id	sid	tid	token	lemma	pos
iajs-850	1	1	2011	2011	NUM
iajs-850	1	2	)	)	PUNCT
iajs-850	1	3	1	1	NUM
iajs-850	1	4	(	(	PUNCT
iajs-850	1	5	24المجلد	24المجلد	NUM
iajs-850	1	6	مجلة	مجلة	VERB
iajs-850	1	7	ابن	ابن	PROPN
iajs-850	1	8	الھیثم	الھیثم	PROPN
iajs-850	1	9	للعلوم	للعلوم	PROPN
iajs-850	1	10	الصرفة	الصرفة	PROPN
iajs-850	1	11	والتطبیقیة	والتطبیقیة	PROPN
iajs-850	1	12	ارثرواسكوربیك	ارثرواسكوربیك	PROPN
iajs-850	1	13	-	-	PUNCT
iajs-850	1	14	dبتیورات	dبتیورات	NOUN
iajs-850	1	15	لحامض	لحامض	NOUN
iajs-850	1	16	ر	ر	X
iajs-850	1	17	مشتقات	مشتقات	VERB
iajs-850	1	18	من	من	PRON
iajs-850	1	19	الباتحضیر	الباتحضیر	NOUN
iajs-850	1	20	2010أیلول	2010أیلول	PROPN
iajs-850	1	21	15	15	NUM
iajs-850	1	22	:	:	PUNCT
iajs-850	1	23	استلم	استلم	PROPN
iajs-850	1	24	البحث	البحث	VERB
iajs-850	1	25	في	في	VERB
iajs-850	1	26	2010تشرین	2010تشرین	NUM
iajs-850	1	27	الثاني	الثاني	NOUN
iajs-850	1	28	9	9	NUM
iajs-850	1	29	:	:	PUNCT
iajs-850	1	30	قبل	قبل	NOUN
iajs-850	1	31	البحث	البحث	VERB
iajs-850	1	32	في	في	PRON
iajs-850	1	33	رمیز	رمیز	NOUN
iajs-850	1	34	رسمیة	رسمیة	PROPN
iajs-850	1	35	محمود	محمود	PROPN
iajs-850	1	36	،	،	PROPN
iajs-850	1	37	انباسمة	انباسمة	PROPN
iajs-850	1	38	محسن	محسن	PROPN
iajs-850	1	39	سرح	سرح	PROPN
iajs-850	1	40	،	،	PROPN
iajs-850	1	41	در	در	PROPN
iajs-850	1	42	مخلصعبد	مخلصعبد	PROPN
iajs-850	2	1	الجبار	الجبار	ADJ
iajs-850	2	2	عبد	عبد	ADJ
iajs-850	2	3	القا	القا	PROPN
iajs-850	2	4	بغداد	بغداد	PROPN
iajs-850	2	5	جامعة	جامعة	PROPN
iajs-850	2	6	،	،	PROPN
iajs-850	2	7	ابن	ابن	PROPN
iajs-850	2	8	الهیثم	الهیثم	PROPN
iajs-850	2	9	-	-	PUNCT
iajs-850	2	10	كلیة	كلیة	PROPN
iajs-850	2	11	التربیة	التربیة	NOUN
iajs-850	2	12	،	،	PROPN
iajs-850	3	1	قسم	قسم	PROPN
iajs-850	3	2	الكیمیاء	الكیمیاء	PROPN
iajs-850	3	3	لخالصةا	لخالصةا	PROPN
iajs-850	4	1	ه	ه	PROPN
iajs-850	4	2	المشـتقات	المشـتقات	PROPN
iajs-850	4	3	ذللحصـول	ذللحصـول	ADJ
iajs-850	4	4	علـى	علـى	NOUN
iajs-850	4	5	هـ	هـ	PROPN
iajs-850	4	6	.	.	PROPN
iajs-850	4	7	ارثرواسـكوربیكd	ارثرواسـكوربیكd	NOUN
iajs-850	4	8	-	-	PUNCT
iajs-850	4	9	تحضیر	تحضیر	NOUN
iajs-850	4	10	مشتقات	مشتقات	NOUN
iajs-850	4	11	جدیـدة	جدیـدة	NOUN
iajs-850	4	12	مـن	مـن	PROPN
iajs-850	4	13	البـاربتیورات	البـاربتیورات	PROPN
iajs-850	4	14	لحـامض	لحـامض	PROPN
iajs-850	4	15	ا	ا	PROPN
iajs-850	4	16	البحثذیتضمن	البحثذیتضمن	PROPN
iajs-850	4	17	ه	ه	PROPN
iajs-850	4	18	مـادة	مـادة	PROPN
iajs-850	4	19	)	)	PUNCT
iajs-850	5	1	3(ربیك	3(ربیك	PROPN
iajs-850	5	2	حـامض	حـامض	PROPN
iajs-850	5	3	االسـكو	االسـكو	PROPN
iajs-850	5	4	l	l	ADJ
iajs-850	5	5	-	-	ADJ
iajs-850	5	6	التـي	التـي	ADJ
iajs-850	5	7	حضـرت	حضـرت	ADJ
iajs-850	5	8	مـن	مـن	PROPN
iajs-850	5	9	تفاعـل	تفاعـل	NOUN
iajs-850	5	10	)	)	PUNCT
iajs-850	5	11	4(حـامض	4(حـامض	NUM
iajs-850	5	12	االسـكوربیك	االسـكوربیك	NOUN
iajs-850	5	13	l	l	PROPN
iajs-850	5	14	--	--	PUNCT
iajs-850	5	15	ایزوبروبیلیدینo--6,5تم	ایزوبروبیلیدینo--6,5تم	PROPN
iajs-850	5	16	اختیار	اختیار	PROPN
iajs-850	5	17	c-3	c-3	PROPN
iajs-850	5	18	و	و	PRON
iajs-850	5	19	c-2تمــت	c-2تمــت	NOUN
iajs-850	5	20	اسـترة	اسـترة	PROPN
iajs-850	5	21	مجـامیع	مجـامیع	PROPN
iajs-850	5	22	الهیدروكســیل	الهیدروكســیل	PROPN
iajs-850	5	23	فـي	فـي	PROPN
iajs-850	5	24	المواقـع	المواقـع	PROPN
iajs-850	5	25	.	.	PUNCT
iajs-850	6	1	مـع	مـع	PROPN
iajs-850	6	2	االســیتون	االســیتون	PROPN
iajs-850	6	3	الجـاف	الجـاف	PROPN
iajs-850	6	4	بوجـود	بوجـود	PROPN
iajs-850	6	5	غــاز	غــاز	PROPN
iajs-850	6	6	كلوریـد	كلوریـد	PROPN
iajs-850	6	7	الهیـدروجین	الهیـدروجین	PROPN
iajs-850	6	8	اولیـة	اولیـة	PROPN
iajs-850	6	9	)	)	PUNCT
iajs-850	7	1	5(التحلـل	5(التحلـل	NUM
iajs-850	7	2	المـائي	المـائي	NOUN
iajs-850	7	3	للمركـب	للمركـب	NOUN
iajs-850	7	4	)	)	PUNCT
iajs-850	7	5	.	.	PUNCT
iajs-850	8	1	5(تـم	5(تـم	NUM
iajs-850	8	2	الحصـول	الحصـول	NOUN
iajs-850	8	3	علـى	علـى	ADP
iajs-850	8	4	المركـب	المركـب	PROPN
iajs-850	8	5	،	،	PROPN
iajs-850	8	6	اذزیادة	اذزیادة	PROPN
iajs-850	9	1	من	من	PROPN
iajs-850	10	1	كلورید	كلورید	ADJ
iajs-850	10	2	البنزویل	البنزویل	NOUN
iajs-850	10	3	بوجود	بوجود	ADP
iajs-850	10	4	البیریـدین	البیریـدین	PROPN
iajs-850	10	5	الجـاف	الجـاف	PROPN
iajs-850	10	6	عمالباست	عمالباست	PROPN
iajs-850	10	7	ببرایـودات	ببرایـودات	ADJ
iajs-850	10	8	الصــودیوم	الصــودیوم	NOUN
iajs-850	10	9	لینــتج	لینــتج	NOUN
iajs-850	10	10	)	)	PUNCT
iajs-850	11	1	6(بعــدها	6(بعــدها	PROPN
iajs-850	11	2	تمــت	تمــت	PROPN
iajs-850	11	3	اكسـدة	اكسـدة	PROPN
iajs-850	11	4	المركــب	المركــب	PROPN
iajs-850	11	5	)	)	PUNCT
iajs-850	11	6	.	.	PUNCT
iajs-850	12	1	6(اعطــى	6(اعطــى	PROPN
iajs-850	12	2	المركـب	المركـب	PROPN
iajs-850	12	3	،	،	PROPN
iajs-850	12	4	اذ	اذ	NOUN
iajs-850	12	5	%	%	NOUN
iajs-850	12	6	)	)	PUNCT
iajs-850	12	7	65(حــامض	65(حــامض	NUM
iajs-850	12	8	الخلیـك	الخلیـك	NOUN
iajs-850	12	9	المعباسـت	المعباسـت	ADV
iajs-850	12	10	ــات	ــات	PROPN
iajs-850	12	11	بوجــود	بوجــود	PROPN
iajs-850	12	12	هیدروكســید	هیدروكســید	PROPN
iajs-850	12	13	البوتاســـیوم	البوتاســـیوم	PROPN
iajs-850	12	14	لیعطــي	لیعطــي	PROPN
iajs-850	12	15	المالونــات	المالونــات	PROPN
iajs-850	12	16	ذالــ	ذالــ	PROPN
iajs-850	12	17	)	)	PUNCT
iajs-850	13	1	7(االلدیهایــد	7(االلدیهایــد	NOUN
iajs-850	13	2	ائي	ائي	VERB
iajs-850	13	3	مثیــل	مثیــل	NOUN
iajs-850	13	4	المالونـ	المالونـ	AUX
iajs-850	13	5	ان	ان	AUX
iajs-850	13	6	تفاعـــل	تفاعـــل	VERB
iajs-850	13	7	)	)	PUNCT
iajs-850	13	8	.	.	PUNCT
iajs-850	14	1	8(ي	8(ي	NUM
iajs-850	14	2	یتفاعــل	یتفاعــل	NOUN
iajs-850	14	3	مـــع	مـــع	VERB
iajs-850	14	4	ثنــ	ثنــ	ADJ
iajs-850	14	5	علــى	علــى	NOUN
iajs-850	14	6	)	)	PUNCT
iajs-850	14	7	11(و	11(و	NUM
iajs-850	14	8	)	)	PUNCT
iajs-850	14	9	10(و	10(و	NUM
iajs-850	14	10	)	)	PUNCT
iajs-850	14	11	9(د	9(د	NUM
iajs-850	14	12	اعطـى	اعطـى	ADJ
iajs-850	14	13	المركبــات	المركبــات	ADJ
iajs-850	14	14	مــع	مــع	PROPN
iajs-850	14	15	الیوریــا	الیوریــا	PROPN
iajs-850	14	16	والثایویوریـا	والثایویوریـا	PROPN
iajs-850	14	17	والكوانــدین	والكوانــدین	NOUN
iajs-850	14	18	هایدروكلورایــ	هایدروكلورایــ	ADJ
iajs-850	14	19	)	)	PUNCT
iajs-850	14	20	8(التكـاثف	8(التكـاثف	NUM
iajs-850	14	21	الحلقــي	الحلقــي	NOUN
iajs-850	14	22	للمركـب	للمركـب	NOUN
iajs-850	14	23	.	.	PUNCT
iajs-850	15	1	التوالي	التوالي	NOUN
iajs-850	15	2	(	(	PUNCT
iajs-850	15	3	ftir)واطیــاف	ftir)واطیــاف	PROPN
iajs-850	15	4	االشـعة	االشـعة	PROPN
iajs-850	15	5	تحـت	تحـت	PROPN
iajs-850	15	6	الحمــراء	الحمــراء	PROPN
iajs-850	15	7	tlc	tlc	PROPN
iajs-850	15	8	)	)	PUNCT
iajs-850	15	9	(	(	PUNCT
iajs-850	15	10	طة	طة	NUM
iajs-850	15	11	كروماتوغرافیـا	كروماتوغرافیـا	ADV
iajs-850	15	12	الطبقـة	الطبقـة	VERB
iajs-850	15	13	الرقیقـةاشخصـت	الرقیقـةاشخصـت	PROPN
iajs-850	15	14	المركبـات	المركبـات	PROPN
iajs-850	15	15	المحضـرة	المحضـرة	PROPN
iajs-850	15	16	بوســ	بوســ	PROPN
iajs-850	15	17	نـوويواطیـاف	نـوويواطیـاف	PROPN
iajs-850	15	18	الـرنین	الـرنین	PROPN
iajs-850	15	19	ال	ال	ADP
iajs-850	15	20	u.v	u.v	PROPN
iajs-850	15	21	-	-	PUNCT
iajs-850	15	22	vis	vis	X
iajs-850	15	23	)	)	PUNCT
iajs-850	15	24	(	(	PUNCT
iajs-850	15	25	طة	طة	PRON
iajs-850	15	26	اطیاف	اطیاف	NOUN
iajs-850	15	27	االشعة	االشعة	ADP
iajs-850	15	28	فوق	فوق	PROPN
iajs-850	15	29	البنفسجیة	البنفسجیة	PROPN
iajs-850	16	1	والمرئیـةاه	والمرئیـةاه	PROPN
iajs-850	16	2	المركبات	المركبات	PROPN
iajs-850	16	3	تم	تم	PROPN
iajs-850	16	4	تشخیصه	تشخیصه	NOUN
iajs-850	16	5	بوسذوبعض	بوسذوبعض	NOUN
iajs-850	16	6	من	من	PROPN
iajs-850	16	7	ه	ه	PROPN
iajs-850	16	8	)	)	PUNCT
iajs-850	16	9	(	(	PUNCT
iajs-850	16	10	المغناطیسي	المغناطیسي	PROPN
iajs-850	16	11	1hnmr	1hnmr	NUM
iajs-850	16	12	13).(واطیاف	13).(واطیاف	NUM
iajs-850	16	13	كاربون	كاربون	PROPN
iajs-850	16	14	الرنین	الرنین	PROPN
iajs-850	16	15	النووي	النووي	PROPN
iajs-850	16	16	المغناطیسيcnm	المغناطیسيcnm	PROPN
iajs-850	16	17	r	r	PROPN
iajs-850	16	18	.اتنالمالو	.اتنالمالو	PUNCT
iajs-850	16	19	،	،	PROPN
iajs-850	16	20	حامض	حامض	PROPN
iajs-850	16	21	االسكوربیك	االسكوربیك	PROPN
iajs-850	16	22	،	،	X
iajs-850	16	23	ثرواسكوربیكحامض	ثرواسكوربیكحامض	PROPN
iajs-850	16	24	االر	االر	NOUN
iajs-850	16	25	،	،	X
iajs-850	16	26	الباربتیورات	الباربتیورات	PROPN
iajs-850	16	27	:	:	PUNCT
iajs-850	16	28	لمفتاحیةاالكلمات	لمفتاحیةاالكلمات	VERB
iajs-850	16	29	ibn	ibn	PROPN
iajs-850	16	30	alhaitham	alhaitham	NOUN
iajs-850	16	31	j.	j.	PROPN
iajs-850	16	32	for	for	ADP
iajs-850	16	33	pure	pure	ADJ
iajs-850	16	34	&	&	CCONJ
iajs-850	16	35	appl	appl	PROPN
iajs-850	16	36	.	.	PUNCT
iajs-850	17	1	sci	sci	PROPN
iajs-850	17	2	.	.	PUNCT
iajs-850	17	3	vol.24	vol.24	NOUN
iajs-850	17	4	(	(	PUNCT
iajs-850	17	5	1	1	NUM
iajs-850	17	6	)	)	PUNCT
iajs-850	17	7	2011	2011	NUM
iajs-850	17	8	synthesis	synthesis	NOUN
iajs-850	17	9	of	of	ADP
iajs-850	17	10	barbiturate	barbiturate	ADJ
iajs-850	17	11	derivatives	derivative	NOUN
iajs-850	17	12	of	of	ADP
iajs-850	17	13	d	d	ADJ
iajs-850	17	14	-	-	ADJ
iajs-850	17	15	erythroascorbic	erythroascorbic	ADJ
iajs-850	17	16	acid	acid	NOUN
iajs-850	17	17	received	receive	VERB
iajs-850	17	18	in	in	ADP
iajs-850	17	19	:	:	PUNCT
iajs-850	17	20	15	15	NUM
iajs-850	17	21	september	september	PROPN
iajs-850	17	22	2010	2010	NUM
iajs-850	17	23	accepted	accept	VERB
iajs-850	17	24	in	in	ADP
iajs-850	17	25	:	:	PUNCT
iajs-850	17	26	9	9	NUM
iajs-850	17	27	november	november	NOUN
iajs-850	17	28	2010	2010	NUM
iajs-850	17	29	a	a	PRON
iajs-850	17	30	-	-	PUNCT
iajs-850	17	31	j.a	j.a	PROPN
iajs-850	17	32	.	.	PROPN
iajs-850	17	33	mukhlis	mukhlis	PROPN
iajs-850	17	34	,	,	PUNCT
iajs-850	17	35	b.	b.	PROPN
iajs-850	17	36	m.	m.	PROPN
iajs-850	17	37	sarhan	sarhan	PROPN
iajs-850	17	38	,	,	PUNCT
iajs-850	17	39	r.	r.	PROPN
iajs-850	17	40	m.	m.	PROPN
iajs-850	17	41	rumez	rumez	PROPN
iajs-850	17	42	department	department	PROPN
iajs-850	17	43	of	of	ADP
iajs-850	17	44	chemistry	chemistry	NOUN
iajs-850	17	45	,	,	PUNCT
iajs-850	17	46	college	college	NOUN
iajs-850	17	47	of	of	ADP
iajs-850	17	48	educationibn	educationibn	PROPN
iajs-850	17	49	-	-	PUNCT
iajs-850	17	50	al	al	PROPN
iajs-850	17	51	-	-	PUNCT
iajs-850	17	52	haitham	haitham	PROPN
iajs-850	17	53	,	,	PUNCT
iajs-850	17	54	university	university	PROPN
iajs-850	17	55	of	of	ADP
iajs-850	17	56	baghdad	baghdad	PROPN
iajs-850	17	57	abstract	abstract	NOUN
iajs-850	17	58	the	the	DET
iajs-850	17	59	aim	aim	NOUN
iajs-850	17	60	of	of	ADP
iajs-850	17	61	this	this	DET
iajs-850	17	62	work	work	NOUN
iajs-850	17	63	is	be	AUX
iajs-850	17	64	the	the	DET
iajs-850	17	65	synthesis	synthesis	NOUN
iajs-850	17	66	of	of	ADP
iajs-850	17	67	new	new	ADJ
iajs-850	17	68	derivatives	derivative	NOUN
iajs-850	17	69	of	of	ADP
iajs-850	17	70	barbiturate	barbiturate	NOUN
iajs-850	17	71	of	of	ADP
iajs-850	17	72	d	d	NOUN
iajs-850	17	73	-	-	ADJ
iajs-850	17	74	erythroascorbic	erythroascorbic	ADJ
iajs-850	17	75	acid	acid	NOUN
iajs-850	17	76	.	.	PUNCT
iajs-850	18	1	to	to	PART
iajs-850	18	2	obtain	obtain	VERB
iajs-850	18	3	these	these	DET
iajs-850	18	4	derivatives	derivative	NOUN
iajs-850	18	5	,	,	PUNCT
iajs-850	18	6	the	the	DET
iajs-850	18	7	5,6	5,6	NUM
iajs-850	18	8	-	-	PUNCT
iajs-850	18	9	o	o	NOUN
iajs-850	18	10	-	-	PUNCT
iajs-850	18	11	isopropylidene	isopropylidene	ADJ
iajs-850	18	12	-	-	PUNCT
iajs-850	18	13	l	l	NOUN
iajs-850	18	14	-	-	ADJ
iajs-850	18	15	ascorbic	ascorbic	ADJ
iajs-850	18	16	acid	acid	NOUN
iajs-850	18	17	(	(	PUNCT
iajs-850	18	18	4	4	NUM
iajs-850	18	19	)	)	PUNCT
iajs-850	18	20	was	be	AUX
iajs-850	18	21	chosen	choose	VERB
iajs-850	18	22	,	,	PUNCT
iajs-850	18	23	which	which	PRON
iajs-850	18	24	was	be	AUX
iajs-850	18	25	prepared	prepare	VERB
iajs-850	18	26	from	from	ADP
iajs-850	18	27	the	the	DET
iajs-850	18	28	reaction	reaction	NOUN
iajs-850	18	29	of	of	ADP
iajs-850	18	30	l	l	ADJ
iajs-850	18	31	-	-	ADJ
iajs-850	18	32	ascorbic	ascorbic	ADJ
iajs-850	18	33	acid	acid	NOUN
iajs-850	18	34	(	(	PUNCT
iajs-850	18	35	3	3	NUM
iajs-850	18	36	)	)	PUNCT
iajs-850	18	37	as	as	ADP
iajs-850	18	38	a	a	DET
iajs-850	18	39	starting	starting	NOUN
iajs-850	18	40	material	material	NOUN
iajs-850	18	41	with	with	ADP
iajs-850	18	42	dry	dry	ADJ
iajs-850	18	43	acetone	acetone	NOUN
iajs-850	18	44	in	in	ADP
iajs-850	18	45	the	the	DET
iajs-850	18	46	presence	presence	NOUN
iajs-850	18	47	of	of	ADP
iajs-850	18	48	hydrogen	hydrogen	NOUN
iajs-850	18	49	chloride	chloride	NOUN
iajs-850	18	50	.	.	PUNCT
iajs-850	19	1	the	the	DET
iajs-850	19	2	esterification	esterification	NOUN
iajs-850	19	3	of	of	ADP
iajs-850	19	4	hydroxyl	hydroxyl	NOUN
iajs-850	19	5	groups	group	NOUN
iajs-850	19	6	at	at	ADP
iajs-850	19	7	c-2	c-2	NOUN
iajs-850	19	8	and	and	CCONJ
iajs-850	19	9	c-3	c-3	PROPN
iajs-850	19	10	positions	position	NOUN
iajs-850	19	11	with	with	ADP
iajs-850	19	12	excess	excess	NOUN
iajs-850	19	13	of	of	ADP
iajs-850	19	14	benzoyl	benzoyl	ADJ
iajs-850	19	15	chloride	chloride	NOUN
iajs-850	19	16	in	in	ADP
iajs-850	19	17	dry	dry	ADJ
iajs-850	19	18	pyridine	pyridine	NOUN
iajs-850	19	19	was	be	AUX
iajs-850	19	20	obtained	obtain	VERB
iajs-850	19	21	compound	compound	NOUN
iajs-850	19	22	(	(	PUNCT
iajs-850	19	23	5	5	NUM
iajs-850	19	24	)	)	PUNCT
iajs-850	19	25	.	.	PUNCT
iajs-850	20	1	hydrolysis	hydrolysis	NOUN
iajs-850	20	2	for	for	ADP
iajs-850	20	3	compound	compound	NOUN
iajs-850	20	4	(	(	PUNCT
iajs-850	20	5	5	5	NUM
iajs-850	20	6	)	)	PUNCT
iajs-850	20	7	in	in	ADP
iajs-850	20	8	acetic	acetic	ADJ
iajs-850	20	9	acid	acid	NOUN
iajs-850	20	10	(	(	PUNCT
iajs-850	20	11	65	65	NUM
iajs-850	20	12	%	%	NOUN
iajs-850	20	13	)	)	PUNCT
iajs-850	20	14	gave	give	VERB
iajs-850	20	15	the	the	DET
iajs-850	20	16	compound	compound	NOUN
iajs-850	20	17	(	(	PUNCT
iajs-850	20	18	6	6	NUM
iajs-850	20	19	)	)	PUNCT
iajs-850	20	20	.	.	PUNCT
iajs-850	21	1	oxidation	oxidation	NOUN
iajs-850	21	2	of	of	ADP
iajs-850	21	3	the	the	DET
iajs-850	21	4	product	product	NOUN
iajs-850	21	5	(	(	PUNCT
iajs-850	21	6	6	6	NUM
iajs-850	21	7	)	)	PUNCT
iajs-850	21	8	with	with	ADP
iajs-850	21	9	sodium	sodium	NOUN
iajs-850	21	10	periodate	periodate	NOUN
iajs-850	21	11	results	result	VERB
iajs-850	21	12	an	an	DET
iajs-850	21	13	aldehyde	aldehyde	NOUN
iajs-850	21	14	(	(	PUNCT
iajs-850	21	15	7	7	NUM
iajs-850	21	16	)	)	PUNCT
iajs-850	21	17	,	,	PUNCT
iajs-850	21	18	which	which	PRON
iajs-850	21	19	was	be	AUX
iajs-850	21	20	reacted	react	VERB
iajs-850	21	21	with	with	ADP
iajs-850	21	22	dimethyl	dimethyl	PROPN
iajs-850	21	23	malonate	malonate	NOUN
iajs-850	21	24	in	in	ADP
iajs-850	21	25	the	the	DET
iajs-850	21	26	presence	presence	NOUN
iajs-850	21	27	of	of	ADP
iajs-850	21	28	potassium	potassium	NOUN
iajs-850	21	29	hydroxide	hydroxide	NOUN
iajs-850	21	30	to	to	PART
iajs-850	21	31	give	give	VERB
iajs-850	21	32	the	the	DET
iajs-850	21	33	malonate	malonate	NOUN
iajs-850	21	34	(	(	PUNCT
iajs-850	21	35	8)	8)	NUM
iajs-850	21	36	.	.	PUNCT
iajs-850	22	1	the	the	DET
iajs-850	22	2	cyclocondensation	cyclocondensation	NOUN
iajs-850	22	3	reaction	reaction	NOUN
iajs-850	22	4	for	for	ADP
iajs-850	22	5	compound	compound	NOUN
iajs-850	22	6	(	(	PUNCT
iajs-850	22	7	8)	8)	NUM
iajs-850	22	8	with	with	ADP
iajs-850	22	9	urea	urea	NOUN
iajs-850	22	10	,	,	PUNCT
iajs-850	22	11	thiourea	thiourea	NOUN
iajs-850	22	12	and	and	CCONJ
iajs-850	22	13	guanidine	guanidine	ADJ
iajs-850	22	14	hydrochloride	hydrochloride	NOUN
iajs-850	22	15	gave	give	VERB
iajs-850	22	16	the	the	DET
iajs-850	22	17	following	following	ADJ
iajs-850	22	18	compounds	compound	NOUN
iajs-850	22	19	(	(	PUNCT
iajs-850	22	20	9	9	NUM
iajs-850	22	21	)	)	PUNCT
iajs-850	22	22	,	,	PUNCT
iajs-850	22	23	(	(	PUNCT
iajs-850	22	24	10	10	NUM
iajs-850	22	25	)	)	PUNCT
iajs-850	22	26	and	and	CCONJ
iajs-850	22	27	(	(	PUNCT
iajs-850	22	28	11	11	NUM
iajs-850	22	29	)	)	PUNCT
iajs-850	22	30	respectively	respectively	ADV
iajs-850	22	31	.	.	PUNCT
iajs-850	23	1	all	all	DET
iajs-850	23	2	these	these	DET
iajs-850	23	3	compounds	compound	NOUN
iajs-850	23	4	were	be	AUX
iajs-850	23	5	characterised	characterise	VERB
iajs-850	23	6	by	by	ADP
iajs-850	23	7	thin	thin	ADJ
iajs-850	23	8	layer	layer	NOUN
iajs-850	23	9	chromatography	chromatography	NOUN
iajs-850	23	10	(	(	PUNCT
iajs-850	23	11	tlc	tlc	NOUN
iajs-850	23	12	)	)	PUNCT
iajs-850	23	13	and	and	CCONJ
iajs-850	23	14	ftir	ftir	PROPN
iajs-850	23	15	spectra	spectra	PROPN
iajs-850	23	16	and	and	CCONJ
