Microsoft Word - numero_41_art_64.docx S. K. Kourkoulis et alii, Frattura ed Integrità Strutturale, 41 (2017) 536-551; DOI: 10.3221/IGF-ESIS.41.64 536 Acoustic Emissions versus Pressure Stimulated Currents during bending of restored marble epistyles: Preliminary results Stavros K. Kourkoulis, Ioanna Dakanali, Ermioni D. Pasiou National Technical University of Athens, School of Applied Mathematical and Physical Sciences, Department of Mechanics, 5 Heroes of Polytechnion Avenue, Theocaris Bld., Zografou Campus, 157 73 Athens, Greece stakkour@central.ntua.gr Ilias Stavrakas, Dimos Triantis Technological Educational Institution of Athens, Department of Electronics, Laboratory of Electronic Devices and Materials, Agiou Spiridonos Street, 122 10, Athens, Greece ABSTRACT. The efficiency of two modern sensing techniques, namely the “Acoustic Emissions” and the “Pressure Stimulated Currents” ones, when they are used as Continuous Structural Health Monitoring tools, is assessed experi- mentally. The protocol includes multi-point bending of an accurate copy of a fractured marble epistyle of the Parthenon’s Temple on the Acropolis of Athens, under a scale of 1:3. The integrity of the epistyle is restored with three pairs of bolted titanium bars, according to the pioneering technique developed by the scientists of the “Committee for the Conservation of the Acropolis Monuments”. The data provided by the above techniques are considered in juxtaposition to each other and also in comparison to data provided by the “Digital Image Correlation” technique. It is concluded that, at least from a qualitative point of view, the data of all three techniques are in good mutual agreement. Combined exploitation of the various sets of experimental data enlightens interesting aspects concerning the succession of failure mechanisms activated during the loading procedure, revealing the critical role of the internal interfaces characterizing the restored epistyle. Moreover it is definitely indicated that both the “Acoustic Emissions” and the “Pressure Stimulated Currents” techniques provide clear signs of upcoming failure well before macroscopically visible damages are detected at the external surface of the specimen. KEYWORDS. Acoustic Emissions; Pressure Stimulated Currents; Digital Image Correlation; Marble Monuments; Restoration/Conservation; Continuous Struc- tural Health Monitoring. Citation: Kourkoulis, S.K., Dakanali, I., Pa- siou, E.D., Stavrakas, I., Triantis, D., Acoustic Emissions versus Pressure Stimulated Currents during bending of restored marble epistyles: Preliminary results, Frattura ed Integrità Strutturale, 41 (2017) 536-551. Received: 30.04.2017 Accepted: 31.05.2017 Published: 01.07.2017 Copyright: © 2017 This is an open access article under the terms of the CC-BY 4.0, which permits unrestricted use, distribution, and reproduction in any medium, provided the original author and source are credited. S. K. Kourkoulis et alii, Frattura ed Integrità Strutturale, 41 (2017) 536-551; DOI: 10.3221/IGF-ESIS.41.64 537 INTRODUCTION ontinuous structural health monitoring (CSHM) is perhaps the most effective tool in hands of structural engineers, in the direction of timely detecting accumulation of damage in structures of any kind. It offers, thus, the time interval, which is necessary in order for proper measures to be undertaken, preventing further damage accumulation that can lead to catastrophic failures. The topic is in the cutting edge of scientific research worldwide, since according to the ancient Greek physician and philosopher Hippocrates “prevention is better than cure”. Nowadays, research is focused on the development and practical implementation of new ideas (both in the hardware and the software level) for CSHM, which are flexible, user-friendly and also effective from the financial point of view. The field of restoration and conservation of cultural heritage monuments is among the ones for which CSHM is a “conditio sine qua non” for an intervention to be considered successful and completed. In the specific field, however, there are quite a few additional requirements (mainly of aesthetic origin) that do not permit the use of traditional sensing techniques. For example, the size of the devices used as sensors should be very small in order to avoid distorting the beauty and harmony of the external appearance of the monuments. Along the same lines, attaching the sensing devices to the structural members should be implemented very carefully in order to avoid harming the integrity of the member’s external surface. Besides the as above practical complexities, additional problems must be solved in case of CSHM of cultural heritage monu- ments, related to the proper interpretation of the data recorded by the sensing devices which are attached on restored structural elements. Indeed, in quite a few cases, restoration of damaged or fractured members is