id	sid	tid	token	lemma	pos
ijpds-3748	1	1	ahmad	ahmad	PROPN
ijpds-3748	1	2	et	et	PROPN
ijpds-3748	1	3	al	al	PROPN
ijpds-3748	1	4	rp	rp	PROPN
ijpds-3748	1	5	-	-	PUNCT
ijpds-3748	1	6	hplc	hplc	NOUN
ijpds-3748	1	7	method	method	NOUN
ijpds-3748	1	8	validation	validation	NOUN
ijpds-3748	1	9	of	of	ADP
ijpds-3748	1	10	empagliflozin	empagliflozin	PROPN
ijpds-3748	1	11	vol	vol	NOUN
ijpds-3748	1	12	2	2	NUM
ijpds-3748	2	1	|	|	NOUN
ijpds-3748	2	2	issue	issue	NOUN
ijpds-3748	2	3	2	2	NUM
ijpds-3748	2	4	|	|	ADV
ijpds-3748	2	5	apr	apr	ADV
ijpds-3748	2	6	–	–	PUNCT
ijpds-3748	2	7	jun	jun	PROPN
ijpds-3748	2	8	2023	2023	NUM
ijpds-3748	2	9	indian	indian	PROPN
ijpds-3748	2	10	j	j	PROPN
ijpds-3748	2	11	pharm	pharm	PROPN
ijpds-3748	2	12	drug	drug	PROPN
ijpds-3748	2	13	studies	study	NOUN
ijpds-3748	2	14	|	|	ADV
ijpds-3748	2	15	76	76	NUM
ijpds-3748	2	16	research	research	NOUN
ijpds-3748	2	17	article	article	NOUN
ijpds-3748	2	18	development	development	NOUN
ijpds-3748	2	19	and	and	CCONJ
ijpds-3748	2	20	validation	validation	NOUN
ijpds-3748	2	21	of	of	ADP
ijpds-3748	2	22	novel	novel	ADJ
ijpds-3748	2	23	stability	stability	NOUN
ijpds-3748	2	24	indicating	indicate	VERB
ijpds-3748	2	25	rp	rp	ADP
ijpds-3748	2	26	hplc	hplc	NOUN
ijpds-3748	2	27	method	method	NOUN
ijpds-3748	2	28	for	for	ADP
ijpds-3748	2	29	quantitative	quantitative	ADJ
ijpds-3748	2	30	estimation	estimation	NOUN
ijpds-3748	2	31	of	of	ADP
ijpds-3748	2	32	empagliflozin	empagliflozin	PROPN
ijpds-3748	2	33	in	in	ADP
ijpds-3748	2	34	tablets	tablet	NOUN
ijpds-3748	2	35	ausuf	ausuf	PROPN
ijpds-3748	2	36	ahmad1	ahmad1	PROPN
ijpds-3748	2	37	,	,	PUNCT
ijpds-3748	2	38	zahra	zahra	PROPN
ijpds-3748	2	39	maryam2	maryam2	PROPN
ijpds-3748	2	40	from	from	ADP
ijpds-3748	2	41	,	,	PUNCT
ijpds-3748	2	42	1department	1department	NUM
ijpds-3748	2	43	of	of	ADP
ijpds-3748	2	44	clinical	clinical	ADJ
ijpds-3748	2	45	and	and	CCONJ
ijpds-3748	2	46	pharmaceutical	pharmaceutical	NOUN
ijpds-3748	2	47	sciences	science	NOUN
ijpds-3748	2	48	,	,	PUNCT
ijpds-3748	2	49	school	school	NOUN
ijpds-3748	2	50	of	of	ADP
ijpds-3748	2	51	life	life	NOUN
ijpds-3748	2	52	and	and	CCONJ
ijpds-3748	2	53	medical	medical	ADJ
ijpds-3748	2	54	sciences	science	NOUN
ijpds-3748	2	55	,	,	PUNCT
ijpds-3748	2	56	university	university	NOUN
ijpds-3748	2	57	of	of	ADP
ijpds-3748	2	58	hertfordshire	hertfordshire	PROPN
ijpds-3748	2	59	,	,	PUNCT
ijpds-3748	2	60	hatfield	hatfield	PROPN
ijpds-3748	2	61	,	,	PUNCT
ijpds-3748	2	62	uk	uk	PROPN
ijpds-3748	2	63	,	,	PUNCT
ijpds-3748	2	64	2department	2department	NUM
ijpds-3748	2	65	of	of	ADP
ijpds-3748	2	66	pharmaceutical	pharmaceutical	ADJ
ijpds-3748	2	67	chemistry	chemistry	NOUN
ijpds-3748	2	68	,	,	PUNCT
ijpds-3748	2	69	faculty	faculty	NOUN
ijpds-3748	2	70	of	of	ADP
ijpds-3748	2	71	pharmacy	pharmacy	NOUN
ijpds-3748	2	72	,	,	PUNCT
ijpds-3748	2	73	anadolu	anadolu	PROPN
ijpds-3748	2	74	university	university	NOUN
ijpds-3748	2	75	,	,	PUNCT
ijpds-3748	2	76	eskişehir	eskişehir	NOUN
ijpds-3748	2	77	26470	26470	NUM
ijpds-3748	2	78	,	,	PUNCT
ijpds-3748	2	79	turkey	turkey	NOUN
ijpds-3748	2	80	.	.	PUNCT
ijpds-3748	3	1	correspondence	correspondence	NOUN
ijpds-3748	3	2	to	to	ADP
ijpds-3748	3	3	:	:	PUNCT
ijpds-3748	3	4	zahra	zahra	PROPN
ijpds-3748	3	5	maryam	maryam	PROPN
ijpds-3748	3	6	,	,	PUNCT
ijpds-3748	3	7	department	department	NOUN
ijpds-3748	3	8	of	of	ADP
ijpds-3748	3	9	pharmaceutical	pharmaceutical	ADJ
ijpds-3748	3	10	chemistry	chemistry	NOUN
ijpds-3748	3	11	,	,	PUNCT
ijpds-3748	3	12	faculty	faculty	NOUN
ijpds-3748	3	13	of	of	ADP
ijpds-3748	3	14	pharmacy	pharmacy	NOUN
ijpds-3748	3	15	,	,	PUNCT
ijpds-3748	3	16	anadolu	anadolu	PROPN
ijpds-3748	3	17	university	university	NOUN
ijpds-3748	3	18	,	,	PUNCT
ijpds-3748	3	19	eskişehir	eskişehir	NOUN
ijpds-3748	3	20	26470	26470	NUM
ijpds-3748	3	21	,	,	PUNCT
ijpds-3748	3	22	turkey	turkey	PROPN
ijpds-3748	3	23	.	.	PUNCT
ijpds-3748	4	1	tel	tel	ADP
ijpds-3748	4	2	:	:	PUNCT
ijpds-3748	4	3	+90	+90	PROPN
ijpds-3748	4	4	-	-	SYM
ijpds-3748	4	5	5411666124	5411666124	NUM
ijpds-3748	4	6	,	,	PUNCT
ijpds-3748	4	7	e	e	NOUN
ijpds-3748	4	8	-	-	NOUN
ijpds-3748	4	9	mail	mail	NOUN
ijpds-3748	4	10	:	:	PUNCT
ijpds-3748	5	1	zahra.maryam489@gmail.com	zahra.maryam489@gmail.com	PROPN
ijpds-3748	5	2	abstract	abstract	ADJ
ijpds-3748	5	3	the	the	DET
ijpds-3748	5	4	current	current	ADJ
ijpds-3748	5	5	study	study	NOUN
ijpds-3748	5	6	was	be	AUX
ijpds-3748	5	7	conducted	conduct	VERB
ijpds-3748	5	8	to	to	PART
ijpds-3748	5	9	develop	develop	VERB
ijpds-3748	5	10	and	and	CCONJ
ijpds-3748	5	11	validate	validate	VERB
ijpds-3748	5	12	a	a	DET
ijpds-3748	5	13	novel	novel	ADJ
ijpds-3748	5	14	method	method	NOUN
ijpds-3748	5	15	for	for	ADP
ijpds-3748	5	16	the	the	DET
ijpds-3748	5	17	qualitative	qualitative	ADJ
ijpds-3748	5	18	and	and	CCONJ
ijpds-3748	5	19	quantitative	quantitative	ADJ
ijpds-3748	5	20	determination	determination	NOUN
ijpds-3748	5	21	of	of	ADP
