id sid tid token lemma pos iajs-1795 1 1 microsoft microsoft PROPN iajs-1795 1 2 word word NOUN iajs-1795 1 3 221 221 NUM iajs-1795 1 4 - - SYM iajs-1795 1 5 234 234 NUM iajs-1795 1 6 ihsciconf ihsciconf NOUN iajs-1795 1 7 2017 2017 NUM iajs-1795 1 8 special special ADJ iajs-1795 1 9 issue issue NOUN iajs-1795 1 10 ibn ibn PROPN iajs-1795 1 11 al al PROPN iajs-1795 1 12 - - PUNCT iajs-1795 1 13 haitham haitham PROPN iajs-1795 1 14 journal journal PROPN iajs-1795 1 15 for for ADP iajs-1795 1 16 pure pure ADJ iajs-1795 1 17 and and CCONJ iajs-1795 1 18 applied apply VERB iajs-1795 1 19 science science NOUN iajs-1795 1 20 https://doi.org/ https://doi.org/ NOUN iajs-1795 1 21 10.30526/2017.ihsciconf.1795 10.30526/2017.ihsciconf.1795 NUM iajs-1795 1 22 for for ADP iajs-1795 1 23 more more ADJ iajs-1795 1 24 information information NOUN iajs-1795 1 25 about about ADP iajs-1795 1 26 the the DET iajs-1795 1 27 conference conference NOUN iajs-1795 1 28 please please INTJ iajs-1795 1 29 visit visit VERB iajs-1795 1 30 the the DET iajs-1795 1 31 websites website NOUN iajs-1795 1 32 : : PUNCT iajs-1795 1 33 http://www.ihsciconf.org/conf/ http://www.ihsciconf.org/conf/ VERB iajs-1795 1 34         SPACE iajs-1795 1 35 www.ihsciconf.org www.ihsciconf.org ADJ iajs-1795 1 36       SPACE iajs-1795 1 37 chemistry chemistry NOUN iajs-1795 1 38 |221 |221 NOUN iajs-1795 1 39     SPACE iajs-1795 1 40 use use NOUN iajs-1795 1 41 of of ADP iajs-1795 1 42 acidic acidic ADJ iajs-1795 1 43 hydrolysis hydrolysis NOUN iajs-1795 1 44 and and CCONJ iajs-1795 1 45 diazo diazo NOUN iajs-1795 1 46 coupling coupling NOUN iajs-1795 1 47 reaction reaction NOUN iajs-1795 1 48 for for ADP iajs-1795 1 49 spectrophotometric spectrophotometric ADJ iajs-1795 1 50 determination determination NOUN iajs-1795 1 51 of of ADP iajs-1795 1 52 furosemide furosemide NOUN iajs-1795 1 53 in in ADP iajs-1795 1 54 urine urine NOUN iajs-1795 1 55 and and CCONJ iajs-1795 1 56 pharmaceutical pharmaceutical NOUN iajs-1795 1 57 formulation formulation NOUN iajs-1795 1 58 hawraa hawraa NOUN iajs-1795 1 59 ali ali PROPN iajs-1795 1 60 sumayha sumayha PROPN iajs-1795 1 61 muhammed muhammed PROPN iajs-1795 1 62 sumayha.mu@gmail.com sumayha.mu@gmail.com PROPN iajs-1795 1 63 dept dept PROPN iajs-1795 1 64 . . PROPN iajs-1795 2 1 of of ADP iajs-1795 2 2 chemistry/ chemistry/ NUM iajs-1795 2 3 college college NOUN iajs-1795 2 4 of of ADP iajs-1795 2 5 education education NOUN iajs-1795 2 6 for for ADP iajs-1795 2 7 pure pure ADJ iajs-1795 2 8 science science NOUN iajs-1795 2 9 ( ( PUNCT iajs-1795 2 10 ibn ibn PROPN iajs-1795 2 11 al al PROPN iajs-1795 2 12 - - PUNCT iajs-1795 2 13 haitham haitham PROPN iajs-1795 2 14 / / SYM iajs-1795 2 15 university university PROPN iajs-1795 2 16 of of ADP iajs-1795 2 17 baghdad baghdad PROPN iajs-1795 2 18 abstract abstract ADJ iajs-1795 2 19 simple simple ADJ iajs-1795 2 20 and and CCONJ iajs-1795 2 21 rapid rapid ADJ iajs-1795 2 22 spectrophotometric spectrophotometric ADJ iajs-1795 2 23 determination determination NOUN iajs-1795 2 24 of of ADP iajs-1795 2 25 furosemide furosemide ADJ iajs-1795 2 26 ( ( PUNCT iajs-1795 2 27 fur fur NOUN iajs-1795 2 28 ) ) PUNCT iajs-1795 2 29 has have AUX iajs-1795 2 30 been be AUX iajs-1795 2 31 investigated investigate VERB iajs-1795 2 32 .the .the DET iajs-1795 2 33 method method NOUN iajs-1795 2 34 is be AUX iajs-1795 2 35 based base VERB iajs-1795 2 36 on on ADP iajs-1795 2 37 acid acid NOUN iajs-1795 2 38 hydrolysis hydrolysis NOUN iajs-1795 2 39 of of ADP iajs-1795 2 40 fur fur NOUN iajs-1795 2 41 to to PART iajs-1795 2 42 free free VERB iajs-1795 2 43 primary primary ADJ iajs-1795 2 44 aromatic aromatic ADJ iajs-1795 2 45 amine amine NOUN iajs-1795 2 46 and and CCONJ iajs-1795 2 47 diazotization diazotization NOUN iajs-1795 2 48 followed follow VERB iajs-1795 2 49 by by ADP iajs-1795 2 50 coupling couple VERB iajs-1795 2 51 with with ADP iajs-1795 2 52 3 3 NUM iajs-1795 2 53 , , PUNCT iajs-1795 2 54 5 5 NUM iajs-1795 2 55 di di NOUN iajs-1795 2 56 methyl methyl NOUN iajs-1795 2 57 phenol phenol NOUN iajs-1795 2 58 ( ( PUNCT iajs-1795 2 59 3 3 NUM iajs-1795 2 60 , , PUNCT iajs-1795 2 61 5 5 NUM iajs-1795 2 62 - - SYM iajs-1795 2 63 dmph dmph NOUN iajs-1795 2 64 ) ) PUNCT iajs-1795 2 65 at at ADP iajs-1795 2 66 basic basic ADJ iajs-1795 2 67 medium medium NOUN iajs-1795 2 68 . . PUNCT iajs-1795 3 1 the the DET iajs-1795 3 2 absorbance absorbance NOUN iajs-1795 3 3 was be AUX iajs-1795 3 4 measured measure VERB iajs-1795 3 5 at at ADP iajs-1795 3 6 434 434 NUM iajs-1795 3 7 nm nm NOUN iajs-1795 3 8 , , PUNCT iajs-1795 3 9 the the DET iajs-1795 3 10 method method NOUN iajs-1795 3 11 was be AUX iajs-1795 3 12 optimized optimize VERB iajs-1795 3 13 for for ADP iajs-1795 3 14 best good ADJ iajs-1795 3 15 condition condition NOUN iajs-1795 3 16 , , PUNCT iajs-1795 3 17 and and CCONJ iajs-1795 3 18 beers beer NOUN iajs-1795 3 19 ’ ' PUNCT iajs-1795 3 20 law law NOUN iajs-1795 3 21 is be AUX iajs-1795 3 22 obeyed obey VERB iajs-1795 3 23 over over ADP iajs-1795 3 24 the the DET iajs-1795 3 25 range range NOUN iajs-1795 3 26 of of ADP iajs-1795 3 27 0.4 0.4 NUM iajs-1795 3 28 - - SYM iajs-1795 3 29 50 50 NUM iajs-1795 3 30 µg.ml-1 µg.ml-1 ADJ iajs-1795 3 31 with with ADP iajs-1795 3 32 molar molar ADJ iajs-1795 3 33 absorptivity absorptivity NOUN iajs-1795 3 34 and and CCONJ iajs-1795 3 35 sandal sandal NOUN iajs-1795 3 36 ’s ’s PART iajs-1795 3 37 sensitivity sensitivity NOUN iajs-1795 3 38 1.3899 1.3899 NUM iajs-1795 3 39 x104 x104 PUNCT iajs-1795 4 1 l l NOUN iajs-1795 4 2 mol-1 mol-1 X iajs-1795 4 3 .cm-1 .cm-1 NUM iajs-1795 4 4 and and CCONJ iajs-1795 4 5 0.0238x104 0.0238x104 NOUN iajs-1795 4 6 µg.cm-2 µg.cm-2 VERB iajs-1795 4 7 respectively respectively ADV iajs-1795 4 8 . . PUNCT iajs-1795 5 1 analysis analysis NOUN iajs-1795 5 2 of of ADP iajs-1795 5 3 solution solution NOUN iajs-1795 5 4 containing contain VERB iajs-1795 5 5 nineteen nineteen NUM iajs-1795 5 6 different different ADJ iajs-1795 5 7 concentrations concentration NOUN iajs-1795 5 8 of of ADP iajs-1795 5 9 fur fur NOUN iajs-1795 5 10 gave give VERB iajs-1795 5 11 a a DET iajs-1795 5 12 correlation correlation NOUN iajs-1795 5 13 coefficient coefficient NOUN iajs-1795 5 14 of of ADP iajs-1795 5 15 ( ( PUNCT iajs-1795 5 16 0.9999 0.9999 NUM iajs-1795 5 17 ) ) PUNCT iajs-1795 5 18 and and CCONJ iajs-1795 5 19 limit limit NOUN iajs-1795 5 20 of of ADP iajs-1795 5 21 