id sid tid token lemma pos iajs-1066 1 1 microsoft microsoft PROPN iajs-1066 1 2 word word NOUN iajs-1066 1 3 131 131 NUM iajs-1066 1 4 - - SYM iajs-1066 1 5 142 142 NUM iajs-1066 1 6 chemistry chemistry NOUN iajs-1066 1 7 | | ADV iajs-1066 1 8 131 131 NUM iajs-1066 1 9 2017عام 2017عام NUM iajs-1066 1 10 ) ) PUNCT iajs-1066 1 11 1(العدد 1(العدد NUM iajs-1066 1 12 30المجلد 30المجلد NUM iajs-1066 1 13 مجلة مجلة VERB iajs-1066 1 14 إبن إبن NOUN iajs-1066 1 15 الھيثم الھيثم NOUN iajs-1066 1 16 للعلوم للعلوم NOUN iajs-1066 1 17 الصرفة الصرفة NOUN iajs-1066 1 18 والتطبيقية والتطبيقية VERB iajs-1066 1 19 ibn ibn PROPN iajs-1066 1 20 al al PROPN iajs-1066 1 21 - - PUNCT iajs-1066 1 22 haitham haitham PROPN iajs-1066 1 23 jour jour X iajs-1066 1 24 . . PROPN iajs-1066 2 1 for for ADP iajs-1066 2 2 pure pure ADJ iajs-1066 2 3 & & CCONJ iajs-1066 2 4 appl appl PROPN iajs-1066 2 5 . . PUNCT iajs-1066 3 1 sci sci PROPN iajs-1066 3 2 . . PUNCT iajs-1066 3 3 vol vol NOUN iajs-1066 3 4 . . PROPN iajs-1066 3 5 30 30 NUM iajs-1066 3 6 ( ( PUNCT iajs-1066 3 7 1 1 NUM iajs-1066 3 8 ) ) PUNCT iajs-1066 3 9 2017 2017 NUM iajs-1066 3 10 metal metal NOUN iajs-1066 3 11 ( ( PUNCT iajs-1066 3 12 ii ii NOUN iajs-1066 3 13 ) ) PUNCT iajs-1066 3 14 complexes complex NOUN iajs-1066 3 15 with with ADP iajs-1066 3 16 tridentate tridentate PROPN iajs-1066 3 17 n n CCONJ iajs-1066 3 18 , , PUNCT iajs-1066 3 19 n n CCONJ iajs-1066 3 20 , , PUNCT iajs-1066 3 21 o o PROPN iajs-1066 3 22 ligand ligand NOUN iajs-1066 3 23 : : PUNCT iajs-1066 3 24 synthesis synthesis NOUN iajs-1066 3 25 , , PUNCT iajs-1066 3 26 characterization characterization NOUN iajs-1066 3 27 and and CCONJ iajs-1066 3 28 biological biological ADJ iajs-1066 3 29 studies study NOUN iajs-1066 3 30     SPACE iajs-1066 3 31 ali ali PROPN iajs-1066 3 32 n. n. PROPN iajs-1066 3 33 niseaf niseaf PROPN iajs-1066 3 34     SPACE iajs-1066 3 35 dept dept NOUN iajs-1066 3 36 . . PUNCT iajs-1066 4 1 of of ADP iajs-1066 4 2 chemistry/ chemistry/ NUM iajs-1066 4 3 college college NOUN iajs-1066 4 4 of of ADP iajs-1066 4 5 education education NOUN iajs-1066 4 6 for for ADP iajs-1066 4 7 pure pure ADJ iajs-1066 4 8 sciences science NOUN iajs-1066 4 9 ( ( PUNCT iajs-1066 4 10 ibn ibn PROPN iajs-1066 4 11 al al PROPN iajs-1066 4 12 - - PUNCT iajs-1066 4 13 haitham)/ haitham)/ PROPN iajs-1066 4 14 university university NOUN iajs-1066 4 15 of of ADP iajs-1066 4 16 baghdad baghdad PROPN iajs-1066 4 17 received receive VERB iajs-1066 4 18 in:12 in:12 PROPN iajs-1066 4 19 / / SYM iajs-1066 4 20 january/2016,acceted january/2016,accete VERB iajs-1066 4 21 in:28 in:28 PROPN iajs-1066 4 22 / / SYM iajs-1066 4 23 june/2016 june/2016 PROPN iajs-1066 4 24 abstract abstract VERB iajs-1066 4 25 the the DET iajs-1066 4 26 preparation preparation NOUN iajs-1066 4 27 of of ADP iajs-1066 4 28 some some DET iajs-1066 4 29 new new ADJ iajs-1066 4 30 coordination coordination NOUN iajs-1066 4 31 compounds compound NOUN iajs-1066 4 32 for for ADP iajs-1066 4 33 nikel nikel NOUN iajs-1066 4 34 ( ( PUNCT iajs-1066 4 35 ii ii NOUN iajs-1066 4 36 ) ) PUNCT iajs-1066 4 37 , , PUNCT iajs-1066 4 38 manganese manganese NOUN iajs-1066 4 39 ( ( PUNCT iajs-1066 4 40 ii ii NOUN iajs-1066 4 41 ) ) PUNCT iajs-1066 4 42 , , PUNCT iajs-1066 4 43 copper copper NOUN iajs-1066 4 44 ( ( PUNCT iajs-1066 4 45 ii ii NOUN iajs-1066 4 46 ) ) PUNCT iajs-1066 4 47 , , PUNCT iajs-1066 4 48 cobalt cobalt NOUN iajs-1066 4 49 ( ( PUNCT iajs-1066 4 50 ii)and ii)and NOUN iajs-1066 4 51 mercury mercury NOUN iajs-1066 4 52 ( ( PUNCT iajs-1066 4 53 ii ii NOUN iajs-1066 4 54 ) ) PUNCT iajs-1066 4 55 , , PUNCT iajs-1066 4 56 with with ADP iajs-1066 4 57 ligand ligand NOUN iajs-1066 4 58 obtained obtain VERB iajs-1066 4 59 from from ADP iajs-1066 4 60 benzoinand2 benzoinand2 NOUN iajs-1066 4 61 - - NOUN iajs-1066 4 62 amino amino ADJ iajs-1066 4 63 pyridine.the pyridine.the DET iajs-1066 4 64 ligand[6-(2 ligand[6-(2 NOUN iajs-1066 4 65 - - PUNCT iajs-1066 4 66 hydroxy-1,2 hydroxy-1,2 NUM iajs-1066 4 67 - - PUNCT iajs-1066 4 68 diphenylethylideneamino)pyridin-3 diphenylethylideneamino)pyridin-3 NOUN iajs-1066 4 69 - - PUNCT iajs-1066 4 70 ylium)](l ylium)](l NOUN iajs-1066 4 71 ) ) PUNCT iajs-1066 4 72 was be AUX iajs-1066 4 73 made make VERB iajs-1066 4 74 from from ADP iajs-1066 4 75 reactin reactin NOUN iajs-1066 4 76 ethanol ethanol NOUN iajs-1066 4 77 with with ADP iajs-1066 4 78 metal metal NOUN iajs-1066 4 79 salts salt NOUN iajs-1066 4 80 in in ADP iajs-1066 4 81 ( ( PUNCT iajs-1066 4 82 1:1)(metal 1:1)(metal NUM iajs-1066 4 83 : : PUNCT iajs-1066 4 84 ligand)ratio.[mlcl ligand)ratio.[mlcl PROPN iajs-1066 4 85 ] ] PUNCT iajs-1066 4 86 was be AUX iajs-1066 4 87 the the DET iajs-1066 4 88 inclusive inclusive ADJ iajs-1066 4 89 formula formula NOUN iajs-1066 4 90 of of ADP iajs-1066 4 91 the the DET iajs-1066 4 92 complexes complex NOUN iajs-1066 4 93 where where SCONJ iajs-1066 4 94 m= m= X iajs-1066 4 95 mn(ii),co(ii),ni(ii),cu(ii mn(ii),co(ii),ni(ii),cu(ii VERB iajs-1066 4 96 ) ) PUNCT iajs-1066 4 97 and and CCONJ iajs-1066 4 98 hg(ii hg(ii PROPN iajs-1066 4 99 ) ) PUNCT iajs-1066 4 100 . . PUNCT iajs-1066 5 1 metal metal NOUN iajs-1066 5 2 analysis analysis NOUN iajs-1066 5 3 by by ADP iajs-1066 5 4 electronic electronic ADJ iajs-1066 5 5 spectra spectra NOUN iajs-1066 5 6 , , PUNCT iajs-1066 5 7 atomic atomic ADJ iajs-1066 5 8 absorption absorption NOUN iajs-1066 5 9 , , PUNCT iajs-1066 5 10 infrared infrared PROPN iajs-1066 5 11 spectra spectra PROPN iajs-1066 5 12 , , PUNCT iajs-1066 5 13 1h&13c 1h&13c NUM iajs-1066 5 14 - - PUNCT iajs-1066 5 15 nmr(only nmr(only ADV iajs-1066 5 16 ligand)spectral ligand)spectral ADJ iajs-1066 5 17 studies study NOUN iajs-1066 5 18 , , PUNCT iajs-1066 5 19 magnetic magnetic ADJ iajs-1066 5 20 moment moment NOUN iajs-1066 5 21 and and CCONJ iajs-1066 5 22 molar molar ADJ iajs-1066 5 23 conductance conductance NOUN iajs-1066 5 24 measurements measurement NOUN iajs-1066 5 25 used use VERB iajs-1066 5 26 to to PART iajs-1066 5 27 describe describe VERB iajs-1066 5 28 the the DET iajs-1066 5 29 compounds.the compounds.the DET iajs-1066 5 30 determinations determination NOUN iajs-1066 5 31 indicated indicate VERB iajs-1066 5 32 that that SCONJ iajs-1066 5 33 the the DET iajs-1066 5 34 ligand ligand NOUN iajs-1066 5 35 coordinates coordinate NOUN iajs-1066 5 36 with with ADP iajs-1066 5 37 the the DET iajs-1066 5 38 metal metal NOUN iajs-1066 5 39 ( ( PUNCT iajs-1066 5 40 ii ii NOUN iajs-1066 5 41 ) ) PUNCT iajs-1066 5 42 ion ion NOUN iajs-1066 5 43 in in ADP iajs-1066 5 44 neutral neutral ADJ iajs-1066 5 45 tridentate tridentate NOUN iajs-1066 5 46 manner manner NOUN iajs-1066 5 47 through through ADP iajs-1066 5 48 the the DET iajs-1066 5 49 azomethine azomethine PROPN iajs-1066 5 50 nitrogen nitrogen NOUN iajs-1066 5 51 atom atom NOUN iajs-1066 5 52 , , PUNCT iajs-1066 5 53 nitrogen nitrogen NOUN iajs-1066 5 54 atom atom NOUN iajs-1066 5 55 for for ADP iajs-1066 5 56 pyridine pyridine NOUN iajs-1066 5 57 and and CCONJ iajs-1066 5 58 oxygen oxygen NOUN iajs-1066 5 59 atom atom NOUN iajs-1066 5 60 of of ADP iajs-1066 5 61 the the DET iajs-1066 5 62 benzoin benzoin NOUN iajs-1066 5 63 , , PUNCT iajs-1066 5 64 all all DET iajs-1066 5 65 the the DET iajs-1066 5 66 studies study NOUN iajs-1066 5 67 reveal reveal VERB iajs-1066 5 68 coordination coordination NOUN iajs-1066 5 69 four four NUM iajs-1066 5 70 for for ADP iajs-1066 5 71 the the DET iajs-1066 5 72 metals metal NOUN iajs-1066 5 73 in in ADP iajs-1066 5 74 all all DET iajs-1066 5 75 the the DET iajs-1066 5 76 complexes complex NOUN iajs-1066 5 77 . . PUNCT iajs-1066 6 1 tetrahedral tetrahedral ADJ iajs-1066 6 2 and and CCONJ iajs-1066 6 3 square square ADJ iajs-1066 6 4 planar planar ADJ iajs-1066 6 5 structures structure NOUN iajs-1066 6 6 were be AUX iajs-1066 6 7 suggested suggest VERB iajs-1066 6 8 for for ADP iajs-1066 6 9 metal metal NOUN iajs-1066 6 10 complexes complex NOUN iajs-1066 6 11 . . PUNCT iajs-1066 7 1 key key ADJ iajs-1066 7 2 words word NOUN iajs-1066 7 3 : : PUNCT iajs-1066 7 4 schiff schiff NOUN iajs-1066 7 5 base base NOUN iajs-1066 7 6 , , PUNCT iajs-1066 7 7 2 2 NUM iajs-1066 7 8 - - PUNCT iajs-1066 7 9 amino amino NOUN iajs-1066 7 10 pyridine pyridine NOUN iajs-1066 7 11 , , PUNCT iajs-1066 7 