id	sid	tid	token	lemma	pos
iajs-524	1	1	úó‘ój	úó‘ój	PROPN
iajs-524	1	2	�	�	PROPN
iajs-524	1	3	n€a@î@úœäñ€a@‚ï‹»‹€@·ró	n€a@î@úœäñ€a@‚ï‹»‹€@·ró	NUM
iajs-524	1	4	:	:	PUNCT
iajs-524	1	5	a@âig@ú‹	a@âig@ú‹	PROPN
iajs-524	1	6	©	©	PROPN
iajs-524	1	7	@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@ü‹1a26@@öü»€a@i1@‚b«@h2013	@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@ü‹1a26@@öü»€a@i1@‚b«@h2013	PROPN
iajs-524	1	8	ibn	ibn	PROPN
iajs-524	1	9	al	al	PROPN
iajs-524	1	10	-	-	PUNCT
iajs-524	1	11	haitham	haitham	PROPN
iajs-524	1	12	jour	jour	X
iajs-524	1	13	.	.	PROPN
iajs-524	2	1	for	for	ADP
iajs-524	2	2	pure	pure	ADJ
iajs-524	2	3	&	&	CCONJ
iajs-524	2	4	appl	appl	PROPN
iajs-524	2	5	.	.	PUNCT
iajs-524	3	1	sci	sci	PROPN
iajs-524	3	2	.	.	PUNCT
iajs-524	3	3	vol	vol	NOUN
iajs-524	3	4	.	.	PROPN
iajs-524	4	1	26	26	NUM
iajs-524	4	2	(	(	PUNCT
iajs-524	4	3	1	1	NUM
iajs-524	4	4	)	)	PUNCT
iajs-524	4	5	2013	2013	NUM
iajs-524	4	6	synthesis	synthesis	NOUN
iajs-524	4	7	and	and	CCONJ
iajs-524	4	8	characterization	characterization	NOUN
iajs-524	4	9	of	of	ADP
iajs-524	4	10	5-(mercapto-1,3,4thiadiazole-2yl)α	5-(mercapto-1,3,4thiadiazole-2yl)α	ADJ
iajs-524	4	11	,	,	PUNCT
iajs-524	4	12	α	α	PRON
iajs-524	4	13	-	-	ADJ
iajs-524	4	14	diphenyl	diphenyl	NOUN
iajs-524	4	15	methanol	methanol	NOUN
iajs-524	4	16	from	from	ADP
iajs-524	4	17	benzilic	benzilic	NOUN
iajs-524	4	18	acid	acid	PROPN
iajs-524	4	19	muhanned	muhanne	VERB
iajs-524	4	20	j.	j.	PROPN
iajs-524	4	21	mahmoud	mahmoud	PROPN
iajs-524	4	22	dept	dept	PROPN
iajs-524	4	23	.	.	PROPN
iajs-524	4	24	of	of	ADP
iajs-524	4	25	chemistry	chemistry	NOUN
iajs-524	4	26	/	/	SYM
iajs-524	4	27	college	college	NOUN
iajs-524	4	28	of	of	ADP
iajs-524	4	29	education	education	NOUN
iajs-524	4	30	for	for	ADP
iajs-524	4	31	pure	pure	ADJ
iajs-524	4	32	science(ibn	science(ibn	PROPN
iajs-524	4	33	alhaitham)/	alhaitham)/	PROPN
iajs-524	4	34	university	university	PROPN
iajs-524	4	35	of	of	ADP
iajs-524	4	36	baghdad	baghdad	PROPN
iajs-524	4	37	redha	redha	PROPN
iajs-524	4	38	i.	i.	PROPN
iajs-524	4	39	al	al	PROPN
iajs-524	4	40	-	-	PUNCT
iajs-524	4	41	bayati	bayati	PROPN
iajs-524	4	42	department	department	NOUN
iajs-524	4	43	of	of	ADP
iajs-524	4	44	chemistry	chemistry	NOUN
iajs-524	4	45	-	-	PUNCT
iajs-524	4	46	college	college	NOUN
iajs-524	4	47	of	of	ADP
iajs-524	4	48	science	science	NOUN
iajs-524	4	49	-	-	PUNCT
iajs-524	4	50	university	university	NOUN
iajs-524	4	51	of	of	ADP
iajs-524	4	52	mustansiriya	mustansiriya	PROPN
iajs-524	4	53	shaimaa	shaimaa	PROPN
iajs-524	4	54	a.	a.	PROPN
iajs-524	4	55	saoud	saoud	PROPN
iajs-524	4	56	ismaeel	ismaeel	PROPN
iajs-524	4	57	y.	y.	PROPN
iajs-524	4	58	majeed	majeed	PROPN
iajs-524	4	59	dept	dept	PROPN
iajs-524	4	60	.	.	PROPN
iajs-524	5	1	of	of	ADP
iajs-524	5	2	chemistry	chemistry	NOUN
iajs-524	5	3	/	/	SYM
iajs-524	5	4	college	college	NOUN
iajs-524	5	5	of	of	ADP
iajs-524	5	6	education	education	NOUN
iajs-524	5	7	for	for	ADP
iajs-524	5	8	pure	pure	ADJ
iajs-524	5	9	science(ibn	science(ibn	PROPN
iajs-524	5	10	alhaitham)/	alhaitham)/	PROPN
iajs-524	5	11	university	university	PROPN
iajs-524	5	12	of	of	ADP
iajs-524	5	13	baghdad	baghdad	PROPN
iajs-524	5	14	received	receive	VERB
iajs-524	5	15	in	in	ADP
iajs-524	5	16	:	:	PUNCT
iajs-524	5	17	31	31	NUM
iajs-524	5	18	december	december	PROPN
iajs-524	5	19	2007	2007	NUM
iajs-524	5	20	,	,	PUNCT
iajs-524	5	21	accepted	accept	VERB
iajs-524	5	22	in	in	ADP
iajs-524	5	23	:	:	PUNCT
iajs-524	5	24	25	25	NUM
iajs-524	5	25	june	june	PROPN
iajs-524	5	26	2008	2008	NUM
iajs-524	5	27	abstract	abstract	ADJ
iajs-524	5	28	5-(mercapto-1,3,4	5-(mercapto-1,3,4	NUM
iajs-524	5	29	-	-	PUNCT
iajs-524	5	30	thiadiazole-2yl)α	thiadiazole-2yl)α	ADJ
iajs-524	5	31	,	,	PUNCT
iajs-524	5	32	α-(diphenyl)methanol	α-(diphenyl)methanol	PROPN
iajs-524	5	33	have	have	AUX
iajs-524	5	34	been	be	AUX
iajs-524	5	35	synthesized	synthesize	VERB
iajs-524	5	36	by	by	ADP
iajs-524	5	37	ring	ring	NOUN
iajs-524	5	38	closer	close	ADJ
iajs-524	5	39	of	of	ADP
iajs-524	5	40	potassium	potassium	NOUN
iajs-524	5	41	xanthate[which	xanthate[which	PRON
iajs-524	5	42	have	have	AUX
iajs-524	5	43	been	be	AUX
iajs-524	5	44	prepared	prepare	VERB
iajs-524	5	45	by	by	ADP
iajs-524	5	46	reaction	reaction	NOUN
iajs-524	5	47	of	of	ADP
iajs-524	5	48	benzilic	benzilic	NOUN
iajs-524	5	49	acid	acid	NOUN
iajs-524	5	50	hydrazide	hydrazide	ADV
iajs-524	5	51	with	with	ADP
iajs-524	5	52	carbon	carbon	NOUN
iajs-524	5	53	disulphide	disulphide	ADV
iajs-524	5	54	in	in	ADP
iajs-524	5	55	potassium	potassium	NOUN
iajs-524	5	56	hydroxide	hydroxide	NOUN
iajs-524	5	57	]	]	PUNCT
iajs-524	5	58	using	use	VERB
iajs-524	5	59	conc.sulphuric	conc.sulphuric	PROPN
iajs-524	5	60	acid	acid	NOUN
iajs-524	5	61	at	at	ADP
iajs-524	5	62	(	(	PUNCT
iajs-524	5	63	0	0	NUM
iajs-524	5	64	-	-	SYM
iajs-524	5	65	5)	5)	NUM
iajs-524	5	66	°	°	PROPN
iajs-524	5	67	c	c	NOUN
iajs-524	5	68	scheme(i	scheme(i	NOUN
iajs-524	5	69	)	)	PUNCT
iajs-524	5	70	.	.	PUNCT
iajs-524	6	1	their	their	PRON
iajs-524	6	2	characterization	characterization	NOUN
iajs-524	6	3	was	be	AUX
iajs-524	6	4	carried	carry	VERB
iajs-524	6	5	out	out	ADP
iajs-524	6	6	from	from	ADP
iajs-524	6	7	t.l.c	t.l.c	ADP
iajs-524	6	8	,	,	PUNCT
iajs-524	6	9	m.p	m.p	PROPN
iajs-524	6	10	,	,	PUNCT
iajs-524	6	11	ft.ir	ft.ir	PROPN
iajs-524	6	12	and	and	CCONJ
iajs-524	6	13	1h	1h	NUM
iajs-524	6	14	-	-	PUNCT
iajs-524	6	15	nmr	nmr	NOUN
iajs-524	6	16	.	.	PUNCT
iajs-524	7	1	key	key	PROPN
iajs-524	7	2	wared	ware	VERB
iajs-524	7	3	:	:	PUNCT
iajs-524	7	4	1,3,4	1,3,4	NUM
iajs-524	7	5	-	-	PUNCT
iajs-524	7	6	thiadiazole	thiadiazole	NOUN
iajs-524	7	7	derivative	derivative	NOUN
iajs-524	7	8	.	.	PUNCT
iajs-524	8	1	185	185	NUM
iajs-524	8	2	|	|	ADV
iajs-524	8	3	chemistry	chemistry	NOUN
iajs-524	8	4	@@@@@@@@@@@@@@@@@úó‘ój	@@@@@@@@@@@@@@@@@úó‘ój	PROPN
iajs-524	8	5	�	�	PROPN
iajs-524	8	6	n€a@î@úœäñ€a@‚ï‹»‹€@·ró	n€a@î@úœäñ€a@‚ï‹»‹€@·ró	NUM
iajs-524	8	7	:	:	PUNCT
iajs-524	8	8	a@âig@ú‹	a@âig@ú‹	PROPN
iajs-524	8	9	©	©	PROPN
iajs-524	8	10	@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@ü‹1a26@@öü»€a@i1@‚b«@h2013	@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@ü‹1a26@@öü»€a@i1@‚b«@h2013	PROPN
iajs-524	8	11	ibn	ibn	PROPN
iajs-524	8	12	al	al	PROPN
iajs-524	8	13	-	-	PUNCT
iajs-524	8	14	haitham	haitham	PROPN
iajs-524	8	15	jour	jour	X
iajs-524	8	16	.	.	PROPN
iajs-524	9	1	for	for	ADP
iajs-524	9	2	pure	pure	ADJ
iajs-524	9	3	&	&	CCONJ
iajs-524	9	4	appl	appl	PROPN
iajs-524	9	5	.	.	PUNCT
iajs-524	10	1	sci	sci	PROPN
iajs-524	10	2	.	.	PUNCT
iajs-524	10	3	vol	vol	NOUN
iajs-524	10	4	.	.	PROPN
iajs-524	11	1	26	26	NUM
iajs-524	11	2	(	(	PUNCT
iajs-524	11	3	1	1	NUM
iajs-524	11	4	)	)	PUNCT
iajs-524	11	5	2013	2013	NUM
iajs-524	11	6	introduction	introduction	NOUN
iajs-524	11	7	1,3,4	1,3,4	NUM
iajs-524	11	8	-	-	PUNCT
iajs-524	11	9	thiadiazole	thiadiazole	NOUN
iajs-524	11	10	is	be	AUX
iajs-524	11	11	one	one	NUM
iajs-524	11	12	of	of	ADP
iajs-524	11	13	a	a	DET
iajs-524	11	14	class	class	NOUN
iajs-524	11	15	of	of	ADP
iajs-524	11	16	organic	organic	ADJ
iajs-524	11	17	heterocyclic	heterocyclic	NOUN
iajs-524	11	18	compounds	compound	NOUN
iajs-524	11	19	containing	contain	VERB
iajs-524	11	20	a	a	DET
iajs-524	11	21	five	five	NUM
iajs-524	11	22	member	member	NOUN
iajs-524	11	23	diunsaturated	diunsaturate	VERB
iajs-524	11	24	ring	ring	NOUN
iajs-524	11	25	structure	structure	NOUN
iajs-524	11	26	composed	compose	VERB
iajs-524	11	27	of	of	ADP
iajs-524	11	28	two	two	NUM
iajs-524	11	29	nitrogen	nitrogen	NOUN
iajs-524	11	30	atoms	atom	NOUN
iajs-524	11	31	at	at	ADP
iajs-524	11	32	positions	position	NOUN
iajs-524	11	33	(	(	PUNCT
iajs-524	11	34	3	3	NUM
iajs-524	11	35	and	and	CCONJ
iajs-524	11	36	4	4	NUM
iajs-524	11	37	)	)	PUNCT
iajs-524	11	38	and	and	CCONJ
iajs-524	11	39	one	one	NUM
iajs-524	11	40	sulphur	sulphur	NOUN
iajs-524	11	41	atom	atom	NOUN
iajs-524	11	42	at	at	ADP
iajs-524	11	43	position	position	NOUN
iajs-524	11	44	[	[	X
iajs-524	11	45	1	1	NUM
iajs-524	11	46	]	]	PUNCT
iajs-524	11	47	.	.	PUNCT
iajs-524	12	1	most	most	ADJ
iajs-524	12	2	of	of	ADP
iajs-524	12	3	published	publish	VERB
iajs-524	12	4	work	work	NOUN
iajs-524	12	5	on	on	ADP
iajs-524	12	6	the	the	DET
iajs-524	12	7	four	four	NUM
iajs-524	12	8	thiadiazoles	thiadiazole	NOUN
iajs-524	12	9	has	have	AUX
iajs-524	12	10	been	be	AUX
iajs-524	12	11	on	on	ADP
iajs-524	12	12	the	the	DET
iajs-524	12	13	1,3,4	1,3,4	NUM
iajs-524	12	14	–	–	PUNCT
iajs-524	12	15	thiadiazoles	thiadiazole	NOUN
iajs-524	12	16	.	.	PUNCT
iajs-524	13	1	physical	physical	ADJ
iajs-524	13	2	,	,	PUNCT
iajs-524	13	3	theoretical	theoretical	ADJ
iajs-524	13	4	,	,	PUNCT
iajs-524	13	5	and	and	CCONJ
iajs-524	13	6	spectroscopic	spectroscopic	ADJ
iajs-524	13	7	properties	property	NOUN
iajs-524	13	8	have	have	AUX
iajs-524	13	9	been	be	AUX
iajs-524	13	10	reviewed[2,3,4,5	reviewed[2,3,4,5	VERB
iajs-524	13	11	]	]	X
iajs-524	13	12	.	.	PUNCT
iajs-524	14	1	a	a	DET
iajs-524	14	2	useful	useful	ADJ
iajs-524	14	3	preparative	preparative	ADJ
iajs-524	14	4	method	method	NOUN
iajs-524	14	5	for	for	ADP
iajs-524	14	6	2	2	NUM
iajs-524	14	7	–	–	PUNCT
iajs-524	14	8	amino	amino	NOUN
iajs-524	14	9	–	–	PUNCT
iajs-524	14	10	5	5	NUM
iajs-524	14	11	-	-	PUNCT
iajs-524	14	12	mercapto–1,3,4	mercapto–1,3,4	ADJ
iajs-524	14	13	–	–	PUNCT
iajs-524	14	14	thiadiazole	thiadiazole	NOUN
iajs-524	14	15	was	be	AUX
iajs-524	14	16	developed	develop	VERB
iajs-524	14	17	by	by	ADP
iajs-524	14	18	guha[6	guha[6	NOUN
iajs-524	14	19	]	]	PUNCT
iajs-524	14	20	which	which	PRON
iajs-524	14	21	showed	show	VERB
iajs-524	14	22	that	that	SCONJ
iajs-524	14	23	when	when	SCONJ
iajs-524	14	24	thiosemicarbazide	thiosemicarbazide	NOUN
iajs-524	14	25	is	be	AUX
iajs-524	14	26	treated	treat	VERB
iajs-524	14	27	with	with	ADP
iajs-524	14	28	carbon	carbon	NOUN
iajs-524	14	29	disulphide	disulphide	NOUN
iajs-524	14	30	and	and	CCONJ
iajs-524	14	31	potassium	potassium	NOUN
iajs-524	14	32	hydroxide	hydroxide	NOUN
iajs-524	14	33	,	,	PUNCT
iajs-524	14	34	the	the	DET
iajs-524	14	35	potassium	potassium	NOUN
iajs-524	14	36	salt	salt	NOUN
iajs-524	14	37	of	of	ADP
iajs-524	14	38	thiosemicarbazide–4	thiosemicarbazide–4	PROPN
iajs-524	14	39	–	–	PUNCT
iajs-524	14	40	dithio	dithio	ADJ
iajs-524	14	41	carboxylic	carboxylic	ADJ
iajs-524	14	42	acid	acid	NOUN
iajs-524	14	43	(	(	PUNCT
iajs-524	14	44	xanthate	xanthate	PROPN
