id	sid	tid	token	lemma	pos
iajs-1146	1	1	ibn	ibn	PROPN
iajs-1146	1	2	alhaitham	alhaitham	NOUN
iajs-1146	1	3	j.	j.	PROPN
iajs-1146	2	1	fo	fo	ADP
iajs-1146	2	2	r	r	NOUN
iajs-1146	2	3	pure	pure	ADJ
iajs-1146	2	4	&	&	CCONJ
iajs-1146	2	5	appl	appl	PROPN
iajs-1146	2	6	.	.	PUNCT
iajs-1146	3	1	sc	sc	PROPN
iajs-1146	4	1	i	i	PRON
iajs-1146	4	2	vo	vo	INTJ
iajs-1146	4	3	l.22	l.22	X
iajs-1146	4	4	(	(	PUNCT
iajs-1146	4	5	4	4	NUM
iajs-1146	4	6	)	)	SYM
iajs-1146	4	7	2009	2009	NUM
iajs-1146	4	8	synthesis	synthesis	NOUN
iajs-1146	4	9	of	of	ADP
iajs-1146	4	10	3	3	NUM
iajs-1146	4	11	-	-	PUNCT
iajs-1146	4	12	c	c	NOUN
iajs-1146	4	13	-	-	PUNCT
iajs-1146	4	14	spiro	spiro	NOUN
iajs-1146	4	15	ring	ring	NOUN
iajs-1146	4	16	nucleoside	nucleoside	NOUN
iajs-1146	4	17	analogues	analogue	NOUN
iajs-1146	4	18	,	,	PUNCT
iajs-1146	4	19	of	of	ADP
iajs-1146	4	20	possible	possible	ADJ
iajs-1146	4	21	biological	biological	ADJ
iajs-1146	4	22	activity	activity	NOUN
iajs-1146	4	23	e.	e.	PROPN
iajs-1146	4	24	m.hussain	m.hussain	PROPN
iajs-1146	4	25	department	department	PROPN
iajs-1146	4	26	of	of	ADP
iajs-1146	4	27	chemistry	chemistry	NOUN
iajs-1146	4	28	,	,	PUNCT
iajs-1146	4	29	college	college	NOUN
iajs-1146	4	30	of	of	ADP
iajs-1146	4	31	education	education	NOUN
iajs-1146	4	32	,	,	PUNCT
iajs-1146	4	33	ibn	ibn	PROPN
iajs-1146	4	34	al	al	PROPN
iajs-1146	4	35	-	-	PUNCT
iajs-1146	4	36	haitham	haitham	PROPN
iajs-1146	4	37	university	university	PROPN
iajs-1146	4	38	of	of	ADP
iajs-1146	4	39	baghdad	baghdad	PROPN
iajs-1146	4	40	abstract	abstract	ADV
iajs-1146	4	41	in	in	ADP
iajs-1146	4	42	this	this	DET
iajs-1146	4	43	study	study	NOUN
iajs-1146	4	44	,	,	PUNCT
iajs-1146	4	45	new	new	ADJ
iajs-1146	4	46	derivatives	derivative	NOUN
iajs-1146	4	47	of	of	ADP
iajs-1146	4	48	3	3	NUM
iajs-1146	4	49	-	-	PUNCT
iajs-1146	4	50	c	c	NOUN
iajs-1146	4	51	-	-	PUNCT
iajs-1146	4	52	sp	sp	NOUN
iajs-1146	4	53	iro	iro	PROPN
iajs-1146	4	54	ring	ring	NOUN
iajs-1146	4	55	nucleoside	nucleoside	NOUN
iajs-1146	4	56	analogues	analogue	NOUN
iajs-1146	4	57	were	be	AUX
iajs-1146	4	58	synthesized	synthesize	VERB
iajs-1146	4	59	.	.	PUNCT
iajs-1146	5	1	the	the	DET
iajs-1146	5	2	structures	structure	NOUN
iajs-1146	5	3	of	of	ADP
iajs-1146	5	4	these	these	DET
iajs-1146	5	5	derivatives	derivative	NOUN
iajs-1146	5	6	were	be	AUX
iajs-1146	5	7	characterized	characterize	VERB
iajs-1146	5	8	by	by	ADP
iajs-1146	5	9	infrared	infrared	ADJ
iajs-1146	5	10	spectroscopy	spectroscopy	NOUN
iajs-1146	5	11	,	,	PUNCT
iajs-1146	5	12	1	1	NUM
iajs-1146	5	13	hnmr	hnmr	NOUN
iajs-1146	5	14	(	(	PUNCT
iajs-1146	5	15	some	some	PRON
iajs-1146	5	16	of	of	ADP
iajs-1146	5	17	them	they	PRON
iajs-1146	5	18	)	)	PUNCT
iajs-1146	5	19	and	and	CCONJ
iajs-1146	5	20	elemental	elemental	ADJ
iajs-1146	5	21	analysis	analysis	NOUN
iajs-1146	5	22	.	.	PUNCT
iajs-1146	6	1	the	the	DET
iajs-1146	6	2	nucleoside	nucleoside	ADJ
iajs-1146	6	3	derivatives	derivative	NOUN
iajs-1146	6	4	were	be	AUX
iajs-1146	6	5	tested	test	VERB
iajs-1146	6	6	for	for	ADP
iajs-1146	6	7	inhibition	inhibition	NOUN
iajs-1146	6	8	of	of	ADP
iajs-1146	6	9	e	e	NOUN
iajs-1146	6	10	-	-	NOUN
iajs-1146	6	11	coli	coli	NOUN
iajs-1146	6	12	and	and	CCONJ
iajs-1146	6	13	were	be	AUX
iajs-1146	6	14	all	all	PRON
iajs-1146	6	15	found	find	VERB
iajs-1146	6	16	to	to	PART
iajs-1146	6	17	be	be	AUX
iajs-1146	6	18	active	active	ADJ
iajs-1146	6	19	.	.	PUNCT
iajs-1146	7	1	introduction	introduction	NOUN
iajs-1146	7	2	nucleosides	nucleoside	VERB
iajs-1146	7	3	and	and	CCONJ
iajs-1146	7	4	nucleotides	nucleotide	NOUN
iajs-1146	7	5	play	play	VERB
iajs-1146	7	6	a	a	DET
iajs-1146	7	7	key	key	ADJ
iajs-1146	7	8	role	role	NOUN
iajs-1146	7	9	in	in	ADP
iajs-1146	7	10	many	many	ADJ
iajs-1146	7	11	biosynthesis	biosynthesis	NOUN
iajs-1146	7	12	and	and	CCONJ
iajs-1146	7	13	regulatory	regulatory	ADJ
iajs-1146	7	14	process	process	NOUN
iajs-1146	7	15	,	,	PUNCT
iajs-1146	7	16	an	an	DET
iajs-1146	7	17	extremely	extremely	ADV
iajs-1146	7	18	important	important	ADJ
iajs-1146	7	19	function	function	NOUN
iajs-1146	7	20	takes	take	VERB
iajs-1146	7	21	place	place	NOUN
iajs-1146	7	22	at	at	ADP
iajs-1146	7	23	the	the	DET
iajs-1146	7	24	level	level	NOUN
iajs-1146	7	25	of	of	ADP
iajs-1146	7	26	structure	structure	NOUN
iajs-1146	7	27	of	of	ADP
iajs-1146	7	28	ribo	ribo	NOUN
iajs-1146	7	29	–	–	PUNCT
iajs-1146	7	30	and	and	CCONJ
iajs-1146	7	31	deoxyribonucleic	deoxyribonucleic	ADJ
iajs-1146	7	32	acids	acid	NOUN
iajs-1146	8	1	[	[	X
iajs-1146	8	2	1	1	NUM
iajs-1146	8	3	]	]	PUNCT
iajs-1146	8	4	.	.	PUNCT
iajs-1146	9	1	several	several	ADJ
iajs-1146	9	2	novel	novel	ADJ
iajs-1146	9	3	5	5	NUM
iajs-1146	9	4	-	-	PUNCT
iajs-1146	9	5	substituted	substitute	VERB
iajs-1146	9	6	2	2	NUM
iajs-1146	9	7	/	/	SYM
iajs-1146	9	8	-deoxyuridine	-deoxyuridine	NOUN
iajs-1146	9	9	analogues	analogue	NOUN
iajs-1146	9	10	were	be	AUX
iajs-1146	9	11	evaluated	evaluate	VERB
iajs-1146	9	12	as	as	ADP
iajs-1146	9	13	substrates	substrate	NOUN
iajs-1146	9	14	for	for	ADP
iajs-1146	9	15	highly	highly	ADV
iajs-1146	9	16	purified	purified	ADJ
iajs-1146	9	17	herpes	herpe	NOUN
iajs-1146	9	18	simplex	simplex	NOUN
iajs-1146	9	19	virus	virus	NOUN
iajs-1146	9	20	type	type	NOUN
iajs-1146	9	21	1	1	NUM
iajs-1146	9	22	(	(	PUNCT
iajs-1146	9	23	hsv-1	hsv-1	X
iajs-1146	9	24	)	)	PUNCT
iajs-1146	9	25	encoded	encode	VERB
iajs-1146	9	26	thymidine	thymidine	ADJ
iajs-1146	9	27	kinase	kinase	PROPN
iajs-1146	9	28	derived	derive	VERB
iajs-1146	9	29	from	from	ADP
iajs-1146	9	30	hsv-1	hsv-1	PRON
iajs-1146	9	31	(	(	PUNCT
iajs-1146	9	32	t	t	PROPN
iajs-1146	9	33	k	k	NOUN
iajs-1146	9	34	)	)	PUNCT
iajs-1146	9	35	genetransfected	genetransfecte	VERB
iajs-1146	9	36	murine	murine	ADJ
iajs-1146	9	37	mammary	mammary	ADJ
iajs-1146	9	38	carcinoma	carcinoma	NOUN
iajs-1146	9	39	cells	cell	NOUN
iajs-1146	9	40	,	,	PUNCT
iajs-1146	9	41	and	and	CCONJ
iajs-1146	9	42	human	human	ADJ
iajs-1146	9	43	platelet	platelet	NOUN
iajs-1146	9	44	thymidine	thymidine	ADJ
iajs-1146	9	45	phosphorylase	phosphorylase	NOUN
iajs-1146	10	1	[	[	X
iajs-1146	10	2	2,3	2,3	NUM
iajs-1146	10	3	]	]	PUNCT
iajs-1146	10	4	.	.	PUNCT
iajs-1146	11	1	the	the	DET
iajs-1146	11	2	potential	potential	ADJ
iajs-1146	11	3	use	use	NOUN
iajs-1146	11	4	of	of	ADP
iajs-1146	11	5	nucleoside	nucleoside	ADJ
iajs-1146	11	6	analogues	analogue	NOUN
iajs-1146	11	7	in	in	ADP
iajs-1146	11	8	antiparasite	antiparasite	ADJ
iajs-1146	11	9	chemotherapy	chemotherapy	NOUN
iajs-1146	11	10	is	be	AUX
iajs-1146	11	11	also	also	ADV
iajs-1146	11	12	of	of	ADP
iajs-1146	11	13	great	great	ADJ
iajs-1146	11	14	importance	importance	NOUN
iajs-1146	11	15	and	and	CCONJ
iajs-1146	11	16	about	about	ADV
iajs-1146	11	17	three	three	NUM
iajs-1146	11	18	billion	billion	NUM
iajs-1146	11	19	people	people	NOUN
iajs-1146	11	20	in	in	ADP
iajs-1146	11	21	the	the	DET
iajs-1146	11	22	world	world	NOUN
iajs-1146	11	23	are	be	AUX
iajs-1146	11	24	affected	affect	VERB
iajs-1146	11	25	by	by	ADP
iajs-1146	11	26	parasitic	parasitic	ADJ
iajs-1146	11	27	diseases	disease	NOUN
iajs-1146	11	28	[	[	X
iajs-1146	11	29	4].protozoan	4].protozoan	NUM
iajs-1146	11	30	and	and	CCONJ
iajs-1146	11	31	helmintic	helmintic	ADJ
iajs-1146	11	32	parasites	parasite	NOUN
iajs-1146	11	33	have	have	VERB
iajs-1146	11	34	both	both	CCONJ
iajs-1146	11	35	a	a	DET
iajs-1146	11	36	deficiency	deficiency	NOUN
iajs-1146	11	37	in	in	ADP
iajs-1146	11	38	denovo	denovo	PROPN
iajs-1146	11	39	synthesis	synthesis	NOUN
iajs-1146	11	40	of	of	ADP
iajs-1146	11	41	purine	purine	NOUN
iajs-1146	11	42	nucleotides	nucleotide	NOUN
iajs-1146	11	43	,	,	PUNCT
iajs-1146	11	44	and	and	CCONJ
iajs-1146	11	45	the	the	DET
iajs-1146	11	46	purine	purine	NOUN
iajs-1146	11	47	salvage	salvage	NOUN
iajs-1146	11	48	pathways	pathway	NOUN
iajs-1146	11	49	are	be	AUX
iajs-1146	11	50	essential	essential	ADJ
iajs-1146	11	51	for	for	ADP
iajs-1146	11	52	their	their	PRON
iajs-1146	11	53	survival	survival	NOUN
iajs-1146	11	54	and	and	CCONJ
iajs-1146	11	55	growth	growth	NOUN
iajs-1146	11	56	[	[	X
iajs-1146	11	57	5,6	5,6	NUM
iajs-1146	11	58	]	]	X
iajs-1146	11	59	.	.	PUNCT
iajs-1146	12	1	thus	thus	ADV
iajs-1146	12	2	,	,	PUNCT
iajs-1146	12	3	formycin	formycin	PROPN
iajs-1146	12	4	b	b	PROPN
iajs-1146	13	1	[	[	X
iajs-1146	13	2	7],allopurinol	7],allopurinol	NUM
iajs-1146	13	3	riboside	riboside	NOUN
iajs-1146	13	4	[	[	X
iajs-1146	13	5	8	8	NUM
iajs-1146	13	6	]	]	PUNCT
iajs-1146	13	7	and	and	CCONJ
iajs-1146	13	8	thiopurinol	thiopurinol	NOUN
iajs-1146	13	9	riboside	riboside	NOUN
iajs-1146	13	10	[	[	X
iajs-1146	13	11	9	9	NUM
iajs-1146	13	12	]	]	SYM
iajs-1146	13	13	figure	figure	NOUN
iajs-1146	13	14	(	(	PUNCT
iajs-1146	13	15	1	1	X
iajs-1146	13	16	)	)	PUNCT
iajs-1146	13	17	are	be	AUX
iajs-1146	13	18	converted	convert	VERB
iajs-1146	13	19	by	by	ADP
iajs-1146	13	20	a	a	DET
iajs-1146	13	21	nucleoside	nucleoside	ADJ
iajs-1146	13	22	phosphotransferase	phosphotransferase	NOUN
iajs-1146	13	23	to	to	ADP
iajs-1146	13	24	their	their	PRON
iajs-1146	13	25	corresponding	correspond	VERB
iajs-1146	13	26	nucleotides	nucleotide	NOUN
iajs-1146	13	27	,	,	PUNCT
iajs-1146	13	28	which	which	PRON
iajs-1146	13	29	can	can	AUX
iajs-1146	13	30	either	either	CCONJ
iajs-1146	13	31	act	act	VERB
iajs-1146	13	32	as	as	ADP
iajs-1146	13	33	inhibitors	inhibitor	NOUN
iajs-1146	13	34	of	of	ADP
iajs-1146	13	35	other	other	ADJ
iajs-1146	13	36	essential	essential	ADJ
iajs-1146	13	37	enzymes	enzyme	NOUN
iajs-1146	13	38	in	in	ADP
iajs-1146	13	39	purine	purine	NOUN
iajs-1146	13	40	metabolism	metabolism	NOUN
iajs-1146	14	1	[	[	X
iajs-1146	14	2	6,9	6,9	NUM
iajs-1146	14	3	]	]	PUNCT
iajs-1146	14	4	or	or	CCONJ
iajs-1146	14	5	be	be	AUX
iajs-1146	14	6	incorporated	incorporate	VERB
iajs-1146	14	7	into	into	ADP
iajs-1146	14	8	the	the	DET
iajs-1146	14	9	nucleic	nucleic	ADJ
iajs-1146	14	10	acids	acid	NOUN
iajs-1146	14	11	of	of	ADP
iajs-1146	14	12	these	these	DET
iajs-1146	14	13	organisms	organism	NOUN
iajs-1146	14	14	[	[	X
iajs-1146	14	15	8,10	8,10	X
iajs-1146	14	16	]	]	PUNCT
iajs-1146	14	17	.	.	PUNCT
iajs-1146	15	1	eman	eman	NOUN
iajs-1146	16	1	[	[	X
iajs-1146	16	2	11	11	NUM
iajs-1146	16	3	]	]	PUNCT
iajs-1146	16	4	has	have	AUX
iajs-1146	16	5	synthesized	synthesize	VERB
iajs-1146	16	6	different	different	ADJ
iajs-1146	16	7	derivatives	derivative	NOUN
iajs-1146	16	8	of	of	ADP
iajs-1146	16	9	3	3	NUM
iajs-1146	16	10	\	\	NOUN
iajs-1146	16	11	-alkyl	-alkyl	NOUN
iajs-1146	16	12	nucleoside	nucleoside	NOUN
iajs-1146	16	13	analogues	analogue	NOUN
iajs-1146	16	14	[	[	X
iajs-1146	16	15	figure	figure	NOUN
iajs-1146	16	16	2	2	NUM
iajs-1146	16	17	]	]	PUNCT
iajs-1146	16	18	.	.	PUNCT
iajs-1146	17	1	these	these	DET
iajs-1146	17	2	derivatives	derivative	NOUN
iajs-1146	17	3	were	be	AUX
iajs-1146	17	4	tested	test	VERB
iajs-1146	17	5	for	for	ADP
iajs-1146	17	6	the	the	DET
iajs-1146	17	7	inhibition	inhibition	NOUN
iajs-1146	17	8	of	of	ADP
iajs-1146	17	9	e	e	NOUN
iajs-1146	17	10	-	-	NOUN
iajs-1146	17	11	coli	coli	NOUN
iajs-1146	17	12	and	and	CCONJ
iajs-1146	17	13	were	be	AUX
iajs-1146	17	14	all	all	PRON
iajs-1146	17	15	found	find	VERB
iajs-1146	17	16	to	to	PART
iajs-1146	17	17	be	be	AUX
iajs-1146	17	18	active	active	ADJ
iajs-1146	17	19	.	.	PUNCT
iajs-1146	18	1	spirobicyclic	spirobicyclic	ADJ
iajs-1146	18	2	cores	core	NOUN
iajs-1146	18	3	display	display	VERB
iajs-1146	18	4	an	an	DET
iajs-1146	18	5	important	important	ADJ
iajs-1146	18	6	role	role	NOUN
iajs-1146	18	7	in	in	ADP
iajs-1146	18	8	the	the	DET
iajs-1146	18	9	field	field	NOUN
iajs-1146	18	10	of	of	ADP
iajs-1146	18	11	the	the	DET
iajs-1146	18	12	development	development	NOUN
iajs-1146	18	13	of	of	ADP
iajs-1146	18	14	new	new	ADJ
iajs-1146	18	15	bioactive	bioactive	ADJ
iajs-1146	18	16	substances	substance	NOUN
iajs-1146	18	17	[	[	X
iajs-1146	18	18	12	12	NUM
iajs-1146	18	19	]	]	PUNCT
iajs-1146	18	20	.	.	PUNCT
iajs-1146	19	1	firas	firas	PROPN
iajs-1146	20	1	[	[	X
iajs-1146	20	2	13	13	NUM
iajs-1146	20	3	]	]	PUNCT
iajs-1146	20	4	has	have	AUX
iajs-1146	20	5	prepared	prepare	VERB
iajs-1146	20	6	some	some	DET
iajs-1146	20	7	derivatives	derivative	NOUN
iajs-1146	20	8	of	of	ADP
iajs-1146	20	9	spiro	spiro	NOUN
iajs-1146	20	10	fused	fuse	VERB
iajs-1146	20	11	ring	ring	NOUN
iajs-1146	20	12	and	and	CCONJ
iajs-1146	20	13	imine	imine	NOUN
iajs-1146	20	14	position	position	NOUN
iajs-1146	20	15	-3	-3	PUNCT
iajs-1146	20	16	of	of	ADP
iajs-1146	20	17	d	d	NOUN
iajs-1146	20	18	-	-	PUNCT
iajs-1146	20	19	glucofuranose	glucofuranose	ADJ
iajs-1146	20	20	figure	figure	NOUN
iajs-1146	20	21	(	(	PUNCT
iajs-1146	20	22	3	3	NUM
iajs-1146	20	23	)	)	PUNCT
iajs-1146	20	24	and	and	CCONJ
iajs-1146	20	25	were	be	AUX
iajs-1146	20	26	all	all	PRON
iajs-1146	20	27	found	find	VERB
iajs-1146	20	28	to	to	PART
iajs-1146	20	29	have	have	VERB
iajs-1146	20	30	biological	biological	ADJ
iajs-1146	20	31	activity	activity	NOUN
iajs-1146	20	32	.	.	PUNCT
iajs-1146	21	1	in	in	ADP
iajs-1146	21	2	this	this	DET
iajs-1146	21	3	work	work	NOUN
iajs-1146	21	4	i	i	PRON
iajs-1146	21	5	decided	decide	VERB
iajs-1146	21	6	to	to	PART
iajs-1146	21	7	synthesize	synthesize	VERB
iajs-1146	21	8	new	new	ADJ
iajs-1146	21	9	derivatives	derivative	NOUN
iajs-1146	21	10	of	of	ADP
iajs-1146	21	11	nucleoside	nucleoside	ADJ
iajs-1146	21	12	analogues	analogue	NOUN
iajs-1146	21	13	with	with	ADP
iajs-1146	21	14	sp	sp	ADP
iajs-1146	21	15	iro	iro	PROPN
iajs-1146	21	16	ring	ring	NOUN
iajs-1146	21	17	at	at	ADP
iajs-1146	21	18	position-3	position-3	PROPN
iajs-1146	21	19	on	on	ADP
iajs-1146	21	20	dglucofuranose	dglucofuranose	PROPN
iajs-1146	21	21	ring	ring	NOUN
iajs-1146	21	22	.	.	PUNCT
iajs-1146	22	1	experimental	experimental	ADJ
iajs-1146	22	2	materials	material	NOUN
iajs-1146	22	3	all	all	DET
iajs-1146	22	4	chemicals	chemical	NOUN
iajs-1146	22	5	which	which	PRON
iajs-1146	22	6	were	be	AUX
iajs-1146	22	7	used	use	VERB
iajs-1146	22	8	were	be	AUX
iajs-1146	22	9	supplied	supply	VERB
iajs-1146	22	10	from	from	ADP
iajs-1146	22	11	merk	merk	PROPN
iajs-1146	22	12	chemical	chemical	PROPN
iajs-1146	22	13	fluka	fluka	PROPN
iajs-1146	22	14	ag	ag	PROPN
iajs-1146	22	15	,	,	PUNCT
iajs-1146	22	16	bdh	bdh	NOUN
iajs-1146	22	17	chemicals	chemical	NOUN
iajs-1146	22	18	,	,	PUNCT
iajs-1146	22	19	riedel	riedel	PROPN
iajs-1146	22	20	.de	.de	PUNCT
iajs-1146	22	21	haen	haen	PROPN
iajs-1146	22	22	ag	ag	PROPN
iajs-1146	22	23	,	,	PUNCT
iajs-1146	22	24	acros	acros	PROPN
iajs-1146	22	25	organics	organic	NOUN
iajs-1146	22	26	,	,	PUNCT
iajs-1146	22	27	janssen	janssen	PROPN
iajs-1146	22	28	chemical	chemical	PROPN
iajs-1146	22	29	and	and	CCONJ
iajs-1146	22	30	hopkin	hopkin	PROPN
iajs-1146	22	31	and	and	CCONJ
iajs-1146	22	32	wiliams	wiliam	NOUN
iajs-1146	22	33	.	.	PUNCT
iajs-1146	23	1	/	/	SYM
iajs-1146	23	2	hnmr	hnmr	PROPN
iajs-1146	23	3	spectra	spectra	PROPN
iajs-1146	23	4	were	be	AUX
iajs-1146	23	5	recorded	record	VERB
iajs-1146	23	6	in	in	ADP
iajs-1146	23	7	hitachi	hitachi	PROPN
iajs-1146	23	8	perkin	perkin	PROPN
iajs-1146	23	9	emelr	emelr	PROPN
iajs-1146	23	10	,	,	PUNCT
iajs-1146	23	11	r-24	r-24	VERB
iajs-1146	23	12	b	b	NOUN
iajs-1146	23	13	at	at	ADP
iajs-1146	23	14	60	60	NUM
iajs-1146	23	15	mhz	mhz	ADJ
iajs-1146	23	16	,	,	PUNCT
iajs-1146	23	17	elemental	elemental	ADJ
iajs-1146	23	18	analyzer	analyzer	NOUN
iajs-1146	23	19	was	be	AUX
iajs-1146	23	20	carried	carry	VERB
iajs-1146	23	21	out	out	ADP
iajs-1146	23	22	by	by	ADP
iajs-1146	23	23	using	use	VERB
iajs-1146	23	24	carlo	carlo	PROPN
iajs-1146	23	25	erba	erba	PROPN
iajs-1146	23	26	/mod	/mod	PROPN
iajs-1146	24	1	1106	1106	NUM
iajs-1146	24	2	and	and	CCONJ
iajs-1146	24	3	infrared	infrared	ADJ
iajs-1146	24	4	spectra	spectra	PROPN
iajs-1146	24	5	were	be	AUX
iajs-1146	24	6	recorded	record	VERB
iajs-1146	24	7	by	by	ADP
iajs-1146	24	8	using	use	VERB
iajs-1146	24	9	shimadzu	shimadzu	PROPN
iajs-1146	24	10	-408	-408	PROPN
iajs-1146	24	11	.all	.all	PUNCT
iajs-1146	24	12	synthesized	synthesize	VERB
iajs-1146	24	13	compounds	compound	NOUN
iajs-1146	24	14	were	be	AUX
iajs-1146	24	15	purified	purify	VERB
iajs-1146	24	16	by	by	ADP
iajs-1146	24	17	column	column	NOUN
iajs-1146	24	18	chromatography	chromatography	NOUN
iajs-1146	24	19	by	by	ADP
iajs-1146	24	20	using	use	VERB
iajs-1146	24	21	silica	silica	NOUN
iajs-1146	24	22	gel	gel	NOUN
iajs-1146	24	23	(	(	PUNCT
iajs-1146	24	24	60	60	NUM
iajs-1146	24	25	-	-	SYM
iajs-1146	24	26	120	120	NUM
iajs-1146	24	27	)	)	PUNCT
iajs-1146	24	28	mesh	mesh	NOUN
iajs-1146	24	29	.the	.the	DET
iajs-1146	24	30	biomaterials	biomaterial	NOUN
iajs-1146	24	31	were	be	AUX
iajs-1146	24	32	obtained	obtain	VERB
iajs-1146	24	33	from	from	ADP
iajs-1146	24	34	biomerieux	biomerieux	PROPN
iajs-1146	24	35	ltd	ltd	PROPN
iajs-1146	24	36	.	.	PUNCT
iajs-1146	24	37	ibn	ibn	PROPN
iajs-1146	24	38	alhaitham	alhaitham	PROPN
iajs-1146	25	1	j.	j.	PROPN
iajs-1146	26	1	fo	fo	ADP
iajs-1146	26	2	r	r	NOUN
iajs-1146	26	3	pure	pure	ADJ
iajs-1146	26	4	&	&	CCONJ
iajs-1146	26	5	appl	appl	PROPN
iajs-1146	26	6	.	.	PUNCT
iajs-1146	27	1	sc	sc	PROPN
iajs-1146	28	1	i	i	PRON
iajs-1146	28	2	vo	vo	INTJ
iajs-1146	28	3	l.22	l.22	X
iajs-1146	28	4	(	(	PUNCT
iajs-1146	28	5	4	4	NUM
iajs-1146	28	6	)	)	SYM
iajs-1146	28	7	2009	2009	NUM
iajs-1146	28	8	synthesis	synthesis	NOUN
iajs-1146	28	9	of	of	ADP
iajs-1146	28	10	1,2:5,6	1,2:5,6	NUM
iajs-1146	28	11	–	–	PUNCT
iajs-1146	28	12	di	di	NOUN
iajs-1146	28	13	-	-	ADJ
iajs-1146	28	14	o	o	NOUN
iajs-1146	28	15	-	-	NOUN
iajs-1146	28	16	isopropylidene	isopropylidene	ADJ
iajs-1146	28	17	-3	-3	NOUN
iajs-1146	28	18	-	-	PUNCT
