Microsoft Word - numero_26_art_4 S. Agnetti, Frattura ed Integrità Strutturale, 26 (2013) 31-40; DOI: 10.3221/IGF-ESIS.26.04 31 Strength on cut edge and ground edge glass beams with the failure analysis method Stefano Agnetti Department of Engineering, University of Perugia, Italy stefano.agnetti@gmail.com ABSTRACT. The aim of this work is the study of the effect of the finishing of the edge of glass when it has a structural function. Experimental investigations carried out for glass specimens are presented. Various series of annealed glass beam were tested, with cut edge and with ground edge. The glass specimens are tested in four-point bending performing flaw detection on the tested specimens after failure, in order to determine glass strength. As a result, bending strength values are obtained for each specimen. Determining some physical parameter as the depth of the flaw and the mirror radius of the fracture, after the failure of a glass element, it could be possible to calculate the failure strength of that. The experimental results were analyzed with the LEFM theory and the glass strength was analyzed with a statistical study using two-parameter Weibull distribution fitting quite well the failure stress data. The results obtained constitute a validation of the theoretical models and show the influence of the edge processing on the failure strength of the glass. Furthermore, series with different sizes were tested in order to evaluate the size effect. SOMMARIO. Il lavoro presentato ha lo scopo di valutare la resistenza di elementi in vetro. Il vetro, materiale elasto-fragile per la sua struttura chimica amorfa, raggiunge la rottura in modo improvviso per valori di resistenza piuttosto dispersi a causa della presenza dei difetti sui bordi del vetro. Sono stati eseguiti test a flessione su quattro punti su elementi in vetro float con differenti finiture superficiali, per valutare l’influenza della lavorazione dei bordi sulla resistenza. Sono state testate alcune serie di elementi con bordi tagliati e altre con bordi molati. Solitamente la rottura di un elemento in vetro avviene a partire del difetto di maggiore grandezza, nella zona maggiormente sollecitata. Grazie alla lavorazione dei bordi si riesce a ridurre l’ampiezza dei difetti, che, sebbene di minore grandezza, sono ugualmente presenti nel vetro. La resistenza del vetro è stata determinata attraverso la teoria della meccanica della frattura lineare e mediante l’analisi post-rottura della superficie da cui si genere la frattura. L’analisi sperimentale ha permesso di valutare l’efficacia della finitura dei bordi in termini d’incremento della resistenza del vetro e la validazione dei modelli per la determinazione della resistenza. KEYWORDS. Edge strength; Fracture mechanic; Glass flaw; Grinding; Size effect. INTRODUCTION or hundreds of years, glass has been used as windows in buildings, while research on structural applications of glass has only just begun. In recent years, the knowledge on glass properties has expanded, bringing to light new ways of using glass, such as full transparent construction. Due to transparent nature of glass, it is used in multiple ways by F http://dx.medra.org/10.3221/IGF-ESIS.26.04&auth=true http://www.gruppofrattura.it S. Agnetti, Frattura ed Integrità Strutturale, 26 (2013) 31-40; DOI: 10.3221/IGF-ESIS.26.04 32 engineers and architects and today the research is further advancing at the field of studying glass properties both in structural aspects and in relation to building technology, energy and light. But glass is a challenging material due to its brittle feature. In order to use glass safely in structural applications, knowledge about its strength is required. The presence of the flaw in glass causes the failure [1]. The fracture mechanics shows how the failure depends on the depth of the flaw, on the number of them and also on the stress corrosion (called static fatigue in literature) [2]. The stress corrosion causes subcritical crack growth in glass. The crack propagation phenomenon occurs in glass when it is exposed to tensile stress and humidity. The particular flaw that produces the fracture is generally called the critical flaw. The processing of the edge of structural glass is studied; the edge has an important role to determine the failure. Indeed the finishing of the edge could remove in part the flaws or in other case it could produce other micro-cracks, without no- benefit for the strength of the glass [3]. The most important type of edge processings object of study [4] are grinding and polishing The strength of the glass can be evaluated through the fracture surface analysis: determining some physical parameter as the depth of the flaw and the mirror radius of the fracture after the failure of a glass element, it could be possible to calculate the failure strength of that [5]. For this evaluation, it was tested a group of glass element, in bending. It results that the edge processing has an influence on the failure strength of the glass. FRACTURE MECHANICS THEORY lass is an elastic material