iajs-524	14	45	)	)	PUNCT
iajs-524	14	46	was	be	AUX
iajs-524	14	47	formed	form	VERB
iajs-524	14	48	.	.	PUNCT
iajs-524	15	1	hiremarth	hiremarth	NOUN
iajs-524	15	2	et.al[7	et.al[7	PROPN
iajs-524	15	3	]	]	PUNCT
iajs-524	15	4	synthesized	synthesize	VERB
iajs-524	15	5	a	a	DET
iajs-524	15	6	series	series	NOUN
iajs-524	15	7	of	of	ADP
iajs-524	15	8	2	2	NUM
iajs-524	15	9	–	–	PUNCT
iajs-524	15	10	amino–5–[4	amino–5–[4	ADJ
iajs-524	15	11	–	–	PUNCT
iajs-524	15	12	(	(	PUNCT
iajs-524	15	13	substituted	substitute	VERB
iajs-524	15	14	)	)	PUNCT
iajs-524	15	15	anilino]–methyl	anilino]–methyl	PROPN
iajs-524	15	16	–	–	PUNCT
iajs-524	15	17	1,3,4	1,3,4	NUM
iajs-524	15	18	–	–	PUNCT
iajs-524	15	19	thiadiazole	thiadiazole	NOUN
iajs-524	15	20	through	through	ADP
iajs-524	15	21	cyclo	cyclo	NOUN
iajs-524	15	22	condensation	condensation	NOUN
iajs-524	15	23	of	of	ADP
iajs-524	15	24	thiosemicarbazide	thiosemicarbazide	ADJ
iajs-524	15	25	derivative	derivative	NOUN
iajs-524	15	26	with	with	ADP
iajs-524	15	27	phosphoric	phosphoric	ADJ
iajs-524	15	28	acid	acid	NOUN
iajs-524	15	29	.	.	PUNCT
iajs-524	16	1	zamani	zamani	PROPN
iajs-524	16	2	et.al.[8	et.al.[8	PROPN
iajs-524	16	3	]	]	PUNCT
iajs-524	16	4	synthesized	synthesize	VERB
iajs-524	16	5	new	new	ADJ
iajs-524	16	6	1,3,4	1,3,4	NUM
iajs-524	16	7	–	–	PUNCT
iajs-524	16	8	thiadiazole	thiadiazole	NOUN
iajs-524	16	9	derivatives	derivative	NOUN
iajs-524	16	10	.	.	PUNCT
iajs-524	17	1	kurzer	kurzer	PROPN
iajs-524	17	2	and	and	CCONJ
iajs-524	17	3	secker[9	secker[9	PRON
iajs-524	17	4	]	]	PUNCT
iajs-524	17	5	found	find	VERB
iajs-524	17	6	that	that	SCONJ
iajs-524	17	7	the	the	DET
iajs-524	17	8	use	use	NOUN
iajs-524	17	9	of	of	ADP
iajs-524	17	10	reactants	reactant	NOUN
iajs-524	17	11	incorporating	incorporate	VERB
iajs-524	17	12	free	free	ADJ
iajs-524	17	13	hydrazine	hydrazine	NOUN
iajs-524	17	14	group	group	NOUN
iajs-524	17	15	provided	provide	VERB
iajs-524	17	16	a	a	DET
iajs-524	17	17	versatile	versatile	ADJ
iajs-524	17	18	route	route	NOUN
iajs-524	17	19	to	to	ADP
iajs-524	17	20	substituted	substitute	VERB
iajs-524	17	21	1,3,4	1,3,4	NUM
iajs-524	17	22	–	–	PUNCT
iajs-524	17	23	thiadiazole	thiadiazole	NOUN
iajs-524	17	24	.	.	PUNCT
iajs-524	18	1	they	they	PRON
iajs-524	18	2	reported	report	VERB
iajs-524	18	3	various	various	ADJ
iajs-524	18	4	approaches	approach	NOUN
iajs-524	18	5	,	,	PUNCT
iajs-524	18	6	employing	employ	VERB
iajs-524	18	7	the	the	DET
iajs-524	18	8	prototype	prototype	NOUN
iajs-524	18	9	hydrazine	hydrazine	NOUN
iajs-524	18	10	it	it	PRON
iajs-524	18	11	self	self	NOUN
iajs-524	18	12	and	and	CCONJ
iajs-524	18	13	some	some	PRON
iajs-524	18	14	of	of	ADP
iajs-524	18	15	its	its	PRON
iajs-524	18	16	simple	simple	ADJ
iajs-524	18	17	congeners	congener	NOUN
iajs-524	18	18	.	.	PUNCT
iajs-524	19	1	onkol	onkol	PROPN
iajs-524	19	2	et.al[10	et.al[10	PART
iajs-524	19	3	]	]	X
iajs-524	19	4	synthesized1,3,4	synthesized1,3,4	NOUN
iajs-524	19	5	–	–	PUNCT
iajs-524	19	6	thiadiazole	thiadiazole	NOUN
iajs-524	19	7	by	by	ADP
iajs-524	19	8	ring	ring	NOUN
iajs-524	19	9	closer	close	ADV
iajs-524	19	10	some	some	DET
iajs-524	19	11	compounds	compound	NOUN
iajs-524	19	12	by	by	ADP
iajs-524	19	13	use	use	NOUN
iajs-524	19	14	conc	conc	NOUN
iajs-524	19	15	.	.	PUNCT
iajs-524	20	1	sulphuric	sulphuric	PROPN
iajs-524	20	2	acid	acid	PROPN
iajs-524	20	3	at	at	ADP
iajs-524	20	4	(	(	PUNCT
iajs-524	20	5	0	0	NUM
iajs-524	20	6	-	-	SYM
iajs-524	20	7	5)	5)	NUM
iajs-524	20	8	°	°	NOUN
iajs-524	20	9	c	c	NOUN
iajs-524	20	10	in	in	ADP
iajs-524	20	11	this	this	DET
iajs-524	20	12	work	work	NOUN
iajs-524	20	13	we	we	PRON
iajs-524	20	14	have	have	AUX
iajs-524	20	15	been	be	AUX
iajs-524	20	16	synthesized	synthesize	VERB
iajs-524	20	17	1,3,4	1,3,4	NUM
iajs-524	20	18	-	-	PUNCT
iajs-524	20	19	thiadiazole	thiadiazole	NOUN
iajs-524	20	20	by	by	ADP
iajs-524	20	21	treated	treat	VERB
iajs-524	20	22	potassium	potassium	NOUN
iajs-524	20	23	xanthate	xanthate	NOUN
iajs-524	20	24	with	with	ADP
iajs-524	20	25	conc	conc	ADJ
iajs-524	20	26	sulphuric	sulphuric	PROPN
iajs-524	20	27	acid	acid	NOUN
iajs-524	20	28	at	at	ADP
iajs-524	20	29	(	(	PUNCT
iajs-524	20	30	0	0	NUM
iajs-524	20	31	-	-	PUNCT
iajs-524	20	32	3)	3)	NUM
iajs-524	20	33	°	°	NOUN
iajs-524	20	34	c	c	NOUN
iajs-524	20	35	.	.	PUNCT
iajs-524	21	1	the	the	DET
iajs-524	21	2	products	product	NOUN
iajs-524	21	3	were	be	AUX
iajs-524	21	4	characterized	characterize	VERB
iajs-524	21	5	by	by	ADP
iajs-524	21	6	t.l.c	t.l.c	ADJ
iajs-524	21	7	,	,	PUNCT
iajs-524	21	8	m.p	m.p	PROPN
iajs-524	21	9	,	,	PUNCT
iajs-524	21	10	ft.ir	ft.ir	PROPN
iajs-524	21	11	and	and	CCONJ
iajs-524	21	12	1h	1h	NUM
iajs-524	21	13	-	-	PUNCT
iajs-524	21	14	nmr	nmr	NOUN
iajs-524	21	15	spectral	spectral	ADJ
iajs-524	21	16	data	datum	NOUN
iajs-524	21	17	.	.	PUNCT
iajs-524	22	1	instruments	instrument	NOUN
iajs-524	22	2	melting	melt	VERB
iajs-524	22	3	points	point	NOUN
iajs-524	22	4	were	be	AUX
iajs-524	22	5	recorded	record	VERB
iajs-524	22	6	using	use	VERB
iajs-524	22	7	hot	hot	ADJ
iajs-524	22	8	stage	stage	NOUN
iajs-524	22	9	gallenkamp	gallenkamp	NOUN
iajs-524	22	10	melting	melting	NOUN
iajs-524	22	11	point	point	NOUN
iajs-524	22	12	apparatus	apparatus	NOUN
iajs-524	22	13	and	and	CCONJ
iajs-524	22	14	were	be	AUX
iajs-524	22	15	uncorrected	uncorrecte	VERB
iajs-524	22	16	.	.	PUNCT
iajs-524	23	1	thin	thin	ADJ
iajs-524	23	2	layer	layer	NOUN
iajs-524	23	3	chromatography	chromatography	NOUN
iajs-524	23	4	(	(	PUNCT
iajs-524	23	5	t.l.c	t.l.c	INTJ
iajs-524	23	6	)	)	PUNCT
iajs-524	23	7	was	be	AUX
iajs-524	23	8	carried	carry	VERB
iajs-524	23	9	out	out	ADP
iajs-524	23	10	using	use	VERB
iajs-524	23	11	fertigfollen	fertigfollen	VERB
iajs-524	23	12	precoated	precoate	VERB
iajs-524	23	13	sheets	sheet	NOUN
iajs-524	23	14	type	type	NOUN
iajs-524	23	15	polygram	polygram	PROPN
iajs-524	23	16	silica	silica	NOUN
iajs-524	23	17	-	-	PUNCT
iajs-524	23	18	gel	gel	NOUN
iajs-524	23	19	as	as	ADP
iajs-524	23	20	stationary	stationary	ADJ
iajs-524	23	21	phase	phase	NOUN
iajs-524	23	22	ethyl	ethyl	PROPN
iajs-524	23	23	acetate	acetate	PROPN
iajs-524	23	24	as	as	ADP
iajs-524	23	25	eluent	eluent	NOUN
iajs-524	23	26	,	,	PUNCT
iajs-524	23	27	and	and	CCONJ
iajs-524	23	28	the	the	DET
iajs-524	23	29	plates	plate	NOUN
iajs-524	23	30	were	be	AUX
iajs-524	23	31	developed	develop	VERB
iajs-524	23	32	with	with	ADP
iajs-524	23	33	iodine	iodine	NOUN
iajs-524	23	34	vapor	vapor	NOUN
iajs-524	23	35	.	.	PUNCT
iajs-524	24	1	infrared	infrared	PROPN
iajs-524	24	2	spectra	spectra	PROPN
iajs-524	24	3	were	be	AUX
iajs-524	24	4	recorded	record	VERB
iajs-524	24	5	using	use	VERB
iajs-524	24	6	fourier	fourier	NOUN
iajs-524	24	7	transform	transform	NOUN
iajs-524	24	8	infrared	infrared	ADJ
iajs-524	24	9	shimadzu	shimadzu	NOUN
iajs-524	24	10	(	(	PUNCT
iajs-524	24	11	8300	8300	NUM
iajs-524	24	12	)	)	PUNCT
iajs-524	24	13	(	(	PUNCT
iajs-524	24	14	ft.ir	ft.ir	ADV
iajs-524	24	15	)	)	PUNCT
iajs-524	24	16	infrared	infrared	PROPN
iajs-524	24	17	spectrophtometer	spectrophtometer	NOUN
iajs-524	24	18	,	,	PUNCT
iajs-524	24	19	kbr	kbr	PROPN
iajs-524	24	20	disc	disc	NOUN
iajs-524	24	21	or	or	CCONJ
iajs-524	24	22	thin	thin	ADJ
iajs-524	24	23	film	film	NOUN
iajs-524	24	24	was	be	AUX
iajs-524	24	25	performed	perform	VERB
iajs-524	24	26	by	by	ADP
iajs-524	24	27	co.s.q.c	co.s.q.c	NOUN
iajs-524	24	28	iraq	iraq	PROPN
iajs-524	24	29	.	.	PUNCT
iajs-524	25	1	1h	1h	NUM
iajs-524	25	2	nmr	nmr	PROPN
iajs-524	25	3	,	,	PUNCT
iajs-524	25	4	13c	13c	NOUN
iajs-524	25	5	–	–	PUNCT
iajs-524	25	6	nmr	nmr	NOUN
iajs-524	25	7	and	and	CCONJ
iajs-524	25	8	mass	mass	ADJ
iajs-524	25	9	spectra	spectra	NOUN
iajs-524	25	10	were	be	AUX
iajs-524	25	11	recorded	record	VERB
iajs-524	25	12	on	on	ADP
iajs-524	25	13	foruier	foruier	NOUN
iajs-524	25	14	transform	transform	VERB
iajs-524	25	15	varian	varian	PROPN
iajs-524	25	16	spectrometer	spectrometer	NOUN
iajs-524	25	17	,	,	PUNCT
iajs-524	25	18	operating	operate	VERB
iajs-524	25	19	at	at	ADP
iajs-524	25	20	300	300	NUM
iajs-524	25	21	mhz	mhz	NOUN
iajs-524	25	22	with	with	ADP
iajs-524	25	23	tetramethylsilane	tetramethylsilane	NOUN
iajs-524	25	24	as	as	ADP
iajs-524	25	25	internal	internal	ADJ
iajs-524	25	26	standared	standared	NOUN
iajs-524	25	27	in	in	ADP
iajs-524	25	28	dmso	dmso	NOUN
iajs-524	25	29	,	,	PUNCT
iajs-524	25	30	measurments	measurment	NOUN
iajs-524	25	31	were	be	AUX
iajs-524	25	32	made	make	VERB
iajs-524	25	33	at	at	ADP
iajs-524	25	34	chemistry	chemistry	NOUN
iajs-524	25	35	department	department	NOUN
iajs-524	25	36	,	,	PUNCT
iajs-524	25	37	al	al	PROPN
iajs-524	25	38	–	–	PUNCT
iajs-524	25	39	al	al	PROPN
iajs-524	25	40	-	-	PUNCT
iajs-524	25	41	bayt	bayt	ADJ
iajs-524	25	42	university	university	NOUN
iajs-524	25	43	,	,	PUNCT
iajs-524	25	44	jordan	jordan	PROPN
iajs-524	25	45	.	.	PUNCT
iajs-524	26	1	experimental	experimental	ADJ
iajs-524	26	2	synthesis	synthesis	NOUN
iajs-524	26	3	of	of	ADP
iajs-524	26	4	methyl	methyl	NOUN
iajs-524	26	5	α	α	PROPN
iajs-524	26	6	-	-	PUNCT
iajs-524	26	7	hydroxy	hydroxy	VERB
iajs-524	26	8	-	-	PUNCT
iajs-524	26	9	α	α	NOUN
iajs-524	26	10	,	,	PUNCT
iajs-524	26	11	α-(diphenyl	α-(diphenyl	NOUN
iajs-524	26	12	)	)	PUNCT
iajs-524	26	13	acetate	acetate	NOUN
iajs-524	27	1	[	[	X
iajs-524	27	2	2	2	NUM
iajs-524	27	3	]	]	PUNCT
iajs-524	27	4	a	a	DET
iajs-524	27	5	mixture	mixture	NOUN
iajs-524	27	6	of	of	ADP
iajs-524	27	7	benzilic	benzilic	NOUN
iajs-524	27	8	acid	acid	NOUN
iajs-524	28	1	[	[	X
iajs-524	28	2	1	1	NUM
iajs-524	28	3	]	]	PUNCT
iajs-524	28	4	(	(	PUNCT
iajs-524	28	5	2	2	NUM
iajs-524	28	6	g	g	NOUN
iajs-524	28	7	,	,	PUNCT
iajs-524	28	8	0.08mol	0.08mol	PRON
iajs-524	28	9	.	.	PUNCT
iajs-524	28	10	)	)	PUNCT
iajs-524	29	1	and	and	CCONJ
iajs-524	29	2	(	(	PUNCT
iajs-524	29	3	0.9	0.9	NUM
iajs-524	29	4	g	g	NOUN
iajs-524	29	5	,	,	PUNCT
iajs-524	29	6	0.08mol	0.08mol	PRON
iajs-524	29	7	.	.	PUNCT
iajs-524	29	8	)	)	PUNCT
iajs-524	29	9	of	of	ADP
iajs-524	29	10	anhydrous	anhydrous	ADJ
iajs-524	29	11	sodium	sodium	NOUN
iajs-524	29	12	carbonate	carbonate	NOUN
iajs-524	29	13	was	be	AUX
iajs-524	29	14	dissolved	dissolve	VERB
iajs-524	29	15	in	in	ADP
iajs-524	29	16	(	(	PUNCT
iajs-524	29	17	20	20	NUM
iajs-524	29	18	ml	ml	NOUN
iajs-524	29	19	)	)	PUNCT
iajs-524	29	20	dry	dry	ADJ
iajs-524	29	21	acetone	acetone	NOUN
iajs-524	29	22	.	.	PUNCT
iajs-524	30	1	to	to	ADP