iajs-1146	28	19	c	c	NOUN
iajs-1146	28	20	-	-	PUNCT
iajs-1146	28	21	p	p	NOUN
iajs-1146	28	22	-	-	PUNCT
iajs-1146	28	23	tolouenoyl	tolouenoyl	NOUN
iajs-1146	28	24	methyl	methyl	NOUN
iajs-1146	28	25	α	α	PROPN
iajs-1146	28	26	–	–	PUNCT
iajs-1146	28	27	d	d	NOUN
iajs-1146	28	28	-	-	PUNCT
iajs-1146	28	29	allo	allo	VERB
iajs-1146	28	30	-	-	PUNCT
iajs-1146	28	31	hexo	hexo	NOUN
iajs-1146	28	32	furanose	furanose	NOUN
iajs-1146	28	33	.	.	PUNCT
iajs-1146	29	1	(	(	PUNCT
iajs-1146	29	2	1	1	X
iajs-1146	29	3	)	)	PUNCT
iajs-1146	29	4	compund	compund	NOUN
iajs-1146	29	5	1	1	NUM
iajs-1146	29	6	was	be	AUX
iajs-1146	29	7	used	use	VERB
iajs-1146	29	8	as	as	ADP
iajs-1146	29	9	astarting	astarte	VERB
iajs-1146	29	10	material	material	NOUN
iajs-1146	29	11	,	,	PUNCT
iajs-1146	29	12	this	this	DET
iajs-1146	29	13	derivative	derivative	NOUN
iajs-1146	29	14	was	be	AUX
iajs-1146	29	15	prepared	prepare	VERB
iajs-1146	29	16	from	from	ADP
iajs-1146	29	17	the	the	DET
iajs-1146	29	18	reaction	reaction	NOUN
iajs-1146	29	19	of	of	ADP
iajs-1146	29	20	3	3	NUM
iajs-1146	29	21	-	-	NUM
iajs-1146	29	22	ulose	ulose	ADJ
iajs-1146	30	1	[	[	X
iajs-1146	30	2	14	14	NUM
iajs-1146	30	3	,	,	PUNCT
iajs-1146	30	4	15	15	NUM
iajs-1146	30	5	]	]	PUNCT
iajs-1146	30	6	with	with	ADP
iajs-1146	30	7	p	p	NOUN
iajs-1146	30	8	-	-	PUNCT
iajs-1146	30	9	methylacetophenon	methylacetophenon	NOUN
iajs-1146	30	10	according	accord	VERB
iajs-1146	30	11	to	to	ADP
iajs-1146	30	12	the	the	DET
iajs-1146	30	13	reference	reference	NOUN
iajs-1146	30	14	[	[	X
iajs-1146	30	15	11	11	NUM
iajs-1146	30	16	]	]	PUNCT
iajs-1146	30	17	.	.	PUNCT
iajs-1146	31	1	synthesis	synthesis	NOUN
iajs-1146	31	2	of	of	ADP
iajs-1146	31	3	3	3	NUM
iajs-1146	31	4	-	-	PUNCT
iajs-1146	31	5	p	p	NUM
iajs-1146	31	6	-	-	PUNCT
iajs-1146	31	7	tolouenoylelhene	tolouenoylelhene	NOUN
iajs-1146	31	8	-1/2:5	-1/2:5	NOUN
iajs-1146	31	9	,	,	PUNCT
iajs-1146	31	10	6	6	NUM
iajs-1146	31	11	-	-	PUNCT
iajs-1146	31	12	di	di	NOUN
iajs-1146	31	13	-	-	ADJ
iajs-1146	31	14	o	o	NOUN
iajs-1146	31	15	-	-	PUNCT
iajs-1146	31	16	isopropylidne	isopropylidne	ADJ
iajs-1146	31	17	-	-	PUNCT
iajs-1146	31	18	α	α	NOUN
iajs-1146	31	19	-	-	PUNCT
iajs-1146	31	20	d	d	NOUN
iajs-1146	31	21	-	-	PUNCT
iajs-1146	31	22	glucofuranose	glucofuranose	NOUN
iajs-1146	31	23	.	.	PUNCT
iajs-1146	32	1	(	(	PUNCT
iajs-1146	32	2	2	2	X
iajs-1146	32	3	)	)	PUNCT
iajs-1146	32	4	the	the	DET
iajs-1146	32	5	mixture	mixture	NOUN
iajs-1146	32	6	of	of	ADP
iajs-1146	32	7	dimethyl	dimethyl	PROPN
iajs-1146	32	8	sulphoxide	sulphoxide	NOUN
iajs-1146	32	9	(	(	PUNCT
iajs-1146	32	10	40ml	40ml	NOUN
iajs-1146	32	11	)	)	PUNCT
iajs-1146	32	12	,	,	PUNCT
iajs-1146	32	13	acetic	acetic	ADJ
iajs-1146	32	14	anhydride	anhydride	NOUN
iajs-1146	32	15	(	(	PUNCT
iajs-1146	32	16	20ml	20ml	NOUN
iajs-1146	32	17	)	)	PUNCT
iajs-1146	32	18	,	,	PUNCT
iajs-1146	32	19	compound	compound	NOUN
iajs-1146	32	20	1	1	NUM
iajs-1146	32	21	(	(	PUNCT
iajs-1146	32	22	5.0	5.0	NUM
iajs-1146	32	23	g	g	NOUN
iajs-1146	32	24	,	,	PUNCT
iajs-1146	32	25	37.26	37.26	NUM
iajs-1146	32	26	mmol	mmol	NOUN
iajs-1146	32	27	)	)	PUNCT
iajs-1146	32	28	is	be	AUX
iajs-1146	32	29	made	make	VERB
iajs-1146	32	30	in	in	ADP
iajs-1146	32	31	a	a	DET
iajs-1146	32	32	stoppered	stopper	VERB
iajs-1146	32	33	conical	conical	ADJ
iajs-1146	32	34	flask	flask	NOUN
iajs-1146	32	35	,	,	PUNCT
iajs-1146	32	36	and	and	CCONJ
iajs-1146	32	37	was	be	AUX
iajs-1146	32	38	stirred	stir	VERB
iajs-1146	32	39	at	at	ADP
iajs-1146	32	40	room	room	NOUN
iajs-1146	32	41	temperature	temperature	NOUN
iajs-1146	32	42	for	for	ADP
iajs-1146	32	43	(	(	PUNCT
iajs-1146	32	44	72h	72h	NOUN
iajs-1146	32	45	)	)	PUNCT
iajs-1146	32	46	and	and	CCONJ
iajs-1146	32	47	tlc	tlc	NOUN
iajs-1146	32	48	(	(	PUNCT
iajs-1146	32	49	benzene	benzene	NOUN
iajs-1146	32	50	:	:	PUNCT
iajs-1146	32	51	ether	ether	NOUN
iajs-1146	32	52	9:1	9:1	NUM
iajs-1146	32	53	)	)	PUNCT
iajs-1146	32	54	showed	show	VERB
iajs-1146	32	55	that	that	SCONJ
iajs-1146	32	56	the	the	DET
iajs-1146	32	57	reaction	reaction	NOUN
iajs-1146	32	58	was	be	AUX
iajs-1146	32	59	complete	complete	ADJ
iajs-1146	32	60	.the	.the	PRON
iajs-1146	32	61	mixture	mixture	NOUN
iajs-1146	32	62	was	be	AUX
iajs-1146	32	63	diluted	dilute	VERB
iajs-1146	32	64	with	with	ADP
iajs-1146	32	65	ice	ice	NOUN
iajs-1146	32	66	water	water	NOUN
iajs-1146	32	67	(	(	PUNCT
iajs-1146	32	68	50ml	50ml	NOUN
iajs-1146	32	69	)	)	PUNCT
iajs-1146	32	70	and	and	CCONJ
iajs-1146	32	71	the	the	DET
iajs-1146	32	72	brown	brown	ADJ
iajs-1146	32	73	syrup	syrup	NOUN
iajs-1146	32	74	was	be	AUX
iajs-1146	32	75	separated	separate	VERB
iajs-1146	32	76	by	by	ADP
iajs-1146	32	77	the	the	DET
iajs-1146	32	78	decantation	decantation	NOUN
iajs-1146	32	79	and	and	CCONJ
iajs-1146	32	80	the	the	DET
iajs-1146	32	81	syrup	syrup	NOUN
iajs-1146	32	82	was	be	AUX
iajs-1146	32	83	washed	wash	VERB
iajs-1146	32	84	with	with	ADP
iajs-1146	32	85	ice	ice	NOUN
iajs-1146	32	86	water	water	NOUN
iajs-1146	32	87	(	(	PUNCT
iajs-1146	32	88	3x20ml	3x20ml	NUM
iajs-1146	32	89	)	)	PUNCT
iajs-1146	32	90	,	,	PUNCT
iajs-1146	32	91	followed	follow	VERB
iajs-1146	32	92	by	by	ADP
iajs-1146	32	93	the	the	DET
iajs-1146	32	94	extraction	extraction	NOUN
iajs-1146	32	95	with	with	ADP
iajs-1146	32	96	chloroform	chloroform	NOUN
iajs-1146	32	97	.the	.the	DET
iajs-1146	32	98	organic	organic	ADJ
iajs-1146	32	99	layer	layer	NOUN
iajs-1146	32	100	was	be	AUX
iajs-1146	32	101	dried	dry	VERB
iajs-1146	32	102	and	and	CCONJ
iajs-1146	32	103	the	the	DET
iajs-1146	32	104	solvent	solvent	NOUN
iajs-1146	32	105	was	be	AUX
iajs-1146	32	106	removed	remove	VERB
iajs-1146	32	107	under	under	ADP
iajs-1146	32	108	reduced	reduce	VERB
iajs-1146	32	109	pressure	pressure	NOUN
iajs-1146	32	110	to	to	PART
iajs-1146	32	111	afford	afford	VERB
iajs-1146	32	112	a	a	DET
iajs-1146	32	113	syrup	syrup	NOUN
iajs-1146	32	114	residue	residue	NOUN
iajs-1146	32	115	of	of	ADP
iajs-1146	32	116	derivative	derivative	ADJ
iajs-1146	32	117	2	2	NUM
iajs-1146	32	118	.	.	PUNCT
iajs-1146	32	119	synthesis	synthesis	NOUN
iajs-1146	32	120	of	of	ADP
iajs-1146	32	121	1-	1-	PROPN
iajs-1146	32	122	[	[	X
iajs-1146	32	123	(	(	PUNCT
iajs-1146	32	124	/1,/2	/1,/2	PROPN
iajs-1146	32	125	–	–	PUNCT
iajs-1146	32	126	o	o	NOUN
iajs-1146	32	127	-	-	NOUN
iajs-1146	32	128	isopropylidene	isopropylidene	ADJ
iajs-1146	32	129	)	)	PUNCT
iajs-1146	32	130	ethyl	ethyl	PROPN
iajs-1146	33	1	]	]	PUNCT
iajs-1146	33	2	-3,4	-3,4	NUM
iajs-1146	33	3	-	-	PUNCT
iajs-1146	33	4	o	o	NOUN
iajs-1146	33	5	-	-	NOUN
iajs-1146	33	6	isopropylidene	isopropylidene	ADJ
iajs-1146	33	7	-8-(/4	-8-(/4	NOUN
iajs-1146	33	8	-	-	PUNCT
iajs-1146	33	9	tolyl)-2oxa-6	tolyl)-2oxa-6	PROPN
iajs-1146	33	10	-	-	PUNCT
iajs-1146	33	11	aza	aza	NOUN
iajs-1146	33	12	phenyl	phenyl	NOUN
iajs-1146	33	13	spiro[4,4	spiro[4,4	PROPN
iajs-1146	33	14	]	]	X
iajs-1146	33	15	nona	nona	PROPN
iajs-1146	33	16	-7	-7	NOUN
iajs-1146	33	17	-	-	NOUN
iajs-1146	33	18	imine	imine	NOUN
iajs-1146	33	19	.	.	PUNCT
iajs-1146	34	1	(	(	PUNCT
iajs-1146	34	2	3	3	X
iajs-1146	34	3	)	)	PUNCT
iajs-1146	34	4	a	a	DET
iajs-1146	34	5	mixture	mixture	NOUN
iajs-1146	34	6	of	of	ADP
iajs-1146	34	7	2	2	NUM
iajs-1146	34	8	(	(	PUNCT
iajs-1146	34	9	5.0	5.0	NUM
iajs-1146	34	10	g	g	NOUN
iajs-1146	34	11	,	,	PUNCT
iajs-1146	34	12	13.36	13.36	NUM
iajs-1146	34	13	mmol	mmol	NOUN
iajs-1146	34	14	)	)	PUNCT
iajs-1146	34	15	,	,	PUNCT
iajs-1146	34	16	phenyl	phenyl	NOUN
iajs-1146	34	17	hydrazine	hydrazine	NOUN
iajs-1146	34	18	(	(	PUNCT
iajs-1146	34	19	1.4	1.4	NUM
iajs-1146	34	20	ml	ml	NOUN
iajs-1146	34	21	)	)	PUNCT
iajs-1146	34	22	and	and	CCONJ
iajs-1146	34	23	(	(	PUNCT
iajs-1146	34	24	5	5	NUM
iajs-1146	34	25	-	-	SYM
iajs-1146	34	26	10	10	NUM
iajs-1146	34	27	drops	drop	NOUN
iajs-1146	34	28	)	)	PUNCT
iajs-1146	34	29	of	of	ADP
iajs-1146	34	30	diethylamine	diethylamine	NOUN
iajs-1146	34	31	dissolved	dissolve	VERB
iajs-1146	34	32	in	in	ADP
iajs-1146	34	33	(	(	PUNCT
iajs-1146	34	34	100ml	100ml	NOUN
iajs-1146	34	35	)	)	PUNCT
iajs-1146	34	36	absolute	absolute	ADJ
iajs-1146	34	37	ethanol	ethanol	NOUN
iajs-1146	34	38	,	,	PUNCT
iajs-1146	34	39	was	be	AUX
iajs-1146	34	40	refluxed	refluxe	VERB
iajs-1146	34	41	for	for	ADP
iajs-1146	34	42	(	(	PUNCT
iajs-1146	34	43	48h	48h	NOUN
iajs-1146	34	44	)	)	PUNCT
iajs-1146	34	45	.	.	PUNCT
iajs-1146	35	1	the	the	DET
iajs-1146	35	2	solvent	solvent	NOUN
iajs-1146	35	3	was	be	AUX
iajs-1146	35	4	evaporated	evaporate	VERB
iajs-1146	35	5	and	and	CCONJ
iajs-1146	35	6	the	the	DET
iajs-1146	35	7	residue	residue	NOUN
iajs-1146	35	8	was	be	AUX
iajs-1146	35	9	diluted	dilute	VERB
iajs-1146	35	10	with	with	ADP
iajs-1146	35	11	water	water	NOUN
iajs-1146	35	12	and	and	CCONJ
iajs-1146	35	13	extracted	extract	VERB
iajs-1146	35	14	with	with	ADP
iajs-1146	35	15	chloroform	chloroform	NOUN
iajs-1146	35	16	(	(	PUNCT
iajs-1146	35	17	3x30ml	3x30ml	NUM
iajs-1146	35	18	)	)	PUNCT
iajs-1146	35	19	.	.	PUNCT
iajs-1146	36	1	the	the	DET
iajs-1146	36	2	organic	organic	ADJ
iajs-1146	36	3	layer	layer	NOUN
iajs-1146	36	4	was	be	AUX
iajs-1146	36	5	dried	dry	VERB
iajs-1146	36	6	over	over	ADP
iajs-1146	36	7	magnesium	magnesium	NOUN
iajs-1146	36	8	sulphate	sulphate	NOUN
iajs-1146	36	9	and	and	CCONJ
iajs-1146	36	10	the	the	DET
iajs-1146	36	11	solvent	solvent	NOUN
iajs-1146	36	12	was	be	AUX
iajs-1146	36	13	removed	remove	VERB
iajs-1146	36	14	to	to	PART
iajs-1146	36	15	give	give	VERB
iajs-1146	36	16	3	3	NUM
iajs-1146	36	17	as	as	ADP
iajs-1146	36	18	asyrup	asyrup	NOUN
iajs-1146	36	19	.	.	PUNCT
iajs-1146	37	1	synthesis	synthesis	NOUN
iajs-1146	37	2	of	of	ADP
iajs-1146	37	3	1-	1-	PROPN
iajs-1146	37	4	[	[	PUNCT
iajs-1146	37	5	/	/	SYM
iajs-1146	37	6	1	1	NUM
iajs-1146	37	7	,	,	PUNCT
iajs-1146	37	8	/	/	SYM
iajs-1146	37	9	2	2	NUM
iajs-1146	37	10	–	–	PUNCT
iajs-1146	37	11	dihydroxy	dihydroxy	ADJ
iajs-1146	37	12	ethyl	ethyl	NOUN
iajs-1146	37	13	]	]	PUNCT
iajs-1146	37	14	-3,4,-o	-3,4,-o	PROPN
iajs-1146	37	15	-	-	PUNCT
iajs-1146	37	16	isopropylidene	isopropylidene	NOUN
iajs-1146	37	17	-8	-8	NOUN
iajs-1146	37	18	(	(	PUNCT
iajs-1146	37	19	/	/	SYM
iajs-1146	37	20	4	4	NUM
iajs-1146	37	21	-	-	PUNCT
iajs-1146	37	22	tolyl	tolyl	ADJ
iajs-1146	37	23	)	)	PUNCT
iajs-1146	37	24	-2	-2	NUM
iajs-1146	37	25	-	-	PUNCT
iajs-1146	37	26	oxa-6	oxa-6	NOUN
iajs-1146	37	27	-	-	PUNCT
iajs-1146	37	28	aza	aza	NOUN
iajs-1146	37	29	phenyl	phenyl	NOUN
iajs-1146	37	30	spiro	spiro	NOUN
iajs-1146	38	1	[	[	X
iajs-1146	38	2	4,4	4,4	X
iajs-1146	38	3	]	]	X
iajs-1146	38	4	nona	nona	NOUN
iajs-1146	38	5	-7	-7	NOUN
iajs-1146	38	6	-	-	NOUN
iajs-1146	38	7	imine	imine	NOUN
iajs-1146	38	8	.	.	PUNCT
iajs-1146	39	1	(	(	PUNCT
iajs-1146	39	2	4	4	X
iajs-1146	39	3	)	)	PUNCT
iajs-1146	39	4	a	a	DET
iajs-1146	39	5	solution	solution	NOUN
iajs-1146	39	6	of	of	ADP
iajs-1146	39	7	3	3	NUM
iajs-1146	39	8	(	(	PUNCT
iajs-1146	39	9	5.0	5.0	NUM
iajs-1146	39	10	g	g	NOUN
iajs-1146	39	11	,	,	PUNCT
iajs-1146	39	12	10.77	10.77	NUM
iajs-1146	39	13	mmol	mmol	NOUN
iajs-1146	39	14	)	)	PUNCT
iajs-1146	39	15	in	in	ADP
iajs-1146	39	16	(	(	PUNCT
iajs-1146	39	17	66	66	NUM
iajs-1146	39	18	%	%	NOUN
iajs-1146	39	19	)	)	PUNCT
iajs-1146	39	20	acetic	acetic	ADJ
iajs-1146	39	21	acid	acid	NOUN
iajs-1146	39	22	(	(	PUNCT
iajs-1146	39	23	20ml	20ml	NOUN
iajs-1146	39	24	)	)	PUNCT
iajs-1146	39	25	was	be	AUX
iajs-1146	39	26	stirred	stir	VERB
iajs-1146	39	27	for	for	ADP
iajs-1146	39	28	(	(	PUNCT
iajs-1146	39	29	24h	24h	NOUN
iajs-1146	39	30	)	)	PUNCT
iajs-1146	39	31	at	at	ADP
iajs-1146	39	32	room	room	NOUN
iajs-1146	39	33	temperature	temperature	NOUN
iajs-1146	39	34	.	.	PUNCT
iajs-1146	40	1	the	the	DET
iajs-1146	40	2	solution	solution	NOUN
iajs-1146	40	3	was	be	AUX
iajs-1146	40	4	evaporated	evaporate	VERB
iajs-1146	40	5	under	under	ADP
iajs-1146	40	6	reduced	reduce	VERB
iajs-1146	40	7	pressure	pressure	NOUN
iajs-1146	40	8	and	and	CCONJ
iajs-1146	40	9	the	the	DET
iajs-1146	40	10	resulting	result	VERB
iajs-1146	40	11	residue	residue	NOUN
iajs-1146	40	12	was	be	AUX
iajs-1146	40	13	re	re	VERB
iajs-1146	40	14	-	-	VERB
iajs-1146	40	15	evaporated	evaporate	VERB
iajs-1146	40	16	with	with	ADP
iajs-1146	40	17	toluene	toluene	NOUN
iajs-1146	40	18	twice	twice	ADV
iajs-1146	40	19	(	(	PUNCT
iajs-1146	40	20	20ml	20ml	NOUN
iajs-1146	40	21	)	)	PUNCT
iajs-1146	40	22	to	to	PART
iajs-1146	40	23	give	give	VERB
iajs-1146	40	24	4	4	NUM
iajs-1146	40	25	as	as	ADP
iajs-1146	40	26	syrup	syrup	NOUN
iajs-1146	40	27	.	.	PUNCT
iajs-1146	41	1	synthesis	synthesis	NOUN
iajs-1146	41	2	of	of	ADP
iajs-1146	41	3	1-	1-	PROPN
iajs-1146	41	4	[	[	PUNCT
iajs-1146	41	5	/	/	SYM
iajs-1146	41	6	1	1	NUM
iajs-1146	41	7	-	-	PUNCT
iajs-1146	41	8	hyroxy	hyroxy	NOUN
iajs-1146	41	9	methyl	methyl	NOUN
iajs-1146	41	10	]	]	X
iajs-1146	41	11	-3	-3	PUNCT
iajs-1146	41	12	,	,	PUNCT
iajs-1146	41	13	4	4	NUM
iajs-1146	41	14	-	-	PUNCT
iajs-1146	41	15	o	o	NOUN
iajs-1146	41	16	-	-	NOUN
iajs-1146	41	17	isopropylidene	isopropylidene	ADJ
iajs-1146	41	18	-8-	-8-	NOUN
iajs-1146	41	19	(	(	PUNCT
iajs-1146	41	20	/	/	SYM
iajs-1146	41	21	4	4	NUM
iajs-1146	41	22	-	-	PUNCT
iajs-1146	41	23	tolyl	tolyl	ADJ
iajs-1146	41	24	)	)	PUNCT
iajs-1146	41	25	–	–	PUNCT
iajs-1146	41	26	2	2	NUM
iajs-1146	41	27	-	-	PUNCT
iajs-1146	41	28	oxa	oxa	NOUN
iajs-1146	41	29	-6	-6	PROPN
iajs-1146	41	30	-	-	PUNCT
iajs-1146	41	31	aza	aza	NOUN
iajs-1146	41	32	phenyl	phenyl	NOUN
iajs-1146	41	33	spiro	spiro	NOUN
iajs-1146	42	1	[	[	X
iajs-1146	42	2	4	4	NUM
iajs-1146	42	3	,	,	PUNCT
iajs-1146	42	4	4	4	NUM
iajs-1146	42	5	]	]	PUNCT
iajs-1146	42	6	nona-7	nona-7	PROPN
iajs-1146	42	7	-	-	PUNCT
iajs-1146	42	8	imine	imine	NOUN
iajs-1146	42	9	.	.	PUNCT
iajs-1146	43	1	(	(	PUNCT
iajs-1146	43	2	5	5	X
iajs-1146	43	3	)	)	PUNCT
iajs-1146	43	4	was	be	AUX
iajs-1146	43	5	added	add	VERB
iajs-1146	43	6	to	to	ADP
iajs-1146	43	7	a	a	DET
iajs-1146	43	8	well	well	ADV
iajs-1146	43	9	stirred	stir	VERB
iajs-1146	43	10	solution	solution	NOUN
iajs-1146	43	11	of	of	ADP
iajs-1146	43	12	4	4	NUM
iajs-1146	43	13	(	(	PUNCT
iajs-1146	43	14	5.0	5.0	NUM
iajs-1146	43	15	g	g	NOUN
iajs-1146	43	16	,	,	PUNCT
iajs-1146	43	17	11.79	11.79	NUM
iajs-1146	43	18	mmol	mmol	NOUN
iajs-1146	43	19	)	)	PUNCT
iajs-1146	43	20	in	in	ADP
iajs-1146	43	21	ethanol	ethanol	NOUN
iajs-1146	43	22	(	(	PUNCT
iajs-1146	43	23	40ml	40ml	NOUN
iajs-1146	43	24	)	)	PUNCT
iajs-1146	43	25	.	.	PUNCT
iajs-1146	44	1	a	a	DET
iajs-1146	44	2	saturated	saturate	VERB
iajs-1146	44	3	solution	solution	NOUN
iajs-1146	44	4	of	of	ADP
iajs-1146	44	5	sodium	sodium	NOUN
iajs-1146	44	6	hydrogen	hydrogen	NOUN
iajs-1146	44	7	carbonate	carbonate	NOUN
iajs-1146	44	8	(	(	PUNCT
iajs-1146	44	9	12ml	12ml	NOUN
iajs-1146	44	10	)	)	PUNCT
iajs-1146	44	11	followed	follow	VERB
iajs-1146	44	12	by	by	ADP
iajs-1146	44	13	a	a	DET
iajs-1146	44	14	solution	solution	NOUN
iajs-1146	44	15	of	of	ADP
iajs-1146	44	16	sodium	sodium	NOUN
iajs-1146	44	17	periodate	periodate	NOUN
iajs-1146	44	18	(	(	PUNCT
iajs-1146	44	19	2.5	2.5	NUM
iajs-1146	44	20	g	g	NOUN
iajs-1146	44	21	,	,	PUNCT
iajs-1146	44	22	10.75	10.75	NUM
iajs-1146	44	23	mmol	mmol	NOUN
iajs-1146	44	24	)	)	PUNCT
iajs-1146	44	25	in	in	ADP
iajs-1146	44	26	(	(	PUNCT
iajs-1146	44	27	50ml	50ml	ADJ
iajs-1146	44	28	)	)	PUNCT
iajs-1146	44	29	water	water	NOUN
iajs-1146	44	30	.	.	PUNCT
iajs-1146	45	1	the	the	DET
iajs-1146	45	2	mixture	mixture	NOUN
iajs-1146	45	3	was	be	AUX
iajs-1146	45	4	stirred	stir	VERB
iajs-1146	45	5	for	for	ADP
iajs-1146	45	6	(	(	PUNCT
iajs-1146	45	7	1h	1h	NOUN
iajs-1146	45	8	)	)	PUNCT
iajs-1146	45	9	at	at	ADP
iajs-1146	45	10	room	room	NOUN
iajs-1146	45	11	temperature	temperature	NOUN
iajs-1146	45	12	.	.	PUNCT
iajs-1146	46	1	ethylene	ethylene	NOUN
iajs-1146	46	2	glycol	glycol	NOUN
iajs-1146	46	3	(	(	PUNCT
iajs-1146	46	4	2ml	2ml	NOUN
iajs-1146	46	5	)	)	PUNCT
iajs-1146	46	6	was	be	AUX
iajs-1146	46	7	added	add	VERB
iajs-1146	46	8	,	,	PUNCT
iajs-1146	46	9	and	and	CCONJ
iajs-1146	46	10	the	the	DET
iajs-1146	46	11	solution	solution	NOUN
iajs-1146	46	12	was	be	AUX
iajs-1146	46	13	further	far	ADV
iajs-1146	46	14	stirred	stir	VERB
iajs-1146	46	15	for	for	ADP
iajs-1146	46	16	(	(	PUNCT
iajs-1146	46	17	5	5	NUM
iajs-1146	46	18	)	)	PUNCT
iajs-1146	46	19	minutes	minute	NOUN
iajs-1146	46	20	.sodium	.sodium	ADP
iajs-1146	46	21	borohydride	borohydride	NOUN
iajs-1146	46	22	(	(	PUNCT
iajs-1146	46	23	0.44	0.44	NUM
iajs-1146	46	24	g	g	NOUN
iajs-1146	46	25	,	,	PUNCT
iajs-1146	46	26	11.62	11.62	NUM
iajs-1146	46	27	mmol	mmol	NOUN
iajs-1146	46	28	)	)	PUNCT
iajs-1146	46	29	was	be	AUX
iajs-1146	46	30	added	add	VERB
iajs-1146	46	31	to	to	ADP
iajs-1146	46	32	the	the	DET
iajs-1146	46	33	resulting	result	VERB
iajs-1146	46	34	aldehydo	aldehydo	ADJ
iajs-1146	46	35	sugar	sugar	NOUN
iajs-1146	46	36	with	with	ADP
iajs-1146	46	37	continuous	continuous	ADJ
iajs-1146	46	38	stirring	stirring	NOUN
iajs-1146	46	39	for	for	ADP
iajs-1146	46	40	(	(	PUNCT
iajs-1146	46	41	1h	1h	NUM
iajs-1146	46	42	)	)	PUNCT
iajs-1146	46	43	.	.	PUNCT
iajs-1146	47	1	the	the	DET
iajs-1146	47	2	reaction	reaction	NOUN
iajs-1146	47	3	mixture	mixture	NOUN
iajs-1146	47	4	was	be	AUX
iajs-1146	47	5	filtrated	filtrate	VERB
iajs-1146	47	6	and	and	CCONJ
iajs-1146	47	7	extracted	extract	VERB
iajs-1146	47	8	with	with	ADP
iajs-1146	47	9	chloroform	chloroform	NOUN
iajs-1146	47	10	.the	.the	DET
iajs-1146	47	11	organic	organic	ADJ
iajs-1146	47	12	layer	layer	NOUN
iajs-1146	47	13	was	be	AUX
iajs-1146	47	14	dried	dry	VERB
iajs-1146	47	15	and	and	CCONJ
iajs-1146	47	16	evaporated	evaporate	VERB
iajs-1146	47	17	to	to	PART
iajs-1146	47	18	give	give	VERB