detection detection NOUN iajs-1795 5 22 , , PUNCT iajs-1795 5 23 limit limit NOUN iajs-1795 5 24 of of ADP iajs-1795 5 25 quantitation quantitation NOUN iajs-1795 5 26 were be AUX iajs-1795 5 27 0.127 0.127 NUM iajs-1795 5 28 , , PUNCT iajs-1795 5 29 0.464µg.ml-1 0.464µg.ml-1 NUM iajs-1795 5 30 respectively respectively ADV iajs-1795 5 31 . . PUNCT iajs-1795 6 1 the the DET iajs-1795 6 2 reaction reaction NOUN iajs-1795 6 3 stoichiometry stoichiometry NOUN iajs-1795 6 4 was be AUX iajs-1795 6 5 evaluated evaluate VERB iajs-1795 6 6 by by ADP iajs-1795 6 7 job job NOUN iajs-1795 6 8 ’s ’s NOUN iajs-1795 6 9 and and CCONJ iajs-1795 6 10 mole mole NOUN iajs-1795 6 11 ratio ratio NOUN iajs-1795 6 12 method method NOUN iajs-1795 6 13 was be AUX iajs-1795 6 14 found find VERB iajs-1795 6 15 to to PART iajs-1795 6 16 be be AUX iajs-1795 6 17 1:1(diazotized 1:1(diazotized NUM iajs-1795 6 18 fur fur NOUN iajs-1795 6 19 : : PUNCT iajs-1795 6 20 3 3 NUM iajs-1795 6 21 , , PUNCT iajs-1795 6 22 5 5 NUM iajs-1795 6 23 - - SYM iajs-1795 6 24 dmph dmph NOUN iajs-1795 6 25 ) ) PUNCT iajs-1795 6 26 .the .the PRON iajs-1795 6 27 method method NOUN iajs-1795 6 28 was be AUX iajs-1795 6 29 applied apply VERB iajs-1795 6 30 in in ADP iajs-1795 6 31 synthetic synthetic ADJ iajs-1795 6 32 urine urine NOUN iajs-1795 6 33 and and CCONJ iajs-1795 6 34 pharmaceutical pharmaceutical NOUN iajs-1795 6 35 formulation formulation NOUN iajs-1795 6 36 . . PUNCT iajs-1795 7 1 the the DET iajs-1795 7 2 recovery recovery NOUN iajs-1795 7 3 of of ADP iajs-1795 7 4 fur fur NOUN iajs-1795 7 5 in in ADP iajs-1795 7 6 spiked spiked ADJ iajs-1795 7 7 urine urine NOUN iajs-1795 7 8 was be AUX iajs-1795 7 9 satisfactory satisfactory ADJ iajs-1795 7 10 resulting result VERB iajs-1795 7 11 in in ADP iajs-1795 7 12 the the DET iajs-1795 7 13 values value NOUN iajs-1795 7 14 of of ADP iajs-1795 7 15 ( ( PUNCT iajs-1795 7 16 99±3.32 99±3.32 NUM iajs-1795 7 17 ) ) PUNCT iajs-1795 7 18 % % NOUN iajs-1795 7 19 , , PUNCT iajs-1795 7 20 the the DET iajs-1795 7 21 results result NOUN iajs-1795 7 22 of of ADP iajs-1795 7 23 the the DET iajs-1795 7 24 suggested suggest VERB iajs-1795 7 25 method method NOUN iajs-1795 7 26 was be AUX iajs-1795 7 27 compared compare VERB iajs-1795 7 28 with with ADP iajs-1795 7 29 available available ADJ iajs-1795 7 30 official official ADJ iajs-1795 7 31 literature literature NOUN iajs-1795 7 32 method method NOUN iajs-1795 7 33 . . PUNCT iajs-1795 8 1 keywords keyword NOUN iajs-1795 8 2 : : PUNCT iajs-1795 8 3 furosemide furosemide ADJ iajs-1795 8 4 , , PUNCT iajs-1795 8 5 3,5 3,5 NUM iajs-1795 8 6 - - PUNCT iajs-1795 8 7 dimethyl dimethyl NOUN iajs-1795 8 8 phenol phenol NOUN iajs-1795 8 9 spectrophotometry spectrophotometry NOUN iajs-1795 8 10 , , PUNCT iajs-1795 8 11 diazotization diazotization NOUN iajs-1795 8 12 . . PUNCT iajs-1795 9 1 ihsciconf ihsciconf PROPN iajs-1795 9 2 2017 2017 NUM iajs-1795 9 3 special special ADJ iajs-1795 9 4 issue issue NOUN iajs-1795 9 5 ibn ibn PROPN iajs-1795 9 6 al al PROPN iajs-1795 9 7 - - PUNCT iajs-1795 9 8 haitham haitham PROPN iajs-1795 9 9 journal journal PROPN iajs-1795 9 10 for for ADP iajs-1795 9 11 pure pure ADJ iajs-1795 9 12 and and CCONJ iajs-1795 9 13 applied apply VERB iajs-1795 9 14 science science NOUN iajs-1795 9 15 https://doi.org/ https://doi.org/ NOUN iajs-1795 9 16 10.30526/2017.ihsciconf.1795 10.30526/2017.ihsciconf.1795 NUM iajs-1795 9 17 for for ADP iajs-1795 9 18 more more ADJ iajs-1795 9 19 information information NOUN iajs-1795 9 20 about about ADP iajs-1795 9 21 the the DET iajs-1795 9 22 conference conference NOUN iajs-1795 9 23 please please INTJ iajs-1795 9 24 visit visit VERB iajs-1795 9 25 the the DET iajs-1795 9 26 websites website NOUN iajs-1795 9 27 : : PUNCT iajs-1795 9 28 http://www.ihsciconf.org/conf/ http://www.ihsciconf.org/conf/ VERB iajs-1795 9 29         SPACE iajs-1795 9 30 www.ihsciconf.org www.ihsciconf.org ADJ iajs-1795 9 31       SPACE iajs-1795 9 32 chemistry chemistry NOUN iajs-1795 9 33 |222 |222 NOUN iajs-1795 9 34     SPACE iajs-1795 9 35 1 1 NUM iajs-1795 9 36 . . PUNCT iajs-1795 10 1 introduction introduction NOUN iajs-1795 10 2 furosemide furosemide ADV iajs-1795 10 3 or or CCONJ iajs-1795 10 4 frusemide frusemide ADJ iajs-1795 10 5 ( ( PUNCT iajs-1795 10 6 4 4 NUM iajs-1795 10 7 - - PUNCT iajs-1795 10 8 chloro chloro NOUN iajs-1795 10 9 - - PUNCT iajs-1795 10 10 n n CCONJ iajs-1795 10 11 - - PUNCT iajs-1795 10 12 furfuyl furfuyl ADJ iajs-1795 10 13 -5 -5 ADJ iajs-1795 10 14 - - PUNCT iajs-1795 10 15 sulfamaylanthranilic sulfamaylanthranilic ADJ iajs-1795 10 16 acid acid NOUN iajs-1795 10 17 is be AUX iajs-1795 10 18 formally formally ADV iajs-1795 10 19 a a DET iajs-1795 10 20 sulfonamide sulfonamide NOUN iajs-1795 10 21 , , PUNCT iajs-1795 10 22 an an DET iajs-1795 10 23 antibacterial antibacterial ADJ iajs-1795 10 24 agent agent NOUN iajs-1795 10 25 . . PUNCT iajs-1795 11 1 however however ADV iajs-1795 11 2 , , PUNCT iajs-1795 11 3 the the DET iajs-1795 11 4 intense intense ADJ iajs-1795 11 5 and and CCONJ iajs-1795 11 6 fast fast ADJ iajs-1795 11 7 dieresis dieresis NOUN iajs-1795 11 8 produced produce VERB iajs-1795 11 9 by by ADP iajs-1795 11 10 this this DET iajs-1795 11 11 drug drug NOUN iajs-1795 11 12 , , PUNCT iajs-1795 11 13 has have AUX iajs-1795 11 14 extended extend VERB iajs-1795 11 15 its its PRON iajs-1795 11 16 application application NOUN iajs-1795 11 17 as as ADP iajs-1795 11 18 a a DET iajs-1795 11 19 powerful powerful ADJ iajs-1795 11 20 acidic acidic ADJ iajs-1795 11 21 diuretic diuretic NOUN iajs-1795 11 22 for for ADP iajs-1795 11 23 diverse diverse ADJ iajs-1795 11 24 treatment treatment NOUN iajs-1795 11 25 in in ADP iajs-1795 11 26 human human ADJ iajs-1795 11 27 and and CCONJ iajs-1795 11 28 veterinary veterinary ADJ iajs-1795 11 29 medicine medicine NOUN iajs-1795 11 30 . . PUNCT iajs-1795 12 1 furosemide furosemide NOUN iajs-1795 12 2 is be AUX iajs-1795 12 3 often often ADV iajs-1795 12 4 classified classify VERB iajs-1795 12 5 as as ADP iajs-1795 12 6 a a DET iajs-1795 12 7 loop loop NOUN iajs-1795 12 8 diuretic diuretic ADJ iajs-1795 12 9 due due ADP iajs-1795 12 10 to to ADP iajs-1795 12 11 its its PRON iajs-1795 12 12 predominate predominate ADJ iajs-1795 12 13 action action NOUN iajs-1795 12 14 in in ADP iajs-1795 12 15 the the DET iajs-1795 12 16 nephron nephron NOUN iajs-1795 12 17 [ [ X iajs-1795 12 18 1 1 NUM iajs-1795 12 