ijpds-3748	5	22	empagliflozin	empagliflozin	PROPN
ijpds-3748	5	23	in	in	ADP
ijpds-3748	5	24	bulk	bulk	ADJ
ijpds-3748	5	25	granules	granule	NOUN
ijpds-3748	5	26	and	and	CCONJ
ijpds-3748	5	27	tablets	tablet	NOUN
ijpds-3748	5	28	.	.	PUNCT
ijpds-3748	6	1	this	this	DET
ijpds-3748	6	2	method	method	NOUN
ijpds-3748	6	3	was	be	AUX
ijpds-3748	6	4	successively	successively	ADV
ijpds-3748	6	5	applied	apply	VERB
ijpds-3748	6	6	to	to	ADP
ijpds-3748	6	7	the	the	DET
ijpds-3748	6	8	analysis	analysis	NOUN
ijpds-3748	6	9	of	of	ADP
ijpds-3748	6	10	the	the	DET
ijpds-3748	6	11	approved	approve	VERB
ijpds-3748	6	12	dosage	dosage	NOUN
ijpds-3748	6	13	form	form	NOUN
ijpds-3748	6	14	of	of	ADP
ijpds-3748	6	15	empagliflozin	empagliflozin	PROPN
ijpds-3748	6	16	available	available	ADJ
ijpds-3748	6	17	in	in	ADP
ijpds-3748	6	18	the	the	DET
ijpds-3748	6	19	market	market	NOUN
ijpds-3748	6	20	with	with	ADP
ijpds-3748	6	21	the	the	DET
ijpds-3748	6	22	brand	brand	NOUN
ijpds-3748	6	23	name	name	NOUN
ijpds-3748	6	24	of	of	ADP
ijpds-3748	6	25	jardiance	jardiance	NOUN
ijpds-3748	6	26	tablets	tablet	NOUN
ijpds-3748	6	27	.	.	PUNCT
ijpds-3748	7	1	the	the	DET
ijpds-3748	7	2	developed	develop	VERB
ijpds-3748	7	3	method	method	NOUN
ijpds-3748	7	4	was	be	AUX
ijpds-3748	7	5	found	find	VERB
ijpds-3748	7	6	to	to	PART
ijpds-3748	7	7	be	be	AUX
ijpds-3748	7	8	precise	precise	ADJ
ijpds-3748	7	9	,	,	PUNCT
ijpds-3748	7	10	economic	economic	ADJ
ijpds-3748	7	11	,	,	PUNCT
ijpds-3748	7	12	and	and	CCONJ
ijpds-3748	7	13	rapid	rapid	ADJ
ijpds-3748	7	14	with	with	ADP
ijpds-3748	7	15	a	a	DET
ijpds-3748	7	16	run	run	ADJ
ijpds-3748	7	17	time	time	NOUN
ijpds-3748	7	18	of	of	ADP
ijpds-3748	7	19	20	20	NUM
ijpds-3748	7	20	minutes	minute	NOUN
ijpds-3748	7	21	.	.	PUNCT
ijpds-3748	8	1	the	the	DET
ijpds-3748	8	2	empagliflozin	empagliflozin	PROPN
ijpds-3748	8	3	peak	peak	NOUN
ijpds-3748	8	4	was	be	AUX
ijpds-3748	8	5	eluted	elute	VERB
ijpds-3748	8	6	at	at	ADP
ijpds-3748	8	7	5.0	5.0	NUM
ijpds-3748	8	8	minutes	minute	NOUN
ijpds-3748	8	9	.	.	PUNCT
ijpds-3748	9	1	this	this	DET
ijpds-3748	9	2	elution	elution	NOUN
ijpds-3748	9	3	was	be	AUX
ijpds-3748	9	4	done	do	VERB
ijpds-3748	9	5	on	on	ADP
ijpds-3748	9	6	the	the	DET
ijpds-3748	9	7	c18	c18	NOUN
ijpds-3748	9	8	column	column	NOUN
ijpds-3748	9	9	(	(	PUNCT
ijpds-3748	9	10	150	150	NUM
ijpds-3748	9	11	x	x	SYM
ijpds-3748	9	12	4.6	4.6	NUM
ijpds-3748	9	13	mm	mm	NOUN
ijpds-3748	9	14	)	)	PUNCT
ijpds-3748	9	15	having	have	VERB
ijpds-3748	9	16	a	a	DET
ijpds-3748	9	17	5μm	5μm	ADJ
ijpds-3748	9	18	particle	particle	NOUN
ijpds-3748	9	19	size	size	NOUN
ijpds-3748	9	20	using	use	VERB
ijpds-3748	9	21	an	an	DET
ijpds-3748	9	22	isocratic	isocratic	ADJ
ijpds-3748	9	23	mobile	mobile	ADJ
ijpds-3748	9	24	phase	phase	NOUN
ijpds-3748	9	25	,	,	PUNCT
ijpds-3748	9	26	a	a	DET
ijpds-3748	9	27	mixture	mixture	NOUN
ijpds-3748	9	28	of	of	ADP
ijpds-3748	9	29	phosphate	phosphate	ADJ
ijpds-3748	9	30	buffer	buffer	NOUN
ijpds-3748	9	31	ph	ph	VERB
ijpds-3748	9	32	3.0	3.0	NUM
ijpds-3748	9	33	and	and	CCONJ
ijpds-3748	9	34	methanol	methanol	NOUN
ijpds-3748	9	35	in	in	ADP
ijpds-3748	9	36	the	the	DET
ijpds-3748	9	37	ratio	ratio	NOUN
ijpds-3748	9	38	of	of	ADP
ijpds-3748	9	39	70:30	70:30	NUM
ijpds-3748	9	40	at	at	ADP
ijpds-3748	9	41	a	a	DET
ijpds-3748	9	42	flow	flow	NOUN
ijpds-3748	9	43	rate	rate	NOUN
ijpds-3748	9	44	of	of	ADP
ijpds-3748	9	45	1.0ml	1.0ml	NUM
ijpds-3748	9	46	/	/	SYM
ijpds-3748	9	47	min	min	NOUN
ijpds-3748	9	48	with	with	ADP
ijpds-3748	9	49	pda	pda	NOUN
ijpds-3748	9	50	detector	detector	NOUN
ijpds-3748	9	51	(	(	PUNCT
ijpds-3748	9	52	maximum	maximum	ADJ
ijpds-3748	9	53	wavelength	wavelength	NOUN
ijpds-3748	9	54	of	of	ADP
ijpds-3748	9	55	224	224	NUM
ijpds-3748	9	56	nm	nm	NOUN
ijpds-3748	9	57	)	)	PUNCT
ijpds-3748	9	58	and	and	CCONJ
ijpds-3748	9	59	column	column	NOUN
ijpds-3748	9	60	temperature	temperature	NOUN
ijpds-3748	9	61	30	30	NUM
ijpds-3748	9	62	°	°	SYM
ijpds-3748	9	63	c	c	NOUN
ijpds-3748	9	64	.	.	PUNCT
ijpds-3748	10	1	the	the	DET
ijpds-3748	10	2	method	method	NOUN
ijpds-3748	10	3	was	be	AUX
ijpds-3748	10	4	found	find	VERB
ijpds-3748	10	5	to	to	PART
ijpds-3748	10	6	be	be	AUX
ijpds-3748	10	7	linear	linear	ADJ
ijpds-3748	10	8	with	with	ADP
ijpds-3748	10	9	lod	lod	PROPN
ijpds-3748	10	10	and	and	CCONJ
ijpds-3748	10	11	loq	loq	PROPN
ijpds-3748	10	12	,	,	PUNCT
ijpds-3748	10	13	0.068	0.068	NUM
ijpds-3748	10	14	μg	μg	PROPN
ijpds-3748	10	15	and	and	CCONJ
ijpds-3748	10	16	0.35	0.35	NUM
ijpds-3748	10	17	μg	μg	NOUN
ijpds-3748	10	18	,	,	PUNCT
ijpds-3748	10	19	respectively	respectively	ADV
ijpds-3748	10	20	.	.	PUNCT
ijpds-3748	11	1	the	the	DET
ijpds-3748	11	2	correlation	correlation	NOUN
ijpds-3748	11	3	coefficient	coefficient	NOUN
ijpds-3748	11	4	r2	r2	PROPN
ijpds-3748	11	5	calculated	calculate	VERB
ijpds-3748	11	6	was	be	AUX
ijpds-3748	11	7	0.996	0.996	NUM
ijpds-3748	11	8	.	.	PUNCT
ijpds-3748	11	9	precision	precision	NOUN
