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PROPN iajs-52 4 5 29 29 NUM iajs-52 4 6 ( ( PUNCT iajs-52 4 7 1 1 NUM iajs-52 4 8 ) ) SYM iajs-52 4 9 2016 2016 NUM iajs-52 4 10 preperation preperation NOUN iajs-52 4 11 and and CCONJ iajs-52 4 12 characterization characterization NOUN iajs-52 4 13 of of ADP iajs-52 4 14 1 1 NUM iajs-52 4 15 , , PUNCT iajs-52 4 16 3 3 NUM iajs-52 4 17 - - PUNCT iajs-52 4 18 bis bis X iajs-52 4 19 ( ( PUNCT iajs-52 4 20 methylsalicylate5 methylsalicylate5 NOUN iajs-52 4 21 - - PUNCT iajs-52 4 22 yl yl NOUN iajs-52 4 23 diazo diazo NOUN iajs-52 4 24 ) ) PUNCT iajs-52 4 25 benzene benzene NOUN iajs-52 4 26 and and CCONJ iajs-52 4 27 its its PRON iajs-52 4 28 complexes complex NOUN iajs-52 4 29 with with ADP iajs-52 4 30 some some PRON iajs-52 4 31 of of ADP iajs-52 4 32 first first ADJ iajs-52 4 33 period period NOUN iajs-52 4 34 transition transition NOUN iajs-52 4 35 metals metal NOUN iajs-52 4 36 khaula khaula PROPN iajs-52 4 37 m. m. PROPN iajs-52 4 38 sultan sultan PROPN iajs-52 4 39 dept dept PROPN iajs-52 4 40 . . PUNCT iajs-52 5 1 of of ADP iajs-52 5 2 chemistry/ chemistry/ NUM iajs-52 5 3 college college NOUN iajs-52 5 4 of of ADP iajs-52 5 5 education education NOUN iajs-52 5 6 for for ADP iajs-52 5 7 pure pure ADJ iajs-52 5 8 science science NOUN iajs-52 5 9 ( ( PUNCT iajs-52 5 10 ibnal ibnal ADJ iajs-52 5 11 haitham)/ haitham)/ PROPN iajs-52 5 12 university university NOUN iajs-52 5 13 of of ADP iajs-52 5 14 baghdad baghdad PROPN iajs-52 5 15 received receive VERB iajs-52 5 16 in:22 in:22 PROPN iajs-52 5 17 / / SYM iajs-52 5 18 march/2015 march/2015 PROPN iajs-52 5 19 , , PUNCT iajs-52 5 20 accepted accept VERB iajs-52 5 21 in:30 in:30 PROPN iajs-52 5 22 / / SYM iajs-52 5 23 june/2015 june/2015 PROPN iajs-52 5 24 abstract abstract NOUN iajs-52 5 25 in in ADP iajs-52 5 26 this this DET iajs-52 5 27 study study NOUN iajs-52 5 28 azo azo NOUN iajs-52 5 29 dye dye NOUN iajs-52 5 30 was be AUX iajs-52 5 31 prepared prepare VERB iajs-52 5 32 by by ADP iajs-52 5 33 the the DET iajs-52 5 34 reaction reaction NOUN iajs-52 5 35 of of ADP iajs-52 5 36 m m NOUN iajs-52 5 37 - - PUNCT iajs-52 5 38 phenylendidiazonium phenylendidiazonium NOUN iajs-52 5 39 chloride chloride NOUN iajs-52 5 40 with with ADP iajs-52 5 41 methyl methyl NOUN iajs-52 5 42 salicylate salicylate NOUN iajs-52 5 43 , , PUNCT iajs-52 5 44 the the DET iajs-52 5 45 resultant resultant NOUN iajs-52 5 46 compound compound NOUN iajs-52 5 47 was be AUX iajs-52 5 48 used use VERB iajs-52 5 49 as as ADP iajs-52 5 50 a a DET iajs-52 5 51 ligand ligand NOUN iajs-52 5 52 for for ADP iajs-52 5 53 complex complex ADJ iajs-52 5 54 formation formation NOUN iajs-52 5 55 with with ADP iajs-52 5 56 fe+2 fe+2 NUM iajs-52 5 57 , , PUNCT iajs-52 5 58 cu+2 cu+2 NOUN iajs-52 5 59 , , PUNCT iajs-52 5 60 zn+2 zn+2 NUM iajs-52 5 61 , , PUNCT iajs-52 5 62 ni+2 ni+2 NUM iajs-52 5 63 and and CCONJ iajs-52 5 64 co+2 co+2 PROPN iajs-52 5 65 ions ion NOUN iajs-52 5 66 . . PUNCT iajs-52 6 1 the the DET iajs-52 6 2 prepared prepared ADJ iajs-52 6 3 ligand ligand NOUN iajs-52 6 4 was be AUX iajs-52 6 5 characterized characterize VERB iajs-52 6 6 by by ADP iajs-52 6 7 h1nmr h1nmr PROPN iajs-52 6 8 , , PUNCT iajs-52 6 9 uv uv NOUN iajs-52 6 10 - - PUNCT iajs-52 6 11 vis vis X iajs-52 6 12 . . PROPN iajs-52 6 13 , , PUNCT iajs-52 6 14 and and CCONJ iajs-52 6 15 ftir ftir PROPN iajs-52 6 16 spectroscopy spectroscopy PROPN iajs-52 6 17 , , PUNCT iajs-52 6 18 chn chn VERB iajs-52 6 19 analysis analysis NOUN iajs-52 6 20 , , PUNCT iajs-52 6 21 in in ADP iajs-52 6 22 addition addition NOUN iajs-52 6 23 the the DET iajs-52 6 24 complexes complex NOUN iajs-52 6 25 were be AUX iajs-52 6 26 characterized characterize VERB iajs-52 6 27 by by ADP iajs-52 6 28 tga tga PROPN iajs-52 6 29 , , PUNCT iajs-52 6 30 uv uv NOUN iajs-52 6 31 - - PUNCT iajs-52 6 32 vis vis X iajs-52 6 33 . . PROPN iajs-52 6 34 , , PUNCT iajs-52 6 35 ftir ftir NOUN iajs-52 6 36 and and CCONJ iajs-52 6 37 conductivity conductivity NOUN iajs-52 6 38 methods method NOUN iajs-52 6 39 . . PUNCT iajs-52 7 1 the the DET iajs-52 7 2 results result NOUN iajs-52 7 3 indicate indicate VERB iajs-52 7 4 that that SCONJ iajs-52 7 5 the the DET iajs-52 7 6 ligand ligand NOUN iajs-52 7 7 chelated chelate VERB iajs-52 7 8 through through ADP iajs-52 7 9 phenoxy phenoxy ADJ iajs-52 7 10 and and CCONJ iajs-52 7 11 carboxyl carboxyl NOUN iajs-52 7 12 groups group NOUN iajs-52 7 13 as as ADP iajs-52 7 14 a a DET iajs-52 7 15 o4 o4 PROPN iajs-52 7 16 quadra quadra PROPN iajs-52 7 17 dentate dentate PROPN iajs-52 7 18 ligand ligand NOUN iajs-52 7 19 , , PUNCT iajs-52 7 20 the the DET iajs-52 7 21 co co X iajs-52 7 22 complex complex PROPN iajs-52 7 23 complet complet PROPN iajs-52 7 24 its its PRON iajs-52 7 25 hexagon hexagon NOUN iajs-52 7 26 coordination coordination NOUN iajs-52 7 27 by by ADP iajs-52 7 28 bonding bond VERB iajs-52 7 29 with with ADP iajs-52 7 30 chlorine chlorine NOUN iajs-52 7 31 and and CCONJ iajs-52 7 32 the the DET iajs-52 7 33 complex complex ADJ iajs-52 7 34 wouid wouid NOUN iajs-52 7 35 be be AUX iajs-52 7 36 electrolytic electrolytic ADJ iajs-52 7 37 in in ADP iajs-52 7 38 opposite opposite ADJ iajs-52 7 39 with with ADP iajs-52 7 40 rest rest NOUN iajs-52 7 41 complexes complex NOUN iajs-52 7 42 . . PUNCT iajs-52 8 1 key key ADJ iajs-52 8 2 words word NOUN iajs-52 8 3 : : PUNCT iajs-52 8 4 azo azo NOUN iajs-52 8 5 compounds compound NOUN iajs-52 8 6 , , PUNCT iajs-52 8 7 3d 3d NUM iajs-52 8 8 metal metal NOUN iajs-52 8 9 complexes complex NOUN iajs-52 8 10 , , PUNCT iajs-52 8 11 transition transition NOUN iajs-52 8 12 metal metal NOUN iajs-52 8 13 complexes complex NOUN iajs-52 8 14 , , PUNCT iajs-52 8 15 azo azo NOUN iajs-52 8 16 ligands ligand NOUN iajs-52 8 17 114 114 NUM iajs-52 8 18 | | NOUN iajs-52 8 19 chemistry chemistry NOUN iajs-52 8 20 2016 2016 NUM iajs-52 8 21 ) ) PUNCT iajs-52 8 22 عام عام ADP iajs-52 8 23 1العدد 1العدد NUM iajs-52 8 24 ( ( PUNCT iajs-52 8 25 29لمجلد 29لمجلد NUM iajs-52 8 26 ا ا X iajs-52 8 27 مجلة مجلة NOUN iajs-52 8 28 إبن إبن VERB iajs-52 8 29 الهيثم الهيثم ADJ iajs-52 8 30 للعلوم للعلوم NOUN iajs-52 8 31 الصرفة الصرفة NOUN iajs-52 8 32 و و PRON iajs-52 8 33 التطبيقية التطبيقية ADJ iajs-52 8 34 ibn ibn PROPN iajs-52 8 35 al al PROPN iajs-52 8 36 - - PUNCT iajs-52 8 37 haitham haitham PROPN iajs-52 8 38 jour jour X iajs-52 8 39 . . PROPN iajs-52 8 40 for for ADP iajs-52 8 41 pure pure ADJ iajs-52 8 42 & & CCONJ iajs-52 8 43 appl appl PROPN iajs-52 8 44 . . PUNCT iajs-52 9 1 sci sci PROPN iajs-52 9 2 . . PUNCT iajs-52 9 3 vol vol NOUN iajs-52 9 4 . . PROPN iajs-52 9 5 29 29 NUM iajs-52 9 6 ( ( PUNCT iajs-52 9 7 1 1 NUM iajs-52 9 8 ) ) SYM iajs-52 9 9 2016 2016 NUM iajs-52 9 10 introduction introduction NOUN iajs-52 9 11 organic organic ADJ iajs-52 9 12 reagents reagent NOUN iajs-52 9 13 have have VERB iajs-52 9 14 wide wide ADV iajs-52 9 15 spread spread NOUN iajs-52 9 16 and and CCONJ iajs-52 9 17 miscellaneous miscellaneous ADJ iajs-52 9 18 applications application NOUN iajs-52 9 19 due due ADP iajs-52 9 20 to to ADP iajs-52 9 21 its its PRON iajs-52 9 22 stability stability NOUN iajs-52 9 23 and and CCONJ iajs-52 9 24 high high ADJ iajs-52 9 25 speed speed NOUN iajs-52 9 26 of of ADP iajs-52 9 27 reaction reaction NOUN iajs-52 9 28 with with ADP iajs-52 9 29 different different ADJ iajs-52 9 30 metal metal NOUN iajs-52 9 31 ions ion NOUN iajs-52 9 32 [ [ X iajs-52 9 33 1 1 NUM iajs-52 9 34 ] ] PUNCT iajs-52 9 35 , , PUNCT iajs-52 9 36 in in ADP iajs-52 9 37 addition addition NOUN iajs-52 9 38 many many ADJ iajs-52 9 39 of of ADP iajs-52 9 40 them they PRON iajs-52 9 41 have have VERB iajs-52 9 42 a a DET iajs-52 9 43 high high ADJ iajs-52 9 44 selectivity selectivity NOUN iajs-52 9 45 and and CCONJ iajs-52 9 46 sensitivity sensitivity NOUN iajs-52 9 47 which which PRON iajs-52 9 48 draw draw VERB iajs-52 9 49 a a DET iajs-52 9 50 considerable considerable ADJ iajs-52 9 51 attention attention NOUN iajs-52 9 52 . . PUNCT iajs-52 10 1 azo azo PROPN iajs-52 10 2 compounds compound NOUN iajs-52 10 3 are be AUX iajs-52 10 4 one one NUM