achieved with the aid of metallic reinforcing elements and suitable adhesive materials. As a result, a three-material complex with material interfaces is created, the constituent elements of which are usually of completely different mechanical behaviour and response to any kind of external stimuli. A typical example of such a restoration approach is the technique adopted nowadays for restoring the integrity of structural elements of the monuments of the Sacred Hill of the Acropolis of Athens. These monuments, which constitute a unique complex of buildings, including the Parthenon, Propylaia, Erechtheion and the temple of Athena Nike, were built by the ancient Greeks during the 5th century B.C. using almost exclusively Pentelic marble. Nowadays, their historical and aesthetic magnificence is recognized worldwide and they are listed among the masterpieces of classical western civilization. The main restorative intervention on the Athenian Acropolis monuments was directed by N. Balanos in 1885. The interventions were of a major scale and their basic principle was that all fragments of structural elements, spread around the monument, should be re-positioned on the monument and the addition of elements made of new material should be as limited as possible. From this moment on, the term “anastylosis” was established as a reconstruction technique whereby ruined monu- ments are restored using the original architectural elements to the greatest degree possible. From a purely archeological point of view Balanos’ intervention was successful due to the minimum possible use of new marble, although the use of scattered ancient fragments as ordinary building material has been strongly criticized. Unfortu- nately from the structural and chemical points of view, the use of metallic reinforcing elements (which were made of steel) without prior verification of their mechanical and physico-chemical compatibility with the ancient material and without taking into account their chemical resistance against air pollution became the source of extensive damage of the monu- ment [1]. In the direction of curing these problems the “Committee for the Conservation of the Acropolis Monuments” (ESMA) was established in 1975 inaugurating a new approach to the restoration of the Acropolis of Athens monuments [1]. The scientific personnel of the committee developed a pioneer technique for the restoration of the structural integrity of the monuments’ structural members, according to which the fractured marble elements are connected by inserting titanium bars into pre-drilled holes. The adhesion between marble and bars is achieved by a proper white cement paste [2, 3]. The aforementioned technique is based on the basic restoration principles, dictated by the “Venice Charter” [4, 5]: Re- versibility (if needed, the monument could be brought to its state prior to the intervention), minimization of the inter- ventions to the extent that guarantees protection of the authentic material from further damage (for this reason the number of titanium bars required by the connection’s design, should be the smallest possible) and finally compatibility between the materials used for the restoration and the authentic ones. The restoration approach described above was assessed a few years ago both experimentally and numerically [6-10]. It has been indicated that, in spite of its efficiency and general acceptance, there are still some open issues that should be further studied, mainly in the direction of reducing the intervention on the authentic building material. In this context an experi- mental protocol was recently implemented [11, 12], during which accurate copies of fractured epistyles, restored according to the as above procedure, were submitted to multi-point bending in order to simulate the actual loading conditions that will be realized after the epistyle is re-placed in its original position. The main innovation of that study was the simultaneous use of traditional and innovative sensing techniques that permitted pumping data both from the outer surface of the speci- mens as well as from their interior and especially from the two interfaces (marble-to-cement and cement-to-metal) which C S. K. Kourkoulis et alii, Frattura ed Integrità Strutturale, 41 (2017) 536-551; DOI: 10.3221/IGF-ESIS.41.64 538 are the areas most suspicious for failure to start. The results were very encouraging, revealing interesting data about the succession of failure mechanisms activated during loading the restored epistyle. In the present study advantage is taken of the experimental data of that protocol along a different line of thought, namely that of detecting indicators that could play the role of pre-failure warnings. In this direction, the data recorded by the Acoustic Emissions (AE) and the Pressure Stimulated Currents (PSC) techniques are considered in juxtaposition to each other as well as in