ijpds-3748	11	10	and	and	CCONJ
ijpds-3748	11	11	accuracy	accuracy	NOUN
ijpds-3748	11	12	of	of	ADP
ijpds-3748	11	13	the	the	DET
ijpds-3748	11	14	method	method	NOUN
ijpds-3748	11	15	evaluated	evaluate	VERB
ijpds-3748	11	16	by	by	ADP
ijpds-3748	11	17	interday	interday	PROPN
ijpds-3748	11	18	,	,	PUNCT
ijpds-3748	11	19	intraday	intraday	NOUN
ijpds-3748	11	20	,	,	PUNCT
ijpds-3748	11	21	and	and	CCONJ
ijpds-3748	11	22	recovery	recovery	NOUN
ijpds-3748	11	23	study	study	NOUN
ijpds-3748	11	24	was	be	AUX
ijpds-3748	11	25	found	find	VERB
ijpds-3748	11	26	to	to	PART
ijpds-3748	11	27	be	be	AUX
ijpds-3748	11	28	within	within	ADP
ijpds-3748	11	29	limits	limit	NOUN
ijpds-3748	11	30	.	.	PUNCT
ijpds-3748	12	1	the	the	DET
ijpds-3748	12	2	forced	force	VERB
ijpds-3748	12	3	degradation	degradation	NOUN
ijpds-3748	12	4	study	study	NOUN
ijpds-3748	12	5	proved	prove	VERB
ijpds-3748	12	6	the	the	DET
ijpds-3748	12	7	stability	stability	NOUN
ijpds-3748	12	8	of	of	ADP
ijpds-3748	12	9	the	the	DET
ijpds-3748	12	10	method	method	NOUN
ijpds-3748	12	11	.	.	PUNCT
ijpds-3748	13	1	objectives	objective	NOUN
ijpds-3748	13	2	:	:	PUNCT
ijpds-3748	13	3	this	this	DET
ijpds-3748	13	4	research	research	NOUN
ijpds-3748	13	5	article	article	NOUN
ijpds-3748	13	6	is	be	AUX
ijpds-3748	13	7	aimed	aim	VERB
ijpds-3748	13	8	at	at	ADP
ijpds-3748	13	9	developing	develop	VERB
ijpds-3748	13	10	a	a	DET
ijpds-3748	13	11	new	new	ADJ
ijpds-3748	13	12	method	method	NOUN
ijpds-3748	13	13	for	for	ADP
ijpds-3748	13	14	developing	develop	VERB
ijpds-3748	13	15	and	and	CCONJ
ijpds-3748	13	16	validating	validate	VERB
ijpds-3748	13	17	a	a	DET
ijpds-3748	13	18	novel	novel	ADJ
ijpds-3748	13	19	method	method	NOUN
ijpds-3748	13	20	for	for	ADP
ijpds-3748	13	21	the	the	DET
ijpds-3748	13	22	qualitative	qualitative	ADJ
ijpds-3748	13	23	and	and	CCONJ
ijpds-3748	13	24	quantitative	quantitative	ADJ
ijpds-3748	13	25	determination	determination	NOUN
ijpds-3748	13	26	of	of	ADP
ijpds-3748	13	27	empagliflozin	empagliflozin	PROPN
ijpds-3748	13	28	in	in	ADP
ijpds-3748	13	29	bulk	bulk	ADJ
ijpds-3748	13	30	granules	granule	NOUN
ijpds-3748	13	31	and	and	CCONJ
ijpds-3748	13	32	tablets	tablet	NOUN
ijpds-3748	13	33	.	.	PUNCT
ijpds-3748	14	1	methods	method	NOUN
ijpds-3748	14	2	:	:	PUNCT
ijpds-3748	14	3	to	to	PART
ijpds-3748	14	4	conduct	conduct	VERB
ijpds-3748	14	5	this	this	DET
ijpds-3748	14	6	research	research	NOUN
ijpds-3748	14	7	,	,	PUNCT
ijpds-3748	14	8	all	all	DET
ijpds-3748	14	9	the	the	DET
ijpds-3748	14	10	validation	validation	NOUN
ijpds-3748	14	11	parameters	parameter	NOUN
ijpds-3748	14	12	were	be	AUX
ijpds-3748	14	13	employed	employ	VERB
ijpds-3748	14	14	according	accord	VERB
ijpds-3748	14	15	to	to	ADP
ijpds-3748	14	16	international	international	ADJ
ijpds-3748	14	17	council	council	NOUN
ijpds-3748	14	18	for	for	ADP
ijpds-3748	14	19	harmonization	harmonization	NOUN
ijpds-3748	14	20	(	(	PUNCT
ijpds-3748	14	21	ich	ich	NOUN
ijpds-3748	14	22	)	)	PUNCT
ijpds-3748	14	23	guidelines	guideline	NOUN
ijpds-3748	14	24	and	and	CCONJ
ijpds-3748	14	25	all	all	DET
ijpds-3748	14	26	the	the	DET
ijpds-3748	14	27	validation	validation	NOUN
ijpds-3748	14	28	parameters	parameter	NOUN
ijpds-3748	14	29	e.g.	e.g.	ADV
ijpds-3748	14	30	,	,	PUNCT
ijpds-3748	14	31	accuracy	accuracy	NOUN
ijpds-3748	14	32	,	,	PUNCT
ijpds-3748	14	33	specificity	specificity	NOUN
ijpds-3748	14	34	,	,	PUNCT
ijpds-3748	14	35	linearity	linearity	NOUN
ijpds-3748	14	36	,	,	PUNCT
ijpds-3748	14	37	lod	lod	PROPN
ijpds-3748	14	38	,	,	PUNCT
ijpds-3748	14	39	loq	loq	PROPN
ijpds-3748	14	40	,	,	PUNCT
ijpds-3748	14	41	robustness	robustness	NOUN
ijpds-3748	14	42	,	,	PUNCT
ijpds-3748	14	43	and	and	CCONJ
ijpds-3748	14	44	degradation	degradation	NOUN
ijpds-3748	14	45	studies	study	NOUN
ijpds-3748	14	46	were	be	AUX
ijpds-3748	14	47	performed	perform	VERB
ijpds-3748	14	48	.	.	PUNCT
ijpds-3748	15	1	results	result	NOUN
ijpds-3748	15	2	:	:	PUNCT
ijpds-3748	15	3	results	result	NOUN
ijpds-3748	15	4	of	of	ADP
ijpds-3748	15	5	the	the	DET
ijpds-3748	15	6	proposed	propose	VERB
ijpds-3748	15	7	technique	technique	NOUN
ijpds-3748	15	8	were	be	AUX
ijpds-3748	15	9	found	find	VERB
ijpds-3748	15	10	to	to	PART
ijpds-3748	15	11	be	be	AUX
ijpds-3748	15	12	trustworthy	trustworthy	ADJ
ijpds-3748	15	13	,	,	PUNCT
ijpds-3748	15	14	accurate	accurate	ADJ
ijpds-3748	15	15	,	,	PUNCT
ijpds-3748	15	16	suitable	suitable	ADJ
ijpds-3748	15	17	,	,	PUNCT
ijpds-3748	15	18	and	and	CCONJ
ijpds-3748	15	19	robust	robust	ADJ
ijpds-3748	15	20	for	for	ADP
ijpds-3748	15	21	everyday	everyday	ADJ
ijpds-3748	15	22	application	application	NOUN
ijpds-3748	15	23	.	.	PUNCT
ijpds-3748	16	1	conclusion	conclusion	NOUN
ijpds-3748	16	2	:	:	PUNCT
ijpds-3748	16	3	conclusively	conclusively	ADV
ijpds-3748	16	4	the	the	DET
ijpds-3748	16	5	results	result	NOUN
ijpds-3748	16	6	of	of	ADP
ijpds-3748	16	7	the	the	DET
ijpds-3748	16	8	study	study	NOUN
ijpds-3748	16	9	indicated	indicate	VERB