iajs-52 10 5 of of ADP iajs-52 10 6 the the DET iajs-52 10 7 mostly mostly ADV iajs-52 10 8 important important ADJ iajs-52 10 9 types type NOUN iajs-52 10 10 of of ADP iajs-52 10 11 organic organic ADJ iajs-52 10 12 reagents reagent NOUN iajs-52 10 13 because because SCONJ iajs-52 10 14 azo azo NOUN iajs-52 10 15 bond bond NOUN iajs-52 10 16 can can AUX iajs-52 10 17 act act VERB iajs-52 10 18 as as ADP iajs-52 10 19 coordination coordination NOUN iajs-52 10 20 center center NOUN iajs-52 10 21 usually usually ADV iajs-52 10 22 [ [ X iajs-52 10 23 2,3 2,3 NUM iajs-52 10 24 ] ] PUNCT iajs-52 10 25 but but CCONJ iajs-52 10 26 not not PART iajs-52 10 27 always[4 always[4 NOUN iajs-52 10 28 ] ] PUNCT iajs-52 10 29 , , PUNCT iajs-52 10 30 at at ADP iajs-52 10 31 the the DET iajs-52 10 32 same same ADJ iajs-52 10 33 time time NOUN iajs-52 10 34 azo azo PROPN iajs-52 10 35 group group NOUN iajs-52 10 36 is be AUX iajs-52 10 37 considered consider VERB iajs-52 10 38 as as ADP iajs-52 10 39 a a DET iajs-52 10 40 strong strong ADJ iajs-52 10 41 chromophoric chromophoric NOUN iajs-52 10 42 center center NOUN iajs-52 10 43 in in ADP iajs-52 10 44 these these DET iajs-52 10 45 compounds compound NOUN iajs-52 10 46 [ [ X iajs-52 10 47 5 5 NUM iajs-52 10 48 ] ] PUNCT iajs-52 10 49 . . PUNCT iajs-52 11 1 this this DET iajs-52 11 2 character character NOUN iajs-52 11 3 makes make VERB iajs-52 11 4 the the DET iajs-52 11 5 azo azo NOUN iajs-52 11 6 compounds compound NOUN iajs-52 11 7 play play VERB iajs-52 11 8 a a DET iajs-52 11 9 major major ADJ iajs-52 11 10 rule rule NOUN iajs-52 11 11 in in ADP iajs-52 11 12 qualitative qualitative ADJ iajs-52 11 13 and and CCONJ iajs-52 11 14 quantitative quantitative ADJ iajs-52 11 15 chemical chemical ADJ iajs-52 11 16 analysis analysis NOUN iajs-52 11 17 of of ADP iajs-52 11 18 metal metal NOUN iajs-52 11 19 ions ion NOUN iajs-52 11 20 [ [ X iajs-52 11 21 6 6 NUM iajs-52 11 22 ] ] PUNCT iajs-52 11 23 , , PUNCT iajs-52 11 24 in in ADP iajs-52 11 25 addition addition NOUN iajs-52 11 26 to to ADP iajs-52 11 27 their their PRON iajs-52 11 28 use use NOUN iajs-52 11 29 as as ADP iajs-52 11 30 indicators indicator NOUN iajs-52 11 31 , , PUNCT iajs-52 11 32 in in ADP iajs-52 11 33 industrial industrial ADJ iajs-52 11 34 field field NOUN iajs-52 11 35 azo azo NOUN iajs-52 11 36 compound compound NOUN iajs-52 11 37 used use VERB iajs-52 11 38 from from ADP iajs-52 11 39 long long ADJ iajs-52 11 40 time time NOUN iajs-52 11 41 as as ADP iajs-52 11 42 drugs drug NOUN iajs-52 11 43 and and CCONJ iajs-52 11 44 dyes dye NOUN iajs-52 11 45 , , PUNCT iajs-52 11 46 at at ADP iajs-52 11 47 present present ADJ iajs-52 11 48 they they PRON iajs-52 11 49 have have VERB iajs-52 11 50 a a DET iajs-52 11 51 wide wide ADJ iajs-52 11 52 application application NOUN iajs-52 11 53 in in ADP iajs-52 11 54 printing printing NOUN iajs-52 11 55 , , PUNCT iajs-52 11 56 electronic electronic ADJ iajs-52 11 57 photography photography NOUN iajs-52 11 58 , , PUNCT iajs-52 11 59 color color NOUN iajs-52 11 60 formers former NOUN iajs-52 11 61 , , PUNCT iajs-52 11 62 liquid liquid ADJ iajs-52 11 63 crystal crystal NOUN iajs-52 11 64 display display NOUN iajs-52 11 65 , , PUNCT iajs-52 11 66 laser laser NOUN iajs-52 11 67 technology technology NOUN iajs-52 11 68 , , PUNCT iajs-52 11 69 data data NOUN iajs-52 11 70 storage storage NOUN iajs-52 11 71 , , PUNCT iajs-52 11 72 optical optical ADJ iajs-52 11 73 actuators actuator NOUN iajs-52 11 74 , , PUNCT iajs-52 11 75 photorefractive photorefractive ADJ iajs-52 11 76 media medium NOUN iajs-52 11 77 , , PUNCT iajs-52 11 78 fiber fiber NOUN iajs-52 11 79 dye dye NOUN iajs-52 11 80 , , PUNCT iajs-52 11 81 food food NOUN iajs-52 11 82 and and CCONJ iajs-52 11 83 cosmetics cosmetic NOUN iajs-52 11 84 industry industry NOUN iajs-52 12 1 [ [ X iajs-52 12 2 7 7 NUM iajs-52 12 3 ] ] PUNCT iajs-52 12 4 . . PUNCT iajs-52 13 1 this this DET iajs-52 13 2 study study NOUN iajs-52 13 3 aims aim VERB iajs-52 13 4 to to PART iajs-52 13 5 prepare prepare VERB iajs-52 13 6 a a DET iajs-52 13 7 ligand ligand NOUN iajs-52 13 8 from from ADP iajs-52 13 9 methylsalicylate methylsalicylate NOUN iajs-52 13 10 with with ADP iajs-52 13 11 m m NOUN iajs-52 13 12 - - NOUN iajs-52 13 13 phenelendiamine phenelendiamine NOUN iajs-52 13 14 by by ADP iajs-52 13 15 diazo diazo NOUN iajs-52 13 16 coupling coupling NOUN iajs-52 13 17 and and CCONJ iajs-52 13 18 then then ADV iajs-52 13 19 attach attach VERB iajs-52 13 20 the the DET iajs-52 13 21 prepared prepare VERB iajs-52 13 22 ligand ligand NOUN iajs-52 13 23 with with ADP iajs-52 13 24 ionic ionic ADJ iajs-52 13 25 metals metal NOUN iajs-52 13 26 co co NOUN iajs-52 13 27 and and CCONJ iajs-52 13 28 ni ni PROPN iajs-52 13 29 . . PROPN iajs-52 13 30 experemental experemental ADJ iajs-52 13 31 materials material NOUN iajs-52 13 32 all all DET iajs-52 13 33 chemicals chemical NOUN iajs-52 13 34 used use VERB iajs-52 13 35 in in ADP iajs-52 13 36 this this DET iajs-52 13 37 study study NOUN iajs-52 13 38 were be AUX iajs-52 13 39 analytical analytical ADJ iajs-52 13 40 grade grade NOUN iajs-52 13 41 and and CCONJ iajs-52 13 42 used use VERB iajs-52 13 43 without without ADP iajs-52 13 44 further further ADJ iajs-52 13 45 purification purification NOUN iajs-52 13 46 . . PUNCT iajs-52 14 1 cocl2.6h2o cocl2.6h2o NOUN iajs-52 14 2 , , PUNCT iajs-52 14 3 nicl2.6h2o nicl2.6h2o NOUN iajs-52 14 4 , , PUNCT iajs-52 14 5 feso4.7h2o feso4.7h2o NOUN iajs-52 14 6 , , PUNCT iajs-52 14 7 znso4 znso4 PROPN iajs-52 14 8 and and CCONJ iajs-52 14 9 cuso4.5h2o cuso4.5h2o NOUN iajs-52 14 10 mphenelyendiamine mphenelyendiamine ADJ iajs-52 14 11 hydrochloride hydrochloride NOUN iajs-52 14 12 , , PUNCT iajs-52 14 13 nano2 nano2 PROPN iajs-52 14 14 , , PUNCT iajs-52 14 15 hcl hcl PROPN iajs-52 14 16 , , PUNCT iajs-52 14 17 methylsalicylate methylsalicylate NOUN iajs-52 14 18 , , PUNCT iajs-52 14 19 methanol methanol NOUN iajs-52 14 20 , , PUNCT iajs-52 14 21 ethanol ethanol NOUN iajs-52 14 22 , , PUNCT iajs-52 14 23 dmso dmso NOUN iajs-52 14 24 , , PUNCT iajs-52 14 25 h2so4 h2so4 PROPN iajs-52 14 26 and and CCONJ iajs-52 14 27 koh koh PROPN iajs-52 14 28 instruments instrument NOUN iajs-52 14 29 c.h.n c.h.n VERB iajs-52 14 30 ( ( PUNCT iajs-52 14 31 shimadzu shimadzu ADJ iajs-52 14 32 ) ) PUNCT iajs-52 14 33 elemental elemental ADJ iajs-52 14 34 analyser analyser NOUN iajs-52 14 35 , , PUNCT iajs-52 14 36 h1nmr h1nmr PROPN iajs-52 14 37 ( ( PUNCT iajs-52 14 38 bruker bruker VERB iajs-52 14 39 400mhz 400mhz NUM iajs-52 14 40 the the DET iajs-52 14 41 solvent solvent ADJ iajs-52 14 42 deuterized deuterize VERB iajs-52 14 43 dmso dmso NOUN iajs-52 14 44 ) ) PUNCT iajs-52 14 45 . . PUNCT iajs-52 15 1 ftir ftir PROPN iajs-52 15 2 spectra spectra PROPN iajs-52 15 3 with with ADP iajs-52 15 4 kbr kbr PROPN iajs-52 15 5 disc disc NOUN iajs-52 15 6 in in ADP iajs-52 15 7 the the DET iajs-52 15 8 range range NOUN iajs-52 15 9 ( ( PUNCT iajs-52 15 10 400 400 NUM iajs-52 15 11 - - SYM iajs-52 15 12 4000 4000 NUM iajs-52 15 13 ) ) PUNCT iajs-52 15 14 cm-1 cm-1 VERB iajs-52 15 15 ( ( PUNCT iajs-52 15 16 shimadzu shimadzu ADJ iajs-52 15 17 ftir-8400s ftir-8400s ADJ iajs-52 15 18 ) ) PUNCT iajs-52 15 19 . . PUNCT iajs-52 16 1 electronic electronic ADJ iajs-52 16 2 spectra spectra NOUN iajs-52 16 3 were be AUX iajs-52 16 4 recorded record VERB iajs-52 16 5 on on ADP iajs-52 16 6 ( ( PUNCT iajs-52 16 7 shimadzu shimadzu VERB iajs-52 16 8 uv uv NOUN iajs-52 16 9 - - PUNCT iajs-52 16 10 vis vis X iajs-52 16 11 . . PUNCT iajs-52 16 12 160a 160a NOUN iajs-52 16 13 ) ) PUNCT iajs-52 16 14 spectrophotometer spectrophotometer NOUN iajs-52 16 15 . . PUNCT iajs-52 17 1 conductivty conductivty PROPN iajs-52 17 2 were be AUX iajs-52 17 3 measured measure VERB iajs-52 17 4 for for ADP iajs-52 17 5 0.0001 0.0001 NUM iajs-52 17 6 m m NOUN iajs-52 17 7 of of ADP iajs-52 17 8 complexes complex NOUN iajs-52 17 9 in in ADP iajs-52 17 10 ethanol ethanol NOUN iajs-52 17 11 at at ADP iajs-52 17 12 250c 250c PROPN iajs-52 17 13 using use VERB iajs-52 17 14 ( ( PUNCT iajs-52 17 15 philips philips PROPN iajs-52 17 16 pw