iajs-1146	47	19	5	5	NUM
iajs-1146	47	20	as	as	ADP
iajs-1146	47	21	syrup	syrup	NOUN
iajs-1146	47	22	.	.	PUNCT
iajs-1146	48	1	synthesis	synthesis	NOUN
iajs-1146	48	2	of	of	ADP
iajs-1146	48	3	1-	1-	PROPN
iajs-1146	48	4	[	[	PUNCT
iajs-1146	48	5	/1	/1	NOUN
iajs-1146	48	6	–	–	PUNCT
iajs-1146	48	7	benzoyl	benzoyl	NOUN
iajs-1146	48	8	methyl	methyl	NOUN
iajs-1146	48	9	]	]	PUNCT
iajs-1146	48	10	-3	-3	PUNCT
iajs-1146	48	11	,	,	PUNCT
iajs-1146	48	12	4	4	NUM
iajs-1146	48	13	-	-	PUNCT
iajs-1146	48	14	oisopropylidine	oisopropylidine	NOUN
iajs-1146	48	15	-8-(/4	-8-(/4	NOUN
iajs-1146	48	16	-	-	PUNCT
iajs-1146	48	17	tolyl	tolyl	ADJ
iajs-1146	48	18	)	)	PUNCT
iajs-1146	48	19	-2	-2	NOUN
iajs-1146	48	20	-	-	PUNCT
iajs-1146	48	21	oxa	oxa	NOUN
iajs-1146	48	22	-6	-6	PROPN
iajs-1146	48	23	-	-	PUNCT
iajs-1146	48	24	aza	aza	NOUN
iajs-1146	48	25	phenyl	phenyl	NOUN
iajs-1146	48	26	spiro	spiro	NOUN
iajs-1146	48	27	[	[	X
iajs-1146	48	28	4	4	NUM
iajs-1146	48	29	,	,	PUNCT
iajs-1146	48	30	4	4	NUM
iajs-1146	48	31	]	]	X
iajs-1146	48	32	nona	nona	NOUN
iajs-1146	48	33	-7	-7	NOUN
iajs-1146	48	34	-	-	NOUN
iajs-1146	48	35	imine	imine	NOUN
iajs-1146	48	36	.	.	PUNCT
iajs-1146	49	1	(	(	PUNCT
iajs-1146	49	2	6	6	X
iajs-1146	49	3	)	)	PUNCT
iajs-1146	49	4	compound	compound	NOUN
iajs-1146	49	5	5	5	NUM
iajs-1146	49	6	(	(	PUNCT
iajs-1146	49	7	4.0g,10.15	4.0g,10.15	NUM
iajs-1146	49	8	mmol	mmol	NOUN
iajs-1146	49	9	)	)	PUNCT
iajs-1146	49	10	in	in	ADP
iajs-1146	49	11	anhydrous	anhydrous	ADJ
iajs-1146	49	12	benzene	benzene	NOUN
iajs-1146	49	13	(	(	PUNCT
iajs-1146	49	14	60	60	NUM
iajs-1146	49	15	ml)containing	ml)containe	VERB
iajs-1146	49	16	pyridine	pyridine	NOUN
iajs-1146	49	17	(	(	PUNCT
iajs-1146	49	18	6ml	6ml	NOUN
iajs-1146	49	19	)	)	PUNCT
iajs-1146	49	20	was	be	AUX
iajs-1146	49	21	benzoylated	benzoylate	VERB
iajs-1146	49	22	with	with	ADP
iajs-1146	49	23	benzoyl	benzoyl	PROPN
iajs-1146	49	24	chloride	chloride	NOUN
iajs-1146	49	25	(	(	PUNCT
iajs-1146	49	26	1.42	1.42	NUM
iajs-1146	49	27	ml,10.10	ml,10.10	DET
iajs-1146	49	28	mmol).after	mmol).after	NOUN
iajs-1146	49	29	stirring	stirring	NOUN
iajs-1146	49	30	for	for	ADP
iajs-1146	49	31	(	(	PUNCT
iajs-1146	49	32	24h	24h	NOUN
iajs-1146	49	33	)	)	PUNCT
iajs-1146	49	34	at	at	ADP
iajs-1146	49	35	room	room	NOUN
iajs-1146	49	36	temperature	temperature	NOUN
iajs-1146	49	37	,	,	PUNCT
iajs-1146	49	38	the	the	DET
iajs-1146	49	39	mixture	mixture	NOUN
iajs-1146	49	40	was	be	AUX
iajs-1146	49	41	poured	pour	VERB
iajs-1146	49	42	into	into	ADP
iajs-1146	49	43	ice	ice	NOUN
iajs-1146	49	44	water	water	NOUN
iajs-1146	49	45	(	(	PUNCT
iajs-1146	49	46	100ml	100ml	NOUN
iajs-1146	49	47	)	)	PUNCT
iajs-1146	49	48	.the	.the	X
iajs-1146	49	49	organic	organic	ADJ
iajs-1146	49	50	layer	layer	NOUN
iajs-1146	49	51	was	be	AUX
iajs-1146	49	52	separated	separate	VERB
iajs-1146	49	53	and	and	CCONJ
iajs-1146	49	54	washed	wash	VERB
iajs-1146	49	55	with	with	ADP
iajs-1146	49	56	water	water	NOUN
iajs-1146	49	57	(	(	PUNCT
iajs-1146	49	58	3x30ml	3x30ml	NUM
iajs-1146	49	59	)	)	PUNCT
iajs-1146	49	60	,	,	PUNCT
iajs-1146	49	61	dried	dry	VERB
iajs-1146	49	62	and	and	CCONJ
iajs-1146	49	63	evaporated	evaporate	VERB
iajs-1146	49	64	to	to	PART
iajs-1146	49	65	give	give	VERB
iajs-1146	49	66	6	6	NUM
iajs-1146	49	67	as	as	ADP
iajs-1146	49	68	syrup	syrup	NOUN
iajs-1146	49	69	.	.	PUNCT
iajs-1146	50	1	synthesis	synthesis	NOUN
iajs-1146	50	2	of	of	ADP
iajs-1146	50	3	1-	1-	PROPN
iajs-1146	50	4	[	[	PUNCT
iajs-1146	50	5	/	/	SYM
iajs-1146	50	6	1	1	NUM
iajs-1146	50	7	-	-	PUNCT
iajs-1146	50	8	benzoyl	benzoyl	VERB
iajs-1146	50	9	methyl]-8	methyl]-8	NOUN
iajs-1146	50	10	(	(	PUNCT
iajs-1146	50	11	/	/	SYM
iajs-1146	50	12	4	4	NUM
iajs-1146	50	13	-	-	PUNCT
iajs-1146	50	14	tolyl)-2	tolyl)-2	NOUN
iajs-1146	50	15	-	-	PUNCT
iajs-1146	50	16	oxa-6	oxa-6	NOUN
iajs-1146	50	17	-	-	PUNCT
iajs-1146	50	18	aza	aza	NOUN
iajs-1146	50	19	phenyl	phenyl	NOUN
iajs-1146	50	20	spiro	spiro	NOUN
iajs-1146	50	21	[	[	X
iajs-1146	50	22	4	4	NUM
iajs-1146	50	23	,	,	PUNCT
iajs-1146	50	24	4	4	NUM
iajs-1146	50	25	]	]	X
iajs-1146	50	26	nona	nona	PROPN
iajs-1146	50	27	-7imino	-7imino	PROPN
iajs-1146	50	28	-3	-3	PUNCT
iajs-1146	50	29	,	,	PUNCT
iajs-1146	50	30	4	4	NUM
iajs-1146	50	31	-	-	PUNCT
iajs-1146	50	32	di	di	NOUN
iajs-1146	50	33	-	-	ADJ
iajs-1146	50	34	o	o	NOUN
iajs-1146	50	35	-	-	NOUN
iajs-1146	50	36	triflouro	triflouro	NOUN
iajs-1146	50	37	acetate	acetate	NOUN
iajs-1146	50	38	.	.	PUNCT
iajs-1146	51	1	(	(	PUNCT
iajs-1146	51	2	7	7	X
iajs-1146	51	3	)	)	PUNCT
iajs-1146	51	4	water	water	NOUN
iajs-1146	51	5	(	(	PUNCT
iajs-1146	51	6	2ml	2ml	NOUN
iajs-1146	51	7	)	)	PUNCT
iajs-1146	51	8	and	and	CCONJ
iajs-1146	51	9	trifluoroacetic	trifluoroacetic	ADJ
iajs-1146	51	10	acid	acid	NOUN
iajs-1146	51	11	(	(	PUNCT
iajs-1146	51	12	20ml	20ml	NOUN
iajs-1146	51	13	)	)	PUNCT
iajs-1146	51	14	was	be	AUX
iajs-1146	51	15	added	add	VERB
iajs-1146	51	16	to	to	ADP
iajs-1146	51	17	a	a	DET
iajs-1146	51	18	solution	solution	NOUN
iajs-1146	51	19	of	of	ADP
iajs-1146	51	20	6(5.0g,10.04mmol	6(5.0g,10.04mmol	NOUN
iajs-1146	51	21	)	)	PUNCT
iajs-1146	51	22	in	in	ADP
iajs-1146	51	23	acetic	acetic	ADJ
iajs-1146	51	24	acid	acid	NOUN
iajs-1146	51	25	(	(	PUNCT
iajs-1146	51	26	20ml	20ml	NOUN
iajs-1146	51	27	)	)	PUNCT
iajs-1146	51	28	,	,	PUNCT
iajs-1146	51	29	.the	.the	DET
iajs-1146	51	30	resulting	result	VERB
iajs-1146	51	31	mixture	mixture	NOUN
iajs-1146	51	32	was	be	AUX
iajs-1146	51	33	stirred	stir	VERB
iajs-1146	51	34	for	for	ADP
iajs-1146	51	35	(	(	PUNCT
iajs-1146	51	36	5h	5h	NOUN
iajs-1146	51	37	)	)	PUNCT
iajs-1146	51	38	at	at	ADP
iajs-1146	51	39	room	room	NOUN
iajs-1146	51	40	temperature	temperature	NOUN
iajs-1146	51	41	.the	.the	PRON
iajs-1146	52	1	reaction	reaction	NOUN
iajs-1146	52	2	mixture	mixture	NOUN
iajs-1146	52	3	was	be	AUX
iajs-1146	52	4	then	then	ADV
iajs-1146	52	5	neutralized	neutralize	VERB
iajs-1146	52	6	with	with	ADP
iajs-1146	52	7	solid	solid	ADJ
iajs-1146	52	8	sodium	sodium	NOUN
iajs-1146	52	9	hydrogen	hydrogen	NOUN
iajs-1146	52	10	carbonate	carbonate	NOUN
iajs-1146	52	11	and	and	CCONJ
iajs-1146	52	12	extracted	extract	VERB
iajs-1146	52	13	with	with	ADP
iajs-1146	52	14	dichloromethane	dichloromethane	NOUN
iajs-1146	52	15	(	(	PUNCT
iajs-1146	52	16	2x100ml).the	2x100ml).the	DET
iajs-1146	52	17	combined	combine	VERB
iajs-1146	52	18	extracts	extract	NOUN
iajs-1146	52	19	were	be	AUX
iajs-1146	52	20	dried	dry	VERB
iajs-1146	52	21	and	and	CCONJ
iajs-1146	52	22	the	the	DET
iajs-1146	52	23	solvent	solvent	NOUN
iajs-1146	52	24	was	be	AUX
iajs-1146	52	25	removed	remove	VERB
iajs-1146	52	26	to	to	PART
iajs-1146	52	27	give	give	VERB
iajs-1146	52	28	a	a	DET
iajs-1146	52	29	syrup	syrup	NOUN
iajs-1146	52	30	.this	.this	PRON
iajs-1146	52	31	syrup	syrup	NOUN
iajs-1146	52	32	was	be	AUX
iajs-1146	52	33	immediately	immediately	ADV
iajs-1146	52	34	treated	treat	VERB
iajs-1146	52	35	with	with	ADP
iajs-1146	52	36	trifluoroacetic	trifluoroacetic	ADJ
iajs-1146	52	37	anhydride	anhydride	NOUN
iajs-1146	52	38	(	(	PUNCT
iajs-1146	52	39	4ml	4ml	NOUN
iajs-1146	52	40	)	)	PUNCT
iajs-1146	52	41	in	in	ADP
iajs-1146	52	42	a	a	DET
iajs-1146	52	43	mixture	mixture	NOUN
iajs-1146	52	44	of	of	ADP
iajs-1146	52	45	anhydrous	anhydrous	ADJ
iajs-1146	52	46	benzene	benzene	NOUN
iajs-1146	52	47	(	(	PUNCT
iajs-1146	52	48	40ml	40ml	NOUN
iajs-1146	52	49	)	)	PUNCT
iajs-1146	52	50	and	and	CCONJ
iajs-1146	52	51	anhydrous	anhydrous	ADJ
iajs-1146	52	52	pyridine	pyridine	NOUN
iajs-1146	52	53	(	(	PUNCT
iajs-1146	52	54	8ml	8ml	NOUN
iajs-1146	52	55	)	)	PUNCT
iajs-1146	52	56	with	with	ADP
iajs-1146	52	57	stirring	stir	VERB
iajs-1146	52	58	for	for	ADP
iajs-1146	52	59	(	(	PUNCT
iajs-1146	52	60	24h	24h	NOUN
iajs-1146	52	61	)	)	PUNCT
iajs-1146	52	62	at	at	ADP
iajs-1146	52	63	room	room	NOUN
iajs-1146	52	64	temperature	temperature	NOUN
iajs-1146	52	65	.ice	.ice	PROPN
iajs-1146	52	66	water	water	PROPN
iajs-1146	52	67	was	be	AUX
iajs-1146	52	68	added	add	VERB
iajs-1146	52	69	to	to	ADP
iajs-1146	52	70	the	the	DET
iajs-1146	52	71	mixture	mixture	NOUN
iajs-1146	52	72	and	and	CCONJ
iajs-1146	52	73	the	the	DET
iajs-1146	52	74	organic	organic	ADJ
iajs-1146	52	75	layer	layer	NOUN
iajs-1146	52	76	was	be	AUX
iajs-1146	52	77	separated	separate	VERB
iajs-1146	52	78	,	,	PUNCT
iajs-1146	52	79	dried	dry	VERB
iajs-1146	52	80	and	and	CCONJ
iajs-1146	52	81	concentrated	concentrate	VERB
iajs-1146	52	82	under	under	ADP
iajs-1146	52	83	reduced	reduce	VERB
iajs-1146	52	84	pressure	pressure	NOUN
iajs-1146	52	85	.traces	.trace	NOUN
iajs-1146	52	86	of	of	ADP
iajs-1146	52	87	pyridine	pyridine	NOUN
iajs-1146	52	88	were	be	AUX
iajs-1146	52	89	removed	remove	VERB
iajs-1146	52	90	by	by	ADP
iajs-1146	52	91	co	co	NOUN
iajs-1146	52	92	-evaporation	-evaporation	NOUN
iajs-1146	52	93	with	with	ADP
iajs-1146	52	94	dry	dry	ADJ
iajs-1146	52	95	toluene	toluene	NOUN
iajs-1146	52	96	(	(	PUNCT
iajs-1146	52	97	2x30	2x30	NUM
iajs-1146	52	98	ml	ml	NOUN
iajs-1146	52	99	)	)	PUNCT
iajs-1146	52	100	to	to	PART
iajs-1146	52	101	give	give	VERB
iajs-1146	52	102	7	7	NUM
iajs-1146	52	103	as	as	ADP
iajs-1146	52	104	syrup	syrup	NOUN
iajs-1146	52	105	.	.	PUNCT
iajs-1146	53	1	synthesis	synthesis	NOUN
iajs-1146	53	2	of	of	ADP
iajs-1146	53	3	7	7	NUM
iajs-1146	53	4	[	[	PUNCT
iajs-1146	53	5	/1	/1	NOUN
iajs-1146	53	6	-	-	PUNCT
iajs-1146	53	7	benzoyl	benzoyl	NOUN
iajs-1146	53	8	methyl	methyl	NOUN
iajs-1146	53	9	]	]	X
iajs-1146	53	10	-/4	-/4	ADJ
iajs-1146	53	11	-	-	PUNCT
iajs-1146	53	12	o	o	NOUN
iajs-1146	53	13	-	-	NOUN
iajs-1146	53	14	trifloouro	trifloouro	NOUN
iajs-1146	53	15	acetyl	acetyl	NOUN
iajs-1146	53	16	-/8-(4	-/8-(4	NOUN
iajs-1146	53	17	-	-	PUNCT
iajs-1146	53	18	tolyl	tolyl	ADJ
iajs-1146	53	19	)	)	PUNCT
iajs-1146	53	20	-/2	-/2	ADJ
iajs-1146	53	21	-	-	PUNCT
iajs-1146	53	22	oxa-/6	oxa-/6	VERB
iajs-1146	53	23	-	-	PUNCT
iajs-1146	53	24	aza	aza	NOUN
iajs-1146	53	25	phenyl	phenyl	NOUN
iajs-1146	53	26	spiro	spiro	NOUN
iajs-1146	54	1	[	[	X
iajs-1146	54	2	4	4	NUM
iajs-1146	54	3	,	,	PUNCT
iajs-1146	54	4	4	4	NUM
iajs-1146	54	5	]	]	SYM
iajs-1146	54	6	nona-/7imino	nona-/7imino	PROPN
iajs-1146	54	7	]	]	PUNCT
iajs-1146	54	8	theophylline	theophylline	NOUN
iajs-1146	54	9	.	.	PUNCT
iajs-1146	55	1	(	(	PUNCT
iajs-1146	55	2	8	8	X
iajs-1146	55	3	)	)	PUNCT
iajs-1146	55	4	ibn	ibn	PROPN
iajs-1146	55	5	alhaitham	alhaitham	NOUN
iajs-1146	55	6	j.	j.	PROPN
iajs-1146	56	1	fo	fo	ADP
iajs-1146	56	2	r	r	NOUN
iajs-1146	56	3	pure	pure	ADJ
iajs-1146	56	4	&	&	CCONJ
iajs-1146	56	5	appl	appl	PROPN
iajs-1146	56	6	.	.	PUNCT
iajs-1146	57	1	sc	sc	PROPN
iajs-1146	58	1	i	i	PRON
iajs-1146	58	2	vo	vo	INTJ
iajs-1146	58	3	l.22	l.22	X
iajs-1146	58	4	(	(	PUNCT
iajs-1146	58	5	4	4	NUM
iajs-1146	58	6	)	)	PUNCT
iajs-1146	58	7	2009	2009	NUM
iajs-1146	58	8	the	the	DET
iajs-1146	58	9	theophylline	theophylline	NOUN
iajs-1146	58	10	mercury	mercury	NOUN
iajs-1146	58	11	salt	salt	NOUN
iajs-1146	58	12	9	9	NUM
iajs-1146	58	13	was	be	AUX
iajs-1146	58	14	synthesized	synthesize	VERB
iajs-1146	58	15	according	accord	VERB
iajs-1146	58	16	to	to	ADP
iajs-1146	58	17	the	the	DET
iajs-1146	58	18	reference	reference	NOUN
iajs-1146	58	19	[	[	X
iajs-1146	58	20	16	16	NUM
iajs-1146	58	21	]	]	PUNCT
iajs-1146	58	22	.	.	PUNCT
iajs-1146	59	1	this	this	DET
iajs-1146	59	2	salt(0.56	salt(0.56	NUM
iajs-1146	59	3	g,1.54	g,1.54	PROPN
iajs-1146	59	4	mmol	mmol	NOUN
iajs-1146	59	5	)	)	PUNCT
iajs-1146	59	6	was	be	AUX
iajs-1146	59	7	powdered	powder	VERB
iajs-1146	59	8	,	,	PUNCT
iajs-1146	59	9	suspended	suspend	VERB
iajs-1146	59	10	in	in	ADP
iajs-1146	59	11	(	(	PUNCT
iajs-1146	59	12	50ml	50ml	ADJ
iajs-1146	59	13	)	)	PUNCT
iajs-1146	59	14	sodium	sodium	NOUN
iajs-1146	59	15	dried	dry	VERB
iajs-1146	59	16	xylene	xylene	NOUN
iajs-1146	59	17	and	and	CCONJ
iajs-1146	59	18	the	the	DET
iajs-1146	59	19	solvent	solvent	NOUN
iajs-1146	59	20	was	be	AUX
iajs-1146	59	21	distilled	distil	VERB
iajs-1146	59	22	of	of	ADP
iajs-1146	59	23	to	to	PART
iajs-1146	59	24	remove	remove	VERB
iajs-1146	59	25	the	the	DET
iajs-1146	59	26	traces	trace	NOUN
iajs-1146	59	27	of	of	ADP
iajs-1146	59	28	water	water	NOUN
iajs-1146	59	29	azeotropically	azeotropically	ADV
iajs-1146	59	30	.when	.when	SCONJ
iajs-1146	59	31	the	the	DET
iajs-1146	59	32	temperature	temperature	NOUN
iajs-1146	59	33	of	of	ADP
iajs-1146	59	34	mixture	mixture	NOUN
iajs-1146	59	35	was	be	AUX
iajs-1146	59	36	raised	raise	VERB
iajs-1146	59	37	to	to	ADP
iajs-1146	59	38	137c	137c	PROPN
iajs-1146	59	39	o	o	NOUN
iajs-1146	59	40	,	,	PUNCT
iajs-1146	59	41	the	the	DET
iajs-1146	59	42	suspension	suspension	NOUN
iajs-1146	59	43	was	be	AUX
iajs-1146	59	44	allowed	allow	VERB
iajs-1146	59	45	to	to	PART
iajs-1146	59	46	cool	cool	VERB
iajs-1146	59	47	(	(	PUNCT
iajs-1146	59	48	below	below	ADP
iajs-1146	59	49	50co	50co	NOUN
iajs-1146	59	50	)	)	PUNCT
iajs-1146	59	51	.compound	.compound	ADV
iajs-1146	59	52	7	7	NUM
iajs-1146	59	53	(	(	PUNCT
iajs-1146	59	54	1g,1.53	1g,1.53	NUM
iajs-1146	59	55	mmol	mmol	NOUN
iajs-1146	59	56	)	)	PUNCT
iajs-1146	59	57	in	in	ADP
iajs-1146	59	58	xylent	xylent	NOUN
iajs-1146	59	59	(	(	PUNCT
iajs-1146	59	60	20ml	20ml	NOUN
iajs-1146	59	61	)	)	PUNCT
iajs-1146	59	62	was	be	AUX
iajs-1146	59	63	added	add	VERB
iajs-1146	59	64	to	to	ADP
iajs-1146	59	65	the	the	DET
iajs-1146	59	66	suspension	suspension	NOUN
iajs-1146	59	67	and	and	CCONJ
iajs-1146	59	68	refluxed	refluxe	VERB
iajs-1146	59	69	with	with	ADP
iajs-1146	59	70	stirring	stir	VERB
iajs-1146	59	71	for	for	ADP
iajs-1146	59	72	(	(	PUNCT
iajs-1146	59	73	30	30	NUM
iajs-1146	59	74	h	h	NOUN
iajs-1146	59	75	)	)	PUNCT
iajs-1146	60	1	.the	.the	PRON
iajs-1146	60	2	traces	trace	NOUN
iajs-1146	60	3	of	of	ADP
iajs-1146	60	4	theophylline	theophylline	ADJ
iajs-1146	60	5	salt	salt	NOUN
iajs-1146	60	6	was	be	AUX
iajs-1146	60	7	filtrated	filtrate	VERB
iajs-1146	60	8	from	from	ADP
iajs-1146	60	9	the	the	DET
iajs-1146	60	10	hot	hot	ADJ
iajs-1146	60	11	xylene	xylene	NOUN
iajs-1146	60	12	and	and	CCONJ
iajs-1146	60	13	washed	wash	VERB
iajs-1146	60	14	with	with	ADP
iajs-1146	60	15	dichloromethane	dichloromethane	NOUN
iajs-1146	60	16	(	(	PUNCT
iajs-1146	60	17	20ml	20ml	NOUN
iajs-1146	60	18	)	)	PUNCT
iajs-1146	60	19	.the	.the	PRON
iajs-1146	60	20	organic	organic	ADJ
iajs-1146	60	21	layer	layer	NOUN
iajs-1146	60	22	was	be	AUX
iajs-1146	60	23	dried	dry	VERB
iajs-1146	60	24	and	and	CCONJ
iajs-1146	60	25	removed	remove	VERB
iajs-1146	60	26	to	to	PART
iajs-1146	60	27	give	give	VERB
iajs-1146	60	28	acetylated	acetylated	ADJ
iajs-1146	60	29	nucleoside	nucleoside	ADV
iajs-1146	60	30	8	8	NUM
iajs-1146	60	31	as	as	ADP
iajs-1146	60	32	a	a	DET
iajs-1146	60	33	syrup	syrup	NOUN
iajs-1146	60	34	.	.	PUNCT
iajs-1146	61	1	1hnmr	1hnmr	NUM
iajs-1146	61	2	(	(	PUNCT
iajs-1146	61	3	cdcl3	cdcl3	NOUN
iajs-1146	61	4	)	)	PUNCT
iajs-1146	61	5	δ:2.5(3h	δ:2.5(3h	NOUN
iajs-1146	61	6	,	,	PUNCT
iajs-1146	61	7	s	s	NOUN
iajs-1146	61	8	,	,	PUNCT
iajs-1146	61	9	ch3ar	ch3ar	NOUN
iajs-1146	61	10	)	)	PUNCT
iajs-1146	61	11	;	;	PUNCT
iajs-1146	61	12	2.82(2h	2.82(2h	NUM
iajs-1146	61	13	,	,	PUNCT
iajs-1146	61	14	s	s	NOUN
iajs-1146	61	15	,	,	PUNCT
iajs-1146	61	16	ch2/9	ch2/9	PROPN
iajs-1146	61	17	)	)	PUNCT
iajs-1146	61	18	;	;	PUNCT
iajs-1146	61	19	3.2,3.4(6h	3.2,3.4(6h	NUM
iajs-1146	61	20	,	,	PUNCT
iajs-1146	61	21	s	s	NOUN
iajs-1146	61	22	,	,	PUNCT
iajs-1146	61	23	s,2nch3	s,2nch3	NOUN
iajs-1146	61	24	)	)	PUNCT
iajs-1146	61	25	;	;	PUNCT
iajs-1146	61	26	3.8	3.8	NUM
iajs-1146	61	27	-	-	SYM
iajs-1146	61	28	4.9	4.9	NUM
iajs-1146	61	29	(	(	PUNCT
iajs-1146	61	30	4h	4h	NUM
iajs-1146	61	31	,	,	PUNCT
iajs-1146	61	32	m	m	PROPN
iajs-1146	61	33	,	,	PUNCT
iajs-1146	61	34	h-/4,h-/1	h-/4,h-/1	PROPN
iajs-1146	61	35	and	and	CCONJ
iajs-1146	61	36	ha	ha	INTJ
iajs-1146	61	37	,	,	PUNCT
iajs-1146	61	38	hb	hb	PROPN
iajs-1146	61	39	ch2obz	ch2obz	PROPN
iajs-1146	61	40	)	)	PUNCT
iajs-1146	61	41	;	;	PUNCT
iajs-1146	61	42	5.9	5.9	NUM
iajs-1146	61	43	(	(	PUNCT
iajs-1146	61	44	1h	1h	NUM
iajs-1146	61	45	,	,	PUNCT
iajs-1146	61	46	d	d	PROPN
iajs-1146	61	47	,	,	PUNCT
iajs-1146	61	48	h-/3	h-/3	PROPN
iajs-1146	61	49	)	)	PUNCT
iajs-1146	61	50	,	,	PUNCT
iajs-1146	61	51	6.8	6.8	NUM
iajs-1146	61	52	-	-	SYM
iajs-1146	61	53	8.8	8.8	NUM
iajs-1146	61	54	(	(	PUNCT
iajs-1146	61	55	15h	15h	NUM
iajs-1146	61	56	,	,	PUNCT
iajs-1146	61	57	m	m	PROPN
iajs-1146	61	58	,	,	PUNCT
iajs-1146	61	59	arh	arh	ADJ
iajs-1146	61	60	and	and	CCONJ
iajs-1146	61	61	base	base	NOUN
iajs-1146	61	62	)	)	PUNCT
iajs-1146	61	63	.	.	PUNCT
iajs-1146	62	1	synthesis	synthesis	NOUN
iajs-1146	62	2	of	of	ADP
iajs-1146	62	3	7	7	NUM
iajs-1146	62	4	[	[	X
iajs-1146	62	5	(	(	PUNCT
iajs-1146	62	6	/1	/1	NOUN
iajs-1146	62	7	-	-	PUNCT
iajs-1146	62	8	hydroxy	hydroxy	NOUN
iajs-1146	62	9	methyl	methyl	NOUN
iajs-1146	62	10	)	)	PUNCT
iajs-1146	62	11	-/4	-/4	ADV
iajs-1146	62	12	-	-	PUNCT
iajs-1146	62	13	hydroxy	hydroxy	ADJ
iajs-1146	62	14	-/8-(4	-/8-(4	NOUN
iajs-1146	62	15	-	-	PUNCT
iajs-1146	62	16	tolyl)-/2	tolyl)-/2	NOUN
iajs-1146	62	17	-	-	PUNCT
iajs-1146	62	18	oxa-/6	oxa-/6	ADJ
iajs-1146	62	19	-	-	PUNCT
iajs-1146	62	20	aza	aza	NOUN
iajs-1146	62	21	phenyl	phenyl	NOUN
iajs-1146	62	22	spiro	spiro	NOUN
iajs-1146	62	23	[	[	X
iajs-1146	62	24	4,4	4,4	X
iajs-1146	62	25	]	]	X
iajs-1146	62	26	nona-/7	nona-/7	NOUN
iajs-1146	62	27	-	-	PUNCT
iajs-1146	62	28	imino	imino	NOUN
iajs-1146	62	29	]	]	PUNCT
iajs-1146	62	30	theophyllene	theophyllene	NOUN
iajs-1146	62	31	.	.	PUNCT
iajs-1146	63	1	(	(	PUNCT
iajs-1146	63	2	10	10	NUM
iajs-1146	63	3	)	)	PUNCT
iajs-1146	63	4	compound	compound	NOUN