ijpds-3748	16	10	that	that	SCONJ
ijpds-3748	16	11	the	the	DET
ijpds-3748	16	12	current	current	ADJ
ijpds-3748	16	13	method	method	NOUN
ijpds-3748	16	14	is	be	AUX
ijpds-3748	16	15	simple	simple	ADJ
ijpds-3748	16	16	,	,	PUNCT
ijpds-3748	16	17	precise	precise	ADJ
ijpds-3748	16	18	,	,	PUNCT
ijpds-3748	16	19	accurate	accurate	ADJ
ijpds-3748	16	20	,	,	PUNCT
ijpds-3748	16	21	stable	stable	ADJ
ijpds-3748	16	22	,	,	PUNCT
ijpds-3748	16	23	and	and	CCONJ
ijpds-3748	16	24	economic	economic	ADJ
ijpds-3748	16	25	,	,	PUNCT
ijpds-3748	16	26	and	and	CCONJ
ijpds-3748	16	27	thus	thus	ADV
ijpds-3748	16	28	can	can	AUX
ijpds-3748	16	29	be	be	AUX
ijpds-3748	16	30	used	use	VERB
ijpds-3748	16	31	for	for	ADP
ijpds-3748	16	32	routine	routine	ADJ
ijpds-3748	16	33	quality	quality	NOUN
ijpds-3748	16	34	control	control	NOUN
ijpds-3748	16	35	testing	testing	NOUN
ijpds-3748	16	36	of	of	ADP
ijpds-3748	16	37	empagliflozin	empagliflozin	PROPN
ijpds-3748	16	38	.	.	PUNCT
ijpds-3748	17	1	keywords	keyword	NOUN
ijpds-3748	17	2	:	:	PUNCT
ijpds-3748	17	3	empagliflozin	empagliflozin	PROPN
ijpds-3748	17	4	,	,	PUNCT
ijpds-3748	17	5	rp	rp	NOUN
ijpds-3748	17	6	-	-	PUNCT
ijpds-3748	17	7	hplc	hplc	NOUN
ijpds-3748	17	8	,	,	PUNCT
ijpds-3748	17	9	method	method	NOUN
ijpds-3748	17	10	validation	validation	NOUN
ijpds-3748	17	11	,	,	PUNCT
ijpds-3748	17	12	qualitative	qualitative	ADJ
ijpds-3748	17	13	determination	determination	NOUN
ijpds-3748	17	14	hemically	hemically	ADV
ijpds-3748	17	15	,	,	PUNCT
ijpds-3748	17	16	empagliflozin	empagliflozin	PROPN
ijpds-3748	17	17	is	be	AUX
ijpds-3748	17	18	(	(	PUNCT
ijpds-3748	17	19	1	1	NUM
ijpds-3748	17	20	-	-	PUNCT
ijpds-3748	17	21	chloro-4[b	chloro-4[b	NOUN
ijpds-3748	17	22	dglucopyranos-1	dglucopyranos-1	PROPN
ijpds-3748	17	23	-	-	PUNCT
ijpds-3748	17	24	y1]-2-[4-([1]-tetrahydrofuran-3	y1]-2-[4-([1]-tetrahydrofuran-3	NOUN
ijpds-3748	17	25	-	-	PUNCT
ijpds-3748	17	26	yloxy	yloxy	ADJ
ijpds-3748	17	27	)	)	PUNCT
ijpds-3748	17	28	benzyl]-benzene	benzyl]-benzene	NOUN
ijpds-3748	18	1	[	[	X
ijpds-3748	18	2	1	1	NUM
ijpds-3748	18	3	-	-	SYM
ijpds-3748	18	4	2	2	NUM
ijpds-3748	18	5	]	]	PUNCT
ijpds-3748	18	6	.	.	PUNCT
ijpds-3748	19	1	empagliflozin	empagliflozin	PROPN
ijpds-3748	19	2	controls	control	VERB
ijpds-3748	19	3	the	the	DET
ijpds-3748	19	4	excess	excess	ADJ
ijpds-3748	19	5	glucose	glucose	NOUN
ijpds-3748	19	6	level	level	NOUN
ijpds-3748	19	7	in	in	ADP
ijpds-3748	19	8	the	the	DET
ijpds-3748	19	9	blood	blood	NOUN
ijpds-3748	19	10	.	.	PUNCT
ijpds-3748	20	1	it	it	PRON
ijpds-3748	20	2	is	be	AUX
ijpds-3748	20	3	an	an	DET
ijpds-3748	20	4	inhibitor	inhibitor	NOUN
ijpds-3748	20	5	of	of	ADP
ijpds-3748	20	6	sodiumglucose	sodiumglucose	NOUN
ijpds-3748	20	7	cotransporter-2(sglt-2	cotransporter-2(sglt-2	PROPN
ijpds-3748	20	8	)	)	PUNCT
ijpds-3748	20	9	and	and	CCONJ
ijpds-3748	20	10	promotes	promote	VERB
ijpds-3748	20	11	the	the	DET
ijpds-3748	20	12	excretion	excretion	NOUN
ijpds-3748	20	13	of	of	ADP
ijpds-3748	20	14	excess	excess	ADJ
ijpds-3748	20	15	glucose	glucose	NOUN
ijpds-3748	20	16	in	in	ADP
ijpds-3748	20	17	urine	urine	NOUN
ijpds-3748	20	18	by	by	ADP
ijpds-3748	20	19	reabsorbing	reabsorb	VERB
ijpds-3748	20	20	it	it	PRON
ijpds-3748	20	21	in	in	ADP
ijpds-3748	20	22	the	the	DET
ijpds-3748	20	23	kidney	kidney	NOUN
ijpds-3748	20	24	,	,	PUNCT
ijpds-3748	20	25	thus	thus	ADV
ijpds-3748	20	26	is	be	AUX
ijpds-3748	20	27	used	use	VERB
ijpds-3748	20	28	in	in	ADP
ijpds-3748	20	29	the	the	DET
ijpds-3748	20	30	treatment	treatment	NOUN
ijpds-3748	20	31	of	of	ADP
ijpds-3748	20	32	type	type	NOUN
ijpds-3748	20	33	2	2	NUM
ijpds-3748	20	34	diabetes	diabetes	NOUN
ijpds-3748	20	35	.	.	PUNCT
ijpds-3748	21	1	[	[	X
ijpds-3748	21	2	1,3	1,3	NUM
ijpds-3748	21	3	-	-	SYM
ijpds-3748	21	4	4	4	NUM
ijpds-3748	21	5	]	]	PUNCT
ijpds-3748	21	6	.	.	PUNCT
ijpds-3748	22	1	the	the	DET
ijpds-3748	22	2	empirical	empirical	ADJ
ijpds-3748	22	3	formula	formula	NOUN
ijpds-3748	22	4	of	of	ADP
ijpds-3748	22	5	empagliflozin	empagliflozin	PROPN
ijpds-3748	22	6	is	be	AUX
ijpds-3748	22	7	c23h27clo7	c23h27clo7	ADJ
ijpds-3748	22	8	and	and	CCONJ
ijpds-3748	22	9	its	its	PRON
ijpds-3748	22	10	molecular	molecular	ADJ
ijpds-3748	22	11	mass	mass	NOUN
ijpds-3748	22	12	is	be	AUX
ijpds-3748	22	13	450.91	450.91	NUM
ijpds-3748	22	14	a.m.u	a.m.u	NOUN
ijpds-3748	23	1	[	[	X
ijpds-3748	23	2	5	5	NUM
ijpds-3748	23	3	-	-	SYM
ijpds-3748	23	4	6	6	NUM
ijpds-3748	23	5	]	]	PUNCT
ijpds-3748	23	6	.	.	PUNCT
ijpds-3748	24	1	empagliflozin	empagliflozin	PROPN
ijpds-3748	24	2	is	be	AUX
ijpds-3748	24	3	available	available	ADJ
ijpds-3748	24	4	in	in	ADP
ijpds-3748	24	5	10	10	NUM
ijpds-3748	24	6	mg	mg	NOUN
ijpds-3748	24	7	and	and	CCONJ
ijpds-3748	24	8	25	25	NUM
ijpds-3748	24	9	mg	mg	PROPN
ijpds-3748	24	10	oral	oral	ADJ
ijpds-3748	24	11	tablet	tablet	NOUN
ijpds-3748	24	12	dosage	dosage	NOUN
ijpds-3748	24	13	forms	form	NOUN
ijpds-3748	24	14	alone	alone	ADJ
ijpds-3748	24	15	or	or	CCONJ