12 characterization characterization NOUN iajs-1066 7 13 , , PUNCT iajs-1066 7 14 metal metal NOUN iajs-1066 7 15 chelate chelate NOUN iajs-1066 7 16 complexes complex NOUN iajs-1066 7 17 . . PUNCT iajs-1066 8 1 chemistry chemistry NOUN iajs-1066 8 2 | | ADV iajs-1066 8 3 132 132 NUM iajs-1066 8 4 2017عام 2017عام NUM iajs-1066 8 5 ) ) PUNCT iajs-1066 8 6 1(العدد 1(العدد NUM iajs-1066 8 7 30المجلد 30المجلد NUM iajs-1066 8 8 مجلة مجلة VERB iajs-1066 8 9 إبن إبن NOUN iajs-1066 8 10 الھيثم الھيثم NOUN iajs-1066 8 11 للعلوم للعلوم NOUN iajs-1066 8 12 الصرفة الصرفة NOUN iajs-1066 8 13 والتطبيقية والتطبيقية VERB iajs-1066 8 14 ibn ibn PROPN iajs-1066 8 15 al al PROPN iajs-1066 8 16 - - PUNCT iajs-1066 8 17 haitham haitham PROPN iajs-1066 8 18 jour jour X iajs-1066 8 19 . . PROPN iajs-1066 9 1 for for ADP iajs-1066 9 2 pure pure ADJ iajs-1066 9 3 & & CCONJ iajs-1066 9 4 appl appl PROPN iajs-1066 9 5 . . PUNCT iajs-1066 10 1 sci sci PROPN iajs-1066 10 2 . . PUNCT iajs-1066 10 3 vol vol NOUN iajs-1066 10 4 . . PROPN iajs-1066 10 5 30 30 NUM iajs-1066 10 6 ( ( PUNCT iajs-1066 10 7 1 1 NUM iajs-1066 10 8 ) ) PUNCT iajs-1066 10 9 2017 2017 NUM iajs-1066 10 10 introduction introduction NOUN iajs-1066 10 11 amino amino NOUN iajs-1066 10 12 compounds compound NOUN iajs-1066 10 13 as as ADP iajs-1066 10 14 heterocyclic heterocyclic NOUN iajs-1066 10 15 containing contain VERB iajs-1066 10 16 one one NUM iajs-1066 10 17 or or CCONJ iajs-1066 10 18 more more ADJ iajs-1066 10 19 possibilitygiver possibilitygiver ADP iajs-1066 10 20 centers center NOUN iajs-1066 10 21 took take VERB iajs-1066 10 22 asignificant asignificant ADJ iajs-1066 10 23 assignment assignment NOUN iajs-1066 10 24 in in ADP iajs-1066 10 25 the the DET iajs-1066 10 26 study study NOUN iajs-1066 10 27 of of ADP iajs-1066 10 28 reaction reaction NOUN iajs-1066 10 29 of of ADP iajs-1066 10 30 atridentate atridentate ADJ iajs-1066 10 31 schiff schiff NOUN iajs-1066 10 32 base base NOUN iajs-1066 10 33 system system NOUN iajs-1066 10 34 [ [ X iajs-1066 10 35 1 1 NUM iajs-1066 10 36 ] ] PUNCT iajs-1066 10 37 . . PUNCT iajs-1066 11 1 they they PRON iajs-1066 11 2 are be AUX iajs-1066 11 3 recognized recognize VERB iajs-1066 11 4 to to PART iajs-1066 11 5 act act VERB iajs-1066 11 6 ligands ligand NOUN iajs-1066 11 7 as as ADP iajs-1066 11 8 bidentate bidentate NOUN iajs-1066 11 9 or or CCONJ iajs-1066 11 10 tridentate tridentate NOUN iajs-1066 11 11 when when SCONJ iajs-1066 11 12 chelated chelate VERB iajs-1066 11 13 to to ADP iajs-1066 11 14 metalion metalion NOUN iajs-1066 11 15 [ [ X iajs-1066 11 16 2 2 NUM iajs-1066 11 17 ] ] PUNCT iajs-1066 11 18 . . PUNCT iajs-1066 12 1 schiff schiff NOUN iajs-1066 12 2 bases basis NOUN iajs-1066 12 3 are be AUX iajs-1066 12 4 a a DET iajs-1066 12 5 grade grade NOUN iajs-1066 12 6 of of ADP iajs-1066 12 7 significant significant ADJ iajs-1066 12 8 compounds compound NOUN iajs-1066 12 9 due due ADP iajs-1066 12 10 to to ADP iajs-1066 12 11 their their PRON iajs-1066 12 12 broad broad ADJ iajs-1066 12 13 domain domain NOUN iajs-1066 12 14 of of ADP iajs-1066 12 15 enforcements enforcement NOUN iajs-1066 12 16 and and CCONJ iajs-1066 12 17 qualities quality NOUN iajs-1066 12 18 [ [ X iajs-1066 12 19 3].schiff 3].schiff NUM iajs-1066 12 20 base base NOUN iajs-1066 12 21 and and CCONJ iajs-1066 12 22 its its PRON iajs-1066 12 23 complexes complex NOUN iajs-1066 12 24 have have AUX iajs-1066 12 25 presented present VERB iajs-1066 12 26 with with ADP iajs-1066 12 27 a a DET iajs-1066 12 28 lot lot NOUN iajs-1066 12 29 notice notice NOUN iajs-1066 12 30 because because SCONJ iajs-1066 12 31 of of ADP iajs-1066 12 32 their their PRON iajs-1066 12 33 use use NOUN iajs-1066 12 34 as as ADP iajs-1066 12 35 models model NOUN iajs-1066 12 36 for for ADP iajs-1066 12 37 biological biological ADJ iajs-1066 12 38 arrangement arrangement NOUN iajs-1066 12 39 and and CCONJ iajs-1066 12 40 applications application NOUN iajs-1066 12 41 as as ADP iajs-1066 12 42 i.e. i.e. X iajs-1066 12 43 in in ADP iajs-1066 12 44 the the DET iajs-1066 12 45 areas area NOUN iajs-1066 12 46 of of ADP iajs-1066 12 47 catalysis catalysis NOUN iajs-1066 12 48 clinical clinical ADJ iajs-1066 12 49 application[4 application[4 NOUN iajs-1066 12 50 ] ] PUNCT iajs-1066 12 51 , , PUNCT iajs-1066 12 52 pharmacologically pharmacologically ADV iajs-1066 12 53 and and CCONJ iajs-1066 12 54 photochemical[5].schiff photochemical[5].schiff PROPN iajs-1066 12 55 bases basis NOUN iajs-1066 12 56 are be AUX iajs-1066 12 57 reported report VERB iajs-1066 12 58 to to PART iajs-1066 12 59 possess possess VERB iajs-1066 12 60 antibacterial[6],antifungal[7],anticancer[8],herbicidal antibacterial[6],antifungal[7],anticancer[8],herbicidal DET iajs-1066 12 61 anticonvulsant anticonvulsant NOUN iajs-1066 12 62 [ [ X iajs-1066 12 63 9 9 NUM iajs-1066 12 64 ] ] PUNCT iajs-1066 12 65 and and CCONJ iajs-1066 12 66 diuretic diuretic ADJ iajs-1066 12 67 activities[10].these activities[10].these ADJ iajs-1066 12 68 ligands ligand NOUN iajs-1066 12 69 have have VERB iajs-1066 12 70 ono ono PROPN iajs-1066 12 71 giver giver NOUN iajs-1066 12 72 atom atom NOUN iajs-1066 12 73 group group NOUN iajs-1066 12 74 were be AUX iajs-1066 12 75 attracted attract VERB iajs-1066 12 76 the the DET iajs-1066 12 77 interest interest NOUN iajs-1066 12 78 of of ADP iajs-1066 12 79 many many ADJ iajs-1066 12 80 authors author NOUN iajs-1066 12 81 are be AUX iajs-1066 12 82 well well ADV iajs-1066 12 83 recognized recognize VERB iajs-1066 12 84 to to PART iajs-1066 12 85 coordinate coordinate VERB iajs-1066 12 86 with with ADP iajs-1066 12 87 various various ADJ iajs-1066 12 88 metal metal NOUN iajs-1066 12 89 ions ion NOUN iajs-1066 12 90 and and CCONJ iajs-1066 12 91 this this PRON iajs-1066 12 92 has have VERB iajs-1066 12 93 [ [ X iajs-1066 12 94 11 11 NUM iajs-1066 12 95 ] ] PUNCT iajs-1066 12 96 . . PUNCT iajs-1066 13 1 in in ADP iajs-1066 13 2 this this DET iajs-1066 13 3 study study NOUN iajs-1066 13 4 , , PUNCT iajs-1066 13 5 schiff schiff NOUN iajs-1066 13 6 base base NOUN iajs-1066 13 7 of of ADP iajs-1066 13 8 2 2 NUM iajs-1066 13 9 - - PUNCT iajs-1066 13 10 aminopyridine aminopyridine NOUN iajs-1066 13 11 with with ADP iajs-1066 13 12 benzoin benzoin NOUN iajs-1066 13 13 has have AUX iajs-1066 13 14 been be AUX iajs-1066 13 15 synthesized synthesize VERB iajs-1066 13 16 , , PUNCT iajs-1066 13 17 characterized characterized ADJ iajs-1066 13 18 and and CCONJ iajs-1066 13 19 antibacterial antibacterial ADJ iajs-1066 13 20 activity activity NOUN iajs-1066 13 21 study study NOUN iajs-1066 13 22 of of ADP iajs-1066 13 23 the the DET iajs-1066 13 24 new new ADJ iajs-1066 13 25 complexes complex NOUN iajs-1066 13 26 were be AUX iajs-1066 13 27 prepared.further prepared.further ADV iajs-1066 13 28 more more ADJ iajs-1066 13 29 , , PUNCT iajs-1066 13 30 the the DET iajs-1066 13 31 structures structure NOUN iajs-1066 13 32 of of ADP iajs-1066 13 33 prepared prepared ADJ iajs-1066 13 34 compounds compound NOUN iajs-1066 13 35 were be AUX iajs-1066 13 36 definite definite ADJ iajs-1066 13 37 by by ADP iajs-1066 13 38 spectral spectral ADJ iajs-1066 13 39 studies.the studies.the NOUN iajs-1066 13 40 arrangement arrangement NOUN iajs-1066 13 41 of of ADP iajs-1066 13 42 the the DET iajs-1066 13 43 compounds compound NOUN iajs-1066 13 44 is be AUX iajs-1066 13 45 displayed display VERB iajs-1066 13 46 in in ADP iajs-1066 13 47 scheme(1 scheme(1 NOUN iajs-1066 13 48 ) ) PUNCT iajs-1066 13 49 and(2 and(2 NOUN iajs-1066 13 50 ) ) PUNCT iajs-1066 13 51 . . PUNCT iajs-1066 14 1 experimental experimental ADJ iajs-1066 14 2 2 2 NUM iajs-1066 14 3 - - PUNCT iajs-1066 14 4 amino amino NOUN iajs-1066 14 5 pyridine pyridine NOUN iajs-1066 14 6 and and CCONJ iajs-1066 14 7 benzoin benzoin NOUN iajs-1066 14 8 were be AUX iajs-1066 14 9 purchased purchase VERB iajs-1066 14 10 from from ADP iajs-1066 14 11 sigma sigma PROPN iajs-1066 14 12 chemical chemical PROPN iajs-1066 14 13 co. co. PROPN iajs-1066 14 14 ( ( PUNCT iajs-1066 14 15 usa usa PROPN iajs-1066 14 16 ) ) PUNCT iajs-1066 14 17 . . PUNCT iajs-1066 15 1 glacial glacial ADJ iajs-1066 15 2 acetic acetic ADJ iajs-1066 15 3 acidreagent acidreagent NOUN iajs-1066 15 4 from from ADP iajs-1066 15 5 " " PUNCT iajs-1066 15 6 ( ( PUNCT iajs-1066 