
eurjchem-976	225	76	44	44	NUM
eurjchem-976	225	77	)	)	PUNCT
eurjchem-976	225	78	.	.	PUNCT
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eurjchem-976	226	4	.	.	PUNCT
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eurjchem-976	227	3	:	:	PUNCT
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eurjchem-976	227	5	,	,	PUNCT
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eurjchem-976	227	9	,	,	PUNCT
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eurjchem-976	227	13	,	,	PUNCT
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eurjchem-976	227	17	;	;	PUNCT
eurjchem-976	227	18	c	c	X
eurjchem-976	227	19	,	,	PUNCT
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eurjchem-976	228	2	,	,	PUNCT
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eurjchem-976	228	9	.	.	PUNCT
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eurjchem-976	230	2	:	:	PUNCT
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eurjchem-976	230	5	.	.	PUNCT
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eurjchem-976	232	2	°	°	PRON
eurjchem-976	232	3	c	c	X
eurjchem-976	232	4	(	(	PUNCT
eurjchem-976	232	5	benzene	benzene	NOUN
eurjchem-976	232	6	)	)	PUNCT
eurjchem-976	232	7	.	.	PUNCT
eurjchem-976	233	1	ir	ir	PROPN
eurjchem-976	233	2	(	(	PUNCT
eurjchem-976	233	3	kbr	kbr	PROPN
eurjchem-976	233	4	,	,	PUNCT
eurjchem-976	233	5	ν	ν	PROPN
eurjchem-976	233	6	,	,	PUNCT
eurjchem-976	233	7	cm‐1	cm‐1	PROPN
eurjchem-976	233	8	):	):	PUNCT
eurjchem-976	233	9	3425	3425	NUM
eurjchem-976	233	10	(	(	PUNCT
eurjchem-976	233	11	oh	oh	INTJ
eurjchem-976	233	12	)	)	PUNCT
eurjchem-976	233	13	(	(	PUNCT
eurjchem-976	233	14	br	br	PROPN
eurjchem-976	233	15	,	,	PUNCT
eurjchem-976	233	16	alcohol	alcohol	NOUN
eurjchem-976	233	17	)	)	PUNCT
eurjchem-976	233	18	,	,	PUNCT
eurjchem-976	233	19	3060	3060	NUM
eurjchem-976	233	20	(	(	PUNCT
eurjchem-976	233	21	ch	ch	NOUN
eurjchem-976	233	22	)	)	PUNCT
eurjchem-976	233	23	(	(	PUNCT
eurjchem-976	233	24	aromatic	aromatic	NOUN
eurjchem-976	233	25	)	)	PUNCT
eurjchem-976	233	26	,	,	PUNCT
eurjchem-976	233	27	2965	2965	NUM
eurjchem-976	233	28	(	(	PUNCT
eurjchem-976	233	29	ch	ch	NOUN
eurjchem-976	233	30	)	)	PUNCT
eurjchem-976	233	31	(	(	PUNCT
eurjchem-976	233	32	alkyl	alkyl	NOUN
eurjchem-976	233	33	)	)	PUNCT
eurjchem-976	233	34	,	,	PUNCT
eurjchem-976	233	35	1668	1668	NUM
eurjchem-976	233	36	(	(	PUNCT
eurjchem-976	233	37	c	c	NOUN
eurjchem-976	233	38	=	=	NOUN
eurjchem-976	233	39	o	o	NOUN
eurjchem-976	233	40	)	)	PUNCT
eurjchem-976	233	41	(	(	PUNCT
eurjchem-976	233	42	amide	amide	NOUN
eurjchem-976	233	43	)	)	PUNCT
eurjchem-976	233	44	,	,	PUNCT
eurjchem-976	233	45	1594	1594	NUM
eurjchem-976	233	46	,	,	PUNCT
eurjchem-976	233	47	1580	1580	NUM
eurjchem-976	233	48	,	,	PUNCT
eurjchem-976	233	49	1455	1455	NUM
eurjchem-976	233	50	,	,	PUNCT
eurjchem-976	233	51	1440	1440	NUM
eurjchem-976	233	52	(	(	PUNCT
eurjchem-976	233	53	c	c	NOUN
eurjchem-976	233	54	=	=	SYM
eurjchem-976	233	55	c	c	NOUN
eurjchem-976	233	56	)	)	PUNCT
eurjchem-976	233	57	(	(	PUNCT
eurjchem-976	233	58	aromatic	aromatic	NOUN
eurjchem-976	233	59	)	)	PUNCT
eurjchem-976	233	60	,	,	PUNCT
eurjchem-976	233	61	1385	1385	NUM
eurjchem-976	233	62	,	,	PUNCT
eurjchem-976	233	63	1320	1320	NUM
eurjchem-976	233	64	,	,	PUNCT
eurjchem-976	233	65	743	743	NUM
eurjchem-976	233	66	.	.	PUNCT
eurjchem-976	233	67	1h	1h	NUM
eurjchem-976	233	68	nmr	nmr	NOUN
eurjchem-976	233	69	(	(	PUNCT
eurjchem-976	233	70	400	400	NUM
eurjchem-976	233	71	mhz	mhz	NOUN
eurjchem-976	233	72	,	,	PUNCT
eurjchem-976	233	73	cdcl3	cdcl3	PROPN
eurjchem-976	233	74	,	,	PUNCT
eurjchem-976	233	75	δ	δ	PROPN
eurjchem-976	233	76	,	,	PUNCT
eurjchem-976	233	77	ppm	ppm	NUM
eurjchem-976	233	78	):	):	PUNCT
eurjchem-976	233	79	0.90	0.90	NUM
eurjchem-976	233	80	(	(	PUNCT
eurjchem-976	233	81	d	d	PROPN
eurjchem-976	233	82	,	,	PUNCT
eurjchem-976	233	83	3h	3h	NUM
eurjchem-976	233	84	,	,	PUNCT
eurjchem-976	233	85	j	j	PROPN
eurjchem-976	233	86	=	=	SYM
eurjchem-976	233	87	9.4	9.4	NUM
eurjchem-976	233	88	hz	hz	NOUN
eurjchem-976	233	89	,	,	PUNCT
eurjchem-976	233	90	ch3	ch3	PROPN
eurjchem-976	233	91	)	)	PUNCT
eurjchem-976	233	92	,	,	PUNCT
eurjchem-976	233	93	1.27	1.27	NUM
eurjchem-976	233	94	(	(	PUNCT
eurjchem-976	233	95	s	s	PROPN
eurjchem-976	233	96	,	,	PUNCT
eurjchem-976	233	97	6h	6h	NUM
eurjchem-976	233	98	,	,	PUNCT
eurjchem-976	233	99	2ch3	2ch3	NUM
eurjchem-976	233	100	)	)	PUNCT
eurjchem-976	233	101	,	,	PUNCT
eurjchem-976	233	102	1.85	1.85	NUM
eurjchem-976	233	103	(	(	PUNCT
eurjchem-976	233	104	p	p	X
eurjchem-976	233	105	,	,	PUNCT
eurjchem-976	233	106	1h	1h	NUM
eurjchem-976	233	107	,	,	PUNCT
eurjchem-976	233	108	j	j	PROPN
eurjchem-976	233	109	=	=	PROPN
eurjchem-976	233	110	12.5	12.5	NUM
eurjchem-976	233	111	hz	hz	NOUN
eurjchem-976	233	112	,	,	PUNCT
eurjchem-976	233	113	‐ch	‐ch	NOUN
eurjchem-976	233	114	)	)	PUNCT
eurjchem-976	233	115	,	,	PUNCT
eurjchem-976	233	116	2.10	2.10	NUM
eurjchem-976	233	117	(	(	PUNCT
eurjchem-976	233	118	s	s	PROPN
eurjchem-976	233	119	,	,	PUNCT
eurjchem-976	233	120	1h	1h	NUM
eurjchem-976	233	121	,	,	PUNCT
eurjchem-976	233	122	oh	oh	INTJ
eurjchem-976	233	123	exchangeable	exchangeable	ADJ
eurjchem-976	233	124	with	with	ADP
eurjchem-976	233	125	d2o	d2o	NOUN
eurjchem-976	233	126	)	)	PUNCT
eurjchem-976	233	127	,	,	PUNCT
eurjchem-976	233	128	2.42	2.42	NUM
eurjchem-976	233	129	(	(	PUNCT
eurjchem-976	233	130	d	d	PROPN
eurjchem-976	233	131	,	,	PUNCT
eurjchem-976	233	132	1h	1h	NUM
eurjchem-976	233	133	,	,	PUNCT
eurjchem-976	233	134	j	j	PROPN
eurjchem-976	233	135	=	=	PROPN
eurjchem-976	233	136	12.5	12.5	NUM
eurjchem-976	233	137	hz	hz	NOUN
eurjchem-976	233	138	,	,	PUNCT
eurjchem-976	233	139	ch	ch	NOUN
eurjchem-976	233	140	)	)	PUNCT
eurjchem-976	233	141	,	,	PUNCT
eurjchem-976	233	142	7.15‐8.25	7.15‐8.25	NUM
eurjchem-976	233	143	(	(	PUNCT
eurjchem-976	233	144	m	m	PROPN
eurjchem-976	233	145	,	,	PUNCT
eurjchem-976	233	146	10h	10h	NUM
eurjchem-976	233	147	,	,	PUNCT
eurjchem-976	233	148	ar‐h	ar‐h	NOUN
eurjchem-976	233	149	)	)	PUNCT
eurjchem-976	233	150	.	.	PUNCT
eurjchem-976	234	1	ms	ms	NOUN
eurjchem-976	234	2	(	(	PUNCT
eurjchem-976	234	3	ei	ei	PROPN
eurjchem-976	234	4	,	,	PUNCT
eurjchem-976	234	5	m	m	PROPN
eurjchem-976	234	6	/	/	SYM
eurjchem-976	234	7	z	z	PROPN
eurjchem-976	234	8	(	(	PUNCT
eurjchem-976	234	9	%	%	NOUN
eurjchem-976	234	10	)	)	PUNCT
eurjchem-976	234	11	):	):	PUNCT
eurjchem-976	234	12	322	322	NUM
eurjchem-976	234	13	(	(	PUNCT
eurjchem-976	234	14	m+	m+	NUM
eurjchem-976	234	15	,	,	PUNCT
eurjchem-976	234	16	10	10	NUM
eurjchem-976	234	17	)	)	PUNCT
eurjchem-976	234	18	,	,	PUNCT
eurjchem-976	234	19	304	304	NUM
eurjchem-976	234	20	(	(	PUNCT
eurjchem-976	234	21	100	100	NUM
eurjchem-976	234	22	)	)	PUNCT
eurjchem-976	234	23	,	,	PUNCT
eurjchem-976	234	24	263	263	NUM
eurjchem-976	234	25	(	(	PUNCT
eurjchem-976	234	26	31	31	NUM
eurjchem-976	234	27	)	)	PUNCT
eurjchem-976	234	28	,	,	PUNCT
eurjchem-976	234	29	245	245	NUM
eurjchem-976	234	30	(	(	PUNCT
eurjchem-976	234	31	75	75	NUM
eurjchem-976	234	32	)	)	PUNCT
eurjchem-976	234	33	,	,	PUNCT
eurjchem-976	234	34	248	248	NUM
eurjchem-976	234	35	(	(	PUNCT
eurjchem-976	234	36	62	62	NUM
eurjchem-976	234	37	)	)	PUNCT
eurjchem-976	234	38	,	,	PUNCT
eurjchem-976	234	39	235	235	NUM
eurjchem-976	234	40	(	(	PUNCT
eurjchem-976	234	41	33	33	NUM
eurjchem-976	234	42	)	)	PUNCT
eurjchem-976	234	43	,	,	PUNCT
eurjchem-976	234	44	194	194	NUM
eurjchem-976	234	45	(	(	PUNCT
eurjchem-976	234	46	37	37	NUM
eurjchem-976	234	47	)	)	PUNCT
eurjchem-976	234	48	,	,	PUNCT
eurjchem-976	234	49	180	180	NUM
eurjchem-976	234	50	(	(	PUNCT
eurjchem-976	234	51	20	20	NUM
eurjchem-976	234	52	)	)	PUNCT
eurjchem-976	234	53	,	,	PUNCT
eurjchem-976	234	54	177	177	NUM
eurjchem-976	234	55	(	(	PUNCT
eurjchem-976	234	56	14	14	NUM
eurjchem-976	234	57	)	)	PUNCT
eurjchem-976	234	58	,	,	PUNCT
eurjchem-976	234	59	168	168	NUM
eurjchem-976	234	60	(	(	PUNCT
eurjchem-976	234	61	21	21	NUM
eurjchem-976	234	62	)	)	PUNCT
eurjchem-976	234	63	,	,	PUNCT
eurjchem-976	234	64	158	158	NUM
eurjchem-976	234	65	(	(	PUNCT
eurjchem-976	234	66	48	48	NUM
eurjchem-976	234	67	)	)	PUNCT
eurjchem-976	234	68	,	,	PUNCT
eurjchem-976	234	69	103	103	NUM
eurjchem-976	234	70	(	(	PUNCT
eurjchem-976	234	71	23	23	NUM
eurjchem-976	234	72	)	)	PUNCT
eurjchem-976	234	73	,	,	PUNCT
eurjchem-976	234	74	91	91	NUM
eurjchem-976	234	75	(	(	PUNCT
eurjchem-976	234	76	35	35	NUM
eurjchem-976	234	77	)	)	PUNCT
eurjchem-976	234	78	,	,	PUNCT
eurjchem-976	234	79	77	77	NUM
eurjchem-976	234	80	(	(	PUNCT
eurjchem-976	234	81	47	47	NUM
eurjchem-976	234	82	)	)	PUNCT
eurjchem-976	234	83	.	.	PUNCT
eurjchem-976	235	1	anal	anal	PROPN
eurjchem-976	235	2	.	.	PUNCT
eurjchem-976	235	3	calcd	calcd	NOUN
eurjchem-976	235	4	.	.	PUNCT
eurjchem-976	236	1	for	for	SCONJ
eurjchem-976	236	2	c20h22n2o2	c20h22n2o2	NOUN
eurjchem-976	236	3	:	:	PUNCT
eurjchem-976	236	4	c	c	X
eurjchem-976	236	5	,	,	PUNCT
eurjchem-976	236	6	74.51	74.51	NUM
eurjchem-976	236	7	;	;	PUNCT
eurjchem-976	236	8	h	h	NOUN
eurjchem-976	236	9	,	,	PUNCT
eurjchem-976	236	10	6.88	6.88	NUM
eurjchem-976	236	11	;	;	PUNCT
eurjchem-976	236	12	n	n	CCONJ
eurjchem-976	236	13	,	,	PUNCT
eurjchem-976	236	14	8.69	8.69	NUM
eurjchem-976	236	15	.	.	PUNCT
eurjchem-976	236	16	found	find	VERB
eurjchem-976	236	17	;	;	PUNCT
eurjchem-976	236	18	c	c	X
eurjchem-976	236	19	,	,	PUNCT
eurjchem-976	236	20	74.62	74.62	NUM
eurjchem-976	236	21	;	;	PUNCT
eurjchem-976	237	1	h	h	NOUN
eurjchem-976	237	2	,	,	PUNCT
eurjchem-976	237	3	6.69	6.69	NUM
eurjchem-976	237	4	;	;	PUNCT
eurjchem-976	237	5	n	n	CCONJ
eurjchem-976	237	6	,	,	PUNCT
eurjchem-976	237	7	8.63	8.63	NUM
eurjchem-976	237	8	%	%	NOUN
eurjchem-976	237	9	.	.	PUNCT
eurjchem-976	238	1	4‐(5‐chloro‐1,3‐diphenyl‐1h‐pyrazol‐4‐yl)‐2‐methylbutan‐2‐	4‐(5‐chloro‐1,3‐diphenyl‐1h‐pyrazol‐4‐yl)‐2‐methylbutan‐2‐	NUM
eurjchem-976	238	2	ol	ol	ADJ
eurjchem-976	238	3	(	(	PUNCT
eurjchem-976	238	4	16a	16a	NOUN
eurjchem-976	238	5	):	):	PUNCT
eurjchem-976	238	6	color	color	NOUN
eurjchem-976	238	7	:	:	PUNCT
eurjchem-976	238	8	white	white	ADJ
eurjchem-976	238	9	needles	needle	NOUN
eurjchem-976	238	10	.	.	PUNCT
eurjchem-976	239	1	yield	yield	NOUN
eurjchem-976	239	2	:	:	PUNCT
eurjchem-976	239	3	85	85	NUM
eurjchem-976	239	4	%	%	NOUN
eurjchem-976	239	5	.	.	PUNCT
eurjchem-976	240	1	m.p	m.p	PROPN
eurjchem-976	240	2	.	.	PROPN
eurjchem-976	240	3	:	:	PUNCT
eurjchem-976	241	1	118	118	NUM
eurjchem-976	241	2	°	°	NUM
eurjchem-976	241	3	c	c	NOUN
eurjchem-976	241	4	(	(	PUNCT
eurjchem-976	241	5	benzene	benzene	NOUN
eurjchem-976	241	6	)	)	PUNCT
eurjchem-976	241	7	.	.	PUNCT
eurjchem-976	242	1	ir	ir	PROPN
eurjchem-976	242	2	(	(	PUNCT
eurjchem-976	242	3	kbr	kbr	PROPN
eurjchem-976	242	4	,	,	PUNCT
eurjchem-976	242	5	ν	ν	PROPN
eurjchem-976	242	6	,	,	PUNCT
eurjchem-976	242	7	cm‐1	cm‐1	PROPN
eurjchem-976	242	8	):	):	PUNCT
eurjchem-976	242	9	3490	3490	NUM
eurjchem-976	242	10	(	(	PUNCT
eurjchem-976	242	11	oh	oh	INTJ
eurjchem-976	242	12	)	)	PUNCT
eurjchem-976	242	13	(	(	PUNCT
eurjchem-976	242	14	alcohol	alcohol	NOUN
eurjchem-976	242	15	)	)	PUNCT
eurjchem-976	242	16	,	,	PUNCT
eurjchem-976	242	17	3075	3075	NUM
eurjchem-976	242	18	(	(	PUNCT
eurjchem-976	242	19	ch	ch	NOUN
eurjchem-976	242	20	)	)	PUNCT
eurjchem-976	242	21	(	(	PUNCT
eurjchem-976	242	22	aromatic	aromatic	NOUN
eurjchem-976	242	23	)	)	PUNCT
eurjchem-976	242	24	,	,	PUNCT
eurjchem-976	242	25	2990	2990	NUM
eurjchem-976	242	26	(	(	PUNCT
eurjchem-976	242	27	ch	ch	NOUN
eurjchem-976	242	28	)	)	PUNCT
eurjchem-976	242	29	(	(	PUNCT
eurjchem-976	242	30	alkyl	alkyl	NOUN
eurjchem-976	242	31	)	)	PUNCT
eurjchem-976	242	32	,	,	PUNCT
eurjchem-976	242	33	1610	1610	NUM
eurjchem-976	242	34	,	,	PUNCT
eurjchem-976	242	35	1490	1490	NUM
eurjchem-976	242	36	,	,	PUNCT
eurjchem-976	242	37	1455	1455	NUM
eurjchem-976	242	38	,	,	PUNCT
eurjchem-976	242	39	1430	1430	NUM
eurjchem-976	242	40	(	(	PUNCT
eurjchem-976	242	41	c	c	X
eurjchem-976	242	42	=	=	SYM
eurjchem-976	242	43	c	c	NOUN
eurjchem-976	242	44	)	)	PUNCT
eurjchem-976	242	45	(	(	PUNCT
eurjchem-976	242	46	aromatic	aromatic	NOUN
eurjchem-976	242	47	)	)	PUNCT
eurjchem-976	242	48	,	,	PUNCT
eurjchem-976	242	49	1386	1386	NUM
eurjchem-976	242	50	,	,	PUNCT
eurjchem-976	242	51	1355	1355	NUM
eurjchem-976	242	52	,	,	PUNCT
eurjchem-976	242	53	1020	1020	NUM
eurjchem-976	242	54	,	,	PUNCT
eurjchem-976	242	55	745	745	NUM
eurjchem-976	242	56	.	.	PUNCT
eurjchem-976	243	1	1h	1h	NUM
eurjchem-976	243	2	nmr	nmr	NOUN
eurjchem-976	243	3	(	(	PUNCT
eurjchem-976	243	4	400	400	NUM
eurjchem-976	243	5	mhz	mhz	NOUN
eurjchem-976	243	6	,	,	PUNCT
eurjchem-976	243	7	cdcl3	cdcl3	PROPN
eurjchem-976	243	8	,	,	PUNCT
eurjchem-976	243	9	δ	δ	PROPN
eurjchem-976	243	10	,	,	PUNCT
eurjchem-976	243	11	ppm	ppm	NUM
eurjchem-976	243	12	):	):	PUNCT
eurjchem-976	243	13	1.10	1.10	NUM
eurjchem-976	243	14	(	(	PUNCT
eurjchem-976	243	15	s	s	PROPN
eurjchem-976	243	16	,	,	PUNCT
eurjchem-976	243	17	6h	6h	NUM
eurjchem-976	243	18	,	,	PUNCT
eurjchem-976	243	19	2ch3	2ch3	NUM
eurjchem-976	243	20	)	)	PUNCT
eurjchem-976	243	21	,	,	PUNCT
eurjchem-976	243	22	1.55	1.55	NUM
eurjchem-976	243	23	(	(	PUNCT
eurjchem-976	243	24	t	t	PROPN
eurjchem-976	243	25	,	,	PUNCT
eurjchem-976	243	26	2h	2h	NUM
eurjchem-976	243	27	,	,	PUNCT
eurjchem-976	243	28	j	j	PROPN
eurjchem-976	243	29	=	=	SYM
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eurjchem-976	243	32	,	,	PUNCT
eurjchem-976	243	33	ch2	ch2	PROPN
eurjchem-976	243	34	)	)	PUNCT
eurjchem-976	243	35	,	,	PUNCT
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eurjchem-976	243	37	(	(	PUNCT
eurjchem-976	243	38	s	s	PROPN
eurjchem-976	243	39	,	,	PUNCT
eurjchem-976	243	40	1h	1h	NUM
eurjchem-976	243	41	,	,	PUNCT
eurjchem-976	243	42	oh	oh	INTJ
eurjchem-976	243	43	exchangeable	exchangeable	ADJ
eurjchem-976	243	44	with	with	ADP
eurjchem-976	243	45	d2o	d2o	NOUN
eurjchem-976	243	46	)	)	PUNCT
eurjchem-976	243	47	,	,	PUNCT
eurjchem-976	243	48	2.40	2.40	NUM
eurjchem-976	243	49	(	(	PUNCT
eurjchem-976	243	50	t	t	PROPN
eurjchem-976	243	51	,	,	PUNCT
eurjchem-976	243	52	2h	2h	NUM
eurjchem-976	243	53	,	,	PUNCT
eurjchem-976	243	54	j	j	PROPN
eurjchem-976	244	1	=	=	SYM
eurjchem-976	244	2	6.2	6.2	NUM
eurjchem-976	244	3	hz	hz	NOUN
eurjchem-976	244	4	,	,	PUNCT
eurjchem-976	244	5	ch2	ch2	PROPN
eurjchem-976	244	6	)	)	PUNCT
eurjchem-976	244	7	,	,	PUNCT
eurjchem-976	244	8	7.22‐8.30	7.22‐8.30	NUM
eurjchem-976	244	9	(	(	PUNCT
eurjchem-976	244	10	m	m	PROPN
eurjchem-976	244	11	,	,	PUNCT
eurjchem-976	244	12	10	10	NUM
eurjchem-976	244	13	h	h	NOUN
eurjchem-976	244	14	,	,	PUNCT
eurjchem-976	244	15	ar‐h	ar‐h	NOUN
eurjchem-976	244	16	)	)	PUNCT
eurjchem-976	244	17	.	.	PUNCT
eurjchem-976	245	1	ms	ms	NOUN
eurjchem-976	245	2	(	(	PUNCT
eurjchem-976	245	3	ei	ei	PROPN
eurjchem-976	245	4	,	,	PUNCT
eurjchem-976	245	5	m	m	PROPN
eurjchem-976	245	6	/	/	SYM
eurjchem-976	245	7	z	z	PROPN
eurjchem-976	245	8	(	(	PUNCT
eurjchem-976	245	9	%	%	NOUN
eurjchem-976	245	10	)	)	PUNCT
eurjchem-976	245	11	):	):	PUNCT
eurjchem-976	245	12	342	342	NUM
eurjchem-976	245	13	(	(	PUNCT
eurjchem-976	245	14	m++2	m++2	PROPN
eurjchem-976	245	15	,	,	PUNCT
eurjchem-976	245	16	9	9	NUM
eurjchem-976	245	17	)	)	PUNCT
eurjchem-976	245	18	,	,	PUNCT
eurjchem-976	245	19	340	340	NUM
eurjchem-976	245	20	(	(	PUNCT
eurjchem-976	245	21	m+	m+	NUM
eurjchem-976	245	22	,	,	PUNCT
eurjchem-976	245	23	22	22	NUM
eurjchem-976	245	24	)	)	PUNCT
eurjchem-976	245	25	,	,	PUNCT
eurjchem-976	245	26	338	338	NUM
eurjchem-976	245	27	(	(	PUNCT
eurjchem-976	245	28	48	48	NUM
eurjchem-976	245	29	)	)	PUNCT
eurjchem-976	245	30	,	,	PUNCT
eurjchem-976	245	31	322	322	NUM
eurjchem-976	245	32	(	(	PUNCT
eurjchem-976	245	33	100	100	NUM
eurjchem-976	245	34	)	)	PUNCT
eurjchem-976	245	35	,	,	PUNCT
eurjchem-976	245	36	281	281	NUM
eurjchem-976	245	37	(	(	PUNCT
eurjchem-976	245	38	51	51	NUM
eurjchem-976	245	39	)	)	PUNCT
eurjchem-976	245	40	,	,	PUNCT
eurjchem-976	245	41	267	267	NUM
eurjchem-976	245	42	(	(	PUNCT
eurjchem-976	245	43	42	42	NUM
eurjchem-976	245	44	)	)	PUNCT
eurjchem-976	245	45	,	,	PUNCT
eurjchem-976	245	46	263	263	NUM
eurjchem-976	245	47	(	(	PUNCT
eurjchem-976	245	48	12	12	NUM
eurjchem-976	245	49	)	)	PUNCT
eurjchem-976	245	50	,	,	PUNCT
eurjchem-976	245	51	253	253	NUM
eurjchem-976	245	52	(	(	PUNCT
eurjchem-976	245	53	70	70	NUM
eurjchem-976	245	54	)	)	PUNCT
eurjchem-976	245	55	,	,	PUNCT
eurjchem-976	245	56	245	245	NUM
eurjchem-976	245	57	(	(	PUNCT
eurjchem-976	245	58	38	38	NUM
eurjchem-976	245	59	)	)	PUNCT
eurjchem-976	245	60	,	,	PUNCT
eurjchem-976	245	61	235	235	NUM
eurjchem-976	245	62	(	(	PUNCT
eurjchem-976	245	63	18	18	NUM
eurjchem-976	245	64	)	)	PUNCT
eurjchem-976	245	65	,	,	PUNCT
eurjchem-976	245	66	194	194	NUM
eurjchem-976	245	67	(	(	PUNCT
eurjchem-976	245	68	42	42	NUM
eurjchem-976	245	69	)	)	PUNCT
eurjchem-976	245	70	,	,	PUNCT
eurjchem-976	245	71	180	180	NUM
eurjchem-976	245	72	(	(	PUNCT
eurjchem-976	245	73	11	11	NUM
eurjchem-976	245	74	)	)	PUNCT
eurjchem-976	245	75	,	,	PUNCT
eurjchem-976	245	76	176	176	NUM
eurjchem-976	245	77	(	(	PUNCT
eurjchem-976	245	78	19	19	NUM
eurjchem-976	245	79	)	)	PUNCT
eurjchem-976	245	80	,	,	PUNCT
eurjchem-976	245	81	167	167	NUM
eurjchem-976	245	82	(	(	PUNCT
eurjchem-976	245	83	30	30	NUM
eurjchem-976	245	84	)	)	PUNCT
eurjchem-976	245	85	,	,	PUNCT
eurjchem-976	245	86	159	159	NUM
eurjchem-976	245	87	(	(	PUNCT
eurjchem-976	245	88	43	43	NUM
eurjchem-976	245	89	)	)	PUNCT
eurjchem-976	245	90	,	,	PUNCT
eurjchem-976	245	91	103	103	NUM
eurjchem-976	245	92	(	(	PUNCT
eurjchem-976	245	93	13	13	NUM
eurjchem-976	245	94	)	)	PUNCT
eurjchem-976	245	95	,	,	PUNCT
eurjchem-976	245	96	91	91	NUM
eurjchem-976	245	97	(	(	PUNCT
eurjchem-976	245	98	38	38	NUM
eurjchem-976	245	99	)	)	PUNCT
eurjchem-976	245	100	,	,	PUNCT
eurjchem-976	245	101	77	77	NUM
eurjchem-976	245	102	(	(	PUNCT
eurjchem-976	245	103	39	39	NUM
eurjchem-976	245	104	)	)	PUNCT
eurjchem-976	245	105	.	.	PUNCT
eurjchem-976	246	1	anal	anal	PROPN
eurjchem-976	246	2	.	.	PUNCT
eurjchem-976	246	3	calcd	calcd	NOUN
eurjchem-976	246	4	.	.	PUNCT
eurjchem-976	247	1	for	for	ADP
eurjchem-976	247	2	c20h21cln2o	c20h21cln2o	NOUN
eurjchem-976	247	3	:	:	PUNCT
eurjchem-976	247	4	c	c	X
eurjchem-976	247	5	,	,	PUNCT
eurjchem-976	247	6	70.48	70.48	NUM
eurjchem-976	247	7	;	;	PUNCT
eurjchem-976	247	8	h	h	NOUN
eurjchem-976	247	9	,	,	PUNCT
eurjchem-976	247	10	6.21	6.21	NUM
eurjchem-976	247	11	;	;	PUNCT
eurjchem-976	247	12	n	n	CCONJ
eurjchem-976	247	13	,	,	PUNCT
eurjchem-976	247	14	8.22	8.22	NUM
eurjchem-976	247	15	.	.	PUNCT
eurjchem-976	247	16	found	find	VERB
eurjchem-976	247	17	;	;	PUNCT
eurjchem-976	247	18	c	c	X
eurjchem-976	247	19	,	,	PUNCT
eurjchem-976	247	20	70.49	70.49	NUM
eurjchem-976	247	21	;	;	PUNCT
eurjchem-976	248	1	h	h	NOUN
eurjchem-976	248	2	,	,	PUNCT
eurjchem-976	248	3	6.26	6.26	NUM
eurjchem-976	248	4	;	;	PUNCT
eurjchem-976	248	5	n	n	CCONJ
eurjchem-976	248	6	,	,	PUNCT
eurjchem-976	248	7	8.05	8.05	NUM
eurjchem-976	248	8	%	%	NOUN
eurjchem-976	248	9	.	.	PUNCT
eurjchem-976	249	1	4‐(5‐chloro‐1,3‐diphenyl‐1h‐pyrazol‐4‐yl)‐2,3‐dimethyl	4‐(5‐chloro‐1,3‐diphenyl‐1h‐pyrazol‐4‐yl)‐2,3‐dimethyl	PROPN
eurjchem-976	249	2	butan‐2‐ol	butan‐2‐ol	PRON
eurjchem-976	249	3	(	(	PUNCT
eurjchem-976	249	4	16b	16b	NUM
eurjchem-976	249	5	):	):	PUNCT
eurjchem-976	249	6	color	color	NOUN
eurjchem-976	249	7	:	:	PUNCT
eurjchem-976	249	8	reddish	reddish	ADJ
eurjchem-976	249	9	viscous	viscous	ADJ
eurjchem-976	249	10	oil	oil	NOUN
eurjchem-976	249	11	.	.	PUNCT
eurjchem-976	250	1	yield	yield	NOUN
eurjchem-976	250	2	:	:	PUNCT
eurjchem-976	250	3	81	81	NUM
eurjchem-976	250	4	%	%	NOUN
eurjchem-976	250	5	.	.	PUNCT
eurjchem-976	251	1	nd25	nd25	PROPN
eurjchem-976	251	2	=	=	PUNCT
eurjchem-976	251	3	1.619	1.619	NUM
eurjchem-976	251	4	.	.	PUNCT
eurjchem-976	252	1	ir	ir	PROPN
eurjchem-976	252	2	(	(	PUNCT
eurjchem-976	252	3	film	film	NOUN
eurjchem-976	252	4	,	,	PUNCT
eurjchem-976	252	5	ν	ν	NOUN
eurjchem-976	252	6	,	,	PUNCT
eurjchem-976	252	7	cm‐1	cm‐1	PROPN
eurjchem-976	252	8	):	):	PUNCT
eurjchem-976	252	9	3465	3465	NUM
eurjchem-976	252	10	(	(	PUNCT
eurjchem-976	252	11	oh	oh	INTJ
eurjchem-976	252	12	)	)	PUNCT
eurjchem-976	252	13	(	(	PUNCT
eurjchem-976	252	14	alcohol	alcohol	NOUN
eurjchem-976	252	15	)	)	PUNCT
eurjchem-976	252	16	,	,	PUNCT
eurjchem-976	252	17	3055	3055	NUM
eurjchem-976	252	18	(	(	PUNCT
eurjchem-976	252	19	ch	ch	NOUN
eurjchem-976	252	20	)	)	PUNCT
eurjchem-976	252	21	(	(	PUNCT
eurjchem-976	252	22	aromatic	aromatic	NOUN
eurjchem-976	252	23	)	)	PUNCT
eurjchem-976	252	24	,	,	PUNCT
eurjchem-976	252	25	2973	2973	NUM
eurjchem-976	252	26	(	(	PUNCT
eurjchem-976	252	27	ch	ch	NOUN
eurjchem-976	252	28	)	)	PUNCT
eurjchem-976	252	29	(	(	PUNCT
eurjchem-976	252	30	alkyl	alkyl	NOUN
eurjchem-976	252	31	)	)	PUNCT
eurjchem-976	252	32	,	,	PUNCT
eurjchem-976	252	33	1590	1590	NUM
eurjchem-976	252	34	,	,	PUNCT
eurjchem-976	252	35	1480	1480	NUM
eurjchem-976	252	36	,	,	PUNCT
eurjchem-976	252	37	1455	1455	NUM
eurjchem-976	252	38	,	,	PUNCT
eurjchem-976	252	39	1440	1440	NUM
eurjchem-976	252	40	(	(	PUNCT
eurjchem-976	252	41	c	c	NOUN
eurjchem-976	252	42	=	=	SYM
eurjchem-976	252	43	c	c	NOUN
eurjchem-976	252	44	)	)	PUNCT
eurjchem-976	252	45	(	(	PUNCT
eurjchem-976	252	46	aromatic	aromatic	NOUN
eurjchem-976	252	47	)	)	PUNCT
eurjchem-976	252	48	,	,	PUNCT
eurjchem-976	252	49	1345	1345	NUM
eurjchem-976	252	50	,	,	PUNCT
eurjchem-976	252	51	745	745	NUM
eurjchem-976	252	52	.	.	NOUN
eurjchem-976	252	53	282	282	NUM
eurjchem-976	252	54	el‐aal	el‐aal	PROPN
eurjchem-976	252	55	et	et	NOUN
eurjchem-976	252	56	al	al	PROPN
eurjchem-976	252	57	.	.	PUNCT
eurjchem-976	252	58	/	/	SYM
eurjchem-976	252	59	european	european	PROPN
eurjchem-976	252	60	journal	journal	PROPN
eurjchem-976	252	61	of	of	ADP
eurjchem-976	252	62	chemistry	chemistry	NOUN
eurjchem-976	252	63	5	5	NUM
eurjchem-976	252	64	(	(	PUNCT
eurjchem-976	252	65	2	2	NUM
eurjchem-976	252	66	)	)	PUNCT
eurjchem-976	252	67	(	(	PUNCT
eurjchem-976	252	68	2014	2014	NUM
eurjchem-976	252	69	)	)	PUNCT
eurjchem-976	252	70	277‐286	277‐286	NUM
eurjchem-976	252	71	table	table	NOUN
eurjchem-976	252	72	2	2	NUM
eurjchem-976	252	73	.	.	PUNCT
eurjchem-976	252	74	friedel‐crafts	friedel‐craft	NOUN
eurjchem-976	252	75	ring	ring	NOUN
eurjchem-976	252	76	closures	closure	NOUN
eurjchem-976	252	77	of	of	ADP
eurjchem-976	252	78	heterocyclic	heterocyclic	ADJ
eurjchem-976	252	79	alkanols	alkanol	NOUN
eurjchem-976	252	80	8	8	NUM
eurjchem-976	252	81	,	,	PUNCT
eurjchem-976	252	82	12a	12a	NUM
eurjchem-976	252	83	,	,	PUNCT
eurjchem-976	252	84	b	b	NOUN
eurjchem-976	252	85	and	and	CCONJ
eurjchem-976	252	86	16a	16a	NOUN
eurjchem-976	252	87	,	,	PUNCT
eurjchem-976	252	88	b.	b.	NOUN
eurjchem-976	252	89	entry	entry	NOUN
eurjchem-976	252	90	substrate	substrate	NOUN
eurjchem-976	252	91	product	product	NOUN
eurjchem-976	252	92	conditions	condition	NOUN
eurjchem-976	252	93	yield	yield	NOUN
eurjchem-976	252	94	(	(	PUNCT
eurjchem-976	252	95	%	%	NOUN
eurjchem-976	252	96	)	)	PUNCT
eurjchem-976	252	97	a	a	DET
eurjchem-976	252	98	1	1	NUM
eurjchem-976	252	99	n	n	CCONJ
eurjchem-976	252	100	n	n	PRON
eurjchem-976	252	101	ph	ph	ADJ
eurjchem-976	252	102	ph	ph	NOUN
eurjchem-976	252	103	ho	ho	ADJ
eurjchem-976	252	104	8	8	NUM
eurjchem-976	252	105	cl	cl	NOUN
eurjchem-976	252	106	alcl3	alcl3	PROPN
eurjchem-976	252	107	/	/	SYM
eurjchem-976	252	108	ch3no2b	ch3no2b	PROPN
eurjchem-976	252	109	,	,	PUNCT
eurjchem-976	252	110	dcmc,20	dcmc,20	NOUN
eurjchem-976	252	111	h	h	PROPN
eurjchem-976	252	112	,	,	PUNCT
eurjchem-976	252	113	rt	rt	PROPN
eurjchem-976	252	114	86	86	NUM
eurjchem-976	252	115	p2o5d	p2o5d	NUM
eurjchem-976	252	116	,	,	PUNCT
eurjchem-976	252	117	toluene	toluene	NOUN
eurjchem-976	252	118	,	,	PUNCT
eurjchem-976	252	119	8	8	NUM
eurjchem-976	252	120	h	h	NOUN
eurjchem-976	252	121	,	,	PUNCT
eurjchem-976	252	122	reflux	reflux	VERB
eurjchem-976	252	123	75	75	NUM
eurjchem-976	252	124	ppae	ppae	NOUN
eurjchem-976	252	125	,	,	PUNCT
eurjchem-976	252	126	4	4	NUM
eurjchem-976	252	127	h	h	NOUN
eurjchem-976	252	128	,	,	PUNCT
eurjchem-976	252	129	200‐210	200‐210	PROPN
eurjchem-976	252	130	°	°	PROPN
eurjchem-976	252	131	c	c	NOUN
eurjchem-976	252	132	72	72	NUM
eurjchem-976	252	133	2	2	NUM
eurjchem-976	252	134	n	n	CCONJ
eurjchem-976	252	135	n	n	PRON
eurjchem-976	252	136	ph	ph	ADJ
eurjchem-976	252	137	ph	ph	NOUN
eurjchem-976	252	138	o	o	NOUN
eurjchem-976	252	139	oh	oh	NUM
eurjchem-976	252	140	12a	12a	NOUN
eurjchem-976	252	141	alcl3	alcl3	SYM
eurjchem-976	252	142	/	/	SYM
eurjchem-976	252	143	ch3no2	ch3no2	PROPN
eurjchem-976	252	144	,	,	PUNCT
eurjchem-976	252	145	dcm	dcm	PROPN
eurjchem-976	252	146	,	,	PUNCT
eurjchem-976	252	147	4	4	NUM
eurjchem-976	252	148	h	h	NOUN
eurjchem-976	252	149	,	,	PUNCT
eurjchem-976	252	150	rt	rt	PROPN
eurjchem-976	252	151	92	92	NUM
eurjchem-976	252	152	p2o5	p2o5	PROPN
eurjchem-976	252	153	,	,	PUNCT
eurjchem-976	252	154	phh	phh	PROPN
eurjchem-976	252	155	,	,	PUNCT
eurjchem-976	252	156	5	5	NUM
eurjchem-976	252	157	h	h	NOUN
eurjchem-976	252	158	,	,	PUNCT
eurjchem-976	252	159	reflux	reflux	VERB
eurjchem-976	252	160	83	83	NUM
eurjchem-976	252	161	ppa	ppa	PROPN
eurjchem-976	252	162	,	,	PUNCT
eurjchem-976	252	163	2	2	NUM
eurjchem-976	252	164	h	h	NOUN
eurjchem-976	252	165	,	,	PUNCT
eurjchem-976	252	166	180‐190	180‐190	PROPN
eurjchem-976	252	167	°	°	PROPN
eurjchem-976	252	168	c	c	NOUN
eurjchem-976	252	169	75	75	NUM
eurjchem-976	252	170	3	3	NUM
eurjchem-976	252	171	n	n	NUM
eurjchem-976	252	172	n	n	PRON
eurjchem-976	252	173	ph	ph	X
eurjchem-976	252	174	o	o	NOUN
eurjchem-976	252	175	2b	2b	NUM
eurjchem-976	252	176	alcl3	alcl3	NOUN
eurjchem-976	252	177	/	/	SYM
eurjchem-976	252	178	ch3no2	ch3no2	PROPN
eurjchem-976	252	179	,	,	PUNCT
eurjchem-976	252	180	dcm	dcm	PROPN
eurjchem-976	252	181	,	,	PUNCT
eurjchem-976	252	182	4	4	NUM
eurjchem-976	252	183	h	h	NOUN
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eurjchem-976	252	185	rt	rt	PROPN
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eurjchem-976	252	188	,	,	PUNCT
eurjchem-976	252	189	phh	phh	PROPN
eurjchem-976	252	190	,	,	PUNCT
eurjchem-976	252	191	3	3	NUM
eurjchem-976	252	192	h	h	NOUN
eurjchem-976	252	193	,	,	PUNCT
eurjchem-976	252	194	reflux	reflux	VERB
eurjchem-976	252	195	80	80	NUM
eurjchem-976	252	196	ppa	ppa	PROPN
eurjchem-976	252	197	,	,	PUNCT
eurjchem-976	252	198	2	2	NUM
eurjchem-976	252	199	h	h	NOUN
eurjchem-976	252	200	,	,	PUNCT
eurjchem-976	252	201	200‐210	200‐210	PROPN
eurjchem-976	252	202	°	°	PROPN
eurjchem-976	252	203	c	c	NOUN
eurjchem-976	252	204	76	76	NUM
eurjchem-976	252	205	4	4	NUM
eurjchem-976	252	206	n	n	NUM
eurjchem-976	252	207	n	n	PRON
eurjchem-976	252	208	ph	ph	ADJ
eurjchem-976	252	209	cl	cl	NOUN
eurjchem-976	252	210	3a	3a	NUM
eurjchem-976	252	211	alcl3	alcl3	SYM
eurjchem-976	252	212	/	/	SYM
eurjchem-976	252	213	ch3no2	ch3no2	PROPN
eurjchem-976	252	214	,	,	PUNCT
eurjchem-976	252	215	dcm	dcm	PROPN
eurjchem-976	252	216	,	,	PUNCT
eurjchem-976	252	217	1	1	NUM
eurjchem-976	252	218	h	h	NOUN
eurjchem-976	252	219	,	,	PUNCT
eurjchem-976	252	220	rt	rt	PROPN
eurjchem-976	252	221	83	83	NUM
eurjchem-976	252	222	p2o5	p2o5	PROPN
eurjchem-976	252	223	,	,	PUNCT
eurjchem-976	252	224	phh	phh	PROPN
eurjchem-976	252	225	,	,	PUNCT
eurjchem-976	252	226	5	5	NUM
eurjchem-976	252	227	h	h	NOUN
eurjchem-976	252	228	,	,	PUNCT
eurjchem-976	252	229	reflux	reflux	VERB
eurjchem-976	252	230	79	79	NUM
eurjchem-976	252	231	ppa	ppa	PROPN
eurjchem-976	252	232	,	,	PUNCT
eurjchem-976	252	233	1h	1h	NUM
eurjchem-976	252	234	,	,	PUNCT
eurjchem-976	252	235	180‐190	180‐190	PROPN
eurjchem-976	252	236	°	°	PROPN
eurjchem-976	252	237	c	c	NOUN
eurjchem-976	252	238	74	74	NUM
eurjchem-976	252	239	5	5	NUM
eurjchem-976	252	240	16b	16b	PROPN
eurjchem-976	252	241	n	n	ADP
eurjchem-976	252	242	n	n	CCONJ
eurjchem-976	252	243	ph	ph	ADJ
eurjchem-976	252	244	ph	ph	NOUN
eurjchem-976	252	245	cl	cl	NOUN
eurjchem-976	253	1	oh	oh	INTJ
eurjchem-976	253	2	n	n	CCONJ
eurjchem-976	253	3	n	n	ADV
eurjchem-976	253	4	ph	ph	ADJ
eurjchem-976	253	5	cl	cl	NOUN
eurjchem-976	253	6	3b	3b	NUM
eurjchem-976	253	7	alcl3	alcl3	SYM
eurjchem-976	253	8	/	/	SYM
eurjchem-976	253	9	ch3no2	ch3no2	PROPN
eurjchem-976	253	10	,	,	PUNCT
eurjchem-976	253	11	dcm	dcm	PROPN
eurjchem-976	253	12	,	,	PUNCT
eurjchem-976	253	13	1	1	NUM
eurjchem-976	253	14	h	h	NOUN
eurjchem-976	253	15	,	,	PUNCT
eurjchem-976	253	16	rt	rt	PROPN
eurjchem-976	253	17	86	86	NUM
eurjchem-976	253	18	p2o5	p2o5	PROPN
eurjchem-976	253	19	,	,	PUNCT
eurjchem-976	253	20	phh	phh	PROPN
eurjchem-976	253	21	,	,	PUNCT
eurjchem-976	253	22	4	4	NUM
eurjchem-976	253	23	h	h	NOUN
eurjchem-976	253	24	,	,	PUNCT
eurjchem-976	253	25	reflux	reflux	VERB
eurjchem-976	253	26	80	80	NUM
eurjchem-976	253	27	ppa	ppa	PROPN
eurjchem-976	253	28	,	,	PUNCT
eurjchem-976	253	29	1	1	NUM
eurjchem-976	253	30	h	h	NOUN
eurjchem-976	253	31	,	,	PUNCT
eurjchem-976	253	32	200‐210	200‐210	PROPN
eurjchem-976	253	33	°	°	PROPN
eurjchem-976	253	34	c	c	PROPN
eurjchem-976	253	35	77	77	NUM
eurjchem-976	253	36	a	a	DET
eurjchem-976	253	37	isolated	isolated	ADJ
eurjchem-976	253	38	yield	yield	NOUN
eurjchem-976	253	39	refer	refer	NOUN
eurjchem-976	253	40	to	to	ADP
eurjchem-976	253	41	substrate	substrate	NOUN
eurjchem-976	253	42	.	.	PUNCT
eurjchem-976	254	1	b	b	NOUN
eurjchem-976	254	2	with	with	ADP
eurjchem-976	254	3	alcl3	alcl3	NOUN
eurjchem-976	254	4	/	/	SYM
eurjchem-976	254	5	ch3no2	ch3no2	NOUN
eurjchem-976	254	6	catalyst	catalyst	NOUN
eurjchem-976	254	7	reactant	reactant	NOUN
eurjchem-976	254	8	proportions	proportion	NOUN