19 ] ] PUNCT iajs-1795 12 20 . . PUNCT iajs-1795 13 1 fur fur NOUN iajs-1795 13 2 acts act NOUN iajs-1795 13 3 inhibiting inhibit VERB iajs-1795 13 4 of of ADP iajs-1795 13 5 sodium sodium NOUN iajs-1795 13 6 on on ADP iajs-1795 13 7 henle henle PROPN iajs-1795 13 8 , , PUNCT iajs-1795 13 9 s s PART iajs-1795 13 10 100 100 NUM iajs-1795 13 11 g g NOUN iajs-1795 13 12 and and CCONJ iajs-1795 13 13 inhibiting inhibit VERB iajs-1795 13 14 the the DET iajs-1795 13 15 co co NOUN iajs-1795 13 16 - - NOUN iajs-1795 13 17 transportation transportation NOUN iajs-1795 13 18 of of ADP iajs-1795 13 19 sodium sodium NOUN iajs-1795 13 20 , , PUNCT iajs-1795 13 21 potassium potassium NOUN iajs-1795 13 22 and and CCONJ iajs-1795 13 23 chloride chloride NOUN iajs-1795 13 24 , , PUNCT iajs-1795 13 25 and and CCONJ iajs-1795 13 26 causes cause VERB iajs-1795 13 27 excretion excretion NOUN iajs-1795 13 28 of of ADP iajs-1795 13 29 calcium calcium NOUN iajs-1795 13 30 , , PUNCT iajs-1795 13 31 magnesium magnesium NOUN iajs-1795 13 32 and and CCONJ iajs-1795 13 33 bicarbonate bicarbonate NOUN iajs-1795 13 34 ion ion NOUN iajs-1795 13 35 . . PUNCT iajs-1795 14 1 intense intense ADJ iajs-1795 14 2 and and CCONJ iajs-1795 14 3 fast fast ADJ iajs-1795 14 4 dieresis dieresis NOUN iajs-1795 14 5 may may AUX iajs-1795 14 6 also also ADV iajs-1795 14 7 mask mask VERB iajs-1795 14 8 the the DET iajs-1795 14 9 ingestion ingestion NOUN iajs-1795 14 10 of of ADP iajs-1795 14 11 other other ADJ iajs-1795 14 12 doping doping NOUN iajs-1795 14 13 agents agent NOUN iajs-1795 14 14 by by ADP iajs-1795 14 15 reducing reduce VERB iajs-1795 14 16 their their PRON iajs-1795 14 17 concentration concentration NOUN iajs-1795 14 18 in in ADP iajs-1795 14 19 urine urine NOUN iajs-1795 14 20 [ [ X iajs-1795 14 21 2 2 NUM iajs-1795 14 22 ] ] PUNCT iajs-1795 14 23 . . PUNCT iajs-1795 15 1 fur fur NOUN iajs-1795 15 2 have have VERB iajs-1795 15 3 a a DET iajs-1795 15 4 large large ADJ iajs-1795 15 5 number number NOUN iajs-1795 15 6 of of ADP iajs-1795 15 7 analytical analytical ADJ iajs-1795 15 8 technique technique NOUN iajs-1795 15 9 to to PART iajs-1795 15 10 determinate determinate VERB iajs-1795 15 11 it it PRON iajs-1795 15 12 in in ADP iajs-1795 15 13 pharmaceutical pharmaceutical ADJ iajs-1795 15 14 and and CCONJ iajs-1795 15 15 biological biological ADJ iajs-1795 15 16 samples sample NOUN iajs-1795 15 17 a a DET iajs-1795 15 18 number number NOUN iajs-1795 15 19 of of ADP iajs-1795 15 20 spectrophotometric spectrophotometric ADJ iajs-1795 15 21 method method NOUN iajs-1795 15 22 have have AUX iajs-1795 15 23 also also ADV iajs-1795 15 24 been be AUX iajs-1795 15 25 reported report VERB iajs-1795 15 26 for for ADP iajs-1795 15 27 furosemide furosemide ADJ iajs-1795 15 28 [ [ X iajs-1795 15 29 3 3 NUM iajs-1795 15 30 - - SYM iajs-1795 15 31 8 8 NUM iajs-1795 15 32 ] ] PUNCT iajs-1795 15 33 . . PUNCT iajs-1795 16 1 also also ADV iajs-1795 16 2 electrochemical electrochemical ADJ iajs-1795 16 3 detection detection NOUN iajs-1795 16 4 and and CCONJ iajs-1795 16 5 capillary capillary ADJ iajs-1795 16 6 electrophoresis electrophoresis NOUN iajs-1795 16 7 have have AUX iajs-1795 16 8 been be AUX iajs-1795 16 9 used use VERB iajs-1795 16 10 to to PART iajs-1795 16 11 quantify quantify VERB iajs-1795 16 12 fur fur NOUN iajs-1795 16 13 [ [ X iajs-1795 16 14 9 9 NUM iajs-1795 16 15 - - SYM iajs-1795 16 16 11 11 NUM iajs-1795 16 17 ] ] PUNCT iajs-1795 16 18 . . PUNCT iajs-1795 17 1 hplc hplc PROPN iajs-1795 17 2 is be AUX iajs-1795 17 3 generally generally ADV iajs-1795 17 4 the the DET iajs-1795 17 5 method method NOUN iajs-1795 17 6 of of ADP iajs-1795 17 7 choice choice NOUN iajs-1795 17 8 for for ADP iajs-1795 17 9 diuretics diuretic NOUN iajs-1795 17 10 quantitation quantitation NOUN iajs-1795 17 11 , , PUNCT iajs-1795 17 12 due due ADP iajs-1795 17 13 to to ADP iajs-1795 17 14 the the DET iajs-1795 17 15 required require VERB iajs-1795 17 16 time time NOUN iajs-1795 17 17 and and CCONJ iajs-1795 17 18 cost cost NOUN iajs-1795 17 19 of of ADP iajs-1795 17 20 the the DET iajs-1795 17 21 analysis analysis NOUN iajs-1795 17 22 [ [ X iajs-1795 17 23 12 12 NUM iajs-1795 17 24 - - SYM iajs-1795 17 25 13 13 NUM iajs-1795 17 26 ] ] PUNCT iajs-1795 17 27 . . PUNCT iajs-1795 18 1 the the DET iajs-1795 18 2 aim aim NOUN iajs-1795 18 3 of of ADP iajs-1795 18 4 this this DET iajs-1795 18 5 study study NOUN iajs-1795 18 6 was be AUX iajs-1795 18 7 to to PART iajs-1795 18 8 develop develop VERB iajs-1795 18 9 and and CCONJ iajs-1795 18 10 validate validate VERB iajs-1795 18 11 a a DET iajs-1795 18 12 new new ADJ iajs-1795 18 13 spectrophotometric spectrophotometric ADJ iajs-1795 18 14 method method NOUN iajs-1795 18 15 for for ADP iajs-1795 18 16 quantitative quantitative ADJ iajs-1795 18 17 determination determination NOUN iajs-1795 18 18 after after ADP iajs-1795 18 19 acidic acidic ADJ iajs-1795 18 20 hydrolysis hydrolysis NOUN iajs-1795 18 21 with with ADP iajs-1795 18 22 strong strong ADJ iajs-1795 18 23 acid acid NOUN iajs-1795 18 24 media medium NOUN iajs-1795 18 25 to to PART iajs-1795 18 26 yield yield VERB iajs-1795 18 27 salumine salumine NOUN iajs-1795 18 28 that that PRON iajs-1795 18 29 can can AUX iajs-1795 18 30 be be AUX iajs-1795 18 31 azotization azotization NOUN iajs-1795 18 32 and and CCONJ iajs-1795 18 33 coupled couple VERB iajs-1795 18 34 with with ADP iajs-1795 18 35 3.5 3.5 NUM iajs-1795 18 36 dimethyl dimethyl NOUN iajs-1795 18 37 phenol phenol NOUN iajs-1795 18 38 to to PART iajs-1795 18 39 form form VERB iajs-1795 18 40 a a DET iajs-1795 18 41 new new ADJ iajs-1795 18 42 orange orange NOUN iajs-1795 18 43 complex complex NOUN iajs-1795 18 44 have have VERB iajs-1795 18 45 a a DET iajs-1795 18 46 maximum maximum ADJ iajs-1795 18 47 absorption absorption NOUN iajs-1795 18 48 at at ADP iajs-1795 18 49 434 434 NUM iajs-1795 18 50 nm nm NOUN iajs-1795 18 51 . . PUNCT iajs-1795 19 1 scheme scheme NOUN iajs-1795 19 2 ( ( PUNCT iajs-1795 19 3 1 1 NUM iajs-1795 19 4 ): ): PUNCT iajs-1795 19 5 chemical chemical ADJ iajs-1795 19 6 structure structure NOUN iajs-1795 19 7 of of ADP iajs-1795 19 8 furosemide furosemide ADJ iajs-1795 19 9 2 2 NUM iajs-1795 19 10 . . 