comparison to the data recorded by the Digital Image Correlation (DIC) technique. It is concluded that the data provided by both the AE and the PSC techniques include clear signs which precede well the upcoming failure of the structure. Taking into account that the AE is already a more or less well established CSHM technique [13-17] (which means that the respective data can be used as a calibration/validation standard) and also the fact that the PSC technique is characterized by very low application cost, it can be concluded that (after proper calibration) the specific technique could be considered as a flexible alternative tool for effective and economically tolerable CSHM, given that its results are here successfully checked against the respective ones of the AE technique. THE EXPERIMENTAL PROTOCOL AND THE SENSING TECHNIQUES USED The specimen and the experimental procedure he experimental procedure is analytically described in ref. [12]. For the convenience of the reader, its main features only are here shortly outlined: An accurate copy of an authentic epistyle of the Parthenon Temple was constructed under a scale 1:3, by experienced technicians of the Parthenon worksite. The epistyle was made of Dionysos marble, the material that is nowadays used, almost exclusively, for the restoration project of the Acropolis monuments, given that the quarries of mount Pentelicon are not accessible, for historic and environmental reasons. The characteristics of Dionysos marble are very close to the respective ones of Pentelic marble form mechanical, geological and physico-chemical points of view [18]. During the construction of the copy every effort was paid for the accurate reproduction of the characteristics of the authentic epistyle especially concerning the orientation of the material layers with respect to the longitudinal axis of the member (and therefore to the direction of the load imposed). It is here recalled that Dionysos and Pentelic marbles are orthotropic materials characterized by three distinct anisotropy axes, although along two of them the mechanical properties are quite close to each other and therefore both materials are usually simulated as transversely isotropic ones [19, 20]. Obviously, in case of bending, optimum load-bearing capacity is achieved when the material layers are normal to the loading line. The copy of the epistyle was asymmetrically fractured into two fragments, which were restored with the aid of three pairs of bolted titanium bars driven in pre-drilled holes, as it can be clearly seen in Fig.1a. The holes are filled with a suitable cement paste (binder and water without aggregates), which acts both as adhesion layer and also as matching element between the two extremely incompatible basic constituents of the complex (i.e., the extremely brittle marble and the extremely ductile titanium) protecting the authentic building stone. The angle of the fracture plane with respect to the axis of the member was 70o. The specific choice is based on observations of fracture planes of epistyles of the Parthenon Temple and it appears to be the maximum one for which the specific arrangement of reinforcing bars could be applied. The bar’s anchoring length (a) (b) Figure 1: (a) The two fragments of the epistyle’s copy during the restoration phase. The three pairs of reinforcing elements are clearly visible; (b) Schematic representation of the multi-point bending loading scheme. T S. K. Kourkoulis et alii, Frattura ed Integrità Strutturale, 41 (2017) 536-551; DOI: 10.3221/IGF-ESIS.41.64 539 for both fragments was equal to 25 cm, symmetrically with respect to the fracture plane. The surfaces of the fragments that were to come in contact were coated with the same cement paste (used to fill the holes) to ensure optimum matching of the fragments rather than to increase the element’s bearing capacity (the tensile strength of the cement paste is negligible). After curing for 28 days the specimen was placed on two marble cubes (simulating the in-situ supporting conditions, i.e. the capitals or abacuses of the Temple) on the platform of a very stiff (capacity 6 MN) servo-hydraulic loading frame. For the load transferred to the epistyle to be as uniformly distributed as possible, a three-level steel construction was placed above the specimen, as it is shown schematically in Fig.1b. The first layer included eight equidistant metallic rods in direct contact to the marble. Above these rods four wide flange H beams (HEB 140) were placed. The second layer consisted of four equidistant rods and two wide flange H beams (HEB 200). The beam of the last layer was supported on the previous layer through two metallic rods and it was loaded with the aid of another rod, in contact to the frame’s traverse. Eight Linear Variable Differential Transformers (LVDTs) were used to measure deflections and two clip gauges were used to measure the relative