15 7 aldrich aldrich PROPN iajs-1066 15 8 and and CCONJ iajs-1066 15 9 sigma)".the sigma)".the PRON iajs-1066 15 10 all all DET iajs-1066 15 11 metal metal NOUN iajs-1066 15 12 salts salt NOUN iajs-1066 15 13 used use VERB iajs-1066 15 14 were be AUX iajs-1066 15 15 gave give VERB iajs-1066 15 16 from from ADP iajs-1066 15 17 ( ( PUNCT iajs-1066 15 18 bdh bdh NOUN iajs-1066 15 19 ) ) PUNCT iajs-1066 15 20 . . PUNCT iajs-1066 16 1 instrumentation instrumentation NOUN iajs-1066 16 2 melting melting NOUN iajs-1066 16 3 point point NOUN iajs-1066 16 4 were be AUX iajs-1066 16 5 determined determine VERB iajs-1066 16 6 on on ADP iajs-1066 16 7 " " PUNCT iajs-1066 16 8 gallenkamp gallenkamp ADJ iajs-1066 16 9 melting melting NOUN iajs-1066 16 10 point point NOUN iajs-1066 16 11 apparatus apparatus NOUN iajs-1066 16 12 " " PUNCT iajs-1066 16 13 .elemental .elemental DET iajs-1066 16 14 microanalysis microanalysis PROPN iajs-1066 16 15 c.h.n c.h.n PROPN iajs-1066 16 16 . . PROPN iajs-1066 16 17 were be AUX iajs-1066 16 18 carried carry VERB iajs-1066 16 19 out out ADP iajs-1066 16 20 using use VERB iajs-1066 16 21 " " PUNCT iajs-1066 16 22 euro euro NOUN iajs-1066 16 23 vector vector NOUN iajs-1066 16 24 ea ea NOUN iajs-1066 16 25 3000 3000 NUM iajs-1066 16 26 a a DET iajs-1066 16 27 analysis".ft analysis".ft PUNCT iajs-1066 16 28 - - PUNCT iajs-1066 16 29 ir ir NOUN iajs-1066 16 30 measurements measurement NOUN iajs-1066 16 31 were be AUX iajs-1066 16 32 recorded record VERB iajs-1066 16 33 on on ADP iajs-1066 16 34 " " PUNCT iajs-1066 16 35 shimadzu8300 shimadzu8300 PROPN iajs-1066 16 36 spectrophotometer spectrophotometer NOUN iajs-1066 16 37 " " PUNCT iajs-1066 16 38 . . 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PUNCT iajs-1066 26 1 ethanol ethanol NOUN iajs-1066 26 2 / / SYM iajs-1066 26 3 haa haa NOUN iajs-1066 26 4 chemistry chemistry NOUN iajs-1066 26 5 | | ADV iajs-1066 26 6 133 133 NUM iajs-1066 26 7 2017عام 2017عام NUM iajs-1066 26 8 ) ) PUNCT iajs-1066 26 9 1(العدد 1(العدد NUM iajs-1066 26 10 30المجلد 30المجلد NUM iajs-1066 26 11 مجلة مجلة VERB iajs-1066 26 12 إبن إبن NOUN iajs-1066 26 13 الھيثم الھيثم NOUN iajs-1066 26 14 للعلوم للعلوم NOUN iajs-1066 26 15 الصرفة الصرفة NOUN iajs-1066 26 16 والتطبيقية والتطبيقية VERB iajs-1066 26 17 ibn ibn PROPN iajs-1066 26 18 al al PROPN iajs-1066 26 19 - - PUNCT iajs-1066 26 20 haitham haitham PROPN iajs-1066 26 21 jour jour X iajs-1066 26 22 . . PROPN iajs-1066 26 23 for for ADP iajs-1066 26 24 pure pure ADJ iajs-1066 26 25 & & CCONJ iajs-1066 26 26 appl appl PROPN iajs-1066 26 27 . . PUNCT iajs-1066 27 1 sci sci PROPN iajs-1066 27 2 . . PUNCT iajs-1066 27 3 vol vol NOUN iajs-1066 27 4 . . PROPN iajs-1066 27 5 30 30 NUM iajs-1066 27 6 ( ( PUNCT iajs-1066 27 7 1 1 NUM iajs-1066 27 8 ) ) SYM iajs-1066 27 9 2017 2017 NUM iajs-1066 27 10 synthesis synthesis NOUN iajs-1066 27 11 of of ADP iajs-1066 27 12 m(ii m(ii NOUN iajs-1066 27 13 ) ) PUNCT iajs-1066 27 14 complexes complexe VERB iajs-1066 27 15 a a DET iajs-1066 27 16 solution solution NOUN iajs-1066 27 17 of of ADP iajs-1066 27 18 metal metal NOUN iajs-1066 27 19 ( ( PUNCT iajs-1066 27 20 ii ii NOUN iajs-1066 27 21 ) ) PUNCT iajs-1066 27 22 chlorides chloride NOUN iajs-1066 27 23 in in ADP iajs-1066 27 24 ethanol ethanol NOUN iajs-1066 27 25 ( ( PUNCT iajs-1066 27 26 2mmole 2mmole NUM iajs-1066 27 27 ) ) PUNCT iajs-1066 27 28 was be AUX iajs-1066 27 29 stirred stir VERB iajs-1066 27 30 with with ADP iajs-1066 27 31 ethanolic ethanolic ADJ iajs-1066 27 32 solution solution NOUN iajs-1066 27 33 of of ADP iajs-1066 27 34 the the DET iajs-1066 27 35 schiff schiff NOUN iajs-1066 27 36 base base NOUN iajs-1066 27 37 ( ( PUNCT iajs-1066 27 38 2mmole)and 2mmole)and NUM iajs-1066 27 39 three three NUM iajs-1066 27 40 drops drop NOUN iajs-1066 27 41 from from ADP iajs-1066 27 42 koh koh PROPN iajs-1066 27 43 solution solution NOUN iajs-1066 27 44 , , PUNCT iajs-1066 27 45 for for ADP iajs-1066 27 46 ca ca NOUN iajs-1066 27 47 . . PUNCT iajs-1066 28 1 2 2 NUM iajs-1066 28 2 h h NOUN iajs-1066 28 3 on on ADP iajs-1066 28 4 a a DET iajs-1066 28 5 magnetic magnetic ADJ iajs-1066 28 6 stirrer stirrer NOUN iajs-1066 28 7 at at ADP iajs-1066 28 8 50oc 50oc PROPN iajs-1066 28 9 . . PUNCT iajs-1066 29 1 the the DET iajs-1066 29 2 solid solid ADJ iajs-1066 29 3 complex complex NOUN iajs-1066 29 4 precipitated precipitate VERB iajs-1066 29 5 was be AUX iajs-1066 29 6 filtered filter VERB iajs-1066 29 7 off off ADP iajs-1066 29 8 and and CCONJ iajs-1066 29 9 washed wash VERB iajs-1066 29 10 thoroughly thoroughly ADV iajs-1066 29 11 with with ADP iajs-1066 29 12 ethanol ethanol NOUN iajs-1066 29 13 and and CCONJ iajs-1066 29 14 dried dry VERB iajs-1066 29 15 in in ADP iajs-1066 29 16 vacuous vacuous ADJ iajs-1066 29 17 , , PUNCT iajs-1066 29 18 recrystallized recrystallize VERB iajs-1066 29 19 from from ADP iajs-1066 29 20 a a DET iajs-1066 29 21 hot hot NOUN iajs-1066 29 22 of of ADP iajs-1066 29 23 ( ( PUNCT iajs-1066 29 24 10ml 10ml ADJ iajs-1066 29 25 ) ) PUNCT iajs-1066 29 26 ethanol ethanol NOUN iajs-1066 29 27 , , PUNCT iajs-1066 29 28 a a DET iajs-1066 29 29 coloured coloured ADJ iajs-1066 29 30 precipitate precipitate NOUN iajs-1066 29 31 was be AUX iajs-1066 29 32 formed form VERB iajs-1066 29 33 [ [ X iajs-1066 29 34 5 5 NUM iajs-1066 29 35 , , PUNCT iajs-1066 29 36 6].the 6].the DET iajs-1066 29 37 physical physical ADJ iajs-1066 29 38 properties property NOUN iajs-1066 29 39 of of ADP iajs-1066 29 40 complexes complex NOUN iajs-1066 29 41 were be AUX iajs-1066 29 42 listed list VERB iajs-1066 29 43 in in ADP iajs-1066 29 44 table table NOUN iajs-1066 29 45 ( ( PUNCT iajs-1066 29 46 1 1 NUM iajs-1066 29 47 ) ) PUNCT iajs-1066 29 48 . . PUNCT iajs-1066 29 49     SPACE iajs-1066 30 1 results result NOUN iajs-1066 30 2 and and CCONJ iajs-1066 30 3 discussion discussion NOUN iajs-1066 30 4 nmr nmr NOUN iajs-1066 30 5 spectrum spectrum VERB iajs-1066 30 6 the the DET iajs-1066 30 7 1h 1h NUM iajs-1066 30 8 nmr nmr NOUN iajs-1066 30 9 spectrum spectrum NOUN iajs-1066 30 10 shows show VERB iajs-1066 30 11 signals signal NOUN iajs-1066 30 12 at at ADP iajs-1066 30 13 : : PUNCT iajs-1066 30 14 1.15 1.15 NUM iajs-1066 30 15 ppm ppm NOUN iajs-1066 30 16 singlet singlet NOUN iajs-1066 30 17 for for ADP iajs-1066 30 18 1h 1h NUM iajs-1066 30 19 benzoin benzoin NOUN iajs-1066 30 20 h h NOUN iajs-1066 30 21 atome atome NOUN iajs-1066 30 22 ; ; PUNCT iajs-1066 30 23 singlet singlet NOUN iajs-1066 30 24 at at ADP iajs-1066 30 25 2.50 2.50 NUM iajs-1066 30 26 ppm ppm NOUN iajs-1066 30 27 due due ADJ iajs-1066 30 28 to to ADP iajs-1066 30 29 dmso dmso ADJ iajs-1066 30 30 solvent solvent NOUN iajs-1066 30 31 ; ; PUNCT iajs-1066 30 32 singlet singlet ADJ iajs-1066 30 33 signal signal NOUN iajs-1066 30 34 at at ADP iajs-1066 30 35 3.385 3.385 NUM iajs-1066 30 36 for for ADP iajs-1066 30 37 1h 1h NUM iajs-1066 30 38 hydroxylic hydroxylic ADJ iajs-1066 30 39 proton proton NOUN iajs-1066 30 40 , , PUNCT iajs-1066 30 41 the the DET iajs-1066 30 42 remaining remain VERB iajs-1066 30 43 [ [ X iajs-1066 30 44 bands band NOUN iajs-1066 30 45 multiplied multiply VERB iajs-1066 30 46 ] ] PUNCT iajs-1066 30 47 from from ADP iajs-1066 30 48 5.6 5.6 NUM iajs-1066 30 49 to to PART iajs-1066 30 50 8.2 8.2 NUM iajs-1066 30 51 ppm ppm NOUN iajs-1066 30 52 belong belong VERB iajs-1066 30 53 to to ADP iajs-1066 30 54 the the DET iajs-1066 30 55 three three NUM iajs-1066 30 56 aromatic aromatic ADJ iajs-1066 30 57 ring ring NOUN iajs-1066 30 58 protons proton NOUN iajs-1066 30 59 that that PRON iajs-1066 30 60 overlap overlap VERB iajs-1066 30 61 with with ADP iajs-1066 30 62 each each DET iajs-1066 30 63 other other ADJ iajs-1066 30 64 [ [ X iajs-1066 30 65 10 10 NUM iajs-1066 30 66 ] ] PUNCT iajs-1066 30 67 . . PUNCT iajs-1066 30 68     SPACE iajs-1066 31 1 the the DET iajs-1066 31 2 13c 13c NUM iajs-1066 31 3 nmr nmr NOUN iajs-1066 31 4 spectrum spectrum NOUN iajs-1066 31 5 : : PUNCT iajs-1066 31 6 in in ADP iajs-1066 31 7 the the DET iajs-1066 31 8 spectrum spectrum NOUN iajs-1066 31 9 the the DET iajs-1066 31 10 40.8 40.8 NUM iajs-1066 31 11 ppm ppm NOUN iajs-1066 31 12 signal signal NOUN iajs-1066 31 13 is be AUX iajs-1066 31 14 due due ADJ iajs-1066 31 15 to to ADP iajs-1066 31 16 the the DET iajs-1066 31 