id	author	title	date	pages	extension	mime	words	sentence	flesch	summary	cache	txt
iajs-524	Mahmoud, Muhanned J.; AL-bayati, Redha I.; Saoud, Shaimaa A.; Majeed, Ismaeel Y.	Synthesis And Characterization of 5-(Mercapto-1,3,4Thiadiazole-2yl)α,α-Diphenyl Methanol From Benzilic Acid	2017	8	.pdf	application/pdf	2001	146	68	The FT.IR showed band 1060 cm–1 due to bending vibration of (C=S)[15] group, appearance band between (1685–1720) cm–1 due to stretching vibration of (C=N) group, also appearance very week band at 2478 cm–1 due to (S–H) group, appearance strong band at (1445–1496) cm–1 due to stretching vibration of (–N–C=S)[16], and appearance band at 3049 cm–1 due to (C–H) Aromatic. [S31] The compound (4)identified by m.p and FT.IR spectra, the FT.IR spectra showed the disappearance of absorption band at the (3251–3300) cm–1 due to the asymmetric and symmetric stretching vibration of the (–NH–NH2) group, appearance band at 1049 cm–1 due to bending vibration of (C=S)(15), also appearance band at (1448–1492) cm–1 due to (–N– C=S)(16) stretching vibration this band according strong evidence to presence the potassium xanthate and also appearance band at 1614 cm–1 due to (C=O) amide while disappearance band at 1700 cm–1 due to (C=O) of α–hydroxyl–α,α–diphenyl acetohydrazide (3) this two evidence to presence this reaction.	cache/iajs-524.pdf	txt/iajs-524.txt