pw PROPN iajs-52 17 17 digital digital PROPN iajs-52 17 18 conductometer conductometer NOUN iajs-52 17 19 ) ) PUNCT iajs-52 17 20 . . PUNCT iajs-52 18 1 thermal thermal ADJ iajs-52 18 2 analysis analysis NOUN iajs-52 18 3 was be AUX iajs-52 18 4 done do VERB iajs-52 18 5 by by ADP iajs-52 18 6 dsc dsc NOUN iajs-52 18 7 - - PUNCT iajs-52 18 8 tga tga PROPN iajs-52 18 9 ( ( PUNCT iajs-52 18 10 linseis linseis NOUN iajs-52 18 11 ) ) PUNCT iajs-52 18 12 . . PUNCT iajs-52 19 1 synthesis synthesis NOUN iajs-52 19 2 of of ADP iajs-52 19 3 the the DET iajs-52 19 4 ligand ligand NOUN iajs-52 19 5 the the DET iajs-52 19 6 ligand ligand NOUN iajs-52 19 7 was be AUX iajs-52 19 8 synthesized synthesize VERB iajs-52 19 9 by by ADP iajs-52 19 10 dissolving dissolve VERB iajs-52 19 11 ( ( PUNCT iajs-52 19 12 2 2 NUM iajs-52 19 13 g g NOUN iajs-52 19 14 ) ) PUNCT iajs-52 19 15 of of ADP iajs-52 19 16 m m PROPN iajs-52 19 17 - - ADJ iajs-52 19 18 phenylenediamine phenylenediamine ADJ iajs-52 19 19 hydrochloride hydrochloride NOUN iajs-52 19 20 in in ADP iajs-52 19 21 a a DET iajs-52 19 22 mixture mixture NOUN iajs-52 19 23 of of ADP iajs-52 19 24 ( ( PUNCT iajs-52 19 25 2 2 NUM iajs-52 19 26 ml ml NOUN iajs-52 19 27 ) ) PUNCT iajs-52 19 28 h2so4 h2so4 PROPN iajs-52 19 29 , , PUNCT iajs-52 19 30 10 10 NUM iajs-52 19 31 ml ml NOUN iajs-52 19 32 ethanol ethanol NOUN iajs-52 19 33 , , PUNCT iajs-52 19 34 10 10 NUM iajs-52 19 35 ml ml NOUN iajs-52 19 36 of of ADP iajs-52 19 37 distilled distil VERB iajs-52 19 38 water water NOUN iajs-52 19 39 , , PUNCT iajs-52 19 40 the the DET iajs-52 19 41 mixture mixture NOUN iajs-52 19 42 was be AUX iajs-52 19 43 cooled cool VERB iajs-52 19 44 to to ADP iajs-52 19 45 50c 50c NUM iajs-52 19 46 . . PUNCT iajs-52 20 1 10ml 10ml NOUN iajs-52 20 2 of of ADP iajs-52 20 3 cooled cool VERB iajs-52 20 4 10 10 NUM iajs-52 20 5 % % NOUN iajs-52 20 6 aqueous aqueous ADJ iajs-52 20 7 solution solution NOUN iajs-52 20 8 of of ADP iajs-52 20 9 nano2 nano2 NOUN iajs-52 20 10 was be AUX iajs-52 20 11 added add VERB iajs-52 20 12 dropwise dropwise NOUN iajs-52 20 13 with with ADP iajs-52 20 14 stirring stir VERB iajs-52 20 15 in in ADP iajs-52 20 16 order order NOUN iajs-52 20 17 to to PART iajs-52 20 18 obtain obtain VERB iajs-52 20 19 the the DET iajs-52 20 20 diazonium diazonium NOUN iajs-52 20 21 salt salt NOUN iajs-52 20 22 solution solution NOUN iajs-52 20 23 . . PUNCT iajs-52 21 1 after after ADP iajs-52 21 2 30 30 NUM iajs-52 21 3 minute minute NOUN iajs-52 21 4 the the DET iajs-52 21 5 diazonium diazonium NOUN iajs-52 21 6 solution solution NOUN iajs-52 21 7 was be AUX iajs-52 21 8 slowly slowly ADV iajs-52 21 9 added add VERB iajs-52 21 10 to to ADP iajs-52 21 11 a a DET iajs-52 21 12 cooled cooled ADJ iajs-52 21 13 solution solution NOUN iajs-52 21 14 of of ADP iajs-52 21 15 a a DET iajs-52 21 16 mixture mixture NOUN iajs-52 21 17 of of ADP iajs-52 21 18 ( ( PUNCT iajs-52 21 19 3 3 NUM iajs-52 21 20 g g NOUN iajs-52 21 21 ) ) PUNCT iajs-52 21 22 methylsalicylate methylsalicylate NOUN iajs-52 21 23 and and CCONJ iajs-52 21 24 ( ( PUNCT iajs-52 21 25 1.2 1.2 NUM iajs-52 21 26 g g NOUN iajs-52 21 27 ) ) PUNCT iajs-52 21 28 of of ADP iajs-52 21 29 koh koh PROPN iajs-52 21 30 to to PART iajs-52 21 31 obtain obtain VERB iajs-52 21 32 the the DET iajs-52 21 33 ligand ligand NOUN iajs-52 21 34 , , PUNCT iajs-52 21 35 the the DET iajs-52 21 36 dark dark ADJ iajs-52 21 37 colored colored ADJ iajs-52 21 38 mixture mixture NOUN iajs-52 21 39 containing contain VERB iajs-52 21 40 the the DET iajs-52 21 41 solid solid ADJ iajs-52 21 42 precipitate precipitate NOUN iajs-52 21 43 was be AUX iajs-52 21 44 filtered filter VERB iajs-52 21 45 off off ADP iajs-52 21 46 , , PUNCT iajs-52 21 47 washed wash VERB iajs-52 21 48 then then ADV iajs-52 21 49 re re VERB iajs-52 21 50 - - VERB iajs-52 21 51 crystallized crystallize VERB iajs-52 21 52 with with ADP iajs-52 21 53 70 70 NUM iajs-52 21 54 % % NOUN iajs-52 21 55 ethanol ethanol NOUN iajs-52 21 56 . . PUNCT iajs-52 22 1 the the DET iajs-52 22 2 reaction reaction NOUN iajs-52 22 3 scheme scheme NOUN iajs-52 22 4 is be AUX iajs-52 22 5 : : PUNCT iajs-52 22 6 115 115 NUM iajs-52 22 7 | | ADV iajs-52 22 8 chemistry chemistry NOUN iajs-52 22 9 2016 2016 NUM iajs-52 22 10 ) ) PUNCT iajs-52 22 11 عام عام ADP iajs-52 22 12 1العدد 1العدد NUM iajs-52 22 13 ( ( PUNCT iajs-52 22 14 29لمجلد 29لمجلد NUM iajs-52 22 15 ا ا X iajs-52 22 16 مجلة مجلة NOUN iajs-52 22 17 إبن إبن VERB iajs-52 22 18 الهيثم الهيثم ADJ iajs-52 22 19 للعلوم للعلوم NOUN iajs-52 22 20 الصرفة الصرفة NOUN iajs-52 23 1 و و PRON iajs-52 23 2 التطبيقية التطبيقية ADJ iajs-52 23 3 ibn ibn PROPN iajs-52 23 4 al al PROPN iajs-52 23 5 - - PUNCT iajs-52 23 6 haitham haitham PROPN iajs-52 23 7 jour jour X iajs-52 23 8 . . PROPN iajs-52 23 9 for for ADP iajs-52 23 10 pure pure ADJ iajs-52 23 11 & & CCONJ iajs-52 23 12 appl appl PROPN iajs-52 23 13 . . PUNCT iajs-52 24 1 sci sci PROPN iajs-52 24 2 . . PUNCT iajs-52 24 3 vol vol NOUN iajs-52 24 4 . . PROPN iajs-52 24 5 29 29 NUM iajs-52 24 6 ( ( PUNCT iajs-52 24 7 1 1 NUM iajs-52 24 8 ) ) SYM iajs-52 24 9 2016 2016 NUM iajs-52 24 10 n n CCONJ iajs-52 24 11 2 2 NUM iajs-52 24 12 n n NUM iajs-52 24 13 2 2 NUM iajs-52 24 14 c c NOUN iajs-52 24 15 o o NOUN iajs-52 24 16 2 2 NUM iajs-52 24 17 c c NOUN iajs-52 24 18 h h NOUN iajs-52 24 19 3 3 NUM iajs-52 24 20 o o NOUN iajs-52 24 21 h h NOUN iajs-52 24 22 5 5 NUM iajs-52 25 1 0 0 NUM iajs-52 25 2 c c NOUN iajs-52 25 3 n n CCONJ iajs-52 25 4 n n CCONJ iajs-52 25 5 n n CCONJ iajs-52 25 6 n n NOUN iajs-52 25 7 o o NOUN iajs-52 25 8 h h NOUN iajs-52 26 1 o o NOUN iajs-52 26 2 h h NOUN iajs-52 27 1 c c NOUN iajs-52 27 2 o o NOUN iajs-52 27 3 2 2 NUM iajs-52 27 4 c c NOUN iajs-52 27 5 h h NOUN iajs-52 28 1 3 3 NUM iajs-52 28 2 c c NOUN iajs-52 28 3 o o NOUN iajs-52 28 4 2 2 NUM iajs-52 28 5 c c NOUN iajs-52 28 6 h h NOUN iajs-52 29 1 3 3 NUM iajs-52 29 2 k k NOUN iajs-52 29 3 o o NOUN iajs-52 29 4 h h NOUN iajs-52 30 1 + + CCONJ iajs-52 30 2 2 2 NUM iajs-52 30 3 preparation preparation NOUN iajs-52 30 4 of of ADP iajs-52 30 5 metal metal NOUN iajs-52 30 6 complexes complex NOUN iajs-52 30 7 the the DET iajs-52 30 8 complexes complex NOUN iajs-52 30 9 was be AUX iajs-52 30 10 prepared prepare VERB iajs-52 30 11 by by ADP iajs-52 30 12 the the DET iajs-52 30 13 addition addition NOUN iajs-52 30 14 of of ADP iajs-52 30 15 ( ( PUNCT iajs-52 30 16 10 10 NUM iajs-52 30 17 ml)aqueous ml)aqueous ADJ iajs-52 30 18 solution solution NOUN iajs-52 30 19 of of ADP iajs-52 30 20 the the DET iajs-52 30 21 metal metal NOUN iajs-52 30 22 salt salt NOUN iajs-52 30 23 its its PRON iajs-52 30 24 concentration concentration NOUN iajs-52 30 25 1 1 NUM iajs-52 30 26 m m NOUN iajs-52 30 27 to to ADP iajs-52 30 28 0.01 0.01 NUM iajs-52 30 29 mmole mmole NOUN iajs-52 30 30 of of ADP iajs-52 30 31 the the DET iajs-52 30 32 ligand ligand NOUN iajs-52 30 33 dissolved dissolve VERB iajs-52 30 34 in in ADP iajs-52 30 35 20 20 NUM iajs-52 30 36 ml ml NUM iajs-52 30 37 50 50 NUM iajs-52 30 38 % % NOUN iajs-52 30 39 methanolic methanolic NOUN iajs-52 30 40 aqueous aqueous ADJ iajs-52 30 41 solution solution NOUN iajs-52 30 42 . . PUNCT iajs-52 31 1 the the DET iajs-52 31 2 darck darck PROPN iajs-52 31 3 precipitate precipitate NOUN iajs-52 31 4 was be AUX iajs-52 31 5 settled settle VERB iajs-52 31 6 over over ADP iajs-52 31 7 night night NOUN iajs-52 31 8 then then ADV iajs-52 31 9 recrysallized recrysallize VERB iajs-52 31 10 from from ADP iajs-52 31 11 70 70 NUM iajs-52 31 12 % % NOUN iajs-52 31 13 ethanol ethanol NOUN iajs-52 31 14 . . PUNCT iajs-52 32 1 results result NOUN iajs-52 32 2 and and CCONJ iajs-52 32 3 discussion discussion NOUN iajs-52 32 4 h1nmr h1nmr PRON iajs-52 32 5 figure(18 figure(18 NOUN iajs-52 32 6 ) ) PUNCT iajs-52 32 7 indicates indicate VERB iajs-52 32 8 h1nmr h1nmr NOUN iajs-52 32 9 spectra spectra NOUN iajs-52 32 10 of of ADP iajs-52 32 11 the the DET iajs-52 32 12 ligand ligand NOUN iajs-52 32 13 contain contain VERB iajs-52 32 14 a a DET iajs-52 32 15 singlet singlet ADJ iajs-52 32 16 band band NOUN iajs-52 32 17 at at ADP iajs-52 32 