iajs-850	23	17	some	some	PRON
iajs-850	23	18	were	be	AUX
iajs-850	23	19	characterised	characterise	VERB
iajs-850	23	20	by	by	ADP
iajs-850	23	21	(	(	PUNCT
iajs-850	23	22	u.v	u.v	PROPN
iajs-850	23	23	-	-	PUNCT
iajs-850	23	24	vis	vis	X
iajs-850	23	25	)	)	PUNCT
iajs-850	23	26	spectra	spectra	NOUN
iajs-850	23	27	,	,	PUNCT
iajs-850	23	28	1	1	NUM
iajs-850	23	29	hnmr	hnmr	NOUN
iajs-850	23	30	spectra	spectra	NOUN
iajs-850	23	31	and	and	CCONJ
iajs-850	23	32	13	13	NUM
iajs-850	23	33	cnm	cnm	PROPN
iajs-850	23	34	r	r	NOUN
iajs-850	23	35	spectra	spectra	NOUN
iajs-850	23	36	.	.	PUNCT
iajs-850	24	1	key	key	ADJ
iajs-850	24	2	words	word	NOUN
iajs-850	24	3	:	:	PUNCT
iajs-850	24	4	barbiturate	barbiturate	ADJ
iajs-850	24	5	,	,	PUNCT
iajs-850	24	6	erythroascorbic	erythroascorbic	ADJ
iajs-850	24	7	acid	acid	NOUN
iajs-850	24	8	,	,	PUNCT
iajs-850	24	9	ascorbic	ascorbic	NOUN
iajs-850	24	10	acid	acid	NOUN
iajs-850	24	11	,	,	PUNCT
iajs-850	24	12	malonate	malonate	NOUN
iajs-850	24	13	.	.	PUNCT
iajs-850	25	1	introduction	introduction	NOUN
iajs-850	25	2	barbituric	barbituric	NOUN
iajs-850	25	3	acid	acid	NOUN
iajs-850	25	4	was	be	AUX
iajs-850	25	5	discovered	discover	VERB
iajs-850	25	6	in	in	ADP
iajs-850	25	7	the	the	DET
iajs-850	25	8	mid-19th	mid-19th	ADJ
iajs-850	25	9	century	century	NOUN
iajs-850	25	10	,	,	PUNCT
iajs-850	25	11	with	with	ADP
iajs-850	25	12	the	the	DET
iajs-850	25	13	first	first	ADJ
iajs-850	25	14	medical	medical	ADJ
iajs-850	25	15	barbiturate	barbiturate	NOUN
iajs-850	25	16	,	,	PUNCT
iajs-850	25	17	barbitone	barbitone	NOUN
iajs-850	25	18	(	(	PUNCT
iajs-850	25	19	1	1	NUM
iajs-850	25	20	)	)	PUNCT
iajs-850	25	21	,	,	PUNCT
iajs-850	25	22	being	be	AUX
iajs-850	25	23	synthesized	synthesize	VERB
iajs-850	25	24	in	in	ADP
iajs-850	25	25	1903	1903	NUM
iajs-850	25	26	.	.	PUNCT
iajs-850	26	1	phenobarbitone	phenobarbitone	NOUN
iajs-850	26	2	(	(	PUNCT
iajs-850	26	3	2	2	X
iajs-850	26	4	)	)	PUNCT
iajs-850	26	5	was	be	AUX
iajs-850	26	6	introduced	introduce	VERB
iajs-850	26	7	as	as	ADP
iajs-850	26	8	a	a	DET
iajs-850	26	9	pharmaceutical	pharmaceutical	NOUN
iajs-850	26	10	in	in	ADP
iajs-850	26	11	1912	1912	NUM
iajs-850	26	12	.	.	PUNCT
iajs-850	27	1	therapeutically	therapeutically	ADV
iajs-850	27	2	,	,	PUNCT
iajs-850	27	3	these	these	DET
iajs-850	27	4	drugs	drug	NOUN
iajs-850	27	5	are	be	AUX
iajs-850	27	6	used	use	VERB
iajs-850	27	7	as	as	ADP
iajs-850	27	8	sedatives	sedative	NOUN
iajs-850	27	9	,	,	PUNCT
iajs-850	27	10	anaesthetics	anaesthetic	NOUN
iajs-850	27	11	and	and	CCONJ
iajs-850	27	12	anticonvulsants	anticonvulsant	NOUN
iajs-850	27	13	.	.	PUNCT
iajs-850	28	1	phenobarbitone	phenobarbitone	NOUN
iajs-850	28	2	is	be	AUX
iajs-850	28	3	also	also	ADV
iajs-850	28	4	used	use	VERB
iajs-850	28	5	in	in	ADP
iajs-850	28	6	the	the	DET
iajs-850	28	7	treatment	treatment	NOUN
iajs-850	28	8	of	of	ADP
iajs-850	28	9	epilepsy[1	epilepsy[1	NUM
iajs-850	28	10	]	]	PUNCT
iajs-850	28	11	.	.	PUNCT
iajs-850	29	1	most	most	ADJ
iajs-850	29	2	of	of	ADP
iajs-850	29	3	the	the	DET
iajs-850	29	4	known	know	VERB
iajs-850	29	5	barbiturate	barbiturate	NOUN
iajs-850	29	6	compounds	compound	NOUN
iajs-850	29	7	possess	possess	VERB
iajs-850	29	8	low	low	ADJ
iajs-850	29	9	solubility	solubility	NOUN
iajs-850	29	10	in	in	ADP
iajs-850	29	11	water	water	NOUN
iajs-850	29	12	,	,	PUNCT
iajs-850	29	13	therefore	therefore	ADV
iajs-850	29	14	,	,	PUNCT
iajs-850	29	15	researches	research	VERB
iajs-850	29	16	claimed	claim	VERB
iajs-850	29	17	synthesis	synthesis	NOUN
iajs-850	29	18	of	of	ADP
iajs-850	29	19	new	new	ADJ
iajs-850	29	20	carbohydrate	carbohydrate	NOUN
iajs-850	29	21	derivatives	derivative	NOUN
iajs-850	29	22	containing	contain	VERB
iajs-850	29	23	barbiturate,[2],[3	barbiturate,[2],[3	PROPN
iajs-850	29	24	]	]	X
iajs-850	29	25	these	these	DET
iajs-850	29	26	derivatives	derivative	NOUN
iajs-850	29	27	have	have	VERB
iajs-850	29	28	high	high	ADJ
iajs-850	29	29	solubility	solubility	NOUN
iajs-850	29	30	in	in	ADP
iajs-850	29	31	water	water	NOUN
iajs-850	29	32	in	in	ADP
iajs-850	29	33	addition	addition	NOUN
iajs-850	29	34	of	of	ADP
iajs-850	29	35	possessing	possess	VERB
iajs-850	29	36	possible	possible	ADJ
iajs-850	29	37	biological	biological	ADJ
iajs-850	29	38	activity	activity	NOUN
iajs-850	29	39	.	.	PUNCT
iajs-850	30	1	khalafi	khalafi	PROPN
iajs-850	30	2	-	-	PUNCT
iajs-850	30	3	nezhad	nezhad	VERB
iajs-850	30	4	et	et	NOUN
iajs-850	30	5	al.[4	al.[4	PROPN
iajs-850	30	6	]	]	PUNCT
iajs-850	30	7	prepared	prepare	VERB
iajs-850	30	8	barbituric	barbituric	NOUN
iajs-850	30	9	acid	acid	NOUN
iajs-850	30	10	derivative	derivative	NOUN
iajs-850	30	11	from	from	ADP
iajs-850	30	12	reaction	reaction	NOUN
iajs-850	30	13	barbituric	barbituric	NOUN
iajs-850	30	14	acid	acid	NOUN
iajs-850	30	15	with	with	ADP
iajs-850	30	16	different	different	ADJ
iajs-850	30	17	aromatic	aromatic	ADJ
iajs-850	30	18	aldehyde	aldehyde	NOUN
iajs-850	30	19	on	on	ADP
iajs-850	30	20	basic	basic	ADJ
iajs-850	30	21	alumina	alumina	NOUN
iajs-850	30	22	was	be	AUX
iajs-850	30	23	performed	perform	VERB
iajs-850	30	24	in	in	ADP
iajs-850	30	25	a	a	DET
iajs-850	30	26	conventional	conventional	ADJ
iajs-850	30	27	microwave	microwave	NOUN
iajs-850	30	28	oven	oven	NOUN
iajs-850	30	29	in	in	ADP
iajs-850	30	30	the	the	DET
iajs-850	30	31	absence	absence	NOUN
iajs-850	30	32	of	of	ADP
iajs-850	30	33	solvent	solvent	NOUN
iajs-850	30	34	.	.	PUNCT
iajs-850	31	1	recently	recently	ADV
iajs-850	31	2	,	,	PUNCT
iajs-850	31	3	kidwai	kidwai	PROPN
iajs-850	31	4	et	et	PROPN
iajs-850	31	5	al.[5	al.[5	PROPN
iajs-850	31	6	]	]	PUNCT
iajs-850	31	7	reported	report	VERB
iajs-850	31	8	the	the	DET
iajs-850	31	9	preparation	preparation	NOUN
iajs-850	31	10	of	of	ADP
iajs-850	31	11	barbituric	barbituric	NOUN
iajs-850	31	12	acid	acid	NOUN
iajs-850	31	13	derivatives	derivative	NOUN
iajs-850	31	14	by	by	ADP
iajs-850	31	15	heating	heating	NOUN
iajs-850	31	16	reactants	reactant	NOUN
iajs-850	31	17	with	with	ADP
iajs-850	31	18	microwave	microwave	NOUN
iajs-850	31	19	irradiation	irradiation	NOUN
iajs-850	31	20	and	and	CCONJ
iajs-850	31	21	confirm	confirm	VERB
iajs-850	31	22	all	all	DET
iajs-850	31	23	the	the	DET
iajs-850	31	24	compounds	compound	NOUN
iajs-850	31	25	synthesized	synthesize	VERB
iajs-850	31	26	were	be	AUX
iajs-850	31	27	found	find	VERB
iajs-850	31	28	to	to	PART
iajs-850	31	29	possess	possess	VERB
iajs-850	31	30	good	good	ADJ
iajs-850	31	31	antifungal	antifungal	ADJ
iajs-850	31	32	activity	activity	NOUN
iajs-850	31	33	.	.	PUNCT
iajs-850	32	1	(	(	PUNCT
iajs-850	32	2	1	1	X
iajs-850	32	3	)	)	PUNCT
iajs-850	32	4	(	(	PUNCT
iajs-850	32	5	2	2	X
iajs-850	32	6	)	)	PUNCT
iajs-850	32	7	n	n	DET
iajs-850	32	8	n	n	PRON
iajs-850	32	9	o	o	NOUN
iajs-850	32	10	oo	oo	INTJ
iajs-850	33	1	h	h	NOUN
iajs-850	33	2	h	h	NOUN
iajs-850	34	1	c	c	NOUN
iajs-850	34	2	h	h	NOUN
iajs-850	35	1	2ch	2ch	ADJ
iajs-850	35	2	3	3	NUM
iajs-850	35	3	c	c	NOUN
iajs-850	35	4	h2c	h2c	NOUN
iajs-850	35	5	h3	h3	NOUN
iajs-850	35	6	n	n	PRON
iajs-850	35	7	n	n	PRON
iajs-850	35	8	o	o	NOUN
iajs-850	35	9	oo	oo	INTJ
iajs-850	35	10	c6h	c6h	PROPN
iajs-850	35	11	5	5	NUM
iajs-850	35	12	h	h	NOUN
iajs-850	35	13	h	h	PROPN
iajs-850	35	14	ch2ch3	ch2ch3	PROPN
iajs-850	35	15	ibn	ibn	PROPN
iajs-850	35	16	alhaitham	alhaitham	PROPN
iajs-850	35	17	j.	j.	PROPN
iajs-850	35	18	for	for	ADP
iajs-850	35	19	pure	pure	ADJ
iajs-850	35	20	&	&	CCONJ
iajs-850	35	21	appl	appl	PROPN
iajs-850	35	22	.	.	PUNCT
iajs-850	36	1	sci	sci	PROPN
iajs-850	36	2	.	.	PUNCT
iajs-850	36	3	vol.24	vol.24	NOUN
iajs-850	36	4	(	(	PUNCT
iajs-850	36	5	1	1	NUM
iajs-850	36	6	)	)	PUNCT
iajs-850	36	7	2011	2011	NUM
iajs-850	36	8	experimental	experimental	ADJ
iajs-850	36	9	melting	melting	NOUN
iajs-850	36	10	points	point	NOUN
iajs-850	36	11	were	be	AUX
iajs-850	36	12	determined	determine	VERB
iajs-850	36	13	by	by	ADP
iajs-850	36	14	electrothermal	electrothermal	ADJ
iajs-850	36	15	stuart	stuart	PROPN
iajs-850	36	16	melting	melt	VERB
iajs-850	36	17	point	point	NOUN
iajs-850	36	18	apparatus	apparatus	NOUN
iajs-850	36	19	and	and	CCONJ
iajs-850	36	20	are	be	AUX
iajs-850	36	21	uncorrected	uncorrecte	VERB
iajs-850	36	22	.	.	PUNCT
iajs-850	37	1	ir	ir	PROPN
iajs-850	37	2	spectra	spectra	PROPN
iajs-850	37	3	(	(	PUNCT
iajs-850	37	4	in	in	ADP
iajs-850	37	5	kbr	kbr	PROPN
iajs-850	37	6	)	)	PUNCT
iajs-850	37	7	were	be	AUX
iajs-850	37	8	recorded	record	VERB
iajs-850	37	9	on	on	ADP
iajs-850	37	10	shimadzu	shimadzu	ADJ
iajs-850	37	11	ft	ft	ADP
iajs-850	37	12	infrared	infrared	ADJ
iajs-850	37	13	spectrophotometer	spectrophotometer	NOUN
iajs-850	37	14	.	.	PUNCT
iajs-850	38	1	1	1	NUM
iajs-850	38	2	h	h	NOUN
iajs-850	38	3	and	and	CCONJ
iajs-850	38	4	13	13	NUM
iajs-850	38	5	cnm	cnm	PROPN
iajs-850	38	6	r	r	NOUN
iajs-850	38	7	spectra	spectra	NOUN
iajs-850	38	8	were	be	AUX
iajs-850	38	9	recorded	record	VERB
iajs-850	38	10	on	on	ADP
iajs-850	38	11	ultra	ultra	ADJ
iajs-850	38	12	shield	shield	NOUN
iajs-850	38	13	(	(	PUNCT
iajs-850	38	14	300	300	NUM
iajs-850	38	15	mhz	mhz	NOUN
iajs-850	38	16	)	)	PUNCT
iajs-850	38	17	spectrophotometer	spectrophotometer	NOUN
iajs-850	38	18	with	with	ADP
iajs-850	38	19	tetramethyl	tetramethyl	NOUN
iajs-850	38	20	silane	silane	NOUN
iajs-850	38	21	as	as	ADP
iajs-850	38	22	internal	internal	ADJ
iajs-850	38	23	standard	standard	NOUN
iajs-850	38	24	.	.	PUNCT
iajs-850	39	1	electronic	electronic	ADJ
iajs-850	39	2	spectra	spectra	NOUN
iajs-850	39	3	were	be	AUX
iajs-850	39	4	obtained	obtain	VERB
iajs-850	39	5	using	use	VERB
iajs-850	39	6	a	a	DET
iajs-850	39	7	(	(	PUNCT
iajs-850	39	8	u.v	u.v	PROPN
iajs-850	39	9	-	-	PUNCT
iajs-850	39	10	vis	vis	X
iajs-850	39	11	)	)	PUNCT
iajs-850	39	12	spectrophotometer	spectrophotometer	NOUN
iajs-850	39	13	type	type	NOUN
iajs-850	39	14	shimadzu	shimadzu	NOUN
iajs-850	39	15	,	,	PUNCT
iajs-850	39	16	(	(	PUNCT
iajs-850	39	17	160a).thin	160a).thin	ADJ
iajs-850	39	18	layer	layer	NOUN
iajs-850	39	19	chromatography	chromatography	NOUN
iajs-850	39	20	(	(	PUNCT
iajs-850	39	21	tlc	tlc	NOUN
iajs-850	39	22	)	)	PUNCT
iajs-850	39	23	was	be	AUX
iajs-850	39	24	performed	perform	VERB
iajs-850	39	25	on	on	ADP
iajs-850	39	26	aluminum	aluminum	NOUN
iajs-850	39	27	plates	plate	NOUN
iajs-850	39	28	coated	coat	VERB
iajs-850	39	29	with	with	ADP
iajs-850	39	30	layer	layer	NOUN
iajs-850	39	31	of	of	ADP
iajs-850	39	32	silica	silica	NOUN
iajs-850	39	33	gel	gel	NOUN
iajs-850	39	34	,	,	PUNCT
iajs-850	39	35	supplied	supply	VERB
iajs-850	39	36	by	by	ADP
iajs-850	39	37	merck	merck	PROPN
iajs-850	39	38	.	.	PUNCT
iajs-850	40	1	the	the	DET
iajs-850	40	2	spots	spot	NOUN
iajs-850	40	3	were	be	AUX
iajs-850	40	4	detected	detect	VERB
iajs-850	40	5	by	by	ADP
iajs-850	40	6	iodine	iodine	NOUN
iajs-850	40	7	vapor	vapor	NOUN
iajs-850	40	8	.	.	PUNCT
iajs-850	41	1	synthesis	synthesis	NOUN
iajs-850	41	2	of	of	ADP
iajs-850	41	3	5,6	5,6	NUM
iajs-850	41	4	-	-	PUNCT
iajs-850	41	5	o	o	NOUN
iajs-850	41	6	-	-	PUNCT
iajs-850	41	7	isopropylidene	isopropylidene	ADJ
iajs-850	41	8	-	-	PUNCT
iajs-850	41	9	l	l	NOUN
iajs-850	41	10	-	-	ADJ
iajs-850	41	11	ascorbic	ascorbic	ADJ
iajs-850	41	12	acid	acid	NOUN
iajs-850	41	13	(	(	PUNCT
iajs-850	41	14	4	4	NUM
iajs-850	41	15	)	)	PUNCT
iajs-850	41	16	dry	dry	ADJ
iajs-850	41	17	hydrogen	hydrogen	NOUN
iajs-850	41	18	chloride	chloride	NOUN
iajs-850	41	19	was	be	AUX
iajs-850	41	20	rapidly	rapidly	ADV
iajs-850	41	21	bubbled	bubble	VERB
iajs-850	41	22	with	with	ADP
iajs-850	41	23	stirring	stir	VERB
iajs-850	41	24	for	for	ADP
iajs-850	41	25	20	20	NUM
iajs-850	41	26	minutes	minute	NOUN
iajs-850	41	27	into	into	ADP
iajs-850	41	28	a	a	DET
iajs-850	41	29	(	(	PUNCT
iajs-850	41	30	250ml	250ml	NOUN
iajs-850	41	31	)	)	PUNCT
iajs-850	41	32	flask	flask	NOUN
iajs-850	41	33	containing	contain	VERB
iajs-850	41	34	(	(	PUNCT
iajs-850	41	35	10	10	NUM
iajs-850	41	36	g	g	NOUN
iajs-850	41	37	,	,	PUNCT
iajs-850	41	38	57mmol	57mmol	NUM
iajs-850	41	39	)	)	PUNCT
iajs-850	41	40	of	of	ADP
iajs-850	41	41	powdered	powdered	ADJ
iajs-850	41	42	l	l	ADJ
iajs-850	41	43	-	-	ADJ
iajs-850	41	44	ascorbic	ascorbic	ADJ
iajs-850	41	45	acid	acid	NOUN
iajs-850	41	46	(	(	PUNCT
iajs-850	41	47	3	3	NUM
iajs-850	41	48	)	)	PUNCT
iajs-850	41	49	and	and	CCONJ
iajs-850	41	50	(	(	PUNCT
iajs-850	41	51	100ml	100ml	NOUN
iajs-850	41	52	)	)	PUNCT
iajs-850	41	53	of	of	ADP
iajs-850	41	54	dry	dry	ADJ
iajs-850	41	55	acetone	acetone	NOUN
iajs-850	41	56	.	.	PUNCT
iajs-850	42	1	after	after	ADP
iajs-850	42	2	addition	addition	NOUN
iajs-850	42	3	of	of	ADP
iajs-850	42	4	(	(	PUNCT
iajs-850	42	5	80ml	80ml	NOUN
iajs-850	42	6	)	)	PUNCT
iajs-850	42	7	n	n	CCONJ
iajs-850	42	8	-	-	PUNCT
iajs-850	42	9	hexane	hexane	NOUN
iajs-850	42	10	,	,	PUNCT
iajs-850	42	11	stirring	stirring	NOUN
iajs-850	42	12	and	and	CCONJ
iajs-850	42	13	cooling	cool	VERB
iajs-850	42	14	in	in	ADP
iajs-850	42	15	an	an	DET
iajs-850	42	16	ice	ice	NOUN
iajs-850	42	17	-	-	PUNCT
iajs-850	42	18	water	water	NOUN
iajs-850	42	19	,	,	PUNCT
iajs-850	42	20	the	the	DET
iajs-850	42	21	supernatant	supernatant	NOUN
iajs-850	42	22	was	be	AUX
iajs-850	42	23	decanted	decant	VERB
iajs-850	42	24	.	.	PUNCT
iajs-850	43	1	the	the	DET
iajs-850	43	2	precipitate	precipitate	NOUN
iajs-850	43	3	was	be	AUX
iajs-850	43	4	washed	wash	VERB
iajs-850	43	5	four	four	NUM
iajs-850	43	6	times	time	NOUN
iajs-850	43	7	with	with	ADP
iajs-850	43	8	(	(	PUNCT
iajs-850	43	9	154ml	154ml	NOUN
iajs-850	43	10	)	)	PUNCT
iajs-850	43	11	of	of	ADP
iajs-850	43	12	acetone	acetone	NOUN
iajs-850	43	13	-	-	PUNCT
iajs-850	43	14	hexane	hexane	NOUN
iajs-850	43	15	mixture	mixture	NOUN
iajs-850	43	16	(	(	PUNCT
iajs-850	43	17	4:7	4:7	NUM
iajs-850	43	18	)	)	PUNCT
iajs-850	43	19	(	(	PUNCT
iajs-850	43	20	v	v	NOUN
iajs-850	43	21	/	/	SYM
iajs-850	43	22	v	v	NOUN
iajs-850	43	23	)	)	PUNCT
iajs-850	43	24	,	,	PUNCT
iajs-850	43	25	cooling	cool	VERB
iajs-850	43	26	in	in	ADP
iajs-850	43	27	an	an	DET
iajs-850	43	28	ice	ice	NOUN
iajs-850	43	29	-	-	PUNCT
iajs-850	43	30	water	water	NOUN
iajs-850	43	31	and	and	CCONJ
iajs-850	43	32	removal	removal	NOUN
iajs-850	43	33	of	of	ADP
iajs-850	43	34	supernatant	supernatant	NOUN
iajs-850	43	35	after	after	ADP
iajs-850	43	36	each	each	DET
iajs-850	43	37	addition	addition	NOUN
iajs-850	43	38	.	.	PUNCT
iajs-850	44	1	the	the	DET
iajs-850	44	2	last	last	ADJ
iajs-850	44	3	precipitate	precipitate	NOUN
iajs-850	44	4	was	be	AUX
iajs-850	44	5	dried	dry	VERB
iajs-850	44	6	under	under	ADP
iajs-850	44	7	reduced	reduce	VERB
iajs-850	44	8	pressure	pressure	NOUN
iajs-850	44	9	to	to	PART
iajs-850	44	10	give	give	VERB
iajs-850	44	11	(	(	PUNCT
iajs-850	44	12	4	4	NUM
iajs-850	44	13	)	)	PUNCT
iajs-850	44	14	(	(	PUNCT
iajs-850	44	15	11.7	11.7	NUM
iajs-850	44	16	g	g	NOUN
iajs-850	44	17	,	,	PUNCT
iajs-850	44	18	95.35	95.35	NUM
iajs-850	44	19	%	%	NOUN
iajs-850	44	20	)	)	PUNCT
iajs-850	44	21	as	as	ADP
iajs-850	44	22	a	a	DET
iajs-850	44	23	white	white	ADJ
iajs-850	44	24	crystalline	crystalline	NOUN
iajs-850	44	25	residue	residue	NOUN
iajs-850	44	26	,	,	PUNCT
iajs-850	44	27	m.p	m.p	X
iajs-850	44	28	(	(	PUNCT
iajs-850	44	29	206	206	NUM
iajs-850	44	30	-	-	SYM
iajs-850	44	31	208˚c	208˚c	NUM
iajs-850	44	32	)	)	PUNCT
iajs-850	44	33	.	.	PUNCT
iajs-850	45	1	rf	rf	PRON
iajs-850	45	2	(	(	PUNCT
iajs-850	45	3	0.68	0.68	NUM
iajs-850	45	4	)	)	PUNCT
iajs-850	45	5	(	(	PUNCT
iajs-850	45	6	benzene	benzene	NOUN
iajs-850	45	7	:	:	PUNCT
iajs-850	45	8	methanol	methanol	NOUN
iajs-850	45	9	,	,	PUNCT
iajs-850	45	10	5:5	5:5	NUM
iajs-850	45	11	)	)	PUNCT
iajs-850	45	12	(	(	PUNCT
iajs-850	45	13	v	v	NOUN
iajs-850	45	14	/	/	SYM
iajs-850	45	15	v	v	NOUN
iajs-850	45	16	)	)	PUNCT
iajs-850	45	17	.	.	PUNCT
iajs-850	46	1	ftir	ftir	PROPN
iajs-850	46	2	(	(	PUNCT
iajs-850	46	3	kbr	kbr	PROPN
iajs-850	46	4	,	,	PUNCT
iajs-850	46	5	cm	cm	NOUN
iajs-850	46	6	-1	-1	PUNCT
iajs-850	46	7	):	):	PUNCT
iajs-850	46	8	3240	3240	NUM
iajs-850	46	9	,	,	PUNCT
iajs-850	46	10	3062	3062	NUM
iajs-850	46	11	(	(	PUNCT
iajs-850	46	12	o	o	NOUN
iajs-850	46	13	-	-	NOUN
iajs-850	46	14	h	h	NOUN
iajs-850	46	15	)	)	PUNCT
iajs-850	46	16	,	,	PUNCT
iajs-850	46	17	2993	2993	NUM
iajs-850	46	18	(	(	PUNCT
iajs-850	46	19	c	c	X
iajs-850	46	20	-	-	PUNCT
iajs-850	46	21	hali	hali	PROPN
iajs-850	46	22	.	.	PUNCT
iajs-850	46	23	)	)	PUNCT
iajs-850	46	24	,	,	PUNCT
iajs-850	46	25	2908	2908	NUM
iajs-850	46	26	(	(	PUNCT
iajs-850	46	27	c	c	NOUN
iajs-850	46	28	-	-	PUNCT
iajs-850	46	29	hace	hace	NOUN
iajs-850	46	30	.	.	PUNCT
iajs-850	46	31	)	)	PUNCT
iajs-850	46	32	,	,	PUNCT
iajs-850	46	33	1751	1751	NUM
iajs-850	46	34	(	(	PUNCT
iajs-850	46	35	c	c	NOUN
iajs-850	46	36	=	=	NOUN
iajs-850	46	37	olac	olac	PROPN
iajs-850	46	38	.	.	PUNCT
iajs-850	46	39	)	)	PUNCT
iajs-850	46	40	,	,	PUNCT
iajs-850	46	41	1662	1662	NUM
iajs-850	46	42	(	(	PUNCT
iajs-850	46	43	c	c	X
iajs-850	46	44	=	=	SYM
iajs-850	46	45	c	c	NOUN
iajs-850	46	46	)	)	PUNCT
iajs-850	46	47	,	,	PUNCT
iajs-850	46	48	1431	1431	NUM
iajs-850	46	49	(	(	PUNCT
iajs-850	46	50	-ch	-ch	NOUN
iajs-850	46	51	-	-	PUNCT
iajs-850	46	52	asy	asy	NOUN
iajs-850	46	53	m	m	PROPN
iajs-850	46	54	)	)	PUNCT
iajs-850	46	55	,	,	PUNCT
iajs-850	46	56	1388	1388	NUM
iajs-850	46	57	(	(	PUNCT
iajs-850	46	58	-ch	-ch	NOUN
iajs-850	46	59	-	-	PUNCT
iajs-850	46	60	sym	sym	NOUN
iajs-850	46	61	)	)	PUNCT
iajs-850	46	62	,	,	PUNCT
iajs-850	46	63	1141	1141	NUM
iajs-850	46	64	-	-	SYM
iajs-850	46	65	900	900	NUM
iajs-850	46	66	(	(	PUNCT
iajs-850	46	67	c	c	NOUN
iajs-850	46	68	-	-	PUNCT
iajs-850	46	69	o	o	NOUN
iajs-850	46	70	)	)	PUNCT
iajs-850	46	71	,	,	PUNCT
iajs-850	46	72	767	767	NUM
iajs-850	46	73	δ(o	δ(o	ADJ
iajs-850	46	74	-	-	PUNCT
iajs-850	46	75	h	h	NOUN
iajs-850	46	76	)	)	PUNCT
iajs-850	46	77	(	(	PUNCT
iajs-850	46	78	o.o.p	o.o.p	NOUN
iajs-850	46	79	.	.	PUNCT
iajs-850	46	80	)	)	PUNCT
iajs-850	46	81	.	.	PUNCT
iajs-850	47	1	synthesis	synthesis	NOUN
iajs-850	47	2	of	of	ADP
iajs-850	47	3	2,3	2,3	NUM
iajs-850	47	4	-	-	ADJ
iajs-850	47	5	o	o	NOUN
iajs-850	47	6	-	-	PUNCT
iajs-850	47	7	dibenzoyl-5,6	dibenzoyl-5,6	NOUN
iajs-850	47	8	-	-	PUNCT
iajs-850	47	9	o	o	NOUN
iajs-850	47	10	-	-	PUNCT
iajs-850	47	11	isopropylidene	isopropylidene	ADJ
iajs-850	47	12	-	-	PUNCT
iajs-850	47	13	l	l	NOUN
iajs-850	47	14	-	-	ADJ
iajs-850	47	15	ascorbic	ascorbic	ADJ
iajs-850	47	16	acid	acid	NOUN
iajs-850	47	17	(	(	PUNCT
iajs-850	47	18	5	5	NUM
iajs-850	47	19	)	)	PUNCT
iajs-850	47	20	to	to	ADP
iajs-850	47	21	a	a	DET
iajs-850	47	22	cold	cold	ADJ
iajs-850	47	23	solution	solution	NOUN
iajs-850	47	24	of	of	ADP
iajs-850	47	25	(	(	PUNCT
iajs-850	47	26	4	4	NUM
iajs-850	47	27	)	)	PUNCT
iajs-850	47	28	(	(	PUNCT
iajs-850	47	29	10	10	NUM
iajs-850	47	30	g	g	NOUN
iajs-850	47	31	,	,	PUNCT
iajs-850	47	32	46mmol	46mmol	NUM
iajs-850	47	33	)	)	PUNCT
iajs-850	47	34	in	in	ADP
iajs-850	47	35	pyridine	pyridine	NOUN
iajs-850	47	36	(	(	PUNCT
iajs-850	47	37	50ml	50ml	NOUN
iajs-850	47	38	)	)	PUNCT
iajs-850	47	39	,	,	PUNCT
iajs-850	47	40	benzoyl	benzoyl	ADJ
iajs-850	47	41	chloride	chloride	NOUN
iajs-850	47	42	was	be	AUX
iajs-850	47	43	added	add	VERB
iajs-850	47	44	as	as	ADP
iajs-850	47	45	drop	drop	NOUN
iajs-850	47	46	wise	wise	ADJ
iajs-850	47	47	(	(	PUNCT
iajs-850	47	48	15ml	15ml	NOUN
iajs-850	47	49	,	,	PUNCT
iajs-850	47	50	129mmol	129mmol	PROPN
iajs-850	47	51	)	)	PUNCT
iajs-850	47	52	with	with	ADP
iajs-850	47	53	stirring	stir	VERB
iajs-850	47	54	.the	.the	NOUN
iajs-850	47	55	resulting	result	VERB
iajs-850	47	56	mixture	mixture	NOUN
iajs-850	47	57	was	be	AUX
iajs-850	47	58	stirred	stir	VERB
iajs-850	47	59	for	for	ADP
iajs-850	47	60	2	2	NUM
iajs-850	47	61	hours	hour	NOUN
iajs-850	47	62	,	,	PUNCT
iajs-850	47	63	then	then	ADV
iajs-850	47	64	kept	keep	VERB
iajs-850	47	65	in	in	ADP
iajs-850	47	66	dark	dark	ADJ
iajs-850	47	67	place	place	NOUN
iajs-850	47	68	at	at	ADP
iajs-850	47	69	room	room	NOUN
iajs-850	47	70	temperature	temperature	NOUN
iajs-850	47	71	for	for	ADP
iajs-850	47	72	22	22	NUM
iajs-850	47	73	hours	hour	NOUN
iajs-850	47	74	.	.	PUNCT
iajs-850	48	1	the	the	DET
iajs-850	48	2	mixture	mixture	NOUN
iajs-850	48	3	was	be	AUX
iajs-850	48	4	poured	pour	VERB
iajs-850	48	5	into	into	ADP
iajs-850	48	6	ice	ice	NOUN
iajs-850	48	7	-	-	PUNCT
iajs-850	48	8	water	water	NOUN
iajs-850	48	9	and	and	CCONJ
iajs-850	48	10	stirred	stir	VERB
iajs-850	48	11	for	for	ADP
iajs-850	48	12	20	20	NUM
iajs-850	48	13	minutes	minute	NOUN
iajs-850	48	14	,	,	PUNCT
iajs-850	48	15	the	the	DET
iajs-850	48	16	supernatant	supernatant	NOUN
iajs-850	48	17	was	be	AUX
iajs-850	48	18	decanted	decant	VERB
iajs-850	48	19	.	.	PUNCT
iajs-850	49	1	extraction	extraction	NOUN
iajs-850	49	2	with	with	ADP
iajs-850	49	3	chloroform	chloroform	NOUN
iajs-850	49	4	(	(	PUNCT
iajs-850	49	5	150	150	NUM
iajs-850	49	6	ml	ml	NOUN
iajs-850	49	7	)	)	PUNCT
iajs-850	49	8	.	.	PUNCT
iajs-850	50	1	the	the	DET
iajs-850	50	2	chloroform	chloroform	NOUN
iajs-850	50	3	layer	layer	NOUN
iajs-850	50	4	was	be	AUX
iajs-850	50	5	washed	wash	VERB
iajs-850	50	6	with	with	ADP
iajs-850	50	7	water	water	NOUN
iajs-850	50	8	,	,	PUNCT
iajs-850	50	9	dilute	dilute	VERB
iajs-850	50	10	hydrochloric	hydrochloric	ADJ
iajs-850	50	11	acid	acid	NOUN
iajs-850	50	12	(	(	PUNCT
iajs-850	50	13	5	5	NUM
iajs-850	50	14	%	%	NOUN
iajs-850	50	15	)	)	PUNCT
iajs-850	51	1	(	(	PUNCT
iajs-850	51	2	2	2	NUM
iajs-850	51	3	×	×	NOUN
iajs-850	51	4	100ml	100ml	NOUN
iajs-850	51	5	.	.	PUNCT
iajs-850	51	6	)	)	PUNCT
iajs-850	51	7	,	,	PUNCT
iajs-850	51	8	water	water	NOUN
iajs-850	51	9	,	,	PUNCT
iajs-850	51	10	saturated	saturate	VERB
iajs-850	51	11	aqueous	aqueous	ADJ
iajs-850	51	12	sodium	sodium	NOUN
iajs-850	51	13	hydrogen	hydrogen	NOUN
iajs-850	51	14	carbonate	carbonate	NOUN
iajs-850	51	15	(	(	PUNCT
iajs-850	51	16	100ml	100ml	NOUN
iajs-850	51	17	)	)	PUNCT
iajs-850	51	18	and	and	CCONJ
iajs-850	51	19	water	water	NOUN
iajs-850	51	20	.	.	PUNCT
iajs-850	52	1	dried	dry	VERB
iajs-850	52	2	over	over	ADP
iajs-850	52	3	anhydrous	anhydrous	ADJ
iajs-850	52	4	magnesium	magnesium	NOUN
iajs-850	52	5	sulfate	sulfate	NOUN
iajs-850	52	6	.	.	PUNCT
iajs-850	53	1	chloroform	chloroform	NOUN
iajs-850	53	2	was	be	AUX
iajs-850	53	3	evaporated	evaporate	VERB
iajs-850	53	4	gave	give	VERB
iajs-850	53	5	a	a	DET
iajs-850	53	6	brown	brown	ADJ
iajs-850	53	7	syrup	syrup	NOUN
iajs-850	53	8	.	.	PUNCT
iajs-850	54	1	the	the	DET
iajs-850	54	2	syrup	syrup	NOUN
iajs-850	54	3	was	be	AUX
iajs-850	54	4	precipitated	precipitate	VERB
iajs-850	54	5	from	from	ADP
iajs-850	54	6	chloroform	chloroform	NOUN
iajs-850	54	7	:	:	PUNCT
iajs-850	54	8	petroleum	petroleum	NOUN
iajs-850	54	9	ether	ether	NOUN
iajs-850	54	10	(	(	PUNCT
iajs-850	54	11	60	60	NUM
iajs-850	54	12	-	-	PUNCT
iajs-850	54	13	80˚c	80˚c	NUM
iajs-850	54	14	)	)	PUNCT
iajs-850	54	15	(	(	PUNCT
iajs-850	54	16	1:5	1:5	NUM
iajs-850	54	17	)	)	PUNCT
iajs-850	54	18	(	(	PUNCT
iajs-850	54	19	v	v	NOUN
iajs-850	54	20	/	/	SYM
iajs-850	54	21	v	v	NOUN
iajs-850	54	22	)	)	PUNCT
iajs-850	54	23	to	to	PART
iajs-850	54	24	give	give	VERB
iajs-850	54	25	(	(	PUNCT
iajs-850	54	26	5	5	NUM
iajs-850	54	27	)	)	PUNCT
iajs-850	54	28	(	(	PUNCT
iajs-850	54	29	15	15	NUM
iajs-850	54	30	g	g	NOUN
iajs-850	54	31	,	,	PUNCT
iajs-850	54	32	76.5	76.5	NUM
iajs-850	54	33	%	%	NOUN
iajs-850	54	34	)	)	PUNCT
iajs-850	54	35	as	as	ADP
iajs-850	54	36	a	a	DET
iajs-850	54	37	pale	pale	ADJ
iajs-850	54	38	brown	brown	NOUN
iajs-850	54	39	solid	solid	ADJ
iajs-850	54	40	,	,	PUNCT
iajs-850	54	41	m.p	m.p	X
iajs-850	54	42	(	(	PUNCT
iajs-850	54	43	83	83	NUM
iajs-850	54	44	-	-	NUM
iajs-850	54	45	85˚c	85˚c	NUM
iajs-850	54	46	)	)	PUNCT
iajs-850	54	47	.	.	PUNCT
iajs-850	55	1	rf	rf	PRON
iajs-850	55	2	(	(	PUNCT
iajs-850	55	3	0.73	0.73	NUM
iajs-850	55	4	)	)	PUNCT
iajs-850	55	5	(	(	PUNCT
iajs-850	55	6	benzene	benzene	NOUN
iajs-850	55	7	:	:	PUNCT
iajs-850	55	8	methanol	methanol	NOUN
iajs-850	55	9	,	,	PUNCT
iajs-850	55	10	5:5	5:5	NUM
iajs-850	55	11	)	)	PUNCT
iajs-850	55	12	(	(	PUNCT
iajs-850	55	13	v	v	NOUN
iajs-850	55	14	/	/	SYM
iajs-850	55	15	v	v	NOUN
iajs-850	55	16	)	)	PUNCT
iajs-850	55	17	.	.	PUNCT
iajs-850	56	1	ftir	ftir	PROPN
iajs-850	56	2	(	(	PUNCT
iajs-850	56	3	kbr	kbr	PROPN
iajs-850	56	4	,	,	PUNCT
iajs-850	56	5	cm	cm	PROPN
iajs-850	56	6	-1	-1	NUM
iajs-850	56	7	):	):	PUNCT
iajs-850	56	8	3062	3062	NUM
iajs-850	56	9	(	(	PUNCT
iajs-850	56	10	c	c	NOUN
iajs-850	56	11	-	-	PUNCT
iajs-850	56	12	har	har	X
iajs-850	56	13	.	.	PUNCT
iajs-850	56	14	)	)	PUNCT
iajs-850	56	15	,	,	PUNCT
iajs-850	56	16	2985	2985	NUM
iajs-850	56	17	(	(	PUNCT
iajs-850	56	18	c	c	NOUN
iajs-850	56	19	-	-	PUNCT
iajs-850	56	20	hali	hali	PROPN
iajs-850	56	21	.	.	PUNCT
iajs-850	56	22	)	)	PUNCT
iajs-850	56	23	,	,	PUNCT
iajs-850	56	24	2931	2931	NUM
iajs-850	56	25	(	(	PUNCT
iajs-850	56	26	chace	chace	NOUN
iajs-850	56	27	.	.	PUNCT
iajs-850	56	28	)	)	PUNCT
iajs-850	56	29	,	,	PUNCT
iajs-850	56	30	1751	1751	NUM
iajs-850	56	31	(	(	PUNCT
iajs-850	56	32	c	c	NOUN
iajs-850	56	33	=	=	NOUN
iajs-850	56	34	olac	olac	PROPN
iajs-850	56	35	.	.	PUNCT
iajs-850	56	36	)	)	PUNCT
iajs-850	56	37	,	,	PUNCT
iajs-850	56	38	1662	1662	NUM
iajs-850	56	39	(	(	PUNCT
iajs-850	56	40	c	c	NOUN
iajs-850	56	41	=	=	X
iajs-850	56	42	oest	o	ADJ
iajs-850	56	43	.	.	PUNCT
iajs-850	56	44	)	)	PUNCT
iajs-850	56	45	,	,	PUNCT
iajs-850	56	46	1627	1627	NUM
iajs-850	56	47	(	(	PUNCT
iajs-850	56	48	c	c	NOUN
iajs-850	56	49	=	=	NOUN
iajs-850	56	50	cali	cali	ADJ
iajs-850	56	51	.	.	PUNCT
iajs-850	56	52	)	)	PUNCT
iajs-850	56	53	,	,	PUNCT
iajs-850	56	54	1600	1600	NUM
iajs-850	56	55	(	(	PUNCT
iajs-850	56	56	c	c	NOUN
iajs-850	56	57	=	=	NOUN
iajs-850	56	58	car	car	NOUN
iajs-850	56	59	.	.	PUNCT
iajs-850	56	60	)	)	PUNCT
iajs-850	56	61	,	,	PUNCT
iajs-850	56	62	1261	1261	NUM
iajs-850	56	63	-	-	SYM
iajs-850	56	64	1118	1118	NUM
iajs-850	56	65	(	(	PUNCT
iajs-850	56	66	c	c	NOUN
iajs-850	56	67	-	-	PUNCT
iajs-850	56	68	o	o	NOUN
iajs-850	56	69	)	)	PUNCT
iajs-850	56	70	,	,	PUNCT
iajs-850	56	71	900600	900600	NUM
iajs-850	56	72	δ(c	δ(c	PROPN
iajs-850	56	73	-	-	PUNCT
iajs-850	56	74	h	h	NOUN
iajs-850	56	75	)	)	PUNCT
iajs-850	56	76	(	(	PUNCT
iajs-850	56	77	o.o.p	o.o.p	NOUN
iajs-850	56	78	.	.	PUNCT
iajs-850	56	79	)	)	PUNCT
iajs-850	56	80	.	.	PUNCT
iajs-850	57	1	synthesis	synthesis	NOUN
iajs-850	57	2	of	of	ADP
iajs-850	57	3	2,3	2,3	NUM
iajs-850	57	4	-	-	ADJ
iajs-850	57	5	o	o	NOUN
iajs-850	57	6	-	-	ADJ
iajs-850	57	7	dibenzoyl	dibenzoyl	ADJ
iajs-850	57	8	-	-	PUNCT
iajs-850	57	9	l	l	NOUN
iajs-850	57	10	-	-	ADJ
iajs-850	57	11	ascorbic	ascorbic	ADJ
iajs-850	57	12	acid	acid	NOUN
iajs-850	57	13	(	(	PUNCT
iajs-850	57	14	6	6	NUM
iajs-850	57	15	)	)	PUNCT
iajs-850	57	16	compound	compound	NOUN
iajs-850	57	17	(	(	PUNCT
iajs-850	57	18	5	5	NUM
iajs-850	57	19	)	)	PUNCT
iajs-850	57	20	(	(	PUNCT
iajs-850	57	21	10	10	NUM
iajs-850	57	22	g	g	NOUN
iajs-850	57	23	,	,	PUNCT
iajs-850	57	24	23.6mmol	23.6mmol	NUM
iajs-850	57	25	)	)	PUNCT
iajs-850	57	26	was	be	AUX
iajs-850	57	27	dissolved	dissolve	VERB
iajs-850	57	28	in	in	ADP
iajs-850	57	29	(	(	PUNCT
iajs-850	57	30	65	65	NUM
iajs-850	57	31	%	%	NOUN
iajs-850	57	32	)	)	PUNCT
iajs-850	57	33	acetic	acetic	ADJ
iajs-850	57	34	acid	acid	NOUN
iajs-850	57	35	(	(	PUNCT
iajs-850	57	36	30ml	30ml	NOUN
iajs-850	57	37	)	)	PUNCT
iajs-850	57	38	,	,	PUNCT
iajs-850	57	39	absolute	absolute	ADJ
iajs-850	57	40	methanol	methanol	NOUN
iajs-850	57	41	(	(	PUNCT
iajs-850	57	42	10ml	10ml	NOUN
iajs-850	57	43	)	)	PUNCT
iajs-850	57	44	and	and	CCONJ
iajs-850	57	45	stirred	stir	VERB
iajs-850	57	46	for	for	ADP
iajs-850	57	47	48	48	NUM
iajs-850	57	48	hours	hour	NOUN
iajs-850	57	49	at	at	ADP
iajs-850	57	50	room	room	NOUN
iajs-850	57	51	temperature	temperature	NOUN
iajs-850	57	52	.	.	PUNCT
iajs-850	58	1	the	the	DET
iajs-850	58	2	tlc	tlc	NOUN
iajs-850	58	3	showed	show	VERB
iajs-850	58	4	that	that	SCONJ
iajs-850	58	5	the	the	DET
iajs-850	58	6	reaction	reaction	NOUN
iajs-850	58	7	was	be	AUX
iajs-850	58	8	complete	complete	ADJ
iajs-850	58	9	(	(	PUNCT
iajs-850	58	10	benzene	benzene	NOUN
iajs-850	58	11	:	:	PUNCT
iajs-850	58	12	methanol	methanol	NOUN
iajs-850	58	13	,	,	PUNCT
iajs-850	58	14	6:4	6:4	NUM
iajs-850	58	15	)	)	PUNCT
iajs-850	58	16	.	.	PUNCT
iajs-850	59	1	benzene	benzene	NOUN
iajs-850	59	2	(	(	PUNCT
iajs-850	59	3	40ml	40ml	NOUN
iajs-850	59	4	)	)	PUNCT
iajs-850	59	5	was	be	AUX
iajs-850	59	6	added	add	VERB
iajs-850	59	7	to	to	ADP
iajs-850	59	8	the	the	DET
iajs-850	59	9	solution	solution	NOUN
iajs-850	59	10	and	and	CCONJ
iajs-850	59	11	evaporated	evaporate	VERB
iajs-850	59	12	the	the	DET
iajs-850	59	13	organic	organic	ADJ
iajs-850	59	14	solvent	solvent	NOUN
iajs-850	59	15	(	(	PUNCT
iajs-850	59	16	repeat	repeat	VERB
iajs-850	59	17	this	this	DET
iajs-850	59	18	process	process	NOUN
iajs-850	59	19	four	four	NUM
iajs-850	59	20	times).the	times).the	DET
iajs-850	59	21	residue	residue	NOUN
iajs-850	59	22	was	be	AUX
iajs-850	59	23	solid	solid	ADJ
iajs-850	59	24	,	,	PUNCT
iajs-850	59	25	recrystallized	recrystallize	VERB
iajs-850	59	26	from	from	ADP
iajs-850	59	27	chloroform	chloroform	NOUN
iajs-850	59	28	and	and	CCONJ
iajs-850	59	29	then	then	ADV
iajs-850	59	30	diethyl	diethyl	VERB
iajs-850	59	31	ether	ether	NOUN
iajs-850	59	32	to	to	PART
iajs-850	59	33	yield	yield	VERB
iajs-850	59	34	(	(	PUNCT
iajs-850	59	35	6	6	NUM
iajs-850	59	36	)	)	PUNCT
iajs-850	59	37	(	(	PUNCT
iajs-850	59	38	7	7	NUM
iajs-850	59	39	g	g	NOUN
iajs-850	59	40	,	,	PUNCT
iajs-850	59	41	77.7	77.7	NUM
iajs-850	59	42	%	%	NOUN
iajs-850	59	43	)	)	PUNCT
iajs-850	59	44	as	as	ADP
iajs-850	59	45	a	a	DET
iajs-850	59	46	white	white	ADJ
iajs-850	59	47	crystals	crystal	NOUN
iajs-850	59	48	,	,	PUNCT
iajs-850	59	49	m.p	m.p	X
iajs-850	59	50	(	(	PUNCT
iajs-850	59	51	115	115	NUM
iajs-850	59	52	-	-	PUNCT
iajs-850	59	53	116˚c	116˚c	NUM
iajs-850	59	54	)	)	PUNCT
iajs-850	59	55	,	,	PUNCT
iajs-850	59	56	rf	rf	NUM
iajs-850	59	57	(	(	PUNCT
iajs-850	59	58	0.35	0.35	NUM
iajs-850	59	59	)	)	PUNCT
iajs-850	59	60	.	.	PUNCT
iajs-850	60	1	ftir	ftir	PROPN
iajs-850	60	2	(	(	PUNCT
iajs-850	60	3	kbr	kbr	PROPN
iajs-850	60	4	,	,	PUNCT
iajs-850	60	5	cm	cm	PROPN
iajs-850	60	6	-1	-1	PRON
iajs-850	60	7	):	):	PUNCT
iajs-850	60	8	3406	3406	NUM
iajs-850	60	9	(	(	PUNCT
iajs-850	60	10	o	o	NOUN
iajs-850	60	11	-	-	NOUN
iajs-850	60	12	h	h	NOUN
iajs-850	60	13	)	)	PUNCT
iajs-850	60	14	,	,	PUNCT
iajs-850	60	15	3074	3074	NUM
iajs-850	60	16	(	(	PUNCT
iajs-850	60	17	c	c	NOUN
iajs-850	60	18	-	-	PUNCT
iajs-850	60	19	har	har	X
iajs-850	60	20	.	.	PUNCT
iajs-850	60	21	)	)	PUNCT
iajs-850	60	22	,	,	PUNCT
iajs-850	60	23	2939	2939	NUM
iajs-850	60	24	(	(	PUNCT
iajs-850	60	25	c	c	NOUN
iajs-850	60	26	-	-	PUNCT
iajs-850	60	27	hali	hali	PROPN
iajs-850	60	28	.	.	PUNCT
iajs-850	60	29	)	)	PUNCT
iajs-850	60	30	,	,	PUNCT
iajs-850	60	31	1716	1716	NUM
iajs-850	60	32	(	(	PUNCT
iajs-850	60	33	c	c	NOUN
iajs-850	60	34	=	=	NOUN
iajs-850	60	35	oest	o	ADJ
iajs-850	60	36	.	.	PUNCT
iajs-850	60	37	)	)	PUNCT
iajs-850	60	38	,	,	PUNCT
iajs-850	60	39	1600	1600	NUM
iajs-850	60	40	(	(	PUNCT
iajs-850	60	41	c	c	NOUN
iajs-850	60	42	=	=	NOUN
iajs-850	60	43	car	car	NOUN
iajs-850	60	44	.	.	PUNCT
iajs-850	60	45	)	)	PUNCT
iajs-850	60	46	,	,	PUNCT
iajs-850	60	47	1273	1273	NUM
iajs-850	60	48	-	-	SYM
iajs-850	60	49	1118	1118	NUM
iajs-850	60	50	(	(	PUNCT
iajs-850	60	51	c	c	NOUN
iajs-850	60	52	-	-	PUNCT
iajs-850	60	53	o	o	NOUN
iajs-850	60	54	)	)	PUNCT
iajs-850	60	55	,	,	PUNCT
iajs-850	60	56	900	900	NUM
iajs-850	60	57	-	-	SYM
iajs-850	60	58	600	600	NUM
iajs-850	60	59	δ(c	δ(c	PROPN
iajs-850	60	60	-	-	PUNCT
iajs-850	60	61	har	har	PROPN
iajs-850	60	62	.	.	PUNCT
iajs-850	60	63	)	)	PUNCT
iajs-850	61	1	(	(	PUNCT
iajs-850	61	2	o.o.p	o.o.p	X
iajs-850	61	3	.	.	PUNCT
iajs-850	61	4	)	)	PUNCT
iajs-850	61	5	.	.	PUNCT
iajs-850	62	1	synthesis	synthesis	NOUN
iajs-850	62	2	of	of	ADP
iajs-850	62	3	pentulosono	pentulosono	NOUN
iajs-850	62	4	-	-	PUNCT
iajs-850	62	5	γ	γ	NOUN
iajs-850	62	6	-	-	PUNCT
iajs-850	62	7	lactone-2,3	lactone-2,3	NOUN
iajs-850	62	8	-	-	PUNCT
iajs-850	62	9	enedibenzoate	enedibenzoate	NOUN
iajs-850	62	10	(	(	PUNCT
iajs-850	62	11	7	7	NUM
iajs-850	62	12	)	)	PUNCT
iajs-850	62	13	to	to	ADP
iajs-850	62	14	the	the	DET
iajs-850	62	15	stirred	stir	VERB
iajs-850	62	16	solution	solution	NOUN