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NOUN iajs-1795 21 1 2 2 NUM iajs-1795 21 2 - - PUNCT iajs-1795 21 3 sartorius sartorius NOUN iajs-1795 21 4 bl210 bl210 NOUN iajs-1795 21 5 electronic electronic ADJ iajs-1795 21 6 balance balance NOUN iajs-1795 21 7 was be AUX iajs-1795 21 8 used use VERB iajs-1795 21 9 for for ADP iajs-1795 21 10 weighing weigh VERB iajs-1795 21 11 the the DET iajs-1795 21 12 samples sample NOUN iajs-1795 21 13 . . PUNCT iajs-1795 22 1 3 3 NUM iajs-1795 22 2 - - PUNCT iajs-1795 22 3 ph ph ADJ iajs-1795 22 4 measurements measurement NOUN iajs-1795 22 5 were be AUX iajs-1795 22 6 taken take VERB iajs-1795 22 7 with with ADP iajs-1795 22 8 jan jan PROPN iajs-1795 22 9 way way NOUN iajs-1795 22 10 ph ph ADJ iajs-1795 22 11 - - PUNCT iajs-1795 22 12 meter meter NOUN iajs-1795 22 13 3310 3310 NUM iajs-1795 22 14 . . PUNCT iajs-1795 23 1 ihsciconf ihsciconf PROPN iajs-1795 23 2 2017 2017 NUM iajs-1795 23 3 special special ADJ iajs-1795 23 4 issue issue NOUN iajs-1795 23 5 ibn ibn PROPN iajs-1795 23 6 al al PROPN iajs-1795 23 7 - - PUNCT iajs-1795 23 8 haitham haitham PROPN iajs-1795 23 9 journal journal PROPN iajs-1795 23 10 for for ADP iajs-1795 23 11 pure pure ADJ iajs-1795 23 12 and and CCONJ iajs-1795 23 13 applied apply VERB iajs-1795 23 14 science science NOUN iajs-1795 23 15 https://doi.org/ https://doi.org/ NOUN iajs-1795 23 16 10.30526/2017.ihsciconf.1795 10.30526/2017.ihsciconf.1795 NUM iajs-1795 23 17 for for ADP iajs-1795 23 18 more more ADJ iajs-1795 23 19 information information NOUN iajs-1795 23 20 about about ADP iajs-1795 23 21 the the DET iajs-1795 23 22 conference conference NOUN iajs-1795 23 23 please please INTJ iajs-1795 23 24 visit visit VERB iajs-1795 23 25 the the DET iajs-1795 23 26 websites website NOUN iajs-1795 23 27 : : PUNCT iajs-1795 23 28 http://www.ihsciconf.org/conf/ http://www.ihsciconf.org/conf/ VERB iajs-1795 23 29         SPACE iajs-1795 23 30 www.ihsciconf.org www.ihsciconf.org ADJ iajs-1795 23 31       SPACE iajs-1795 23 32 chemistry chemistry NOUN iajs-1795 23 33 |223 |223 NOUN iajs-1795 23 34     SPACE iajs-1795 23 35 material material NOUN iajs-1795 23 36 and and CCONJ iajs-1795 23 37 reagents reagent NOUN iajs-1795 23 38 : : PUNCT iajs-1795 23 39 all all DET iajs-1795 23 40 chemicals chemical NOUN iajs-1795 23 41 used use VERB iajs-1795 23 42 were be AUX iajs-1795 23 43 of of ADP iajs-1795 23 44 analytical analytical ADJ iajs-1795 23 45 grade grade NOUN iajs-1795 23 46 or or CCONJ iajs-1795 23 47 chemically chemically ADV iajs-1795 23 48 pure pure ADJ iajs-1795 23 49 , , PUNCT iajs-1795 23 50 distilled distil VERB iajs-1795 23 51 water water NOUN iajs-1795 23 52 was be AUX iajs-1795 23 53 used use VERB iajs-1795 23 54 for for ADP iajs-1795 23 55 all all DET iajs-1795 23 56 dilutions dilution NOUN iajs-1795 23 57 of of ADP iajs-1795 23 58 reagents reagent NOUN iajs-1795 23 59 and and CCONJ iajs-1795 23 60 samples sample NOUN iajs-1795 23 61 expect expect VERB iajs-1795 23 62 3 3 NUM iajs-1795 23 63 , , PUNCT iajs-1795 23 64 5dmph 5dmph NUM iajs-1795 23 65 which which PRON iajs-1795 23 66 was be AUX iajs-1795 23 67 dissolved dissolve VERB iajs-1795 23 68 in in ADP iajs-1795 23 69 methanol methanol NOUN iajs-1795 23 70 . . PUNCT iajs-1795 24 1 standard standard ADJ iajs-1795 24 2 grade grade NOUN iajs-1795 24 3 of of ADP iajs-1795 24 4 furosemide furosemide NOUN iajs-1795 24 5 was be AUX iajs-1795 24 6 kindly kindly ADV iajs-1795 24 7 provided provide VERB iajs-1795 24 8 by by ADP iajs-1795 24 9 state state NOUN iajs-1795 24 10 company company NOUN iajs-1795 24 11 for for ADP iajs-1795 24 12 drug drug NOUN iajs-1795 24 13 industries industry NOUN iajs-1795 24 14 and and CCONJ iajs-1795 24 15 medical medical ADJ iajs-1795 24 16 appliances appliance NOUN iajs-1795 24 17 ( ( PUNCT iajs-1795 24 18 s.d.i s.d.i NOUN iajs-1795 24 19 ) ) PUNCT iajs-1795 24 20 , , PUNCT iajs-1795 24 21 samara samara PROPN iajs-1795 24 22 - - PUNCT iajs-1795 24 23 iraq iraq PROPN iajs-1795 24 24 . . PUNCT iajs-1795 25 1 standard standard ADJ iajs-1795 25 2 hydrolyzed hydrolyze VERB iajs-1795 25 3 furosemide furosemide NOUN iajs-1795 25 4 ( ( PUNCT iajs-1795 25 5 100 100 NUM iajs-1795 25 6 µg.ml-1 µg.ml-1 ADJ iajs-1795 25 7 ) ) PUNCT iajs-1795 25 8 standard standard ADJ iajs-1795 25 9 fur fur NOUN iajs-1795 25 10 was be AUX iajs-1795 25 11 prepared prepare VERB iajs-1795 25 12 by by ADP iajs-1795 25 13 dissolving dissolve VERB iajs-1795 25 14 0.25 0.25 NUM iajs-1795 25 15 g g NOUN iajs-1795 25 16 of of ADP iajs-1795 25 17 pure pure ADJ iajs-1795 25 18 drug drug NOUN iajs-1795 25 19 in in ADP iajs-1795 25 20 methanol methanol NOUN iajs-1795 25 21 and and CCONJ iajs-1795 25 22 diluting dilute VERB iajs-1795 25 23 to to ADP iajs-1795 25 24 the the DET iajs-1795 25 25 mark mark NOUN iajs-1795 25 26 in in ADP iajs-1795 25 27 250ml 250ml NOUN iajs-1795 25 28 volumetric volumetric NOUN iajs-1795 25 29 flask flask NOUN iajs-1795 25 30 with with ADP iajs-1795 25 31 distilled distil VERB iajs-1795 25 32 water water NOUN iajs-1795 25 33 to to PART iajs-1795 25 34 prepare prepare VERB iajs-1795 25 35 ( ( PUNCT iajs-1795 25 36 1000 1000 NUM iajs-1795 25 37 µg.ml-1 µg.ml-1 ADJ iajs-1795 25 38 ) ) PUNCT iajs-1795 25 39 . . PUNCT iajs-1795 26 1 transfer transfer NOUN iajs-1795 26 2 150ml 150ml NOUN iajs-1795 26 3 of of ADP iajs-1795 26 4 prepared prepared ADJ iajs-1795 26 5 solution solution NOUN iajs-1795 26 6 with with ADP iajs-1795 26 7 25ml 25ml ADJ iajs-1795 26 8 hcl hcl PROPN iajs-1795 26 9 ( ( PUNCT iajs-1795 26 10 m m PROPN iajs-1795 26 11 11.8 11.8 NUM iajs-1795 26 12 to to PART iajs-1795 26 13 volumetric volumetric VERB iajs-1795 26 14 flask flask NOUN iajs-1795 26 15 of of ADP iajs-1795 26 16 250ml 250ml NOUN iajs-1795 26 17 and and CCONJ iajs-1795 26 18 diluting dilute VERB iajs-1795 26 19 to to ADP iajs-1795 26 20 the the DET iajs-1795 26 21 mark mark NOUN iajs-1795 26 22 with with ADP iajs-1795 26 23 distilled distil VERB iajs-1795 26 24 water water NOUN iajs-1795 26 25 to to PART iajs-1795 26 26 prepare prepare VERB iajs-1795 26 27 ( ( PUNCT iajs-1795 26 28 600µg.ml-1 600µg.ml-1 PROPN iajs-1795 26 29 ) ) PUNCT iajs-1795 26 30 of of ADP iajs-1795 26 31 fur fur NOUN iajs-1795 26 32 . . PUNCT iajs-1795 27 1 the the DET iajs-1795 27 2 obtained obtain VERB iajs-1795 27 3 solution solution NOUN iajs-1795 27 4 was be AUX iajs-1795 27 5 reflexed reflexe VERB iajs-1795 27 6 3hr 3hr ADV iajs-1795 27 7 at at ADP iajs-1795 27 8 70c 70c NOUN iajs-1795 27 9 ° ° NOUN iajs-1795 27 10 until until SCONJ iajs-1795 27 11 it it PRON iajs-1795 27 12 would would AUX iajs-1795 27 13 be be AUX iajs-1795 27 14 clear clear ADJ iajs-1795 