ijpds-3748	24	16	in	in	ADP
ijpds-3748	24	17	combination	combination	NOUN
ijpds-3748	24	18	with	with	ADP
ijpds-3748	24	19	other	other	ADJ
ijpds-3748	24	20	drugs	drug	NOUN
ijpds-3748	24	21	.	.	PUNCT
ijpds-3748	25	1	jardiance	jardiance	NOUN
ijpds-3748	25	2	,	,	PUNCT
ijpds-3748	25	3	glyxambi	glyxambi	NOUN
ijpds-3748	25	4	,	,	PUNCT
ijpds-3748	25	5	synjardy	synjardy	NOUN
ijpds-3748	25	6	,	,	PUNCT
ijpds-3748	25	7	and	and	CCONJ
ijpds-3748	25	8	synjardy	synjardy	NOUN
ijpds-3748	25	9	xr	xr	PROPN
ijpds-3748	25	10	are	be	AUX
ijpds-3748	25	11	examples	example	NOUN
ijpds-3748	25	12	of	of	ADP
ijpds-3748	25	13	empagliflozin	empagliflozin	PROPN
ijpds-3748	25	14	tablets	tablet	NOUN
ijpds-3748	25	15	[	[	PUNCT
ijpds-3748	25	16	7	7	NUM
ijpds-3748	25	17	-	-	SYM
ijpds-3748	25	18	10	10	NUM
ijpds-3748	25	19	]	]	PUNCT
ijpds-3748	25	20	.	.	PUNCT
ijpds-3748	26	1	figure	figure	NOUN
ijpds-3748	26	2	1	1	NUM
ijpds-3748	26	3	–	–	PUNCT
ijpds-3748	26	4	structure	structure	NOUN
ijpds-3748	26	5	of	of	ADP
ijpds-3748	26	6	empagliflozin	empagliflozin	PROPN
ijpds-3748	26	7	the	the	DET
ijpds-3748	26	8	development	development	NOUN
ijpds-3748	26	9	of	of	ADP
ijpds-3748	26	10	a	a	DET
ijpds-3748	26	11	quantitative	quantitative	ADJ
ijpds-3748	26	12	method	method	NOUN
ijpds-3748	26	13	and	and	CCONJ
ijpds-3748	26	14	its	its	PRON
ijpds-3748	26	15	validation	validation	NOUN
ijpds-3748	26	16	are	be	AUX
ijpds-3748	26	17	fundamental	fundamental	ADJ
ijpds-3748	26	18	and	and	CCONJ
ijpds-3748	26	19	essential	essential	ADJ
ijpds-3748	26	20	phases	phase	NOUN
ijpds-3748	26	21	in	in	ADP
ijpds-3748	26	22	pharmaceutical	pharmaceutical	ADJ
ijpds-3748	26	23	analysis	analysis	NOUN
ijpds-3748	26	24	to	to	PART
ijpds-3748	26	25	ensure	ensure	VERB
ijpds-3748	26	26	that	that	SCONJ
ijpds-3748	26	27	the	the	DET
ijpds-3748	26	28	results	result	NOUN
ijpds-3748	26	29	of	of	ADP
ijpds-3748	26	30	the	the	DET
ijpds-3748	26	31	proposed	propose	VERB
ijpds-3748	26	32	technique	technique	NOUN
ijpds-3748	26	33	are	be	AUX
ijpds-3748	26	34	trustworthy	trustworthy	ADJ
ijpds-3748	26	35	,	,	PUNCT
ijpds-3748	26	36	accurate	accurate	ADJ
ijpds-3748	26	37	,	,	PUNCT
ijpds-3748	26	38	suitable	suitable	ADJ
ijpds-3748	26	39	,	,	PUNCT
ijpds-3748	26	40	and	and	CCONJ
ijpds-3748	26	41	robust	robust	ADJ
ijpds-3748	26	42	for	for	ADP
ijpds-3748	26	43	everyday	everyday	ADJ
ijpds-3748	26	44	application	application	NOUN
ijpds-3748	26	45	.	.	PUNCT
ijpds-3748	27	1	the	the	DET
ijpds-3748	27	2	literature	literature	PROPN
ijpds-3748	27	3	review	review	NOUN
ijpds-3748	27	4	revealed	reveal	VERB
ijpds-3748	27	5	that	that	SCONJ
ijpds-3748	27	6	empagliflozin	empagliflozin	PROPN
ijpds-3748	27	7	can	can	AUX
ijpds-3748	27	8	be	be	AUX
ijpds-3748	27	9	detected	detect	VERB
ijpds-3748	27	10	both	both	CCONJ
ijpds-3748	27	11	qualitatively	qualitatively	ADV
ijpds-3748	27	12	and	and	CCONJ
ijpds-3748	27	13	quantitatively	quantitatively	ADV
ijpds-3748	27	14	by	by	ADP
ijpds-3748	27	15	using	use	VERB
ijpds-3748	27	16	liquid	liquid	ADJ
ijpds-3748	27	17	chromatography	chromatography	NOUN
ijpds-3748	27	18	(	(	PUNCT
ijpds-3748	27	19	lc	lc	PROPN
ijpds-3748	27	20	)	)	PUNCT
ijpds-3748	27	21	,	,	PUNCT
ijpds-3748	27	22	ultraviolet	ultraviolet	ADJ
ijpds-3748	27	23	spectrophotometer	spectrophotometer	NOUN
ijpds-3748	27	24	(	(	PUNCT
ijpds-3748	27	25	uv	uv	NOUN
ijpds-3748	27	26	)	)	PUNCT
ijpds-3748	27	27	,	,	PUNCT
ijpds-3748	27	28	high	high	ADJ
ijpds-3748	27	29	-	-	PUNCT
ijpds-3748	27	30	performance	performance	NOUN
ijpds-3748	27	31	liquid	liquid	ADJ
ijpds-3748	27	32	chromatography	chromatography	NOUN
ijpds-3748	27	33	(	(	PUNCT
ijpds-3748	27	34	hplc	hplc	PROPN
ijpds-3748	27	35	)	)	PUNCT
ijpds-3748	27	36	,	,	PUNCT
ijpds-3748	27	37	and	and	CCONJ
ijpds-3748	27	38	ultra	ultra	ADJ
ijpds-3748	27	39	performance	performance	NOUN
ijpds-3748	27	40	liquid	liquid	ADJ
ijpds-3748	27	41	chromatography	chromatography	NOUN
ijpds-3748	27	42	(	(	PUNCT
ijpds-3748	27	43	uplc	uplc	ADJ
ijpds-3748	27	44	)	)	PUNCT
ijpds-3748	27	45	techniques	technique	NOUN
ijpds-3748	27	46	[	[	X
ijpds-3748	27	47	11	11	NUM
ijpds-3748	27	48	-	-	SYM
ijpds-3748	27	49	15	15	NUM
ijpds-3748	27	50	]	]	PUNCT
ijpds-3748	27	51	.	.	PUNCT
ijpds-3748	28	1	however	however	ADV
ijpds-3748	28	2	,	,	PUNCT
ijpds-3748	28	3	few	few	ADJ
ijpds-3748	28	4	reports	report	NOUN
ijpds-3748	28	5	are	be	AUX
ijpds-3748	28	6	available	available	ADJ
ijpds-3748	28	7	for	for	ADP
ijpds-3748	28	8	the	the	DET
ijpds-3748	28	9	rp	rp	NOUN
ijpds-3748	28	10	-	-	PUNCT
ijpds-3748	28	11	hplc	hplc	NOUN
ijpds-3748	28	12	measurement	measurement	NOUN
ijpds-3748	28	13	of	of	ADP
ijpds-3748	28	14	empagliflozin	empagliflozin	PROPN
ijpds-3748	28	15	in	in	ADP
ijpds-3748	28	16	pharmaceutical	pharmaceutical	ADJ
ijpds-3748	28	17	preparations	preparation	NOUN
ijpds-3748	28	18	.	.	PUNCT
ijpds-3748	29	1	in	in	ADP
ijpds-3748	29	2	this	this	DET
ijpds-3748	29	3	article	article	NOUN
ijpds-3748	29	4	,	,	PUNCT