iajs-1146	63	5	8(0.5	8(0.5	NUM
iajs-1146	63	6	g	g	NOUN
iajs-1146	63	7	,	,	PUNCT
iajs-1146	63	8	0.69	0.69	NUM
iajs-1146	63	9	mmol	mmol	NOUN
iajs-1146	63	10	)	)	PUNCT
iajs-1146	63	11	and	and	CCONJ
iajs-1146	63	12	sodium	sodium	NOUN
iajs-1146	63	13	methoxid	methoxid	NOUN
iajs-1146	63	14	(	(	PUNCT
iajs-1146	63	15	0.3	0.3	NUM
iajs-1146	63	16	g	g	NOUN
iajs-1146	63	17	,	,	PUNCT
iajs-1146	63	18	5.55	5.55	NUM
iajs-1146	63	19	mmol	mmol	NOUN
iajs-1146	63	20	)	)	PUNCT
iajs-1146	63	21	were	be	AUX
iajs-1146	63	22	dissolved	dissolve	VERB
iajs-1146	63	23	in	in	ADP
iajs-1146	63	24	ethanol	ethanol	NOUN
iajs-1146	63	25	(	(	PUNCT
iajs-1146	63	26	30ml	30ml	NOUN
iajs-1146	63	27	)	)	PUNCT
iajs-1146	63	28	.the	.the	PRON
iajs-1146	63	29	solution	solution	NOUN
iajs-1146	63	30	was	be	AUX
iajs-1146	63	31	stirred	stir	VERB
iajs-1146	63	32	under	under	ADP
iajs-1146	63	33	reflux	reflux	NOUN
iajs-1146	63	34	for	for	ADP
iajs-1146	63	35	(	(	PUNCT
iajs-1146	63	36	24h	24h	NOUN
iajs-1146	63	37	)	)	PUNCT
iajs-1146	63	38	.the	.the	PUNCT
iajs-1146	64	1	solvent	solvent	PROPN
iajs-1146	64	2	was	be	AUX
iajs-1146	64	3	removed	remove	VERB
iajs-1146	64	4	to	to	PART
iajs-1146	64	5	give	give	VERB
iajs-1146	64	6	10	10	NUM
iajs-1146	64	7	as	as	ADP
iajs-1146	64	8	a	a	DET
iajs-1146	64	9	syrup	syrup	NOUN
iajs-1146	64	10	.	.	PUNCT
iajs-1146	65	1	synthesis	synthesis	NOUN
iajs-1146	65	2	of	of	ADP
iajs-1146	65	3	1	1	NUM
iajs-1146	65	4	[	[	X
iajs-1146	65	5	(	(	PUNCT
iajs-1146	65	6	/1	/1	NOUN
iajs-1146	65	7	-	-	PUNCT
iajs-1146	65	8	benzoyl	benzoyl	NOUN
iajs-1146	65	9	methyl)-/4	methyl)-/4	NOUN
iajs-1146	65	10	-	-	PUNCT
iajs-1146	65	11	o	o	NOUN
iajs-1146	65	12	-	-	NOUN
iajs-1146	65	13	triflouro	triflouro	NOUN
iajs-1146	65	14	acetyl-/8-(4	acetyl-/8-(4	PROPN
iajs-1146	65	15	-	-	PUNCT
iajs-1146	65	16	tolyl	tolyl	ADJ
iajs-1146	65	17	)	)	PUNCT
iajs-1146	65	18	-/2	-/2	NOUN
iajs-1146	65	19	-	-	PUNCT
iajs-1146	65	20	oxa-/6aza	oxa-/6aza	NOUN
iajs-1146	65	21	phenyl	phenyl	NOUN
iajs-1146	65	22	spiro	spiro	NOUN
iajs-1146	65	23	[	[	X
iajs-1146	65	24	4	4	NUM
iajs-1146	65	25	,	,	PUNCT
iajs-1146	65	26	4	4	NUM
iajs-1146	65	27	]	]	X
iajs-1146	65	28	nona	nona	PROPN
iajs-1146	65	29	-/7	-/7	NOUN
iajs-1146	65	30	-	-	PUNCT
iajs-1146	65	31	imino	imino	NOUN
iajs-1146	65	32	]	]	PUNCT
iajs-1146	65	33	uracil	uracil	PROPN
iajs-1146	65	34	.	.	PUNCT
iajs-1146	66	1	(	(	PUNCT
iajs-1146	66	2	12	12	NUM
iajs-1146	66	3	)	)	PUNCT
iajs-1146	66	4	anhydrous	anhydrous	ADJ
iajs-1146	66	5	stannic	stannic	ADJ
iajs-1146	66	6	chloride	chloride	NOUN
iajs-1146	66	7	(	(	PUNCT
iajs-1146	66	8	0.6	0.6	NUM
iajs-1146	66	9	ml	ml	NOUN
iajs-1146	66	10	)	)	PUNCT
iajs-1146	66	11	and	and	CCONJ
iajs-1146	66	12	few	few	ADJ
iajs-1146	66	13	pellets	pellet	NOUN
iajs-1146	66	14	of	of	ADP
iajs-1146	66	15	molecular	molecular	ADJ
iajs-1146	66	16	sive	sive	ADJ
iajs-1146	66	17	4a	4a	NOUN
iajs-1146	66	18	was	be	AUX
iajs-1146	66	19	added	add	VERB
iajs-1146	66	20	to	to	ADP
iajs-1146	66	21	a	a	DET
iajs-1146	66	22	mixture	mixture	NOUN
iajs-1146	66	23	of	of	ADP
iajs-1146	66	24	7	7	NUM
iajs-1146	66	25	(	(	PUNCT
iajs-1146	66	26	2.0g,3.07	2.0g,3.07	NUM
iajs-1146	66	27	mmol	mmol	NOUN
iajs-1146	66	28	)	)	PUNCT
iajs-1146	66	29	and	and	CCONJ
iajs-1146	66	30	silylated	silylate	VERB
iajs-1146	66	31	uracil	uracil	PROPN
iajs-1146	66	32	13	13	NUM
iajs-1146	66	33	(	(	PUNCT
iajs-1146	66	34	0.8g,3.12	0.8g,3.12	NUM
iajs-1146	66	35	mmol)[compound	mmol)[compound	ADP
iajs-1146	66	36	13	13	NUM
iajs-1146	66	37	was	be	AUX
iajs-1146	66	38	synthesized	synthesize	VERB
iajs-1146	66	39	by	by	ADP
iajs-1146	66	40	using	use	VERB
iajs-1146	66	41	the	the	DET
iajs-1146	66	42	reference	reference	NOUN
iajs-1146	66	43	[	[	X
iajs-1146	66	44	17	17	NUM
iajs-1146	66	45	]	]	PUNCT
iajs-1146	66	46	]	]	PUNCT
iajs-1146	66	47	in	in	ADP
iajs-1146	66	48	(	(	PUNCT
iajs-1146	66	49	40ml	40ml	NOUN
iajs-1146	66	50	)	)	PUNCT
iajs-1146	66	51	of	of	ADP
iajs-1146	66	52	anhydrous	anhydrous	ADJ
iajs-1146	66	53	dichloromethane.the	dichloromethane.the	DET
iajs-1146	66	54	mixture	mixture	NOUN
iajs-1146	66	55	was	be	AUX
iajs-1146	66	56	stirred	stir	VERB
iajs-1146	66	57	at	at	ADP
iajs-1146	66	58	20c	20c	NOUN
iajs-1146	66	59	o	o	NOUN
iajs-1146	66	60	for	for	SCONJ
iajs-1146	66	61	(	(	PUNCT
iajs-1146	66	62	24h)the	24h)the	NOUN
iajs-1146	66	63	reaction	reaction	NOUN
iajs-1146	66	64	mixture	mixture	NOUN
iajs-1146	66	65	was	be	AUX
iajs-1146	66	66	poured	pour	VERB
iajs-1146	66	67	in	in	ADP
iajs-1146	66	68	to	to	ADP
iajs-1146	66	69	an	an	DET
iajs-1146	66	70	excess	excess	NOUN
iajs-1146	66	71	of	of	ADP
iajs-1146	66	72	sodium	sodium	NOUN
iajs-1146	66	73	bicarbonate	bicarbonate	NOUN
iajs-1146	66	74	solution	solution	NOUN
iajs-1146	66	75	and	and	CCONJ
iajs-1146	66	76	extracted	extract	VERB
iajs-1146	66	77	with	with	ADP
iajs-1146	66	78	dichloromethane	dichloromethane	NOUN
iajs-1146	66	79	(	(	PUNCT
iajs-1146	66	80	3x40ml	3x40ml	NUM
iajs-1146	66	81	)	)	PUNCT
iajs-1146	66	82	.the	.the	X
iajs-1146	66	83	organic	organic	ADJ
iajs-1146	66	84	layer	layer	NOUN
iajs-1146	66	85	was	be	AUX
iajs-1146	66	86	dried	dry	VERB
iajs-1146	66	87	and	and	CCONJ
iajs-1146	66	88	removed	remove	VERB
iajs-1146	66	89	to	to	PART
iajs-1146	66	90	give	give	VERB
iajs-1146	66	91	12	12	NUM
iajs-1146	66	92	as	as	ADP
iajs-1146	66	93	semi	semi	ADV
iajs-1146	66	94	solid	solid	ADJ
iajs-1146	66	95	.1hnmr	.1hnmr	INTJ
iajs-1146	66	96	(	(	PUNCT
iajs-1146	66	97	cdcl3).δ:2.4(3h	cdcl3).δ:2.4(3h	NOUN
iajs-1146	66	98	,	,	PUNCT
iajs-1146	66	99	s	s	NOUN
iajs-1146	66	100	,	,	PUNCT
iajs-1146	66	101	ch3ar	ch3ar	NOUN
iajs-1146	66	102	)	)	PUNCT
iajs-1146	66	103	;	;	PUNCT
iajs-1146	66	104	2.7	2.7	NUM
iajs-1146	66	105	(	(	PUNCT
iajs-1146	66	106	2h	2h	NUM
iajs-1146	66	107	,	,	PUNCT
iajs-1146	66	108	s	s	X
iajs-1146	66	109	,	,	PUNCT
iajs-1146	66	110	ch2/9	ch2/9	PROPN
iajs-1146	66	111	)	)	PUNCT
iajs-1146	66	112	;	;	PUNCT
iajs-1146	66	113	3.7	3.7	NUM
iajs-1146	66	114	-	-	SYM
iajs-1146	66	115	4.9	4.9	NUM
iajs-1146	66	116	[	[	X
iajs-1146	66	117	6h	6h	NUM
iajs-1146	66	118	,	,	PUNCT
iajs-1146	66	119	m	m	PROPN
iajs-1146	66	120	,	,	PUNCT
iajs-1146	66	121	h-/1,h-/4,h-4,h-5,and	h-/1,h-/4,h-4,h-5,and	NOUN
iajs-1146	66	122	(	(	PUNCT
iajs-1146	66	123	ha	ha	INTJ
iajs-1146	66	124	,	,	PUNCT
iajs-1146	66	125	hb	hb	PROPN
iajs-1146	66	126	)	)	PUNCT
iajs-1146	66	127	ch2	ch2	PROPN
iajs-1146	66	128	-	-	PUNCT
iajs-1146	66	129	obz];5.8(1h	obz];5.8(1h	NUM
iajs-1146	66	130	,	,	PUNCT
iajs-1146	66	131	d	d	PROPN
iajs-1146	66	132	,	,	PUNCT
iajs-1146	66	133	h-/3	h-/3	PROPN
iajs-1146	66	134	)	)	PUNCT
iajs-1146	66	135	;	;	PUNCT
iajs-1146	66	136	6.5(1h	6.5(1h	NUM
iajs-1146	66	137	,	,	PUNCT
iajs-1146	66	138	b	b	PROPN
iajs-1146	66	139	,	,	PUNCT
iajs-1146	66	140	nh	nh	PROPN
iajs-1146	66	141	)	)	PUNCT
iajs-1146	66	142	;	;	PUNCT
iajs-1146	66	143	6.9	6.9	NUM
iajs-1146	66	144	-	-	PUNCT
iajs-1146	66	145	8.9(14h	8.9(14h	NUM
iajs-1146	66	146	,	,	PUNCT
iajs-1146	66	147	m	m	NOUN
iajs-1146	66	148	,	,	PUNCT
iajs-1146	66	149	arh	arh	ADJ
iajs-1146	66	150	)	)	PUNCT
iajs-1146	66	151	.	.	PUNCT
iajs-1146	67	1	synthesis	synthesis	NOUN
iajs-1146	67	2	of	of	ADP
iajs-1146	67	3	1	1	NUM
iajs-1146	67	4	[	[	X
iajs-1146	67	5	(	(	PUNCT
iajs-1146	67	6	/1	/1	NOUN
iajs-1146	67	7	-	-	PUNCT
iajs-1146	67	8	hydroxy	hydroxy	NOUN
iajs-1146	67	9	methyl	methyl	NOUN
iajs-1146	67	10	)	)	PUNCT
iajs-1146	67	11	-/4	-/4	ADV
iajs-1146	67	12	-	-	PUNCT
iajs-1146	67	13	hydroxy	hydroxy	ADJ
iajs-1146	67	14	-/8(4	-/8(4	ADV
iajs-1146	67	15	-	-	PUNCT
iajs-1146	67	16	tolyl	tolyl	ADJ
iajs-1146	67	17	)	)	PUNCT
iajs-1146	67	18	-/2	-/2	ADJ
iajs-1146	67	19	-	-	PUNCT
iajs-1146	67	20	oxa-/6	oxa-/6	VERB
iajs-1146	67	21	-	-	PUNCT
iajs-1146	67	22	aza	aza	NOUN
iajs-1146	67	23	phenyl	phenyl	NOUN
iajs-1146	67	24	spiro	spiro	NOUN
iajs-1146	67	25	[	[	X
iajs-1146	67	26	4	4	NUM
iajs-1146	67	27	,	,	PUNCT
iajs-1146	67	28	4	4	NUM
iajs-1146	67	29	]	]	X
iajs-1146	67	30	nona	nona	PROPN
iajs-1146	67	31	-/7	-/7	NOUN
iajs-1146	67	32	-	-	PUNCT
iajs-1146	67	33	imino	imino	NOUN
iajs-1146	67	34	]	]	PUNCT
iajs-1146	67	35	uracil	uracil	PROPN
iajs-1146	67	36	.	.	PUNCT
iajs-1146	68	1	(	(	PUNCT
iajs-1146	68	2	14	14	NUM
iajs-1146	68	3	)	)	PUNCT
iajs-1146	68	4	flowing	flow	VERB
iajs-1146	68	5	the	the	DET
iajs-1146	68	6	same	same	ADJ
iajs-1146	68	7	procedure	procedure	NOUN
iajs-1146	68	8	of	of	ADP
iajs-1146	68	9	the	the	DET
iajs-1146	68	10	preparation	preparation	NOUN
iajs-1146	68	11	of	of	ADP
iajs-1146	68	12	compound	compound	NOUN
iajs-1146	68	13	10	10	NUM
iajs-1146	68	14	,	,	PUNCT
iajs-1146	68	15	the	the	DET
iajs-1146	68	16	compound	compound	NOUN
iajs-1146	68	17	12	12	NUM
iajs-1146	68	18	(	(	PUNCT
iajs-1146	68	19	0.5	0.5	NUM
iajs-1146	68	20	g	g	NOUN
iajs-1146	68	21	,	,	PUNCT
iajs-1146	68	22	0.74	0.74	NUM
iajs-1146	68	23	mmol	mmol	NOUN
iajs-1146	68	24	)	)	PUNCT
iajs-1146	68	25	and	and	CCONJ
iajs-1146	68	26	sodium	sodium	NOUN
iajs-1146	68	27	methoxide	methoxide	NOUN
iajs-1146	68	28	(	(	PUNCT
iajs-1146	68	29	0.3	0.3	NUM
iajs-1146	68	30	g	g	NOUN
iajs-1146	68	31	,	,	PUNCT
iajs-1146	68	32	5.55mmol	5.55mmol	PROPN
iajs-1146	68	33	)	)	PUNCT
iajs-1146	68	34	were	be	AUX
iajs-1146	68	35	dissolved	dissolve	VERB
iajs-1146	68	36	in	in	ADP
iajs-1146	68	37	ethanol	ethanol	NOUN
iajs-1146	68	38	(	(	PUNCT
iajs-1146	68	39	30ml	30ml	NOUN
iajs-1146	68	40	)	)	PUNCT
iajs-1146	68	41	.	.	PUNCT
iajs-1146	69	1	the	the	DET
iajs-1146	69	2	reaction	reaction	NOUN
iajs-1146	69	3	mixture	mixture	NOUN
iajs-1146	69	4	was	be	AUX
iajs-1146	69	5	stirred	stir	VERB
iajs-1146	69	6	under	under	ADP
iajs-1146	69	7	reflux	reflux	NOUN
iajs-1146	69	8	for	for	ADP
iajs-1146	69	9	(	(	PUNCT
iajs-1146	69	10	18h	18h	NOUN
iajs-1146	69	11	)	)	PUNCT
iajs-1146	69	12	to	to	PART
iajs-1146	69	13	give	give	VERB
iajs-1146	69	14	14	14	NUM
iajs-1146	69	15	as	as	ADP
iajs-1146	69	16	a	a	DET
iajs-1146	69	17	syrup	syrup	NOUN
iajs-1146	69	18	.	.	PUNCT
iajs-1146	70	1	results	result	NOUN
iajs-1146	70	2	and	and	CCONJ
iajs-1146	70	3	discussions	discussion	NOUN
iajs-1146	70	4	compound	compound	NOUN
iajs-1146	70	5	(	(	PUNCT
iajs-1146	70	6	1	1	X
iajs-1146	70	7	)	)	PUNCT
iajs-1146	70	8	was	be	AUX
iajs-1146	70	9	chosen	choose	VERB
iajs-1146	70	10	as	as	ADP
iajs-1146	70	11	a	a	DET
iajs-1146	70	12	starting	starting	NOUN
iajs-1146	70	13	material	material	NOUN
iajs-1146	70	14	for	for	ADP
iajs-1146	70	15	the	the	DET
iajs-1146	70	16	synthesis	synthesis	NOUN
iajs-1146	70	17	of	of	ADP
iajs-1146	70	18	a	a	DET
iajs-1146	70	19	new	new	ADJ
iajs-1146	70	20	derivative	derivative	NOUN
iajs-1146	70	21	of	of	ADP
iajs-1146	70	22	3	3	NUM
iajs-1146	70	23	-	-	PUNCT
iajs-1146	70	24	c	c	NOUN
iajs-1146	70	25	-	-	PUNCT
iajs-1146	70	26	sp	sp	NOUN
iajs-1146	70	27	iro	iro	PROPN
iajs-1146	70	28	ring	ring	NOUN
iajs-1146	70	29	nucleoside	nucleoside	NOUN
iajs-1146	70	30	analogues	analogue	NOUN
iajs-1146	70	31	.the	.the	PRON
iajs-1146	70	32	strategy	strategy	NOUN
iajs-1146	70	33	used	use	VERB
iajs-1146	70	34	for	for	ADP
iajs-1146	70	35	the	the	DET
iajs-1146	70	36	synthesis	synthesis	NOUN
iajs-1146	70	37	of	of	ADP
iajs-1146	70	38	2	2	NUM
iajs-1146	70	39	,	,	PUNCT
iajs-1146	70	40	3	3	NUM
iajs-1146	70	41	,	,	PUNCT
iajs-1146	70	42	4	4	NUM
iajs-1146	70	43	,	,	PUNCT
iajs-1146	70	44	5,6,7,8,10,11,12	5,6,7,8,10,11,12	NUM
iajs-1146	70	45	and	and	CCONJ
iajs-1146	70	46	14	14	NUM
iajs-1146	70	47	was	be	AUX
iajs-1146	70	48	started	start	VERB
iajs-1146	70	49	with	with	ADP
iajs-1146	70	50	derivative	derivative	ADJ
iajs-1146	70	51	1	1	NUM
iajs-1146	70	52	in	in	ADP
iajs-1146	70	53	a	a	DET
iajs-1146	70	54	series	series	NOUN
iajs-1146	70	55	of	of	ADP
iajs-1146	70	56	reactions	reaction	NOUN
iajs-1146	71	1	[	[	X
iajs-1146	71	2	scheme	scheme	NOUN
iajs-1146	71	3	1	1	NUM
iajs-1146	71	4	]	]	PUNCT
iajs-1146	71	5	.	.	PUNCT
iajs-1146	72	1	compound	compound	NOUN
iajs-1146	72	2	2	2	NUM
iajs-1146	72	3	was	be	AUX
iajs-1146	72	4	synthesized	synthesize	VERB
iajs-1146	72	5	by	by	ADP
iajs-1146	72	6	the	the	DET
iajs-1146	72	7	dehydration	dehydration	NOUN
iajs-1146	72	8	of	of	ADP
iajs-1146	72	9	1	1	NUM
iajs-1146	72	10	with	with	ADP
iajs-1146	72	11	dmso	dmso	NOUN
iajs-1146	72	12	/	/	SYM
iajs-1146	72	13	ac2o	ac2o	PROPN
iajs-1146	73	1	[	[	X
iajs-1146	73	2	18	18	NUM
iajs-1146	73	3	,	,	PUNCT
iajs-1146	73	4	19	19	NUM
iajs-1146	73	5	]	]	PUNCT
iajs-1146	73	6	and	and	CCONJ
iajs-1146	73	7	gave	give	VERB
iajs-1146	73	8	2	2	NUM
iajs-1146	73	9	.	.	PUNCT
iajs-1146	74	1	the	the	DET
iajs-1146	74	2	ir	ir	PROPN
iajs-1146	74	3	spectra	spectra	NOUN
iajs-1146	74	4	of	of	ADP
iajs-1146	74	5	2	2	NUM
iajs-1146	74	6	showed	show	VERB
iajs-1146	74	7	the	the	DET
iajs-1146	74	8	disappearance	disappearance	NOUN
iajs-1146	74	9	of	of	ADP
iajs-1146	74	10	stretching	stretch	VERB
iajs-1146	74	11	band	band	NOUN
iajs-1146	74	12	at	at	ADP
iajs-1146	74	13	3360	3360	NUM
iajs-1146	74	14	cm	cm	NOUN
iajs-1146	74	15	-1	-1	PUNCT
iajs-1146	74	16	for	for	ADP
iajs-1146	74	17	hydroxyl	hydroxyl	PROPN
iajs-1146	74	18	group	group	NOUN
iajs-1146	74	19	with	with	ADP
iajs-1146	74	20	appearance	appearance	NOUN
iajs-1146	74	21	of	of	ADP
iajs-1146	74	22	stretching	stretch	VERB
iajs-1146	74	23	band	band	NOUN
iajs-1146	74	24	at	at	ADP
iajs-1146	74	25	1640cm-1	1640cm-1	NUM
iajs-1146	74	26	for	for	ADP
iajs-1146	74	27	(	(	PUNCT
iajs-1146	74	28	c	c	X
iajs-1146	74	29	=	=	SYM
iajs-1146	74	30	c).tables	c).table	NOUN
iajs-1146	74	31	(	(	PUNCT
iajs-1146	74	32	1	1	NUM
iajs-1146	74	33	)	)	PUNCT
iajs-1146	74	34	and	and	CCONJ
iajs-1146	74	35	(	(	PUNCT
iajs-1146	74	36	2	2	X
iajs-1146	74	37	)	)	PUNCT
iajs-1146	74	38	showed	show	VERB
iajs-1146	74	39	the	the	DET
iajs-1146	74	40	characteristic	characteristic	ADJ
iajs-1146	74	41	ir	ir	PROPN
iajs-1146	74	42	absorption	absorption	NOUN
iajs-1146	74	43	bands	band	NOUN
iajs-1146	74	44	and	and	CCONJ
iajs-1146	74	45	physical	physical	ADJ
iajs-1146	74	46	properties	property	NOUN
iajs-1146	74	47	for	for	ADP
iajs-1146	74	48	all	all	PRON
iajs-1146	74	49	of	of	ADP
iajs-1146	74	50	the	the	DET
iajs-1146	74	51	new	new	ADJ
iajs-1146	74	52	derivations	derivation	NOUN
iajs-1146	74	53	.the	.the	PUNCT
iajs-1146	74	54	α	α	X
iajs-1146	74	55	,	,	PUNCT
iajs-1146	74	56	β	β	ADJ
iajs-1146	74	57	-	-	ADJ
iajs-1146	74	58	unsaturated	unsaturated	ADJ
iajs-1146	74	59	branched	branched	ADJ
iajs-1146	74	60	chain	chain	NOUN
iajs-1146	74	61	2	2	NUM
iajs-1146	74	62	undergoes	undergo	VERB
iajs-1146	74	63	1/3	1/3	NUM
iajs-1146	74	64	-	-	PUNCT
iajs-1146	74	65	and	and	CCONJ
iajs-1146	74	66	adding	add	VERB
iajs-1146	74	67	the	the	DET
iajs-1146	74	68	diamine	diamine	NOUN
iajs-1146	74	69	(	(	PUNCT
iajs-1146	74	70	phenyl	phenyl	NOUN
iajs-1146	74	71	hydrazine	hydrazine	NOUN
iajs-1146	74	72	)	)	PUNCT
iajs-1146	74	73	to	to	PART
iajs-1146	74	74	give	give	VERB
iajs-1146	74	75	the	the	PRON
iajs-1146	74	76	sp	sp	ADP
iajs-1146	74	77	iro	iro	PROPN
iajs-1146	75	1	derivative	derivative	NOUN
iajs-1146	75	2	3	3	NUM
iajs-1146	75	3	[	[	X
iajs-1146	75	4	20,21].compound	20,21].compound	NUM
iajs-1146	75	5	3	3	NUM
iajs-1146	75	6	was	be	AUX
iajs-1146	75	7	characterized	characterize	VERB
iajs-1146	75	8	by	by	ADP
iajs-1146	75	9	ir	ir	NOUN
iajs-1146	75	10	and	and	CCONJ
iajs-1146	75	11	elemental	elemental	ADJ
iajs-1146	75	12	analysis	analysis	NOUN
iajs-1146	75	13	.the	.the	X
iajs-1146	75	14	ir	ir	PROPN
iajs-1146	75	15	spectra	spectra	PROPN
iajs-1146	75	16	of	of	ADP
iajs-1146	75	17	3	3	NUM
iajs-1146	75	18	showed	show	VERB
iajs-1146	75	19	the	the	DET
iajs-1146	75	20	disappearance	disappearance	NOUN
iajs-1146	75	21	of	of	ADP
iajs-1146	75	22	stretching	stretch	VERB
iajs-1146	75	23	band	band	NOUN
iajs-1146	75	24	at	at	ADP
iajs-1146	75	25	1640	1640	NUM
iajs-1146	75	26	cm	cm	NOUN
iajs-1146	75	27	-1	-1	PUNCT
iajs-1146	75	28	for	for	ADP
iajs-1146	75	29	(	(	PUNCT
iajs-1146	75	30	c	c	X
iajs-1146	75	31	=	=	NOUN
iajs-1146	75	32	c	c	NOUN
iajs-1146	75	33	)	)	PUNCT
iajs-1146	75	34	and	and	CCONJ
iajs-1146	75	35	disappearance	disappearance	NOUN
iajs-1146	75	36	of	of	ADP
iajs-1146	75	37	(	(	PUNCT
iajs-1146	75	38	co	co	NOUN
iajs-1146	75	39	)	)	PUNCT
iajs-1146	75	40	group	group	NOUN
iajs-1146	75	41	at	at	ADP
iajs-1146	75	42	1690cm-1.to	1690cm-1.to	NUM
iajs-1146	75	43	obtain	obtain	VERB
iajs-1146	75	44	the	the	DET
iajs-1146	75	45	derivative	derivative	ADJ
iajs-1146	75	46	5	5	NUM
iajs-1146	75	47	,	,	PUNCT
iajs-1146	75	48	the	the	DET
iajs-1146	75	49	isopropylidene	isopropylidene	ADJ
iajs-1146	75	50	acetal	acetal	NOUN
iajs-1146	75	51	at	at	ADP
iajs-1146	75	52	c/	c/	NOUN
iajs-1146	75	53	1	1	NUM
iajs-1146	75	54	and	and	CCONJ
iajs-1146	75	55	c/	c/	NOUN
iajs-1146	75	56	2	2	NUM
iajs-1146	75	57	was	be	AUX
iajs-1146	75	58	removed	remove	VERB
iajs-1146	75	59	with	with	ADP
iajs-1146	75	60	acetic	acetic	ADJ
iajs-1146	75	61	acid	acid	NOUN
iajs-1146	75	62	followed	follow	VERB
iajs-1146	75	63	by	by	ADP
iajs-1146	75	64	periodate	periodate	NOUN
iajs-1146	75	65	oxidation	oxidation	NOUN
iajs-1146	75	66	and	and	CCONJ
iajs-1146	75	67	borohydride	borohydride	NOUN
iajs-1146	75	68	reduction	reduction	NOUN
iajs-1146	75	69	.the	.the	X
iajs-1146	75	70	/1	/1	NOUN
iajs-1146	75	71	-	-	PUNCT
iajs-1146	75	72	hydroxyl	hydroxyl	NOUN
iajs-1146	75	73	group	group	NOUN
iajs-1146	75	74	was	be	AUX
iajs-1146	75	75	protected	protect	VERB
iajs-1146	75	76	with	with	ADP
iajs-1146	75	77	benzoyl	benzoyl	NOUN
iajs-1146	75	78	group	group	NOUN
iajs-1146	75	79	by	by	ADP
iajs-1146	75	80	using	use	VERB
iajs-1146	75	81	benzoyl	benzoyl	ADJ
iajs-1146	75	82	chloride	chloride	NOUN
iajs-1146	75	83	to	to	PART
iajs-1146	75	84	give	give	VERB