displacement of two knife-edges attached on the fault’s either side. The overall specimen’s deform- ation was also monitored with the aid of innovative sensing techniques gaining data from suitable sensors, mounted on the specimen’s surface. A proper arrangement of sensors of various types was designed, aiming to the most efficient pumping of data both from the external surface and the interior of the epistyle: Eight acoustic sensors were attached around the fault’s area for the spatiotemporal determination of the location of sources of Acoustic Emissions and four electric con- tacts which permitted recording of the Pressure Stimulated Currents. In addition, the three dimensional displacement field of the epistyle’s area in the immediate vicinity of the fracture plane was recorded using the Digital Image Correlation (DIC) technique. DIC is a full-field image analysis method, based on a sequence of digital images, which permits the de- termination of the contour and the displacements of mechanically loaded bodies. The epistyle was loaded monotonically under displacement-control mode at a rate ensuring quasi-static loading conditions. A general view of the overall experimental set-up and the sensors attached is shown in Fig.2. Further details, concerning the exact position of each sensor, the position of the reinforcing bars, the dimensions of the epistyle’s copy and the loading scheme can be found in ref. [11, 12]. Figure 2: An overview of the experimental arrangement. The Acoustic Emissions (AE) technique When a rigid body is under mechanical loading and the stress field developed exceeds certain limits (depending on the body’s material) elastic waves are emitted due to the nucleation of free surfaces and the subsequent release of stored elastic strain energy. These waves can be detected by proper acoustic sensors suitably attached on the material’s surface. Monitoring AE provides useful information related to the spatiotemporal evolution of internal damage. Proper analysis of AE data is useful, among others, for the prediction of upcoming failure since they are strongly correlated with crack initiation and propagation [13]. The characteristics of the acoustic events recorded differ, in accordance to the nature of the sources of the events. It is nowadays accepted that, the signals caused by cracking are “explosive” with low duration while, on the other hand, signals related to shear phenomena (for example friction) are characterized by higher duration [13, 14]. In concrete, the classification of the type of cracks is standardized and implemented using the combination of the S. K. Kourkoulis et alii, Frattura ed Integrità Strutturale, 41 (2017) 536-551; DOI: 10.3221/IGF-ESIS.41.64 540 average frequency of the pulse recorded by the sensors and a parameter called RA, which is in fact the ratio of the rise time (i.e., the time required for the pulse to reach its maximum value) over the maximum amplitude of the pulse. Signals of high frequency and low RA parameter are attributed to tensile cracks while signals of low frequency and high RA para- meter are attributed to either shear- or mixed-mode cracks [15-17]. Another approach widely used to evaluate AE signals is the so called b-value analysis [21, 22]. Conventionally, the b-value analysis is based on the Gutenberg-Richter relationship, which is used in seismology and correlates events of high amplitude and lower frequency with events of low amplitude and higher frequency. Due to the fact that the determination of b-value is somehow subjective, an “Improved b-value” (Ib-value) was proposed in 1994 by Shiotani et al. [23, 24]. The Ib- value uses statistical parameters, as it is the mean and standard deviation of AE amplitude, which vary during the test. It is considered that increased Ib-values indicate that the system approaches a “critical stage”, or in other words failure is impending. The Ib-value is defined as:       10 1 10 2 1 2 log log b N N I         (1) with ω1=μ-α1σ, ω2=μ+α2σ, where σ is the standard deviation, μ is the mean value of the amplitude distribution, α1 is a coef- ficient related to the smaller amplitude and α2 is a coefficient related to the fracture level. The values of α1 and α2 vary in the range 0.5-5.0, however it is proven that changing their value within the specific range does not significantly affect the Ib-value [23, 24]. In this context in the protocol described here it was considered that α1=α2=1.0. The Pressure Stimulated Currents (PSC) technique The PSC technique is based on the detection of weak electrical signals emitted during the formation and growth of micro cracks within the material’s bulk. The PSC technique has been applied on several materials (marble, amphibolite, cement based materials etc) [25-28] and under several mechanical loading types and so far it is proven that (at least in the laboratory scale) it provides consistent pre-failure