id sid tid token lemma pos iajs-308 1 1 microsoft microsoft PROPN iajs-308 1 2 word word NOUN iajs-308 1 3 10 10 NUM iajs-308 1 4 435 435 NUM iajs-308 1 5 | | ADV iajs-308 1 6 chemistry chemistry NOUN iajs-308 1 7 2014 2014 NUM iajs-308 1 8 ) ) PUNCT iajs-308 1 9 عام عام ADP iajs-308 1 10 3العدد 3العدد NUM iajs-308 1 11 ( ( PUNCT iajs-308 1 12 27مجلة 27مجلة NUM iajs-308 1 13 إبن إبن VERB iajs-308 1 14 الھيثم الھيثم NOUN iajs-308 1 15 للعلوم للعلوم NOUN iajs-308 1 16 الصرفة الصرفة NOUN iajs-308 2 1 و و PRON iajs-308 2 2 التطبيقية التطبيقية ADV iajs-308 2 3 المجلد المجلد VERB iajs-308 2 4 ibn ibn PROPN iajs-308 2 5 al al PROPN iajs-308 2 6 - - PUNCT iajs-308 2 7 haitham haitham PROPN iajs-308 2 8 jour jour X iajs-308 2 9 . . PROPN iajs-308 3 1 for for ADP iajs-308 3 2 pure pure ADJ iajs-308 3 3 & & CCONJ iajs-308 3 4 appl appl PROPN iajs-308 3 5 . . PUNCT iajs-308 4 1 sci sci PROPN iajs-308 4 2 . . PUNCT iajs-308 4 3 vol vol NOUN iajs-308 4 4 . . PROPN iajs-308 5 1 27 27 NUM iajs-308 5 2 ( ( PUNCT iajs-308 5 3 3 3 NUM iajs-308 5 4 ) ) PUNCT iajs-308 5 5 2014 2014 NUM iajs-308 5 6 synthesis synthesis NOUN iajs-308 5 7 and and CCONJ iajs-308 5 8 characterization characterization NOUN iajs-308 5 9 new new ADJ iajs-308 5 10 schiff schiff NOUN iajs-308 5 11 bases basis NOUN iajs-308 5 12 , , PUNCT iajs-308 5 13 pyrazole pyrazole NOUN iajs-308 5 14 and and CCONJ iajs-308 5 15 pyrazoline pyrazoline NOUN iajs-308 5 16 compounds compound NOUN iajs-308 5 17 derived derive VERB iajs-308 5 18 from from ADP iajs-308 5 19 acid acid PROPN iajs-308 5 20 hydrazide hydrazide ADV iajs-308 5 21 containing contain VERB iajs-308 5 22 isoxazoline isoxazoline NOUN iajs-308 5 23 ring ring NOUN iajs-308 5 24 nebras nebras PROPN iajs-308 5 25 m.jamel m.jamel NOUN iajs-308 5 26 dhuha dhuha PROPN iajs-308 5 27 f. f. PROPN iajs-308 5 28 hussein hussein PROPN iajs-308 6 1 jumbad jumbad PROPN iajs-308 6 2 h.tomma h.tomma PROPN iajs-308 7 1 dept.of dept.of PROPN iajs-308 7 2 chemistry chemistry NOUN iajs-308 7 3 / / SYM iajs-308 7 4 college college NOUN iajs-308 7 5 of of ADP iajs-308 7 6 education education NOUN iajs-308 7 7 for for ADP iajs-308 7 8 pure pure ADJ iajs-308 7 9 science science NOUN iajs-308 7 10 ( ( PUNCT iajs-308 7 11 ibn ibn NOUN iajs-308 7 12 al al PROPN iajs-308 7 13 haitham)/university haitham)/university NOUN iajs-308 7 14 of of ADP iajs-308 7 15 baghdad baghdad PROPN iajs-308 7 16 received receive VERB iajs-308 7 17 in in ADP iajs-308 7 18 : : SYM iajs-308 7 19 15 15 NUM iajs-308 7 20 june2014,accepted june2014,accepte VERB iajs-308 7 21 in in ADP iajs-308 7 22 : : PUNCT iajs-308 7 23 29 29 NUM iajs-308 7 24 september september PROPN iajs-308 7 25 2014 2014 NUM iajs-308 7 26 abstract abstract NOUN iajs-308 7 27 the the DET iajs-308 7 28 work work NOUN iajs-308 7 29 involves involve VERB iajs-308 7 30 synthesis synthesis NOUN iajs-308 7 31 of of ADP iajs-308 7 32 new new ADJ iajs-308 7 33 schiff schiff NOUN iajs-308 7 34 bases basis NOUN iajs-308 7 35 ( ( PUNCT iajs-308 7 36 [ [ X iajs-308 7 37 v]a v]a NOUN iajs-308 7 38 , , PUNCT iajs-308 7 39 b b PROPN iajs-308 7 40 and and CCONJ iajs-308 7 41 [ [ X iajs-308 7 42 vi]a vi]a PROPN iajs-308 7 43 , , PUNCT iajs-308 7 44 b b NOUN iajs-308 7 45 ) ) PUNCT iajs-308 7 46 , , PUNCT iajs-308 7 47 pyrazoles[vii]a pyrazoles[vii]a NOUN iajs-308 7 48 , , PUNCT iajs-308 7 49 b b NOUN iajs-308 7 50 and and CCONJ iajs-308 7 51 pyrazolines[viii]a pyrazolines[viii]a PROPN iajs-308 7 52 , , PUNCT iajs-308 7 53 b b NOUN iajs-308 7 54 derivatives derivative NOUN iajs-308 7 55 containing contain VERB iajs-308 7 56 isoxazoline isoxazoline NOUN iajs-308 7 57 unit unit NOUN iajs-308 7 58 starting start VERB iajs-308 7 59 with with ADP iajs-308 7 60 chalcones chalcone NOUN iajs-308 7 61 . . PUNCT iajs-308 8 1 4bromoacetophenone 4bromoacetophenone NUM iajs-308 8 2 was be AUX iajs-308 8 3 reacted react VERB iajs-308 8 4 with with ADP iajs-308 8 5 4 4 NUM iajs-308 8 6 - - PUNCT iajs-308 8 7 hydroxybenzaldehyde hydroxybenzaldehyde NOUN iajs-308 8 8 or or CCONJ iajs-308 8 9 4 4 NUM iajs-308 8 10 - - PUNCT iajs-308 8 11 hydroxyacetophenone hydroxyacetophenone NOUN iajs-308 8 12 was be AUX iajs-308 8 13 reacted react VERB iajs-308 8 14 with with ADP iajs-308 8 15 4 4 NUM iajs-308 8 16 - - PUNCT iajs-308 8 17 bromobenzaldehyde bromobenzaldehyde NOUN iajs-308 8 18 in in ADP iajs-308 8 19 basic basic ADJ iajs-308 8 20 medium medium NOUN iajs-308 8 21 to to PART iajs-308 8 22 give give VERB iajs-308 8 23 chalcone chalcone NOUN iajs-308 8 24 by by ADP iajs-308 8 25 claisen claisen PROPN iajs-308 8 26 - - PUNCT iajs-308 8 27 schemidt schemidt ADJ iajs-308 8 28 reaction reaction NOUN iajs-308 8 29 . . PUNCT iajs-308 9 1 the the DET iajs-308 9 2 chalcons chalcon NOUN iajs-308 9 3 [ [ X iajs-308 9 4 i]a i]a NOUN iajs-308 9 5 , , PUNCT iajs-308 9 6 b b PROPN iajs-308 9 7 was be AUX iajs-308 9 8 reacted react VERB iajs-308 9 9 with with ADP iajs-308 9 10 hydroxylamine hydroxylamine ADJ iajs-308 9 11 hydrochloride hydrochloride NOUN iajs-308 9 12 to to PART iajs-308 9 13 form form VERB iajs-308 9 14 isoxazolines isoxazoline NOUN iajs-308 10 1 [ [ X iajs-308 10 2 ii]a ii]a PROPN iajs-308 10 3 , , PUNCT iajs-308 10 4 b. b. PROPN iajs-308 10 5 which which PRON iajs-308 10 6 were be AUX iajs-308 10 7 reacted react VERB iajs-308 10 8 with with ADP iajs-308 10 9 ethyl ethyl PROPN iajs-308 10 10 chloro chloro NOUN iajs-308 10 11 acetate acetate NOUN iajs-308 10 12 in in ADP iajs-308 10 13 basic basic ADJ iajs-308 10 14 medium medium NOUN iajs-308 10 15 to to PART iajs-308 10 16 get get VERB iajs-308 10 17 ester ester NOUN iajs-308 10 18 compounds[iii]a compounds[iii]a NOUN iajs-308 10 19 , , PUNCT iajs-308 10 20 b b X iajs-308 10 21 .the .the DET iajs-308 10 22 condensation condensation NOUN iajs-308 10 23 new new ADJ iajs-308 10 24 ester[iii]a ester[iii]a PROPN iajs-308 10 25 , , PUNCT iajs-308 10 26 b b PROPN iajs-308 10 27 with with ADP iajs-308 10 28 hydrazine hydrazine NOUN iajs-308 10 29 hydrate80 hydrate80 NOUN iajs-308 10 30 % % NOUN iajs-308 10 31 yieldedacid yieldedacid ADJ iajs-308 10 32 hydrazide hydrazide ADV iajs-308 11 1 [ [ X iajs-308 11 2 iv]a iv]a PROPN iajs-308 11 3 , , PUNCT iajs-308 11 4 b.the b.the DET iajs-308 11 5 later later ADV iajs-308 11 6 compound compound NOUN iajs-308 11 7 refluxing refluxing NOUN iajs-308 11 8 with with ADP iajs-308 11 9 4 4 NUM iajs-308 11 10 - - PUNCT iajs-308 11 11 substituted substitute VERB iajs-308 11 12 benzaldehyde benzaldehyde NOUN iajs-308 11 13 in in ADP iajs-308 11 14 dry dry ADJ iajs-308 11 15 benzene benzene NOUN iajs-308 11 16 to to PART iajs-308 11 17 give give VERB iajs-308 11 18 schiff schiff PROPN iajs-308 11 19 bases([v]a bases([v]a PROPN iajs-308 11 20 , , PUNCT iajs-308 11 21 band band NOUN iajs-308 12 1 [ [ X iajs-308 12 2 vi]a vi]a NOUN iajs-308 12 3 , , PUNCT iajs-308 12 4 b)while b)while VERB iajs-308 12 5 the the DET iajs-308 12 6 reaction reaction NOUN iajs-308 12 7 of of ADP iajs-308 12 8 acid acid ADJ iajs-308 12 9 hydrazide hydrazide NOUN iajs-308 13 1 [ [ X iajs-308 13 2 iv]a iv]a PROPN iajs-308 13 3 , , PUNCT iajs-308 13 4 b b NOUN iajs-308 13 5 with with ADP iajs-308 13 6 acetylacetone acetylacetone NOUN iajs-308 13 7 or or CCONJ iajs-308 13 8 ethyl ethyl PROPN iajs-308 13 9 aceto aceto PROPN iajs-308 13 10 acetate acetate PROPN iajs-308 13 11 to to PART iajs-308 13 12 get get VERB iajs-308 13 13 pyrazole[vii]a pyrazole[vii]a NOUN iajs-308 13 14 , , PUNCT iajs-308 13 15 b b NOUN iajs-308 13 16 , , PUNCT iajs-308 13 17 pyrazolone[viii]a pyrazolone[viii]a PROPN iajs-308 13 18 , , PUNCT iajs-308 13 19 b b PROPN iajs-308 13 20 , , PUNCT iajs-308 13 21 respectively.the respectively.the DET iajs-308 13 22 synthesized synthesize VERB iajs-308 13 23 compounds compound NOUN iajs-308 13 24 were be AUX iajs-308 13 25 characterized characterize VERB iajs-308 13 26 by by ADP iajs-308 13 27 melting melt VERB iajs-308 13 28 points point NOUN iajs-308 13 29 , , PUNCT iajs-308 13 30 ftir ftir PROPN iajs-308 13 31 , , PUNCT iajs-308 13 32 mass mass PROPN iajs-308 13 33 and and CCONJ iajs-308 13 34 1h 1h NUM iajs-308 13 35 nmr nmr NOUN iajs-308 13 36 spectroscopy(of spectroscopy(of NOUN iajs-308 13 37 someof someof VERB iajs-308 13 38 them they PRON iajs-308 13 39 ) ) PUNCT iajs-308 13 40 . . PUNCT iajs-308 14 1 key key ADJ iajs-308 14 2 words word NOUN iajs-308 14 3 : : PUNCT iajs-308 14 4 chalcones chalcone NOUN iajs-308 14 5 , , PUNCT iajs-308 14 6 schiff schiff NOUN iajs-308 14 7 bases basis NOUN iajs-308 14 8 , , PUNCT iajs-308 14 9 isoxazoline isoxazoline NOUN iajs-308 14 10 , , PUNCT iajs-308 14 11 pyrazole pyrazole NOUN iajs-308 14 12 , , PUNCT iajs-308 14 13 pyrazoline pyrazoline NOUN iajs-308 14 14 . . PUNCT iajs-308 15 1 436 436 NUM iajs-308 16 1 | | ADV iajs-308 16 2 chemistry chemistry NOUN iajs-308 16 3 2014 2014 NUM iajs-308 16 4 ) ) PUNCT iajs-308 16 5 عام عام ADP iajs-308 16 6 3العدد 3العدد NUM iajs-308 16 7 ( ( PUNCT iajs-308 16 8 27مجلة 27مجلة NUM iajs-308 16 9 إبن إبن VERB iajs-308 16 10 الھيثم الھيثم NOUN iajs-308 16 11 للعلوم للعلوم NOUN iajs-308 16 12 الصرفة الصرفة NOUN iajs-308 17 1 و و PRON iajs-308 17 2 التطبيقية التطبيقية ADV iajs-308 17 3 المجلد المجلد VERB iajs-308 17 4 ibn ibn PROPN iajs-308 17 5 al al PROPN iajs-308 17 6 - - PUNCT iajs-308 17 7 haitham haitham PROPN iajs-308 17 8 jour jour X iajs-308 17 9 . . PROPN iajs-308 18 1 for for ADP iajs-308 18 2 pure pure ADJ iajs-308 18 3 & & CCONJ iajs-308 18 4 appl appl PROPN iajs-308 18 5 . . PUNCT iajs-308 19 1 sci sci PROPN iajs-308 19 2 . . PUNCT iajs-308 19 3 vol vol NOUN iajs-308 19 4 . . PROPN iajs-308 20 1 27 27 NUM iajs-308 20 2 ( ( PUNCT iajs-308 20 3 3 3 NUM iajs-308 20 4 ) ) PUNCT iajs-308 20 5 2014 2014 NUM iajs-308 20 6 introduction introduction NOUN iajs-308 20 7 chalcones chalcone NOUN iajs-308 20 8 were be AUX iajs-308 20 9 prepared prepare VERB iajs-308 20 10 by by ADP iajs-308 20 11 condensation condensation NOUN iajs-308 20 12 of of ADP iajs-308 20 13 acetophenone acetophenone NOUN iajs-308 20 14 with with ADP iajs-308 20 15 aromatic aromatic ADJ iajs-308 20 16 aldehydes aldehyde NOUN iajs-308 20 17 in in ADP iajs-308 20 18 presence presence NOUN iajs-308 20 19 of of ADP iajs-308 20 20 basic basic ADJ iajs-308 20 21 medium medium NOUN iajs-308 20 22 [ [ X iajs-308 20 23 1 1 NUM iajs-308 20 24 ] ] PUNCT iajs-308 20 25 . . PUNCT iajs-308 21 1 the the DET iajs-308 21 2 chalcone chalcone NOUN iajs-308 21 3 derivatives derivative NOUN iajs-308 21 4 are be AUX iajs-308 21 5 important important ADJ iajs-308 21 6 intermediate intermediate ADJ iajs-308 21 7 and and CCONJ iajs-308 21 8 also also ADV iajs-308 21 9 act act VERB iajs-308 21 10 as as ADP iajs-308 21 11 precursor precursor NOUN iajs-308 21 12 for for ADP iajs-308 21 13 the the DET iajs-308 21 14 synthesis synthesis NOUN iajs-308 21 15 of of ADP iajs-308 21 16 novel novel ADJ iajs-308 21 17 cyanopyridines cyanopyridine NOUN iajs-308 21 18 , , PUNCT iajs-308 21 19 pyrazolines pyrazoline NOUN iajs-308 21 20 , , PUNCT iajs-308 21 21 isoxazoles isoxazole NOUN iajs-308 21 22 , , PUNCT iajs-308 21 23 pyrimidines pyrimidine NOUN iajs-308 21 24 and and CCONJ iajs-308 21 25 tetrazole tetrazole NOUN iajs-308 21 26 [ [ X iajs-308 21 27 2 2 NUM iajs-308 21 28 ] ] PUNCT iajs-308 21 29 . . PUNCT iajs-308 22 1 five five NUM iajs-308 22 2 - - PUNCT iajs-308 22 3 member member NOUN iajs-308 22 4 heterocyclic heterocyclic NOUN iajs-308 22 5 compounds compound VERB iajs-308 22 6 isoxazoline isoxazoline NOUN iajs-308 22 7 are be AUX iajs-308 22 8 important important ADJ iajs-308 22 9 for for ADP iajs-308 22 10 pharmaceutical pharmaceutical NOUN iajs-308 22 11 industry industry NOUN iajs-308 22 12 and and CCONJ iajs-308 22 13 material material NOUN iajs-308 22 14 science science NOUN iajs-308 22 15 due due ADP iajs-308 22 16 to to ADP iajs-308 22 17 their their PRON iajs-308 22 18 various various ADJ iajs-308 22 19 applications application NOUN iajs-308 22 20 . . PUNCT iajs-308 23 1 isoxazoline isoxazoline NOUN iajs-308 23 2 are be AUX iajs-308 23 3 present present ADJ iajs-308 23 4 in in ADP iajs-308 23 5 the the DET iajs-308 23 6 structures structure NOUN iajs-308 23 7 of of ADP iajs-308 23 8 many many ADJ iajs-308 23 9 natural natural ADJ iajs-308 23 10 products product NOUN iajs-308 23 11 . . PUNCT iajs-308 24 1 in in ADP iajs-308 24 2 fact fact NOUN iajs-308 24 3 , , PUNCT iajs-308 24 4 isoxazoline isoxazoline NOUN iajs-308 24 5 have have VERB iajs-308 24 6 a a DET iajs-308 24 7 broad broad ADJ iajs-308 24 8 spectrum spectrum NOUN iajs-308 24 9 of of ADP iajs-308 24 10 their their PRON iajs-308 24 11 biological biological ADJ iajs-308 24 12 and and CCONJ iajs-308 24 13 pharmacological pharmacological ADJ iajs-308 24 14 activities activity NOUN iajs-308 24 15 [ [ X iajs-308 24 16 3 3 NUM iajs-308 24 17 - - SYM iajs-308 24 18 6 6 NUM iajs-308 24 19 ] ] PUNCT iajs-308 24 20 . . PUNCT iajs-308 25 1 pyrazoles pyrazole NOUN iajs-308 25 2 are be AUX iajs-308 25 3 one one NUM iajs-308 25 4 of of ADP iajs-308 25 5 the the DET iajs-308 25 6 important important ADJ iajs-308 25 7 members member NOUN iajs-308 25 8 of of ADP iajs-308 25 9 heterocyclic heterocyclic ADJ iajs-308 25 10 compounds compound NOUN iajs-308 25 11 with with ADP iajs-308 25 12 two two NUM iajs-308 25 13 adjacent adjacent ADJ iajs-308 25 14 nitrogens nitrogen NOUN iajs-308 25 15 in in ADP iajs-308 25 16 a a DET iajs-308 25 17 five five NUM iajs-308 25 18 - - PUNCT iajs-308 25 19 membered membere VERB iajs-308 25 20 ring ring NOUN iajs-308 25 21 system system NOUN iajs-308 25 22 . . PUNCT iajs-308 26 1 because because SCONJ iajs-308 26 2 of of ADP iajs-308 26 3 their their PRON iajs-308 26 4 aromaticity aromaticity NOUN iajs-308 26 5 and and CCONJ iajs-308 26 6 wide wide ADJ iajs-308 26 7 application application NOUN iajs-308 26 8 in in ADP iajs-308 26 9 pharmaceutical pharmaceutical NOUN iajs-308 26 10 and and CCONJ iajs-308 26 11 material material NOUN iajs-308 26 12 industry industry NOUN iajs-308 26 13 , , PUNCT iajs-308 26 14 they they PRON iajs-308 26 15 have have AUX iajs-308 26 16 gained gain VERB iajs-308 26 17 significant significant ADJ iajs-308 26 18 interest interest NOUN iajs-308 26 19 among among ADP iajs-308 26 20 the the DET iajs-308 26 21 scientist scientist NOUN iajs-308 26 22 [ [ X iajs-308 26 23 7 7 NUM iajs-308 26 24 - - SYM iajs-308 26 25 10 10 NUM iajs-308 26 26 ] ] PUNCT iajs-308 26 27 . . PUNCT iajs-308 27 1 also also ADV iajs-308 27 2 the the DET iajs-308 27 3 pyrazoline pyrazoline NOUN iajs-308 27 4 showed show VERB iajs-308 27 5 a a DET iajs-308 27 6 wide wide ADJ iajs-308 27 7 spectrum spectrum NOUN iajs-308 27 8 of of ADP iajs-308 27 9 biological biological ADJ iajs-308 27 10 activities activity NOUN iajs-308 27 11 such such ADJ iajs-308 27 12 as as ADP iajs-308 27 13 anti anti ADJ iajs-308 27 14 - - ADJ iajs-308 27 15 bacterial bacterial ADJ iajs-308 27 16 , , PUNCT iajs-308 27 17 antifungal antifungal ADJ iajs-308 27 18 , , PUNCT iajs-308 27 19 herbicidal herbicidal NOUN iajs-308 27 20 and and CCONJ iajs-308 27 21 anti anti ADJ iajs-308 27 22 - - ADJ iajs-308 27 23 choligenic choligenic ADJ iajs-308 27 24 [ [ PUNCT iajs-308 27 25 11 11 NUM iajs-308 27 26 - - SYM iajs-308 27 27 14 14 NUM iajs-308 27 28 ] ] PUNCT iajs-308 27 29 . . PUNCT iajs-308 28 1 in in ADP iajs-308 28 2 the the DET iajs-308 28 3 view view NOUN iajs-308 28 4 of of ADP iajs-308 28 5 the the DET iajs-308 28 6 varied varied ADJ iajs-308 28 7 biological biological ADJ iajs-308 28 8 , , PUNCT iajs-308 28 9 pharmacological pharmacological NOUN iajs-308 28 10 and and CCONJ iajs-308 28 11 industry industry NOUN iajs-308 28 12 applications application NOUN iajs-308 28 13 , , PUNCT iajs-308 28 14 we we PRON iajs-308 28 15 have have AUX iajs-308 28 16 planned plan VERB iajs-308 28 17 to to PART iajs-308 28 18 synthesis synthesis VERB iajs-308 28 19 some some DET iajs-308 28 20 isoxazoline isoxazoline NOUN iajs-308 28 21 derivatives derivative NOUN iajs-308 28 22 containing contain VERB iajs-308 28 23 imine imine NOUN iajs-308 28 24 , , PUNCT iajs-308 28 25 pyrazole pyrazole NOUN iajs-308 28 26 or or CCONJ iajs-308 28 27 pyrazoline pyrazoline NOUN iajs-308 28 28 unit unit NOUN iajs-308 28 29 . . PUNCT iajs-308 29 1 experimental experimental ADJ iajs-308 29 2 chemicals chemical NOUN iajs-308 29 3 all all DET iajs-308 29 4 chemicals chemical NOUN iajs-308 29 5 were be AUX iajs-308 29 6 supplied supply VERB iajs-308 29 7 by by ADP iajs-308 29 8 fluka fluka NOUN iajs-308 29 9 , , PUNCT iajs-308 29 10 gcc gcc NOUN iajs-308 29 11 , , PUNCT iajs-308 29 12 merck merck PROPN iajs-308 29 13 and and CCONJ iajs-308 29 14 sigma sigma PROPN iajs-308 29 15 - - PUNCT iajs-308 29 16 aldrich aldrich PROPN iajs-308 29 17 chemicals chemicals PROPN iajs-308 29 18 co. co. PROPN iajs-308 29 19 and and CCONJ iajs-308 29 20 used use VERB iajs-308 29 21 as as SCONJ iajs-308 29 22 received receive VERB iajs-308 29 23 . . PUNCT iajs-308 30 1 techniques technique NOUN iajs-308 30 2 ftir ftir PROPN iajs-308 30 3 spectra spectra PROPN iajs-308 30 4 were be AUX iajs-308 30 5 recorded record VERB iajs-308 30 6 using use VERB iajs-308 30 7 potassium potassium NOUN iajs-308 30 8 bromide bromide NOUN iajs-308 30 9 discs disc NOUN iajs-308 30 10 on on ADP iajs-308 30 11 a a DET iajs-308 30 12 shimadzu(ir shimadzu(ir ADJ iajs-308 30 13 prestige prestige NOUN iajs-308 30 14 21 21 NUM iajs-308 30 15 ) ) PUNCT iajs-308 30 16 1hnmr 1hnmr NUM iajs-308 30 17 spectra spectra NOUN iajs-308 30 18 were be AUX iajs-308 30 19 carried carry VERB iajs-308 30 20 out out ADP iajs-308 30 21 by by ADP iajs-308 30 22 company company NOUN iajs-308 30 23 : : PUNCT iajs-308 30 24 bruker bruker PROPN iajs-308 30 25 , , PUNCT iajs-308 30 26 model model NOUN iajs-308 30 27 : : PUNCT iajs-308 30 28 ultra ultra ADJ iajs-308 30 29 - - ADJ iajs-308 30 30 shield shield ADJ iajs-308 30 31 400mhz 400mhz NUM iajs-308 30 32 , , PUNCT iajs-308 30 33 origin origin NOUN iajs-308 30 34 : : PUNCT iajs-308 30 35 switzerland switzerland NOUN iajs-308 30 36 and and CCONJ iajs-308 30 37 are be AUX iajs-308 30 38 reported report VERB iajs-308 30 39 in in ADP iajs-308 30 40 ppm(δ ppm(δ PROPN iajs-308 30 41 ) ) PUNCT iajs-308 30 42 dmso dmso NOUN iajs-308 30 43 were be AUX iajs-308 30 44 used use VERB iajs-308 30 45 as as ADP iajs-308 30 46 a a DET iajs-308 30 47 solvent solvent NOUN iajs-308 30 48 with with ADP iajs-308 30 49 tms tms PROPN iajs-308 30 50 as as ADP iajs-308 30 51 an an DET iajs-308 30 52 internal internal ADJ iajs-308 30 53 standard standard NOUN iajs-308 30 54 , , PUNCT iajs-308 30 55 measurements measurement NOUN iajs-308 30 56 were be AUX iajs-308 30 57 made make VERB iajs-308 30 58 at at ADP iajs-308 30 59 chemistry chemistry NOUN iajs-308 30 60 department department NOUN iajs-308 30 61 , , PUNCT iajs-308 30 62 science science NOUN iajs-308 30 63 and and CCONJ iajs-308 30 64 technology technology NOUN iajs-308 30 65 university university PROPN iajs-308 30 66 , , PUNCT iajs-308 30 67 jordan jordan PROPN iajs-308 30 68 . . PUNCT iajs-308 31 1 the the DET iajs-308 31 2 mass mass PROPN iajs-308 31 3 spectrum spectrum PROPN iajs-308 31 4 was be AUX iajs-308 31 5 recorded record VERB iajs-308 31 6 on on ADP iajs-308 31 7 shimadzu shimadzu ADJ iajs-308 31 8 model model NOUN iajs-308 31 9 6cms 6cms PROPN iajs-308 31 10 ql ql PROPN iajs-308 31 11 1000 1000 NUM iajs-308 31 12 ex ex NOUN iajs-308 31 13 , , PUNCT iajs-308 31 14 made make VERB iajs-308 31 15 in in ADP iajs-308 31 16 japan japan PROPN iajs-308 31 17 . . PUNCT iajs-308 32 1 uncorrected uncorrecte VERB iajs-308 32 2 melting melting NOUN iajs-308 32 3 points point NOUN iajs-308 32 4 were be AUX iajs-308 32 5 determined determine VERB iajs-308 32 6 by by ADP iajs-308 32 7 using use VERB iajs-308 32 8 hot hot ADJ iajs-308 32 9 - - PUNCT iajs-308 32 10 stage stage NOUN iajs-308 32 11 , , PUNCT iajs-308 32 12 gallen gallen PROPN iajs-308 32 13 kamp kamp PROPN iajs-308 32 14 melting melting NOUN iajs-308 32 15 point point NOUN iajs-308 32 16 apparatus apparatus NOUN iajs-308 32 17 . . PUNCT iajs-308 33 1 synthesis synthesis NOUN iajs-308 33 2 new new ADJ iajs-308 33 3 compounds compound NOUN iajs-308 33 4 are be AUX iajs-308 33 5 synthesized synthesize VERB iajs-308 33 6 according accord VERB iajs-308 33 7 to to ADP iajs-308 33 8 scheme1 scheme1 NOUN iajs-308 33 9 synthesis synthesis NOUN iajs-308 33 10 of of ADP iajs-308 33 11 ( ( PUNCT iajs-308 33 12 chalcones chalcones PROPN iajs-308 33 13 ) ) PUNCT iajs-308 33 14 3-(4 3-(4 NUM iajs-308 33 15 - - PUNCT iajs-308 33 16 hydroxyphenyl)(4¯-bromophenyl)-2 hydroxyphenyl)(4¯-bromophenyl)-2 PROPN iajs-308 33 17 - - PUNCT iajs-308 33 18 propene-1 propene-1 NOUN iajs-308 33 19 - - PUNCT iajs-308 33 20 one[i]a one[i]a PROPN iajs-308 33 21 and and CCONJ iajs-308 33 22 3-(4¯-bromophenyl)-1-(4 3-(4¯-bromophenyl)-1-(4 NUM iajs-308 33 23 - - PUNCT iajs-308 33 24 hydroxyphenyl)prop-2 hydroxyphenyl)prop-2 NOUN iajs-308 33 25 - - PUNCT iajs-308 33 26 en-1 en-1 NOUN iajs-308 33 27 - - PUNCT iajs-308 33 28 one[i]b one[i]b PRON iajs-308 33 29 equimolar equimolar ADJ iajs-308 33 30 quantities quantity NOUN iajs-308 33 31 of of ADP iajs-308 33 32 4 4 NUM iajs-308 33 33 - - PUNCT iajs-308 33 34 bromo bromo NOUN iajs-308 33 35 or or CCONJ iajs-308 33 36 4 4 NUM iajs-308 33 37 - - PUNCT iajs-308 33 38 hydroxy hydroxy ADJ iajs-308 33 39 acetophenone acetophenone NOUN iajs-308 33 40 ( ( PUNCT iajs-308 33 41 0.01 0.01 NUM iajs-308 33 42 mol),and mol),and NOUN iajs-308 33 43 4 4 NUM iajs-308 33 44 - - PUNCT iajs-308 33 45 bromo bromo NOUN iajs-308 33 46 or4hydroxy or4hydroxy NOUN iajs-308 33 47 benzaldehyde benzaldehyde NOUN iajs-308 33 48 ( ( PUNCT iajs-308 33 49 0.01 0.01 NUM iajs-308 33 50 mol mol NOUN