iajs-1146	75	85	the	the	DET
iajs-1146	75	86	derivative	derivative	ADJ
iajs-1146	75	87	6.the	6.the	DET
iajs-1146	75	88	ir	ir	PROPN
iajs-1146	75	89	spectra	spectra	NOUN
iajs-1146	75	90	of	of	ADP
iajs-1146	75	91	6	6	NUM
iajs-1146	75	92	showed	show	VERB
iajs-1146	75	93	a	a	DET
iajs-1146	75	94	stretching	stretch	VERB
iajs-1146	75	95	band	band	NOUN
iajs-1146	75	96	at	at	ADP
iajs-1146	75	97	1700cm-1	1700cm-1	NUM
iajs-1146	75	98	for	for	SCONJ
iajs-1146	75	99	(	(	PUNCT
iajs-1146	75	100	co	co	NOUN
iajs-1146	75	101	)	)	PUNCT
iajs-1146	75	102	group	group	NOUN
iajs-1146	75	103	with	with	ADP
iajs-1146	75	104	the	the	DET
iajs-1146	75	105	disappearance	disappearance	NOUN
iajs-1146	75	106	of	of	ADP
iajs-1146	75	107	(	(	PUNCT
iajs-1146	75	108	oh	oh	INTJ
iajs-1146	75	109	)	)	PUNCT
iajs-1146	75	110	group	group	NOUN
iajs-1146	75	111	at	at	ADP
iajs-1146	75	112	3385cm1.compound	3385cm1.compound	PROPN
iajs-1146	75	113	6	6	NUM
iajs-1146	75	114	was	be	AUX
iajs-1146	75	115	treated	treat	VERB
iajs-1146	75	116	with	with	ADP
iajs-1146	75	117	a	a	DET
iajs-1146	75	118	mixture	mixture	NOUN
iajs-1146	75	119	of	of	ADP
iajs-1146	75	120	trifluoroacetic	trifluoroacetic	ADJ
iajs-1146	75	121	acid	acid	NOUN
iajs-1146	75	122	and	and	CCONJ
iajs-1146	75	123	acetic	acetic	ADJ
iajs-1146	75	124	acid	acid	NOUN
iajs-1146	75	125	followed	follow	VERB
iajs-1146	75	126	by	by	ADP
iajs-1146	75	127	the	the	DET
iajs-1146	75	128	reaction	reaction	NOUN
iajs-1146	75	129	with	with	ADP
iajs-1146	75	130	trifluoroacetic	trifluoroacetic	ADJ
iajs-1146	75	131	anhydride	anhydride	NOUN
iajs-1146	75	132	gave	give	VERB
iajs-1146	75	133	7	7	NUM
iajs-1146	75	134	.	.	PUNCT
iajs-1146	76	1	compound	compound	NOUN
iajs-1146	76	2	8	8	NUM
iajs-1146	76	3	was	be	AUX
iajs-1146	76	4	prepared	prepare	VERB
iajs-1146	76	5	by	by	ADP
iajs-1146	76	6	using	use	VERB
iajs-1146	76	7	the	the	DET
iajs-1146	76	8	koenigs	koenig	NOUN
iajs-1146	76	9	-	-	PUNCT
iajs-1146	76	10	knorr	knorr	NOUN
iajs-1146	76	11	condensation	condensation	NOUN
iajs-1146	76	12	method	method	NOUN
iajs-1146	76	13	[	[	X
iajs-1146	76	14	22,23].the	22,23].the	PROPN
iajs-1146	76	15	1hnmr	1hnmr	NUM
iajs-1146	76	16	spectrum	spectrum	NOUN
iajs-1146	76	17	of	of	ADP
iajs-1146	76	18	8	8	NUM
iajs-1146	76	19	showed	show	VERB
iajs-1146	76	20	a	a	DET
iajs-1146	76	21	singlet	singlet	NOUN
iajs-1146	76	22	at	at	ADP
iajs-1146	76	23	2.5	2.5	NUM
iajs-1146	76	24	for	for	ADP
iajs-1146	76	25	p	p	NOUN
iajs-1146	76	26	-	-	PUNCT
iajs-1146	76	27	methyl	methyl	NOUN
iajs-1146	76	28	group	group	NOUN
iajs-1146	76	29	,	,	PUNCT
iajs-1146	76	30	singlet	singlet	NOUN
iajs-1146	76	31	at	at	ADP
iajs-1146	76	32	2.82	2.82	NUM
iajs-1146	76	33	for	for	ADP
iajs-1146	76	34	methylene	methylene	ADJ
iajs-1146	76	35	group	group	NOUN
iajs-1146	76	36	(	(	PUNCT
iajs-1146	76	37	ch2	ch2	PROPN
iajs-1146	76	38	-	-	PUNCT
iajs-1146	76	39	9	9	NUM
iajs-1146	76	40	/	/	SYM
iajs-1146	76	41	)	)	PUNCT
iajs-1146	76	42	,	,	PUNCT
iajs-1146	76	43	two	two	NUM
iajs-1146	76	44	singlet	singlet	NOUN
iajs-1146	76	45	at	at	ADP
iajs-1146	76	46	3.2	3.2	NUM
iajs-1146	76	47	,	,	PUNCT
iajs-1146	76	48	3.4	3.4	NUM
iajs-1146	76	49	for	for	ADP
iajs-1146	76	50	(	(	PUNCT
iajs-1146	76	51	2nch3	2nch3	NUM
iajs-1146	76	52	)	)	PUNCT
iajs-1146	76	53	,	,	PUNCT
iajs-1146	76	54	multiplet	multiplet	NOUN
iajs-1146	76	55	at	at	ADP
iajs-1146	76	56	3.8	3.8	NUM
iajs-1146	76	57	-	-	SYM
iajs-1146	76	58	4.9	4.9	NUM
iajs-1146	76	59	for	for	ADP
iajs-1146	76	60	(	(	PUNCT
iajs-1146	76	61	h-4/,h-1	h-4/,h-1	PROPN
iajs-1146	76	62	/	/	SYM
iajs-1146	76	63	and	and	CCONJ
iajs-1146	76	64	ha	ha	INTJ
iajs-1146	76	65	,	,	PUNCT
iajs-1146	76	66	hb	hb	PROPN
iajs-1146	76	67	ch2obz	ch2obz	PROPN
iajs-1146	76	68	)	)	PUNCT
iajs-1146	76	69	,	,	PUNCT
iajs-1146	76	70	doublet	doublet	VERB
iajs-1146	76	71	at	at	ADP
iajs-1146	76	72	5.9	5.9	NUM
iajs-1146	76	73	for	for	ADP
iajs-1146	76	74	h-3/	h-3/	NOUN
iajs-1146	76	75	and	and	CCONJ
iajs-1146	76	76	ibn	ibn	PROPN
iajs-1146	76	77	alhaitham	alhaitham	NOUN
iajs-1146	76	78	j.	j.	PROPN
iajs-1146	77	1	fo	fo	ADP
iajs-1146	77	2	r	r	NOUN
iajs-1146	77	3	pure	pure	ADJ
iajs-1146	77	4	&	&	CCONJ
iajs-1146	77	5	appl	appl	PROPN
iajs-1146	77	6	.	.	PUNCT
iajs-1146	78	1	sc	sc	PROPN
iajs-1146	79	1	i	i	PRON
iajs-1146	79	2	vo	vo	INTJ
iajs-1146	79	3	l.22	l.22	X
iajs-1146	79	4	(	(	PUNCT
iajs-1146	79	5	4	4	NUM
iajs-1146	79	6	)	)	PUNCT
iajs-1146	79	7	2009	2009	NUM
iajs-1146	79	8	multiplet	multiplet	NOUN
iajs-1146	79	9	signals	signal	NOUN
iajs-1146	79	10	at	at	ADP
iajs-1146	79	11	6.8	6.8	NUM
iajs-1146	79	12	-	-	SYM
iajs-1146	79	13	8.8	8.8	NUM
iajs-1146	79	14	for	for	ADP
iajs-1146	79	15	aromatic	aromatic	ADJ
iajs-1146	79	16	rings	ring	NOUN
iajs-1146	79	17	protons	proton	NOUN
iajs-1146	79	18	and	and	CCONJ
iajs-1146	79	19	base	base	NOUN
iajs-1146	79	20	.	.	PUNCT
iajs-1146	80	1	the	the	DET
iajs-1146	80	2	treatment	treatment	NOUN
iajs-1146	80	3	of	of	ADP
iajs-1146	80	4	compound	compound	NOUN
iajs-1146	80	5	8	8	NUM
iajs-1146	80	6	with	with	ADP
iajs-1146	80	7	sodium	sodium	NOUN
iajs-1146	80	8	methoxide	methoxide	NOUN
iajs-1146	80	9	in	in	ADP
iajs-1146	80	10	ethanol	ethanol	NOUN
iajs-1146	80	11	under	under	ADP
iajs-1146	80	12	reflux	reflux	NOUN
iajs-1146	80	13	[	[	X
iajs-1146	80	14	24]gave	24]gave	NUM
iajs-1146	80	15	10.compound	10.compound	NUM
iajs-1146	80	16	7	7	NUM
iajs-1146	80	17	was	be	AUX
iajs-1146	80	18	treated	treat	VERB
iajs-1146	80	19	with	with	ADP
iajs-1146	80	20	silylated	silylate	VERB
iajs-1146	80	21	uracil	uracil	PROPN
iajs-1146	81	1	[	[	X
iajs-1146	81	2	17	17	NUM
iajs-1146	81	3	]	]	X
iajs-1146	81	4	gave12.the	gave12.the	PRON
iajs-1146	81	5	suggested	suggest	VERB
iajs-1146	81	6	mechanism	mechanism	NOUN
iajs-1146	81	7	of	of	ADP
iajs-1146	81	8	the	the	DET
iajs-1146	81	9	nucleoside	nucleoside	ADJ
iajs-1146	81	10	formation	formation	NOUN
iajs-1146	81	11	12	12	NUM
iajs-1146	81	12	is	be	AUX
iajs-1146	81	13	given	give	VERB
iajs-1146	81	14	below	below	ADP
iajs-1146	81	15	[	[	AUX
iajs-1146	81	16	scheme	scheme	VERB
iajs-1146	81	17	2].the	2].the	DET
iajs-1146	81	18	1hnmr	1hnmr	NUM
iajs-1146	81	19	spectrum	spectrum	NOUN
iajs-1146	81	20	of	of	ADP
iajs-1146	81	21	12	12	NUM
iajs-1146	81	22	showed	show	VERB
iajs-1146	81	23	a	a	DET
iajs-1146	81	24	singlet	singlet	NOUN
iajs-1146	81	25	at	at	ADP
iajs-1146	81	26	2.4	2.4	NUM
iajs-1146	81	27	for	for	ADP
iajs-1146	81	28	p	p	NOUN
iajs-1146	81	29	-	-	PUNCT
iajs-1146	81	30	methyl	methyl	NOUN
iajs-1146	81	31	group	group	NOUN
iajs-1146	81	32	,	,	PUNCT
iajs-1146	81	33	singlet	singlet	NOUN
iajs-1146	81	34	at	at	ADP
iajs-1146	81	35	2.7	2.7	NUM
iajs-1146	81	36	for	for	ADP
iajs-1146	81	37	methylene	methylene	ADJ
iajs-1146	81	38	group	group	NOUN
iajs-1146	81	39	,	,	PUNCT
iajs-1146	81	40	multiplet	multiplet	NOUN
iajs-1146	81	41	at	at	ADP
iajs-1146	81	42	3.7	3.7	NUM
iajs-1146	81	43	-	-	SYM
iajs-1146	81	44	4.9	4.9	NUM
iajs-1146	81	45	for	for	ADP
iajs-1146	81	46	h/	h/	NOUN
iajs-1146	81	47	1	1	NUM
iajs-1146	81	48	,	,	PUNCT
iajs-1146	81	49	h/	h/	NOUN
iajs-1146	81	50	4	4	NUM
iajs-1146	81	51	,	,	PUNCT
iajs-1146	81	52	h-4	h-4	NOUN
iajs-1146	81	53	,	,	PUNCT
iajs-1146	81	54	h-5	h-5	PROPN
iajs-1146	81	55	and	and	CCONJ
iajs-1146	81	56	h	h	NOUN
iajs-1146	81	57	a	a	X
iajs-1146	81	58	,	,	PUNCT
iajs-1146	81	59	hb	hb	PROPN
iajs-1146	81	60	for	for	ADP
iajs-1146	81	61	ch2	ch2	PROPN
iajs-1146	81	62	-	-	PUNCT
iajs-1146	81	63	obz	obz	NOUN
iajs-1146	81	64	,	,	PUNCT
iajs-1146	81	65	doublet	doublet	ADJ
iajs-1146	81	66	at	at	ADP
iajs-1146	81	67	5.8	5.8	NUM
iajs-1146	81	68	for	for	ADP
iajs-1146	81	69	h-/3	h-/3	PRON
iajs-1146	81	70	,	,	PUNCT
iajs-1146	81	71	broad	broad	ADJ
iajs-1146	81	72	signal	signal	NOUN
iajs-1146	81	73	at	at	ADP
iajs-1146	81	74	6.5	6.5	NUM
iajs-1146	81	75	for	for	ADP
iajs-1146	81	76	nh	nh	PROPN
iajs-1146	81	77	uracil	uracil	PROPN
iajs-1146	81	78	and	and	CCONJ
iajs-1146	81	79	multiplet	multiplet	NOUN
iajs-1146	81	80	at	at	ADP
iajs-1146	81	81	6.9	6.9	NUM
iajs-1146	81	82	-	-	SYM
iajs-1146	81	83	8.9	8.9	NUM
iajs-1146	81	84	for	for	ADP
iajs-1146	81	85	aromatic	aromatic	ADJ
iajs-1146	81	86	protons	proton	NOUN
iajs-1146	81	87	.	.	PUNCT
iajs-1146	82	1	the	the	DET
iajs-1146	82	2	treatment	treatment	NOUN
iajs-1146	82	3	of	of	ADP
iajs-1146	82	4	compound	compound	NOUN
iajs-1146	82	5	12	12	NUM
iajs-1146	82	6	with	with	ADP
iajs-1146	82	7	sodium	sodium	NOUN
iajs-1146	82	8	methoxide	methoxide	NOUN
iajs-1146	82	9	in	in	ADP
iajs-1146	82	10	ethanol	ethanol	NOUN
iajs-1146	82	11	gave	give	VERB
iajs-1146	82	12	14	14	NUM
iajs-1146	82	13	as	as	ADP
iajs-1146	82	14	a	a	DET
iajs-1146	82	15	syrup	syrup	NOUN
iajs-1146	82	16	.compound	.compound	ADP
iajs-1146	82	17	10	10	NUM
iajs-1146	82	18	and	and	CCONJ
iajs-1146	82	19	14	14	NUM
iajs-1146	82	20	exhibited	exhibit	VERB
iajs-1146	82	21	a	a	DET
iajs-1146	82	22	biological	biological	ADJ
iajs-1146	82	23	activity	activity	NOUN
iajs-1146	82	24	against	against	ADP
iajs-1146	82	25	e	e	NOUN
iajs-1146	82	26	-	-	NOUN
iajs-1146	82	27	coli	coli	NOUN
iajs-1146	82	28	bacteria	bacteria	NOUN
iajs-1146	82	29	.	.	PUNCT
iajs-1146	83	1	compound	compound	NOUN
iajs-1146	83	2	10	10	NUM
iajs-1146	83	3	exhibited	exhibit	VERB
iajs-1146	83	4	ahigher	ahigher	ADJ
iajs-1146	83	5	degree	degree	NOUN
iajs-1146	83	6	of	of	ADP
iajs-1146	83	7	activity	activity	NOUN
iajs-1146	83	8	than	than	ADP
iajs-1146	83	9	the	the	DET
iajs-1146	83	10	other	other	ADJ
iajs-1146	83	11	(	(	PUNCT
iajs-1146	83	12	table	table	NOUN
iajs-1146	83	13	3	3	NUM
iajs-1146	83	14	)	)	PUNCT
iajs-1146	83	15	.	.	PUNCT
iajs-1146	84	1	references	reference	NOUN
iajs-1146	84	2	1.perigaud	1.perigaud	NUM
iajs-1146	84	3	,	,	PUNCT
iajs-1146	84	4	c.and	c.and	PRON
iajs-1146	84	5	gosselin	gosselin	PROPN
iajs-1146	84	6	,	,	PUNCT
iajs-1146	84	7	g.	g.	PROPN
iajs-1146	84	8	(	(	PUNCT
iajs-1146	84	9	1992	1992	NUM
iajs-1146	84	10	)	)	PUNCT
iajs-1146	84	11	j.l	j.l	PROPN
iajs-1146	84	12	:	:	PUNCT
iajs-1146	84	13	imbach	imbach	NOUN
iajs-1146	84	14	,	,	PUNCT
iajs-1146	84	15	nucleosides	nucleoside	NOUN
iajs-1146	84	16	and	and	CCONJ
iajs-1146	84	17	nucleotides	nucleotide	NOUN
iajs-1146	84	18	;	;	PUNCT
iajs-1146	84	19	11(2	11(2	X
iajs-1146	84	20	-	-	SYM
iajs-1146	84	21	4	4	NUM
iajs-1146	84	22	):	):	PUNCT
iajs-1146	84	23	903	903	NUM
iajs-1146	84	24	-	-	SYM
iajs-1146	84	25	945	945	NUM
iajs-1146	84	26	.	.	NUM
iajs-1146	84	27	2.clercq	2.clercq	NUM
iajs-1146	84	28	,	,	PUNCT
iajs-1146	84	29	de	de	X
iajs-1146	84	30	.	.	X
iajs-1146	84	31	(	(	PUNCT
iajs-1146	84	32	1993	1993	NUM
iajs-1146	84	33	)	)	PUNCT
iajs-1146	84	34	e	e	NOUN
iajs-1146	84	35	,	,	PUNCT
iajs-1146	84	36	adv.virus	adv.viru	NOUN
iajs-1146	84	37	,	,	PUNCT
iajs-1146	84	38	42	42	NUM
iajs-1146	84	39	:	:	SYM
iajs-1146	84	40	1	1	NUM
iajs-1146	84	41	-	-	SYM
iajs-1146	84	42	55	55	NUM
iajs-1146	84	43	.	.	PUNCT
iajs-1146	85	1	3.christina	3.christina	NUM
iajs-1146	85	2	bohman	bohman	NOUN
iajs-1146	85	3	,	,	PUNCT
iajs-1146	85	4	jan	jan	PROPN
iajs-1146	85	5	balzarini	balzarini	PROPN
iajs-1146	85	6	,	,	PUNCT
iajs-1146	85	7	pict	pict	NOUN
iajs-1146	85	8	wigerinck	wigerinck	NOUN
iajs-1146	85	9	,	,	PUNCT
iajs-1146	85	10	arthur	arthur	PROPN
iajs-1146	85	11	van	van	PROPN
iajs-1146	85	12	aershot	aershot	PROPN
iajs-1146	85	13	,	,	PUNCT
iajs-1146	85	14	piet	piet	PROPN
iajs-1146	85	15	herdewijn	herdewijn	NOUN
iajs-1146	85	16	,	,	PUNCT
iajs-1146	85	17	and	and	CCONJ
iajs-1146	85	18	erik	erik	PROPN
iajs-1146	85	19	de	de	PROPN
iajs-1146	85	20	clercq(1994)american	clercq(1994)american	PROPN
iajs-1146	85	21	society	society	NOUN
iajs-1146	85	22	biochemistry	biochemistry	NOUN
iajs-1146	85	23	and	and	CCONJ
iajs-1146	85	24	molecular	molecular	ADJ
iajs-1146	85	25	biology	biology	NOUN
iajs-1146	85	26	,	,	PUNCT
iajs-1146	85	27	ine,269,11,8036	ine,269,11,8036	NOUN
iajs-1146	85	28	-	-	PUNCT
iajs-1146	85	29	8043	8043	NUM
iajs-1146	85	30	.	.	PUNCT
iajs-1146	86	1	4.wang	4.wang	NUM
iajs-1146	86	2	,	,	PUNCT
iajs-1146	86	3	c.c	c.c	PROPN
iajs-1146	86	4	.	.	PROPN
iajs-1146	86	5	(	(	PUNCT
iajs-1146	86	6	1982	1982	NUM
iajs-1146	86	7	)	)	PUNCT
iajs-1146	86	8	treds	tred	NOUN
iajs-1146	86	9	biochem.sci	biochem.sci	NOUN
iajs-1146	86	10	;	;	PUNCT
iajs-1146	86	11	7:354	7:354	NOUN
iajs-1146	86	12	-	-	SYM
iajs-1146	86	13	356	356	NUM
iajs-1146	86	14	.	.	PUNCT
iajs-1146	87	1	5.wang	5.wang	NUM
iajs-1146	87	2	,	,	PUNCT
iajs-1146	87	3	c.c	c.c	PROPN
iajs-1146	87	4	.	.	PROPN
iajs-1146	87	5	(	(	PUNCT
iajs-1146	87	6	1984	1984	NUM
iajs-1146	87	7	)	)	PUNCT
iajs-1146	87	8	j.m	j.m	NOUN
iajs-1146	87	9	ed.chem	ed.chem	NOUN
iajs-1146	87	10	.	.	PUNCT
iajs-1146	88	1	27:1	27:1	NUM
iajs-1146	88	2	-	-	SYM
iajs-1146	88	3	9	9	NUM
iajs-1146	88	4	.	.	PUNCT
iajs-1146	89	1	6.jaffe	6.jaffe	NUM
iajs-1146	89	2	,	,	PUNCT
iajs-1146	89	3	j.j	j.j	PROPN
iajs-1146	89	4	.	.	PROPN
iajs-1146	89	5	and	and	CCONJ
iajs-1146	89	6	ann.n.y	ann.n.y	NOUN
iajs-1146	89	7	.	.	PUNCT
iajs-1146	90	1	(	(	PUNCT
iajs-1146	90	2	1975	1975	NUM
iajs-1146	90	3	)	)	PUNCT
iajs-1146	90	4	,	,	PUNCT
iajs-1146	90	5	acad.sci	acad.sci	X
iajs-1146	90	6	,	,	PUNCT
iajs-1146	90	7	255:306	255:306	NOUN
iajs-1146	90	8	-	-	SYM
iajs-1146	90	9	316	316	NUM
iajs-1146	90	10	.	.	PUNCT
iajs-1146	91	1	7.carsan	7.carsan	NUM
iajs-1146	91	2	,	,	PUNCT
iajs-1146	91	3	d.a.and	d.a.and	PROPN
iajs-1146	91	4	chang	chang	PROPN
iajs-1146	91	5	,	,	PUNCT
iajs-1146	91	6	k.p	k.p	PROPN
iajs-1146	91	7	.	.	PROPN
iajs-1146	91	8	(	(	PUNCT
iajs-1146	91	9	1981	1981	NUM
iajs-1146	91	10	)	)	PUNCT
iajs-1146	91	11	biochem.biophys	biochem.biophy	NOUN
iajs-1146	91	12	,	,	PUNCT
iajs-1146	91	13	res	re	NOUN
iajs-1146	91	14	.	.	PROPN
iajs-1146	91	15	,	,	PUNCT
iajs-1146	91	16	100:1377	100:1377	NUM
iajs-1146	91	17	-	-	SYM
iajs-1146	91	18	1383	1383	NUM
iajs-1146	91	19	.	.	PUNCT
iajs-1146	92	1	8.nelson	8.nelson	NUM
iajs-1146	92	2	,	,	PUNCT
iajs-1146	92	3	d.j	d.j	PROPN
iajs-1146	92	4	.	.	PROPN
iajs-1146	92	5	;	;	PUNCT
iajs-1146	92	6	lafon	lafon	PROPN
iajs-1146	92	7	,	,	PUNCT
iajs-1146	92	8	s.w	s.w	PROPN
iajs-1146	92	9	.	.	PROPN
iajs-1146	92	10	;	;	PUNCT
iajs-1146	92	11	tuttle	tuttle	PROPN
iajs-1146	92	12	,	,	PUNCT
iajs-1146	92	13	j.v	j.v	PROPN
iajs-1146	92	14	.	.	PROPN
iajs-1146	92	15	;	;	PUNCT
iajs-1146	92	16	miller	miller	PROPN
iajs-1146	92	17	,	,	PUNCT
iajs-1146	92	18	w.h	w.h	PROPN
iajs-1146	92	19	.	.	PROPN
iajs-1146	92	20	;	;	PUNCT
iajs-1146	92	21	miller	miller	PROPN
iajs-1146	92	22	,	,	PUNCT
iajs-1146	92	23	r.l	r.l	PROPN
iajs-1146	92	24	.	.	PROPN
iajs-1146	92	25	;	;	PUNCT
iajs-1146	92	26	krenitsky	krenitsky	NOUN
iajs-1146	92	27	,	,	PUNCT
iajs-1146	92	28	t.	t.	NOUN
iajs-1146	92	29	a.	a.	NOUN
iajs-1146	92	30	;	;	PUNCT
iajs-1146	92	31	elion	elion	NOUN
iajs-1146	92	32	,	,	PUNCT
iajs-1146	92	33	g.b	g.b	PROPN
iajs-1146	92	34	.	.	PROPN
iajs-1146	92	35	;	;	PUNCT
iajs-1146	92	36	beodns	beodns	NOUN
iajs-1146	92	37	,	,	PUNCT
iajs-1146	92	38	r.l	r.l	PROPN
iajs-1146	92	39	and	and	CCONJ
iajs-1146	92	40	marr	marr	ADJ
iajs-1146	92	41	,	,	PUNCT
iajs-1146	92	42	j.j,(1979	j.j,(1979	NOUN
iajs-1146	92	43	)	)	PUNCT
iajs-1146	92	44	,	,	PUNCT
iajs-1146	92	45	biol.chem	biol.chem	PROPN
iajs-1146	92	46	.	.	PROPN
iajs-1146	92	47	,	,	PUNCT
iajs-1146	92	48	245:11544	245:11544	NUM
iajs-1146	92	49	-	-	NOUN
iajs-1146	92	50	11549	11549	NUM
iajs-1146	92	51	.	.	PUNCT
iajs-1146	93	1	9.marr	9.marr	NUM
iajs-1146	93	2	,	,	PUNCT
iajs-1146	93	3	j.j.;berens	j.j.;berens	PROPN
iajs-1146	93	4	,	,	PUNCT
iajs-1146	93	5	r.l.;nelson	r.l.;nelson	NOUN
iajs-1146	93	6	,	,	PUNCT
iajs-1146	93	7	d.j.;krenitsky	d.j.;krenitsky	ADV
iajs-1146	93	8	,	,	PUNCT
iajs-1146	93	9	t.a.;spector	t.a.;spector	NOUN
iajs-1146	93	10	,	,	PUNCT
iajs-1146	93	11	t.;lafon	t.;lafon	NUM
iajs-1146	93	12	,	,	PUNCT
iajs-1146	93	13	s.w.and	s.w.and	NOUN
iajs-1146	93	14	elion	elion	NOUN
iajs-1146	93	15	,	,	PUNCT
iajs-1146	93	16	g.b	g.b	PROPN
iajs-1146	93	17	.	.	PUNCT
iajs-1146	93	18	(	(	PUNCT
iajs-1146	93	19	1982	1982	NUM
iajs-1146	93	20	)	)	PUNCT
iajs-1146	93	21	,	,	PUNCT
iajs-1146	93	22	biohem.pharmacol	biohem.pharmacol	PROPN
iajs-1146	93	23	.	.	PROPN
iajs-1146	93	24	,	,	PUNCT
iajs-1146	93	25	31:143	31:143	NUM
iajs-1146	93	26	-	-	SYM
iajs-1146	93	27	148	148	NUM
iajs-1146	93	28	.	.	PUNCT
iajs-1146	94	1	10	10	NUM
iajs-1146	94	2	.	.	PUNCT
iajs-1146	95	1	rainey	rainey	NOUN
iajs-1146	95	2	,	,	PUNCT
iajs-1146	95	3	p.	p.	NOUN
iajs-1146	95	4	;	;	PUNCT
iajs-1146	95	5	santi	santi	ADJ
iajs-1146	95	6	,	,	PUNCT
iajs-1146	95	7	d.v.i	d.v.i	PROPN
iajs-1146	95	8	.	.	PROPN
iajs-1146	95	9	,	,	PUNCT
iajs-1146	95	10	(	(	PUNCT
iajs-1146	95	11	1983	1983	NUM
iajs-1146	95	12	)	)	PUNCT
iajs-1146	95	13	,	,	PUNCT
iajs-1146	95	14	natal	natal	NOUN
iajs-1146	95	15	acad	acad	NOUN
iajs-1146	95	16	.sci.usa	.sci.usa	X
iajs-1146	95	17	,	,	PUNCT
iajs-1146	95	18	80:288	80:288	NUM
iajs-1146	95	19	-	-	SYM
iajs-1146	95	20	292	292	NUM
iajs-1146	95	21	.	.	PUNCT
iajs-1146	96	1	11.eman	11.eman	NUM
iajs-1146	96	2	,	,	PUNCT
iajs-1146	96	3	m.h	m.h	PROPN
iajs-1146	96	4	.	.	PROPN
iajs-1146	96	5	(	(	PUNCT
iajs-1146	96	6	2001	2001	NUM
iajs-1146	96	7	)	)	PUNCT
iajs-1146	96	8	;	;	PUNCT
iajs-1146	96	9	''	''	PUNCT
iajs-1146	96	10	synthesis	synthesis	NOUN
iajs-1146	96	11	of	of	ADP
iajs-1146	96	12	3/	3/	NUM
iajs-1146	96	13	-c	-c	ADJ
iajs-1146	96	14	-	-	PUNCT
iajs-1146	96	15	alkyl	alkyl	ADJ
iajs-1146	96	16	nucleoside	nucleoside	ADJ
iajs-1146	96	17	analogues	analogue	NOUN
iajs-1146	96	18	of	of	ADP
iajs-1146	96	19	possible	possible	ADJ
iajs-1146	96	20	biological	biological	ADJ
iajs-1146	96	21	activity	activity	NOUN
iajs-1146	96	22	''	''	PUNCT
iajs-1146	96	23	;	;	PUNCT
iajs-1146	96	24	.ph.d.thesis	.ph.d.thesis	X
