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PUNCT iajs-2441 6 1 the the DET iajs-2441 6 2 developed develop VERB iajs-2441 6 3 diazonium diazonium NOUN iajs-2441 6 4 coupling coupling NOUN iajs-2441 6 5 methods method NOUN iajs-2441 6 6 include include VERB iajs-2441 6 7 an an DET iajs-2441 6 8 optimization optimization NOUN iajs-2441 6 9 study study NOUN iajs-2441 6 10 . . 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PUNCT iajs-2441 11 1 keywords keyword NOUN iajs-2441 11 2 : : PUNCT iajs-2441 11 3 ceftriaxone ceftriaxone PROPN iajs-2441 11 4 ; ; PUNCT iajs-2441 11 5 azo azo PROPN iajs-2441 11 6 dye dye PROPN iajs-2441 11 7 ; ; PUNCT iajs-2441 11 8 coupling coupling NOUN iajs-2441 11 9 ; ; PUNCT iajs-2441 11 10 spectrophotometric spectrophotometric ADJ iajs-2441 11 11 ; ; PUNCT iajs-2441 11 12 2,5 2,5 NUM iajs-2441 11 13 - - PUNCT iajs-2441 11 14 dimethylphenol dimethylphenol NOUN iajs-2441 11 15 ; ; PUNCT iajs-2441 11 16 4 4 NUM iajs-2441 11 17 - - NOUN iajs-2441 11 18 tertbutylphenol tertbutylphenol NOUN iajs-2441 11 19 . . PUNCT iajs-2441 12 1 1 1 X iajs-2441 12 2 . . X iajs-2441 12 3 introduction introduction NOUN iajs-2441 12 4 cephalosporins cephalosporin NOUN iajs-2441 12 5 consist consist VERB iajs-2441 12 6 of of ADP iajs-2441 12 7 two two NUM iajs-2441 12 8 – – PUNCT iajs-2441 12 9 incorporated incorporate VERB iajs-2441 12 10 rings ring NOUN iajs-2441 12 11 system system NOUN iajs-2441 12 12 of of ADP iajs-2441 12 13 beta beta NOUN iajs-2441 12 14 - - PUNCT iajs-2441 12 15 lactam lactam NOUN iajs-2441 12 16 and and CCONJ iajs-2441 12 17 dihydrothiazine dihydrothiazine NOUN iajs-2441 13 1 [ [ X iajs-2441 13 2 1 1 NUM iajs-2441 13 3 ] ] PUNCT iajs-2441 13 4 . . PUNCT iajs-2441 14 1 ceftriaxone ceftriaxone PROPN iajs-2441 14 2 sodium sodium PROPN iajs-2441 14 3 ( ( PUNCT iajs-2441 14 4 cft cft PROPN iajs-2441 14 5 ) ) PUNCT iajs-2441 14 6 is be AUX iajs-2441 14 7 one one NUM iajs-2441 14 8 of of ADP iajs-2441 14 9 the the DET iajs-2441 14 10 third third ADJ iajs-2441 14 11 generation generation NOUN iajs-2441 14 12 cephalosporins cephalosporin NOUN iajs-2441 14 13 and and CCONJ iajs-2441 14 14 one one NUM iajs-2441 14 15 of of ADP iajs-2441 14 16 the the DET iajs-2441 14 17 most most ADV iajs-2441 14 18 widely widely ADV iajs-2441 14 19 used use VERB iajs-2441 14 20 antibiotics antibiotic NOUN iajs-2441 14 21 to to PART iajs-2441 14 22 treat treat VERB iajs-2441 14 23 both both DET iajs-2441 14 24 bacterial bacterial ADJ iajs-2441 14 25 infections infection NOUN iajs-2441 14 26 gram gram NOUN iajs-2441 14 27 positive positive ADJ iajs-2441 14 28 and and CCONJ iajs-2441 14 29 gram gram NOUN iajs-2441 14 30 negative negative ADJ iajs-2441 14 31 [ [ X iajs-2441 14 32 2 2 NUM iajs-2441 14 33 , , PUNCT iajs-2441 14 34 3 3 NUM iajs-2441 14 35 ] ] PUNCT iajs-2441 14 36 . . 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PUNCT iajs-2441 21 5 structure structure NOUN iajs-2441 21 6 of of ADP iajs-2441 21 7 ceftriaxone ceftriaxone PROPN iajs-2441 21 8 sodium sodium NOUN iajs-2441 21 9 . . PUNCT iajs-2441 22 1 ibn ibn PROPN iajs-2441 22 2 al al PROPN iajs-2441 22 3 haitham haitham PROPN iajs-2441 22 4 journal journal PROPN iajs-2441 22 5 for for ADP iajs-2441 22 6 pure pure ADJ iajs-2441 22 7 and and CCONJ iajs-2441 22 8 applied apply VERB iajs-2441 22 9 science science NOUN iajs-2441 22 10 journal journal PROPN iajs-2441 22 11 homepage homepage NOUN iajs-2441 22 12 : : PUNCT iajs-2441 22 13 http://jih.uobaghdad.edu.iq/index.php/j/index http://jih.uobaghdad.edu.iq/index.php/j/index NOUN iajs-2441 22 14 doi doi NOUN iajs-2441 22 15 : : PUNCT iajs-2441 22 16 10.30526/33.2.2441 10.30526/33.2.2441 PROPN iajs-2441 22 17 aya aya PROPN iajs-2441 22 18 w. w. PROPN iajs-2441 22 19 ahmed ahmed PROPN iajs-2441 22 20     SPACE iajs-2441 22 21 salam salam PROPN iajs-2441 22 22 a.h a.h PROPN iajs-2441 22 23 . . PROPN iajs-2441 22 24 al al PROPN iajs-2441 22 25 - - PUNCT iajs-2441 22 26 ameri ameri PROPN iajs-2441 22 27 department department NOUN iajs-2441 22 28 of of ADP iajs-2441 22 29 chemistry chemistry NOUN iajs-2441 22 30 , , PUNCT iajs-2441 22 31 college college NOUN iajs-2441 22 32 of of ADP iajs-2441 22 33 science science NOUN iajs-2441 22 34 , , PUNCT iajs-2441 22 35 university university NOUN iajs-2441 22 36 of of ADP iajs-2441 22 37 mustansiriyah mustansiriyah NOUN iajs-2441 22 38 ayawaleed47@yahoo.com ayawaleed47@yahoo.com PROPN iajs-2441 22 39 article article NOUN iajs-2441 22 40 history history NOUN iajs-2441 22 41 : : PUNCT iajs-2441 22 42 received receive VERB iajs-2441 22 43 17 17 NUM iajs-2441 22 44 june june PROPN iajs-2441 22 45 2019 2019 NUM iajs-2441 22 46 , , PUNCT iajs-2441 22 47 accepted accept VERB iajs-2441 22 48 6 6 NUM iajs-2441 22 49 august august PROPN iajs-2441 22 50 2019 2019 NUM iajs-2441 22 51 , , PUNCT iajs-2441 22 52 published publish VERB iajs-2441 22 53 in in ADP iajs-2441 22 54 april april PROPN iajs-2441 22 55 2020 2020 NUM iajs-2441 22 56 . . PUNCT iajs-2441 22 57     SPACE iajs-2441 23 1 34 34 NUM iajs-2441 23 2 ibn ibn PROPN iajs-2441 23 3 al al PROPN iajs-2441 23 4 - - PUNCT iajs-2441 23 5 haitham haitham PROPN iajs-2441 23 6 jour jour X iajs-2441 23 7 . . PROPN iajs-2441 23 8 for for ADP iajs-2441 23 9 pure pure ADJ iajs-2441 23 10 & & CCONJ iajs-2441 23 11 appl appl PROPN iajs-2441 23 12 . . PUNCT iajs-2441 24 1 sci sci PROPN iajs-2441 24 2 . . PROPN iajs-2441 25 1 33 33 NUM iajs-2441 25 2 ( ( PUNCT iajs-2441 25 3 2 2 NUM iajs-2441 25 4 ) ) PUNCT iajs-2441 25 5 2020 2020 NUM iajs-2441 25 6 several several ADJ iajs-2441 25 7 analytical analytical ADJ iajs-2441 25 8 methods method NOUN iajs-2441 25 9 have have AUX iajs-2441 25 10 been be AUX iajs-2441 25 11 reported report VERB iajs-2441 25 12 for for ADP iajs-2441 25 13 the the DET iajs-2441 25 14 estimation estimation NOUN iajs-2441 25 15 of of ADP iajs-2441 25 16 cft cft NOUN iajs-2441 25 17 in in ADP iajs-2441 25 18 pure pure ADJ iajs-2441 25 19 and and CCONJ iajs-2441 25 20 pharmaceuticals pharmaceutical NOUN iajs-2441 25 21 such such ADJ iajs-2441 25 22 as as ADP iajs-2441 25 23 spectrophotometric spectrophotometric ADJ iajs-2441 25 24 [ [ X iajs-2441 25 25 5 5 NUM iajs-2441 25 26 - - SYM iajs-2441 25 27 8 8 NUM iajs-2441 25 28 ] ] PUNCT iajs-2441 25 29 . . 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PUNCT iajs-2441 38 1 the the DET iajs-2441 38 2 idea idea NOUN iajs-2441 38 3 of of ADP iajs-2441 38 4 this this DET iajs-2441 38 5 work work NOUN iajs-2441 38 6 is be AUX iajs-2441 38 7 to to PART iajs-2441 38 8 develop develop VERB iajs-2441 38 9 a a DET iajs-2441 38 10 simple simple ADJ iajs-2441 38 11 , , PUNCT iajs-2441 38 12 sensitive sensitive ADJ iajs-2441 38 13 and and CCONJ iajs-2441 38 14 effective effective ADJ iajs-2441 38 15 method method NOUN iajs-2441 38 16 for for ADP iajs-2441 38 17 the the DET iajs-2441 38 18 validation validation NOUN iajs-2441 38 19 of of ADP iajs-2441 38 20 the the DET iajs-2441 38 21 ceftriaxone ceftriaxone NOUN iajs-2441 38 22 in in ADP iajs-2441 38 23 pure pure ADJ iajs-2441 38 24 and and CCONJ iajs-2441 38 25 commercial commercial ADJ iajs-2441 38 26 preparation preparation NOUN iajs-2441 38 27 as as ADP iajs-2441 38 28 a a DET iajs-2441 38 29 quality quality NOUN iajs-2441 38 30 control control NOUN iajs-2441 38 31 purpose purpose NOUN iajs-2441 38 32 . . PUNCT iajs-2441 39 1 2 2 X iajs-2441 39 2 . . X iajs-2441 39 3 materials material NOUN iajs-2441 39 4 and and CCONJ iajs-2441 39 5 methods method NOUN iajs-2441 39 6 2 2 NUM iajs-2441 39 7 - - SYM iajs-2441 39 8 1 1 NUM iajs-2441 39 9 . . PUNCT iajs-2441 39 10 chemicals chemical NOUN iajs-2441 39 11 and and CCONJ iajs-2441 39 12 equipment equipment NOUN