ijpds-3748	29	5	we	we	PRON
ijpds-3748	29	6	discussed	discuss	VERB
ijpds-3748	29	7	the	the	DET
ijpds-3748	29	8	validation	validation	NOUN
ijpds-3748	29	9	of	of	ADP
ijpds-3748	29	10	a	a	DET
ijpds-3748	29	11	novel	novel	ADJ
ijpds-3748	29	12	technique	technique	NOUN
ijpds-3748	29	13	for	for	ADP
ijpds-3748	29	14	precise	precise	ADJ
ijpds-3748	29	15	empagliflozin	empagliflozin	NOUN
ijpds-3748	29	16	quantification	quantification	NOUN
ijpds-3748	29	17	in	in	ADP
ijpds-3748	29	18	pharmaceutical	pharmaceutical	ADJ
ijpds-3748	29	19	dosage	dosage	NOUN
ijpds-3748	29	20	forms	form	NOUN
ijpds-3748	29	21	and	and	CCONJ
ijpds-3748	29	22	bulk	bulk	ADJ
ijpds-3748	29	23	pharmaceuticals	pharmaceutical	NOUN
ijpds-3748	29	24	.	.	PUNCT
ijpds-3748	30	1	the	the	DET
ijpds-3748	30	2	validation	validation	NOUN
ijpds-3748	30	3	is	be	AUX
ijpds-3748	30	4	important	important	ADJ
ijpds-3748	30	5	as	as	SCONJ
ijpds-3748	30	6	drug	drug	NOUN
ijpds-3748	30	7	regulatory	regulatory	ADJ
ijpds-3748	30	8	governing	governing	NOUN
ijpds-3748	30	9	bodies	body	NOUN
ijpds-3748	30	10	play	play	VERB
ijpds-3748	30	11	a	a	DET
ijpds-3748	30	12	vital	vital	ADJ
ijpds-3748	30	13	role	role	NOUN
ijpds-3748	30	14	and	and	CCONJ
ijpds-3748	30	15	have	have	AUX
ijpds-3748	30	16	placed	place	VERB
ijpds-3748	30	17	emphasis	emphasis	NOUN
ijpds-3748	30	18	on	on	ADP
ijpds-3748	30	19	drug	drug	NOUN
ijpds-3748	30	20	manufacturing	manufacturing	NOUN
ijpds-3748	30	21	companies	company	NOUN
ijpds-3748	30	22	to	to	PART
ijpds-3748	30	23	offer	offer	VERB
ijpds-3748	30	24	comprehensive	comprehensive	ADJ
ijpds-3748	30	25	information	information	NOUN
ijpds-3748	30	26	regarding	regard	VERB
ijpds-3748	30	27	the	the	DET
ijpds-3748	30	28	process	process	NOUN
ijpds-3748	30	29	for	for	ADP
ijpds-3748	30	30	the	the	DET
ijpds-3748	30	31	validation	validation	NOUN
ijpds-3748	30	32	of	of	ADP
ijpds-3748	30	33	analytical	analytical	ADJ
ijpds-3748	30	34	methods	method	NOUN
ijpds-3748	30	35	c	c	PROPN
ijpds-3748	30	36	mailto:zahra.maryam489@gmail.com	mailto:zahra.maryam489@gmail.com	PROPN
ijpds-3748	30	37	ahmad	ahmad	PROPN
ijpds-3748	30	38	et	et	PROPN
ijpds-3748	30	39	al	al	PROPN
ijpds-3748	30	40	rp	rp	PROPN
ijpds-3748	30	41	-	-	PUNCT
ijpds-3748	30	42	hplc	hplc	NOUN
ijpds-3748	30	43	method	method	NOUN
ijpds-3748	30	44	validation	validation	NOUN
ijpds-3748	30	45	of	of	ADP
ijpds-3748	30	46	empagliflozin	empagliflozin	PROPN
ijpds-3748	30	47	vol	vol	NOUN
ijpds-3748	30	48	2	2	NUM
ijpds-3748	30	49	|	|	NOUN
ijpds-3748	30	50	issue	issue	NOUN
ijpds-3748	30	51	2	2	NUM
ijpds-3748	30	52	|	|	ADV
ijpds-3748	30	53	apr	apr	ADV
ijpds-3748	30	54	–	–	PUNCT
ijpds-3748	30	55	jun	jun	PROPN
ijpds-3748	30	56	2023	2023	NUM
ijpds-3748	30	57	indian	indian	PROPN
ijpds-3748	30	58	j	j	PROPN
ijpds-3748	30	59	pharm	pharm	PROPN
ijpds-3748	30	60	drug	drug	PROPN
ijpds-3748	30	61	studies	study	NOUN
ijpds-3748	30	62	|	|	ADV
ijpds-3748	30	63	77	77	NUM
ijpds-3748	31	1	[	[	X
ijpds-3748	31	2	15	15	NUM
ijpds-3748	31	3	]	]	PUNCT
ijpds-3748	31	4	.	.	PUNCT
ijpds-3748	32	1	we	we	PRON
ijpds-3748	32	2	performed	perform	VERB
ijpds-3748	32	3	the	the	DET
ijpds-3748	32	4	validation	validation	NOUN
ijpds-3748	32	5	in	in	ADP
ijpds-3748	32	6	accordance	accordance	NOUN
ijpds-3748	32	7	with	with	ADP
ijpds-3748	32	8	ich	ich	NOUN
ijpds-3748	32	9	[	[	X
ijpds-3748	32	10	1618	1618	NUM
ijpds-3748	32	11	]	]	PUNCT
ijpds-3748	32	12	.	.	PUNCT
ijpds-3748	33	1	the	the	DET
ijpds-3748	33	2	current	current	ADJ
ijpds-3748	33	3	strategy	strategy	NOUN
ijpds-3748	33	4	,	,	PUNCT
ijpds-3748	33	5	which	which	PRON
ijpds-3748	33	6	is	be	AUX
ijpds-3748	33	7	brand	brand	NOUN
ijpds-3748	33	8	-	-	PUNCT
ijpds-3748	33	9	new	new	ADJ
ijpds-3748	33	10	to	to	ADP
ijpds-3748	33	11	the	the	DET
ijpds-3748	33	12	market	market	NOUN
ijpds-3748	33	13	,	,	PUNCT
ijpds-3748	33	14	uses	use	VERB
ijpds-3748	33	15	several	several	ADJ
ijpds-3748	33	16	mobile	mobile	ADJ
ijpds-3748	33	17	phase	phase	NOUN
ijpds-3748	33	18	compositions	composition	NOUN
ijpds-3748	33	19	to	to	PART
ijpds-3748	33	20	estimate	estimate	VERB
ijpds-3748	33	21	empagliflozin	empagliflozin	PROPN
ijpds-3748	33	22	in	in	ADP
ijpds-3748	33	23	a	a	DET
ijpds-3748	33	24	quality	quality	NOUN
ijpds-3748	33	25	control	control	NOUN
ijpds-3748	33	26	laboratory	laboratory	NOUN
ijpds-3748	33	27	.	.	PUNCT
ijpds-3748	34	1	in	in	ADP
ijpds-3748	34	2	accordance	accordance	NOUN
ijpds-3748	34	3	with	with	ADP
ijpds-3748	34	4	the	the	DET
ijpds-3748	34	5	recommendations	recommendation	NOUN
ijpds-3748	34	6	of	of	ADP
ijpds-3748	34	7	the	the	DET
ijpds-3748	34	8	international	international	ADJ
ijpds-3748	34	9	council	council	NOUN
ijpds-3748	34	10	for	for	ADP
ijpds-3748	34	11	harmonization	harmonization	NOUN
ijpds-3748	34	12	,	,	PUNCT
ijpds-3748	34	13	the	the	DET
ijpds-3748	34	14	method	method	NOUN
ijpds-3748	34	15	's	's	PART
ijpds-3748	34	16	performance	performance	NOUN
ijpds-3748	34	17	was	be	AUX