27 15 and and CCONJ iajs-1795 27 16 yield yield VERB iajs-1795 27 17 a a DET iajs-1795 27 18 light light ADJ iajs-1795 27 19 yellowish yellowish NOUN iajs-1795 27 20 solution solution NOUN iajs-1795 27 21 pointed point VERB iajs-1795 27 22 to to PART iajs-1795 27 23 complete complete VERB iajs-1795 27 24 the the DET iajs-1795 27 25 acidic acidic ADJ iajs-1795 27 26 hydrolysis hydrolysis NOUN iajs-1795 27 27 , , PUNCT iajs-1795 27 28 leave leave VERB iajs-1795 27 29 it it PRON iajs-1795 27 30 to to PART iajs-1795 27 31 cool cool VERB iajs-1795 27 32 in in ADP iajs-1795 27 33 ice ice NOUN iajs-1795 27 34 bath bath NOUN iajs-1795 27 35 then then ADV iajs-1795 27 36 transfer transfer VERB iajs-1795 27 37 16.6ml 16.6ml NUM iajs-1795 27 38 to to ADP iajs-1795 27 39 100ml 100ml ADJ iajs-1795 27 40 volumetric volumetric ADJ iajs-1795 27 41 flask flask NOUN iajs-1795 27 42 then then ADV iajs-1795 27 43 diluted dilute VERB iajs-1795 27 44 to to ADP iajs-1795 27 45 the the DET iajs-1795 27 46 mark mark NOUN iajs-1795 27 47 with with ADP iajs-1795 27 48 distilled distil VERB iajs-1795 27 49 water water NOUN iajs-1795 27 50 to to PART iajs-1795 27 51 prepare prepare VERB iajs-1795 27 52 ( ( PUNCT iajs-1795 27 53 100µg.ml-1 100µg.ml-1 NOUN iajs-1795 27 54 ) ) PUNCT iajs-1795 27 55 of of ADP iajs-1795 27 56 hydrolyzed hydrolyzed ADJ iajs-1795 27 57 fur fur NOUN iajs-1795 27 58 . . PUNCT iajs-1795 28 1 reagent reagent ADJ iajs-1795 28 2 solutions solution NOUN iajs-1795 28 3 1 1 NUM iajs-1795 28 4 - - PUNCT iajs-1795 28 5 sodium sodium NOUN iajs-1795 28 6 nitrate nitrate NOUN iajs-1795 28 7 solution solution NOUN iajs-1795 28 8 ( ( PUNCT iajs-1795 28 9 1 1 NUM iajs-1795 28 10 % % NOUN iajs-1795 28 11 ) ) PUNCT iajs-1795 28 12 was be AUX iajs-1795 28 13 prepared prepare VERB iajs-1795 28 14 by by ADP iajs-1795 28 15 dissolving dissolve VERB iajs-1795 28 16 1 1 NUM iajs-1795 28 17 g g NOUN iajs-1795 28 18 of of ADP iajs-1795 28 19 nano2 nano2 NOUN iajs-1795 28 20 ( ( PUNCT iajs-1795 28 21 merck merck PROPN iajs-1795 28 22 ) ) PUNCT iajs-1795 28 23 in in ADP iajs-1795 28 24 distilled distil VERB iajs-1795 28 25 water water NOUN iajs-1795 28 26 and and CCONJ iajs-1795 28 27 dilute dilute VERB iajs-1795 28 28 to to ADP iajs-1795 28 29 the the DET iajs-1795 28 30 mark mark NOUN iajs-1795 28 31 in in ADP iajs-1795 28 32 100ml 100ml ADJ iajs-1795 28 33 volumetric volumetric ADJ iajs-1795 28 34 flask flask NOUN iajs-1795 28 35 . . PUNCT iajs-1795 29 1 2 2 NUM iajs-1795 29 2 - - PUNCT iajs-1795 29 3 sodium sodium NOUN iajs-1795 29 4 hydroxide hydroxide NOUN iajs-1795 29 5 solution solution NOUN iajs-1795 29 6 ( ( PUNCT iajs-1795 29 7 1.5 1.5 NUM iajs-1795 29 8 m m NOUN iajs-1795 29 9 ) ) PUNCT iajs-1795 29 10 was be AUX iajs-1795 29 11 prepared prepare VERB iajs-1795 29 12 by by ADP iajs-1795 29 13 dissolving dissolve VERB iajs-1795 29 14 1.5 1.5 NUM iajs-1795 29 15 g g NOUN iajs-1795 29 16 of of ADP iajs-1795 29 17 naoh naoh NOUN iajs-1795 29 18 ( ( PUNCT iajs-1795 29 19 merck merck PROPN iajs-1795 29 20 ) ) PUNCT iajs-1795 29 21 in in ADP iajs-1795 29 22 distilled distil VERB iajs-1795 29 23 water water NOUN iajs-1795 29 24 and and CCONJ iajs-1795 29 25 dilute dilute VERB iajs-1795 29 26 to to ADP iajs-1795 29 27 the the DET iajs-1795 29 28 mark mark NOUN iajs-1795 29 29 in in ADP iajs-1795 29 30 25ml 25ml ADJ iajs-1795 29 31 volumetric volumetric NOUN iajs-1795 29 32 flask flask NOUN iajs-1795 29 33 . . PUNCT iajs-1795 30 1 3buffer 3buffer NUM iajs-1795 30 2 solution solution NOUN iajs-1795 30 3 ( ( PUNCT iajs-1795 30 4 ph11 ph11 PROPN iajs-1795 30 5 ) ) PUNCT iajs-1795 30 6 was be AUX iajs-1795 30 7 prepared prepare VERB iajs-1795 30 8 by by ADP iajs-1795 30 9 mixing mix VERB iajs-1795 30 10 100ml 100ml NOUN iajs-1795 30 11 of of ADP iajs-1795 30 12 0.025 0.025 NUM iajs-1795 30 13 m m NOUN iajs-1795 30 14 borax borax NOUN iajs-1795 30 15 with with ADP iajs-1795 30 16 41ml 41ml ADJ iajs-1795 30 17 of of ADP iajs-1795 30 18 0.1 0.1 NUM iajs-1795 30 19 m m NOUN iajs-1795 30 20 hcl hcl PROPN iajs-1795 30 21 4 4 NUM iajs-1795 30 22 - - PUNCT iajs-1795 30 23 sodium sodium NOUN iajs-1795 30 24 carbonate carbonate NOUN iajs-1795 30 25 solution solution NOUN iajs-1795 30 26 ( ( PUNCT iajs-1795 30 27 1.5 1.5 NUM iajs-1795 30 28 m m NOUN iajs-1795 30 29 ) ) PUNCT iajs-1795 30 30 was be AUX iajs-1795 30 31 prepared prepare VERB iajs-1795 30 32 by by ADP iajs-1795 30 33 dissolving dissolve VERB iajs-1795 30 34 3.9 3.9 NUM iajs-1795 30 35 g g NOUN iajs-1795 30 36 of of ADP iajs-1795 30 37 salt salt NOUN iajs-1795 30 38 in in ADP iajs-1795 30 39 distilled distil VERB iajs-1795 30 40 water water NOUN iajs-1795 30 41 and and CCONJ iajs-1795 30 42 dilute dilute VERB iajs-1795 30 43 to to ADP iajs-1795 30 44 the the DET iajs-1795 30 45 mark mark NOUN iajs-1795 30 46 in in ADP iajs-1795 30 47 25ml 25ml ADJ iajs-1795 30 48 volumetric volumetric NOUN iajs-1795 30 49 flask flask NOUN iajs-1795 30 50 . . PUNCT iajs-1795 31 1 pharmaceutical pharmaceutical NOUN iajs-1795 31 2 and and CCONJ iajs-1795 31 3 synthetic synthetic ADJ iajs-1795 31 4 urine urine NOUN iajs-1795 31 5 solutions solution NOUN iajs-1795 31 6 a a DET iajs-1795 31 7 _ _ NOUN iajs-1795 31 8 synthetic synthetic ADJ iajs-1795 31 9 urine urine NOUN iajs-1795 31 10 sample sample NOUN iajs-1795 31 11 was be AUX iajs-1795 31 12 spiked spike VERB iajs-1795 31 13 in in ADP iajs-1795 31 14 order order NOUN iajs-1795 31 15 to to PART iajs-1795 31 16 achieve achieve VERB iajs-1795 31 17 concentration concentration NOUN iajs-1795 31 18 close close ADV iajs-1795 31 19 to to ADP iajs-1795 31 20 ( ( PUNCT iajs-1795 31 21 4.0x10 4.0x10 NUM iajs-1795 31 22 - - SYM iajs-1795 31 23 4 4 NUM iajs-1795 31 24 ) ) PUNCT iajs-1795 31 25 m. m. 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PUNCT iajs-1795 34 1 a a DET iajs-1795 34 2 portion portion NOUN iajs-1795 34 3 of of ADP iajs-1795 34 4 the the DET iajs-1795 34 5 result result NOUN iajs-1795 34 6 powder powder NOUN iajs-1795 34 7 ( ( PUNCT iajs-1795 34 8 containing contain VERB iajs-1795 34 9 0.25 0.25 NUM iajs-1795 34 10 g g ADP iajs-1795 34 11 fur fur NOUN iajs-1795 34 12 ) ) PUNCT iajs-1795 34 13 was be AUX iajs-1795 34 14 used use VERB iajs-1795 34 15 for for ADP iajs-1795 34 16 the the DET iajs-1795 34 17 preparation preparation NOUN iajs-1795 34 18 of of ADP iajs-1795 34 19 the the DET iajs-1795 34 20 solution solution NOUN iajs-1795 34 21 as as SCONJ iajs-1795 34 22 described describe VERB iajs-1795 34 23 before before ADV iajs-1795 34 24 . . PUNCT iajs-1795 35 1 calibration calibration NOUN iajs-1795 35 2 curve curve NOUN iajs-1795 35 3 procedure procedure NOUN iajs-1795 35 4 . . 