iajs-524	30	2	this	this	DET
iajs-524	30	3	solution	solution	NOUN
iajs-524	30	4	(	(	PUNCT
iajs-524	30	5	1.1	1.1	NUM
iajs-524	30	6	g	g	NOUN
iajs-524	30	7	,	,	PUNCT
iajs-524	30	8	0.08mol	0.08mol	PRON
iajs-524	30	9	.	.	PUNCT
iajs-524	30	10	)	)	PUNCT
iajs-524	30	11	of	of	ADP
iajs-524	30	12	dimethyl	dimethyl	NOUN
iajs-524	30	13	sulphate	sulphate	NOUN
iajs-524	30	14	was	be	AUX
iajs-524	30	15	added.the	added.the	DET
iajs-524	30	16	resulting	result	VERB
iajs-524	30	17	mixture	mixture	NOUN
iajs-524	30	18	was	be	AUX
iajs-524	30	19	heated	heat	VERB
iajs-524	30	20	under	under	ADP
iajs-524	30	21	reflux	reflux	NOUN
iajs-524	30	22	for	for	ADP
iajs-524	30	23	4	4	NUM
iajs-524	30	24	hr	hr	NOUN
iajs-524	30	25	.	.	PROPN
iajs-524	31	1	186	186	NUM
iajs-524	31	2	|	|	ADV
iajs-524	31	3	chemistry	chemistry	NOUN
iajs-524	31	4	@@@@@@@@@@@@@@@@@úó‘ój	@@@@@@@@@@@@@@@@@úó‘ój	PROPN
iajs-524	31	5	�	�	PROPN
iajs-524	31	6	n€a@î@úœäñ€a@‚ï‹»‹€@·ró	n€a@î@úœäñ€a@‚ï‹»‹€@·ró	NUM
iajs-524	31	7	:	:	PUNCT
iajs-524	31	8	a@âig@ú‹	a@âig@ú‹	PROPN
iajs-524	31	9	©	©	PROPN
iajs-524	31	10	@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@ü‹1a26@@öü»€a@i1@‚b«@h2013	@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@ü‹1a26@@öü»€a@i1@‚b«@h2013	PROPN
iajs-524	31	11	ibn	ibn	PROPN
iajs-524	31	12	al	al	PROPN
iajs-524	31	13	-	-	PUNCT
iajs-524	31	14	haitham	haitham	PROPN
iajs-524	31	15	jour	jour	X
iajs-524	31	16	.	.	PROPN
iajs-524	32	1	for	for	ADP
iajs-524	32	2	pure	pure	ADJ
iajs-524	32	3	&	&	CCONJ
iajs-524	32	4	appl	appl	PROPN
iajs-524	32	5	.	.	PUNCT
iajs-524	33	1	sci	sci	PROPN
iajs-524	33	2	.	.	PUNCT
iajs-524	33	3	vol	vol	NOUN
iajs-524	33	4	.	.	PROPN
iajs-524	34	1	26	26	NUM
iajs-524	34	2	(	(	PUNCT
iajs-524	34	3	1	1	NUM
iajs-524	34	4	)	)	PUNCT
iajs-524	34	5	2013	2013	NUM
iajs-524	34	6	the	the	DET
iajs-524	34	7	reaction	reaction	NOUN
iajs-524	34	8	mixture	mixture	NOUN
iajs-524	34	9	was	be	AUX
iajs-524	34	10	then	then	ADV
iajs-524	34	11	allowed	allow	VERB
iajs-524	34	12	at	at	ADP
iajs-524	34	13	cool	cool	ADJ
iajs-524	34	14	down	down	ADP
iajs-524	34	15	to	to	ADP
iajs-524	34	16	room	room	NOUN
iajs-524	34	17	temperature	temperature	NOUN
iajs-524	34	18	,	,	PUNCT
iajs-524	34	19	the	the	DET
iajs-524	34	20	reaction	reaction	NOUN
iajs-524	34	21	was	be	AUX
iajs-524	34	22	followed	follow	VERB
iajs-524	34	23	by	by	ADP
iajs-524	34	24	(	(	PUNCT
iajs-524	34	25	t.l.c	t.l.c	ADJ
iajs-524	34	26	)	)	PUNCT
iajs-524	34	27	*	*	PUNCT
iajs-524	34	28	,	,	PUNCT
iajs-524	34	29	extraction	extraction	NOUN
iajs-524	34	30	with	with	ADP
iajs-524	34	31	ethyl	ethyl	PROPN
iajs-524	34	32	acetate	acetate	NOUN
iajs-524	34	33	and	and	CCONJ
iajs-524	34	34	evaporation	evaporation	NOUN
iajs-524	34	35	of	of	ADP
iajs-524	34	36	the	the	DET
iajs-524	34	37	dried	dry	VERB
iajs-524	34	38	organic	organic	ADJ
iajs-524	34	39	layer	layer	NOUN
iajs-524	34	40	,	,	PUNCT
iajs-524	34	41	the	the	DET
iajs-524	34	42	product	product	NOUN
iajs-524	34	43	was	be	AUX
iajs-524	34	44	white	white	ADJ
iajs-524	34	45	crystille	crystille	PROPN
iajs-524	34	46	,	,	PUNCT
iajs-524	34	47	recrystillized	recrystillize	VERB
iajs-524	34	48	from	from	ADP
iajs-524	34	49	ethanol	ethanol	NOUN
iajs-524	34	50	(	(	PUNCT
iajs-524	34	51	1.82	1.82	NUM
iajs-524	34	52	g	g	NOUN
iajs-524	34	53	,	,	PUNCT
iajs-524	34	54	yield	yield	VERB
iajs-524	34	55	86	86	NUM
iajs-524	34	56	%	%	NOUN
iajs-524	34	57	,	,	PUNCT
iajs-524	34	58	m.p=	m.p=	NOUN
iajs-524	34	59	50	50	NUM
iajs-524	34	60	–	–	PUNCT
iajs-524	34	61	52	52	NUM
iajs-524	34	62	°	°	NUM
iajs-524	34	63	c	c	NOUN
iajs-524	34	64	)	)	PUNCT
iajs-524	34	65	.	.	PUNCT
iajs-524	35	1	*	*	PUNCT
iajs-524	35	2	silica	silica	NOUN
iajs-524	35	3	gel	gel	NOUN
iajs-524	35	4	as	as	ADP
iajs-524	35	5	stationary	stationary	ADJ
iajs-524	35	6	phase	phase	NOUN
iajs-524	35	7	ethyl	ethyl	PROPN
iajs-524	35	8	acetate	acetate	PROPN
iajs-524	35	9	as	as	ADP
iajs-524	35	10	eluent	eluent	NOUN
iajs-524	35	11	synthesis	synthesis	NOUN
iajs-524	35	12	of	of	ADP
iajs-524	35	13	α	α	NOUN
iajs-524	35	14	-	-	PUNCT
iajs-524	35	15	hydroxy	hydroxy	VERB
iajs-524	35	16	-	-	PUNCT
iajs-524	35	17	α	α	NOUN
iajs-524	35	18	,	,	PUNCT
iajs-524	35	19	α	α	NOUN
iajs-524	35	20	-	-	ADJ
iajs-524	35	21	diphenyl	diphenyl	NOUN
iajs-524	35	22	acid	acid	NOUN
iajs-524	35	23	hydrazide[11](3	hydrazide[11](3	NOUN
iajs-524	35	24	)	)	PUNCT
iajs-524	35	25	.	.	PUNCT
iajs-524	36	1	compound	compound	VERB
iajs-524	37	1	[	[	X
iajs-524	37	2	3	3	X
iajs-524	37	3	]	]	PUNCT
iajs-524	37	4	was	be	AUX
iajs-524	37	5	synthesized	synthesize	VERB
iajs-524	37	6	by	by	ADP
iajs-524	37	7	addition	addition	NOUN
iajs-524	37	8	of	of	ADP
iajs-524	37	9	the	the	DET
iajs-524	37	10	hydrazine	hydrazine	NOUN
iajs-524	37	11	monohydrate	monohydrate	NOUN
iajs-524	37	12	98	98	NUM
iajs-524	37	13	%	%	NOUN
iajs-524	37	14	(	(	PUNCT
iajs-524	37	15	0.2	0.2	NUM
iajs-524	37	16	g	g	NOUN
iajs-524	37	17	,	,	PUNCT
iajs-524	37	18	0.004mol	0.004mol	NOUN
iajs-524	37	19	.	.	PUNCT
iajs-524	37	20	)	)	PUNCT
iajs-524	37	21	to	to	ADP
iajs-524	37	22	methyl	methyl	NOUN
iajs-524	37	23	ester	ester	NOUN
iajs-524	38	1	[	[	X
iajs-524	38	2	2	2	NUM
iajs-524	38	3	]	]	PUNCT
iajs-524	38	4	(	(	PUNCT
iajs-524	38	5	1	1	NUM
iajs-524	38	6	g	g	NOUN
iajs-524	38	7	,	,	PUNCT
iajs-524	38	8	0.004mol	0.004mol	NOUN
iajs-524	38	9	.	.	PUNCT
iajs-524	38	10	)	)	PUNCT
iajs-524	38	11	.	.	PUNCT
iajs-524	39	1	with	with	ADP
iajs-524	39	2	stirring	stirring	NOUN
iajs-524	39	3	,	,	PUNCT
iajs-524	39	4	then	then	ADV
iajs-524	39	5	the	the	DET
iajs-524	39	6	absolute	absolute	ADJ
iajs-524	39	7	ethanol	ethanol	NOUN
iajs-524	39	8	(	(	PUNCT
iajs-524	39	9	10	10	NUM
iajs-524	39	10	ml	ml	NOUN
iajs-524	39	11	)	)	PUNCT
iajs-524	39	12	was	be	AUX
iajs-524	39	13	added	add	VERB
iajs-524	39	14	and	and	CCONJ
iajs-524	39	15	refluxed	refluxe	VERB
iajs-524	39	16	until	until	ADP
iajs-524	39	17	the	the	DET
iajs-524	39	18	precipitate	precipitate	NOUN
iajs-524	39	19	formed(1.5	formed(1.5	NOUN
iajs-524	39	20	hrs	hrs	NOUN
iajs-524	39	21	)	)	PUNCT
iajs-524	39	22	.	.	PUNCT
iajs-524	40	1	after	after	ADP
iajs-524	40	2	cooling	cool	VERB
iajs-524	40	3	,	,	PUNCT
iajs-524	40	4	the	the	DET
iajs-524	40	5	precipitate	precipitate	NOUN
iajs-524	40	6	was	be	AUX
iajs-524	40	7	filtered	filter	VERB
iajs-524	40	8	off	off	ADP
iajs-524	40	9	and	and	CCONJ
iajs-524	40	10	recrystallized	recrystallize	VERB
iajs-524	40	11	from	from	ADP
iajs-524	40	12	ethanol	ethanol	NOUN
iajs-524	40	13	,	,	PUNCT
iajs-524	40	14	(	(	PUNCT
iajs-524	40	15	0.74	0.74	NUM
iajs-524	40	16	g	g	NOUN
iajs-524	40	17	)	)	PUNCT
iajs-524	40	18	yield	yield	NOUN
iajs-524	40	19	74	74	NUM
iajs-524	40	20	%	%	NOUN
iajs-524	40	21	,	,	PUNCT
iajs-524	41	1	m.p	m.p	PROPN
iajs-524	41	2	.	.	PROPN
iajs-524	41	3	150	150	NUM
iajs-524	41	4	°	°	SYM
iajs-524	41	5	c	c	NOUN
iajs-524	41	6	.	.	PUNCT
iajs-524	42	1	synthesis	synthesis	NOUN
iajs-524	42	2	of	of	ADP
iajs-524	42	3	potassium	potassium	NOUN
iajs-524	42	4	xanthate[12](4	xanthate[12](4	PRON
iajs-524	42	5	)	)	PUNCT
iajs-524	42	6	.	.	PUNCT
iajs-524	43	1	(	(	PUNCT
iajs-524	43	2	1	1	NUM
iajs-524	43	3	g	g	NOUN
iajs-524	43	4	,	,	PUNCT
iajs-524	43	5	0.004mol	0.004mol	NOUN
iajs-524	43	6	.	.	PUNCT
iajs-524	43	7	)	)	PUNCT
iajs-524	44	1	of	of	ADP
iajs-524	44	2	acid	acid	PROPN
iajs-524	44	3	hydrazide	hydrazide	ADV
iajs-524	44	4	(	(	PUNCT
iajs-524	44	5	3	3	X
iajs-524	44	6	)	)	PUNCT
iajs-524	44	7	was	be	AUX
iajs-524	44	8	dissolved	dissolve	VERB
iajs-524	44	9	in	in	ADP
iajs-524	44	10	absolute	absolute	ADJ
iajs-524	44	11	ethanol	ethanol	NOUN
iajs-524	44	12	99.9	99.9	NUM
iajs-524	44	13	%	%	NOUN
iajs-524	44	14	(	(	PUNCT
iajs-524	44	15	10	10	NUM
iajs-524	44	16	ml	ml	NOUN
iajs-524	44	17	)	)	PUNCT
iajs-524	44	18	with	with	ADP
iajs-524	44	19	(	(	PUNCT
iajs-524	44	20	0.23	0.23	NUM
iajs-524	44	21	g	g	NOUN
iajs-524	44	22	,	,	PUNCT
iajs-524	44	23	0.004mol	0.004mol	NOUN
iajs-524	44	24	.	.	PUNCT
iajs-524	44	25	)	)	PUNCT
iajs-524	44	26	of	of	ADP
iajs-524	44	27	potassium	potassium	NOUN
iajs-524	44	28	hydroxide	hydroxide	NOUN
iajs-524	44	29	.	.	PUNCT
iajs-524	45	1	the	the	DET
iajs-524	45	2	mixture	mixture	NOUN
iajs-524	45	3	was	be	AUX
iajs-524	45	4	stirred	stir	VERB
iajs-524	45	5	for	for	ADP
iajs-524	45	6	15	15	NUM
iajs-524	45	7	minute	minute	NOUN
iajs-524	45	8	then	then	ADV
iajs-524	45	9	(	(	PUNCT
iajs-524	45	10	0.31	0.31	NUM
iajs-524	45	11	g	g	NOUN
iajs-524	45	12	,	,	PUNCT
iajs-524	45	13	0.004mol	0.004mol	NOUN
iajs-524	45	14	.	.	PUNCT
iajs-524	45	15	)	)	PUNCT
iajs-524	45	16	of	of	ADP
iajs-524	45	17	carbon	carbon	NOUN
iajs-524	45	18	disulphide	disulphide	ADV
iajs-524	45	19	was	be	AUX
iajs-524	45	20	added	add	VERB
iajs-524	45	21	,	,	PUNCT
iajs-524	45	22	and	and	CCONJ
iajs-524	45	23	continue	continue	VERB
iajs-524	45	24	stirring	stir	VERB
iajs-524	45	25	for	for	ADP
iajs-524	45	26	24	24	NUM
iajs-524	45	27	hrs	hrs	NOUN
iajs-524	45	28	.	.	PUNCT
iajs-524	46	1	at	at	ADP
iajs-524	46	2	room	room	NOUN
iajs-524	46	3	temperature	temperature	NOUN
iajs-524	46	4	,	,	PUNCT
iajs-524	46	5	the	the	DET
iajs-524	46	6	precipitate	precipitate	NOUN
iajs-524	46	7	was	be	AUX
iajs-524	46	8	filtered	filter	VERB
iajs-524	46	9	and	and	CCONJ
iajs-524	46	10	dried	dry	VERB
iajs-524	46	11	,	,	PUNCT
iajs-524	46	12	washed	wash	VERB
iajs-524	46	13	with	with	ADP
iajs-524	46	14	ether	ether	NOUN
iajs-524	46	15	,	,	PUNCT
iajs-524	46	16	yield	yield	NOUN
iajs-524	46	17	(	(	PUNCT
iajs-524	46	18	0.74	0.74	NUM
iajs-524	46	19	g	g	NOUN
iajs-524	46	20	,	,	PUNCT
iajs-524	46	21	50	50	NUM
iajs-524	46	22	%	%	NOUN
iajs-524	46	23	)	)	PUNCT
iajs-524	46	24	,	,	PUNCT
iajs-524	46	25	mp	mp	PROPN
iajs-524	46	26	(	(	PUNCT
iajs-524	46	27	280	280	NUM
iajs-524	46	28	°	°	NOUN
iajs-524	46	29	c	c	PROPN
iajs-524	46	30	dec	dec	PROPN
iajs-524	46	31	.	.	PROPN
iajs-524	46	32	)	)	PUNCT
iajs-524	46	33	.	.	PUNCT
iajs-524	47	1	synthesis	synthesis	NOUN
iajs-524	47	2	of	of	ADP
iajs-524	47	3	5-(mercapto-1,3,4	5-(mercapto-1,3,4	NUM
iajs-524	47	4	-	-	PUNCT
iajs-524	47	5	thiadiazole-2yl	thiadiazole-2yl	NOUN
iajs-524	47	6	)	)	PUNCT
iajs-524	47	7	(	(	PUNCT
iajs-524	47	8	diphenyl	diphenyl	NOUN
iajs-524	47	9	)	)	PUNCT
iajs-524	47	10	methanol[5	methanol[5	NOUN
iajs-524	47	11	]	]	PUNCT
iajs-524	47	12	.	.	PUNCT
iajs-524	48	1	potassium	potassium	NOUN
iajs-524	48	2	xanthate	xanthate	NOUN
iajs-524	48	3	(	(	PUNCT
iajs-524	48	4	4	4	NUM
iajs-524	48	5	)	)	PUNCT
iajs-524	48	6	(	(	PUNCT
iajs-524	48	7	0.76	0.76	NUM