18 2.4 2.4 NUM iajs-52 32 19 ppm ppm NOUN iajs-52 32 20 belong belong VERB iajs-52 32 21 to to ADP iajs-52 32 22 the the DET iajs-52 32 23 methyl methyl NOUN iajs-52 32 24 protons proton NOUN iajs-52 32 25 , , PUNCT iajs-52 32 26 a a DET iajs-52 32 27 multiplet multiplet NOUN iajs-52 32 28 band band NOUN iajs-52 32 29 between between ADP iajs-52 32 30 ( ( PUNCT iajs-52 32 31 6 6 NUM iajs-52 32 32 - - PUNCT iajs-52 32 33 9ppm 9ppm NUM iajs-52 32 34 ) ) PUNCT iajs-52 32 35 belongs belong VERB iajs-52 32 36 to to ADP iajs-52 32 37 the the DET iajs-52 32 38 aromatic aromatic ADJ iajs-52 32 39 protons proton NOUN iajs-52 32 40 , , PUNCT iajs-52 32 41 finally finally ADV iajs-52 32 42 a a DET iajs-52 32 43 singlet singlet ADJ iajs-52 32 44 band band NOUN iajs-52 32 45 at at ADP iajs-52 32 46 ( ( PUNCT iajs-52 32 47 10.512 10.512 NUM iajs-52 32 48 ppm ppm NOUN iajs-52 32 49 ) ) PUNCT iajs-52 32 50 belongs belong VERB iajs-52 32 51 to to ADP iajs-52 32 52 the the DET iajs-52 32 53 phenolic phenolic ADJ iajs-52 32 54 protons proton NOUN iajs-52 32 55 . . PUNCT iajs-52 33 1 electric electric ADJ iajs-52 33 2 conductivity conductivity NOUN iajs-52 33 3 the the DET iajs-52 33 4 measured measure VERB iajs-52 33 5 electric electric ADJ iajs-52 33 6 conductivity conductivity NOUN iajs-52 33 7 for for ADP iajs-52 33 8 the the DET iajs-52 33 9 complexes complex NOUN iajs-52 33 10 in in ADP iajs-52 33 11 dmso dmso ADJ iajs-52 33 12 solvent solvent NOUN iajs-52 33 13 , , PUNCT iajs-52 33 14 the the DET iajs-52 33 15 results result NOUN iajs-52 33 16 indicates indicate VERB iajs-52 33 17 that that SCONJ iajs-52 33 18 the the DET iajs-52 33 19 co co NOUN iajs-52 33 20 complex complex NOUN iajs-52 33 21 is be AUX iajs-52 33 22 charged charge VERB iajs-52 33 23 complex complex ADJ iajs-52 33 24 while while SCONJ iajs-52 33 25 the the DET iajs-52 33 26 other other ADJ iajs-52 33 27 complexes complex NOUN iajs-52 33 28 were be AUX iajs-52 33 29 neutral neutral ADJ iajs-52 33 30 complexes complex NOUN iajs-52 33 31 . . PUNCT iajs-52 34 1 thermal thermal ADJ iajs-52 34 2 analysis analysis NOUN iajs-52 34 3 the the DET iajs-52 34 4 tga tga PROPN iajs-52 34 5 thermograms thermogram NOUN iajs-52 34 6 of of ADP iajs-52 34 7 , , PUNCT iajs-52 34 8 figures(1,2,3,4 figures(1,2,3,4 ADJ iajs-52 34 9 and and CCONJ iajs-52 34 10 5 5 NUM iajs-52 34 11 ) ) PUNCT iajs-52 34 12 co co NOUN iajs-52 34 13 , , PUNCT iajs-52 34 14 fe fe X iajs-52 34 15 , , PUNCT iajs-52 34 16 zn zn PROPN iajs-52 34 17 and and CCONJ iajs-52 34 18 cu cu PROPN iajs-52 34 19 complexes complex NOUN iajs-52 34 20 showing show VERB iajs-52 34 21 two two NUM iajs-52 34 22 conversion conversion NOUN iajs-52 34 23 regions region NOUN iajs-52 34 24 while while SCONJ iajs-52 34 25 in in ADP iajs-52 34 26 ni ni PROPN iajs-52 34 27 complex complex NOUN iajs-52 34 28 they they PRON iajs-52 34 29 were be AUX iajs-52 34 30 three three NUM iajs-52 34 31 . . PUNCT iajs-52 35 1 the the DET iajs-52 35 2 first first ADJ iajs-52 35 3 one one NOUN iajs-52 35 4 is be AUX iajs-52 35 5 represented represent VERB iajs-52 35 6 by by ADP iajs-52 35 7 losing lose VERB iajs-52 35 8 of of ADP iajs-52 35 9 hydration hydration NOUN iajs-52 35 10 water water NOUN iajs-52 35 11 molecules molecule NOUN iajs-52 35 12 in in ADP iajs-52 35 13 all all DET iajs-52 35 14 complexes complex NOUN iajs-52 35 15 [ [ X iajs-52 35 16 8 8 NUM iajs-52 35 17 ] ] PUNCT iajs-52 35 18 . . PUNCT iajs-52 36 1 the the DET iajs-52 36 2 second second ADJ iajs-52 36 3 conversion conversion NOUN iajs-52 36 4 region region NOUN iajs-52 36 5 is be AUX iajs-52 36 6 the the DET iajs-52 36 7 most most ADV iajs-52 36 8 characteristic characteristic ADJ iajs-52 36 9 and and CCONJ iajs-52 36 10 it it PRON iajs-52 36 11 represents represent VERB iajs-52 36 12 the the DET iajs-52 36 13 decomposition decomposition NOUN iajs-52 36 14 point point NOUN iajs-52 36 15 of of ADP iajs-52 36 16 the the DET iajs-52 36 17 complex complex NOUN iajs-52 36 18 , , PUNCT iajs-52 36 19 at at ADP iajs-52 36 20 this this DET iajs-52 36 21 stage stage NOUN iajs-52 36 22 all all DET iajs-52 36 23 the the DET iajs-52 36 24 complexes complex NOUN iajs-52 36 25 lose lose VERB iajs-52 36 26 their their PRON iajs-52 36 27 organic organic ADJ iajs-52 36 28 part part NOUN iajs-52 36 29 leaving leave VERB iajs-52 36 30 the the DET iajs-52 36 31 metal metal NOUN iajs-52 36 32 ( ( PUNCT iajs-52 36 33 ii ii NOUN iajs-52 36 34 ) ) PUNCT iajs-52 36 35 oxide oxide NOUN iajs-52 36 36 , , PUNCT iajs-52 36 37 in in ADP iajs-52 36 38 co co NOUN iajs-52 36 39 complex complex ADJ iajs-52 36 40 case case NOUN iajs-52 36 41 this this PRON iajs-52 36 42 its its PRON iajs-52 36 43 producing produce VERB iajs-52 36 44 oxide oxide NOUN iajs-52 36 45 was be AUX iajs-52 36 46 combined combine VERB iajs-52 36 47 with with ADP iajs-52 36 48 kcl kcl PROPN iajs-52 36 49 while while SCONJ iajs-52 36 50 in in ADP iajs-52 36 51 ni ni PROPN iajs-52 36 52 complex complex NOUN iajs-52 36 53 this this DET iajs-52 36 54 stage stage NOUN iajs-52 36 55 produces produce VERB iajs-52 36 56 nico3 nico3 VERB iajs-52 36 57 which which PRON iajs-52 36 58 is be AUX iajs-52 36 59 further far ADV iajs-52 36 60 decomposed decompose VERB iajs-52 36 61 at at ADP iajs-52 36 62 the the DET iajs-52 36 63 third third ADJ iajs-52 36 64 conversion conversion NOUN iajs-52 36 65 to to ADP iajs-52 36 66 nio nio PROPN iajs-52 36 67 [ [ X iajs-52 36 68 9,10 9,10 NUM iajs-52 36 69 ] ] X iajs-52 36 70 . . PUNCT iajs-52 37 1 116 116 NUM iajs-52 38 1 | | ADV iajs-52 38 2 chemistry chemistry NOUN iajs-52 38 3 2016 2016 NUM iajs-52 38 4 ) ) PUNCT iajs-52 38 5 عام عام ADP iajs-52 38 6 1العدد 1العدد NUM iajs-52 38 7 ( ( PUNCT iajs-52 38 8 29لمجلد 29لمجلد NUM iajs-52 38 9 ا ا X iajs-52 38 10 مجلة مجلة NOUN iajs-52 38 11 إبن إبن VERB iajs-52 38 12 الهيثم الهيثم ADJ iajs-52 38 13 للعلوم للعلوم NOUN iajs-52 38 14 الصرفة الصرفة NOUN iajs-52 39 1 و و PRON iajs-52 39 2 التطبيقية التطبيقية ADJ iajs-52 39 3 ibn ibn PROPN iajs-52 39 4 al al PROPN iajs-52 39 5 - - PUNCT iajs-52 39 6 haitham haitham PROPN iajs-52 39 7 jour jour X iajs-52 39 8 . . PROPN iajs-52 39 9 for for ADP iajs-52 39 10 pure pure ADJ iajs-52 39 11 & & CCONJ iajs-52 39 12 appl appl PROPN iajs-52 39 13 . . PUNCT iajs-52 40 1 sci sci PROPN iajs-52 40 2 . . PUNCT iajs-52 40 3 vol vol NOUN iajs-52 40 4 . . PROPN iajs-52 40 5 29 29 NUM iajs-52 40 6 ( ( PUNCT iajs-52 40 7 1 1 NUM iajs-52 40 8 ) ) PUNCT iajs-52 40 9 2016 2016 NUM iajs-52 41 1 .6 .6 NUM iajs-52 41 2 19 19 NUM iajs-52 41 3 ∆ ∆ PROPN iajs-52 41 4 . . PUNCT iajs-52 42 1 15.5762 15.5762 NUM iajs-52 42 2 ∆ ∆ PROPN iajs-52 42 3 . . PUNCT iajs-52 42 4 . . PUNCT iajs-52 43 1 3.767 3.767 NUM iajs-52 43 2 ∆ ∆ NOUN iajs-52 43 3 . . PUNCT iajs-52 44 1 2.37 2.37 NUM iajs-52 44 2 . . PUNCT iajs-52 45 1 17.7 17.7 NUM iajs-52 45 2 ∆ ∆ X iajs-52 45 3 ~ ~ PUNCT iajs-52 45 4 17.0702 17.0702 NUM iajs-52 45 5 ∆ ∆ X iajs-52 45 6 . . PUNCT iajs-52 46 1 2.1192 2.1192 NUM iajs-52 46 2 . . PUNCT iajs-52 46 3 18 18 NUM iajs-52 46 4 ∆ ∆ NOUN iajs-52 46 5 ~ ~ PUNCT iajs-52 46 6 17.3714 17.3714 NUM iajs-52 46 7 ∆ ∆ X iajs-52 46 8 . . PUNCT iajs-52 47 1 2.9956 2.9956 NUM iajs-52 47 2 . . PUNCT iajs-52 48 1 20.5 20.5 NUM iajs-52 48 2 ∆ ∆ X iajs-52 48 3 ~ ~ PUNCT iajs-52 48 4 19.7814 19.7814 NUM iajs-52 48 5 ∆ ∆ PROPN iajs-52 48 6 . . PUNCT iajs-52 49 1 3.1549 3.1549 NUM iajs-52 49 2 . . PUNCT iajs-52 49 3 4 4 NUM iajs-52 49 4 ∆ ∆ PROPN iajs-52 49 5 3.9010 3.9010 NUM iajs-52 49 6 ∆ ∆ PROPN iajs-52 49 7 . . PUNCT iajs-52 50 1 2 2 NUM iajs-52 50 2 1.3994 1.3994 NUM iajs-52 50 3 ftir ftir NOUN iajs-52 50 4 spectra spectra NOUN iajs-52 50 5 : : PUNCT iajs-52 50 6 figure figure NOUN iajs-52 50 7 ( ( PUNCT iajs-52 50 8 6 6 NUM iajs-52 50 9 ) ) PUNCT iajs-52 50 10 shows show VERB iajs-52 50 11 the the DET iajs-52 50 12 ftir ftir PROPN iajs-52 50 13 spectrum spectrum NOUN iajs-52 50 14 for for ADP iajs-52 50 15 the the DET iajs-52 50 16 ligand ligand NOUN iajs-52 50 17 that that PRON iajs-52 50 18 display display VERB iajs-52 50 19 a a DET iajs-52 50 20 broad broad ADJ iajs-52 50 21 band band NOUN iajs-52 50 22 at at ADP iajs-52 50 23 3381 3381 NUM iajs-52 