iajs-2441 39 13 : : PUNCT iajs-2441 39 14 all all DET iajs-2441 39 15 chemicals chemical NOUN iajs-2441 39 16 used use VERB iajs-2441 39 17 were be AUX iajs-2441 39 18 of of ADP iajs-2441 39 19 analytical analytical ADJ iajs-2441 39 20 reagent reagent ADJ iajs-2441 39 21 grade grade NOUN iajs-2441 39 22 with with ADP iajs-2441 39 23 high high ADJ iajs-2441 39 24 purity purity NOUN iajs-2441 39 25 . . PUNCT iajs-2441 40 1 sodium sodium NOUN iajs-2441 40 2 nitrite nitrite NOUN iajs-2441 40 3 , , PUNCT iajs-2441 40 4 hydrochloric hydrochloric ADJ iajs-2441 40 5 acid acid NOUN iajs-2441 40 6 , , PUNCT iajs-2441 40 7 potassium potassium NOUN iajs-2441 40 8 hydroxide hydroxide NOUN iajs-2441 40 9 , , PUNCT iajs-2441 40 10 analytical analytical ADJ iajs-2441 40 11 standard standard NOUN iajs-2441 40 12 of of ADP iajs-2441 40 13 ceftriaxone ceftriaxone PROPN iajs-2441 40 14 sodium sodium NOUN iajs-2441 40 15 , , PUNCT iajs-2441 40 16 analytical analytical ADJ iajs-2441 40 17 standard standard NOUN iajs-2441 40 18 of of ADP iajs-2441 40 19 2,5 2,5 NUM iajs-2441 40 20 - - PUNCT iajs-2441 40 21 dmp dmp NOUN iajs-2441 40 22 and and CCONJ iajs-2441 40 23 4 4 NUM iajs-2441 40 24 - - PUNCT iajs-2441 40 25 tbp tbp NOUN iajs-2441 40 26 were be AUX iajs-2441 40 27 purchased purchase VERB iajs-2441 40 28 from from ADP iajs-2441 40 29 sigma sigma PROPN iajs-2441 40 30 - - PUNCT iajs-2441 40 31 aldrich aldrich PROPN iajs-2441 40 32 , , PUNCT iajs-2441 40 33 al al PROPN iajs-2441 40 34 qiffaf qiffaf PROPN iajs-2441 40 35 scientific scientific ADJ iajs-2441 40 36 company company NOUN iajs-2441 40 37 baghdad baghdad PROPN iajs-2441 40 38 , , PUNCT iajs-2441 40 39 iraq iraq PROPN iajs-2441 40 40 . . 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PUNCT iajs-2441 41 17     SPACE iajs-2441 41 18 for for ADP iajs-2441 41 19 all all DET iajs-2441 41 20 absorbance absorbance NOUN iajs-2441 41 21 detection detection NOUN iajs-2441 41 22 , , PUNCT iajs-2441 41 23 a a DET iajs-2441 41 24 double double ADJ iajs-2441 41 25 beam beam NOUN iajs-2441 41 26 dual dual ADJ iajs-2441 41 27 chopper chopper NOUN iajs-2441 41 28 , , PUNCT iajs-2441 41 29 uv uv NOUN iajs-2441 41 30 - - PUNCT iajs-2441 41 31 vis vis X iajs-2441 41 32 spectrophotometer spectrophotometer NOUN iajs-2441 41 33 , , PUNCT iajs-2441 41 34 varian varian PROPN iajs-2441 41 35 , , PUNCT iajs-2441 41 36 cary cary PROPN iajs-2441 41 37 100 100 NUM iajs-2441 41 38 , , PUNCT iajs-2441 41 39 australia australia PROPN iajs-2441 41 40 was be AUX iajs-2441 41 41 used use VERB iajs-2441 41 42 ph ph ADJ iajs-2441 41 43 s-3e s-3e PROPN iajs-2441 41 44 precision precision NOUN iajs-2441 41 45 acidity acidity NOUN iajs-2441 41 46 meter meter NOUN iajs-2441 41 47 , , PUNCT iajs-2441 41 48 ray ray PROPN iajs-2441 41 49 magnetic magnetic PROPN iajs-2441 41 50 instrument instrument PROPN iajs-2441 41 51 factory factory NOUN iajs-2441 41 52 , , PUNCT iajs-2441 41 53 shanghai shanghai PROPN iajs-2441 41 54 , , PUNCT iajs-2441 41 55 china china PROPN iajs-2441 41 56 . . PUNCT iajs-2441 42 1 mettler mettler PROPN iajs-2441 42 2 ae ae PROPN iajs-2441 42 3 200 200 NUM iajs-2441 42 4 electronic electronic ADJ iajs-2441 42 5 balance balance NOUN iajs-2441 42 6 , , PUNCT iajs-2441 42 7 germany germany PROPN iajs-2441 42 8 and and CCONJ iajs-2441 42 9 shaker shaker NOUN iajs-2441 42 10 . . PUNCT iajs-2441 42 11     SPACE iajs-2441 43 1 2 2 NUM iajs-2441 43 2 - - SYM iajs-2441 43 3 2 2 NUM iajs-2441 43 4 . . PUNCT iajs-2441 43 5 preparation preparation NOUN iajs-2441 43 6 of of ADP iajs-2441 43 7 a a DET iajs-2441 43 8 ceftriaxone ceftriaxone PROPN iajs-2441 43 9 sodium sodium NOUN iajs-2441 43 10 stock stock NOUN iajs-2441 43 11 solution solution NOUN iajs-2441 43 12 a a DET iajs-2441 43 13 1000 1000 NUM iajs-2441 43 14 µg µg NOUN iajs-2441 43 15 . . PUNCT iajs-2441 43 16 ml-1 ml-1 PART iajs-2441 44 1 of of ADP iajs-2441 44 2 standard standard ADJ iajs-2441 44 3 cft cft PROPN iajs-2441 44 4 was be AUX iajs-2441 44 5 prepared prepare VERB iajs-2441 44 6 by by ADP iajs-2441 44 7 dissolving dissolve VERB iajs-2441 44 8 0.1 0.1 NUM iajs-2441 44 9 g g NOUN iajs-2441 44 10 in in ADP iajs-2441 44 11 100 100 NUM iajs-2441 44 12 ml ml NOUN iajs-2441 44 13 of of ADP iajs-2441 44 14 distilled distil VERB iajs-2441 44 15 water water NOUN iajs-2441 44 16 then then ADV iajs-2441 44 17 prepared prepare VERB iajs-2441 44 18 a a DET iajs-2441 44 19 diluted diluted ADJ iajs-2441 44 20 solution solution NOUN iajs-2441 44 21 . . PUNCT iajs-2441 44 22     SPACE iajs-2441 45 1 2 2 NUM iajs-2441 45 2 - - SYM iajs-2441 45 3 3 3 NUM iajs-2441 45 4 . . PUNCT iajs-2441 45 5 general general ADJ iajs-2441 45 6 procedures procedure NOUN iajs-2441 45 7 : : PUNCT iajs-2441 45 8 2 2 NUM iajs-2441 45 9 - - SYM iajs-2441 45 10 3 3 NUM iajs-2441 45 11 - - SYM iajs-2441 45 12 1 1 NUM iajs-2441 45 13 . . PUNCT iajs-2441 45 14 coupling couple VERB iajs-2441 45 15 the the DET iajs-2441 45 16 ceftriaxone ceftriaxone NOUN iajs-2441 45 17 with with ADP iajs-2441 45 18 the the DET iajs-2441 45 19 2,5 2,5 NUM iajs-2441 45 20 - - PUNCT iajs-2441 45 21 dmp dmp NOUN iajs-2441 45 22 reagent reagent NOUN iajs-2441 45 23 : : PUNCT iajs-2441 45 24 in in ADP iajs-2441 45 25 an an DET iajs-2441 45 26 ice ice NOUN iajs-2441 45 27 bath bath NOUN iajs-2441 45 28 at at ADP iajs-2441 45 29 zero zero NUM iajs-2441 45 30 to to ADP iajs-2441 45 31 5 5 NUM iajs-2441 45 32 ᵒc ᵒc NOUN iajs-2441 45 33 ; ; PUNCT iajs-2441 45 34 in in ADP iajs-2441 45 35 a a DET iajs-2441 45 36 20 20 NUM iajs-2441 45 37 ml ml NOUN iajs-2441 45 38 volumetric volumetric NOUN iajs-2441 45 39 flasks flask NOUN iajs-2441 45 40 take take VERB iajs-2441 45 41 a a DET iajs-2441 45 42 0.5 0.5 NUM iajs-2441 45 43 ml ml NOUN iajs-2441 45 44 of of ADP iajs-2441 45 45 1000 1000 NUM iajs-2441 45 46 µg µg NOUN iajs-2441 45 47 . . PUNCT iajs-2441 45 48 ml-1 ml-1 PART iajs-2441 46 1 of of ADP iajs-2441 46 2 standard standard ADJ iajs-2441 46 3 cft cft NOUN iajs-2441 46 4 solution solution NOUN iajs-2441 46 5 then then ADV iajs-2441 46 6 add add VERB iajs-2441 46 7 2.0 2.0 NUM iajs-2441 46 8 ml ml NOUN iajs-2441 46 9 of of ADP iajs-2441 46 10 0.57 0.57 NUM iajs-2441 46 11 m m NOUN iajs-2441 46 12 hcl hcl PROPN iajs-2441 46 13 and and CCONJ iajs-2441 46 14 0.5 0.5 NUM iajs-2441 46 15 ml ml NOUN iajs-2441 46 16 of of ADP iajs-2441 46 17 0.14 0.14 NUM iajs-2441 46 18 m m NOUN iajs-2441 46 19 nano2 nano2 NOUN iajs-2441 46 20 which which PRON iajs-2441 46 21 lead lead VERB iajs-2441 46 22 to to ADP iajs-2441 46 23 forming form VERB iajs-2441 46 24 a a DET iajs-2441 46 25 diazonium diazonium NOUN iajs-2441 46 26 salt salt NOUN iajs-2441 46 27 after after ADP iajs-2441 46 28 leaving leave VERB iajs-2441 46 29 the the DET iajs-2441 46 30 solution solution NOUN iajs-2441 46 31 for for ADP iajs-2441 46 32 10 10 NUM iajs-2441 46 33 minutes minute NOUN iajs-2441 46 34 which which PRON iajs-2441 46 35 coupling couple VERB iajs-2441 46 36 with with ADP iajs-2441 46 37 1.5 1.5 NUM iajs-2441 46 38 ml ml NOUN iajs-2441 46 39 of of ADP iajs-2441 46 40 2.0 2.0 NUM iajs-2441 46 41 x x SYM iajs-2441 46 42 10 10 NUM iajs-2441 46 43 - - SYM iajs-2441 46 44 3 3 NUM iajs-2441 46 45 m m NUM iajs-2441 46 46 2,5 2,5 NUM iajs-2441 46 47 - - PUNCT iajs-2441 46 48 dmp dmp NOUN iajs-2441 46 49 reagent reagent NOUN iajs-2441 46 50 in in ADP iajs-2441 46 51 alkali alkali ADJ iajs-2441 46 52 media medium NOUN iajs-2441 46 53 by by ADP iajs-2441 46 54 using use VERB iajs-2441 46 55 1.5 1.5 NUM iajs-2441 46 56 ml ml NOUN iajs-2441 46 57 of of ADP iajs-2441 46 58 0.45 0.45 NUM iajs-2441 46 59 m m NOUN iajs-2441 46 60 koh koh PROPN iajs-2441 46 61 . . 