iajs-308 33 51 ) ) PUNCT iajs-308 33 52 were be AUX iajs-308 33 53 dissolved dissolve VERB iajs-308 33 54 in in ADP iajs-308 33 55 minimum minimum NOUN iajs-308 33 56 amount amount NOUN iajs-308 33 57 of of ADP iajs-308 33 58 alcohol alcohol NOUN iajs-308 33 59 . . PUNCT iajs-308 34 1 sodium sodium NOUN iajs-308 34 2 hydroxide hydroxide NOUN iajs-308 34 3 solution solution NOUN iajs-308 34 4 ( ( PUNCT iajs-308 34 5 0.02 0.02 NUM iajs-308 34 6 mol mol NOUN iajs-308 34 7 ) ) PUNCT iajs-308 34 8 was be AUX iajs-308 34 9 added add VERB iajs-308 34 10 slowly slowly ADV iajs-308 34 11 and and CCONJ iajs-308 34 12 the the DET iajs-308 34 13 mixture mixture NOUN iajs-308 34 14 became become VERB iajs-308 34 15 cold cold ADJ iajs-308 34 16 . . PUNCT iajs-308 35 1 then then ADV iajs-308 35 2 the the DET iajs-308 35 3 mixture mixture NOUN iajs-308 35 4 was be AUX iajs-308 35 5 poured pour VERB iajs-308 35 6 slowly slowly ADV iajs-308 35 7 into into ADP iajs-308 35 8 400 400 NUM iajs-308 35 9 ml ml NOUN iajs-308 35 10 of of ADP iajs-308 35 11 ice ice NOUN iajs-308 35 12 water water NOUN iajs-308 35 13 with with ADP iajs-308 35 14 constant constant ADJ iajs-308 35 15 stirring stirring NOUN iajs-308 35 16 and and CCONJ iajs-308 35 17 kept keep VERB iajs-308 35 18 in in ADP iajs-308 35 19 refrigerator refrigerator NOUN iajs-308 35 20 for for ADP iajs-308 35 21 24 24 NUM iajs-308 35 22 hrs hrs NOUN iajs-308 35 23 . . PUNCT iajs-308 36 1 the the DET iajs-308 36 2 precipitate precipitate NOUN iajs-308 36 3 obtained obtain VERB iajs-308 36 4 was be AUX iajs-308 36 5 filtered filter VERB iajs-308 36 6 [ [ X iajs-308 36 7 15],washed 15],washe VERB iajs-308 36 8 and and CCONJ iajs-308 36 9 recrystallized recrystallize VERB iajs-308 36 10 from from ADP iajs-308 36 11 ethanol ethanol NOUN iajs-308 36 12 . . PUNCT iajs-308 37 1 synthesis synthesis NOUN iajs-308 37 2 of of ADP iajs-308 37 3 4-(3-(4`-bromophenyl)-4,5 4-(3-(4`-bromophenyl)-4,5 NUM iajs-308 37 4 - - PUNCT iajs-308 37 5 dihydroisoxazol-5 dihydroisoxazol-5 NUM iajs-308 37 6 - - PUNCT iajs-308 37 7 yl)phenol yl)phenol NOUN iajs-308 38 1 [ [ X iajs-308 38 2 ii]a ii]a NOUN iajs-308 38 3 and and CCONJ iajs-308 38 4 4-(5-(4`bromophenyl)-4,5 4-(5-(4`bromophenyl)-4,5 NUM iajs-308 38 5 - - PUNCT iajs-308 38 6 dihydroisoxazol-3 dihydroisoxazol-3 NUM iajs-308 38 7 - - PUNCT iajs-308 38 8 yl)phenol[ii]b yl)phenol[ii]b NOUN iajs-308 38 9 a a DET iajs-308 38 10 mixture mixture NOUN iajs-308 38 11 of of ADP iajs-308 38 12 chalcone chalcone NOUN iajs-308 38 13 ( ( PUNCT iajs-308 38 14 0.02 0.02 NUM iajs-308 38 15 mol mol NOUN iajs-308 38 16 ) ) PUNCT iajs-308 38 17 , , PUNCT iajs-308 38 18 hydroxylamine hydroxylamine ADJ iajs-308 38 19 hydrochloride hydrochloride NOUN iajs-308 38 20 ( ( PUNCT iajs-308 38 21 0.02 0.02 NUM iajs-308 38 22 mol mol NOUN iajs-308 38 23 , , PUNCT iajs-308 38 24 1.39 1.39 NUM iajs-308 38 25 gm gm PROPN iajs-308 38 26 ) ) PUNCT iajs-308 38 27 and and CCONJ iajs-308 38 28 sodium sodium NOUN iajs-308 38 29 hydroxide hydroxide NOUN iajs-308 38 30 solution solution NOUN iajs-308 38 31 ( ( PUNCT iajs-308 38 32 0.5 0.5 NUM iajs-308 38 33 g g PROPN iajs-308 38 34 naoh naoh NOUN iajs-308 38 35 in in ADP iajs-308 38 36 25 25 NUM iajs-308 38 37 ml ml NOUN iajs-308 38 38 of of ADP iajs-308 38 39 water water NOUN iajs-308 38 40 ) ) PUNCT iajs-308 38 41 in in ADP iajs-308 38 42 ethanol ethanol NOUN iajs-308 38 43 ( ( PUNCT iajs-308 38 44 60 60 NUM iajs-308 38 45 ml ml NOUN iajs-308 38 46 ) ) PUNCT iajs-308 38 47 was be AUX iajs-308 38 48 refluxed refluxe VERB iajs-308 38 49 for for ADP iajs-308 38 50 6hrs 6hrs NUM iajs-308 38 51 . . PUNCT iajs-308 39 1 the the DET iajs-308 39 2 mixture mixture NOUN iajs-308 39 3 was be AUX iajs-308 39 4 concentrated concentrate VERB iajs-308 39 5 under under ADP iajs-308 39 6 vacuum vacuum NOUN iajs-308 39 7 and and CCONJ iajs-308 39 8 poured pour VERB iajs-308 39 9 into into ADP iajs-308 39 10 ice ice NOUN iajs-308 39 11 water[16 water[16 PROPN iajs-308 39 12 ] ] PUNCT iajs-308 39 13 . . PUNCT iajs-308 40 1 the the DET iajs-308 40 2 precipitate precipitate NOUN iajs-308 40 3 obtained obtain VERB iajs-308 40 4 was be AUX iajs-308 40 5 filtered filter VERB iajs-308 40 6 , , PUNCT iajs-308 40 7 washed wash VERB iajs-308 40 8 and and CCONJ iajs-308 40 9 recrystallized recrystallize VERB iajs-308 40 10 from from ADP iajs-308 40 11 chloroform chloroform NOUN iajs-308 40 12 . . PUNCT iajs-308 41 1 synthesis synthesis NOUN iajs-308 41 2 of of ADP iajs-308 41 3 new new ADJ iajs-308 41 4 ester ester NOUN iajs-308 41 5 derivatives[iii derivatives[iii VERB iajs-308 41 6 ] ] PUNCT iajs-308 41 7 a a DET iajs-308 41 8 mixtuer mixtuer NOUN iajs-308 41 9 of of ADP iajs-308 41 10 compound compound NOUN iajs-308 42 1 [ [ X iajs-308 42 2 ii]a ii]a NOUN iajs-308 42 3 , , PUNCT iajs-308 42 4 b(0.01mol b(0.01mol ADP iajs-308 42 5 ) ) PUNCT iajs-308 42 6 , , PUNCT iajs-308 42 7 ethyl ethyl PROPN iajs-308 42 8 αchloro αchloro PROPN iajs-308 42 9 acetate acetate PROPN iajs-308 42 10 ( ( PUNCT iajs-308 42 11 0.01 0.01 NUM iajs-308 42 12 mol mol NOUN iajs-308 42 13 ) ) PUNCT iajs-308 42 14 and and CCONJ iajs-308 42 15 fused fuse VERB iajs-308 42 16 sodium sodium NOUN iajs-308 42 17 acetate acetate NOUN iajs-308 42 18 ( ( PUNCT iajs-308 42 19 0.03mol,2.46gm 0.03mol,2.46gm PROPN iajs-308 42 20 ) ) PUNCT iajs-308 42 21 in in ADP iajs-308 42 22 ethanol ethanol NOUN iajs-308 42 23 25ml 25ml NOUN iajs-308 42 24 was be AUX iajs-308 42 25 refluxed refluxe VERB iajs-308 42 26 for for ADP iajs-308 42 27 4 4 NUM iajs-308 42 28 hrs hrs NOUN iajs-308 42 29 .then .then AUX iajs-308 42 30 cooled cool VERB iajs-308 42 31 and and CCONJ iajs-308 42 32 437 437 NUM iajs-308 42 33 | | ADV iajs-308 42 34 chemistry chemistry NOUN iajs-308 42 35 2014 2014 NUM iajs-308 42 36 ) ) PUNCT iajs-308 42 37 عام عام ADP iajs-308 42 38 3العدد 3العدد NUM iajs-308 42 39 ( ( PUNCT iajs-308 42 40 27مجلة 27مجلة NUM iajs-308 42 41 إبن إبن VERB iajs-308 42 42 الھيثم الھيثم NOUN iajs-308 42 43 للعلوم للعلوم NOUN iajs-308 42 44 الصرفة الصرفة NOUN iajs-308 43 1 و و PRON iajs-308 43 2 التطبيقية التطبيقية ADV iajs-308 43 3 المجلد المجلد VERB iajs-308 43 4 ibn ibn PROPN iajs-308 43 5 al al PROPN iajs-308 43 6 - - PUNCT iajs-308 43 7 haitham haitham PROPN iajs-308 43 8 jour jour X iajs-308 43 9 . . PROPN iajs-308 44 1 for for ADP iajs-308 44 2 pure pure ADJ iajs-308 44 3 & & CCONJ iajs-308 44 4 appl appl PROPN iajs-308 44 5 . . PUNCT iajs-308 45 1 sci sci PROPN iajs-308 45 2 . . PUNCT iajs-308 45 3 vol vol NOUN iajs-308 45 4 . . PROPN iajs-308 46 1 27 27 NUM iajs-308 46 2 ( ( PUNCT iajs-308 46 3 3 3 NUM iajs-308 46 4 ) ) PUNCT iajs-308 46 5 2014 2014 NUM iajs-308 46 6 poured pour VERB iajs-308 46 7 into into ADP iajs-308 46 8 cold cold ADJ iajs-308 46 9 water water NOUN iajs-308 46 10 , , PUNCT iajs-308 46 11 the the DET iajs-308 46 12 resulting result VERB iajs-308 46 13 soiled soil VERB iajs-308 46 14 was be AUX iajs-308 46 15 filtered filter VERB iajs-308 46 16 and and CCONJ iajs-308 46 17 from from ADP iajs-308 46 18 recrystallized recrystallized ADJ iajs-308 46 19 ethanol ethanol NOUN iajs-308 47 1 [ [ X iajs-308 47 2 17 17 NUM iajs-308 47 3 ] ] PUNCT iajs-308 47 4 to to PART iajs-308 47 5 give give VERB iajs-308 47 6 a a DET iajs-308 47 7 new new ADJ iajs-308 47 8 ester ester NOUN iajs-308 47 9 . . PUNCT iajs-308 48 1 c c NOUN iajs-308 49 1 o o NOUN iajs-308 49 2 x x X iajs-308 49 3 cy cy PROPN iajs-308 49 4 o o PROPN iajs-308 49 5 h h NOUN iajs-308 49 6 naoh naoh NOUN iajs-308 49 7 x x PROPN iajs-308 50 1 c c NOUN iajs-308 50 2 o o NOUN iajs-308 50 3 ch ch NOUN iajs-308 50 4 ch ch NOUN iajs-308 50 5 x x PUNCT iajs-308 50 6 n n PROPN iajs-308 50 7 o o X iajs-308 50 8 nh nh INTJ iajs-308 51 1 oh oh INTJ iajs-308 51 2 .hcl .hcl PUNCT iajs-308 52 1 y y PROPN iajs-308 52 2 clch clch PROPN iajs-308 52 3 co co VERB iajs-308 52 4 et et PROPN iajs-308 52 5 br br NOUN iajs-308 52 6 n n ADV iajs-308 52 7 o o NOUN iajs-308 52 8 n n PRON iajs-308 52 9 o o X iajs-308 52 10 och2conhn och2conhn X iajs-308 52 11 naoh naoh NOUN iajs-308 52 12 etoh etoh PROPN iajs-308 52 13 y y PROPN iajs-308 52 14 och2co2et och2co2et PROPN iajs-308 52 15 och2conhnh2br och2conhnh2br PROPN iajs-308 52 16 n n CCONJ iajs-308 52 17 o o PROPN iajs-308 52 18 ch3 ch3 PROPN iajs-308 52 19 br br NOUN iajs-308 52 20 ch ch NOUN iajs-308 52 21 r r NOUN iajs-308 52 22 4 4 NUM iajs-308 52 23 - - PUNCT iajs-308 52 24 r r NOUN iajs-308 52 25 c c NOUN iajs-308 52 26 h h NOUN iajs-308 52 27 cho6 cho6 NOUN iajs-308 52 28 4 4 NUM iajs-308 52 29 och2cobr och2cobr PROPN iajs-308 52 30 n n NUM iajs-308 52 31 o o NOUN iajs-308 52 32 n n CCONJ iajs-308 52 33 n n NOUN iajs-308 52 34 ch3h3c ch3h3c PROPN iajs-308 53 1 och2cobr och2cobr VERB iajs-308 53 2 n n NUM iajs-308 53 3 o o NOUN iajs-308 53 4 n n CCONJ iajs-308 53 5 n n CCONJ iajs-308 53 6 ch3o ch3o PROPN iajs-308 53 7 ethyl ethyl PROPN iajs-308 53 8 aceto aceto PROPN iajs-308 53 9 acetate acetate PROPN iajs-308 53 10 acetyl acetyl NOUN iajs-308 53 11 acetone acetone NOUN iajs-308 54 1 [ [ X iajs-308 54 2 i i X iajs-308 54 3 ] ] X iajs-308 55 1 [ [ X iajs-308 55 2 ii ii X iajs-308 55 3 ] ] X iajs-308 56 1 [ [ X iajs-308 56 2 iii iii X iajs-308 56 3 ] ] X iajs-308 57 1 [ [ X iajs-308 57 2 iv iv X iajs-308 57 3 ] ] X iajs-308 58 1 [ [ X iajs-308 58 2 v v X iajs-308 58 3 ] ] X iajs-308 59 1 [ [ X iajs-308 59 2 vii vii X iajs-308 59 3 [ [ X iajs-308 59 4 viii viii X iajs-308 59 5 ] ] X iajs-308 59 6 a a DET iajs-308 59 7 a a PROPN iajs-308 59 8 , , PUNCT iajs-308 59 9 b b PROPN iajs-308 59 10 a a PRON iajs-308 59 11 , , PUNCT iajs-308 59 12 b b PROPN iajs-308 59 13 a a DET iajs-308 59 14 a a DET iajs-308 59 15 a a NOUN iajs-308 59 16 , , PUNCT iajs-308 59 17 b b NOUN iajs-308 59 18 a a NOUN iajs-308 59 19 and and CCONJ iajs-308 59 20 [ [ X iajs-308 59 21 vi]a vi]a NOUN iajs-308 59 22 , , PUNCT iajs-308 59 23 b b X iajs-308 59 24 ] ] SYM iajs-308 59 25 2 2 NUM iajs-308 59 26 2 2 NUM iajs-308 59 27 2 2 NUM iajs-308 59 28 nh nh PROPN iajs-308 59 29 nh nh PROPN iajs-308 59 30 .h .h PROPN iajs-308 59 31 o2 o2 PROPN iajs-308 59 32 2 2 NUM iajs-308 59 33 2 2 NUM iajs-308 59 34 clch clch NOUN iajs-308 59 35 co co X iajs-308 59 36 et2 et2 PROPN iajs-308 59 37 2 2 PROPN iajs-308 59 38 eto2ch2co eto2ch2co PROPN iajs-308 59 39 n n NUM iajs-308 59 40 o o NOUN iajs-308 59 41 br br X iajs-308 60 1 [ [ X iajs-308 60 2 iii]b iii]b VERB iajs-308 60 3 etoh etoh PROPN iajs-308 60 4 nh nh PROPN iajs-308 60 5 nh nh PROPN iajs-308 60 6 .h .h PROPN iajs-308 60 7 o2 o2 PROPN iajs-308 60 8 2 2 NUM iajs-308 60 9 2 2 NUM iajs-308 60 10 br br NOUN iajs-308 60 11 n n ADP iajs-308 60 12 o o NOUN iajs-308 60 13 h2nhnoch2co h2nhnoch2co PROPN iajs-308 61 1 [ [ X iajs-308 61 2 iv iv ADP iajs-308 61 3 ] ] PUNCT iajs-308 61 4 b b PROPN iajs-308 61 5 r r NOUN iajs-308 61 6 nhnoch2co nhnoch2co PROPN iajs-308 61 7 n n