indicators. According to the fundamental principles of the technique, the electric charge produced while a material is subjected to an external mechanical load is attributed to several reasons such as moving charged dislocations, the piezoelectric effect and the fracto-emissions. The dislocations are a type of defect in crystals. The dislocations (point, linear, planar, bulk) are areas where the atoms are out of position in the crystal structure and move when a stress field is applied. They are not symmetric with respect to positive and negative charge and when deformation occurs, the dislocations start moving transporting charge. Piezoelec- tric effect is the ability of certain materials to generate electric charge in response to externally applied mechanical stress. In piezoelectric crystals, the unit cell is not symmetrical. Normally, piezoelectric crystals are electrically neutral, the atoms inside them may not be symmetrically arranged, but their electrical charges are perfectly balanced. The deformation of a piezoelectric material leads to push some of the atoms closer together or further apart, upsetting the balance of positive and negative, and causing net electrical charges to appear. Fracto-emission is the emission of particles (e.g., electrons, ions, ground state and excited neutrals, and photons) during and following fracture. The origin of electron and photon emission from fracture has frequently been attributed to either (a) field emission due to electric fields produced by charge separation or to (b) various non adiabatic processes involving fundamental excitations of creation and recombination of point like defects and charge carriers. Dickinson et al. [29] proposed a simple model for systems involving charge separation during fracture already since 1983. EXPERIMENTAL RESULTS The overall mechanical response of the restored epistyle he load-deflection curve, plotted in Fig.3a, exhibits five distinct characteristic regimes, which do not appear in case an intact marble epistyle is subjected to bending [19, 20]. For almost three quarters of the maximum load imposed (i.e. the load that caused catastrophic failure and which was equal to about 375 kN) the epistyle behaves as an intact structure (portion OA of the graph in Fig.3a) and its response is almost perfectly linear, although the overall “stiffness” is well below of that characterizing intact Dionysos marble under bending [20]. It will be indicated later (by taking advantage of data provided by the Acoustic Emissions technique), that point A corresponds (quite possibly) to the time instant at which fracture of the cement layer between the marble fragments starts. The linear portion of the graph is followed by a non-linear response of the restored epistyle (portion AB of the graph), which is in turn followed by a “plateau” BC. The specific behaviour appears similar to that of ductile metallic elements, (like T S. K. Kourkoulis et alii, Frattura ed Integrità Strutturale, 41 (2017) 536-551; DOI: 10.3221/IGF-ESIS.41.64 541 0 150 300 450 0.0 1.5 3.0 4.5 L oa d, P [k N ] Opening of the fault, ζ [mm] P ζ Α΄ Β΄ C΄ D΄ E΄ 0 150 300 450 0 1 2 3 L oa d, P [k N ] Deflection, δ [mm] Α Β C D E P δ   (a) (b) Figure 3: The overall load imposed versus the (a) deflection, δ, of the epistyle’s central section and (b) the opening of the fault, ζ, at the lowest edge of the epistyle. (a) (b) Figure 4: (a) First macroscopically visible cracking of the upper corner of the left fragment at time instant t~1140s. (b) The epistyle after the final failure (fracture of all reinforcing titanium bars). titanium) under tension indicating, perhaps, some kind of yield and flow of the lowest level of reinforcing bars. The abrupt load drop following (portion CD of the graph) is difficult to be explained, however it could be attributed to either a local fracture of the upper corner of one of the two fragments (which is clearly seen in Fig.4) or to fracture of the titanium bars of the lowest layer or even to both of them. After this sudden drop the load starts increasing again, indicating that the ad- ditional load imposed is undertaken by the bars of the upper level, for which the stress level is below the respective yield limit. The maximum deflection recorded (at the maximum load imposed) was equal to about 2.7 mm. The second mechanical parameter, of crucial importance, from the engineering point of view, is the opening, ζ, of the fault, i.e. the increase of the distance between the two fragments, which was measured with the aid of traditional clip- gauges attached at the lowest edge of the epistyle and also at the level of the lowest layer of restoring bars. The variation of ζ versus the overall load imposed is plotted in Fig.3b. It exhibits a behaviour quite similar (from a qualitative point of view) with that of the deflection (Fig.3a). Again the dependence is initially linear, followed by a regime