eurjchem-976	254	9	were	be	AUX
eurjchem-976	254	10	:	:	PUNCT
eurjchem-976	254	11	carbinol	carbinol	ADJ
eurjchem-976	254	12	or	or	CCONJ
eurjchem-976	254	13	acid	acid	NOUN
eurjchem-976	254	14	(	(	PUNCT
eurjchem-976	254	15	0.002	0.002	NUM
eurjchem-976	254	16	moe	moe	NOUN
eurjchem-976	254	17	)	)	PUNCT
eurjchem-976	254	18	,	,	PUNCT
eurjchem-976	254	19	alcl3	alcl3	X
eurjchem-976	255	1	(	(	PUNCT
eurjchem-976	255	2	0.0024	0.0024	NUM
eurjchem-976	255	3	mol	mol	NUM
eurjchem-976	255	4	)	)	PUNCT
eurjchem-976	255	5	,	,	PUNCT
eurjchem-976	256	1	ch3no2	ch3no2	NOUN
eurjchem-976	256	2	(	(	PUNCT
eurjchem-976	256	3	0.024	0.024	NUM
eurjchem-976	256	4	mol	mol	NOUN
eurjchem-976	256	5	)	)	PUNCT
eurjchem-976	256	6	,	,	PUNCT
eurjchem-976	256	7	solvent	solvent	NOUN
eurjchem-976	256	8	(	(	PUNCT
eurjchem-976	256	9	10	10	NUM
eurjchem-976	256	10	ml	ml	NOUN
eurjchem-976	256	11	)	)	PUNCT
eurjchem-976	256	12	.	.	PUNCT
eurjchem-976	257	1	c	c	NOUN
eurjchem-976	257	2	dichloromethane	dichloromethane	NOUN
eurjchem-976	257	3	.	.	PUNCT
eurjchem-976	258	1	d	d	NOUN
eurjchem-976	258	2	with	with	SCONJ
eurjchem-976	258	3	p2o5	p2o5	ADP
eurjchem-976	258	4	catalyst	catalyst	NOUN
eurjchem-976	258	5	reactant	reactant	NOUN
eurjchem-976	258	6	proportions	proportion	NOUN
eurjchem-976	258	7	were	be	AUX
eurjchem-976	258	8	:	:	PUNCT
eurjchem-976	258	9	carbinol	carbinol	ADJ
eurjchem-976	258	10	or	or	CCONJ
eurjchem-976	258	11	acid	acid	NOUN
eurjchem-976	258	12	(	(	PUNCT
eurjchem-976	258	13	0.4	0.4	NUM
eurjchem-976	258	14	g	g	NOUN
eurjchem-976	258	15	)	)	PUNCT
eurjchem-976	258	16	and	and	CCONJ
eurjchem-976	258	17	p2o5	p2o5	X
eurjchem-976	258	18	(	(	PUNCT
eurjchem-976	258	19	4	4	NUM
eurjchem-976	258	20	g	g	NOUN
eurjchem-976	258	21	)	)	PUNCT
eurjchem-976	258	22	in	in	ADP
eurjchem-976	258	23	anhydrous	anhydrous	ADJ
eurjchem-976	258	24	toluene	toluene	NOUN
eurjchem-976	258	25	or	or	CCONJ
eurjchem-976	258	26	benzene	benzene	NOUN
eurjchem-976	258	27	(	(	PUNCT
eurjchem-976	258	28	15	15	NUM
eurjchem-976	258	29	ml	ml	NOUN
eurjchem-976	258	30	)	)	PUNCT
eurjchem-976	258	31	.	.	PUNCT
eurjchem-976	259	1	e	e	X
eurjchem-976	259	2	with	with	ADP
eurjchem-976	259	3	ppa	ppa	PROPN
eurjchem-976	259	4	catalyst	catalyst	NOUN
eurjchem-976	259	5	reactant	reactant	NOUN
eurjchem-976	259	6	proportions	proportion	NOUN
eurjchem-976	259	7	were	be	AUX
eurjchem-976	259	8	:	:	PUNCT
eurjchem-976	259	9	carbinol	carbinol	ADJ
eurjchem-976	259	10	or	or	CCONJ
eurjchem-976	259	11	acid	acid	NOUN
eurjchem-976	259	12	(	(	PUNCT
eurjchem-976	259	13	0.5	0.5	NUM
eurjchem-976	259	14	g	g	NOUN
eurjchem-976	259	15	)	)	PUNCT
eurjchem-976	259	16	and	and	CCONJ
eurjchem-976	259	17	ppa	ppa	PROPN
eurjchem-976	259	18	(	(	PUNCT
eurjchem-976	259	19	5	5	NUM
eurjchem-976	259	20	g	g	NOUN
eurjchem-976	259	21	)	)	PUNCT
eurjchem-976	259	22	.	.	PUNCT
eurjchem-976	260	1	1h	1h	NUM
eurjchem-976	260	2	nmr	nmr	NOUN
eurjchem-976	260	3	(	(	PUNCT
eurjchem-976	260	4	400	400	NUM
eurjchem-976	260	5	mhz	mhz	NOUN
eurjchem-976	260	6	,	,	PUNCT
eurjchem-976	260	7	cdcl3	cdcl3	PROPN
eurjchem-976	260	8	,	,	PUNCT
eurjchem-976	260	9	δ	δ	PROPN
eurjchem-976	260	10	,	,	PUNCT
eurjchem-976	260	11	ppm	ppm	NOUN
eurjchem-976	260	12	):	):	PUNCT
eurjchem-976	260	13	0.95	0.95	NUM
eurjchem-976	260	14	(	(	PUNCT
eurjchem-976	260	15	d	d	PROPN
eurjchem-976	260	16	,	,	PUNCT
eurjchem-976	260	17	3h	3h	NUM
eurjchem-976	260	18	,	,	PUNCT
eurjchem-976	260	19	j	j	PROPN
eurjchem-976	260	20	=	=	PROPN
eurjchem-976	261	1	10.4	10.4	NUM
eurjchem-976	261	2	hz	hz	NOUN
eurjchem-976	261	3	,	,	PUNCT
eurjchem-976	261	4	ch3	ch3	PROPN
eurjchem-976	261	5	)	)	PUNCT
eurjchem-976	261	6	,	,	PUNCT
eurjchem-976	261	7	1.30	1.30	NUM
eurjchem-976	261	8	(	(	PUNCT
eurjchem-976	261	9	s	s	PROPN
eurjchem-976	261	10	,	,	PUNCT
eurjchem-976	261	11	6h	6h	NUM
eurjchem-976	261	12	,	,	PUNCT
eurjchem-976	261	13	2ch3	2ch3	NUM
eurjchem-976	261	14	)	)	PUNCT
eurjchem-976	261	15	,	,	PUNCT
eurjchem-976	261	16	2,21	2,21	NUM
eurjchem-976	261	17	(	(	PUNCT
eurjchem-976	261	18	dt	dt	PROPN
eurjchem-976	261	19	,	,	PUNCT
eurjchem-976	261	20	1h	1h	NUM
eurjchem-976	261	21	,	,	PUNCT
eurjchem-976	261	22	j	j	PROPN
eurjchem-976	261	23	=	=	SYM
eurjchem-976	261	24	9.3	9.3	NUM
eurjchem-976	261	25	hz	hz	VERB
eurjchem-976	261	26	,	,	PUNCT
eurjchem-976	261	27	‐ch	‐ch	NOUN
eurjchem-976	261	28	)	)	PUNCT
eurjchem-976	261	29	,	,	PUNCT
eurjchem-976	261	30	2.42	2.42	NUM
eurjchem-976	261	31	(	(	PUNCT
eurjchem-976	261	32	t	t	PROPN
eurjchem-976	261	33	,	,	PUNCT
eurjchem-976	261	34	ha	ha	INTJ
eurjchem-976	261	35	,	,	PUNCT
eurjchem-976	261	36	j	j	PROPN
eurjchem-976	261	37	=	=	PROPN
eurjchem-976	261	38	16.3	16.3	NUM
eurjchem-976	261	39	hz	hz	NOUN
eurjchem-976	261	40	,	,	PUNCT
eurjchem-976	261	41	ch2	ch2	PROPN
eurjchem-976	261	42	)	)	PUNCT
eurjchem-976	261	43	,	,	PUNCT
eurjchem-976	261	44	2.64	2.64	NUM
eurjchem-976	261	45	(	(	PUNCT
eurjchem-976	261	46	app.t	app.t	PROPN
eurjchem-976	261	47	,	,	PUNCT
eurjchem-976	261	48	hb	hb	PROPN
eurjchem-976	261	49	,	,	PUNCT
eurjchem-976	261	50	j	j	PROPN
eurjchem-976	261	51	=	=	PROPN
eurjchem-976	261	52	16.3	16.3	NUM
eurjchem-976	261	53	hz	hz	NOUN
eurjchem-976	261	54	,	,	PUNCT
eurjchem-976	261	55	ch2	ch2	PROPN
eurjchem-976	261	56	)	)	PUNCT
eurjchem-976	261	57	,	,	PUNCT
eurjchem-976	261	58	2.50	2.50	NUM
eurjchem-976	261	59	(	(	PUNCT
eurjchem-976	261	60	s	s	PROPN
eurjchem-976	261	61	,	,	PUNCT
eurjchem-976	261	62	1h	1h	NUM
eurjchem-976	261	63	,	,	PUNCT
eurjchem-976	261	64	oh	oh	INTJ
eurjchem-976	261	65	exchangeable	exchangeable	ADJ
eurjchem-976	261	66	with	with	ADP
eurjchem-976	261	67	d2o	d2o	NOUN
eurjchem-976	261	68	)	)	PUNCT
eurjchem-976	261	69	,	,	PUNCT
eurjchem-976	261	70	7.22‐8.15	7.22‐8.15	NUM
eurjchem-976	261	71	(	(	PUNCT
eurjchem-976	261	72	m	m	PROPN
eurjchem-976	261	73	,	,	PUNCT
eurjchem-976	261	74	10	10	NUM
eurjchem-976	261	75	h	h	NOUN
eurjchem-976	261	76	,	,	PUNCT
eurjchem-976	261	77	ar‐h	ar‐h	NOUN
eurjchem-976	261	78	)	)	PUNCT
eurjchem-976	261	79	.	.	PUNCT
eurjchem-976	262	1	ms	ms	NOUN
eurjchem-976	262	2	(	(	PUNCT
eurjchem-976	262	3	ei	ei	PROPN
eurjchem-976	262	4	,	,	PUNCT
eurjchem-976	262	5	m	m	PROPN
eurjchem-976	262	6	/	/	SYM
eurjchem-976	262	7	z	z	PROPN
eurjchem-976	262	8	(	(	PUNCT
eurjchem-976	262	9	%	%	NOUN
eurjchem-976	262	10	)	)	PUNCT
eurjchem-976	262	11	):	):	PUNCT
eurjchem-976	262	12	356	356	NUM
eurjchem-976	262	13	(	(	PUNCT
eurjchem-976	262	14	m++2	m++2	PROPN
eurjchem-976	262	15	,	,	PUNCT
eurjchem-976	262	16	5	5	NUM
eurjchem-976	262	17	)	)	PUNCT
eurjchem-976	262	18	,	,	PUNCT
eurjchem-976	262	19	354	354	NUM
eurjchem-976	262	20	(	(	PUNCT
eurjchem-976	262	21	m+	m+	NUM
eurjchem-976	262	22	,	,	PUNCT
eurjchem-976	262	23	13	13	NUM
eurjchem-976	262	24	)	)	PUNCT
eurjchem-976	262	25	,	,	PUNCT
eurjchem-976	262	26	336	336	NUM
eurjchem-976	262	27	(	(	PUNCT
eurjchem-976	262	28	100	100	NUM
eurjchem-976	262	29	)	)	PUNCT
eurjchem-976	262	30	,	,	PUNCT
eurjchem-976	262	31	295	295	NUM
eurjchem-976	262	32	(	(	PUNCT
eurjchem-976	262	33	74	74	NUM
eurjchem-976	262	34	)	)	PUNCT
eurjchem-976	262	35	,	,	PUNCT
eurjchem-976	262	36	280	280	NUM
eurjchem-976	262	37	(	(	PUNCT
eurjchem-976	262	38	48	48	NUM
eurjchem-976	262	39	)	)	PUNCT
eurjchem-976	262	40	,	,	PUNCT
eurjchem-976	262	41	267	267	NUM
eurjchem-976	262	42	(	(	PUNCT
eurjchem-976	262	43	35	35	NUM
eurjchem-976	262	44	)	)	PUNCT
eurjchem-976	262	45	,	,	PUNCT
eurjchem-976	262	46	252	252	NUM
eurjchem-976	262	47	(	(	PUNCT
eurjchem-976	262	48	84	84	NUM
eurjchem-976	262	49	)	)	PUNCT
eurjchem-976	262	50	,	,	PUNCT
eurjchem-976	262	51	245	245	NUM
eurjchem-976	262	52	(	(	PUNCT
eurjchem-976	262	53	24	24	NUM
eurjchem-976	262	54	)	)	PUNCT
eurjchem-976	262	55	,	,	PUNCT
eurjchem-976	262	56	235	235	NUM
eurjchem-976	262	57	(	(	PUNCT
eurjchem-976	262	58	13	13	NUM
eurjchem-976	262	59	)	)	PUNCT
eurjchem-976	262	60	,	,	PUNCT
eurjchem-976	262	61	194	194	NUM
eurjchem-976	262	62	(	(	PUNCT
eurjchem-976	262	63	48	48	NUM
eurjchem-976	262	64	)	)	PUNCT
eurjchem-976	262	65	,	,	PUNCT
eurjchem-976	262	66	180	180	NUM
eurjchem-976	262	67	(	(	PUNCT
eurjchem-976	262	68	14	14	NUM
eurjchem-976	262	69	)	)	PUNCT
eurjchem-976	262	70	,	,	PUNCT
eurjchem-976	262	71	176	176	NUM
eurjchem-976	262	72	(	(	PUNCT
eurjchem-976	262	73	26	26	NUM
eurjchem-976	262	74	)	)	PUNCT
eurjchem-976	262	75	,	,	PUNCT
eurjchem-976	262	76	167	167	NUM
eurjchem-976	262	77	(	(	PUNCT
eurjchem-976	262	78	35	35	NUM
eurjchem-976	262	79	)	)	PUNCT
eurjchem-976	262	80	,	,	PUNCT
eurjchem-976	262	81	159	159	NUM
eurjchem-976	262	82	(	(	PUNCT
eurjchem-976	262	83	52	52	NUM
eurjchem-976	262	84	)	)	PUNCT
eurjchem-976	262	85	,	,	PUNCT
eurjchem-976	262	86	103	103	NUM
eurjchem-976	262	87	(	(	PUNCT
eurjchem-976	262	88	15	15	NUM
eurjchem-976	262	89	)	)	PUNCT
eurjchem-976	262	90	,	,	PUNCT
eurjchem-976	262	91	91	91	NUM
eurjchem-976	262	92	(	(	PUNCT
eurjchem-976	262	93	48	48	NUM
eurjchem-976	262	94	)	)	PUNCT
eurjchem-976	262	95	,	,	PUNCT
eurjchem-976	262	96	77	77	NUM
eurjchem-976	262	97	(	(	PUNCT
eurjchem-976	262	98	42	42	NUM
eurjchem-976	262	99	)	)	PUNCT
eurjchem-976	262	100	.	.	PUNCT
eurjchem-976	263	1	anal	anal	PROPN
eurjchem-976	263	2	.	.	PUNCT
eurjchem-976	263	3	calcd	calcd	NOUN
eurjchem-976	263	4	.	.	PUNCT
eurjchem-976	264	1	for	for	ADP
eurjchem-976	264	2	c21h23cln2o	c21h23cln2o	NOUN
eurjchem-976	264	3	:	:	PUNCT
eurjchem-976	264	4	c	c	NOUN
eurjchem-976	264	5	,	,	PUNCT
eurjchem-976	264	6	71.07	71.07	NUM
eurjchem-976	264	7	;	;	PUNCT
eurjchem-976	264	8	h	h	NOUN
eurjchem-976	264	9	,	,	PUNCT
eurjchem-976	264	10	6.53	6.53	NUM
eurjchem-976	264	11	;	;	PUNCT
eurjchem-976	264	12	n	n	CCONJ
eurjchem-976	264	13	,	,	PUNCT
eurjchem-976	264	14	7.89	7.89	NUM
eurjchem-976	264	15	.	.	PUNCT
eurjchem-976	264	16	found	find	VERB
eurjchem-976	264	17	;	;	PUNCT
eurjchem-976	264	18	c	c	X
eurjchem-976	264	19	,	,	PUNCT
eurjchem-976	264	20	71.11	71.11	NUM
eurjchem-976	264	21	;	;	PUNCT
eurjchem-976	265	1	h	h	NOUN
eurjchem-976	265	2	,	,	PUNCT
eurjchem-976	265	3	6.53	6.53	NUM
eurjchem-976	265	4	;	;	PUNCT
eurjchem-976	265	5	n	n	CCONJ
eurjchem-976	265	6	,	,	PUNCT
eurjchem-976	265	7	7.65	7.65	NUM
eurjchem-976	265	8	%	%	NOUN
eurjchem-976	265	9	.	.	PUNCT
eurjchem-976	266	1	2.2.9	2.2.9	X
eurjchem-976	266	2	.	.	PUNCT
eurjchem-976	267	1	friedel‐crafts	friedel‐craft	VERB
eurjchem-976	267	2	cyclialkylations	cyclialkylation	NOUN
eurjchem-976	267	3	procedures	procedure	VERB
eurjchem-976	267	4	the	the	DET
eurjchem-976	267	5	procedures	procedure	NOUN
eurjchem-976	268	1	[	[	X
eurjchem-976	268	2	46‐54	46‐54	X
eurjchem-976	268	3	]	]	X
eurjchem-976	268	4	described	describe	VERB
eurjchem-976	268	5	earlier	early	ADV
eurjchem-976	268	6	for	for	ADP
eurjchem-976	268	7	cyclialkylation	cyclialkylation	NOUN
eurjchem-976	268	8	of	of	ADP
eurjchem-976	268	9	acids	acid	NOUN
eurjchem-976	268	10	and	and	CCONJ
eurjchem-976	268	11	alcohols	alcohol	NOUN
eurjchem-976	268	12	with	with	ADP
eurjchem-976	268	13	alcl3	alcl3	NOUN
eurjchem-976	268	14	/	/	SYM
eurjchem-976	268	15	ch3no2	ch3no2	NOUN
eurjchem-976	268	16	or	or	CCONJ
eurjchem-976	268	17	p2o5	p2o5	AUX
eurjchem-976	268	18	or	or	CCONJ
eurjchem-976	268	19	ppa	ppa	PROPN
eurjchem-976	268	20	catalysts	catalyst	NOUN
eurjchem-976	268	21	were	be	AUX
eurjchem-976	268	22	essentially	essentially	ADV
eurjchem-976	268	23	followed	follow	VERB
eurjchem-976	268	24	.	.	PUNCT
eurjchem-976	269	1	in	in	ADP
eurjchem-976	269	2	all	all	DET
eurjchem-976	269	3	reactions	reaction	NOUN
eurjchem-976	269	4	,	,	PUNCT
eurjchem-976	269	5	the	the	DET
eurjchem-976	269	6	crude	crude	NOUN
eurjchem-976	269	7	oily	oily	ADJ
eurjchem-976	269	8	or	or	CCONJ
eurjchem-976	269	9	solid	solid	ADJ
eurjchem-976	269	10	products	product	NOUN
eurjchem-976	269	11	were	be	AUX
eurjchem-976	269	12	purified	purify	VERB
eurjchem-976	269	13	by	by	ADP
eurjchem-976	269	14	flash	flash	NOUN
eurjchem-976	269	15	column	column	NOUN
eurjchem-976	269	16	chromatography	chromatography	NOUN
eurjchem-976	269	17	(	(	PUNCT
eurjchem-976	269	18	basic	basic	ADJ
eurjchem-976	269	19	alumina	alumina	NOUN
eurjchem-976	269	20	,	,	PUNCT
eurjchem-976	269	21	etoac	etoac	ADJ
eurjchem-976	269	22	:	:	PUNCT
eurjchem-976	269	23	n‐hexane	n‐hexane	ADJ
eurjchem-976	269	24	,	,	PUNCT
eurjchem-976	269	25	3:1	3:1	NUM
eurjchem-976	269	26	,	,	PUNCT
eurjchem-976	269	27	v	v	NOUN
eurjchem-976	269	28	:	:	SYM
eurjchem-976	269	29	v	v	NOUN
eurjchem-976	269	30	)	)	PUNCT
eurjchem-976	269	31	gave	give	VERB
eurjchem-976	269	32	the	the	DET
eurjchem-976	269	33	pure	pure	ADJ
eurjchem-976	269	34	products	product	NOUN
eurjchem-976	269	35	1a	1a	NOUN
eurjchem-976	269	36	,	,	PUNCT
eurjchem-976	269	37	b	b	NOUN
eurjchem-976	269	38	,	,	PUNCT
eurjchem-976	269	39	2a‐d	2a‐d	NOUN
eurjchem-976	269	40	and	and	CCONJ
eurjchem-976	269	41	3a‐d	3a‐d	NOUN
eurjchem-976	269	42	.	.	PUNCT
eurjchem-976	270	1	the	the	DET
eurjchem-976	270	2	conditions	condition	NOUN
eurjchem-976	270	3	and	and	CCONJ
eurjchem-976	270	4	yields	yield	NOUN
eurjchem-976	270	5	for	for	ADP
eurjchem-976	270	6	all	all	DET
eurjchem-976	270	7	products	product	NOUN
eurjchem-976	270	8	are	be	AUX
eurjchem-976	270	9	shown	show	VERB
eurjchem-976	270	10	in	in	ADP
eurjchem-976	270	11	table	table	NOUN
eurjchem-976	270	12	2	2	NUM
eurjchem-976	270	13	and	and	CCONJ
eurjchem-976	270	14	3	3	NUM
eurjchem-976	270	15	while	while	SCONJ
eurjchem-976	270	16	the	the	DET
eurjchem-976	270	17	physical	physical	ADJ
eurjchem-976	270	18	and	and	CCONJ
eurjchem-976	270	19	spectral	spectral	ADJ
eurjchem-976	270	20	data	datum	NOUN
eurjchem-976	270	21	of	of	ADP
eurjchem-976	270	22	the	the	DET
eurjchem-976	270	23	products	product	NOUN
eurjchem-976	270	24	are	be	AUX
eurjchem-976	270	25	given	give	VERB
eurjchem-976	270	26	below	below	ADV
eurjchem-976	270	27	.	.	PUNCT
eurjchem-976	271	1	3‐chloro‐2,4‐dihydro‐4,4‐dimethyl‐2‐phenylindeno[1,2‐c	3‐chloro‐2,4‐dihydro‐4,4‐dimethyl‐2‐phenylindeno[1,2‐c	NUM
eurjchem-976	271	2	]	]	X
eurjchem-976	271	3	pyrazole	pyrazole	NOUN
eurjchem-976	271	4	(	(	PUNCT
eurjchem-976	271	5	1a	1a	NUM
eurjchem-976	271	6	):	):	PUNCT
eurjchem-976	271	7	color	color	NOUN
eurjchem-976	271	8	:	:	PUNCT
eurjchem-976	271	9	white	white	ADJ
eurjchem-976	271	10	needles	needle	NOUN
eurjchem-976	271	11	.	.	PUNCT
eurjchem-976	272	1	m.p	m.p	PROPN
eurjchem-976	272	2	.	.	PROPN
eurjchem-976	272	3	:	:	PUNCT
eurjchem-976	273	1	117	117	NUM
eurjchem-976	273	2	°	°	NUM
eurjchem-976	273	3	c	c	X
eurjchem-976	273	4	(	(	PUNCT
eurjchem-976	273	5	acetone	acetone	NOUN
eurjchem-976	273	6	)	)	PUNCT
eurjchem-976	273	7	.	.	PUNCT
eurjchem-976	274	1	ir	ir	PROPN
eurjchem-976	274	2	(	(	PUNCT
eurjchem-976	274	3	kbr	kbr	PROPN
eurjchem-976	274	4	,	,	PUNCT
eurjchem-976	274	5	ν	ν	PROPN
eurjchem-976	274	6	,	,	PUNCT
eurjchem-976	274	7	cm‐1	cm‐1	PROPN
eurjchem-976	274	8	):	):	PUNCT
eurjchem-976	274	9	3075	3075	NUM
eurjchem-976	274	10	(	(	PUNCT
eurjchem-976	274	11	ch	ch	NOUN
eurjchem-976	274	12	)	)	PUNCT
eurjchem-976	274	13	(	(	PUNCT
eurjchem-976	274	14	aromatic	aromatic	NOUN
eurjchem-976	274	15	)	)	PUNCT
eurjchem-976	274	16	,	,	PUNCT
eurjchem-976	274	17	2980	2980	NUM
eurjchem-976	274	18	(	(	PUNCT
eurjchem-976	274	19	ch	ch	NOUN
eurjchem-976	274	20	)	)	PUNCT
eurjchem-976	274	21	(	(	PUNCT
eurjchem-976	274	22	alkyl	alkyl	NOUN
eurjchem-976	274	23	)	)	PUNCT
eurjchem-976	274	24	,	,	PUNCT
eurjchem-976	274	25	1600	1600	NUM
eurjchem-976	274	26	,	,	PUNCT
eurjchem-976	274	27	1480	1480	NUM
eurjchem-976	274	28	,	,	PUNCT
eurjchem-976	274	29	1460	1460	NUM
eurjchem-976	274	30	,	,	PUNCT
eurjchem-976	274	31	1435	1435	NUM
eurjchem-976	274	32	(	(	PUNCT
eurjchem-976	274	33	c	c	NOUN
eurjchem-976	274	34	=	=	SYM
eurjchem-976	274	35	c	c	NOUN
eurjchem-976	274	36	)	)	PUNCT
eurjchem-976	274	37	(	(	PUNCT
eurjchem-976	274	38	aromatic	aromatic	NOUN
eurjchem-976	274	39	)	)	PUNCT
eurjchem-976	274	40	,	,	PUNCT
eurjchem-976	274	41	1355	1355	NUM
eurjchem-976	274	42	,	,	PUNCT
eurjchem-976	274	43	1220	1220	NUM
eurjchem-976	274	44	,	,	PUNCT
eurjchem-976	274	45	748	748	NUM
eurjchem-976	274	46	.	.	PUNCT
eurjchem-976	275	1	1h	1h	NUM
eurjchem-976	275	2	nmr	nmr	NOUN
eurjchem-976	275	3	(	(	PUNCT
eurjchem-976	275	4	400	400	NUM
eurjchem-976	275	5	mhz	mhz	NOUN
eurjchem-976	275	6	,	,	PUNCT
eurjchem-976	275	7	cdcl3	cdcl3	PROPN
eurjchem-976	275	8	,	,	PUNCT
eurjchem-976	275	9	δ	δ	PROPN
eurjchem-976	275	10	,	,	PUNCT
eurjchem-976	275	11	ppm	ppm	NOUN
eurjchem-976	275	12	):	):	PUNCT
eurjchem-976	275	13	1.42	1.42	NUM
eurjchem-976	275	14	(	(	PUNCT
eurjchem-976	275	15	s	s	PROPN
eurjchem-976	275	16	,	,	PUNCT
eurjchem-976	275	17	6h	6h	NUM
eurjchem-976	275	18	,	,	PUNCT
eurjchem-976	275	19	2ch3	2ch3	NUM
eurjchem-976	275	20	)	)	PUNCT
eurjchem-976	275	21	,	,	PUNCT
eurjchem-976	275	22	7.15‐8.35	7.15‐8.35	NUM
eurjchem-976	275	23	(	(	PUNCT
eurjchem-976	275	24	m	m	PROPN
eurjchem-976	275	25	,	,	PUNCT
eurjchem-976	275	26	9h	9h	NUM
eurjchem-976	275	27	,	,	PUNCT
eurjchem-976	275	28	ar‐h	ar‐h	NOUN
eurjchem-976	275	29	)	)	PUNCT
eurjchem-976	275	30	.	.	PUNCT
eurjchem-976	276	1	13c	13c	NOUN
eurjchem-976	276	2	nmr	nmr	NOUN
eurjchem-976	276	3	(	(	PUNCT
eurjchem-976	276	4	100	100	NUM
eurjchem-976	276	5	mhz	mhz	NOUN
eurjchem-976	276	6	,	,	PUNCT
eurjchem-976	276	7	cdcl3	cdcl3	PROPN
eurjchem-976	276	8	,	,	PUNCT
eurjchem-976	276	9	δ	δ	PROPN
eurjchem-976	276	10	,	,	PUNCT
eurjchem-976	276	11	ppm	ppm	NUM
eurjchem-976	276	12	):	):	PUNCT
eurjchem-976	276	13	27.6	27.6	NUM
eurjchem-976	276	14	(	(	PUNCT
eurjchem-976	276	15	1c	1c	NOUN
eurjchem-976	276	16	,	,	PUNCT
eurjchem-976	276	17	‐c(ch3)2	‐c(ch3)2	ADJ
eurjchem-976	276	18	)	)	PUNCT
eurjchem-976	276	19	,	,	PUNCT
eurjchem-976	276	20	31.4	31.4	NUM
eurjchem-976	276	21	(	(	PUNCT
eurjchem-976	276	22	2c	2c	NOUN
eurjchem-976	276	23	,	,	PUNCT
eurjchem-976	276	24	‐c(ch3)2	‐c(ch3)2	ADJ
eurjchem-976	276	25	)	)	PUNCT
eurjchem-976	276	26	,	,	PUNCT
eurjchem-976	276	27	117.4	117.4	NUM
eurjchem-976	276	28	(	(	PUNCT
eurjchem-976	276	29	1c	1c	NOUN
eurjchem-976	276	30	,	,	PUNCT
eurjchem-976	276	31	c‐3a	c‐3a	PROPN
eurjchem-976	276	32	)	)	PUNCT
eurjchem-976	276	33	,	,	PUNCT
eurjchem-976	276	34	123.4	123.4	NUM
eurjchem-976	276	35	(	(	PUNCT
eurjchem-976	276	36	2c	2c	NUM
eurjchem-976	276	37	,	,	PUNCT
eurjchem-976	276	38	ar	ar	PROPN
eurjchem-976	276	39	.	.	PROPN
eurjchem-976	276	40	,	,	PUNCT
eurjchem-976	276	41	c‐2	c‐2	NOUN
eurjchem-976	276	42	'	'	PUNCT
eurjchem-976	276	43	,	,	PUNCT
eurjchem-976	276	44	c‐6	c‐6	NOUN
eurjchem-976	276	45	'	'	PUNCT
eurjchem-976	276	46	)	)	PUNCT
eurjchem-976	276	47	,	,	PUNCT
eurjchem-976	276	48	126.3	126.3	NUM
eurjchem-976	276	49	(	(	PUNCT
eurjchem-976	276	50	1c	1c	NOUN
eurjchem-976	276	51	,	,	PUNCT
eurjchem-976	276	52	ar	ar	PROPN
eurjchem-976	276	53	.	.	PROPN
eurjchem-976	276	54	,	,	PUNCT
eurjchem-976	276	55	c‐4	c‐4	PROPN
eurjchem-976	276	56	'	'	PUNCT
eurjchem-976	276	57	)	)	PUNCT
eurjchem-976	276	58	,	,	PUNCT
eurjchem-976	276	59	126.7	126.7	NUM
eurjchem-976	276	60	(	(	PUNCT
eurjchem-976	276	61	1c	1c	X
eurjchem-976	276	62	,	,	PUNCT
eurjchem-976	276	63	ar	ar	PROPN
eurjchem-976	276	64	.	.	PROPN
eurjchem-976	276	65	,	,	PUNCT
eurjchem-976	276	66	c‐7	c‐7	PROPN
eurjchem-976	276	67	)	)	PUNCT
eurjchem-976	276	68	,	,	PUNCT
eurjchem-976	276	69	127.4	127.4	NUM
eurjchem-976	276	70	(	(	PUNCT
eurjchem-976	276	71	1c	1c	NOUN
eurjchem-976	276	72	,	,	PUNCT
eurjchem-976	276	73	ar	ar	PROPN
eurjchem-976	276	74	.	.	PROPN
eurjchem-976	276	75	,	,	PUNCT
eurjchem-976	276	76	c‐5	c‐5	NOUN
eurjchem-976	276	77	)	)	PUNCT
eurjchem-976	276	78	,	,	PUNCT
eurjchem-976	276	79	128.2	128.2	NUM
eurjchem-976	276	80	(	(	PUNCT
eurjchem-976	276	81	1c	1c	X
eurjchem-976	276	82	,	,	PUNCT
eurjchem-976	276	83	n‐c(cl)=	n‐c(cl)=	NOUN
eurjchem-976	276	84	,	,	PUNCT
eurjchem-976	276	85	c‐3	c‐3	PROPN
eurjchem-976	276	86	)	)	PUNCT
eurjchem-976	276	87	,	,	PUNCT
eurjchem-976	276	88	129.2	129.2	NUM
eurjchem-976	276	89	(	(	PUNCT
eurjchem-976	276	90	1c	1c	X
eurjchem-976	276	91	,	,	PUNCT
eurjchem-976	276	92	ar	ar	PROPN
eurjchem-976	276	93	.	.	PROPN
eurjchem-976	276	94	,	,	PUNCT
eurjchem-976	276	95	c‐8	c‐8	PROPN
eurjchem-976	276	96	)	)	PUNCT
eurjchem-976	276	97	,	,	PUNCT
eurjchem-976	276	98	129.4	129.4	NUM
eurjchem-976	276	99	(	(	PUNCT
eurjchem-976	276	100	1c	1c	NOUN
eurjchem-976	276	101	,	,	PUNCT
eurjchem-976	276	102	ar	ar	PROPN
eurjchem-976	276	103	.	.	PROPN
eurjchem-976	276	104	,	,	PUNCT
eurjchem-976	276	105	c‐	c‐	NOUN
eurjchem-976	276	106	6	6	NUM
eurjchem-976	276	107	)	)	PUNCT
eurjchem-976	276	108	,	,	PUNCT
eurjchem-976	276	109	132.4	132.4	NUM
eurjchem-976	276	110	(	(	PUNCT
eurjchem-976	276	111	2c	2c	NUM
eurjchem-976	276	112	,	,	PUNCT
eurjchem-976	276	113	ar	ar	PROPN
eurjchem-976	276	114	.	.	PROPN
eurjchem-976	276	115	,	,	PUNCT
eurjchem-976	276	116	c‐3	c‐3	PROPN
eurjchem-976	276	117	'	'	PUNCT
eurjchem-976	276	118	,	,	PUNCT
eurjchem-976	276	119	c‐5	c‐5	NOUN
eurjchem-976	276	120	'	'	PUNCT
eurjchem-976	276	121	)	)	PUNCT
eurjchem-976	276	122	,	,	PUNCT
eurjchem-976	276	123	134.7	134.7	NUM
eurjchem-976	276	124	(	(	PUNCT
eurjchem-976	276	125	1c	1c	NOUN
eurjchem-976	276	126	,	,	PUNCT
eurjchem-976	276	127	ar	ar	PROPN
eurjchem-976	276	128	.	.	PROPN
eurjchem-976	276	129	,	,	PUNCT
eurjchem-976	276	130	c‐8a	c‐8a	PROPN
eurjchem-976	276	131	)	)	PUNCT
eurjchem-976	276	132	,	,	PUNCT
eurjchem-976	276	133	142.7	142.7	NUM
eurjchem-976	276	134	(	(	PUNCT
eurjchem-976	276	135	1c	1c	NOUN
eurjchem-976	276	136	,	,	PUNCT
eurjchem-976	276	137	ar	ar	PROPN
eurjchem-976	276	138	.	.	PROPN
eurjchem-976	276	139	,	,	PUNCT
eurjchem-976	276	140	c‐1	c‐1	NOUN
eurjchem-976	276	141	'	'	PUNCT
eurjchem-976	276	142	)	)	PUNCT
eurjchem-976	276	143	,	,	PUNCT
eurjchem-976	276	144	156.1	156.1	NUM
eurjchem-976	276	145	(	(	PUNCT
eurjchem-976	276	146	1c	1c	NUM
eurjchem-976	276	147	,	,	PUNCT
eurjchem-976	276	148	n	n	CCONJ
eurjchem-976	276	149	=	=	NOUN
eurjchem-976	276	150	c‐	c‐	NOUN
eurjchem-976	276	151	,	,	PUNCT
eurjchem-976	276	152	c‐8b	c‐8b	PROPN
eurjchem-976	276	153	)	)	PUNCT
eurjchem-976	276	154	,	,	PUNCT
eurjchem-976	276	155	160.4	160.4	NUM
eurjchem-976	276	156	(	(	PUNCT
eurjchem-976	276	157	1c	1c	NOUN
eurjchem-976	276	158	,	,	PUNCT
eurjchem-976	276	159	ar	ar	PROPN
eurjchem-976	276	160	.	.	PROPN
eurjchem-976	276	161	,	,	PUNCT
eurjchem-976	276	162	c‐4a	c‐4a	NOUN
eurjchem-976	276	163	)	)	PUNCT
eurjchem-976	276	164	.	.	PUNCT
eurjchem-976	277	1	anal	anal	PROPN
eurjchem-976	277	2	.	.	PUNCT
eurjchem-976	277	3	calcd	calcd	NOUN
eurjchem-976	277	4	.	.	PUNCT
eurjchem-976	278	1	for	for	ADP
eurjchem-976	278	2	c18h15cln2	c18h15cln2	PROPN
eurjchem-976	278	3	:	:	PUNCT
eurjchem-976	278	4	c	c	X
eurjchem-976	278	5	,	,	PUNCT
eurjchem-976	278	6	73.34	73.34	NUM
eurjchem-976	278	7	;	;	PUNCT
eurjchem-976	278	8	h	h	NOUN
eurjchem-976	278	9	,	,	PUNCT
eurjchem-976	278	10	5.13	5.13	NUM
eurjchem-976	278	11	;	;	PUNCT
eurjchem-976	278	12	n	n	CCONJ
eurjchem-976	278	13	,	,	PUNCT
eurjchem-976	278	14	9.50	9.50	NUM
eurjchem-976	278	15	.	.	PUNCT
eurjchem-976	278	16	found	find	VERB
eurjchem-976	278	17	;	;	PUNCT
eurjchem-976	278	18	c	c	X
eurjchem-976	278	19	,	,	PUNCT
eurjchem-976	278	20	73.38	73.38	NUM
eurjchem-976	278	21	;	;	PUNCT
eurjchem-976	279	1	h	h	NOUN
eurjchem-976	279	2	,	,	PUNCT
eurjchem-976	279	3	5.14	5.14	NUM
eurjchem-976	279	4	;	;	PUNCT
eurjchem-976	279	5	n	n	CCONJ
eurjchem-976	279	6	,	,	PUNCT
eurjchem-976	279	7	9.37	9.37	NUM
eurjchem-976	279	8	%	%	NOUN
eurjchem-976	279	9	.	.	PUNCT
eurjchem-976	280	1	4,5‐dihydro‐5,5‐dimethyl‐2‐phenyl‐2h‐benzo[g]indazol‐3	4,5‐dihydro‐5,5‐dimethyl‐2‐phenyl‐2h‐benzo[g]indazol‐3	NUM
eurjchem-976	280	2	(	(	PUNCT
eurjchem-976	280	3	3ah)‐one	3ah)‐one	NUM
eurjchem-976	280	4	(	(	PUNCT
eurjchem-976	280	5	2a	2a	NUM
eurjchem-976	280	6	):	):	PUNCT
eurjchem-976	280	7	color	color	NOUN
eurjchem-976	280	8	:	:	PUNCT
eurjchem-976	280	9	white	white	ADJ
eurjchem-976	280	10	needles	needle	NOUN
eurjchem-976	280	11	.	.	PUNCT
eurjchem-976	281	1	m.p	m.p	PROPN
eurjchem-976	281	2	.	.	PROPN
eurjchem-976	281	3	:	:	PUNCT
eurjchem-976	282	1	92	92	NUM
eurjchem-976	282	2	°	°	NUM
eurjchem-976	282	3	c	c	X
eurjchem-976	282	4	(	(	PUNCT
eurjchem-976	282	5	acetone	acetone	NOUN
eurjchem-976	282	6	)	)	PUNCT
eurjchem-976	282	7	.	.	PUNCT
eurjchem-976	283	1	ir	ir	PROPN
eurjchem-976	283	2	(	(	PUNCT
eurjchem-976	283	3	kbr	kbr	PROPN
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eurjchem-976	283	11	ch	ch	NOUN
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eurjchem-976	283	13	(	(	PUNCT
eurjchem-976	283	14	aromatic	aromatic	NOUN
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eurjchem-976	283	16	,	,	PUNCT
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eurjchem-976	283	18	(	(	PUNCT
eurjchem-976	283	19	ch	ch	NOUN
eurjchem-976	283	20	)	)	PUNCT
eurjchem-976	283	21	(	(	PUNCT
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eurjchem-976	283	23	)	)	PUNCT
eurjchem-976	283	24	,	,	PUNCT
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eurjchem-976	283	26	(	(	PUNCT
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eurjchem-976	283	29	o	o	NOUN
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eurjchem-976	283	31	(	(	PUNCT
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eurjchem-976	283	34	,	,	PUNCT
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eurjchem-976	283	36	,	,	PUNCT
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eurjchem-976	283	43	c	c	NOUN
eurjchem-976	283	44	=	=	SYM
eurjchem-976	283	45	c	c	NOUN
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eurjchem-976	283	47	(	(	PUNCT
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eurjchem-976	283	50	,	,	PUNCT
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eurjchem-976	283	52	,	,	PUNCT
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eurjchem-976	284	2	nmr	nmr	NOUN
eurjchem-976	284	3	(	(	PUNCT
eurjchem-976	284	4	400	400	NUM
eurjchem-976	284	5	mhz	mhz	NOUN
eurjchem-976	284	6	,	,	PUNCT
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eurjchem-976	284	8	,	,	PUNCT
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eurjchem-976	284	12	):	):	PUNCT
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eurjchem-976	284	14	(	(	PUNCT
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eurjchem-976	284	17	6h	6h	NUM
eurjchem-976	284	18	,	,	PUNCT
eurjchem-976	284	19	2ch3	2ch3	NUM
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eurjchem-976	284	21	,	,	PUNCT
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eurjchem-976	284	23	(	(	PUNCT
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eurjchem-976	284	25	,	,	PUNCT
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eurjchem-976	284	28	,	,	PUNCT
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eurjchem-976	284	30	=	=	PROPN
eurjchem-976	284	31	14.2	14.2	NUM
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eurjchem-976	284	33	,	,	PUNCT
eurjchem-976	284	34	ch2	ch2	PROPN
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eurjchem-976	284	36	,	,	PUNCT
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eurjchem-976	284	42	,	,	PUNCT
eurjchem-976	284	43	j	j	PROPN
eurjchem-976	284	44	=	=	PROPN
eurjchem-976	284	45	14.2	14.2	NUM
eurjchem-976	284	46	hz	hz	NOUN
eurjchem-976	284	47	,	,	PUNCT
eurjchem-976	284	48	ch2	ch2	PROPN
eurjchem-976	284	49	)	)	PUNCT
eurjchem-976	284	50	,	,	PUNCT
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eurjchem-976	284	52	(	(	PUNCT
eurjchem-976	284	53	app	app	X
eurjchem-976	284	54	.	.	PROPN
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eurjchem-976	285	2	,	,	PUNCT
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eurjchem-976	285	4	,	,	PUNCT
eurjchem-976	285	5	j	j	PROPN
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eurjchem-976	285	7	10.4	10.4	NUM
eurjchem-976	285	8	hz	hz	NOUN
eurjchem-976	285	9	,	,	PUNCT
eurjchem-976	285	10	ch	ch	NOUN
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eurjchem-976	285	12	,	,	PUNCT
eurjchem-976	285	13	6.85‐8.11	6.85‐8.11	NUM
eurjchem-976	285	14	(	(	PUNCT
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eurjchem-976	286	3	(	(	PUNCT
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eurjchem-976	286	19	,	,	PUNCT
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eurjchem-976	286	42	,	,	PUNCT
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eurjchem-976	286	45	,	,	PUNCT
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eurjchem-976	286	90	,	,	PUNCT
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eurjchem-976	286	100	,	,	PUNCT
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eurjchem-976	286	124	,	,	PUNCT
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eurjchem-976	286	134	,	,	PUNCT
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eurjchem-976	286	137	1c	1c	X
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eurjchem-976	286	146	,	,	PUNCT
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eurjchem-976	288	13	,	,	PUNCT
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eurjchem-976	289	2	,	,	PUNCT
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eurjchem-976	290	3	(	(	PUNCT
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eurjchem-976	292	13	(	(	PUNCT
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eurjchem-976	292	21	(	(	PUNCT
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eurjchem-976	292	47	(	(	PUNCT
eurjchem-976	292	48	aromatic	aromatic	NOUN
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eurjchem-976	292	50	,	,	PUNCT
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eurjchem-976	292	52	,	,	PUNCT
eurjchem-976	292	53	7453	7453	NUM
eurjchem-976	292	54	.	.	PUNCT
eurjchem-976	293	1	1h	1h	NUM
eurjchem-976	293	2	nmr	nmr	NOUN