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PUNCT iajs-1795 37 1 samples sample NOUN iajs-1795 37 2 for for ADP iajs-1795 37 3 each each DET iajs-1795 37 4 test test NOUN iajs-1795 37 5 were be AUX iajs-1795 37 6 prepared prepare VERB iajs-1795 37 7 by by ADP iajs-1795 37 8 adding add VERB iajs-1795 37 9 0.5 0.5 NUM iajs-1795 37 10 ml ml NOUN iajs-1795 37 11 of of ADP iajs-1795 37 12 freshly freshly ADV iajs-1795 37 13 1 1 NUM iajs-1795 37 14 % % NOUN iajs-1795 37 15 nano2 nano2 NOUN iajs-1795 37 16 , , PUNCT iajs-1795 37 17 then then ADV iajs-1795 37 18 0.5 0.5 NUM iajs-1795 37 19 ml ml NOUN iajs-1795 37 20 of of ADP iajs-1795 37 21 3,5_dmph 3,5_dmph NUM iajs-1795 37 22 added add VERB iajs-1795 37 23 to to ADP iajs-1795 37 24 the the DET iajs-1795 37 25 resulting result VERB iajs-1795 37 26 solutions solution NOUN iajs-1795 37 27 followed follow VERB iajs-1795 37 28 addition addition NOUN iajs-1795 37 29 of of ADP iajs-1795 37 30 0.7 0.7 NUM iajs-1795 37 31 ml ml NOUN iajs-1795 37 32 buffer buffer NOUN iajs-1795 37 33 solution solution NOUN iajs-1795 37 34 . . 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PUNCT iajs-1795 44 1 3 3 X iajs-1795 44 2 . . 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PUNCT iajs-1795 53 1 the the DET iajs-1795 53 2 suggested suggest VERB iajs-1795 53 3 mechanism mechanism NOUN iajs-1795 53 4 for for ADP iajs-1795 53 5 the the DET iajs-1795 53 6 hydrolysis hydrolysis NOUN iajs-1795 53 7 and and CCONJ iajs-1795 53 8 diazotization diazotization NOUN iajs-1795 53 9 with with ADP iajs-1795 53 10 coupling coupling NOUN iajs-1795 53 11 reaction reaction NOUN iajs-1795 53 12 is be AUX iajs-1795 53 13 shown show VERB iajs-1795 53 14 in in ADP iajs-1795 53 15 scheme scheme NOUN iajs-1795 53 16 ( ( PUNCT iajs-1795 53 17 2 2 NUM iajs-1795 53 18 ): ): PUNCT iajs-1795 53 19 ihsciconf ihsciconf NOUN iajs-1795 53 20 2017 2017 NUM iajs-1795 53 21 special special ADJ iajs-1795 53 22 issue issue NOUN iajs-1795 53 23 ibn ibn PROPN iajs-1795 53 24 al al PROPN iajs-1795 53 25 - - PUNCT iajs-1795 53 26 haitham haitham PROPN iajs-1795 53 27 journal journal PROPN iajs-1795 53 28 for for ADP iajs-1795 53 29 pure pure ADJ iajs-1795 53 30 and and CCONJ iajs-1795 53 31 applied apply VERB iajs-1795 53 32 science science NOUN iajs-1795 53 33 https://doi.org/ https://doi.org/ NOUN iajs-1795 53 34 10.30526/2017.ihsciconf.1795 10.30526/2017.ihsciconf.1795 NUM iajs-1795 53 35 for for ADP iajs-1795 53 36 more more ADJ iajs-1795 53 37 information information NOUN iajs-1795 53 38 about about ADP iajs-1795 53 39 the the DET iajs-1795 53 40 conference conference NOUN iajs-1795 53 41 please please INTJ iajs-1795 53 42 visit visit VERB iajs-1795 53 43 the the DET iajs-1795 53 44 websites website NOUN iajs-1795 53 45 : : PUNCT iajs-1795 54 1 http://www.ihsciconf.org/conf/ http://www.ihsciconf.org/conf/ VERB iajs-1795 54 2         SPACE iajs-1795 54 3 www.ihsciconf.org www.ihsciconf.org ADJ iajs-1795 54 4       SPACE iajs-1795 54 5 chemistry chemistry NOUN iajs-1795 54 6 |225 |225 PUNCT iajs-1795 54 7             SPACE iajs-1795 54 8 final final ADJ iajs-1795 54 9 absorption absorption NOUN iajs-1795 54 10 spectra spectra NOUN iajs-1795 54 11 the the DET iajs-1795 54 12 absorption absorption NOUN iajs-1795 54 13 of of ADP iajs-1795 54 14 the the DET iajs-1795 54 15 spectrum spectrum NOUN iajs-1795 54 16 colored color VERB iajs-1795 54 17 produced produce VERB iajs-1795 54 18 under under ADP iajs-1795 54 19 optimum optimum ADJ iajs-1795 54 20 reaction reaction NOUN iajs-1795 54 21 condition condition NOUN iajs-1795 54 22 , , PUNCT iajs-1795 54 23 shows show NOUN iajs-1795 54 24 , , PUNCT iajs-1795 54 25 maximum maximum ADJ iajs-1795 54 26 absorption absorption NOUN iajs-1795 54 27 at at ADP iajs-1795 54 28 434 434 NUM iajs-1795 54 29 nm nm NOUN iajs-1795 54 30 against against ADP iajs-1795 54 31 reagent reagent ADJ iajs-1795 54 32 blank blank ADJ iajs-1795 54 33 figure figure NOUN iajs-1795 54 34 ( ( PUNCT iajs-1795 54 35 5 5 NUM iajs-1795 54 36 ) ) PUNCT iajs-1795 54 37 calibration calibration NOUN iajs-1795 54 38 curve curve NOUN iajs-1795 54 39 and and CCONJ iajs-1795 54 40 analytical analytical ADJ iajs-1795 54 41 data datum NOUN iajs-1795 54 42 employing employ VERB iajs-1795 54 43 the the DET iajs-1795 54 44 optimum optimum ADJ iajs-1795 54 45 conditions condition NOUN iajs-1795 54 46 , , PUNCT iajs-1795 54 47 the the DET iajs-1795 54 48 measured measured ADJ iajs-1795 54 49 absorbance absorbance NOUN iajs-1795 54 50 at at ADP iajs-1795 54 51 434 434 NUM iajs-1795 54 52 nm nm NOUN iajs-1795 54 53 versus versus ADP iajs-1795 54 54 different different ADJ iajs-1795 54 55 standard standard ADJ iajs-1795 54 56 concentrations concentration NOUN iajs-1795 54 57 of of ADP iajs-1795 54 58 fur fur NOUN iajs-1795 54 59 were be AUX iajs-1795 54 60 plotted plot VERB iajs-1795 54 61 to to PART iajs-1795 54 62 construct construct VERB iajs-1795 54 63 calibration calibration NOUN iajs-1795 54 64 curve curve NOUN iajs-1795 54 65 . . PUNCT iajs-1795 55 1 the the DET iajs-1795 55 2 linearity linearity NOUN iajs-1795 55 3 of of ADP iajs-1795 55 4 the the DET iajs-1795 55 5 obtained obtain VERB iajs-1795 55 6 plot plot NOUN iajs-1795 55 7 was be AUX iajs-1795 55 8 in in ADP iajs-1795 55 9 the the DET iajs-1795 55 10 concentration concentration NOUN iajs-1795 55 11 range range NOUN iajs-1795 55 12 ( ( PUNCT iajs-1795 55 13 0.4 0.4 NUM iajs-1795 55 14 _ _ NOUN iajs-1795 55 15 50 50 NUM iajs-1795 55 16 ) ) PUNCT iajs-1795 55 17 µg.ml-1 µg.ml-1 ADJ iajs-1795 55 18 as as SCONJ iajs-1795 55 19 shown show VERB iajs-1795 55 20 in in ADP iajs-1795 55 21 figure figure NOUN iajs-1795 55 22 ( ( PUNCT iajs-1795 55 23 6 6 NUM iajs-1795 55 24 ) ) PUNCT iajs-1795 55 25 . . PUNCT iajs-1795 56 1 evaluating evaluate VERB iajs-1795 56 2 the the DET iajs-1795 56 3 liner liner NOUN iajs-1795 56 4 regression regression NOUN iajs-1795 56 5 evaluating evaluate VERB iajs-1795 56 6 the the DET iajs-1795 56 7 liner liner NOUN iajs-1795 56 8 regression regression NOUN iajs-1795 56 9 of of ADP iajs-1795 56 10 the the DET iajs-1795 56 11 suggested suggest VERB iajs-1795 56 12 method method NOUN iajs-1795 56 13 is be AUX iajs-1795 56 14 done do VERB iajs-1795 