iajs-1146	96	25	,	,	PUNCT
iajs-1146	96	26	baghdad	baghdad	PROPN
iajs-1146	96	27	university	university	NOUN
iajs-1146	96	28	.	.	PUNCT
iajs-1146	97	1	12.boivin	12.boivin	NUM
iajs-1146	97	2	,	,	PUNCT
iajs-1146	97	3	t.l.b.(1987	t.l.b.(1987	NUM
iajs-1146	97	4	)	)	PUNCT
iajs-1146	97	5	,	,	PUNCT
iajs-1146	97	6	tetrahedron	tetrahedron	NOUN
iajs-1146	97	7	,	,	PUNCT
iajs-1146	97	8	43:3309	43:3309	PROPN
iajs-1146	97	9	.	.	PUNCT
iajs-1146	97	10	13.al	13.al	NOUN
iajs-1146	97	11	-	-	PUNCT
iajs-1146	97	12	joboury	joboury	NOUN
iajs-1146	97	13	,	,	PUNCT
iajs-1146	97	14	f.s	f.s	PROPN
iajs-1146	97	15	.	.	PROPN
iajs-1146	97	16	(	(	PUNCT
iajs-1146	97	17	2006	2006	NUM
iajs-1146	97	18	)	)	PUNCT
iajs-1146	97	19	synthesis	synthesis	NOUN
iajs-1146	97	20	of	of	ADP
iajs-1146	97	21	new	new	ADJ
iajs-1146	97	22	spiro	spiro	NOUN
iajs-1146	97	23	,	,	PUNCT
iajs-1146	97	24	fused	fuse	VERB
iajs-1146	97	25	ring	ring	NOUN
iajs-1146	97	26	and	and	CCONJ
iajs-1146	97	27	imine	imine	ADJ
iajs-1146	97	28	derivatives	derivative	NOUN
iajs-1146	97	29	of	of	ADP
iajs-1146	97	30	d	d	NOUN
iajs-1146	97	31	glucose	glucose	NOUN
iajs-1146	97	32	at	at	ADP
iajs-1146	97	33	c-3	c-3	NOUN
iajs-1146	97	34	and	and	CCONJ
iajs-1146	97	35	study	study	VERB
iajs-1146	97	36	their	their	PRON
iajs-1146	97	37	effect	effect	NOUN
iajs-1146	97	38	on	on	ADP
iajs-1146	97	39	serum	serum	NOUN
iajs-1146	97	40	(	(	PUNCT
iajs-1146	97	41	alp	alp	NOUN
iajs-1146	97	42	and	and	CCONJ
iajs-1146	97	43	ggt	ggt	NOUN
iajs-1146	97	44	)	)	PUNCT
iajs-1146	97	45	''	''	PUNCT
iajs-1146	97	46	.	.	PUNCT
iajs-1146	98	1	ph.d.thesis	ph.d.thesis	PROPN
iajs-1146	98	2	,	,	PUNCT
iajs-1146	98	3	baghdad	baghdad	PROPN
iajs-1146	98	4	university	university	PROPN
iajs-1146	98	5	.	.	PUNCT
iajs-1146	99	1	14.glen	14.glen	NUM
iajs-1146	99	2	,	,	PUNCT
iajs-1146	99	3	w.l.;myers	w.l.;myer	NOUN
iajs-1146	99	4	,	,	PUNCT
iajs-1146	99	5	g.s	g.s	PROPN
iajs-1146	99	6	.	.	PROPN
iajs-1146	99	7	and	and	CCONJ
iajs-1146	99	8	grant	grant	PROPN
iajs-1146	99	9	,	,	PUNCT
iajs-1146	99	10	g.a	g.a	PROPN
iajs-1146	99	11	.	.	PROPN
iajs-1146	99	12	(	(	PUNCT
iajs-1146	99	13	1951	1951	NUM
iajs-1146	99	14	)	)	PUNCT
iajs-1146	100	1	j.chem.soc	j.chem.soc	PROPN
iajs-1146	100	2	.	.	PROPN
iajs-1146	100	3	,2569	,2569	PROPN
iajs-1146	100	4	.	.	PUNCT
iajs-1146	101	1	15.butterworth	15.butterworth	NUM
iajs-1146	101	2	,	,	PUNCT
iajs-1146	101	3	r.f	r.f	PROPN
iajs-1146	101	4	.	.	PROPN
iajs-1146	101	5	(	(	PUNCT
iajs-1146	101	6	1971	1971	NUM
iajs-1146	101	7	)	)	PUNCT
iajs-1146	101	8	,	,	PUNCT
iajs-1146	101	9	hanessian	hanessian	NOUN
iajs-1146	101	10	,	,	PUNCT
iajs-1146	101	11	s.synthesis	s.synthesis	NOUN
iajs-1146	101	12	,	,	PUNCT
iajs-1146	101	13	76	76	NUM
iajs-1146	101	14	:	:	SYM
iajs-1146	101	15	16.freestone	16.freestone	NUM
iajs-1146	101	16	,	,	PUNCT
iajs-1146	101	17	a.j	a.j	PROPN
iajs-1146	101	18	.	.	PROPN
iajs-1146	101	19	;	;	PUNCT
iajs-1146	101	20	hough	hough	PROPN
iajs-1146	101	21	,	,	PUNCT
iajs-1146	101	22	l.	l.	PROPN
iajs-1146	101	23	and	and	CCONJ
iajs-1146	101	24	richardson	richardson	PROPN
iajs-1146	101	25	,	,	PUNCT
iajs-1146	101	26	a.c	a.c	PROPN
iajs-1146	101	27	.	.	PROPN
iajs-1146	101	28	(	(	PUNCT
iajs-1146	101	29	1973	1973	NUM
iajs-1146	101	30	)	)	PUNCT
iajs-1146	101	31	,	,	PUNCT
iajs-1146	101	32	carbohydrate	carbohydrate	VERB
iajs-1146	101	33	research	research	NOUN
iajs-1146	101	34	,	,	PUNCT
iajs-1146	101	35	28:382	28:382	NUM
iajs-1146	101	36	.	.	PUNCT
iajs-1146	102	1	17.el	17.el	NUM
iajs-1146	102	2	-	-	SYM
iajs-1146	102	3	barbary	barbary	NOUN
iajs-1146	102	4	,	,	PUNCT
iajs-1146	102	5	a.a.;el	a.a.;el	NOUN
iajs-1146	102	6	-	-	PUNCT
iajs-1146	102	7	brollosy	brollosy	NOUN
iajs-1146	102	8	,	,	PUNCT
iajs-1146	102	9	n.a.and	n.a.and	PROPN
iajs-1146	102	10	pedersen	pedersen	PROPN
iajs-1146	102	11	,	,	PUNCT
iajs-1146	102	12	e.b	e.b	PROPN
iajs-1146	102	13	.	.	PUNCT
iajs-1146	103	1	(	(	PUNCT
iajs-1146	103	2	1996),nielsen	1996),nielsen	NUM
iajs-1146	103	3	c.	c.	PROPN
iajs-1146	103	4	sulur	sulur	PROPN
iajs-1146	103	5	letters,20:36	letters,20:36	PROPN
iajs-1146	103	6	.	.	PUNCT
iajs-1146	104	1	18.al	18.al	NUM
iajs-1146	104	2	-	-	ADJ
iajs-1146	104	3	ghrary	ghrary	ADJ
iajs-1146	104	4	,	,	PUNCT
iajs-1146	104	5	n.f	n.f	PROPN
iajs-1146	104	6	.	.	PROPN
iajs-1146	104	7	(	(	PUNCT
iajs-1146	104	8	1997	1997	NUM
iajs-1146	104	9	)	)	PUNCT
iajs-1146	104	10	,	,	PUNCT
iajs-1146	104	11	''	''	PUNCT
iajs-1146	104	12	sythesis	sythesis	NOUN
iajs-1146	104	13	of	of	ADP
iajs-1146	104	14	3/	3/	NUM
iajs-1146	104	15	,	,	PUNCT
iajs-1146	104	16	3	3	NUM
iajs-1146	104	17	-	-	PUNCT
iajs-1146	104	18	gem	gem	NOUN
iajs-1146	104	19	-	-	PUNCT
iajs-1146	104	20	di	di	NOUN
iajs-1146	104	21	-	-	PUNCT
iajs-1146	104	22	c	c	NOUN
iajs-1146	104	23	-	-	PUNCT
iajs-1146	104	24	nitromethyl	nitromethyl	NOUN
iajs-1146	104	25	nucleoside	nucleoside	NOUN
iajs-1146	104	26	analogues	analogue	NOUN
iajs-1146	104	27	of	of	ADP
iajs-1146	104	28	possible	possible	ADJ
iajs-1146	104	29	biological	biological	ADJ
iajs-1146	104	30	activity	activity	NOUN
iajs-1146	104	31	''	''	PUNCT
iajs-1146	104	32	.ph.d.thesis	.ph.d.thesis	PROPN
iajs-1146	104	33	,	,	PUNCT
iajs-1146	104	34	baghdad	baghdad	PROPN
iajs-1146	104	35	university	university	PROPN
iajs-1146	104	36	.	.	PUNCT
iajs-1146	105	1	19.al	19.al	NUM
iajs-1146	105	2	-	-	PUNCT
iajs-1146	105	3	shara	shara	PROPN
iajs-1146	105	4	,	,	PUNCT
iajs-1146	105	5	ey	ey	NOUN
iajs-1146	105	6	,	,	PUNCT
iajs-1146	105	7	a.a.(2000	a.a.(2000	NUM
iajs-1146	105	8	)	)	PUNCT
iajs-1146	105	9	,	,	PUNCT
iajs-1146	105	10	''	''	PUNCT
iajs-1146	105	11	sythesis	sythesis	NOUN
iajs-1146	105	12	of	of	ADP
iajs-1146	105	13	3/,3/-gem	3/,3/-gem	PROPN
iajs-1146	105	14	-	-	PUNCT
iajs-1146	105	15	di	di	NOUN
iajs-1146	105	16	-	-	PUNCT
iajs-1146	105	17	c	c	NOUN
iajs-1146	105	18	-	-	PUNCT
iajs-1146	105	19	alkyl	alkyl	ADJ
iajs-1146	105	20	and	and	CCONJ
iajs-1146	105	21	3/-c	3/-c	NUM
iajs-1146	105	22	-	-	PUNCT
iajs-1146	105	23	alkyl	alkyl	ADJ
iajs-1146	105	24	nucleoside	nucleoside	NOUN
iajs-1146	105	25	analogues''.ph.d.thesis	analogues''.ph.d.thesis	NOUN
iajs-1146	105	26	,	,	PUNCT
iajs-1146	105	27	baghdad	baghdad	PROPN
iajs-1146	105	28	university	university	PROPN
iajs-1146	105	29	.	.	PUNCT
iajs-1146	106	1	20.kennedy	20.kennedy	NUM
iajs-1146	106	2	j.f	j.f	PROPN
iajs-1146	106	3	.	.	PROPN
iajs-1146	106	4	and	and	CCONJ
iajs-1146	106	5	willams.n.r	willams.n.r	PROPN
iajs-1146	106	6	.	.	PUNCT
iajs-1146	107	1	(	(	PUNCT
iajs-1146	107	2	1979	1979	NUM
iajs-1146	107	3	)	)	PUNCT
iajs-1146	107	4	,	,	PUNCT
iajs-1146	107	5	carbohyd	carbohyd	VERB
iajs-1146	107	6	.chem	.chem	NOUN
iajs-1146	107	7	.	.	PUNCT
iajs-1146	108	1	13:96	13:96	NUM
iajs-1146	108	2	.	.	PUNCT
iajs-1146	109	1	21.rosenthal	21.rosenthal	NUM
iajs-1146	109	2	.a	.a	PROPN
iajs-1146	109	3	.	.	PUNCT
iajs-1146	110	1	and	and	CCONJ
iajs-1146	110	2	dooley.k	dooley.k	PROPN
iajs-1146	110	3	.	.	PUNCT
iajs-1146	111	1	(	(	PUNCT
iajs-1146	111	2	1976	1976	NUM
iajs-1146	111	3	)	)	PUNCT
iajs-1146	111	4	,	,	PUNCT
iajs-1146	111	5	carbohyd	carbohyd	INTJ
iajs-1146	111	6	.	.	PUNCT
iajs-1146	112	1	res	re	NOUN
iajs-1146	112	2	.	.	PROPN
iajs-1146	112	3	,	,	PUNCT
iajs-1146	112	4	52:79	52:79	NUM
iajs-1146	112	5	.	.	PUNCT
iajs-1146	113	1	22.motgmery	22.motgmery	NUM
iajs-1146	113	2	,	,	PUNCT
iajs-1146	113	3	j.a	j.a	PROPN
iajs-1146	113	4	.	.	PROPN
iajs-1146	113	5	and	and	CCONJ
iajs-1146	113	6	thomas	thomas	PROPN
iajs-1146	113	7	,	,	PUNCT
iajs-1146	113	8	h.j	h.j	PROPN
iajs-1146	113	9	.	.	PROPN
iajs-1146	113	10	,(1962),advan.carbohydr	,(1962),advan.carbohydr	PROPN
iajs-1146	113	11	.	.	PUNCT
iajs-1146	114	1	chem	chem	PROPN
iajs-1146	114	2	.	.	PUNCT
iajs-1146	114	3	,	,	PUNCT
iajs-1146	114	4	301	301	NUM
iajs-1146	114	5	:	:	SYM
iajs-1146	114	6	17	17	NUM
iajs-1146	114	7	.	.	PUNCT
iajs-1146	114	8	.	.	PUNCT
iajs-1146	115	1	638:3,.ed.inter.chem.angew,)1964	638:3,.ed.inter.chem.angew,)1964	PROPN
iajs-1146	115	2	(	(	PUNCT
iajs-1146	115	3	.w	.w	PROPN
iajs-1146	115	4	,	,	PUNCT
iajs-1146	115	5	pflidererand	pflidererand	NOUN
iajs-1146	115	6	.	.	PUNCT
iajs-1146	116	1	e	e	X
iajs-1146	116	2	,	,	PUNCT
iajs-1146	116	3	buhler	buhler	NOUN
iajs-1146	116	4	.	.	PUNCT
iajs-1146	117	1	23	23	NUM
iajs-1146	118	1	ibn	ibn	PROPN
iajs-1146	118	2	alhaitham	alhaitham	NOUN
iajs-1146	118	3	j.	j.	PROPN
iajs-1146	119	1	fo	fo	ADP
iajs-1146	119	2	r	r	NOUN
iajs-1146	119	3	pure	pure	ADJ
iajs-1146	119	4	&	&	CCONJ
iajs-1146	119	5	appl	appl	PROPN
iajs-1146	119	6	.	.	PUNCT
iajs-1146	120	1	sc	sc	PROPN
iajs-1146	121	1	i	i	PRON
iajs-1146	121	2	vo	vo	INTJ
iajs-1146	121	3	l.22	l.22	X
iajs-1146	121	4	(	(	PUNCT
iajs-1146	121	5	4	4	NUM
iajs-1146	121	6	)	)	PUNCT
iajs-1146	121	7	2009	2009	NUM
iajs-1146	121	8	(	(	PUNCT
iajs-1146	121	9	scheme	scheme	NOUN
iajs-1146	121	10	1	1	NUM
iajs-1146	121	11	)	)	PUNCT
iajs-1146	121	12	h3c	h3c	VERB
iajs-1146	121	13	h3c	h3c	VERB
iajs-1146	122	1	o	o	NOUN
iajs-1146	123	1	o	o	X
iajs-1146	123	2	o	o	X
iajs-1146	123	3	o	o	X
iajs-1146	124	1	o	o	X
iajs-1146	124	2	ch3	ch3	PROPN
iajs-1146	124	3	ch3	ch3	PROPN
iajs-1146	124	4	ch2c	ch2c	PROPN
iajs-1146	124	5	o	o	PROPN
iajs-1146	124	6	h3c	h3c	VERB
iajs-1146	124	7	ho	ho	PROPN
iajs-1146	125	1	h3c	h3c	VERB
iajs-1146	125	2	h3c	h3c	PROPN
iajs-1146	126	1	o	o	NOUN
iajs-1146	127	1	o	o	X
iajs-1146	127	2	o	o	X
iajs-1146	128	1	o	o	X
iajs-1146	128	2	ch3	ch3	PROPN
iajs-1146	128	3	ch3h3c	ch3h3c	X
iajs-1146	129	1	c	c	PROPN
iajs-1146	129	2	ch	ch	NOUN
iajs-1146	130	1	o	o	INTJ
iajs-1146	130	2	o	o	X
iajs-1146	130	3	h3c	h3c	VERB
iajs-1146	130	4	h3c	h3c	X
iajs-1146	131	1	o	o	X
iajs-1146	131	2	o	o	X
iajs-1146	131	3	o	o	X
iajs-1146	131	4	ph	ph	PROPN
iajs-1146	131	5	n	n	PROPN
iajs-1146	131	6	n	n	NOUN
iajs-1146	131	7	c	c	NOUN
iajs-1146	131	8	ch2	ch2	PROPN
iajs-1146	131	9	r	r	NOUN
iajs-1146	131	10	o	o	NOUN
iajs-1146	131	11	o	o	X
iajs-1146	131	12	ch3	ch3	PROPN
iajs-1146	131	13	ch3	ch3	PROPN
iajs-1146	131	14	o	o	PROPN
iajs-1146	131	15	ho	ho	PROPN
iajs-1146	131	16	ho	ho	PROPN
iajs-1146	131	17	ph	ph	PROPN
iajs-1146	131	18	n	n	PROPN
iajs-1146	131	19	n	n	NOUN
iajs-1146	131	20	c	c	NOUN
iajs-1146	131	21	r	r	NOUN
iajs-1146	131	22	ch2	ch2	NOUN
iajs-1146	132	1	o	o	NOUN
iajs-1146	132	2	o	o	PROPN
iajs-1146	132	3	ch3	ch3	PROPN
iajs-1146	132	4	ch3	ch3	PROPN
iajs-1146	132	5	ho	ho	PROPN
iajs-1146	132	6	ph	ph	PROPN
iajs-1146	132	7	n	n	PROPN
iajs-1146	132	8	n	n	NOUN
iajs-1146	132	9	c	c	NOUN
iajs-1146	132	10	r	r	NOUN
iajs-1146	132	11	ch2	ch2	NOUN
iajs-1146	132	12	o	o	NOUN
iajs-1146	132	13	o	o	X
iajs-1146	132	14	o	o	X
iajs-1146	132	15	ch3	ch3	PROPN
iajs-1146	132	16	ch3	ch3	PROPN
iajs-1146	132	17	bzo	bzo	PROPN
iajs-1146	132	18	ph	ph	PROPN
iajs-1146	132	19	n	n	VERB
iajs-1146	132	20	n	n	NOUN
iajs-1146	132	21	c	c	NOUN
iajs-1146	132	22	r	r	NOUN
iajs-1146	132	23	ch2	ch2	NOUN
iajs-1146	132	24	o	o	NOUN
iajs-1146	132	25	o	o	X
iajs-1146	132	26	o	o	X
iajs-1146	132	27	ch3	ch3	PROPN
iajs-1146	132	28	ch3	ch3	PROPN
iajs-1146	132	29	bzo	bzo	PROPN
iajs-1146	132	30	ph	ph	PROPN
iajs-1146	132	31	n	n	VERB
iajs-1146	132	32	n	n	NOUN
iajs-1146	132	33	c	c	NOUN
iajs-1146	132	34	r	r	NOUN
iajs-1146	132	35	ch2	ch2	NOUN
iajs-1146	132	36	o	o	NOUN
iajs-1146	132	37	o	o	X
iajs-1146	133	1	c	c	NOUN
iajs-1146	133	2	o	o	NOUN
iajs-1146	133	3	cf3	cf3	NOUN
iajs-1146	134	1	o	o	NOUN
iajs-1146	135	1	c	c	NOUN
iajs-1146	135	2	o	o	NOUN
iajs-1146	135	3	cf3	cf3	NOUN
iajs-1146	135	4	bzo	bzo	NOUN
iajs-1146	135	5	ph	ph	PROPN
iajs-1146	135	6	n	n	VERB
iajs-1146	135	7	n	n	NOUN
iajs-1146	135	8	c	c	NOUN
iajs-1146	135	9	r	r	NOUN
iajs-1146	135	10	ch2	ch2	NOUN
iajs-1146	135	11	o	o	PROPN
iajs-1146	135	12	n	n	CCONJ
iajs-1146	135	13	n	n	CCONJ
iajs-1146	135	14	n	n	CCONJ
iajs-1146	135	15	n	n	ADV
iajs-1146	135	16	o	o	NOUN
iajs-1146	135	17	o	o	X
iajs-1146	135	18	ch3	ch3	PROPN
iajs-1146	135	19	ch3	ch3	PROPN
iajs-1146	136	1	o	o	PROPN
iajs-1146	137	1	c	c	NOUN
iajs-1146	137	2	cf3	cf3	NOUN
iajs-1146	137	3	o	o	NOUN
iajs-1146	137	4	n	n	CCONJ
iajs-1146	137	5	n	n	NOUN
iajs-1146	137	6	o	o	NOUN
iajs-1146	137	7	h	h	NOUN
iajs-1146	138	1	oo	oo	INTJ
iajs-1146	138	2	bz	bz	PROPN
iajs-1146	138	3	o	o	INTJ
iajs-1146	138	4	ph	ph	PROPN
iajs-1146	138	5	n	n	PROPN
iajs-1146	138	6	n	n	NOUN
iajs-1146	139	1	c	c	NOUN
iajs-1146	139	2	r	r	NOUN
iajs-1146	139	3	ch2	ch2	NOUN
iajs-1146	139	4	o	o	NOUN
iajs-1146	140	1	c	c	NOUN
iajs-1146	141	1	o	o	NOUN
iajs-1146	141	2	cf3	cf3	NOUN
iajs-1146	141	3	n	n	CCONJ
iajs-1146	141	4	n	n	ADV
iajs-1146	141	5	o	o	NOUN
iajs-1146	141	6	h	h	NOUN
iajs-1146	141	7	o	o	NOUN
iajs-1146	141	8	oho	oho	NOUN
iajs-1146	141	9	ph	ph	VERB
iajs-1146	141	10	n	n	PRON
iajs-1146	141	11	n	n	NOUN
iajs-1146	141	12	c	c	NOUN
iajs-1146	142	1	r	r	NOUN
iajs-1146	142	2	ch2	ch2	NOUN
iajs-1146	143	1	oh	oh	INTJ
iajs-1146	143	2	n	n	CCONJ
iajs-1146	143	3	nn	nn	PROPN
iajs-1146	143	4	n	n	CCONJ
iajs-1146	143	5	ch3	ch3	PROPN
iajs-1146	143	6	o	o	PROPN
iajs-1146	143	7	ch3	ch3	PROPN
iajs-1146	144	1	o	o	X
iajs-1146	144	2	o	o	X
iajs-1146	145	1	oh	oh	INTJ
iajs-1146	146	1	ch2	ch2	NOUN
iajs-1146	146	2	c	c	NOUN
iajs-1146	146	3	r	r	PROPN
iajs-1146	146	4	n	n	CCONJ
iajs-1146	146	5	n	n	CCONJ
iajs-1146	146	6	ph	ph	NOUN
iajs-1146	146	7	ho	ho	PROPN
iajs-1146	146	8	r=	r=	PROPN
iajs-1146	146	9	ch3	ch3	PROPN
iajs-1146	146	10	a	a	PRON
iajs-1146	146	11	:	:	PUNCT
iajs-1146	146	12	dmso	dmso	NOUN
iajs-1146	146	13	,	,	PUNCT
iajs-1146	146	14	ac2o	ac2o	PROPN
iajs-1146	146	15	.	.	PUNCT
iajs-1146	147	1	b	b	X
iajs-1146	147	2	:	:	PUNCT
iajs-1146	147	3	phenyl	phenyl	NOUN
iajs-1146	147	4	hydrazine	hydrazine	NOUN
iajs-1146	147	5	,	,	PUNCT
iajs-1146	147	6	diethyl	diethyl	NOUN
iajs-1146	147	7	amine	amine	PROPN
iajs-1146	147	8	,	,	PUNCT
iajs-1146	147	9	absolute	absolute	ADJ
iajs-1146	147	10	ethanol	ethanol	NOUN
iajs-1146	147	11	.	.	PUNCT
iajs-1146	148	1	c:66%acoh	c:66%acoh	PROPN
iajs-1146	148	2	,	,	PUNCT
iajs-1146	148	3	d	d	NOUN
iajs-1146	148	4	:	:	PUNCT
iajs-1146	148	5	naio4	naio4	NOUN
iajs-1146	148	6	then	then	ADV
iajs-1146	148	7	nabh4	nabh4	NOUN
iajs-1146	148	8	.	.	PUNCT
iajs-1146	149	1	e	e	X
iajs-1146	149	2	:	:	PUNCT
iajs-1146	149	3	bzcl	bzcl	ADJ
iajs-1146	149	4	,	,	PUNCT
iajs-1146	149	5	pyridine	pyridine	NOUN
iajs-1146	149	6	,	,	PUNCT
iajs-1146	149	7	benzene	benzene	NOUN
iajs-1146	149	8	.	.	PUNCT
iajs-1146	150	1	f	f	X
iajs-1146	150	2	:	:	PUNCT
iajs-1146	150	3	cf3cooh	cf3cooh	PROPN
iajs-1146	150	4	,	,	PUNCT
iajs-1146	150	5	ch3cooh	ch3cooh	PROPN
iajs-1146	150	6	,	,	PUNCT
iajs-1146	150	7	h2o	h2o	PROPN
iajs-1146	150	8	than	than	ADP
iajs-1146	150	9	(	(	PUNCT
iajs-1146	150	10	cf3co)2o	cf3co)2o	NOUN
iajs-1146	150	11	,	,	PUNCT
iajs-1146	150	12	benzene	benzene	NOUN
iajs-1146	150	13	,	,	PUNCT
iajs-1146	150	14	pyridine	pyridine	NOUN
iajs-1146	150	15	.	.	PUNCT
iajs-1146	151	1	g	g	NOUN
iajs-1146	151	2	:	:	PUNCT
iajs-1146	151	3	theophylline	theophylline	ADJ
iajs-1146	151	4	mercuric	mercuric	ADJ
iajs-1146	151	5	salt	salt	NOUN
iajs-1146	151	6	,	,	PUNCT
iajs-1146	151	7	xylene	xylene	NOUN
iajs-1146	151	8	,	,	PUNCT
iajs-1146	151	9	δ	δ	PROPN
iajs-1146	151	10	.	.	PUNCT
iajs-1146	152	1	h	h	NOUN
iajs-1146	152	2	:	:	PUNCT
iajs-1146	152	3	ch3ona	ch3ona	PROPN
iajs-1146	152	4	,	,	PUNCT
iajs-1146	152	5	c2	c2	PROPN
iajs-1146	152	6	h5oh	h5oh	PUNCT
iajs-1146	152	7	,	,	PUNCT
iajs-1146	152	8	reflux	reflux	NOUN
iajs-1146	152	9	.	.	PUNCT
iajs-1146	153	1	i	i	PRON
iajs-1146	153	2	:	:	PUNCT
iajs-1146	153	3	silylated	silylate	VERB
iajs-1146	153	4	uracil	uracil	PROPN
iajs-1146	153	5	,	,	PUNCT
iajs-1146	153	6	ch2cl2	ch2cl2	PROPN
iajs-1146	153	7	.	.	PUNCT
iajs-1146	154	1	a	a	PRON
iajs-1146	154	2	b	b	NOUN
iajs-1146	154	3	c	c	NOUN
iajs-1146	155	1	d	d	NOUN
iajs-1146	155	2	i	i	PRON
iajs-1146	155	3	h	h	NOUN
iajs-1146	155	4	f	f	NOUN
iajs-1146	155	5	g	g	PROPN
iajs-1146	155	6	e	e	X
iajs-1146	155	7	(	(	PUNCT
iajs-1146	155	8	4	4	NUM
iajs-1146	155	9	)	)	PUNCT
iajs-1146	155	10	(	(	PUNCT
iajs-1146	155	11	3	3	X
iajs-1146	155	12	)	)	PUNCT
iajs-1146	155	13	(	(	PUNCT
iajs-1146	155	14	2	2	NUM
iajs-1146	155	15	)	)	PUNCT
iajs-1146	155	16	(	(	PUNCT
iajs-1146	155	17	1	1	X
iajs-1146	155	18	)	)	PUNCT
iajs-1146	155	19	(	(	PUNCT
iajs-1146	155	20	10	10	NUM
iajs-1146	155	21	)	)	PUNCT
iajs-1146	155	22	(	(	PUNCT
iajs-1146	155	23	8)	8)	NUM
iajs-1146	155	24	(	(	PUNCT
iajs-1146	155	25	6	6	NUM
iajs-1146	155	26	)	)	PUNCT
iajs-1146	155	27	(	(	PUNCT
iajs-1146	155	28	5	5	NUM
iajs-1146	155	29	)	)	PUNCT
iajs-1146	155	30	(	(	PUNCT
iajs-1146	155	31	12	12	NUM
iajs-1146	155	32	)	)	PUNCT
iajs-1146	155	33	(	(	PUNCT
iajs-1146	155	34	14	14	NUM
iajs-1146	155	35	)	)	PUNCT
iajs-1146	155	36	(	(	PUNCT
iajs-1146	155	37	7	7	X
iajs-1146	155	38	)	)	PUNCT
iajs-1146	155	39	h	h	NOUN
iajs-1146	155	40	ibn	ibn	PROPN
iajs-1146	155	41	alhaitham	alhaitham	NOUN
iajs-1146	155	42	j.	j.	PROPN
iajs-1146	156	1	fo	fo	ADP
iajs-1146	156	2	r	r	NOUN
iajs-1146	156	3	pure	pure	ADJ
iajs-1146	156	4	&	&	CCONJ
iajs-1146	156	5	appl	appl	PROPN
iajs-1146	156	6	.	.	PUNCT
iajs-1146	157	1	sc	sc	PROPN
iajs-1146	158	1	i	i	PRON
iajs-1146	158	2	vo	vo	INTJ
iajs-1146	158	3	l.22	l.22	X
iajs-1146	158	4	(	(	PUNCT
iajs-1146	158	5	4	4	NUM
iajs-1146	158	6	)	)	PUNCT
iajs-1146	158	7	2009	2009	NUM
iajs-1146	158	8	(	(	PUNCT
iajs-1146	158	9	scheme	scheme	NOUN
iajs-1146	158	10	2	2	NUM
iajs-1146	158	11	)	)	PUNCT
iajs-1146	158	12	fig.1	fig.1	ADJ
iajs-1146	158	13	fig	fig	NOUN
iajs-1146	158	14	.	.	PUNCT
iajs-1146	159	1	(	(	PUNCT
iajs-1146	159	2	2	2	NUM
iajs-1146	159	3	)	)	PUNCT
iajs-1146	159	4	n	n	CCONJ
iajs-1146	159	5	n	n	CCONJ
iajs-1146	159	6	n	n	CCONJ
iajs-1146	159	7	n	n	NOUN
iajs-1146	159	8	o	o	NOUN
iajs-1146	160	1	x	x	X
iajs-1146	160	2	hoho	hoho	NOUN