50 24 cm-1 cm-1 X iajs-52 50 25 belongs belong VERB iajs-52 50 26 to to ADP iajs-52 50 27 the the DET iajs-52 50 28 stretching stretch VERB iajs-52 50 29 vibration vibration NOUN iajs-52 50 30 of of ADP iajs-52 50 31 phenolic phenolic ADJ iajs-52 50 32 oh oh NUM iajs-52 50 33 group group NOUN iajs-52 50 34 . . PUNCT iajs-52 51 1 this this DET iajs-52 51 2 band band NOUN iajs-52 51 3 is be AUX iajs-52 51 4 merged merge VERB iajs-52 51 5 with with ADP iajs-52 51 6 weak weak ADJ iajs-52 51 7 aromatic aromatic ADJ iajs-52 51 8 and and CCONJ iajs-52 51 9 aliphaic aliphaic ADJ iajs-52 51 10 c c X iajs-52 51 11 - - PUNCT iajs-52 51 12 h h NOUN iajs-52 51 13 stretching stretch VERB iajs-52 51 14 bands band NOUN iajs-52 51 15 at at ADP iajs-52 51 16 3067 3067 NUM iajs-52 51 17 and and CCONJ iajs-52 51 18 2953 2953 NUM iajs-52 51 19 cm-1 cm-1 NOUN iajs-52 51 20 respectively respectively ADV iajs-52 51 21 . . PUNCT iajs-52 52 1 a a DET iajs-52 52 2 strong strong ADJ iajs-52 52 3 band band NOUN iajs-52 52 4 at at ADP iajs-52 52 5 1674 1674 NUM iajs-52 52 6 cm-1 cm-1 VERB iajs-52 52 7 is be AUX iajs-52 52 8 due due ADJ iajs-52 52 9 to to ADP iajs-52 52 10 stretching stretch VERB iajs-52 52 11 vibration vibration NOUN iajs-52 52 12 of of ADP iajs-52 52 13 c c NOUN iajs-52 52 14 = = NOUN iajs-52 52 15 o o NOUN iajs-52 52 16 bond bond NOUN iajs-52 52 17 . . PUNCT iajs-52 53 1 the the DET iajs-52 53 2 low low ADJ iajs-52 53 3 value value NOUN iajs-52 53 4 that that PRON iajs-52 53 5 took take VERB iajs-52 53 6 place place NOUN iajs-52 53 7 as as ADP iajs-52 53 8 a a DET iajs-52 53 9 result result NOUN iajs-52 53 10 of of ADP iajs-52 53 11 the the DET iajs-52 53 12 resonance resonance NOUN iajs-52 53 13 with with ADP iajs-52 53 14 aromatic aromatic ADJ iajs-52 53 15 ring ring NOUN iajs-52 53 16 which which PRON iajs-52 53 17 decreases decrease VERB iajs-52 53 18 its its PRON iajs-52 53 19 bond bond NOUN iajs-52 53 20 order order NOUN iajs-52 53 21 and and CCONJ iajs-52 53 22 hence hence ADV iajs-52 53 23 its its PRON iajs-52 53 24 force force NOUN iajs-52 53 25 constant constant ADJ iajs-52 53 26 [ [ X iajs-52 53 27 11 11 NUM iajs-52 53 28 ] ] PUNCT iajs-52 53 29 . . PUNCT iajs-52 54 1 in in ADP iajs-52 54 2 addition addition NOUN iajs-52 54 3 , , PUNCT iajs-52 54 4 the the DET iajs-52 54 5 stretching stretch VERB iajs-52 54 6 vibration vibration NOUN iajs-52 54 7 of of ADP iajs-52 54 8 n n CCONJ iajs-52 54 9 = = NOUN iajs-52 54 10 n n PRON iajs-52 54 11 bond bond NOUN iajs-52 54 12 appears appear VERB iajs-52 54 13 at at ADP iajs-52 54 14 1612 1612 NUM iajs-52 54 15 cm-1 cm-1 NOUN iajs-52 54 16 . . PUNCT iajs-52 55 1 the the DET iajs-52 55 2 co co X iajs-52 55 3 vibration vibration PROPN iajs-52 55 4 frequency frequency NOUN iajs-52 55 5 displays display VERB iajs-52 55 6 two two NUM iajs-52 55 7 values value NOUN iajs-52 55 8 , , PUNCT iajs-52 55 9 the the DET iajs-52 55 10 first first ADJ iajs-52 55 11 one one NUM iajs-52 55 12 at at ADP iajs-52 55 13 1215 1215 NUM iajs-52 55 14 cm-1 cm-1 VERB iajs-52 55 15 belongs belong VERB iajs-52 55 16 to to ADP iajs-52 55 17 phenolic phenolic ADJ iajs-52 55 18 group group NOUN iajs-52 55 19 , , PUNCT iajs-52 55 20 and and CCONJ iajs-52 55 21 the the DET iajs-52 55 22 second second ADJ iajs-52 55 23 one one NOUN iajs-52 55 24 is be AUX iajs-52 55 25 part part NOUN iajs-52 55 26 of of ADP iajs-52 55 27 carboxyl carboxyl NOUN iajs-52 55 28 group group NOUN iajs-52 55 29 . . PUNCT iajs-52 56 1 finally finally ADV iajs-52 56 2 , , PUNCT iajs-52 56 3 there there PRON iajs-52 56 4 is be VERB iajs-52 56 5 a a DET iajs-52 56 6 very very ADV iajs-52 56 7 important important ADJ iajs-52 56 8 absorption absorption NOUN iajs-52 56 9 band band NOUN iajs-52 56 10 at at ADP iajs-52 56 11 847 847 NUM iajs-52 56 12 cm-1 cm-1 X iajs-52 56 13 belongs belong VERB iajs-52 56 14 to to ADP iajs-52 56 15 out out ADP iajs-52 56 16 of of ADP iajs-52 56 17 the the DET iajs-52 56 18 plane plane NOUN iajs-52 56 19 bending bend VERB iajs-52 56 20 vibration vibration NOUN iajs-52 56 21 of of ADP iajs-52 56 22 c c NOUN iajs-52 56 23 - - PUNCT iajs-52 56 24 h h NOUN iajs-52 56 25 aromatic aromatic ADJ iajs-52 56 26 group group NOUN iajs-52 56 27 which which PRON iajs-52 56 28 is be AUX iajs-52 56 29 characteristic characteristic ADJ iajs-52 56 30 to to ADP iajs-52 56 31 the the DET iajs-52 56 32 para para NOUN iajs-52 56 33 substituted substitute VERB iajs-52 56 34 aromatic aromatic ADJ iajs-52 56 35 compounds compound NOUN iajs-52 56 36 [ [ X iajs-52 56 37 12 12 NUM iajs-52 56 38 ] ] PUNCT iajs-52 56 39 . . PUNCT iajs-52 57 1 the the DET iajs-52 57 2 existence existence NOUN iajs-52 57 3 of of ADP iajs-52 57 4 this this DET iajs-52 57 5 group group NOUN iajs-52 57 6 is be AUX iajs-52 57 7 a a DET iajs-52 57 8 good good ADJ iajs-52 57 9 indicator indicator NOUN iajs-52 57 10 to to PART iajs-52 57 11 explain explain VERB iajs-52 57 12 that that SCONJ iajs-52 57 13 : : PUNCT iajs-52 57 14 the the DET iajs-52 57 15 azo azo NOUN iajs-52 57 16 group group NOUN iajs-52 57 17 takes take VERB iajs-52 57 18 the the DET iajs-52 57 19 para para NOUN iajs-52 57 20 position position NOUN iajs-52 57 21 relative relative ADJ iajs-52 57 22 to to ADP iajs-52 57 23 phenolic phenolic ADJ iajs-52 57 24 oh oh INTJ iajs-52 57 25 group group NOUN iajs-52 57 26 and and CCONJ iajs-52 57 27 does do AUX iajs-52 57 28 not not PART iajs-52 57 29 take take VERB iajs-52 57 30 the the DET iajs-52 57 31 ortho ortho PROPN iajs-52 57 32 position position NOUN iajs-52 57 33 . . PUNCT iajs-52 58 1 figures figure NOUN iajs-52 58 2 ( ( PUNCT iajs-52 58 3 7 7 NUM iajs-52 58 4 , , PUNCT iajs-52 58 5 8 8 NUM iajs-52 58 6 , , PUNCT iajs-52 58 7 9 9 NUM iajs-52 58 8 , , PUNCT iajs-52 58 9 10 10 NUM iajs-52 58 10 and and CCONJ iajs-52 58 11 11 11 NUM iajs-52 58 12 ) ) PUNCT iajs-52 58 13 show show VERB iajs-52 58 14 the the DET iajs-52 58 15 ftir ftir PROPN iajs-52 58 16 spectra spectra NOUN iajs-52 58 17 of of ADP iajs-52 58 18 the the DET iajs-52 58 19 complexes complex NOUN iajs-52 58 20 . . PUNCT iajs-52 59 1 in in ADP iajs-52 59 2 complexes complex NOUN iajs-52 59 3 there there PRON iajs-52 59 4 is be VERB iajs-52 59 5 an an DET iajs-52 59 6 existence existence NOUN iajs-52 59 7 of of ADP iajs-52 59 8 weak weak ADJ iajs-52 59 9 broad broad ADJ iajs-52 59 10 band band NOUN iajs-52 59 11 above above ADP iajs-52 59 12 3300 3300 NUM iajs-52 59 13 cm-1 cm-1 NOUN iajs-52 59 14 assigned assign VERB iajs-52 59 15 to to ADP iajs-52 59 16 stretching stretch VERB iajs-52 59 17 vibration vibration NOUN iajs-52 59 18 of of ADP iajs-52 59 19 oh oh NUM iajs-52 59 20 groups group NOUN iajs-52 59 21 in in ADP iajs-52 59 22 hydration hydration NOUN iajs-52 59 23 water water NOUN iajs-52 59 24 molecules molecule NOUN iajs-52 59 25 [ [ X iajs-52 59 26 13 13 NUM iajs-52 59 27 ] ] PUNCT iajs-52 59 28 . . PUNCT iajs-52 60 1 there there PRON iajs-52 60 2 is be VERB iajs-52 60 3 a a DET iajs-52 60 4 great great ADJ iajs-52 60 5 alteration alteration NOUN iajs-52 60 6 in in ADP iajs-52 60 7 the the DET iajs-52 60 8 c c PROPN iajs-52 60 9 = = NOUN iajs-52 60 10 o o NOUN iajs-52 60 11 absorption absorption NOUN iajs-52 60 12 band band NOUN iajs-52 60 13 in in ADP iajs-52 60 14 all all DET iajs-52 60 15 complexes complex NOUN iajs-52 60 16 . . PUNCT iajs-52 61 1 this this PRON iajs-52 61 2 suggests suggest VERB iajs-52 61 3 that that SCONJ iajs-52 61 4 the the DET iajs-52 61 5 carbonyl carbonyl NOUN iajs-52 61 6 group group NOUN iajs-52 61 7 plays play VERB iajs-52 61 8 a a DET iajs-52 61 9 major major ADJ iajs-52 61 10 rule rule NOUN iajs-52 61 11 in in ADP iajs-52 61 12 the the DET iajs-52 61 13 coordination coordination NOUN iajs-52 61 14 with with ADP iajs-52 61 15 the the DET iajs-52 61 16 metal metal NOUN iajs-52 61 17 ion ion NOUN iajs-52 61 18 . . PUNCT iajs-52 62 1 the the DET iajs-52 62 2 stretching stretch VERB iajs-52 62 3 vibration vibration NOUN iajs-52 62 4 of of ADP iajs-52 62 5 azo azo NOUN iajs-52 62 6 group group NOUN iajs-52 62 7 is be AUX iajs-52 62 8 red red ADJ iajs-52 62 9 shifted shift VERB iajs-52 62 10 to to ADP iajs-52 62 11 lower low ADJ iajs-52 