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PUNCT iajs-2441 49 7 coupling couple VERB iajs-2441 49 8 the the DET iajs-2441 49 9 ceftriaxone ceftriaxone NOUN iajs-2441 49 10 with with ADP iajs-2441 49 11 the the DET iajs-2441 49 12 4 4 NUM iajs-2441 49 13 - - PUNCT iajs-2441 49 14 tbp tbp NOUN iajs-2441 49 15 reagent reagent NOUN iajs-2441 49 16 : : PUNCT iajs-2441 49 17 in in ADP iajs-2441 49 18 an an DET iajs-2441 49 19 ice ice NOUN iajs-2441 49 20 bath bath NOUN iajs-2441 49 21 at at ADP iajs-2441 49 22 zero zero NUM iajs-2441 49 23 to to ADP iajs-2441 49 24 5 5 NUM iajs-2441 49 25 ᵒc ᵒc NOUN iajs-2441 49 26 ; ; PUNCT iajs-2441 49 27 in in ADP iajs-2441 49 28 a a DET iajs-2441 49 29 20 20 NUM iajs-2441 49 30 ml ml NOUN iajs-2441 49 31 , , PUNCT iajs-2441 49 32 volumetric volumetric NOUN iajs-2441 49 33 flasks flask VERB iajs-2441 49 34 a a DET iajs-2441 49 35 0.5 0.5 NUM iajs-2441 49 36 ml ml NOUN iajs-2441 49 37 of of ADP iajs-2441 49 38 1000 1000 NUM iajs-2441 49 39 µg µg NOUN iajs-2441 49 40 . . PUNCT iajs-2441 49 41 ml-1 ml-1 PART iajs-2441 50 1 of of ADP iajs-2441 50 2 standard standard ADJ iajs-2441 50 3 cft cft NOUN iajs-2441 50 4 solution solution NOUN iajs-2441 50 5 was be AUX iajs-2441 50 6 taken take VERB iajs-2441 50 7 then then ADV iajs-2441 50 8 a1.5 a1.5 PROPN iajs-2441 50 9 ml ml ADP iajs-2441 50 10 of of ADP iajs-2441 50 11 0.57 0.57 NUM iajs-2441 50 12 m m NOUN iajs-2441 50 13 hcl hcl PROPN iajs-2441 50 14 and and CCONJ iajs-2441 50 15 1.0 1.0 NUM iajs-2441 50 16 ml ml NOUN iajs-2441 50 17 of of ADP iajs-2441 50 18 0.14 0.14 NUM iajs-2441 50 19 m m PROPN iajs-2441 50 20 nano2 nano2 NOUN iajs-2441 50 21 was be AUX iajs-2441 50 22 added add VERB iajs-2441 50 23 that that SCONJ iajs-2441 50 24 led lead VERB iajs-2441 50 25 to to PART iajs-2441 50 26 form form VERB iajs-2441 50 27 a a DET iajs-2441 50 28 diazonium diazonium NOUN iajs-2441 50 29 salt salt NOUN iajs-2441 50 30 after after ADP iajs-2441 50 31 leaving leave VERB iajs-2441 50 32 the the DET iajs-2441 50 33 solution solution NOUN iajs-2441 50 34 for for ADP iajs-2441 50 35 10 10 NUM iajs-2441 50 36 minutes minute NOUN iajs-2441 50 37 which which PRON iajs-2441 50 38 coupling couple VERB iajs-2441 50 39 with with ADP iajs-2441 50 40 1.5 1.5 NUM iajs-2441 50 41 ml ml NOUN iajs-2441 50 42 of of ADP iajs-2441 50 43 2.5 2.5 NUM iajs-2441 50 44 x x SYM iajs-2441 50 45 10 10 NUM iajs-2441 50 46 - - SYM iajs-2441 50 47 3 3 NUM iajs-2441 50 48 m m NOUN iajs-2441 50 49 4 4 NUM iajs-2441 50 50 - - PUNCT iajs-2441 50 51 tbp tbp NOUN iajs-2441 50 52 reagent reagent NOUN iajs-2441 50 53 in in ADP iajs-2441 50 54 alkali alkali ADJ iajs-2441 50 55 media medium NOUN iajs-2441 50 56 by by ADP iajs-2441 50 57 using use VERB iajs-2441 50 58 2.0 2.0 NUM iajs-2441 50 59 ml ml NOUN iajs-2441 50 60 of of ADP iajs-2441 50 61 0.45 0.45 NUM iajs-2441 50 62 m m NOUN iajs-2441 50 63 koh koh PROPN iajs-2441 50 64 . . 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NOUN iajs-2441 53 3 result result NOUN iajs-2441 53 4 and and CCONJ iajs-2441 53 5 discussion discussion NOUN iajs-2441 53 6 initial initial ADJ iajs-2441 53 7 tests test NOUN iajs-2441 53 8 were be AUX iajs-2441 53 9 performed perform VERB iajs-2441 53 10 via via ADP iajs-2441 53 11 the the DET iajs-2441 53 12 spectrophotometric spectrophotometric ADJ iajs-2441 53 13 method method NOUN iajs-2441 53 14 for for ADP iajs-2441 53 15 the the DET iajs-2441 53 16 estimating estimating NOUN iajs-2441 53 17 of of ADP iajs-2441 53 18 cft cft NOUN iajs-2441 53 19 by by ADP iajs-2441 53 20 using use VERB iajs-2441 53 21 2,5 2,5 NUM iajs-2441 53 22 - - PUNCT iajs-2441 53 23 dmp dmp NOUN iajs-2441 53 24 and and CCONJ iajs-2441 53 25 4 4 NUM iajs-2441 53 26 - - PUNCT iajs-2441 53 27 tbp tbp NOUN iajs-2441 53 28 reagents reagent NOUN iajs-2441 53 29 and and CCONJ iajs-2441 53 30 a a DET iajs-2441 53 31 red red ADJ iajs-2441 53 32 color color NOUN iajs-2441 53 33 of of ADP iajs-2441 53 34 the the DET iajs-2441 53 35 azo azo NOUN iajs-2441 53 36 dye dye NOUN iajs-2441 53 37 formed form VERB iajs-2441 53 38 was be AUX iajs-2441 53 39 illustrate illustrate ADJ iajs-2441 53 40 , , PUNCT iajs-2441 53 41 figure figure VERB iajs-2441 53 42 1 1 NUM iajs-2441 53 43 a a PRON iajs-2441 53 44 , , PUNCT iajs-2441 53 45 b. b. 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PUNCT iajs-2441 56 10 initial initial ADJ iajs-2441 56 11 uv uv NOUN iajs-2441 56 12 - - PUNCT iajs-2441 56 13 vis vis X iajs-2441 56 14 spectra spectra NOUN iajs-2441 56 15 for for ADP iajs-2441 56 16 cft cft PROPN iajs-2441 56 17 azo azo PROPN iajs-2441 56 18 dye dye PROPN iajs-2441 56 19 with with ADP iajs-2441 56 20 ( ( PUNCT iajs-2441 56 21 a a PRON iajs-2441 56 22 ) ) PUNCT iajs-2441 56 23 2,5 2,5 NUM iajs-2441 56 24 - - PUNCT iajs-2441 56 25 dmp dmp NOUN iajs-2441 56 26 and and CCONJ iajs-2441 56 27 ( ( PUNCT iajs-2441 56 28 b b NOUN iajs-2441 56 29 ) ) PUNCT iajs-2441 56 30 4 4 NUM iajs-2441 56 31 - - PUNCT iajs-2441 56 32 tbp tbp NOUN iajs-2441 56 33 reagents reagent NOUN iajs-2441 56 34 . . PUNCT iajs-2441 57 1 3 3 NUM iajs-2441 57 2 - - SYM iajs-2441 57 3 1 1 NUM iajs-2441 57 4 . . PUNCT iajs-2441 57 5 method method NOUN iajs-2441 57 6 optimization optimization NOUN iajs-2441 57 7 this this DET iajs-2441 57 8 spectrophotometric spectrophotometric ADJ iajs-2441 57 9 method method NOUN iajs-2441 57 10 for for ADP iajs-2441 57 11 cft cft NOUN iajs-2441 57 12 estimation estimation NOUN iajs-2441 57 13 including include VERB iajs-2441 57 14 diazonium diazonium NOUN iajs-2441 57 15 coupling coupling NOUN iajs-2441 57 16 was be AUX iajs-2441 57 17 optimized optimize VERB iajs-2441 57 18 . . 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PUNCT iajs-2441 63 4 effect effect NOUN iajs-2441 63 5 of of ADP iajs-2441 63 6 different different ADJ iajs-2441 63 7 hcl hcl PROPN iajs-2441 63 8 concentration concentration NOUN iajs-2441 63 9 ( ( PUNCT iajs-2441 63 10 volume volume NOUN iajs-2441 63 11 ) ) PUNCT iajs-2441 63 12 on on ADP iajs-2441 63 13 the the DET iajs-2441 63 14 cft cft PROPN iajs-2441 63 15 azo azo PROPN iajs-2441 63 16 dye dye NOUN iajs-2441 63 17 formation formation NOUN iajs-2441 63 18 via via ADP iajs-2441 63 19 2,5 2,5 NUM iajs-2441 63 20 - - PUNCT iajs-2441 63 21 dmp dmp NOUN iajs-2441 63 22 and and CCONJ iajs-2441 63 23 4 4 NUM iajs-2441 63 24 - - PUNCT iajs-2441 63 25 tbp tbp NOUN iajs-2441 63 26 reagents reagent NOUN iajs-2441 63 27 . . PUNCT iajs-2441 64 1 3 3 NUM iajs-2441 64 2 - - SYM iajs-2441 64 3 1 1 NUM iajs-2441 64 4 - - SYM iajs-2441 64 5 2 2 NUM iajs-2441 64 6 . . 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PUNCT iajs-2441 66 1 the the DET iajs-2441 66 2 best good ADJ iajs-2441 66 3 of of ADP iajs-2441 66 4 the the DET iajs-2441 66 5 volume volume NOUN iajs-2441 66 6 of of ADP iajs-2441 66 7 sodium sodium NOUN iajs-2441 66 8 nitrate nitrate NOUN iajs-2441 66 9 were be AUX iajs-2441 66 10 0.5 0.5 NUM iajs-2441 66 11 and and CCONJ iajs-2441 66 12 1.0 1.0 NUM iajs-2441 66 13 ml ml NOUN iajs-2441 66 14 and and CCONJ iajs-2441 66 15 the the DET iajs-2441 66 16 product product NOUN iajs-2441 66 17 dyes dye NOUN iajs-2441 66 18 measured measure VERB iajs-2441 66 19 at at ADP iajs-2441 66 20 500 500 NUM iajs-2441 66 21 nm nm NOUN iajs-2441 66 22 and and CCONJ iajs-2441 66 23 520 520 NUM iajs-2441 66 24 nm nm NOUN iajs-2441 66 25 for for ADP iajs-2441 66 26 4 4 NUM iajs-2441 66 27 - - PUNCT iajs-2441 66 28 tbp tbp NOUN iajs-2441 66 29 and and CCONJ iajs-2441 66 30 2,5 2,5 NUM iajs-2441 66 31 - - PUNCT iajs-2441 66 32 dmp dmp NOUN iajs-2441 66 33 reagents reagent NOUN iajs-2441 66 34 respectively respectively ADV iajs-2441 66 35 as as ADP iajs-2441 66 36 in in ADP iajs-2441 66 37 figure figure NOUN iajs-2441 66 38 3 3 NUM iajs-2441 66 39 . . 