id	author	title	date	pages	extension	mime	words	sentence	flesch	summary	cache	txt
hjic-83	Temesvári, K.; Aranyi, A.; Balogh, S.; Bánkuti, Gy.; Csukás, B.	Separation of a Two-Component Steroid Mixture by Simulated Moving Bed Chromatography	2004	8	.pdf	application/pdf	3906	165	56	Analytical Method for Measurement of SMB Samples The samples of SMB experiments were examined by analytical HPLC which consisted of a gradient pump (SpectraSYSTEM P2000), a controller (SpectraSYSTEM SN4000), a light scattering detector (Polymer Laboratories PL-ELS 2100), a thermostat (JET-STREAM Plus) and an injection valve (Rheodyne, 20 µL loop). [mg/(g min)] Specific solvent consumption (ml/mg A) Recovery (%) Purity (%) Isocratic, 8 columns, 4 zones, column connection: 2-2-2-2 SMB-5 36:9 0.7891 0.2429 98.62 100 Isocratic, 16 columns, 4 zones SMB-7 2-6-6-2 36:9 0.8114 0.2376 100 97.46 SMB-8 2-6-6-2 36:9 0.7920 0.2471 99.31 100 SMB-10 3-4-7-2 36:9 0.8065 0.1907 99.25 100 Gradient, 16 columns, 3 zones SMB-11 3-5-8 48:12 1.0175 0.2015 99.86 100 Therefore in the following the main goal was to decrease the specific solvent consumption by changing the column distribution in the four zones of the SMB unit.	cache/hjic-83.pdf	txt/hjic-83.txt