62 12 frequency frequency NOUN iajs-52 62 13 . . PUNCT iajs-52 63 1 this this PRON iajs-52 63 2 happens happen VERB iajs-52 63 3 due due ADP iajs-52 63 4 to to ADP iajs-52 63 5 the the DET iajs-52 63 6 change change NOUN iajs-52 63 7 of of ADP iajs-52 63 8 the the DET iajs-52 63 9 resonance resonance NOUN iajs-52 63 10 state state NOUN iajs-52 63 11 in in ADP iajs-52 63 12 the the DET iajs-52 63 13 aromatic aromatic ADJ iajs-52 63 14 ring ring NOUN iajs-52 63 15 that that PRON iajs-52 63 16 which which PRON iajs-52 63 17 caused cause VERB iajs-52 63 18 by by ADP iajs-52 63 19 the the DET iajs-52 63 20 alteration alteration NOUN iajs-52 63 21 in in ADP iajs-52 63 22 its its PRON iajs-52 63 23 electronic electronic ADJ iajs-52 63 24 density density NOUN iajs-52 63 25 through through ADP iajs-52 63 26 the the DET iajs-52 63 27 formation formation NOUN iajs-52 63 28 of of ADP iajs-52 63 29 the the DET iajs-52 63 30 complex complex NOUN iajs-52 63 31 . . PUNCT iajs-52 64 1 the the DET iajs-52 64 2 c c NOUN iajs-52 64 3 - - PUNCT iajs-52 64 4 o o NOUN iajs-52 64 5 bands band NOUN iajs-52 64 6 is be AUX iajs-52 64 7 also also ADV iajs-52 64 8 affected affect VERB iajs-52 64 9 by by ADP iajs-52 64 10 117 117 NUM iajs-52 64 11 | | NOUN iajs-52 64 12 chemistry chemistry NOUN iajs-52 64 13 2016 2016 NUM iajs-52 64 14 ) ) PUNCT iajs-52 64 15 عام عام ADP iajs-52 64 16 1العدد 1العدد NUM iajs-52 64 17 ( ( PUNCT iajs-52 64 18 29لمجلد 29لمجلد NUM iajs-52 64 19 ا ا X iajs-52 65 1 مجلة مجلة NOUN iajs-52 65 2 إبن إبن VERB iajs-52 65 3 الهيثم الهيثم ADJ iajs-52 65 4 للعلوم للعلوم NOUN iajs-52 65 5 الصرفة الصرفة NOUN iajs-52 66 1 و و PRON iajs-52 66 2 التطبيقية التطبيقية ADJ iajs-52 66 3 ibn ibn PROPN iajs-52 66 4 al al PROPN iajs-52 66 5 - - PUNCT iajs-52 66 6 haitham haitham PROPN iajs-52 66 7 jour jour X iajs-52 66 8 . . PROPN iajs-52 66 9 for for ADP iajs-52 66 10 pure pure ADJ iajs-52 66 11 & & CCONJ iajs-52 66 12 appl appl PROPN iajs-52 66 13 . . PUNCT iajs-52 67 1 sci sci PROPN iajs-52 67 2 . . PUNCT iajs-52 67 3 vol vol NOUN iajs-52 67 4 . . PROPN iajs-52 67 5 29 29 NUM iajs-52 67 6 ( ( PUNCT iajs-52 67 7 1 1 NUM iajs-52 67 8 ) ) SYM iajs-52 67 9 2016 2016 NUM iajs-52 67 10 coordination coordination NOUN iajs-52 67 11 we we PRON iajs-52 67 12 believe believe VERB iajs-52 67 13 the the DET iajs-52 67 14 later later ADJ iajs-52 67 15 band band NOUN iajs-52 67 16 that that PRON iajs-52 67 17 belongs belong VERB iajs-52 67 18 to to ADP iajs-52 67 19 phenolic phenolic NOUN iajs-52 67 20 c c NOUN iajs-52 67 21 - - PUNCT iajs-52 67 22 o o NOUN iajs-52 67 23 , , PUNCT iajs-52 67 24 bond bond NOUN iajs-52 67 25 has have AUX iajs-52 67 26 lost lose VERB iajs-52 67 27 its its PRON iajs-52 67 28 h h NOUN iajs-52 67 29 atom atom NOUN iajs-52 67 30 and and CCONJ iajs-52 67 31 coordinated coordinate VERB iajs-52 67 32 with with ADP iajs-52 67 33 metal metal NOUN iajs-52 67 34 ion ion NOUN iajs-52 67 35 to to PART iajs-52 67 36 form form VERB iajs-52 67 37 the the DET iajs-52 67 38 complex complex NOUN iajs-52 67 39 . . PUNCT iajs-52 68 1 as as ADP iajs-52 68 2 a a DET iajs-52 68 3 result result NOUN iajs-52 68 4 of of ADP iajs-52 68 5 this this DET iajs-52 68 6 coordination coordination NOUN iajs-52 68 7 , , PUNCT iajs-52 68 8 we we PRON iajs-52 68 9 observed observe VERB iajs-52 68 10 the the DET iajs-52 68 11 appearance appearance NOUN iajs-52 68 12 of of ADP iajs-52 68 13 a a DET iajs-52 68 14 new new ADJ iajs-52 68 15 band band NOUN iajs-52 68 16 below below ADP iajs-52 68 17 520 520 NUM iajs-52 68 18 cm-1 cm-1 ADV iajs-52 68 19 assigned assign VERB iajs-52 68 20 to to ADP iajs-52 68 21 m m NOUN iajs-52 68 22 - - NOUN iajs-52 68 23 o o NOUN iajs-52 68 24 bond bond NOUN iajs-52 68 25 . . PUNCT iajs-52 69 1 electronic electronic ADJ iajs-52 69 2 spectra spectra NOUN iajs-52 69 3 the the DET iajs-52 69 4 electronic electronic ADJ iajs-52 69 5 spectra spectra NOUN iajs-52 69 6 of of ADP iajs-52 69 7 compounds compound NOUN iajs-52 69 8 in in ADP iajs-52 69 9 dmso dmso ADJ iajs-52 69 10 solvent solvent NOUN iajs-52 69 11 are be AUX iajs-52 69 12 shown show VERB iajs-52 69 13 in in ADP iajs-52 69 14 figures figure NOUN iajs-52 69 15 ( ( PUNCT iajs-52 69 16 12 12 NUM iajs-52 69 17 , , PUNCT iajs-52 69 18 13 13 NUM iajs-52 69 19 , , PUNCT iajs-52 69 20 14 14 NUM iajs-52 69 21 , , PUNCT iajs-52 69 22 15 15 NUM iajs-52 69 23 , , PUNCT iajs-52 69 24 16 16 NUM iajs-52 69 25 and and CCONJ iajs-52 69 26 17 17 NUM iajs-52 69 27 ) ) PUNCT iajs-52 69 28 . . PUNCT iajs-52 70 1 the the DET iajs-52 70 2 ligand ligand NOUN iajs-52 70 3 shows show VERB iajs-52 70 4 strong strong ADJ iajs-52 70 5 absorption absorption NOUN iajs-52 70 6 bands band NOUN iajs-52 70 7 at at ADP iajs-52 70 8 310 310 NUM iajs-52 70 9 , , PUNCT iajs-52 70 10 364 364 NUM iajs-52 70 11 and and CCONJ iajs-52 70 12 457 457 NUM iajs-52 70 13 nm nm NOUN iajs-52 70 14 with with ADP iajs-52 70 15 molar molar ADJ iajs-52 70 16 absorbance absorbance NOUN iajs-52 70 17 5 5 NUM iajs-52 70 18 * * SYM iajs-52 70 19 103 103 NUM iajs-52 70 20 , , PUNCT iajs-52 70 21 5.6 5.6 NUM iajs-52 70 22 * * SYM iajs-52 70 23 103 103 NUM iajs-52 70 24 , , PUNCT iajs-52 70 25 and and CCONJ iajs-52 70 26 4.8 4.8 NUM iajs-52 70 27 * * SYM iajs-52 70 28 103 103 NUM iajs-52 70 29 mole.cm-2 mole.cm-2 NOUN iajs-52 70 30 respectively respectively ADV iajs-52 70 31 . . PUNCT iajs-52 71 1 the the DET iajs-52 71 2 uv uv NOUN iajs-52 71 3 - - PUNCT iajs-52 71 4 vis vis X iajs-52 71 5 . . PUNCT iajs-52 72 1 spectrum spectrum PROPN iajs-52 72 2 indicates indicate VERB iajs-52 72 3 that that SCONJ iajs-52 72 4 the the DET iajs-52 72 5 364 364 NUM iajs-52 72 6 nm nm PRON iajs-52 72 7 band band NOUN iajs-52 72 8 belongs belong VERB iajs-52 72 9 to to ADP iajs-52 72 10 → → SYM iajs-52 72 11 ∗ ∗ NOUN iajs-52 72 12 transition transition NOUN iajs-52 72 13 of of ADP iajs-52 72 14 – – PUNCT iajs-52 72 15 n n CCONJ iajs-52 72 16 = = PROPN iajs-52 72 17 nazo nazo PROPN iajs-52 72 18 chromophoric chromophoric PROPN iajs-52 72 19 group[14 group[14 PROPN iajs-52 72 20 ] ] PUNCT iajs-52 72 21 . . PUNCT iajs-52 73 1 while while SCONJ iajs-52 73 2 the the DET iajs-52 73 3 310 310 NUM iajs-52 73 4 nm nm PRON iajs-52 73 5 band band NOUN iajs-52 73 6 belongs belong VERB iajs-52 73 7 to to ADP iajs-52 73 8 → → SYM iajs-52 73 9 ∗transition ∗transition NOUN iajs-52 73 10 of of ADP iajs-52 73 11 phenolic phenolic NOUN iajs-52 73 12 group[5 group[5 NOUN iajs-52 73 13 ] ] X iajs-52 73 14 , , PUNCT iajs-52 73 15 finally finally ADV iajs-52 73 16 the the DET iajs-52 73 17 shoulder shoulder NOUN iajs-52 73 18 band band NOUN iajs-52 73 19 at at ADP iajs-52 73 20 457 457 NUM iajs-52 73 21 nm nm NOUN iajs-52 73 22 is be AUX iajs-52 73 23 due due ADJ iajs-52 73 24 to to ADP iajs-52 73 25 → → SYM iajs-52 73 26 ∗transition ∗transition NOUN iajs-52 73 27 of of ADP iajs-52 73 28 the the DET iajs-52 73 29 same same ADJ iajs-52 73 30 group[5 group[5 NOUN iajs-52 73 31 ] ] PUNCT iajs-52 73 32 . . PUNCT iajs-52 74 1 the the DET iajs-52 74 2 excited excited ADJ iajs-52 74 3 state state NOUN iajs-52 74 4 in in ADP iajs-52 74 5 the the DET iajs-52 74 6 → → SYM iajs-52 74 7 ∗transition ∗transition NOUN iajs-52 74 8 of of ADP iajs-52 74 9 azo azo PROPN iajs-52 74 10 group group NOUN iajs-52 74 11 plays play VERB iajs-52 74 12 a a DET iajs-52 74 13 major major ADJ iajs-52 74 14 rule rule NOUN iajs-52 74 15 in in ADP iajs-52 74 16 the the DET iajs-52 74 17 conformational conformational ADJ iajs-52 74 18 transformations transformation NOUN iajs-52 74 19 in in ADP iajs-52 74 20 the the DET iajs-52 74 21 ligand ligand NOUN iajs-52 74 22 , , PUNCT iajs-52 74 23 because because SCONJ iajs-52 74 24 it it PRON iajs-52 74 25 acts act VERB iajs-52 74 26 to to PART iajs-52 74 27 ease ease VERB iajs-52 74 28 the the DET iajs-52 74 29 rotation rotation NOUN iajs-52 74 30 n n CCONJ iajs-52 74 31 = = NOUN iajs-52 74 32 n n PRON iajs-52 74 33 bond bond NOUN iajs-52 74 34 . . PUNCT iajs-52 75 1 this this DET iajs-52 75 2 process process NOUN iajs-52 75 3 is be AUX iajs-52 75 4 observed observe VERB iajs-52 75 5 in in ADP iajs-52 75 6 the the DET iajs-52 75 7 cis cis NOUN iajs-52 