eurjchem-976	293	3	(	(	PUNCT
eurjchem-976	293	4	400	400	NUM
eurjchem-976	293	5	mhz	mhz	NOUN
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eurjchem-976	293	8	,	,	PUNCT
eurjchem-976	293	9	δ	δ	PROPN
eurjchem-976	293	10	,	,	PUNCT
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eurjchem-976	293	12	):	):	PUNCT
eurjchem-976	293	13	1.10	1.10	NUM
eurjchem-976	293	14	(	(	PUNCT
eurjchem-976	293	15	d	d	PROPN
eurjchem-976	293	16	,	,	PUNCT
eurjchem-976	293	17	3h	3h	NUM
eurjchem-976	293	18	,	,	PUNCT
eurjchem-976	293	19	j	j	PROPN
eurjchem-976	293	20	=	=	SYM
eurjchem-976	293	21	9.4	9.4	NUM
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eurjchem-976	293	23	,	,	PUNCT
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eurjchem-976	293	26	,	,	PUNCT
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eurjchem-976	293	28	(	(	PUNCT
eurjchem-976	293	29	s	s	PROPN
eurjchem-976	293	30	,	,	PUNCT
eurjchem-976	293	31	6h	6h	NUM
eurjchem-976	293	32	,	,	PUNCT
eurjchem-976	293	33	2ch3	2ch3	NUM
eurjchem-976	293	34	)	)	PUNCT
eurjchem-976	293	35	,	,	PUNCT
eurjchem-976	293	36	2.21	2.21	NUM
eurjchem-976	293	37	(	(	PUNCT
eurjchem-976	293	38	p	p	X
eurjchem-976	293	39	,	,	PUNCT
eurjchem-976	293	40	1h	1h	NUM
eurjchem-976	293	41	,	,	PUNCT
eurjchem-976	293	42	j	j	PROPN
eurjchem-976	293	43	=	=	PROPN
eurjchem-976	293	44	12.5	12.5	NUM
eurjchem-976	293	45	hz	hz	NOUN
eurjchem-976	293	46	,	,	PUNCT
eurjchem-976	293	47	ch	ch	NOUN
eurjchem-976	293	48	)	)	PUNCT
eurjchem-976	293	49	,	,	PUNCT
eurjchem-976	293	50	2.38	2.38	NUM
eurjchem-976	293	51	(	(	PUNCT
eurjchem-976	293	52	app	app	PROPN
eurjchem-976	293	53	.	.	PROPN
eurjchem-976	293	54	t	t	PROPN
eurjchem-976	293	55	,	,	PUNCT
eurjchem-976	293	56	1h	1h	NUM
eurjchem-976	293	57	,	,	PUNCT
eurjchem-976	293	58	j	j	PROPN
eurjchem-976	293	59	=	=	PROPN
eurjchem-976	293	60	12.5	12.5	NUM
eurjchem-976	293	61	hz	hz	NOUN
eurjchem-976	293	62	,	,	PUNCT
eurjchem-976	293	63	ch	ch	NOUN
eurjchem-976	293	64	)	)	PUNCT
eurjchem-976	293	65	,	,	PUNCT
eurjchem-976	293	66	7.19‐8.35	7.19‐8.35	NUM
eurjchem-976	293	67	(	(	PUNCT
eurjchem-976	293	68	m	m	PROPN
eurjchem-976	293	69	,	,	PUNCT
eurjchem-976	293	70	9h	9h	NUM
eurjchem-976	293	71	,	,	PUNCT
eurjchem-976	293	72	ar‐h	ar‐h	NOUN
eurjchem-976	293	73	)	)	PUNCT
eurjchem-976	293	74	.	.	PUNCT
eurjchem-976	294	1	13c	13c	NOUN
eurjchem-976	294	2	nmr	nmr	NOUN
eurjchem-976	294	3	(	(	PUNCT
eurjchem-976	294	4	100	100	NUM
eurjchem-976	294	5	mhz	mhz	NOUN
eurjchem-976	294	6	,	,	PUNCT
eurjchem-976	294	7	cdcl3	cdcl3	PROPN
eurjchem-976	294	8	,	,	PUNCT
eurjchem-976	294	9	δ	δ	PROPN
eurjchem-976	294	10	,	,	PUNCT
eurjchem-976	294	11	ppm	ppm	NUM
eurjchem-976	294	12	):	):	PUNCT
eurjchem-976	294	13	14.2	14.2	NUM
eurjchem-976	294	14	(	(	PUNCT
eurjchem-976	294	15	1c	1c	NOUN
eurjchem-976	294	16	,	,	PUNCT
eurjchem-976	294	17	‐ch(ch3	‐ch(ch3	ADJ
eurjchem-976	294	18	)	)	PUNCT
eurjchem-976	294	19	)	)	PUNCT
eurjchem-976	294	20	,	,	PUNCT
eurjchem-976	294	21	28.3	28.3	NUM
eurjchem-976	294	22	(	(	PUNCT
eurjchem-976	294	23	2c	2c	NOUN
eurjchem-976	294	24	,	,	PUNCT
eurjchem-976	294	25	‐c(ch3)2	‐c(ch3)2	ADJ
eurjchem-976	294	26	)	)	PUNCT
eurjchem-976	294	27	,	,	PUNCT
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eurjchem-976	294	30	1c	1c	NOUN
eurjchem-976	294	31	,	,	PUNCT
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eurjchem-976	294	33	,	,	PUNCT
eurjchem-976	294	34	c‐5	c‐5	NOUN
eurjchem-976	294	35	)	)	PUNCT
eurjchem-976	294	36	,	,	PUNCT
eurjchem-976	294	37	42.8	42.8	NUM
eurjchem-976	294	38	(	(	PUNCT
eurjchem-976	294	39	1c	1c	NOUN
eurjchem-976	294	40	,	,	PUNCT
eurjchem-976	294	41	‐c(ch3	‐c(ch3	NUM
eurjchem-976	294	42	)	)	PUNCT
eurjchem-976	294	43	,	,	PUNCT
eurjchem-976	294	44	c‐4	c‐4	PROPN
eurjchem-976	294	45	)	)	PUNCT
eurjchem-976	294	46	,	,	PUNCT
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eurjchem-976	294	49	1c	1c	NOUN
eurjchem-976	294	50	,	,	PUNCT
eurjchem-976	294	51	‐	‐	ADJ
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eurjchem-976	294	53	,	,	PUNCT
eurjchem-976	294	54	c‐3a	c‐3a	PROPN
eurjchem-976	294	55	)	)	PUNCT
eurjchem-976	294	56	,	,	PUNCT
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eurjchem-976	294	58	(	(	PUNCT
eurjchem-976	294	59	2c	2c	NUM
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eurjchem-976	294	68	'	'	PUNCT
eurjchem-976	294	69	)	)	PUNCT
eurjchem-976	294	70	,	,	PUNCT
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eurjchem-976	294	73	1c	1c	NOUN
eurjchem-976	294	74	,	,	PUNCT
eurjchem-976	294	75	ar	ar	PROPN
eurjchem-976	294	76	.	.	PROPN
eurjchem-976	294	77	,	,	PUNCT
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eurjchem-976	294	80	)	)	PUNCT
eurjchem-976	294	81	,	,	PUNCT
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eurjchem-976	294	84	1c	1c	NOUN
eurjchem-976	294	85	,	,	PUNCT
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eurjchem-976	294	88	,	,	PUNCT
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eurjchem-976	294	91	,	,	PUNCT
eurjchem-976	294	92	126.7	126.7	NUM
eurjchem-976	294	93	(	(	PUNCT
eurjchem-976	294	94	1c	1c	X
eurjchem-976	294	95	,	,	PUNCT
eurjchem-976	294	96	ar	ar	PROPN
eurjchem-976	294	97	.	.	PROPN
eurjchem-976	294	98	,	,	PUNCT
eurjchem-976	294	99	c‐9a	c‐9a	PROPN
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eurjchem-976	294	101	,	,	PUNCT
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eurjchem-976	294	104	1c	1c	NUM
eurjchem-976	294	105	,	,	PUNCT
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eurjchem-976	294	107	.	.	PROPN
eurjchem-976	294	108	,	,	PUNCT
eurjchem-976	294	109	c‐8	c‐8	PROPN
eurjchem-976	294	110	)	)	PUNCT
eurjchem-976	294	111	,	,	PUNCT
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eurjchem-976	294	113	(	(	PUNCT
eurjchem-976	294	114	1c	1c	X
eurjchem-976	294	115	,	,	PUNCT
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eurjchem-976	294	118	,	,	PUNCT
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eurjchem-976	294	121	,	,	PUNCT
eurjchem-976	294	122	132.2	132.2	NUM
eurjchem-976	294	123	(	(	PUNCT
eurjchem-976	294	124	2c	2c	NUM
eurjchem-976	294	125	,	,	PUNCT
eurjchem-976	294	126	ar	ar	PROPN
eurjchem-976	294	127	.	.	PROPN
eurjchem-976	294	128	,	,	PUNCT
eurjchem-976	294	129	c‐3	c‐3	PROPN
eurjchem-976	294	130	'	'	PUNCT
eurjchem-976	294	131	,	,	PUNCT
eurjchem-976	294	132	c‐5	c‐5	NOUN
eurjchem-976	294	133	'	'	PUNCT
eurjchem-976	294	134	)	)	PUNCT
eurjchem-976	294	135	,	,	PUNCT
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eurjchem-976	294	137	(	(	PUNCT
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eurjchem-976	294	139	,	,	PUNCT
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eurjchem-976	294	142	,	,	PUNCT
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eurjchem-976	294	146	,	,	PUNCT
eurjchem-976	294	147	144.2	144.2	NUM
eurjchem-976	294	148	(	(	PUNCT
eurjchem-976	294	149	1c	1c	NOUN
eurjchem-976	294	150	,	,	PUNCT
eurjchem-976	294	151	ar	ar	PROPN
eurjchem-976	294	152	.	.	PROPN
eurjchem-976	294	153	,	,	PUNCT
eurjchem-976	294	154	c‐1	c‐1	NOUN
eurjchem-976	294	155	'	'	PUNCT
eurjchem-976	294	156	)	)	PUNCT
eurjchem-976	294	157	,	,	PUNCT
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eurjchem-976	294	159	(	(	PUNCT
eurjchem-976	294	160	1c	1c	NUM
eurjchem-976	294	161	,	,	PUNCT
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eurjchem-976	294	166	,	,	PUNCT
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eurjchem-976	294	168	(	(	PUNCT
eurjchem-976	294	169	1c	1c	X
eurjchem-976	294	170	,	,	PUNCT
eurjchem-976	294	171	ar	ar	PROPN
eurjchem-976	294	172	.	.	PROPN
eurjchem-976	294	173	,	,	PUNCT
eurjchem-976	294	174	c‐	c‐	NOUN
eurjchem-976	294	175	5a	5a	NUM
eurjchem-976	294	176	)	)	PUNCT
eurjchem-976	294	177	,	,	PUNCT
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eurjchem-976	294	179	(	(	PUNCT
eurjchem-976	294	180	1c	1c	NOUN
eurjchem-976	294	181	,	,	PUNCT
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eurjchem-976	294	183	=	=	SYM
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eurjchem-976	294	185	,	,	PUNCT
eurjchem-976	294	186	c‐3	c‐3	NOUN
eurjchem-976	294	187	)	)	PUNCT
eurjchem-976	294	188	.	.	PUNCT
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eurjchem-976	295	2	.	.	PUNCT
eurjchem-976	295	3	calcd	calcd	NOUN
eurjchem-976	295	4	.	.	PUNCT
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eurjchem-976	296	2	c20h20n2o	c20h20n2o	NOUN
eurjchem-976	296	3	:	:	PUNCT
eurjchem-976	296	4	c	c	X
eurjchem-976	296	5	,	,	PUNCT
eurjchem-976	296	6	78.92	78.92	NUM
eurjchem-976	296	7	;	;	PUNCT
eurjchem-976	296	8	h	h	NOUN
eurjchem-976	296	9	,	,	PUNCT
eurjchem-976	296	10	6.62	6.62	NUM
eurjchem-976	296	11	;	;	PUNCT
eurjchem-976	296	12	n	n	CCONJ
eurjchem-976	296	13	,	,	PUNCT
eurjchem-976	296	14	9.20	9.20	NUM
eurjchem-976	296	15	.	.	PUNCT
eurjchem-976	296	16	found	find	VERB
eurjchem-976	296	17	;	;	PUNCT
eurjchem-976	296	18	c	c	X
eurjchem-976	296	19	,	,	PUNCT
eurjchem-976	296	20	78.79	78.79	NUM
eurjchem-976	296	21	;	;	PUNCT
eurjchem-976	297	1	h	h	NOUN
eurjchem-976	297	2	,	,	PUNCT
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eurjchem-976	297	9	.	.	PUNCT
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eurjchem-976	298	2	]	]	X
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eurjchem-976	298	4	(	(	PUNCT
eurjchem-976	298	5	3a	3a	NUM
eurjchem-976	298	6	):	):	PUNCT
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eurjchem-976	298	8	:	:	PUNCT
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eurjchem-976	298	12	.	.	PUNCT
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eurjchem-976	299	2	=	=	PUNCT
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eurjchem-976	299	4	.	.	PUNCT
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eurjchem-976	300	4	.	.	PUNCT
eurjchem-976	300	5	/	/	SYM
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eurjchem-976	300	14	(	(	PUNCT
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eurjchem-976	300	23	ring	ring	NOUN
eurjchem-976	300	24	closures	closure	NOUN
eurjchem-976	300	25	of	of	ADP
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eurjchem-976	300	28	6	6	NUM
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eurjchem-976	300	35	,	,	PUNCT
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eurjchem-976	300	39	product	product	NOUN
eurjchem-976	300	40	conditions	condition	NOUN
eurjchem-976	300	41	yield	yield	NOUN
eurjchem-976	300	42	(	(	PUNCT
eurjchem-976	300	43	%	%	NOUN
eurjchem-976	300	44	)	)	PUNCT
eurjchem-976	300	45	1	1	NUM
eurjchem-976	300	46	n	n	NUM
eurjchem-976	300	47	n	n	PRON
eurjchem-976	300	48	ph	ph	NOUN
eurjchem-976	300	49	o	o	NOUN
eurjchem-976	300	50	cl	cl	NOUN
eurjchem-976	300	51	1b	1b	NUM
eurjchem-976	300	52	alcl3	alcl3	SYM
eurjchem-976	300	53	/	/	SYM
eurjchem-976	300	54	ch3no2	ch3no2	PROPN
eurjchem-976	300	55	,	,	PUNCT
eurjchem-976	300	56	dcm	dcm	PROPN
eurjchem-976	300	57	,	,	PUNCT
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eurjchem-976	300	59	h	h	NOUN
eurjchem-976	300	60	,	,	PUNCT
eurjchem-976	300	61	reflux	reflux	VERB
eurjchem-976	300	62	90	90	NUM
eurjchem-976	300	63	p2o5,toluene	p2o5,toluene	NOUN
eurjchem-976	300	64	,	,	PUNCT
eurjchem-976	300	65	6	6	NUM
eurjchem-976	300	66	h	h	NOUN
eurjchem-976	300	67	,	,	PUNCT
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eurjchem-976	301	3	,	,	PUNCT
eurjchem-976	301	4	5	5	NUM
eurjchem-976	301	5	h	h	NOUN
eurjchem-976	301	6	,	,	PUNCT
eurjchem-976	301	7	210‐220	210‐220	PROPN
eurjchem-976	301	8	°	°	ADP
eurjchem-976	301	9	c	c	PROPN
eurjchem-976	301	10	77	77	NUM
eurjchem-976	301	11	2	2	NUM
eurjchem-976	301	12	alcl3	alcl3	NOUN
eurjchem-976	301	13	/	/	SYM
eurjchem-976	301	14	ch3no2	ch3no2	PROPN
eurjchem-976	301	15	,	,	PUNCT
eurjchem-976	301	16	dcm	dcm	PROPN
eurjchem-976	301	17	,	,	PUNCT
eurjchem-976	301	18	10	10	NUM
eurjchem-976	301	19	h	h	NOUN
eurjchem-976	301	20	,	,	PUNCT
eurjchem-976	301	21	reflux	reflux	NOUN
eurjchem-976	301	22	89	89	NUM
eurjchem-976	301	23	p2o5	p2o5	NOUN
eurjchem-976	301	24	,	,	PUNCT
eurjchem-976	301	25	toluene	toluene	NOUN
eurjchem-976	301	26	,	,	PUNCT
eurjchem-976	301	27	6	6	NUM
eurjchem-976	301	28	h	h	NOUN
eurjchem-976	301	29	,	,	PUNCT
eurjchem-976	301	30	reflux	reflux	VERB
eurjchem-976	301	31	82	82	NUM
eurjchem-976	301	32	ppa	ppa	PROPN
eurjchem-976	301	33	,	,	PUNCT
eurjchem-976	301	34	4	4	NUM
eurjchem-976	301	35	h	h	NOUN
eurjchem-976	301	36	,	,	PUNCT
eurjchem-976	301	37	190‐200	190‐200	NUM
eurjchem-976	301	38	°	°	ADP
eurjchem-976	301	39	c	c	PROPN
eurjchem-976	301	40	73	73	NUM
eurjchem-976	301	41	3	3	NUM
eurjchem-976	301	42	n	n	CCONJ
eurjchem-976	301	43	n	n	PRON
eurjchem-976	301	44	ph	ph	ADJ
eurjchem-976	301	45	ph	ph	NOUN
eurjchem-976	301	46	10b	10b	NOUN
eurjchem-976	301	47	o	o	NOUN
eurjchem-976	301	48	cooh	cooh	NOUN
eurjchem-976	301	49	alcl3	alcl3	PROPN
eurjchem-976	301	50	/	/	SYM
eurjchem-976	301	51	ch3no2	ch3no2	PROPN
eurjchem-976	301	52	,	,	PUNCT
eurjchem-976	301	53	dcm	dcm	PROPN
eurjchem-976	301	54	,	,	PUNCT
eurjchem-976	301	55	8	8	NUM
eurjchem-976	301	56	h	h	NOUN
eurjchem-976	301	57	,	,	PUNCT
eurjchem-976	301	58	reflux	reflux	VERB
eurjchem-976	301	59	81	81	NUM
eurjchem-976	301	60	p2o5	p2o5	NOUN
eurjchem-976	301	61	,	,	PUNCT
eurjchem-976	301	62	toluene	toluene	NOUN
eurjchem-976	301	63	,	,	PUNCT
eurjchem-976	301	64	3	3	NUM
eurjchem-976	301	65	h	h	NOUN
eurjchem-976	301	66	,	,	PUNCT
eurjchem-976	301	67	reflux	reflux	PROPN
eurjchem-976	301	68	89	89	NUM
eurjchem-976	301	69	ppa	ppa	PROPN
eurjchem-976	301	70	,	,	PUNCT
eurjchem-976	301	71	2	2	NUM
eurjchem-976	301	72	h	h	NOUN
eurjchem-976	301	73	,	,	PUNCT
eurjchem-976	301	74	200‐210	200‐210	PROPN
eurjchem-976	301	75	°	°	PROPN
eurjchem-976	301	76	c	c	PROPN
eurjchem-976	301	77	79	79	NUM
eurjchem-976	301	78	4	4	NUM
eurjchem-976	301	79	alcl3	alcl3	NOUN
eurjchem-976	301	80	/	/	SYM
eurjchem-976	301	81	ch3no2	ch3no2	PROPN
eurjchem-976	301	82	,	,	PUNCT
eurjchem-976	301	83	dcm	dcm	PROPN
eurjchem-976	301	84	,	,	PUNCT
eurjchem-976	301	85	8	8	NUM
eurjchem-976	301	86	h	h	NOUN
eurjchem-976	301	87	,	,	PUNCT
eurjchem-976	301	88	reflux	reflux	VERB
eurjchem-976	301	89	92	92	NUM
eurjchem-976	301	90	p2o5	p2o5	NOUN
eurjchem-976	301	91	,	,	PUNCT
eurjchem-976	301	92	toluene	toluene	NOUN
eurjchem-976	301	93	,	,	PUNCT
eurjchem-976	301	94	5	5	NUM
eurjchem-976	301	95	h	h	NOUN
eurjchem-976	301	96	,	,	PUNCT
eurjchem-976	301	97	reflux	reflux	VERB
eurjchem-976	301	98	82	82	NUM
eurjchem-976	301	99	ppa	ppa	PROPN
eurjchem-976	301	100	,	,	PUNCT
eurjchem-976	301	101	2h	2h	NUM
eurjchem-976	301	102	,	,	PUNCT
eurjchem-976	301	103	190‐200	190‐200	NUM
eurjchem-976	301	104	°	°	SYM
eurjchem-976	301	105	c	c	PROPN
eurjchem-976	301	106	79	79	NUM
eurjchem-976	301	107	5	5	NUM
eurjchem-976	301	108	alcl3	alcl3	NOUN
eurjchem-976	301	109	/	/	SYM
eurjchem-976	301	110	ch3no2	ch3no2	PROPN
eurjchem-976	301	111	,	,	PUNCT
eurjchem-976	301	112	dcm	dcm	PROPN
eurjchem-976	301	113	,	,	PUNCT
eurjchem-976	301	114	4	4	NUM
eurjchem-976	301	115	h	h	NOUN
eurjchem-976	301	116	,	,	PUNCT
eurjchem-976	301	117	reflux	reflux	NOUN
eurjchem-976	301	118	88	88	NUM
eurjchem-976	301	119	p2o5	p2o5	NOUN
eurjchem-976	301	120	,	,	PUNCT
eurjchem-976	301	121	toluene	toluene	NOUN
eurjchem-976	301	122	,	,	PUNCT
eurjchem-976	301	123	4	4	NUM
eurjchem-976	301	124	h	h	NOUN
eurjchem-976	301	125	,	,	PUNCT
eurjchem-976	301	126	reflux	reflux	VERB
eurjchem-976	302	1	81	81	NUM
eurjchem-976	302	2	ppa	ppa	PROPN
eurjchem-976	302	3	,	,	PUNCT
eurjchem-976	302	4	2	2	NUM
eurjchem-976	302	5	h	h	NOUN
eurjchem-976	302	6	,	,	PUNCT
eurjchem-976	302	7	200‐210	200‐210	PROPN
eurjchem-976	302	8	°	°	PROPN
eurjchem-976	302	9	c	c	PROPN
eurjchem-976	302	10	80	80	NUM
eurjchem-976	302	11	ir	ir	NOUN
eurjchem-976	302	12	(	(	PUNCT
eurjchem-976	302	13	film	film	NOUN
eurjchem-976	302	14	,	,	PUNCT
eurjchem-976	302	15	ν	ν	NOUN
eurjchem-976	302	16	,	,	PUNCT
eurjchem-976	302	17	cm‐1	cm‐1	PROPN
eurjchem-976	302	18	):	):	PUNCT
eurjchem-976	302	19	3090	3090	NUM
eurjchem-976	302	20	(	(	PUNCT
eurjchem-976	302	21	ch	ch	NOUN
eurjchem-976	302	22	)	)	PUNCT
eurjchem-976	302	23	(	(	PUNCT
eurjchem-976	302	24	aromatic	aromatic	NOUN
eurjchem-976	302	25	)	)	PUNCT
eurjchem-976	302	26	,	,	PUNCT
eurjchem-976	302	27	2980	2980	NUM
eurjchem-976	302	28	(	(	PUNCT
eurjchem-976	302	29	ch	ch	NOUN
eurjchem-976	302	30	)	)	PUNCT
eurjchem-976	302	31	(	(	PUNCT
eurjchem-976	302	32	alkyl	alkyl	NOUN
eurjchem-976	302	33	)	)	PUNCT
eurjchem-976	302	34	,	,	PUNCT
eurjchem-976	302	35	1604	1604	NUM
eurjchem-976	302	36	,	,	PUNCT
eurjchem-976	302	37	1485	1485	NUM
eurjchem-976	302	38	,	,	PUNCT
eurjchem-976	302	39	1465	1465	NUM
eurjchem-976	302	40	,	,	PUNCT
eurjchem-976	302	41	1442	1442	NUM
eurjchem-976	302	42	(	(	PUNCT
eurjchem-976	302	43	c	c	NOUN
eurjchem-976	302	44	=	=	SYM
eurjchem-976	302	45	c	c	NOUN
eurjchem-976	302	46	)	)	PUNCT
eurjchem-976	302	47	(	(	PUNCT
eurjchem-976	302	48	aromatic	aromatic	NOUN
eurjchem-976	302	49	)	)	PUNCT
eurjchem-976	302	50	,	,	PUNCT
eurjchem-976	302	51	1350	1350	NUM
eurjchem-976	302	52	,	,	PUNCT
eurjchem-976	302	53	695	695	NUM
eurjchem-976	302	54	.	.	PUNCT
eurjchem-976	302	55	1h	1h	NUM
eurjchem-976	302	56	nmr	nmr	NOUN
eurjchem-976	302	57	(	(	PUNCT
eurjchem-976	302	58	400	400	NUM
eurjchem-976	302	59	mhz	mhz	NOUN
eurjchem-976	302	60	,	,	PUNCT
eurjchem-976	302	61	cdcl3	cdcl3	PROPN
eurjchem-976	302	62	,	,	PUNCT
eurjchem-976	302	63	δ	δ	PROPN
eurjchem-976	302	64	,	,	PUNCT
eurjchem-976	302	65	ppm	ppm	NOUN
eurjchem-976	302	66	):	):	PUNCT
eurjchem-976	302	67	1.27	1.27	NUM
eurjchem-976	302	68	(	(	PUNCT
eurjchem-976	302	69	s	s	PROPN
eurjchem-976	302	70	,	,	PUNCT
eurjchem-976	302	71	6h	6h	NUM
eurjchem-976	302	72	,	,	PUNCT
eurjchem-976	302	73	2ch3	2ch3	NUM
eurjchem-976	302	74	)	)	PUNCT
eurjchem-976	302	75	,	,	PUNCT
eurjchem-976	302	76	1.75	1.75	NUM
eurjchem-976	302	77	(	(	PUNCT
eurjchem-976	302	78	t	t	PROPN
eurjchem-976	302	79	,	,	PUNCT
eurjchem-976	302	80	2h	2h	NUM
eurjchem-976	302	81	,	,	PUNCT
eurjchem-976	302	82	j	j	PROPN
eurjchem-976	302	83	=	=	SYM
eurjchem-976	302	84	6.2	6.2	NUM
eurjchem-976	302	85	hz	hz	NOUN
eurjchem-976	302	86	,	,	PUNCT
eurjchem-976	302	87	ch2	ch2	PROPN
eurjchem-976	302	88	)	)	PUNCT
eurjchem-976	302	89	,	,	PUNCT
eurjchem-976	302	90	2.64	2.64	NUM
eurjchem-976	302	91	(	(	PUNCT
eurjchem-976	302	92	t	t	PROPN
eurjchem-976	302	93	,	,	PUNCT
eurjchem-976	302	94	2h	2h	NUM
eurjchem-976	302	95	,	,	PUNCT
eurjchem-976	302	96	j	j	PROPN
eurjchem-976	302	97	=	=	SYM
eurjchem-976	302	98	6.2	6.2	NUM
eurjchem-976	302	99	hz	hz	NOUN
eurjchem-976	302	100	,	,	PUNCT
eurjchem-976	302	101	ch2	ch2	PROPN
eurjchem-976	302	102	)	)	PUNCT
eurjchem-976	302	103	,	,	PUNCT
eurjchem-976	302	104	7.21‐8.14	7.21‐8.14	NUM
eurjchem-976	302	105	(	(	PUNCT
eurjchem-976	302	106	9h	9h	NUM
eurjchem-976	302	107	,	,	PUNCT
eurjchem-976	302	108	m	m	PROPN
eurjchem-976	302	109	,	,	PUNCT
eurjchem-976	302	110	ar‐h	ar‐h	PROPN
eurjchem-976	302	111	)	)	PUNCT
eurjchem-976	302	112	.	.	PUNCT
eurjchem-976	303	1	13c	13c	NOUN
eurjchem-976	303	2	nmr	nmr	NOUN
eurjchem-976	303	3	(	(	PUNCT
eurjchem-976	303	4	100	100	NUM
eurjchem-976	303	5	mhz	mhz	NOUN
eurjchem-976	303	6	,	,	PUNCT
eurjchem-976	303	7	cdcl3	cdcl3	PROPN
eurjchem-976	303	8	,	,	PUNCT
eurjchem-976	303	9	δ	δ	PROPN
eurjchem-976	303	10	,	,	PUNCT
eurjchem-976	303	11	ppm	ppm	NUM
eurjchem-976	303	12	):	):	PUNCT
eurjchem-976	303	13	17.5	17.5	NUM
eurjchem-976	303	14	(	(	PUNCT
eurjchem-976	303	15	1c	1c	NOUN
eurjchem-976	303	16	,	,	PUNCT
eurjchem-976	303	17	‐ch2‐	‐ch2‐	PROPN
eurjchem-976	303	18	,	,	PUNCT
eurjchem-976	303	19	c‐4	c‐4	PROPN
eurjchem-976	303	20	)	)	PUNCT
eurjchem-976	303	21	,	,	PUNCT
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eurjchem-976	303	23	(	(	PUNCT
eurjchem-976	303	24	2c	2c	NOUN
eurjchem-976	303	25	,	,	PUNCT
eurjchem-976	303	26	‐c(ch3)2	‐c(ch3)2	ADJ
eurjchem-976	303	27	)	)	PUNCT
eurjchem-976	303	28	,	,	PUNCT
eurjchem-976	303	29	42.6	42.6	NUM
eurjchem-976	303	30	(	(	PUNCT
eurjchem-976	303	31	1c	1c	X
eurjchem-976	303	32	,	,	PUNCT
eurjchem-976	303	33	‐c(ch3)2	‐c(ch3)2	ADJ
eurjchem-976	303	34	,	,	PUNCT
eurjchem-976	303	35	c‐6	c‐6	NOUN
eurjchem-976	303	36	)	)	PUNCT
eurjchem-976	303	37	,	,	PUNCT
eurjchem-976	303	38	49.2	49.2	NUM
eurjchem-976	303	39	(	(	PUNCT
eurjchem-976	303	40	1c	1c	X
eurjchem-976	303	41	,	,	PUNCT
eurjchem-976	303	42	‐ch2‐	‐ch2‐	NOUN
eurjchem-976	303	43	,	,	PUNCT
eurjchem-976	303	44	c‐5	c‐5	NOUN
eurjchem-976	303	45	)	)	PUNCT
eurjchem-976	303	46	,	,	PUNCT
eurjchem-976	303	47	119.3	119.3	NUM
eurjchem-976	303	48	(	(	PUNCT
eurjchem-976	303	49	1c	1c	X
eurjchem-976	303	50	,	,	PUNCT
eurjchem-976	303	51	c‐3a	c‐3a	PROPN
eurjchem-976	303	52	)	)	PUNCT
eurjchem-976	303	53	,	,	PUNCT
eurjchem-976	303	54	122.4	122.4	NUM
eurjchem-976	303	55	(	(	PUNCT
eurjchem-976	303	56	2c	2c	NUM
eurjchem-976	303	57	,	,	PUNCT
eurjchem-976	303	58	ar	ar	PROPN
eurjchem-976	303	59	.	.	PROPN
eurjchem-976	303	60	,	,	PUNCT
eurjchem-976	303	61	c‐2	c‐2	NOUN
eurjchem-976	303	62	'	'	PUNCT
eurjchem-976	303	63	,	,	PUNCT
eurjchem-976	303	64	c‐6	c‐6	NOUN
eurjchem-976	303	65	'	'	PUNCT
eurjchem-976	303	66	)	)	PUNCT
eurjchem-976	303	67	,	,	PUNCT
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eurjchem-976	303	70	1c	1c	NOUN
eurjchem-976	303	71	,	,	PUNCT
eurjchem-976	303	72	ar	ar	PROPN
eurjchem-976	303	73	.	.	PROPN
eurjchem-976	303	74	,	,	PUNCT
eurjchem-976	303	75	c‐7	c‐7	PROPN
eurjchem-976	303	76	)	)	PUNCT
eurjchem-976	303	77	,	,	PUNCT
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eurjchem-976	303	79	(	(	PUNCT
eurjchem-976	303	80	1c	1c	X
eurjchem-976	303	81	,	,	PUNCT
eurjchem-976	303	82	ar	ar	PROPN
eurjchem-976	303	83	.	.	PROPN
eurjchem-976	303	84	,	,	PUNCT
eurjchem-976	303	85	c‐10a	c‐10a	PROPN
eurjchem-976	303	86	)	)	PUNCT
eurjchem-976	303	87	,	,	PUNCT
eurjchem-976	303	88	126.2	126.2	NUM
eurjchem-976	303	89	(	(	PUNCT
eurjchem-976	303	90	1c	1c	NOUN
eurjchem-976	303	91	,	,	PUNCT
eurjchem-976	303	92	ar	ar	PROPN
eurjchem-976	303	93	.	.	PROPN
eurjchem-976	303	94	,	,	PUNCT
eurjchem-976	303	95	c‐9	c‐9	PROPN
eurjchem-976	303	96	)	)	PUNCT
eurjchem-976	303	97	,	,	PUNCT
eurjchem-976	303	98	126.8	126.8	NUM
eurjchem-976	303	99	(	(	PUNCT
eurjchem-976	303	100	1c	1c	NOUN
eurjchem-976	303	101	,	,	PUNCT
eurjchem-976	303	102	ar	ar	PROPN
eurjchem-976	303	103	.	.	PROPN
eurjchem-976	303	104	,	,	PUNCT
eurjchem-976	303	105	c‐4	c‐4	PROPN
eurjchem-976	303	106	'	'	PUNCT
eurjchem-976	303	107	)	)	PUNCT
eurjchem-976	303	108	,	,	PUNCT
eurjchem-976	303	109	127.4	127.4	NUM
eurjchem-976	303	110	(	(	PUNCT
eurjchem-976	303	111	1c	1c	X
eurjchem-976	303	112	,	,	PUNCT
eurjchem-976	303	113	n‐c(cl)=	n‐c(cl)=	NOUN
eurjchem-976	303	114	,	,	PUNCT
eurjchem-976	303	115	c‐3	c‐3	PROPN
eurjchem-976	303	116	)	)	PUNCT
eurjchem-976	303	117	,	,	PUNCT
eurjchem-976	303	118	127.8	127.8	NUM
eurjchem-976	303	119	(	(	PUNCT
eurjchem-976	303	120	1c	1c	X
eurjchem-976	303	121	,	,	PUNCT
eurjchem-976	303	122	ar	ar	PROPN
eurjchem-976	303	123	.	.	PROPN
eurjchem-976	303	124	,	,	PUNCT
eurjchem-976	303	125	c‐10	c‐10	NOUN
eurjchem-976	303	126	)	)	PUNCT
eurjchem-976	303	127	,	,	PUNCT
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eurjchem-976	303	129	(	(	PUNCT
eurjchem-976	303	130	1c	1c	NOUN
eurjchem-976	303	131	,	,	PUNCT
eurjchem-976	303	132	ar	ar	PROPN
eurjchem-976	303	133	.	.	PROPN
eurjchem-976	303	134	,	,	PUNCT
eurjchem-976	303	135	c‐	c‐	NOUN
eurjchem-976	303	136	8)	8)	NUM
eurjchem-976	303	137	,	,	PUNCT
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eurjchem-976	303	139	(	(	PUNCT
eurjchem-976	303	140	2c	2c	NUM
eurjchem-976	303	141	,	,	PUNCT
eurjchem-976	303	142	ar	ar	PROPN
eurjchem-976	303	143	.	.	PROPN
eurjchem-976	303	144	,	,	PUNCT
eurjchem-976	303	145	c‐3	c‐3	PROPN
eurjchem-976	303	146	'	'	PUNCT
eurjchem-976	303	147	,	,	PUNCT
eurjchem-976	303	148	c‐5	c‐5	NOUN
eurjchem-976	303	149	'	'	PUNCT
eurjchem-976	303	150	)	)	PUNCT
eurjchem-976	303	151	,	,	PUNCT
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eurjchem-976	303	153	(	(	PUNCT
eurjchem-976	303	154	1c	1c	NOUN
eurjchem-976	303	155	,	,	PUNCT
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eurjchem-976	303	157	.	.	PROPN
eurjchem-976	303	158	,	,	PUNCT
eurjchem-976	303	159	c‐1	c‐1	NOUN
eurjchem-976	303	160	'	'	PUNCT
eurjchem-976	303	161	)	)	PUNCT
eurjchem-976	303	162	,	,	PUNCT
eurjchem-976	303	163	149.1	149.1	NUM
eurjchem-976	303	164	(	(	PUNCT
eurjchem-976	303	165	1c	1c	X
eurjchem-976	303	166	,	,	PUNCT
eurjchem-976	303	167	ar	ar	PROPN
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eurjchem-976	303	172	,	,	PUNCT
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eurjchem-976	305	5	,	,	PUNCT
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eurjchem-976	305	9	,	,	PUNCT
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eurjchem-976	305	18	c	c	X
eurjchem-976	305	19	,	,	PUNCT
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eurjchem-976	305	23	,	,	PUNCT
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eurjchem-976	305	27	,	,	PUNCT
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eurjchem-976	306	5	3b	3b	NUM
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eurjchem-976	308	7	.	.	PUNCT
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eurjchem-976	309	2	(	(	PUNCT
eurjchem-976	309	3	kbr	kbr	PROPN
eurjchem-976	309	4	,	,	PUNCT
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eurjchem-976	309	8	):	):	PUNCT
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eurjchem-976	309	16	,	,	PUNCT
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eurjchem-976	309	18	(	(	PUNCT
eurjchem-976	309	19	ch	ch	NOUN
eurjchem-976	309	20	)	)	PUNCT
eurjchem-976	309	21	(	(	PUNCT
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eurjchem-976	309	23	)	)	PUNCT
eurjchem-976	309	24	,	,	PUNCT
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eurjchem-976	309	30	,	,	PUNCT
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eurjchem-976	309	33	c	c	NOUN
eurjchem-976	309	34	=	=	SYM
eurjchem-976	309	35	c	c	NOUN
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eurjchem-976	309	37	(	(	PUNCT
eurjchem-976	309	38	aromatic	aromatic	NOUN
eurjchem-976	309	39	)	)	PUNCT
eurjchem-976	309	40	,	,	PUNCT
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eurjchem-976	309	42	,	,	PUNCT
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eurjchem-976	309	44	,	,	PUNCT
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eurjchem-976	309	46	,	,	PUNCT
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eurjchem-976	310	1	1h	1h	NUM
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eurjchem-976	310	3	(	(	PUNCT
eurjchem-976	310	4	400	400	NUM
eurjchem-976	310	5	mhz	mhz	NOUN
eurjchem-976	310	6	,	,	PUNCT
eurjchem-976	310	7	cdcl3	cdcl3	PROPN
eurjchem-976	310	8	,	,	PUNCT
eurjchem-976	310	9	δ	δ	PROPN
eurjchem-976	310	10	,	,	PUNCT
eurjchem-976	310	11	ppm	ppm	NOUN
eurjchem-976	310	12	):	):	PUNCT
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eurjchem-976	310	14	(	(	PUNCT
eurjchem-976	310	15	d	d	PROPN
eurjchem-976	310	16	,	,	PUNCT
eurjchem-976	310	17	3h	3h	NUM
eurjchem-976	310	18	,	,	PUNCT
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eurjchem-976	311	1	=	=	SYM
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eurjchem-976	311	4	,	,	PUNCT
eurjchem-976	311	5	ch3	ch3	PROPN
eurjchem-976	311	6	)	)	PUNCT
eurjchem-976	311	7	,	,	PUNCT
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eurjchem-976	311	9	(	(	PUNCT
eurjchem-976	311	10	s	s	PROPN
eurjchem-976	311	11	,	,	PUNCT
eurjchem-976	311	12	6h	6h	NUM
eurjchem-976	311	13	,	,	PUNCT
eurjchem-976	311	14	2ch3	2ch3	NUM
eurjchem-976	311	15	)	)	PUNCT
eurjchem-976	311	16	,	,	PUNCT
eurjchem-976	311	17	2.33	2.33	NUM
eurjchem-976	311	18	(	(	PUNCT
eurjchem-976	311	19	dd	dd	NOUN
eurjchem-976	311	20	,	,	PUNCT
eurjchem-976	311	21	ha	ha	INTJ
eurjchem-976	311	22	,	,	PUNCT
eurjchem-976	311	23	j	j	PROPN
eurjchem-976	312	1	=	=	PROPN
eurjchem-976	312	2	16.3	16.3	NUM
eurjchem-976	312	3	hz	hz	NOUN
eurjchem-976	312	4	,	,	PUNCT
eurjchem-976	312	5	ch2	ch2	PROPN
eurjchem-976	312	6	)	)	PUNCT
eurjchem-976	312	7	,	,	PUNCT
eurjchem-976	312	8	2.42	2.42	NUM
eurjchem-976	312	9	(	(	PUNCT
eurjchem-976	312	10	p	p	X
eurjchem-976	312	11	,	,	PUNCT
eurjchem-976	312	12	1h	1h	NUM
eurjchem-976	312	13	,	,	PUNCT
eurjchem-976	312	14	j	j	PROPN
eurjchem-976	313	1	=	=	SYM
eurjchem-976	313	2	9.3	9.3	NUM
eurjchem-976	313	3	hz	hz	VERB
eurjchem-976	313	4	,	,	PUNCT
eurjchem-976	313	5	‐ch	‐ch	NOUN
eurjchem-976	313	6	)	)	PUNCT
eurjchem-976	313	7	,	,	PUNCT
eurjchem-976	313	8	2.64	2.64	NUM
eurjchem-976	313	9	(	(	PUNCT
eurjchem-976	313	10	app.t	app.t	PROPN
eurjchem-976	313	11	,	,	PUNCT
eurjchem-976	313	12	hb	hb	PROPN
eurjchem-976	313	13	,	,	PUNCT
eurjchem-976	313	14	j	j	PROPN
eurjchem-976	314	1	=	=	PROPN
eurjchem-976	314	2	16.3	16.3	NUM
eurjchem-976	314	3	hz	hz	NOUN
eurjchem-976	314	4	,	,	PUNCT
eurjchem-976	314	5	ch2	ch2	PROPN
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eurjchem-976	314	7	,	,	PUNCT
eurjchem-976	314	8	7.11‐8.25	7.11‐8.25	NUM
eurjchem-976	314	9	(	(	PUNCT
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eurjchem-976	314	11	,	,	PUNCT
eurjchem-976	314	12	9h	9h	NUM
eurjchem-976	314	13	,	,	PUNCT
eurjchem-976	314	14	ar‐h	ar‐h	NOUN
eurjchem-976	314	15	)	)	PUNCT
eurjchem-976	314	16	.	.	PUNCT
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eurjchem-976	315	2	nmr	nmr	NOUN
eurjchem-976	315	3	(	(	PUNCT
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eurjchem-976	315	6	,	,	PUNCT
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eurjchem-976	315	8	,	,	PUNCT