ijpds-3748	34	18	validated	validate	VERB
ijpds-3748	34	19	.	.	PUNCT
ijpds-3748	35	1	this	this	DET
ijpds-3748	35	2	study	study	NOUN
ijpds-3748	35	3	was	be	AUX
ijpds-3748	35	4	conducted	conduct	VERB
ijpds-3748	35	5	to	to	PART
ijpds-3748	35	6	develop	develop	VERB
ijpds-3748	35	7	and	and	CCONJ
ijpds-3748	35	8	validate	validate	VERB
ijpds-3748	35	9	the	the	DET
ijpds-3748	35	10	novel	novel	NOUN
ijpds-3748	35	11	,	,	PUNCT
ijpds-3748	35	12	accurate	accurate	ADJ
ijpds-3748	35	13	,	,	PUNCT
ijpds-3748	35	14	precise	precise	ADJ
ijpds-3748	35	15	,	,	PUNCT
ijpds-3748	35	16	and	and	CCONJ
ijpds-3748	35	17	stability	stability	NOUN
ijpds-3748	35	18	-	-	PUNCT
ijpds-3748	35	19	indicating	indicate	VERB
ijpds-3748	35	20	rp	rp	NOUN
ijpds-3748	35	21	-	-	PUNCT
ijpds-3748	35	22	hplc	hplc	NOUN
ijpds-3748	35	23	method	method	NOUN
ijpds-3748	35	24	for	for	ADP
ijpds-3748	35	25	the	the	DET
ijpds-3748	35	26	analysis	analysis	NOUN
ijpds-3748	35	27	of	of	ADP
ijpds-3748	35	28	empagliflozin	empagliflozin	PROPN
ijpds-3748	35	29	in	in	ADP
ijpds-3748	35	30	bulk	bulk	ADJ
ijpds-3748	35	31	granules	granule	NOUN
ijpds-3748	35	32	and	and	CCONJ
ijpds-3748	35	33	tablets	tablet	NOUN
ijpds-3748	35	34	.	.	PUNCT
ijpds-3748	36	1	in	in	ADP
ijpds-3748	36	2	the	the	DET
ijpds-3748	36	3	development	development	NOUN
ijpds-3748	36	4	stage	stage	NOUN
ijpds-3748	36	5	,	,	PUNCT
ijpds-3748	36	6	the	the	DET
ijpds-3748	36	7	wavelength	wavelength	NOUN
ijpds-3748	36	8	detection	detection	NOUN
ijpds-3748	36	9	study	study	NOUN
ijpds-3748	36	10	was	be	AUX
ijpds-3748	36	11	conducted	conduct	VERB
ijpds-3748	36	12	by	by	ADP
ijpds-3748	36	13	scanning	scan	VERB
ijpds-3748	36	14	the	the	DET
ijpds-3748	36	15	sample	sample	NOUN
ijpds-3748	36	16	between	between	ADP
ijpds-3748	36	17	200	200	NUM
ijpds-3748	36	18	nm	nm	NOUN
ijpds-3748	36	19	and	and	CCONJ
ijpds-3748	36	20	400	400	NUM
ijpds-3748	36	21	nm	nm	NOUN
ijpds-3748	36	22	.	.	PUNCT
ijpds-3748	37	1	a	a	DET
ijpds-3748	37	2	major	major	ADJ
ijpds-3748	37	3	peak	peak	NOUN
ijpds-3748	37	4	was	be	AUX
ijpds-3748	37	5	found	find	VERB
ijpds-3748	37	6	at	at	ADP
ijpds-3748	37	7	224	224	NUM
ijpds-3748	37	8	nm	nm	NOUN
ijpds-3748	37	9	(	(	PUNCT
ijpds-3748	37	10	λ	λ	X
ijpds-3748	37	11	max	max	PROPN
ijpds-3748	37	12	)	)	PUNCT
ijpds-3748	37	13	.	.	PUNCT
ijpds-3748	38	1	then	then	ADV
ijpds-3748	38	2	the	the	DET
ijpds-3748	38	3	method	method	NOUN
ijpds-3748	38	4	was	be	AUX
ijpds-3748	38	5	validated	validate	VERB
ijpds-3748	38	6	for	for	ADP
ijpds-3748	38	7	validation	validation	NOUN
ijpds-3748	38	8	parameters	parameter	NOUN
ijpds-3748	38	9	i	i	PROPN
ijpds-3748	38	10	-	-	PUNCT
ijpds-3748	38	11	e	e	NOUN
ijpds-3748	38	12	accuracy	accuracy	NOUN
ijpds-3748	38	13	,	,	PUNCT
ijpds-3748	38	14	precision	precision	NOUN
ijpds-3748	38	15	(	(	PUNCT
ijpds-3748	38	16	repeatability	repeatability	NOUN
ijpds-3748	38	17	,	,	PUNCT
ijpds-3748	38	18	intermediate	intermediate	ADJ
ijpds-3748	38	19	precision	precision	NOUN
ijpds-3748	38	20	)	)	PUNCT
ijpds-3748	38	21	,	,	PUNCT
ijpds-3748	38	22	specificity	specificity	NOUN
ijpds-3748	38	23	,	,	PUNCT
ijpds-3748	38	24	the	the	DET
ijpds-3748	38	25	limit	limit	NOUN
ijpds-3748	38	26	of	of	ADP
ijpds-3748	38	27	detection	detection	NOUN
ijpds-3748	38	28	,	,	PUNCT
ijpds-3748	38	29	the	the	DET
ijpds-3748	38	30	limit	limit	NOUN
ijpds-3748	38	31	of	of	ADP
ijpds-3748	38	32	quantification	quantification	NOUN
ijpds-3748	38	33	,	,	PUNCT
ijpds-3748	38	34	linearity	linearity	NOUN
ijpds-3748	38	35	,	,	PUNCT
ijpds-3748	38	36	range	range	NOUN
ijpds-3748	38	37	,	,	PUNCT
ijpds-3748	38	38	and	and	CCONJ
ijpds-3748	38	39	robustness	robustness	NOUN
ijpds-3748	38	40	as	as	ADP
ijpds-3748	38	41	per	per	ADP
ijpds-3748	38	42	ich	ich	NOUN
ijpds-3748	38	43	and	and	CCONJ
ijpds-3748	38	44	united	united	PROPN
ijpds-3748	38	45	states	states	PROPN
ijpds-3748	38	46	pharmacopeia	pharmacopeia	PROPN
ijpds-3748	38	47	(	(	PUNCT
ijpds-3748	38	48	usp	usp	NOUN
ijpds-3748	38	49	)	)	PUNCT
ijpds-3748	38	50	guidelines	guideline	NOUN
ijpds-3748	38	51	using	use	VERB
ijpds-3748	38	52	hplc	hplc	NOUN
ijpds-3748	38	53	[	[	X
ijpds-3748	38	54	11	11	NUM
ijpds-3748	38	55	,	,	PUNCT
ijpds-3748	38	56	19	19	NUM
ijpds-3748	38	57	]	]	PUNCT
ijpds-3748	38	58	.	.	PUNCT
ijpds-3748	39	1	stress	stress	PROPN
ijpds-3748	39	2	study	study	NOUN
ijpds-3748	39	3	was	be	AUX
ijpds-3748	39	4	performed	perform	VERB
ijpds-3748	39	5	in	in	ADP
ijpds-3748	39	6	acid	acid	NOUN
ijpds-3748	39	7	,	,	PUNCT
ijpds-3748	39	8	base	base	NOUN
ijpds-3748	39	9	,	,	PUNCT
ijpds-3748	39	10	peroxide	peroxide	NOUN
ijpds-3748	39	11	solutions	solution	NOUN
ijpds-3748	39	12	,	,	PUNCT
ijpds-3748	39	13	thermal	thermal	ADJ
ijpds-3748	39	14	,	,	PUNCT
ijpds-3748	39	15	and	and	CCONJ
ijpds-3748	39	16	photolytic	photolytic	ADJ
ijpds-3748	39	17	stress	stress	NOUN
ijpds-3748	39	18	conditions	condition	NOUN
ijpds-3748	39	19	to	to	PART
ijpds-3748	39	20	check	check	VERB
ijpds-3748	39	21	the	the	DET