17 solvent solvent NOUN iajs-1066 31 18 c c NOUN iajs-1066 31 19 atoms atom NOUN iajs-1066 31 20 of of ADP iajs-1066 31 21 dmso dmso NOUN iajs-1066 31 22 ; ; PUNCT iajs-1066 31 23 73.2 73.2 NUM iajs-1066 31 24 attributed attribute VERB iajs-1066 31 25 to to ADP iajs-1066 31 26 c c NOUN iajs-1066 31 27 - - PUNCT iajs-1066 31 28 ohmoiety ohmoiety NOUN iajs-1066 31 29 ; ; PUNCT iajs-1066 31 30 the the DET iajs-1066 31 31 aromatic aromatic ADJ iajs-1066 31 32 carbon carbon NOUN iajs-1066 31 33 peaks peak NOUN iajs-1066 31 34 appeared appear VERB iajs-1066 31 35 in in ADP iajs-1066 31 36 the the DET iajs-1066 31 37 range range NOUN iajs-1066 31 38 from from ADP iajs-1066 31 39 124.43 124.43 NUM iajs-1066 31 40 to to ADP iajs-1066 31 41 149.88 149.88 NUM iajs-1066 31 42 ppm ppm NOUN iajs-1066 31 43 , , PUNCT iajs-1066 31 44 finely finely ADV iajs-1066 31 45 the the DET iajs-1066 31 46 two two NUM iajs-1066 31 47 peaks peak NOUN iajs-1066 31 48 above above ADP iajs-1066 31 49 160 160 NUM iajs-1066 31 50 ppm ppm NOUN iajs-1066 31 51 , , PUNCT iajs-1066 31 52 returned return VERB iajs-1066 31 53 to to ADP iajs-1066 31 54 the the DET iajs-1066 31 55 two two NUM iajs-1066 31 56 sp2 sp2 NOUN iajs-1066 31 57 carbone carbone NOUN iajs-1066 31 58 atom atom NOUN iajs-1066 31 59 that that PRON iajs-1066 31 60 linked link VERB iajs-1066 31 61 with with ADP iajs-1066 31 62 nitrogen nitrogen NOUN iajs-1066 31 63 , , PUNCT iajs-1066 31 64 the the DET iajs-1066 31 65 firs fir NOUN iajs-1066 31 66 are be AUX iajs-1066 31 67 for for ADP iajs-1066 31 68 schiff schiff NOUN iajs-1066 31 69 base base NOUN iajs-1066 31 70 band band NOUN iajs-1066 31 71 and and CCONJ iajs-1066 31 72 the the DET iajs-1066 31 73 other other ADJ iajs-1066 31 74 one one NUM iajs-1066 31 75 returns return NOUN iajs-1066 31 76 to to ADP iajs-1066 31 77 α α NOUN iajs-1066 31 78 – – PUNCT iajs-1066 31 79 imine imine ADJ iajs-1066 31 80 pyridine pyridine NOUN iajs-1066 31 81 [ [ X iajs-1066 31 82 12 12 NUM iajs-1066 31 83 ] ] PUNCT iajs-1066 31 84 . . 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PROPN iajs-1066 35 1 for for ADP iajs-1066 35 2 pure pure ADJ iajs-1066 35 3 & & CCONJ iajs-1066 35 4 appl appl PROPN iajs-1066 35 5 . . PUNCT iajs-1066 36 1 sci sci PROPN iajs-1066 36 2 . . PUNCT iajs-1066 36 3 vol vol NOUN iajs-1066 36 4 . . PROPN iajs-1066 36 5 30 30 NUM iajs-1066 36 6 ( ( PUNCT iajs-1066 36 7 1 1 NUM iajs-1066 36 8 ) ) PUNCT iajs-1066 36 9 2017 2017 NUM iajs-1066 36 10 the the DET iajs-1066 36 11 ir ir PROPN iajs-1066 36 12 spectra spectra NOUN iajs-1066 36 13 for for ADP iajs-1066 36 14 the the DET iajs-1066 36 15 ligand ligand NOUN iajs-1066 36 16 and and CCONJ iajs-1066 36 17 its its PRON iajs-1066 36 18 complexes complex NOUN iajs-1066 36 19 the the DET iajs-1066 36 20 important important ADJ iajs-1066 36 21 ir ir PROPN iajs-1066 36 22 absorption absorption NOUN iajs-1066 36 23 bands band NOUN iajs-1066 36 24 for for ADP iajs-1066 36 25 the the DET iajs-1066 36 26 synthesized synthesize VERB iajs-1066 36 27 schiff schiff NOUN iajs-1066 36 28 bases basis NOUN iajs-1066 36 29 are be AUX iajs-1066 36 30 listed list VERB iajs-1066 36 31 . . PUNCT iajs-1066 37 1 in in ADP iajs-1066 37 2 the the DET iajs-1066 37 3 l l NOUN iajs-1066 37 4 , , PUNCT iajs-1066 37 5 the the DET iajs-1066 37 6 band band NOUN iajs-1066 37 7 shows show VERB iajs-1066 37 8 at at ADP iajs-1066 37 9 1604 1604 NUM iajs-1066 37 10 cm-1that cm-1that X iajs-1066 37 11 it it PRON iajs-1066 37 12 was be AUX iajs-1066 37 13 assigned assign VERB iajs-1066 37 14 to to ADP iajs-1066 37 15 the the DET iajs-1066 37 16 v(c v(c NOUN iajs-1066 37 17 = = SYM iajs-1066 37 18 n n CCONJ iajs-1066 37 19 ) ) PUNCT iajs-1066 37 20 stretching stretch VERB iajs-1066 37 21 mode mode NOUN iajs-1066 37 22 . . PUNCT iajs-1066 38 1 in in ADP iajs-1066 38 2 complexes complex NOUN iajs-1066 38 3 this this DET iajs-1066 38 4 band band NOUN iajs-1066 38 5 was be AUX iajs-1066 38 6 shifted shift VERB iajs-1066 38 7 to to ADP iajs-1066 38 8 lower low ADJ iajs-1066 38 9 regions region NOUN iajs-1066 38 10 , , PUNCT iajs-1066 38 11 1598cm-1 1598cm-1 NUM iajs-1066 38 12 , , PUNCT iajs-1066 38 13 1593cm-1,1591cm-11595cm-1 1593cm-1,1591cm-11595cm-1 NUM iajs-1066 38 14 , , PUNCT iajs-1066 38 15 and and CCONJ iajs-1066 38 16 1596cm-1 1596cm-1 NUM iajs-1066 38 17 for for ADP iajs-1066 38 18 mn(ii),co(ii),ni(ii),cu(ii mn(ii),co(ii),ni(ii),cu(ii NUM iajs-1066 38 19 ) ) PUNCT iajs-1066 38 20 and and CCONJ iajs-1066 38 21 hg(ii)complexes hg(ii)complexe NOUN iajs-1066 38 22 respectively respectively ADV iajs-1066 38 23 , , PUNCT iajs-1066 38 24 suggesting suggest VERB iajs-1066 38 25 the the DET iajs-1066 38 26 coordination coordination NOUN iajs-1066 38 27 of of ADP iajs-1066 38 28 azomethine azomethine PROPN iajs-1066 38 29 nitrogen nitrogen NOUN iajs-1066 38 30 to to ADP iajs-1066 38 31 metal metal VERB iajs-1066 38 32 atom atom NOUN iajs-1066 38 33 in in ADP iajs-1066 38 34 complexation complexation NOUN iajs-1066 38 35 [ [ X iajs-1066 38 36 13].the 13].the PRON iajs-1066 38 37 ( ( PUNCT iajs-1066 38 38 ir ir NOUN iajs-1066 38 39 ) ) PUNCT iajs-1066 38 40 spectra spectra NOUN iajs-1066 38 41 of of ADP iajs-1066 38 42 the the DET iajs-1066 38 43 complexes complex NOUN iajs-1066 38 44 showed show VERB iajs-1066 38 45 band band NOUN iajs-1066 38 46 at at ADP iajs-1066 38 47 the the DET iajs-1066 38 48 range(1576 range(1576 NOUN iajs-1066 38 49 - - PUNCT iajs-1066 38 50 1581 1581 NUM iajs-1066 38 51 ) ) PUNCT iajs-1066 38 52 cm-1were cm-1were NOUN iajs-1066 38 53 assigned assign VERB iajs-1066 38 54 to to ADP iajs-1066 38 55 υ(c υ(c PROPN iajs-1066 38 56 = = SYM iajs-1066 38 57 n n CCONJ iajs-1066 38 58 ) ) PUNCT iajs-1066 38 59 groups group NOUN iajs-1066 38 60 for for ADP iajs-1066 38 61 the the DET iajs-1066 38 62 pyridine pyridine NOUN iajs-1066 38 63 ring ring NOUN iajs-1066 38 64 in in ADP iajs-1066 38 65 2 2 NUM iajs-1066 38 66 - - PUNCT iajs-1066 38 67 amino amino NOUN iajs-1066 38 68 pyridine pyridine NOUN iajs-1066 38 69 , , PUNCT iajs-1066 38 70 which which PRON iajs-1066 38 71 shifted shift VERB iajs-1066 38 72 the the DET iajs-1066 38 73 frequency frequency NOUN iajs-1066 38 74 to to ADP iajs-1066 38 75 a a DET iajs-1066 38 76 lower low ADJ iajs-1066 38 77 in in ADP iajs-1066 38 78 comparison comparison NOUN iajs-1066 38 79 with with ADP iajs-1066 38 80 that that PRON iajs-1066 38 81 of of ADP iajs-1066 38 82 schiff schiff NOUN iajs-1066 38 83 base base NOUN iajs-1066 38 84 was be AUX iajs-1066 38 85 showed show VERB iajs-1066 38 86 at at ADP iajs-1066 38 87 ( ( PUNCT iajs-1066 38 88 1588)cm-1,when 1588)cm-1,when NUM iajs-1066 38 89 coordination coordination NOUN iajs-1066 38 90 with with ADP iajs-1066 38 91 the the DET iajs-1066 38 92 metal metal NOUN iajs-1066 38 93 ion ion NOUN iajs-1066 38 94 referring refer VERB iajs-1066 38 95 to to ADP iajs-1066 38 96 share share NOUN iajs-1066 38 97 of of ADP iajs-1066 38 98 two two NUM iajs-1066 38 99 nitrogen'sv(-c nitrogen'sv(-c NOUN iajs-1066 38 100 = = NUM iajs-1066 38 101 n).the n).the ADJ iajs-1066 38 102 bands band NOUN iajs-1066 38 103 show show VERB iajs-1066 38 104 at at ADP iajs-1066 38 105 1531 1531 NUM iajs-1066 38 106 cm-1 cm-1 NOUN iajs-1066 38 107 and and CCONJ iajs-1066 38 108 1498 1498 NUM iajs-1066 38 109 cm-1were cm-1were ADV iajs-1066 38 110 assigned assign VERB iajs-1066 38 111 to to ADP iajs-1066 38 112 the the DET iajs-1066 38 113 v(c v(c PROPN iajs-1066 38 114 = = SYM iajs-1066 38 115 c c NOUN iajs-1066 38 116 ) ) PUNCT iajs-1066 38 117 stretching stretch VERB iajs-1066 38 118 mode mode NOUN iajs-1066 38 119 in in ADP iajs-1066 38 120 the the DET iajs-1066 38 121 ligand.these ligand.these PROPN iajs-1066 38 122 bands band NOUN iajs-1066 38 123 prove prove VERB iajs-1066 38 124 the the DET iajs-1066 38 125 presence presence NOUN iajs-1066 38 126 of of ADP iajs-1066 38 127 benzene benzene NOUN iajs-1066 38 128 . . PUNCT iajs-1066 39 1 ir ir PROPN iajs-1066 39 2 spectrum spectrum NOUN iajs-1066 39 3 of of ADP iajs-1066 39 4 the the DET iajs-1066 39 5 ligand ligand NOUN iajs-1066 39 6 showed show VERB iajs-1066 39 7 a a DET iajs-1066 39 8 board board NOUN iajs-1066 39 9 band band NOUN iajs-1066 39 10 at at ADP iajs-1066 39 11 3344 3344 NUM iajs-1066 39 12 cm-1 cm-1 NOUN iajs-1066 39 13 due due ADP iajs-1066 