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PUNCT iajs-2441 68 1 0 0 NUM iajs-2441 68 2 0.05 0.05 NUM iajs-2441 68 3 0.1 0.1 NUM iajs-2441 68 4 0.15 0.15 NUM iajs-2441 68 5 0.2 0.2 NUM iajs-2441 68 6 0.25 0.25 NUM iajs-2441 68 7 0 0 NUM iajs-2441 68 8 0.5 0.5 NUM iajs-2441 68 9 1 1 NUM iajs-2441 68 10 1.5 1.5 NUM iajs-2441 68 11 2 2 NUM iajs-2441 68 12 2.5 2.5 NUM iajs-2441 68 13 3 3 NUM iajs-2441 68 14 volume volume NOUN iajs-2441 68 15     SPACE iajs-2441 68 16 of of ADP iajs-2441 68 17     SPACE iajs-2441 68 18 acid acid NOUN iajs-2441 68 19     SPACE iajs-2441 68 20 ml ml NOUN iajs-2441 68 21 4‐ 4‐ PROPN iajs-2441 68 22 tbp tbp NOUN iajs-2441 68 23 2 2 NUM iajs-2441 68 24 , , PUNCT iajs-2441 68 25 5‐dmp 5‐dmp NUM iajs-2441 68 26     SPACE iajs-2441 68 27 36 36 NUM iajs-2441 68 28 ibn ibn PROPN iajs-2441 68 29 al al PROPN iajs-2441 68 30 - - PUNCT iajs-2441 68 31 haitham haitham PROPN iajs-2441 68 32 jour jour X iajs-2441 68 33 . . 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PUNCT iajs-2441 73 21 effect effect NOUN iajs-2441 73 22 of of ADP iajs-2441 73 23 different different ADJ iajs-2441 73 24 reaction reaction NOUN iajs-2441 73 25 time time NOUN iajs-2441 73 26 on on ADP iajs-2441 73 27 the the DET iajs-2441 73 28 cft cft PROPN iajs-2441 73 29 azo azo PROPN iajs-2441 73 30 dye dye NOUN iajs-2441 73 31 formation formation NOUN iajs-2441 73 32 via via ADP iajs-2441 73 33 2,5 2,5 NUM iajs-2441 73 34 - - PUNCT iajs-2441 73 35 dmp dmp NOUN iajs-2441 73 36 and and CCONJ iajs-2441 73 37 4 4 NUM iajs-2441 73 38 - - PUNCT iajs-2441 73 39 tbp tbp NOUN iajs-2441 73 40 reagents reagent NOUN iajs-2441 73 41 . . PUNCT iajs-2441 74 1 3 3 NUM iajs-2441 74 2 - - SYM iajs-2441 74 3 1 1 NUM iajs-2441 74 4 - - SYM iajs-2441 74 5 4 4 NUM iajs-2441 74 6 . . 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PUNCT iajs-2441 81 1 the the DET iajs-2441 81 2 results result NOUN iajs-2441 81 3 showed show VERB iajs-2441 81 4 that that SCONJ iajs-2441 81 5 the the DET iajs-2441 81 6 1.5 1.5 NUM iajs-2441 81 7 ml ml NOUN iajs-2441 81 8 of of ADP iajs-2441 81 9 2,5 2,5 NUM iajs-2441 81 10 - - PUNCT iajs-2441 81 11 dmp dmp NOUN iajs-2441 81 12 and and CCONJ iajs-2441 81 13 4 4 NUM iajs-2441 81 14 - - PUNCT iajs-2441 81 15 tbp tbp NOUN iajs-2441 81 16 is be AUX iajs-2441 81 17 the the DET iajs-2441 81 18 best good ADJ iajs-2441 81 19 volume volume NOUN iajs-2441 81 20 , , PUNCT iajs-2441 81 21 as as ADP iajs-2441 81 22 in in ADP iajs-2441 81 23 figure figure NOUN iajs-2441 81 24 6 6 NUM iajs-2441 81 25 . . PUNCT iajs-2441 81 26         SPACE iajs-2441 81 27 figure figure NOUN iajs-2441 81 28 6 6 NUM iajs-2441 81 29 . . PUNCT iajs-2441 82 1 effect effect NOUN iajs-2441 82 2 of of ADP iajs-2441 82 3 different different ADJ iajs-2441 82 4 2,5 2,5 NUM iajs-2441 82 5 - - PUNCT iajs-2441 82 6 dmp dmp NOUN iajs-2441 82 7 and and CCONJ iajs-2441 82 8 4 4 NUM iajs-2441 82 9 - - PUNCT iajs-2441 82 10 tbp tbp NOUN iajs-2441 82 11 reagents reagent NOUN iajs-2441 82 12 on on ADP iajs-2441 82 13 the the DET iajs-2441 82 14 cft cft PROPN iajs-2441 82 15 azo azo PROPN iajs-2441 82 16 dye dye NOUN iajs-2441 82 17 formation formation NOUN iajs-2441 82 18 . . PUNCT iajs-2441 83 1 3 3 NUM iajs-2441 83 2 - - SYM iajs-2441 83 3 2 2 NUM iajs-2441 83 4 . . PUNCT iajs-2441 83 5 calibration calibration NOUN iajs-2441 83 6 curve curve NOUN iajs-2441 83 7 and and CCONJ iajs-2441 83 8 analytical analytical ADJ iajs-2441 83 9 merits merit NOUN iajs-2441 83 10 calibration calibration NOUN iajs-2441 83 11 curves curve NOUN iajs-2441 83 12 was be AUX iajs-2441 83 13 constructed construct VERB iajs-2441 83 14 using use VERB iajs-2441 83 15 2.0 2.0 NUM iajs-2441 83 16 x x SYM iajs-2441 83 17 10 10 NUM iajs-2441 83 18 -3 -3 NOUN iajs-2441 83 19 m m VERB iajs-2441 83 20 2,5 2,5 NUM iajs-2441 83 21 - - PUNCT iajs-2441 83 22 dmp dmp NOUN iajs-2441 83 23 and and CCONJ iajs-2441 83 24 2.5 2.5 NUM iajs-2441 83 25 x x SYM iajs-2441 83 26 10 10 NUM iajs-2441 83 27 - - SYM iajs-2441 83 28 3 3 NUM iajs-2441 83 29 m m NOUN iajs-2441 83 30 4 4 NUM iajs-2441 83 31 - - PUNCT iajs-2441 83 32 tbp tbp NOUN iajs-2441 83 33 solutions solution NOUN iajs-2441 83 34 with with ADP iajs-2441 83 35 a a DET iajs-2441 83 36 concentration concentration NOUN iajs-2441 83 37 ranges range NOUN iajs-2441 83 38 of of ADP iajs-2441 83 39 3.0 3.0 NUM iajs-2441 83 40 50 50 NUM iajs-2441 83 41 µg µg NOUN iajs-2441 83 42 . . PUNCT iajs-2441 83 43 ml-1 ml-1 PART iajs-2441 84 1 and and CCONJ iajs-2441 84 2 1030 1030 NUM iajs-2441 84 3 µg µg NOUN iajs-2441 84 4 . . PROPN iajs-2441 85 1 ml-1 ml-1 PART iajs-2441 85 2 of of ADP iajs-2441 85 3 cft cft PROPN iajs-2441 85 4 solution solution NOUN iajs-2441 85 5 via via ADP iajs-2441 85 6 2,5 2,5 NUM iajs-2441 85 7 - - PUNCT iajs-2441 85 8 dmp dmp NOUN iajs-2441 85 9 and and CCONJ iajs-2441 85 10 4 4 NUM iajs-2441 85 11 - - PUNCT iajs-2441 85 12 tbp tbp NOUN iajs-2441 85 13 respectively respectively ADV iajs-2441 85 14 versus versus SCONJ iajs-2441 85 15 the the DET iajs-2441 85 16 absorbance absorbance NOUN iajs-2441 85 17 resulted result VERB iajs-2441 85 18 , , PUNCT iajs-2441 85 19 as as ADP iajs-2441 85 20 in in ADP iajs-2441 85 21 figure figure NOUN iajs-2441 85 22 7 7 NUM iajs-2441 85 23 . . 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PUNCT iajs-2441 87 1 all all DET iajs-2441 87 2 the the DET iajs-2441 87 3 analytical analytical ADJ iajs-2441 87 4 data datum NOUN iajs-2441 87 5 such such ADJ iajs-2441 87 6 as as ADP iajs-2441 87 7 limit limit NOUN iajs-2441 87 8 of of ADP iajs-2441 87 9 detection detection NOUN iajs-2441 87 10 ( ( PUNCT iajs-2441 87 11 lod lod PROPN iajs-2441 87 12 ) ) PUNCT iajs-2441 87 13 , , PUNCT iajs-2441 87 14 limit limit NOUN iajs-2441 87 15 of of ADP iajs-2441 87 16 quantification quantification NOUN iajs-2441 87 17 ( ( PUNCT iajs-2441 87 18 loq loq PROPN iajs-2441 87 19 ) ) PUNCT iajs-2441 87 20 and and CCONJ iajs-2441 87 21 relative relative ADJ iajs-2441 87 22 standard standard ADJ iajs-2441 87 23 deviation deviation NOUN iajs-2441 87 24 ( ( PUNCT iajs-2441 87 25 % % INTJ iajs-2441 87 26 rsd rsd NOUN iajs-2441 87 27 ) ) PUNCT iajs-2441 87 28 were be AUX iajs-2441 87 29 summarized summarize VERB iajs-2441 87 30 in in ADP iajs-2441 87 31 table table NOUN iajs-2441 87 32 1 1 NUM iajs-2441 87 33 . . PUNCT iajs-2441 88 1 [ [ X iajs-2441 88 2 21 21 NUM iajs-2441 88 3 ] ] PUNCT iajs-2441 88 4 . . PUNCT iajs-2441 88 5         SPACE iajs-2441 89 1 38 38 NUM iajs-2441 89 2 ibn ibn PROPN iajs-2441 89 3 al al PROPN iajs-2441 89 4 - - PUNCT iajs-2441 89 5 haitham haitham PROPN iajs-2441 89 6 jour jour X iajs-2441 89 7 . . PROPN iajs-2441 89 8 for for ADP iajs-2441 89 9 pure pure ADJ iajs-2441 89 10 & & CCONJ iajs-2441 89 11 appl appl PROPN iajs-2441 89 12 . . PUNCT iajs-2441 90 1 sci sci PROPN iajs-2441 90 2 . . PROPN iajs-2441 91 1 33 33 NUM iajs-2441 91 2 ( ( PUNCT iajs-2441 91 3 2 2 NUM iajs-2441 91 4 ) ) PUNCT iajs-2441 91 5 2020 2020 NUM iajs-2441 91 6           SPACE iajs-2441 91 7 figure figure NOUN iajs-2441 91 8 7 7 NUM iajs-2441 91 9 . . PUNCT iajs-2441 91 10 calibration calibration NOUN iajs-2441 91 11 graph graph NOUN iajs-2441 91 12 of of ADP iajs-2441 91 13 10 10 NUM iajs-2441 91 14 – – SYM iajs-2441 91 15 30 30 NUM iajs-2441 91 16 and and CCONJ iajs-2441 91 17 3.0 3.0 NUM iajs-2441 91 18 – – SYM iajs-2441 91 19 50 50 NUM iajs-2441 91 20 µg µg NOUN iajs-2441 91 21 . . PUNCT iajs-2441 91 22 ml-1 ml-1 PART iajs-2441 91 23 of of ADP iajs-2441 91 24 cft cft NOUN iajs-2441 91 25 with with ADP iajs-2441 91 26 2.0 2.0 NUM iajs-2441 91 27 x x SYM iajs-2441 91 28 10 10 NUM iajs-2441 91 29 -3 -3 NUM iajs-2441 91 