iajs-524	48	8	g	g	NOUN
iajs-524	48	9	,	,	PUNCT
iajs-524	48	10	0.002	0.002	NUM
iajs-524	48	11	mol	mol	NOUN
iajs-524	48	12	.	.	PUNCT
iajs-524	48	13	)	)	PUNCT
iajs-524	48	14	was	be	AUX
iajs-524	48	15	dissolved	dissolve	VERB
iajs-524	48	16	in	in	ADP
iajs-524	48	17	distilled	distil	VERB
iajs-524	48	18	cold	cold	ADJ
iajs-524	48	19	water	water	NOUN
iajs-524	48	20	and	and	CCONJ
iajs-524	48	21	then	then	ADV
iajs-524	48	22	carefully	carefully	ADV
iajs-524	48	23	acidified	acidify	VERB
iajs-524	48	24	with	with	ADP
iajs-524	48	25	conc	conc	NOUN
iajs-524	48	26	.	.	PUNCT
iajs-524	49	1	sulphuric	sulphuric	PROPN
iajs-524	49	2	acid	acid	PROPN
iajs-524	49	3	(	(	PUNCT
iajs-524	49	4	h2so4	h2so4	PROPN
iajs-524	49	5	)	)	PUNCT
iajs-524	49	6	98	98	NUM
iajs-524	49	7	%	%	NOUN
iajs-524	49	8	at	at	ADP
iajs-524	49	9	(	(	PUNCT
iajs-524	49	10	0–5)	0–5)	NOUN
iajs-524	49	11	°	°	ADP
iajs-524	49	12	c	c	NOUN
iajs-524	49	13	until	until	SCONJ
iajs-524	49	14	the	the	DET
iajs-524	49	15	precipitate	precipitate	NOUN
iajs-524	49	16	formed	form	VERB
iajs-524	49	17	.	.	PUNCT
iajs-524	50	1	the	the	DET
iajs-524	50	2	precipitate	precipitate	NOUN
iajs-524	50	3	was	be	AUX
iajs-524	50	4	filtered	filter	VERB
iajs-524	50	5	and	and	CCONJ
iajs-524	50	6	dried	dry	VERB
iajs-524	50	7	,	,	PUNCT
iajs-524	50	8	recrystillization	recrystillization	NOUN
iajs-524	50	9	from	from	ADP
iajs-524	50	10	ethanol	ethanol	NOUN
iajs-524	50	11	.	.	PUNCT
iajs-524	51	1	yielding	yield	VERB
iajs-524	51	2	comp	comp	NOUN
iajs-524	51	3	.	.	PUNCT
iajs-524	52	1	(	(	PUNCT
iajs-524	52	2	5	5	NUM
iajs-524	52	3	)	)	PUNCT
iajs-524	52	4	(	(	PUNCT
iajs-524	52	5	0.42	0.42	NUM
iajs-524	52	6	g	g	NOUN
iajs-524	52	7	,	,	PUNCT
iajs-524	52	8	66	66	NUM
iajs-524	52	9	%	%	NOUN
iajs-524	52	10	)	)	PUNCT
iajs-524	52	11	m.p	m.p	PROPN
iajs-524	52	12	122–124	122–124	NUM
iajs-524	52	13	°	°	PROPN
iajs-524	52	14	c	c	NOUN
iajs-524	52	15	.	.	PUNCT
iajs-524	53	1	187	187	NUM
iajs-524	53	2	|	|	ADV
iajs-524	53	3	chemistry	chemistry	NOUN
iajs-524	53	4	@@@@@@@@@@@@@@@@@úó‘ój	@@@@@@@@@@@@@@@@@úó‘ój	PROPN
iajs-524	53	5	�	�	PROPN
iajs-524	53	6	n€a@î@úœäñ€a@‚ï‹»‹€@·ró	n€a@î@úœäñ€a@‚ï‹»‹€@·ró	NUM
iajs-524	53	7	:	:	PUNCT
iajs-524	53	8	a@âig@ú‹	a@âig@ú‹	PROPN
iajs-524	53	9	©	©	PROPN
iajs-524	53	10	@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@ü‹1a26@@öü»€a@i1@‚b«@h2013	@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@ü‹1a26@@öü»€a@i1@‚b«@h2013	PROPN
iajs-524	53	11	ibn	ibn	PROPN
iajs-524	53	12	al	al	PROPN
iajs-524	53	13	-	-	PUNCT
iajs-524	53	14	haitham	haitham	PROPN
iajs-524	53	15	jour	jour	X
iajs-524	53	16	.	.	PROPN
iajs-524	54	1	for	for	ADP
iajs-524	54	2	pure	pure	ADJ
iajs-524	54	3	&	&	CCONJ
iajs-524	54	4	appl	appl	PROPN
iajs-524	54	5	.	.	PUNCT
iajs-524	55	1	sci	sci	PROPN
iajs-524	55	2	.	.	PUNCT
iajs-524	55	3	vol	vol	NOUN
iajs-524	55	4	.	.	PROPN
iajs-524	56	1	26	26	NUM
iajs-524	56	2	(	(	PUNCT
iajs-524	56	3	1	1	NUM
iajs-524	56	4	)	)	PUNCT
iajs-524	56	5	2013	2013	NUM
iajs-524	56	6	result	result	NOUN
iajs-524	56	7	and	and	CCONJ
iajs-524	56	8	discussion	discussion	NOUN
iajs-524	56	9	synthesis	synthesis	NOUN
iajs-524	56	10	and	and	CCONJ
iajs-524	56	11	identification	identification	NOUN
iajs-524	56	12	of	of	ADP
iajs-524	56	13	methyl	methyl	NOUN
iajs-524	56	14	α	α	PROPN
iajs-524	56	15	-	-	PUNCT
iajs-524	56	16	hydroxy	hydroxy	VERB
iajs-524	56	17	-	-	PUNCT
iajs-524	56	18	α	α	NOUN
iajs-524	56	19	,	,	PUNCT
iajs-524	56	20	α-(diphenyl	α-(diphenyl	NOUN
iajs-524	56	21	)	)	PUNCT
iajs-524	56	22	acetate	acetate	NOUN
iajs-524	57	1	[	[	X
iajs-524	57	2	2	2	NUM
iajs-524	57	3	]	]	PUNCT
iajs-524	57	4	.	.	PUNCT
iajs-524	58	1	the	the	DET
iajs-524	58	2	benzilic	benzilic	NOUN
iajs-524	58	3	acid	acid	NOUN
iajs-524	58	4	was	be	AUX
iajs-524	58	5	converted	convert	VERB
iajs-524	58	6	to	to	ADP
iajs-524	58	7	methyl	methyl	NOUN
iajs-524	58	8	-	-	PUNCT
iajs-524	58	9	α	α	NOUN
iajs-524	58	10	-	-	PUNCT
iajs-524	58	11	hydroxy	hydroxy	VERB
iajs-524	58	12	-	-	PUNCT
iajs-524	58	13	α	α	NOUN
iajs-524	58	14	,	,	PUNCT
iajs-524	58	15	α(diphenyl	α(diphenyl	NOUN
iajs-524	58	16	)	)	PUNCT
iajs-524	58	17	acetate	acetate	NOUN
iajs-524	58	18	(	(	PUNCT
iajs-524	58	19	2	2	NUM
iajs-524	58	20	)	)	PUNCT
iajs-524	58	21	by	by	ADP
iajs-524	58	22	the	the	DET
iajs-524	58	23	common	common	ADJ
iajs-524	58	24	esterification	esterification	NOUN
iajs-524	58	25	process	process	NOUN
iajs-524	58	26	,	,	PUNCT
iajs-524	58	27	using	use	VERB
iajs-524	58	28	dimethylsulphate	dimethylsulphate	NOUN
iajs-524	58	29	in	in	ADP
iajs-524	58	30	presence	presence	NOUN
iajs-524	58	31	of	of	ADP
iajs-524	58	32	anhydrous	anhydrous	ADJ
iajs-524	58	33	sodium	sodium	NOUN
iajs-524	58	34	carbonate	carbonate	NOUN
iajs-524	58	35	in	in	ADP
iajs-524	58	36	dry	dry	ADJ
iajs-524	58	37	acetone.the	acetone.the	DET
iajs-524	58	38	(	(	PUNCT
iajs-524	58	39	2	2	NUM
iajs-524	58	40	)	)	PUNCT
iajs-524	58	41	was	be	AUX
iajs-524	58	42	identified	identify	VERB
iajs-524	58	43	by	by	ADP
iajs-524	58	44	t.l.c	t.l.c	ADJ
iajs-524	58	45	,	,	PUNCT
iajs-524	58	46	m.p	m.p	PROPN
iajs-524	58	47	and	and	CCONJ
iajs-524	58	48	ft.ir	ft.ir	ADJ
iajs-524	58	49	spectra	spectra	NOUN
iajs-524	58	50	,	,	PUNCT
iajs-524	58	51	which	which	PRON
iajs-524	58	52	showed	show	VERB
iajs-524	58	53	the	the	DET
iajs-524	58	54	disappearance	disappearance	NOUN
iajs-524	58	55	of	of	ADP
iajs-524	58	56	the	the	DET
iajs-524	58	57	absorption	absorption	NOUN
iajs-524	58	58	band	band	NOUN
iajs-524	58	59	at	at	ADP
iajs-524	58	60	1720	1720	NUM
iajs-524	58	61	cm–1	cm–1	NUM
iajs-524	58	62	which	which	PRON
iajs-524	58	63	is	be	AUX
iajs-524	58	64	due	due	ADJ
iajs-524	58	65	to	to	ADP
iajs-524	58	66	stretching	stretch	VERB
iajs-524	58	67	vibration	vibration	NOUN
iajs-524	58	68	of	of	ADP
iajs-524	58	69	the	the	DET
iajs-524	58	70	carbonyl	carbonyl	NOUN
iajs-524	58	71	group	group	NOUN
iajs-524	58	72	of	of	ADP
iajs-524	58	73	the	the	DET
iajs-524	58	74	acid	acid	NOUN
iajs-524	58	75	,	,	PUNCT
iajs-524	58	76	while	while	SCONJ
iajs-524	58	77	appearance	appearance	NOUN
iajs-524	58	78	of	of	ADP
iajs-524	58	79	the	the	DET
iajs-524	58	80	characteristic	characteristic	ADJ
iajs-524	58	81	absorption	absorption	NOUN
iajs-524	58	82	band	band	NOUN
iajs-524	58	83	at	at	ADP
iajs-524	58	84	1722	1722	NUM
iajs-524	58	85	cm–1	cm–1	X
iajs-524	58	86	due	due	ADP
iajs-524	58	87	to	to	ADP
iajs-524	58	88	stretching	stretch	VERB
iajs-524	58	89	vibration	vibration	NOUN
iajs-524	58	90	of	of	ADP
iajs-524	58	91	the	the	DET
iajs-524	58	92	(	(	PUNCT
iajs-524	58	93	c	c	NOUN
iajs-524	58	94	=	=	NOUN
iajs-524	58	95	o	o	NOUN
iajs-524	58	96	)	)	PUNCT
iajs-524	58	97	for	for	ADP
iajs-524	58	98	the	the	DET
iajs-524	58	99	forming	form	VERB
iajs-524	58	100	ester	ester	NOUN
iajs-524	58	101	,	,	PUNCT
iajs-524	58	102	also	also	ADV
iajs-524	58	103	disappearance	disappearance	NOUN
iajs-524	58	104	of	of	ADP
iajs-524	58	105	the	the	DET
iajs-524	58	106	wide	wide	ADJ
iajs-524	58	107	absorption	absorption	NOUN
iajs-524	58	108	bands	band	NOUN
iajs-524	58	109	at	at	ADP
iajs-524	58	110	the	the	DET
iajs-524	58	111	region	region	NOUN
iajs-524	58	112	(	(	PUNCT
iajs-524	58	113	2838–3560	2838–3560	NOUN
iajs-524	58	114	)	)	PUNCT
iajs-524	58	115	cm–1	cm–1	PRON
iajs-524	58	116	which	which	PRON
iajs-524	58	117	belongs	belong	VERB
iajs-524	58	118	to	to	ADP
iajs-524	58	119	the	the	DET
iajs-524	58	120	stretching	stretch	VERB
iajs-524	58	121	vibration	vibration	NOUN
iajs-524	58	122	of	of	ADP
iajs-524	58	123	(	(	PUNCT
iajs-524	58	124	-oh	-oh	NOUN
iajs-524	58	125	)	)	PUNCT
iajs-524	58	126	group	group	NOUN
iajs-524	58	127	for	for	ADP
iajs-524	58	128	the	the	DET
iajs-524	58	129	benzilic	benzilic	NOUN
iajs-524	58	130	acid	acid	NOUN
iajs-524	58	131	also	also	ADV
iajs-524	58	132	appearance	appearance	NOUN
iajs-524	58	133	band	band	NOUN
iajs-524	58	134	at	at	ADP
iajs-524	58	135	1168	1168	NUM
iajs-524	58	136	cm	cm	NOUN
iajs-524	58	137	–	–	PUNCT
iajs-524	58	138	1	1	NUM
iajs-524	58	139	due	due	ADP
iajs-524	58	140	to	to	ADP
iajs-524	58	141	(	(	PUNCT
iajs-524	58	142	–	–	PUNCT
iajs-524	58	143	o	o	NOUN
iajs-524	58	144	–	–	PUNCT
iajs-524	58	145	ch3	ch3	NOUN
iajs-524	58	146	)	)	PUNCT
iajs-524	58	147	of	of	ADP
iajs-524	58	148	methyl	methyl	PROPN
iajs-524	58	149	benzilate	benzilate	PROPN
iajs-524	58	150	ester	ester	NOUN
iajs-524	58	151	.	.	PUNCT
iajs-524	59	1	synthesis	synthesis	NOUN
iajs-524	59	2	and	and	CCONJ
iajs-524	59	3	identification	identification	NOUN
iajs-524	59	4	of	of	ADP
iajs-524	59	5	α	α	NOUN
iajs-524	59	6	-	-	PUNCT
iajs-524	59	7	hydroxy	hydroxy	VERB
iajs-524	59	8	-	-	PUNCT
iajs-524	59	9	α	α	NOUN
iajs-524	59	10	,	,	PUNCT
iajs-524	59	11	α	α	NOUN
iajs-524	59	12	-	-	ADJ
iajs-524	59	13	diphenyl	diphenyl	NOUN
iajs-524	59	14	acid	acid	NOUN
iajs-524	59	15	hydrazide[3	hydrazide[3	NOUN
iajs-524	59	16	]	]	PUNCT
iajs-524	59	17	.	.	PUNCT
iajs-524	60	1	the	the	DET
iajs-524	60	2	reaction	reaction	NOUN
iajs-524	60	3	of	of	ADP
iajs-524	60	4	hydrazine	hydrazine	NOUN
iajs-524	60	5	hydrate	hydrate	NOUN
iajs-524	60	6	in	in	ADP
iajs-524	60	7	absolute	absolute	ADJ
iajs-524	60	8	ethanol	ethanol	NOUN
iajs-524	60	9	.	.	PUNCT
iajs-524	61	1	most	most	ADJ
iajs-524	61	2	common	common	ADJ
iajs-524	61	3	reactions	reaction	NOUN
iajs-524	61	4	to	to	PART
iajs-524	61	5	synthesize	synthesize	VERB
iajs-524	61	6	the	the	DET
iajs-524	61	7	acid	acid	NOUN
iajs-524	61	8	hydrazide	hydrazide	ADJ
iajs-524	61	9	derivatives	derivative	NOUN
iajs-524	61	10	.	.	PUNCT
iajs-524	62	1	the	the	DET
iajs-524	62	2	hydrazide	hydrazide	ADJ
iajs-524	62	3	derivatives	derivative	NOUN
iajs-524	62	4	were	be	AUX
iajs-524	62	5	identified	identify	VERB
iajs-524	62	6	by	by	ADP
iajs-524	62	7	m.p	m.p	PROPN
iajs-524	62	8	and	and	CCONJ
iajs-524	62	9	ft.ir	ft.ir	ADJ
iajs-524	62	10	spectra	spectra	NOUN
iajs-524	62	11	which	which	PRON
iajs-524	62	12	showed	show	VERB
iajs-524	62	13	the	the	DET
iajs-524	62	14	appearance	appearance	NOUN
iajs-524	62	15	of	of	ADP
iajs-524	62	16	the	the	DET
iajs-524	62	17	characteristic	characteristic	ADJ
iajs-524	62	18	absorption	absorption	NOUN
iajs-524	62	19	band	band	NOUN
iajs-524	62	20	at	at	ADP
iajs-524	62	21	the	the	DET
iajs-524	62	22	region	region	NOUN
iajs-524	62	23	(	(	PUNCT
iajs-524	62	24	3251–3300	3251–3300	NUM
iajs-524	62	25	)	)	PUNCT
iajs-524	62	26	cm–1	cm–1	X
iajs-524	62	27	due	due	ADP
iajs-524	62	28	to	to	ADP
iajs-524	62	29	the	the	DET
iajs-524	62	30	asymmetric	asymmetric	ADJ