56 15 by by ADP iajs-1795 56 16 plotting plot VERB iajs-1795 56 17 the the DET iajs-1795 56 18 standardized standardized ADJ iajs-1795 56 19 concentration concentration NOUN iajs-1795 56 20 residuals residual NOUN iajs-1795 56 21 vs vs ADP iajs-1795 56 22 the the DET iajs-1795 56 23 predicated predicate VERB iajs-1795 56 24 concentration concentration NOUN iajs-1795 56 25 of of ADP iajs-1795 56 26 the the DET iajs-1795 56 27 tested test VERB iajs-1795 56 28 standard standard ADJ iajs-1795 56 29 solutions solution NOUN iajs-1795 56 30 . . PUNCT iajs-1795 57 1 the the DET iajs-1795 57 2 residuals residual NOUN iajs-1795 57 3 for for ADP iajs-1795 57 4 fur fur NOUN iajs-1795 57 5 in in ADP iajs-1795 57 6 all all DET iajs-1795 57 7 points point NOUN iajs-1795 57 8 appear appear VERB iajs-1795 57 9 to to PART iajs-1795 57 10 be be AUX iajs-1795 57 11 randomly randomly ADV iajs-1795 57 12 distributed distribute VERB iajs-1795 57 13 around around ADP iajs-1795 57 14 zero zero NUM iajs-1795 57 15 as as SCONJ iajs-1795 57 16 show show NOUN iajs-1795 57 17 in in ADP iajs-1795 57 18 figure figure NOUN iajs-1795 57 19 ( ( PUNCT iajs-1795 57 20 7 7 NUM iajs-1795 57 21 ) ) PUNCT iajs-1795 57 22 stoichiometry stoichiometry NOUN iajs-1795 57 23 of of ADP iajs-1795 57 24 the the DET iajs-1795 57 25 product product NOUN iajs-1795 57 26 jobs job NOUN iajs-1795 57 27 and and CCONJ iajs-1795 57 28 mole mole NOUN iajs-1795 57 29 ratio ratio NOUN iajs-1795 57 30 methods method NOUN iajs-1795 57 31 have have AUX iajs-1795 57 32 been be AUX iajs-1795 57 33 used use VERB iajs-1795 57 34 to to PART iajs-1795 57 35 determine determine VERB iajs-1795 57 36 the the DET iajs-1795 57 37 stoichiometry stoichiometry NOUN iajs-1795 57 38 of of ADP iajs-1795 57 39 the the DET iajs-1795 57 40 colored colored ADJ iajs-1795 57 41 product product NOUN iajs-1795 57 42 . . PUNCT iajs-1795 58 1 fur fur NOUN iajs-1795 58 2 and and CCONJ iajs-1795 58 3 3 3 NUM iajs-1795 58 4 , , PUNCT iajs-1795 58 5 5_dmph 5_dmph NUM iajs-1795 58 6 solution solution NOUN iajs-1795 58 7 of of ADP iajs-1795 58 8 1.38x10 1.38x10 NUM iajs-1795 58 9 - - SYM iajs-1795 58 10 3 3 NUM iajs-1795 58 11 m m NOUN iajs-1795 58 12 were be AUX iajs-1795 58 13 prepared prepare VERB iajs-1795 58 14 and and CCONJ iajs-1795 58 15 mixed mix VERB iajs-1795 58 16 in in ADP iajs-1795 58 17 various various ADJ iajs-1795 58 18 molar molar ADJ iajs-1795 58 19 ratio ratio NOUN iajs-1795 58 20 in in ADP iajs-1795 58 21 5ml 5ml ADJ iajs-1795 58 22 volumetric volumetric ADJ iajs-1795 58 23 flask flask NOUN iajs-1795 58 24 . . PUNCT iajs-1795 59 1 according accord VERB iajs-1795 59 2 to to ADP iajs-1795 59 3 the the DET iajs-1795 59 4 suggested suggest VERB iajs-1795 59 5 procedure procedure NOUN iajs-1795 59 6 , , PUNCT iajs-1795 59 7 the the DET iajs-1795 59 8 absorbance absorbance NOUN iajs-1795 59 9 was be AUX iajs-1795 59 10 measured measure VERB iajs-1795 59 11 at434 at434 PROPN iajs-1795 59 12 nm nm NOUN iajs-1795 59 13 . . PUNCT iajs-1795 60 1 the the DET iajs-1795 60 2 graph graph NOUN iajs-1795 60 3 of of ADP iajs-1795 60 4 the the DET iajs-1795 60 5 results result NOUN iajs-1795 60 6 obtained obtain VERB iajs-1795 60 7 as as ADP iajs-1795 60 8 in in ADP iajs-1795 60 9 figure figure NOUN iajs-1795 60 10 ( ( PUNCT iajs-1795 60 11 8) 8) NUM iajs-1795 60 12 & & CCONJ iajs-1795 60 13 ( ( PUNCT iajs-1795 60 14 9 9 NUM iajs-1795 60 15 ) ) PUNCT iajs-1795 60 16 gave give VERB iajs-1795 60 17 maximum maximum ADJ iajs-1795 60 18 mole mole NOUN iajs-1795 60 19 ratio ratio NOUN iajs-1795 60 20 xmax= xmax= NUM iajs-1795 60 21 0.5 0.5 NUM iajs-1795 60 22 , , PUNCT iajs-1795 60 23 x= x= NUM iajs-1795 60 24 1 1 NUM iajs-1795 60 25 in in ADP iajs-1795 60 26 jobs job NOUN iajs-1795 60 27 and and CCONJ iajs-1795 60 28 mole mole NOUN iajs-1795 60 29 ratio ratio NOUN iajs-1795 60 30 method method NOUN iajs-1795 60 31 respectively respectively ADV iajs-1795 60 32 and and CCONJ iajs-1795 60 33 showed show VERB iajs-1795 60 34 that1:1 that1:1 NOUN iajs-1795 60 35 fur fur NOUN iajs-1795 60 36 : : PUNCT iajs-1795 60 37 3 3 NUM iajs-1795 60 38 , , PUNCT iajs-1795 60 39 5_dmph 5_dmph NUM iajs-1795 60 40 . . PUNCT iajs-1795 60 41 scheme scheme NOUN iajs-1795 60 42 ( ( PUNCT iajs-1795 60 43 2 2 NUM iajs-1795 60 44 ): ): PUNCT iajs-1795 60 45 the the DET iajs-1795 60 46 hydrolysis hydrolysis NOUN iajs-1795 60 47 and and CCONJ iajs-1795 60 48 diazotization diazotization NOUN iajs-1795 60 49 with with ADP iajs-1795 60 50 coupling couple VERB iajs-1795 60 51 reaction reaction NOUN iajs-1795 60 52 of of ADP iajs-1795 60 53 fur fur NOUN iajs-1795 60 54 with with ADP iajs-1795 60 55 3 3 NUM iajs-1795 60 56 , , PUNCT iajs-1795 60 57 5 5 NUM iajs-1795 60 58 - - PUNCT iajs-1795 60 59 dmph dmph ADJ iajs-1795 60 60 ihsciconf ihsciconf NOUN iajs-1795 60 61 2017 2017 NUM iajs-1795 60 62 special special ADJ iajs-1795 60 63 issue issue NOUN iajs-1795 60 64 ibn ibn PROPN iajs-1795 60 65 al al PROPN iajs-1795 60 66 - - PUNCT iajs-1795 60 67 haitham haitham PROPN iajs-1795 60 68 journal journal PROPN iajs-1795 60 69 for for ADP iajs-1795 60 70 pure pure ADJ iajs-1795 60 71 and and CCONJ iajs-1795 60 72 applied apply VERB iajs-1795 60 73 science science NOUN iajs-1795 60 74 https://doi.org/ https://doi.org/ NOUN iajs-1795 60 75 10.30526/2017.ihsciconf.1795 10.30526/2017.ihsciconf.1795 NUM iajs-1795 60 76 for for ADP iajs-1795 60 77 more more ADJ iajs-1795 60 78 information information NOUN iajs-1795 60 79 about about ADP iajs-1795 60 80 the the DET iajs-1795 60 81 conference conference NOUN iajs-1795 60 82 please please INTJ iajs-1795 60 83 visit visit VERB iajs-1795 60 84 the the DET iajs-1795 60 85 websites website NOUN iajs-1795 60 86 : : PUNCT iajs-1795 60 87 http://www.ihsciconf.org/conf/ http://www.ihsciconf.org/conf/ VERB iajs-1795 60 88         SPACE iajs-1795 60 89 www.ihsciconf.org www.ihsciconf.org ADJ iajs-1795 60 90       SPACE iajs-1795 60 91 chemistry chemistry NOUN iajs-1795 60 92 |226 |226 PROPN iajs-1795 60 93     SPACE iajs-1795 60 94 precision precision NOUN iajs-1795 60 95 and and CCONJ iajs-1795 60 96 accuracy accuracy NOUN iajs-1795 60 97 the the DET iajs-1795 60 98 precision precision NOUN iajs-1795 60 99 and and CCONJ iajs-1795 60 100 accuracy accuracy NOUN iajs-1795 60 101 of of ADP iajs-1795 60 102 the the DET iajs-1795 60 103 proposed propose VERB iajs-1795 60 104 method method NOUN iajs-1795 60 105 was be AUX iajs-1795 60 106 tested