iajs-850	62	17	of	of	ADP
iajs-850	62	18	sodium	sodium	NOUN
iajs-850	62	19	periodate	periodate	NOUN
iajs-850	62	20	(	(	PUNCT
iajs-850	62	21	5.6	5.6	NUM
iajs-850	62	22	g	g	NOUN
iajs-850	62	23	)	)	PUNCT
iajs-850	62	24	in	in	ADP
iajs-850	62	25	distilled	distil	VERB
iajs-850	62	26	water	water	NOUN
iajs-850	62	27	(	(	PUNCT
iajs-850	62	28	60ml	60ml	NOUN
iajs-850	62	29	)	)	PUNCT
iajs-850	62	30	at	at	ADP
iajs-850	62	31	(	(	PUNCT
iajs-850	62	32	0˚c	0˚c	NUM
iajs-850	62	33	)	)	PUNCT
iajs-850	62	34	,	,	PUNCT
iajs-850	62	35	a	a	DET
iajs-850	62	36	solution	solution	NOUN
iajs-850	62	37	of	of	ADP
iajs-850	62	38	(	(	PUNCT
iajs-850	62	39	6	6	NUM
iajs-850	62	40	)	)	PUNCT
iajs-850	62	41	(	(	PUNCT
iajs-850	62	42	10	10	NUM
iajs-850	62	43	g	g	NOUN
iajs-850	62	44	,	,	PUNCT
iajs-850	62	45	26mmol	26mmol	NUM
iajs-850	62	46	)	)	PUNCT
iajs-850	62	47	in	in	ADP
iajs-850	62	48	absolute	absolute	ADJ
iajs-850	62	49	ethanol	ethanol	NOUN
iajs-850	62	50	(	(	PUNCT
iajs-850	62	51	60ml	60ml	NOUN
iajs-850	62	52	)	)	PUNCT
iajs-850	62	53	was	be	AUX
iajs-850	62	54	added	add	VERB
iajs-850	62	55	drop	drop	NOUN
iajs-850	62	56	wise	wise	ADJ
iajs-850	62	57	.	.	PUNCT
iajs-850	63	1	after	after	ADP
iajs-850	63	2	15	15	NUM
iajs-850	63	3	minutes	minute	NOUN
iajs-850	63	4	,	,	PUNCT
iajs-850	63	5	ethy	ethy	ADJ
iajs-850	63	6	lene	lene	NOUN
iajs-850	63	7	glycol	glycol	NOUN
iajs-850	63	8	(	(	PUNCT
iajs-850	63	9	0.5ml	0.5ml	NUM
iajs-850	63	10	)	)	PUNCT
iajs-850	63	11	was	be	AUX
iajs-850	63	12	added	add	VERB
iajs-850	63	13	as	as	ADP
iajs-850	63	14	drop	drop	NOUN
iajs-850	63	15	wise	wise	ADJ
iajs-850	63	16	,	,	PUNCT
iajs-850	63	17	stirring	stir	VERB
iajs-850	63	18	was	be	AUX
iajs-850	63	19	continued	continue	VERB
iajs-850	63	20	at	at	ADP
iajs-850	63	21	room	room	NOUN
iajs-850	63	22	temperature	temperature	NOUN
iajs-850	63	23	for	for	ADP
iajs-850	63	24	1	1	NUM
iajs-850	63	25	hour	hour	NOUN
iajs-850	63	26	.	.	PUNCT
iajs-850	64	1	the	the	DET
iajs-850	64	2	mixture	mixture	NOUN
iajs-850	64	3	was	be	AUX
iajs-850	64	4	filtered	filter	VERB
iajs-850	64	5	and	and	CCONJ
iajs-850	64	6	water	water	NOUN
iajs-850	64	7	(	(	PUNCT
iajs-850	64	8	40ml	40ml	NOUN
iajs-850	64	9	)	)	PUNCT
iajs-850	64	10	was	be	AUX
iajs-850	64	11	added	add	VERB
iajs-850	64	12	to	to	ADP
iajs-850	64	13	the	the	DET
iajs-850	64	14	filtrate	filtrate	NOUN
iajs-850	64	15	.	.	PUNCT
iajs-850	65	1	extraction	extraction	NOUN
iajs-850	65	2	with	with	ADP
iajs-850	65	3	ethy	ethy	ADJ
iajs-850	65	4	l	l	NOUN
iajs-850	65	5	acetate	acetate	NOUN
iajs-850	65	6	(	(	PUNCT
iajs-850	65	7	3×50ml	3×50ml	PROPN
iajs-850	65	8	)	)	PUNCT
iajs-850	65	9	,	,	PUNCT
iajs-850	65	10	the	the	DET
iajs-850	65	11	extracts	extract	NOUN
iajs-850	65	12	dried	dry	VERB
iajs-850	65	13	by	by	ADP
iajs-850	65	14	anhydrous	anhydrous	ADJ
iajs-850	65	15	magnesium	magnesium	NOUN
iajs-850	65	16	sulfate	sulfate	NOUN
iajs-850	65	17	.	.	PUNCT
iajs-850	66	1	evaporation	evaporation	NOUN
iajs-850	66	2	and	and	CCONJ
iajs-850	66	3	the	the	DET
iajs-850	66	4	residue	residue	NOUN
iajs-850	66	5	recrystallized	recrystallize	VERB
iajs-850	66	6	from	from	ADP
iajs-850	66	7	benzene	benzene	NOUN
iajs-850	66	8	to	to	PART
iajs-850	66	9	yield	yield	VERB
iajs-850	66	10	the	the	DET
iajs-850	66	11	pure	pure	ADJ
iajs-850	66	12	product	product	NOUN
iajs-850	66	13	(	(	PUNCT
iajs-850	66	14	7	7	NUM
iajs-850	66	15	)	)	PUNCT
iajs-850	66	16	(	(	PUNCT
iajs-850	66	17	4	4	NUM
iajs-850	66	18	g	g	NOUN
iajs-850	66	19	,	,	PUNCT
iajs-850	66	20	44.4	44.4	NUM
iajs-850	66	21	%	%	NOUN
iajs-850	66	22	)	)	PUNCT
iajs-850	66	23	as	as	ADP
iajs-850	66	24	a	a	DET
iajs-850	66	25	white	white	ADJ
iajs-850	66	26	crystals	crystal	NOUN
iajs-850	66	27	,	,	PUNCT
iajs-850	66	28	m.p	m.p	X
iajs-850	66	29	(	(	PUNCT
iajs-850	66	30	110	110	NUM
iajs-850	66	31	-	-	PUNCT
iajs-850	66	32	112˚c	112˚c	NUM
iajs-850	66	33	)	)	PUNCT
iajs-850	66	34	.	.	PUNCT
iajs-850	67	1	rf	rf	PRON
iajs-850	67	2	(	(	PUNCT
iajs-850	67	3	0.63	0.63	NUM
iajs-850	67	4	)	)	PUNCT
iajs-850	67	5	(	(	PUNCT
iajs-850	67	6	benzene	benzene	NOUN
iajs-850	67	7	:	:	PUNCT
iajs-850	67	8	methanol	methanol	NOUN
iajs-850	67	9	,	,	PUNCT
iajs-850	67	10	6:4	6:4	NUM
iajs-850	67	11	)	)	PUNCT
iajs-850	67	12	(	(	PUNCT
iajs-850	67	13	v	v	NOUN
iajs-850	67	14	/	/	SYM
iajs-850	67	15	v	v	NOUN
iajs-850	67	16	)	)	PUNCT
iajs-850	67	17	.	.	PUNCT
iajs-850	68	1	ftir	ftir	PROPN
iajs-850	68	2	(	(	PUNCT
iajs-850	68	3	kbr	kbr	PROPN
iajs-850	68	4	,	,	PUNCT
iajs-850	68	5	cm	cm	NOUN
iajs-850	68	6	-1	-1	PRON
iajs-850	68	7	):	):	PUNCT
iajs-850	68	8	3080	3080	NUM
iajs-850	68	9	ibn	ibn	PROPN
iajs-850	68	10	alhaitham	alhaitham	NOUN
iajs-850	68	11	j.	j.	PROPN
iajs-850	68	12	for	for	ADP
iajs-850	68	13	pure	pure	ADJ
iajs-850	68	14	&	&	CCONJ
iajs-850	68	15	appl	appl	PROPN
iajs-850	68	16	.	.	PUNCT
iajs-850	69	1	sci	sci	PROPN
iajs-850	69	2	.	.	PUNCT
iajs-850	69	3	vol.24	vol.24	NOUN
iajs-850	69	4	(	(	PUNCT
iajs-850	69	5	1	1	NUM
iajs-850	69	6	)	)	PUNCT
iajs-850	69	7	2011	2011	NUM
iajs-850	69	8	(	(	PUNCT
iajs-850	69	9	c	c	NOUN
iajs-850	69	10	-	-	PUNCT
iajs-850	69	11	har	har	X
iajs-850	69	12	.	.	PUNCT
iajs-850	69	13	)	)	PUNCT
iajs-850	69	14	,	,	PUNCT
iajs-850	69	15	2839	2839	NUM
iajs-850	69	16	,	,	PUNCT
iajs-850	69	17	2677	2677	NUM
iajs-850	69	18	(	(	PUNCT
iajs-850	69	19	c	c	NOUN
iajs-850	69	20	-	-	PUNCT
iajs-850	69	21	hald	hald	NOUN
iajs-850	69	22	.	.	PUNCT
iajs-850	69	23	)	)	PUNCT
iajs-850	69	24	,	,	PUNCT
iajs-850	69	25	1689	1689	NUM
iajs-850	69	26	(	(	PUNCT
iajs-850	69	27	c	c	NOUN
iajs-850	69	28	=	=	NOUN
iajs-850	69	29	oald	oald	NOUN
iajs-850	69	30	.	.	PUNCT
iajs-850	69	31	)	)	PUNCT
iajs-850	69	32	,	,	PUNCT
iajs-850	69	33	900	900	NUM
iajs-850	69	34	-	-	SYM
iajs-850	69	35	600	600	NUM
iajs-850	69	36	δ(c	δ(c	PROPN
iajs-850	69	37	-	-	PUNCT
iajs-850	69	38	har	har	PROPN
iajs-850	69	39	.	.	PUNCT
iajs-850	69	40	)	)	PUNCT
iajs-850	70	1	(	(	PUNCT
iajs-850	70	2	o.o.p	o.o.p	X
iajs-850	70	3	.	.	PUNCT
iajs-850	70	4	)	)	PUNCT
iajs-850	70	5	.	.	PUNCT
iajs-850	71	1	1	1	NUM
iajs-850	71	2	hnmr	hnmr	NOUN
iajs-850	71	3	(	(	PUNCT
iajs-850	71	4	cdcl3	cdcl3	NOUN
iajs-850	71	5	):	):	PUNCT
iajs-850	71	6	δ(4.97	δ(4.97	NOUN
iajs-850	71	7	)	)	PUNCT
iajs-850	71	8	ppm	ppm	NOUN
iajs-850	71	9	(	(	PUNCT
iajs-850	71	10	s	s	PROPN
iajs-850	71	11	,	,	PUNCT
iajs-850	71	12	1h	1h	NUM
iajs-850	71	13	,	,	PUNCT
iajs-850	71	14	h4	h4	PROPN
iajs-850	71	15	)	)	PUNCT
iajs-850	71	16	,	,	PUNCT
iajs-850	71	17	δ	δ	PROPN
iajs-850	71	18	(	(	PUNCT
iajs-850	71	19	7.28	7.28	NUM
iajs-850	71	20	-	-	SYM
iajs-850	71	21	8.17	8.17	NUM
iajs-850	71	22	)	)	PUNCT
iajs-850	71	23	ppm	ppm	NOUN
iajs-850	71	24	(	(	PUNCT
iajs-850	71	25	m	m	PROPN
iajs-850	71	26	,	,	PUNCT
iajs-850	71	27	10h	10h	NUM
iajs-850	71	28	,	,	PUNCT
iajs-850	71	29	aromatic	aromatic	NOUN
iajs-850	71	30	)	)	PUNCT
iajs-850	71	31	,	,	PUNCT
iajs-850	71	32	δ(11.4	δ(11.4	NOUN
iajs-850	71	33	)	)	PUNCT
iajs-850	71	34	ppm	ppm	NOUN
iajs-850	71	35	(	(	PUNCT
iajs-850	71	36	br	br	PROPN
iajs-850	71	37	,	,	PUNCT
iajs-850	71	38	1h	1h	NUM
iajs-850	71	39	,	,	PUNCT
iajs-850	71	40	cho	cho	NOUN
iajs-850	71	41	.	.	PUNCT
iajs-850	71	42	)	)	PUNCT
iajs-850	71	43	.	.	PUNCT
iajs-850	72	1	13cnm	13cnm	INTJ
iajs-850	73	1	r	r	NOUN
iajs-850	73	2	(	(	PUNCT
iajs-850	73	3	cdcl3	cdcl3	NOUN
iajs-850	73	4	):	):	PUNCT
iajs-850	73	5	δ(172.44	δ(172.44	NOUN
iajs-850	73	6	)	)	PUNCT
iajs-850	73	7	ppm	ppm	NOUN
iajs-850	73	8	(	(	PUNCT
iajs-850	73	9	c	c	NOUN
iajs-850	73	10	=	=	NOUN
iajs-850	73	11	o	o	NOUN
iajs-850	73	12	)	)	PUNCT
iajs-850	73	13	,	,	PUNCT
iajs-850	73	14	δ(133.83	δ(133.83	PROPN
iajs-850	73	15	)	)	PUNCT
iajs-850	73	16	ppm	ppm	NOUN
iajs-850	73	17	(	(	PUNCT
iajs-850	73	18	c-3	c-3	NOUN
iajs-850	73	19	)	)	PUNCT
iajs-850	73	20	,	,	PUNCT
iajs-850	73	21	δ(133.47	δ(133.47	PROPN
iajs-850	73	22	)	)	PUNCT
iajs-850	73	23	ppm	ppm	NOUN
iajs-850	73	24	(	(	PUNCT
iajs-850	73	25	c-2	c-2	NOUN
iajs-850	73	26	)	)	PUNCT
iajs-850	73	27	,	,	PUNCT
iajs-850	73	28	δ(130.23	δ(130.23	PROPN
iajs-850	73	29	-	-	PUNCT
iajs-850	73	30	128.03	128.03	NUM
iajs-850	73	31	)	)	PUNCT
iajs-850	73	32	ppm	ppm	NOUN
iajs-850	73	33	(	(	PUNCT
iajs-850	73	34	car	car	NOUN
iajs-850	73	35	.	.	PUNCT
iajs-850	73	36	)	)	PUNCT
iajs-850	73	37	,	,	PUNCT
iajs-850	73	38	δ(77.46	δ(77.46	PROPN
iajs-850	73	39	)	)	PUNCT
iajs-850	73	40	ppm	ppm	NOUN
iajs-850	73	41	(	(	PUNCT
iajs-850	73	42	c-4	c-4	NOUN
iajs-850	73	43	)	)	PUNCT
iajs-850	73	44	.	.	PUNCT
iajs-850	74	1	the	the	DET
iajs-850	74	2	signal	signal	NOUN
iajs-850	74	3	of	of	ADP
iajs-850	74	4	aldehydic	aldehydic	ADJ
iajs-850	74	5	carbonyl	carbonyl	NOUN
iajs-850	74	6	was	be	AUX
iajs-850	74	7	disappeared	disappear	VERB
iajs-850	74	8	due	due	ADP
iajs-850	74	9	to	to	ADP
iajs-850	74	10	it	it	PRON
iajs-850	74	11	which	which	PRON
iajs-850	74	12	showed	show	VERB
iajs-850	74	13	out	out	ADP
iajs-850	74	14	of	of	ADP
iajs-850	74	15	the	the	DET
iajs-850	74	16	scale.[6	scale.[6	PRON
iajs-850	74	17	]	]	PUNCT
iajs-850	74	18	synthesis	synthesis	NOUN
iajs-850	74	19	of	of	ADP
iajs-850	74	20	5	5	NUM
iajs-850	74	21	-	-	PUNCT
iajs-850	74	22	c	c	NOUN
iajs-850	74	23	-	-	PUNCT
iajs-850	74	24	dimethyl	dimethyl	NOUN
iajs-850	74	25	malonyl	malonyl	NOUN
iajs-850	74	26	-	-	PUNCT
iajs-850	74	27	pentulose	pentulose	ADJ
iajs-850	74	28	-	-	PUNCT
iajs-850	74	29	γ	γ	NOUN
iajs-850	74	30	-	-	PUNCT
iajs-850	74	31	lactone-2,3	lactone-2,3	NOUN
iajs-850	74	32	-	-	PUNCT
iajs-850	74	33	enedibenzoate	enedibenzoate	NOUN
iajs-850	74	34	(	(	PUNCT
iajs-850	74	35	8)	8)	NUM
iajs-850	74	36	the	the	DET
iajs-850	74	37	mixture	mixture	NOUN
iajs-850	74	38	of	of	ADP
iajs-850	74	39	potassium	potassium	NOUN
iajs-850	74	40	hydroxide	hydroxide	NOUN
iajs-850	74	41	(	(	PUNCT
iajs-850	74	42	1.9	1.9	NUM
iajs-850	74	43	g	g	NOUN
iajs-850	74	44	,	,	PUNCT
iajs-850	74	45	34mmol	34mmol	NUM
iajs-850	74	46	)	)	PUNCT
iajs-850	74	47	and	and	CCONJ
iajs-850	74	48	dimethyl	dimethyl	NOUN
iajs-850	74	49	malonate	malonate	NOUN
iajs-850	74	50	(	(	PUNCT
iajs-850	74	51	3.9ml	3.9ml	PROPN
iajs-850	74	52	,	,	PUNCT
iajs-850	74	53	34mmol	34mmol	NUM
iajs-850	74	54	)	)	PUNCT
iajs-850	74	55	was	be	AUX
iajs-850	74	56	stirred	stir	VERB
iajs-850	74	57	for	for	ADP
iajs-850	74	58	30	30	NUM
iajs-850	74	59	minutes	minute	NOUN
iajs-850	74	60	,	,	PUNCT
iajs-850	74	61	a	a	DET
iajs-850	74	62	solution	solution	NOUN
iajs-850	74	63	of	of	ADP
iajs-850	74	64	(	(	PUNCT
iajs-850	74	65	7	7	NUM
iajs-850	74	66	)	)	PUNCT
iajs-850	74	67	(	(	PUNCT
iajs-850	74	68	10	10	NUM
iajs-850	74	69	g	g	NOUN
iajs-850	74	70	,	,	PUNCT
iajs-850	74	71	28.4mmol	28.4mmol	NUM
iajs-850	74	72	)	)	PUNCT
iajs-850	74	73	in	in	ADP
iajs-850	74	74	absolute	absolute	ADJ
iajs-850	74	75	ethanol	ethanol	NOUN
iajs-850	74	76	(	(	PUNCT
iajs-850	74	77	60ml	60ml	NOUN
iajs-850	74	78	)	)	PUNCT
iajs-850	74	79	was	be	AUX
iajs-850	74	80	added	add	VERB
iajs-850	74	81	.	.	PUNCT
iajs-850	75	1	after	after	ADP
iajs-850	75	2	stirring	stir	VERB
iajs-850	75	3	for	for	ADP
iajs-850	75	4	24	24	NUM
iajs-850	75	5	hours	hour	NOUN
iajs-850	75	6	at	at	ADP
iajs-850	75	7	room	room	NOUN
iajs-850	75	8	temperature	temperature	NOUN
iajs-850	75	9	,	,	PUNCT
iajs-850	75	10	the	the	DET
iajs-850	75	11	tlc	tlc	NOUN
iajs-850	75	12	showed	show	VERB
iajs-850	75	13	that	that	SCONJ
iajs-850	75	14	the	the	DET
iajs-850	75	15	reaction	reaction	NOUN
iajs-850	75	16	was	be	AUX
iajs-850	75	17	complete	complete	ADJ
iajs-850	75	18	(	(	PUNCT
iajs-850	75	19	benzene	benzene	NOUN
iajs-850	75	20	:	:	PUNCT
iajs-850	75	21	methanol	methanol	NOUN
iajs-850	75	22	,	,	PUNCT
iajs-850	75	23	4:6	4:6	NUM
iajs-850	75	24	)	)	PUNCT
iajs-850	75	25	and	and	CCONJ
iajs-850	75	26	the	the	DET
iajs-850	75	27	resulting	result	VERB
iajs-850	75	28	mixture	mixture	NOUN
iajs-850	75	29	was	be	AUX
iajs-850	75	30	filtered	filter	VERB
iajs-850	75	31	then	then	ADV
iajs-850	75	32	the	the	DET
iajs-850	75	33	solvent	solvent	NOUN
iajs-850	75	34	was	be	AUX
iajs-850	75	35	evaporated	evaporate	VERB
iajs-850	75	36	,	,	PUNCT
iajs-850	75	37	the	the	DET
iajs-850	75	38	combined	combined	ADJ
iajs-850	75	39	residue	residue	NOUN
iajs-850	75	40	was	be	AUX
iajs-850	75	41	washed	wash	VERB
iajs-850	75	42	with	with	ADP
iajs-850	75	43	chloroform	chloroform	NOUN
iajs-850	75	44	and	and	CCONJ
iajs-850	75	45	then	then	ADV
iajs-850	75	46	petroleum	petroleum	NOUN
iajs-850	75	47	ether	ether	NOUN
iajs-850	75	48	(	(	PUNCT
iajs-850	75	49	6080˚c	6080˚c	NUM
iajs-850	75	50	)	)	PUNCT
iajs-850	75	51	to	to	PART
iajs-850	75	52	give	give	VERB
iajs-850	75	53	(	(	PUNCT
iajs-850	75	54	8)	8)	NUM
iajs-850	75	55	(	(	PUNCT
iajs-850	75	56	10	10	NUM
iajs-850	75	57	g	g	NOUN
iajs-850	75	58	,	,	PUNCT
iajs-850	75	59	72.7	72.7	NUM
iajs-850	75	60	%	%	NOUN
iajs-850	75	61	)	)	PUNCT
iajs-850	75	62	as	as	ADP
iajs-850	75	63	a	a	DET
iajs-850	75	64	white	white	ADJ
iajs-850	75	65	crystals	crystal	NOUN
iajs-850	75	66	,	,	PUNCT
iajs-850	75	67	m.p	m.p	X
iajs-850	75	68	(	(	PUNCT
iajs-850	75	69	dec.240˚c	dec.240˚c	NOUN
iajs-850	75	70	)	)	PUNCT
iajs-850	75	71	,	,	PUNCT
iajs-850	75	72	rf	rf	ADJ
iajs-850	75	73	(	(	PUNCT
iajs-850	75	74	0.65	0.65	NUM
iajs-850	75	75	)	)	PUNCT
iajs-850	75	76	.	.	PUNCT
iajs-850	76	1	ftir	ftir	PROPN
iajs-850	76	2	(	(	PUNCT
iajs-850	76	3	kbr	kbr	PROPN
iajs-850	76	4	,	,	PUNCT
iajs-850	76	5	cm-1	cm-1	PROPN
iajs-850	76	6	):	):	PUNCT
iajs-850	76	7	3402	3402	NUM
iajs-850	76	8	(	(	PUNCT
iajs-850	76	9	o	o	NOUN
iajs-850	76	10	-	-	NOUN
iajs-850	76	11	h	h	NOUN
iajs-850	76	12	)	)	PUNCT
iajs-850	76	13	,	,	PUNCT
iajs-850	76	14	3055	3055	NUM
iajs-850	76	15	(	(	PUNCT
iajs-850	76	16	c	c	NOUN
iajs-850	76	17	-	-	PUNCT
iajs-850	76	18	har	har	X
iajs-850	76	19	.	.	PUNCT
iajs-850	76	20	)	)	PUNCT
iajs-850	76	21	,	,	PUNCT
iajs-850	76	22	2904	2904	NUM
iajs-850	76	23	(	(	PUNCT
iajs-850	76	24	c	c	NOUN
iajs-850	76	25	-	-	PUNCT
iajs-850	76	26	hali	hali	PROPN
iajs-850	76	27	.	.	PUNCT
iajs-850	76	28	)	)	PUNCT
iajs-850	76	29	,	,	PUNCT
iajs-850	76	30	1720	1720	NUM
iajs-850	76	31	(	(	PUNCT
iajs-850	76	32	c	c	NOUN
iajs-850	76	33	=	=	NOUN
iajs-850	76	34	oest	o	ADJ
iajs-850	76	35	.	.	PUNCT
iajs-850	76	36	)	)	PUNCT
iajs-850	76	37	,	,	PUNCT
iajs-850	76	38	1581	1581	NUM
iajs-850	76	39	(	(	PUNCT
iajs-850	76	40	c	c	X
iajs-850	76	41	=	=	NOUN
iajs-850	76	42	cali	cali	ADJ
iajs-850	76	43	.	.	PUNCT
iajs-850	76	44	)	)	PUNCT
iajs-850	76	45	,	,	PUNCT
iajs-850	76	46	1450(c	1450(c	NUM
iajs-850	76	47	=	=	SYM
iajs-850	76	48	car	car	NOUN
iajs-850	76	49	.	.	PUNCT
iajs-850	76	50	)	)	PUNCT
iajs-850	76	51	,	,	PUNCT
iajs-850	76	52	1400	1400	NUM
iajs-850	76	53	-	-	SYM
iajs-850	76	54	1000	1000	NUM
iajs-850	76	55	(	(	PUNCT
iajs-850	76	56	c	c	NOUN
iajs-850	76	57	-	-	PUNCT
iajs-850	76	58	o	o	NOUN
iajs-850	76	59	)	)	PUNCT
iajs-850	76	60	,	,	PUNCT
iajs-850	76	61	900	900	NUM
iajs-850	76	62	-	-	SYM
iajs-850	76	63	600	600	NUM
iajs-850	76	64	δ(c	δ(c	PROPN
iajs-850	76	65	-	-	PUNCT
iajs-850	76	66	har	har	PROPN
iajs-850	76	67	.	.	PUNCT
iajs-850	76	68	)	)	PUNCT
iajs-850	77	1	(	(	PUNCT
iajs-850	77	2	o.o.p	o.o.p	X
iajs-850	77	3	.	.	PUNCT
iajs-850	77	4	)	)	PUNCT
iajs-850	77	5	.	.	PUNCT
iajs-850	78	1	1hnmr	1hnmr	NUM
iajs-850	78	2	(	(	PUNCT
iajs-850	78	3	dm	dm	NOUN
iajs-850	78	4	so	so	ADV
iajs-850	78	5	):	):	PUNCT
iajs-850	78	6	δ(2.50	δ(2.50	PROPN
iajs-850	78	7	)	)	PUNCT
iajs-850	78	8	ppm	ppm	NOUN
iajs-850	78	9	(	(	PUNCT
iajs-850	78	10	dm	dm	NOUN
iajs-850	78	11	so	so	ADV
iajs-850	78	12	)	)	PUNCT
iajs-850	78	13	,	,	PUNCT
iajs-850	78	14	δ(2.72	δ(2.72	PROPN
iajs-850	78	15	)	)	PUNCT
iajs-850	78	16	ppm	ppm	NOUN
iajs-850	78	17	(	(	PUNCT
iajs-850	78	18	d	d	NOUN
iajs-850	78	19	,	,	PUNCT
iajs-850	78	20	1h	1h	NUM
iajs-850	78	21	,	,	PUNCT
iajs-850	78	22	ch	ch	NOUN
iajs-850	78	23	malonate	malonate	NOUN
iajs-850	78	24	)	)	PUNCT
iajs-850	78	25	,	,	PUNCT
iajs-850	78	26	δ(3.16	δ(3.16	PROPN
iajs-850	78	27	)	)	PUNCT
iajs-850	78	28	ppm	ppm	NOUN
iajs-850	78	29	(	(	PUNCT
iajs-850	78	30	s	s	X
iajs-850	78	31	,	,	PUNCT
iajs-850	78	32	1h	1h	NUM
iajs-850	78	33	,	,	PUNCT
iajs-850	78	34	oh	oh	INTJ
iajs-850	78	35	)	)	PUNCT
iajs-850	78	36	,	,	PUNCT
iajs-850	78	37	δ(3.56	δ(3.56	PROPN
iajs-850	78	38	-	-	PUNCT
iajs-850	78	39	3.58	3.58	NUM