iajs-524	62	31	and	and	CCONJ
iajs-524	62	32	symmetric	symmetric	ADJ
iajs-524	62	33	stretching	stretch	VERB
iajs-524	62	34	vibration	vibration	NOUN
iajs-524	62	35	of	of	ADP
iajs-524	62	36	the	the	DET
iajs-524	62	37	(	(	PUNCT
iajs-524	62	38	–	–	PUNCT
iajs-524	62	39	nh	nh	NOUN
iajs-524	62	40	–	–	PUNCT
iajs-524	62	41	nh2	nh2	NOUN
iajs-524	62	42	)	)	PUNCT
iajs-524	62	43	group	group	NOUN
iajs-524	62	44	,	,	PUNCT
iajs-524	62	45	the	the	DET
iajs-524	62	46	ft.ir	ft.ir	PROPN
iajs-524	62	47	also	also	ADV
iajs-524	62	48	showed	show	VERB
iajs-524	62	49	the	the	DET
iajs-524	62	50	disappearance	disappearance	NOUN
iajs-524	62	51	of	of	ADP
iajs-524	62	52	absorption	absorption	NOUN
iajs-524	62	53	bands	band	NOUN
iajs-524	62	54	at	at	ADP
iajs-524	62	55	the	the	DET
iajs-524	62	56	region	region	NOUN
iajs-524	62	57	1722	1722	NUM
iajs-524	62	58	cm–1	cm–1	X
iajs-524	62	59	due	due	ADJ
iajs-524	62	60	the	the	DET
iajs-524	62	61	stretching	stretch	VERB
iajs-524	62	62	vibration	vibration	NOUN
iajs-524	62	63	of	of	ADP
iajs-524	62	64	carbonyl	carbonyl	NOUN
iajs-524	62	65	group	group	NOUN
iajs-524	62	66	of	of	ADP
iajs-524	62	67	ester	ester	NOUN
iajs-524	62	68	,	,	PUNCT
iajs-524	62	69	while	while	SCONJ
iajs-524	62	70	a	a	DET
iajs-524	62	71	new	new	ADJ
iajs-524	62	72	band	band	NOUN
iajs-524	62	73	appeared	appear	VERB
iajs-524	62	74	at	at	ADP
iajs-524	62	75	the	the	DET
iajs-524	62	76	region	region	NOUN
iajs-524	62	77	1700	1700	NUM
iajs-524	62	78	cm–1	cm–1	X
iajs-524	62	79	due	due	ADP
iajs-524	62	80	to	to	ADP
iajs-524	62	81	stretching	stretch	VERB
iajs-524	62	82	vibration	vibration	NOUN
iajs-524	62	83	of	of	ADP
iajs-524	62	84	amide	amide	NOUN
iajs-524	62	85	band	band	NOUN
iajs-524	62	86	.	.	PUNCT
iajs-524	62	87	,	,	PUNCT
iajs-524	62	88	also	also	ADV
iajs-524	62	89	appearance	appearance	NOUN
iajs-524	62	90	band	band	NOUN
iajs-524	62	91	at	at	ADP
iajs-524	62	92	1537	1537	NUM
iajs-524	62	93	cm–1	cm–1	NUM
iajs-524	62	94	due	due	ADP
iajs-524	62	95	to	to	ADP
iajs-524	62	96	bending	bend	VERB
iajs-524	62	97	vibration	vibration	NOUN
iajs-524	62	98	of	of	ADP
iajs-524	62	99	(	(	PUNCT
iajs-524	62	100	n	n	CCONJ
iajs-524	62	101	–	–	PUNCT
iajs-524	62	102	h	h	NOUN
iajs-524	62	103	)	)	PUNCT
iajs-524	62	104	moiety	moiety	NOUN
iajs-524	62	105	.	.	PUNCT
iajs-524	63	1	synthesis	synthesis	NOUN
iajs-524	63	2	and	and	CCONJ
iajs-524	63	3	identification	identification	NOUN
iajs-524	63	4	of	of	ADP
iajs-524	63	5	potassium	potassium	NOUN
iajs-524	63	6	xanthate	xanthate	NOUN
iajs-524	64	1	[	[	X
iajs-524	64	2	4	4	NUM
iajs-524	64	3	]	]	PUNCT
iajs-524	64	4	.	.	PUNCT
iajs-524	65	1	the	the	DET
iajs-524	65	2	acid	acid	PROPN
iajs-524	65	3	hydrazide	hydrazide	NOUN
iajs-524	65	4	was	be	AUX
iajs-524	65	5	treated	treat	VERB
iajs-524	65	6	with	with	ADP
iajs-524	65	7	carbon	carbon	NOUN
iajs-524	65	8	disulphide	disulphide	ADV
iajs-524	65	9	in	in	ADP
iajs-524	65	10	potassium	potassium	NOUN
iajs-524	65	11	hydroxide	hydroxide	NOUN
iajs-524	65	12	to	to	PART
iajs-524	65	13	afford	afford	VERB
iajs-524	65	14	the	the	DET
iajs-524	65	15	salt	salt	NOUN
iajs-524	65	16	as	as	ADP
iajs-524	65	17	in	in	ADP
iajs-524	65	18	the	the	DET
iajs-524	65	19	following	following	ADJ
iajs-524	65	20	mechanism[14	mechanism[14	PROPN
iajs-524	65	21	]	]	PUNCT
iajs-524	65	22	.	.	PUNCT
iajs-524	66	1	188	188	NUM
iajs-524	66	2	|	|	ADV
iajs-524	66	3	chemistry	chemistry	NOUN
iajs-524	66	4	@@@@@@@@@@@@@@@@@úó‘ój	@@@@@@@@@@@@@@@@@úó‘ój	PROPN
iajs-524	66	5	�	�	PROPN
iajs-524	66	6	n€a@î@úœäñ€a@‚ï‹»‹€@·ró	n€a@î@úœäñ€a@‚ï‹»‹€@·ró	NUM
iajs-524	66	7	:	:	PUNCT
iajs-524	66	8	a@âig@ú‹	a@âig@ú‹	PROPN
iajs-524	66	9	©	©	PROPN
iajs-524	66	10	@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@ü‹1a26@@öü»€a@i1@‚b«@h2013	@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@ü‹1a26@@öü»€a@i1@‚b«@h2013	PROPN
iajs-524	66	11	ibn	ibn	PROPN
iajs-524	66	12	al	al	PROPN
iajs-524	66	13	-	-	PUNCT
iajs-524	66	14	haitham	haitham	PROPN
iajs-524	66	15	jour	jour	X
iajs-524	66	16	.	.	PROPN
iajs-524	66	17	for	for	ADP
iajs-524	66	18	pure	pure	ADJ
iajs-524	66	19	&	&	CCONJ
iajs-524	66	20	appl	appl	PROPN
iajs-524	66	21	.	.	PUNCT
iajs-524	67	1	sci	sci	PROPN
iajs-524	67	2	.	.	PUNCT
iajs-524	67	3	vol	vol	NOUN
iajs-524	67	4	.	.	PROPN
iajs-524	68	1	26	26	NUM
iajs-524	68	2	(	(	PUNCT
iajs-524	68	3	1	1	NUM
iajs-524	68	4	)	)	PUNCT
iajs-524	68	5	2013	2013	NUM
iajs-524	69	1	hph	hph	NOUN
iajs-524	69	2	c	c	NOUN
iajs-524	69	3	c	c	NOUN
iajs-524	70	1	oh	oh	INTJ
iajs-524	70	2	h	h	NOUN
iajs-524	70	3	n	n	ADV
iajs-524	70	4	ph	ph	NOUN
iajs-524	70	5	c	c	NOUN
iajs-524	70	6	sk	sk	INTJ
iajs-524	70	7	o	o	PROPN
iajs-524	70	8	h	h	NOUN
iajs-524	71	1	n	n	NOUN
iajs-524	71	2	s	s	NOUN
iajs-524	71	3	ph	ph	NOUN
iajs-524	71	4	c	c	NOUN
iajs-524	72	1	oh	oh	INTJ
iajs-524	72	2	ph	ph	INTJ
iajs-524	73	1	oh	oh	INTJ
iajs-524	73	2	c	c	INTJ
iajs-524	74	1	hn	hn	INTJ
iajs-524	74	2	c	c	NOUN
iajs-524	74	3	h	h	NOUN
iajs-524	75	1	n	n	NOUN
iajs-524	75	2	s	s	X
iajs-524	75	3	sk	sk	INTJ
iajs-524	75	4	ph	ph	PROPN
iajs-524	75	5	c	c	NOUN
iajs-524	76	1	oh	oh	INTJ
iajs-524	76	2	ph	ph	INTJ
iajs-524	76	3	nn	nn	PROPN
iajs-524	76	4	c	c	NOUN
iajs-524	76	5	s	s	PROPN
iajs-524	77	1	c	c	NOUN
iajs-524	77	2	h	h	NOUN
iajs-524	77	3	o	o	INTJ
iajs-524	77	4	sk	sk	INTJ
iajs-524	77	5	h	h	NOUN
iajs-524	77	6	-h2oph	-h2oph	PROPN
iajs-524	78	1	c	c	NOUN
iajs-524	79	1	oh	oh	INTJ
iajs-524	79	2	ph	ph	INTJ
iajs-524	79	3	nn	nn	PROPN
iajs-524	79	4	c	c	NOUN
iajs-524	79	5	s	s	PROPN
iajs-524	79	6	c	c	NOUN
iajs-524	79	7	sk	sk	PROPN
iajs-524	79	8	h	h	NOUN
iajs-524	79	9	ph	ph	PROPN
iajs-524	79	10	c	c	NOUN
iajs-524	79	11	oh	oh	INTJ
iajs-524	79	12	ph	ph	INTJ
iajs-524	79	13	nn	nn	PROPN
iajs-524	79	14	c	c	NOUN
iajs-524	79	15	s	s	PART
iajs-524	79	16	c	c	NOUN
iajs-524	79	17	sh	sh	NOUN
iajs-524	80	1	[	[	X
iajs-524	80	2	s31	s31	NOUN
iajs-524	80	3	]	]	PUNCT
iajs-524	80	4	the	the	DET
iajs-524	80	5	compound	compound	NOUN
iajs-524	80	6	(	(	PUNCT
iajs-524	80	7	4)identified	4)identifie	VERB
iajs-524	80	8	by	by	ADP
iajs-524	80	9	m.p	m.p	PROPN
iajs-524	80	10	and	and	CCONJ
iajs-524	80	11	ft.ir	ft.ir	PROPN
iajs-524	80	12	spectra	spectra	NOUN
iajs-524	80	13	,	,	PUNCT
iajs-524	80	14	the	the	DET
iajs-524	80	15	ft.ir	ft.ir	PROPN
iajs-524	80	16	spectra	spectra	NOUN
iajs-524	80	17	showed	show	VERB
iajs-524	80	18	the	the	DET
iajs-524	80	19	disappearance	disappearance	NOUN
iajs-524	80	20	of	of	ADP
iajs-524	80	21	absorption	absorption	NOUN
iajs-524	80	22	band	band	NOUN
iajs-524	80	23	at	at	ADP
iajs-524	80	24	the	the	DET
iajs-524	80	25	(	(	PUNCT
iajs-524	80	26	3251–3300	3251–3300	NUM
iajs-524	80	27	)	)	PUNCT
iajs-524	80	28	cm–1	cm–1	X
iajs-524	80	29	due	due	ADP
iajs-524	80	30	to	to	ADP
iajs-524	80	31	the	the	DET
iajs-524	80	32	asymmetric	asymmetric	ADJ
iajs-524	80	33	and	and	CCONJ
iajs-524	80	34	symmetric	symmetric	ADJ
iajs-524	80	35	stretching	stretch	VERB
iajs-524	80	36	vibration	vibration	NOUN
iajs-524	80	37	of	of	ADP
iajs-524	80	38	the	the	DET
iajs-524	80	39	(	(	PUNCT
iajs-524	80	40	–	–	PUNCT
iajs-524	80	41	nh	nh	NOUN
iajs-524	80	42	–	–	PUNCT
iajs-524	80	43	nh2	nh2	NOUN
iajs-524	80	44	)	)	PUNCT
iajs-524	80	45	group	group	NOUN
iajs-524	80	46	,	,	PUNCT
iajs-524	80	47	appearance	appearance	NOUN
iajs-524	80	48	band	band	NOUN
iajs-524	80	49	at	at	ADP
iajs-524	80	50	1049	1049	NUM
iajs-524	80	51	cm–1	cm–1	X
iajs-524	80	52	due	due	ADP
iajs-524	80	53	to	to	ADP
iajs-524	80	54	bending	bend	VERB
iajs-524	80	55	vibration	vibration	NOUN
iajs-524	80	56	of	of	ADP
iajs-524	80	57	(	(	PUNCT
iajs-524	80	58	c	c	NOUN
iajs-524	80	59	=	=	SYM
iajs-524	80	60	s)(15	s)(15	NOUN
iajs-524	80	61	)	)	PUNCT
iajs-524	80	62	,	,	PUNCT
iajs-524	80	63	also	also	ADV
iajs-524	80	64	appearance	appearance	NOUN
iajs-524	80	65	band	band	NOUN
iajs-524	80	66	at	at	ADP
iajs-524	80	67	(	(	PUNCT
iajs-524	80	68	1448–1492	1448–1492	NUM
iajs-524	80	69	)	)	PUNCT
iajs-524	80	70	cm–1	cm–1	X
iajs-524	80	71	due	due	ADP
iajs-524	80	72	to	to	PART
iajs-524	80	73	(	(	PUNCT
iajs-524	80	74	–	–	PUNCT
iajs-524	80	75	n	n	CCONJ
iajs-524	80	76	–	–	PUNCT
iajs-524	80	77	c	c	NOUN
iajs-524	80	78	=	=	SYM
iajs-524	80	79	s)(16	s)(16	NOUN
iajs-524	80	80	)	)	PUNCT
iajs-524	80	81	stretching	stretch	VERB
iajs-524	80	82	vibration	vibration	NOUN
iajs-524	80	83	this	this	DET
iajs-524	80	84	band	band	NOUN
iajs-524	80	85	according	accord	VERB
iajs-524	80	86	strong	strong	ADJ
iajs-524	80	87	evidence	evidence	NOUN
iajs-524	80	88	to	to	PART
iajs-524	80	89	presence	presence	VERB
iajs-524	80	90	the	the	DET
iajs-524	80	91	potassium	potassium	NOUN
iajs-524	80	92	xanthate	xanthate	NOUN
iajs-524	80	93	and	and	CCONJ
iajs-524	80	94	also	also	ADV
iajs-524	80	95	appearance	appearance	NOUN
iajs-524	80	96	band	band	NOUN
iajs-524	80	97	at	at	ADP
iajs-524	80	98	1614	1614	NUM
iajs-524	80	99	cm–1	cm–1	X
iajs-524	80	100	due	due	ADP
iajs-524	80	101	to	to	PART
iajs-524	80	102	(	(	PUNCT
iajs-524	80	103	c	c	NOUN
iajs-524	80	104	=	=	NOUN
iajs-524	80	105	o	o	NOUN
iajs-524	80	106	)	)	PUNCT
iajs-524	80	107	amide	amide	NOUN
iajs-524	80	108	while	while	SCONJ
iajs-524	80	109	disappearance	disappearance	NOUN
iajs-524	80	110	band	band	NOUN
iajs-524	80	111	at	at	ADP
iajs-524	80	112	1700	1700	NUM
iajs-524	80	113	cm–1	cm–1	NUM
iajs-524	80	114	due	due	ADP
iajs-524	80	115	to	to	PART
iajs-524	80	116	(	(	PUNCT
iajs-524	80	117	c	c	NOUN
iajs-524	80	118	=	=	NOUN
iajs-524	80	119	o	o	NOUN
iajs-524	80	120	)	)	PUNCT
iajs-524	80	121	of	of	ADP
iajs-524	80	122	α	α	NOUN
iajs-524	80	123	–	–	PUNCT
iajs-524	80	124	hydroxyl	hydroxyl	NOUN
iajs-524	80	125	–	–	PUNCT
iajs-524	80	126	α	α	NOUN
iajs-524	80	127	,	,	PUNCT
iajs-524	80	128	α	α	NOUN
iajs-524	80	129	–	–	PUNCT
iajs-524	80	130	diphenyl	diphenyl	NOUN
iajs-524	80	131	acetohydrazide	acetohydrazide	ADV
iajs-524	80	132	(	(	PUNCT
iajs-524	80	133	3	3	X
iajs-524	80	134	)	)	PUNCT
iajs-524	80	135	this	this	DET
iajs-524	80	136	two	two	NUM
iajs-524	80	137	evidence	evidence	NOUN
iajs-524	80	138	to	to	PART
iajs-524	80	139	presence	presence	VERB
iajs-524	80	140	this	this	DET
iajs-524	80	141	reaction	reaction	NOUN
iajs-524	80	142	.	.	PUNCT
iajs-524	81	1	synthesis	synthesis	NOUN
iajs-524	81	2	and	and	CCONJ
iajs-524	81	3	identification	identification	NOUN
iajs-524	81	4	of	of	ADP
iajs-524	81	5	5–(mercapto–1,3,4	5–(mercapto–1,3,4	NUM
iajs-524	81	6	–	–	PUNCT
iajs-524	81	7	thiadiazole–2	thiadiazole–2	NOUN
iajs-524	81	8	–	–	PUNCT