CCONJ iajs-308 61 8 o o NOUN iajs-308 61 9 brhc brhc NOUN iajs-308 61 10 4 4 NUM iajs-308 61 11 - - PUNCT iajs-308 61 12 r r NOUN iajs-308 61 13 c c NOUN iajs-308 61 14 h h NOUN iajs-308 61 15 cho6 cho6 VERB iajs-308 61 16 4 4 NUM iajs-308 61 17 br br NOUN iajs-308 61 18 n n ADP iajs-308 61 19 o o NOUN iajs-308 62 1 och2conn och2conn NOUN iajs-308 62 2 ch3h3c ch3h3c PROPN iajs-308 62 3 [ [ X iajs-308 62 4 vii vii X iajs-308 62 5 ] ] X iajs-308 62 6 b b PROPN iajs-308 62 7 br br NOUN iajs-308 62 8 n n ADP iajs-308 62 9 o o NOUN iajs-308 63 1 och2conn och2conn NOUN iajs-308 63 2 h3c h3c X iajs-308 63 3 o o X iajs-308 64 1 [ [ X iajs-308 64 2 viii viii X iajs-308 64 3 ] ] X iajs-308 64 4 b b PROPN iajs-308 64 5 x= x= PROPN iajs-308 64 6 br br PROPN iajs-308 64 7 , , PUNCT iajs-308 64 8 y y PROPN iajs-308 64 9 = = PUNCT iajs-308 65 1 oh oh INTJ iajs-308 65 2 ; ; PUNCT iajs-308 66 1 [ [ X iajs-308 66 2 i i X iajs-308 66 3 ] ] PUNCT iajs-308 66 4 , , PUNCT iajs-308 66 5 [ [ X iajs-308 66 6 ii ii X iajs-308 66 7 ] ] X iajs-308 66 8 and[iii]a and[iii]a NOUN iajs-308 67 1 a a PRON iajs-308 67 2 a a PRON iajs-308 67 3 x= x= NOUN iajs-308 68 1 oh oh INTJ iajs-308 68 2 , , PUNCT iajs-308 68 3 y y PROPN iajs-308 68 4 = = PUNCT iajs-308 68 5 br br PROPN iajs-308 68 6 ; ; PUNCT iajs-308 69 1 [ [ X iajs-308 69 2 i i X iajs-308 69 3 ] ] PUNCT iajs-308 69 4 , , PUNCT iajs-308 69 5 [ [ X iajs-308 69 6 ii ii X iajs-308 69 7 ] ] X iajs-308 69 8 and[iii]b and[iii]b VERB iajs-308 69 9 b b X iajs-308 69 10 b b NOUN iajs-308 69 11 r r NOUN iajs-308 69 12 = = NOUN iajs-308 69 13 no no NOUN iajs-308 69 14 , , PUNCT iajs-308 69 15 br2 br2 PROPN iajs-308 69 16 acetyl acetyl NOUN iajs-308 69 17 acetone acetone NOUN iajs-308 69 18 ethyl ethyl PROPN iajs-308 69 19 aceto aceto PROPN iajs-308 69 20 acetate acetate PROPN iajs-308 69 21 scheme scheme PROPN iajs-308 69 22 ( ( PUNCT iajs-308 69 23 1 1 NUM iajs-308 69 24 ) ) PUNCT iajs-308 69 25 synthesis synthesis NOUN iajs-308 69 26 of of ADP iajs-308 69 27 hydrazid hydrazid NOUN iajs-308 69 28 derivatives derivative NOUN iajs-308 69 29 [ [ X iajs-308 69 30 iv]a iv]a PROPN iajs-308 69 31 , , PUNCT iajs-308 69 32 b b PROPN iajs-308 69 33 a a DET iajs-308 69 34 solution solution NOUN iajs-308 69 35 of of ADP iajs-308 69 36 ester ester NOUN iajs-308 69 37 [ [ X iajs-308 69 38 iii]a iii]a PROPN iajs-308 69 39 , , PUNCT iajs-308 69 40 b b PROPN iajs-308 69 41 ( ( PUNCT iajs-308 69 42 0.06 0.06 NUM iajs-308 69 43 mol mol NOUN iajs-308 69 44 ) ) PUNCT iajs-308 69 45 and and CCONJ iajs-308 69 46 hydrazine hydrazine NOUN iajs-308 69 47 hydrate(15ml hydrate(15ml NOUN iajs-308 69 48 ) ) PUNCT iajs-308 69 49 in(25ml in(25ml NOUN iajs-308 69 50 ) ) PUNCT iajs-308 69 51 of of ADP iajs-308 69 52 ethanol ethanol NOUN iajs-308 69 53 was be AUX iajs-308 69 54 heated heat VERB iajs-308 69 55 to to PART iajs-308 69 56 reflux reflux VERB iajs-308 69 57 during during ADP iajs-308 69 58 4hrs 4hrs PROPN iajs-308 69 59 . . PUNCT iajs-308 70 1 the the DET iajs-308 70 2 mixture mixture NOUN iajs-308 70 3 was be AUX iajs-308 70 4 then then ADV iajs-308 70 5 cooled cool VERB iajs-308 70 6 to to ADP iajs-308 70 7 room room NOUN iajs-308 70 8 temperature[18 temperature[18 PROPN iajs-308 70 9 ] ] PUNCT iajs-308 70 10 , , PUNCT iajs-308 70 11 and and CCONJ iajs-308 70 12 the the DET iajs-308 70 13 solid solid ADJ iajs-308 70 14 obtained obtain VERB iajs-308 70 15 was be AUX iajs-308 70 16 filtered filter VERB iajs-308 70 17 and and CCONJ iajs-308 70 18 recrystallized recrystallize VERB iajs-308 70 19 from from ADP iajs-308 70 20 ethanol ethanol NOUN iajs-308 70 21 . . PUNCT iajs-308 71 1 the the DET iajs-308 71 2 physical physical ADJ iajs-308 71 3 properties property NOUN iajs-308 71 4 of of ADP iajs-308 71 5 synthesized synthesize VERB iajs-308 71 6 compounds compound NOUN iajs-308 71 7 [ [ X iajs-308 71 8 i]-[iv i]-[iv X iajs-308 71 9 ] ] PUNCT iajs-308 71 10 were be AUX iajs-308 71 11 given give VERB iajs-308 71 12 in in ADP iajs-308 71 13 table table NOUN iajs-308 71 14 1 1 NUM iajs-308 71 15 . . PUNCT iajs-308 71 16 synthesis synthesis NOUN iajs-308 71 17 of of ADP iajs-308 71 18 schiff schiff NOUN iajs-308 71 19 base base PROPN iajs-308 71 20 derivatives[v]a derivatives[v]a PROPN iajs-308 71 21 , , PUNCT iajs-308 71 22 b b NOUN iajs-308 71 23 , , PUNCT iajs-308 71 24 [ [ X iajs-308 71 25 vi vi X iajs-308 71 26 ] ] X iajs-308 71 27 a a PRON iajs-308 71 28 , , PUNCT iajs-308 71 29 b b NOUN iajs-308 71 30 a a DET iajs-308 71 31 mixture mixture NOUN iajs-308 71 32 of of ADP iajs-308 71 33 new new ADJ iajs-308 71 34 hydrazide[iv]a hydrazide[iv]a NOUN iajs-308 71 35 , , PUNCT iajs-308 71 36 b b PROPN iajs-308 71 37 ( ( PUNCT iajs-308 71 38 0.01 0.01 NUM iajs-308 71 39 mol mol NOUN iajs-308 71 40 ) ) PUNCT iajs-308 71 41 , , PUNCT iajs-308 71 42 different different ADJ iajs-308 71 43 aromatic aromatic ADJ iajs-308 71 44 aldehyde aldehyde NOUN iajs-308 71 45 ( ( PUNCT iajs-308 71 46 0.012 0.012 NUM iajs-308 71 47 mol mol NOUN iajs-308 71 48 ) ) PUNCT iajs-308 71 49 , , PUNCT iajs-308 71 50 dry dry ADJ iajs-308 71 51 benzene benzene NOUN iajs-308 71 52 ( ( PUNCT iajs-308 71 53 10 10 NUM iajs-308 71 54 ml ml NOUN iajs-308 71 55 ) ) PUNCT iajs-308 71 56 and and CCONJ iajs-308 71 57 2drops 2drops NUM iajs-308 71 58 of of ADP iajs-308 71 59 glacial glacial ADJ iajs-308 71 60 acetic acetic ADJ iajs-308 71 61 acid acid NOUN iajs-308 71 62 was be AUX iajs-308 71 63 refluxed refluxe VERB iajs-308 71 64 for for ADP iajs-308 71 65 3hrs 3hrs NUM iajs-308 71 66 . . PUNCT iajs-308 72 1 the the DET iajs-308 72 2 solvent solvent NOUN iajs-308 72 3 was be AUX iajs-308 72 4 evaporated evaporate VERB iajs-308 72 5 under under ADP iajs-308 72 6 vacuum vacuum NOUN iajs-308 72 7 and and CCONJ iajs-308 72 8 the the DET iajs-308 72 9 residue residue NOUN iajs-308 72 10 crystallized crystallize VERB iajs-308 72 11 from from ADP iajs-308 72 12 chloroform[19 chloroform[19 ADV iajs-308 72 13 ] ] PUNCT iajs-308 72 14 . . PUNCT iajs-308 73 1 synthesis synthesis NOUN iajs-308 73 2 of of ADP iajs-308 73 3 pyrazole pyrazole NOUN iajs-308 73 4 and and CCONJ iajs-308 73 5 pyrazoline pyrazoline NOUN iajs-308 73 6 derivatives derivative NOUN iajs-308 73 7 [ [ X iajs-308 73 8 vii]a vii]a PROPN iajs-308 73 9 , , PUNCT iajs-308 73 10 b,[viii]a b,[viii]a PROPN iajs-308 73 11 , , PUNCT iajs-308 73 12 b b NOUN iajs-308 73 13 438 438 NUM iajs-308 73 14 | | ADV iajs-308 73 15 chemistry chemistry NOUN iajs-308 73 16 2014 2014 NUM iajs-308 73 17 ) ) PUNCT iajs-308 73 18 عام عام ADP iajs-308 73 19 3العدد 3العدد NUM iajs-308 73 20 ( ( PUNCT iajs-308 73 21 27مجلة 27مجلة NUM iajs-308 73 22 إبن إبن VERB iajs-308 73 23 الھيثم الھيثم NOUN iajs-308 73 24 للعلوم للعلوم NOUN iajs-308 73 25 الصرفة الصرفة NOUN iajs-308 74 1 و و PRON iajs-308 74 2 التطبيقية التطبيقية ADV iajs-308 74 3 المجلد المجلد VERB iajs-308 74 4 ibn ibn PROPN iajs-308 74 5 al al PROPN iajs-308 74 6 - - PUNCT iajs-308 74 7 haitham haitham PROPN iajs-308 74 8 jour jour X iajs-308 74 9 . . PROPN iajs-308 75 1 for for ADP iajs-308 75 2 pure pure ADJ iajs-308 75 3 & & CCONJ iajs-308 75 4 appl appl PROPN iajs-308 75 5 . . PUNCT iajs-308 76 1 sci sci PROPN iajs-308 76 2 . . PUNCT iajs-308 76 3 vol vol NOUN iajs-308 76 4 . . PROPN iajs-308 77 1 27 27 NUM iajs-308 77 2 ( ( PUNCT iajs-308 77 3 3 3 NUM iajs-308 77 4 ) ) PUNCT iajs-308 77 5 2014 2014 NUM iajs-308 77 6 a a DET iajs-308 77 7 mixture mixture NOUN iajs-308 77 8 of of ADP iajs-308 77 9 new new ADJ iajs-308 77 10 hydriozide hydriozide NOUN iajs-308 77 11 [ [ X iajs-308 77 12 iv]a iv]a PROPN iajs-308 77 13 , , PUNCT iajs-308 77 14 b b PROPN iajs-308 77 15 ( ( PUNCT iajs-308 77 16 0.0028 0.0028 NUM iajs-308 77 17 mol mol NOUN iajs-308 77 18 ) ) PUNCT iajs-308 77 19 and and CCONJ iajs-308 77 20 ch3coch2coch3or ch3coch2coch3or PROPN iajs-308 77 21 ch3coch2co2et ch3coch2co2et NOUN iajs-308 77 22 ( ( PUNCT iajs-308 77 23 0.0028 0.0028 NUM iajs-308 77 24 mol mol NOUN iajs-308 77 25 ) ) PUNCT iajs-308 77 26 in in ADP iajs-308 77 27 abs ab NOUN iajs-308 77 28 . . PUNCT iajs-308 78 1 etoh(20ml etoh(20ml PROPN iajs-308 78 2 ) ) PUNCT iajs-308 78 3 was be AUX iajs-308 78 4 refluxed refluxe VERB iajs-308 78 5 for for ADP iajs-308 78 6 3hrs 3hrs NUM iajs-308 78 7 . . PUNCT iajs-308 79 1 the the DET iajs-308 79 2 reaction reaction NOUN iajs-308 79 3 mixture mixture NOUN iajs-308 79 4 was be AUX iajs-308 79 5 cooled cool VERB iajs-308 79 6 and and CCONJ iajs-308 79 7 the the DET iajs-308 79 8 formed form VERB iajs-308 79 9 precipitate precipitate NOUN iajs-308 79 10 was be AUX iajs-308 79 11 filtered filter VERB iajs-308 79 12 off off ADP iajs-308 79 13 and and CCONJ iajs-308 79 14 recrystallized recrystallize VERB iajs-308 79 15 to to PART iajs-308 79 16 give give VERB iajs-308 79 17 new new ADJ iajs-308 79 18 pyrazoles pyrazole NOUN iajs-308 80 1 [ [ X iajs-308 80 2 vii]a vii]a PROPN iajs-308 80 3 , , PUNCT iajs-308 80 4 b b NOUN iajs-308 80 5 or or CCONJ iajs-308 80 6 pyrazoline[viii]a pyrazoline[viii]a PROPN iajs-308 80 7 , , PUNCT iajs-308 80 8 b b NOUN iajs-308 80 9 , , PUNCT iajs-308 80 10 respectively respectively ADV iajs-308 80 11 . . PUNCT iajs-308 81 1 the the DET iajs-308 81 2 physical physical ADJ iajs-308 81 3 properties property NOUN iajs-308 81 4 of of ADP iajs-308 81 5 synthesized synthesize VERB iajs-308 81 6 compounds compound NOUN iajs-308 81 7 [ [ X iajs-308 81 8 v]-[viii v]-[viii X iajs-308 81 9 ] ] PUNCT iajs-308 81 10 were be AUX iajs-308 81 11 listed list VERB iajs-308 81 12 in in ADP iajs-308 81 13 table table NOUN iajs-308 81 14 2 2 NUM iajs-308 81 15 . . NOUN iajs-308 81 16 results result NOUN iajs-308 81 17 and and CCONJ iajs-308 81 18 discussion discussion VERB iajs-308 81 19 the the DET iajs-308 81 20 chalcones chalcone NOUN iajs-308 82 1 [ [ X iajs-308 82 2 i]a i]a NOUN iajs-308 82 3 , , PUNCT iajs-308 82 4 b b PROPN iajs-308 82 5 were be AUX iajs-308 82 6 synthesized synthesize VERB iajs-308 82 7 by by ADP iajs-308 82 8 claisen claisen PROPN iajs-308 82 9 - - PUNCT iajs-308 82 10 schemidt schemidt ADJ iajs-308 82 11 reaction reaction NOUN iajs-308 82 12 from from ADP iajs-308 82 13 condensation condensation NOUN iajs-308 82 14 aromatic aromatic ADJ iajs-308 82 15 aldehyde aldehyde NOUN iajs-308 82 16 with with ADP iajs-308 82 17     SPACE iajs-308 82 18 acetophenone acetophenone NOUN iajs-308 82 19 in in ADP iajs-308 82 20 naoh naoh NOUN iajs-308 82 21 . . PUNCT iajs-308 83 1 the the DET iajs-308 83 2 compounds compound NOUN iajs-308 83 3 [ [ X iajs-308 83 4 i]a i]a NOUN iajs-308 83 5 , , PUNCT iajs-308 83 6 b b PROPN iajs-308 83 7 were be AUX iajs-308 83 8 characterized characterize VERB iajs-308 83 9 by by ADP iajs-308 83 10 melting melt VERB iajs-308 83 11 points point NOUN iajs-308 83 12 , , PUNCT iajs-308 83 13 ftir ftir PROPN iajs-308 83 14 spectroscopy spectroscopy PROPN iajs-308 83 15 .the .the PUNCT