39 14 to to ADP iajs-1066 39 15 v v NOUN iajs-1066 39 16 ( ( PUNCT iajs-1066 39 17 oh oh INTJ iajs-1066 39 18 ) ) PUNCT iajs-1066 39 19 stretching stretch VERB iajs-1066 39 20 mode mode NOUN iajs-1066 39 21 in in ADP iajs-1066 39 22 the the DET iajs-1066 39 23 ligand ligand NOUN iajs-1066 39 24 [ [ X iajs-1066 39 25 14 14 NUM iajs-1066 39 26 ] ] PUNCT iajs-1066 39 27 . . PUNCT iajs-1066 40 1 this this DET iajs-1066 40 2 band band NOUN iajs-1066 40 3 was be AUX iajs-1066 40 4 absent absent ADJ iajs-1066 40 5 in in ADP iajs-1066 40 6 the the DET iajs-1066 40 7 spectra spectra NOUN iajs-1066 40 8 of of ADP iajs-1066 40 9 complexes complex NOUN iajs-1066 40 10 , , PUNCT iajs-1066 40 11 they they PRON iajs-1066 40 12 indicate indicate VERB iajs-1066 40 13 the the DET iajs-1066 40 14 disappearing disappearing NOUN iajs-1066 40 15 of of ADP iajs-1066 40 16 the the DET iajs-1066 40 17 alcoholic alcoholic ADJ iajs-1066 40 18 proton proton NOUN iajs-1066 40 19 on on ADP iajs-1066 40 20 complexation complexation NOUN iajs-1066 40 21 and and CCONJ iajs-1066 40 22 involvement involvement NOUN iajs-1066 40 23 of of ADP iajs-1066 40 24 alcoholic alcoholic ADJ iajs-1066 40 25 anionic anionic ADJ iajs-1066 40 26 oxygen oxygen NOUN iajs-1066 40 27 in in ADP iajs-1066 40 28 coordination coordination NOUN iajs-1066 40 29 [ [ X iajs-1066 40 30 15 15 NUM iajs-1066 40 31 ] ] PUNCT iajs-1066 40 32 . . PUNCT iajs-1066 41 1 moreover moreover ADV iajs-1066 41 2 , , PUNCT iajs-1066 41 3 the the DET iajs-1066 41 4 strong strong ADJ iajs-1066 41 5 band band NOUN iajs-1066 41 6 at1187 at1187 VERB iajs-1066 41 7 cm−1is cm−1is NUM iajs-1066 41 8 due due ADJ iajs-1066 41 9 to to ADP iajs-1066 41 10 v(c v(c ADJ iajs-1066 41 11 - - PUNCT iajs-1066 41 12 o o NOUN iajs-1066 41 13 ) ) PUNCT iajs-1066 41 14 ( ( PUNCT iajs-1066 41 15 alcoholic alcoholic NOUN iajs-1066 41 16 ) ) PUNCT iajs-1066 41 17 in in ADP iajs-1066 41 18 the the DET iajs-1066 41 19 ligand ligand NOUN iajs-1066 41 20 . . PUNCT iajs-1066 42 1 amedium amedium NOUN iajs-1066 42 2 band band NOUN iajs-1066 42 3 corresponding correspond VERB iajs-1066 42 4 to to ADP iajs-1066 42 5 pyridine pyridine ADJ iajs-1066 42 6 nitrogen nitrogen NOUN iajs-1066 42 7 v(c v(c PROPN iajs-1066 42 8 - - PUNCT iajs-1066 42 9 n n CCONJ iajs-1066 42 10 ) ) PUNCT iajs-1066 42 11 was be AUX iajs-1066 42 12 observed observe VERB iajs-1066 42 13 at at ADP iajs-1066 42 14 1253 1253 NUM iajs-1066 42 15 cm−1[16,17].the cm−1[16,17].the ADJ iajs-1066 42 16 bands band NOUN iajs-1066 42 17 arising arise VERB iajs-1066 42 18 due due ADP iajs-1066 42 19 to to ADP iajs-1066 42 20 vibration vibration NOUN iajs-1066 42 21 v(c v(c PROPN iajs-1066 42 22 - - PUNCT iajs-1066 42 23 o o NOUN iajs-1066 42 24 ) ) PUNCT iajs-1066 42 25 mode mode NOUN iajs-1066 42 26 at at ADP iajs-1066 42 27 1187 1187 NUM iajs-1066 42 28 cm−1and cm−1and ADP iajs-1066 42 29 the the DET iajs-1066 42 30 v(c v(c PROPN iajs-1066 42 31 - - PUNCT iajs-1066 42 32 n n CCONJ iajs-1066 42 33 ) ) PUNCT iajs-1066 42 34 frequency frequency NOUN iajs-1066 42 35 in in ADP iajs-1066 42 36 the the DET iajs-1066 42 37 free free ADJ iajs-1066 42 38 ligand ligand NOUN iajs-1066 42 39 at at ADP iajs-1066 42 40 1253 1253 NUM iajs-1066 42 41 cm−1were cm−1were ADV iajs-1066 42 42 observed observe VERB iajs-1066 42 43 to to PART iajs-1066 42 44 be be AUX iajs-1066 42 45 shifted shift VERB iajs-1066 42 46 to to ADP iajs-1066 42 47 higher high ADJ iajs-1066 42 48 or or CCONJ iajs-1066 42 49 lower low ADJ iajs-1066 42 50 frequencies frequency NOUN iajs-1066 42 51 , , PUNCT iajs-1066 42 52 at at ADP iajs-1066 42 53 1240–1257 1240–1257 NUM iajs-1066 42 54 cm-1 cm-1 NOUN iajs-1066 42 55 and and CCONJ iajs-1066 42 56 1183–1198 1183–1198 NUM iajs-1066 42 57 cm-1.alsothe cm-1.alsothe DET iajs-1066 42 58 bands band NOUN iajs-1066 42 59 show show VERB iajs-1066 42 60 at at ADP iajs-1066 42 61 ( ( PUNCT iajs-1066 42 62 582 582 NUM iajs-1066 42 63 - - NUM iajs-1066 42 64 547 547 NUM iajs-1066 42 65 ) ) PUNCT iajs-1066 42 66 , , PUNCT iajs-1066 42 67 ( ( PUNCT iajs-1066 42 68 460 460 NUM iajs-1066 42 69 - - NUM iajs-1066 42 70 482 482 NUM iajs-1066 42 71 ) ) PUNCT iajs-1066 42 72 due due ADP iajs-1066 42 73 to to ADP iajs-1066 42 74 v(m v(m NOUN iajs-1066 42 75 - - PUNCT iajs-1066 42 76 o o NOUN iajs-1066 42 77 ) ) PUNCT iajs-1066 42 78 and and CCONJ iajs-1066 42 79 v(m v(m NOUN iajs-1066 42 80 - - PUNCT iajs-1066 42 81 n n CCONJ iajs-1066 42 82 ) ) PUNCT iajs-1066 42 83 , , PUNCT iajs-1066 42 84 respectively.in respectively.in PRON iajs-1066 42 85 the the DET iajs-1066 42 86 metal metal NOUN iajs-1066 42 87 complexes complex NOUN iajs-1066 42 88 indicating indicate VERB iajs-1066 42 89 the the DET iajs-1066 42 90 involvement involvement NOUN iajs-1066 42 91 of of ADP iajs-1066 42 92 nitrogen nitrogen NOUN iajs-1066 42 93 of of ADP iajs-1066 42 94 pyridine pyridine NOUN iajs-1066 42 95 ring ring NOUN iajs-1066 42 96 and and CCONJ iajs-1066 42 97 oxygen oxygen NOUN iajs-1066 42 98 of of ADP iajs-1066 42 99 the the DET iajs-1066 42 100 alcoholic alcoholic ADJ iajs-1066 42 101 group group NOUN iajs-1066 42 102 in in ADP iajs-1066 42 103 the the DET iajs-1066 42 104 complex complex ADJ iajs-1066 42 105 formation formation NOUN iajs-1066 43 1 [ [ X iajs-1066 43 2 18 18 NUM iajs-1066 43 3 - - SYM iajs-1066 43 4 19 19 NUM iajs-1066 43 5 ] ] PUNCT iajs-1066 43 6 . . PUNCT iajs-1066 43 7     SPACE iajs-1066 44 1 the the DET iajs-1066 44 2 uvspectral uvspectral ADJ iajs-1066 44 3 studies study NOUN iajs-1066 44 4     SPACE iajs-1066 44 5 the the DET iajs-1066 44 6 cu(ii cu(ii PROPN iajs-1066 44 7 ) ) PUNCT iajs-1066 44 8 , , PUNCT iajs-1066 44 9 co(ii co(ii PROPN iajs-1066 44 10 ) ) PUNCT iajs-1066 44 11 , , PUNCT iajs-1066 44 12 ni(ii ni(ii PROPN iajs-1066 44 13 ) ) PUNCT iajs-1066 44 14 , , PUNCT iajs-1066 44 15 mn(ii mn(ii PROPN iajs-1066 44 16 ) ) PUNCT iajs-1066 44 17 and and CCONJ iajs-1066 44 18 hg(ii hg(ii PROPN iajs-1066 44 19 ) ) PUNCT iajs-1066 44 20 complexes complex NOUN iajs-1066 44 21 of of ADP iajs-1066 44 22 ligand ligand ADJ iajs-1066 44 23 l l PROPN iajs-1066 44 24 were be AUX iajs-1066 44 25 subjected subject VERB iajs-1066 44 26 to to ADP iajs-1066 44 27 their their PRON iajs-1066 44 28 uv uv NOUN iajs-1066 44 29 - - PUNCT iajs-1066 44 30 visible visible ADJ iajs-1066 44 31 spectral spectral ADJ iajs-1066 44 32 studies study NOUN iajs-1066 44 33 at at ADP iajs-1066 44 34 room room NOUN iajs-1066 44 35 temperature temperature NOUN iajs-1066 44 36 in in ADP iajs-1066 44 37 the the DET iajs-1066 44 38 range range NOUN iajs-1066 44 39 of of ADP iajs-1066 44 40 200–1100 200–1100 NUM iajs-1066 44 41 nm nm NOUN iajs-1066 44 42 by by ADP iajs-1066 44 43 using use VERB iajs-1066 44 44 dmf dmf PROPN iajs-1066 44 45 as as ADP iajs-1066 44 46 a a DET iajs-1066 44 47 solvent solvent NOUN iajs-1066 44 48 , , PUNCT iajs-1066 44 49 and and CCONJ iajs-1066 44 50 the the DET iajs-1066 44 51 data datum NOUN iajs-1066 44 52 of of ADP iajs-1066 44 53 the the DET iajs-1066 44 54 ligand ligand NOUN iajs-1066 44 55 ( ( PUNCT iajs-1066 44 56 l l NOUN iajs-1066 44 57 ) ) PUNCT iajs-1066 44 58 were be AUX iajs-1066 44 59 recording recording NOUN iajs-1066 44 60 table table NOUN iajs-1066 44 61 ( ( PUNCT iajs-1066 44 62 5 5 NUM iajs-1066 44 63 ) ) PUNCT iajs-1066 44 64 . . PUNCT iajs-1066 45 1 the the DET iajs-1066 45 2 u.v u.v PROPN iajs-1066 45 3 - - PUNCT iajs-1066 45 4 vis vis X iajs-1066 45 5 spectrum spectrum NOUN iajs-1066 45 6 of of ADP iajs-1066 45 7 schiff schiff NOUN iajs-1066 45 8 base base NOUN iajs-1066 45 9 , , PUNCT iajs-1066 45 10 fig.(3 fig.