iajs-850	78	40	)	)	PUNCT
iajs-850	78	41	ppm	ppm	NOUN
iajs-850	78	42	(	(	PUNCT
iajs-850	78	43	s	s	PROPN
iajs-850	78	44	,	,	PUNCT
iajs-850	78	45	6h	6h	NUM
iajs-850	78	46	,	,	PUNCT
iajs-850	78	47	2ch3	2ch3	NUM
iajs-850	78	48	malonate	malonate	NOUN
iajs-850	78	49	)	)	PUNCT
iajs-850	78	50	,	,	PUNCT
iajs-850	78	51	δ(7.14	δ(7.14	PROPN
iajs-850	78	52	-	-	PUNCT
iajs-850	78	53	8.86	8.86	NUM
iajs-850	78	54	)	)	PUNCT
iajs-850	78	55	ppm	ppm	NOUN
iajs-850	78	56	(	(	PUNCT
iajs-850	78	57	m	m	PROPN
iajs-850	78	58	,	,	PUNCT
iajs-850	78	59	10h	10h	NUM
iajs-850	78	60	,	,	PUNCT
iajs-850	78	61	aromatic	aromatic	NOUN
iajs-850	78	62	)	)	PUNCT
iajs-850	78	63	.	.	PUNCT
iajs-850	79	1	13cnm	13cnm	INTJ
iajs-850	80	1	r	r	NOUN
iajs-850	80	2	(	(	PUNCT
iajs-850	80	3	cdcl3	cdcl3	NOUN
iajs-850	80	4	):	):	PUNCT
iajs-850	80	5	δ(168.82	δ(168.82	PROPN
iajs-850	80	6	)	)	PUNCT
iajs-850	80	7	ppm	ppm	NOUN
iajs-850	80	8	(	(	PUNCT
iajs-850	80	9	c	c	NOUN
iajs-850	80	10	=	=	NOUN
iajs-850	80	11	o	o	NOUN
iajs-850	80	12	)	)	PUNCT
iajs-850	80	13	,	,	PUNCT
iajs-850	80	14	δ(135.26	δ(135.26	PROPN
iajs-850	80	15	)	)	PUNCT
iajs-850	80	16	ppm	ppm	NOUN
iajs-850	80	17	(	(	PUNCT
iajs-850	80	18	c-3	c-3	NOUN
iajs-850	80	19	)	)	PUNCT
iajs-850	80	20	,	,	PUNCT
iajs-850	80	21	δ(131.55	δ(131.55	NOUN
iajs-850	80	22	)	)	PUNCT
iajs-850	80	23	ppm	ppm	NOUN
iajs-850	80	24	(	(	PUNCT
iajs-850	80	25	c-2	c-2	NOUN
iajs-850	80	26	)	)	PUNCT
iajs-850	80	27	,	,	PUNCT
iajs-850	80	28	δ(129.58,128.40	δ(129.58,128.40	PROPN
iajs-850	80	29	)	)	PUNCT
iajs-850	80	30	ppm	ppm	NOUN
iajs-850	80	31	(	(	PUNCT
iajs-850	80	32	car	car	NOUN
iajs-850	80	33	.	.	PUNCT
iajs-850	80	34	)	)	PUNCT
iajs-850	80	35	,	,	PUNCT
iajs-850	80	36	δ(51.63	δ(51.63	X
iajs-850	80	37	)	)	PUNCT
iajs-850	80	38	ppm	ppm	NOUN
iajs-850	80	39	(	(	PUNCT
iajs-850	80	40	c-4	c-4	NOUN
iajs-850	80	41	)	)	PUNCT
iajs-850	80	42	,	,	PUNCT
iajs-850	80	43	δ(44.67	δ(44.67	PROPN
iajs-850	80	44	)	)	PUNCT
iajs-850	80	45	ppm	ppm	NOUN
iajs-850	80	46	(	(	PUNCT
iajs-850	80	47	c-5	c-5	NOUN
iajs-850	80	48	)	)	PUNCT
iajs-850	80	49	,	,	PUNCT
iajs-850	80	50	δ(40.78	δ(40.78	NOUN
iajs-850	80	51	-	-	PUNCT
iajs-850	80	52	39.11	39.11	NUM
iajs-850	80	53	)	)	PUNCT
iajs-850	80	54	ppm	ppm	NOUN
iajs-850	80	55	(	(	PUNCT
iajs-850	80	56	c-6	c-6	NOUN
iajs-850	80	57	and	and	CCONJ
iajs-850	80	58	carbon	carbon	NOUN
iajs-850	80	59	2ch3	2ch3	NUM
iajs-850	80	60	malonate	malonate	NOUN
iajs-850	80	61	)	)	PUNCT
iajs-850	80	62	.	.	PUNCT
iajs-850	81	1	synthesis	synthesis	NOUN
iajs-850	81	2	of	of	ADP
iajs-850	81	3	pentulose	pentulose	ADJ
iajs-850	81	4	-	-	PUNCT
iajs-850	81	5	γ	γ	NOUN
iajs-850	81	6	-	-	PUNCT
iajs-850	81	7	lactone-2,3	lactone-2,3	ADJ
iajs-850	81	8	-	-	PUNCT
iajs-850	81	9	enedibenzoate	enedibenzoate	NOUN
iajs-850	81	10	barbituric	barbituric	NOUN
iajs-850	81	11	acid	acid	NOUN
iajs-850	81	12	(	(	PUNCT
iajs-850	81	13	9	9	NUM
iajs-850	81	14	)	)	PUNCT
iajs-850	81	15	or	or	CCONJ
iajs-850	81	16	thiobarbituric	thiobarbituric	ADJ
iajs-850	81	17	acid	acid	NOUN
iajs-850	81	18	(	(	PUNCT
iajs-850	81	19	10	10	NUM
iajs-850	81	20	)	)	PUNCT
iajs-850	81	21	or	or	CCONJ
iajs-850	81	22	azhydrobarbituric	azhydrobarbituric	ADJ
iajs-850	81	23	acid	acid	NOUN
iajs-850	81	24	(	(	PUNCT
iajs-850	81	25	11	11	NUM
iajs-850	81	26	)	)	PUNCT
iajs-850	81	27	to	to	ADP
iajs-850	81	28	the	the	DET
iajs-850	81	29	solution	solution	NOUN
iajs-850	81	30	of	of	ADP
iajs-850	81	31	sodium	sodium	NOUN
iajs-850	81	32	methoxide	methoxide	NOUN
iajs-850	81	33	(	(	PUNCT
iajs-850	81	34	30.9mmol	30.9mmol	NUM
iajs-850	81	35	of	of	ADP
iajs-850	81	36	sodium	sodium	NOUN
iajs-850	81	37	metal	metal	NOUN
iajs-850	81	38	dissolved	dissolve	VERB
iajs-850	81	39	in	in	ADP
iajs-850	81	40	absolute	absolute	ADJ
iajs-850	81	41	methanol	methanol	NOUN
iajs-850	81	42	(	(	PUNCT
iajs-850	81	43	20ml	20ml	NOUN
iajs-850	81	44	)	)	PUNCT
iajs-850	81	45	)	)	PUNCT
iajs-850	81	46	,	,	PUNCT
iajs-850	81	47	dry	dry	ADJ
iajs-850	81	48	urea	urea	NOUN
iajs-850	81	49	or	or	CCONJ
iajs-850	81	50	thiourea	thiourea	NOUN
iajs-850	81	51	or	or	CCONJ
iajs-850	81	52	guanidine	guanidine	ADJ
iajs-850	81	53	hydrochloride	hydrochloride	NOUN
iajs-850	81	54	(	(	PUNCT
iajs-850	81	55	15.5mmol	15.5mmol	NOUN
iajs-850	81	56	)	)	PUNCT
iajs-850	81	57	was	be	AUX
iajs-850	81	58	added	add	VERB
iajs-850	81	59	,	,	PUNCT
iajs-850	81	60	stirring	stir	VERB
iajs-850	81	61	at	at	ADP
iajs-850	81	62	room	room	NOUN
iajs-850	81	63	temperature	temperature	NOUN
iajs-850	81	64	for	for	ADP
iajs-850	81	65	1	1	NUM
iajs-850	81	66	hour	hour	NOUN
iajs-850	81	67	.	.	PUNCT
iajs-850	82	1	the	the	DET
iajs-850	82	2	compound	compound	NOUN
iajs-850	82	3	(	(	PUNCT
iajs-850	82	4	8)	8)	NUM
iajs-850	82	5	(	(	PUNCT
iajs-850	82	6	5	5	NUM
iajs-850	82	7	g	g	NOUN
iajs-850	82	8	,	,	PUNCT
iajs-850	82	9	10.3mmol	10.3mmol	NUM
iajs-850	82	10	)	)	PUNCT
iajs-850	82	11	in	in	ADP
iajs-850	82	12	absolute	absolute	ADJ
iajs-850	82	13	methanol	methanol	NOUN
iajs-850	82	14	(	(	PUNCT
iajs-850	82	15	30ml	30ml	NOUN
iajs-850	82	16	)	)	PUNCT
iajs-850	82	17	was	be	AUX
iajs-850	82	18	added	add	VERB
iajs-850	82	19	,	,	PUNCT
iajs-850	82	20	stirring	stirring	NOUN
iajs-850	82	21	was	be	AUX
iajs-850	82	22	continued	continue	VERB
iajs-850	82	23	at	at	ADP
iajs-850	82	24	room	room	NOUN
iajs-850	82	25	temperature	temperature	NOUN
iajs-850	82	26	for	for	ADP
iajs-850	82	27	48	48	NUM
iajs-850	82	28	hours	hour	NOUN
iajs-850	82	29	.	.	PUNCT
iajs-850	83	1	the	the	DET
iajs-850	83	2	tlc	tlc	NOUN
iajs-850	83	3	showed	show	VERB
iajs-850	83	4	that	that	SCONJ
iajs-850	83	5	the	the	DET
iajs-850	83	6	reaction	reaction	NOUN
iajs-850	83	7	was	be	AUX
iajs-850	83	8	complete	complete	ADJ
iajs-850	83	9	(	(	PUNCT
iajs-850	83	10	benzene	benzene	NOUN
iajs-850	83	11	:	:	PUNCT
iajs-850	83	12	methanol	methanol	NOUN
iajs-850	83	13	,	,	PUNCT
iajs-850	83	14	4:6	4:6	NUM
iajs-850	83	15	)	)	PUNCT
iajs-850	83	16	.	.	PUNCT
iajs-850	84	1	the	the	DET
iajs-850	84	2	solvent	solvent	NOUN
iajs-850	84	3	was	be	AUX
iajs-850	84	4	evaporated	evaporate	VERB
iajs-850	84	5	;	;	PUNCT
iajs-850	84	6	the	the	DET
iajs-850	84	7	combined	combined	ADJ
iajs-850	84	8	residue	residue	NOUN
iajs-850	84	9	was	be	AUX
iajs-850	84	10	washed	wash	VERB
iajs-850	84	11	with	with	ADP
iajs-850	84	12	hot	hot	ADJ
iajs-850	84	13	absolute	absolute	ADJ
iajs-850	84	14	ethanol	ethanol	NOUN
iajs-850	84	15	to	to	PART
iajs-850	84	16	give	give	VERB
iajs-850	84	17	(	(	PUNCT
iajs-850	84	18	9	9	NUM
iajs-850	84	19	)	)	PUNCT
iajs-850	84	20	,	,	PUNCT
iajs-850	84	21	(	(	PUNCT
iajs-850	84	22	10	10	NUM
iajs-850	84	23	)	)	PUNCT
iajs-850	84	24	,	,	PUNCT
iajs-850	84	25	and	and	CCONJ
iajs-850	84	26	(	(	PUNCT
iajs-850	84	27	11	11	NUM
iajs-850	84	28	)	)	PUNCT
iajs-850	84	29	respectively	respectively	ADV
iajs-850	84	30	.	.	PUNCT
iajs-850	85	1	the	the	DET
iajs-850	85	2	physical	physical	ADJ
iajs-850	85	3	properties	property	NOUN
iajs-850	85	4	for	for	ADP
iajs-850	85	5	prepared	prepared	ADJ
iajs-850	85	6	compounds	compound	NOUN
iajs-850	85	7	showed	show	VERB
iajs-850	85	8	in	in	ADP
iajs-850	85	9	table	table	NOUN
iajs-850	85	10	(	(	PUNCT
iajs-850	85	11	1	1	NUM
iajs-850	85	12	)	)	PUNCT
iajs-850	85	13	.	.	PUNCT
iajs-850	86	1	the	the	DET
iajs-850	86	2	ftir	ftir	PROPN
iajs-850	86	3	,	,	PUNCT
iajs-850	86	4	1hnmr	1hnmr	NUM
iajs-850	86	5	and	and	CCONJ
iajs-850	86	6	13cnm	13cnm	NOUN
iajs-850	86	7	r	r	PROPN
iajs-850	86	8	spectra	spectra	ADJ
iajs-850	86	9	data	datum	NOUN
iajs-850	86	10	are	be	AUX
iajs-850	86	11	given	give	VERB
iajs-850	86	12	in	in	ADP
iajs-850	86	13	tables	table	NOUN
iajs-850	86	14	(	(	PUNCT
iajs-850	86	15	2	2	NUM
iajs-850	86	16	)	)	PUNCT
iajs-850	86	17	,	,	PUNCT
iajs-850	86	18	(	(	PUNCT
iajs-850	86	19	3	3	X
iajs-850	86	20	)	)	PUNCT
iajs-850	86	21	and	and	CCONJ
iajs-850	86	22	(	(	PUNCT
iajs-850	86	23	4	4	NUM
iajs-850	86	24	)	)	PUNCT
iajs-850	86	25	.	.	PUNCT
iajs-850	87	1	results	result	NOUN
iajs-850	87	2	and	and	CCONJ
iajs-850	87	3	discussion	discussion	NOUN
iajs-850	87	4	l	l	ADJ
iajs-850	87	5	-	-	ADJ
iajs-850	87	6	ascorbic	ascorbic	ADJ
iajs-850	87	7	acid	acid	NOUN
iajs-850	87	8	(	(	PUNCT
iajs-850	87	9	3	3	NUM
iajs-850	87	10	)	)	PUNCT
iajs-850	87	11	is	be	AUX
iajs-850	87	12	one	one	NUM
iajs-850	87	13	of	of	ADP
iajs-850	87	14	the	the	DET
iajs-850	87	15	natural	natural	ADJ
iajs-850	87	16	antioxidant	antioxidant	NOUN
iajs-850	87	17	present	present	NOUN
iajs-850	87	18	in	in	ADP
iajs-850	87	19	biological	biological	ADJ
iajs-850	87	20	system	system	NOUN
iajs-850	87	21	because	because	SCONJ
iajs-850	87	22	of	of	ADP
iajs-850	87	23	its	its	PRON
iajs-850	87	24	activity	activity	NOUN
iajs-850	87	25	to	to	PART
iajs-850	87	26	attack	attack	VERB
iajs-850	87	27	the	the	DET
iajs-850	87	28	free	free	ADJ
iajs-850	87	29	radicals	radical	NOUN
iajs-850	87	30	and	and	CCONJ
iajs-850	87	31	other	other	ADJ
iajs-850	87	32	reactive	reactive	ADJ
iajs-850	87	33	oxygen	oxygen	NOUN
iajs-850	87	34	species	specie	NOUN
iajs-850	87	35	,	,	PUNCT
iajs-850	87	36	as	as	SCONJ
iajs-850	87	37	the	the	DET
iajs-850	87	38	literatures	literature	NOUN
iajs-850	87	39	points	point	VERB
iajs-850	87	40	to	to	ADP
iajs-850	87	41	the	the	DET
iajs-850	87	42	great	great	ADJ
iajs-850	87	43	role	role	NOUN
iajs-850	87	44	which	which	PRON
iajs-850	87	45	ascorbic	ascorbic	NOUN
iajs-850	87	46	acid	acid	NOUN
iajs-850	87	47	plays	play	VERB
iajs-850	87	48	to	to	PART
iajs-850	87	49	prevent	prevent	VERB
iajs-850	87	50	a	a	DET
iajs-850	87	51	number	number	NOUN
iajs-850	87	52	of	of	ADP
iajs-850	87	53	disease	disease	NOUN
iajs-850	87	54	and	and	CCONJ
iajs-850	87	55	its	its	PRON
iajs-850	87	56	importance	importance	NOUN
iajs-850	87	57	in	in	ADP
iajs-850	87	58	food	food	NOUN
iajs-850	87	59	industry.[7],[8	industry.[7],[8	PROPN
iajs-850	87	60	]	]	X
iajs-850	87	61	one	one	NUM
iajs-850	87	62	strategy	strategy	NOUN
iajs-850	87	63	allows	allow	VERB
iajs-850	87	64	the	the	DET
iajs-850	87	65	synthesis	synthesis	NOUN
iajs-850	87	66	of	of	ADP
iajs-850	87	67	compounds	compound	NOUN
iajs-850	87	68	(	(	PUNCT
iajs-850	87	69	9	9	NUM
iajs-850	87	70	)	)	PUNCT
iajs-850	87	71	,	,	PUNCT
iajs-850	87	72	(	(	PUNCT
iajs-850	87	73	10	10	NUM
iajs-850	87	74	)	)	PUNCT
iajs-850	87	75	and	and	CCONJ
iajs-850	87	76	(	(	PUNCT
iajs-850	87	77	11	11	NUM
iajs-850	87	78	)	)	PUNCT
iajs-850	87	79	in	in	ADP
iajs-850	87	80	(	(	PUNCT
iajs-850	87	81	6	6	NUM
iajs-850	87	82	)	)	PUNCT
iajs-850	87	83	steps	step	NOUN
iajs-850	87	84	starting	start	VERB
iajs-850	87	85	from	from	ADP
iajs-850	87	86	l	l	ADJ
iajs-850	87	87	-	-	ADJ
iajs-850	87	88	ascorbic	ascorbic	ADJ
iajs-850	87	89	acid	acid	NOUN
iajs-850	87	90	,	,	PUNCT
iajs-850	87	91	scheme	scheme	NOUN
iajs-850	87	92	(	(	PUNCT
iajs-850	87	93	1	1	NUM
iajs-850	87	94	)	)	PUNCT
iajs-850	87	95	.	.	PUNCT
iajs-850	88	1	the	the	DET
iajs-850	88	2	first	first	ADJ
iajs-850	88	3	step	step	NOUN
iajs-850	88	4	employs	employ	VERB
iajs-850	88	5	the	the	DET
iajs-850	88	6	protection	protection	NOUN
iajs-850	88	7	of	of	ADP
iajs-850	88	8	the	the	DET
iajs-850	88	9	hydroxyl	hydroxyl	NOUN
iajs-850	88	10	groups	group	NOUN
iajs-850	88	11	at	at	ADP
iajs-850	88	12	c-5	c-5	NOUN
iajs-850	88	13	and	and	CCONJ
iajs-850	88	14	c-6	c-6	NOUN
iajs-850	88	15	positions	position	NOUN
iajs-850	88	16	in	in	ADP
iajs-850	88	17	lascorbic	lascorbic	ADJ
iajs-850	88	18	acid	acid	NOUN
iajs-850	88	19	with	with	ADP
iajs-850	88	20	acetal	acetal	ADJ
iajs-850	88	21	formation	formation	NOUN
iajs-850	88	22	leading	lead	VERB
iajs-850	88	23	to	to	ADP
iajs-850	88	24	compound	compound	NOUN
iajs-850	88	25	(	(	PUNCT
iajs-850	88	26	4	4	X
iajs-850	88	27	)	)	PUNCT
iajs-850	88	28	using	use	VERB
iajs-850	88	29	dry	dry	ADJ
iajs-850	88	30	acetone	acetone	NOUN
iajs-850	88	31	in	in	ADP
iajs-850	88	32	acidic	acidic	ADJ
iajs-850	88	33	media	medium	NOUN
iajs-850	88	34	,	,	PUNCT
iajs-850	88	35	following	follow	VERB
iajs-850	88	36	salomon[9	salomon[9	ADV
iajs-850	88	37	]	]	PUNCT
iajs-850	88	38	method	method	NOUN
iajs-850	88	39	.	.	PUNCT
iajs-850	89	1	this	this	PRON
iajs-850	89	2	is	be	AUX
iajs-850	89	3	followed	follow	VERB
iajs-850	89	4	by	by	ADP
iajs-850	89	5	esterification	esterification	NOUN
iajs-850	89	6	of	of	ADP
iajs-850	89	7	the	the	DET
iajs-850	89	8	hydroxyl	hydroxyl	NOUN
iajs-850	89	9	groups	group	NOUN
iajs-850	89	10	at	at	ADP
iajs-850	89	11	c-2	c-2	NOUN
iajs-850	89	12	and	and	CCONJ
iajs-850	89	13	c-3	c-3	PROPN
iajs-850	89	14	positions	position	NOUN
iajs-850	89	15	with	with	ADP
iajs-850	89	16	excess	excess	NOUN
iajs-850	89	17	of	of	ADP
iajs-850	89	18	benzoyl	benzoyl	ADJ
iajs-850	89	19	chloride	chloride	NOUN
iajs-850	89	20	in	in	ADP
iajs-850	89	21	dry	dry	ADJ
iajs-850	89	22	pyridine	pyridine	NOUN
iajs-850	89	23	.	.	PUNCT
iajs-850	90	1	the	the	DET
iajs-850	90	2	ftir	ftir	PROPN
iajs-850	90	3	spectra	spectra	PROPN
iajs-850	90	4	for	for	ADP
iajs-850	90	5	compound	compound	NOUN
iajs-850	90	6	(	(	PUNCT
iajs-850	90	7	4	4	NUM
iajs-850	90	8	)	)	PUNCT
iajs-850	90	9	and	and	CCONJ
iajs-850	90	10	(	(	PUNCT
iajs-850	90	11	5	5	X
iajs-850	90	12	)	)	PUNCT
iajs-850	90	13	were	be	AUX
iajs-850	90	14	confirmed	confirm	VERB
iajs-850	90	15	the	the	DET
iajs-850	90	16	formation	formation	NOUN
iajs-850	90	17	of	of	ADP
iajs-850	90	18	compound	compound	NOUN
iajs-850	90	19	(	(	PUNCT
iajs-850	90	20	5	5	NUM
iajs-850	90	21	)	)	PUNCT
iajs-850	90	22	by	by	ADP
iajs-850	90	23	disappearance	disappearance	NOUN
iajs-850	90	24	of	of	ADP
iajs-850	90	25	the	the	DET
iajs-850	90	26	bands	band	NOUN
iajs-850	90	27	for	for	ADP
iajs-850	90	28	(	(	PUNCT
iajs-850	90	29	o	o	NOUN
iajs-850	90	30	-	-	NOUN
iajs-850	90	31	h	h	NOUN
iajs-850	90	32	)	)	PUNCT
iajs-850	90	33	of	of	ADP
iajs-850	90	34	compound	compound	NOUN
iajs-850	90	35	(	(	PUNCT
iajs-850	90	36	4	4	NUM
iajs-850	90	37	)	)	PUNCT
iajs-850	90	38	and	and	CCONJ
iajs-850	90	39	exhibited	exhibit	VERB
iajs-850	90	40	the	the	DET
iajs-850	90	41	band	band	NOUN
iajs-850	90	42	at	at	ADP
iajs-850	90	43	(	(	PUNCT
iajs-850	90	44	1662	1662	NUM
iajs-850	90	45	)	)	PUNCT
iajs-850	90	46	cm	cm	NOUN
iajs-850	90	47	-1	-1	NOUN
iajs-850	90	48	for	for	ADP
iajs-850	90	49	(	(	PUNCT
iajs-850	90	50	c	c	NOUN
iajs-850	90	51	=	=	NOUN
iajs-850	90	52	o	o	NOUN
iajs-850	90	53	)	)	PUNCT
iajs-850	90	54	of	of	ADP
iajs-850	90	55	the	the	DET
iajs-850	90	56	ester	ester	NOUN
iajs-850	90	57	in	in	ADP
iajs-850	90	58	compound	compound	NOUN
iajs-850	90	59	(	(	PUNCT
iajs-850	90	60	5	5	NUM
iajs-850	90	61	)	)	PUNCT
iajs-850	90	62	spectrum	spectrum	NOUN
iajs-850	90	63	.	.	PUNCT
iajs-850	91	1	in	in	ADP
iajs-850	91	2	order	order	NOUN
iajs-850	91	3	to	to	ADP
iajs-850	91	4	p	p	PROPN
iajs-850	91	5	repare	repare	PROPN
iajs-850	91	6	aldehyde	aldehyde	NOUN
iajs-850	91	7	(	(	PUNCT
iajs-850	91	8	7	7	NUM
iajs-850	91	9	)	)	PUNCT
iajs-850	91	10	,	,	PUNCT
iajs-850	91	11	the	the	DET
iajs-850	91	12	acetal	acetal	ADJ
iajs-850	91	13	moiety	moiety	NOUN
iajs-850	91	14	was	be	AUX
iajs-850	91	15	cleaved	cleave	VERB
iajs-850	91	16	under	under	ADP
iajs-850	91	17	acidic	acidic	ADJ
iajs-850	91	18	condition[10	condition[10	NOUN
iajs-850	91	19	]	]	PUNCT
iajs-850	91	20	(	(	PUNCT
iajs-850	91	21	65	65	NUM
iajs-850	91	22	%	%	NOUN
iajs-850	91	23	acetic	acetic	ADJ
iajs-850	91	24	acid	acid	NOUN
iajs-850	91	25	)	)	PUNCT
iajs-850	91	26	for	for	ADP
iajs-850	91	27	compound	compound	NOUN
iajs-850	91	28	(	(	PUNCT
iajs-850	91	29	5	5	NUM
iajs-850	91	30	)	)	PUNCT
iajs-850	91	31	to	to	PART
iajs-850	91	32	give	give	VERB
iajs-850	91	33	(	(	PUNCT
iajs-850	91	34	6	6	NUM
iajs-850	91	35	)	)	PUNCT
iajs-850	91	36	and	and	CCONJ
iajs-850	91	37	oxidation	oxidation	NOUN
iajs-850	91	38	of	of	ADP
iajs-850	91	39	the	the	DET
iajs-850	91	40	product	product	NOUN
iajs-850	91	41	with	with	ADP
iajs-850	91	42	sodium	sodium	NOUN
iajs-850	91	43	periodate	periodate	NOUN
iajs-850	91	44	to	to	PART
iajs-850	91	45	result	result	VERB
iajs-850	91	46	(	(	PUNCT
iajs-850	91	47	7	7	NUM
iajs-850	91	48	)	)	PUNCT
iajs-850	91	49	,	,	PUNCT
iajs-850	91	50	which	which	PRON
iajs-850	91	51	gave	give	VERB
iajs-850	91	52	a	a	DET
iajs-850	91	53	positive	positive	ADJ
iajs-850	91	54	tolen	tolen	NOUN