iajs-308 83 16 ftir ftir PROPN iajs-308 83 17 spectra spectra PROPN iajs-308 83 18 of of ADP iajs-308 83 19 compound[i]a compound[i]a PROPN iajs-308 83 20 , , PUNCT iajs-308 83 21 b b PROPN iajs-308 83 22 showed show VERB iajs-308 83 23 appearance appearance NOUN iajs-308 83 24 broad broad ADJ iajs-308 83 25 band band NOUN iajs-308 83 26 ν ν X iajs-308 83 27 o o NOUN iajs-308 83 28 - - NOUN iajs-308 83 29 h h NOUN iajs-308 83 30 between between ADP iajs-308 83 31 ( ( PUNCT iajs-308 83 32 3448 3448 NUM iajs-308 83 33 - - SYM iajs-308 83 34 3250)cm-1 3250)cm-1 NUM iajs-308 83 35 , , PUNCT iajs-308 83 36 absorption absorption NOUN iajs-308 83 37 sharp sharp ADJ iajs-308 83 38 stretching stretch VERB iajs-308 83 39 band band NOUN iajs-308 83 40 in in ADP iajs-308 83 41 the the DET iajs-308 83 42 region(1681 region(1681 PROPN iajs-308 83 43 - - PUNCT iajs-308 83 44 1645)cm-1 1645)cm-1 NUM iajs-308 83 45 due due ADP iajs-308 83 46 to to ADP iajs-308 83 47 c c NOUN iajs-308 83 48 = = NOUN iajs-308 83 49 o o X iajs-308 83 50 stretching stretch VERB iajs-308 83 51 with with ADP iajs-308 83 52 the the DET iajs-308 83 53 appearance appearance NOUN iajs-308 83 54 band band NOUN iajs-308 83 55 between between ADP iajs-308 83 56 ( ( PUNCT iajs-308 83 57 1654 1654 NUM iajs-308 83 58 - - SYM iajs-308 83 59 1610 1610 NUM iajs-308 83 60 ) ) PUNCT iajs-308 83 61 cm-1 cm-1 VERB iajs-308 84 1 due due ADP iajs-308 84 2 to to ADP iajs-308 84 3 ν ν X iajs-308 84 4 c c NOUN iajs-308 84 5 = = SYM iajs-308 84 6 c c NOUN iajs-308 84 7 of of ADP iajs-308 84 8 chalcone chalcone NOUN iajs-308 84 9 unit unit NOUN iajs-308 84 10 and and CCONJ iajs-308 84 11 a a DET iajs-308 84 12 stretching stretch VERB iajs-308 84 13 band band NOUN iajs-308 84 14 at at ADP iajs-308 84 15 ( ( PUNCT iajs-308 84 16 680 680 NUM iajs-308 84 17 - - PUNCT iajs-308 84 18 675)cm-1due 675)cm-1due NUM iajs-308 84 19 to to ADP iajs-308 84 20 c-br.also c-br.also PROPN iajs-308 84 21 the the DET iajs-308 84 22 spectra spectra NOUN iajs-308 84 23 showed show VERB iajs-308 84 24 disappearance disappearance NOUN iajs-308 84 25 characteristic characteristic ADJ iajs-308 84 26 bands band NOUN iajs-308 84 27 of of ADP iajs-308 84 28 starting start VERB iajs-308 84 29 materials material NOUN iajs-308 84 30 . . PUNCT iajs-308 85 1 the the DET iajs-308 85 2 isoxazoline isoxazoline NOUN iajs-308 85 3 compound compound NOUN iajs-308 86 1 [ [ X iajs-308 86 2 ii]a ii]a PROPN iajs-308 86 3 , , PUNCT iajs-308 86 4 b b PROPN iajs-308 86 5 was be AUX iajs-308 86 6 synthesized synthesize VERB iajs-308 86 7 by by ADP iajs-308 86 8 the the DET iajs-308 86 9 reaction reaction NOUN iajs-308 86 10 of of ADP iajs-308 86 11 compound[i]a compound[i]a PROPN iajs-308 86 12 , , PUNCT iajs-308 86 13 b b NOUN iajs-308 86 14 with with ADP iajs-308 86 15 hydroxylamine hydroxylamine ADJ iajs-308 86 16 hydrochloride hydrochloride NOUN iajs-308 86 17 in in ADP iajs-308 86 18 basic basic ADJ iajs-308 86 19 medium medium NOUN iajs-308 86 20 .the .the PROPN iajs-308 86 21 ftir ftir PROPN iajs-308 86 22 spectra spectra PROPN iajs-308 86 23 of of ADP iajs-308 86 24 compound compound NOUN iajs-308 86 25 [ [ X iajs-308 86 26 ii]a ii]a PROPN iajs-308 86 27 showed show VERB iajs-308 86 28 disappearance disappearance NOUN iajs-308 86 29 the the DET iajs-308 86 30 bands band NOUN iajs-308 86 31 of of ADP iajs-308 86 32 c c NOUN iajs-308 86 33 = = NOUN iajs-308 86 34 o o NOUN iajs-308 86 35 and and CCONJ iajs-308 86 36 c c X iajs-308 86 37 = = NOUN iajs-308 86 38 c c NOUN iajs-308 86 39 for for ADP iajs-308 86 40 chalcone chalcone NOUN iajs-308 86 41 moiety moiety NOUN iajs-308 86 42 with with ADP iajs-308 86 43 the the DET iajs-308 86 44 appearance appearance NOUN iajs-308 86 45 of of ADP iajs-308 86 46 new new ADJ iajs-308 86 47 bands band NOUN iajs-308 86 48 for for ADP iajs-308 86 49 ν ν NOUN iajs-308 86 50 c c NOUN iajs-308 86 51 - - PUNCT iajs-308 86 52 haliph haliph NOUN iajs-308 86 53 . . PUNCT iajs-308 87 1 in in ADP iajs-308 87 2 the the DET iajs-308 87 3 region region NOUN iajs-308 87 4 ( ( PUNCT iajs-308 87 5 2920 2920 NUM iajs-308 87 6 - - SYM iajs-308 87 7 2854 2854 NUM iajs-308 87 8 ) ) PUNCT iajs-308 87 9 cm-1 cm-1 NOUN iajs-308 87 10 and and CCONJ iajs-308 87 11 appearance appearance NOUN iajs-308 87 12 of of ADP iajs-308 87 13 a a DET iajs-308 87 14 stretching stretch VERB iajs-308 87 15 band band NOUN iajs-308 87 16 at at ADP iajs-308 87 17 ( ( PUNCT iajs-308 87 18 1643 1643 NUM iajs-308 87 19 - - SYM iajs-308 87 20 1640 1640 NUM iajs-308 87 21 ) ) PUNCT iajs-308 87 22 cm-1 cm-1 VERB iajs-308 88 1 due due ADP iajs-308 88 2 to to ADP iajs-308 88 3 ν ν PROPN iajs-308 88 4 c c NOUN iajs-308 88 5 = = NOUN iajs-308 88 6 n n PROPN iajs-308 88 7 of of ADP iajs-308 88 8 isoexaline isoexaline NOUN iajs-308 88 9 ring ring NOUN iajs-308 88 10 ( ( PUNCT iajs-308 88 11 endo endo NOUN iajs-308 88 12 cyclic cyclic NOUN iajs-308 88 13 ) ) PUNCT iajs-308 88 14 and and CCONJ iajs-308 88 15 ν ν X iajs-308 88 16 c c X iajs-308 88 17 - - PUNCT iajs-308 88 18 o o NOUN iajs-308 88 19 of of ADP iajs-308 88 20 isoexaline isoexaline NOUN iajs-308 88 21 ring ring NOUN iajs-308 88 22 between between ADP iajs-308 88 23 ( ( PUNCT iajs-308 88 24 1095 1095 NUM iajs-308 88 25 - - SYM iajs-308 88 26 1070 1070 NUM iajs-308 88 27 ) ) PUNCT iajs-308 88 28 cm-1 cm-1 VERB iajs-308 88 29 . . PUNCT iajs-308 89 1 the the DET iajs-308 89 2 ester ester NOUN iajs-308 89 3 compounds compound VERB iajs-308 89 4 [ [ X iajs-308 89 5 iii]a iii]a PROPN iajs-308 89 6 , , PUNCT iajs-308 89 7 b b PROPN iajs-308 89 8 were be AUX iajs-308 89 9 synthesized synthesize VERB iajs-308 89 10 by by ADP iajs-308 89 11 the the DET iajs-308 89 12 reaction reaction NOUN iajs-308 89 13 of of ADP iajs-308 89 14 compounds compound NOUN iajs-308 90 1 [ [ X iajs-308 90 2 ii]a ii]a NOUN iajs-308 90 3 , , PUNCT iajs-308 90 4 b b NOUN iajs-308 90 5 with with ADP iajs-308 90 6 ethylα ethylα NOUN iajs-308 90 7 - - PUNCT iajs-308 90 8 chloro chloro NOUN iajs-308 90 9 acetate acetate NOUN iajs-308 90 10 in in ADP iajs-308 90 11 fused fuse VERB iajs-308 90 12 sodium sodium NOUN iajs-308 90 13 acetate acetate NOUN iajs-308 90 14 . . PUNCT iajs-308 91 1 the the DET iajs-308 91 2 ftir ftir PROPN iajs-308 91 3 spectra spectra PROPN iajs-308 91 4 of of ADP iajs-308 91 5 compounds compound NOUN iajs-308 91 6 [ [ X iajs-308 91 7 iii]a iii]a PROPN iajs-308 91 8 , , PUNCT iajs-308 91 9 b b PROPN iajs-308 91 10 showed show VERB iajs-308 91 11 a a DET iajs-308 91 12 significant significant ADJ iajs-308 91 13 band band NOUN iajs-308 91 14 at at ADP iajs-308 91 15 1735cm-1 1735cm-1 NUM iajs-308 91 16 which which PRON iajs-308 91 17 could could AUX iajs-308 91 18 be be AUX iajs-308 91 19 attributed attribute VERB iajs-308 91 20 to to ADP iajs-308 91 21 stretching stretch VERB iajs-308 91 22 vibration vibration NOUN iajs-308 91 23 of of ADP iajs-308 91 24 the the DET iajs-308 91 25 carbonyl carbonyl NOUN iajs-308 91 26 of of ADP iajs-308 91 27 ester ester NOUN iajs-308 91 28 group group NOUN iajs-308 91 29 , , PUNCT iajs-308 91 30 together together ADV iajs-308 91 31 with with ADP iajs-308 91 32 disappearance disappearance NOUN iajs-308 91 33 absorption absorption NOUN iajs-308 91 34 band band NOUN iajs-308 91 35 due due ADP iajs-308 91 36 to to ADP iajs-308 91 37 ν ν X iajs-308 91 38 o o ADJ iajs-308 91 39 - - PROPN iajs-308 91 40 h h PROPN iajs-308 91 41 group group NOUN iajs-308 91 42 for for ADP iajs-308 91 43 compound[iii]a compound[iii]a PROPN iajs-308 91 44 , , PUNCT iajs-308 91 45 b b X iajs-308 91 46 .the1hnmr .the1hnmr SYM iajs-308 91 47 spectrum spectrum NOUN iajs-308 91 48 of of ADP iajs-308 91 49 ester ester NOUN iajs-308 91 50 compound compound NOUN iajs-308 92 1 [ [ X iajs-308 92 2 iii]a iii]a PROPN iajs-308 92 3 ( ( PUNCT iajs-308 92 4 in in ADP iajs-308 92 5 dmso dmso NOUN iajs-308 92 6 as as ADP iajs-308 92 7 a a DET iajs-308 92 8 solvent solvent NOUN iajs-308 92 9 ) ) PUNCT iajs-308 92 10 , , PUNCT iajs-308 92 11 figure(1 figure(1 X iajs-308 92 12 ) ) PUNCT iajs-308 92 13 showed show VERB iajs-308 92 14 the the DET iajs-308 92 15 following follow VERB iajs-308 92 16 characteristics characteristic NOUN iajs-308 92 17 chemical chemical ADJ iajs-308 92 18 shifts shift NOUN iajs-308 92 19 : : PUNCT iajs-308 92 20 a a DET iajs-308 92 21 singlet singlet ADJ iajs-308 92 22 signal signal NOUN iajs-308 92 23 at at ADP iajs-308 92 24 δ4.25 δ4.25 PROPN iajs-308 92 25 ppm ppm VERB iajs-308 92 26 for for ADP iajs-308 92 27 two two NUM iajs-308 92 28 protons proton NOUN iajs-308 92 29 of of ADP iajs-308 92 30 och2 och2 PROPN iajs-308 92 31 group group NOUN iajs-308 92 32 while while SCONJ iajs-308 92 33 the the DET iajs-308 92 34 aquaterale aquaterale NOUN iajs-308 92 35 signal signal NOUN iajs-308 92 36 of of ADP iajs-308 92 37 protons proton NOUN iajs-308 92 38 of of ADP iajs-308 92 39 ch2 ch2 PROPN iajs-308 92 40 group group PROPN iajs-308 92 41 appear appear VERB iajs-308 92 42 at at ADP iajs-308 92 43 δ δ PROPN iajs-308 92 44 ( ( PUNCT iajs-308 92 45 3.12 3.12 NUM iajs-308 92 46 - - SYM iajs-308 92 47 3.20 3.20 NUM iajs-308 92 48 ) ) PUNCT iajs-308 92 49 ppm ppm NOUN iajs-308 92 50 , , PUNCT iajs-308 92 51 and and CCONJ iajs-308 92 52 a a DET iajs-308 92 53 triplet triplet NOUN iajs-308 92 54 signal signal NOUN iajs-308 92 55 at at ADP iajs-308 92 56 δ1.79 δ1.79 PROPN iajs-308 92 57 ppm ppm VERB iajs-308 92 58 due due ADP iajs-308 92 59 to to PART iajs-308 92 60 three three NUM iajs-308 92 61 protons proton NOUN iajs-308 92 62 of of ADP iajs-308 92 63 ch3group ch3group NOUN iajs-308 92 64 . . PUNCT iajs-308 93 1 also also ADV iajs-308 93 2 the the DET iajs-308 93 3 spectrum spectrum NOUN iajs-308 93 4 showed show VERB iajs-308 93 5 many many ADJ iajs-308 93 6 signals signal NOUN iajs-308 93 7 in in ADP iajs-308 93 8 the the DET iajs-308 93 9 region region NOUN iajs-308 93 10 δ δ PROPN iajs-308 93 11 ( ( PUNCT iajs-308 93 12 6.79 6.79 NUM iajs-308 93 13 - - SYM iajs-308 93 14 8.04 8.04 NUM iajs-308 93 15 ) ) PUNCT iajs-308 93 16 ppm ppm NOUN iajs-308 93 17 could could AUX iajs-308 93 18 be be AUX iajs-308 93 19 attributed attribute VERB iajs-308 93 20 to to ADP iajs-308 93 21 eight eight NUM iajs-308 93 22 aromatic aromatic ADJ iajs-308 93 23 protons proton NOUN iajs-308 93 24 , , PUNCT iajs-308 93 25 a a DET iajs-308 93 26 triplet triplet NOUN iajs-308 93 27 signal signal NOUN iajs-308 93 28 at at ADP iajs-308 93 29 δ δ PROPN iajs-308 93 30 ( ( PUNCT iajs-308 93 31 3.95 3.95 NUM iajs-308 93 32 - - SYM iajs-308 93 33 4.05 4.05 NUM iajs-308 93 34 ) ) PUNCT iajs-308 93 35 ppm ppm NOUN iajs-308 93 36 and and CCONJ iajs-308 93 37 doublet doublet NOUN iajs-308 93 38 of of ADP iajs-308 93 39 doublet doublet NOUN iajs-308 93 40 at at ADP iajs-308 93 41 δ δ PROPN iajs-308 93 42 ( ( PUNCT iajs-308 93 43 2.953.02 2.953.02 NUM iajs-308 93 44 ) ) PUNCT iajs-308 