(3 NOUN iajs-1066 45 11 ) ) PUNCT iajs-1066 45 12 in in ADP iajs-1066 45 13 table table NOUN iajs-1066 45 14 ( ( PUNCT iajs-1066 45 15 5)displayed 5)displayed NUM iajs-1066 45 16 two two NUM iajs-1066 45 17 absorptions absorption NOUN iajs-1066 45 18 . . PUNCT iajs-1066 46 1 the the DET iajs-1066 46 2 first first ADJ iajs-1066 46 3 absorption absorption NOUN iajs-1066 46 4 at at ADP iajs-1066 46 5 ( ( PUNCT iajs-1066 46 6 280)nm 280)nm NUM iajs-1066 46 7 ( ( PUNCT iajs-1066 46 8 35714cm-1 35714cm-1 NOUN iajs-1066 46 9 ) ) PUNCT iajs-1066 46 10 may may AUX iajs-1066 46 11 be be AUX iajs-1066 46 12 assigned assign VERB iajs-1066 46 13 to to ADP iajs-1066 46 14 π π PROPN iajs-1066 46 15 – – PUNCT iajs-1066 46 16 σ σ PROPN iajs-1066 46 17 * * PROPN iajs-1066 46 18 transition transition NOUN iajs-1066 46 19 . . PUNCT iajs-1066 47 1 the the DET iajs-1066 47 2 second second ADJ iajs-1066 47 3 peak peak NOUN iajs-1066 47 4 at at ADP iajs-1066 47 5 ( ( PUNCT iajs-1066 47 6 312 312 NUM iajs-1066 47 7 ) ) PUNCT iajs-1066 47 8 nm nm NOUN iajs-1066 47 9 ( ( PUNCT iajs-1066 47 10 32051cm-1 32051cm-1 NUM iajs-1066 47 11 ) ) PUNCT iajs-1066 47 12 was be AUX iajs-1066 47 13 attributed attribute VERB iajs-1066 47 14 to to ADP iajs-1066 47 15 n n CCONJ iajs-1066 47 16 – – PUNCT iajs-1066 47 17 π π NOUN iajs-1066 47 18 * * ADJ iajs-1066 47 19 electronic electronic ADJ iajs-1066 47 20 transition transition NOUN iajs-1066 48 1 [ [ X iajs-1066 48 2 20 20 NUM iajs-1066 48 3 ] ] PUNCT iajs-1066 48 4 . . PUNCT iajs-1066 49 1 the the DET iajs-1066 49 2 electronic electronic ADJ iajs-1066 49 3 spectrum spectrum NOUN iajs-1066 49 4 of of ADP iajs-1066 49 5 the the DET iajs-1066 49 6 co co X iajs-1066 49 7 ( ( PUNCT iajs-1066 49 8 ii)complex ii)complex PROPN iajs-1066 49 9 showed show VERB iajs-1066 49 10 two two NUM iajs-1066 49 11 peaks peak NOUN iajs-1066 49 12 , , PUNCT iajs-1066 49 13 the the DET iajs-1066 49 14 first first ADJ iajs-1066 49 15 peak peak NOUN iajs-1066 49 16 ( ( PUNCT iajs-1066 49 17 331)nm 331)nm NUM iajs-1066 49 18 ( ( PUNCT iajs-1066 49 19 30211cm-1)which 30211cm-1)which ADV iajs-1066 49 20 was be AUX iajs-1066 49 21 assigned assign VERB iajs-1066 49 22 to to PART iajs-1066 49 23 c.t c.t VERB iajs-1066 49 24 transition.the transition.the DET iajs-1066 49 25 second second ADJ iajs-1066 49 26 peak peak NOUN iajs-1066 49 27 at at ADP iajs-1066 49 28 ( ( PUNCT iajs-1066 49 29 611 611 NUM iajs-1066 49 30 ) ) PUNCT iajs-1066 49 31 nm nm NOUN iajs-1066 49 32 ( ( PUNCT iajs-1066 49 33 16366 16366 NUM iajs-1066 49 34 ) ) PUNCT iajs-1066 49 35 cm1 cm1 PROPN iajs-1066 49 36 was be AUX iajs-1066 49 37 allocated allocate VERB iajs-1066 49 38 to(d to(d NOUN iajs-1066 49 39 - - SYM iajs-1066 49 40 d d NOUN iajs-1066 49 41 ) ) PUNCT iajs-1066 49 42 electronic electronic ADJ iajs-1066 49 43 transition transition NOUN iajs-1066 49 44 type4a2 type4a2 INTJ iajs-1066 50 1 ( ( PUNCT iajs-1066 50 2 f f X iajs-1066 50 3 ) ) PUNCT iajs-1066 50 4 → → SYM iajs-1066 50 5 4t1 4t1 NUM iajs-1066 50 6 ( ( PUNCT iajs-1066 50 7 p).(5.71 p).(5.71 NOUN iajs-1066 50 8 ) ) PUNCT iajs-1066 50 9 b.m b.m PROPN iajs-1066 50 10 . . PROPN iajs-1066 50 11 is be AUX iajs-1066 50 12 a a DET iajs-1066 50 13 magnetic magnetic ADJ iajs-1066 50 14 sensibility sensibility NOUN iajs-1066 50 15 of of ADP iajs-1066 50 16 this this DET iajs-1066 50 17 complex complex NOUN iajs-1066 50 18 . . PUNCT iajs-1066 51 1 [ [ X iajs-1066 51 2 21 21 NUM iajs-1066 51 3 ] ] X iajs-1066 51 4 it it PRON iajs-1066 51 5 has have AUX iajs-1066 51 6 been be AUX iajs-1066 51 7 a a DET iajs-1066 51 8 tetrahedral tetrahedral ADJ iajs-1066 51 9 environment environment NOUN iajs-1066 51 10 [ [ X iajs-1066 51 11 22 22 NUM iajs-1066 51 12 ] ] PUNCT iajs-1066 51 13 . . PUNCT iajs-1066 52 1 the the DET iajs-1066 52 2 u.v u.v PROPN iajs-1066 52 3 - - PUNCT iajs-1066 52 4 vis vis X iajs-1066 52 5 spectrum spectrum NOUN iajs-1066 52 6 of of ADP iajs-1066 52 7 the the DET iajs-1066 52 8 ni ni PROPN iajs-1066 52 9 ( ( PUNCT iajs-1066 52 10 ii)complex ii)complex PROPN iajs-1066 52 11 displayed display VERB iajs-1066 52 12 two two NUM iajs-1066 52 13 peaks peak NOUN iajs-1066 52 14 , , PUNCT iajs-1066 52 15 the the DET iajs-1066 52 16 first first ADJ iajs-1066 52 17 peak peak NOUN iajs-1066 52 18 ( ( PUNCT iajs-1066 52 19 332 332 NUM iajs-1066 52 20 ) ) PUNCT iajs-1066 52 21 nm nm NOUN iajs-1066 52 22 ( ( PUNCT iajs-1066 52 23 30120cm-1 30120cm-1 NUM iajs-1066 52 24 ) ) PUNCT iajs-1066 52 25 which which PRON iajs-1066 52 26 was be AUX iajs-1066 52 27 assigned assign VERB iajs-1066 52 28 to to ADP iajs-1066 52 29 c c NOUN iajs-1066 52 30 ttransition.the ttransition.the DET iajs-1066 52 31 second second ADJ iajs-1066 52 32 peak peak NOUN iajs-1066 52 33 at at ADP iajs-1066 52 34 ( ( PUNCT iajs-1066 52 35 770 770 NUM iajs-1066 52 36 ) ) PUNCT iajs-1066 52 37 nm nm NOUN iajs-1066 52 38 ( ( PUNCT iajs-1066 52 39 12987 12987 NUM iajs-1066 52 40 cm cm NUM iajs-1066 52 41 – – PUNCT iajs-1066 52 42 1)was 1)was NUM iajs-1066 52 43 allocated allocate VERB iajs-1066 52 44 to(d to(d NOUN iajs-1066 52 45 - - SYM iajs-1066 52 46 d d NOUN iajs-1066 52 47 ) ) PUNCT iajs-1066 52 48 electronic electronic ADJ iajs-1066 52 49 transition transition NOUN iajs-1066 52 50 type1a1g(f)→ type1a1g(f)→ PROPN iajs-1066 52 51 2eg 2eg PROPN iajs-1066 52 52 .it .it PUNCT iajs-1066 52 53 has have AUX iajs-1066 52 54 been be AUX iajs-1066 52 55 asquare asquare VERB iajs-1066 52 56 planar planar ADJ iajs-1066 52 57 configuration configuration NOUN iajs-1066 52 58 . . PUNCT iajs-1066 53 1 diamagnetic diamagnetic ADJ iajs-1066 53 2 is be AUX iajs-1066 53 3 amagnetic amagnetic ADJ iajs-1066 53 4 sensibility sensibility NOUN iajs-1066 53 5 of of ADP iajs-1066 53 6 this this DET iajs-1066 53 7 complex[23 complex[23 NOUN iajs-1066 53 8 ] ] PUNCT iajs-1066 53 9 . . PUNCT iajs-1066 54 1 the the DET iajs-1066 54 2 u.v u.v PROPN iajs-1066 54 3 - - PUNCT iajs-1066 54 4 vis vis X iajs-1066 54 5 spectrum spectrum NOUN iajs-1066 54 6 of of ADP iajs-1066 54 7 the the DET iajs-1066 54 8 copper copper NOUN iajs-1066 54 9 ( ( PUNCT iajs-1066 54 10 ii)complex ii)complex PROPN iajs-1066 54 11 showed show VERB iajs-1066 54 12 two two NUM iajs-1066 54 13 peaks peak NOUN iajs-1066 54 14 , , PUNCT iajs-1066 54 15 the the DET iajs-1066 54 16 first first ADJ iajs-1066 54 17 peak(327)nm peak(327)nm NOUN iajs-1066 54 18 ( ( PUNCT iajs-1066 54 19 30581cm-1)which 30581cm-1)which NUM iajs-1066 54 20 was be AUX iajs-1066 54 21 assigned assign VERB iajs-1066 54 22 to to ADP iajs-1066 54 23 c.t c.t PROPN iajs-1066 54 24 . . PUNCT iajs-1066 55 1 transition.the transition.the DET iajs-1066 55 2 second second ADJ iajs-1066 55 3 peak peak NOUN iajs-1066 55 4 at(543)nm(18416 at(543)nm(18416 ADP iajs-1066 55 5 cm cm NUM iajs-1066 55 6 – – PUNCT iajs-1066 55 7 1)was 1)was NUM iajs-1066 55 8 referred refer VERB iajs-1066 55 9 to to ADP iajs-1066 55 10 ( ( PUNCT iajs-1066 55 11 d d NOUN iajs-1066 55 12 - - PUNCT iajs-1066 55 13 d d NOUN iajs-1066 55 14 ) ) PUNCT iajs-1066 55 15 transition transition NOUN iajs-1066 55 16 type1b1g→ type1b1g→ NOUN iajs-1066 55 17 2a1 2a1 NOUN iajs-1066 55 18 g g NOUN iajs-1066 55 19 . . PUNCT iajs-1066 56 1 1.76b.m 1.76b.m NUM iajs-1066 56 2 is be AUX iajs-1066 56 3 a a DET iajs-1066 56 4 magnetic magnetic ADJ iajs-1066 56 5 moment.it moment.it NUM iajs-1066 56 6 has have AUX iajs-1066 56 7 been be AUX iajs-1066 56 8 asquare asquare VERB iajs-1066 56 9 planar planar ADJ iajs-1066 56 10 configuration configuration NOUN iajs-1066 56 11 of of ADP iajs-1066 56 12 this this DET iajs-1066 56 13 complex.[24 complex.[24 PROPN iajs-1066 56 14 ] ] PUNCT iajs-1066 56 15 . . PUNCT iajs-1066 57 1 while while SCONJ iajs-1066 57 2 the the DET iajs-1066 57 3 absorptions absorption NOUN iajs-1066 57 4 of of ADP iajs-1066 57 5 manganese manganese NOUN iajs-1066 57 6 ( ( PUNCT iajs-1066 57 7 ii)complex ii)complex PROPN iajs-1066 57 8 showed show VERB iajs-1066 57 9 three three NUM iajs-1066 57 10 bands band NOUN iajs-1066 57 11 , , PUNCT iajs-1066 57 12 the the DET iajs-1066 57 13 first first ADJ iajs-1066 57 14 bond bond NOUN iajs-1066 57 15 ( ( PUNCT iajs-1066 57 16 335)nm 335)nm NUM iajs-1066 57 17 ( ( PUNCT iajs-1066 57 18 29650cm-1)which 29650cm-1)which NUM iajs-1066 57 19 was be AUX iajs-1066 57 20 assigned assign VERB iajs-1066 57 21 to to ADP iajs-1066 57 22 c c NOUN iajs-1066 57 23 ttransition.the ttransition.the DET iajs-1066 57 24 second second ADJ iajs-1066 57 25 and and CCONJ iajs-1066 57 26 third third ADJ iajs-1066 57 27 bonds bond NOUN iajs-1066 57 28 at at ADP iajs-1066 57 29 453 453 NUM iajs-1066 57 30 nm nm NOUN iajs-1066 57 31 ( ( PUNCT iajs-1066 57 32 12903cm-1 12903cm-1 NOUN iajs-1066 57 33 ) ) PUNCT iajs-1066 57 34 and and CCONJ iajs-1066 57 35 586 586 NUM iajs-1066 57 36 nm nm ADJ iajs-1066 57 37 ( ( PUNCT iajs-1066 57 38 22075cm-1 22075cm-1 NOUN iajs-1066 57 39 ) ) PUNCT iajs-1066 57 40 which which PRON iajs-1066 57 41 have have AUX iajs-1066 57 42 been be AUX iajs-1066 57 43 assigned assign VERB