iajs-1146	160	3	ho	ho	PROPN
iajs-1146	160	4	n	n	CCONJ
iajs-1146	160	5	n	n	CCONJ
iajs-1146	160	6	n	n	ADV
iajs-1146	160	7	o	o	NOUN
iajs-1146	160	8	ho	ho	PROPN
iajs-1146	160	9	ho	ho	PROPN
iajs-1146	160	10	ho	ho	PROPN
iajs-1146	161	1	oh	oh	INTJ
iajs-1146	161	2	allopurinol	allopurinol	NOUN
iajs-1146	161	3	riboside	riboside	NOUN
iajs-1146	161	4	(	(	PUNCT
iajs-1146	161	5	x	x	NOUN
iajs-1146	161	6	=	=	NOUN
iajs-1146	161	7	oh	oh	NOUN
iajs-1146	161	8	)	)	PUNCT
iajs-1146	161	9	thiopurinol	thiopurinol	NOUN
iajs-1146	161	10	riboside	riboside	NOUN
iajs-1146	161	11	(	(	PUNCT
iajs-1146	161	12	x	x	X
iajs-1146	161	13	=	=	NOUN
iajs-1146	161	14	sh	sh	NOUN
iajs-1146	161	15	)	)	PUNCT
iajs-1146	161	16	formycin	formycin	PROPN
iajs-1146	161	17	b	b	PROPN
iajs-1146	161	18	n	n	CCONJ
iajs-1146	161	19	n	n	CCONJ
iajs-1146	161	20	n	n	CCONJ
iajs-1146	161	21	n	n	NOUN
iajs-1146	161	22	oho	oho	NOUN
iajs-1146	162	1	ho	ho	PROPN
iajs-1146	163	1	oh	oh	INTJ
iajs-1146	163	2	ch3	ch3	PROPN
iajs-1146	163	3	o	o	X
iajs-1146	164	1	o	o	X
iajs-1146	164	2	ch3	ch3	PROPN
iajs-1146	164	3	r	r	NOUN
iajs-1146	164	4	n	n	ADP
iajs-1146	164	5	n	n	NUM
iajs-1146	164	6	o	o	NOUN
iajs-1146	164	7	ho	ho	INTJ
iajs-1146	165	1	oh	oh	INTJ
iajs-1146	165	2	r	r	NOUN
iajs-1146	165	3	h	h	NOUN
iajs-1146	165	4	o	o	NOUN
iajs-1146	165	5	ho	ho	PROPN
iajs-1146	165	6	)	)	PUNCT
iajs-1146	165	7	ch3ch	ch3ch	NUM
iajs-1146	166	1	oh	oh	INTJ
iajs-1146	166	2	c	c	NOUN
iajs-1146	166	3	h	h	NOUN
iajs-1146	166	4	h	h	NOUN
iajs-1146	166	5	,	,	PUNCT
iajs-1146	166	6	n	n	CCONJ
iajs-1146	166	7	n	n	ADV
iajs-1146	166	8	h3c	h3c	VERB
iajs-1146	166	9	h3c	h3c	VERB
iajs-1146	167	1	o	o	NOUN
iajs-1146	167	2	r	r	NOUN
iajs-1146	167	3	=	=	SYM
iajs-1146	167	4	(	(	PUNCT
iajs-1146	167	5	ibn	ibn	PROPN
iajs-1146	167	6	alhaitham	alhaitham	NOUN
iajs-1146	167	7	j.	j.	PROPN
iajs-1146	168	1	fo	fo	ADP
iajs-1146	168	2	r	r	NOUN
iajs-1146	168	3	pure	pure	ADJ
iajs-1146	168	4	&	&	CCONJ
iajs-1146	168	5	appl	appl	PROPN
iajs-1146	168	6	.	.	PUNCT
iajs-1146	169	1	sc	sc	PROPN
iajs-1146	170	1	i	i	PRON
iajs-1146	170	2	vo	vo	INTJ
iajs-1146	170	3	l.22	l.22	X
iajs-1146	170	4	(	(	PUNCT
iajs-1146	170	5	4	4	NUM
iajs-1146	170	6	)	)	PUNCT
iajs-1146	170	7	2009	2009	NUM
iajs-1146	170	8	fig	fig	NOUN
iajs-1146	170	9	.	.	PUNCT
iajs-1146	171	1	(	(	PUNCT
iajs-1146	171	2	3	3	NUM
iajs-1146	171	3	)	)	PUNCT
iajs-1146	171	4	table	table	NOUN
iajs-1146	171	5	(	(	PUNCT
iajs-1146	171	6	1	1	NUM
iajs-1146	171	7	):	):	PUNCT
iajs-1146	171	8	characteristic	characteristic	ADJ
iajs-1146	171	9	ir	ir	PROPN
iajs-1146	171	10	absorption	absorption	NOUN
iajs-1146	171	11	bands	band	NOUN
iajs-1146	171	12	of	of	ADP
iajs-1146	171	13	the	the	DET
iajs-1146	171	14	new	new	ADJ
iajs-1146	171	15	derivatives	derivative	NOUN
iajs-1146	171	16	infrared	infrare	VERB
iajs-1146	171	17	data	datum	NOUN
iajs-1146	171	18	(	(	PUNCT
iajs-1146	171	19	υmax	υmax	PROPN
iajs-1146	171	20	cm-1	cm-1	PROPN
iajs-1146	171	21	)	)	PUNCT
iajs-1146	171	22	(	(	PUNCT
iajs-1146	171	23	film	film	NOUN
iajs-1146	171	24	)	)	PUNCT
iajs-1146	171	25	compound	compound	NOUN
iajs-1146	171	26	no	no	INTJ
iajs-1146	171	27	.	.	PUNCT
iajs-1146	172	1	(	(	PUNCT
iajs-1146	172	2	c	c	X
iajs-1146	172	3	=	=	SYM
iajs-1146	172	4	c	c	NOUN
iajs-1146	172	5	)	)	PUNCT
iajs-1146	172	6	stretching	stretch	VERB
iajs-1146	172	7	aliphatic	aliphatic	ADJ
iajs-1146	172	8	1640;(co)1690	1640;(co)1690	NUM
iajs-1146	172	9	;	;	PUNCT
iajs-1146	172	10	(	(	PUNCT
iajs-1146	172	11	c	c	X
iajs-1146	172	12	=	=	SYM
iajs-1146	172	13	c	c	NOUN
iajs-1146	172	14	)	)	PUNCT
iajs-1146	172	15	aromatic	aromatic	ADJ
iajs-1146	172	16	ring	ring	NOUN
iajs-1146	172	17	1480	1480	NUM
iajs-1146	172	18	–	–	PUNCT
iajs-1146	172	19	1610	1610	NUM
iajs-1146	172	20	;	;	PUNCT
iajs-1146	172	21	(	(	PUNCT
iajs-1146	172	22	c	c	X
iajs-1146	172	23	=	=	SYM
iajs-1146	172	24	c	c	NOUN
iajs-1146	172	25	)	)	PUNCT
iajs-1146	172	26	bending	bend	VERB
iajs-1146	172	27	815	815	NUM
iajs-1146	172	28	2	2	NUM
iajs-1146	172	29	(	(	PUNCT
iajs-1146	172	30	c	c	NOUN
iajs-1146	172	31	=	=	SYM
iajs-1146	172	32	c	c	NOUN
iajs-1146	172	33	)	)	PUNCT
iajs-1146	172	34	aromatic	aromatic	ADJ
iajs-1146	172	35	ring	ring	NOUN
iajs-1146	172	36	1460	1460	NUM
iajs-1146	172	37	-	-	SYM
iajs-1146	172	38	1630;(c	1630;(c	NUM
iajs-1146	172	39	=	=	NOUN
iajs-1146	172	40	n	n	CCONJ
iajs-1146	172	41	)	)	PUNCT
iajs-1146	172	42	1660	1660	NUM
iajs-1146	172	43	;	;	PUNCT
iajs-1146	172	44	(	(	PUNCT
iajs-1146	172	45	c	c	X
iajs-1146	172	46	=	=	SYM
iajs-1146	172	47	c	c	NOUN
iajs-1146	172	48	)	)	PUNCT
iajs-1146	172	49	bending	bend	VERB
iajs-1146	172	50	780	780	NUM
iajs-1146	172	51	.	.	PUNCT
iajs-1146	173	1	3	3	NUM
iajs-1146	173	2	(	(	PUNCT
iajs-1146	173	3	oh	oh	INTJ
iajs-1146	173	4	)	)	PUNCT
iajs-1146	173	5	3400	3400	NUM
iajs-1146	173	6	;	;	PUNCT
iajs-1146	173	7	(	(	PUNCT
iajs-1146	173	8	c	c	X
iajs-1146	173	9	=	=	SYM
iajs-1146	173	10	c	c	NOUN
iajs-1146	173	11	)	)	PUNCT
iajs-1146	173	12	aromatic	aromatic	ADJ
iajs-1146	173	13	ring	ring	NOUN
iajs-1146	173	14	1480	1480	NUM
iajs-1146	173	15	-	-	SYM
iajs-1146	173	16	1640,(c	1640,(c	NUM
iajs-1146	173	17	=	=	SYM
iajs-1146	173	18	n	n	CCONJ
iajs-1146	173	19	)	)	PUNCT
iajs-1146	173	20	1660	1660	NUM
iajs-1146	173	21	;	;	PUNCT
iajs-1146	173	22	(	(	PUNCT
iajs-1146	173	23	c	c	X
iajs-1146	173	24	=	=	SYM
iajs-1146	173	25	c	c	NOUN
iajs-1146	173	26	)	)	PUNCT
iajs-1146	173	27	bending	bend	VERB
iajs-1146	173	28	800	800	NUM
iajs-1146	173	29	.	.	NOUN
iajs-1146	173	30	4	4	NUM
iajs-1146	173	31	(	(	PUNCT
iajs-1146	173	32	oh	oh	INTJ
iajs-1146	173	33	)	)	PUNCT
iajs-1146	173	34	broad	broad	NOUN
iajs-1146	173	35	3385;(c	3385;(c	NUM
iajs-1146	173	36	=	=	SYM
iajs-1146	173	37	c	c	NOUN
iajs-1146	173	38	)	)	PUNCT
iajs-1146	173	39	aromatic	aromatic	ADJ
iajs-1146	173	40	ring1500	ring1500	PROPN
iajs-1146	173	41	-	-	PUNCT
iajs-1146	173	42	1620;(c	1620;(c	PROPN
iajs-1146	173	43	=	=	NOUN
iajs-1146	173	44	n	n	CCONJ
iajs-1146	173	45	)	)	PUNCT
iajs-1146	173	46	1640	1640	NUM
iajs-1146	173	47	(	(	PUNCT
iajs-1146	173	48	c	c	NOUN
iajs-1146	173	49	=	=	SYM
iajs-1146	173	50	c	c	NOUN
iajs-1146	173	51	)	)	PUNCT
iajs-1146	173	52	bending	bend	VERB
iajs-1146	173	53	815	815	NUM
iajs-1146	173	54	.	.	NOUN
iajs-1146	173	55	5	5	NUM
iajs-1146	173	56	(	(	PUNCT
iajs-1146	173	57	co)1700;(c	co)1700;(c	VERB
iajs-1146	173	58	=	=	ADJ
iajs-1146	173	59	c	c	NOUN
iajs-1146	173	60	)	)	PUNCT
iajs-1146	173	61	aromatic	aromatic	ADJ
iajs-1146	173	62	ring	ring	NOUN
iajs-1146	173	63	1480	1480	NUM
iajs-1146	173	64	-	-	SYM
iajs-1146	173	65	1610	1610	NUM
iajs-1146	173	66	;	;	PUNCT
iajs-1146	173	67	(	(	PUNCT
iajs-1146	173	68	c	c	X
iajs-1146	173	69	=	=	SYM
iajs-1146	173	70	n)1630;(c	n)1630;(c	NOUN
iajs-1146	173	71	=	=	SYM
iajs-1146	173	72	c)bending	c)bende	VERB
iajs-1146	173	73	for	for	ADP
iajs-1146	173	74	p	p	NOUN
iajs-1146	173	75	-	-	PUNCT
iajs-1146	173	76	substitutions	substitution	NOUN
iajs-1146	173	77	ring	ring	NOUN
iajs-1146	173	78	830	830	NUM
iajs-1146	173	79	;	;	PUNCT
iajs-1146	173	80	(	(	PUNCT
iajs-1146	173	81	c	c	X
iajs-1146	173	82	=	=	SYM
iajs-1146	173	83	c)bending	c)bende	VERB
iajs-1146	173	84	for	for	ADP
iajs-1146	173	85	benzoyl	benzoyl	NOUN
iajs-1146	173	86	ring	ring	NOUN
iajs-1146	173	87	670	670	NUM
iajs-1146	173	88	.	.	PROPN
iajs-1146	173	89	6	6	NUM
iajs-1146	173	90	(	(	PUNCT
iajs-1146	173	91	co	co	NOUN
iajs-1146	173	92	)	)	PUNCT
iajs-1146	173	93	for	for	ADP
iajs-1146	173	94	obz	obz	NOUN
iajs-1146	173	95	1710;(co	1710;(co	NUM
iajs-1146	173	96	)	)	PUNCT
iajs-1146	173	97	for	for	ADP
iajs-1146	173	98	co2cf3	co2cf3	PROPN
iajs-1146	173	99	1690;(c	1690;(c	NUM
iajs-1146	173	100	=	=	SYM
iajs-1146	173	101	c	c	NOUN
iajs-1146	173	102	)	)	PUNCT
iajs-1146	173	103	aromatic	aromatic	ADJ
iajs-1146	173	104	ring	ring	NOUN
iajs-1146	173	105	1460	1460	NUM
iajs-1146	173	106	-	-	SYM
iajs-1146	173	107	1610;(c	1610;(c	NUM
iajs-1146	173	108	=	=	SYM
iajs-1146	173	109	n	n	CCONJ
iajs-1146	173	110	)	)	PUNCT
iajs-1146	173	111	1630;(c	1630;(c	NUM
iajs-1146	173	112	=	=	SYM
iajs-1146	173	113	c	c	NOUN
iajs-1146	173	114	)	)	PUNCT
iajs-1146	173	115	bending	bend	VERB
iajs-1146	173	116	810	810	NUM
iajs-1146	173	117	-	-	SYM
iajs-1146	173	118	720	720	NUM
iajs-1146	173	119	.	.	NOUN
iajs-1146	173	120	7	7	NUM
iajs-1146	173	121	(	(	PUNCT
iajs-1146	173	122	co	co	NOUN
iajs-1146	173	123	)	)	PUNCT
iajs-1146	173	124	for	for	ADP
iajs-1146	173	125	obz	obz	NUM
iajs-1146	173	126	and	and	CCONJ
iajs-1146	173	127	co2cf3	co2cf3	PROPN
iajs-1146	173	128	1700,1685;(co	1700,1685;(co	NUM
iajs-1146	173	129	)	)	PUNCT
iajs-1146	173	130	for	for	ADP
iajs-1146	173	131	conh	conh	NOUN
iajs-1146	173	132	1675;(c	1675;(c	PROPN
iajs-1146	173	133	=	=	SYM
iajs-1146	173	134	c	c	NOUN
iajs-1146	173	135	)	)	PUNCT
iajs-1146	173	136	aromatic	aromatic	ADJ
iajs-1146	173	137	ring	ring	NOUN
iajs-1146	173	138	1445	1445	NUM
iajs-1146	173	139	-	-	PUNCT
iajs-1146	173	140	1620;(c	1620;(c	PROPN
iajs-1146	173	141	=	=	PROPN
iajs-1146	173	142	n	n	CCONJ
iajs-1146	173	143	)	)	PUNCT
iajs-1146	173	144	1640	1640	NUM
iajs-1146	173	145	(	(	PUNCT
iajs-1146	173	146	c	c	NOUN
iajs-1146	173	147	=	=	SYM
iajs-1146	173	148	c	c	NOUN
iajs-1146	173	149	)	)	PUNCT
iajs-1146	173	150	bending	bend	VERB
iajs-1146	173	151	700,800	700,800	NUM
iajs-1146	173	152	.	.	NOUN
iajs-1146	173	153	8	8	NUM
iajs-1146	173	154	(	(	PUNCT
iajs-1146	173	155	oh)3340,(co	oh)3340,(co	NOUN
iajs-1146	173	156	)	)	PUNCT
iajs-1146	174	1	1680;(c	1680;(c	PROPN
iajs-1146	174	2	=	=	SYM
iajs-1146	174	3	c)1520	c)1520	PROPN
iajs-1146	174	4	-	-	PUNCT
iajs-1146	174	5	1600;(c	1600;(c	PROPN
iajs-1146	174	6	=	=	SYM
iajs-1146	174	7	n)1610	n)1610	PROPN
iajs-1146	174	8	;	;	PUNCT
iajs-1146	174	9	(	(	PUNCT
iajs-1146	174	10	c	c	X
iajs-1146	174	11	=	=	SYM
iajs-1146	174	12	c	c	NOUN
iajs-1146	174	13	)	)	PUNCT
iajs-1146	174	14	bending	bend	VERB
iajs-1146	174	15	820	820	NUM
iajs-1146	174	16	.	.	PUNCT
iajs-1146	175	1	10	10	NUM
iajs-1146	175	2	(	(	PUNCT
iajs-1146	175	3	nh)3410;(co	nh)3410;(co	NOUN
iajs-1146	175	4	)	)	PUNCT
iajs-1146	175	5	for	for	ADP
iajs-1146	175	6	obz	obz	PROPN
iajs-1146	175	7	andco2cf3	andco2cf3	NOUN
iajs-1146	175	8	1700,1680;conh	1700,1680;conh	NUM
iajs-1146	175	9	1670;(c	1670;(c	NUM
iajs-1146	175	10	=	=	SYM
iajs-1146	175	11	c),aromatic	c),aromatic	ADJ
iajs-1146	175	12	ring	ring	NOUN
iajs-1146	175	13	1460	1460	NUM
iajs-1146	175	14	-	-	SYM
iajs-1146	175	15	1610;(c	1610;(c	NUM
iajs-1146	175	16	=	=	ADJ
iajs-1146	175	17	n)1620	n)1620	PROPN
iajs-1146	175	18	(	(	PUNCT
iajs-1146	175	19	c	c	X
iajs-1146	175	20	=	=	SYM
iajs-1146	175	21	c	c	NOUN
iajs-1146	175	22	)	)	PUNCT
iajs-1146	175	23	bending	bend	VERB
iajs-1146	175	24	710,825	710,825	NUM
iajs-1146	175	25	.	.	PUNCT
iajs-1146	176	1	12	12	NUM
iajs-1146	176	2	(	(	PUNCT
iajs-1146	176	3	nh	nh	NOUN
iajs-1146	176	4	,	,	PUNCT
iajs-1146	176	5	oh)3200,3400;(co)1670	oh)3200,3400;(co)1670	PROPN
iajs-1146	176	6	;	;	PUNCT
iajs-1146	176	7	(	(	PUNCT
iajs-1146	176	8	c	c	X
iajs-1146	176	9	=	=	SYM
iajs-1146	176	10	c	c	NOUN
iajs-1146	176	11	)	)	PUNCT
iajs-1146	176	12	aromatic	aromatic	ADJ
iajs-1146	176	13	ring	ring	NOUN
iajs-1146	176	14	1500	1500	NUM
iajs-1146	176	15	-	-	SYM
iajs-1146	176	16	1610	1610	NUM
iajs-1146	176	17	;	;	PUNCT
iajs-1146	176	18	(	(	PUNCT
iajs-1146	176	19	c	c	X
iajs-1146	176	20	=	=	X
iajs-1146	176	21	n)1620	n)1620	PROPN
iajs-1146	176	22	;	;	PUNCT
iajs-1146	176	23	(	(	PUNCT
iajs-1146	176	24	c	c	X
iajs-1146	176	25	=	=	SYM
iajs-1146	176	26	c	c	NOUN
iajs-1146	176	27	)	)	PUNCT
iajs-1146	176	28	bending	bend	VERB
iajs-1146	176	29	810	810	NUM
iajs-1146	176	30	.	.	PUNCT
iajs-1146	177	1	14	14	NUM
iajs-1146	177	2	h3	h3	NOUN
iajs-1146	177	3	c	c	NOUN
iajs-1146	177	4	h3c	h3c	VERB
iajs-1146	178	1	o	o	X
iajs-1146	179	1	o	o	X
iajs-1146	179	2	o	o	X
iajs-1146	179	3	o	o	X
iajs-1146	179	4	o	o	X
iajs-1146	179	5	ch3	ch3	PROPN
iajs-1146	179	6	ch	ch	PROPN
iajs-1146	179	7	3nh	3nh	PROPN
iajs-1146	180	1	o	o	X
iajs-1146	181	1	o	o	X
iajs-1146	181	2	o	o	X
iajs-1146	181	3	h3c	h3c	VERB
iajs-1146	181	4	h3c	h3c	VERB
iajs-1146	182	1	o	o	NOUN
iajs-1146	183	1	o	o	X
iajs-1146	184	1	o	o	X
iajs-1146	185	1	o	o	X
iajs-1146	185	2	o	o	X
iajs-1146	185	3	o	o	X
iajs-1146	185	4	n	n	CCONJ
iajs-1146	185	5	och3	och3	ADJ
iajs-1146	186	1	o	o	X
iajs-1146	186	2	o	o	X
iajs-1146	186	3	ch3	ch3	PROPN
iajs-1146	186	4	ch3	ch3	PROPN
iajs-1146	186	5	ibn	ibn	PROPN
iajs-1146	186	6	alhaitham	alhaitham	PROPN
iajs-1146	186	7	j.	j.	PROPN
iajs-1146	187	1	fo	fo	ADP
iajs-1146	187	2	r	r	NOUN
iajs-1146	187	3	pure	pure	ADJ
iajs-1146	187	4	&	&	CCONJ
iajs-1146	187	5	appl	appl	PROPN
iajs-1146	187	6	.	.	PUNCT
iajs-1146	188	1	sc	sc	PROPN
iajs-1146	189	1	i	i	PRON
iajs-1146	189	2	vo	vo	INTJ
iajs-1146	189	3	l.22	l.22	X
iajs-1146	189	4	(	(	PUNCT
iajs-1146	189	5	4	4	NUM
iajs-1146	189	6	)	)	PUNCT
iajs-1146	189	7	2009	2009	NUM
iajs-1146	189	8	table	table	NOUN
iajs-1146	189	9	(	(	PUNCT
iajs-1146	189	10	2	2	NUM
iajs-1146	189	11	):	):	PUNCT
iajs-1146	189	12	physical	physical	ADJ
iajs-1146	189	13	properties	property	NOUN
iajs-1146	189	14	and	and	CCONJ
iajs-1146	189	15	elemental	elemental	ADJ
iajs-1146	189	16	analysis	analysis	NOUN
iajs-1146	189	17	for	for	ADP
iajs-1146	189	18	new	new	ADJ
iajs-1146	189	19	derivatives	derivative	NOUN
iajs-1146	189	20	.	.	PUNCT
iajs-1146	190	1	elemental	elemental	ADJ
iajs-1146	190	2	analysis	analysis	NOUN
iajs-1146	190	3	calculated(found	calculated(found	NOUN
iajs-1146	190	4	)	)	PUNCT
iajs-1146	191	1	yiel	yiel	PROPN
iajs-1146	191	2	d	d	PROPN
iajs-1146	191	3	%	%	NOUN
iajs-1146	191	4	n%	n%	VERB
iajs-1146	192	1	h%	h%	ADV
iajs-1146	192	2	c%	c%	ADJ
iajs-1146	192	3	rat	rat	NOUN
iajs-1146	192	4	of	of	ADP
iajs-1146	192	5	flow	flow	NOUN
iajs-1146	192	6	in	in	ADP
iajs-1146	192	7	thin	thin	ADJ
iajs-1146	192	8	lyer	lyer	PROPN
iajs-1146	192	9	chromatograp	chromatograp	PROPN
iajs-1146	192	10	hy	hy	PROPN
iajs-1146	192	11	(	(	PUNCT
iajs-1146	192	12	tlc),rf	tlc),rf	X
iajs-1146	192	13	(	(	PUNCT
iajs-1146	192	14	solvent	solvent	NOUN
iajs-1146	192	15	)	)	PUNCT
iajs-1146	192	16	physic	physic	NOUN
iajs-1146	192	17	al	al	PROPN
iajs-1146	192	18	state	state	PROPN
iajs-1146	192	19	formula	formula	NOUN
iajs-1146	192	20	&	&	CCONJ
iajs-1146	192	21	comp	comp	PROPN
iajs-1146	192	22	.	.	PUNCT
iajs-1146	193	1	no	no	INTJ
iajs-1146	193	2	.	.	NOUN
iajs-1146	194	1	65	65	NUM
iajs-1146	194	2	6.95	6.95	NUM
iajs-1146	194	3	(	(	PUNCT
iajs-1146	194	4	7.15	7.15	NUM
iajs-1146	194	5	)	)	PUNCT
iajs-1146	194	6	67.37	67.37	NUM
iajs-1146	194	7	(	(	PUNCT
iajs-1146	194	8	67.1	67.1	NUM
iajs-1146	194	9	)	)	PUNCT
iajs-1146	194	10	0.62	0.62	NUM
iajs-1146	194	11	(	(	PUNCT
iajs-1146	194	12	benzene	benzene	NOUN
iajs-1146	194	13	:	:	PUNCT
iajs-1146	194	14	ether	ether	NOUN
iajs-1146	194	15	9:1	9:1	NUM
iajs-1146	194	16	)	)	PUNCT
iajs-1146	194	17	syrup	syrup	NOUN
iajs-1146	194	18	c21	c21	NOUN
iajs-1146	194	19	h26	h26	PROPN
iajs-1146	194	20	o6	o6	PROPN
iajs-1146	194	21	(	(	PUNCT
iajs-1146	194	22	2	2	NUM
iajs-1146	194	23	)	)	PUNCT
iajs-1146	194	24	50.2	50.2	NUM
iajs-1146	194	25	7	7	NUM
iajs-1146	194	26	6.03	6.03	NUM
iajs-1146	194	27	(	(	PUNCT
iajs-1146	194	28	5.89	5.89	NUM
iajs-1146	194	29	)	)	PUNCT
iajs-1146	194	30	6.89	6.89	NUM
iajs-1146	194	31	(	(	PUNCT
iajs-1146	194	32	6.77	6.77	NUM
iajs-1146	194	33	)	)	PUNCT
iajs-1146	194	34	69.82	69.82	NUM
iajs-1146	194	35	(	(	PUNCT
iajs-1146	194	36	70	70	NUM
iajs-1146	194	37	)	)	PUNCT
iajs-1146	194	38	0.57	0.57	NUM
iajs-1146	194	39	(	(	PUNCT
iajs-1146	194	40	benzene	benzene	NOUN
iajs-1146	194	41	:	:	PUNCT
iajs-1146	194	42	nhexane9:1	nhexane9:1	ADJ
iajs-1146	194	43	)	)	PUNCT
iajs-1146	194	44	syrup	syrup	NOUN
iajs-1146	194	45	c27h32n2o5	c27h32n2o5	PROPN
iajs-1146	194	46	(	(	PUNCT
iajs-1146	194	47	3	3	X
iajs-1146	194	48	)	)	PUNCT
iajs-1146	194	49	elemental	elemental	ADJ
iajs-1146	194	50	analysis	analysis	NOUN
iajs-1146	194	51	calculated(found	calculated(found	NOUN
iajs-1146	194	52	)	)	PUNCT
iajs-1146	195	1	yiel	yiel	PROPN
iajs-1146	195	2	d	d	PROPN
iajs-1146	195	3	%	%	NOUN
iajs-1146	195	4	n%	n%	VERB
iajs-1146	196	1	h%	h%	ADV
iajs-1146	196	2	c%	c%	ADJ
iajs-1146	196	3	rat	rat	NOUN
iajs-1146	196	4	of	of	ADP
iajs-1146	196	5	flow	flow	NOUN
iajs-1146	196	6	in	in	ADP
iajs-1146	196	7	thin	thin	ADJ
iajs-1146	196	8	lyer	lyer	PROPN
iajs-1146	196	9	chromatograp	chromatograp	PROPN
iajs-1146	196	10	hy	hy	PROPN
iajs-1146	196	11	(	(	PUNCT
iajs-1146	196	12	tlc),rf	tlc),rf	X
iajs-1146	196	13	(	(	PUNCT
iajs-1146	196	14	solvent	solvent	NOUN
iajs-1146	196	15	)	)	PUNCT
iajs-1146	196	16	physic	physic	NOUN
iajs-1146	196	17	al	al	PROPN
iajs-1146	196	18	state	state	PROPN
iajs-1146	196	19	formula	formula	NOUN
iajs-1146	196	20	&	&	CCONJ
iajs-1146	196	21	comp	comp	PROPN
iajs-1146	196	22	.	.	PUNCT
iajs-1146	197	1	no	no	INTJ
iajs-1146	197	2	.	.	NOUN
iajs-1146	198	1	60.5	60.5	NUM
iajs-1146	198	2	5	5	NUM
iajs-1146	198	3	6.6	6.6	NUM
iajs-1146	198	4	(	(	PUNCT
iajs-1146	198	5	6.35	6.35	NUM
iajs-1146	198	6	)	)	PUNCT
iajs-1146	198	7	6.6	6.6	NUM
iajs-1146	198	8	(	(	PUNCT
iajs-1146	198	9	6.15	6.15	NUM
iajs-1146	198	10	)	)	PUNCT
iajs-1146	198	11	67.92	67.92	NUM
iajs-1146	198	12	(	(	PUNCT
iajs-1146	198	13	68.12	68.12	NUM
iajs-1146	198	14	)	)	PUNCT
iajs-1146	198	15	03.5	03.5	NUM
iajs-1146	198	16	(	(	PUNCT
iajs-1146	198	17	benzene	benzene	NOUN
iajs-1146	198	18	;	;	PUNCT
iajs-1146	198	19	methanol	methanol	NOUN
iajs-1146	198	20	9.5	9.5	NUM
iajs-1146	198	21	:	:	SYM
iajs-1146	198	22	0.5	0.5	NUM
iajs-1146	198	23	)	)	PUNCT
iajs-1146	198	24	syrup	syrup	NOUN
iajs-1146	198	25	c24h28n2o5	c24h28n2o5	NOUN
iajs-1146	198	26	(	(	PUNCT
iajs-1146	198	27	4	4	NUM