of non-linear response. However, instead of a “plateau” (as it was the case of the P-δ graph) the non-linear portion is terminated by a sudden drop and the characteristic “plateau” appears afterwards. Then the opening of the fault starts increasing again slowly until a value equal to about ζ=3.2 mm. From this point on, the increase becomes steeper attaining a S. K. Kourkoulis et alii, Frattura ed Integrità Strutturale, 41 (2017) 536-551; DOI: 10.3221/IGF-ESIS.41.64 542 0.0 1.5 3.0 4.5 0 500 1000 1500 δ, ζ [m m ] Time [s] δ ζ0.5 1.5 2.5 3.5 1110 1130 1150 1170 0 1 2 3 0.0 1.5 3.0 4.5 D ef le ct io n, δ [m m ] Opening of the fault, ζ [mm] C, D΄ Β, Β΄ C΄ (a) (b) Figure 5: (a) The time evolution of deflection, δ, of the epistyle’s central section and of the opening of the fault, ζ, at the lowest edge of the epistyle. (b) The dependence of δ on ζ. maximum value equal to about ζ=3.5 mm. The letters designating these characteristic intervals in Fig.3b are in accordance to those of Fig.3a. Attention should be paid, however, to the fact that their succession is not identical. In order to follow the time evolution of δ and ζ, the time dependence of them is plotted in Fig.5a. The similarity of the two graphs is quite interesting. Both quantities exhibit an almost perfectly linear portion, followed by a non-linear one which is terminated by a characteristic “plateau” until about t=1130 s and then the deformation (either in terms of δ or ζ) starts increasing quite abruptly. From Fig.5a it could be concluded that the two “plateaus” do not appear simultaneously. As it is more clearly seen in the plot embedded in Fig.5a, a time shift between them appears. In the authors’ opinion this should be attributed to differences in the sampling rate between the devises recording deflection (LVDTs) and those re- cording the fault’s opening (clip-gauges) as well as to inevitable time-delays. This opinion can be supported by Fig.5b where δ and ζ are plotted against each other. It is reasonable to assume that neither δ can increase with ζ remaining constant (portion ΒC of the graph) nor can ζ increase with δ remaining constant (portion D΄C΄). Given that the number of experi- mental points between (B, B΄) and C΄ is very small it could be perhaps more wise to ignore the BCC΄ (or B΄D΄C΄) path and consider a virtual linear segment BC΄ instead. In spite of the above discussed criticism, it is to be emphasized that, in general, the data provided by the clip-gauges for the opening of the fault are quite reliable. This was verified since they were found in excellent agreement with the respect- ive data obtained from the Digital Image Correlation technique [32, 33]. The displacement field of both fragments was monitored by the cameras of the system during the whole duration of the loading procedure [11, 12]. A typical view of the epistyle as it is seen by the two cameras is shown in Figs.6(a,b). The specific images correspond to the very last loading steps. As a next step the axial (horizontal) component of the displacement vector was determined for both fragments. Typical colour-scale images of the axial displacement of the two fragments are exhibited in Figs.6(c,d,e) for three char- acteristic time instants. Fig.6c corresponds to a very early loading stage (t=10 s), Fig.6d corresponds to the load-level at which separation of the fragments starts (t=405 s) and Fig.6e to a load level relatively close to the entrance to the “critical stage” of the loaded system (t=1085s). For the quantitative correlation of the data provided by the DIC and the clip-gauges, two pairs of elementary areas of the fragments on either side of the fault were isolated in the immediate vicinity of the clips and the distance between them was determined as a function of time. The data concerning the opening of the fault as obtained from the DIC system are plotted in Fig.6f, in juxtaposition to those of the clip-gauges. It can be seen that the agreement between DIC and clip- gauges is excellent and the differences recorded do not exceed 1% for the whole duration of the loading procedure. S. K. Kourkoulis et alii, Frattura ed Integrità Strutturale, 41 (2017) 536-551; DOI: 10.3221/IGF-ESIS.41.64 543 0.030 0.020 0.010 0.000 0.025 0.015 0.005 -0.005 -0.010 -0.015 -0.020 -0.025 -0.030 -0.035 -0.040 -0.045 -0.050 Displacement X [mm] Displacement X [mm] -0.015 -0.025 -0.035 -0.045 -0.020 -0.030 -0.040 -0.050 -0.055 -0.060 -0.065 -0.070 -0.075 -0.080 -0.085 -0.090 -0.095 0.350 0.300 0.250 0.200 0.150 0.100 0.050 0.000 -0.050 -0.100 Displacement X [mm] 0.0 1.0 2.0 3.0 4.0 0 500 1000 1500 Fa ul t’s o pe ni ng , ζ [m m ] Time [s] y=0.00- DIC y=0.00- clip gauge y=0.07m- DIC y=0.07- clip gauge y=0.00 - DIC y=0.00 - clip gauge y=0.07m - DIC y=0.07m - clip gauge (a) (b) (c) (d) (e) (f) Figure 6: (a) (b) Typical view of the restored epistyle as it seen by the two cameras of the DIC system while failure is impending; (c) The