iajs-1066 57 44 to6a1→ to6a1→ PROPN iajs-1066 57 45 4a1 4a1 PROPN iajs-1066 57 46 ( ( PUNCT iajs-1066 57 47 g g NOUN iajs-1066 57 48 ) ) PUNCT iajs-1066 57 49 and and CCONJ iajs-1066 57 50 6a1→ 6a1→ NUM iajs-1066 57 51 4e 4e NOUN iajs-1066 57 52 ( ( PUNCT iajs-1066 57 53 g g NOUN iajs-1066 57 54 ) ) PUNCT iajs-1066 57 55 transitions transition NOUN iajs-1066 57 56 respectively respectively ADV iajs-1066 57 57 . . PUNCT iajs-1066 58 1 5.75b.m 5.75b.m X iajs-1066 58 2 . . PUNCT iajs-1066 58 3 is be AUX iajs-1066 58 4 amagnetic amagnetic ADJ iajs-1066 58 5 sensibility sensibility NOUN iajs-1066 58 6 of of ADP iajs-1066 58 7 this this PRON iajs-1066 58 8 complex.it complex.it NUM iajs-1066 58 9 has have AUX iajs-1066 58 10 been be AUX iajs-1066 58 11 a a DET iajs-1066 58 12 tetrahedral tetrahedral ADJ iajs-1066 58 13 configuration configuration NOUN iajs-1066 58 14 [ [ X iajs-1066 58 15 25 25 NUM iajs-1066 58 16 ] ] PUNCT iajs-1066 58 17 . . PUNCT iajs-1066 59 1 chemistry chemistry NOUN iajs-1066 59 2 | | ADV iajs-1066 59 3 135 135 NUM iajs-1066 59 4 2017عام 2017عام NUM iajs-1066 59 5 ) ) PUNCT iajs-1066 59 6 1(العدد 1(العدد NUM iajs-1066 59 7 30المجلد 30المجلد NUM iajs-1066 59 8 مجلة مجلة VERB iajs-1066 59 9 إبن إبن NOUN iajs-1066 59 10 الھيثم الھيثم NOUN iajs-1066 59 11 للعلوم للعلوم NOUN iajs-1066 59 12 الصرفة الصرفة NOUN iajs-1066 59 13 والتطبيقية والتطبيقية VERB iajs-1066 59 14 ibn ibn PROPN iajs-1066 59 15 al al PROPN iajs-1066 59 16 - - PUNCT iajs-1066 59 17 haitham haitham PROPN iajs-1066 59 18 jour jour X iajs-1066 59 19 . . PROPN iajs-1066 60 1 for for ADP iajs-1066 60 2 pure pure ADJ iajs-1066 60 3 & & CCONJ iajs-1066 60 4 appl appl PROPN iajs-1066 60 5 . . PUNCT iajs-1066 61 1 sci sci PROPN iajs-1066 61 2 . . PUNCT iajs-1066 61 3 vol vol NOUN iajs-1066 61 4 . . PROPN iajs-1066 61 5 30 30 NUM iajs-1066 61 6 ( ( PUNCT iajs-1066 61 7 1 1 NUM iajs-1066 61 8 ) ) PUNCT iajs-1066 61 9 2017 2017 NUM iajs-1066 61 10 the the DET iajs-1066 61 11 complex complex ADJ iajs-1066 61 12 mercury mercury NOUN iajs-1066 61 13 ( ( PUNCT iajs-1066 61 14 ii ii NOUN iajs-1066 61 15 ) ) PUNCT iajs-1066 61 16 is be AUX iajs-1066 61 17 diamagnetic diamagnetic ADJ iajs-1066 61 18 giving give VERB iajs-1066 61 19 two two NUM iajs-1066 61 20 peaks peak NOUN iajs-1066 61 21 at at ADP iajs-1066 61 22 334 334 NUM iajs-1066 61 23 nm nm NOUN iajs-1066 61 24 ( ( PUNCT iajs-1066 61 25 29940cm-1 29940cm-1 NUM iajs-1066 61 26 ) ) PUNCT iajs-1066 61 27 and and CCONJ iajs-1066 61 28 410 410 NUM iajs-1066 61 29 nm nm NOUN iajs-1066 61 30 ( ( PUNCT iajs-1066 61 31 24390cm-1 24390cm-1 NOUN iajs-1066 61 32 ) ) PUNCT iajs-1066 61 33 were be AUX iajs-1066 61 34 allocated allocate VERB iajs-1066 61 35 to to ADP iajs-1066 61 36 c c PROPN iajs-1066 61 37 t t PROPN iajs-1066 61 38 transitions transition NOUN iajs-1066 61 39 . . PUNCT iajs-1066 62 1 the the DET iajs-1066 62 2 peaks peak NOUN iajs-1066 62 3 disappear disappear VERB iajs-1066 62 4 in in ADP iajs-1066 62 5 the the DET iajs-1066 62 6 visible visible ADJ iajs-1066 62 7 region region NOUN iajs-1066 62 8 . . PUNCT iajs-1066 63 1 it it PRON iajs-1066 63 2 has have AUX iajs-1066 63 3 been be AUX iajs-1066 63 4 a a DET iajs-1066 63 5 tetrahedral tetrahedral ADJ iajs-1066 63 6 configuration[26 configuration[26 NOUN iajs-1066 63 7 ] ] PUNCT iajs-1066 63 8 . . PUNCT iajs-1066 64 1 biological biological ADJ iajs-1066 64 2 activities activity NOUN iajs-1066 64 3 tridentate tridentate VERB iajs-1066 64 4 schiff schiff PROPN iajs-1066 64 5 base base PROPN iajs-1066 64 6 ligand ligand NOUN iajs-1066 64 7 derived derive VERB iajs-1066 64 8 by by ADP iajs-1066 64 9 the the DET iajs-1066 64 10 condensation2 condensation2 NOUN iajs-1066 64 11 - - PUNCT iajs-1066 64 12 amino amino NOUN iajs-1066 64 13 pyridine pyridine NOUN iajs-1066 64 14 with with ADP iajs-1066 64 15 benzoin benzoin NOUN iajs-1066 64 16 and and CCONJ iajs-1066 64 17 its its PRON iajs-1066 64 18 complexes complex NOUN iajs-1066 64 19 showed show VERB iajs-1066 64 20 biological biological ADJ iajs-1066 64 21 activities activity NOUN iajs-1066 64 22 against against ADP iajs-1066 64 23 the the DET iajs-1066 64 24 type type NOUN iajs-1066 64 25 of of ADP iajs-1066 64 26 bacterial(bacillus bacterial(bacillus PROPN iajs-1066 64 27 ) ) PUNCT iajs-1066 64 28 except[cu(l)cl].[27 except[cu(l)cl].[27 PROPN iajs-1066 64 29 and and CCONJ iajs-1066 64 30 28].the 28].the DET iajs-1066 64 31 results result NOUN iajs-1066 64 32 indicate indicate VERB iajs-1066 64 33 that that SCONJ iajs-1066 64 34 the the DET iajs-1066 64 35 complexes complex NOUN iajs-1066 64 36 showed show VERB iajs-1066 64 37 more more ADJ iajs-1066 64 38 activity activity NOUN iajs-1066 64 39 than than ADP iajs-1066 64 40 the the DET iajs-1066 64 41 ligand ligand NOUN iajs-1066 64 42 under under ADP iajs-1066 64 43 similar similar ADJ iajs-1066 64 44 experimental experimental ADJ iajs-1066 64 45 conditions condition NOUN iajs-1066 64 46 , , PUNCT iajs-1066 64 47 table table NOUN iajs-1066 64 48 ( ( PUNCT iajs-1066 64 49 6 6 NUM iajs-1066 64 50 ) ) PUNCT iajs-1066 64 51 dmf dmf PROPN iajs-1066 64 52 ( ( PUNCT iajs-1066 64 53 which which PRON iajs-1066 64 54 was be AUX iajs-1066 64 55 used use VERB iajs-1066 64 56 as as ADP iajs-1066 64 57 a a DET iajs-1066 64 58 solvent solvent NOUN iajs-1066 64 59 and and CCONJ iajs-1066 64 60 controller controller NOUN iajs-1066 64 61 ) ) PUNCT iajs-1066 64 62 was be AUX iajs-1066 64 63 a a DET iajs-1066 64 64 good good ADJ iajs-1066 64 65 solvent solvent NOUN iajs-1066 64 66 to to PART iajs-1066 64 67 prepare prepare VERB iajs-1066 64 68 1ppm 1ppm NUM iajs-1066 64 69 of of ADP iajs-1066 64 70 each each DET iajs-1066 64 71 tested test VERB iajs-1066 64 72 sample sample NOUN iajs-1066 64 73     SPACE iajs-1066 64 74 .all .all SCONJ iajs-1066 64 75 compounds compound NOUN iajs-1066 64 76 ligand ligand VERB iajs-1066 64 77 and and CCONJ iajs-1066 64 78 its its PRON iajs-1066 64 79 complexes complex NOUN iajs-1066 64 80 have have VERB iajs-1066 64 81 good good ADJ iajs-1066 64 82 biological biological ADJ iajs-1066 64 83 activity activity NOUN iajs-1066 64 84 against against ADP iajs-1066 64 85 the the DET iajs-1066 64 86 type type NOUN iajs-1066 64 87 of of ADP iajs-1066 64 88 bacterial bacterial ADJ iajs-1066 64 89 ( ( PUNCT iajs-1066 64 90 escherichia escherichia NOUN iajs-1066 64 91 coli coli NOUN iajs-1066 64 92 ) ) PUNCT iajs-1066 64 93 , , PUNCT iajs-1066 64 94 ( ( PUNCT iajs-1066 64 95 staphylococcusaureu staphylococcusaureu NOUN iajs-1066 64 96 ) ) PUNCT iajs-1066 64 97 and and CCONJ iajs-1066 64 98 ( ( PUNCT iajs-1066 64 99 escherichia escherichia NOUN iajs-1066 64 100 coli coli NOUN iajs-1066 64 101 ) ) PUNCT iajs-1066 64 102 in in ADP iajs-1066 64 103 fig fig NOUN iajs-1066 64 104 ( ( PUNCT iajs-1066 64 105 5).table 5).table NUM iajs-1066 64 106 ( ( PUNCT iajs-1066 64 107 6 6 NUM iajs-1066 64 108 ) ) PUNCT iajs-1066 64 109 diameter diameter NOUN iajs-1066 64 110 of of ADP iajs-1066 64 111 zone zone NOUN iajs-1066 64 112 of of ADP iajs-1066 64 113 inhibition inhibition NOUN iajs-1066 64 114 . . PUNCT iajs-1066 65 1 molar molar ADJ iajs-1066 65 2 conductivity conductivity NOUN iajs-1066 65 3 the the DET iajs-1066 65 4 conductance conductance NOUN iajs-1066 65 5 values value NOUN iajs-1066 65 6 in in ADP iajs-1066 65 7 dmfof dmfof NOUN iajs-1066 65 8 the the DET iajs-1066 65 9 complexes complex NOUN iajs-1066 65 10 show show VERB iajs-1066 65 11 in in ADP iajs-1066 65 12 the the DET iajs-1066 65 13 ambit10 ambit10 NOUN iajs-1066 65 14 to to ADP iajs-1066 65 15 25 25 NUM iajs-1066 65 16 ohm1.cm2mol-1 ohm1.cm2mol-1 PROPN iajs-1066 65 17 which which PRON iajs-1066 65 18 is be AUX iajs-1066 65 19 quite quite ADV iajs-1066 65 20 lower low ADJ iajs-1066 65 21 than than ADP iajs-1066 65 22 that that PRON iajs-1066 65 23 expected expect VERB iajs-1066 65 24 for for ADP iajs-1066 65 25 an an DET iajs-1066 65 26 electrolyte electrolyte NOUN iajs-1066 65 27 and and CCONJ iajs-1066 65 28 appear appear VERB iajs-1066 65 29 their their PRON iajs-1066 65 30 nonelectrolytic nonelectrolytic ADJ iajs-1066 65 31 nature nature NOUN iajs-1066 65 32 as as ADP iajs-1066 65 33 in in ADP iajs-1066 65 34 table(5 table(5 PROPN iajs-1066 65 35 ) ) PUNCT iajs-1066 65 36 . . PUNCT iajs-1066 65 37     SPACE iajs-1066 66 1 conclusion conclusion