75 8 - - PUNCT iajs-52 75 9 trans trans ADJ iajs-52 75 10 transformations transformation NOUN iajs-52 75 11 of of ADP iajs-52 75 12 the the DET iajs-52 75 13 azo azo NOUN iajs-52 75 14 compounds compound NOUN iajs-52 75 15 . . PUNCT iajs-52 76 1 in in ADP iajs-52 76 2 the the DET iajs-52 76 3 electronic electronic ADJ iajs-52 76 4 spectra spectra NOUN iajs-52 76 5 of of ADP iajs-52 76 6 the the DET iajs-52 76 7 complexes complex NOUN iajs-52 76 8 , , PUNCT iajs-52 76 9 we we PRON iajs-52 76 10 have have AUX iajs-52 76 11 observed observe VERB iajs-52 76 12 that that SCONJ iajs-52 76 13 the the DET iajs-52 76 14 → → SYM iajs-52 76 15 ∗transition ∗transition NOUN iajs-52 76 16 of of ADP iajs-52 76 17 azo azo NOUN iajs-52 76 18 group group NOUN iajs-52 76 19 is be AUX iajs-52 76 20 not not PART iajs-52 76 21 greatly greatly ADV iajs-52 76 22 affected affect VERB iajs-52 76 23 by by ADP iajs-52 76 24 coordination coordination NOUN iajs-52 76 25 which which PRON iajs-52 76 26 supported support VERB iajs-52 76 27 the the DET iajs-52 76 28 assumption assumption NOUN iajs-52 76 29 that that SCONJ iajs-52 76 30 the the DET iajs-52 76 31 azo azo NOUN iajs-52 76 32 group group NOUN iajs-52 76 33 did do AUX iajs-52 76 34 not not PART iajs-52 76 35 act act VERB iajs-52 76 36 as as ADP iajs-52 76 37 a a DET iajs-52 76 38 coordination coordination NOUN iajs-52 76 39 center center NOUN iajs-52 76 40 with with ADP iajs-52 76 41 metals metal NOUN iajs-52 76 42 . . PUNCT iajs-52 77 1 on on ADP iajs-52 77 2 the the DET iajs-52 77 3 other other ADJ iajs-52 77 4 hand hand NOUN iajs-52 77 5 there there PRON iajs-52 77 6 is be VERB iajs-52 77 7 a a DET iajs-52 77 8 considerable considerable ADJ iajs-52 77 9 alteration alteration NOUN iajs-52 77 10 of of ADP iajs-52 77 11 the the DET iajs-52 77 12 bands band NOUN iajs-52 77 13 that that PRON iajs-52 77 14 belong belong VERB iajs-52 77 15 to to ADP iajs-52 77 16 phenolic phenolic ADJ iajs-52 77 17 group group NOUN iajs-52 77 18 which which PRON iajs-52 77 19 considered consider VERB iajs-52 77 20 as as ADP iajs-52 77 21 evidence evidence NOUN iajs-52 77 22 that that SCONJ iajs-52 77 23 the the DET iajs-52 77 24 phenolic phenolic ADJ iajs-52 77 25 group group NOUN iajs-52 77 26 is be AUX iajs-52 77 27 one one NUM iajs-52 77 28 of of ADP iajs-52 77 29 the the DET iajs-52 77 30 coordination coordination NOUN iajs-52 77 31 centers center NOUN iajs-52 77 32 that that PRON iajs-52 77 33 chelated chelate VERB iajs-52 77 34 with with ADP iajs-52 77 35 metal metal NOUN iajs-52 77 36 ion ion NOUN iajs-52 77 37 . . PUNCT iajs-52 78 1 in in ADP iajs-52 78 2 addition addition NOUN iajs-52 78 3 we we PRON iajs-52 78 4 observed observe VERB iajs-52 78 5 the the DET iajs-52 78 6 increase increase NOUN iajs-52 78 7 of of ADP iajs-52 78 8 the the DET iajs-52 78 9 intensity intensity NOUN iajs-52 78 10 of of ADP iajs-52 78 11 band band NOUN iajs-52 78 12 of of ADP iajs-52 78 13 azo azo PROPN iajs-52 78 14 group group NOUN iajs-52 78 15 , , PUNCT iajs-52 78 16 this this PRON iajs-52 78 17 may may AUX iajs-52 78 18 relate relate VERB iajs-52 78 19 to to ADP iajs-52 78 20 the the DET iajs-52 78 21 fact fact NOUN iajs-52 78 22 that that SCONJ iajs-52 78 23 the the DET iajs-52 78 24 quantum quantum ADJ iajs-52 78 25 probabilistic probabilistic ADJ iajs-52 78 26 transition transition NOUN iajs-52 78 27 of of ADP iajs-52 78 28 this this DET iajs-52 78 29 bond bond NOUN iajs-52 78 30 is be AUX iajs-52 78 31 stabilized stabilize VERB iajs-52 78 32 after after ADP iajs-52 78 33 complex complex ADJ iajs-52 78 34 formation formation NOUN iajs-52 78 35 . . PUNCT iajs-52 79 1 indeed indeed ADV iajs-52 79 2 the the DET iajs-52 79 3 formation formation NOUN iajs-52 79 4 of of ADP iajs-52 79 5 complex complex NOUN iajs-52 79 6 through through ADP iajs-52 79 7 the the DET iajs-52 79 8 contribution contribution NOUN iajs-52 79 9 of of ADP iajs-52 79 10 the the DET iajs-52 79 11 phenoloic phenoloic NOUN iajs-52 79 12 and and CCONJ iajs-52 79 13 the the DET iajs-52 79 14 carbonyl carbonyl NOUN iajs-52 79 15 groups group NOUN iajs-52 79 16 upon upon SCONJ iajs-52 79 17 complexation complexation NOUN iajs-52 79 18 through through ADP iajs-52 79 19 the the DET iajs-52 79 20 chelating chelating NOUN iajs-52 79 21 with with ADP iajs-52 79 22 metal metal NOUN iajs-52 79 23 ions ion NOUN iajs-52 79 24 require require VERB iajs-52 79 25 fold fold NOUN iajs-52 79 26 of of ADP iajs-52 79 27 the the DET iajs-52 79 28 two two NUM iajs-52 79 29 salicylic salicylic ADJ iajs-52 79 30 parts part NOUN iajs-52 79 31 that that PRON iajs-52 79 32 close close ADV iajs-52 79 33 to to ADP iajs-52 79 34 each each DET iajs-52 79 35 other other ADJ iajs-52 79 36 in in ADP iajs-52 79 37 the the DET iajs-52 79 38 ligand ligand NOUN iajs-52 79 39 which which PRON iajs-52 79 40 are be AUX iajs-52 79 41 accomplished accomplish VERB iajs-52 79 42 by by ADP iajs-52 79 43 twisting twisting NOUN iajs-52 79 44 of of ADP iajs-52 79 45 the the DET iajs-52 79 46 – – PUNCT iajs-52 79 47 n n CCONJ iajs-52 79 48 = = NOUN iajs-52 79 49 nbond nbond NOUN iajs-52 79 50 . . PUNCT iajs-52 80 1 the the DET iajs-52 80 2 transition transition NOUN iajs-52 80 3 state state NOUN iajs-52 80 4 of of ADP iajs-52 80 5 this this DET iajs-52 80 6 bond bond NOUN iajs-52 80 7 may may AUX iajs-52 80 8 help help VERB iajs-52 80 9 to to PART iajs-52 80 10 satisfy satisfy VERB iajs-52 80 11 this this DET iajs-52 80 12 condition condition NOUN iajs-52 80 13 . . PUNCT iajs-52 81 1 the the DET iajs-52 81 2 above above ADJ iajs-52 81 3 discussion discussion NOUN iajs-52 81 4 is be AUX iajs-52 81 5 proceeding proceed VERB iajs-52 81 6 for for ADP iajs-52 81 7 all all DET iajs-52 81 8 complexes complex NOUN iajs-52 81 9 as as ADV iajs-52 81 10 well well ADV iajs-52 81 11 . . PUNCT iajs-52 82 1 finally finally ADV iajs-52 82 2 , , PUNCT iajs-52 82 3 the the DET iajs-52 82 4 high high ADJ iajs-52 82 5 values value NOUN iajs-52 82 6 of of ADP iajs-52 82 7 the the DET iajs-52 82 8 molar molar ADJ iajs-52 82 9 absorbance absorbance NOUN iajs-52 82 10 of of ADP iajs-52 82 11 the the DET iajs-52 82 12 ligand ligand ADJ iajs-52 82 13 chromophores chromophore NOUN iajs-52 82 14 act act VERB iajs-52 82 15 to to PART iajs-52 82 16 cover cover VERB iajs-52 82 17 the the DET iajs-52 82 18 d d PROPN iajs-52 82 19 - - PUNCT iajs-52 82 20 d d NOUN iajs-52 82 21 transitions transition NOUN iajs-52 82 22 in in ADP iajs-52 82 23 the the DET iajs-52 82 24 metal metal NOUN iajs-52 82 25 ions ion NOUN iajs-52 82 26 of of ADP iajs-52 82 27 the the DET iajs-52 82 28 complexes complex NOUN iajs-52 82 29 [ [ X iajs-52 82 30 15 15 NUM iajs-52 82 31 ] ] PUNCT iajs-52 82 32 . . 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NOUN iajs-52 148 19 of of ADP iajs-52 148 20 the the DET iajs-52 148 21 co co NOUN iajs-52 148 22 complex complex PROPN iajs-52 148 23 . . PUNCT iajs-52 149 1 figure figure NOUN iajs-52 149 2 ( ( PUNCT iajs-52 149 3 15 15 NUM iajs-52 149 4 ): ): PUNCT iajs-52 149 5 uv uv NOUN iajs-52 149 6 - - PUNCT iajs-52 149 7 vis vis X iajs-52 149 8 . . NOUN iajs-52 149 9 of of ADP iajs-52 149 10 the the DET iajs-52 149 11 cu cu PROPN iajs-52 149 12 complex complex NOUN iajs-52 149 13 . . PUNCT iajs-52 150 1 figure figure NOUN iajs-52 150 2 ( ( PUNCT iajs-52 150 3 16 16 NUM iajs-52 150 4 ) ) PUNCT iajs-52 150 5 : : PUNCT iajs-52 150 6 uv uv NOUN iajs-52 150 7 - - PUNCT iajs-52 150 8 vis vis X iajs-52 150 9 . . NOUN iajs-52 150 10 of of ADP iajs-52 150 11 the the DET iajs-52 150 12 fe fe PROPN iajs-52 150 13 complex complex PROPN iajs-52 150 14 . . PUNCT iajs-52 151 1 figure figure NOUN iajs-52 151 2 ( ( PUNCT iajs-52 151 3 17 17 NUM iajs-52 151 4 ): ): PUNCT iajs-52 151 5 uv uv NOUN iajs-52 151 6 - - PUNCT iajs-52 151 7 vis vis X iajs-52 151 8 . . NOUN iajs-52 151 9 of of ADP iajs-52 151 10 the the DET iajs-52 151 11 zn zn PROPN iajs-52 151 12 complex complex NOUN iajs-52 151 13 . . PUNCT iajs-52 152 1 123 123 NUM iajs-52 152 2 | | ADV iajs-52 152 3 chemistry chemistry NOUN iajs-52 152 4 2016 2016 NUM iajs-52 152 5 ) ) PUNCT iajs-52 152 6 عام عام ADP iajs-52 152 7 1العدد 1العدد NUM iajs-52 152 8 ( ( PUNCT iajs-52 153 1 29لمجلد 29لمجلد NUM iajs-52 153 2 ا ا X iajs-52 153 3 مجلة مجلة NOUN iajs-52 153 4 إبن إبن VERB iajs-52 153 5 الهيثم الهيثم ADJ iajs-52 153 6 للعلوم للعلوم NOUN iajs-52 153 7 الصرفة الصرفة NOUN iajs-52 154 1 و و PRON iajs-52 154 2 التطبيقية التطبيقية ADJ iajs-52 154 3 ibn ibn PROPN iajs-52 154 4 al al PROPN iajs-52 154 5 - - PUNCT iajs-52 154 6 haitham haitham PROPN iajs-52 154 7 jour jour X iajs-52 154 8 . . PROPN iajs-52 154 9 for for ADP iajs-52 154 10 pure pure ADJ iajs-52 154 11 & & CCONJ iajs-52 154 12 appl appl PROPN iajs-52 154 13 . . PUNCT iajs-52 155 1 sci sci PROPN iajs-52 155 2 . . PUNCT iajs-52 155 3 vol vol NOUN iajs-52 155 4 . . PROPN iajs-52 155 5 29 29 NUM iajs-52 155 6 ( ( PUNCT iajs-52 155 7 1 1 NUM iajs-52 155 8 ) ) SYM iajs-52 155 9 2016 2016 NUM iajs-52 155 10 figure figure NOUN iajs-52 155 11 ( ( PUNCT iajs-52 155 12 18 18 NUM iajs-52 155 13 ): ): PUNCT iajs-52 155 14 h1nmr h1nmr NOUN iajs-52 155 15 spectrum spectrum NOUN iajs-52 155 16 of of ADP iajs-52 155 17 the the DET iajs-52 155 18 ligand ligand NOUN iajs-52 155 19 . . PUNCT iajs-52 156 1 figure figure NOUN iajs-52 156 2 ( ( PUNCT iajs-52 156 3 19 19 NUM iajs-52 156 4 ): ): PUNCT iajs-52 156 5 the the DET iajs-52 156 6 general general ADJ iajs-52 156 7 structure structure NOUN iajs-52 156 8 of of ADP iajs-52 156 9 ni ni PROPN iajs-52 156 10 , , PUNCT iajs-52 156 11 cu cu PROPN iajs-52 156 12 , , PUNCT iajs-52 156 13 fe fe X iajs-52 156 14 and and CCONJ iajs-52 156 15 zn zn PROPN iajs-52 156 16 complexes complex NOUN iajs-52 156 17 . . PUNCT iajs-52 157 1 figure figure NOUN iajs-52 157 2 ( ( PUNCT iajs-52 157 3 20 20 NUM iajs-52 157 4 ) ) PUNCT iajs-52 157 5 : : PUNCT iajs-52 157 6 the the DET iajs-52 157 7 general general ADJ iajs-52 157 8 structure structure NOUN iajs-52 157 9 of of ADP iajs-52 157 10 co co NOUN iajs-52 157 11 complex complex PROPN iajs-52 157 12 . . PUNCT iajs-52 158 1 124 124 NUM iajs-52 158 2 | | ADV iajs-52 158 3 chemistry chemistry NOUN iajs-52 158 4 2016 2016 NUM iajs-52 158 5 ) ) PUNCT iajs-52 158 6 عام عام ADP iajs-52 158 7 1العدد 1العدد NUM iajs-52 158 8 ( ( PUNCT iajs-52 159 1 29لمجلد 29لمجلد NUM iajs-52 159 2 ا ا X iajs-52 159 3 مجلة مجلة NOUN iajs-52 159 4 إبن إبن VERB iajs-52 159 5 الهيثم الهيثم ADJ iajs-52 159 6 للعلوم للعلوم NOUN iajs-52 159 7 الصرفة الصرفة NOUN iajs-52 160 1 و و PRON iajs-52 160 2 التطبيقية التطبيقية ADJ iajs-52 160 3 ibn ibn PROPN iajs-52 160 4 al al PROPN iajs-52 160 5 - - PUNCT iajs-52 160 6 haitham haitham PROPN iajs-52 160 7 jour jour X iajs-52 160 8 . . PROPN iajs-52 160 9 for for ADP iajs-52 160 10 pure pure ADJ iajs-52 160 11 & & CCONJ iajs-52 160 12 appl appl PROPN iajs-52 160 13 . . PUNCT iajs-52 161 1 sci sci PROPN iajs-52 161 2 . . PUNCT iajs-52 161 3 vol vol NOUN iajs-52 161 4 . . PROPN iajs-52 161 5 29 29 NUM iajs-52 161 6 ( ( PUNCT iajs-52 161 7 1 1 NUM iajs-52 161 8 ) ) PUNCT iajs-52 161 9 2016 2016 NUM iajs-52 161 10 bis bis X iajs-52 161 11 ( ( PUNCT iajs-52 161 12 methylsalicylate5 methylsalicylate5 NOUN iajs-52 161 13 - - PUNCT iajs-52 161 14 yl yl NOUN iajs-52 161 15 diazo)benzene-1,3تحضير diazo)benzene-1,3تحضير PROPN iajs-52 161 16 و و PRON iajs-52 161 17 تشخيص تشخيص VERB iajs-52 161 18 مع مع ADP iajs-52 161 19 معقداته معقداته PROPN iajs-52 161 20 لبعض لبعض PROPN iajs-52 161 21 عناصر عناصر PROPN iajs-52 161 22 الدورة الدورة PROPN iajs-52 161 23 االنتقالية االنتقالية PROPN iajs-52 161 24 االولى االولى PROPN iajs-52 162 1 خولة خولة NOUN iajs-52 162 2 محمد محمد PROPN iajs-52 162 3 سلطان سلطان PUNCT iajs-52 162 4 بغداد بغداد PROPN iajs-52 162 5 جامعة جامعة PROPN iajs-52 162 6     SPACE iajs-52 162 7 ) ) PUNCT iajs-52 162 8 /ابن /ابن PROPN iajs-52 162 9 الهيثم(كلية الهيثم(كلية NOUN iajs-52 162 10 التربية التربية NOUN iajs-52 162 11 للعلوم للعلوم NOUN iajs-52 162 12 الصرفة الصرفة NOUN iajs-52 162 13 /قسم /قسم X iajs-52 162 14 الكيمياء الكيمياء PROPN iajs-52 163 1 2015حزيران//30قبل 2015حزيران//30قبل NUM iajs-52 163 2 في في NOUN iajs-52 163 3 : : PUNCT iajs-52 163 4 ، ، NOUN iajs-52 163 5 2015اذار//22 2015اذار//22 NUM iajs-52 163 6 : : PUNCT iajs-52 163 7 فيم فيم AUX iajs-52 163 8 لاست لاست PROPN iajs-52 163 9 الخالصة الخالصة PROPN iajs-52 163 10 هذه هذه PROPN iajs-52 163 11 في في PROPN iajs-52 163 12 . . PUNCT iajs-52 163 13 methyl methyl PROPN iajs-52 163 14 salicylateمع salicylateمع PROPN iajs-52 163 15 m m NOUN iajs-52 163 16 - - NOUN iajs-52 163 17 phenylendidiazonium phenylendidiazonium NOUN iajs-52 163 18 chloride chloride NOUN iajs-52 163 19 تم تم NOUN iajs-52 163 20 تحضير تحضير ADJ iajs-52 163 21 صبغة صبغة PROPN iajs-52 163 22 ازو ازو PROPN iajs-52 163 23 من من PROPN iajs-52 163 24 تفاعل تفاعل INTJ iajs-52 163 25 تم تم NOUN iajs-52 163 26 اذ اذ NOUN iajs-52 163 27 co+2ni co+2ni PROPN iajs-52 163 28 , , PUNCT iajs-52 163 29 +2 +2 PROPN iajs-52 163 30 , , PUNCT iajs-52 163 31 zn+2 zn+2 NUM iajs-52 163 32 , , PUNCT iajs-52 163 33 cu+2fe cu+2fe NOUN iajs-52 163 34 , , PUNCT iajs-52 163 35 2+استعمل 2+استعمل NUM iajs-52 163 36 المركب المركب NOUN iajs-52 163 37 المحضر المحضر PROPN iajs-52 163 38 كليكند كليكند NOUN iajs-52 163 39 لتكوين لتكوين NOUN iajs-52 163 40 معقدات معقدات ADJ iajs-52 163 41 تناسقية تناسقية ADV iajs-52 164 1 مع مع INTJ iajs-52 164 2 ايونات ايونات INTJ iajs-52 165 1 الدراسة الدراسة PROPN iajs-52 166 1 ان ان INTJ iajs-52 166 2 فضال فضال PROPN iajs-52 166 3 عن عن PROPN iajs-52 166 4 chn chn PROPN iajs-52 166 5 . . PUNCT iajs-52 167 1 وتحليل وتحليل PROPN iajs-52 167 2 العناصر العناصر NOUN iajs-52 167 3 vis vis X iajs-52 167 4 - - NOUN iajs-52 167 5 uv uv NOUN iajs-52 167 6 . . PUNCT iajs-52 168 1 و و PRON iajs-52 168 2 ftirو ftirو PROPN iajs-52 168 3 nmrh1تشخيص nmrh1تشخيص PROPN iajs-52 168 4 الليكند الليكند PROPN iajs-52 168 5 المحضر المحضر PROPN iajs-52 168 6 مع مع PROPN iajs-52 168 7 معقداته معقداته PROPN iajs-52 168 8 بمطيافيتي بمطيافيتي PROPN iajs-52 168 9 بينت بينت PROPN iajs-52 168 10 النتائج النتائج NOUN iajs-52 168 11 ان ان ADP iajs-52 168 12 الليكند الليكند PROPN iajs-52 168 13 يرتبط يرتبط NOUN iajs-52 168 14 مغ مغ PROPN iajs-52 168 15 اذ اذ NOUN iajs-52 168 16 . . PUNCT iajs-52 169 1 و و PRON iajs-52 169 2 التوصيلية التوصيلية PROPN iajs-52 169 3 .uv .uv PROPN iajs-52 169 4 - - PUNCT iajs-52 169 5 visو visو ADJ iajs-52 169 6 tga tga NOUN iajs-52 169 7 ftirاس ftirاس NOUN iajs-52 169 8 المعقدات المعقدات PROPN iajs-52 169 9 المحضرة المحضرة PROPN iajs-52 169 10 شخصت شخصت PROPN iajs-52 169 11 ايضا ايضا PROPN iajs-52 169 12 بقي بقي NOUN iajs-52 169 13 . . PUNCT iajs-52 170 1 كما كما PROPN iajs-52 170 2 انه انه VERB iajs-52 170 3 في في ADP iajs-52 170 4 معقد معقد X iajs-52 170 5 الكوبلت الكوبلت PROPN iajs-52 170 6 o4االيونات o4االيونات PROPN iajs-52 170 7 من من PROPN iajs-52 170 8 خالل خالل PROPN iajs-52 170 9 مجاميع مجاميع AUX iajs-52 170 10 الفينوكسي الفينوكسي VERB iajs-52 170 11 و و PRON iajs-52 170 12 الكاربونيل الكاربونيل NOUN iajs-52 170 13 و و PRON iajs-52 170 14 بذلك بذلك PROPN iajs-52 170 15 يكون يكون PROPN iajs-52 170 16 ليكند ليكند PROPN iajs-52 170 17 رباعي رباعي PROPN iajs-52 170 18 السن السن NOUN iajs-52 170 19 من من NOUN iajs-52 170 20 نوع نوع NOUN iajs-52 170 21 . . PUNCT iajs-52 171 1 االخرى االخرى PROPN iajs-52 171 2 عقد عقد PROPN iajs-52 171 3 الكتروليتي الكتروليتي PROPN iajs-52 171 4 بخالف بخالف PROPN iajs-52 171 5 المعقداتفانه المعقداتفانه PROPN iajs-52 171 6 يتم يتم PROPN iajs-52 171 7 اكمال اكمال PROPN iajs-52 171 8 التناسق التناسق PROPN iajs-52 171 9 السداسي السداسي PROPN iajs-52 171 10 من من PROPN iajs-52 171 11 خالل خالل PROPN iajs-52 171 12 االرتباط االرتباط PROPN iajs-52 171 13 بالكلور بالكلور VERB iajs-52 171 14 وبذلك وبذلك PROPN iajs-52 171 15 يكون يكون PROPN iajs-52 171 16 هذا هذا NOUN iajs-52 171 17 الم الم NOUN iajs-52 171 18 . . PUNCT iajs-52 172 1 , , PUNCT iajs-52 172 2 ليكندات ليكندات VERB iajs-52 172 3 االزوالعناصر االزوالعناصر NOUN iajs-52 172 4 االنتقالية االنتقالية NOUN iajs-52 172 5 , , PUNCT iajs-52 172 6 معقدات معقدات ADJ iajs-52 172 7 3dمعقدات 3dمعقدات NUM iajs-52 172 8 عناصر عناصر NOUN iajs-52 172 9 مركبات مركبات PROPN iajs-52 172 10 االزو االزو PROPN iajs-52 172 11 , , PUNCT iajs-52 172 12 : : PUNCT iajs-52 172 13 الكلمات الكلمات VERB iajs-52 172 14 المفتاحية المفتاحية VERB