eurjchem-976	315	9	δ	δ	PROPN
eurjchem-976	315	10	,	,	PUNCT
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eurjchem-976	315	14	(	(	PUNCT
eurjchem-976	315	15	1c	1c	NOUN
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eurjchem-976	315	19	,	,	PUNCT
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eurjchem-976	315	21	(	(	PUNCT
eurjchem-976	315	22	2c	2c	NOUN
eurjchem-976	315	23	,	,	PUNCT
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eurjchem-976	315	25	)	)	PUNCT
eurjchem-976	315	26	,	,	PUNCT
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eurjchem-976	315	29	1c	1c	NOUN
eurjchem-976	315	30	,	,	PUNCT
eurjchem-976	315	31	‐ch2‐	‐ch2‐	PROPN
eurjchem-976	315	32	,	,	PUNCT
eurjchem-976	315	33	c‐4	c‐4	PROPN
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eurjchem-976	315	35	,	,	PUNCT
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eurjchem-976	315	37	(	(	PUNCT
eurjchem-976	315	38	1c	1c	NOUN
eurjchem-976	315	39	,	,	PUNCT
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eurjchem-976	315	41	,	,	PUNCT
eurjchem-976	315	42	c‐6	c‐6	NOUN
eurjchem-976	315	43	)	)	PUNCT
eurjchem-976	315	44	,	,	PUNCT
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eurjchem-976	315	47	1c	1c	NOUN
eurjchem-976	315	48	,	,	PUNCT
eurjchem-976	315	49	‐chch3	‐chch3	ADJ
eurjchem-976	315	50	,	,	PUNCT
eurjchem-976	315	51	c‐5	c‐5	NOUN
eurjchem-976	315	52	)	)	PUNCT
eurjchem-976	315	53	,	,	PUNCT
eurjchem-976	315	54	119.2	119.2	NUM
eurjchem-976	315	55	(	(	PUNCT
eurjchem-976	315	56	1c	1c	X
eurjchem-976	315	57	,	,	PUNCT
eurjchem-976	315	58	c‐3a	c‐3a	PROPN
eurjchem-976	315	59	)	)	PUNCT
eurjchem-976	315	60	,	,	PUNCT
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eurjchem-976	315	62	(	(	PUNCT
eurjchem-976	315	63	2c	2c	NUM
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eurjchem-976	315	67	,	,	PUNCT
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eurjchem-976	315	70	,	,	PUNCT
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eurjchem-976	315	72	'	'	PUNCT
eurjchem-976	315	73	)	)	PUNCT
eurjchem-976	315	74	,	,	PUNCT
eurjchem-976	315	75	125.2	125.2	NUM
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eurjchem-976	315	77	1c	1c	NOUN
eurjchem-976	315	78	,	,	PUNCT
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eurjchem-976	315	84	,	,	PUNCT
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eurjchem-976	315	87	1c	1c	NOUN
eurjchem-976	315	88	,	,	PUNCT
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eurjchem-976	315	90	.	.	PROPN
eurjchem-976	315	91	,	,	PUNCT
eurjchem-976	315	92	c‐	c‐	NOUN
eurjchem-976	315	93	10a	10a	NOUN
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eurjchem-976	315	95	,	,	PUNCT
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eurjchem-976	315	98	2c	2c	NUM
eurjchem-976	315	99	,	,	PUNCT
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eurjchem-976	315	102	,	,	PUNCT
eurjchem-976	315	103	c‐4	c‐4	PROPN
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eurjchem-976	315	106	c‐9	c‐9	VERB
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eurjchem-976	315	108	,	,	PUNCT
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eurjchem-976	315	111	1c	1c	X
eurjchem-976	315	112	,	,	PUNCT
eurjchem-976	315	113	n‐c(cl)=	n‐c(cl)=	NOUN
eurjchem-976	315	114	,	,	PUNCT
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eurjchem-976	315	117	,	,	PUNCT
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eurjchem-976	315	120	1c	1c	NUM
eurjchem-976	315	121	,	,	PUNCT
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eurjchem-976	315	124	,	,	PUNCT
eurjchem-976	315	125	c‐10	c‐10	NOUN
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eurjchem-976	315	127	,	,	PUNCT
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eurjchem-976	315	129	(	(	PUNCT
eurjchem-976	315	130	1c	1c	X
eurjchem-976	315	131	,	,	PUNCT
eurjchem-976	315	132	ar	ar	PROPN
eurjchem-976	315	133	.	.	PROPN
eurjchem-976	315	134	,	,	PUNCT
eurjchem-976	315	135	c‐8	c‐8	PROPN
eurjchem-976	315	136	)	)	PUNCT
eurjchem-976	315	137	,	,	PUNCT
eurjchem-976	315	138	129.5	129.5	NUM
eurjchem-976	315	139	(	(	PUNCT
eurjchem-976	315	140	2c	2c	NUM
eurjchem-976	315	141	,	,	PUNCT
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eurjchem-976	315	143	.	.	PROPN
eurjchem-976	315	144	,	,	PUNCT
eurjchem-976	315	145	c‐3	c‐3	PROPN
eurjchem-976	315	146	'	'	PUNCT
eurjchem-976	315	147	,	,	PUNCT
eurjchem-976	315	148	c‐5	c‐5	NOUN
eurjchem-976	315	149	'	'	PUNCT
eurjchem-976	315	150	)	)	PUNCT
eurjchem-976	315	151	,	,	PUNCT
eurjchem-976	315	152	142.7	142.7	NUM
eurjchem-976	315	153	(	(	PUNCT
eurjchem-976	315	154	1c	1c	NOUN
eurjchem-976	315	155	,	,	PUNCT
eurjchem-976	315	156	ar	ar	PROPN
eurjchem-976	315	157	.	.	PROPN
eurjchem-976	315	158	,	,	PUNCT
eurjchem-976	315	159	c‐1	c‐1	NOUN
eurjchem-976	315	160	'	'	PUNCT
eurjchem-976	315	161	)	)	PUNCT
eurjchem-976	315	162	,	,	PUNCT
eurjchem-976	315	163	151.4	151.4	NUM
eurjchem-976	315	164	(	(	PUNCT
eurjchem-976	315	165	1c	1c	NOUN
eurjchem-976	315	166	,	,	PUNCT
eurjchem-976	315	167	ar	ar	PROPN
eurjchem-976	315	168	.	.	PROPN
eurjchem-976	315	169	,	,	PUNCT
eurjchem-976	315	170	c‐6a	c‐6a	PROPN
eurjchem-976	315	171	)	)	PUNCT
eurjchem-976	315	172	,	,	PUNCT
eurjchem-976	315	173	157.4	157.4	NUM
eurjchem-976	315	174	(	(	PUNCT
eurjchem-976	315	175	1c	1c	NOUN
eurjchem-976	315	176	,	,	PUNCT
eurjchem-976	315	177	n	n	CCONJ
eurjchem-976	315	178	=	=	NOUN
eurjchem-976	315	179	c‐,c‐	c‐,c‐	NOUN
eurjchem-976	315	180	10b	10b	NOUN
eurjchem-976	315	181	)	)	PUNCT
eurjchem-976	315	182	.	.	PUNCT
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eurjchem-976	316	2	.	.	PUNCT
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eurjchem-976	316	4	.	.	PUNCT
eurjchem-976	317	1	for	for	ADP
eurjchem-976	317	2	c21h21cln2	c21h21cln2	VERB
eurjchem-976	317	3	:	:	PUNCT
eurjchem-976	317	4	c	c	X
eurjchem-976	317	5	,	,	PUNCT
eurjchem-976	317	6	74.88	74.88	NUM
eurjchem-976	317	7	;	;	PUNCT
eurjchem-976	317	8	h	h	NOUN
eurjchem-976	317	9	,	,	PUNCT
eurjchem-976	317	10	6.28	6.28	NUM
eurjchem-976	317	11	;	;	PUNCT
eurjchem-976	317	12	n	n	CCONJ
eurjchem-976	317	13	,	,	PUNCT
eurjchem-976	317	14	8.32	8.32	NUM
eurjchem-976	317	15	.	.	PUNCT
eurjchem-976	317	16	found	find	VERB
eurjchem-976	317	17	;	;	PUNCT
eurjchem-976	317	18	c	c	X
eurjchem-976	317	19	,	,	PUNCT
eurjchem-976	317	20	74.64	74.64	NUM
eurjchem-976	317	21	;	;	PUNCT
eurjchem-976	317	22	h	h	NOUN
eurjchem-976	317	23	,	,	PUNCT
eurjchem-976	317	24	6.40	6.40	NUM
eurjchem-976	317	25	;	;	PUNCT
eurjchem-976	317	26	n	n	CCONJ
eurjchem-976	317	27	,	,	PUNCT
eurjchem-976	317	28	8.52	8.52	NUM
eurjchem-976	317	29	%	%	NOUN
eurjchem-976	317	30	.	.	PUNCT
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eurjchem-976	318	2	(	(	PUNCT
eurjchem-976	318	3	1b	1b	NUM
eurjchem-976	318	4	):	):	PUNCT
eurjchem-976	318	5	color	color	NOUN
eurjchem-976	318	6	:	:	PUNCT
eurjchem-976	318	7	white	white	ADJ
eurjchem-976	318	8	crystals	crystal	NOUN
eurjchem-976	318	9	.	.	PUNCT
eurjchem-976	319	1	m.p	m.p	PROPN
eurjchem-976	319	2	.	.	PROPN
eurjchem-976	319	3	:	:	PUNCT
eurjchem-976	320	1	144	144	NUM
eurjchem-976	320	2	°	°	ADP
eurjchem-976	320	3	c	c	NOUN
eurjchem-976	320	4	(	(	PUNCT
eurjchem-976	320	5	ethanol	ethanol	NOUN
eurjchem-976	320	6	)	)	PUNCT
eurjchem-976	320	7	.	.	PUNCT
eurjchem-976	321	1	ir	ir	PROPN
eurjchem-976	321	2	(	(	PUNCT
eurjchem-976	321	3	kbr	kbr	PROPN
eurjchem-976	321	4	,	,	PUNCT
eurjchem-976	321	5	ν	ν	PROPN
eurjchem-976	321	6	,	,	PUNCT
eurjchem-976	321	7	cm‐1	cm‐1	PROPN
eurjchem-976	321	8	):	):	PUNCT
eurjchem-976	321	9	3032	3032	NUM
eurjchem-976	321	10	(	(	PUNCT
eurjchem-976	321	11	ch	ch	NOUN
eurjchem-976	321	12	)	)	PUNCT
eurjchem-976	321	13	(	(	PUNCT
eurjchem-976	321	14	aromatic	aromatic	NOUN
eurjchem-976	321	15	)	)	PUNCT
eurjchem-976	321	16	,	,	PUNCT
eurjchem-976	321	17	2963	2963	NUM
eurjchem-976	321	18	(	(	PUNCT
eurjchem-976	321	19	ch	ch	NOUN
eurjchem-976	321	20	)	)	PUNCT
eurjchem-976	321	21	(	(	PUNCT
eurjchem-976	321	22	alkyl	alkyl	NOUN
eurjchem-976	321	23	)	)	PUNCT
eurjchem-976	321	24	,	,	PUNCT
eurjchem-976	321	25	1687	1687	NUM
eurjchem-976	321	26	(	(	PUNCT
eurjchem-976	321	27	c	c	NOUN
eurjchem-976	321	28	=	=	NOUN
eurjchem-976	321	29	o	o	NOUN
eurjchem-976	321	30	)	)	PUNCT
eurjchem-976	321	31	(	(	PUNCT
eurjchem-976	321	32	ketone	ketone	NOUN
eurjchem-976	321	33	)	)	PUNCT
eurjchem-976	321	34	,	,	PUNCT
eurjchem-976	321	35	1590	1590	NUM
eurjchem-976	321	36	,	,	PUNCT
eurjchem-976	321	37	1485	1485	NUM
eurjchem-976	321	38	,	,	PUNCT
eurjchem-976	321	39	1455	1455	NUM
eurjchem-976	321	40	,	,	PUNCT
eurjchem-976	321	41	1430	1430	NUM
eurjchem-976	321	42	(	(	PUNCT
eurjchem-976	321	43	c	c	X
eurjchem-976	321	44	=	=	SYM
eurjchem-976	321	45	c	c	NOUN
eurjchem-976	321	46	)	)	PUNCT
eurjchem-976	321	47	(	(	PUNCT
eurjchem-976	321	48	aromatic	aromatic	NOUN
eurjchem-976	321	49	)	)	PUNCT
eurjchem-976	321	50	,	,	PUNCT
eurjchem-976	321	51	1385	1385	NUM
eurjchem-976	321	52	,	,	PUNCT
eurjchem-976	321	53	1260	1260	NUM
eurjchem-976	321	54	,	,	PUNCT
eurjchem-976	321	55	742	742	NUM
eurjchem-976	321	56	.	.	PUNCT
eurjchem-976	321	57	1h	1h	NUM
eurjchem-976	321	58	nmr	nmr	NOUN
eurjchem-976	321	59	(	(	PUNCT
eurjchem-976	321	60	400	400	NUM
eurjchem-976	321	61	mhz	mhz	NOUN
eurjchem-976	321	62	,	,	PUNCT
eurjchem-976	321	63	cdcl3	cdcl3	PROPN
eurjchem-976	321	64	,	,	PUNCT
eurjchem-976	321	65	δ	δ	PROPN
eurjchem-976	321	66	,	,	PUNCT
eurjchem-976	321	67	ppm	ppm	NUM
eurjchem-976	321	68	):	):	PUNCT
eurjchem-976	321	69	7.27‐8.34	7.27‐8.34	NUM
eurjchem-976	321	70	(	(	PUNCT
eurjchem-976	321	71	9h	9h	NUM
eurjchem-976	321	72	,	,	PUNCT
eurjchem-976	321	73	m	m	PROPN
eurjchem-976	321	74	,	,	PUNCT
eurjchem-976	321	75	ar‐h	ar‐h	PROPN
eurjchem-976	321	76	)	)	PUNCT
eurjchem-976	321	77	.	.	PUNCT
eurjchem-976	322	1	13c	13c	NOUN
eurjchem-976	322	2	nmr	nmr	NOUN
eurjchem-976	322	3	(	(	PUNCT
eurjchem-976	322	4	100	100	NUM
eurjchem-976	322	5	mhz	mhz	NOUN
eurjchem-976	322	6	,	,	PUNCT
eurjchem-976	322	7	cdcl3	cdcl3	PROPN
eurjchem-976	322	8	,	,	PUNCT
eurjchem-976	322	9	δ	δ	PROPN
eurjchem-976	322	10	,	,	PUNCT
eurjchem-976	322	11	ppm	ppm	NOUN
eurjchem-976	322	12	):	):	PUNCT
eurjchem-976	322	13	109.4	109.4	NUM
eurjchem-976	322	14	(	(	PUNCT
eurjchem-976	322	15	1c	1c	NOUN
eurjchem-976	322	16	,	,	PUNCT
eurjchem-976	322	17	c‐3a	c‐3a	PROPN
eurjchem-976	322	18	)	)	PUNCT
eurjchem-976	322	19	,	,	PUNCT
eurjchem-976	322	20	122.6	122.6	NUM
eurjchem-976	322	21	(	(	PUNCT
eurjchem-976	322	22	2c	2c	NUM
eurjchem-976	322	23	,	,	PUNCT
eurjchem-976	322	24	ar	ar	PROPN
eurjchem-976	322	25	.	.	PROPN
eurjchem-976	322	26	,	,	PUNCT
eurjchem-976	322	27	c‐2	c‐2	NOUN
eurjchem-976	322	28	'	'	PUNCT
eurjchem-976	322	29	,	,	PUNCT
eurjchem-976	322	30	c‐6	c‐6	NOUN
eurjchem-976	322	31	'	'	PUNCT
eurjchem-976	322	32	)	)	PUNCT
eurjchem-976	322	33	,	,	PUNCT
eurjchem-976	322	34	126.8	126.8	NUM
eurjchem-976	322	35	(	(	PUNCT
eurjchem-976	322	36	1c	1c	NOUN
eurjchem-976	322	37	,	,	PUNCT
eurjchem-976	322	38	ar	ar	PROPN
eurjchem-976	322	39	.	.	PROPN
eurjchem-976	322	40	,	,	PUNCT
eurjchem-976	322	41	c‐4	c‐4	PROPN
eurjchem-976	322	42	'	'	PUNCT
eurjchem-976	322	43	)	)	PUNCT
eurjchem-976	322	44	,	,	PUNCT
eurjchem-976	322	45	127.4	127.4	NUM
eurjchem-976	322	46	(	(	PUNCT
eurjchem-976	322	47	1c	1c	NOUN
eurjchem-976	322	48	,	,	PUNCT
eurjchem-976	322	49	ar	ar	PROPN
eurjchem-976	322	50	.	.	PROPN
eurjchem-976	322	51	,	,	PUNCT
eurjchem-976	322	52	c‐8	c‐8	PROPN
eurjchem-976	322	53	)	)	PUNCT
eurjchem-976	322	54	,	,	PUNCT
eurjchem-976	322	55	128.9	128.9	NUM
eurjchem-976	322	56	(	(	PUNCT
eurjchem-976	322	57	1c	1c	X
eurjchem-976	322	58	,	,	PUNCT
eurjchem-976	322	59	ar	ar	PROPN
eurjchem-976	322	60	.	.	PROPN
eurjchem-976	322	61	,	,	PUNCT
eurjchem-976	322	62	c‐6	c‐6	PROPN
eurjchem-976	322	63	)	)	PUNCT
eurjchem-976	322	64	,	,	PUNCT
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eurjchem-976	322	66	(	(	PUNCT
eurjchem-976	322	67	2c	2c	NUM
eurjchem-976	322	68	,	,	PUNCT
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eurjchem-976	322	71	,	,	PUNCT
eurjchem-976	322	72	c‐3	c‐3	PROPN
eurjchem-976	322	73	'	'	PUNCT
eurjchem-976	322	74	,	,	PUNCT
eurjchem-976	322	75	c‐5	c‐5	NOUN
eurjchem-976	322	76	'	'	PUNCT
eurjchem-976	322	77	)	)	PUNCT
eurjchem-976	322	78	,	,	PUNCT
eurjchem-976	322	79	130.6	130.6	NUM
eurjchem-976	322	80	(	(	PUNCT
eurjchem-976	322	81	1c	1c	NOUN
eurjchem-976	322	82	,	,	PUNCT
eurjchem-976	322	83	ar	ar	PROPN
eurjchem-976	322	84	.	.	PROPN
eurjchem-976	322	85	,	,	PUNCT
eurjchem-976	322	86	c‐5	c‐5	NOUN
eurjchem-976	322	87	)	)	PUNCT
eurjchem-976	322	88	,	,	PUNCT
eurjchem-976	322	89	131.6	131.6	NUM
eurjchem-976	322	90	(	(	PUNCT
eurjchem-976	322	91	1c	1c	X
eurjchem-976	322	92	,	,	PUNCT
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eurjchem-976	322	94	,	,	PUNCT
eurjchem-976	322	95	c‐3	c‐3	PROPN
eurjchem-976	322	96	)	)	PUNCT
eurjchem-976	322	97	,	,	PUNCT
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eurjchem-976	322	99	(	(	PUNCT
eurjchem-976	322	100	1c	1c	NUM
eurjchem-976	322	101	,	,	PUNCT
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eurjchem-976	322	103	.	.	PROPN
eurjchem-976	322	104	,	,	PUNCT
eurjchem-976	322	105	c‐7	c‐7	PROPN
eurjchem-976	322	106	)	)	PUNCT
eurjchem-976	322	107	,	,	PUNCT
eurjchem-976	322	108	137.2	137.2	NUM
eurjchem-976	322	109	(	(	PUNCT
eurjchem-976	322	110	1c	1c	NOUN
eurjchem-976	322	111	,	,	PUNCT
eurjchem-976	322	112	ar	ar	PROPN
eurjchem-976	322	113	.	.	PROPN
eurjchem-976	322	114	,	,	PUNCT
eurjchem-976	322	115	c‐4a	c‐4a	PROPN
eurjchem-976	322	116	)	)	PUNCT
eurjchem-976	322	117	.	.	PUNCT
eurjchem-976	323	1	142.7	142.7	NUM
eurjchem-976	323	2	(	(	PUNCT
eurjchem-976	323	3	1c	1c	NOUN
eurjchem-976	323	4	,	,	PUNCT
eurjchem-976	323	5	ar	ar	PROPN
eurjchem-976	323	6	.	.	PROPN
eurjchem-976	323	7	,	,	PUNCT
eurjchem-976	323	8	c‐1	c‐1	NOUN
eurjchem-976	323	9	'	'	PUNCT
eurjchem-976	323	10	)	)	PUNCT
eurjchem-976	323	11	,	,	PUNCT
eurjchem-976	323	12	145.2	145.2	NUM
eurjchem-976	323	13	(	(	PUNCT
eurjchem-976	323	14	1c	1c	X
eurjchem-976	323	15	,	,	PUNCT
eurjchem-976	323	16	ar	ar	PROPN
eurjchem-976	323	17	.	.	PROPN
eurjchem-976	323	18	,	,	PUNCT
eurjchem-976	323	19	c‐8a	c‐8a	PROPN
eurjchem-976	323	20	)	)	PUNCT
eurjchem-976	323	21	,	,	PUNCT
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eurjchem-976	323	23	(	(	PUNCT
eurjchem-976	323	24	1c	1c	NUM
eurjchem-976	323	25	,	,	PUNCT
eurjchem-976	323	26	n	n	CCONJ
eurjchem-976	323	27	=	=	NOUN
eurjchem-976	323	28	c‐	c‐	NOUN
eurjchem-976	323	29	,	,	PUNCT
eurjchem-976	323	30	c‐	c‐	NOUN
eurjchem-976	323	31	8b	8b	NUM
eurjchem-976	323	32	)	)	PUNCT
eurjchem-976	323	33	,	,	PUNCT
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eurjchem-976	323	35	(	(	PUNCT
eurjchem-976	323	36	1c	1c	NOUN
eurjchem-976	323	37	,	,	PUNCT
eurjchem-976	323	38	c	c	NOUN
eurjchem-976	323	39	=	=	SYM
eurjchem-976	323	40	o	o	NOUN
eurjchem-976	323	41	,	,	PUNCT
eurjchem-976	323	42	c‐4	c‐4	PROPN
eurjchem-976	323	43	)	)	PUNCT
eurjchem-976	323	44	.	.	PUNCT
eurjchem-976	324	1	anal	anal	PROPN
eurjchem-976	324	2	.	.	PUNCT
eurjchem-976	324	3	calcd	calcd	NOUN
eurjchem-976	324	4	.	.	PUNCT
eurjchem-976	325	1	for	for	ADP
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eurjchem-976	325	3	:	:	PUNCT
eurjchem-976	325	4	c	c	X
eurjchem-976	325	5	,	,	PUNCT
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eurjchem-976	325	7	;	;	PUNCT
eurjchem-976	325	8	h	h	NOUN
eurjchem-976	325	9	,	,	PUNCT
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eurjchem-976	325	11	;	;	PUNCT
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eurjchem-976	325	13	,	,	PUNCT
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eurjchem-976	325	15	.	.	PUNCT
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eurjchem-976	325	17	;	;	PUNCT
eurjchem-976	325	18	c	c	X
eurjchem-976	325	19	,	,	PUNCT
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eurjchem-976	325	21	;	;	PUNCT
eurjchem-976	325	22	h	h	NOUN
eurjchem-976	325	23	,	,	PUNCT
eurjchem-976	325	24	3.05	3.05	NUM
eurjchem-976	325	25	;	;	PUNCT
eurjchem-976	325	26	n	n	CCONJ
eurjchem-976	325	27	,	,	PUNCT
eurjchem-976	325	28	10.18	10.18	NUM
eurjchem-976	325	29	%	%	NOUN
eurjchem-976	325	30	.	.	PUNCT
eurjchem-976	326	1	3a,4‐dihydro‐2‐phenyl‐2h‐benzo[g]indazole‐3,5‐dione	3a,4‐dihydro‐2‐phenyl‐2h‐benzo[g]indazole‐3,5‐dione	NUM
eurjchem-976	326	2	(	(	PUNCT
eurjchem-976	326	3	2c	2c	NUM
eurjchem-976	326	4	):	):	PUNCT
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eurjchem-976	326	6	:	:	PUNCT
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eurjchem-976	326	9	.	.	PUNCT
eurjchem-976	327	1	m.p	m.p	PROPN
eurjchem-976	327	2	.	.	PROPN
eurjchem-976	327	3	:	:	PUNCT
eurjchem-976	328	1	126	126	NUM
eurjchem-976	328	2	°	°	NUM
eurjchem-976	328	3	c	c	NOUN
eurjchem-976	328	4	(	(	PUNCT
eurjchem-976	328	5	ethanol	ethanol	NOUN
eurjchem-976	328	6	)	)	PUNCT
eurjchem-976	328	7	.	.	PUNCT
eurjchem-976	329	1	ir	ir	PROPN
eurjchem-976	329	2	(	(	PUNCT
eurjchem-976	329	3	kbr	kbr	PROPN
eurjchem-976	329	4	,	,	PUNCT
eurjchem-976	329	5	ν	ν	PROPN
eurjchem-976	329	6	,	,	PUNCT
eurjchem-976	329	7	cm‐1	cm‐1	PROPN
eurjchem-976	329	8	):	):	PUNCT
eurjchem-976	329	9	3035	3035	NUM
eurjchem-976	329	10	(	(	PUNCT
eurjchem-976	329	11	ch	ch	NOUN
eurjchem-976	329	12	)	)	PUNCT
eurjchem-976	329	13	(	(	PUNCT
eurjchem-976	329	14	aromatic	aromatic	NOUN
eurjchem-976	329	15	)	)	PUNCT
eurjchem-976	329	16	,	,	PUNCT
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eurjchem-976	329	18	(	(	PUNCT
eurjchem-976	329	19	ch	ch	NOUN
eurjchem-976	329	20	)	)	PUNCT
eurjchem-976	329	21	(	(	PUNCT
eurjchem-976	329	22	alkyl	alkyl	NOUN
eurjchem-976	329	23	)	)	PUNCT
eurjchem-976	329	24	,	,	PUNCT
eurjchem-976	329	25	1693	1693	NUM
eurjchem-976	329	26	(	(	PUNCT
eurjchem-976	329	27	c	c	NOUN
eurjchem-976	329	28	=	=	NOUN
eurjchem-976	329	29	o	o	NOUN
eurjchem-976	329	30	)	)	PUNCT
eurjchem-976	329	31	(	(	PUNCT
eurjchem-976	329	32	ketone	ketone	NOUN
eurjchem-976	329	33	)	)	PUNCT
eurjchem-976	329	34	,	,	PUNCT
eurjchem-976	329	35	1655	1655	NUM
eurjchem-976	329	36	(	(	PUNCT
eurjchem-976	329	37	c	c	NOUN
eurjchem-976	329	38	=	=	NOUN
eurjchem-976	329	39	o	o	NOUN
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eurjchem-976	329	41	(	(	PUNCT
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eurjchem-976	329	43	)	)	PUNCT
eurjchem-976	329	44	,	,	PUNCT
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eurjchem-976	329	46	,	,	PUNCT
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eurjchem-976	329	48	,	,	PUNCT
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eurjchem-976	329	50	(	(	PUNCT
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eurjchem-976	329	52	=	=	SYM
eurjchem-976	329	53	c	c	NOUN
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eurjchem-976	329	55	(	(	PUNCT
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eurjchem-976	329	58	,	,	PUNCT
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eurjchem-976	330	1	1h	1h	NUM
eurjchem-976	330	2	nmr	nmr	NOUN
eurjchem-976	330	3	(	(	PUNCT
eurjchem-976	330	4	400	400	NUM
eurjchem-976	330	5	mhz	mhz	NOUN
eurjchem-976	330	6	,	,	PUNCT
eurjchem-976	330	7	cdcl3	cdcl3	PROPN
eurjchem-976	330	8	,	,	PUNCT
eurjchem-976	330	9	δ	δ	PROPN
eurjchem-976	330	10	,	,	PUNCT
eurjchem-976	330	11	ppm	ppm	NUM
eurjchem-976	330	12	):	):	PUNCT
eurjchem-976	330	13	2.71	2.71	NUM
eurjchem-976	330	14	(	(	PUNCT
eurjchem-976	330	15	dt	dt	PROPN
eurjchem-976	330	16	,	,	PUNCT
eurjchem-976	330	17	1	1	NUM
eurjchem-976	330	18	ha	ha	INTJ
eurjchem-976	330	19	,	,	PUNCT
eurjchem-976	330	20	j	j	PROPN
eurjchem-976	330	21	=	=	PROPN
eurjchem-976	330	22	14.2	14.2	NUM
eurjchem-976	330	23	hz	hz	NOUN
eurjchem-976	330	24	,	,	PUNCT
eurjchem-976	330	25	ch2	ch2	PROPN
eurjchem-976	330	26	)	)	PUNCT
eurjchem-976	330	27	,	,	PUNCT
eurjchem-976	330	28	2.84	2.84	NUM
eurjchem-976	330	29	(	(	PUNCT
eurjchem-976	330	30	dd	dd	PROPN
eurjchem-976	330	31	,	,	PUNCT
eurjchem-976	330	32	1h	1h	NUM
eurjchem-976	330	33	,	,	PUNCT
eurjchem-976	330	34	j	j	PROPN
eurjchem-976	330	35	=	=	PROPN
eurjchem-976	330	36	10.4	10.4	NUM
eurjchem-976	330	37	hz	hz	NOUN
eurjchem-976	330	38	,	,	PUNCT
eurjchem-976	330	39	ch	ch	NOUN
eurjchem-976	330	40	)	)	PUNCT
eurjchem-976	330	41	,	,	PUNCT
eurjchem-976	330	42	3.11	3.11	NUM
eurjchem-976	331	1	(	(	PUNCT
eurjchem-976	331	2	app	app	PROPN
eurjchem-976	331	3	.	.	PROPN
eurjchem-976	331	4	t	t	PROPN
eurjchem-976	331	5	,	,	PUNCT
eurjchem-976	331	6	1hb	1hb	NOUN
eurjchem-976	331	7	,	,	PUNCT
eurjchem-976	331	8	j	j	PROPN
eurjchem-976	331	9	=	=	PROPN
eurjchem-976	331	10	14.2	14.2	NUM
eurjchem-976	331	11	hz	hz	NOUN
eurjchem-976	331	12	,	,	PUNCT
eurjchem-976	331	13	ch2	ch2	PROPN
eurjchem-976	331	14	)	)	PUNCT
eurjchem-976	331	15	,	,	PUNCT
eurjchem-976	331	16	7.32‐8.30	7.32‐8.30	NUM
eurjchem-976	331	17	(	(	PUNCT
eurjchem-976	331	18	9h	9h	NUM
eurjchem-976	331	19	,	,	PUNCT
eurjchem-976	331	20	m	m	PROPN
eurjchem-976	331	21	,	,	PUNCT
eurjchem-976	331	22	ar‐h	ar‐h	PROPN
eurjchem-976	331	23	)	)	PUNCT
eurjchem-976	331	24	.	.	PUNCT
eurjchem-976	332	1	13c	13c	NOUN
eurjchem-976	332	2	nmr	nmr	NOUN
eurjchem-976	332	3	(	(	PUNCT
eurjchem-976	332	4	100	100	NUM
eurjchem-976	332	5	mhz	mhz	NOUN
eurjchem-976	332	6	,	,	PUNCT
eurjchem-976	332	7	cdcl3	cdcl3	PROPN
eurjchem-976	332	8	,	,	PUNCT
eurjchem-976	332	9	δ	δ	PROPN
eurjchem-976	332	10	,	,	PUNCT
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eurjchem-976	332	12	):	):	PUNCT
eurjchem-976	332	13	38.6	38.6	NUM
eurjchem-976	332	14	(	(	PUNCT
eurjchem-976	332	15	1c	1c	NOUN
eurjchem-976	332	16	,	,	PUNCT
eurjchem-976	332	17	‐ch2‐	‐ch2‐	PROPN
eurjchem-976	332	18	,	,	PUNCT
eurjchem-976	332	19	c‐4	c‐4	PROPN
eurjchem-976	332	20	)	)	PUNCT
eurjchem-976	332	21	,	,	PUNCT
eurjchem-976	332	22	42.3	42.3	NUM
eurjchem-976	332	23	(	(	PUNCT
eurjchem-976	332	24	1c	1c	NOUN
eurjchem-976	332	25	,	,	PUNCT
eurjchem-976	332	26	c‐3a	c‐3a	PROPN
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eurjchem-976	332	28	,	,	PUNCT
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eurjchem-976	332	30	(	(	PUNCT
eurjchem-976	332	31	2c	2c	NUM
eurjchem-976	332	32	,	,	PUNCT
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eurjchem-976	332	34	.	.	PROPN
eurjchem-976	332	35	,	,	PUNCT
eurjchem-976	332	36	c‐2	c‐2	NOUN
eurjchem-976	332	37	'	'	PUNCT
eurjchem-976	332	38	,	,	PUNCT
eurjchem-976	332	39	c‐6	c‐6	NOUN
eurjchem-976	332	40	'	'	PUNCT
eurjchem-976	332	41	)	)	PUNCT
eurjchem-976	332	42	,	,	PUNCT
eurjchem-976	332	43	126.4	126.4	NUM
eurjchem-976	332	44	(	(	PUNCT
eurjchem-976	332	45	1c	1c	NUM
eurjchem-976	332	46	,	,	PUNCT
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eurjchem-976	332	49	,	,	PUNCT
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eurjchem-976	332	51	'	'	PUNCT
eurjchem-976	332	52	)	)	PUNCT
eurjchem-976	332	53	,	,	PUNCT
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eurjchem-976	332	55	(	(	PUNCT
eurjchem-976	332	56	1c	1c	NOUN
eurjchem-976	332	57	,	,	PUNCT
eurjchem-976	332	58	ar	ar	PROPN
eurjchem-976	332	59	.	.	PROPN
eurjchem-976	332	60	,	,	PUNCT
eurjchem-976	332	61	c‐6	c‐6	PROPN
eurjchem-976	332	62	)	)	PUNCT
eurjchem-976	332	63	,	,	PUNCT
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eurjchem-976	332	65	(	(	PUNCT
eurjchem-976	332	66	2c	2c	NUM
eurjchem-976	332	67	,	,	PUNCT
eurjchem-976	332	68	ar	ar	PROPN
eurjchem-976	332	69	.	.	PROPN
eurjchem-976	332	70	,	,	PUNCT
eurjchem-976	332	71	c‐3	c‐3	PROPN
eurjchem-976	332	72	'	'	PUNCT
eurjchem-976	332	73	,	,	PUNCT
eurjchem-976	332	74	c‐5	c‐5	NOUN
eurjchem-976	332	75	'	'	PUNCT
eurjchem-976	332	76	)	)	PUNCT
eurjchem-976	332	77	,	,	PUNCT
eurjchem-976	332	78	130.4	130.4	NUM
eurjchem-976	332	79	(	(	PUNCT
eurjchem-976	332	80	1c	1c	X
eurjchem-976	332	81	,	,	PUNCT
eurjchem-976	332	82	ar	ar	PROPN
eurjchem-976	332	83	.	.	PROPN
eurjchem-976	332	84	,	,	PUNCT
eurjchem-976	332	85	c‐9	c‐9	PROPN
eurjchem-976	332	86	)	)	PUNCT
eurjchem-976	332	87	,	,	PUNCT
eurjchem-976	332	88	130.9	130.9	NUM
eurjchem-976	332	89	(	(	PUNCT
eurjchem-976	332	90	1c	1c	NOUN
eurjchem-976	332	91	,	,	PUNCT
eurjchem-976	332	92	ar	ar	PROPN
eurjchem-976	332	93	.	.	PROPN
eurjchem-976	332	94	,	,	PUNCT
eurjchem-976	332	95	c‐9a	c‐9a	PROPN
eurjchem-976	332	96	)	)	PUNCT
eurjchem-976	332	97	,	,	PUNCT
eurjchem-976	332	98	132.1	132.1	NUM
eurjchem-976	332	99	(	(	PUNCT
eurjchem-976	332	100	1c	1c	NOUN
eurjchem-976	332	101	,	,	PUNCT
eurjchem-976	332	102	ar	ar	PROPN
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eurjchem-976	332	104	,	,	PUNCT
eurjchem-976	332	105	c‐7	c‐7	PROPN
eurjchem-976	332	106	)	)	PUNCT
eurjchem-976	332	107	,	,	PUNCT
eurjchem-976	332	108	133.5	133.5	NUM
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eurjchem-976	332	110	1c	1c	NOUN
eurjchem-976	332	111	,	,	PUNCT
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eurjchem-976	332	114	,	,	PUNCT
eurjchem-976	332	115	c‐8	c‐8	PROPN
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eurjchem-976	332	117	,	,	PUNCT
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eurjchem-976	332	119	(	(	PUNCT
eurjchem-976	332	120	1c	1c	NUM
eurjchem-976	332	121	,	,	PUNCT
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eurjchem-976	332	123	.	.	PROPN
eurjchem-976	332	124	,	,	PUNCT
eurjchem-976	332	125	c‐5a	c‐5a	PROPN
eurjchem-976	332	126	)	)	PUNCT
eurjchem-976	332	127	,	,	PUNCT
eurjchem-976	332	128	145.4	145.4	NUM
eurjchem-976	332	129	(	(	PUNCT
eurjchem-976	332	130	1c	1c	NUM
eurjchem-976	332	131	,	,	PUNCT
eurjchem-976	332	132	ar	ar	PROPN
eurjchem-976	332	133	.	.	PROPN
eurjchem-976	332	134	,	,	PUNCT
eurjchem-976	332	135	c‐1	c‐1	NOUN
eurjchem-976	332	136	'	'	PUNCT
eurjchem-976	332	137	)	)	PUNCT
eurjchem-976	332	138	,	,	PUNCT
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eurjchem-976	332	140	(	(	PUNCT
eurjchem-976	332	141	1c	1c	NOUN
eurjchem-976	332	142	,	,	PUNCT
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eurjchem-976	332	144	=	=	SYM
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eurjchem-976	332	147	,	,	PUNCT
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eurjchem-976	332	149	(	(	PUNCT
eurjchem-976	332	150	1c	1c	NOUN
eurjchem-976	332	151	,	,	PUNCT
eurjchem-976	332	152	n‐c	n‐c	PROPN
eurjchem-976	332	153	=	=	SYM
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eurjchem-976	332	155	,	,	PUNCT
eurjchem-976	332	156	c‐	c‐	NOUN
eurjchem-976	332	157	3	3	NUM
eurjchem-976	332	158	)	)	PUNCT
eurjchem-976	332	159	,	,	PUNCT
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eurjchem-976	332	161	(	(	PUNCT
eurjchem-976	332	162	1c	1c	NOUN
eurjchem-976	332	163	,	,	PUNCT
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eurjchem-976	332	165	=	=	SYM
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eurjchem-976	332	167	,	,	PUNCT
eurjchem-976	332	168	c‐5	c‐5	NOUN
eurjchem-976	332	169	)	)	PUNCT
eurjchem-976	332	170	.	.	PUNCT
eurjchem-976	333	1	anal	anal	PROPN
eurjchem-976	333	2	.	.	PUNCT
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eurjchem-976	333	4	.	.	PUNCT
eurjchem-976	334	1	for	for	SCONJ
eurjchem-976	334	2	c17h12n2o2	c17h12n2o2	NOUN
eurjchem-976	334	3	:	:	PUNCT
eurjchem-976	334	4	c	c	X
eurjchem-976	334	5	,	,	PUNCT
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eurjchem-976	334	7	;	;	PUNCT
eurjchem-976	334	8	h	h	NOUN
eurjchem-976	334	9	,	,	PUNCT
eurjchem-976	334	10	4.38	4.38	NUM
eurjchem-976	334	11	;	;	PUNCT
eurjchem-976	334	12	n	n	CCONJ
eurjchem-976	334	13	,	,	PUNCT
eurjchem-976	334	14	10.14	10.14	NUM
eurjchem-976	334	15	.	.	PUNCT
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eurjchem-976	334	17	;	;	PUNCT
eurjchem-976	334	18	c	c	X
eurjchem-976	334	19	,	,	PUNCT
eurjchem-976	334	20	73.76	73.76	NUM
eurjchem-976	334	21	;	;	PUNCT
eurjchem-976	335	1	h	h	NOUN
eurjchem-976	335	2	,	,	PUNCT
eurjchem-976	335	3	4.49	4.49	NUM
eurjchem-976	335	4	;	;	PUNCT
eurjchem-976	335	5	n	n	CCONJ
eurjchem-976	335	6	,	,	PUNCT
eurjchem-976	335	7	10.22	10.22	NUM
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eurjchem-976	335	9	.	.	PUNCT
eurjchem-976	336	1	3a,4‐dihydro‐4‐methyl‐2‐phenyl‐2h‐benzo[g]indazole‐3,5‐	3a,4‐dihydro‐4‐methyl‐2‐phenyl‐2h‐benzo[g]indazole‐3,5‐	NUM
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eurjchem-976	336	3	(	(	PUNCT
eurjchem-976	336	4	2d	2d	NOUN
eurjchem-976	336	5	):	):	PUNCT
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eurjchem-976	336	7	:	:	PUNCT
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eurjchem-976	337	3	:	:	PUNCT
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eurjchem-976	338	2	°	°	NUM
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eurjchem-976	338	4	(	(	PUNCT
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eurjchem-976	339	2	(	(	PUNCT
eurjchem-976	339	3	kbr	kbr	PROPN
eurjchem-976	339	4	,	,	PUNCT
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eurjchem-976	339	6	,	,	PUNCT
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eurjchem-976	339	8	):	):	PUNCT
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eurjchem-976	339	10	(	(	PUNCT
eurjchem-976	339	11	ch	ch	NOUN
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eurjchem-976	339	13	(	(	PUNCT
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eurjchem-976	339	16	,	,	PUNCT
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eurjchem-976	339	18	(	(	PUNCT
eurjchem-976	339	19	ch	ch	NOUN
eurjchem-976	339	20	)	)	PUNCT
eurjchem-976	339	21	(	(	PUNCT
eurjchem-976	339	22	alkyl	alkyl	NOUN
eurjchem-976	339	23	)	)	PUNCT
eurjchem-976	339	24	,	,	PUNCT
eurjchem-976	339	25	1705	1705	NUM