93 45 ppm ppm NOUN iajs-308 93 46 were be AUX iajs-308 93 47 assigned assign VERB iajs-308 93 48 to to ADP iajs-308 93 49 one one NUM iajs-308 93 50 proton proton NOUN iajs-308 93 51 at at ADP iajs-308 93 52 c-5 c-5 NOUN iajs-308 93 53 and and CCONJ iajs-308 93 54 two two NUM iajs-308 93 55 protons proton NOUN iajs-308 93 56 at at ADP iajs-308 93 57 c-4,respectively c-4,respectively ADV iajs-308 93 58 of of ADP iajs-308 93 59 isoxazoline isoxazoline NOUN iajs-308 93 60 ring ring NOUN iajs-308 93 61 . . PUNCT iajs-308 94 1 the the DET iajs-308 94 2 condensation condensation NOUN iajs-308 94 3 of of ADP iajs-308 94 4 ester ester NOUN iajs-308 94 5 with with ADP iajs-308 94 6 hydrazine hydrazine NOUN iajs-308 94 7 hydrate hydrate NOUN iajs-308 94 8 to to PART iajs-308 94 9 get get VERB iajs-308 94 10 new new ADJ iajs-308 94 11 acid acid NOUN iajs-308 94 12 hydrazides[iv]a hydrazides[iv]a NOUN iajs-308 94 13 , , PUNCT iajs-308 94 14 b. b. PROPN iajs-308 94 15 the the DET iajs-308 94 16 ftir ftir PROPN iajs-308 94 17 spectra spectra PROPN iajs-308 94 18 of of ADP iajs-308 94 19 compounds[iv]a compounds[iv]a NOUN iajs-308 94 20 , , PUNCT iajs-308 94 21 b b PROPN iajs-308 94 22 showed show VERB iajs-308 94 23 a a DET iajs-308 94 24 shift shift NOUN iajs-308 94 25 in in ADP iajs-308 94 26 the the DET iajs-308 94 27 carbonyl carbonyl NOUN iajs-308 94 28 stretching stretch VERB iajs-308 94 29 band band NOUN iajs-308 94 30 to to ADP iajs-308 94 31 ester ester NOUN iajs-308 94 32 group group NOUN iajs-308 94 33 of of ADP iajs-308 94 34 compound[iii]a compound[iii]a PROPN iajs-308 94 35 , , PUNCT iajs-308 94 36 b b PROPN iajs-308 94 37 to to ADP iajs-308 94 38 1645cm-1 1645cm-1 PRON iajs-308 94 39 for for ADP iajs-308 94 40 amide amide NOUN iajs-308 94 41 group group NOUN iajs-308 94 42 of of ADP iajs-308 94 43 hydrazide[iv]a hydrazide[iv]a PROPN iajs-308 94 44 , , PUNCT iajs-308 94 45 b b PROPN iajs-308 94 46 also also ADV iajs-308 94 47 showed show VERB iajs-308 94 48 three three NUM iajs-308 94 49 bands band NOUN iajs-308 94 50 in in ADP iajs-308 94 51 the the DET iajs-308 94 52 range(3334 range(3334 NOUN iajs-308 94 53 - - PUNCT iajs-308 94 54 3115 3115 NUM iajs-308 94 55 ) ) PUNCT iajs-308 94 56 cm-1 cm-1 NOUN iajs-308 94 57 which which PRON iajs-308 94 58 is be AUX iajs-308 94 59 assigned assign VERB iajs-308 94 60 to to ADP iajs-308 94 61 asymmetric asymmetric ADJ iajs-308 94 62 and and CCONJ iajs-308 94 63 symmetric symmetric ADJ iajs-308 94 64 bands band NOUN iajs-308 94 65 of of ADP iajs-308 94 66 nh2and nh2and ADV iajs-308 94 67 nh nh PROPN iajs-308 94 68 groups group NOUN iajs-308 94 69 . . PUNCT iajs-308 95 1 the1hnmr the1hnmr PROPN iajs-308 95 2 spectrum spectrum NOUN iajs-308 95 3 of of ADP iajs-308 95 4 acid acid ADJ iajs-308 95 5 hydrazide[iv]b hydrazide[iv]b NOUN iajs-308 95 6 ( ( PUNCT iajs-308 95 7 in in ADP iajs-308 95 8 dmso dmso NOUN iajs-308 95 9 as as ADP iajs-308 95 10 a a DET iajs-308 95 11 solvent solvent NOUN iajs-308 95 12 ) ) PUNCT iajs-308 95 13 , , PUNCT iajs-308 95 14 figure(2 figure(2 PROPN iajs-308 95 15 ) ) PUNCT iajs-308 95 16 exhibited exhibit VERB iajs-308 95 17 a a DET iajs-308 95 18 sharp sharp ADJ iajs-308 95 19 singlet singlet NOUN iajs-308 95 20 at at ADP iajs-308 95 21 δ4.21 δ4.21 PROPN iajs-308 95 22 ppm ppm NOUN iajs-308 95 23 for for ADP iajs-308 95 24 two two NUM iajs-308 95 25 proton proton NOUN iajs-308 95 26 of of ADP iajs-308 95 27 och2 och2 PROPN iajs-308 95 28 group group NOUN iajs-308 95 29 , , PUNCT iajs-308 95 30 two two NUM iajs-308 95 31 signals signal NOUN iajs-308 95 32 at at ADP iajs-308 95 33 δ3.83 δ3.83 ADV iajs-308 95 34 ppm ppm NOUN iajs-308 95 35 and and CCONJ iajs-308 95 36 δ δ PROPN iajs-308 95 37 4.46 4.46 NUM iajs-308 95 38 ppm ppm NOUN iajs-308 95 39 due due ADP iajs-308 95 40 to to ADP iajs-308 95 41 two two NUM iajs-308 95 42 protons proton NOUN iajs-308 95 43 at at ADP iajs-308 95 44 c-4 c-4 NOUN iajs-308 95 45 and and CCONJ iajs-308 95 46 one one NUM iajs-308 95 47 proton proton NOUN iajs-308 95 48 at at ADP iajs-308 95 49 c-5 c-5 NOUN iajs-308 95 50 , , PUNCT iajs-308 95 51 respectively respectively ADV iajs-308 95 52 of of ADP iajs-308 95 53 isoxazoline isoxazoline NOUN iajs-308 95 54 ring ring NOUN iajs-308 95 55 . . PUNCT iajs-308 96 1 a a DET iajs-308 96 2 broad broad ADJ iajs-308 96 3 signal signal NOUN iajs-308 96 4 at at ADP iajs-308 96 5 δ3.4 δ3.4 NOUN iajs-308 96 6 ppm ppm NOUN iajs-308 96 7 could could AUX iajs-308 96 8 be be AUX iajs-308 96 9 assigned assign VERB iajs-308 96 10 for for ADP iajs-308 96 11 two two NUM iajs-308 96 12 protons proton NOUN iajs-308 96 13 of of ADP iajs-308 96 14 nh2 nh2 NOUN iajs-308 96 15 group group NOUN iajs-308 96 16 and and CCONJ iajs-308 96 17 another another DET iajs-308 96 18 broad broad ADJ iajs-308 96 19 signal signal NOUN iajs-308 96 20 at at ADP iajs-308 96 21 δ11.3 δ11.3 PROPN iajs-308 96 22 ppm ppm NOUN iajs-308 96 23 due due ADP iajs-308 96 24 to to ADP iajs-308 96 25 proton proton NOUN iajs-308 96 26 of of ADP iajs-308 96 27 nh nh PROPN iajs-308 96 28 group group NOUN iajs-308 96 29 . . PUNCT iajs-308 97 1 finaly finaly VERB iajs-308 97 2 many many ADJ iajs-308 97 3 signals signal NOUN iajs-308 97 4 between between ADP iajs-308 97 5 δ δ PROPN iajs-308 97 6 ( ( PUNCT iajs-308 97 7 6.63 6.63 NUM iajs-308 97 8 - - NUM iajs-308 97 9 7.87 7.87 NUM iajs-308 97 10 ) ) PUNCT iajs-308 97 11 ppm ppm NOUN iajs-308 97 12 for for ADP iajs-308 97 13 eight eight NUM iajs-308 97 14 aromatic aromatic ADJ iajs-308 97 15 protons proton NOUN iajs-308 97 16 . . PUNCT iajs-308 98 1 the the DET iajs-308 98 2 new new ADJ iajs-308 98 3 schiff schiff NOUN iajs-308 98 4 bases basis NOUN iajs-308 98 5 compound compound VERB iajs-308 99 1 [ [ X iajs-308 99 2 v]a v]a NOUN iajs-308 99 3 , , PUNCT iajs-308 99 4 b b X iajs-308 99 5 and[vi and[vi NOUN iajs-308 99 6 ] ] PUNCT iajs-308 99 7 a a PRON iajs-308 99 8 , , PUNCT iajs-308 99 9 b b PROPN iajs-308 99 10 were be AUX iajs-308 99 11 synthesized synthesize VERB iajs-308 99 12 by by ADP iajs-308 99 13 the the DET iajs-308 99 14 refluxing refluxing NOUN iajs-308 99 15 of of ADP iajs-308 99 16 compound compound NOUN iajs-308 100 1 [ [ X iajs-308 100 2 iv]a iv]a PROPN iajs-308 100 3 , , PUNCT iajs-308 100 4 b b NOUN iajs-308 100 5 with with ADP iajs-308 100 6 different different ADJ iajs-308 100 7 aromatic aromatic ADJ iajs-308 100 8 aldehydes aldehyde NOUN iajs-308 100 9 in in ADP iajs-308 100 10 benzene benzene NOUN iajs-308 100 11 . . PUNCT iajs-308 101 1 the the DET iajs-308 101 2 compounds compound NOUN iajs-308 101 3 were be AUX iajs-308 101 4 characterized characterize VERB iajs-308 101 5 by by ADP iajs-308 101 6 melting melt VERB iajs-308 101 7 points point NOUN iajs-308 101 8 , , PUNCT iajs-308 101 9 ftir ftir PROPN iajs-308 101 10 spectroscopy spectroscopy NOUN iajs-308 101 11 . . PUNCT iajs-308 102 1 the the DET iajs-308 102 2 characteristic characteristic PROPN iajs-308 102 3 ftir ftir PROPN iajs-308 102 4 absorption absorption NOUN iajs-308 102 5 bands band NOUN iajs-308 102 6 of of ADP iajs-308 102 7 compounds compound NOUN iajs-308 102 8 [ [ X iajs-308 102 9 v]a v]a NOUN iajs-308 102 10 , , PUNCT iajs-308 102 11 b b X iajs-308 102 12 and[vi and[vi NOUN iajs-308 102 13 ] ] PUNCT iajs-308 102 14 a a PRON iajs-308 102 15 , , PUNCT iajs-308 102 16 b b NOUN iajs-308 102 17 as as ADP iajs-308 102 18 figure(3 figure(3 NOUN iajs-308 102 19 ) ) PUNCT iajs-308 102 20 showed show VERB iajs-308 102 21 the the DET iajs-308 102 22 disappearance disappearance NOUN iajs-308 102 23 of of ADP iajs-308 102 24 two two NUM iajs-308 102 25 absorption absorption NOUN iajs-308 102 26 bands band NOUN iajs-308 102 27 due due ADP iajs-308 102 28 to to ADP iajs-308 102 29 nh2 nh2 PROPN iajs-308 102 30 stretching stretch VERB iajs-308 102 31 of of ADP iajs-308 102 32 acid acid NOUN iajs-308 102 33 hydrazide hydrazide ADV iajs-308 102 34 together together ADV iajs-308 102 35 with with ADP iajs-308 102 36 the the DET iajs-308 102 37 appearance appearance NOUN iajs-308 102 38 of of ADP iajs-308 102 39 a a DET iajs-308 102 40 439 439 NUM iajs-308 102 41 | | NOUN iajs-308 102 42 chemistry chemistry NOUN iajs-308 102 43 2014 2014 NUM iajs-308 102 44 ) ) PUNCT iajs-308 102 45 عام عام ADP iajs-308 102 46 3العدد 3العدد NUM iajs-308 102 47 ( ( PUNCT iajs-308 102 48 27مجلة 27مجلة NUM iajs-308 102 49 إبن إبن VERB iajs-308 102 50 الھيثم الھيثم NOUN iajs-308 102 51 للعلوم للعلوم NOUN iajs-308 102 52 الصرفة الصرفة NOUN iajs-308 103 1 و و PRON iajs-308 103 2 التطبيقية التطبيقية ADV iajs-308 103 3 المجلد المجلد VERB iajs-308 103 4 ibn ibn PROPN iajs-308 103 5 al al PROPN iajs-308 103 6 - - PUNCT iajs-308 103 7 haitham haitham PROPN iajs-308 103 8 jour jour X iajs-308 103 9 . . PROPN iajs-308 104 1 for for ADP iajs-308 104 2 pure pure ADJ iajs-308 104 3 & & CCONJ iajs-308 104 4 appl appl PROPN iajs-308 104 5 . . PUNCT iajs-308 105 1 sci sci PROPN iajs-308 105 2 . . PUNCT iajs-308 105 3 vol vol NOUN iajs-308 105 4 . . PROPN iajs-308 106 1 27 27 NUM iajs-308 106 2 ( ( PUNCT iajs-308 106 3 3 3 NUM iajs-308 106 4 ) ) PUNCT iajs-308 106 5 2014 2014 NUM iajs-308 106 6 stretching stretch VERB iajs-308 106 7 bands band NOUN iajs-308 106 8 at at ADP iajs-308 106 9 ( ( PUNCT iajs-308 106 10 1682 1682 NUM iajs-308 106 11 - - SYM iajs-308 106 12 1671)cm-1 1671)cm-1 NUM iajs-308 106 13 assignable assignable ADJ iajs-308 106 14 to to ADP iajs-308 106 15 ν ν NOUN iajs-308 106 16 c c NOUN iajs-308 106 17 = = NOUN iajs-308 106 18 n n NUM iajs-308 106 19 the the DET iajs-308 106 20 characteristics characteristic NOUN iajs-308 106 21 ftir ftir VERB iajs-308 106 22 absorption absorption NOUN iajs-308 106 23 bands band NOUN iajs-308 106 24 of of ADP iajs-308 106 25 new new ADJ iajs-308 106 26 schiff schiff NOUN iajs-308 106 27 bases basis NOUN iajs-308 106 28 [ [ X iajs-308 106 29 v]a v]a NOUN iajs-308 106 30 , , PUNCT iajs-308 106 31 b b NOUN iajs-308 106 32 and and CCONJ iajs-308 106 33 [ [ X iajs-308 106 34 vi vi X iajs-308 106 35 ] ] X iajs-308 106 36 a a PRON iajs-308 106 37 , , PUNCT iajs-308 106 38 b b PROPN iajs-308 106 39 were be AUX iajs-308 106 40 listed list VERB iajs-308 106 41 in in ADP iajs-308 106 42 table table NOUN iajs-308 106 43 3.the 3.the PRON iajs-308 106 44 refluxing refluxing NOUN iajs-308 106 45 hydrazide hydrazide ADV iajs-308 107 1 [ [ X iajs-308 107 2 iv iv X iajs-308 107 3 ] ] PUNCT iajs-308 107 4 with with ADP iajs-308 107 5 acetyl acetyl NOUN iajs-308 107 6 acetone acetone NOUN iajs-308 107 7 led lead VERB iajs-308 107 8 to to PART iajs-308 107 9 form form VERB iajs-308 107 10 new new ADJ iajs-308 107 11 pyrazoles pyrazole NOUN iajs-308 108 1 [ [ X iajs-308 108 2 vii]a vii]a PROPN iajs-308 108 3 , , PUNCT iajs-308 108 4 b b PROPN iajs-308 108 5 .these .these PUNCT iajs-308 108 6 compounds compound NOUN iajs-308 108 7 were be AUX iajs-308 108 8 characterized