contours of the axial displacement of the epistyle at time instants (c) t=10s; (d) t=405s; and (e) t=1085s; (f) The time variation of the opening of the fault as extracted by the DIC system and by the two clip gauges. S. K. Kourkoulis et alii, Frattura ed Integrità Strutturale, 41 (2017) 536-551; DOI: 10.3221/IGF-ESIS.41.64 544 0.0 0.3 0.5 0.8 1.0 1.3 1.5 1.8 2.0 0 100 200 300 400 0 1 2 3 4 PS C [n A ] L oa d [k N ] ζ [mm] ζ at y=0.07m Load PSC 0.18 1.04 2.26 3.05 0.57 Concerning the overall response of the restored epistyle it was concluded by the data of the DIC system that (in excellent agreement with the conclusions drawn by the data of the remaining systems that will be analyzed in next sections) the epistyle behaves as an intact structure up to about t=400s. Then the fragments start separating from each other and their distance increases relatively smoothly. Then at a time instant equal to about t=1100 s the separation tendency is accelerated denoting entrance of the system to its “critical stage” which will lead the structure to final collapse. Data provided by the Acoustic Emission and the Pressure Stimulated Currents techniques The variation of the PSC recordings against the opening of the fault is plotted in Fig.7 in juxtaposition to the respective variation of the load imposed. It is observed from this figure that the electric current produced during loading follows, according to a quite satisfactory manner, the respective variation of the load imposed. The PSC increases almost linearly during the very first steps of the loading procedure and then it is almost stabilized in the period of non-linear mechanical response of the restored epistyle. At the time instant of the sudden load drop the PSC starts increasing smoothly attaining a maximum value equal to about 2 nA. After this maximum its value starts decreasing more or less smoothly. A sudden drop is observed when the load level is equal to about 320 kN, i.e., the load level at which the crack opening starts increasing (see Fig.3b) designating approach to the final “critical stage” of the structure. Figure 7: The variation of the load and the PSC versus the opening, ζ, of the fault. It is quite interesting to note that the variation of PSC against the opening of the fault exhibits characteristic slope changes at points where the respective load-opening of the fault graph exhibits similar changes. These points, indicated by blue lines in Fig.7, are detected for values of the fault’s opening equal to ζ=0.18, 0.57, 1.04, 2.26 and 3.05 mm. According to the previous discussion the first increasing part of the PSC graph (i.e., that until ζ=0.18) can be attributed to the fracturing of the cement paste between the two fragments, the second one (i.e., that from ζ=1.04) to cracking of the cement-paste surrounding the bars, while the last one (i.e., that after ζ=3.05 mm) corresponds to the entrance of the “system” (restored epistyle) in its “critical stage” (i.e., the epistyle approaches its catastrophic failure) and can be safely considered as a relatively early “pre-failure” indicator. In general, the two phases of PSC increase (i.e., from ζ=0 το ζ=0.18 mm and from ζ=1.04 mm to ζ=2.26 mm) can be attributed to production of electric charge due to micro-cracking in the cement paste (and perhaps in the marble’s body), while the drops of its value are attributed to the appearance of cracks of larger size which interrupt conductive paths. As a next step, in the direction of gaining an overview of the acoustic activity within the structure, the time rate of cumulative hits is plotted against time in Fig.8. In the same figure the time variation of the deflection, δ, and that of the fault’s opening, ζ, is also plotted for comparison. It is quite encouraging to observe that the time variation of the cumulative hits per second is quite similar (from a qualitative point of view) to the respective one of the PSC: It exhibits, also, characteristics slope changes at exactly the same time instants (or equivalently at the same values of the fault’s opening) as it was observed for the PSC. These changes are indicated by dotted lines in Fig.8, together with the respective values of the fault’s opening (mm). S. K. Kourkoulis et alii, Frattura ed Integrità Strutturale, 41 (2017) 536-551; DOI: 10.3221/IGF-ESIS.41.64 545 0.00 0.50 1.00 1.50 2.00 2.50 3.00 0.0E+00 3.0E+08 6.0E+08 9.0E+08 1.2E+09 1.5E+09 1.8E+09 0 100 200 300 400 δ [m m ] C um ul at iv e en er gy [a J] Load [kN] cumEnergy δ 0.0 0.5 1.0 1.5 2.0 0.0E+00 4.0E+08 8.0E+08 1.2E+09 1.6E+09 0 100 200 300 400 PS C [n A ] C um ul at iv e E ne rg y A E [a J] Load [kN] cumEnergy PSC 0.18 0.57 1.04 3.07 2.25 0.0 1.0 2.0 3.0 4.0 5.0 0 10000 20000 30000 40000 50000 0 300 600 900 1200 1500 δ, ζ [m m ] C um ul at iv e hi ts /s Time [s] cumulative hits/s COD- y=0.07 LVDT (central) ζ δ 2.25 Figure 8: The time dependence of the cumulative hits