eurjchem-976	339	26	(	(	PUNCT
eurjchem-976	339	27	c	c	NOUN
eurjchem-976	339	28	=	=	NOUN
eurjchem-976	339	29	o	o	NOUN
eurjchem-976	339	30	)	)	PUNCT
eurjchem-976	339	31	(	(	PUNCT
eurjchem-976	339	32	ketone	ketone	NOUN
eurjchem-976	339	33	)	)	PUNCT
eurjchem-976	339	34	,	,	PUNCT
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eurjchem-976	339	36	(	(	PUNCT
eurjchem-976	339	37	c	c	NOUN
eurjchem-976	339	38	=	=	NOUN
eurjchem-976	339	39	o	o	NOUN
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eurjchem-976	339	41	(	(	PUNCT
eurjchem-976	339	42	amide),1597	amide),1597	PROPN
eurjchem-976	339	43	,	,	PUNCT
eurjchem-976	339	44	1575	1575	NUM
eurjchem-976	339	45	,	,	PUNCT
eurjchem-976	339	46	1480	1480	NUM
eurjchem-976	339	47	,	,	PUNCT
eurjchem-976	339	48	1444	1444	NUM
eurjchem-976	339	49	(	(	PUNCT
eurjchem-976	339	50	c	c	NOUN
eurjchem-976	339	51	=	=	SYM
eurjchem-976	339	52	c	c	NOUN
eurjchem-976	339	53	)	)	PUNCT
eurjchem-976	339	54	(	(	PUNCT
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eurjchem-976	339	57	,	,	PUNCT
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eurjchem-976	339	59	,	,	PUNCT
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eurjchem-976	339	62	1h	1h	NUM
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eurjchem-976	339	64	(	(	PUNCT
eurjchem-976	339	65	400	400	NUM
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eurjchem-976	339	71	,	,	PUNCT
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eurjchem-976	339	73	):	):	PUNCT
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eurjchem-976	339	75	(	(	PUNCT
eurjchem-976	339	76	d	d	PROPN
eurjchem-976	339	77	,	,	PUNCT
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eurjchem-976	339	79	,	,	PUNCT
eurjchem-976	339	80	j	j	PROPN
eurjchem-976	339	81	=	=	SYM
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eurjchem-976	339	83	hz	hz	NOUN
eurjchem-976	339	84	,	,	PUNCT
eurjchem-976	339	85	ch3	ch3	PROPN
eurjchem-976	339	86	)	)	PUNCT
eurjchem-976	339	87	,	,	PUNCT
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eurjchem-976	339	89	(	(	PUNCT
eurjchem-976	339	90	d	d	PROPN
eurjchem-976	339	91	,	,	PUNCT
eurjchem-976	339	92	1h	1h	NUM
eurjchem-976	339	93	,	,	PUNCT
eurjchem-976	339	94	j	j	PROPN
eurjchem-976	339	95	=	=	PROPN
eurjchem-976	339	96	12.5	12.5	NUM
eurjchem-976	339	97	hz	hz	NOUN
eurjchem-976	339	98	,	,	PUNCT
eurjchem-976	339	99	ch	ch	NOUN
eurjchem-976	339	100	)	)	PUNCT
eurjchem-976	339	101	,	,	PUNCT
eurjchem-976	339	102	3.37	3.37	NUM
eurjchem-976	339	103	(	(	PUNCT
eurjchem-976	339	104	p,1h	p,1h	PROPN
eurjchem-976	339	105	,	,	PUNCT
eurjchem-976	339	106	j	j	PROPN
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eurjchem-976	348	20	=	=	SYM
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eurjchem-976	350	72	,	,	PUNCT
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eurjchem-976	350	75	1c	1c	NOUN
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eurjchem-976	350	82	,	,	PUNCT
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eurjchem-976	350	85	1c	1c	NOUN
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eurjchem-976	350	89	,	,	PUNCT
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eurjchem-976	350	92	,	,	PUNCT
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eurjchem-976	350	99	,	,	PUNCT
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eurjchem-976	350	102	,	,	PUNCT
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eurjchem-976	350	112	,	,	PUNCT
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eurjchem-976	350	116	,	,	PUNCT
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eurjchem-976	350	119	1c	1c	NUM
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eurjchem-976	350	123	,	,	PUNCT
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eurjchem-976	350	126	,	,	PUNCT
eurjchem-976	350	127	135.7	135.7	NUM
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eurjchem-976	350	129	1c	1c	NUM
eurjchem-976	350	130	,	,	PUNCT
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eurjchem-976	350	133	,	,	PUNCT
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eurjchem-976	350	139	1c	1c	NUM
eurjchem-976	350	140	,	,	PUNCT
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eurjchem-976	350	146	1c	1c	NOUN
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eurjchem-976	350	150	,	,	PUNCT
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eurjchem-976	350	152	'	'	PUNCT
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eurjchem-976	350	157	1c	1c	NOUN
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eurjchem-976	350	160	=	=	NOUN
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eurjchem-976	350	176	.	.	PUNCT
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eurjchem-976	352	10	4.24	4.24	NUM
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eurjchem-976	352	18	c	c	X
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eurjchem-976	352	22	h	h	NOUN
eurjchem-976	352	23	,	,	PUNCT
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eurjchem-976	352	26	n	n	CCONJ
eurjchem-976	352	27	,	,	PUNCT
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eurjchem-976	353	4	3d	3d	NOUN
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eurjchem-976	354	42	,	,	PUNCT
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eurjchem-976	357	9	1a	1a	X
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eurjchem-976	357	18	:	:	PUNCT
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eurjchem-976	359	43	c	c	NOUN
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eurjchem-976	361	9	.	.	NOUN
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eurjchem-976	361	17	=	=	SYM
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eurjchem-976	361	20	,	,	PUNCT
eurjchem-976	361	21	‐ch	‐ch	NOUN
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eurjchem-976	361	23	,	,	PUNCT
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eurjchem-976	361	25	(	(	PUNCT
eurjchem-976	361	26	m	m	PROPN
eurjchem-976	361	27	,	,	PUNCT
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eurjchem-976	361	29	,	,	PUNCT
eurjchem-976	361	30	ar‐h	ar‐h	NOUN
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eurjchem-976	361	32	.	.	PUNCT
eurjchem-976	362	1	13c	13c	NOUN
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eurjchem-976	362	3	(	(	PUNCT
eurjchem-976	362	4	100	100	NUM
eurjchem-976	362	5	mhz	mhz	NOUN
eurjchem-976	362	6	,	,	PUNCT
eurjchem-976	362	7	cdcl3	cdcl3	PROPN
eurjchem-976	362	8	,	,	PUNCT
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eurjchem-976	362	10	,	,	PUNCT
eurjchem-976	362	11	ppm	ppm	NUM
eurjchem-976	362	12	):	):	PUNCT
eurjchem-976	362	13	19.4	19.4	NUM
eurjchem-976	362	14	(	(	PUNCT
eurjchem-976	362	15	1c	1c	NOUN
eurjchem-976	362	16	,	,	PUNCT
eurjchem-976	362	17	‐chch3	‐chch3	ADJ
eurjchem-976	362	18	)	)	PUNCT
eurjchem-976	362	19	,	,	PUNCT
eurjchem-976	362	20	29.5	29.5	NUM
eurjchem-976	362	21	(	(	PUNCT
eurjchem-976	362	22	1c	1c	NOUN
eurjchem-976	362	23	,	,	PUNCT
eurjchem-976	362	24	‐ch2‐	‐ch2‐	PROPN
eurjchem-976	362	25	,	,	PUNCT
eurjchem-976	362	26	c‐4	c‐4	PROPN
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eurjchem-976	362	28	,	,	PUNCT
eurjchem-976	362	29	47.2	47.2	NUM
eurjchem-976	362	30	(	(	PUNCT
eurjchem-976	362	31	1c	1c	NOUN
eurjchem-976	362	32	,	,	PUNCT
eurjchem-976	362	33	‐chch3	‐chch3	ADJ
eurjchem-976	362	34	,	,	PUNCT
eurjchem-976	362	35	c‐5	c‐5	NOUN
eurjchem-976	362	36	)	)	PUNCT
eurjchem-976	362	37	,	,	PUNCT
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eurjchem-976	362	39	(	(	PUNCT
eurjchem-976	362	40	1c	1c	X
eurjchem-976	362	41	,	,	PUNCT
eurjchem-976	362	42	c‐3a	c‐3a	PROPN
eurjchem-976	362	43	)	)	PUNCT
eurjchem-976	362	44	,	,	PUNCT
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eurjchem-976	362	46	(	(	PUNCT
eurjchem-976	362	47	2c	2c	NUM
eurjchem-976	362	48	,	,	PUNCT
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eurjchem-976	362	51	,	,	PUNCT
eurjchem-976	362	52	c‐2	c‐2	NOUN
eurjchem-976	362	53	'	'	PUNCT
eurjchem-976	362	54	,	,	PUNCT
eurjchem-976	362	55	c‐6	c‐6	NOUN
eurjchem-976	362	56	'	'	PUNCT
eurjchem-976	362	57	)	)	PUNCT
eurjchem-976	362	58	,	,	PUNCT
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eurjchem-976	362	60	(	(	PUNCT
eurjchem-976	362	61	1c	1c	NOUN
eurjchem-976	362	62	,	,	PUNCT
eurjchem-976	362	63	ar	ar	PROPN
eurjchem-976	362	64	.	.	PROPN
eurjchem-976	362	65	,	,	PUNCT
eurjchem-976	362	66	c‐4	c‐4	PROPN
eurjchem-976	362	67	'	'	PUNCT
eurjchem-976	362	68	)	)	PUNCT
eurjchem-976	362	69	,	,	PUNCT
eurjchem-976	362	70	127.2	127.2	NUM
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eurjchem-976	362	72	1c	1c	X
eurjchem-976	362	73	,	,	PUNCT
eurjchem-976	362	74	n‐c(cl)=	n‐c(cl)=	NOUN
eurjchem-976	362	75	,	,	PUNCT
eurjchem-976	362	76	c‐3	c‐3	PROPN
eurjchem-976	362	77	)	)	PUNCT
eurjchem-976	362	78	,	,	PUNCT
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eurjchem-976	362	81	1c	1c	NOUN
eurjchem-976	362	82	,	,	PUNCT
eurjchem-976	362	83	ar	ar	PROPN
eurjchem-976	362	84	.	.	PROPN
eurjchem-976	362	85	,	,	PUNCT
eurjchem-976	362	86	c‐	c‐	NOUN
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eurjchem-976	362	89	,	,	PUNCT
eurjchem-976	362	90	128.9	128.9	NUM
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eurjchem-976	362	92	1c	1c	X
eurjchem-976	362	93	,	,	PUNCT
eurjchem-976	362	94	ar	ar	PROPN
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eurjchem-976	362	96	,	,	PUNCT
eurjchem-976	362	97	c‐8	c‐8	PROPN
eurjchem-976	362	98	)	)	PUNCT
eurjchem-976	362	99	,	,	PUNCT
eurjchem-976	362	100	129.2	129.2	NUM
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eurjchem-976	362	102	1c	1c	X
eurjchem-976	362	103	,	,	PUNCT
eurjchem-976	362	104	ar	ar	PROPN
eurjchem-976	362	105	.	.	PROPN
eurjchem-976	362	106	,	,	PUNCT
eurjchem-976	362	107	c‐7	c‐7	PROPN
eurjchem-976	362	108	)	)	PUNCT
eurjchem-976	362	109	,	,	PUNCT
eurjchem-976	362	110	130.3	130.3	NUM
eurjchem-976	362	111	(	(	PUNCT
eurjchem-976	362	112	2c	2c	NUM
eurjchem-976	362	113	,	,	PUNCT
eurjchem-976	362	114	ar	ar	PROPN
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eurjchem-976	362	116	,	,	PUNCT
eurjchem-976	362	117	c‐3	c‐3	PROPN
eurjchem-976	362	118	'	'	PUNCT
eurjchem-976	362	119	,	,	PUNCT
eurjchem-976	362	120	c‐5	c‐5	NOUN
eurjchem-976	362	121	'	'	PUNCT
eurjchem-976	362	122	)	)	PUNCT
eurjchem-976	362	123	,	,	PUNCT
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eurjchem-976	362	126	1c	1c	X
eurjchem-976	362	127	,	,	PUNCT
eurjchem-976	362	128	ar	ar	PROPN
eurjchem-976	362	129	.	.	PROPN
eurjchem-976	362	130	,	,	PUNCT
eurjchem-976	362	131	c‐10a	c‐10a	PROPN
eurjchem-976	362	132	)	)	PUNCT
eurjchem-976	362	133	,	,	PUNCT
eurjchem-976	362	134	134.7	134.7	NUM
eurjchem-976	362	135	(	(	PUNCT
eurjchem-976	362	136	1c	1c	NOUN
eurjchem-976	362	137	,	,	PUNCT
eurjchem-976	362	138	ar	ar	PROPN
eurjchem-976	362	139	.	.	PROPN
eurjchem-976	362	140	,	,	PUNCT
eurjchem-976	362	141	c‐9	c‐9	PROPN
eurjchem-976	362	142	)	)	PUNCT
eurjchem-976	362	143	,	,	PUNCT
eurjchem-976	362	144	138.9	138.9	NUM
eurjchem-976	362	145	(	(	PUNCT
eurjchem-976	362	146	1c	1c	X
eurjchem-976	362	147	,	,	PUNCT
eurjchem-976	362	148	ar	ar	PROPN
eurjchem-976	362	149	.	.	PROPN
eurjchem-976	362	150	,	,	PUNCT
eurjchem-976	362	151	c‐6a	c‐6a	PROPN
eurjchem-976	362	152	)	)	PUNCT
eurjchem-976	362	153	,	,	PUNCT
eurjchem-976	362	154	144.5	144.5	NUM
eurjchem-976	362	155	(	(	PUNCT
eurjchem-976	362	156	1c	1c	X
eurjchem-976	362	157	,	,	PUNCT
eurjchem-976	362	158	ar	ar	PROPN
eurjchem-976	362	159	.	.	PROPN
eurjchem-976	362	160	,	,	PUNCT
eurjchem-976	362	161	c‐1	c‐1	NOUN
eurjchem-976	362	162	'	'	PUNCT
eurjchem-976	362	163	)	)	PUNCT
eurjchem-976	362	164	,	,	PUNCT
eurjchem-976	362	165	157.3	157.3	NUM
eurjchem-976	362	166	(	(	PUNCT
eurjchem-976	362	167	1c	1c	NUM
eurjchem-976	362	168	,	,	PUNCT
eurjchem-976	362	169	n	n	CCONJ
eurjchem-976	362	170	=	=	NOUN
eurjchem-976	362	171	c‐	c‐	NOUN
eurjchem-976	362	172	,	,	PUNCT
eurjchem-976	362	173	c‐10b	c‐10b	NOUN
eurjchem-976	362	174	)	)	PUNCT
eurjchem-976	362	175	,	,	PUNCT
eurjchem-976	362	176	208.2	208.2	NUM
eurjchem-976	362	177	(	(	PUNCT
eurjchem-976	362	178	1c	1c	NOUN
eurjchem-976	362	179	,	,	PUNCT
eurjchem-976	362	180	c	c	NOUN
eurjchem-976	362	181	=	=	SYM
eurjchem-976	362	182	o	o	NOUN
eurjchem-976	362	183	,	,	PUNCT
eurjchem-976	362	184	c‐6	c‐6	NOUN
eurjchem-976	362	185	)	)	PUNCT
eurjchem-976	362	186	.	.	PUNCT
eurjchem-976	363	1	anal	anal	PROPN
eurjchem-976	363	2	.	.	PUNCT
eurjchem-976	363	3	calcd	calcd	NOUN
eurjchem-976	363	4	.	.	PUNCT
eurjchem-976	364	1	for	for	ADP
eurjchem-976	364	2	c19h15cln2o	c19h15cln2o	NOUN
eurjchem-976	364	3	:	:	PUNCT
eurjchem-976	364	4	c	c	X
eurjchem-976	364	5	,	,	PUNCT
eurjchem-976	364	6	70.70	70.70	NUM
eurjchem-976	364	7	;	;	PUNCT
eurjchem-976	364	8	h	h	NOUN
eurjchem-976	364	9	,	,	PUNCT
eurjchem-976	364	10	4.68	4.68	NUM
eurjchem-976	364	11	;	;	PUNCT
eurjchem-976	364	12	n	n	CCONJ
eurjchem-976	364	13	,	,	PUNCT
eurjchem-976	364	14	8.68	8.68	NUM
eurjchem-976	364	15	.	.	PUNCT
eurjchem-976	364	16	found	find	VERB
eurjchem-976	364	17	;	;	PUNCT
eurjchem-976	364	18	c	c	X
eurjchem-976	364	19	,	,	PUNCT
eurjchem-976	364	20	70.92	70.92	NUM
eurjchem-976	364	21	;	;	PUNCT
eurjchem-976	365	1	h	h	NOUN
eurjchem-976	365	2	,	,	PUNCT
eurjchem-976	365	3	4.45	4.45	NUM
eurjchem-976	365	4	;	;	PUNCT
eurjchem-976	365	5	n	n	CCONJ
eurjchem-976	365	6	,	,	PUNCT
eurjchem-976	365	7	8.52	8.52	NUM
eurjchem-976	365	8	%	%	NOUN
eurjchem-976	365	9	.	.	PUNCT
eurjchem-976	366	1	3	3	X
eurjchem-976	366	2	.	.	NOUN
eurjchem-976	366	3	results	result	NOUN
eurjchem-976	366	4	and	and	CCONJ
eurjchem-976	366	5	discussion	discussion	NOUN
eurjchem-976	366	6	we	we	PRON
eurjchem-976	366	7	first	first	ADV
eurjchem-976	366	8	attempted	attempt	VERB
eurjchem-976	366	9	to	to	PART
eurjchem-976	366	10	prepare	prepare	VERB
eurjchem-976	366	11	the	the	DET
eurjchem-976	366	12	precursors	precursor	NOUN
eurjchem-976	366	13	heteroaryl	heteroaryl	NOUN
eurjchem-976	366	14	acids	acid	NOUN
eurjchem-976	366	15	required	require	VERB
eurjchem-976	366	16	for	for	ADP
eurjchem-976	366	17	this	this	DET
eurjchem-976	366	18	work	work	NOUN
eurjchem-976	366	19	(	(	PUNCT
eurjchem-976	366	20	6	6	NUM
eurjchem-976	366	21	,	,	PUNCT
eurjchem-976	366	22	10a	10a	NUM
eurjchem-976	366	23	,	,	PUNCT
eurjchem-976	366	24	b	b	NOUN
eurjchem-976	366	25	and	and	CCONJ
eurjchem-976	366	26	14a	14a	NOUN
eurjchem-976	366	27	,	,	PUNCT
eurjchem-976	366	28	b	b	NOUN
eurjchem-976	366	29	)	)	PUNCT
eurjchem-976	366	30	which	which	PRON
eurjchem-976	366	31	are	be	AUX
eurjchem-976	366	32	easily	easily	ADV
eurjchem-976	366	33	obtained	obtain	VERB
eurjchem-976	366	34	via	via	ADP
eurjchem-976	366	35	three	three	NUM
eurjchem-976	366	36	different	different	ADJ
eurjchem-976	366	37	synthetic	synthetic	ADJ
eurjchem-976	366	38	routes	route	NOUN
eurjchem-976	366	39	starting	start	VERB
eurjchem-976	366	40	from	from	ADP
eurjchem-976	366	41	the	the	DET
eurjchem-976	366	42	easily	easily	ADV
eurjchem-976	366	43	prepared	prepare	VERB
eurjchem-976	366	44	1,3‐diphenyl‐1h‐pyrazol‐5(4h)‐one	1,3‐diphenyl‐1h‐pyrazol‐5(4h)‐one	NUM
eurjchem-976	366	45	(	(	PUNCT
eurjchem-976	366	46	4	4	NUM
eurjchem-976	366	47	)	)	PUNCT
eurjchem-976	367	1	[	[	X
eurjchem-976	367	2	56	56	NUM
eurjchem-976	367	3	]	]	PUNCT
eurjchem-976	367	4	as	as	SCONJ
eurjchem-976	367	5	formulated	formulate	VERB
eurjchem-976	367	6	in	in	ADP
eurjchem-976	367	7	scheme	scheme	NOUN
eurjchem-976	367	8	1	1	NUM
eurjchem-976	367	9	and	and	CCONJ
eurjchem-976	367	10	2	2	NUM
eurjchem-976	367	11	.	.	PUNCT
eurjchem-976	367	12	the	the	DET
eurjchem-976	367	13	first	first	ADJ
eurjchem-976	367	14	path	path	NOUN
eurjchem-976	367	15	comprised	comprise	VERB
eurjchem-976	367	16	the	the	DET
eurjchem-976	367	17	formation	formation	NOUN
eurjchem-976	367	18	of	of	ADP
eurjchem-976	367	19	5‐chloro‐1,3‐	5‐chloro‐1,3‐	PROPN
eurjchem-976	367	20	diphenyl‐1h‐pyrazole‐4‐carbaldehyde	diphenyl‐1h‐pyrazole‐4‐carbaldehyde	NOUN
eurjchem-976	367	21	(	(	PUNCT
eurjchem-976	367	22	5	5	NUM
eurjchem-976	367	23	)	)	PUNCT
eurjchem-976	367	24	following	follow	VERB
eurjchem-976	367	25	standard	standard	ADJ
eurjchem-976	367	26	literature	literature	NOUN
eurjchem-976	367	27	procedure	procedure	NOUN
eurjchem-976	367	28	by	by	ADP
eurjchem-976	367	29	chloroformylation	chloroformylation	NOUN
eurjchem-976	367	30	of	of	ADP
eurjchem-976	367	31	pyrazolone	pyrazolone	NOUN
eurjchem-976	367	32	4	4	NUM
eurjchem-976	367	33	under	under	ADP
eurjchem-976	367	34	vilsmeier	vilsmeier	ADJ
eurjchem-976	367	35	conditions	condition	NOUN
eurjchem-976	367	36	[	[	X
eurjchem-976	367	37	55	55	NUM
eurjchem-976	367	38	]	]	PUNCT
eurjchem-976	367	39	.	.	PUNCT
eurjchem-976	368	1	this	this	DET
eurjchem-976	368	2	aldehyde	aldehyde	NOUN
eurjchem-976	368	3	was	be	AUX
eurjchem-976	368	4	oxidized	oxidize	VERB
eurjchem-976	368	5	by	by	ADP
eurjchem-976	368	6	kmno4	kmno4	NOUN
eurjchem-976	368	7	solution	solution	NOUN
eurjchem-976	368	8	[	[	X
eurjchem-976	368	9	57	57	NUM
eurjchem-976	368	10	]	]	PUNCT
eurjchem-976	368	11	to	to	PART
eurjchem-976	368	12	afford	afford	VERB
eurjchem-976	368	13	5‐chloro‐1,3‐diphenyl‐1h‐	5‐chloro‐1,3‐diphenyl‐1h‐	PROPN
eurjchem-976	368	14	pyrazole‐4‐carboxylic	pyrazole‐4‐carboxylic	PROPN
eurjchem-976	368	15	acid	acid	NOUN
eurjchem-976	368	16	(	(	PUNCT
eurjchem-976	368	17	6	6	NUM
eurjchem-976	368	18	)	)	PUNCT
eurjchem-976	368	19	.	.	PUNCT
eurjchem-976	369	1	the	the	DET
eurjchem-976	369	2	second	second	ADJ
eurjchem-976	369	3	path	path	NOUN
eurjchem-976	369	4	included	include	VERB
eurjchem-976	369	5	the	the	DET
eurjchem-976	369	6	conversion	conversion	NOUN
eurjchem-976	369	7	of	of	ADP
eurjchem-976	369	8	substrate	substrate	NOUN
eurjchem-976	369	9	4	4	NUM
eurjchem-976	369	10	to	to	ADP
eurjchem-976	369	11	4‐bromo‐1,3‐diphenyl‐1h‐pyrazol‐	4‐bromo‐1,3‐diphenyl‐1h‐pyrazol‐	NUM
eurjchem-976	369	12	5(4h)‐one	5(4h)‐one	NUM
eurjchem-976	369	13	(	(	PUNCT
eurjchem-976	369	14	9	9	NUM
eurjchem-976	369	15	)	)	PUNCT
eurjchem-976	369	16	following	follow	VERB
eurjchem-976	369	17	the	the	DET
eurjchem-976	369	18	literature	literature	NOUN
eurjchem-976	369	19	procedure	procedure	NOUN
eurjchem-976	369	20	[	[	X
eurjchem-976	369	21	58	58	NUM
eurjchem-976	369	22	]	]	PUNCT
eurjchem-976	369	23	in	in	ADP
eurjchem-976	369	24	the	the	DET
eurjchem-976	369	25	presence	presence	NOUN
eurjchem-976	369	26	of	of	ADP
eurjchem-976	369	27	bromine	bromine	NOUN
eurjchem-976	369	28	in	in	ADP
eurjchem-976	369	29	acetic	acetic	ADJ
eurjchem-976	369	30	acid	acid	NOUN
eurjchem-976	369	31	.	.	PUNCT
eurjchem-976	370	1	the	the	DET
eurjchem-976	370	2	resulting	result	VERB
eurjchem-976	370	3	bromide	bromide	NOUN
eurjchem-976	370	4	9	9	NUM
eurjchem-976	370	5	was	be	AUX
eurjchem-976	370	6	allowed	allow	VERB
eurjchem-976	370	7	to	to	PART
eurjchem-976	370	8	react	react	VERB
eurjchem-976	370	9	with	with	ADP
eurjchem-976	370	10	excess	excess	NOUN
eurjchem-976	370	11	of	of	ADP
eurjchem-976	370	12	sodio‐diethyl	sodio‐diethyl	NOUN
eurjchem-976	370	13	malonates	malonate	NOUN
eurjchem-976	370	14	[	[	X
eurjchem-976	370	15	59	59	NUM
eurjchem-976	370	16	]	]	PUNCT
eurjchem-976	370	17	in	in	ADP
eurjchem-976	370	18	ethanol	ethanol	NOUN
eurjchem-976	370	19	followed	follow	VERB
eurjchem-976	370	20	by	by	ADP
eurjchem-976	370	21	decarboxylation	decarboxylation	NOUN
eurjchem-976	370	22	to	to	PART
eurjchem-976	370	23	afford	afford	VERB
eurjchem-976	370	24	substituted	substitute	VERB
eurjchem-976	370	25	acetic	acetic	ADJ
eurjchem-976	370	26	acids	acid	NOUN
eurjchem-976	370	27	10a	10a	NOUN
eurjchem-976	370	28	,	,	PUNCT
eurjchem-976	370	29	b.	b.	PROPN
eurjchem-976	370	30	on	on	ADP
eurjchem-976	370	31	the	the	DET
eurjchem-976	370	32	other	other	ADJ
eurjchem-976	370	33	hand	hand	NOUN
eurjchem-976	370	34	,	,	PUNCT
eurjchem-976	370	35	the	the	DET
eurjchem-976	370	36	third	third	ADJ
eurjchem-976	370	37	route	route	NOUN
eurjchem-976	370	38	(	(	PUNCT
eurjchem-976	370	39	path	path	NOUN
eurjchem-976	370	40	3	3	NUM
eurjchem-976	370	41	)	)	PUNCT
eurjchem-976	370	42	involved	involve	VERB
eurjchem-976	370	43	the	the	DET
eurjchem-976	370	44	production	production	NOUN
eurjchem-976	370	45	of	of	ADP
eurjchem-976	370	46	acid	acid	NOUN
eurjchem-976	370	47	precursors	precursor	NOUN
eurjchem-976	370	48	14a	14a	NOUN
eurjchem-976	370	49	,	,	PUNCT
eurjchem-976	370	50	b	b	PROPN
eurjchem-976	370	51	(	(	PUNCT
eurjchem-976	370	52	scheme	scheme	NOUN
eurjchem-976	370	53	2	2	NUM
eurjchem-976	370	54	)	)	PUNCT
eurjchem-976	370	55	.	.	PUNCT
eurjchem-976	371	1	these	these	DET
eurjchem-976	371	2	acids	acid	NOUN
eurjchem-976	371	3	were	be	AUX
eurjchem-976	371	4	smoothly	smoothly	ADV
eurjchem-976	371	5	prepared	prepare	VERB
eurjchem-976	371	6	through	through	ADP
eurjchem-976	371	7	the	the	DET
eurjchem-976	371	8	perkin‐type	perkin‐type	ADJ
eurjchem-976	371	9	reaction	reaction	NOUN
eurjchem-976	371	10	[	[	X
eurjchem-976	371	11	60	60	NUM
eurjchem-976	371	12	]	]	PUNCT
eurjchem-976	371	13	of	of	ADP
eurjchem-976	371	14	aldehyde	aldehyde	NOUN
eurjchem-976	371	15	5	5	NUM
eurjchem-976	371	16	with	with	ADP
eurjchem-976	371	17	acid	acid	NOUN
eurjchem-976	371	18	anhydrides	anhydride	NOUN
eurjchem-976	371	19	and	and	CCONJ
eurjchem-976	371	20	the	the	DET
eurjchem-976	371	21	corresponding	corresponding	ADJ
eurjchem-976	371	22	sodium	sodium	NOUN
eurjchem-976	371	23	salts	salt	NOUN
eurjchem-976	371	24	of	of	ADP
eurjchem-976	371	25	acids	acid	NOUN
eurjchem-976	371	26	to	to	PART
eurjchem-976	371	27	give	give	VERB
eurjchem-976	371	28	substituted	substitute	VERB
eurjchem-976	371	29	3‐(5‐chloro‐1,3‐	3‐(5‐chloro‐1,3‐	NUM
eurjchem-976	371	30	diphenyl‐1h‐pyrazol‐4‐yl)acrylic	diphenyl‐1h‐pyrazol‐4‐yl)acrylic	ADJ
eurjchem-976	371	31	acids	acid	NOUN
eurjchem-976	371	32	(	(	PUNCT
eurjchem-976	371	33	11a	11a	NOUN
eurjchem-976	371	34	,	,	PUNCT
eurjchem-976	371	35	b	b	NOUN
eurjchem-976	371	36	)	)	PUNCT
eurjchem-976	371	37	.	.	PUNCT
eurjchem-976	372	1	the	the	DET
eurjchem-976	372	2	resulting	result	VERB
eurjchem-976	372	3	acids	acid	NOUN
eurjchem-976	372	4	13a	13a	NOUN
eurjchem-976	372	5	,	,	PUNCT
eurjchem-976	372	6	b	b	NUM
eurjchem-976	372	7	were	be	AUX
eurjchem-976	372	8	reduced	reduce	VERB
eurjchem-976	372	9	by	by	ADP
eurjchem-976	372	10	sodium	sodium	NOUN
eurjchem-976	372	11	amalgam	amalgam	NOUN
eurjchem-976	372	12	in	in	ADP
eurjchem-976	372	13	sodium	sodium	NOUN
eurjchem-976	372	14	hydroxide	hydroxide	NOUN
eurjchem-976	372	15	solution	solution	NOUN
eurjchem-976	372	16	to	to	PART
eurjchem-976	372	17	afford	afford	VERB
eurjchem-976	372	18	14a	14a	NOUN
eurjchem-976	372	19	,	,	PUNCT
eurjchem-976	372	20	b.	b.	NOUN
eurjchem-976	372	21	upon	upon	SCONJ
eurjchem-976	372	22	intermediate	intermediate	ADJ
eurjchem-976	372	23	acids	acid	NOUN
eurjchem-976	372	24	6	6	NUM
eurjchem-976	372	25	,	,	PUNCT
eurjchem-976	372	26	10a	10a	NUM
eurjchem-976	372	27	,	,	PUNCT
eurjchem-976	372	28	b	b	NOUN
eurjchem-976	372	29	and	and	CCONJ
eurjchem-976	372	30	14a	14a	NOUN
eurjchem-976	372	31	,	,	PUNCT
eurjchem-976	372	32	b	b	NUM
eurjchem-976	372	33	are	be	AUX
eurjchem-976	372	34	formed	form	VERB
eurjchem-976	372	35	,	,	PUNCT
eurjchem-976	372	36	they	they	PRON
eurjchem-976	372	37	could	could	AUX
eurjchem-976	372	38	be	be	AUX
eurjchem-976	372	39	converted	convert	VERB
eurjchem-976	372	40	into	into	ADP
eurjchem-976	372	41	ethyl	ethyl	PROPN
eurjchem-976	372	42	esters	ester	NOUN
eurjchem-976	372	43	7	7	NUM
eurjchem-976	372	44	,	,	PUNCT
eurjchem-976	372	45	11a	11a	NUM
eurjchem-976	372	46	,	,	PUNCT
eurjchem-976	372	47	b	b	NOUN
eurjchem-976	372	48	and	and	CCONJ
eurjchem-976	372	49	15a	15a	NOUN
eurjchem-976	372	50	,	,	PUNCT
eurjchem-976	372	51	b	b	NOUN
eurjchem-976	372	52	by	by	ADP
eurjchem-976	372	53	reaction	reaction	NOUN
eurjchem-976	372	54	with	with	ADP
eurjchem-976	372	55	ethanol	ethanol	NOUN
eurjchem-976	372	56	and	and	CCONJ
eurjchem-976	372	57	h2so4	h2so4	NOUN
eurjchem-976	373	1	[	[	X
eurjchem-976	373	2	61	61	NUM
eurjchem-976	373	3	]	]	PUNCT
eurjchem-976	373	4	.	.	PUNCT
eurjchem-976	374	1	the	the	DET
eurjchem-976	374	2	resulting	result	VERB
eurjchem-976	374	3	esters	ester	NOUN
eurjchem-976	374	4	were	be	AUX
eurjchem-976	374	5	converted	convert	VERB
eurjchem-976	374	6	to	to	ADP
eurjchem-976	374	7	the	the	DET
eurjchem-976	374	8	corresponding	corresponding	ADJ
eurjchem-976	374	9	alcohols	alcohol	NOUN
eurjchem-976	374	10	8	8	NUM
eurjchem-976	374	11	,	,	PUNCT
eurjchem-976	374	12	12a	12a	NUM
eurjchem-976	374	13	,	,	PUNCT
eurjchem-976	374	14	b	b	NOUN
eurjchem-976	374	15	and	and	CCONJ
eurjchem-976	374	16	16a	16a	NOUN
eurjchem-976	374	17	,	,	PUNCT
eurjchem-976	374	18	b	b	X
eurjchem-976	374	19	(	(	PUNCT
eurjchem-976	374	20	schemes	scheme	NOUN
eurjchem-976	374	21	1	1	NUM
eurjchem-976	374	22	and	and	CCONJ
eurjchem-976	374	23	2	2	NUM
eurjchem-976	374	24	;	;	PUNCT
eurjchem-976	374	25	table	table	NOUN
eurjchem-976	374	26	1	1	NUM
eurjchem-976	374	27	)	)	PUNCT
eurjchem-976	374	28	by	by	ADP
eurjchem-976	374	29	addition	addition	NOUN
eurjchem-976	374	30	of	of	ADP
eurjchem-976	374	31	two	two	NUM
eurjchem-976	374	32	equivalents	equivalent	NOUN
eurjchem-976	374	33	of	of	ADP
eurjchem-976	374	34	methymagnesium	methymagnesium	NOUN
eurjchem-976	374	35	iodide	iodide	NOUN
eurjchem-976	374	36	[	[	X
eurjchem-976	374	37	62	62	NUM
eurjchem-976	374	38	]	]	PUNCT
eurjchem-976	374	39	in	in	ADP
eurjchem-976	374	40	et2o	et2o	ADJ
eurjchem-976	374	41	/	/	SYM
eurjchem-976	374	42	thf	thf	NOUN
eurjchem-976	374	43	solution	solution	NOUN
eurjchem-976	374	44	.	.	PUNCT
eurjchem-976	375	1	the	the	DET
eurjchem-976	375	2	structures	structure	NOUN
eurjchem-976	375	3	of	of	ADP
eurjchem-976	375	4	all	all	DET
eurjchem-976	375	5	new	new	ADJ
eurjchem-976	375	6	alcohols	alcohol	NOUN
eurjchem-976	375	7	were	be	AUX
eurjchem-976	375	8	appropriately	appropriately	ADV
eurjchem-976	375	9	established	establish	VERB
eurjchem-976	375	10	by	by	ADP
eurjchem-976	375	11	the	the	DET
eurjchem-976	375	12	usual	usual	ADJ
eurjchem-976	375	13	spectroscopic	spectroscopic	ADJ
eurjchem-976	375	14	methods	method	NOUN
eurjchem-976	375	15	.	.	PUNCT
eurjchem-976	376	1	the	the	DET
eurjchem-976	376	2	structural	structural	ADJ
eurjchem-976	376	3	elucidation	elucidation	NOUN
eurjchem-976	376	4	of	of	ADP
eurjchem-976	376	5	alcohols	alcohol	NOUN
eurjchem-976	376	6	8	8	NUM
eurjchem-976	376	7	,	,	PUNCT
eurjchem-976	376	8	12a	12a	NUM
eurjchem-976	376	9	,	,	PUNCT
eurjchem-976	376	10	b	b	NOUN
eurjchem-976	376	11	,	,	PUNCT
eurjchem-976	376	12	and	and	CCONJ
eurjchem-976	376	13	16a	16a	NOUN
eurjchem-976	376	14	,	,	PUNCT
eurjchem-976	376	15	b	b	NUM
eurjchem-976	376	16	was	be	AUX
eurjchem-976	376	17	mainly	mainly	ADV
eurjchem-976	376	18	based	base	VERB
eurjchem-976	376	19	on	on	ADP
eurjchem-976	376	20	ir	ir	PROPN
eurjchem-976	376	21	,	,	PUNCT
eurjchem-976	376	22	1h	1h	NUM
eurjchem-976	376	23	nmr	nmr	NOUN
eurjchem-976	376	24	,	,	PUNCT
eurjchem-976	376	25	ms	ms	NOUN
eurjchem-976	376	26	and	and	CCONJ
eurjchem-976	376	27	elemental	elemental	ADJ
eurjchem-976	376	28	analyses	analysis	NOUN
eurjchem-976	376	29	.	.	PUNCT
eurjchem-976	377	1	the	the	DET
eurjchem-976	377	2	ir	ir	PROPN
eurjchem-976	377	3	spectra	spectra	NOUN
eurjchem-976	377	4	of	of	ADP
eurjchem-976	377	5	alcohols	alcohol	NOUN
eurjchem-976	377	6	1a‐c	1a‐c	PROPN
eurjchem-976	377	7	showed	show	VERB
eurjchem-976	377	8	absorption	absorption	NOUN
eurjchem-976	377	9	bands	band	NOUN
eurjchem-976	377	10	for	for	ADP
eurjchem-976	377	11	a	a	DET
eurjchem-976	377	12	oh	oh	NOUN
eurjchem-976	377	13	groups	group	NOUN
eurjchem-976	377	14	as	as	ADP
eurjchem-976	377	15	broad	broad	ADJ
eurjchem-976	377	16	bands	band	NOUN
eurjchem-976	377	17	in	in	ADP
eurjchem-976	377	18	the	the	DET
eurjchem-976	377	19	range	range	NOUN
eurjchem-976	377	20	3340‐3490	3340‐3490	NUM
eurjchem-976	377	21	cm‐1	cm‐1	NOUN
eurjchem-976	377	22	.	.	PUNCT
eurjchem-976	378	1	the	the	DET
eurjchem-976	378	2	1h	1h	NUM
eurjchem-976	378	3	nmr	nmr	NOUN
eurjchem-976	378	4	data	datum	NOUN
eurjchem-976	378	5	allowed	allow	VERB
eurjchem-976	378	6	an	an	DET
eurjchem-976	378	7	unambiguous	unambiguous	ADJ
eurjchem-976	378	8	statement	statement	NOUN
eurjchem-976	378	9	of	of	ADP
eurjchem-976	378	10	the	the	DET
eurjchem-976	378	11	heterocyclic	heterocyclic	ADJ
eurjchem-976	378	12	alkanols	alkanol	NOUN
eurjchem-976	378	13	formation	formation	NOUN
eurjchem-976	378	14	.	.	PUNCT
eurjchem-976	379	1	thus	thus	ADV
eurjchem-976	379	2	,	,	PUNCT
eurjchem-976	379	3	the	the	DET
eurjchem-976	379	4	1h	1h	NUM
eurjchem-976	379	5	nmr	nmr	NOUN
eurjchem-976	379	6	spectrum	spectrum	NOUN
eurjchem-976	379	7	displayed	display	VERB
eurjchem-976	379	8	five	five	NUM
eurjchem-976	379	9	signals	signal	NOUN
eurjchem-976	379	10	for	for	ADP
eurjchem-976	379	11	compound	compound	NOUN
eurjchem-976	379	12	12a	12a	NOUN
eurjchem-976	379	13	.	.	PUNCT
eurjchem-976	380	1	the	the	DET
eurjchem-976	380	2	tenth	tenth	ADJ
eurjchem-976	380	3	aromatic	aromatic	ADJ
eurjchem-976	380	4	protons	proton	NOUN
eurjchem-976	380	5	appear	appear	VERB
eurjchem-976	380	6	at	at	ADP
eurjchem-976	380	7	δ	δ	PROPN
eurjchem-976	380	8	7.15‐8.25	7.15‐8.25	NUM
eurjchem-976	380	9	ppm	ppm	NOUN
eurjchem-976	380	10	.	.	PUNCT
eurjchem-976	381	1	el‐aal	el‐aal	NOUN
eurjchem-976	381	2	et	et	NOUN
eurjchem-976	381	3	al	al	PROPN
eurjchem-976	381	4	.	.	PUNCT
eurjchem-976	381	5	/	/	SYM
eurjchem-976	381	6	european	european	PROPN
eurjchem-976	381	7	journal	journal	PROPN
eurjchem-976	381	8	of	of	ADP
eurjchem-976	381	9	chemistry	chemistry	NOUN
eurjchem-976	381	10	5	5	NUM