30 m m VERB iajs-2441 91 31 2,5 2,5 NUM iajs-2441 91 32 - - PUNCT iajs-2441 91 33 dmp dmp NOUN iajs-2441 91 34 and and CCONJ iajs-2441 91 35 2.5 2.5 NUM iajs-2441 91 36 x x SYM iajs-2441 91 37 10 10 NUM iajs-2441 91 38 - - SYM iajs-2441 91 39 3 3 NUM iajs-2441 91 40 m m NOUN iajs-2441 91 41 4 4 NUM iajs-2441 91 42 - - PUNCT iajs-2441 91 43 tbp tbp NOUN iajs-2441 91 44 respectively respectively ADV iajs-2441 91 45 . . PUNCT iajs-2441 91 46         SPACE iajs-2441 91 47 figure figure NOUN iajs-2441 91 48 8 8 NUM iajs-2441 91 49 . . PUNCT iajs-2441 92 1 uv uv NOUN iajs-2441 92 2 - - PUNCT iajs-2441 92 3 vis vis X iajs-2441 92 4 spectra spectra NOUN iajs-2441 92 5 of of ADP iajs-2441 92 6 calibration calibration NOUN iajs-2441 92 7 graph graph NOUN iajs-2441 92 8 of of ADP iajs-2441 92 9 10 10 NUM iajs-2441 92 10 – – SYM iajs-2441 92 11 30 30 NUM iajs-2441 92 12 and and CCONJ iajs-2441 92 13 3.0 3.0 NUM iajs-2441 92 14 – – SYM iajs-2441 92 15 50 50 NUM iajs-2441 92 16 µg µg NOUN iajs-2441 92 17 . . PUNCT iajs-2441 93 1 ml-1 ml-1 PART iajs-2441 93 2 of of ADP iajs-2441 93 3 cft cft NOUN iajs-2441 93 4 with with ADP iajs-2441 93 5 2.0 2.0 NUM iajs-2441 93 6 x x SYM iajs-2441 93 7 10 10 NUM iajs-2441 93 8 -3 -3 NUM iajs-2441 93 9 m m VERB iajs-2441 93 10 2,5 2,5 NUM iajs-2441 93 11 - - PUNCT iajs-2441 93 12 dmp dmp NOUN iajs-2441 93 13 and and CCONJ iajs-2441 93 14 2.5 2.5 NUM iajs-2441 93 15 x x SYM iajs-2441 93 16 10 10 NUM iajs-2441 93 17 - - SYM iajs-2441 93 18 3 3 NUM iajs-2441 93 19 m m NOUN iajs-2441 93 20 4 4 NUM iajs-2441 93 21 - - PUNCT iajs-2441 93 22 tbp tbp NOUN iajs-2441 93 23 respectively respectively ADV iajs-2441 93 24 . . PUNCT iajs-2441 93 25                                                                     SPACE iajs-2441 94 1 y y PROPN iajs-2441 94 2     SPACE iajs-2441 94 3 = = NOUN iajs-2441 94 4     SPACE iajs-2441 94 5 0.0134x 0.0134x NOUN iajs-2441 94 6     SPACE iajs-2441 94 7 ‐ ‐ VERB iajs-2441 94 8 0.0152 0.0152 NUM iajs-2441 94 9 r² r² NOUN iajs-2441 94 10     SPACE iajs-2441 94 11 = = NOUN iajs-2441 94 12 0.998 0.998 NUM iajs-2441 94 13 y y NOUN iajs-2441 94 14     SPACE iajs-2441 94 15 = = NOUN iajs-2441 94 16     SPACE iajs-2441 94 17 0.0079x 0.0079x NOUN iajs-2441 94 18     SPACE iajs-2441 94 19 + + NOUN iajs-2441 94 20     SPACE iajs-2441 94 21 0.0057 0.0057 NUM iajs-2441 94 22 r² r² NOUN iajs-2441 94 23     SPACE iajs-2441 94 24 = = PUNCT iajs-2441 95 1 0.9989 0.9989 NUM iajs-2441 95 2 0 0 NUM iajs-2441 95 3 0.05 0.05 NUM iajs-2441 95 4 0.1 0.1 NUM iajs-2441 95 5 0.15 0.15 NUM iajs-2441 95 6 0.2 0.2 NUM iajs-2441 95 7 0.25 0.25 NUM iajs-2441 95 8 0.3 0.3 NUM iajs-2441 95 9 0.35 0.35 NUM iajs-2441 95 10 0.4 0.4 NUM iajs-2441 95 11 0.45 0.45 NUM iajs-2441 95 12 0 0 NUM iajs-2441 95 13 10 10 NUM iajs-2441 95 14 20 20 NUM iajs-2441 95 15 30 30 NUM iajs-2441 95 16 40 40 NUM iajs-2441 95 17 50 50 NUM iajs-2441 95 18 60 60 NUM iajs-2441 95 19 conc conc NOUN iajs-2441 95 20 . . 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PROPN iajs-2441 98 1 33 33 NUM iajs-2441 98 2 ( ( PUNCT iajs-2441 98 3 2 2 NUM iajs-2441 98 4 ) ) PUNCT iajs-2441 98 5 2020 2020 NUM iajs-2441 98 6 table table NOUN iajs-2441 98 7 1 1 NUM iajs-2441 98 8 . . PUNCT iajs-2441 98 9 analytical analytical ADJ iajs-2441 98 10 data datum NOUN iajs-2441 98 11 of of ADP iajs-2441 98 12 the the DET iajs-2441 98 13 proposed propose VERB iajs-2441 98 14 diazotization diazotization NOUN iajs-2441 98 15 - - PUNCT iajs-2441 98 16 coupling couple VERB iajs-2441 98 17 methods method NOUN iajs-2441 98 18 . . PUNCT iajs-2441 99 1 parameters parameter NOUN iajs-2441 99 2 2,5 2,5 NUM iajs-2441 99 3 - - PUNCT iajs-2441 99 4 dmp dmp NOUN iajs-2441 99 5 4 4 NUM iajs-2441 99 6 - - PUNCT iajs-2441 99 7 tbp tbp NOUN iajs-2441 99 8 color color NOUN iajs-2441 99 9 red red PROPN iajs-2441 99 10 orange orange PROPN iajs-2441 99 11 λmax λmax PROPN iajs-2441 99 12 , , PUNCT iajs-2441 99 13 nm nm ADP iajs-2441 99 14 520 520 NUM iajs-2441 99 15 500 500 NUM iajs-2441 99 16 linearity linearity NOUN iajs-2441 99 17 range range NOUN iajs-2441 99 18 , , PUNCT iajs-2441 99 19 µg µg INTJ iajs-2441 99 20 . . PUNCT iajs-2441 99 21 ml-1 ml-1 PART iajs-2441 100 1 ( ( PUNCT iajs-2441 100 2 3 3 NUM iajs-2441 100 3 - - SYM iajs-2441 100 4 50 50 NUM iajs-2441 100 5 ) ) PUNCT iajs-2441 100 6 ( ( PUNCT iajs-2441 100 7 10 10 NUM iajs-2441 100 8 - - SYM iajs-2441 100 9 30 30 NUM iajs-2441 100 10 ) ) PUNCT iajs-2441 100 11 molar molar ADJ iajs-2441 100 12 absorptivity absorptivity NOUN iajs-2441 100 13 , , PUNCT iajs-2441 100 14 ε ε PROPN iajs-2441 100 15 , , PUNCT iajs-2441 100 16 l. l. PROPN iajs-2441 100 17 mol-1.cm-1 mol-1.cm-1 PROPN iajs-2441 100 18 4.377×103 4.377×103 NUM iajs-2441 100 19 7.446×103 7.446×103 NUM iajs-2441 100 20 slope slope NOUN iajs-2441 100 21 , , PUNCT iajs-2441 100 22 b b PROPN iajs-2441 100 23 0.0079 0.0079 NUM iajs-2441 100 24 0.0134 0.0134 NUM iajs-2441 100 25 intercept intercept NOUN iajs-2441 100 26 , , PUNCT iajs-2441 100 27 a a DET iajs-2441 100 28 0.0057 0.0057 NUM iajs-2441 100 29 -0.0152 -0.0152 NOUN iajs-2441 100 30 sandal sandal NOUN iajs-2441 100 31 sensitivity sensitivity NOUN iajs-2441 100 32 , , PUNCT iajs-2441 100 33 s s VERB iajs-2441 100 34 0.1267 0.1267 NUM iajs-2441 100 35 0.0745 0.0745 NUM iajs-2441 100 36 coefficient coefficient NOUN iajs-2441 100 37 of of ADP iajs-2441 100 38 determination determination NOUN iajs-2441 100 39 , , PUNCT iajs-2441 100 40 % % INTJ iajs-2441 100 41 r² r² VERB iajs-2441 100 42 99.89 99.89 NUM iajs-2441 100 43 99.8 99.8 NUM iajs-2441 100 44 correlation correlation NOUN iajs-2441 100 45 coefficient coefficient NOUN iajs-2441 100 46 , , PUNCT iajs-2441 100 47 r r NOUN iajs-2441 100 48 ) ) PUNCT iajs-2441 100 49 0.9994 0.9994 NUM iajs-2441 100 50 0.9990 0.9990 NUM iajs-2441 100 51 limit limit NOUN iajs-2441 100 52 of of ADP iajs-2441 100 53 detection detection NOUN iajs-2441 100 54 , , PUNCT iajs-2441 100 55 lod lod PROPN iajs-2441 100 56 , , PUNCT iajs-2441 100 57 µg µg NOUN iajs-2441 100 58 . . PUNCT iajs-2441 100 59 ml-1 ml-1 PART iajs-2441 101 1 0.4820 0.4820 NUM iajs-2441 101 2 0.2840 0.2840 NUM iajs-2441 101 3 limit limit NOUN iajs-2441 101 4 of of ADP iajs-2441 101 5 quantification quantification NOUN iajs-2441 101 6 , , PUNCT iajs-2441 101 7 loq loq PROPN iajs-2441 101 8 , , PUNCT iajs-2441 101 9 µg µg NOUN iajs-2441 101 10 . . PUNCT iajs-2441 101 11 ml-1 ml-1 PART iajs-2441 102 1 1.6080 1.6080 NUM iajs-2441 102 2 0.9454 0.9454 NUM iajs-2441 102 3 at at ADP iajs-2441 102 4 a a DET iajs-2441 102 5 linear linear ADJ iajs-2441 102 6 concentration concentration NOUN iajs-2441 102 7 range range NOUN iajs-2441 102 8 between between ADP iajs-2441 102 9 3.0 3.0 NUM iajs-2441 102 10 -50 -50 PUNCT iajs-2441 102 11 and and CCONJ iajs-2441 102 12 10 10 NUM iajs-2441 102 13 -30 -30 NUM iajs-2441 102 14 µg µg NOUN iajs-2441 102 15 . . PUNCT iajs-2441 103 1 ml-1 ml-1 PART iajs-2441 104 1 , , PUNCT iajs-2441 104 2 the the DET iajs-2441 104 3 results result NOUN iajs-2441 104 4 showed show VERB iajs-2441 104 5 a a DET iajs-2441 104 6 limit limit NOUN iajs-2441 104 7 of of ADP iajs-2441 104 8 detection detection NOUN iajs-2441 104 9 and and CCONJ iajs-2441 104 10 a a DET iajs-2441 104 11 limit limit NOUN iajs-2441 104 12 of of ADP iajs-2441 104 13 quantification quantification NOUN iajs-2441 104 14 of of ADP iajs-2441 104 15 0.482 0.482 NUM iajs-2441 104 16 , , PUNCT iajs-2441 104 17 0.284 0.284 NUM iajs-2441 104 18 and and CCONJ iajs-2441 104 19 1.608 1.608 NUM iajs-2441 104 20 , , PUNCT iajs-2441 104 21 0.945 0.945 NUM iajs-2441 104 22 µg µg NOUN iajs-2441 104 23 . . PUNCT iajs-2441 104 24 ml-1 ml-1 PART iajs-2441 105 1 with with ADP iajs-2441 105 2 