with a brittle behaviour at failure. Therefore linear elastic fracture mechanics (LEFM) is an ideal theory to model its behaviour. In fact, glass was the material used for the development of the basis of LEFM. In LEFM, mechanical material behaviour is modeled by looking at cracks. If we think at glass, as a material without flaws and defects, its resistance would be very high. But it doesn’t occur in practice because of the presence of the flaws. This phenomenon is explained by LEFM theory. According to the stress analysis conducted of an elliptical cavity in a uniformly stressed plate, the local stresses about a sharp notch or corner could raise to a level several times higher than the applied stress. It thus became apparent that even submicroscopic flaws might be potential sources of weakness in solids. Introducing the concept of the stress intensity factor (SIF), expressed to evaluate the failure, glass element fails when this value reaches the critical value KIc. The general relationship between the stress intensity factor KI, the nominal tensile stress normal to the crack’s plane σn, a correction factor Y, and some representative geometric parameter a, in general the crack depth or half of the crack length, is given by: K Y a I n   (1) The fracture toughness KIc, also known as the critical stress intensity factor, is the SIF that leads to instantaneous failure. KIc is a constant value and is also called fracture toughness. Values KIc are available in literature, for soda-lime glass it is 0.75 MPa m1/2. From LEFM is possible obtaining the failure stress form the measure of the depth of the flaw, as shown in [6] and [7]. Stress corrosion Glass is noted for its chemical inertness and general resistance to corrosion; therefore, it is used in the chemical industry and in the laboratory when chemical inertness is required. Despite this well-known property, glass is extremely susceptible to stress corrosion cracking caused by water in the environment. This phenomenon is known in the glass literature as static fatigue or delayed failure. The susceptibility of glass to stress corrosion cracking was observed noting a time delay to failure and a loading rate dependence of strength. This effect is an activated process caused by water in the environment. Static fatigue of glass results from the growth of small cracks in the surface of glass under the combined influence of water vapor and applied load. Actually, glass is time dependent if it is in presence of humidity (only in vacuum it is time-independent). Stress corrosion causes flaws to grow slowly when they are exposed to a positive crack opening stress. A glass element stressed below its momentary strength (e.g. the static load) will still fail after the time necessary for the most critical flaw to grow to its critical size at a particular stress level. G http://dx.medra.org/10.3221/IGF-ESIS.26.04&auth=true http://www.gruppofrattura.it S. Agnetti, Frattura ed Integrità Strutturale, 26 (2013) 31-40; DOI: 10.3221/IGF-ESIS.26.04 33 A kinematic relationship between crack velocity v and stress intensity factor KI exists and it is commonly used for glass lifetime prediction. For values of KI close to the critical value of KIc (that represents the glass toughness), v is independent of the environment and the crack propagates very rapidly (for soda lime silica glass is about 1500 m/s). In the v-KI logarithmic-curve, v0 represents the position and n is its slope. Below certain threshold stress intensity Kth no crack growth occurs. The value of v0 and n parameters are discussed by Haldimann [1], for laboratory condition, v0 can be assumed equal to 0.01 mm/s, instead it is 6 mm/s in environmental condition. The parameter n is assumed 16. According to the theory of fracture mechanics, glass failure stress was defined using stress intensity factor KI. This equation is only valid in testing conditions where stress corrosion could be eliminated. If the subcritical crack growth is considered, the crack propagates as a function of loading time. This approach is presented by Haldimann [1], in which the crack velocity parameter v0 has the dimension of a velocity, instead n is dimensionless.   2 2 0 0 2 ( ) ( ) n n ntn nn i Ic n a t a v K Y d n               (2) The same relation can be expressed in terms of the value σ with a static loading time. It is possible to obtain the failure stress σf, knowing the tf (s), i.e. the failure loading time and assuming aci (m) corresponding to the initial crack flaw depth.   1 2 2 0 2 2 ( ) ( ) / n f f n n f Ic ci t t n v Y K a                (3) Until a certain loading time, the inert strength is considered to determine the failure. But with the increase of the loading time, in presence of the stress corrosion, the relation (3) is used to determine the failure strength. The theoretical transition time loading between inert condition and time-depending condition, tref, that could be considered a reference value is obtained by Eq. (1) and (3). 0 2 2( ) ref a t n v   (4) It t>tref the strength decreases following (3), instead if t