iajs-850	91	55	’s	’s	PART
iajs-850	91	56	test	test	NOUN
iajs-850	91	57	by	by	ADP
iajs-850	91	58	the	the	DET
iajs-850	91	59	formation	formation	NOUN
iajs-850	91	60	of	of	ADP
iajs-850	91	61	a	a	DET
iajs-850	91	62	silver	silver	ADJ
iajs-850	91	63	mirror.[11],[12	mirror.[11],[12	NOUN
iajs-850	91	64	]	]	X
iajs-850	91	65	the	the	DET
iajs-850	91	66	ftir	ftir	PROPN
iajs-850	91	67	spectra	spectra	PROPN
iajs-850	91	68	for	for	ADP
iajs-850	91	69	compound	compound	NOUN
iajs-850	91	70	(	(	PUNCT
iajs-850	91	71	6	6	NUM
iajs-850	91	72	)	)	PUNCT
iajs-850	91	73	and	and	CCONJ
iajs-850	91	74	(	(	PUNCT
iajs-850	91	75	7	7	X
iajs-850	91	76	)	)	PUNCT
iajs-850	91	77	confirmed	confirm	VERB
iajs-850	91	78	the	the	DET
iajs-850	91	79	formation	formation	NOUN
iajs-850	91	80	of	of	ADP
iajs-850	91	81	compound	compound	NOUN
iajs-850	91	82	(	(	PUNCT
iajs-850	91	83	7	7	NUM
iajs-850	91	84	)	)	PUNCT
iajs-850	91	85	by	by	ADP
iajs-850	91	86	disappearance	disappearance	NOUN
iajs-850	91	87	of	of	ADP
iajs-850	91	88	the	the	DET
iajs-850	91	89	bands	band	NOUN
iajs-850	91	90	for	for	ADP
iajs-850	91	91	(	(	PUNCT
iajs-850	91	92	o	o	NOUN
iajs-850	91	93	-	-	NOUN
iajs-850	91	94	h	h	NOUN
iajs-850	91	95	)	)	PUNCT
iajs-850	91	96	of	of	ADP
iajs-850	91	97	compound	compound	NOUN
iajs-850	91	98	(	(	PUNCT
iajs-850	91	99	6	6	NUM
iajs-850	91	100	)	)	PUNCT
iajs-850	91	101	and	and	CCONJ
iajs-850	91	102	exhibited	exhibit	VERB
iajs-850	91	103	the	the	DET
iajs-850	91	104	band	band	NOUN
iajs-850	91	105	at	at	ADP
iajs-850	91	106	(	(	PUNCT
iajs-850	91	107	1689	1689	NUM
iajs-850	91	108	)	)	PUNCT
iajs-850	91	109	cm	cm	NOUN
iajs-850	91	110	-1	-1	NOUN
iajs-850	91	111	for	for	ADP
iajs-850	91	112	(	(	PUNCT
iajs-850	91	113	c	c	NOUN
iajs-850	91	114	=	=	NOUN
iajs-850	91	115	o	o	NOUN
iajs-850	91	116	)	)	PUNCT
iajs-850	91	117	in	in	ADP
iajs-850	91	118	compound	compound	NOUN
iajs-850	91	119	(	(	PUNCT
iajs-850	91	120	7	7	NUM
iajs-850	91	121	)	)	PUNCT
iajs-850	91	122	spectrum	spectrum	NOUN
iajs-850	91	123	.	.	PUNCT
iajs-850	92	1	the	the	DET
iajs-850	92	2	structure	structure	NOUN
iajs-850	92	3	of	of	ADP
iajs-850	92	4	(	(	PUNCT
iajs-850	92	5	7	7	X
iajs-850	92	6	)	)	PUNCT
iajs-850	92	7	was	be	AUX
iajs-850	92	8	confirmed	confirm	VERB
iajs-850	92	9	ibn	ibn	PROPN
iajs-850	92	10	alhaitham	alhaitham	PROPN
iajs-850	92	11	j.	j.	PROPN
iajs-850	92	12	for	for	ADP
iajs-850	92	13	pure	pure	ADJ
iajs-850	92	14	&	&	CCONJ
iajs-850	92	15	appl	appl	PROPN
iajs-850	92	16	.	.	PUNCT
iajs-850	93	1	sci	sci	PROPN
iajs-850	93	2	.	.	PUNCT
iajs-850	93	3	vol.24	vol.24	NOUN
iajs-850	93	4	(	(	PUNCT
iajs-850	93	5	1	1	NUM
iajs-850	93	6	)	)	PUNCT
iajs-850	93	7	2011	2011	NUM
iajs-850	93	8	by	by	ADP
iajs-850	93	9	1	1	NUM
iajs-850	93	10	hnmr	hnmr	NOUN
iajs-850	93	11	which	which	PRON
iajs-850	93	12	exhibited	exhibit	VERB
iajs-850	93	13	a	a	DET
iajs-850	93	14	signal	signal	NOUN
iajs-850	93	15	at	at	ADP
iajs-850	93	16	δ(11.4	δ(11.4	NOUN
iajs-850	93	17	)	)	PUNCT
iajs-850	93	18	ppm	ppm	NOUN
iajs-850	93	19	for	for	ADP
iajs-850	93	20	(	(	PUNCT
iajs-850	93	21	cho	cho	NOUN
iajs-850	93	22	)	)	PUNCT
iajs-850	93	23	and	and	CCONJ
iajs-850	93	24	was	be	AUX
iajs-850	93	25	characterised	characterise	VERB
iajs-850	93	26	by	by	ADP
iajs-850	93	27	13cnmr	13cnmr	PROPN
iajs-850	93	28	and	and	CCONJ
iajs-850	93	29	(	(	PUNCT
iajs-850	93	30	u.v	u.v	PROPN
iajs-850	93	31	-	-	PUNCT
iajs-850	93	32	vis	vis	X
iajs-850	93	33	)	)	PUNCT
iajs-850	93	34	spectrum	spectrum	NOUN
iajs-850	93	35	which	which	PRON
iajs-850	93	36	showed	show	VERB
iajs-850	93	37	one	one	NUM
iajs-850	93	38	peak	peak	NOUN
iajs-850	93	39	at	at	ADP
iajs-850	93	40	(	(	PUNCT
iajs-850	93	41	295	295	NUM
iajs-850	93	42	)	)	PUNCT
iajs-850	93	43	nm	nm	NOUN
iajs-850	93	44	(	(	PUNCT
iajs-850	93	45	33898	33898	NUM
iajs-850	93	46	cm-1	cm-1	NOUN
iajs-850	93	47	)	)	PUNCT
iajs-850	93	48	(	(	PUNCT
iajs-850	93	49	εmax	εmax	NOUN
iajs-850	93	50	=	=	SYM
iajs-850	93	51	156	156	NUM
iajs-850	93	52	molar-1cm-1	molar-1cm-1	NOUN
iajs-850	93	53	)	)	PUNCT
iajs-850	93	54	assigned	assign	VERB
iajs-850	93	55	to	to	ADP
iajs-850	93	56	(	(	PUNCT
iajs-850	93	57	n	n	X
iajs-850	93	58	π	π	NOUN
iajs-850	93	59	*	*	NOUN
iajs-850	93	60	)	)	PUNCT
iajs-850	93	61	transition	transition	NOUN
iajs-850	93	62	.	.	PUNCT
iajs-850	94	1	the	the	DET
iajs-850	94	2	other	other	ADJ
iajs-850	94	3	step	step	NOUN
iajs-850	94	4	was	be	AUX
iajs-850	94	5	the	the	DET
iajs-850	94	6	formation	formation	NOUN
iajs-850	94	7	of	of	ADP
iajs-850	94	8	compound	compound	NOUN
iajs-850	94	9	(	(	PUNCT
iajs-850	94	10	8)	8)	NUM
iajs-850	94	11	from	from	ADP
iajs-850	94	12	the	the	DET
iajs-850	94	13	reaction	reaction	NOUN
iajs-850	94	14	of	of	ADP
iajs-850	94	15	an	an	DET
iajs-850	94	16	aldehyde	aldehyde	NOUN
iajs-850	94	17	(	(	PUNCT
iajs-850	94	18	7	7	NUM
iajs-850	94	19	)	)	PUNCT
iajs-850	94	20	with	with	ADP
iajs-850	94	21	dimethyl	dimethyl	PROPN
iajs-850	94	22	malonate	malonate	PROPN
iajs-850	94	23	.	.	PUNCT
iajs-850	95	1	the	the	DET
iajs-850	95	2	ftir	ftir	PROPN
iajs-850	95	3	spectrum	spectrum	PROPN
iajs-850	95	4	of	of	ADP
iajs-850	95	5	(	(	PUNCT
iajs-850	95	6	8)	8)	NUM
iajs-850	95	7	showed	show	VERB
iajs-850	95	8	the	the	DET
iajs-850	95	9	bands	band	NOUN
iajs-850	95	10	at	at	ADP
iajs-850	95	11	(	(	PUNCT
iajs-850	95	12	3402	3402	NUM
iajs-850	95	13	)	)	PUNCT
iajs-850	95	14	cm-1	cm-1	PROPN
iajs-850	95	15	and	and	CCONJ
iajs-850	95	16	(	(	PUNCT
iajs-850	95	17	1720	1720	NUM
iajs-850	95	18	)	)	PUNCT
iajs-850	95	19	cm	cm	NOUN
iajs-850	95	20	-1	-1	PUNCT
iajs-850	95	21	due	due	ADP
iajs-850	95	22	to	to	PART
iajs-850	95	23	(	(	PUNCT
iajs-850	95	24	o	o	NOUN
iajs-850	95	25	-	-	NOUN
iajs-850	95	26	h	h	NOUN
iajs-850	95	27	)	)	PUNCT
iajs-850	95	28	and	and	CCONJ
iajs-850	95	29	(	(	PUNCT
iajs-850	95	30	c	c	X
iajs-850	95	31	=	=	NOUN
iajs-850	95	32	o	o	NOUN
iajs-850	95	33	)	)	PUNCT
iajs-850	95	34	of	of	ADP
iajs-850	95	35	the	the	DET
iajs-850	95	36	ester	ester	NOUN
iajs-850	95	37	respectively	respectively	ADV
iajs-850	95	38	and	and	CCONJ
iajs-850	95	39	disappearance	disappearance	NOUN
iajs-850	95	40	of	of	ADP
iajs-850	95	41	the	the	DET
iajs-850	95	42	band	band	NOUN
iajs-850	95	43	for	for	ADP
iajs-850	95	44	(	(	PUNCT
iajs-850	95	45	c	c	NOUN
iajs-850	95	46	=	=	NOUN
iajs-850	95	47	o	o	NOUN
iajs-850	95	48	)	)	PUNCT
iajs-850	95	49	aldehydic	aldehydic	ADJ
iajs-850	95	50	.	.	PUNCT
iajs-850	96	1	the	the	DET
iajs-850	96	2	structure	structure	NOUN
iajs-850	96	3	of	of	ADP
iajs-850	96	4	(	(	PUNCT
iajs-850	96	5	8)	8)	NUM
iajs-850	96	6	was	be	AUX
iajs-850	96	7	confirmed	confirm	VERB
iajs-850	96	8	by	by	ADP
iajs-850	96	9	the	the	DET
iajs-850	96	10	disappeared	disappear	VERB
iajs-850	96	11	of	of	ADP
iajs-850	96	12	a	a	DET
iajs-850	96	13	signal	signal	NOUN
iajs-850	96	14	at	at	ADP
iajs-850	96	15	δ(11.4	δ(11.4	NOUN
iajs-850	96	16	)	)	PUNCT
iajs-850	96	17	ppm	ppm	NOUN
iajs-850	96	18	for	for	ADP
iajs-850	96	19	(	(	PUNCT
iajs-850	96	20	cho	cho	NOUN
iajs-850	96	21	)	)	PUNCT
iajs-850	96	22	by	by	ADP
iajs-850	96	23	1hnmr	1hnmr	NUM
iajs-850	96	24	and	and	CCONJ
iajs-850	96	25	was	be	AUX
iajs-850	96	26	characterised	characterise	VERB
iajs-850	96	27	by	by	ADP
iajs-850	96	28	13cnm	13cnm	NOUN
iajs-850	96	29	r	r	NOUN
iajs-850	96	30	and	and	CCONJ
iajs-850	96	31	(	(	PUNCT
iajs-850	96	32	u.v	u.v	PROPN
iajs-850	96	33	-	-	PUNCT
iajs-850	96	34	vis	vis	X
iajs-850	96	35	)	)	PUNCT
iajs-850	96	36	spectrum	spectrum	NOUN
iajs-850	96	37	which	which	PRON
iajs-850	96	38	showed	show	VERB
iajs-850	96	39	one	one	NUM
iajs-850	96	40	peak	peak	NOUN
iajs-850	96	41	at	at	ADP
iajs-850	96	42	(	(	PUNCT
iajs-850	96	43	297	297	NUM
iajs-850	96	44	)	)	PUNCT
iajs-850	96	45	nm	nm	NOUN
iajs-850	96	46	(	(	PUNCT
iajs-850	96	47	33670	33670	NUM
iajs-850	96	48	cm-1	cm-1	NOUN
iajs-850	96	49	)	)	PUNCT
iajs-850	96	50	(	(	PUNCT
iajs-850	96	51	εmax	εmax	NOUN
iajs-850	96	52	=	=	SYM
iajs-850	96	53	102	102	NUM
iajs-850	96	54	molar-1cm-1	molar-1cm-1	NOUN
iajs-850	96	55	)	)	PUNCT
iajs-850	96	56	assigned	assign	VERB
iajs-850	96	57	to	to	ADP
iajs-850	96	58	(	(	PUNCT
iajs-850	96	59	n	n	X
iajs-850	96	60	π	π	NOUN
iajs-850	96	61	*	*	NOUN
iajs-850	96	62	)	)	PUNCT
iajs-850	96	63	transition	transition	NOUN
iajs-850	96	64	.	.	PUNCT
iajs-850	97	1	in	in	ADP
iajs-850	97	2	order	order	NOUN
iajs-850	97	3	to	to	PART
iajs-850	97	4	obtain	obtain	VERB
iajs-850	97	5	our	our	PRON
iajs-850	97	6	target	target	NOUN
iajs-850	97	7	compounds	compound	NOUN
iajs-850	97	8	(	(	PUNCT
iajs-850	97	9	9	9	NUM
iajs-850	97	10	)	)	PUNCT
iajs-850	97	11	,	,	PUNCT
iajs-850	97	12	(	(	PUNCT
iajs-850	97	13	10	10	NUM
iajs-850	97	14	)	)	PUNCT
iajs-850	97	15	and	and	CCONJ
iajs-850	97	16	(	(	PUNCT
iajs-850	97	17	11	11	NUM
iajs-850	97	18	)	)	PUNCT
iajs-850	97	19	,	,	PUNCT
iajs-850	97	20	the	the	DET
iajs-850	97	21	cyclocondensation	cyclocondensation	NOUN
iajs-850	97	22	reaction	reaction	NOUN
iajs-850	97	23	of	of	ADP
iajs-850	97	24	malonate	malonate	NOUN
iajs-850	97	25	(	(	PUNCT
iajs-850	97	26	8)	8)	NUM
iajs-850	97	27	with	with	ADP
iajs-850	97	28	urea	urea	NOUN
iajs-850	97	29	,	,	PUNCT
iajs-850	97	30	thiourea	thiourea	NOUN
iajs-850	97	31	and	and	CCONJ
iajs-850	97	32	guanidine	guanidine	ADJ
iajs-850	97	33	hydrochloride	hydrochloride	NOUN
iajs-850	97	34	in	in	ADP
iajs-850	97	35	alkaline	alkaline	NOUN
iajs-850	97	36	media	medium	NOUN
iajs-850	97	37	(	(	PUNCT
iajs-850	97	38	sodium	sodium	NOUN
iajs-850	97	39	methoxide	methoxide	NOUN
iajs-850	97	40	)	)	PUNCT
iajs-850	97	41	leads	lead	VERB
iajs-850	97	42	to	to	ADP
iajs-850	97	43	these	these	DET
iajs-850	97	44	compounds	compound	NOUN
iajs-850	97	45	.	.	PUNCT
iajs-850	98	1	all	all	DET
iajs-850	98	2	ftir	ftir	PROPN
iajs-850	98	3	spectra	spectra	PROPN
iajs-850	98	4	for	for	ADP
iajs-850	98	5	these	these	DET
iajs-850	98	6	compounds	compound	NOUN
iajs-850	98	7	exhibited	exhibit	VERB
iajs-850	98	8	disappearance	disappearance	NOUN
iajs-850	98	9	of	of	ADP
iajs-850	98	10	the	the	DET
iajs-850	98	11	band	band	NOUN
iajs-850	98	12	at	at	ADP
iajs-850	98	13	(	(	PUNCT
iajs-850	98	14	1720	1720	NUM
iajs-850	98	15	)	)	PUNCT
iajs-850	98	16	cm	cm	NOUN
iajs-850	98	17	-1	-1	NOUN
iajs-850	98	18	for	for	ADP
iajs-850	98	19	(	(	PUNCT
iajs-850	98	20	c	c	NOUN
iajs-850	98	21	=	=	NOUN
iajs-850	98	22	o	o	NOUN
iajs-850	98	23	)	)	PUNCT
iajs-850	98	24	of	of	ADP
iajs-850	98	25	the	the	DET
iajs-850	98	26	ester	ester	NOUN
iajs-850	98	27	for	for	ADP
iajs-850	98	28	compound	compound	NOUN
iajs-850	98	29	(	(	PUNCT
iajs-850	98	30	8)	8)	NUM
iajs-850	98	31	and	and	CCONJ
iajs-850	98	32	displayed	display	VERB
iajs-850	98	33	of	of	ADP
iajs-850	98	34	the	the	DET
iajs-850	98	35	bands	band	NOUN
iajs-850	98	36	at	at	ADP
iajs-850	98	37	(	(	PUNCT
iajs-850	98	38	1662	1662	NUM
iajs-850	98	39	,	,	PUNCT
iajs-850	98	40	1597	1597	NUM
iajs-850	98	41	,	,	PUNCT
iajs-850	98	42	1643	1643	NUM
iajs-850	98	43	)	)	PUNCT
iajs-850	98	44	cm-1	cm-1	VERB
iajs-850	99	1	due	due	ADP
iajs-850	99	2	to	to	ADP
iajs-850	99	3	(	(	PUNCT
iajs-850	99	4	c	c	NOUN
iajs-850	99	5	=	=	X
iajs-850	99	6	o	o	X
iajs-850	99	7	in	in	ADP
iajs-850	99	8	chconh	chconh	PROPN
iajs-850	99	9	)	)	PUNCT
iajs-850	99	10	for	for	ADP
iajs-850	99	11	compounds	compound	NOUN
iajs-850	99	12	(	(	PUNCT
iajs-850	99	13	9	9	NUM
iajs-850	99	14	)	)	PUNCT
iajs-850	99	15	,	,	PUNCT
iajs-850	99	16	(	(	PUNCT
iajs-850	99	17	10	10	NUM
iajs-850	99	18	)	)	PUNCT
iajs-850	99	19	and	and	CCONJ
iajs-850	99	20	(	(	PUNCT
iajs-850	99	21	11	11	NUM
iajs-850	99	22	)	)	PUNCT
iajs-850	99	23	respectively	respectively	ADV
iajs-850	99	24	.	.	PUNCT
iajs-850	100	1	the	the	DET
iajs-850	100	2	ftir	ftir	PROPN
iajs-850	100	3	spectra	spectra	PROPN
iajs-850	100	4	of	of	ADP
iajs-850	100	5	(	(	PUNCT
iajs-850	100	6	9	9	NUM
iajs-850	100	7	)	)	PUNCT
iajs-850	100	8	,	,	PUNCT
iajs-850	100	9	(	(	PUNCT
iajs-850	100	10	10	10	NUM
iajs-850	100	11	)	)	PUNCT
iajs-850	100	12	and	and	CCONJ
iajs-850	100	13	(	(	PUNCT
iajs-850	100	14	11	11	NUM
iajs-850	100	15	)	)	PUNCT
iajs-850	100	16	showed	show	VERB
iajs-850	100	17	the	the	DET
iajs-850	100	18	bands	band	NOUN
iajs-850	100	19	at	at	ADP
iajs-850	100	20	(	(	PUNCT
iajs-850	100	21	1627	1627	NUM
iajs-850	100	22	)	)	PUNCT
iajs-850	100	23	cm	cm	NOUN
iajs-850	100	24	-1	-1	NOUN
iajs-850	100	25	,	,	PUNCT
iajs-850	100	26	(	(	PUNCT
iajs-850	100	27	1153	1153	NUM
iajs-850	100	28	)	)	PUNCT
iajs-850	100	29	cm-1	cm-1	VERB
iajs-850	100	30	and	and	CCONJ
iajs-850	100	31	(	(	PUNCT
iajs-850	100	32	1597	1597	NUM
iajs-850	100	33	)	)	PUNCT
iajs-850	100	34	cm-1	cm-1	VERB
iajs-850	101	1	due	due	ADP
iajs-850	101	2	to	to	ADP
iajs-850	101	3	(	(	PUNCT
iajs-850	101	4	c	c	NOUN
iajs-850	101	5	=	=	X
iajs-850	101	6	o	o	X
iajs-850	101	7	in	in	ADP
iajs-850	101	8	hnconh	hnconh	NOUN
iajs-850	101	9	)	)	PUNCT
iajs-850	101	10	,	,	PUNCT
iajs-850	101	11	(	(	PUNCT
iajs-850	101	12	c	c	X
iajs-850	101	13	=	=	SYM
iajs-850	101	14	s	s	PART
iajs-850	101	15	)	)	PUNCT
iajs-850	101	16	and	and	CCONJ
iajs-850	101	17	(	(	PUNCT
iajs-850	101	18	c	c	NOUN
iajs-850	101	19	=	=	SYM
iajs-850	101	20	n	n	CCONJ
iajs-850	101	21	)	)	PUNCT
iajs-850	101	22	respectively	respectively	ADV
iajs-850	101	23	.	.	PUNCT
iajs-850	102	1	the	the	DET
iajs-850	102	2	structures	structure	NOUN
iajs-850	102	3	of	of	ADP
iajs-850	102	4	these	these	DET
iajs-850	102	5	compounds	compound	NOUN
iajs-850	102	6	were	be	AUX
iajs-850	102	7	confirmed	confirm	VERB
iajs-850	102	8	by	by	ADP
iajs-850	102	9	1hnmr	1hnmr	NUM
iajs-850	102	10	and	and	CCONJ
iajs-850	102	11	13cnm	13cnm	NOUN
iajs-850	102	12	r	r	NOUN
iajs-850	102	13	,	,	PUNCT
iajs-850	102	14	which	which	PRON
iajs-850	102	15	showed	show	VERB
iajs-850	102	16	disappearance	disappearance	NOUN
iajs-850	102	17	of	of	ADP
iajs-850	102	18	the	the	DET
iajs-850	102	19	signals	signal	NOUN
iajs-850	102	20	at	at	ADP
iajs-850	102	21	δ(3.56	δ(3.56	PROPN
iajs-850	102	22	-	-	PUNCT
iajs-850	102	23	3.58)ppm	3.58)ppm	NUM
iajs-850	102	24	and	and	CCONJ
iajs-850	102	25	δ(40.78	δ(40.78	PROPN
iajs-850	102	26	-	-	PUNCT
iajs-850	102	27	39.11	39.11	NUM
iajs-850	102	28	)	)	PUNCT
iajs-850	102	29	ppm	ppm	NOUN
iajs-850	102	30	from	from	ADP
iajs-850	102	31	1hnmr	1hnmr	NUM
iajs-850	102	32	and	and	CCONJ
iajs-850	102	33	13cnm	13cnm	NOUN
iajs-850	102	34	r	r	NOUN
iajs-850	102	35	spectra	spectra	NOUN
iajs-850	102	36	for	for	ADP
iajs-850	102	37	compound	compound	NOUN
iajs-850	102	38	(	(	PUNCT
iajs-850	102	39	8)	8)	NUM
iajs-850	102	40	.	.	PUNCT
iajs-850	103	1	the	the	DET
iajs-850	103	2	(	(	PUNCT
iajs-850	103	3	u.v	u.v	PROPN
iajs-850	103	4	-	-	PUNCT
iajs-850	103	5	vis	vis	X
iajs-850	103	6	)	)	PUNCT
iajs-850	103	7	spectra	spectra	ADJ
iajs-850	103	8	data	datum	NOUN
iajs-850	103	9	are	be	AUX
iajs-850	103	10	given	give	VERB
iajs-850	103	11	in	in	ADP
iajs-850	103	12	table	table	NOUN
iajs-850	103	13	(	(	PUNCT
iajs-850	103	14	5	5	NUM
iajs-850	103	15	)	)	PUNCT
iajs-850	103	16	.	.	PUNCT
iajs-850	104	1	o	o	X
iajs-850	104	2	o	o	INTJ
iajs-850	104	3	ohho	ohho	ADJ
iajs-850	104	4	ho	ho	PROPN
iajs-850	104	5	ho	ho	PROPN
iajs-850	104	6	(	(	PUNCT
iajs-850	104	7	3	3	NUM
iajs-850	104	8	)	)	PUNCT
iajs-850	105	1	o	o	NOUN
iajs-850	106	1	o	o	X
iajs-850	107	1	o	o	X
iajs-850	107	2	oh3c	oh3c	X
iajs-850	107	3	h3c	h3c	VERB
iajs-850	107	4	ho	ho	PROPN
iajs-850	108	1	oh	oh	INTJ
iajs-850	108	2	(	(	PUNCT
iajs-850	108	3	4	4	NUM
iajs-850	108	4	)	)	PUNCT
iajs-850	108	5	o	o	NOUN
iajs-850	109	1	o	o	NOUN
iajs-850	109	2	o	o	INTJ
iajs-850	110	1	oh3	oh3	INTJ
iajs-850	110	2	c	c	NOUN
iajs-850	110	3	h3c	h3c	X
iajs-850	110	4	(	(	PUNCT
iajs-850	110	5	5	5	NUM
iajs-850	110	6	)	)	PUNCT
iajs-850	110	7	obzbzo	obzbzo	NOUN
iajs-850	111	1	o	o	NOUN
iajs-850	111	2	o	o	X
iajs-850	111	3	ho	ho	PROPN
iajs-850	111	4	ho	ho	PROPN
iajs-850	111	5	(	(	PUNCT
iajs-850	111	6	6	6	NUM
iajs-850	111	7	)	)	PUNCT
iajs-850	111	8	obzbzo	obzbzo	NOUN
iajs-850	111	9	o	o	INTJ
iajs-850	112	1	o	o	X
iajs-850	112	2	obz	obz	ADJ
iajs-850	112	3	bzo	bzo	NOUN
iajs-850	113	1	c	c	PROPN
iajs-850	113	2	h	h	NOUN
iajs-850	114	1	o	o	NOUN
iajs-850	114	2	(	(	PUNCT
iajs-850	114	3	7	7	NUM
iajs-850	114	4	)	)	PUNCT
iajs-850	114	5	o	o	NOUN
iajs-850	115	1	o	o	INTJ
iajs-850	115	2	obzbzo	obzbzo	ADJ