iajs-1146	198	28	)	)	PUNCT
iajs-1146	198	29	30.2	30.2	NUM
iajs-1146	198	30	7.10	7.10	NUM
iajs-1146	198	31	(	(	PUNCT
iajs-1146	198	32	6.88	6.88	NUM
iajs-1146	198	33	)	)	PUNCT
iajs-1146	198	34	6.59	6.59	NUM
iajs-1146	198	35	(	(	PUNCT
iajs-1146	198	36	6.25	6.25	NUM
iajs-1146	198	37	)	)	PUNCT
iajs-1146	198	38	70.05	70.05	NUM
iajs-1146	198	39	(	(	PUNCT
iajs-1146	198	40	70.3	70.3	NUM
iajs-1146	198	41	)	)	PUNCT
iajs-1146	198	42	0.42	0.42	NUM
iajs-1146	198	43	(	(	PUNCT
iajs-1146	198	44	benzene	benzene	NOUN
iajs-1146	198	45	;	;	PUNCT
iajs-1146	198	46	methanol	methanol	NOUN
iajs-1146	198	47	9:0.5	9:0.5	NUM
iajs-1146	198	48	)	)	PUNCT
iajs-1146	198	49	syrup	syrup	NOUN
iajs-1146	198	50	c23h26n2o4	c23h26n2o4	NOUN
iajs-1146	198	51	(	(	PUNCT
iajs-1146	198	52	5	5	NUM
iajs-1146	198	53	)	)	PUNCT
iajs-1146	198	54	67.8	67.8	NUM
iajs-1146	198	55	5.62	5.62	NUM
iajs-1146	198	56	5.33	5.33	NUM
iajs-1146	198	57	)	)	PUNCT
iajs-1146	198	58	(	(	PUNCT
iajs-1146	198	59	6.02	6.02	NUM
iajs-1146	198	60	(	(	PUNCT
iajs-1146	198	61	6.04	6.04	NUM
iajs-1146	198	62	)	)	PUNCT
iajs-1146	198	63	72.28	72.28	NUM
iajs-1146	198	64	(	(	PUNCT
iajs-1146	198	65	71.91	71.91	NUM
iajs-1146	198	66	)	)	PUNCT
iajs-1146	198	67	0.72	0.72	NUM
iajs-1146	198	68	(	(	PUNCT
iajs-1146	198	69	benzene;ethy	benzene;ethy	PROPN
iajs-1146	198	70	la	la	PROPN
iajs-1146	198	71	cetate	cetate	PROPN
iajs-1146	198	72	9.5;0.5	9.5;0.5	NUM
iajs-1146	198	73	)	)	PUNCT
iajs-1146	198	74	syrup	syrup	NOUN
iajs-1146	198	75	c30h30n2o5	c30h30n2o5	NOUN
iajs-1146	198	76	(	(	PUNCT
iajs-1146	198	77	6	6	NUM
iajs-1146	198	78	)	)	PUNCT
iajs-1146	198	79	48	48	NUM
iajs-1146	198	80	4.3	4.3	NUM
iajs-1146	198	81	3.98	3.98	NUM
iajs-1146	198	82	)	)	PUNCT
iajs-1146	198	83	(	(	PUNCT
iajs-1146	198	84	3.69	3.69	NUM
iajs-1146	198	85	(	(	PUNCT
iajs-1146	198	86	3.49	3.49	NUM
iajs-1146	198	87	)	)	PUNCT
iajs-1146	198	88	57.23	57.23	NUM
iajs-1146	198	89	(	(	PUNCT
iajs-1146	198	90	56.89	56.89	NUM
iajs-1146	198	91	)	)	PUNCT
iajs-1146	198	92	0.65	0.65	NUM
iajs-1146	198	93	(	(	PUNCT
iajs-1146	198	94	benzene	benzene	NOUN
iajs-1146	198	95	:	:	PUNCT
iajs-1146	198	96	methanol	methanol	NOUN
iajs-1146	198	97	9:0.5	9:0.5	NUM
iajs-1146	198	98	)	)	PUNCT
iajs-1146	198	99	syrup	syrup	NOUN
iajs-1146	198	100	c31h24n2	c31h24n2	PROPN
iajs-1146	198	101	o7f6	o7f6	PROPN
iajs-1146	198	102	(	(	PUNCT
iajs-1146	198	103	7	7	NUM
iajs-1146	198	104	)	)	PUNCT
iajs-1146	198	105	71.5	71.5	NUM
iajs-1146	198	106	4.3	4.3	NUM
iajs-1146	198	107	(	(	PUNCT
iajs-1146	198	108	3.98	3.98	NUM
iajs-1146	198	109	)	)	PUNCT
iajs-1146	198	110	3.69	3.69	NUM
iajs-1146	198	111	(	(	PUNCT
iajs-1146	198	112	3.44	3.44	NUM
iajs-1146	198	113	)	)	PUNCT
iajs-1146	198	114	57.23	57.23	NUM
iajs-1146	198	115	(	(	PUNCT
iajs-1146	198	116	56.89	56.89	NUM
iajs-1146	198	117	)	)	PUNCT
iajs-1146	198	118	0.48	0.48	NUM
iajs-1146	198	119	(	(	PUNCT
iajs-1146	198	120	benzene	benzene	NOUN
iajs-1146	198	121	:	:	PUNCT
iajs-1146	198	122	methanol	methanol	NOUN
iajs-1146	198	123	9:0.5	9:0.5	NUM
iajs-1146	198	124	)	)	PUNCT
iajs-1146	198	125	syrup	syrup	NOUN
iajs-1146	198	126	c36	c36	NOUN
iajs-1146	198	127	h31	h31	PROPN
iajs-1146	198	128	n6	n6	PROPN
iajs-1146	198	129	o7f3	o7f3	X
iajs-1146	198	130	(	(	PUNCT
iajs-1146	198	131	8)	8)	NUM
iajs-1146	198	132	55	55	NUM
iajs-1146	198	133	11.7	11.7	NUM
iajs-1146	198	134	3	3	NUM
iajs-1146	198	135	(	(	PUNCT
iajs-1146	198	136	11.5	11.5	NUM
iajs-1146	198	137	3	3	NUM
iajs-1146	198	138	)	)	PUNCT
iajs-1146	198	139	4.32	4.32	NUM
iajs-1146	198	140	(	(	PUNCT
iajs-1146	198	141	4.59	4.59	NUM
iajs-1146	198	142	)	)	PUNCT
iajs-1146	198	143	62.79	62.79	NUM
iajs-1146	198	144	(	(	PUNCT
iajs-1146	198	145	63.11	63.11	NUM
iajs-1146	198	146	)	)	PUNCT
iajs-1146	198	147	0.33	0.33	NUM
iajs-1146	198	148	(	(	PUNCT
iajs-1146	198	149	benzene	benzene	NOUN
iajs-1146	198	150	:	:	PUNCT
iajs-1146	198	151	methanol	methanol	NOUN
iajs-1146	198	152	9:0.5	9:0.5	NUM
iajs-1146	198	153	)	)	PUNCT
iajs-1146	198	154	syrup	syrup	NOUN
iajs-1146	198	155	c27h28n6o5	c27h28n6o5	PROPN
iajs-1146	198	156	(	(	PUNCT
iajs-1146	198	157	10	10	NUM
iajs-1146	198	158	)	)	PUNCT
iajs-1146	198	159	79.2	79.2	NUM
iajs-1146	198	160	8.64	8.64	NUM
iajs-1146	198	161	(	(	PUNCT
iajs-1146	198	162	8.28	8.28	NUM
iajs-1146	198	163	)	)	PUNCT
iajs-1146	198	164	4.16	4.16	NUM
iajs-1146	198	165	(	(	PUNCT
iajs-1146	198	166	3.86	3.86	NUM
iajs-1146	198	167	)	)	PUNCT
iajs-1146	198	168	61.11	61.11	NUM
iajs-1146	198	169	(	(	PUNCT
iajs-1146	198	170	61.46	61.46	NUM
iajs-1146	198	171	)	)	PUNCT
iajs-1146	198	172	0.52	0.52	NUM
iajs-1146	198	173	(	(	PUNCT
iajs-1146	198	174	benzene	benzene	NOUN
iajs-1146	198	175	:	:	PUNCT
iajs-1146	198	176	methanol	methanol	NOUN
iajs-1146	198	177	9:0.5	9:0.5	NUM
iajs-1146	198	178	)	)	PUNCT
iajs-1146	198	179	semi	semi	ADV
iajs-1146	198	180	solid	solid	ADJ
iajs-1146	198	181	c33h27n4o7f3	c33h27n4o7f3	NOUN
iajs-1146	198	182	(	(	PUNCT
iajs-1146	198	183	12	12	NUM
iajs-1146	198	184	)	)	PUNCT
iajs-1146	198	185	42.3	42.3	NUM
iajs-1146	198	186	12.5	12.5	NUM
iajs-1146	198	187	(	(	PUNCT
iajs-1146	198	188	12.2	12.2	NUM
iajs-1146	198	189	1	1	NUM
iajs-1146	198	190	)	)	PUNCT
iajs-1146	198	191	5.35	5.35	NUM
iajs-1146	198	192	4.97	4.97	NUM
iajs-1146	198	193	)	)	PUNCT
iajs-1146	198	194	(	(	PUNCT
iajs-1146	198	195	64.28	64.28	NUM
iajs-1146	198	196	(	(	PUNCT
iajs-1146	198	197	64.81	64.81	NUM
iajs-1146	198	198	)	)	PUNCT
iajs-1146	198	199	0.4	0.4	NUM
iajs-1146	198	200	(	(	PUNCT
iajs-1146	198	201	benzene	benzene	NOUN
iajs-1146	198	202	:	:	PUNCT
iajs-1146	198	203	methanol	methanol	NOUN
iajs-1146	198	204	9:0.5	9:0.5	NUM
iajs-1146	198	205	)	)	PUNCT
iajs-1146	198	206	syrup	syrup	NOUN
iajs-1146	198	207	c24h24n4o5	c24h24n4o5	PROPN
iajs-1146	198	208	(	(	PUNCT
iajs-1146	198	209	14	14	NUM
iajs-1146	198	210	)	)	PUNCT
iajs-1146	198	211	ibn	ibn	NOUN
iajs-1146	198	212	alhaitham	alhaitham	NOUN
iajs-1146	198	213	j.	j.	PROPN
iajs-1146	199	1	fo	fo	ADP
iajs-1146	199	2	r	r	NOUN
iajs-1146	199	3	pure	pure	ADJ
iajs-1146	199	4	&	&	CCONJ
iajs-1146	199	5	appl	appl	PROPN
iajs-1146	199	6	.	.	PUNCT
iajs-1146	200	1	sc	sc	PROPN
iajs-1146	201	1	i	i	PRON
iajs-1146	201	2	vo	vo	INTJ
iajs-1146	201	3	l.22	l.22	X
iajs-1146	201	4	(	(	PUNCT
iajs-1146	201	5	4	4	NUM
iajs-1146	201	6	)	)	PUNCT
iajs-1146	201	7	2009	2009	NUM
iajs-1146	201	8	table	table	NOUN
iajs-1146	201	9	(	(	PUNCT
iajs-1146	201	10	3):effect	3):effect	NUM
iajs-1146	201	11	of	of	ADP
iajs-1146	201	12	antimicrobial	antimicrobial	ADJ
iajs-1146	201	13	agents	agent	NOUN
iajs-1146	201	14	on	on	ADP
iajs-1146	201	15	escherichia	escherichia	NOUN
iajs-1146	201	16	coil	coil	NOUN
iajs-1146	201	17	effect	effect	NOUN
iajs-1146	201	18	of	of	ADP
iajs-1146	201	19	nucleoside	nucleoside	ADJ
iajs-1146	201	20	derivatives	derivative	NOUN
iajs-1146	201	21	on	on	ADP
iajs-1146	201	22	the	the	DET
iajs-1146	201	23	growth	growth	NOUN
iajs-1146	201	24	of	of	ADP
iajs-1146	201	25	e	e	NOUN
iajs-1146	201	26	-	-	NOUN
iajs-1146	201	27	coli	coli	ADJ
iajs-1146	201	28	bacteria	bacteria	NOUN
iajs-1146	201	29	con	con	NOUN
iajs-1146	201	30	.	.	PUNCT
iajs-1146	202	1	gm	gm	PROPN
iajs-1146	202	2	/	/	SYM
iajs-1146	202	3	m	m	PROPN
iajs-1146	202	4	l	l	NOUN
iajs-1146	202	5	0.0	0.0	NUM
iajs-1146	202	6	9	9	NUM
iajs-1146	202	7	0.1	0.1	NUM
iajs-1146	202	8	0.2	0.2	NUM
iajs-1146	202	9	0.3	0.3	NUM
iajs-1146	202	10	0.4	0.4	NUM
iajs-1146	202	11	0.5	0.5	NUM
iajs-1146	202	12	0.6	0.6	NUM
iajs-1146	202	13	0.7	0.7	NUM
iajs-1146	202	14	0.8	0.8	NUM
iajs-1146	202	15	0	0	NUM
iajs-1146	202	16	.	.	PUNCT
iajs-1146	202	17	9	9	NUM
iajs-1146	202	18	1	1	NUM
iajs-1146	202	19	com	com	NOUN
iajs-1146	202	20	.	.	PUNCT
iajs-1146	203	1	no	no	INTJ
iajs-1146	203	2	.	.	PUNCT
iajs-1146	204	1	+	+	PUNCT
iajs-1146	204	2	_	_	PUNCT
iajs-1146	205	1	_	_	PUNCT
iajs-1146	206	1	_	_	PUNCT
iajs-1146	207	1	_	_	PUNCT
iajs-1146	208	1	_	_	PUNCT
iajs-1146	209	1	_	_	PUNCT
iajs-1146	210	1	_	_	PUNCT
iajs-1146	211	1	_	_	PUNCT
iajs-1146	212	1	_	_	PUNCT
iajs-1146	213	1	_	_	PUNCT
iajs-1146	214	1	10	10	NUM
iajs-1146	215	1	+	+	NUM
iajs-1146	215	2	_	_	PUNCT
iajs-1146	216	1	_	_	PUNCT
iajs-1146	217	1	_	_	PUNCT
iajs-1146	218	1	_	_	PUNCT
iajs-1146	219	1	_	_	PUNCT
iajs-1146	220	1	_	_	PUNCT
iajs-1146	221	1	_	_	PUNCT
iajs-1146	222	1	14	14	NUM
iajs-1146	223	1	+	+	CCONJ
iajs-1146	223	2	u.	u.	NOUN
iajs-1146	223	3	base	base	NOUN
iajs-1146	223	4	+	+	CCONJ
iajs-1146	223	5	t.	t.	NOUN
iajs-1146	223	6	base	base	NOUN
iajs-1146	223	7	+	+	CCONJ
iajs-1146	223	8	blan	blan	PROPN
iajs-1146	223	9	k	k	PROPN
iajs-1146	223	10	(	(	PUNCT
iajs-1146	223	11	-	-	PUNCT
iajs-1146	223	12	)	)	PUNCT
iajs-1146	223	13	no	no	DET
iajs-1146	223	14	growth	growth	NOUN
iajs-1146	223	15	,	,	PUNCT
iajs-1146	223	16	u	u	NOUN
iajs-1146	223	17	=	=	NOUN
iajs-1146	223	18	uracil	uracil	ADJ
iajs-1146	223	19	(	(	PUNCT
iajs-1146	223	20	+	+	ADJ
iajs-1146	223	21	)	)	PUNCT
iajs-1146	223	22	growth	growth	NOUN
iajs-1146	223	23	,	,	PUNCT
iajs-1146	223	24	t	t	NOUN
iajs-1146	223	25	=	=	NOUN
iajs-1146	223	26	theophylline	theophylline	NOUN
iajs-1146	223	27	2009	2009	NUM
iajs-1146	223	28	)	)	PUNCT
iajs-1146	223	29	4	4	NUM
iajs-1146	223	30	(	(	PUNCT
iajs-1146	223	31	22مجلة	22مجلة	NUM
iajs-1146	223	32	ابن	ابن	VERB
iajs-1146	223	33	الهیثم	الهیثم	PROPN
iajs-1146	223	34	للعلوم	للعلوم	PROPN
iajs-1146	223	35	الصرفة	الصرفة	PROPN
iajs-1146	223	36	والتطبیقیة	والتطبیقیة	PROPN
iajs-1146	223	37	المجلد	المجلد	PROPN
iajs-1146	223	38	فعالیة	فعالیة	PROPN
iajs-1146	223	39	بایولوجیة	بایولوجیة	NOUN
iajs-1146	223	40	و	و	PRON
iajs-1146	223	41	ذویرسباحلقة	ذویرسباحلقة	PROPN
iajs-1146	223	42	c-3	c-3	PROPN
iajs-1146	223	43	–	–	PUNCT
iajs-1146	223	44	وسید	وسید	ADJ
iajs-1146	223	45	من	من	PROPN
iajs-1146	223	46	نوع	نوع	ADJ
iajs-1146	223	47	تحضیر	تحضیر	NOUN
iajs-1146	223	48	ممثالت	ممثالت	PROPN
iajs-1146	223	49	نیوكلی	نیوكلی	PROPN
iajs-1146	223	50	محتملة	محتملة	PROPN
iajs-1146	223	51	محمد	محمد	PROPN
iajs-1146	223	52	حسینأیمان	حسینأیمان	PROPN
iajs-1146	223	53	جامعة	جامعة	PROPN
iajs-1146	223	54	بغداد	بغداد	PROPN
iajs-1146	223	55	،	،	PROPN
iajs-1146	223	56	ابن	ابن	PROPN
iajs-1146	223	57	الھیثم	الھیثم	PROPN
iajs-1146	223	58	–	–	PUNCT
iajs-1146	223	59	كلیة	كلیة	PROPN
iajs-1146	223	60	التربیة	التربیة	NOUN
iajs-1146	223	61	،	،	NOUN
iajs-1146	223	62	الكیمیاءقسم	الكیمیاءقسم	PROPN
iajs-1146	223	63	الخالصة	الخالصة	PROPN
iajs-1146	223	64	اختیـر	اختیـر	PROPN
iajs-1146	223	65	اذ3	اذ3	PROPN
iajs-1146	224	1	فـي	فـي	NOUN
iajs-1146	224	2	موقـع	موقـع	PROPN
iajs-1146	224	3	وسـبا	وسـبا	ADV
iajs-1146	224	4	یـر	یـر	PROPN
iajs-1146	224	5	النیوكلیوسـید	النیوكلیوسـید	PROPN
iajs-1146	224	6	تحتـوي	تحتـوي	PROPN
iajs-1146	224	7	علـى	علـى	ADP
iajs-1146	224	8	حلقـة	حلقـة	NOUN
iajs-1146	224	9	لمماثالتتم	لمماثالتتم	ADP
iajs-1146	224	10	في	في	SCONJ
iajs-1146	224	11	هذا	هذا	NOUN
iajs-1146	224	12	البحث	البحث	NOUN
iajs-1146	224	13	تحضیر	تحضیر	NOUN
iajs-1146	224	14	مشتقات	مشتقات	PROPN
iajs-1146	224	15	جدیدة	جدیدة	PROPN
iajs-1146	224	16	مـع	مـع	PROPN
iajs-1146	224	17	1	1	NUM
iajs-1146	224	18	المـشتق	المـشتق	NOUN
iajs-1146	224	19	مفاعلـهتـم	مفاعلـهتـم	VERB
iajs-1146	224	20	اذ	اذ	PROPN
iajs-1146	224	21	،	،	NOUN
iajs-1146	224	22	التفـاعالتسله	التفـاعالتسله	VERB
iajs-1146	224	23	من	من	PRON
iajs-1146	224	24	النیوكلیوسید	النیوكلیوسید	PROPN
iajs-1146	224	25	بعد	بعد	PROPN
iajs-1146	224	26	مروره	مروره	PROPN
iajs-1146	224	27	بسل	بسل	PROPN
iajs-1146	224	28	مماثالت	مماثالت	PROPN
iajs-1146	224	29	لغرض	لغرض	PROPN
iajs-1146	224	30	تحضیر	تحضیر	NOUN
iajs-1146	224	31	ابتدائیةة	ابتدائیةة	ADJ
iajs-1146	224	32	ماد1المشتق	ماد1المشتق	PROPN
iajs-1146	224	33	لغــرض	لغــرض	NOUN
iajs-1146	224	34	.	.	PUNCT
iajs-1146	225	1	2المــشتق	2المــشتق	NUM
iajs-1146	225	2	مــن	مــن	PROPN
iajs-1146	225	3	الموقــع	الموقــع	VERB
iajs-1146	225	4	ثالثــة	ثالثــة	PROPN
iajs-1146	225	5	للحــصول	للحــصول	PROPN
iajs-1146	225	6	علــى	علــى	PROPN
iajs-1146	225	7	مــاءجریئــةهیدریــد	مــاءجریئــةهیدریــد	PROPN
iajs-1146	225	8	الخلیــك	الخلیــك	PART
iajs-1146	225	9	لغــرض	لغــرض	ADJ
iajs-1146	225	10	ســحب	ســحب	ADJ
iajs-1146	225	11	نالسلفوكــسید	نالسلفوكــسید	ADJ
iajs-1146	225	12	وا	وا	PROPN
iajs-1146	225	13	ثنـائي	ثنـائي	PROPN
iajs-1146	225	14	مثیــل	مثیــل	PROPN
iajs-1146	225	15	ـةالحـصول	ـةالحـصول	PROPN
iajs-1146	225	16	علــى	علــى	PROPN
iajs-1146	225	17	حلقــة	حلقــة	ADJ
iajs-1146	225	18	ســبایرو	ســبایرو	NOUN
iajs-1146	225	19	فــي	فــي	ADJ
iajs-1146	225	20	موقـع	موقـع	PROPN
iajs-1146	225	21	تحــیزا	تحــیزا	NOUN
iajs-1146	225	22	.	.	PUNCT
iajs-1146	226	1	3طــى	3طــى	PROPN
iajs-1146	226	2	المــشتق	المــشتق	NOUN
iajs-1146	226	3	أع،اذالفنیــل	أع،اذالفنیــل	NOUN
iajs-1146	226	4	هیــدرازین	هیــدرازین	ADJ
iajs-1146	226	5	مـع	مـع	PROPN
iajs-1146	226	6	2	2	NUM
iajs-1146	226	7	المــشتق	المــشتق	PROPN
iajs-1146	226	8	ةمفاعلــ	ةمفاعلــ	PROPN
iajs-1146	226	9	تمــت	تمــت	PROPN
iajs-1146	226	10	ثالثـ	ثالثـ	PROPN
iajs-1146	226	11	حــامض	حــامض	PROPN
iajs-1146	226	12	الخلیـك	الخلیـك	PROPN
iajs-1146	226	13	تبعتهـا	تبعتهـا	PROPN
iajs-1146	226	14	عملیـة	عملیـة	PROPN
iajs-1146	226	15	أكـسدة	أكـسدة	PROPN
iajs-1146	226	16	واختـزال	واختـزال	PROPN
iajs-1146	226	17	للحـصول	للحـصول	PROPN
iajs-1146	226	18	علــى	علــى	PROPN
iajs-1146	226	19	المع	المع	PROPN
iajs-1146	226	20	باسـت2و1فـي	باسـت2و1فـي	PROPN
iajs-1146	226	21	الموقـع	الموقـع	NOUN
iajs-1146	226	22	)	)	PUNCT
iajs-1146	227	1	دیناالیزوبروبیلـ(مجموعـة	دیناالیزوبروبیلـ(مجموعـة	PROPN
iajs-1146	227	2	الحمایـة	الحمایـة	VERB
iajs-1146	227	3	ــل	ــل	X
iajs-1146	227	4	یــوفر	یــوفر	ADJ
iajs-1146	227	5	الفرصـــة	الفرصـــة	ADJ
iajs-1146	227	6	1	1	NUM
iajs-1146	227	7	-	-	PUNCT
iajs-1146	227	8	أن	أن	NUM
iajs-1146	227	9	حمایـــة	حمایـــة	ADJ
iajs-1146	227	10	مجموعـــة	مجموعـــة	PROPN
iajs-1146	227	11	الهیدروكــسیل	الهیدروكــسیل	PROPN
iajs-1146	227	12	فـــي	فـــي	PROPN
iajs-1146	227	13	الموقـــع	الموقـــع	PROPN
iajs-1146	227	14	.	.	PUNCT
iajs-1146	228	1	5	5	NUM
iajs-1146	228	2	المــشتق	المــشتق	PROPN
iajs-1146	228	3	ـةالمناســـبة	ـةالمناســـبة	PROPN
iajs-1146	228	4	باســتخدام	باســتخدام	VERB
iajs-1146	228	5	كاوریـــد	كاوریـــد	NOUN
iajs-1146	228	6	البنزویـ	البنزویـ	PROPN
iajs-1146	228	7	إلزاحــ	إلزاحــ	PROPN
iajs-1146	228	8	بمـزیج	بمـزیج	VERB
iajs-1146	228	9	مـن	مـن	PROPN
iajs-1146	228	10	حـامض	حـامض	PROPN
iajs-1146	228	11	الخلیـك	الخلیـك	PROPN
iajs-1146	228	12	وثالثـي	وثالثـي	PROPN
iajs-1146	228	13	فلوریـد	فلوریـد	PROPN
iajs-1146	228	14	6	6	NUM
iajs-1146	228	15	عومـل	عومـل	NOUN
iajs-1146	228	16	المـشتق	المـشتق	NOUN
iajs-1146	228	17	.	.	PUNCT
iajs-1146	229	1	6عطـى	6عطـى	NUM
iajs-1146	229	2	المـشتق	المـشتق	NOUN
iajs-1146	229	3	،	،	NOUN
iajs-1146	229	4	اذ	اذ	NOUN
iajs-1146	229	5	أ	أ	ADP
iajs-1146	229	6	4	4	NUM
iajs-1146	229	7	و3	و3	ADJ
iajs-1146	229	8	-	-	PUNCT
iajs-1146	229	9	ي	ي	NOUN
iajs-1146	229	10	الموقـع	الموقـع	NOUN
iajs-1146	229	11	فـمجموعـة	فـمجموعـة	NOUN
iajs-1146	229	12	االسـیتال	االسـیتال	PROPN
iajs-1146	229	13	مـع	مـع	PROPN
iajs-1146	229	14	ملـح	ملـح	PROPN
iajs-1146	229	15	الزئبـق	الزئبـق	ADJ
iajs-1146	229	16	للثیـوفلین	للثیـوفلین	VERB
iajs-1146	229	17	7	7	NUM
iajs-1146	229	18	المـشتق	المـشتق	NOUN
iajs-1146	229	19	ةمفاعلـتمـت	ةمفاعلـتمـت	NOUN
iajs-1146	229	20	.	.	PUNCT
iajs-1146	230	1	7	7	NUM
iajs-1146	230	2	المـشتق	المـشتق	NOUN
iajs-1146	230	3	إلعطـاءالخلیـك	إلعطـاءالخلیـك	NOUN
iajs-1146	230	4	الخلیك	الخلیك	PROPN
iajs-1146	230	5	تبعه	تبعه	PROPN
iajs-1146	230	6	التفاعل	التفاعل	PROPN
iajs-1146	230	7	مع	مع	PROPN
iajs-1146	230	8	ثالثي	ثالثي	PROPN
iajs-1146	230	9	فلورید	فلورید	PROPN
iajs-1146	230	10	انهیدریـد	انهیدریـد	PROPN
iajs-1146	230	11	أن	أن	PROPN
iajs-1146	230	12	.	.	PUNCT
iajs-1146	231	1	12النیوكلیوســید	12النیوكلیوســید	PROPN
iajs-1146	231	2	مماثـلأعطـى	مماثـلأعطـى	ADJ
iajs-1146	231	3	مـع	مـع	PROPN
iajs-1146	231	4	مـشتق	مـشتق	PROPN
iajs-1146	231	5	الـسیالیل	الـسیالیل	ADJ
iajs-1146	231	6	للیوراسـیل	للیوراسـیل	ADJ
iajs-1146	231	7	7	7	NUM
iajs-1146	231	8	المـشتق	المـشتق	NOUN
iajs-1146	231	9	تفاعـلأن	تفاعـلأن	NOUN
iajs-1146	231	10	.	.	PUNCT
iajs-1146	232	1	8مماثـل	8مماثـل	NUM
iajs-1146	232	2	النیوكایوسـید	النیوكایوسـید	NOUN
iajs-1146	232	3	الـذي	الـذي	NOUN
iajs-1146	232	4	أعطـى	أعطـى	ADJ
iajs-1146	232	5	14	14	NUM
iajs-1146	232	6	و	و	NOUN
iajs-1146	232	7	10یوسـید	10یوسـید	NOUN
iajs-1146	232	8	الحـرة	الحـرة	ADV
iajs-1146	232	9	المیثـانول	المیثـانول	PROPN
iajs-1146	232	10	أعطـى	أعطـى	PROPN
iajs-1146	232	11	مـشتقات	مـشتقات	PROPN
iajs-1146	232	12	النیوكل	النیوكل	PROPN
iajs-1146	232	13	كل	كل	PROPN
iajs-1146	232	14	علـى	علـى	INTJ
iajs-1146	232	15	انفـراد	انفـراد	VERB
iajs-1146	232	16	مـع	مـع	PROPN
iajs-1146	232	17	میثوكـسید	میثوكـسید	PROPN
iajs-1146	232	18	الـصودیوم	الـصودیوم	PROPN
iajs-1146	232	19	فـي12و8تسخین	فـي12و8تسخین	PROPN
iajs-1146	232	20	المشتقین	المشتقین	PROPN
iajs-1146	232	21	ـةأقــد	ـةأقــد	PROPN
iajs-1146	232	22	وجـد	وجـد	PROPN
iajs-1146	232	23	ضـد	ضـد	PROPN
iajs-1146	232	24	بكتریــا	بكتریــا	ADP
iajs-1146	232	25	القولـون	القولـون	NOUN
iajs-1146	232	26	و14	و14	PROPN
iajs-1146	233	1	و	و	PRON
iajs-1146	233	2	10البایولوجیـة	10البایولوجیـة	PROPN
iajs-1146	233	3	للمــشتقات	للمــشتقات	PROPN
iajs-1146	233	4	تمــت	تمــت	PROPN
iajs-1146	233	5	دراسـة	دراسـة	PROPN
iajs-1146	233	6	الفعالیــة	الفعالیــة	PROPN
iajs-1146	233	7	.	.	PUNCT
iajs-1146	234	1	علـى	علـى	NOUN
iajs-1146	235	1	التـوالي	التـوالي	ADP
iajs-1146	235	2	ة	ة	ADP
iajs-1146	235	3	بایولوجیـ	بایولوجیـ	NOUN
iajs-1146	235	4	ـا	ـا	NOUN
iajs-1146	235	5	فعالیـ	فعالیـ	VERB
iajs-1146	235	6	ن	ن	PROPN
iajs-1146	235	7	لهـ	لهـ	NOUN
iajs-1146	235	8	.10وأكثرها	.10وأكثرها	PUNCT
iajs-1146	236	1	فاعلیة	فاعلیة	PROPN
iajs-1146	236	2	كان	كان	PROPN
iajs-1146	236	3	المشتق	المشتق	NOUN