iajs-524	81	9	yl	yl	NOUN
iajs-524	81	10	)	)	PUNCT
iajs-524	81	11	(	(	PUNCT
iajs-524	81	12	diphenyl	diphenyl	NOUN
iajs-524	81	13	)	)	PUNCT
iajs-524	81	14	methanol	methanol	NOUN
iajs-524	81	15	(	(	PUNCT
iajs-524	81	16	5	5	NUM
iajs-524	81	17	)	)	PUNCT
iajs-524	81	18	.	.	PUNCT
iajs-524	82	1	the	the	DET
iajs-524	82	2	addition	addition	NOUN
iajs-524	82	3	of	of	ADP
iajs-524	82	4	sulphuric	sulphuric	ADJ
iajs-524	82	5	acid	acid	NOUN
iajs-524	82	6	95–98	95–98	NUM
iajs-524	82	7	%	%	NOUN
iajs-524	82	8	at	at	ADP
iajs-524	82	9	(	(	PUNCT
iajs-524	82	10	0–3	0–3	NOUN
iajs-524	82	11	)	)	PUNCT
iajs-524	82	12	°	°	PROPN
iajs-524	82	13	c	c	NOUN
iajs-524	82	14	lead	lead	NOUN
iajs-524	82	15	to	to	ADP
iajs-524	82	16	the	the	DET
iajs-524	82	17	cyclization	cyclization	NOUN
iajs-524	82	18	which	which	PRON
iajs-524	82	19	produce	produce	VERB
iajs-524	82	20	the	the	DET
iajs-524	82	21	thiadiazole	thiadiazole	NOUN
iajs-524	82	22	(	(	PUNCT
iajs-524	82	23	5	5	NUM
iajs-524	82	24	)	)	PUNCT
iajs-524	82	25	as	as	ADP
iajs-524	82	26	in	in	ADP
iajs-524	82	27	the	the	DET
iajs-524	82	28	following	following	NOUN
iajs-524	82	29	suggest	suggest	VERB
iajs-524	82	30	mechanism[17	mechanism[17	PROPN
iajs-524	82	31	]	]	X
iajs-524	82	32	:	:	PUNCT
iajs-524	82	33	the	the	DET
iajs-524	82	34	compound	compound	NOUN
iajs-524	83	1	[	[	X
iajs-524	83	2	5	5	NUM
iajs-524	83	3	]	]	PUNCT
iajs-524	83	4	was	be	AUX
iajs-524	83	5	identified	identify	VERB
iajs-524	83	6	by	by	ADP
iajs-524	83	7	m.p	m.p	PROPN
iajs-524	83	8	.	.	PROPN
iajs-524	83	9	ft.ir	ft.ir	PROPN
iajs-524	83	10	,	,	PUNCT
iajs-524	83	11	1h	1h	NUM
iajs-524	83	12	-	-	PUNCT
iajs-524	83	13	nmr	nmr	NOUN
iajs-524	83	14	spectroscopy	spectroscopy	NOUN
iajs-524	83	15	.	.	PUNCT
iajs-524	84	1	the	the	DET
iajs-524	84	2	ft.ir	ft.ir	PROPN
iajs-524	84	3	showed	show	VERB
iajs-524	84	4	band	band	NOUN
iajs-524	84	5	1060	1060	NUM
iajs-524	84	6	cm–1	cm–1	X
iajs-524	84	7	due	due	ADP
iajs-524	84	8	to	to	ADP
iajs-524	84	9	bending	bend	VERB
iajs-524	84	10	vibration	vibration	NOUN
iajs-524	84	11	of	of	ADP
iajs-524	84	12	(	(	PUNCT
iajs-524	84	13	c	c	NOUN
iajs-524	84	14	=	=	SYM
iajs-524	84	15	s)[15	s)[15	NOUN
iajs-524	84	16	]	]	X
iajs-524	84	17	group	group	NOUN
iajs-524	84	18	,	,	PUNCT
iajs-524	84	19	appearance	appearance	NOUN
iajs-524	84	20	band	band	NOUN
iajs-524	84	21	between	between	ADP
iajs-524	84	22	(	(	PUNCT
iajs-524	84	23	1685–1720	1685–1720	NUM
iajs-524	84	24	)	)	PUNCT
iajs-524	84	25	cm–1	cm–1	X
iajs-524	84	26	due	due	ADP
iajs-524	84	27	to	to	ADP
iajs-524	84	28	stretching	stretch	VERB
iajs-524	84	29	vibration	vibration	NOUN
iajs-524	84	30	of	of	ADP
iajs-524	84	31	(	(	PUNCT
iajs-524	84	32	c	c	NOUN
iajs-524	84	33	=	=	SYM
iajs-524	84	34	n	n	CCONJ
iajs-524	84	35	)	)	PUNCT
iajs-524	84	36	group	group	NOUN
iajs-524	84	37	,	,	PUNCT
iajs-524	84	38	also	also	ADV
iajs-524	84	39	appearance	appearance	NOUN
iajs-524	84	40	very	very	ADV
iajs-524	84	41	week	week	NOUN
iajs-524	84	42	band	band	NOUN
iajs-524	84	43	at	at	ADP
iajs-524	84	44	2478	2478	NUM
iajs-524	84	45	cm–1	cm–1	X
iajs-524	84	46	due	due	ADP
iajs-524	84	47	to	to	PART
iajs-524	84	48	(	(	PUNCT
iajs-524	84	49	s	s	NOUN
iajs-524	84	50	–	–	PUNCT
iajs-524	84	51	h	h	NOUN
iajs-524	84	52	)	)	PUNCT
iajs-524	84	53	group	group	NOUN
iajs-524	84	54	,	,	PUNCT
iajs-524	84	55	appearance	appearance	NOUN
iajs-524	84	56	strong	strong	ADJ
iajs-524	84	57	band	band	NOUN
iajs-524	84	58	at	at	ADP
iajs-524	84	59	(	(	PUNCT
iajs-524	84	60	1445–1496	1445–1496	NUM
iajs-524	84	61	)	)	PUNCT
iajs-524	84	62	cm–1	cm–1	X
iajs-524	84	63	due	due	ADP
iajs-524	84	64	to	to	ADP
iajs-524	84	65	stretching	stretch	VERB
iajs-524	84	66	vibration	vibration	NOUN
iajs-524	84	67	of	of	ADP
iajs-524	84	68	(	(	PUNCT
iajs-524	84	69	–	–	PUNCT
iajs-524	84	70	n	n	CCONJ
iajs-524	84	71	–	–	PUNCT
iajs-524	84	72	c	c	NOUN
iajs-524	84	73	=	=	SYM
iajs-524	84	74	s)[16	s)[16	NOUN
iajs-524	84	75	]	]	PUNCT
iajs-524	84	76	,	,	PUNCT
iajs-524	84	77	and	and	CCONJ
iajs-524	84	78	appearance	appearance	NOUN
iajs-524	84	79	band	band	NOUN
iajs-524	84	80	at	at	ADP
iajs-524	84	81	3049	3049	NUM
iajs-524	84	82	cm–1	cm–1	X
iajs-524	84	83	due	due	ADP
iajs-524	84	84	to	to	PART
iajs-524	84	85	(	(	PUNCT
iajs-524	84	86	c	c	NOUN
iajs-524	84	87	–	–	PUNCT
iajs-524	84	88	h	h	NOUN
iajs-524	84	89	)	)	PUNCT
iajs-524	84	90	aromatic	aromatic	NOUN
iajs-524	84	91	.	.	PUNCT
iajs-524	85	1	189	189	NUM
iajs-524	85	2	|	|	ADV
iajs-524	85	3	chemistry	chemistry	NOUN
iajs-524	85	4	@@@@@@@@@@@@@@@@@úó‘ój	@@@@@@@@@@@@@@@@@úó‘ój	PROPN
iajs-524	85	5	�	�	PROPN
iajs-524	85	6	n€a@î@úœäñ€a@‚ï‹»‹€@·ró	n€a@î@úœäñ€a@‚ï‹»‹€@·ró	NUM
iajs-524	85	7	:	:	PUNCT
iajs-524	85	8	a@âig@ú‹	a@âig@ú‹	PROPN
iajs-524	85	9	©	©	PROPN
iajs-524	85	10	@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@ü‹1a26@@öü»€a@i1@‚b«@h2013	@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@ü‹1a26@@öü»€a@i1@‚b«@h2013	PROPN
iajs-524	85	11	ibn	ibn	PROPN
iajs-524	85	12	al	al	PROPN
iajs-524	85	13	-	-	PUNCT
iajs-524	85	14	haitham	haitham	PROPN
iajs-524	85	15	jour	jour	X
iajs-524	85	16	.	.	PROPN
iajs-524	86	1	for	for	ADP
iajs-524	86	2	pure	pure	ADJ
iajs-524	86	3	&	&	CCONJ
iajs-524	86	4	appl	appl	PROPN
iajs-524	86	5	.	.	PUNCT
iajs-524	87	1	sci	sci	PROPN
iajs-524	87	2	.	.	PUNCT
iajs-524	87	3	vol	vol	NOUN
iajs-524	87	4	.	.	PROPN
iajs-524	88	1	26	26	NUM
iajs-524	88	2	(	(	PUNCT
iajs-524	88	3	1	1	NUM
iajs-524	88	4	)	)	PUNCT
iajs-524	88	5	2013	2013	NUM
iajs-524	88	6	1h	1h	NUM
iajs-524	88	7	–	–	PUNCT
iajs-524	88	8	nmr	nmr	NOUN
iajs-524	88	9	spectrum	spectrum	NOUN
iajs-524	88	10	showed	show	VERB
iajs-524	88	11	the	the	DET
iajs-524	88	12	following	follow	VERB
iajs-524	88	13	characteristics	characteristic	NOUN
iajs-524	88	14	chemical	chemical	ADJ
iajs-524	88	15	shifts	shift	NOUN
iajs-524	88	16	(	(	PUNCT
iajs-524	88	17	dmso	dmso	NOUN
iajs-524	88	18	as	as	ADP
iajs-524	88	19	a	a	DET
iajs-524	88	20	solvent	solvent	NOUN
iajs-524	88	21	)	)	PUNCT
iajs-524	88	22	were	be	AUX
iajs-524	88	23	appeared	appear	VERB
iajs-524	88	24	:	:	PUNCT
iajs-524	88	25	the	the	DET
iajs-524	88	26	singlet	singlet	ADJ
iajs-524	88	27	signal	signal	NOUN
iajs-524	88	28	at	at	ADP
iajs-524	88	29	δ	δ	PROPN
iajs-524	88	30	2.5	2.5	NUM
iajs-524	88	31	suggested	suggest	VERB
iajs-524	88	32	the	the	DET
iajs-524	88	33	attribution	attribution	NOUN
iajs-524	88	34	to	to	ADP
iajs-524	88	35	the	the	DET
iajs-524	88	36	proton	proton	NOUN
iajs-524	88	37	of	of	ADP
iajs-524	88	38	(	(	PUNCT
iajs-524	88	39	o	o	NOUN
iajs-524	88	40	–	–	PUNCT
iajs-524	88	41	h	h	NOUN
iajs-524	88	42	)	)	PUNCT
iajs-524	88	43	group	group	NOUN
iajs-524	88	44	,	,	PUNCT
iajs-524	88	45	while	while	SCONJ
iajs-524	88	46	a	a	DET
iajs-524	88	47	singlet	singlet	NOUN
iajs-524	88	48	at	at	ADP
iajs-524	88	49	δ	δ	PROPN
iajs-524	88	50	3.94	3.94	NUM
iajs-524	88	51	suggested	suggest	VERB
iajs-524	88	52	the	the	DET
iajs-524	88	53	attribution	attribution	NOUN
iajs-524	88	54	to	to	ADP
iajs-524	88	55	the	the	DET
iajs-524	88	56	proton	proton	NOUN
iajs-524	88	57	of	of	ADP
iajs-524	88	58	(	(	PUNCT
iajs-524	88	59	s	s	NOUN
iajs-524	88	60	–	–	PUNCT
iajs-524	88	61	h	h	NOUN
iajs-524	88	62	)	)	PUNCT
iajs-524	88	63	group	group	NOUN
iajs-524	88	64	,	,	PUNCT
iajs-524	88	65	[	[	X
iajs-524	88	66	addition	addition	NOUN
iajs-524	88	67	of	of	ADP
iajs-524	88	68	d2o	d2o	PROPN
iajs-524	88	69	caused	cause	VERB
iajs-524	88	70	the	the	DET
iajs-524	88	71	signal	signal	NOUN
iajs-524	88	72	at	at	ADP
iajs-524	88	73	δ	δ	PROPN
iajs-524	88	74	2.5	2.5	NUM
iajs-524	88	75	and	and	CCONJ
iajs-524	88	76	δ	δ	PROPN
iajs-524	88	77	3.94	3.94	NUM
iajs-524	88	78	to	to	PART
iajs-524	88	79	disappear	disappear	VERB
iajs-524	88	80	,	,	PUNCT
iajs-524	88	81	fig	fig	NOUN
iajs-524	88	82	.	.	PUNCT
iajs-524	89	1	(	(	PUNCT
iajs-524	89	2	3.44	3.44	NUM
iajs-524	89	3	)	)	PUNCT
iajs-524	89	4	]	]	PUNCT
iajs-524	89	5	,	,	PUNCT
iajs-524	89	6	the	the	DET
iajs-524	89	7	singlet	singlet	ADJ
iajs-524	89	8	signal	signal	NOUN
iajs-524	89	9	at	at	ADP
iajs-524	89	10	δ	δ	PROPN
iajs-524	89	11	7.3	7.3	NUM
iajs-524	89	12	suggesting	suggest	VERB
iajs-524	89	13	the	the	DET
iajs-524	89	14	attribution	attribution	NOUN
iajs-524	89	15	of	of	ADP
iajs-524	89	16	ten	ten	NUM
iajs-524	89	17	protons	proton	NOUN
iajs-524	89	18	of	of	ADP
iajs-524	89	19	two	two	NUM
iajs-524	89	20	benzene	benzene	NOUN
iajs-524	89	21	rings	ring	NOUN
iajs-524	89	22	.	.	PUNCT
iajs-524	90	1	references	reference	NOUN
iajs-524	90	2	1	1	NUM
iajs-524	90	3	.	.	PUNCT
iajs-524	91	1	palmer	palmer	PROPN
iajs-524	91	2	,	,	PUNCT
iajs-524	91	3	m.h	m.h	PROPN
iajs-524	91	4	.	.	PROPN
iajs-524	91	5	(	(	PUNCT
iajs-524	91	6	1967	1967	NUM
iajs-524	91	7	)	)	PUNCT
iajs-524	91	8	"	"	PUNCT
iajs-524	91	9	the	the	DET
iajs-524	91	10	structure	structure	NOUN
iajs-524	91	11	and	and	CCONJ
iajs-524	91	12	reactions	reaction	NOUN
iajs-524	91	13	of	of	ADP
iajs-524	91	14	heterocyclic	heterocyclic	ADJ
iajs-524	91	15	compounds	compound	NOUN
iajs-524	91	16	"	"	PUNCT
iajs-524	91	17	,	,	PUNCT
iajs-524	91	18	ed	ed	NOUN
iajs-524	91	19	.	.	PUNCT
iajs-524	92	1	by	by	ADP
iajs-524	92	2	e.	e.	PROPN
iajs-524	92	3	arnol	arnol	PROPN
iajs-524	92	4	,	,	PUNCT
iajs-524	92	5	academic	academic	ADJ
iajs-524	92	6	press	press	NOUN
iajs-524	92	7	.	.	PUNCT
iajs-524	92	8	inc	inc	PROPN
iajs-524	92	9	.	.	PROPN
iajs-524	92	10	,	,	PUNCT
iajs-524	92	11	london	london	PROPN
iajs-524	92	12	175	175	NUM
iajs-524	92	13	.	.	PUNCT
iajs-524	93	1	2	2	NUM
iajs-524	93	2	.	.	X
iajs-524	93	3	katarizky	katarizky	PROPN
iajs-524	93	4	,	,	PUNCT
iajs-524	93	5	a.	a.	PROPN
iajs-524	93	6	r.	r.	PROPN
iajs-524	93	7	and	and	CCONJ
iajs-524	93	8	boulton	boulton	PROPN
iajs-524	93	9	,	,	PUNCT
iajs-524	93	10	a.j	a.j	PROPN
iajs-524	93	11	.	.	PROPN
iajs-524	93	12	(	(	PUNCT
iajs-524	93	13	1966	1966	NUM
iajs-524	93	14	)	)	PUNCT
iajs-524	93	15	"	"	PUNCT
iajs-524	93	16	advances	advance	NOUN
iajs-524	93	17	in	in	ADP
iajs-524	93	18	heterocyclic	heterocyclic	ADJ
iajs-524	93	19	chemistry	chemistry	NOUN
iajs-524	93	20	"	"	PUNCT
iajs-524	93	21	,	,	PUNCT
iajs-524	93	22	academic	academic	ADJ
iajs-524	93	23	press	press	NOUN
iajs-524	93	24	.	.	PUNCT
iajs-524	94	1	new	new	PROPN
iajs-524	94	2	york	york	PROPN
iajs-524	94	3	7	7	NUM
iajs-524	94	4	:	:	SYM
iajs-524	94	5	52	52	NUM
iajs-524	94	6	3	3	NUM
iajs-524	94	7	.	.	PUNCT
iajs-524	95	1	gilchrist	gilchrist	PROPN
iajs-524	95	2	,	,	PUNCT
iajs-524	95	3	t.l	t.l	PROPN
iajs-524	95	4	.	.	PUNCT