characterize VERB iajs-308 108 9 by by ADP iajs-308 108 10 melting melt VERB iajs-308 108 11 points point NOUN iajs-308 108 12 and and CCONJ iajs-308 108 13 ftir ftir PROPN iajs-308 108 14 spectroscopy spectroscopy NOUN iajs-308 108 15 . . PUNCT iajs-308 109 1 the the DET iajs-308 109 2 ftir ftir PROPN iajs-308 109 3 spectra spectra PROPN iajs-308 109 4 as as ADP iajs-308 109 5 figure(4 figure(4 PROPN iajs-308 109 6 ) ) PUNCT iajs-308 109 7 showed show VERB iajs-308 109 8 the the DET iajs-308 109 9 disappearance disappearance NOUN iajs-308 109 10 of of ADP iajs-308 109 11 three three NUM iajs-308 109 12 absorption absorption NOUN iajs-308 109 13 bands band NOUN iajs-308 109 14 due due ADP iajs-308 109 15 to to ADP iajs-308 109 16 nh2 nh2 PROPN iajs-308 109 17 and and CCONJ iajs-308 109 18 nh nh NOUN iajs-308 109 19 groups group NOUN iajs-308 109 20 together together ADV iajs-308 109 21 with with ADP iajs-308 109 22 the the DET iajs-308 109 23 appearance appearance NOUN iajs-308 109 24 of of ADP iajs-308 109 25 the the DET iajs-308 109 26 stretching stretch VERB iajs-308 109 27 bands band NOUN iajs-308 109 28 near near ADP iajs-308 109 29 ( ( PUNCT iajs-308 109 30 1645 1645 NUM iajs-308 109 31 ) ) PUNCT iajs-308 109 32 cm-1 cm-1 VERB iajs-308 109 33 assignable assignable ADJ iajs-308 109 34 to to ADP iajs-308 109 35 ν ν NOUN iajs-308 109 36 c c NOUN iajs-308 109 37 = = SYM iajs-308 109 38 n n PRON iajs-308 109 39 group group NOUN iajs-308 109 40 and and CCONJ iajs-308 109 41 1371 1371 NUM iajs-308 109 42 cm-1 cm-1 X iajs-308 109 43 due due ADP iajs-308 109 44 to to ADP iajs-308 109 45 n n CCONJ iajs-308 109 46 - - PUNCT iajs-308 109 47 n n NOUN iajs-308 109 48 for for ADP iajs-308 109 49 pyrazole pyrazole NOUN iajs-308 109 50 ring ring NOUN iajs-308 109 51 .also .also ADV iajs-308 109 52 pyrazoline pyrazoline VERB iajs-308 110 1 [ [ X iajs-308 110 2 viii]a viii]a NOUN iajs-308 110 3 , , PUNCT iajs-308 110 4 b b PROPN iajs-308 110 5 is be AUX iajs-308 110 6 produced produce VERB iajs-308 110 7 from from ADP iajs-308 110 8 the the DET iajs-308 110 9 reaction reaction NOUN iajs-308 110 10 hydrazide hydrazide ADV iajs-308 110 11 with with ADP iajs-308 110 12 ethyl ethyl PROPN iajs-308 110 13 aceto aceto PROPN iajs-308 110 14 acetate acetate PROPN iajs-308 110 15 . . PUNCT iajs-308 111 1 this this DET iajs-308 111 2 compound compound NOUN iajs-308 111 3 is be AUX iajs-308 111 4 identified identify VERB iajs-308 111 5 by by ADP iajs-308 111 6 melting melt VERB iajs-308 111 7 points point NOUN iajs-308 111 8 , , PUNCT iajs-308 111 9 ftir ftir PROPN iajs-308 111 10 spectra spectra PROPN iajs-308 111 11 and and CCONJ iajs-308 111 12 mass mass ADJ iajs-308 111 13 spectroscopy spectroscopy NOUN iajs-308 111 14 .the .the PUNCT iajs-308 111 15 ftir ftir PROPN iajs-308 111 16 spectra spectra PROPN iajs-308 111 17 as as ADP iajs-308 111 18 figure(5 figure(5 VERB iajs-308 111 19 ) ) PUNCT iajs-308 111 20 showed show VERB iajs-308 111 21 the the DET iajs-308 111 22 disappearance disappearance NOUN iajs-308 111 23 of of ADP iajs-308 111 24 three three NUM iajs-308 111 25 absorption absorption NOUN iajs-308 111 26 bands band NOUN iajs-308 111 27 due due ADP iajs-308 111 28 to to ADP iajs-308 111 29 nh2 nh2 PROPN iajs-308 111 30 and and CCONJ iajs-308 111 31 nh nh NOUN iajs-308 111 32 groups group NOUN iajs-308 111 33 together together ADV iajs-308 111 34 with with ADP iajs-308 111 35 the the DET iajs-308 111 36 appearance appearance NOUN iajs-308 111 37 of of ADP iajs-308 111 38 the the DET iajs-308 111 39 a a DET iajs-308 111 40 stretching stretch VERB iajs-308 111 41 band band NOUN iajs-308 111 42 around around ADP iajs-308 111 43 1650 1650 NUM iajs-308 111 44 cm-1 cm-1 NOUN iajs-308 111 45 due due ADP iajs-308 111 46 to to ADP iajs-308 111 47 ν ν PROPN iajs-308 111 48 c c NOUN iajs-308 111 49 = = NOUN iajs-308 111 50 n n PRON iajs-308 111 51 band band NOUN iajs-308 111 52 and and CCONJ iajs-308 111 53 new new ADJ iajs-308 111 54 absorption absorption NOUN iajs-308 111 55 band band NOUN iajs-308 111 56 at at ADP iajs-308 111 57 ( ( PUNCT iajs-308 111 58 1735 1735 NUM iajs-308 111 59 - - SYM iajs-308 111 60 1729)cm-1 1729)cm-1 NUM iajs-308 111 61 due due ADP iajs-308 111 62 to to ADP iajs-308 111 63 c c NOUN iajs-308 111 64 = = NOUN iajs-308 111 65 o o X iajs-308 111 66 ( ( PUNCT iajs-308 111 67 endo endo NOUN iajs-308 111 68 cyclic cyclic NOUN iajs-308 111 69 ) ) PUNCT iajs-308 111 70 . . 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- PUNCT iajs-308 167 80 yl yl NOUN iajs-308 167 81 ] ] PUNCT iajs-308 167 82 phenoxy}acetohydrazide phenoxy}acetohydrazide PROPN iajs-308 167 83 n n NUM iajs-308 167 84 o o NOUN iajs-308 167 85 brch2co brch2co NOUN iajs-308 167 86 o o X iajs-308 167 87 h2nhn h2nhn X iajs-308 167 88 c17h16n3o3br c17h16n3o3br PROPN iajs-308 167 89 120 120 NUM iajs-308 167 90 - - SYM iajs-308 167 91 122 122 NUM iajs-308 167 92 65 65 NUM iajs-308 167 93 pale pale ADJ iajs-308 167 94 green green NOUN iajs-308 167 95 442 442 NUM iajs-308 168 1 | | NOUN iajs-308 168 2 chemistry chemistry NOUN iajs-308 168 3 2014 2014 NUM iajs-308 168 4 ) ) PUNCT iajs-308 168 5 عام عام ADP iajs-308 168 6 3العدد 3العدد NUM iajs-308 168 7 ( ( PUNCT iajs-308 168 8 27مجلة 27مجلة NUM iajs-308 168 9 إبن إبن VERB iajs-308 168 10 الھيثم الھيثم NOUN iajs-308 168 11 للعلوم للعلوم NOUN iajs-308 168 12 الصرفة الصرفة NOUN iajs-308 169 1 و و PRON iajs-308 169 2 التطبيقية التطبيقية ADV iajs-308 169 3 المجلد المجلد VERB iajs-308 169 4 ibn ibn PROPN iajs-308 169 5 al al PROPN iajs-308 169 6 - - PUNCT iajs-308 169 7 haitham haitham PROPN iajs-308 169 8 jour jour X iajs-308 169 9 . . PROPN iajs-308 170 1 for for ADP iajs-308 170 2 pure pure ADJ iajs-308 170 3 & & CCONJ iajs-308 170 4 appl appl PROPN iajs-308 170 5 . . PUNCT iajs-308 171 1 sci sci PROPN iajs-308 171 2 . . PUNCT iajs-308 171 3 vol vol NOUN iajs-308 171 4 . . PROPN iajs-308 172 1 27 27 NUM iajs-308 172 2 ( ( PUNCT iajs-308 172 3 3 3 NUM iajs-308 172 4 ) ) PUNCT iajs-308 172 5 2014 2014 NUM iajs-308 172 6 table table NOUN iajs-308 172 7 no.(2 no.(2 NOUN iajs-308 172 8 ) ) PUNCT iajs-308 172 9 the the DET iajs-308 172 10 physical physical ADJ iajs-308 172 11 properties property NOUN iajs-308 172 12 of of ADP iajs-308 172 13 compounds compound NOUN iajs-308 172 14 [ [ X iajs-308 172 15 v]a v]a NOUN iajs-308 172 16 , , PUNCT iajs-308 172 17 b-[viii]a b-[viii]a NOUN iajs-308 172 18 , , PUNCT iajs-308 172 19 b b X iajs-308 172 20 com com NOUN iajs-308 172 21 . . PUNCT iajs-308 172 22 no no INTJ iajs-308 172 23 . . PUNCT iajs-308 173 1 nomenclature nomenclature ADJ iajs-308 173 2 structural structural ADJ iajs-308 173 3 formula formula NOUN iajs-308 173 4 molecular molecular ADJ iajs-308 173 5 formula formula NOUN iajs-308 173 6 m. m. NOUN iajs-308 173 7 p p PROPN iajs-308 173 8 0c 0c X iajs-308 173 9 yie yie PROPN iajs-308 173 10 ld ld PROPN iajs-308 173 11 % % NOUN iajs-308 173 12 color color NOUN iajs-308 174 1 [ [ X iajs-308 174 2 v]a v]a NOUN iajs-308 174 3 { { PUNCT iajs-308 174 4 4-[3-(4`-bromophenyl 4-[3-(4`-bromophenyl NUM iajs-308 174 5 ) ) PUNCT iajs-308 174 6 4,5 4,5 NUM iajs-308 174 7 - - PUNCT iajs-308 174 8 dihydro dihydro NOUN iajs-308 174 9 - - PUNCT iajs-308 174 10 isoxazol-5 isoxazol-5 NUM iajs-308 174 11 yl]phenoxy}(4``-nitro yl]phenoxy}(4``-nitro NUM iajs-308 174 12 benzylidine)acetic benzylidine)acetic PROPN iajs-308 174 13 hydrazide hydrazide ADJ iajs-308 174 14 . . PUNCT iajs-308 175 1 n n CCONJ iajs-308 175 2 o o NOUN iajs-308 175 3 och2cbr och2cbr NOUN iajs-308 175 4 o o X iajs-308 175 5 nhn nhn PROPN iajs-308 175 6 hc hc PROPN iajs-308 175 7 no2 no2 PROPN iajs-308 175 8 c24h19n4o5br c24h19n4o5br PROPN iajs-308 175 9 288290 288290 NUM iajs-308 175 10 82 82 NUM iajs-308 175 11 brown brown NOUN iajs-308 176 1 [ [ X iajs-308 176 2 v]b v]b X iajs-308 176 3 { { PUNCT iajs-308 176 4 4-[5-(4`-bromophenyl 4-[5-(4`-bromophenyl NUM iajs-308 176 5 ) ) PUNCT iajs-308 176 6 4,5 4,5 NUM iajs-308 176 7 - - PUNCT iajs-308 176 8 dihydro dihydro NOUN iajs-308 176 9 - - PUNCT iajs-308 176 10 isoxazol-3yl]phenoxy}(4``-nitro isoxazol-3yl]phenoxy}(4``-nitro PROPN iajs-308 176 11 benzylidine)acetic benzylidine)acetic PROPN iajs-308 176 12 hydrazide hydrazide ADJ iajs-308 176 13 . . PUNCT iajs-308 177 1 n n CCONJ iajs-308 178 1 o o NOUN iajs-308 178 2 brch2co brch2co NOUN iajs-308 178 3 o o NOUN iajs-308 179 1 = = NOUN iajs-308 179 2 nhno2n nhno2n PROPN iajs-308 179 3 ch ch NOUN iajs-308 179 4 c24h19n4o5br c24h19n4o5br PROPN iajs-308 179 5 276279 276279 NUM iajs-308 179 6 46 46 NUM iajs-308 179 7 yellow yellow ADJ iajs-308 180 1 [ [ X iajs-308 180 2 vi]a vi]a NOUN iajs-308 180 3 { { PUNCT iajs-308 180 4 4-[3-(4`-bromophenyl 4-[3-(4`-bromophenyl PROPN iajs-308 180 5 ) ) PUNCT iajs-308 180 6 4,5 4,5 NUM iajs-308 180 7 - - PUNCT iajs-308 180 8 dihydro dihydro NOUN iajs-308 180 9 - - PUNCT iajs-308 180 10 isoxazol-5 isoxazol-5 NUM iajs-308 180 11 yl]phenoxy}(4``bromobenzylidine yl]phenoxy}(4``bromobenzylidine NOUN iajs-308 180 12 ) ) PUNCT iajs-308 180 13 acetichydrazide acetichydrazide ADV iajs-308 180 14 . . PUNCT iajs-308 181 1 n n CCONJ iajs-308 182 1 o o NOUN iajs-308 182 2 och2cbr och2cbr NOUN iajs-308 182 3 o o X iajs-308 182 4 nhn nhn PROPN iajs-308 182 5 hc hc PROPN iajs-308 182 6 br br PROPN iajs-308 182 7 c24h19 c24h19 VERB iajs-308 182 8 n3o3br2 n3o3br2 PRON iajs-308 182 9 158160 158160 NUM iajs-308 182 10 82 82 NUM iajs-308 182 11 brown brown NOUN iajs-308 183 1 [ [ X iajs-308 183 2 vi]b vi]b NOUN iajs-308 183 3 { { PUNCT iajs-308 183 4 4-[5-(4`-bromophenyl 4-[5-(4`-bromophenyl NUM iajs-308 183 5 ) ) PUNCT iajs-308 183 6 4,5 4,5 NUM iajs-308 183 7 - - PUNCT iajs-308 183 8 dihydro dihydro NOUN iajs-308 183 9 - - PUNCT iajs-308 183 10 isoxazol-3 isoxazol-3 NUM iajs-308 183 11 yl]phenoxy}(4``bromobenzylidine yl]phenoxy}(4``bromobenzylidine NOUN iajs-308 183 12 ) ) PUNCT iajs-308 183 13 acetichydrazide acetichydrazide ADV iajs-308 183 14 . . PUNCT iajs-308 184 1 n n CCONJ iajs-308 184 2 o o NOUN iajs-308 184 3 brch2co brch2co NOUN iajs-308 184 4 o o NOUN iajs-308 185 1 = = NOUN iajs-308 185 2 nhnbr nhnbr ADJ iajs-308 185 3 ch ch NOUN iajs-308 185 4 c24h19 c24h19 VERB iajs-308 185 5 n3o3br2 n3o3br2 PRON iajs-308 185 6 110114 110114 NUM iajs-308 185 7 92 92 NUM iajs-308 185 8 pale pale ADJ iajs-308 185 9 brown brown NOUN iajs-308 186 1 [ [ X iajs-308 186 2 vii]a vii]a PROPN iajs-308 186 3 2-{4-[3-(4`-bromo 2-{4-[3-(4`-bromo NOUN iajs-308 186 4 phenyl phenyl NOUN iajs-308 186 5 ) ) PUNCT iajs-308 186 6 -4,5 -4,5 PROPN iajs-308 186 7 - - PUNCT iajs-308 186 8 dihydroisoxazol-5yl]phenoxy}-1(3,5dimethyl dihydroisoxazol-5yl]phenoxy}-1(3,5dimethyl NOUN iajs-308 186 9 - - PUNCT iajs-308 186 10 pyrazol pyrazol NOUN iajs-308 186 11 -1yl)ethanone -1yl)ethanone NOUN iajs-308 186 12 . . PUNCT iajs-308 187 1 n n CCONJ iajs-308 187 2 o o NOUN iajs-308 187 3 och2cbr