eurjchem-976	381	11	(	(	PUNCT
eurjchem-976	381	12	2	2	NUM
eurjchem-976	381	13	)	)	PUNCT
eurjchem-976	381	14	(	(	PUNCT
eurjchem-976	381	15	2014	2014	NUM
eurjchem-976	381	16	)	)	PUNCT
eurjchem-976	381	17	277‐286	277‐286	NUM
eurjchem-976	381	18	285	285	NUM
eurjchem-976	381	19	figure	figure	NOUN
eurjchem-976	381	20	2	2	NUM
eurjchem-976	381	21	.	.	PUNCT
eurjchem-976	381	22	diastereotopic	diastereotopic	NOUN
eurjchem-976	381	23	protons	proton	NOUN
eurjchem-976	381	24	embraced	embrace	VERB
eurjchem-976	381	25	in	in	ADP
eurjchem-976	381	26	pyrazolones	pyrazolone	NOUN
eurjchem-976	381	27	heteropolycycles	heteropolycycle	NOUN
eurjchem-976	381	28	.	.	PUNCT
eurjchem-976	382	1	the	the	DET
eurjchem-976	382	2	aliphatic	aliphatic	ADJ
eurjchem-976	382	3	acyclic	acyclic	ADJ
eurjchem-976	382	4	protons	proton	NOUN
eurjchem-976	382	5	of	of	ADP
eurjchem-976	382	6	the	the	DET
eurjchem-976	382	7	two	two	NUM
eurjchem-976	382	8	methyls	methyls	NOUN
eurjchem-976	382	9	and	and	CCONJ
eurjchem-976	382	10	methylene	methylene	NOUN
eurjchem-976	382	11	groups	group	NOUN
eurjchem-976	382	12	of	of	ADP
eurjchem-976	382	13	the	the	DET
eurjchem-976	382	14	new	new	ADJ
eurjchem-976	382	15	alcohol	alcohol	NOUN
eurjchem-976	382	16	appeared	appear	VERB
eurjchem-976	382	17	as	as	ADP
eurjchem-976	382	18	two	two	NUM
eurjchem-976	382	19	sets	set	NOUN
eurjchem-976	382	20	of	of	ADP
eurjchem-976	382	21	splitting	splitting	NOUN
eurjchem-976	382	22	.	.	PUNCT
eurjchem-976	383	1	the	the	DET
eurjchem-976	383	2	singlet	singlet	NOUN
eurjchem-976	383	3	gem‐dimethyls	gem‐dimethyls	PROPN
eurjchem-976	383	4	appear	appear	VERB
eurjchem-976	383	5	at	at	ADP
eurjchem-976	383	6	δ	δ	PROPN
eurjchem-976	383	7	1.30	1.30	NUM
eurjchem-976	383	8	ppm	ppm	NOUN
eurjchem-976	383	9	while	while	SCONJ
eurjchem-976	383	10	doublet	doublet	ADJ
eurjchem-976	383	11	at	at	ADP
eurjchem-976	383	12	δ	δ	PROPN
eurjchem-976	383	13	2.0	2.0	NUM
eurjchem-976	383	14	ppm	ppm	NOUN
eurjchem-976	383	15	was	be	AUX
eurjchem-976	383	16	assigned	assign	VERB
eurjchem-976	383	17	to	to	ADP
eurjchem-976	383	18	the	the	DET
eurjchem-976	383	19	up‐field	up‐field	ADJ
eurjchem-976	383	20	proton	proton	NOUN
eurjchem-976	383	21	ch2	ch2	PROPN
eurjchem-976	383	22	.	.	PUNCT
eurjchem-976	384	1	a	a	DET
eurjchem-976	384	2	forth	forth	ADV
eurjchem-976	384	3	broad	broad	ADJ
eurjchem-976	384	4	singlet	singlet	NOUN
eurjchem-976	384	5	at	at	ADP
eurjchem-976	384	6	δ	δ	PROPN
eurjchem-976	384	7	2.55	2.55	NUM
eurjchem-976	384	8	ppm	ppm	NOUN
eurjchem-976	384	9	was	be	AUX
eurjchem-976	384	10	assigned	assign	VERB
eurjchem-976	384	11	to	to	ADP
eurjchem-976	384	12	oh	oh	INTJ
eurjchem-976	384	13	.	.	PUNCT
eurjchem-976	385	1	in	in	ADP
eurjchem-976	385	2	all	all	DET
eurjchem-976	385	3	ir	ir	PROPN
eurjchem-976	385	4	spectra	spectra	NOUN
eurjchem-976	385	5	of	of	ADP
eurjchem-976	385	6	the	the	DET
eurjchem-976	385	7	synthesized	synthesize	VERB
eurjchem-976	385	8	carbinols	carbinol	NOUN
eurjchem-976	385	9	,	,	PUNCT
eurjchem-976	385	10	the	the	DET
eurjchem-976	385	11	characteristic	characteristic	ADJ
eurjchem-976	385	12	peak	peak	NOUN
eurjchem-976	385	13	of	of	ADP
eurjchem-976	385	14	carbonyl	carbonyl	NOUN
eurjchem-976	385	15	groups	group	NOUN
eurjchem-976	385	16	was	be	AUX
eurjchem-976	385	17	absent	absent	ADJ
eurjchem-976	385	18	.	.	PUNCT
eurjchem-976	386	1	the	the	DET
eurjchem-976	386	2	cyclialkylations	cyclialkylation	NOUN
eurjchem-976	386	3	of	of	ADP
eurjchem-976	386	4	alcohols	alcohol	NOUN
eurjchem-976	386	5	8	8	NUM
eurjchem-976	386	6	,	,	PUNCT
eurjchem-976	386	7	12a	12a	NUM
eurjchem-976	386	8	,	,	PUNCT
eurjchem-976	386	9	b	b	NOUN
eurjchem-976	386	10	and	and	CCONJ
eurjchem-976	386	11	16a	16a	NOUN
eurjchem-976	386	12	,	,	PUNCT
eurjchem-976	386	13	b	b	NUM
eurjchem-976	386	14	were	be	AUX
eurjchem-976	386	15	smoothly	smoothly	ADV
eurjchem-976	386	16	carried	carry	VERB
eurjchem-976	386	17	out	out	ADP
eurjchem-976	386	18	in	in	ADP
eurjchem-976	386	19	the	the	DET
eurjchem-976	386	20	presence	presence	NOUN
eurjchem-976	386	21	of	of	ADP
eurjchem-976	386	22	alcl3	alcl3	PROPN
eurjchem-976	386	23	/	/	SYM
eurjchem-976	386	24	ch3no2	ch3no2	NOUN
eurjchem-976	386	25	or	or	CCONJ
eurjchem-976	386	26	p2o5	p2o5	X
eurjchem-976	386	27	or	or	CCONJ
eurjchem-976	386	28	ppa	ppa	VERB
eurjchem-976	386	29	catalysts	catalyst	NOUN
eurjchem-976	386	30	under	under	ADP
eurjchem-976	386	31	different	different	ADJ
eurjchem-976	386	32	reaction	reaction	NOUN
eurjchem-976	386	33	conditions	condition	NOUN
eurjchem-976	386	34	gave	give	VERB
eurjchem-976	386	35	substituted	substitute	VERB
eurjchem-976	386	36	2,4‐dihydroindeno[1,2‐c]pyrazole	2,4‐dihydroindeno[1,2‐c]pyrazole	PROPN
eurjchem-976	386	37	1a	1a	NOUN
eurjchem-976	386	38	,	,	PUNCT
eurjchem-976	386	39	4,5‐dihydro‐	4,5‐dihydro‐	PROPN
eurjchem-976	386	40	2h‐benzo[g]indazol‐3(3ah)‐ones	2h‐benzo[g]indazol‐3(3ah)‐ones	NUM
eurjchem-976	386	41	2a	2a	NUM
eurjchem-976	386	42	,	,	PUNCT
eurjchem-976	386	43	b	b	NOUN
eurjchem-976	386	44	and	and	CCONJ
eurjchem-976	386	45	4,5,6‐trihydro	4,5,6‐trihydro	NUM
eurjchem-976	386	46	benzo[6,7]cyclohepta[1,2‐c]pyrazoles	benzo[6,7]cyclohepta[1,2‐c]pyrazole	NOUN
eurjchem-976	386	47	3a	3a	NUM
eurjchem-976	386	48	,	,	PUNCT
eurjchem-976	386	49	b	b	NOUN
eurjchem-976	386	50	in	in	ADP
eurjchem-976	386	51	good	good	ADJ
eurjchem-976	386	52	overall	overall	ADJ
eurjchem-976	386	53	yields	yield	NOUN
eurjchem-976	386	54	(	(	PUNCT
eurjchem-976	386	55	table	table	NOUN
eurjchem-976	386	56	2	2	NUM
eurjchem-976	386	57	,	,	PUNCT
eurjchem-976	386	58	scheme	scheme	NOUN
eurjchem-976	386	59	3	3	NUM
eurjchem-976	386	60	and	and	CCONJ
eurjchem-976	386	61	4	4	NUM
eurjchem-976	386	62	)	)	PUNCT
eurjchem-976	386	63	.	.	PUNCT
eurjchem-976	387	1	on	on	ADP
eurjchem-976	387	2	the	the	DET
eurjchem-976	387	3	other	other	ADJ
eurjchem-976	387	4	hand	hand	NOUN
eurjchem-976	387	5	,	,	PUNCT
eurjchem-976	387	6	cyclialkylations	cyclialkylation	NOUN
eurjchem-976	387	7	of	of	ADP
eurjchem-976	387	8	acids	acid	NOUN
eurjchem-976	387	9	6	6	NUM
eurjchem-976	387	10	,	,	PUNCT
eurjchem-976	387	11	10a	10a	NUM
eurjchem-976	387	12	,	,	PUNCT
eurjchem-976	387	13	b	b	NOUN
eurjchem-976	387	14	and	and	CCONJ
eurjchem-976	387	15	14a	14a	NOUN
eurjchem-976	387	16	,	,	PUNCT
eurjchem-976	387	17	b	b	NUM
eurjchem-976	387	18	were	be	AUX
eurjchem-976	387	19	carried	carry	VERB
eurjchem-976	387	20	out	out	ADP
eurjchem-976	387	21	in	in	ADP
eurjchem-976	387	22	the	the	DET
eurjchem-976	387	23	presence	presence	NOUN
eurjchem-976	387	24	of	of	ADP
eurjchem-976	387	25	the	the	DET
eurjchem-976	387	26	same	same	ADJ
eurjchem-976	387	27	catalysts	catalyst	NOUN
eurjchem-976	387	28	under	under	ADP
eurjchem-976	387	29	varying	vary	VERB
eurjchem-976	387	30	conditions	condition	NOUN
eurjchem-976	387	31	to	to	PART
eurjchem-976	387	32	give	give	VERB
eurjchem-976	387	33	substituted	substitute	VERB
eurjchem-976	387	34	tricyclic	tricyclic	ADJ
eurjchem-976	387	35	pyrazolones	pyrazolone	NOUN
eurjchem-976	387	36	1b	1b	NUM
eurjchem-976	387	37	,	,	PUNCT
eurjchem-976	387	38	2c	2c	NUM
eurjchem-976	387	39	,	,	PUNCT
eurjchem-976	387	40	d	d	PROPN
eurjchem-976	387	41	and	and	CCONJ
eurjchem-976	387	42	3c	3c	NUM
eurjchem-976	387	43	,	,	PUNCT
eurjchem-976	387	44	d.	d.	PROPN
eurjchem-976	387	45	the	the	DET
eurjchem-976	387	46	results	result	NOUN
eurjchem-976	387	47	are	be	AUX
eurjchem-976	387	48	embedded	embed	VERB
eurjchem-976	387	49	in	in	ADP
eurjchem-976	387	50	table	table	NOUN
eurjchem-976	387	51	2	2	NUM
eurjchem-976	387	52	and	and	CCONJ
eurjchem-976	387	53	scheme	scheme	NOUN
eurjchem-976	387	54	5	5	NUM
eurjchem-976	387	55	.	.	PUNCT
eurjchem-976	388	1	the	the	DET
eurjchem-976	388	2	1h	1h	NUM
eurjchem-976	388	3	nmr	nmr	NOUN
eurjchem-976	388	4	data	datum	NOUN
eurjchem-976	388	5	allowed	allow	VERB
eurjchem-976	388	6	an	an	DET
eurjchem-976	388	7	unambiguous	unambiguous	ADJ
eurjchem-976	388	8	statement	statement	NOUN
eurjchem-976	388	9	of	of	ADP
eurjchem-976	388	10	the	the	DET
eurjchem-976	388	11	formation	formation	NOUN
eurjchem-976	388	12	of	of	ADP
eurjchem-976	388	13	heterocyclic	heterocyclic	ADJ
eurjchem-976	388	14	products	product	NOUN
eurjchem-976	388	15	.	.	PUNCT
eurjchem-976	389	1	the	the	DET
eurjchem-976	389	2	assignment	assignment	NOUN
eurjchem-976	389	3	of	of	ADP
eurjchem-976	389	4	the	the	DET
eurjchem-976	389	5	diastereotopic	diastereotopic	NOUN
eurjchem-976	389	6	protons	proton	NOUN
eurjchem-976	389	7	of	of	ADP
eurjchem-976	389	8	the	the	DET
eurjchem-976	389	9	methylene	methylene	NOUN
eurjchem-976	389	10	group	group	NOUN
eurjchem-976	389	11	directly	directly	ADV
eurjchem-976	389	12	bonded	bond	VERB
eurjchem-976	389	13	to	to	PART
eurjchem-976	389	14	pyrazole	pyrazole	VERB
eurjchem-976	389	15	or	or	CCONJ
eurjchem-976	389	16	pyrazolone	pyrazolone	NOUN
eurjchem-976	389	17	rings	ring	NOUN
eurjchem-976	389	18	(	(	PUNCT
eurjchem-976	389	19	2a	2a	NUM
eurjchem-976	389	20	,	,	PUNCT
eurjchem-976	389	21	c	c	NOUN
eurjchem-976	389	22	and	and	CCONJ
eurjchem-976	389	23	3b	3b	NUM
eurjchem-976	389	24	,	,	PUNCT
eurjchem-976	389	25	d	d	NOUN
eurjchem-976	389	26	)	)	PUNCT
eurjchem-976	389	27	beside	beside	ADP
eurjchem-976	389	28	their	their	PRON
eurjchem-976	389	29	intermediates	intermediate	NOUN
eurjchem-976	389	30	alcohols	alcohol	NOUN
eurjchem-976	389	31	and	and	CCONJ
eurjchem-976	389	32	acids	acid	NOUN
eurjchem-976	389	33	(	(	PUNCT
eurjchem-976	389	34	12a	12a	NOUN
eurjchem-976	389	35	,	,	PUNCT
eurjchem-976	389	36	16b	16b	NUM
eurjchem-976	389	37	and	and	CCONJ
eurjchem-976	389	38	10a	10a	NOUN
eurjchem-976	389	39	,	,	PUNCT
eurjchem-976	389	40	14b	14b	NUM
eurjchem-976	389	41	)	)	PUNCT
eurjchem-976	389	42	were	be	AUX
eurjchem-976	389	43	made	make	VERB
eurjchem-976	389	44	on	on	ADP
eurjchem-976	389	45	the	the	DET
eurjchem-976	389	46	basis	basis	NOUN
eurjchem-976	389	47	of	of	ADP
eurjchem-976	389	48	j‐values	j‐value	NOUN
eurjchem-976	389	49	that	that	PRON
eurjchem-976	389	50	were	be	AUX
eurjchem-976	389	51	obtained	obtain	VERB
eurjchem-976	389	52	by	by	ADP
eurjchem-976	389	53	direct	direct	ADJ
eurjchem-976	389	54	inspection	inspection	NOUN
eurjchem-976	389	55	of	of	ADP
eurjchem-976	389	56	the	the	DET
eurjchem-976	389	57	1h	1h	NUM
eurjchem-976	389	58	nmr	nmr	NOUN
eurjchem-976	389	59	spectrum	spectrum	NOUN
eurjchem-976	389	60	which	which	PRON
eurjchem-976	389	61	in	in	ADP
eurjchem-976	389	62	turn	turn	NOUN
eurjchem-976	389	63	showed	show	VERB
eurjchem-976	389	64	a	a	DET
eurjchem-976	389	65	greatly	greatly	ADV
eurjchem-976	389	66	change	change	NOUN
eurjchem-976	389	67	in	in	ADP
eurjchem-976	389	68	chemical	chemical	ADJ
eurjchem-976	389	69	shifts	shift	NOUN
eurjchem-976	389	70	.	.	PUNCT
eurjchem-976	390	1	it	it	PRON
eurjchem-976	390	2	is	be	AUX
eurjchem-976	390	3	known	know	VERB
eurjchem-976	390	4	that	that	SCONJ
eurjchem-976	390	5	the	the	DET
eurjchem-976	390	6	extent	extent	NOUN
eurjchem-976	390	7	of	of	ADP
eurjchem-976	390	8	shielding	shielding	NOUN
eurjchem-976	390	9	is	be	AUX
eurjchem-976	390	10	proportional	proportional	ADJ
eurjchem-976	390	11	to	to	ADP
eurjchem-976	390	12	the	the	DET
eurjchem-976	390	13	electronegativity	electronegativity	NOUN
eurjchem-976	390	14	exerted	exert	VERB
eurjchem-976	390	15	by	by	ADP
eurjchem-976	390	16	the	the	DET
eurjchem-976	390	17	heterocyclic	heterocyclic	ADJ
eurjchem-976	390	18	ring	ring	NOUN
eurjchem-976	390	19	or	or	CCONJ
eurjchem-976	390	20	the	the	DET
eurjchem-976	390	21	neighbored	neighbored	ADJ
eurjchem-976	390	22	functional	functional	ADJ
eurjchem-976	390	23	groups	group	NOUN
eurjchem-976	390	24	and	and	CCONJ
eurjchem-976	390	25	its	its	PRON
eurjchem-976	390	26	proximity	proximity	NOUN
eurjchem-976	390	27	to	to	ADP
eurjchem-976	390	28	the	the	DET
eurjchem-976	390	29	hydrogen	hydrogen	NOUN
eurjchem-976	391	1	[	[	X
eurjchem-976	391	2	63‐66	63‐66	NOUN
eurjchem-976	391	3	]	]	PUNCT
eurjchem-976	391	4	.	.	PUNCT
eurjchem-976	392	1	this	this	DET
eurjchem-976	392	2	trend	trend	NOUN
eurjchem-976	392	3	has	have	AUX
eurjchem-976	392	4	been	be	AUX
eurjchem-976	392	5	observed	observe	VERB
eurjchem-976	392	6	from	from	ADP
eurjchem-976	392	7	the	the	DET
eurjchem-976	392	8	chemical	chemical	ADJ
eurjchem-976	392	9	shifts	shift	NOUN
eurjchem-976	392	10	of	of	ADP
eurjchem-976	392	11	diastereotopic	diastereotopic	ADJ
eurjchem-976	392	12	hydrogens	hydrogen	NOUN
eurjchem-976	392	13	(	(	PUNCT
eurjchem-976	392	14	ha	ha	INTJ
eurjchem-976	392	15	and	and	CCONJ
eurjchem-976	392	16	hb	hb	NOUN
eurjchem-976	392	17	)	)	PUNCT
eurjchem-976	392	18	of	of	ADP
eurjchem-976	392	19	ch2	ch2	PROPN
eurjchem-976	392	20	group	group	PROPN
eurjchem-976	392	21	characterized	characterize	VERB
eurjchem-976	392	22	by	by	ADP
eurjchem-976	392	23	the	the	DET
eurjchem-976	392	24	a2b	a2b	PROPN
eurjchem-976	392	25	system	system	NOUN
eurjchem-976	392	26	obtained	obtain	VERB
eurjchem-976	392	27	in	in	ADP
eurjchem-976	392	28	each	each	DET
eurjchem-976	392	29	series	series	NOUN
eurjchem-976	392	30	(	(	PUNCT
eurjchem-976	392	31	figure	figure	NOUN
eurjchem-976	392	32	2	2	NUM
eurjchem-976	392	33	)	)	PUNCT
eurjchem-976	392	34	.	.	PUNCT
eurjchem-976	393	1	for	for	ADP
eurjchem-976	393	2	instance	instance	NOUN
eurjchem-976	393	3	,	,	PUNCT
eurjchem-976	393	4	the	the	DET
eurjchem-976	393	5	1h	1h	NUM
eurjchem-976	393	6	nmr	nmr	NOUN
eurjchem-976	393	7	of	of	ADP
eurjchem-976	393	8	tricyclic	tricyclic	ADJ
eurjchem-976	393	9	compound	compound	PROPN
eurjchem-976	393	10	2a	2a	NUM
eurjchem-976	393	11	displayed	display	VERB
eurjchem-976	393	12	five	five	NUM
eurjchem-976	393	13	signals	signal	NOUN
eurjchem-976	393	14	in	in	ADP
eurjchem-976	393	15	which	which	PRON
eurjchem-976	393	16	aromatic	aromatic	ADJ
eurjchem-976	393	17	protons	proton	NOUN
eurjchem-976	393	18	appeared	appear	VERB
eurjchem-976	393	19	at	at	ADP
eurjchem-976	393	20	δ	δ	PROPN
eurjchem-976	393	21	6.85‐8.11	6.85‐8.11	PROPN
eurjchem-976	393	22	ppm	ppm	NOUN
eurjchem-976	393	23	and	and	CCONJ
eurjchem-976	393	24	the	the	DET
eurjchem-976	393	25	gem‐dimethyls	gem‐dimethyls	ADJ
eurjchem-976	393	26	groups	group	NOUN
eurjchem-976	393	27	appeared	appear	VERB
eurjchem-976	393	28	as	as	ADP
eurjchem-976	393	29	singlet	singlet	NOUN
eurjchem-976	393	30	at	at	ADP
eurjchem-976	393	31	δ	δ	PROPN
eurjchem-976	393	32	1.40	1.40	NUM
eurjchem-976	393	33	ppm	ppm	NOUN
eurjchem-976	393	34	,	,	PUNCT
eurjchem-976	393	35	respectively	respectively	ADV
eurjchem-976	393	36	.	.	PUNCT
eurjchem-976	394	1	the	the	DET
eurjchem-976	394	2	third	third	ADJ
eurjchem-976	394	3	quartet	quartet	NOUN
eurjchem-976	394	4	appeared	appear	VERB
eurjchem-976	394	5	at	at	ADP
eurjchem-976	394	6	2.35	2.35	NUM
eurjchem-976	394	7	ppm	ppm	NOUN
eurjchem-976	394	8	with	with	ADP
eurjchem-976	394	9	coupling	couple	VERB
eurjchem-976	394	10	constant	constant	ADJ
eurjchem-976	394	11	of	of	ADP
eurjchem-976	394	12	10.4	10.4	NUM
eurjchem-976	394	13	hz	hz	NOUN
eurjchem-976	394	14	.	.	PUNCT
eurjchem-976	395	1	as	as	SCONJ
eurjchem-976	395	2	expected	expect	VERB
eurjchem-976	395	3	,	,	PUNCT
eurjchem-976	395	4	the	the	DET
eurjchem-976	395	5	remaining	remain	VERB
eurjchem-976	395	6	two	two	NUM
eurjchem-976	395	7	signals	signal	NOUN
eurjchem-976	395	8	for	for	ADP
eurjchem-976	395	9	the	the	DET
eurjchem-976	395	10	diastereotopic	diastereotopic	PROPN
eurjchem-976	395	11	ch2	ch2	PROPN
eurjchem-976	395	12	group	group	PROPN
eurjchem-976	395	13	exhibits	exhibit	VERB
eurjchem-976	395	14	a	a	DET
eurjchem-976	395	15	complex	complex	ADJ
eurjchem-976	395	16	set	set	NOUN
eurjchem-976	395	17	of	of	ADP
eurjchem-976	395	18	overlapped	overlapped	ADJ
eurjchem-976	395	19	signals	signal	NOUN
eurjchem-976	395	20	which	which	PRON
eurjchem-976	395	21	were	be	AUX
eurjchem-976	395	22	assigned	assign	VERB
eurjchem-976	395	23	to	to	PART
eurjchem-976	395	24	be	be	AUX
eurjchem-976	395	25	shielded	shield	VERB
eurjchem-976	395	26	and	and	CCONJ
eurjchem-976	395	27	displayed	display	VERB
eurjchem-976	395	28	as	as	ADP
eurjchem-976	395	29	a	a	DET
eurjchem-976	395	30	second	second	ADJ
eurjchem-976	395	31	order	order	NOUN
eurjchem-976	395	32	set	set	NOUN
eurjchem-976	395	33	of	of	ADP
eurjchem-976	395	34	signals	signal	NOUN
eurjchem-976	395	35	showed	show	VERB
eurjchem-976	395	36	a	a	DET
eurjchem-976	395	37	triplet	triplet	NOUN
eurjchem-976	395	38	in	in	ADP
eurjchem-976	395	39	average	average	NOUN
eurjchem-976	395	40	at	at	ADP
eurjchem-976	395	41	δ	δ	PROPN
eurjchem-976	395	42	1.84	1.84	NUM
eurjchem-976	395	43	ppm	ppm	NOUN
eurjchem-976	395	44	with	with	ADP
eurjchem-976	395	45	coupling	couple	VERB
eurjchem-976	395	46	constant	constant	ADJ
eurjchem-976	395	47	of	of	ADP
eurjchem-976	395	48	14.2	14.2	NUM
eurjchem-976	395	49	hz	hz	VERB
eurjchem-976	395	50	for	for	ADP
eurjchem-976	395	51	one	one	NUM
eurjchem-976	395	52	hydrogen	hydrogen	NOUN
eurjchem-976	395	53	and	and	CCONJ
eurjchem-976	395	54	doublet	doublet	NOUN
eurjchem-976	395	55	of	of	ADP
eurjchem-976	395	56	doublets	doublet	NOUN
eurjchem-976	395	57	at	at	ADP
eurjchem-976	395	58	an	an	DET
eurjchem-976	395	59	average	average	NOUN
eurjchem-976	395	60	of	of	ADP
eurjchem-976	395	61	2.17	2.17	NUM
eurjchem-976	395	62	ppm	ppm	NOUN
eurjchem-976	395	63	for	for	ADP
eurjchem-976	395	64	the	the	DET
eurjchem-976	395	65	other	other	ADJ
eurjchem-976	395	66	one	one	NUM
eurjchem-976	395	67	.	.	PUNCT
eurjchem-976	396	1	in	in	ADP
eurjchem-976	396	2	comparison	comparison	NOUN
eurjchem-976	396	3	with	with	ADP
eurjchem-976	396	4	the	the	DET
eurjchem-976	396	5	compound	compound	NOUN
eurjchem-976	396	6	2a	2a	NUM
eurjchem-976	396	7	,	,	PUNCT
eurjchem-976	396	8	the	the	DET
eurjchem-976	396	9	tricyclic	tricyclic	ADJ
eurjchem-976	396	10	pyrazolone	pyrazolone	NOUN
eurjchem-976	396	11	2c	2c	NOUN
eurjchem-976	396	12	showed	show	VERB
eurjchem-976	396	13	the	the	DET
eurjchem-976	396	14	1h	1h	NUM
eurjchem-976	396	15	nmr	nmr	NOUN
eurjchem-976	396	16	chemical	chemical	ADJ
eurjchem-976	396	17	shifts	shift	NOUN
eurjchem-976	396	18	for	for	ADP
eurjchem-976	396	19	ch2	ch2	NOUN
eurjchem-976	396	20	protons	proton	NOUN
eurjchem-976	396	21	(	(	PUNCT
eurjchem-976	396	22	ha	ha	INTJ
eurjchem-976	396	23	and	and	CCONJ
eurjchem-976	396	24	hb	hb	NOUN
eurjchem-976	396	25	)	)	PUNCT
eurjchem-976	396	26	as	as	ADP
eurjchem-976	396	27	a	a	DET
eurjchem-976	396	28	characteristic	characteristic	ADJ
eurjchem-976	396	29	doublet	doublet	NOUN
eurjchem-976	396	30	of	of	ADP
eurjchem-976	396	31	triplet	triplet	NOUN
eurjchem-976	396	32	for	for	ADP
eurjchem-976	396	33	ha	ha	INTJ
eurjchem-976	396	34	at	at	ADP
eurjchem-976	396	35	an	an	DET
eurjchem-976	396	36	average	average	NOUN
eurjchem-976	396	37	of	of	ADP
eurjchem-976	396	38	δ	δ	PROPN
eurjchem-976	396	39	2.71	2.71	NUM
eurjchem-976	396	40	ppm	ppm	NOUN
eurjchem-976	396	41	with	with	ADP
eurjchem-976	396	42	a	a	DET
eurjchem-976	396	43	coupling	coupling	NOUN
eurjchem-976	396	44	constant	constant	ADJ
eurjchem-976	396	45	of	of	ADP
eurjchem-976	396	46	14.2	14.2	NUM
eurjchem-976	396	47	hz	hz	NOUN
eurjchem-976	396	48	and	and	CCONJ
eurjchem-976	396	49	a	a	DET
eurjchem-976	396	50	apparently	apparently	ADV
eurjchem-976	396	51	triplet	triplet	NOUN
eurjchem-976	396	52	for	for	ADP
eurjchem-976	396	53	hb	hb	PROPN
eurjchem-976	396	54	near	near	ADP
eurjchem-976	396	55	δ	δ	PROPN
eurjchem-976	396	56	3.11	3.11	NUM
eurjchem-976	396	57	ppm	ppm	NOUN
eurjchem-976	396	58	.	.	PUNCT
eurjchem-976	397	1	4	4	X
eurjchem-976	397	2	.	.	X
eurjchem-976	397	3	conclusion	conclusion	NOUN
eurjchem-976	397	4	in	in	ADP
eurjchem-976	397	5	conclusion	conclusion	NOUN
eurjchem-976	397	6	,	,	PUNCT
eurjchem-976	397	7	we	we	PRON
eurjchem-976	397	8	have	have	AUX
eurjchem-976	397	9	developed	develop	VERB
eurjchem-976	397	10	a	a	DET
eurjchem-976	397	11	simple	simple	ADJ
eurjchem-976	397	12	and	and	CCONJ
eurjchem-976	397	13	attractive	attractive	ADJ
eurjchem-976	397	14	method	method	NOUN
eurjchem-976	397	15	for	for	ADP
eurjchem-976	397	16	the	the	DET
eurjchem-976	397	17	synthesis	synthesis	NOUN
eurjchem-976	397	18	of	of	ADP
eurjchem-976	397	19	variety	variety	NOUN
eurjchem-976	397	20	of	of	ADP
eurjchem-976	397	21	new	new	ADJ
eurjchem-976	397	22	fused	fuse	VERB
eurjchem-976	397	23	tricyclic	tricyclic	ADJ
eurjchem-976	397	24	pyrazoles	pyrazole	NOUN
eurjchem-976	397	25	bearing	bear	VERB
eurjchem-976	397	26	small	small	ADJ
eurjchem-976	397	27	to	to	ADP
eurjchem-976	397	28	medium‐sized	medium‐size	VERB
eurjchem-976	397	29	alkyl	alkyl	NOUN
eurjchem-976	397	30	residues	residue	NOUN
eurjchem-976	397	31	.	.	PUNCT
eurjchem-976	398	1	the	the	DET
eurjchem-976	398	2	synthetic	synthetic	ADJ
eurjchem-976	398	3	approach	approach	NOUN
eurjchem-976	398	4	involved	involve	VERB
eurjchem-976	398	5	friedel‐crafts	friedel‐craft	NOUN
eurjchem-976	398	6	cyclialkylations	cyclialkylation	NOUN
eurjchem-976	398	7	of	of	ADP
eurjchem-976	398	8	heteroaryl	heteroaryl	NOUN
eurjchem-976	398	9	alkanols	alkanol	NOUN
eurjchem-976	398	10	and	and	CCONJ
eurjchem-976	398	11	acids	acid	NOUN
eurjchem-976	398	12	catalyzed	catalyze	VERB
eurjchem-976	398	13	by	by	ADP
eurjchem-976	398	14	alcl3	alcl3	PROPN
eurjchem-976	398	15	/	/	SYM
eurjchem-976	398	16	ch3no2	ch3no2	NOUN
eurjchem-976	398	17	or	or	CCONJ
eurjchem-976	398	18	p2o5	p2o5	X
eurjchem-976	398	19	or	or	CCONJ
eurjchem-976	398	20	ppa	ppa	PROPN
eurjchem-976	398	21	.	.	PUNCT
eurjchem-976	398	22	to	to	ADP
eurjchem-976	398	23	the	the	DET
eurjchem-976	398	24	best	good	ADJ
eurjchem-976	398	25	of	of	ADP
eurjchem-976	398	26	our	our	PRON
eurjchem-976	398	27	knowledge	knowledge	NOUN
eurjchem-976	398	28	,	,	PUNCT
eurjchem-976	398	29	this	this	PRON
eurjchem-976	398	30	is	be	AUX
eurjchem-976	398	31	the	the	DET
eurjchem-976	398	32	first	first	ADJ
eurjchem-976	398	33	time	time	NOUN
eurjchem-976	398	34	that	that	PRON
eurjchem-976	398	35	such	such	ADJ
eurjchem-976	398	36	novel	novel	ADJ
eurjchem-976	398	37	substituted	substitute	VERB
eurjchem-976	398	38	pyrazoles	pyrazole	NOUN
eurjchem-976	398	39	have	have	AUX
eurjchem-976	398	40	been	be	AUX
eurjchem-976	398	41	described	describe	VERB
eurjchem-976	398	42	.	.	PUNCT
eurjchem-976	399	1	the	the	DET
eurjchem-976	399	2	results	result	NOUN
eurjchem-976	399	3	proved	prove	VERB
eurjchem-976	399	4	that	that	SCONJ
eurjchem-976	399	5	friedel‐crafts	friedel‐craft	NOUN
eurjchem-976	399	6	cyclialkylations	cyclialkylation	NOUN
eurjchem-976	399	7	can	can	AUX
eurjchem-976	399	8	be	be	AUX
eurjchem-976	399	9	considered	consider	VERB
eurjchem-976	399	10	as	as	ADP
eurjchem-976	399	11	useful	useful	ADJ
eurjchem-976	399	12	pathways	pathway	NOUN
eurjchem-976	399	13	to	to	ADP
eurjchem-976	399	14	the	the	DET
eurjchem-976	399	15	syntheses	synthesis	NOUN
eurjchem-976	399	16	of	of	ADP
eurjchem-976	399	17	heteropolycycles	heteropolycycle	NOUN
eurjchem-976	399	18	.	.	PUNCT
eurjchem-976	400	1	acknowledgements	acknowledgement	NOUN
eurjchem-976	400	2	the	the	DET
eurjchem-976	400	3	authors	author	NOUN
eurjchem-976	400	4	are	be	AUX
eurjchem-976	400	5	grateful	grateful	ADJ
eurjchem-976	400	6	for	for	ADP
eurjchem-976	400	7	the	the	DET
eurjchem-976	400	8	financial	financial	ADJ
eurjchem-976	400	9	support	support	NOUN
eurjchem-976	400	10	and	and	CCONJ
eurjchem-976	400	11	all	all	DET
eurjchem-976	400	12	the	the	DET
eurjchem-976	400	13	facilities	facility	NOUN
eurjchem-976	400	14	received	receive	VERB
eurjchem-976	400	15	while	while	SCONJ
eurjchem-976	400	16	performing	perform	VERB
eurjchem-976	400	17	and	and	CCONJ
eurjchem-976	400	18	writing	write	VERB
eurjchem-976	400	19	this	this	DET
eurjchem-976	400	20	work	work	NOUN
eurjchem-976	400	21	by	by	ADP
eurjchem-976	400	22	the	the	DET
eurjchem-976	400	23	chemistry	chemistry	NOUN
eurjchem-976	400	24	department	department	NOUN
eurjchem-976	400	25	,	,	PUNCT
eurjchem-976	400	26	faculty	faculty	NOUN
eurjchem-976	400	27	of	of	ADP
eurjchem-976	400	28	science	science	PROPN
eurjchem-976	400	29	assiut	assiut	PROPN
eurjchem-976	400	30	university	university	PROPN
eurjchem-976	400	31	,	,	PUNCT
eurjchem-976	400	32	assiut	assiut	PROPN
eurjchem-976	400	33	,	,	PUNCT
eurjchem-976	400	34	egypt	egypt	PROPN
eurjchem-976	400	35	.	.	PUNCT
eurjchem-976	401	1	references	reference	NOUN
eurjchem-976	401	2	[	[	X
eurjchem-976	401	3	1	1	NUM
eurjchem-976	401	4	]	]	PUNCT
eurjchem-976	401	5	.	.	PUNCT
eurjchem-976	402	1	kleemann	kleemann	PROPN
eurjchem-976	402	2	,	,	PUNCT
eurjchem-976	402	3	a.	a.	PROPN
eurjchem-976	402	4	;	;	PUNCT
eurjchem-976	402	5	engel	engel	PROPN
eurjchem-976	402	6	,	,	PUNCT
eurjchem-976	402	7	j.	j.	PROPN
eurjchem-976	402	8	;	;	PUNCT
eurjchem-976	402	9	kutscher	kutscher	PROPN
eurjchem-976	402	10	,	,	PUNCT
eurjchem-976	402	11	b.	b.	PROPN
eurjchem-976	402	12	;	;	PUNCT
eurjchem-976	402	13	reichert	reichert	PROPN
eurjchem-976	402	14	,	,	PUNCT
eurjchem-976	402	15	d.	d.	PROPN
eurjchem-976	402	16	pharmaceutical	pharmaceutical	PROPN
eurjchem-976	402	17	substances	substance	NOUN
eurjchem-976	402	18	,	,	PUNCT
eurjchem-976	402	19	3rd	3rd	ADJ
eurjchem-976	402	20	edition	edition	NOUN
eurjchem-976	402	21	.	.	PUNCT
eurjchem-976	402	22	;	;	PUNCT
eurjchem-976	402	23	georg	georg	NOUN
eurjchem-976	402	24	thieme	thieme	NOUN
eurjchem-976	402	25	verlag	verlag	PROPN
eurjchem-976	402	26	:	:	PUNCT
eurjchem-976	402	27	stuttgart	stuttgart	PROPN
eurjchem-976	402	28	/	/	SYM
eurjchem-976	402	29	new	new	PROPN
eurjchem-976	402	30	york	york	PROPN
eurjchem-976	402	31	,	,	PUNCT
eurjchem-976	402	32	1999	1999	NUM
eurjchem-976	402	33	,	,	PUNCT
eurjchem-976	402	34	p	p	NOUN
eurjchem-976	402	35	1725‐1727	1725‐1727	NUM
eurjchem-976	402	36	.	.	PUNCT
eurjchem-976	403	1	[	[	X
eurjchem-976	403	2	2	2	NUM
eurjchem-976	403	3	]	]	PUNCT
eurjchem-976	403	4	.	.	PUNCT
eurjchem-976	404	1	deng	deng	PROPN
eurjchem-976	404	2	,	,	PUNCT
eurjchem-976	404	3	x.	x.	PROPN
eurjchem-976	404	4	;	;	PUNCT
eurjchem-976	404	5	mani	mani	NOUN
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eurjchem-976	404	7	n.	n.	PROPN
eurjchem-976	404	8	s.	s.	PROPN
eurjchem-976	404	9	org	org	PROPN
eurjchem-976	404	10	.	.	PUNCT
eurjchem-976	405	1	lett	lett	PROPN
eurjchem-976	405	2	.	.	PROPN
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eurjchem-976	405	4	,	,	PUNCT
eurjchem-976	405	5	10	10	NUM
eurjchem-976	405	6	,	,	PUNCT
eurjchem-976	405	7	1307‐1310	1307‐1310	NUM
eurjchem-976	405	8	.	.	PUNCT
eurjchem-976	406	1	[	[	X
eurjchem-976	406	2	3	3	NUM
eurjchem-976	406	3	]	]	PUNCT
eurjchem-976	406	4	.	.	PUNCT
eurjchem-976	407	1	bhat	bhat	PROPN
eurjchem-976	407	2	,	,	PUNCT
eurjchem-976	407	3	b.	b.	PROPN
eurjchem-976	407	4	a.	a.	PROPN
eurjchem-976	407	5	;	;	PUNCT
eurjchem-976	407	6	dhar	dhar	PROPN
eurjchem-976	407	7	,	,	PUNCT
eurjchem-976	407	8	k.	k.	PROPN
eurjchem-976	407	9	l.	l.	PROPN
eurjchem-976	407	10	;	;	PUNCT
eurjchem-976	407	11	puri	puri	PROPN
eurjchem-976	407	12	,	,	PUNCT
eurjchem-976	407	13	s.	s.	PROPN
eurjchem-976	407	14	c.	c.	PROPN
eurjchem-976	407	15	;	;	PUNCT
eurjchem-976	407	16	saxena	saxena	PROPN
eurjchem-976	407	17	,	,	PUNCT
eurjchem-976	407	18	a.	a.	PROPN
eurjchem-976	407	19	k.	k.	PROPN
eurjchem-976	407	20	;	;	PUNCT
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eurjchem-976	407	22	,	,	PUNCT
eurjchem-976	407	23	m.	m.	NOUN
eurjchem-976	407	24	;	;	PUNCT
eurjchem-976	407	25	qazi	qazi	PROPN
eurjchem-976	407	26	,	,	PUNCT
eurjchem-976	407	27	g.	g.	PROPN
eurjchem-976	407	28	n.	n.	PROPN
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eurjchem-976	407	30	.	.	PUNCT
eurjchem-976	408	1	med	med	PROPN
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eurjchem-976	408	4	.	.	PUNCT
eurjchem-976	409	1	lett	lett	PROPN
eurjchem-976	409	2	.	.	PUNCT
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eurjchem-976	410	2	,	,	PUNCT
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eurjchem-976	410	4	,	,	PUNCT
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eurjchem-976	410	6	.	.	PUNCT
eurjchem-976	411	1	[	[	X
eurjchem-976	411	2	4	4	NUM
eurjchem-976	411	3	]	]	PUNCT
eurjchem-976	411	4	.	.	PUNCT
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eurjchem-976	411	6	,	,	PUNCT
eurjchem-976	411	7	d.	d.	PROPN
eurjchem-976	411	8	n.	n.	PROPN
eurjchem-976	411	9	;	;	PUNCT
eurjchem-976	411	10	patil	patil	PROPN
eurjchem-976	411	11	,	,	PUNCT
eurjchem-976	411	12	a.	a.	PROPN
eurjchem-976	411	13	s.	s.	PROPN
eurjchem-976	411	14	;	;	PUNCT
eurjchem-976	411	15	awate	awate	PROPN
eurjchem-976	411	16	,	,	PUNCT
eurjchem-976	411	17	b.	b.	PROPN
eurjchem-976	411	18	g.	g.	PROPN
eurjchem-976	411	19	;	;	PUNCT
eurjchem-976	411	20	naik	naik	PROPN
eurjchem-976	411	21	,	,	PUNCT
eurjchem-976	411	22	l.	l.	PROPN
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eurjchem-976	411	26	,	,	PUNCT
eurjchem-976	411	27	16	16	NUM
eurjchem-976	411	28	,	,	PUNCT
eurjchem-976	411	29	27‐28	27‐28	NUM
eurjchem-976	411	30	.	.	PUNCT
eurjchem-976	412	1	[	[	X
eurjchem-976	412	2	5	5	NUM
eurjchem-976	412	3	]	]	PUNCT
eurjchem-976	412	4	.	.	PUNCT
eurjchem-976	412	5	elguero	elguero	PROPN
eurjchem-976	412	6	,	,	PUNCT
eurjchem-976	412	7	j.	j.	PROPN
eurjchem-976	412	8	;	;	PUNCT
eurjchem-976	412	9	goya	goya	PROPN
eurjchem-976	412	10	,	,	PUNCT
eurjchem-976	412	11	p.	p.	PROPN
eurjchem-976	412	12	;	;	PUNCT
eurjchem-976	412	13	jagerovic	jagerovic	ADJ
eurjchem-976	412	14	,	,	PUNCT
eurjchem-976	412	15	n.	n.	NOUN
eurjchem-976	412	16	;	;	PUNCT
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eurjchem-976	412	29	.	.	PUNCT
eurjchem-976	413	1	in	in	ADP
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eurjchem-976	413	10	,	,	PUNCT
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eurjchem-976	413	12	,	,	PUNCT
eurjchem-976	413	13	o.	o.	PROPN
eurjchem-976	413	14	a.	a.	PROPN