2,5 2,5 NUM iajs-2441 105 3 - - PUNCT iajs-2441 105 4 dmp dmp NOUN iajs-2441 105 5 and and CCONJ iajs-2441 105 6 4tbp 4tbp NOUN iajs-2441 105 7 respectively respectively ADV iajs-2441 105 8 with with ADP iajs-2441 105 9 recovery recovery NOUN iajs-2441 105 10 of of ADP iajs-2441 105 11 100.89 100.89 NUM iajs-2441 105 12 % % NOUN iajs-2441 105 13 and and CCONJ iajs-2441 105 14 103.37 103.37 NUM iajs-2441 105 15 % % NOUN iajs-2441 105 16 , , PUNCT iajs-2441 105 17 with with ADP iajs-2441 105 18 molar molar ADJ iajs-2441 105 19 absorptivity absorptivity NOUN iajs-2441 105 20 of of ADP iajs-2441 105 21 4.377×103 4.377×103 NUM iajs-2441 105 22 and and CCONJ iajs-2441 105 23 7.446×103 7.446×103 NUM iajs-2441 105 24 l. l. PROPN iajs-2441 105 25 mol-1.cm-1 mol-1.cm-1 NOUN iajs-2441 105 26 for for ADP iajs-2441 105 27 2,5 2,5 NUM iajs-2441 105 28 - - PUNCT iajs-2441 105 29 dmp dmp NOUN iajs-2441 105 30 and and CCONJ iajs-2441 105 31 4 4 NUM iajs-2441 105 32 - - PUNCT iajs-2441 105 33 tbp tbp NOUN iajs-2441 105 34 respectively respectively ADV iajs-2441 105 35 . . PUNCT iajs-2441 106 1 3 3 NUM iajs-2441 106 2 - - SYM iajs-2441 106 3 3 3 NUM iajs-2441 106 4 . . NOUN iajs-2441 106 5 accuracy accuracy NOUN iajs-2441 106 6 and and CCONJ iajs-2441 106 7 precision precision VERB iajs-2441 106 8 the the DET iajs-2441 106 9 precision precision NOUN iajs-2441 106 10 and and CCONJ iajs-2441 106 11 accuracy accuracy NOUN iajs-2441 106 12 were be AUX iajs-2441 106 13 calculated calculate VERB iajs-2441 106 14 by by ADP iajs-2441 106 15 the the DET iajs-2441 106 16 analysis analysis NOUN iajs-2441 106 17 a a DET iajs-2441 106 18 five five NUM iajs-2441 106 19 replicates replicate NOUN iajs-2441 106 20 for for ADP iajs-2441 106 21 three three NUM iajs-2441 106 22 different different ADJ iajs-2441 106 23 cft cft NOUN iajs-2441 106 24 concentrations concentration NOUN iajs-2441 106 25 [ [ X iajs-2441 106 26 21 21 NUM iajs-2441 106 27 ] ] PUNCT iajs-2441 106 28 . . PUNCT iajs-2441 107 1 the the DET iajs-2441 107 2 precision precision NOUN iajs-2441 107 3 was be AUX iajs-2441 107 4 estimation estimation NOUN iajs-2441 107 5 by by ADP iajs-2441 107 6 the the DET iajs-2441 107 7 determine determine NOUN iajs-2441 107 8 of of ADP iajs-2441 107 9 percent percent NOUN iajs-2441 107 10 relative relative ADJ iajs-2441 107 11 error error NOUN iajs-2441 107 12 % % NOUN iajs-2441 107 13 r.e r.e PROPN iajs-2441 107 14 whereas whereas SCONJ iajs-2441 107 15 the the DET iajs-2441 107 16 accuracy accuracy NOUN iajs-2441 107 17 was be AUX iajs-2441 107 18 determination determination NOUN iajs-2441 107 19 by by ADP iajs-2441 107 20 calculating calculate VERB iajs-2441 107 21 the the DET iajs-2441 107 22 percent percent NOUN iajs-2441 107 23 relative relative ADJ iajs-2441 107 24 standard standard ADJ iajs-2441 107 25 deviation deviation NOUN iajs-2441 107 26 % % NOUN iajs-2441 107 27 rsd rsd NOUN iajs-2441 107 28 . . PUNCT iajs-2441 108 1 an an DET iajs-2441 108 2 reasonable reasonable ADJ iajs-2441 108 3 precision precision NOUN iajs-2441 108 4 with with ADP iajs-2441 108 5 acceptable acceptable ADJ iajs-2441 108 6 accuracy accuracy NOUN iajs-2441 108 7 was be AUX iajs-2441 108 8 obtained obtain VERB iajs-2441 108 9 which which PRON iajs-2441 108 10 illustrated illustrate VERB iajs-2441 108 11 a a DET iajs-2441 108 12 0.46 0.46 NUM iajs-2441 108 13 and and CCONJ iajs-2441 108 14 0.37 0.37 NUM iajs-2441 108 15 for for ADP iajs-2441 108 16 2,5 2,5 NUM iajs-2441 108 17 - - PUNCT iajs-2441 108 18 dmp dmp NOUN iajs-2441 108 19 and and CCONJ iajs-2441 108 20 4 4 NUM iajs-2441 108 21 - - PUNCT iajs-2441 108 22 tbp tbp NOUN iajs-2441 108 23 as as ADP iajs-2441 108 24 in in ADP iajs-2441 108 25 table table NOUN iajs-2441 108 26 2 2 NUM iajs-2441 108 27 . . PUNCT iajs-2441 108 28 table table NOUN iajs-2441 108 29 2 2 NUM iajs-2441 108 30 . . PUNCT iajs-2441 109 1 the the DET iajs-2441 109 2 accuracy accuracy NOUN iajs-2441 109 3 and and CCONJ iajs-2441 109 4 precision precision NOUN iajs-2441 109 5 of of ADP iajs-2441 109 6 the the DET iajs-2441 109 7 developed develop VERB iajs-2441 109 8 method method NOUN iajs-2441 109 9 with with ADP iajs-2441 109 10 2,5 2,5 NUM iajs-2441 109 11 - - PUNCT iajs-2441 109 12 dmp dmp NOUN iajs-2441 109 13 and and CCONJ iajs-2441 109 14 4 4 NUM iajs-2441 109 15 - - PUNCT iajs-2441 109 16 tbp tbp NOUN iajs-2441 109 17 reagents reagent NOUN iajs-2441 109 18 . . PUNCT iajs-2441 110 1 * * PUNCT iajs-2441 110 2 average average ADJ iajs-2441 110 3 for for ADP iajs-2441 110 4 5 5 NUM iajs-2441 110 5 determinations determination NOUN iajs-2441 110 6 . . PUNCT iajs-2441 111 1 * * PUNCT iajs-2441 111 2 * * PUNCT iajs-2441 111 3 average average ADJ iajs-2441 111 4 for for ADP iajs-2441 111 5 15 15 NUM iajs-2441 111 6 determinations determination NOUN iajs-2441 111 7 . . PUNCT iajs-2441 112 1 type type NOUN iajs-2441 112 2 of of ADP iajs-2441 112 3 reagent reagent ADJ iajs-2441 112 4     SPACE iajs-2441 112 5 conc conc NOUN iajs-2441 112 6 . . PUNCT iajs-2441 113 1 taken take VERB iajs-2441 113 2 , , PUNCT iajs-2441 113 3 µg µg NOUN iajs-2441 113 4 . . PUNCT iajs-2441 113 5 ml-1 ml-1 ADV iajs-2441 113 6     SPACE iajs-2441 113 7 conc conc NOUN iajs-2441 113 8 . . PUNCT iajs-2441 114 1 found find VERB iajs-2441 114 2 µg µg NOUN iajs-2441 114 3 . . PUNCT iajs-2441 115 1 ml-1 ml-1 ADV iajs-2441 115 2     SPACE iajs-2441 115 3 relative relative ADJ iajs-2441 115 4 error% error% PUNCT iajs-2441 115 5     SPACE iajs-2441 115 6 % % NOUN iajs-2441 115 7 rsd rsd PROPN iajs-2441 115 8 * * PROPN iajs-2441 115 9 recovery recovery NOUN iajs-2441 115 10 , , PUNCT iajs-2441 115 11 % % INTJ iajs-2441 115 12     SPACE iajs-2441 115 13 * * PUNCT iajs-2441 115 14 * * PUNCT iajs-2441 115 15 average average ADJ iajs-2441 115 16 recovery recovery NOUN iajs-2441 115 17     SPACE iajs-2441 115 18 2,5 2,5 NUM iajs-2441 115 19 - - PUNCT iajs-2441 115 20 dmp dmp NOUN iajs-2441 115 21     SPACE iajs-2441 115 22 1.0 1.0 NUM iajs-2441 115 23     SPACE iajs-2441 115 24 0.98 0.98 NUM iajs-2441 115 25 -2.0 -2.0 NOUN iajs-2441 115 26 0.46 0.46 NUM iajs-2441 115 27 98.0 98.0 NUM iajs-2441 115 28     SPACE iajs-2441 115 29 100.89 100.89 NUM iajs-2441 115 30 3.0 3.0 NUM iajs-2441 115 31 3.08 3.08 NUM iajs-2441 115 32 2.7 2.7 NUM iajs-2441 115 33 102.7 102.7 NUM iajs-2441 115 34 5.0 5.0 NUM iajs-2441 115 35     SPACE iajs-2441 115 36 5.1 5.1 NUM iajs-2441 115 37 2.0 2.0 NUM iajs-2441 115 38 102.0 102.0 NUM iajs-2441 115 39     SPACE iajs-2441 115 40 4 4 NUM iajs-2441 115 41 - - PUNCT iajs-2441 115 42 tbp tbp NOUN iajs-2441 115 43     SPACE iajs-2441 115 44 1.0 1.0 NUM iajs-2441 115 45     SPACE iajs-2441 115 46 1.09 1.09 NUM iajs-2441 115 47 9.0 9.0 NUM iajs-2441 115 48 0.37 0.37 NUM iajs-2441 115 49 109.0 109.0 NUM iajs-2441 115 50     SPACE iajs-2441 115 51 103.378 103.378 NUM iajs-2441 115 52 3.0 3.0 NUM iajs-2441 115 53 3.1 3.1 NUM iajs-2441 115 54 3.3 3.3 NUM iajs-2441 115 55 103.3 103.3 NUM iajs-2441 115 56 5.0 5.0 NUM iajs-2441 115 57     SPACE iajs-2441 115 58 4.89 4.89 NUM iajs-2441 115 59 -2.2 -2.2 NUM iajs-2441 115 60 97.8 97.8 NUM iajs-2441 115 61         SPACE iajs-2441 115 62 40 40 NUM iajs-2441 115 63 ibn ibn PROPN iajs-2441 115 64 al al PROPN iajs-2441 115 65 - - PUNCT iajs-2441 115 66 haitham haitham PROPN iajs-2441 115 67 jour jour X iajs-2441 115 68 . . PROPN iajs-2441 116 1 for for ADP iajs-2441 116 2 pure pure ADJ iajs-2441 116 3 & & CCONJ iajs-2441 116 4 appl appl PROPN iajs-2441 116 5 . . PUNCT iajs-2441 117 1 sci sci PROPN iajs-2441 117 2 . . PROPN iajs-2441 118 1 33 33 NUM iajs-2441 118 2 ( ( PUNCT iajs-2441 118 3 2 2 NUM iajs-2441 118 4 ) ) PUNCT iajs-2441 118 5 2020 2020 NUM iajs-2441 118 6 3 3 NUM