iajs-850	115	3	ho	ho	PROPN
iajs-850	115	4	hc	hc	PROPN
iajs-850	115	5	co2ch3	co2ch3	ADJ
iajs-850	115	6	co2	co2	NOUN
iajs-850	115	7	ch3	ch3	PROPN
iajs-850	115	8	(	(	PUNCT
iajs-850	115	9	8)	8)	NUM
iajs-850	115	10	nhhn	nhhn	NOUN
iajs-850	116	1	oo	oo	INTJ
iajs-850	116	2	x	x	X
iajs-850	116	3	o	o	NOUN
iajs-850	116	4	o	o	X
iajs-850	116	5	obzbzo	obzbzo	ADJ
iajs-850	116	6	ho	ho	PROPN
iajs-850	116	7	acetone	acetone	NOUN
iajs-850	116	8	hcl(g	hcl(g	PROPN
iajs-850	116	9	)	)	PUNCT
iajs-850	117	1	bzcl	bzcl	PROPN
iajs-850	117	2	py	py	PROPN
iajs-850	117	3	.	.	PROPN
iajs-850	117	4	acoh	acoh	PROPN
iajs-850	117	5	65	65	NUM
iajs-850	117	6	%	%	NOUN
iajs-850	117	7	naio4ch2(co2ch3)2	naio4ch2(co2ch3)2	PROPN
iajs-850	117	8	koh	koh	PROPN
iajs-850	117	9	urea	urea	NOUN
iajs-850	117	10	or	or	CCONJ
iajs-850	117	11	thiourea	thiourea	NOUN
iajs-850	117	12	or	or	CCONJ
iajs-850	117	13	guanidine	guanidine	VERB
iajs-850	117	14	hydrochloride	hydrochloride	NOUN
iajs-850	117	15	ch3ona	ch3ona	PROPN
iajs-850	117	16	(	(	PUNCT
iajs-850	117	17	9	9	NUM
iajs-850	117	18	)	)	PUNCT
iajs-850	117	19	,	,	PUNCT
iajs-850	117	20	x	x	PUNCT
iajs-850	118	1	=	=	PUNCT
iajs-850	118	2	o	o	X
iajs-850	118	3	(	(	PUNCT
iajs-850	118	4	10	10	NUM
iajs-850	118	5	)	)	PUNCT
iajs-850	118	6	,	,	PUNCT
iajs-850	118	7	x	x	X
iajs-850	119	1	=	=	SYM
iajs-850	119	2	s	s	X
iajs-850	119	3	(	(	PUNCT
iajs-850	119	4	11	11	NUM
iajs-850	119	5	)	)	PUNCT
iajs-850	119	6	,	,	PUNCT
iajs-850	119	7	x	x	X
iajs-850	119	8	=	=	SYM
iajs-850	119	9	nh	nh	PROPN
iajs-850	119	10	1	1	NUM
iajs-850	119	11	23	23	NUM
iajs-850	119	12	4	4	NUM
iajs-850	119	13	5	5	NUM
iajs-850	119	14	6	6	NUM
iajs-850	119	15	scheme	scheme	NOUN
iajs-850	119	16	(	(	PUNCT
iajs-850	119	17	1	1	NUM
iajs-850	119	18	)	)	PUNCT
iajs-850	119	19	the	the	DET
iajs-850	119	20	scheme	scheme	NOUN
iajs-850	119	21	of	of	ADP
iajs-850	119	22	prepared	prepare	VERB
iajs-850	119	23	compounds	compound	NOUN
iajs-850	119	24	ibn	ibn	PROPN
iajs-850	119	25	alhaitham	alhaitham	NOUN
iajs-850	119	26	j.	j.	PROPN
iajs-850	120	1	fo	fo	ADP
iajs-850	120	2	r	r	NOUN
iajs-850	120	3	pure	pure	ADJ
iajs-850	120	4	&	&	CCONJ
iajs-850	120	5	appl	appl	PROPN
iajs-850	120	6	.	.	PUNCT
iajs-850	121	1	sci	sci	PROPN
iajs-850	121	2	.	.	PROPN
iajs-850	122	1	vo	vo	INTJ
iajs-850	122	2	l.24	l.24	PROPN
iajs-850	122	3	(	(	PUNCT
iajs-850	122	4	1	1	NUM
iajs-850	122	5	)	)	PUNCT
iajs-850	122	6	2011	2011	NUM
iajs-850	122	7	references	reference	NOUN
iajs-850	122	8	1	1	NUM
iajs-850	122	9	.	.	PUNCT
iajs-850	122	10	cole	cole	PROPN
iajs-850	122	11	,	,	PUNCT
iajs-850	122	12	m.	m.	PROPN
iajs-850	122	13	d.	d.	PROPN
iajs-850	122	14	(	(	PUNCT
iajs-850	122	15	2003	2003	NUM
iajs-850	122	16	)	)	PUNCT
iajs-850	122	17	“	"	PUNCT
iajs-850	122	18	the	the	DET
iajs-850	122	19	analysis	analysis	NOUN
iajs-850	122	20	of	of	ADP
iajs-850	122	21	controlled	control	VERB
iajs-850	122	22	substances	substance	NOUN
iajs-850	122	23	”	"	PUNCT
iajs-850	122	24	,	,	PUNCT
iajs-850	122	25	john	john	PROPN
iajs-850	122	26	wiley	wiley	PROPN
iajs-850	122	27	and	and	CCONJ
iajs-850	122	28	sons	son	NOUN
iajs-850	122	29	,	,	PUNCT
iajs-850	122	30	ltd	ltd	PROPN
iajs-850	122	31	.	.	PROPN
iajs-850	122	32	chapter	chapter	NOUN
iajs-850	122	33	9	9	NUM
iajs-850	122	34	:	:	SYM
iajs-850	122	35	139,140	139,140	NUM
iajs-850	122	36	.	.	NOUN
iajs-850	123	1	2	2	X
iajs-850	123	2	.	.	X
iajs-850	123	3	al	al	PROPN
iajs-850	123	4	-	-	PUNCT
iajs-850	123	5	qase	qase	PROPN
iajs-850	123	6	,	,	PUNCT
iajs-850	123	7	a.	a.	PROPN
iajs-850	123	8	h.	h.	PROPN
iajs-850	123	9	j.(2000	j.(2000	PROPN
iajs-850	123	10	)	)	PUNCT
iajs-850	123	11	m	m	PROPN
iajs-850	123	12	.	.	PUNCT
iajs-850	124	1	sc	sc	PROPN
iajs-850	124	2	.	.	PUNCT
iajs-850	125	1	thesis	thesis	PROPN
iajs-850	125	2	,	,	PUNCT
iajs-850	125	3	college	college	NOUN
iajs-850	125	4	of	of	ADP
iajs-850	125	5	education	education	PROPN
iajs-850	125	6	/	/	SYM
iajs-850	125	7	ibn	ibn	PROPN
iajs-850	125	8	-	-	PUNCT
iajs-850	125	9	al	al	PROPN
iajs-850	125	10	-	-	PUNCT
iajs-850	125	11	haitham	haitham	PROPN
iajs-850	125	12	,	,	PUNCT
iajs-850	125	13	university	university	NOUN
iajs-850	125	14	of	of	ADP
iajs-850	125	15	baghdad	baghdad	PROPN
iajs-850	125	16	3	3	NUM
iajs-850	125	17	.	.	PUNCT
iajs-850	126	1	fayad	fayad	PROPN
iajs-850	126	2	,	,	PUNCT
iajs-850	126	3	a.	a.	NOUN
iajs-850	126	4	a.	a.	NOUN
iajs-850	126	5	(	(	PUNCT
iajs-850	126	6	2008)ph	2008)ph	PROPN
iajs-850	126	7	.	.	PROPN
iajs-850	126	8	d.	d.	PROPN
iajs-850	126	9	thesis	thesis	PROPN
iajs-850	126	10	,	,	PUNCT
iajs-850	126	11	college	college	NOUN
iajs-850	126	12	of	of	ADP
iajs-850	126	13	education	education	PROPN
iajs-850	126	14	/	/	SYM
iajs-850	126	15	ibn	ibn	PROPN
iajs-850	126	16	-	-	PUNCT
iajs-850	126	17	al	al	PROPN
iajs-850	126	18	-	-	PUNCT
iajs-850	126	19	haitham	haitham	PROPN
iajs-850	126	20	,	,	PUNCT
iajs-850	126	21	university	university	NOUN
iajs-850	126	22	of	of	ADP
iajs-850	126	23	baghdad	baghdad	PROPN
iajs-850	126	24	4	4	NUM
iajs-850	126	25	.	.	PUNCT
iajs-850	127	1	khalafi	khalafi	NOUN
iajs-850	127	2	-	-	PUNCT
iajs-850	127	3	nezhad	nezhad	VERB
iajs-850	127	4	,	,	PUNCT
iajs-850	127	5	a.	a.	NOUN
iajs-850	127	6	and	and	CCONJ
iajs-850	127	7	hashemi	hashemi	PROPN
iajs-850	127	8	,	,	PUNCT
iajs-850	127	9	a.	a.	NOUN
iajs-850	127	10	(	(	PUNCT
iajs-850	127	11	2001	2001	NUM
iajs-850	127	12	)	)	PUNCT
iajs-850	127	13	“	"	PUNCT
iajs-850	127	14	microwave	microwave	NOUN
iajs-850	127	15	enhanced	enhance	VERB
iajs-850	127	16	knoevenagel	knoevenagel	NOUN
iajs-850	127	17	condensation	condensation	NOUN
iajs-850	127	18	of	of	ADP
iajs-850	127	19	barbituric	barbituric	NOUN
iajs-850	127	20	acid	acid	NOUN
iajs-850	127	21	with	with	ADP
iajs-850	127	22	aromatic	aromatic	ADJ
iajs-850	127	23	aldehydes	aldehyde	NOUN
iajs-850	127	24	on	on	ADP
iajs-850	127	25	basic	basic	ADJ
iajs-850	127	26	alumina	alumina	NOUN
iajs-850	127	27	”	"	PUNCT
iajs-850	127	28	,	,	PUNCT
iajs-850	127	29	iran	iran	PROPN
iajs-850	127	30	.	.	PUNCT
iajs-850	128	1	j.	j.	PROPN
iajs-850	128	2	chem	chem	PROPN
iajs-850	128	3	.	.	PUNCT
iajs-850	128	4	&	&	CCONJ
iajs-850	128	5	chem	chem	PROPN
iajs-850	128	6	.	.	PUNCT
iajs-850	129	1	eng	eng	PROPN
iajs-850	129	2	.	.	PROPN
iajs-850	129	3	20	20	NUM
iajs-850	129	4	(	(	PUNCT
iajs-850	129	5	1):9	1):9	NUM
iajs-850	129	6	-	-	SYM
iajs-850	129	7	11	11	NUM
iajs-850	129	8	.	.	PUNCT
iajs-850	130	1	5	5	NUM
iajs-850	130	2	.	.	X
iajs-850	130	3	kidwai	kidwai	PROPN
iajs-850	130	4	,	,	PUNCT
iajs-850	130	5	m.	m.	NOUN
iajs-850	130	6	;	;	PUNCT
iajs-850	130	7	thakur	thakur	PROPN
iajs-850	130	8	,	,	PUNCT
iajs-850	130	9	r.	r.	PROPN
iajs-850	130	10	and	and	CCONJ
iajs-850	130	11	mohan	mohan	PROPN
iajs-850	130	12	,	,	PUNCT
iajs-850	130	13	r.	r.	PROPN
iajs-850	130	14	(	(	PUNCT
iajs-850	130	15	2005	2005	NUM
iajs-850	130	16	)	)	PUNCT
iajs-850	130	17	“	"	PUNCT
iajs-850	130	18	ecofriendly	ecofriendly	ADV
iajs-850	130	19	synthesis	synthesis	NOUN
iajs-850	130	20	of	of	ADP
iajs-850	130	21	novel	novel	ADJ
iajs-850	130	22	antifungal	antifungal	NOUN
iajs-850	130	23	(	(	PUNCT
iajs-850	130	24	thio	thio	NOUN
iajs-850	130	25	)	)	PUNCT
iajs-850	130	26	barbituric	barbituric	NOUN
iajs-850	130	27	acid	acid	NOUN
iajs-850	130	28	derivatives	derivative	NOUN
iajs-850	130	29	”	"	PUNCT
iajs-850	130	30	acta	acta	PROPN
iajs-850	130	31	chim	chim	PROPN
iajs-850	130	32	.	.	PUNCT
iajs-850	131	1	slov	slov	PROPN
iajs-850	131	2	.	.	PROPN
iajs-850	131	3	,	,	PUNCT
iajs-850	131	4	52	52	NUM
iajs-850	131	5	:	:	SYM
iajs-850	131	6	88	88	NUM
iajs-850	131	7	-	-	SYM
iajs-850	131	8	92	92	NUM
iajs-850	131	9	.	.	PUNCT
iajs-850	132	1	6	6	NUM
iajs-850	132	2	.	.	X
iajs-850	132	3	carey	carey	PROPN
iajs-850	132	4	,	,	PUNCT
iajs-850	132	5	f.	f.	PROPN
iajs-850	132	6	a.	a.	PROPN
iajs-850	132	7	(	(	PUNCT
iajs-850	132	8	2006	2006	NUM
iajs-850	132	9	)	)	PUNCT
iajs-850	132	10	“	"	PUNCT
iajs-850	132	11	organic	organic	ADJ
iajs-850	132	12	chemistry	chemistry	NOUN
iajs-850	132	13	”	"	PUNCT
iajs-850	132	14	,	,	PUNCT
iajs-850	132	15	6th	6th	ADJ
iajs-850	132	16	ed	ed	NOUN
iajs-850	132	17	.	.	PROPN
iajs-850	132	18	,	,	PUNCT
iajs-850	132	19	the	the	DET
iajs-850	132	20	mcgraw	mcgraw	PROPN
iajs-850	132	21	-	-	PUNCT
iajs-850	132	22	hill	hill	NOUN
iajs-850	132	23	companies	company	NOUN
iajs-850	132	24	,	,	PUNCT
iajs-850	132	25	inc	inc	PROPN
iajs-850	132	26	.	.	PROPN
iajs-850	132	27	,	,	PUNCT
iajs-850	132	28	new	new	PROPN
iajs-850	132	29	york	york	PROPN
iajs-850	132	30	,	,	PUNCT
iajs-850	132	31	pp	pp	X
iajs-850	132	32	.	.	PUNCT
iajs-850	133	1	767	767	NUM
iajs-850	133	2	.	.	X
iajs-850	134	1	7	7	X
iajs-850	134	2	.	.	X
iajs-850	134	3	beifuss	beifuss	ADJ
iajs-850	134	4	,	,	PUNCT
iajs-850	134	5	u.	u.	PROPN
iajs-850	134	6	;	;	PUNCT
iajs-850	134	7	kunz	kunz	PROPN
iajs-850	134	8	,	,	PUNCT
iajs-850	134	9	o.	o.	NOUN
iajs-850	134	10	and	and	CCONJ
iajs-850	134	11	aguado	aguado	NOUN
iajs-850	134	12	,	,	PUNCT
iajs-850	134	13	g.	g.	PROPN
iajs-850	134	14	p.	p.	PROPN
iajs-850	134	15	(	(	PUNCT
iajs-850	134	16	1999	1999	NUM
iajs-850	134	17	)	)	PUNCT
iajs-850	134	18	synlett	synlett	NOUN
iajs-850	134	19	,	,	PUNCT
iajs-850	134	20	147	147	NUM
iajs-850	134	21	-	-	SYM
iajs-850	134	22	149	149	NUM
iajs-850	134	23	.	.	NOUN
iajs-850	134	24	8	8	NUM
iajs-850	134	25	.	.	X
iajs-850	134	26	beifuss	beifuss	VERB
iajs-850	134	27	,	,	PUNCT
iajs-850	134	28	u.	u.	PROPN
iajs-850	134	29	;	;	PUNCT
iajs-850	134	30	kunz	kunz	PROPN
iajs-850	134	31	,	,	PUNCT
iajs-850	134	32	o.	o.	PROPN
iajs-850	134	33	and	and	CCONJ
iajs-850	134	34	voss	voss	PROPN
iajs-850	134	35	,	,	PUNCT
iajs-850	134	36	g.	g.	PROPN
iajs-850	134	37	(	(	PUNCT
iajs-850	134	38	2000	2000	NUM
iajs-850	134	39	)	)	PUNCT
iajs-850	134	40	“	"	PUNCT
iajs-850	134	41	regioselective	regioselective	ADJ
iajs-850	134	42	synthesis	synthesis	NOUN
iajs-850	134	43	of	of	ADP
iajs-850	134	44	3	3	NUM
iajs-850	134	45	-	-	PUNCT
iajs-850	134	46	o	o	NOUN
iajs-850	134	47	-	-	ADJ
iajs-850	134	48	alkyl	alkyl	ADJ
iajs-850	134	49	ethers	ether	NOUN
iajs-850	134	50	of	of	ADP
iajs-850	134	51	ascorbic	ascorbic	NOUN
iajs-850	134	52	acid	acid	NOUN
iajs-850	134	53	without	without	ADP
iajs-850	134	54	protecting	protect	VERB
iajs-850	134	55	groups	group	NOUN
iajs-850	134	56	in	in	ADP
iajs-850	134	57	a	a	DET
iajs-850	134	58	single	single	ADJ
iajs-850	134	59	step	step	NOUN
iajs-850	134	60	”	"	PUNCT
iajs-850	134	61	,	,	PUNCT
iajs-850	134	62	tetrahedron	tetrahedron	NOUN
iajs-850	134	63	,	,	PUNCT
iajs-850	134	64	,	,	PUNCT
iajs-850	134	65	56:357	56:357	NUM
iajs-850	134	66	363	363	NUM
iajs-850	134	67	.	.	PUNCT
iajs-850	135	1	9	9	NUM
iajs-850	135	2	.	.	X
iajs-850	135	3	salomon	salomon	PROPN
iajs-850	135	4	,	,	PUNCT
iajs-850	135	5	l.	l.	PROPN
iajs-850	135	6	l.	l.	PROPN
iajs-850	135	7	(	(	PUNCT
iajs-850	135	8	1963	1963	NUM
iajs-850	135	9	)	)	PUNCT
iajs-850	135	10	experientia	experientia	NOUN
iajs-850	135	11	,	,	PUNCT
iajs-850	135	12	,	,	PUNCT
iajs-850	135	13	19	19	NUM
iajs-850	135	14	(	(	PUNCT
iajs-850	135	15	12	12	NUM
iajs-850	135	16	):	):	PUNCT
iajs-850	135	17	619	619	NUM
iajs-850	135	18	.	.	PUNCT
iajs-850	136	1	10	10	NUM
iajs-850	136	2	.	.	PUNCT
iajs-850	137	1	gazivoda	gazivoda	NOUN
iajs-850	137	2	,	,	PUNCT
iajs-850	137	3	t.	t.	PROPN
iajs-850	137	4	;	;	PUNCT
iajs-850	137	5	wittine	wittine	NOUN
iajs-850	137	6	,	,	PUNCT
iajs-850	137	7	k.	k.	PROPN
iajs-850	137	8	;	;	PUNCT
iajs-850	137	9	lovric	lovric	PROPN
iajs-850	137	10	,	,	PUNCT
iajs-850	137	11	i.	i.	NOUN
iajs-850	137	12	;	;	PUNCT
iajs-850	137	13	makuc	makuc	PROPN
iajs-850	137	14	,	,	PUNCT
iajs-850	137	15	d.	d.	PROPN
iajs-850	137	16	;	;	PUNCT
iajs-850	137	17	plavec	plavec	PROPN
iajs-850	137	18	,	,	PUNCT
iajs-850	137	19	j.	j.	PROPN
iajs-850	137	20	;	;	PUNCT
iajs-850	137	21	cetina	cetina	PROPN
iajs-850	137	22	,	,	PUNCT
iajs-850	137	23	m.	m.	NOUN
iajs-850	137	24	;	;	PUNCT
iajs-850	137	25	mrvos	mrvos	NOUN
iajs-850	137	26	-	-	PUNCT
iajs-850	137	27	sermek	sermek	PROPN
iajs-850	137	28	,	,	PUNCT
iajs-850	137	29	d.	d.	PROPN
iajs-850	137	30	;	;	PUNCT
iajs-850	137	31	suman	suman	PROPN
iajs-850	137	32	,	,	PUNCT
iajs-850	137	33	l.	l.	PROPN
iajs-850	137	34	;	;	PUNCT
iajs-850	137	35	kralj	kralj	PROPN
iajs-850	137	36	,	,	PUNCT
iajs-850	137	37	m.	m.	NOUN
iajs-850	137	38	;	;	PUNCT
iajs-850	137	39	pavelic	pavelic	PROPN
iajs-850	137	40	,	,	PUNCT
iajs-850	137	41	k.	k.	PROPN
iajs-850	137	42	;	;	PUNCT
iajs-850	137	43	mintas	minta	NOUN
iajs-850	137	44	,	,	PUNCT
iajs-850	137	45	m	m	PROPN
iajs-850	137	46	.	.	PUNCT
iajs-850	138	1	and	and	CCONJ
iajs-850	138	2	raic	raic	NOUN
iajs-850	138	3	-	-	PUNCT
iajs-850	138	4	malic	malic	ADJ
iajs-850	138	5	s.	s.	PROPN
iajs-850	138	6	(	(	PUNCT
iajs-850	138	7	2006)“synthesis	2006)“synthesis	NUM
iajs-850	138	8	,	,	PUNCT
iajs-850	138	9	structural	structural	ADJ
iajs-850	138	10	studies	study	NOUN
iajs-850	138	11	,	,	PUNCT
iajs-850	138	12	and	and	CCONJ
iajs-850	138	13	cytostatic	cytostatic	ADJ
iajs-850	138	14	evaluation	evaluation	NOUN
iajs-850	138	15	of	of	ADP
iajs-850	138	16	5,6	5,6	NUM
iajs-850	138	17	-	-	PUNCT
iajs-850	138	18	di	di	AUX
iajs-850	138	19	-	-	PUNCT
iajs-850	138	20	o	o	NOUN
iajs-850	138	21	-	-	PUNCT
iajs-850	138	22	modified	modify	VERB
iajs-850	138	23	l	l	ADJ
iajs-850	138	24	-	-	ADJ
iajs-850	138	25	ascorbic	ascorbic	ADJ
iajs-850	138	26	acid	acid	NOUN
iajs-850	138	27	derivatives	derivative	NOUN
iajs-850	138	28	”	"	PUNCT
iajs-850	138	29	,	,	PUNCT
iajs-850	138	30	carbohydr	carbohydr	NOUN
iajs-850	138	31	.	.	PUNCT
iajs-850	139	1	res	re	NOUN
iajs-850	139	2	.	.	PROPN
iajs-850	139	3	,	,	PUNCT
iajs-850	139	4	,	,	PUNCT
iajs-850	139	5	341	341	NUM
iajs-850	139	6	(	(	PUNCT
iajs-850	139	7	4):433	4):433	NUM
iajs-850	139	8	-	-	PUNCT
iajs-850	139	9	442	442	NUM
iajs-850	139	10	.	.	PUNCT
iajs-850	140	1	11	11	NUM
iajs-850	140	2	.	.	PUNCT
iajs-850	141	1	vogel	vogel	PROPN
iajs-850	141	2	,	,	PUNCT
iajs-850	141	3	a.	a.	NOUN
iajs-850	141	4	i.	i.	PROPN
iajs-850	141	5	(	(	PUNCT
iajs-850	141	6	1989	1989	NUM
iajs-850	141	7	)	)	PUNCT
iajs-850	141	8	“	"	PUNCT
iajs-850	141	9	vogel	vogel	NOUN
iajs-850	141	10	's	's	PART
iajs-850	141	11	textbook	textbook	NOUN
iajs-850	141	12	of	of	ADP
iajs-850	141	13	practical	practical	ADJ
iajs-850	141	14	organic	organic	ADJ
iajs-850	141	15	chemistry	chemistry	NOUN
iajs-850	141	16	”	"	PUNCT
iajs-850	141	17	,	,	PUNCT
iajs-850	141	18	5	5	NUM
iajs-850	141	19	th	th	NUM
iajs-850	141	20	ed	ed	NOUN
iajs-850	141	21	.	.	PROPN
iajs-850	141	22	,	,	PUNCT
iajs-850	141	23	john	john	PROPN
iajs-850	141	24	wiley	wiley	PROPN
iajs-850	141	25	and	and	CCONJ
iajs-850	141	26	sons	son	NOUN
iajs-850	141	27	,	,	PUNCT
iajs-850	141	28	inc	inc	PROPN
iajs-850	141	29	.	.	PROPN
iajs-850	141	30	,	,	PUNCT
iajs-850	141	31	new	new	PROPN
iajs-850	141	32	york	york	PROPN
iajs-850	141	33	,	,	PUNCT
iajs-850	141	34	,	,	PUNCT
iajs-850	141	35	pp	pp	ADJ
iajs-850	141	36	.	.	PUNCT
iajs-850	141	37	1219	1219	NUM
iajs-850	141	38	.	.	PUNCT
iajs-850	142	1	12	12	NUM
iajs-850	142	2	.	.	PUNCT
iajs-850	142	3	fieser	fieser	PROPN
iajs-850	142	4	,	,	PUNCT
iajs-850	142	5	l.	l.	PROPN
iajs-850	142	6	f.	f.	PROPN
iajs-850	142	7	and	and	CCONJ
iajs-850	142	8	williamson	williamson	PROPN
iajs-850	142	9	,	,	PUNCT
iajs-850	142	10	k.	k.	PROPN
iajs-850	142	11	l.	l.	PROPN
iajs-850	142	12	(	(	PUNCT
iajs-850	142	13	1983	1983	NUM
iajs-850	142	14	)	)	PUNCT
iajs-850	142	15	“	"	PUNCT
iajs-850	142	16	organic	organic	ADJ
iajs-850	142	17	experiments	experiment	NOUN
iajs-850	142	18	”	"	PUNCT
iajs-850	142	19	,	,	PUNCT
iajs-850	142	20	5	5	NUM
iajs-850	142	21	th	th	NUM
iajs-850	142	22	ed	ed	NOUN
iajs-850	142	23	.	.	PROPN
iajs-850	142	24	,	,	PUNCT
iajs-850	142	25	d.	d.	PROPN
iajs-850	142	26	c.	c.	PROPN
iajs-850	142	27	heath	heath	PROPN
iajs-850	142	28	and	and	CCONJ
iajs-850	142	29	company	company	NOUN
iajs-850	142	30	,	,	PUNCT
iajs-850	142	31	the	the	DET
iajs-850	142	32	united	united	PROPN
iajs-850	142	33	states	states	PROPN
iajs-850	142	34	of	of	ADP
iajs-850	142	35	america	america	PROPN
iajs-850	142	36	,	,	PUNCT
iajs-850	142	37	,	,	PUNCT
iajs-850	142	38	pp	pp	ADP
iajs-850	142	39	.	.	PUNCT
iajs-850	143	1	160	160	NUM