eurjchem-976	413	15	;	;	PUNCT
eurjchem-976	413	16	spinelli	spinelli	PROPN
eurjchem-976	413	17	,	,	PUNCT
eurjchem-976	413	18	d.	d.	PROPN
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eurjchem-976	413	24	of	of	ADP
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eurjchem-976	413	26	,	,	PUNCT
eurjchem-976	413	27	roma	roma	PROPN
eurjchem-976	413	28	,	,	PUNCT
eurjchem-976	413	29	italy	italy	PROPN
eurjchem-976	413	30	,	,	PUNCT
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eurjchem-976	413	32	,	,	PUNCT
eurjchem-976	413	33	pp	pp	ADJ
eurjchem-976	413	34	.	.	PUNCT
eurjchem-976	414	1	52‐98	52‐98	NUM
eurjchem-976	414	2	.	.	PUNCT
eurjchem-976	415	1	[	[	X
eurjchem-976	415	2	6	6	NUM
eurjchem-976	415	3	]	]	PUNCT
eurjchem-976	415	4	.	.	PUNCT
eurjchem-976	416	1	ishii	ishii	PROPN
eurjchem-976	416	2	,	,	PUNCT
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eurjchem-976	416	4	;	;	PUNCT
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eurjchem-976	416	6	,	,	PUNCT
eurjchem-976	416	7	h.	h.	PROPN
eurjchem-976	416	8	;	;	PUNCT
eurjchem-976	416	9	tanaka	tanaka	PROPN
eurjchem-976	416	10	,	,	PUNCT
eurjchem-976	416	11	y.	y.	PROPN
eurjchem-976	416	12	;	;	PUNCT
eurjchem-976	416	13	ishikawa	ishikawa	PROPN
eurjchem-976	416	14	,	,	PUNCT
eurjchem-976	416	15	k.	k.	PROPN
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eurjchem-976	416	18	,	,	PUNCT
eurjchem-976	416	19	jp	jp	NOUN
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eurjchem-976	416	21	,	,	PUNCT
eurjchem-976	416	22	168	168	NUM
eurjchem-976	416	23	,	,	PUNCT
eurjchem-976	416	24	675	675	NUM
eurjchem-976	416	25	chem	chem	NOUN
eurjchem-976	416	26	.	.	PUNCT
eurjchem-976	417	1	abstr	abstr	PROPN
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eurjchem-976	417	8	35854	35854	NUM
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eurjchem-976	418	1	[	[	X
eurjchem-976	418	2	7	7	NUM
eurjchem-976	418	3	]	]	PUNCT
eurjchem-976	418	4	.	.	PUNCT
eurjchem-976	419	1	robin	robin	PROPN
eurjchem-976	419	2	,	,	PUNCT
eurjchem-976	419	3	e.	e.	PROPN
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eurjchem-976	419	5	;	;	PUNCT
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eurjchem-976	419	10	;	;	PUNCT
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eurjchem-976	419	12	,	,	PUNCT
eurjchem-976	419	13	s.	s.	PROPN
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eurjchem-976	419	20	.	.	PUNCT
eurjchem-976	420	1	[	[	X
eurjchem-976	420	2	8	8	NUM
eurjchem-976	420	3	]	]	PUNCT
eurjchem-976	420	4	.	.	PUNCT
eurjchem-976	421	1	karthikeyan	karthikeyan	PROPN
eurjchem-976	421	2	,	,	PUNCT
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eurjchem-976	421	5	;	;	PUNCT
eurjchem-976	421	6	holla	holla	PROPN
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eurjchem-976	421	8	b.	b.	PROPN
eurjchem-976	421	9	s.	s.	PROPN
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eurjchem-976	421	11	kumari	kumari	PROPN
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eurjchem-976	422	1	j.	j.	PROPN
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eurjchem-976	423	2	,	,	PUNCT
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eurjchem-976	423	4	,	,	PUNCT
eurjchem-976	423	5	30‐36	30‐36	NUM
eurjchem-976	423	6	.	.	PUNCT
eurjchem-976	424	1	[	[	X
eurjchem-976	424	2	9	9	NUM
eurjchem-976	424	3	]	]	PUNCT
eurjchem-976	424	4	.	.	PUNCT
eurjchem-976	425	1	gokhan‐kelekci	gokhan‐kelekci	VERB
eurjchem-976	425	2	,	,	PUNCT
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eurjchem-976	425	4	;	;	PUNCT
eurjchem-976	425	5	yabanoglu	yabanoglu	PROPN
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eurjchem-976	425	7	s.	s.	PROPN
eurjchem-976	425	8	;	;	PUNCT
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eurjchem-976	425	24	;	;	PUNCT
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eurjchem-976	425	28	;	;	PUNCT
eurjchem-976	425	29	kendi	kendi	PROPN
eurjchem-976	425	30	,	,	PUNCT
eurjchem-976	425	31	e.	e.	PROPN
eurjchem-976	425	32	;	;	PUNCT
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eurjchem-976	425	36	;	;	PUNCT
eurjchem-976	425	37	bilgin	bilgin	NOUN
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eurjchem-976	425	40	a.	a.	NOUN
eurjchem-976	425	41	bioorg	bioorg	PROPN
eurjchem-976	425	42	.	.	PUNCT
eurjchem-976	426	1	med	med	PROPN
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eurjchem-976	426	4	.	.	PUNCT
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eurjchem-976	427	2	,	,	PUNCT
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eurjchem-976	427	4	,	,	PUNCT
eurjchem-976	427	5	5775‐5786	5775‐5786	NUM
eurjchem-976	427	6	.	.	PUNCT
eurjchem-976	428	1	[	[	X
eurjchem-976	428	2	10	10	NUM
eurjchem-976	428	3	]	]	PUNCT
eurjchem-976	428	4	.	.	PUNCT
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eurjchem-976	429	2	,	,	PUNCT
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eurjchem-976	429	4	;	;	PUNCT
eurjchem-976	429	5	fan	fan	PROPN
eurjchem-976	429	6	,	,	PUNCT
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eurjchem-976	429	9	.	.	PUNCT
eurjchem-976	429	10	;	;	PUNCT
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eurjchem-976	429	17	zhao	zhao	PROPN
eurjchem-976	429	18	,	,	PUNCT
eurjchem-976	429	19	j.	j.	PROPN
eurjchem-976	429	20	;	;	PUNCT
eurjchem-976	429	21	shin	shin	PROPN
eurjchem-976	429	22	,	,	PUNCT
eurjchem-976	429	23	d.	d.	PROPN
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eurjchem-976	429	25	.	.	PUNCT
eurjchem-976	429	26	;	;	PUNCT
eurjchem-976	429	27	miao	miao	PROPN
eurjchem-976	429	28	,	,	PUNCT
eurjchem-976	429	29	j.	j.	PROPN
eurjchem-976	429	30	y.	y.	PROPN
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eurjchem-976	429	32	.	.	PUNCT
eurjchem-976	430	1	j.	j.	PROPN
eurjchem-976	430	2	med	med	PROPN
eurjchem-976	430	3	.	.	PROPN
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eurjchem-976	430	5	.	.	PUNCT
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eurjchem-976	431	2	,	,	PUNCT
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eurjchem-976	431	4	,	,	PUNCT
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eurjchem-976	431	6	.	.	PUNCT
eurjchem-976	432	1	[	[	X
eurjchem-976	432	2	11	11	NUM
eurjchem-976	432	3	]	]	PUNCT
eurjchem-976	432	4	.	.	PUNCT
eurjchem-976	433	1	huang	huang	PROPN
eurjchem-976	433	2	,	,	PUNCT
eurjchem-976	433	3	y.	y.	PROPN
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eurjchem-976	433	5	;	;	PUNCT
eurjchem-976	433	6	katzenellenbogen	katzenellenbogen	PROPN
eurjchem-976	433	7	,	,	PUNCT
eurjchem-976	433	8	j.	j.	PROPN
eurjchem-976	433	9	a.	a.	PROPN
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eurjchem-976	433	11	.	.	PUNCT
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eurjchem-976	435	2	,	,	PUNCT
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eurjchem-976	435	4	,	,	PUNCT
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eurjchem-976	435	6	.	.	PUNCT
eurjchem-976	436	1	[	[	X
eurjchem-976	436	2	12	12	NUM
eurjchem-976	436	3	]	]	PUNCT
eurjchem-976	436	4	.	.	PUNCT
eurjchem-976	437	1	sarojini	sarojini	PROPN
eurjchem-976	437	2	,	,	PUNCT
eurjchem-976	437	3	b.	b.	PROPN
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eurjchem-976	437	5	;	;	PUNCT
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eurjchem-976	437	12	c.	c.	PROPN
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eurjchem-976	437	14	;	;	PUNCT
eurjchem-976	437	15	bharath	bharath	PROPN
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eurjchem-976	437	17	b.	b.	PROPN
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eurjchem-976	437	24	.	.	PUNCT
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eurjchem-976	438	5	.	.	PUNCT
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eurjchem-976	439	2	,	,	PUNCT
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eurjchem-976	439	4	,	,	PUNCT
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eurjchem-976	439	6	.	.	PUNCT
eurjchem-976	440	1	[	[	X
eurjchem-976	440	2	13	13	NUM
eurjchem-976	440	3	]	]	PUNCT
eurjchem-976	440	4	.	.	PUNCT
eurjchem-976	440	5	behr	behr	PROPN
eurjchem-976	440	6	,	,	PUNCT
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eurjchem-976	440	9	;	;	PUNCT
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eurjchem-976	440	42	;	;	PUNCT
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eurjchem-976	442	1	[	[	X
eurjchem-976	442	2	14	14	NUM
eurjchem-976	442	3	]	]	PUNCT
eurjchem-976	442	4	.	.	PUNCT
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eurjchem-976	443	2	,	,	PUNCT
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eurjchem-976	443	4	;	;	PUNCT
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eurjchem-976	443	9	;	;	PUNCT
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eurjchem-976	444	2	.	.	PUNCT
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eurjchem-976	445	2	,	,	PUNCT
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eurjchem-976	445	4	,	,	PUNCT
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eurjchem-976	445	6	.	.	PUNCT
eurjchem-976	446	1	[	[	X
eurjchem-976	446	2	15	15	NUM
eurjchem-976	446	3	]	]	PUNCT
eurjchem-976	446	4	.	.	PUNCT
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eurjchem-976	447	4	;	;	PUNCT
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eurjchem-976	448	1	[	[	X
eurjchem-976	448	2	16	16	NUM
eurjchem-976	448	3	]	]	PUNCT
eurjchem-976	448	4	.	.	PUNCT
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eurjchem-976	449	5	;	;	PUNCT
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eurjchem-976	449	10	;	;	PUNCT
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eurjchem-976	450	2	,	,	PUNCT
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eurjchem-976	450	4	,	,	PUNCT
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eurjchem-976	450	6	.	.	PUNCT
eurjchem-976	451	1	[	[	X
eurjchem-976	451	2	17	17	NUM
eurjchem-976	451	3	]	]	PUNCT
eurjchem-976	451	4	.	.	PUNCT
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eurjchem-976	452	1	j.	j.	PROPN
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eurjchem-976	454	6	.	.	PUNCT
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eurjchem-976	455	2	18	18	NUM
eurjchem-976	455	3	]	]	PUNCT
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eurjchem-976	455	16	nermien	nermien	PROPN
eurjchem-976	455	17	,	,	PUNCT
eurjchem-976	455	18	m.	m.	NOUN
eurjchem-976	455	19	s.	s.	PROPN
eurjchem-976	455	20	;	;	PUNCT
eurjchem-976	455	21	mohamed	mohamed	PROPN
eurjchem-976	455	22	,	,	PUNCT
eurjchem-976	455	23	m.	m.	NOUN
eurjchem-976	455	24	eur	eur	PROPN
eurjchem-976	455	25	.	.	PUNCT
eurjchem-976	456	1	j.	j.	PROPN
eurjchem-976	456	2	med	med	PROPN
eurjchem-976	456	3	.	.	PROPN
eurjchem-976	456	4	chem	chem	PROPN
eurjchem-976	456	5	.	.	PUNCT
eurjchem-976	457	1	2009	2009	NUM
eurjchem-976	457	2	,	,	PUNCT
eurjchem-976	457	3	44	44	NUM
eurjchem-976	457	4	,	,	PUNCT
eurjchem-976	457	5	4787‐4792	4787‐4792	NUM
eurjchem-976	457	6	.	.	PUNCT
eurjchem-976	458	1	[	[	X
eurjchem-976	458	2	19	19	NUM
eurjchem-976	458	3	]	]	PUNCT
eurjchem-976	458	4	.	.	PUNCT
eurjchem-976	459	1	barcelo	barcelo	PROPN
eurjchem-976	459	2	,	,	PUNCT
eurjchem-976	459	3	m.	m.	NOUN
eurjchem-976	459	4	;	;	PUNCT
eurjchem-976	459	5	ravina	ravina	PROPN
eurjchem-976	459	6	,	,	PUNCT
eurjchem-976	459	7	e.	e.	PROPN
eurjchem-976	459	8	;	;	PUNCT
eurjchem-976	459	9	masaguer	masaguer	PROPN
eurjchem-976	459	10	,	,	PUNCT
eurjchem-976	459	11	c.	c.	PROPN
eurjchem-976	459	12	f.	f.	PROPN
eurjchem-976	459	13	;	;	PUNCT
eurjchem-976	459	14	dominuez	dominuez	PROPN
eurjchem-976	459	15	,	,	PUNCT
eurjchem-976	459	16	e.	e.	PROPN
eurjchem-976	459	17	;	;	PUNCT
eurjchem-976	459	18	areias	areias	PROPN
eurjchem-976	459	19	,	,	PUNCT
eurjchem-976	459	20	f.	f.	PROPN
eurjchem-976	459	21	m.	m.	PROPN
eurjchem-976	459	22	;	;	PUNCT
eurjchem-976	459	23	brea	brea	PROPN
eurjchem-976	459	24	,	,	PUNCT
eurjchem-976	459	25	j.	j.	PROPN
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eurjchem-976	459	27	loza	loza	PROPN
eurjchem-976	459	28	,	,	PUNCT
eurjchem-976	459	29	m.	m.	NOUN
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eurjchem-976	459	31	.	.	PUNCT
eurjchem-976	460	1	bioorg	bioorg	PROPN
eurjchem-976	460	2	.	.	PUNCT
eurjchem-976	461	1	med	med	PROPN
eurjchem-976	461	2	.	.	PROPN
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eurjchem-976	461	4	.	.	PUNCT
eurjchem-976	462	1	lett	lett	PROPN
eurjchem-976	462	2	.	.	PUNCT
eurjchem-976	463	1	2007	2007	NUM
eurjchem-976	463	2	,	,	PUNCT
eurjchem-976	463	3	17	17	NUM
eurjchem-976	463	4	,	,	PUNCT
eurjchem-976	463	5	4873‐4877	4873‐4877	NUM
eurjchem-976	463	6	.	.	PUNCT
eurjchem-976	464	1	[	[	X
eurjchem-976	464	2	20	20	NUM
eurjchem-976	464	3	]	]	PUNCT
eurjchem-976	464	4	.	.	PUNCT
eurjchem-976	465	1	chou	chou	PROPN
eurjchem-976	465	2	,	,	PUNCT
eurjchem-976	465	3	l.	l.	PROPN
eurjchem-976	465	4	‐c	‐c	PROPN
eurjchem-976	465	5	.	.	PROPN
eurjchem-976	465	6	;	;	PUNCT
eurjchem-976	465	7	huang	huang	PROPN
eurjchem-976	465	8	,	,	PUNCT
eurjchem-976	465	9	l.	l.	PROPN
eurjchem-976	465	10	‐j	‐j	PROPN
eurjchem-976	465	11	.	.	PROPN
eurjchem-976	465	12	;	;	PUNCT
eurjchem-976	465	13	yang	yang	PROPN
eurjchem-976	465	14	,	,	PUNCT
eurjchem-976	465	15	j.	j.	PROPN
eurjchem-976	465	16	‐s	‐s	PROPN
eurjchem-976	465	17	.	.	PUNCT
eurjchem-976	465	18	;	;	PUNCT
eurjchem-976	465	19	lee	lee	PROPN
eurjchem-976	465	20	,	,	PUNCT
eurjchem-976	465	21	f.	f.	PROPN
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eurjchem-976	465	23	.	.	PUNCT
eurjchem-976	465	24	;	;	PUNCT
eurjchem-976	466	1	teng	teng	PROPN
eurjchem-976	466	2	,	,	PUNCT
eurjchem-976	466	3	c.	c.	PROPN
eurjchem-976	466	4	‐m	‐m	PROPN
eurjchem-976	466	5	.	.	PUNCT
eurjchem-976	466	6	;	;	PUNCT
eurjchem-976	466	7	kuo	kuo	PROPN
eurjchem-976	466	8	,	,	PUNCT
eurjchem-976	466	9	s.	s.	PROPN
eurjchem-976	466	10	‐c	‐c	PROPN
eurjchem-976	466	11	.	.	PUNCT
eurjchem-976	467	1	bioorg	bioorg	PROPN
eurjchem-976	467	2	.	.	PUNCT
eurjchem-976	468	1	med	med	PROPN
eurjchem-976	468	2	.	.	PROPN
eurjchem-976	468	3	chem	chem	PROPN
eurjchem-976	468	4	.	.	PUNCT
eurjchem-976	469	1	2007	2007	NUM
eurjchem-976	469	2	,	,	PUNCT
eurjchem-976	469	3	15	15	NUM
eurjchem-976	469	4	,	,	PUNCT
eurjchem-976	469	5	1732‐1740	1732‐1740	NUM
eurjchem-976	469	6	.	.	PUNCT
eurjchem-976	470	1	[	[	X
eurjchem-976	470	2	21	21	NUM
eurjchem-976	470	3	]	]	PUNCT
eurjchem-976	470	4	.	.	PUNCT
eurjchem-976	471	1	narasimhulu	narasimhulu	VERB
eurjchem-976	471	2	,	,	PUNCT
eurjchem-976	471	3	b.	b.	PROPN
eurjchem-976	471	4	n.	n.	PROPN
eurjchem-976	471	5	;	;	PUNCT
eurjchem-976	471	6	jacques	jacques	PROPN
eurjchem-976	471	7	,	,	PUNCT
eurjchem-976	471	8	b.	b.	PROPN
eurjchem-976	471	9	;	;	PUNCT
eurjchem-976	471	10	francis	francis	PROPN
eurjchem-976	471	11	,	,	PUNCT
eurjchem-976	471	12	b.	b.	PROPN
eurjchem-976	471	13	;	;	PUNCT
eurjchem-976	471	14	timothy	timothy	PROPN
eurjchem-976	471	15	,	,	PUNCT
eurjchem-976	471	16	p.	p.	PROPN
eurjchem-976	471	17	c.	c.	PROPN
eurjchem-976	471	18	;	;	PUNCT
eurjchem-976	471	19	mark	mark	PROPN
eurjchem-976	471	20	,	,	PUNCT
eurjchem-976	471	21	r.	r.	PROPN
eurjchem-976	471	22	k.	k.	PROPN
eurjchem-976	471	23	;	;	PUNCT
eurjchem-976	471	24	john	john	PROPN
eurjchem-976	471	25	,	,	PUNCT
eurjchem-976	471	26	d.	d.	PROPN
eurjchem-976	471	27	m.	m.	PROPN
eurjchem-976	471	28	;	;	PUNCT
eurjchem-976	471	29	carl	carl	PROPN
eurjchem-976	471	30	,	,	PUNCT
eurjchem-976	471	31	o.	o.	PROPN
eurjchem-976	471	32	;	;	PUNCT
eurjchem-976	471	33	serge	serge	PROPN
eurjchem-976	471	34	,	,	PUNCT
eurjchem-976	471	35	p.	p.	PROPN
eurjchem-976	471	36	;	;	PUNCT
eurjchem-976	471	37	roger	roger	PROPN
eurjchem-976	471	38	,	,	PUNCT
eurjchem-976	471	39	r.	r.	PROPN
eurjchem-976	471	40	;	;	PUNCT
eurjchem-976	471	41	margaret	margaret	PROPN
eurjchem-976	471	42	,	,	PUNCT
eurjchem-976	471	43	e.	e.	PROPN
eurjchem-976	471	44	s.	s.	PROPN
eurjchem-976	471	45	;	;	PUNCT
eurjchem-976	471	46	yasutsugu	yasutsugu	ADJ
eurjchem-976	471	47	,	,	PUNCT
eurjchem-976	471	48	u.	u.	PROPN
eurjchem-976	471	49	;	;	PUNCT
eurjchem-976	471	50	michael	michael	PROPN
eurjchem-976	471	51	,	,	PUNCT
eurjchem-976	471	52	a.	a.	PROPN
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eurjchem-976	471	56	patent	patent	NOUN
eurjchem-976	471	57	7511037	7511037	NUM
eurjchem-976	471	58	,	,	PUNCT
eurjchem-976	471	59	us	we	PRON
eurjchem-976	471	60	7	7	NUM
eurjchem-976	471	61	,	,	PUNCT
eurjchem-976	471	62	511	511	NUM
eurjchem-976	471	63	,	,	PUNCT
eurjchem-976	471	64	037b2	037b2	NUM
eurjchem-976	471	65	,	,	PUNCT
eurjchem-976	471	66	2009	2009	NUM
eurjchem-976	471	67	.	.	PUNCT
eurjchem-976	472	1	[	[	X
eurjchem-976	472	2	22	22	NUM
eurjchem-976	472	3	]	]	PUNCT
eurjchem-976	472	4	.	.	PUNCT
eurjchem-976	473	1	moser	moser	PROPN
eurjchem-976	473	2	,	,	PUNCT
eurjchem-976	473	3	h.	h.	PROPN
eurjchem-976	473	4	;	;	PUNCT
eurjchem-976	473	5	boehner	boehner	PROPN
eurjchem-976	473	6	,	,	PUNCT
eurjchem-976	473	7	b.	b.	PROPN
eurjchem-976	473	8	;	;	PUNCT
eurjchem-976	473	9	foery	foery	PROPN
eurjchem-976	473	10	,	,	PUNCT
eurjchem-976	473	11	w.	w.	PROPN
eurjchem-976	473	12	;	;	PUNCT
eurjchem-976	473	13	european	european	PROPN
eurjchem-976	473	14	patent	patent	NOUN
eurjchem-976	473	15	,	,	PUNCT
eurjchem-976	473	16	ep	ep	PROPN
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eurjchem-976	473	18	,	,	PUNCT
eurjchem-976	473	19	554	554	NUM
eurjchem-976	473	20	,	,	PUNCT
eurjchem-976	473	21	chem	chem	NOUN
eurjchem-976	473	22	.	.	PUNCT
eurjchem-976	474	1	abstr	abstr	PROPN
eurjchem-976	474	2	.	.	PROPN
eurjchem-976	474	3	,	,	PUNCT
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eurjchem-976	474	5	,	,	PUNCT
eurjchem-976	474	6	110	110	NUM
eurjchem-976	474	7	,	,	PUNCT
eurjchem-976	474	8	23879	23879	NUM
eurjchem-976	474	9	.	.	PUNCT
eurjchem-976	475	1	286	286	NUM
eurjchem-976	475	2	el‐aal	el‐aal	PROPN
eurjchem-976	475	3	et	et	NOUN
eurjchem-976	475	4	al	al	PROPN
eurjchem-976	475	5	.	.	PUNCT
eurjchem-976	475	6	/	/	SYM
eurjchem-976	475	7	european	european	PROPN
eurjchem-976	475	8	journal	journal	PROPN
eurjchem-976	475	9	of	of	ADP
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eurjchem-976	475	12	(	(	PUNCT
eurjchem-976	475	13	2	2	NUM
eurjchem-976	475	14	)	)	PUNCT
eurjchem-976	475	15	(	(	PUNCT
eurjchem-976	475	16	2014	2014	NUM
eurjchem-976	475	17	)	)	PUNCT
eurjchem-976	475	18	277‐286	277‐286	NUM
eurjchem-976	476	1	[	[	X
eurjchem-976	476	2	23	23	NUM
eurjchem-976	476	3	]	]	PUNCT
eurjchem-976	476	4	.	.	PUNCT
eurjchem-976	476	5	natsume	natsume	PROPN
eurjchem-976	476	6	,	,	PUNCT
eurjchem-976	476	7	b.	b.	PROPN
eurjchem-976	476	8	;	;	PUNCT
eurjchem-976	476	9	kyomura	kyomura	NOUN
eurjchem-976	476	10	,	,	PUNCT
eurjchem-976	476	11	n.	n.	NOUN
eurjchem-976	476	12	;	;	PUNCT
eurjchem-976	476	13	kikutake	kikutake	PROPN
eurjchem-976	476	14	,	,	PUNCT
eurjchem-976	476	15	k.	k.	PROPN
eurjchem-976	476	16	;	;	PUNCT
eurjchem-976	476	17	fukuch	fukuch	PROPN
eurjchem-976	476	18	,	,	PUNCT
eurjchem-976	476	19	t.	t.	PROPN
eurjchem-976	476	20	eur	eur	PROPN
eurjchem-976	476	21	.	.	PUNCT
eurjchem-976	477	1	pat	pat	PROPN
eurjchem-976	477	2	.	.	PROPN
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eurjchem-976	477	4	.	.	PUNCT
eurjchem-976	478	1	ep	ep	PROPN
eurjchem-976	478	2	.	.	PROPN
eurjchem-976	478	3	,	,	PUNCT
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eurjchem-976	478	5	,	,	PUNCT
eurjchem-976	478	6	573	573	NUM
eurjchem-976	478	7	,	,	PUNCT
eurjchem-976	478	8	chem	chem	NOUN
eurjchem-976	478	9	.	.	PUNCT
eurjchem-976	479	1	abstr	abstr	PROPN
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eurjchem-976	479	3	,	,	PUNCT
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eurjchem-976	479	5	,	,	PUNCT
eurjchem-976	479	6	116	116	NUM
eurjchem-976	479	7	,	,	PUNCT
eurjchem-976	479	8	128	128	NUM
eurjchem-976	479	9	.	.	PUNCT
eurjchem-976	480	1	[	[	X
eurjchem-976	480	2	24	24	NUM
eurjchem-976	480	3	]	]	PUNCT
eurjchem-976	480	4	.	.	PUNCT
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eurjchem-976	481	7	,	,	PUNCT
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eurjchem-976	481	10	,	,	PUNCT
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eurjchem-976	481	12	and	and	CCONJ
eurjchem-976	481	13	co.	co.	PROPN
eurjchem-976	481	14	,	,	PUNCT
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eurjchem-976	481	17	new	new	PROPN
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eurjchem-976	481	19	,	,	PUNCT
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eurjchem-976	481	21	.	.	PUNCT
eurjchem-976	482	1	[	[	X
eurjchem-976	482	2	25	25	NUM
eurjchem-976	482	3	]	]	PUNCT
eurjchem-976	482	4	.	.	PUNCT
eurjchem-976	483	1	kim	kim	PROPN
eurjchem-976	483	2	,	,	PUNCT
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eurjchem-976	483	4	;	;	PUNCT
eurjchem-976	483	5	sim	sim	PROPN
eurjchem-976	483	6	,	,	PUNCT
eurjchem-976	483	7	c.	c.	PROPN
eurjchem-976	483	8	;	;	PUNCT
eurjchem-976	483	9	shin	shin	PROPN
eurjchem-976	483	10	,	,	PUNCT
eurjchem-976	483	11	d.	d.	PROPN
eurjchem-976	483	12	;	;	PUNCT
eurjchem-976	483	13	suh	suh	PROPN
eurjchem-976	483	14	,	,	PUNCT
eurjchem-976	483	15	e.	e.	PROPN
eurjchem-976	483	16	;	;	PUNCT
eurjchem-976	483	17	cho	cho	PROPN
eurjchem-976	483	18	,	,	PUNCT
eurjchem-976	483	19	k.	k.	PROPN
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eurjchem-976	483	23	,	,	PUNCT
eurjchem-976	483	24	25	25	NUM
eurjchem-976	483	25	,	,	PUNCT
eurjchem-976	483	26	542‐	542‐	NUM
eurjchem-976	483	27	548	548	NUM
eurjchem-976	483	28	.	.	PUNCT
eurjchem-976	484	1	[	[	X
eurjchem-976	484	2	26	26	NUM
eurjchem-976	484	3	]	]	PUNCT
eurjchem-976	484	4	.	.	PUNCT
eurjchem-976	485	1	fahmy	fahmy	PROPN
eurjchem-976	485	2	,	,	PUNCT
eurjchem-976	485	3	s.	s.	PROPN
eurjchem-976	485	4	m.	m.	PROPN
eurjchem-976	485	5	;	;	PUNCT
eurjchem-976	485	6	badran	badran	VERB
eurjchem-976	485	7	,	,	PUNCT
eurjchem-976	485	8	a.	a.	PROPN
eurjchem-976	485	9	h.	h.	PROPN
eurjchem-976	485	10	;	;	PUNCT
eurjchem-976	486	1	elnagdi	elnagdi	PROPN
eurjchem-976	486	2	,	,	PUNCT
eurjchem-976	486	3	m.	m.	NOUN
eurjchem-976	486	4	h.	h.	PROPN
eurjchem-976	486	5	j.	j.	PROPN
eurjchem-976	486	6	chem	chem	PROPN
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eurjchem-976	486	8	.	.	PUNCT
eurjchem-976	487	1	b	b	X
eurjchem-976	487	2	:	:	PUNCT
eurjchem-976	487	3	technol	technol	ADJ
eurjchem-976	487	4	.	.	PUNCT
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eurjchem-976	487	6	,	,	PUNCT
eurjchem-976	487	7	30	30	NUM
eurjchem-976	487	8	,	,	PUNCT
eurjchem-976	487	9	390‐395	390‐395	NUM
eurjchem-976	487	10	.	.	PUNCT
eurjchem-976	488	1	[	[	X
eurjchem-976	488	2	27	27	NUM
eurjchem-976	488	3	]	]	PUNCT
eurjchem-976	488	4	.	.	PUNCT
eurjchem-976	489	1	eicher	eicher	PROPN
eurjchem-976	489	2	,	,	PUNCT
eurjchem-976	489	3	t.	t.	PROPN
eurjchem-976	489	4	;	;	PUNCT
eurjchem-976	489	5	hauptmann	hauptmann	PROPN
eurjchem-976	489	6	,	,	PUNCT
eurjchem-976	489	7	s.	s.	PROPN
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eurjchem-976	489	12	:	:	PUNCT
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eurjchem-976	489	14	,	,	PUNCT
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eurjchem-976	489	16	,	,	PUNCT
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eurjchem-976	489	18	,	,	PUNCT
eurjchem-976	489	19	and	and	CCONJ
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eurjchem-976	489	21	,	,	PUNCT
eurjchem-976	489	22	2nd	2nd	PROPN
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eurjchem-976	489	24	,	,	PUNCT
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eurjchem-976	489	26	,	,	PUNCT
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eurjchem-976	489	31	.	.	PUNCT
eurjchem-976	490	1	[	[	X
eurjchem-976	490	2	28	28	NUM
eurjchem-976	490	3	]	]	PUNCT
eurjchem-976	490	4	.	.	PUNCT
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eurjchem-976	491	2	,	,	PUNCT
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eurjchem-976	491	4	j.	j.	PROPN
eurjchem-976	491	5	ann	ann	PROPN
eurjchem-976	491	6	.	.	PROPN
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eurjchem-976	491	8	.	.	PUNCT
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eurjchem-976	491	10	,	,	PUNCT
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eurjchem-976	492	1	[	[	X
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eurjchem-976	492	3	]	]	PUNCT
eurjchem-976	492	4	.	.	PUNCT
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eurjchem-976	493	2	,	,	PUNCT
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eurjchem-976	493	4	k.	k.	PROPN
eurjchem-976	493	5	;	;	PUNCT
eurjchem-976	493	6	vicente	vicente	PROPN
eurjchem-976	493	7	,	,	PUNCT
eurjchem-976	493	8	d.	d.	PROPN
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eurjchem-976	493	10	;	;	PUNCT
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eurjchem-976	493	17	.	.	PUNCT
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eurjchem-976	494	2	,	,	PUNCT
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eurjchem-976	494	4	,	,	PUNCT
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eurjchem-976	494	6	.	.	PUNCT
eurjchem-976	495	1	[	[	X
eurjchem-976	495	2	30	30	NUM
eurjchem-976	495	3	]	]	PUNCT
eurjchem-976	495	4	.	.	PUNCT
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eurjchem-976	496	2	,	,	PUNCT
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eurjchem-976	496	7	,	,	PUNCT
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eurjchem-976	496	14	a.	a.	PROPN
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eurjchem-976	496	19	c.	c.	PROPN
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eurjchem-976	496	23	,	,	PUNCT
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eurjchem-976	496	26	,	,	PUNCT
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eurjchem-976	496	30	,	,	PUNCT
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eurjchem-976	496	32	.	.	PUNCT
eurjchem-976	497	1	167‐303	167‐303	NUM
eurjchem-976	497	2	.	.	PUNCT
eurjchem-976	498	1	[	[	X
eurjchem-976	498	2	31	31	NUM
eurjchem-976	498	3	]	]	PUNCT
eurjchem-976	498	4	.	.	PUNCT
eurjchem-976	499	1	deng	deng	PROPN
eurjchem-976	499	2	,	,	PUNCT
eurjchem-976	499	3	x.	x.	PROPN
eurjchem-976	499	4	;	;	PUNCT
eurjchem-976	499	5	mani	mani	NOUN
eurjchem-976	499	6	,	,	PUNCT
eurjchem-976	499	7	n.	n.	PROPN
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eurjchem-976	499	10	.	.	PUNCT
eurjchem-976	500	1	lett	lett	PROPN
eurjchem-976	500	2	.	.	PUNCT
eurjchem-976	501	1	2006	2006	NUM
eurjchem-976	501	2	,	,	PUNCT
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eurjchem-976	501	4	,	,	PUNCT
eurjchem-976	501	5	3505‐3508	3505‐3508	NUM
eurjchem-976	501	6	.	.	PUNCT
eurjchem-976	502	1	[	[	X
eurjchem-976	502	2	32	32	NUM
eurjchem-976	502	3	]	]	PUNCT
eurjchem-976	502	4	.	.	PUNCT
eurjchem-976	503	1	noguchi	noguchi	PROPN
eurjchem-976	503	2	,	,	PUNCT
eurjchem-976	503	3	m.	m.	NOUN
eurjchem-976	503	4	;	;	PUNCT
eurjchem-976	503	5	sunagawa	sunagawa	PROPN
eurjchem-976	503	6	,	,	PUNCT
eurjchem-976	503	7	t.	t.	PROPN
eurjchem-976	503	8	;	;	PUNCT
eurjchem-976	503	9	akao	akao	NOUN
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eurjchem-976	503	12	;	;	PUNCT
eurjchem-976	503	13	yamada	yamada	PROPN
eurjchem-976	503	14	,	,	PUNCT
eurjchem-976	503	15	h.	h.	PROPN
eurjchem-976	503	16	;	;	PUNCT
eurjchem-976	503	17	yamamoto	yamamoto	PROPN
eurjchem-976	503	18	,	,	PUNCT
eurjchem-976	503	19	h.	h.	PROPN
eurjchem-976	503	20	;	;	PUNCT
eurjchem-976	503	21	kakehi	kakehi	PROPN
eurjchem-976	503	22	,	,	PUNCT
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eurjchem-976	503	26	,	,	PUNCT
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eurjchem-976	503	28	,	,	PUNCT
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eurjchem-976	503	30	.	.	PUNCT
eurjchem-976	504	1	[	[	X
eurjchem-976	504	2	33	33	NUM
eurjchem-976	504	3	]	]	PUNCT
eurjchem-976	504	4	.	.	PUNCT
eurjchem-976	505	1	bhat	bhat	PROPN
eurjchem-976	505	2	,	,	PUNCT
eurjchem-976	505	3	b.	b.	PROPN
eurjchem-976	505	4	a.	a.	PROPN
eurjchem-976	505	5	;	;	PUNCT
eurjchem-976	505	6	puri	puri	PROPN
eurjchem-976	505	7	,	,	PUNCT
eurjchem-976	505	8	s.	s.	PROPN
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eurjchem-976	505	10	;	;	PUNCT
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eurjchem-976	505	12	,	,	PUNCT
eurjchem-976	505	13	m.	m.	NOUN
eurjchem-976	505	14	a.	a.	PROPN
eurjchem-976	505	15	;	;	PUNCT
eurjchem-976	505	16	dhar	dhar	PROPN
eurjchem-976	505	17	,	,	PUNCT
eurjchem-976	505	18	k.	k.	PROPN
eurjchem-976	505	19	l.	l.	PROPN
eurjchem-976	505	20	;	;	PUNCT
eurjchem-976	505	21	qazi	qazi	PROPN
eurjchem-976	505	22	,	,	PUNCT
eurjchem-976	505	23	g.	g.	PROPN
eurjchem-976	505	24	n.	n.	PROPN
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eurjchem-976	505	26	.	.	PUNCT
eurjchem-976	506	1	commun	commun	PROPN
eurjchem-976	506	2	.	.	PUNCT
eurjchem-976	507	1	2005	2005	NUM
eurjchem-976	507	2	,	,	PUNCT
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eurjchem-976	507	4	,	,	PUNCT
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eurjchem-976	507	6	.	.	PUNCT
eurjchem-976	508	1	[	[	X
eurjchem-976	508	2	34	34	NUM
eurjchem-976	508	3	]	]	PUNCT
eurjchem-976	508	4	.	.	PUNCT
eurjchem-976	509	1	almazroa	almazroa	PROPN
eurjchem-976	509	2	,	,	PUNCT
eurjchem-976	509	3	s.	s.	PROPN
eurjchem-976	509	4	;	;	PUNCT
eurjchem-976	509	5	elnagdi	elnagdi	PROPN
eurjchem-976	509	6	,	,	PUNCT
eurjchem-976	509	7	m.	m.	PROPN
eurjchem-976	509	8	h.	h.	PROPN
eurjchem-976	509	9	;	;	PUNCT
eurjchem-976	509	10	salah	salah	PROPN