iajs-524	95	5	(	(	PUNCT
iajs-524	95	6	1975	1975	NUM
iajs-524	95	7	)	)	PUNCT
iajs-524	95	8	"	"	PUNCT
iajs-524	95	9	aromatic	aromatic	ADJ
iajs-524	95	10	and	and	CCONJ
iajs-524	95	11	heteroaromatic	heteroaromatic	ADJ
iajs-524	95	12	chemistry	chemistry	NOUN
iajs-524	95	13	"	"	PUNCT
iajs-524	95	14	(	(	PUNCT
iajs-524	95	15	special	special	ADJ
iajs-524	95	16	list	list	NOUN
iajs-524	95	17	periodic	periodic	ADJ
iajs-524	95	18	reports	report	NOUN
iajs-524	95	19	)	)	PUNCT
iajs-524	95	20	,	,	PUNCT
iajs-524	95	21	the	the	DET
iajs-524	95	22	chemical	chemical	NOUN
iajs-524	95	23	society	society	NOUN
iajs-524	95	24	,	,	PUNCT
iajs-524	95	25	london	london	PROPN
iajs-524	95	26	,	,	PUNCT
iajs-524	95	27	3(11):123	3(11):123	PROPN
iajs-524	95	28	4	4	NUM
iajs-524	95	29	.	.	PUNCT
iajs-524	95	30	elderfield	elderfield	PROPN
iajs-524	95	31	,	,	PUNCT
iajs-524	95	32	r.	r.	PROPN
iajs-524	95	33	c.	c.	PROPN
iajs-524	95	34	(	(	PUNCT
iajs-524	95	35	1971	1971	NUM
iajs-524	95	36	)	)	PUNCT
iajs-524	95	37	"	"	PUNCT
iajs-524	95	38	heterocyclic	heterocyclic	ADJ
iajs-524	95	39	compounds	compound	NOUN
iajs-524	95	40	"	"	PUNCT
iajs-524	95	41	,	,	PUNCT
iajs-524	95	42	john	john	PROPN
iajs-524	95	43	wiley	wiley	PROPN
iajs-524	95	44	&	&	CCONJ
iajs-524	95	45	sons	sons	PROPN
iajs-524	95	46	,	,	PUNCT
iajs-524	95	47	inc	inc	PROPN
iajs-524	95	48	.	.	PROPN
iajs-524	95	49	,	,	PUNCT
iajs-524	95	50	new	new	PROPN
iajs-524	95	51	york	york	PROPN
iajs-524	95	52	,	,	PUNCT
iajs-524	95	53	7	7	NUM
iajs-524	95	54	:	:	PUNCT
iajs-524	95	55	384–461	384–461	NUM
iajs-524	95	56	5	5	NUM
iajs-524	95	57	.	.	PUNCT
iajs-524	95	58	guha	guha	PROPN
iajs-524	95	59	,	,	PUNCT
iajs-524	95	60	(	(	PUNCT
iajs-524	95	61	1922	1922	NUM
iajs-524	95	62	)	)	PUNCT
iajs-524	95	63	constitution	constitution	NOUN
iajs-524	95	64	of	of	ADP
iajs-524	95	65	the	the	DET
iajs-524	95	66	so	so	ADV
iajs-524	95	67	-	-	PUNCT
iajs-524	95	68	called	call	VERB
iajs-524	95	69	dithio	dithio	NOUN
iajs-524	95	70	-	-	PUNCT
iajs-524	95	71	urazole	urazole	NOUN
iajs-524	95	72	of	of	ADP
iajs-524	95	73	martin	martin	PROPN
iajs-524	95	74	freund	freund	PROPN
iajs-524	95	75	.	.	PUNCT
iajs-524	96	1	j.	j.	PROPN
iajs-524	96	2	am	am	PROPN
iajs-524	96	3	.	.	PUNCT
iajs-524	97	1	chem	chem	NOUN
iajs-524	97	2	.	.	PUNCT
iajs-524	98	1	soc	soc	PROPN
iajs-524	98	2	.	.	PUNCT
iajs-524	99	1	44:1510	44:1510	NUM
iajs-524	99	2	6	6	NUM
iajs-524	99	3	.	.	PUNCT
iajs-524	100	1	hiremath	hiremath	PROPN
iajs-524	100	2	,	,	PUNCT
iajs-524	100	3	s.p	s.p	PROPN
iajs-524	100	4	.	.	PUNCT
iajs-524	100	5	;	;	PUNCT
iajs-524	100	6	biradar	biradar	NOUN
iajs-524	100	7	,	,	PUNCT
iajs-524	100	8	j.s	j.s	PROPN
iajs-524	100	9	.	.	PROPN
iajs-524	100	10	and	and	CCONJ
iajs-524	100	11	kudari	kudari	PROPN
iajs-524	100	12	,	,	PUNCT
iajs-524	100	13	s.m	s.m	PROPN
iajs-524	100	14	.	.	PROPN
iajs-524	100	15	(	(	PUNCT
iajs-524	100	16	1984	1984	NUM
iajs-524	100	17	)	)	PUNCT
iajs-524	100	18	j.	j.	PROPN
iajs-524	100	19	indian	indian	PROPN
iajs-524	100	20	chem	chem	PROPN
iajs-524	100	21	.	.	PUNCT
iajs-524	101	1	soc	soc	PROPN
iajs-524	101	2	.	.	PUNCT
iajs-524	102	1	lxi	lxi	PROPN
iajs-524	102	2	:	:	PUNCT
iajs-524	102	3	74	74	NUM
iajs-524	102	4	7	7	NUM
iajs-524	102	5	.	.	PUNCT
iajs-524	103	1	zamani	zamani	PROPN
iajs-524	103	2	,	,	PUNCT
iajs-524	103	3	k.	k.	PROPN
iajs-524	103	4	;	;	PUNCT
iajs-524	103	5	faghihi	faghihi	PROPN
iajs-524	103	6	,	,	PUNCT
iajs-524	103	7	k.	k.	PROPN
iajs-524	103	8	;	;	PUNCT
iajs-524	103	9	tofighi	tofighi	PROPN
iajs-524	103	10	,	,	PUNCT
iajs-524	103	11	t.	t.	PROPN
iajs-524	103	12	and	and	CCONJ
iajs-524	103	13	mohammad	mohammad	PROPN
iajs-524	103	14	,	,	PUNCT
iajs-524	103	15	r.	r.	PROPN
iajs-524	103	16	(	(	PUNCT
iajs-524	103	17	2004	2004	NUM
iajs-524	103	18	)	)	PUNCT
iajs-524	103	19	synthesis	synthesis	NOUN
iajs-524	103	20	and	and	CCONJ
iajs-524	103	21	antimicrobial	antimicrobial	ADJ
iajs-524	103	22	activity	activity	NOUN
iajs-524	103	23	of	of	ADP
iajs-524	103	24	some	some	DET
iajs-524	103	25	pyridyl	pyridyl	NOUN
iajs-524	103	26	and	and	CCONJ
iajs-524	103	27	naphthyl	naphthyl	PROPN
iajs-524	103	28	substituted	substitute	VERB
iajs-524	103	29	1,2,4	1,2,4	NUM
iajs-524	103	30	-	-	PUNCT
iajs-524	103	31	triazole	triazole	NOUN
iajs-524	103	32	and	and	CCONJ
iajs-524	103	33	1,3,4	1,3,4	NUM
iajs-524	103	34	-	-	PUNCT
iajs-524	103	35	thiadiazole	thiadiazole	NOUN
iajs-524	103	36	derivatives	derivative	NOUN
iajs-524	103	37	,	,	PUNCT
iajs-524	103	38	turk	turk	PROPN
iajs-524	103	39	.	.	PUNCT
iajs-524	104	1	j.	j.	PROPN
iajs-524	104	2	chem	chem	PROPN
iajs-524	104	3	.	.	PUNCT
iajs-524	105	1	28:95	28:95	NUM
iajs-524	105	2	8	8	NUM
iajs-524	105	3	.	.	PUNCT
iajs-524	106	1	kurzer	kurzer	PROPN
iajs-524	106	2	,	,	PUNCT
iajs-524	106	3	f.	f.	PROPN
iajs-524	106	4	and	and	CCONJ
iajs-524	106	5	secker	secker	PROPN
iajs-524	106	6	,	,	PUNCT
iajs-524	106	7	j.l	j.l	PROPN
iajs-524	106	8	.	.	PROPN
iajs-524	106	9	(	(	PUNCT
iajs-524	106	10	1989	1989	NUM
iajs-524	106	11	)	)	PUNCT
iajs-524	106	12	addition	addition	NOUN
iajs-524	106	13	-	-	PUNCT
iajs-524	106	14	cyclization	cyclization	NOUN
iajs-524	106	15	of	of	ADP
iajs-524	106	16	ethoxy	ethoxy	ADJ
iajs-524	106	17	carbonyl	carbonyl	NOUN
iajs-524	106	18	isothiocyanate	isothiocyanate	NOUN
iajs-524	106	19	with	with	ADP
iajs-524	106	20	hydrazine	hydrazine	NOUN
iajs-524	106	21	derivatives	derivative	NOUN
iajs-524	106	22	as	as	ADP
iajs-524	106	23	asource	asource	NOUN
iajs-524	106	24	of	of	ADP
iajs-524	106	25	thiadiazoles	thiadiazole	NOUN
iajs-524	106	26	and	and	CCONJ
iajs-524	106	27	triazoles	triazole	NOUN
iajs-524	106	28	,	,	PUNCT
iajs-524	106	29	j.	j.	PROPN
iajs-524	106	30	heterocyclic	heterocyclic	PROPN
iajs-524	106	31	chem	chem	PROPN
iajs-524	106	32	.	.	PUNCT
iajs-524	107	1	26	26	NUM
iajs-524	107	2	:	:	SYM
iajs-524	107	3	355	355	NUM
iajs-524	107	4	9	9	NUM
iajs-524	107	5	.	.	PUNCT
iajs-524	108	1	önkol	önkol	NOUN
iajs-524	108	2	,	,	PUNCT
iajs-524	108	3	t.	t.	PROPN
iajs-524	108	4	;	;	PUNCT
iajs-524	108	5	çakir	çakir	PROPN
iajs-524	108	6	,	,	PUNCT
iajs-524	108	7	b.	b.	PROPN
iajs-524	108	8	and	and	CCONJ
iajs-524	108	9	şahin	şahin	PROPN
iajs-524	108	10	,	,	PUNCT
iajs-524	108	11	m.f	m.f	PROPN
iajs-524	108	12	.	.	PUNCT
iajs-524	108	13	(	(	PUNCT
iajs-524	108	14	2004	2004	NUM
iajs-524	108	15	)	)	PUNCT
iajs-524	108	16	şahin,"synthesis	şahin,"synthesis	NOUN
iajs-524	108	17	and	and	CCONJ
iajs-524	108	18	antinociceptive	antinociceptive	ADJ
iajs-524	108	19	activity	activity	NOUN
iajs-524	108	20	of	of	ADP
iajs-524	108	21	2-[(2	2-[(2	NOUN
iajs-524	108	22	-	-	PUNCT
iajs-524	108	23	oxobenzothiazoline-3	oxobenzothiazoline-3	NUM
iajs-524	108	24	-	-	PUNCT
iajs-524	108	25	yl)methyl]-5	yl)methyl]-5	NOUN
iajs-524	108	26	-	-	PUNCT
iajs-524	108	27	amino	amino	NOUN
iajs-524	108	28	alkyl	alkyl	NOUN
iajs-524	108	29	/	/	SYM
iajs-524	108	30	aryl-1,3,4	aryl-1,3,4	ADJ
iajs-524	108	31	-	-	PUNCT
iajs-524	108	32	thiadiazole	thiadiazole	NOUN
iajs-524	108	33	turk	turk	PROPN
iajs-524	108	34	.	.	PUNCT
iajs-524	109	1	j.	j.	PROPN
iajs-524	109	2	chem	chem	PROPN
iajs-524	109	3	.	.	PUNCT
iajs-524	110	1	28	28	NUM
iajs-524	110	2	:	:	PUNCT
iajs-524	110	3	461	461	NUM
iajs-524	110	4	.	.	NOUN
iajs-524	111	1	10	10	NUM
iajs-524	111	2	.	.	PUNCT
iajs-524	112	1	saoud	saoud	ADJ
iajs-524	112	2	,	,	PUNCT
iajs-524	112	3	s.a	s.a	PROPN
iajs-524	112	4	.	.	PROPN
iajs-524	113	1	(	(	PUNCT
iajs-524	113	2	2007	2007	NUM
iajs-524	113	3	)	)	PUNCT
iajs-524	113	4	m.sc	m.sc	PROPN
iajs-524	113	5	.	.	PUNCT
iajs-524	114	1	thesis	thesis	NOUN
iajs-524	114	2	,	,	PUNCT
iajs-524	114	3	college	college	NOUN
iajs-524	114	4	of	of	ADP
iajs-524	114	5	education	education	PROPN
iajs-524	114	6	ibn	ibn	PROPN
iajs-524	114	7	-	-	PUNCT
iajs-524	114	8	al	al	PROPN
iajs-524	114	9	-	-	PUNCT
iajs-524	114	10	haitham	haitham	PROPN
iajs-524	114	11	11	11	NUM
iajs-524	114	12	.	.	PUNCT
iajs-524	115	1	el	el	PROPN
iajs-524	115	2	–	–	PUNCT
iajs-524	115	3	tamaty	tamaty	NOUN
iajs-524	115	4	,	,	PUNCT
iajs-524	115	5	e.s	e.s	PROPN
iajs-524	115	6	.	.	PROPN
iajs-524	115	7	;	;	PUNCT
iajs-524	115	8	abdel	abdel	PROPN
iajs-524	115	9	–	–	PUNCT
iajs-524	115	10	fattah	fattah	PROPN
iajs-524	115	11	,	,	PUNCT
iajs-524	115	12	m.	m.	PROPN
iajs-524	115	13	e.	e.	PROPN
iajs-524	115	14	and	and	CCONJ
iajs-524	115	15	el	el	PROPN
iajs-524	115	16	–	–	PUNCT
iajs-524	115	17	deen	deen	PROPN
iajs-524	115	18	,	,	PUNCT
iajs-524	115	19	i.	i.	PROPN
iajs-524	115	20	m.	m.	PROPN
iajs-524	115	21	(	(	PUNCT
iajs-524	115	22	1996	1996	NUM
iajs-524	115	23	)	)	PUNCT
iajs-524	115	24	indian	indian	PROPN
iajs-524	115	25	j.	j.	PROPN
iajs-524	115	26	chem	chem	PROPN
iajs-524	115	27	.	.	PUNCT
iajs-524	115	28	,	,	PUNCT
iajs-524	115	29	35b:1067	35b:1067	NUM
iajs-524	115	30	12	12	NUM
iajs-524	115	31	.	.	PUNCT
iajs-524	116	1	ismaeel	ismaeel	PROPN
iajs-524	116	2	,	,	PUNCT
iajs-524	116	3	y.	y.	PROPN
iajs-524	116	4	m.	m.	PROPN
iajs-524	116	5	(	(	PUNCT
iajs-524	116	6	2003	2003	NUM
iajs-524	116	7	)	)	PUNCT
iajs-524	117	1	m.sc	m.sc	PROPN
iajs-524	117	2	.	.	PUNCT
iajs-524	118	1	thesis	thesis	NOUN
iajs-524	118	2	,	,	PUNCT
iajs-524	118	3	college	college	NOUN
iajs-524	118	4	of	of	ADP
iajs-524	118	5	education	education	PROPN
iajs-524	118	6	ibn	ibn	PROPN
iajs-524	118	7	al	al	PROPN
iajs-524	118	8	–	–	PUNCT
iajs-524	118	9	haitham	haitham	PROPN
iajs-524	118	10	baghdad	baghdad	PROPN
iajs-524	118	11	university	university	PROPN
iajs-524	118	12	,	,	PUNCT
iajs-524	118	13	iraq	iraq	PROPN
iajs-524	118	14	.	.	PUNCT
iajs-524	119	1	13	13	NUM
iajs-524	119	2	.	.	X
iajs-524	119	3	tao	tao	PROPN
iajs-524	119	4	,	,	PUNCT
iajs-524	119	5	e.	e.	PROPN
iajs-524	119	6	v.	v.	PROPN
iajs-524	119	7	and	and	CCONJ
iajs-524	119	8	christie	christie	PROPN
iajs-524	119	9	,	,	PUNCT
iajs-524	119	10	c.	c.	PROPN
iajs-524	119	11	f.	f.	PROPN
iajs-524	119	12	(	(	PUNCT
iajs-524	119	13	1975	1975	NUM
iajs-524	119	14	)	)	PUNCT
iajs-524	119	15	org	org	NOUN
iajs-524	119	16	.	.	PUNCT
iajs-524	120	1	prep	prep	PROPN
iajs-524	120	2	.	.	PUNCT
iajs-524	121	1	proced	proce	VERB
iajs-524	121	2	.	.	PUNCT
iajs-524	122	1	int	int	NOUN
iajs-524	122	2	.	.	PUNCT
iajs-524	123	1	7:179	7:179	NUM
iajs-524	123	2	14	14	NUM
iajs-524	123	3	.	.	PUNCT
iajs-524	124	1	hoggarth	hoggarth	PROPN
iajs-524	124	2	,	,	PUNCT
iajs-524	124	3	f.	f.	PROPN
iajs-524	124	4	(	(	PUNCT
iajs-524	124	5	1952	1952	NUM
iajs-524	124	6	)	)	PUNCT
iajs-524	124	7	j.	j.	PROPN
iajs-524	124	8	chem	chem	PROPN