test VERB iajs-1795 60 107 by by ADP iajs-1795 60 108 analyzing analyze VERB iajs-1795 60 109 five five NUM iajs-1795 60 110 replicate replicate NOUN iajs-1795 60 111 of of ADP iajs-1795 60 112 fur fur NOUN iajs-1795 60 113 in in ADP iajs-1795 60 114 three three NUM iajs-1795 60 115 different different ADJ iajs-1795 60 116 levels level NOUN iajs-1795 60 117 ( ( PUNCT iajs-1795 60 118 within within ADP iajs-1795 60 119 beers beer NOUN iajs-1795 60 120 ' ' PART iajs-1795 60 121 law law NOUN iajs-1795 60 122 range range NOUN iajs-1795 60 123 ) ) PUNCT iajs-1795 60 124 . . PUNCT iajs-1795 61 1 the the DET iajs-1795 61 2 result result NOUN iajs-1795 61 3 list list NOUN iajs-1795 61 4 in in ADP iajs-1795 61 5 table table NOUN iajs-1795 61 6 ( ( PUNCT iajs-1795 61 7 3 3 X iajs-1795 61 8 ) ) PUNCT iajs-1795 61 9 indicates indicate VERB iajs-1795 61 10 an an DET iajs-1795 61 11 acceptable acceptable ADJ iajs-1795 61 12 accuracy accuracy NOUN iajs-1795 61 13 and and CCONJ iajs-1795 61 14 precision precision NOUN iajs-1795 61 15 to to PART iajs-1795 61 16 suggested suggest VERB iajs-1795 61 17 work work NOUN iajs-1795 61 18 . . PUNCT iajs-1795 62 1 interferences interference NOUN iajs-1795 62 2 study study VERB iajs-1795 62 3 the the DET iajs-1795 62 4 presence presence NOUN iajs-1795 62 5 of of ADP iajs-1795 62 6 different different ADJ iajs-1795 62 7 quantity quantity NOUN iajs-1795 62 8 ( ( PUNCT iajs-1795 62 9 2 2 NUM iajs-1795 62 10 , , PUNCT iajs-1795 62 11 6 6 NUM iajs-1795 62 12 and and CCONJ iajs-1795 62 13 12ml 12ml NUM iajs-1795 62 14 ) ) PUNCT iajs-1795 62 15 of of ADP iajs-1795 62 16 1000µg.ml-1 1000µg.ml-1 PROPN iajs-1795 62 17 for for ADP iajs-1795 62 18 excipients excipient NOUN iajs-1795 62 19 can can AUX iajs-1795 62 20 be be AUX iajs-1795 62 21 tolerates tolerate NOUN iajs-1795 62 22 in in ADP iajs-1795 62 23 the the DET iajs-1795 62 24 analysis analysis NOUN iajs-1795 62 25 5µg.ml-1 5µg.ml-1 PRON iajs-1795 62 26 fur fur NOUN iajs-1795 62 27 since since SCONJ iajs-1795 62 28 it it PRON iajs-1795 62 29 would would AUX iajs-1795 62 30 cause cause VERB iajs-1795 62 31 relative relative ADJ iajs-1795 62 32 error error NOUN iajs-1795 62 33 percent percent NOUN iajs-1795 62 34 less less ADJ iajs-1795 62 35 than than ADP iajs-1795 62 36 5 5 NUM iajs-1795 62 37 % % NOUN iajs-1795 62 38 as as SCONJ iajs-1795 62 39 it it PRON iajs-1795 62 40 shown show VERB iajs-1795 62 41 in in ADP iajs-1795 62 42 table table NOUN iajs-1795 62 43 ( ( PUNCT iajs-1795 62 44 4 4 NUM iajs-1795 62 45 ) ) PUNCT iajs-1795 62 46 . . PUNCT iajs-1795 63 1 application application NOUN iajs-1795 63 2 in in ADP iajs-1795 63 3 pharmaceutical pharmaceutical ADJ iajs-1795 63 4 forms form NOUN iajs-1795 63 5 in in ADP iajs-1795 63 6 order order NOUN iajs-1795 63 7 to to PART iajs-1795 63 8 demonstrate demonstrate VERB iajs-1795 63 9 the the DET iajs-1795 63 10 applicability applicability NOUN iajs-1795 63 11 of of ADP iajs-1795 63 12 the the DET iajs-1795 63 13 proposed propose VERB iajs-1795 63 14 method method NOUN iajs-1795 63 15 in in ADP iajs-1795 63 16 determination determination NOUN iajs-1795 63 17 of of ADP iajs-1795 63 18 fur fur NOUN iajs-1795 63 19 , , PUNCT iajs-1795 63 20 the the DET iajs-1795 63 21 method method NOUN iajs-1795 63 22 was be AUX iajs-1795 63 23 applied apply VERB iajs-1795 63 24 to to ADP iajs-1795 63 25 different different ADJ iajs-1795 63 26 manufacturing manufacturing NOUN iajs-1795 63 27 source source NOUN iajs-1795 63 28 containing contain VERB iajs-1795 63 29 fur fur NOUN iajs-1795 63 30 : : PUNCT iajs-1795 63 31 1 1 NUM iajs-1795 63 32 _ _ NOUN iajs-1795 63 33 furosemide furosemide ADV iajs-1795 63 34 ( ( PUNCT iajs-1795 63 35 tablet tablet NOUN iajs-1795 63 36 40 40 NUM iajs-1795 63 37 mg mg NOUN iajs-1795 63 38 ) ) PUNCT iajs-1795 63 39 ajanta ajanta PROPN iajs-1795 63 40 ( ( PUNCT iajs-1795 63 41 india india PROPN iajs-1795 63 42 ) ) PUNCT iajs-1795 63 43 2 2 NUM iajs-1795 63 44 _ _ PRON iajs-1795 63 45 lazine lazine NOUN iajs-1795 63 46 ( ( PUNCT iajs-1795 63 47 furosemide furosemide VERB iajs-1795 63 48 injection injection NOUN iajs-1795 63 49 20 20 NUM iajs-1795 63 50 mg mg NUM iajs-1795 63 51 ) ) PUNCT iajs-1795 63 52 ( ( PUNCT iajs-1795 63 53 syria syria PROPN iajs-1795 63 54 ) ) PUNCT iajs-1795 63 55 to to PART iajs-1795 63 56 apply apply VERB iajs-1795 63 57 the the DET iajs-1795 63 58 suggested suggest VERB iajs-1795 63 59 method method NOUN iajs-1795 63 60 on on ADP iajs-1795 63 61 pharmaceutical pharmaceutical ADJ iajs-1795 63 62 formulation formulation NOUN iajs-1795 63 63 , , PUNCT iajs-1795 63 64 an an PRON iajs-1795 63 65 accurately accurately ADV iajs-1795 63 66 weighed weigh VERB iajs-1795 63 67 1.212 1.212 NUM iajs-1795 63 68 g g NOUN iajs-1795 63 69 from from ADP iajs-1795 63 70 tablet tablet NOUN iajs-1795 63 71 ( ( PUNCT iajs-1795 63 72 40 40 NUM iajs-1795 63 73 mg mg NUM iajs-1795 63 74 ) ) PUNCT iajs-1795 63 75 and and CCONJ iajs-1795 63 76 12.5ml-1 12.5ml-1 NUM iajs-1795 63 77 ( ( PUNCT iajs-1795 63 78 20 20 NUM iajs-1795 63 79 mg mg NUM iajs-1795 63 80 ) ) PUNCT iajs-1795 63 81 from from ADP iajs-1795 63 82 ampule ampule NOUN iajs-1795 63 83 which which PRON iajs-1795 63 84 contains contain VERB iajs-1795 63 85 0.25 0.25 NUM iajs-1795 63 86 g g NOUN iajs-1795 63 87 of of ADP iajs-1795 63 88 pure pure ADJ iajs-1795 63 89 furosemide furosemide NOUN iajs-1795 63 90 to to PART iajs-1795 63 91 prepare prepare VERB iajs-1795 63 92 the the DET iajs-1795 63 93 solutions solution NOUN iajs-1795 63 94 as as SCONJ iajs-1795 63 95 described describe VERB iajs-1795 63 96 before before ADV iajs-1795 63 97 . . PUNCT iajs-1795 64 1 five five NUM iajs-1795 64 2 replicate replicate NOUN iajs-1795 64 3 of of ADP iajs-1795 64 4 three three NUM iajs-1795 64 5 concentration concentration NOUN iajs-1795 64 6 levels level NOUN iajs-1795 64 7 ( ( PUNCT iajs-1795 64 8 2 2 NUM iajs-1795 64 9 , , PUNCT iajs-1795 64 10 6 6 NUM iajs-1795 64 11 and and CCONJ iajs-1795 64 12 12µg.ml-1 12µg.ml-1 NUM iajs-1795 64 13 ) ) PUNCT iajs-1795 64 14 were be AUX iajs-1795 64 15 taken take VERB iajs-1795 64 16 and and CCONJ iajs-1795 64 17 calculated calculate VERB iajs-1795 64 18 the the DET iajs-1795 64 19 recovery recovery NOUN iajs-1795 64 20 and and CCONJ iajs-1795 64 21 relative relative ADJ iajs-1795 64 22 standard standard ADJ iajs-1795 64 23 deviation deviation NOUN iajs-1795 64 24 . . 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