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eurjchem-976	509	12	,	,	PUNCT
eurjchem-976	509	13	a.	a.	NOUN
eurjchem-976	509	14	m.	m.	PROPN
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eurjchem-976	509	17	.	.	PUNCT
eurjchem-976	510	1	chem	chem	PROPN
eurjchem-976	510	2	.	.	PUNCT
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eurjchem-976	511	2	,	,	PUNCT
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eurjchem-976	511	4	,	,	PUNCT
eurjchem-976	511	5	267‐272	267‐272	NUM
eurjchem-976	511	6	.	.	PUNCT
eurjchem-976	512	1	[	[	X
eurjchem-976	512	2	35	35	NUM
eurjchem-976	512	3	]	]	SYM
eurjchem-976	512	4	.	.	PUNCT
eurjchem-976	513	1	fustero	fustero	PROPN
eurjchem-976	513	2	,	,	PUNCT
eurjchem-976	513	3	s.	s.	PROPN
eurjchem-976	513	4	;	;	PUNCT
eurjchem-976	513	5	roman	roman	PROPN
eurjchem-976	513	6	,	,	PUNCT
eurjchem-976	513	7	r.	r.	PROPN
eurjchem-976	513	8	;	;	PUNCT
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eurjchem-976	513	11	j.	j.	PROPN
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eurjchem-976	513	13	;	;	PUNCT
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eurjchem-976	513	18	;	;	PUNCT
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eurjchem-976	513	21	a.	a.	PROPN
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eurjchem-976	513	23	;	;	PUNCT
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eurjchem-976	513	25	,	,	PUNCT
eurjchem-976	513	26	s.	s.	PROPN
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eurjchem-976	513	29	,	,	PUNCT
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eurjchem-976	513	33	.	.	PUNCT
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eurjchem-976	514	2	,	,	PUNCT
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eurjchem-976	514	4	,	,	PUNCT
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eurjchem-976	514	6	.	.	PUNCT
eurjchem-976	515	1	[	[	X
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eurjchem-976	515	4	.	.	PUNCT
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eurjchem-976	516	6	;	;	PUNCT
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eurjchem-976	516	8	,	,	PUNCT
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eurjchem-976	516	10	;	;	PUNCT
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eurjchem-976	516	13	a.	a.	NOUN
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eurjchem-976	517	2	.	.	PUNCT
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eurjchem-976	518	2	,	,	PUNCT
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eurjchem-976	518	4	,	,	PUNCT
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eurjchem-976	518	6	.	.	PUNCT
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eurjchem-976	519	4	.	.	PUNCT
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eurjchem-976	520	2	,	,	PUNCT
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eurjchem-976	520	4	;	;	PUNCT
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eurjchem-976	520	9	.	.	PUNCT
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eurjchem-976	521	4	.	.	PUNCT
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eurjchem-976	522	2	,	,	PUNCT
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eurjchem-976	522	6	.	.	PUNCT
eurjchem-976	523	1	[	[	X
eurjchem-976	523	2	38	38	NUM
eurjchem-976	523	3	]	]	PUNCT
eurjchem-976	523	4	.	.	PUNCT
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eurjchem-976	524	5	;	;	PUNCT
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eurjchem-976	524	8	d.	d.	PROPN
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eurjchem-976	524	10	;	;	PUNCT
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eurjchem-976	524	13	s.	s.	PROPN
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eurjchem-976	524	15	;	;	PUNCT
eurjchem-976	524	16	huang	huang	PROPN
eurjchem-976	524	17	,	,	PUNCT
eurjchem-976	524	18	z.	z.	PROPN
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eurjchem-976	524	20	;	;	PUNCT
eurjchem-976	524	21	ji	ji	PROPN
eurjchem-976	524	22	,	,	PUNCT
eurjchem-976	524	23	s.	s.	PROPN
eurjchem-976	524	24	j.	j.	PROPN
eurjchem-976	524	25	;	;	PUNCT
eurjchem-976	524	26	ji	ji	PROPN
eurjchem-976	524	27	,	,	PUNCT
eurjchem-976	524	28	m.	m.	NOUN
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eurjchem-976	524	30	,	,	PUNCT
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eurjchem-976	524	32	,	,	PUNCT
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eurjchem-976	524	36	.	.	PUNCT
eurjchem-976	525	1	[	[	X
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eurjchem-976	525	3	]	]	PUNCT
eurjchem-976	525	4	.	.	PUNCT
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eurjchem-976	526	2	,	,	PUNCT
eurjchem-976	526	3	p.	p.	NOUN
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eurjchem-976	526	5	;	;	PUNCT
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eurjchem-976	526	9	;	;	PUNCT
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eurjchem-976	526	13	;	;	PUNCT
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eurjchem-976	526	17	;	;	PUNCT
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eurjchem-976	526	19	,	,	PUNCT
eurjchem-976	526	20	j.	j.	PROPN
eurjchem-976	526	21	;	;	PUNCT
eurjchem-976	526	22	cuny	cuny	PROPN
eurjchem-976	526	23	,	,	PUNCT
eurjchem-976	526	24	g.	g.	PROPN
eurjchem-976	526	25	d.	d.	PROPN
eurjchem-976	526	26	j.	j.	PROPN
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eurjchem-976	526	28	.	.	PROPN
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eurjchem-976	526	30	.	.	PUNCT
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eurjchem-976	527	2	,	,	PUNCT
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eurjchem-976	527	6	.	.	PUNCT
eurjchem-976	528	1	[	[	X
eurjchem-976	528	2	40	40	NUM
eurjchem-976	528	3	]	]	PUNCT
eurjchem-976	528	4	.	.	PUNCT
eurjchem-976	529	1	el‐rayyes	el‐rayyes	PROPN
eurjchem-976	529	2	,	,	PUNCT
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eurjchem-976	529	8	a.	a.	PROPN
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eurjchem-976	529	11	.	.	PUNCT
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eurjchem-976	530	2	.	.	PUNCT
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eurjchem-976	531	2	,	,	PUNCT
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eurjchem-976	531	4	,	,	PUNCT
eurjchem-976	531	5	135‐140	135‐140	NUM
eurjchem-976	531	6	.	.	PUNCT
eurjchem-976	532	1	[	[	X
eurjchem-976	532	2	41	41	NUM
eurjchem-976	532	3	]	]	PUNCT
eurjchem-976	532	4	.	.	PUNCT
eurjchem-976	533	1	klimova	klimova	PROPN
eurjchem-976	533	2	,	,	PUNCT
eurjchem-976	533	3	e.	e.	PROPN
eurjchem-976	533	4	i.	i.	PROPN
eurjchem-976	533	5	;	;	PUNCT
eurjchem-976	533	6	klimova	klimova	PROPN
eurjchem-976	533	7	,	,	PUNCT
eurjchem-976	533	8	t.	t.	PROPN
eurjchem-976	533	9	;	;	PUNCT
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eurjchem-976	533	18	e.	e.	PROPN
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eurjchem-976	533	25	;	;	PUNCT
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eurjchem-976	533	29	j.	j.	PROPN
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eurjchem-976	533	38	.	.	PUNCT
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eurjchem-976	534	2	.	.	PUNCT
eurjchem-976	535	1	2003	2003	NUM
eurjchem-976	535	2	,	,	PUNCT
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eurjchem-976	535	4	,	,	PUNCT
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eurjchem-976	536	1	[	[	X
eurjchem-976	536	2	42	42	NUM
eurjchem-976	536	3	]	]	PUNCT
eurjchem-976	536	4	.	.	PUNCT
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eurjchem-976	537	2	,	,	PUNCT
eurjchem-976	537	3	s.	s.	PROPN
eurjchem-976	537	4	;	;	PUNCT
eurjchem-976	537	5	brecht	brecht	PROPN
eurjchem-976	537	6	,	,	PUNCT
eurjchem-976	537	7	r.	r.	PROPN
eurjchem-976	537	8	;	;	PUNCT
eurjchem-976	537	9	büttner	büttner	PROPN
eurjchem-976	537	10	,	,	PUNCT
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eurjchem-976	537	12	;	;	PUNCT
eurjchem-976	537	13	guenard	guenard	PROPN
eurjchem-976	537	14	,	,	PUNCT
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eurjchem-976	537	16	;	;	PUNCT
eurjchem-976	537	17	gust	gust	PROPN
eurjchem-976	537	18	,	,	PUNCT
eurjchem-976	537	19	r.	r.	PROPN
eurjchem-976	537	20	;	;	PUNCT
eurjchem-976	537	21	seitz	seitz	PROPN
eurjchem-976	537	22	,	,	PUNCT
eurjchem-976	537	23	g.	g.	PROPN
eurjchem-976	537	24	;	;	PUNCT
eurjchem-976	537	25	stubbs	stubbs	PROPN
eurjchem-976	537	26	,	,	PUNCT
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eurjchem-976	537	28	t.	t.	PROPN
eurjchem-976	537	29	;	;	PUNCT
eurjchem-976	537	30	thoret	thoret	PROPN
eurjchem-976	537	31	,	,	PUNCT
eurjchem-976	537	32	s.	s.	PROPN
eurjchem-976	537	33	,	,	PUNCT
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eurjchem-976	537	35	.	.	PUNCT
eurjchem-976	538	1	med	med	PROPN
eurjchem-976	538	2	.	.	PROPN
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eurjchem-976	538	4	.	.	PUNCT
eurjchem-976	539	1	2003	2003	NUM
eurjchem-976	539	2	,	,	PUNCT
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eurjchem-976	539	4	,	,	PUNCT
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eurjchem-976	539	6	.	.	PUNCT
eurjchem-976	540	1	[	[	X
eurjchem-976	540	2	43	43	NUM
eurjchem-976	540	3	]	]	PUNCT
eurjchem-976	540	4	.	.	PUNCT
eurjchem-976	541	1	boolell	boolell	PROPN
eurjchem-976	541	2	,	,	PUNCT
eurjchem-976	541	3	m.	m.	NOUN
eurjchem-976	541	4	;	;	PUNCT
eurjchem-976	541	5	gepi‐attee	gepi‐attee	PROPN
eurjchem-976	541	6	,	,	PUNCT
eurjchem-976	541	7	s.	s.	PROPN
eurjchem-976	541	8	;	;	PUNCT
eurjchem-976	541	9	gingell	gingell	PROPN
eurjchem-976	541	10	,	,	PUNCT
eurjchem-976	541	11	j.	j.	PROPN
eurjchem-976	541	12	c.	c.	PROPN
eurjchem-976	541	13	;	;	PUNCT
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eurjchem-976	541	17	j.	j.	PROPN
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eurjchem-976	541	19	.	.	PUNCT
eurjchem-976	542	1	j.	j.	PROPN
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eurjchem-976	542	3	.	.	PUNCT
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eurjchem-976	542	5	,	,	PUNCT
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eurjchem-976	542	7	,	,	PUNCT
eurjchem-976	542	8	257‐261	257‐261	NUM
eurjchem-976	542	9	.	.	PUNCT
eurjchem-976	543	1	[	[	X
eurjchem-976	543	2	44	44	NUM
eurjchem-976	543	3	]	]	PUNCT
eurjchem-976	543	4	.	.	PUNCT
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eurjchem-976	544	2	,	,	PUNCT
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eurjchem-976	544	4	;	;	PUNCT
eurjchem-976	544	5	nivorozhkin	nivorozhkin	PROPN
eurjchem-976	544	6	,	,	PUNCT
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eurjchem-976	544	8	;	;	PUNCT
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eurjchem-976	544	13	.	.	PUNCT
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eurjchem-976	545	2	.	.	PROPN
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eurjchem-976	545	4	,	,	PUNCT
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eurjchem-976	545	6	,	,	PUNCT
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eurjchem-976	545	9	.	.	PUNCT
eurjchem-976	546	1	[	[	X
eurjchem-976	546	2	45	45	NUM
eurjchem-976	546	3	]	]	PUNCT
eurjchem-976	546	4	.	.	PUNCT
eurjchem-976	547	1	li	li	PROPN
eurjchem-976	547	2	,	,	PUNCT
eurjchem-976	547	3	a.	a.	PROPN
eurjchem-976	547	4	;	;	PUNCT
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eurjchem-976	547	6	,	,	PUNCT
eurjchem-976	547	7	t.	t.	PROPN
eurjchem-976	547	8	m.	m.	NOUN
eurjchem-976	547	9	;	;	PUNCT
eurjchem-976	547	10	klumpp	klumpp	PROPN
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eurjchem-976	547	13	a.	a.	PROPN
eurjchem-976	547	14	j.	j.	PROPN
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eurjchem-976	547	16	.	.	PUNCT
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eurjchem-976	547	18	.	.	PUNCT
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eurjchem-976	548	2	,	,	PUNCT
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eurjchem-976	548	4	,	,	PUNCT
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eurjchem-976	548	6	.	.	PUNCT
eurjchem-976	549	1	[	[	X
eurjchem-976	549	2	46	46	NUM
eurjchem-976	549	3	]	]	PUNCT
eurjchem-976	549	4	.	.	PUNCT
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eurjchem-976	550	2	,	,	PUNCT
eurjchem-976	550	3	a.	a.	NOUN
eurjchem-976	550	4	a.	a.	NOUN
eurjchem-976	550	5	;	;	PUNCT
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eurjchem-976	550	7	,	,	PUNCT
eurjchem-976	550	8	a.	a.	NOUN
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eurjchem-976	550	10	;	;	PUNCT
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eurjchem-976	551	4	.	.	PUNCT
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eurjchem-976	552	3	,	,	PUNCT
eurjchem-976	552	4	h.	h.	PROPN
eurjchem-976	552	5	a.	a.	PROPN
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eurjchem-976	552	7	;	;	PUNCT
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eurjchem-976	552	9	,	,	PUNCT
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eurjchem-976	552	15	,	,	PUNCT
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eurjchem-976	553	1	[	[	X
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eurjchem-976	553	3	]	]	PUNCT
eurjchem-976	553	4	.	.	PUNCT
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eurjchem-976	554	3	,	,	PUNCT
eurjchem-976	554	4	h.	h.	PROPN
eurjchem-976	554	5	a.	a.	PROPN
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eurjchem-976	554	7	;	;	PUNCT
eurjchem-976	555	1	khalaf	khalaf	PROPN
eurjchem-976	555	2	,	,	PUNCT
eurjchem-976	555	3	a.	a.	PROPN
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eurjchem-976	555	6	.	.	PUNCT
eurjchem-976	556	1	j.	j.	PROPN
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eurjchem-976	556	4	,	,	PUNCT
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eurjchem-976	556	6	,	,	PUNCT
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eurjchem-976	557	4	.	.	PUNCT
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eurjchem-976	558	5	;	;	PUNCT
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eurjchem-976	558	10	;	;	PUNCT
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eurjchem-976	559	4	.	.	PUNCT
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eurjchem-976	560	24	,	,	PUNCT
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eurjchem-976	561	1	[	[	X
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eurjchem-976	561	3	]	]	PUNCT
eurjchem-976	561	4	.	.	PUNCT
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eurjchem-976	562	8	;	;	PUNCT
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eurjchem-976	563	3	;	;	PUNCT
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eurjchem-976	564	4	.	.	PUNCT
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eurjchem-976	565	19	a.	a.	PROPN
eurjchem-976	565	20	ed	ed	PROPN
eurjchem-976	565	21	.	.	PUNCT
eurjchem-976	565	22	;	;	PUNCT
eurjchem-976	565	23	interscience	interscience	NOUN
eurjchem-976	565	24	,	,	PUNCT
eurjchem-976	565	25	new	new	PROPN
eurjchem-976	565	26	york	york	PROPN
eurjchem-976	565	27	,	,	PUNCT
eurjchem-976	565	28	1964	1964	NUM
eurjchem-976	565	29	,	,	PUNCT
eurjchem-976	565	30	chap	chap	NOUN
eurjchem-976	565	31	.	.	PUNCT
eurjchem-976	566	1	22	22	NUM
eurjchem-976	566	2	and	and	CCONJ
eurjchem-976	566	3	references	reference	NOUN
eurjchem-976	566	4	therein	therein	ADV
eurjchem-976	566	5	.	.	PUNCT
eurjchem-976	567	1	[	[	X
eurjchem-976	567	2	53	53	NUM
eurjchem-976	567	3	]	]	PUNCT
eurjchem-976	567	4	.	.	PUNCT
eurjchem-976	568	1	roberts	roberts	PROPN
eurjchem-976	568	2	,	,	PUNCT
eurjchem-976	568	3	r.	r.	PROPN
eurjchem-976	568	4	m.	m.	PROPN
eurjchem-976	568	5	;	;	PUNCT
eurjchem-976	568	6	khalaf	khalaf	PROPN
eurjchem-976	568	7	,	,	PUNCT
eurjchem-976	568	8	a.	a.	NOUN
eurjchem-976	568	9	a.	a.	NOUN
eurjchem-976	568	10	friedel‐crafts	friedel‐crafts	PROPN
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eurjchem-976	568	12	:	:	PUNCT
eurjchem-976	568	13	a	a	DET
eurjchem-976	568	14	century	century	NOUN
eurjchem-976	568	15	of	of	ADP
eurjchem-976	568	16	discovery	discovery	NOUN
eurjchem-976	568	17	,	,	PUNCT
eurjchem-976	568	18	marcel	marcel	PROPN
eurjchem-976	568	19	dekker	dekker	PROPN
eurjchem-976	568	20	:	:	PUNCT
eurjchem-976	568	21	new	new	PROPN
eurjchem-976	568	22	york	york	PROPN
eurjchem-976	568	23	,	,	PUNCT
eurjchem-976	568	24	ny	ny	PROPN
eurjchem-976	568	25	,	,	PUNCT
eurjchem-976	568	26	1984	1984	NUM
eurjchem-976	568	27	.	.	PUNCT
eurjchem-976	569	1	[	[	X
eurjchem-976	569	2	54	54	NUM
eurjchem-976	569	3	]	]	SYM
eurjchem-976	569	4	.	.	PUNCT
eurjchem-976	570	1	poulsen	poulsen	PROPN
eurjchem-976	570	2	,	,	PUNCT
eurjchem-976	570	3	t.	t.	PROPN
eurjchem-976	570	4	b.	b.	PROPN
eurjchem-976	570	5	;	;	PUNCT
eurjchem-976	570	6	jørgensen	jørgensen	PROPN
eurjchem-976	570	7	,	,	PUNCT
eurjchem-976	570	8	k.	k.	PROPN
eurjchem-976	570	9	a.	a.	PROPN
eurjchem-976	570	10	chem	chem	PROPN
eurjchem-976	570	11	.	.	PUNCT
eurjchem-976	571	1	rev	rev	PROPN
eurjchem-976	571	2	.	.	PROPN
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eurjchem-976	571	4	,	,	PUNCT
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eurjchem-976	571	6	,	,	PUNCT
eurjchem-976	571	7	2903‐2915	2903‐2915	NUM
eurjchem-976	571	8	.	.	PUNCT
eurjchem-976	572	1	[	[	X
eurjchem-976	572	2	55	55	NUM
eurjchem-976	572	3	]	]	PUNCT
eurjchem-976	572	4	.	.	PUNCT
eurjchem-976	573	1	el‐shekeil	el‐shekeil	PROPN
eurjchem-976	573	2	,	,	PUNCT
eurjchem-976	573	3	a.	a.	NOUN
eurjchem-976	573	4	;	;	PUNCT
eurjchem-976	573	5	babaqi	babaqi	PROPN
eurjchem-976	573	6	,	,	PUNCT
eurjchem-976	573	7	a.	a.	PROPN
eurjchem-976	573	8	;	;	PUNCT
eurjchem-976	573	9	hassan	hassan	PROPN
eurjchem-976	573	10	,	,	PUNCT
eurjchem-976	573	11	m.	m.	NOUN
eurjchem-976	573	12	;	;	PUNCT
eurjchem-976	573	13	shiba	shiba	PROPN
eurjchem-976	573	14	,	,	PUNCT
eurjchem-976	573	15	s.	s.	PROPN
eurjchem-976	573	16	heterocycles	heterocycles	PROPN
eurjchem-976	573	17	1988	1988	NUM
eurjchem-976	573	18	,	,	PUNCT
eurjchem-976	573	19	27	27	NUM
eurjchem-976	573	20	,	,	PUNCT
eurjchem-976	573	21	2577‐8250	2577‐8250	NUM
eurjchem-976	573	22	.	.	PUNCT
eurjchem-976	574	1	[	[	X
eurjchem-976	574	2	56	56	NUM
eurjchem-976	574	3	]	]	PUNCT
eurjchem-976	574	4	.	.	PUNCT
eurjchem-976	575	1	li	li	PROPN
eurjchem-976	575	2	,	,	PUNCT
eurjchem-976	575	3	j.	j.	PROPN
eurjchem-976	575	4	y.	y.	PROPN
eurjchem-976	575	5	;	;	PUNCT
eurjchem-976	575	6	wang	wang	PROPN
eurjchem-976	575	7	,	,	PUNCT
eurjchem-976	575	8	x.	x.	PROPN
eurjchem-976	575	9	y.	y.	PROPN
eurjchem-976	575	10	;	;	PUNCT
eurjchem-976	575	11	zhao	zhao	PROPN
eurjchem-976	575	12	,	,	PUNCT
eurjchem-976	575	13	q.	q.	PROPN
eurjchem-976	575	14	h.	h.	PROPN
eurjchem-976	575	15	chem	chem	PROPN
eurjchem-976	575	16	.	.	PUNCT
eurjchem-976	575	17	reag	reag	PROPN
eurjchem-976	575	18	.	.	PUNCT
eurjchem-976	576	1	1997	1997	NUM
eurjchem-976	576	2	,	,	PUNCT
eurjchem-976	576	3	19	19	NUM
eurjchem-976	576	4	,	,	PUNCT
eurjchem-976	576	5	112‐117	112‐117	NUM
eurjchem-976	576	6	.	.	PUNCT
eurjchem-976	577	1	[	[	X
eurjchem-976	577	2	57	57	NUM
eurjchem-976	577	3	]	]	PUNCT
eurjchem-976	577	4	.	.	PUNCT
eurjchem-976	577	5	datterl	datterl	PROPN
eurjchem-976	577	6	,	,	PUNCT
eurjchem-976	577	7	b.	b.	PROPN
eurjchem-976	577	8	;	;	PUNCT
eurjchem-976	577	9	trostner	trostner	PROPN
eurjchem-976	577	10	,	,	PUNCT
eurjchem-976	577	11	n.	n.	PROPN
eurjchem-976	577	12	;	;	PUNCT
eurjchem-976	577	13	kucharski	kucharski	PROPN
eurjchem-976	577	14	,	,	PUNCT
eurjchem-976	577	15	d.	d.	PROPN
eurjchem-976	577	16	;	;	PUNCT
eurjchem-976	577	17	holzer	holzer	PROPN
eurjchem-976	577	18	,	,	PUNCT
eurjchem-976	577	19	w.	w.	PROPN
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eurjchem-976	577	22	,	,	PUNCT
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eurjchem-976	577	24	,	,	PUNCT
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eurjchem-976	577	26	.	.	PUNCT
eurjchem-976	578	1	[	[	X
eurjchem-976	578	2	58	58	NUM
eurjchem-976	578	3	]	]	PUNCT
eurjchem-976	578	4	.	.	PUNCT
eurjchem-976	579	1	smith	smith	PROPN
eurjchem-976	579	2	,	,	PUNCT
eurjchem-976	579	3	l.	l.	PROPN
eurjchem-976	579	4	kgl	kgl	PROPN
eurjchem-976	579	5	.	.	PUNCT
eurjchem-976	580	1	fysiograf	fysiograf	PROPN
eurjchem-976	580	2	.	.	PUNCT
eurjchem-976	581	1	sällskap	sällskap	PROPN
eurjchem-976	581	2	.	.	PUNCT
eurjchem-976	582	1	lun	lun	PROPN
eurjchem-976	582	2	.	.	PROPN
eurjchem-976	582	3	,	,	PUNCT
eurjchem-976	582	4	förh	förh	PROPN
eurjchem-976	582	5	.	.	PROPN
eurjchem-976	583	1	1948	1948	NUM
eurjchem-976	583	2	,	,	PUNCT
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eurjchem-976	583	4	,	,	PUNCT
eurjchem-976	583	5	3‐5	3‐5	NUM
eurjchem-976	583	6	.	.	PUNCT
eurjchem-976	583	7	chem	chem	PROPN
eurjchem-976	583	8	.	.	PUNCT
eurjchem-976	584	1	abstr	abstr	PROPN
eurjchem-976	584	2	.	.	PROPN
eurjchem-976	584	3	,	,	PUNCT
eurjchem-976	584	4	1950	1950	NUM
eurjchem-976	584	5	,	,	PUNCT
eurjchem-976	584	6	44	44	NUM
eurjchem-976	584	7	,	,	PUNCT
eurjchem-976	584	8	1949e	1949e	NUM
eurjchem-976	584	9	.	.	PUNCT
eurjchem-976	585	1	[	[	X
eurjchem-976	585	2	59	59	NUM
eurjchem-976	585	3	]	]	PUNCT
eurjchem-976	585	4	.	.	PUNCT
eurjchem-976	585	5	bachmann	bachmann	PROPN
eurjchem-976	585	6	,	,	PUNCT
eurjchem-976	585	7	w.	w.	PROPN
eurjchem-976	585	8	e.	e.	PROPN
eurjchem-976	585	9	and	and	CCONJ
eurjchem-976	585	10	sheehan	sheehan	PROPN
eurjchem-976	585	11	,	,	PUNCT
eurjchem-976	585	12	j.	j.	PROPN
eurjchem-976	585	13	c.	c.	PROPN
eurjchem-976	585	14	,	,	PUNCT
eurjchem-976	585	15	j.	j.	PROPN
eurjchem-976	585	16	am	am	PROPN
eurjchem-976	585	17	.	.	PUNCT
eurjchem-976	586	1	chem	chem	NOUN
eurjchem-976	586	2	.	.	PUNCT
eurjchem-976	587	1	soc	soc	PROPN
eurjchem-976	587	2	.	.	PUNCT
eurjchem-976	587	3	,	,	PUNCT
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eurjchem-976	587	5	,	,	PUNCT
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eurjchem-976	587	7	,	,	PUNCT
eurjchem-976	587	8	204‐	204‐	NUM
eurjchem-976	587	9	206	206	NUM
eurjchem-976	587	10	.	.	PUNCT
eurjchem-976	588	1	[	[	X
eurjchem-976	588	2	60	60	NUM
eurjchem-976	588	3	]	]	PUNCT
eurjchem-976	588	4	.	.	PUNCT
eurjchem-976	589	1	li	li	PROPN
eurjchem-976	589	2	,	,	PUNCT
eurjchem-976	589	3	l.	l.	PROPN
eurjchem-976	589	4	;	;	PUNCT
eurjchem-976	589	5	elliott	elliott	PROPN
eurjchem-976	589	6	,	,	PUNCT
eurjchem-976	589	7	w.	w.	PROPN
eurjchem-976	589	8	h.	h.	PROPN
eurjchem-976	589	9	j.	j.	PROPN
eurjchem-976	589	10	am	am	PROPN
eurjchem-976	589	11	.	.	PUNCT
eurjchem-976	590	1	chem	chem	PROPN
eurjchem-976	590	2	.	.	PUNCT
eurjchem-976	591	1	soc	soc	PROPN
eurjchem-976	591	2	.	.	PUNCT
eurjchem-976	592	1	1952	1952	NUM
eurjchem-976	592	2	,	,	PUNCT
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eurjchem-976	592	4	,	,	PUNCT
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eurjchem-976	592	6	.	.	PUNCT
eurjchem-976	593	1	[	[	X
eurjchem-976	593	2	61	61	NUM
eurjchem-976	593	3	]	]	PUNCT
eurjchem-976	593	4	.	.	PUNCT
eurjchem-976	594	1	jones	jones	PROPN
eurjchem-976	594	2	,	,	PUNCT
eurjchem-976	594	3	r.	r.	PROPN
eurjchem-976	594	4	g.	g.	PROPN
eurjchem-976	594	5	;	;	PUNCT
eurjchem-976	594	6	soper	soper	PROPN
eurjchem-976	594	7	,	,	PUNCT
eurjchem-976	594	8	q.	q.	PROPN
eurjchem-976	594	9	f.	f.	PROPN
eurjchem-976	594	10	;	;	PUNCT
eurjchem-976	594	11	behrens	behrens	PROPN
eurjchem-976	594	12	,	,	PUNCT
eurjchem-976	594	13	o.	o.	PROPN
eurjchem-976	594	14	k.	k.	PROPN
eurjchem-976	594	15	;	;	PUNCT
eurjchem-976	594	16	corse	corse	PROPN
eurjchem-976	594	17	,	,	PUNCT
eurjchem-976	594	18	j.	j.	PROPN
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eurjchem-976	594	20	j.	j.	PROPN
eurjchem-976	594	21	am	am	PROPN
eurjchem-976	594	22	.	.	PUNCT
eurjchem-976	595	1	chem	chem	PROPN
eurjchem-976	595	2	.	.	PUNCT
eurjchem-976	596	1	soc	soc	PROPN
eurjchem-976	596	2	.	.	PUNCT
eurjchem-976	597	1	1948	1948	NUM
eurjchem-976	597	2	,	,	PUNCT
eurjchem-976	597	3	70	70	NUM
eurjchem-976	597	4	,	,	PUNCT
eurjchem-976	597	5	2843‐2848	2843‐2848	NUM
eurjchem-976	597	6	.	.	PUNCT
eurjchem-976	598	1	[	[	X
eurjchem-976	598	2	62	62	NUM
eurjchem-976	598	3	]	]	PUNCT
eurjchem-976	598	4	.	.	PUNCT
eurjchem-976	599	1	perold	perold	PROPN
eurjchem-976	599	2	,	,	PUNCT
eurjchem-976	599	3	g.	g.	PROPN
eurjchem-976	599	4	w.	w.	PROPN
eurjchem-976	599	5	;	;	PUNCT
eurjchem-976	599	6	steyn	steyn	PROPN
eurjchem-976	599	7	,	,	PUNCT
eurjchem-976	599	8	a.	a.	NOUN
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eurjchem-976	599	10	;	;	PUNCT
eurjchem-976	599	11	von	von	PROPN
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eurjchem-976	599	13	,	,	PUNCT
eurjchem-976	599	14	f.	f.	PROPN
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eurjchem-976	599	16	k.	k.	PROPN
eurjchem-976	599	17	j.	j.	PROPN
eurjchem-976	599	18	am	am	PROPN
eurjchem-976	599	19	.	.	PUNCT
eurjchem-976	600	1	chem	chem	PROPN
eurjchem-976	600	2	.	.	PUNCT
eurjchem-976	601	1	soc	soc	PROPN
eurjchem-976	601	2	.	.	PUNCT
eurjchem-976	602	1	1957	1957	NUM
eurjchem-976	602	2	,	,	PUNCT
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eurjchem-976	602	4	,	,	PUNCT
eurjchem-976	602	5	462‐465	462‐465	NUM
eurjchem-976	602	6	.	.	PUNCT
eurjchem-976	603	1	[	[	X
eurjchem-976	603	2	63	63	NUM
eurjchem-976	603	3	]	]	PUNCT
eurjchem-976	603	4	.	.	PUNCT
eurjchem-976	603	5	hesse	hesse	PROPN
eurjchem-976	603	6	,	,	PUNCT
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eurjchem-976	603	8	;	;	PUNCT
eurjchem-976	603	9	meier	meier	PROPN
eurjchem-976	603	10	,	,	PUNCT
eurjchem-976	603	11	h.	h.	PROPN
eurjchem-976	603	12	;	;	PUNCT
eurjchem-976	603	13	zeeh	zeeh	NOUN
eurjchem-976	603	14	,	,	PUNCT
eurjchem-976	603	15	b.	b.	PROPN
eurjchem-976	603	16	spektroskopische	spektroskopische	PROPN
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eurjchem-976	603	21	chemie	chemie	PROPN
eurjchem-976	603	22	,	,	PUNCT
eurjchem-976	603	23	4th	4th	ADJ
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eurjchem-976	603	25	,	,	PUNCT
eurjchem-976	603	26	thieme	thieme	NOUN
eurjchem-976	603	27	verlag	verlag	PROPN
eurjchem-976	603	28	:	:	PUNCT
eurjchem-976	603	29	new	new	PROPN
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eurjchem-976	603	31	,	,	PUNCT
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eurjchem-976	603	33	.	.	PUNCT
eurjchem-976	604	1	[	[	X
eurjchem-976	604	2	64	64	NUM
eurjchem-976	604	3	]	]	PUNCT
eurjchem-976	604	4	.	.	PUNCT
eurjchem-976	605	1	bonacorso	bonacorso	PROPN
eurjchem-976	605	2	,	,	PUNCT
eurjchem-976	605	3	h.	h.	PROPN
eurjchem-976	605	4	g.	g.	PROPN
eurjchem-976	605	5	;	;	PUNCT
eurjchem-976	605	6	correa	correa	PROPN
eurjchem-976	605	7	,	,	PUNCT
eurjchem-976	605	8	m.	m.	PROPN
eurjchem-976	605	9	s.	s.	PROPN
eurjchem-976	605	10	;	;	PUNCT
eurjchem-976	605	11	porte	porte	PROPN
eurjchem-976	605	12	,	,	PUNCT
eurjchem-976	605	13	l.	l.	PROPN
eurjchem-976	605	14	m.	m.	PROPN
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eurjchem-976	605	16	;	;	PUNCT
eurjchem-976	605	17	pittaluga	pittaluga	PROPN
eurjchem-976	605	18	,	,	PUNCT
eurjchem-976	605	19	e.	e.	PROPN
eurjchem-976	605	20	p.	p.	PROPN
eurjchem-976	605	21	;	;	PUNCT
eurjchem-976	605	22	zanatta	zanatta	PROPN
eurjchem-976	605	23	,	,	PUNCT
eurjchem-976	605	24	n.	n.	NOUN
eurjchem-976	605	25	;	;	PUNCT
eurjchem-976	605	26	martins	martin	NOUN
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eurjchem-976	605	29	a.	a.	PROPN
eurjchem-976	605	30	p.	p.	PROPN
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eurjchem-976	605	33	.	.	PUNCT
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eurjchem-976	606	2	,	,	PUNCT
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eurjchem-976	606	4	,	,	PUNCT
eurjchem-976	606	5	5488‐5491	5488‐5491	NUM
eurjchem-976	606	6	.	.	PUNCT
eurjchem-976	607	1	[	[	X
eurjchem-976	607	2	65	65	NUM
eurjchem-976	607	3	]	]	PUNCT
eurjchem-976	607	4	.	.	PUNCT
eurjchem-976	608	1	becker	becker	PROPN
eurjchem-976	608	2	,	,	PUNCT
eurjchem-976	608	3	e.	e.	PROPN
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eurjchem-976	608	11	,	,	PUNCT
eurjchem-976	608	12	3rd	3rd	ADJ
eurjchem-976	608	13	edition	edition	NOUN
eurjchem-976	608	14	,	,	PUNCT
eurjchem-976	608	15	academic	academic	ADJ
eurjchem-976	608	16	press	press	NOUN
eurjchem-976	608	17	,	,	PUNCT
eurjchem-976	608	18	2000	2000	NUM
eurjchem-976	608	19	,	,	PUNCT
eurjchem-976	608	20	pp	pp	ADV
eurjchem-976	608	21	139‐181	139‐181	NUM
eurjchem-976	608	22	.	.	PUNCT
eurjchem-976	609	1	[	[	X
eurjchem-976	609	2	66	66	NUM
eurjchem-976	609	3	]	]	PUNCT
eurjchem-976	609	4	.	.	PUNCT
eurjchem-976	610	1	silverstein	silverstein	PROPN
eurjchem-976	610	2	,	,	PUNCT
eurjchem-976	610	3	r.	r.	PROPN
eurjchem-976	610	4	m.	m.	PROPN
eurjchem-976	610	5	;	;	PUNCT
eurjchem-976	610	6	webster	webster	PROPN
eurjchem-976	610	7	,	,	PUNCT
eurjchem-976	610	8	f.	f.	PROPN
eurjchem-976	610	9	x.	x.	PROPN
eurjchem-976	610	10	;	;	PUNCT
eurjchem-976	610	11	kiemle	kiemle	NOUN
eurjchem-976	610	12	,	,	PUNCT
eurjchem-976	610	13	d.	d.	PROPN
eurjchem-976	610	14	j.	j.	PROPN
eurjchem-976	610	15	spectrometric	spectrometric	PROPN
eurjchem-976	610	16	identification	identification	NOUN
eurjchem-976	610	17	of	of	ADP
eurjchem-976	610	18	organic	organic	ADJ
eurjchem-976	610	19	compounds	compound	NOUN
eurjchem-976	610	20	,	,	PUNCT
eurjchem-976	610	21	7th	7th	ADJ
eurjchem-976	610	22	edition	edition	NOUN
eurjchem-976	610	23	,	,	PUNCT
eurjchem-976	610	24	wiley	wiley	PROPN
eurjchem-976	610	25	,	,	PUNCT
eurjchem-976	610	26	hoboken	hoboken	PROPN
eurjchem-976	610	27	,	,	PUNCT
eurjchem-976	610	28	2005	2005	NUM
eurjchem-976	610	29	.	.	PUNCT