iajs-524	124	9	.	.	PUNCT
iajs-524	125	1	soc	soc	PROPN
iajs-524	125	2	.	.	PUNCT
iajs-524	126	1	4811	4811	NUM
iajs-524	126	2	15	15	NUM
iajs-524	126	3	.	.	PUNCT
iajs-524	127	1	nadia	nadia	PROPN
iajs-524	127	2	,	,	PUNCT
iajs-524	127	3	a.	a.	PROPN
iajs-524	127	4	s.	s.	PROPN
iajs-524	127	5	(	(	PUNCT
iajs-524	127	6	2005	2005	NUM
iajs-524	127	7	)	)	PUNCT
iajs-524	127	8	ph	ph	PROPN
iajs-524	127	9	.	.	PROPN
iajs-524	127	10	d.	d.	PROPN
iajs-524	127	11	thesis	thesis	PROPN
iajs-524	127	12	,	,	PUNCT
iajs-524	127	13	college	college	NOUN
iajs-524	127	14	of	of	ADP
iajs-524	127	15	science	science	PROPN
iajs-524	127	16	,	,	PUNCT
iajs-524	127	17	al	al	PROPN
iajs-524	127	18	–	–	PROPN
iajs-524	127	19	nahrain	nahrain	PROPN
iajs-524	127	20	university	university	PROPN
iajs-524	127	21	,	,	PUNCT
iajs-524	127	22	iraq	iraq	PROPN
iajs-524	127	23	.	.	PUNCT
iajs-524	128	1	16	16	NUM
iajs-524	128	2	.	.	PUNCT
iajs-524	129	1	koji	koji	PROPN
iajs-524	129	2	,	,	PUNCT
iajs-524	129	3	n.	n.	PROPN
iajs-524	129	4	(	(	PUNCT
iajs-524	129	5	1962	1962	NUM
iajs-524	129	6	)	)	PUNCT
iajs-524	129	7	.	.	PUNCT
iajs-524	130	1	"	"	PUNCT
iajs-524	130	2	infrared	infrared	ADJ
iajs-524	130	3	absorption	absorption	NOUN
iajs-524	130	4	spectroscopy	spectroscopy	NOUN
iajs-524	130	5	"	"	PUNCT
iajs-524	130	6	nankoda	nankoda	PROPN
iajs-524	130	7	company	company	NOUN
iajs-524	130	8	limited	limit	VERB
iajs-524	130	9	,	,	PUNCT
iajs-524	130	10	tokyo	tokyo	PROPN
iajs-524	130	11	,	,	PUNCT
iajs-524	130	12	pp	pp	ADP
iajs-524	130	13	.	.	PUNCT
iajs-524	131	1	54	54	NUM
iajs-524	131	2	17	17	NUM
iajs-524	131	3	.	.	PUNCT
iajs-524	132	1	hassan	hassan	PROPN
iajs-524	132	2	,	,	PUNCT
iajs-524	132	3	a.j	a.j	PROPN
iajs-524	132	4	.	.	PROPN
iajs-524	132	5	(	(	PUNCT
iajs-524	132	6	2002	2002	NUM
iajs-524	132	7	)	)	PUNCT
iajs-524	132	8	m.sc	m.sc	PROPN
iajs-524	132	9	.	.	PROPN
iajs-524	132	10	,	,	PUNCT
iajs-524	132	11	thesis	thesis	NOUN
iajs-524	132	12	,	,	PUNCT
iajs-524	132	13	college	college	NOUN
iajs-524	132	14	of	of	ADP
iajs-524	132	15	baghdad	baghdad	PROPN
iajs-524	132	16	university	university	PROPN
iajs-524	132	17	,	,	PUNCT
iajs-524	132	18	iraq	iraq	PROPN
iajs-524	132	19	,	,	PUNCT
iajs-524	132	20	190	190	NUM
iajs-524	132	21	|	|	ADV
iajs-524	132	22	chemistry	chemistry	NOUN
iajs-524	132	23	@@@@@@@@@@@@@@@@@úó‘ój	@@@@@@@@@@@@@@@@@úó‘ój	PROPN
iajs-524	132	24	�	�	PROPN
iajs-524	132	25	n€a@î@úœäñ€a@‚ï‹»‹€@·ró	n€a@î@úœäñ€a@‚ï‹»‹€@·ró	NUM
iajs-524	132	26	:	:	PUNCT
iajs-524	132	27	a@âig@ú‹	a@âig@ú‹	PROPN
iajs-524	133	1	©	©	PROPN
iajs-524	133	2	@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@ü‹1a26@@öü»€a@i1@‚b«@h2013	@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@ü‹1a26@@öü»€a@i1@‚b«@h2013	PROPN
iajs-524	133	3	ibn	ibn	PROPN
iajs-524	133	4	al	al	PROPN
iajs-524	133	5	-	-	PUNCT
iajs-524	133	6	haitham	haitham	PROPN
iajs-524	133	7	jour	jour	X
iajs-524	133	8	.	.	PROPN
iajs-524	134	1	for	for	ADP
iajs-524	134	2	pure	pure	ADJ
iajs-524	134	3	&	&	CCONJ
iajs-524	134	4	appl	appl	PROPN
iajs-524	134	5	.	.	PUNCT
iajs-524	135	1	sci	sci	PROPN
iajs-524	135	2	.	.	PUNCT
iajs-524	135	3	vol	vol	NOUN
iajs-524	135	4	.	.	PROPN
iajs-524	136	1	26	26	NUM
iajs-524	136	2	(	(	PUNCT
iajs-524	136	3	1	1	NUM
iajs-524	136	4	)	)	PUNCT
iajs-524	136	5	2013	2013	NUM
iajs-524	136	6	scheme	scheme	NOUN
iajs-524	136	7	(	(	PUNCT
iajs-524	136	8	3	3	NUM
iajs-524	136	9	)	)	SYM
iajs-524	136	10	191	191	NUM
iajs-524	137	1	|	|	ADV
iajs-524	137	2	chemistry	chemistry	NOUN
iajs-524	137	3	@@@@@@@@@@@@@@@@@úó‘ój	@@@@@@@@@@@@@@@@@úó‘ój	PROPN
iajs-524	137	4	�	�	PROPN
iajs-524	137	5	n€a@î@úœäñ€a@‚ï‹»‹€@·ró	n€a@î@úœäñ€a@‚ï‹»‹€@·ró	NUM
iajs-524	137	6	:	:	PUNCT
iajs-524	137	7	a@âig@ú‹	a@âig@ú‹	PROPN
iajs-524	137	8	©	©	PROPN
iajs-524	137	9	@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@ü‹1a26@@öü»€a@i1@‚b«@h2013	@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@@ü‹1a26@@öü»€a@i1@‚b«@h2013	PROPN
iajs-524	137	10	ibn	ibn	PROPN
iajs-524	137	11	al	al	PROPN
iajs-524	137	12	-	-	PUNCT
iajs-524	137	13	haitham	haitham	PROPN
iajs-524	137	14	jour	jour	X
iajs-524	137	15	.	.	PROPN
iajs-524	138	1	for	for	ADP
iajs-524	138	2	pure	pure	ADJ
iajs-524	138	3	&	&	CCONJ
iajs-524	138	4	appl	appl	PROPN
iajs-524	138	5	.	.	PUNCT
iajs-524	139	1	sci	sci	PROPN
iajs-524	139	2	.	.	PUNCT
iajs-524	139	3	vol	vol	NOUN
iajs-524	139	4	.	.	PROPN
iajs-524	140	1	26	26	NUM
iajs-524	140	2	(	(	PUNCT
iajs-524	140	3	1	1	NUM
iajs-524	140	4	)	)	PUNCT
iajs-524	140	5	2013	2013	NUM
iajs-524	140	6	ثنائي	ثنائي	NOUN
iajs-524	140	7	فنیل	فنیل	NOUN
iajs-524	140	8	-α	-α	PROPN
iajs-524	140	9	,	,	PUNCT
iajs-524	140	10	α	α	X
iajs-524	140	11	-	-	PUNCT
iajs-524	140	12	یل)-2	یل)-2	NOUN
iajs-524	140	13	-	-	PUNCT
iajs-524	140	14	ثایادایزول-4,3,1-(مركبتو-5تحضیر	ثایادایزول-4,3,1-(مركبتو-5تحضیر	ADJ
iajs-524	140	15	وتشخیص	وتشخیص	NOUN
iajs-524	140	16	المركب	المركب	NOUN
iajs-524	140	17	میثانول	میثانول	NOUN
iajs-524	140	18	من	من	PROPN
iajs-524	140	19	حامض	حامض	PROPN
iajs-524	140	20	البنزیلك	البنزیلك	PROPN
iajs-524	140	21	مھند	مھند	PROPN
iajs-524	140	22	جمیل	جمیل	PROPN
iajs-524	140	23	محمود	محمود	PROPN
iajs-524	140	24	جامعة	جامعة	PROPN
iajs-524	140	25	بغداد	بغداد	PROPN
iajs-524	140	26	/	/	SYM
iajs-524	140	27	)	)	PUNCT
iajs-524	140	28	ابن	ابن	PROPN
iajs-524	140	29	الھیثم(كلیة	الھیثم(كلیة	PROPN
iajs-524	140	30	التربیة	التربیة	NOUN
iajs-524	140	31	للعلوم	للعلوم	NOUN
iajs-524	140	32	الصرفة	الصرفة	NOUN
iajs-524	140	33	/	/	PUNCT
iajs-524	141	1	قسم	قسم	PROPN
iajs-524	141	2	الكیمیاء	الكیمیاء	PROPN
iajs-524	141	3	رضا	رضا	PROPN
iajs-524	141	4	أبراھیم	أبراھیم	PROPN
iajs-524	141	5	البیاتي	البیاتي	ADV
iajs-524	141	6	الجامعة	الجامعة	VERB
iajs-524	141	7	المستنصریة	المستنصریة	PROPN
iajs-524	141	8	/كلیة	/كلیة	PUNCT
iajs-524	141	9	العلوم	العلوم	PROPN
iajs-524	141	10	/قسم	/قسم	PROPN
iajs-524	141	11	الكیمیاء	الكیمیاء	ADJ
iajs-524	141	12	شیماء	شیماء	PROPN
iajs-524	141	13	عبد	عبد	VERB
iajs-524	141	14	سعود	سعود	NOUN
iajs-524	141	15	أسماعیل	أسماعیل	PROPN
iajs-524	141	16	یاسین	یاسین	PROPN
iajs-524	141	17	مجید	مجید	PROPN
iajs-524	141	18	جامعة	جامعة	PROPN
iajs-524	141	19	بغداد	بغداد	PROPN
iajs-524	141	20	/	/	SYM
iajs-524	141	21	)	)	PUNCT
iajs-524	141	22	ابن	ابن	PROPN
iajs-524	141	23	الھیثم(كلیة	الھیثم(كلیة	PROPN
iajs-524	141	24	التربیة	التربیة	NOUN
iajs-524	141	25	للعلوم	للعلوم	NOUN
iajs-524	141	26	الصرفة	الصرفة	NOUN
iajs-524	141	27	/	/	PUNCT
iajs-524	142	1	قسم	قسم	PROPN
iajs-524	142	2	الكیمیاء	الكیمیاء	VERB
iajs-524	143	1	2008حزیران	2008حزیران	NUM
iajs-524	143	2	25	25	NUM
iajs-524	143	3	:	:	PUNCT
iajs-524	143	4	قبل	قبل	NOUN
iajs-524	143	5	البحث	البحث	VERB
iajs-524	143	6	في	في	PRON
iajs-524	143	7	،	،	PROPN
iajs-524	143	8	2007كانون	2007كانون	PROPN
iajs-524	143	9	األول	األول	PROPN
iajs-524	143	10	31استلم	31استلم	NUM
iajs-524	143	11	البحث	البحث	VERB
iajs-524	143	12	في	في	PRON
iajs-524	143	13	:	:	PUNCT
iajs-524	143	14	الخالصة	الخالصة	PROPN
iajs-524	143	15	الذي	الذي	PROPN
iajs-524	143	16	(	(	PUNCT
iajs-524	143	17	ثنائي	ثنائي	PROPN
iajs-524	143	18	فنیل	فنیل	VERB
iajs-524	143	19	میثانول	میثانول	NOUN
iajs-524	143	20	بالغلق	بالغلق	PROPN
iajs-524	143	21	الحلقي	الحلقي	PROPN
iajs-524	143	22	لملح	لملح	ADJ
iajs-524	143	23	الزانثیت	الزانثیت	PROPN
iajs-524	144	1	-α	-α	PROPN
iajs-524	144	2	,	,	PUNCT
iajs-524	144	3	α	α	NOUN
iajs-524	144	4	-	-	PUNCT
iajs-524	144	5	یل)-2	یل)-2	NOUN
iajs-524	144	6	-	-	NUM
iajs-524	144	7	ثایادایزول-4,3,1-(مركبتو-5	ثایادایزول-4,3,1-(مركبتو-5	ADJ
iajs-524	144	8	حضر	حضر	PROPN
iajs-524	144	9	المركب	المركب	PROPN
iajs-524	144	10	ربون	ربون	VERB
iajs-524	144	11	بوجود	بوجود	ADP
iajs-524	144	12	ھیدروكسید	ھیدروكسید	ADJ
iajs-524	144	13	كبریتید	كبریتید	NOUN
iajs-524	144	14	الكاحضر	الكاحضر	PROPN
iajs-524	145	1	من	من	PROPN
iajs-524	145	2	تفاعل	تفاعل	PROPN
iajs-524	145	3	مركب	مركب	PROPN
iajs-524	145	4	الھایدرازاید	الھایدرازاید	PROPN
iajs-524	145	5	(	(	PUNCT
iajs-524	145	6	المشتق	المشتق	VERB
iajs-524	145	7	من	من	PROPN
iajs-524	145	8	حامض	حامض	PROPN
iajs-524	145	9	البنزایلك	البنزایلك	PROPN
iajs-524	145	10	)	)	PUNCT
iajs-524	145	11	مع	مع	VERB
iajs-524	145	12	ثنائي	ثنائي	ADV
iajs-524	145	13	)	)	PUNCT
iajs-524	145	14	كما	كما	VERB
iajs-524	145	15	موضح	موضح	NOUN
iajs-524	145	16	في	في	SCONJ
iajs-524	145	17	المخطط.5	المخطط.5	PROPN
iajs-524	145	18	-مع	-مع	ADP
iajs-524	145	19	حامض	حامض	PROPN
iajs-524	145	20	الكبریتیك	الكبریتیك	PROPN
iajs-524	145	21	المركز	المركز	PROPN
iajs-524	145	22	في	في	ADP
iajs-524	145	23	درجة	درجة	ADJ
iajs-524	145	24	حرارة	حرارة	NOUN
iajs-524	145	25	(	(	PUNCT
iajs-524	145	26	صفر	صفر	NOUN
iajs-524	145	27	)	)	PUNCT
iajs-524	145	28	البوتاسیوم	البوتاسیوم	PROPN
iajs-524	146	1	وشخصت	وشخصت	PROPN
iajs-524	146	2	المركبات	المركبات	PROPN
iajs-524	146	3	المحضرة	المحضرة	PROPN
iajs-524	146	4	بكرموتوكرافیا	بكرموتوكرافیا	VERB
iajs-524	146	5	الطبقة	الطبقة	PROPN
iajs-524	146	6	الرقیقة	الرقیقة	PROPN
iajs-524	146	7	،	،	PROPN
iajs-524	146	8	درجة	درجة	PROPN
iajs-524	146	9	االنصھار	االنصھار	PROPN
iajs-524	146	10	،	،	PROPN
iajs-524	146	11	مطیافیة	مطیافیة	PROPN
iajs-524	146	12	االشعة	االشعة	PROPN
iajs-524	146	13	تحت	تحت	PROPN
iajs-524	146	14	الحمراء	الحمراء	PROPN
iajs-524	146	15	والرنین	والرنین	PROPN
iajs-524	146	16	النووي	النووي	PROPN
iajs-524	146	17	المغناطیسي	المغناطیسي	PROPN
iajs-524	146	18	.	.	PUNCT
iajs-524	147	1	ثایادایزول	ثایادایزول	PROPN
iajs-524	148	1	-4,3,1	-4,3,1	ADJ
iajs-524	148	2	:	:	PUNCT
iajs-524	148	3	مشتق	مشتق	PROPN
iajs-524	148	4	احیةالكلمات	احیةالكلمات	VERB
iajs-524	148	5	المفت	المفت	PROPN
iajs-524	148	6	192	192	NUM
iajs-524	148	7	|	|	NOUN
iajs-524	148	8	chemistry	chemistry	NOUN
iajs-524	148	9	muhanned	muhanne	VERB
iajs-524	148	10	j.	j.	PROPN
iajs-524	148	11	mahmoud	mahmoud	PROPN
iajs-524	148	12	redha	redha	PROPN
iajs-524	148	13	i.	i.	PROPN
iajs-524	148	14	al	al	PROPN
iajs-524	148	15	-	-	PUNCT
iajs-524	148	16	bayati	bayati	PROPN
iajs-524	148	17	department	department	NOUN
iajs-524	148	18	of	of	ADP
iajs-524	148	19	chemistry	chemistry	NOUN
iajs-524	148	20	-	-	PUNCT
iajs-524	148	21	college	college	NOUN
iajs-524	148	22	of	of	ADP
iajs-524	148	23	science	science	NOUN
iajs-524	148	24	-	-	PUNCT
iajs-524	148	25	university	university	NOUN
iajs-524	148	26	of	of	ADP
iajs-524	148	27	mustansiriya	mustansiriya	PROPN
iajs-524	148	28	shaimaa	shaimaa	PROPN
iajs-524	148	29	a.	a.	PROPN
iajs-524	148	30	saoud	saoud	PROPN
iajs-524	149	1	ismaeel	ismaeel	PROPN
iajs-524	149	2	y.	y.	PROPN
iajs-524	149	3	majeed	majeed	PROPN