iajs-2441 118 7 - - SYM iajs-2441 118 8 4 4 NUM iajs-2441 118 9 . . PUNCT iajs-2441 119 1 cft cft NOUN iajs-2441 119 2 : : PUNCT iajs-2441 119 3 reagent reagent ADJ iajs-2441 119 4 stoichiometry stoichiometry NOUN iajs-2441 119 5 a a DET iajs-2441 119 6 continuous continuous ADJ iajs-2441 119 7 variation variation NOUN iajs-2441 119 8 ( ( PUNCT iajs-2441 119 9 job job NOUN iajs-2441 119 10 ) ) PUNCT iajs-2441 119 11 method method NOUN iajs-2441 120 1 [ [ X iajs-2441 120 2 22 22 NUM iajs-2441 120 3 ] ] PUNCT iajs-2441 120 4 . . PUNCT iajs-2441 121 1 was be AUX iajs-2441 121 2 applied apply VERB iajs-2441 121 3 for for ADP iajs-2441 121 4 the the DET iajs-2441 121 5 estimation estimation NOUN iajs-2441 121 6 of of ADP iajs-2441 121 7 cft cft NOUN iajs-2441 121 8 : : PUNCT iajs-2441 121 9 reagent reagent ADJ iajs-2441 121 10 stoichiometry stoichiometry NOUN iajs-2441 121 11 . . PUNCT iajs-2441 122 1 the the DET iajs-2441 122 2 solutions solution NOUN iajs-2441 122 3 were be AUX iajs-2441 122 4 prepared prepare VERB iajs-2441 122 5 at at ADP iajs-2441 122 6 an an DET iajs-2441 122 7 equal equal ADJ iajs-2441 122 8 concentration concentration NOUN iajs-2441 122 9 of of ADP iajs-2441 122 10 2.0 2.0 NUM iajs-2441 122 11 × × NOUN iajs-2441 122 12 10 10 NUM iajs-2441 122 13 - - SYM iajs-2441 122 14 3 3 NUM iajs-2441 122 15 m m NOUN iajs-2441 122 16 for for ADP iajs-2441 122 17 cft cft NOUN iajs-2441 122 18 with with ADP iajs-2441 122 19 2.5dmp 2.5dmp NUM iajs-2441 122 20 and and CCONJ iajs-2441 122 21 2.5 2.5 NUM iajs-2441 122 22 × × NOUN iajs-2441 122 23 10 10 NUM iajs-2441 122 24 - - SYM iajs-2441 122 25 3 3 NUM iajs-2441 122 26 m m NOUN iajs-2441 122 27 for for ADP iajs-2441 122 28 cft cft NOUN iajs-2441 122 29 and and CCONJ iajs-2441 122 30 4 4 NUM iajs-2441 122 31 - - PUNCT iajs-2441 122 32 tbp tbp NOUN iajs-2441 122 33 . . PUNCT iajs-2441 123 1 this this DET iajs-2441 123 2 method method NOUN iajs-2441 123 3 was be AUX iajs-2441 123 4 applied apply VERB iajs-2441 123 5 by by ADP iajs-2441 123 6 increasing increase VERB iajs-2441 123 7 the the DET iajs-2441 123 8 volumes volume NOUN iajs-2441 123 9 from from ADP iajs-2441 123 10 0.1 0.1 NUM iajs-2441 123 11 to to PART iajs-2441 123 12 0.9 0.9 NUM iajs-2441 123 13 ml ml NOUN iajs-2441 123 14 of of ADP iajs-2441 123 15 cft cft NOUN iajs-2441 123 16 and and CCONJ iajs-2441 123 17 reducing reduce VERB iajs-2441 123 18 the the DET iajs-2441 123 19 volumes volume NOUN iajs-2441 123 20 from from ADP iajs-2441 123 21 0.9 0.9 NUM iajs-2441 123 22 to to ADP iajs-2441 123 23 0.1 0.1 NUM iajs-2441 123 24 ml ml NOUN iajs-2441 123 25 of of ADP iajs-2441 123 26 reagents reagent NOUN iajs-2441 123 27 to to ADP iajs-2441 123 28 a a DET iajs-2441 123 29 final final ADJ iajs-2441 123 30 volume volume NOUN iajs-2441 123 31 of of ADP iajs-2441 123 32 1.0 1.0 NUM iajs-2441 123 33 ml ml NOUN iajs-2441 123 34 . . PUNCT iajs-2441 124 1 the the DET iajs-2441 124 2 results result NOUN iajs-2441 124 3 showed show VERB iajs-2441 124 4 a a DET iajs-2441 124 5 conjugated conjugated ADJ iajs-2441 124 6 ratio ratio NOUN iajs-2441 124 7 is be AUX iajs-2441 124 8 of of ADP iajs-2441 124 9 1:1 1:1 NUM iajs-2441 124 10 between between ADP iajs-2441 124 11 cft cft NOUN iajs-2441 124 12 with with ADP iajs-2441 124 13 two two NUM iajs-2441 124 14 reagents reagent NOUN iajs-2441 124 15 , , PUNCT iajs-2441 124 16 figure figure NOUN iajs-2441 124 17 9 9 NUM iajs-2441 124 18 , , PUNCT iajs-2441 124 19 10 10 NUM iajs-2441 124 20 . . PUNCT iajs-2441 124 21     SPACE iajs-2441 124 22 figure figure NOUN iajs-2441 124 23 9 9 NUM iajs-2441 124 24 . . PUNCT iajs-2441 124 25 continuous continuous ADJ iajs-2441 124 26 variation variation NOUN iajs-2441 124 27 method method NOUN iajs-2441 124 28 for for ADP iajs-2441 124 29 cft cft NOUN iajs-2441 124 30 : : PUNCT iajs-2441 124 31 reagent reagent ADJ iajs-2441 124 32 stoichometry stoichometry NOUN iajs-2441 124 33 with with ADP iajs-2441 124 34 2,5 2,5 NUM iajs-2441 124 35 - - PUNCT iajs-2441 124 36 dmp dmp NOUN iajs-2441 124 37 at at ADP iajs-2441 124 38 520 520 NUM iajs-2441 124 39 nm nm NOUN iajs-2441 124 40 and and CCONJ iajs-2441 124 41 with with ADP iajs-2441 124 42 4 4 NUM iajs-2441 124 43 - - PUNCT iajs-2441 124 44 tbp tbp NOUN iajs-2441 124 45 at at ADP iajs-2441 124 46 500 500 NUM iajs-2441 124 47 nm nm NOUN iajs-2441 124 48 . . PUNCT iajs-2441 124 49       SPACE iajs-2441 125 1 3 3 NUM iajs-2441 125 2 - - SYM iajs-2441 125 3 5 5 NUM iajs-2441 125 4 . . PUNCT iajs-2441 125 5 application application NOUN iajs-2441 125 6 of of ADP iajs-2441 125 7 the the DET iajs-2441 125 8 developed develop VERB iajs-2441 125 9 method method NOUN iajs-2441 125 10 for for ADP iajs-2441 125 11 the the DET iajs-2441 125 12 cft cft PROPN iajs-2441 125 13 estimation estimation NOUN iajs-2441 125 14 in in ADP iajs-2441 125 15 pharmaceuticals pharmaceutical NOUN iajs-2441 125 16 this this DET iajs-2441 125 17 developed develop VERB iajs-2441 125 18 method method NOUN iajs-2441 125 19 was be AUX iajs-2441 125 20 successfully successfully ADV iajs-2441 125 21 used use VERB iajs-2441 125 22 for for ADP iajs-2441 125 23 the the DET iajs-2441 125 24 cft cft PROPN iajs-2441 125 25 determine determine NOUN iajs-2441 125 26 in in ADP iajs-2441 125 27 commercial commercial ADJ iajs-2441 125 28 pharmaceuticals pharmaceutical NOUN iajs-2441 125 29 for for ADP iajs-2441 125 30 diverse diverse ADJ iajs-2441 125 31 products product NOUN iajs-2441 125 32 from from ADP iajs-2441 125 33 malaysia malaysia PROPN iajs-2441 125 34 , , PUNCT iajs-2441 125 35 jordan jordan PROPN iajs-2441 125 36 and and CCONJ iajs-2441 125 37 united united PROPN iajs-2441 125 38 arab arab PROPN iajs-2441 125 39 of of ADP iajs-2441 125 40 emirate emirate NOUN iajs-2441 125 41 at at ADP iajs-2441 125 42 a a DET iajs-2441 125 43 concentration concentration NOUN iajs-2441 125 44 of of ADP iajs-2441 125 45 6.0 6.0 NUM iajs-2441 125 46 and and CCONJ iajs-2441 125 47 10 10 NUM iajs-2441 125 48 µg µg NOUN iajs-2441 125 49 . . PUNCT iajs-2441 126 1 ml-1 ml-1 PROPN iajs-2441 126 2 . . PUNCT iajs-2441 127 1 the the DET iajs-2441 127 2 results result NOUN iajs-2441 127 3 were be AUX iajs-2441 127 4 summarized summarize VERB iajs-2441 127 5 in in ADP iajs-2441 127 6 tables table NOUN iajs-2441 127 7 3 3 NUM iajs-2441 127 8 , , PUNCT iajs-2441 127 9 4 4 NUM iajs-2441 127 10 . . NOUN iajs-2441 127 11 table table NOUN iajs-2441 127 12 3 3 NUM iajs-2441 127 13 . . X iajs-2441 128 1 assay assay PROPN iajs-2441 128 2 of of ADP iajs-2441 128 3 cft cft NOUN iajs-2441 128 4 in in ADP iajs-2441 128 5 pharmaceutical pharmaceutical ADJ iajs-2441 128 6 preparations preparation NOUN iajs-2441 128 7 using use VERB iajs-2441 128 8 2,5 2,5 NUM iajs-2441 128 9 - - PUNCT iajs-2441 128 10 dmp dmp NOUN iajs-2441 128 11 reagent reagent NOUN iajs-2441 128 12 . . PUNCT iajs-2441 129 1 pharmaceuticals pharmaceutical NOUN iajs-2441 129 2 of of ADP iajs-2441 129 3 cft cft PROPN iajs-2441 129 4 conc.taken conc.taken PROPN iajs-2441 129 5 µg µg NOUN iajs-2441 129 6 . . PUNCT iajs-2441 129 7 ml-1 ml-1 PROPN iajs-2441 130 1 conc.found conc.found PROPN iajs-2441 130 2 µg µg NOUN iajs-2441 130 3 . . 