per second in conjunction to that of the deflection and the opening of the fault. An alternative approach of quantifying the acoustic activity within the restored epistyle is attempted in Fig. 9a: The cumu- lative energy of the acoustic emissions is plotted against the level of the mechanical load imposed to the structure in juxta- position to that of the deflection, δ, of the epistyle’s central section. The two plots exhibit the same qualitative character- istics: A stage of more or less smooth increase followed by a “plateau”, a sudden change at the instant of the first load drop and again a stage of increase. The correlation of the cumulative energy of the acoustic emissions with the PSC is shown in Fig.9b, in which the dependence of both quantities on the load level is plotted. Besides partial differences it is evident that the overall behaviour of the two plots is quite similar to each other. (a) (b) Figure 9: (a) The variation of the cumulative energy of the AE and δ versus the load applied; (b) The variation of the cumulative energy of the AE and PSC recordings versus the load applied. Further exploitation of the experimental data provided by the acoustic sensors is achieved by calculating the respective Ib- value. In Fig.10 the time variation of the Ib-value is plotted in juxtaposition to the respective one of the load imposed. It is very interesting to observe that the Ib-value remains almost constant, equal to about Ib=1.5 for over 90% of the experiment’s overall duration. At t=1150 s a decrease of the Ib-value is observed almost simultaneously with the abrupt S. K. Kourkoulis et alii, Frattura ed Integrità Strutturale, 41 (2017) 536-551; DOI: 10.3221/IGF-ESIS.41.64 546 0 100 200 300 400 1.0 1.5 2.0 2.5 3.0 0 500 1000 1500 L oa d [k N ] Ib [- ] Time [s] ib value load 0.5 1.0 1.5 2.0 2.5 3.0 0 5000 10000 15000 20000 25000 0 500 1000 1500 Ib -v al ue R A [μ s/ V ] Time [s] mRA Ib value RA Ib-value 0.5 1.0 1.5 2.0 2.5 3.0 0.00 0.60 1.20 1.80 2.40 3.00 0 500 1000 1500 Ib -v al ue E ne rg y (P SC ) [ aA 2 s] Time [s] Energy (PSC) Ib value Energy (PSC) Ib-value Energy (PSC) Ib-value Figure 10: Time variation of the Ib-value in juxtaposition to the respective variation of the load imposed load drop caused by the local fracture of the upper corner of one of the two fragments (Fig.4), which results, in fact, to an instantaneous relief of the stress field within the epistyle’s body. After this time instant the load starts increasing again and the Ib-value increases abruptly reaching finally values even exceeding Ib=2.5. Similar behaviour of the Ib-value has been already observed and discussed in refs.[34, 35]. At the time instant at which the Ib-value starts increasing again after its drop at t=1150 s, a similar behaviour is exhibited by the RA parameter. This is clearly seen in Fig.11a, in which the time variation of RA is plotted in juxtaposition to that of the Ib-value: RA is very low, varying in the region 0> /ColorImageDict << /QFactor 0.15 /HSamples [1 1 1 1] /VSamples [1 1 1 1] >> /JPEG2000ColorACSImageDict << /TileWidth 256 /TileHeight 256 /Quality 30 >> /JPEG2000ColorImageDict << /TileWidth 256 /TileHeight 256 /Quality 30 >> /AntiAliasGrayImages false /CropGrayImages true /GrayImageMinResolution 300 /GrayImageMinResolutionPolicy /OK /DownsampleGrayImages true /GrayImageDownsampleType /Bicubic /GrayImageResolution 300 /GrayImageDepth -1 /GrayImageMinDownsampleDepth 2 /GrayImageDownsampleThreshold 1.50000 /EncodeGrayImages true /GrayImageFilter /DCTEncode /AutoFilterGrayImages true /GrayImageAutoFilterStrategy /JPEG /GrayACSImageDict << /QFactor 0.15 /HSamples [1 1 1 1] /VSamples [1 1 1 1] >> /GrayImageDict << /QFactor 0.15 /HSamples [1 1 1 1] /VSamples [1 1 1 1] >> /JPEG2000GrayACSImageDict << /TileWidth 256 /TileHeight 256 /Quality 30 >> /JPEG2000GrayImageDict << /TileWidth 256 /TileHeight 256 /Quality 30 >> /AntiAliasMonoImages false /CropMonoImages true /MonoImageMinResolution 1200 /MonoImageMinResolutionPolicy /OK /DownsampleMonoImages true /MonoImageDownsampleType /Bicubic /MonoImageResolution 1200 /MonoImageDepth -1 /MonoImageDownsampleThreshold 1.50000 /EncodeMonoImages true /MonoImageFilter /CCITTFaxEncode /MonoImageDict << /K -1 >> /AllowPSXObjects false /CheckCompliance [ /None ] /PDFX1aCheck false /PDFX3Check false /PDFXCompliantPDFOnly false /PDFXNoTrimBoxError true /PDFXTrimBoxToMediaBoxOffset [ 0.00000 0.00000 0.00000 0.00000 ] /PDFXSetBleedBoxToMediaBox true /PDFXBleedBoxToTrimBoxOffset [ 0.00000 0.00000 0.00000 0.00000 ] /PDFXOutputIntentProfile () /PDFXOutputConditionIdentifier () /PDFXOutputCondition () /PDFXRegistryName () /PDFXTrapped /False /CreateJDFFile false /Description << /ARA /BGR /CHS /CHT /CZE /DAN /DEU /ESP /ETI /FRA /GRE /HEB /HRV (Za stvaranje Adobe PDF dokumenata najpogodnijih za visokokvalitetni ispis prije tiskanja koristite ove postavke. 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