och2cbr NOUN iajs-308 187 4 o o NOUN iajs-308 187 5 n n CCONJ iajs-308 187 6 n n PROPN iajs-308 188 1 h3c h3c VERB iajs-308 188 2 ch3 ch3 PROPN iajs-308 188 3 c22h c22h PROPN iajs-308 188 4 20 20 NUM iajs-308 188 5 n3o3br n3o3br PROPN iajs-308 188 6 190192 190192 NUM iajs-308 188 7 43 43 NUM iajs-308 188 8 brown brown NOUN iajs-308 189 1 [ [ X iajs-308 189 2 vii]b vii]b NOUN iajs-308 189 3 2-{4-[5-(4`-bromo 2-{4-[5-(4`-bromo NUM iajs-308 189 4 phenyl phenyl NOUN iajs-308 189 5 ) ) PUNCT iajs-308 189 6 -4,5 -4,5 NOUN iajs-308 189 7 - - PUNCT iajs-308 189 8 dihydro dihydro NOUN iajs-308 189 9 isoxazol-3yl]phenoxy isoxazol-3yl]phenoxy VERB iajs-308 189 10 } } PUNCT iajs-308 189 11 -1(3,5dimethyl -1(3,5dimethyl NOUN iajs-308 189 12 - - PUNCT iajs-308 189 13 pyrazol pyrazol ADJ iajs-308 189 14 -1yl)ethanone -1yl)ethanone NOUN iajs-308 189 15 . . PUNCT iajs-308 190 1 n n CCONJ iajs-308 191 1 o o NOUN iajs-308 191 2 brch2co brch2co NOUN iajs-308 191 3 o o PROPN iajs-308 191 4 nn nn PROPN iajs-308 191 5 h3c h3c PROPN iajs-308 191 6 ch3 ch3 PROPN iajs-308 191 7 c22h c22h PROPN iajs-308 191 8 20 20 NUM iajs-308 191 9 n3o3br n3o3br PROPN iajs-308 191 10 100103 100103 NUM iajs-308 191 11 89 89 NUM iajs-308 191 12 brown brown NOUN iajs-308 191 13 a[viii a[viii X iajs-308 191 14 ] ] X iajs-308 191 15 2(2-{4-[3-(4`-bromo 2(2-{4-[3-(4`-bromo NUM iajs-308 191 16 phenyl)-4,5 phenyl)-4,5 PROPN iajs-308 191 17 - - PUNCT iajs-308 191 18 dihydroisoxazol-5 dihydroisoxazol-5 NUM iajs-308 191 19 - - PUNCT iajs-308 191 20 yl]phenoxy yl]phenoxy PROPN iajs-308 191 21 } } PUNCT iajs-308 191 22 acetyl)-5 acetyl)-5 PROPN iajs-308 191 23 - - PUNCT iajs-308 191 24 methyl methyl NOUN iajs-308 191 25 pyrazolin-3 pyrazolin-3 PROPN iajs-308 191 26 - - PUNCT iajs-308 191 27 one one NUM iajs-308 191 28 n n NOUN iajs-308 191 29 o o NOUN iajs-308 191 30 och2cbr och2cbr NOUN iajs-308 191 31 o o NOUN iajs-308 191 32 n n CCONJ iajs-308 191 33 n n CCONJ iajs-308 191 34 ch3o ch3o ADJ iajs-308 191 35 c21h18 c21h18 NOUN iajs-308 191 36 n3o4br n3o4br ADV iajs-308 191 37 60 60 NUM iajs-308 191 38 - - SYM iajs-308 191 39 62 62 NUM iajs-308 191 40 67 67 NUM iajs-308 191 41 brown brown NOUN iajs-308 191 42 [ [ X iajs-308 191 43 viii]b viii]b NOUN iajs-308 191 44 2(2-{4-[5-(4`-bromo 2(2-{4-[5-(4`-bromo NUM iajs-308 191 45 phenyl)-4,5 phenyl)-4,5 NOUN iajs-308 191 46 - - PUNCT iajs-308 191 47 dihydroisoxazol-3 dihydroisoxazol-3 NOUN iajs-308 191 48 - - PUNCT iajs-308 191 49 yl]phenoxy yl]phenoxy PROPN iajs-308 191 50 } } PUNCT iajs-308 191 51 acetyl)-5 acetyl)-5 PROPN iajs-308 191 52 - - PUNCT iajs-308 191 53 methyl methyl NOUN iajs-308 191 54 pyrazolin-3 pyrazolin-3 PROPN iajs-308 191 55 - - PUNCT iajs-308 191 56 one one NUM iajs-308 191 57 n n NOUN iajs-308 191 58 o o NOUN iajs-308 191 59 brch2co brch2co NOUN iajs-308 191 60 o o PROPN iajs-308 191 61 nn nn PROPN iajs-308 191 62 h3c h3c PROPN iajs-308 191 63 o o PROPN iajs-308 191 64 c21h18 c21h18 ADJ iajs-308 191 65 n3o4br n3o4br ADV iajs-308 191 66 107109 107109 NUM iajs-308 191 67 83 83 NUM iajs-308 191 68 brown brown ADJ iajs-308 191 69 443 443 NUM iajs-308 191 70 | | ADV iajs-308 191 71 chemistry chemistry NOUN iajs-308 191 72 2014 2014 NUM iajs-308 191 73 ) ) PUNCT iajs-308 191 74 عام عام ADP iajs-308 191 75 3العدد 3العدد NUM iajs-308 191 76 ( ( PUNCT iajs-308 191 77 27مجلة 27مجلة NUM iajs-308 191 78 إبن إبن VERB iajs-308 191 79 الھيثم الھيثم NOUN iajs-308 191 80 للعلوم للعلوم NOUN iajs-308 191 81 الصرفة الصرفة NOUN iajs-308 192 1 و و PRON iajs-308 192 2 التطبيقية التطبيقية ADV iajs-308 192 3 المجلد المجلد VERB iajs-308 192 4 ibn ibn PROPN iajs-308 192 5 al al PROPN iajs-308 192 6 - - PUNCT iajs-308 192 7 haitham haitham PROPN iajs-308 192 8 jour jour X iajs-308 192 9 . . 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PROPN iajs-308 227 1 27 27 NUM iajs-308 227 2 ( ( PUNCT iajs-308 227 3 3 3 NUM iajs-308 227 4 ) ) PUNCT iajs-308 227 5 2014 2014 NUM iajs-308 227 6 مشتقة مشتقة ADJ iajs-308 227 7 تحضير تحضير ADJ iajs-308 227 8 و و PRON iajs-308 227 9 تشخيص تشخيص VERB iajs-308 227 10 مركبات مركبات PROPN iajs-308 227 11 قواعد قواعد PROPN iajs-308 227 12 شف شف ADP iajs-308 227 13 و و PRON iajs-308 227 14 بايارازول بايارازول VERB iajs-308 227 15 و و PRON iajs-308 227 16 بايارازولين بايارازولين NOUN iajs-308 227 17 جديدة جديدة NOUN iajs-308 227 18 من من ADP iajs-308 227 19 حامض حامض PROPN iajs-308 227 20 الھيدرازيد الھيدرازيد PROPN iajs-308 227 21 الحاوي الحاوي VERB iajs-308 227 22 على على NOUN iajs-308 227 23 حلقة حلقة PROPN iajs-308 227 24 األيزوكزولين األيزوكزولين NOUN iajs-308 227 25 . . PUNCT iajs-308 228 1 نبراس نبراس PROPN iajs-308 228 2 مظفر مظفر PROPN iajs-308 228 3 جميل جميل NOUN iajs-308 228 4 ضحى ضحى PROPN iajs-308 228 5 فاروق فاروق PROPN iajs-308 228 6 حسين حسين PROPN iajs-308 228 7 جمبد جمبد PROPN iajs-308 228 8 ھرمز ھرمز NOUN iajs-308 228 9 توما توما NOUN iajs-308 228 10 للعلوم للعلوم PROPN iajs-308 228 11 الصرفة الصرفة NOUN iajs-308 228 12 ( ( PUNCT iajs-308 228 13 ابن ابن PROPN iajs-308 228 14 الھيثم)/جامعة الھيثم)/جامعة PROPN iajs-308 228 15 بغداد بغداد PROPN iajs-308 228 16 – – PUNCT iajs-308 228 17 قسم قسم PROPN iajs-308 228 18 الكيمياء الكيمياء PROPN iajs-308 228 19 /كلية /كلية PROPN iajs-308 228 20 التربية التربية PROPN iajs-308 228 21 2014ايلول 2014ايلول PROPN iajs-308 228 22 29,قبل 29,قبل NUM iajs-308 228 23 البحث البحث VERB iajs-308 228 24 في في ADP iajs-308 228 25 : : PUNCT iajs-308 228 26 2014حزيران 2014حزيران NUM iajs-308 228 27 15ستلم 15ستلم NUM iajs-308 228 28 البحث البحث NOUN iajs-308 228 29 : : PUNCT iajs-308 228 30 ا ا PROPN iajs-308 228 31 الخالصة الخالصة PROPN iajs-308 228 32 a a PRON iajs-308 228 33 , , PUNCT iajs-308 228 34 b b PROPN iajs-308 229 1 [ [ X iajs-308 229 2 vii],بايرازول vii],بايرازول X iajs-308 229 3 a a X iajs-308 229 4 , , PUNCT iajs-308 229 5 b[vi]و b[vi]و NOUN iajs-308 229 6 a a NOUN iajs-308 229 7 , , PUNCT iajs-308 229 8 b[v]شف b[v]شف PROPN iajs-308 229 9 تحضير تحضير ADJ iajs-308 229 10 مشتقات مشتقات PROPN iajs-308 229 11 جديدة جديدة NOUN iajs-308 229 12 لقواعد لقواعد PROPN iajs-308 229 13 البحث البحث NOUN iajs-308 229 14 ھذا ھذا VERB iajs-308 229 15 يتضمن يتضمن PROPN iajs-308 229 16 -4ستعمال -4ستعمال PROPN iajs-308 229 17 الجالكون الجالكون PROPN iajs-308 229 18 مادة مادة PROPN iajs-308 229 19 أساسية أساسية NOUN iajs-308 229 20 , , PUNCT iajs-308 229 21 يحضر يحضر PROPN iajs-308 229 22 الجالكون الجالكون PROPN iajs-308 229 23 من من INTJ iajs-308 229 24 تفاعل تفاعل PROPN iajs-308 229 25 باتحتوي باتحتوي PROPN iajs-308 229 26 على على PROPN iajs-308 229 27 وحدةااليزوكزولين وحدةااليزوكزولين PROPN iajs-308 229 28 a a PROPN iajs-308 229 29 , , PUNCT iajs-308 229 30 b[viii]وبايرازولين b[viii]وبايرازولين PROPN iajs-308 229 31 برومو برومو PROPN iajs-308 229 32 بنزالديھايد بنزالديھايد NOUN iajs-308 229 33 في في X iajs-308 229 34 وسط وسط NOUN iajs-308 229 35 -4ھيدروكسي -4ھيدروكسي PROPN iajs-308 229 36 أسيتوفينون أسيتوفينون NOUN iajs-308 229 37 مع مع ADP iajs-308 229 38 4ھيدروكسي 4ھيدروكسي NUM iajs-308 229 39 بنزالديھايد بنزالديھايد NOUN iajs-308 229 40 أوتفاعل أوتفاعل NOUN iajs-308 229 41 -4برومو -4برومو PROPN iajs-308 229 42 أسيتوفينون أسيتوفينون VERB iajs-308 229 43 مع مع VERB iajs-308 229 44 a a PRON iajs-308 229 45 , , PUNCT iajs-308 229 46 [ [ X iajs-308 229 47 ii]مع ii]مع ADJ iajs-308 229 48 ھيدروكسيل ھيدروكسيل ADJ iajs-308 229 49 أمين أمين NOUN iajs-308 229 50 ھايدروكلورايد ھايدروكلورايد NOUN iajs-308 229 51 ليعطي ليعطي NOUN iajs-308 229 52 االيزوكزولين االيزوكزولين X iajs-308 229 53 a a PRON iajs-308 229 54 , , PUNCT iajs-308 229 55 b[i]الجالكون b[i]الجالكون PROPN iajs-308 229 56 . . PUNCT iajs-308 230 1 يتفاعل يتفاعل PROPN iajs-308 230 2 بتفاعل بتفاعل PROPN iajs-308 230 3 كلسين كلسين PROPN iajs-308 230 4 شمدت شمدت PROPN iajs-308 230 5 قاعدي قاعدي PROPN iajs-308 230 6 b b PROPN iajs-308 231 1 الذي الذي PROPN iajs-308 231 2 تمت تمت NOUN iajs-308 231 3 مفاعلتة مفاعلتة NOUN iajs-308 231 4 مع مع PRON iajs-308 231 5 أثيل أثيل ADJ iajs-308 231 6 كلورو كلورو ADJ iajs-308 231 7 أسيتيت أسيتيت NOUN iajs-308 231 8 في في INTJ iajs-308 232 1 وسط وسط INTJ iajs-308 232 2 قاعدي قاعدي PROPN iajs-308 232 3 لنحصل لنحصل PROPN iajs-308 232 4 على على PROPN iajs-308 232 5 مركب مركب PROPN iajs-308 232 6 أستري أستري PROPN iajs-308 232 7 , , PUNCT iajs-308 232 8 a a PRON iajs-308 232 9 , , PUNCT iajs-308 232 10 b[iii b[iii PRON iajs-308 232 11 ] ] X iajs-308 232 12 وحدة وحدة NOUN iajs-308 232 13 تكثيف تكثيف NOUN iajs-308 232 14 األستر األستر VERB iajs-308 232 15 الذي الذي ADJ iajs-308 232 16 يصعد يصعد PROPN iajs-308 232 17 عكسيا عكسيا PROPN iajs-308 232 18 مع مع X iajs-308 232 19 البنزلديھايد البنزلديھايد X iajs-308 232 20 المعوض المعوض PROPN iajs-308 232 21 ليعطي ليعطي NOUN iajs-308 232 22 قواعد قواعد PROPN iajs-308 232 23 a a PRON iajs-308 232 24 , , PUNCT iajs-308 232 25 bv][iالناتج bv][iالناتج PROPN iajs-308 232 26 مع مع PRON iajs-308 233 1 الھايدرازين الھايدرازين PROPN iajs-308 233 2 نحصل نحصل NOUN iajs-308 233 3 على على NOUN iajs-308 233 4 حامض حامض PROPN iajs-308 233 5 الھايدرازايد الھايدرازايد VERB iajs-308 233 6 ومن ومن PROPN iajs-308 233 7 تفاعل تفاعل PROPN iajs-308 233 8 حامض حامض PROPN iajs-308 233 9 الھايدرازايد الھايدرازايد VERB iajs-308 233 10 مع مع PROPN iajs-308 233 11 أستيل أستيل PROPN iajs-308 233 12 أسيتون أسيتون PROPN iajs-308 233 13 أو أو ADP iajs-308 233 14 أثيل أثيل ADV iajs-308 233 15 أسيتو أسيتو VERB iajs-308 233 16 أستيت أستيت PROPN iajs-308 233 17 نحصل نحصل NOUN iajs-308 233 18 على على NOUN iajs-308 233 19 a a PRON iajs-308 233 20 , , PUNCT iajs-308 233 21 b[vi b[vi PROPN iajs-308 233 22 ] ] X iajs-308 233 23 a a PRON iajs-308 233 24 , , PUNCT iajs-308 233 25 b b X iajs-308 234 1 [ [ X iajs-308 234 2 v]شيف v]شيف NOUN iajs-308 234 3 على على NOUN iajs-308 234 4 التوالي التوالي NOUN iajs-308 234 5 .شخصت .شخصت PUNCT iajs-308 234 6 جميع جميع PROPN iajs-308 234 7 المركبات المركبات PROPN iajs-308 234 8 المحضرة المحضرة PROPN iajs-308 234 9 بوساطة بوساطة VERB iajs-308 234 10 قياس قياس PROPN iajs-308 234 11 درجات درجات NOUN iajs-308 234 12 a a DET iajs-308 234 13 , , PUNCT iajs-308 234 14 b[viii]و b[viii]و PROPN iajs-308 234 15 بايارازولين بايارازولين NOUN iajs-308 234 16 a a PRON iajs-308 234 17 , , PUNCT iajs-308 234 18 b[vii]بايارازول b[vii]بايارازول PROPN iajs-308 234 19 ( ( PUNCT iajs-308 234 20 لبعض لبعض PROPN iajs-308 234 21 منھا)h منھا)h PROPN iajs-308 234 22 nmr1و nmr1و NUM iajs-308 234 23 ftirأنصھارھا ftirأنصھارھا NOUN iajs-308 234 24 , , PUNCT iajs-308 234 25 طيف طيف PROPN iajs-308 234 26 يزوكزولين يزوكزولين PROPN iajs-308 234 27 , , PUNCT iajs-308 234 28 البايارازول البايارازول ADJ iajs-308 234 29 , , PUNCT iajs-308 234 30 البايارازوليناأل البايارازوليناأل PROPN iajs-308 234 31 , , PUNCT iajs-308 234 32 قواعدشف قواعدشف NOUN iajs-308 234 33 , , PUNCT iajs-308 234 34 الجالكون الجالكون NOUN iajs-308 234 35 : : PUNCT iajs-308 234 36 المفتاحية المفتاحية NOUN iajs-308 234 37 الكلمات الكلمات VERB iajs-308 234 38     SPACE