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PROPN iajs-2441 195 5 2014 2014 NUM iajs-2441 195 6 , , PUNCT iajs-2441 195 7 961 961 NUM iajs-2441 195 8 , , PUNCT iajs-2441 195 9 97 97 NUM iajs-2441 195 10 - - SYM iajs-2441 195 11 102 102 NUM iajs-2441 195 12 . . PUNCT iajs-2441 195 13 18 18 NUM iajs-2441 195 14 . . X iajs-2441 196 1 shah shah PROPN iajs-2441 196 2 , , PUNCT iajs-2441 196 3 j. j. PROPN iajs-2441 196 4 ; ; PUNCT iajs-2441 196 5 rasul rasul PROPN iajs-2441 196 6 jan jan PROPN iajs-2441 196 7 , , PUNCT iajs-2441 196 8 m. m. NOUN iajs-2441 196 9 ; ; PUNCT iajs-2441 196 10 shah shah PROPN iajs-2441 196 11 , , PUNCT iajs-2441 196 12 s. s. PROPN iajs-2441 196 13 ; ; PUNCT iajs-2441 196 14 naeem naeem PROPN iajs-2441 196 15 khan khan PROPN iajs-2441 196 16 , , PUNCT iajs-2441 196 17 m.j.j.o.t.m.c.s m.j.j.o.t.m.c.s PROPN iajs-2441 196 18 . . PUNCT iajs-2441 196 19 development development NOUN iajs-2441 196 20 and and CCONJ iajs-2441 196 21 validation validation NOUN iajs-2441 196 22 of of ADP iajs-2441 196 23 hplc hplc NOUN iajs-2441 196 24 method method NOUN iajs-2441 196 25 for for ADP iajs-2441 196 26 simultaneous simultaneous ADJ iajs-2441 196 27 determination determination NOUN iajs-2441 196 28 of of ADP iajs-2441 196 29 ceftriaxone ceftriaxone NOUN iajs-2441 196 30 and and CCONJ iajs-2441 196 31 cefaclor cefaclor NOUN iajs-2441 196 32 in in ADP iajs-2441 196 33 commercial commercial ADJ iajs-2441 196 34 formulations formulation NOUN iajs-2441 196 35 and and CCONJ iajs-2441 196 36 biological biological ADJ iajs-2441 196 37 samples sample NOUN iajs-2441 196 38 . . PUNCT iajs-2441 197 1 journal journal NOUN iajs-2441 197 2 of of ADP iajs-2441 197 3 the the DET iajs-2441 197 4 mexican mexican PROPN iajs-2441 197 5 chemical chemical PROPN iajs-2441 197 6 society society NOUN iajs-2441 197 7 . . PUNCT iajs-2441 198 1 2013 2013 NUM iajs-2441 198 2 , , PUNCT iajs-2441 198 3 57 57 NUM iajs-2441 198 4 , , PUNCT iajs-2441 198 5 4 4 NUM iajs-2441 198 6 , , PUNCT iajs-2441 198 7 314 314 NUM iajs-2441 198 8 - - SYM iajs-2441 198 9 320 320 NUM iajs-2441 198 10 . . PUNCT iajs-2441 199 1 19 19 NUM iajs-2441 199 2 . . X iajs-2441 199 3 sun sun PROPN iajs-2441 199 4 , , PUNCT iajs-2441 199 5 h. h. PROPN iajs-2441 199 6 ; ; PUNCT iajs-2441 199 7 wang wang PROPN iajs-2441 199 8 , , PUNCT iajs-2441 199 9 h. h. PROPN iajs-2441 199 10 ; ; PUNCT iajs-2441 199 11 ge ge PROPN iajs-2441 199 12 , , PUNCT iajs-2441 199 13 x.j.j.o.c x.j.j.o.c PROPN iajs-2441 199 14 . . PUNCT iajs-2441 200 1 l.a l.a PROPN iajs-2441 200 2 . . PUNCT iajs-2441 200 3 simultaneous simultaneous ADJ iajs-2441 200 4 determination determination NOUN iajs-2441 200 5 of of ADP iajs-2441 200 6 the the DET iajs-2441 200 7 combined combine VERB iajs-2441 200 8 drugs drug NOUN iajs-2441 200 9 of of ADP iajs-2441 200 10 ceftriaxone ceftriaxone PROPN iajs-2441 200 11 sodium sodium NOUN iajs-2441 200 12 , , PUNCT iajs-2441 200 13 metronidazole metronidazole NOUN iajs-2441 200 14 , , PUNCT iajs-2441 200 15 and and CCONJ iajs-2441 200 16 levofloxacin levofloxacin NOUN iajs-2441 200 17 in in ADP iajs-2441 200 18 human human ADJ iajs-2441 200 19 urine urine NOUN iajs-2441 200 20 by by ADP iajs-2441 200 21 high high ADJ iajs-2441 200 22 - - PUNCT iajs-2441 200 23 performance performance NOUN iajs-2441 200 24 liquid liquid ADJ iajs-2441 200 25 chromatography chromatography NOUN iajs-2441 200 26 . . PUNCT iajs-2441 201 1 journal journal NOUN iajs-2441 201 2 of of ADP iajs-2441 201 3 clinical clinical ADJ iajs-2441 201 4 laboratory laboratory NOUN iajs-2441 201 5 analysis analysis NOUN iajs-2441 201 6 . . PUNCT iajs-2441 202 1 2012 2012 NUM iajs-2441 202 2 , , PUNCT iajs-2441 202 3 26 26 NUM iajs-2441 202 4 , , PUNCT iajs-2441 202 5 6 6 NUM iajs-2441 202 6 , , PUNCT iajs-2441 202 7 486 486 NUM iajs-2441 202 8 - - SYM iajs-2441 202 9 492 492 NUM iajs-2441 202 10 . . NOUN iajs-2441 203 1 20 20 NUM iajs-2441 203 2 . . X iajs-2441 203 3 briscoe briscoe PROPN iajs-2441 203 4 , , PUNCT iajs-2441 203 5 s.e s.e PROPN iajs-2441 203 6 . . PROPN iajs-2441 203 7 ; ; PUNCT iajs-2441 203 8 mcwhinney mcwhinney PROPN iajs-2441 203 9 , , PUNCT iajs-2441 203 10 b.c b.c PROPN iajs-2441 203 11 . . PROPN iajs-2441 203 12 ; ; PUNCT iajs-2441 203 13 lipman lipman PROPN iajs-2441 203 14 , , PUNCT iajs-2441 203 15 j. j. PROPN iajs-2441 203 16 ; ; PUNCT iajs-2441 203 17 roberts roberts PROPN iajs-2441 203 18 , , PUNCT iajs-2441 203 19 j.a j.a PROPN iajs-2441 203 20 . . PROPN iajs-2441 203 21 ; ; PUNCT iajs-2441 203 22 ungerer ungerer PROPN iajs-2441 203 23 , , PUNCT iajs-2441 203 24 j.p.j.j.o.c.b j.p.j.j.o.c.b PROPN iajs-2441 203 25 . . PUNCT iajs-2441 204 1 a a DET iajs-2441 204 2 method method NOUN iajs-2441 204 3 for for ADP iajs-2441 204 4 determining determine VERB iajs-2441 204 5 the the DET iajs-2441 204 6 free free ADJ iajs-2441 204 7 ( ( PUNCT iajs-2441 204 8 unbound unbound ADJ iajs-2441 204 9 ) ) PUNCT iajs-2441 204 10 concentration concentration NOUN iajs-2441 204 11 of of ADP iajs-2441 204 12 ten ten NUM iajs-2441 204 13 beta beta NOUN iajs-2441 204 14 - - PUNCT iajs-2441 204 15 lactam lactam NOUN iajs-2441 204 16 antibiotics antibiotic NOUN iajs-2441 204 17 in in ADP iajs-2441 204 18 human human ADJ iajs-2441 204 19 plasma plasma NOUN iajs-2441 204 20 using use VERB iajs-2441 204 21 high high ADJ iajs-2441 204 22 performance performance NOUN iajs-2441 204 23 liquid liquid NOUN iajs-2441 204 24 chromatography chromatography NOUN iajs-2441 204 25 with with ADP iajs-2441 204 26 ultraviolet ultraviolet ADJ iajs-2441 204 27 detection detection NOUN iajs-2441 204 28 . . PUNCT iajs-2441 205 1 journal journal PROPN iajs-2441 205 2 of of ADP iajs-2441 205 3 chromatography chromatography PROPN iajs-2441 205 4 b. b. PROPN iajs-2441 205 5 2012 2012 NUM iajs-2441 205 6 , , PUNCT iajs-2441 205 7 907 907 NUM iajs-2441 205 8 , , PUNCT iajs-2441 205 9 178 178 NUM iajs-2441 205 10 - - SYM iajs-2441 205 11 184 184 NUM iajs-2441 205 12 . . PUNCT iajs-2441 205 13 21 21 NUM iajs-2441 205 14 . . PUNCT iajs-2441 206 1 james james PROPN iajs-2441 206 2 n.m n.m PROPN iajs-2441 206 3 . . PROPN iajs-2441 206 4 ; ; PUNCT iajs-2441 206 5 jane jane PROPN iajs-2441 206 6 , , PUNCT iajs-2441 206 7 c.m c.m PROPN iajs-2441 206 8 . . PROPN iajs-2441 206 9 statistics statistic NOUN iajs-2441 206 10 and and CCONJ iajs-2441 206 11 chemometrics chemometric NOUN iajs-2441 206 12 for for ADP iajs-2441 206 13 analytical analytical ADJ iajs-2441 206 14 chemistry chemistry NOUN iajs-2441 206 15 , , PUNCT iajs-2441 206 16 p. p. PROPN iajs-2441 206 17 e. e. PROPN iajs-2441 206 18 l. l. PROPN iajs-2441 206 19 , , PUNCT iajs-2441 206 20 prentice prentice NOUN iajs-2441 206 21 hall hall NOUN iajs-2441 206 22 , , PUNCT iajs-2441 206 23 5th 5th ADJ iajs-2441 206 24 ed ed NOUN iajs-2441 206 25 . . PUNCT iajs-2441 206 26 2005 2005 NUM iajs-2441 206 27 . . PUNCT iajs-2441 207 1 22 22 NUM iajs-2441 207 2 . . PUNCT iajs-2441 208 1 renny renny PROPN iajs-2441 208 2 , , PUNCT iajs-2441 208 3 j.s j.s PROPN iajs-2441 208 4 . . PROPN iajs-2441 208 5 ; ; PUNCT iajs-2441 208 6 tomasevich tomasevich PROPN iajs-2441 208 7 , , PUNCT iajs-2441 208 8 l.l l.l PROPN iajs-2441 208 9 . . PROPN iajs-2441 208 10 ; ; PUNCT iajs-2441 208 11 tallmadge tallmadge PROPN iajs-2441 208 12 , , PUNCT iajs-2441 208 13 e.h e.h PROPN iajs-2441 208 14 . . PROPN iajs-2441 208 15 ; ; PUNCT iajs-2441 208 16 collum collum PROPN iajs-2441 208 17 , , PUNCT iajs-2441 208 18 d.b.j.a.c.i.e d.b.j.a.c.i.e NOUN iajs-2441 208 19 . . PUNCT iajs-2441 208 20 method method NOUN iajs-2441 208 21 of of ADP iajs-2441 208 22 continuous continuous ADJ iajs-2441 208 23 variations variation NOUN iajs-2441 208 24 : : PUNCT iajs-2441 208 25 applications application NOUN iajs-2441 208 26 of of ADP iajs-2441 208 27 job job NOUN iajs-2441 208 28 plots plot NOUN iajs-2441 208 29 to to ADP iajs-2441 208 30 the the DET iajs-2441 208 31 study study NOUN iajs-2441 208 32 of of ADP iajs-2441 208 33 molecular molecular ADJ iajs-2441 208 34 associations association NOUN iajs-2441 208 35 in in ADP iajs-2441 208 36 organometallic organometallic ADJ iajs-2441 208 37 chemistry chemistry NOUN iajs-2441 208 38 . . 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