iajs-850	143	2	-	-	SYM
iajs-850	143	3	161	161	NUM
iajs-850	143	4	.	.	PUNCT
iajs-850	143	5	table	table	NOUN
iajs-850	143	6	(	(	PUNCT
iajs-850	143	7	1	1	NUM
iajs-850	143	8	)	)	PUNCT
iajs-850	143	9	:	:	PUNCT
iajs-850	143	10	physical	physical	ADJ
iajs-850	143	11	properties	property	NOUN
iajs-850	143	12	for	for	ADP
iajs-850	143	13	prepared	prepared	ADJ
iajs-850	143	14	compounds	compound	NOUN
iajs-850	143	15	(	(	PUNCT
iajs-850	143	16	9	9	NUM
iajs-850	143	17	)	)	PUNCT
iajs-850	143	18	,	,	PUNCT
iajs-850	143	19	(	(	PUNCT
iajs-850	143	20	10	10	NUM
iajs-850	143	21	)	)	PUNCT
iajs-850	143	22	and	and	CCONJ
iajs-850	143	23	(	(	PUNCT
iajs-850	143	24	11	11	NUM
iajs-850	143	25	)	)	PUNCT
iajs-850	143	26	comp	comp	NOUN
iajs-850	143	27	.	.	PUNCT
iajs-850	144	1	no	no	INTJ
iajs-850	144	2	.	.	PUNCT
iajs-850	145	1	formula	formula	NOUN
iajs-850	145	2	molecular	molecular	ADJ
iajs-850	145	3	weight	weight	NOUN
iajs-850	145	4	(	(	PUNCT
iajs-850	145	5	g	g	NOUN
iajs-850	145	6	/	/	SYM
iajs-850	145	7	mol	mol	NOUN
iajs-850	145	8	)	)	PUNCT
iajs-850	145	9	weight	weight	NOUN
iajs-850	145	10	of	of	ADP
iajs-850	145	11	product	product	NOUN
iajs-850	145	12	(	(	PUNCT
iajs-850	145	13	g	g	NOUN
iajs-850	145	14	)	)	PUNCT
iajs-850	145	15	yield	yield	NOUN
iajs-850	145	16	%	%	NOUN
iajs-850	145	17	m.p˚c	m.p˚c	NOUN
iajs-850	145	18	or	or	CCONJ
iajs-850	145	19	dec	dec	PROPN
iajs-850	145	20	.	.	PROPN
iajs-850	146	1	physica	physica	PROPN
iajs-850	146	2	l	l	PROPN
iajs-850	146	3	state	state	NOUN
iajs-850	146	4	rf	rf	ADJ
iajs-850	146	5	9	9	NUM
iajs-850	146	6	c23h16o10n2	c23h16o10n2	NOUN
iajs-850	146	7	480	480	NUM
iajs-850	146	8	3.57	3.57	NUM
iajs-850	146	9	72	72	NUM
iajs-850	146	10	210(dec	210(dec	NUM
iajs-850	146	11	.	.	PUNCT
iajs-850	146	12	)	)	PUNCT
iajs-850	147	1	white	white	ADJ
iajs-850	147	2	solid	solid	ADJ
iajs-850	148	1	0.52	0.52	NUM
iajs-850	148	2	10	10	NUM
iajs-850	148	3	c23h16o9n2	c23h16o9n2	NOUN
iajs-850	148	4	s	s	PART
iajs-850	148	5	496	496	NUM
iajs-850	148	6	3	3	NUM
iajs-850	148	7	60	60	NUM
iajs-850	148	8	225(dec	225(dec	NUM
iajs-850	148	9	)	)	PUNCT
iajs-850	148	10	yellow	yellow	ADJ
iajs-850	148	11	solid	solid	ADJ
iajs-850	148	12	0.60	0.60	NUM
iajs-850	148	13	11	11	NUM
iajs-850	148	14	c23h17o9n3	c23h17o9n3	PROPN
iajs-850	148	15	479	479	NUM
iajs-850	148	16	4.25	4.25	NUM
iajs-850	148	17	86	86	NUM
iajs-850	148	18	205(dec	205(dec	NUM
iajs-850	148	19	.	.	PUNCT
iajs-850	148	20	)	)	PUNCT
iajs-850	149	1	pale	pale	ADJ
iajs-850	149	2	yellow	yellow	ADJ
iajs-850	149	3	solid	solid	ADJ
iajs-850	149	4	0.33	0.33	NUM
iajs-850	149	5	ibn	ibn	PROPN
iajs-850	149	6	alhaitham	alhaitham	NOUN
iajs-850	149	7	j.	j.	PROPN
iajs-850	150	1	fo	fo	ADP
iajs-850	150	2	r	r	NOUN
iajs-850	150	3	pure	pure	ADJ
iajs-850	150	4	&	&	CCONJ
iajs-850	150	5	appl	appl	PROPN
iajs-850	150	6	.	.	PUNCT
iajs-850	151	1	sci	sci	PROPN
iajs-850	151	2	.	.	PROPN
iajs-850	152	1	vo	vo	INTJ
iajs-850	152	2	l.24	l.24	PROPN
iajs-850	152	3	(	(	PUNCT
iajs-850	152	4	1	1	NUM
iajs-850	152	5	)	)	PUNCT
iajs-850	152	6	2011	2011	NUM
iajs-850	152	7	table	table	NOUN
iajs-850	152	8	(	(	PUNCT
iajs-850	152	9	2	2	NUM
iajs-850	152	10	):	):	PUNCT
iajs-850	152	11	infrared	infrared	ADJ
iajs-850	152	12	spectra	spectra	PROPN
iajs-850	152	13	data	datum	NOUN
iajs-850	152	14	(	(	PUNCT
iajs-850	152	15	wave	wave	NOUN
iajs-850	152	16	number	number	NOUN
iajs-850	152	17	ύ	ύ	NOUN
iajs-850	152	18	)	)	PUNCT
iajs-850	152	19	cm	cm	NOUN
iajs-850	152	20	-1	-1	NOUN
iajs-850	152	21	of	of	ADP
iajs-850	152	22	the	the	DET
iajs-850	152	23	compounds	compound	NOUN
iajs-850	152	24	(	(	PUNCT
iajs-850	152	25	9	9	NUM
iajs-850	152	26	)	)	PUNCT
iajs-850	152	27	,	,	PUNCT
iajs-850	152	28	(	(	PUNCT
iajs-850	152	29	10	10	NUM
iajs-850	152	30	)	)	PUNCT
iajs-850	152	31	and	and	CCONJ
iajs-850	152	32	(	(	PUNCT
iajs-850	152	33	11	11	NUM
iajs-850	152	34	)	)	PUNCT
iajs-850	152	35	compound	compound	NOUN
iajs-850	152	36	υ(n	υ(n	PROPN
iajs-850	152	37	-	-	PUNCT
iajs-850	152	38	h	h	NOUN
iajs-850	152	39	)	)	PUNCT
iajs-850	152	40	and	and	CCONJ
iajs-850	152	41	υ(o	υ(o	PROPN
iajs-850	152	42	-	-	PUNCT
iajs-850	152	43	h	h	NOUN
iajs-850	152	44	)	)	PUNCT
iajs-850	152	45	υ(c	υ(c	PROPN
iajs-850	152	46	=	=	SYM
iajs-850	152	47	o	o	NOUN
iajs-850	152	48	)	)	PUNCT
iajs-850	152	49	in	in	ADP
iajs-850	152	50	(	(	PUNCT
iajs-850	152	51	chconh	chconh	PROPN
iajs-850	152	52	,	,	PUNCT
iajs-850	152	53	hnconh	hnconh	NOUN
iajs-850	152	54	)	)	PUNCT
iajs-850	152	55	υ(c	υ(c	PROPN
iajs-850	152	56	=	=	SYM
iajs-850	152	57	n	n	CCONJ
iajs-850	152	58	)	)	PUNCT
iajs-850	152	59	υ(c	υ(c	PROPN
iajs-850	152	60	-	-	PUNCT
iajs-850	152	61	n	n	CCONJ
iajs-850	152	62	)	)	PUNCT
iajs-850	152	63	υ(c	υ(c	PROPN
iajs-850	152	64	=	=	SYM
iajs-850	152	65	s	s	PART
iajs-850	152	66	)	)	PUNCT
iajs-850	152	67	9	9	NUM
iajs-850	152	68	3471(s	3471(s	NUM
iajs-850	152	69	)	)	PUNCT
iajs-850	152	70	1662(s	1662(s	NOUN
iajs-850	152	71	)	)	PUNCT
iajs-850	152	72	1627(s	1627(s	NUM
iajs-850	152	73	)	)	PUNCT
iajs-850	153	1	1346(w	1346(w	NUM
iajs-850	153	2	)	)	PUNCT
iajs-850	153	3	10	10	NUM
iajs-850	153	4	3383(s	3383(s	NOUN
iajs-850	153	5	)	)	PUNCT
iajs-850	153	6	1597(s	1597(s	NUM
iajs-850	153	7	)	)	PUNCT
iajs-850	153	8	1392(s	1392(s	NOUN
iajs-850	153	9	)	)	PUNCT
iajs-850	153	10	1153(m	1153(m	NUM
iajs-850	153	11	)	)	PUNCT
iajs-850	153	12	11	11	NUM
iajs-850	153	13	3421(br	3421(br	NOUN
iajs-850	153	14	)	)	PUNCT
iajs-850	153	15	1643(m	1643(m	NOUN
iajs-850	153	16	)	)	PUNCT
iajs-850	153	17	1597(s	1597(s	X
iajs-850	153	18	)	)	PUNCT
iajs-850	154	1	1334(w	1334(w	NUM
iajs-850	154	2	)	)	PUNCT
iajs-850	155	1	where	where	SCONJ
iajs-850	155	2	:	:	PUNCT
iajs-850	155	3	s	s	X
iajs-850	155	4	=	=	SYM
iajs-850	155	5	strong	strong	ADJ
iajs-850	155	6	,	,	PUNCT
iajs-850	155	7	m	m	VERB
iajs-850	155	8	=	=	ADJ
iajs-850	155	9	medium	medium	ADJ
iajs-850	155	10	,	,	PUNCT
iajs-850	155	11	w	w	NOUN
iajs-850	155	12	=	=	SYM
iajs-850	155	13	weak	weak	ADJ
iajs-850	155	14	,	,	PUNCT
iajs-850	155	15	br	br	NOUN
iajs-850	155	16	=	=	SYM
iajs-850	155	17	broad	broad	ADJ
iajs-850	155	18	table	table	NOUN
iajs-850	155	19	(	(	PUNCT
iajs-850	155	20	3	3	NUM
iajs-850	155	21	):	):	SYM
iajs-850	155	22	1	1	NUM
iajs-850	155	23	hnmr	hnmr	NOUN
iajs-850	155	24	data	datum	NOUN
iajs-850	155	25	for	for	ADP
iajs-850	155	26	the	the	DET
iajs-850	155	27	compounds	compound	NOUN
iajs-850	155	28	(	(	PUNCT
iajs-850	155	29	9	9	NUM
iajs-850	155	30	)	)	PUNCT
iajs-850	155	31	,	,	PUNCT
iajs-850	155	32	(	(	PUNCT
iajs-850	155	33	10	10	NUM
iajs-850	155	34	)	)	PUNCT
iajs-850	155	35	and	and	CCONJ
iajs-850	155	36	(	(	PUNCT
iajs-850	155	37	11	11	NUM
iajs-850	155	38	)	)	PUNCT
iajs-850	155	39	measured	measure	VERB
iajs-850	155	40	in	in	ADP
iajs-850	155	41	d2o	d2o	PROPN
iajs-850	155	42	with	with	ADP
iajs-850	155	43	tetramethyl	tetramethyl	NOUN
iajs-850	155	44	silane	silane	NOUN
iajs-850	155	45	(	(	PUNCT
iajs-850	155	46	tms	tms	PROPN
iajs-850	155	47	)	)	PUNCT
iajs-850	155	48	as	as	ADP
iajs-850	155	49	internal	internal	ADJ
iajs-850	155	50	standard	standard	ADJ
iajs-850	155	51	and	and	CCONJ
iajs-850	155	52	chemical	chemical	NOUN
iajs-850	155	53	shift	shift	NOUN
iajs-850	155	54	in	in	ADP
iajs-850	155	55	ppm	ppm	PROPN
iajs-850	155	56	(	(	PUNCT
iajs-850	155	57	δ	δ	NOUN
iajs-850	155	58	)	)	PUNCT
iajs-850	155	59	compound	compound	ADJ
iajs-850	155	60	functional	functional	ADJ
iajs-850	155	61	group	group	NOUN
iajs-850	155	62	δ(ppm	δ(ppm	NOUN
iajs-850	155	63	)	)	PUNCT
iajs-850	155	64	9	9	NUM
iajs-850	155	65	d	d	PROPN
iajs-850	155	66	,	,	PUNCT
iajs-850	155	67	1h	1h	NUM
iajs-850	155	68	,	,	PUNCT
iajs-850	155	69	ch	ch	NOUN
iajs-850	155	70	malonate	malonate	VERB
iajs-850	155	71	3	3	NUM
iajs-850	155	72	d	d	PROPN
iajs-850	155	73	,	,	PUNCT
iajs-850	155	74	1h	1h	NUM
iajs-850	155	75	,	,	PUNCT
iajs-850	155	76	lactone	lactone	NOUN
iajs-850	155	77	ring	ring	NOUN
iajs-850	155	78	h4	h4	PROPN
iajs-850	155	79	4.70	4.70	NUM
iajs-850	155	80	-	-	SYM
iajs-850	155	81	4.78	4.78	NUM
iajs-850	155	82	m	m	PROPN
iajs-850	155	83	,	,	PUNCT
iajs-850	155	84	10h	10h	NUM
iajs-850	155	85	,	,	PUNCT
iajs-850	155	86	aromatic	aromatic	ADJ
iajs-850	155	87	7.25	7.25	NUM
iajs-850	155	88	-	-	SYM
iajs-850	155	89	7.73	7.73	NUM
iajs-850	155	90	10	10	NUM
iajs-850	155	91	d	d	PROPN
iajs-850	155	92	,	,	PUNCT
iajs-850	155	93	1h	1h	NUM
iajs-850	155	94	,	,	PUNCT
iajs-850	155	95	ch	ch	NOUN
iajs-850	155	96	malonate	malonate	VERB
iajs-850	155	97	3	3	NUM
iajs-850	155	98	t	t	PROPN
iajs-850	155	99	,	,	PUNCT
iajs-850	155	100	1h	1h	NUM
iajs-850	155	101	,	,	PUNCT
iajs-850	155	102	ch	ch	NOUN
iajs-850	155	103	-	-	PROPN
iajs-850	156	1	oh	oh	NUM
iajs-850	156	2	3.22	3.22	NUM
iajs-850	156	3	d	d	PROPN
iajs-850	156	4	,	,	PUNCT
iajs-850	156	5	1h	1h	NUM
iajs-850	156	6	,	,	PUNCT
iajs-850	156	7	lactone	lactone	NOUN
iajs-850	156	8	ring	ring	NOUN
iajs-850	156	9	h4	h4	PROPN
iajs-850	156	10	4.69	4.69	NUM
iajs-850	156	11	m	m	PROPN
iajs-850	156	12	,	,	PUNCT
iajs-850	156	13	10h	10h	NUM
iajs-850	156	14	,	,	PUNCT
iajs-850	156	15	aromatic	aromatic	ADJ
iajs-850	156	16	7.32	7.32	NUM
iajs-850	156	17	-	-	SYM
iajs-850	156	18	7.76	7.76	NUM
iajs-850	156	19	11	11	NUM
iajs-850	156	20	d	d	PROPN
iajs-850	156	21	,	,	PUNCT
iajs-850	156	22	1h	1h	NUM
iajs-850	156	23	,	,	PUNCT
iajs-850	156	24	ch	ch	NOUN
iajs-850	156	25	malonate	malonate	VERB
iajs-850	156	26	3	3	NUM
iajs-850	156	27	t	t	PROPN
iajs-850	156	28	,	,	PUNCT
iajs-850	156	29	1h	1h	NUM
iajs-850	156	30	,	,	PUNCT
iajs-850	156	31	ch	ch	NOUN
iajs-850	156	32	-	-	PROPN
iajs-850	156	33	oh	oh	NUM
iajs-850	156	34	3.23	3.23	NUM
iajs-850	156	35	d	d	PROPN
iajs-850	156	36	,	,	PUNCT
iajs-850	156	37	1h	1h	NUM
iajs-850	156	38	,	,	PUNCT
iajs-850	156	39	lactone	lactone	NOUN
iajs-850	156	40	ring	ring	NOUN
iajs-850	156	41	h4	h4	PROPN
iajs-850	156	42	4.70	4.70	NUM
iajs-850	156	43	-	-	SYM
iajs-850	156	44	4.78	4.78	NUM
iajs-850	156	45	m	m	PROPN
iajs-850	156	46	,	,	PUNCT
iajs-850	156	47	10h	10h	NUM
iajs-850	156	48	,	,	PUNCT
iajs-850	156	49	aromatic	aromatic	ADJ
iajs-850	156	50	7.34	7.34	NUM
iajs-850	156	51	-	-	SYM
iajs-850	156	52	7.77	7.77	NUM
iajs-850	156	53	ibn	ibn	PROPN
iajs-850	156	54	alhaitham	alhaitham	NOUN
iajs-850	156	55	j.	j.	PROPN
iajs-850	157	1	fo	fo	ADP
iajs-850	157	2	r	r	NOUN
iajs-850	157	3	pure	pure	ADJ
iajs-850	157	4	&	&	CCONJ
iajs-850	157	5	appl	appl	PROPN
iajs-850	157	6	.	.	PUNCT
iajs-850	158	1	sci	sci	PROPN
iajs-850	158	2	.	.	PROPN
iajs-850	159	1	vo	vo	INTJ
iajs-850	159	2	l.24	l.24	PROPN
iajs-850	159	3	(	(	PUNCT
iajs-850	159	4	1	1	NUM
iajs-850	159	5	)	)	PUNCT
iajs-850	159	6	2011	2011	NUM
iajs-850	159	7	table	table	NOUN
iajs-850	159	8	(	(	PUNCT
iajs-850	159	9	4	4	NUM
iajs-850	159	10	):	):	PUNCT
iajs-850	159	11	13cnmr	13cnmr	NUM
iajs-850	159	12	data	datum	NOUN
iajs-850	159	13	for	for	ADP
iajs-850	159	14	the	the	DET
iajs-850	159	15	compounds	compound	NOUN
iajs-850	159	16	(	(	PUNCT
iajs-850	159	17	9	9	NUM
iajs-850	159	18	)	)	PUNCT
iajs-850	159	19	,	,	PUNCT
iajs-850	159	20	(	(	PUNCT
iajs-850	159	21	10	10	NUM
iajs-850	159	22	)	)	PUNCT
iajs-850	159	23	and	and	CCONJ
iajs-850	159	24	(	(	PUNCT
iajs-850	159	25	11	11	NUM
iajs-850	159	26	)	)	PUNCT
iajs-850	159	27	measured	measure	VERB
iajs-850	159	28	in	in	ADP
iajs-850	159	29	cdcl3	cdcl3	NOUN
iajs-850	159	30	and	and	CCONJ
iajs-850	159	31	chemical	chemical	NOUN
iajs-850	159	32	shift	shift	NOUN
iajs-850	159	33	in	in	ADP
iajs-850	159	34	ppm	ppm	PROPN
iajs-850	159	35	(	(	PUNCT
iajs-850	159	36	δ	δ	NOUN
iajs-850	159	37	)	)	PUNCT
iajs-850	159	38	compound	compound	ADJ
iajs-850	159	39	functional	functional	ADJ
iajs-850	159	40	group	group	NOUN
iajs-850	159	41	δ(ppm	δ(ppm	NOUN
iajs-850	159	42	)	)	PUNCT
iajs-850	159	43	9	9	NUM
iajs-850	159	44	c	c	X
iajs-850	159	45	=	=	X
iajs-850	159	46	o	o	X
iajs-850	159	47	in	in	ADP
iajs-850	159	48	hnconh	hnconh	NOUN
iajs-850	159	49	177.53	177.53	NUM
iajs-850	159	50	c	c	X
iajs-850	159	51	=	=	X
iajs-850	159	52	o	o	X
iajs-850	159	53	in	in	ADP
iajs-850	159	54	chconh	chconh	PROPN
iajs-850	159	55	175.65	175.65	NUM
iajs-850	159	56	c	c	X
iajs-850	159	57	=	=	X
iajs-850	159	58	o	o	NOUN
iajs-850	159	59	in	in	ADP
iajs-850	159	60	ester	ester	NOUN
iajs-850	159	61	,	,	PUNCT
iajs-850	159	62	lactone	lactone	NOUN
iajs-850	159	63	ring	ring	PROPN
iajs-850	159	64	164.53	164.53	NUM
iajs-850	159	65	c-3	c-3	NOUN
iajs-850	159	66	136.14	136.14	NUM
iajs-850	159	67	c-2	c-2	NOUN
iajs-850	159	68	131.63	131.63	NUM
iajs-850	159	69	c	c	NOUN
iajs-850	159	70	,	,	PUNCT
iajs-850	159	71	aromatic	aromatic	ADJ
iajs-850	159	72	131.24	131.24	NUM
iajs-850	159	73	-	-	SYM
iajs-850	159	74	127.85	127.85	NUM
iajs-850	159	75	c-4	c-4	NOUN
iajs-850	159	76	61.24	61.24	NUM
iajs-850	159	77	c-5	c-5	NOUN
iajs-850	159	78	,	,	PUNCT
iajs-850	159	79	c-6	c-6	NOUN
iajs-850	159	80	47.85	47.85	NUM
iajs-850	159	81	10	10	NUM
iajs-850	160	1	c	c	X
iajs-850	160	2	=	=	NOUN
iajs-850	160	3	o	o	X
iajs-850	160	4	161.70	161.70	NUM
iajs-850	160	5	c-3	c-3	NOUN
iajs-850	160	6	136.00	136.00	NUM
iajs-850	160	7	c-2	c-2	NOUN
iajs-850	160	8	131.20	131.20	NUM
iajs-850	160	9	c	c	NOUN
iajs-850	160	10	,	,	PUNCT
iajs-850	160	11	aromatic	aromatic	ADJ
iajs-850	160	12	128.73	128.73	NUM
iajs-850	160	13	,	,	PUNCT
iajs-850	160	14	128.25	128.25	NUM
iajs-850	160	15	11	11	NUM
iajs-850	160	16	c	c	X
iajs-850	160	17	=	=	X
iajs-850	160	18	nh	nh	PROPN
iajs-850	160	19	177.43	177.43	NUM
iajs-850	160	20	c	c	NOUN
iajs-850	160	21	=	=	X
iajs-850	160	22	o	o	X
iajs-850	160	23	in	in	ADP
iajs-850	160	24	chconh	chconh	PROPN
iajs-850	160	25	175.76	175.76	NUM
iajs-850	161	1	c	c	X
iajs-850	161	2	=	=	X
iajs-850	161	3	o	o	X
iajs-850	161	4	in	in	ADP
iajs-850	161	5	ester	ester	NOUN
iajs-850	161	6	,	,	PUNCT
iajs-850	161	7	lactone	lactone	NOUN
iajs-850	161	8	ring	ring	NOUN
iajs-850	161	9	163.31	163.31	NUM
iajs-850	161	10	c-3	c-3	NOUN
iajs-850	161	11	136.18	136.18	NUM
iajs-850	161	12	c-2	c-2	NOUN
iajs-850	161	13	131.25	131.25	NUM
iajs-850	161	14	c	c	NOUN
iajs-850	161	15	,	,	PUNCT
iajs-850	161	16	aromatic	aromatic	ADJ
iajs-850	161	17	128.75	128.75	NUM
iajs-850	161	18	,	,	PUNCT
iajs-850	161	19	128.29	128.29	NUM
iajs-850	161	20	c-4	c-4	NOUN
iajs-850	161	21	48.88	48.88	NUM
iajs-850	161	22	c-5	c-5	NOUN
iajs-850	161	23	,	,	PUNCT
iajs-850	161	24	c-6	c-6	NOUN
iajs-850	161	25	47.71	47.71	NUM
iajs-850	161	26	table	table	NOUN
iajs-850	161	27	(	(	PUNCT
iajs-850	161	28	5	5	NUM
iajs-850	161	29	):	):	PUNCT
iajs-850	161	30	electronic	electronic	ADJ
iajs-850	161	31	spectra	spectra	ADJ
iajs-850	161	32	data	datum	NOUN
iajs-850	161	33	for	for	ADP
iajs-850	161	34	the	the	DET
iajs-850	161	35	compounds	compound	NOUN
iajs-850	161	36	(	(	PUNCT
iajs-850	161	37	9	9	NUM
iajs-850	161	38	)	)	PUNCT
iajs-850	161	39	,	,	PUNCT
iajs-850	161	40	(	(	PUNCT
iajs-850	161	41	10	10	NUM
iajs-850	161	42	)	)	PUNCT
iajs-850	161	43	and	and	CCONJ
iajs-850	161	44	(	(	PUNCT
iajs-850	161	45	11	11	NUM
iajs-850	161	46	)	)	PUNCT
iajs-850	161	47	compound	compound	NOUN
iajs-850	161	48	λmax	λmax	NOUN
iajs-850	161	49	nm	nm	PRON
iajs-850	161	50	wave	wave	NOUN
iajs-850	161	51	number	number	NOUN
iajs-850	161	52	cm-1	cm-1	PART
iajs-850	161	53	εmax	εmax	PROPN
iajs-850	161	54	molar-1cm-1	molar-1cm-1	PROPN
iajs-850	161	55	assignment	assignment	NOUN
iajs-850	161	56	9	9	NUM
iajs-850	161	57	294	294	NUM
iajs-850	161	58	34013	34013	NUM
iajs-850	161	59	66	66	NUM
iajs-850	161	60	n	n	NUM
iajs-850	161	61	π	π	PROPN
iajs-850	161	62	*	*	PROPN
iajs-850	161	63	10	10	NUM
iajs-850	161	64	257	257	NUM
iajs-850	161	65	291	291	NUM
iajs-850	161	66	38910	38910	NUM
iajs-850	161	67	34364	34364	NUM
iajs-850	161	68	140	140	NUM
iajs-850	161	69	195	195	NUM
iajs-850	161	70	π	π	PROPN
iajs-850	161	71	π	π	X
iajs-850	161	72	*	*	PROPN
iajs-850	161	73	n	n	PROPN
iajs-850	161	74	π	π	PROPN
iajs-850	161	75	*	*	PROPN
iajs-850	161	76	11	11	NUM
iajs-850	161	77	232	232	NUM
iajs-850	161	78	297	297	NUM
iajs-850	161	79	43103	43103	NUM
iajs-850	161	80	33670	33670	NUM
iajs-850	161	81	15	15	NUM
iajs-850	161	82	192	192	NUM
iajs-850	161	83	π	π	PROPN
iajs-850	161	84	π	π	X
iajs-850	161	85	*	*	PROPN
iajs-850	161	86	n	n	PROPN
iajs-850	161	87	π	π	NOUN
iajs-850	161	88	*	*	PUNCT