NOUN iajs-1066 66 2 the the DET iajs-1066 66 3 new new ADJ iajs-1066 66 4 ligand ligand NOUN iajs-1066 66 5 ( ( PUNCT iajs-1066 66 6 l l NOUN iajs-1066 66 7 ) ) PUNCT iajs-1066 66 8 and and CCONJ iajs-1066 66 9 all all DET iajs-1066 66 10 complexes complex NOUN iajs-1066 66 11 were be AUX iajs-1066 66 12 synthesis synthesis NOUN iajs-1066 66 13 . . PUNCT iajs-1066 67 1 the the DET iajs-1066 67 2 metal metal NOUN iajs-1066 67 3 ( ( PUNCT iajs-1066 67 4 ii ii NOUN iajs-1066 67 5 ) ) PUNCT iajs-1066 67 6 ions ion NOUN iajs-1066 67 7 are be AUX iajs-1066 67 8 coordinated coordinate VERB iajs-1066 67 9 by by ADP iajs-1066 67 10 one one NUM iajs-1066 67 11 amine amine NOUN iajs-1066 67 12 ( ( PUNCT iajs-1066 67 13 h h NOUN iajs-1066 67 14 - - PUNCT iajs-1066 67 15 c c NOUN iajs-1066 67 16 = = NOUN iajs-1066 67 17 n n CCONJ iajs-1066 67 18 ) ) PUNCT iajs-1066 67 19 atom atom NOUN iajs-1066 67 20 , , PUNCT iajs-1066 67 21 n n NOUN iajs-1066 67 22 of of ADP iajs-1066 67 23 pyridine pyridine NOUN iajs-1066 67 24 and and CCONJ iajs-1066 67 25 o o NOUN iajs-1066 67 26 atom atom NOUN iajs-1066 67 27 of of ADP iajs-1066 67 28 benzoin benzoin NOUN iajs-1066 67 29 . . PUNCT iajs-1066 68 1 spectroscopic spectroscopic ADJ iajs-1066 68 2 and and CCONJ iajs-1066 68 3 structural structural ADJ iajs-1066 68 4 data datum NOUN iajs-1066 68 5 display(4)-chelate display(4)-chelate VERB iajs-1066 68 6 in in ADP iajs-1066 68 7 metal metal NOUN iajs-1066 68 8 complexes complex NOUN iajs-1066 68 9 obtaining obtain VERB iajs-1066 68 10 to to ADP iajs-1066 68 11 the the DET iajs-1066 68 12 bind bind NOUN iajs-1066 68 13 of of ADP iajs-1066 68 14 tridentates tridentate NOUN iajs-1066 68 15 ligand ligand NOUN iajs-1066 68 16 groups group NOUN iajs-1066 68 17 with with ADP iajs-1066 68 18 one one NUM iajs-1066 68 19 chelated chelate VERB iajs-1066 68 20 chloride chloride NOUN iajs-1066 68 21 in in ADP iajs-1066 68 22 schemes scheme NOUN iajs-1066 68 23 ( ( PUNCT iajs-1066 68 24 1&2 1&2 NUM iajs-1066 68 25 ) ) PUNCT iajs-1066 68 26 . . PUNCT iajs-1066 69 1 references reference NOUN iajs-1066 69 2 1 1 NUM iajs-1066 69 3 . . PUNCT iajs-1066 69 4 aggar aggar PROPN iajs-1066 69 5 n. n. PROPN iajs-1066 69 6 ; ; PUNCT iajs-1066 69 7 wal wal PROPN iajs-1066 69 8 , , PUNCT iajs-1066 69 9 r. r. PROPN iajs-1066 69 10 kumar kumar PROPN iajs-1066 69 11 ; ; PUNCT iajs-1066 69 12 dureja dureja PROPN iajs-1066 69 13 , , PUNCT iajs-1066 69 14 p.andrawat p.andrawat PROPN iajs-1066 69 15 , , PUNCT iajs-1066 69 16 d.s.;(2009 d.s.;(2009 NUM iajs-1066 69 17 ) ) PUNCT iajs-1066 69 18 , , PUNCT iajs-1066 69 19 schiff schiff NOUN iajs-1066 69 20 base base NOUN iajs-1066 69 21 as as ADP iajs-1066 69 22 potential potential ADJ iajs-1066 69 23 fungicides fungicide NOUN iajs-1066 69 24 and and CCONJ iajs-1066 69 25 nitrification nitrification NOUN iajs-1066 69 26 inhibitors inhibitor NOUN iajs-1066 69 27 , , PUNCT iajs-1066 69 28 j. j. PROPN iajs-1066 69 29 agric agric PROPN iajs-1066 69 30 . . PUNCT iajs-1066 70 1 food food NOUN iajs-1066 70 2 chem chem NOUN iajs-1066 70 3 . . PUNCT iajs-1066 70 4 , , PUNCT iajs-1066 70 5 57 57 NUM iajs-1066 70 6 , , PUNCT iajs-1066 70 7 8520 8520 NUM iajs-1066 70 8 - - SYM iajs-1066 70 9 8525 8525 NUM iajs-1066 70 10 . . PUNCT iajs-1066 71 1 2 2 X iajs-1066 71 2 . . NUM iajs-1066 71 3 banik banik X iajs-1066 71 4 , , PUNCT iajs-1066 71 5 j. j. PROPN iajs-1066 71 6 and and CCONJ iajs-1066 71 7 banik banik X iajs-1066 71 8 , , PUNCT iajs-1066 71 9 b. b. PROPN iajs-1066 71 10 n. n. 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PROPN iajs-1066 108 31 chem chem PROPN iajs-1066 108 32 . . PUNCT iajs-1066 108 33 ,10,557 ,10,557 PUNCT iajs-1066 108 34 - - PUNCT iajs-1066 108 35 560 560 NUM iajs-1066 108 36 16 16 NUM iajs-1066 108 37 . . PUNCT iajs-1066 109 1 chaurasia chaurasia PROPN iajs-1066 109 2 , , PUNCT iajs-1066 109 3 m.r m.r PROPN iajs-1066 109 4 . . PROPN iajs-1066 109 5 ; ; PUNCT iajs-1066 109 6 miss miss PROPN iajs-1066 109 7 p. p. PROPN iajs-1066 109 8 s. s. 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PUNCT iajs-1066 111 43 cotton cotton NOUN iajs-1066 111 44 , , PUNCT iajs-1066 111 45 a. a. NOUN iajs-1066 111 46 ; ; PUNCT iajs-1066 111 47 fandwilkenson fandwilkenson NOUN iajs-1066 111 48 , , PUNCT iajs-1066 111 49 g.;(1988 g.;(1988 NOUN iajs-1066 111 50 ) ) PUNCT iajs-1066 111 51 advanced advanced ADJ iajs-1066 111 52 inorganic inorganic ADJ iajs-1066 111 53 chemistry,5th chemistry,5th PROPN iajs-1066 111 54 edition edition NOUN iajs-1066 111 55 ; ; PUNCT iajs-1066 111 56 johnwiley johnwiley NOUN iajs-1066 111 57 and and CCONJ iajs-1066 111 58 sons son NOUN iajs-1066 111 59 , , PUNCT iajs-1066 111 60 usa usa PROPN iajs-1066 111 61 , , PUNCT iajs-1066 111 62 37 37 NUM iajs-1066 111 63 - - SYM iajs-1066 111 64 50 50 NUM iajs-1066 111 65 . . PUNCT iajs-1066 111 66 19 19 NUM iajs-1066 111 67 . . PUNCT iajs-1066 111 68 cozzi cozzi PROPN iajs-1066 111 69 , , PUNCT iajs-1066 111 70 p.g p.g PROPN iajs-1066 111 71 . . PROPN iajs-1066 111 72 , , PUNCT iajs-1066 111 73 metal metal PROPN iajs-1066 111 74 – – PUNCT iajs-1066 111 75 salen salen PROPN iajs-1066 111 76 schiff schiff NOUN iajs-1066 111 77 base base NOUN iajs-1066 111 78 complexes complex NOUN iajs-1066 111 79 in in ADP iajs-1066 111 80 catalysis;(2004 catalysis;(2004 PROPN iajs-1066 111 81 ) ) PUNCT iajs-1066 111 82 , , PUNCT iajs-1066 111 83 practical practical ADJ iajs-1066 111 84 aspects aspect NOUN iajs-1066 111 85 . . PUNCT iajs-1066 112 1 chem chem NOUN iajs-1066 112 2 . . PUNCT iajs-1066 113 1 soc soc PROPN iajs-1066 113 2 . . PUNCT iajs-1066 114 1 rev rev PROPN iajs-1066 114 2 . . PROPN iajs-1066 114 3 , , PUNCT iajs-1066 114 4 33 33 NUM iajs-1066 114 5 , , PUNCT iajs-1066 114 6 410 410 NUM iajs-1066 114 7 - - SYM iajs-1066 114 8 421 421 NUM iajs-1066 114 9 . . PUNCT iajs-1066 115 1 20 20 NUM iajs-1066 115 2 . . X iajs-1066 116 1 alsha'alan alsha'alan ADJ iajs-1066 116 2 , , PUNCT iajs-1066 116 3 n. n. PROPN iajs-1066 116 4 h. h. 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PUNCT iajs-1066 117 30 , , PUNCT iajs-1066 117 31 synth synth ADJ iajs-1066 117 32 react react NOUN iajs-1066 117 33 inorg inorg PROPN iajs-1066 117 34 met meet VERB iajs-1066 117 35 - - PUNCT iajs-1066 117 36 orgchem orgchem NOUN iajs-1066 117 37 . . PUNCT iajs-1066 118 1 16:257–272 16:257–272 NUM iajs-1066 118 2 . . PUNCT iajs-1066 119 1 chemistry chemistry NOUN iajs-1066 119 2 | | ADV iajs-1066 119 3 137 137 NUM iajs-1066 119 4 2017عام 2017عام NUM iajs-1066 119 5 ) ) PUNCT iajs-1066 120 1 1(العدد 1(العدد NUM iajs-1066 120 2 30المجلد 30المجلد NUM iajs-1066 120 3 مجلة مجلة VERB iajs-1066 120 4 إبن إبن NOUN iajs-1066 120 5 الھيثم الھيثم NOUN iajs-1066 120 6 للعلوم للعلوم NOUN iajs-1066 120 7 الصرفة الصرفة NOUN iajs-1066 120 8 والتطبيقية والتطبيقية VERB iajs-1066 120 9 ibn ibn PROPN iajs-1066 120 10 al al PROPN iajs-1066 120 11 - - PUNCT iajs-1066 120 12 haitham haitham PROPN iajs-1066 120 13 jour jour X iajs-1066 120 14 . . PROPN iajs-1066 121 1 for for ADP iajs-1066 121 2 pure pure ADJ iajs-1066 121 3 & & CCONJ iajs-1066 121 4 appl appl PROPN iajs-1066 121 5 . . PUNCT iajs-1066 122 1 sci sci PROPN iajs-1066 122 2 . . PUNCT iajs-1066 122 3 vol vol NOUN iajs-1066 122 4 . . PROPN iajs-1066 122 5 30 30 NUM iajs-1066 122 6 ( ( PUNCT iajs-1066 122 7 1 1 NUM iajs-1066 122 8 ) ) PUNCT iajs-1066 122 9 2017 2017 NUM iajs-1066 122 10 22 22 NUM iajs-1066 122 11 . . PUNCT iajs-1066 123 1 hamurcu hamurcu PROPN iajs-1066 123 2 , , PUNCT iajs-1066 123 3 f. f. PROPN iajs-1066 123 4 ; ; PUNCT iajs-1066 123 5 gunduzalp gunduzalp PROPN iajs-1066 123 6 , , PUNCT iajs-1066 123 7 a. a. PROPN iajs-1066 123 8 b. b. PROPN iajs-1066 123 9 ; ; PUNCT iajs-1066 123 10 cetes.anderk cetes.anderk PROPN iajs-1066 123 11 , , PUNCT iajs-1066 123 12 b. b. 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PUNCT iajs-1066 124 1 m.chem m.chem PROPN iajs-1066 124 2 . . PUNCT iajs-1066 125 1 , , PUNCT iajs-1066 125 2 33 33 NUM iajs-1066 125 3 : : SYM iajs-1066 125 4 141 141 NUM iajs-1066 125 5 . . X iajs-1066 125 6 23 23 NUM iajs-1066 125 7 . . PUNCT iajs-1066 125 8 a. a. NOUN iajs-1066 125 9 a. a. PROPN iajs-1066 125 10 ahmed ahmed PROPN iajs-1066 125 11 and and CCONJ iajs-1066 125 12 s. s. PROPN iajs-1066 125 13 a. a. 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