ijpds-3748	39	22	stability	stability	NOUN
ijpds-3748	39	23	of	of	ADP
ijpds-3748	39	24	dosage	dosage	NOUN
ijpds-3748	39	25	form	form	NOUN
ijpds-3748	39	26	as	as	ADV
ijpds-3748	39	27	well	well	ADV
ijpds-3748	39	28	as	as	ADP
ijpds-3748	39	29	the	the	DET
ijpds-3748	39	30	robustness	robustness	NOUN
ijpds-3748	39	31	of	of	ADP
ijpds-3748	39	32	the	the	DET
ijpds-3748	39	33	method	method	NOUN
ijpds-3748	39	34	[	[	X
ijpds-3748	39	35	20	20	NUM
ijpds-3748	39	36	-	-	SYM
ijpds-3748	39	37	21	21	NUM
ijpds-3748	39	38	]	]	PUNCT
ijpds-3748	39	39	.	.	PUNCT
ijpds-3748	40	1	materials	material	NOUN
ijpds-3748	40	2	and	and	CCONJ
ijpds-3748	40	3	methods	method	NOUN
ijpds-3748	40	4	all	all	DET
ijpds-3748	40	5	the	the	DET
ijpds-3748	40	6	chemicals	chemical	NOUN
ijpds-3748	40	7	,	,	PUNCT
ijpds-3748	40	8	methanol	methanol	NOUN
ijpds-3748	40	9	,	,	PUNCT
ijpds-3748	40	10	acetonitrile	acetonitrile	NOUN
ijpds-3748	40	11	,	,	PUNCT
ijpds-3748	40	12	hydrochloric	hydrochloric	ADJ
ijpds-3748	40	13	acid	acid	NOUN
ijpds-3748	40	14	,	,	PUNCT
ijpds-3748	40	15	hydrogen	hydrogen	NOUN
ijpds-3748	40	16	peroxide	peroxide	NOUN
ijpds-3748	40	17	,	,	PUNCT
ijpds-3748	40	18	sodium	sodium	NOUN
ijpds-3748	40	19	hydroxide	hydroxide	NOUN
ijpds-3748	40	20	,	,	PUNCT
ijpds-3748	40	21	and	and	CCONJ
ijpds-3748	40	22	monobasic	monobasic	ADJ
ijpds-3748	40	23	hydrogen	hydrogen	NOUN
ijpds-3748	40	24	phosphate	phosphate	NOUN
ijpds-3748	40	25	were	be	AUX
ijpds-3748	40	26	purchased	purchase	VERB
ijpds-3748	40	27	from	from	ADP
ijpds-3748	40	28	science	science	NOUN
ijpds-3748	40	29	center	center	PROPN
ijpds-3748	40	30	merk	merk	PROPN
ijpds-3748	40	31	distributor	distributor	PROPN
ijpds-3748	40	32	islamabad	islamabad	PROPN
ijpds-3748	40	33	.	.	PUNCT
ijpds-3748	41	1	all	all	DET
ijpds-3748	41	2	the	the	DET
ijpds-3748	41	3	chemicals	chemical	NOUN
ijpds-3748	41	4	were	be	AUX
ijpds-3748	41	5	used	use	VERB
ijpds-3748	41	6	without	without	ADP
ijpds-3748	41	7	any	any	DET
ijpds-3748	41	8	further	further	ADJ
ijpds-3748	41	9	purification	purification	NOUN
ijpds-3748	41	10	.	.	PUNCT
ijpds-3748	42	1	instrumentation	instrumentation	NOUN
ijpds-3748	42	2	:	:	PUNCT
ijpds-3748	42	3	gradient	gradient	NOUN
ijpds-3748	42	4	hplc	hplc	NOUN
ijpds-3748	42	5	model	model	NOUN
ijpds-3748	42	6	lc20	lc20	PROPN
ijpds-3748	42	7	(	(	PUNCT
ijpds-3748	42	8	shimadzu	shimadzu	PROPN
ijpds-3748	42	9	japan	japan	PROPN
ijpds-3748	42	10	)	)	PUNCT
ijpds-3748	42	11	(	(	PUNCT
ijpds-3748	42	12	lc20at	lc20at	NOUN
ijpds-3748	42	13	)	)	PUNCT
ijpds-3748	42	14	equipped	equip	VERB
ijpds-3748	42	15	with	with	ADP
ijpds-3748	42	16	pda	pda	NOUN
ijpds-3748	42	17	detector	detector	NOUN
ijpds-3748	42	18	(	(	PUNCT
ijpds-3748	42	19	spd	spd	NOUN
ijpds-3748	42	20	m-20a	m-20a	NOUN
ijpds-3748	42	21	)	)	PUNCT
ijpds-3748	42	22	,	,	PUNCT
ijpds-3748	42	23	autosampler	autosampler	NOUN
ijpds-3748	42	24	(	(	PUNCT
ijpds-3748	42	25	sil-20aht	sil-20aht	PROPN
ijpds-3748	42	26	)	)	PUNCT
ijpds-3748	42	27	,	,	PUNCT
ijpds-3748	42	28	column	column	NOUN
ijpds-3748	42	29	oven	oven	NOUN
ijpds-3748	42	30	(	(	PUNCT
ijpds-3748	42	31	cto-20a	cto-20a	NUM
ijpds-3748	42	32	)	)	PUNCT
ijpds-3748	42	33	and	and	CCONJ
ijpds-3748	42	34	degassing	degas	VERB
ijpds-3748	42	35	unit	unit	NOUN
ijpds-3748	42	36	(	(	PUNCT
ijpds-3748	42	37	dgu-20asr	dgu-20asr	PROPN
ijpds-3748	42	38	)	)	PUNCT
ijpds-3748	42	39	was	be	AUX
ijpds-3748	42	40	used	use	VERB
ijpds-3748	42	41	for	for	ADP
ijpds-3748	42	42	the	the	DET
ijpds-3748	42	43	study	study	NOUN
ijpds-3748	42	44	.	.	PUNCT
ijpds-3748	43	1	computer	computer	NOUN
ijpds-3748	43	2	-	-	PUNCT
ijpds-3748	43	3	supported	support	VERB
ijpds-3748	43	4	software	software	NOUN
ijpds-3748	43	5	-	-	PUNCT
ijpds-3748	43	6	based	base	VERB
ijpds-3748	43	7	spectrophotometer	spectrophotometer	NOUN
ijpds-3748	43	8	model	model	NOUN
ijpds-3748	43	9	1800	1800	NUM
ijpds-3748	43	10	(	(	PUNCT
ijpds-3748	43	11	shimadzu	shimadzu	PROPN
ijpds-3748	43	12	japan	japan	PROPN
ijpds-3748	43	13	)	)	PUNCT
ijpds-3748	43	14	for	for	ADP
ijpds-3748	43	15	wavelength	wavelength	NOUN
ijpds-3748	43	16	detection	detection	NOUN
ijpds-3748	43	17	and	and	CCONJ
ijpds-3748	43	18	ft	ft	PROPN
ijpds-3748	43	19	-	-	PUNCT
ijpds-3748	43	20	ir	ir	PROPN
ijpds-3748	43	21	model	model	NOUN
ijpds-3748	43	22	alpha	alpha	NOUN
ijpds-3748	43	23	(	(	PUNCT
ijpds-3748	43	24	germany	germany	PROPN
ijpds-3748	43	25	)	)	PUNCT
ijpds-3748	43	26	with	with	ADP
ijpds-3748	43	27	atr	atr	PROPN
ijpds-3748	43	28	diamond	diamond	NOUN
ijpds-3748	43	29	atr	atr	NOUN
ijpds-3748	43	30	module	module	NOUN
ijpds-3748	43	31	for	for	ADP
ijpds-3748	43	32	identification	identification	NOUN
ijpds-3748	43	33	of	of	ADP
ijpds-3748	43	34	empagliflozin	empagliflozin	PROPN
ijpds-3748	43	35	were	be	AUX
ijpds-3748	43	36	employed	employ	VERB
ijpds-3748	43	37	.	.	PUNCT
ijpds-3748	44	1	calibrated	calibrate	VERB
ijpds-3748	44	2	analytical	analytical	ADJ
ijpds-3748	44	3	balance	balance	NOUN
ijpds-3748	44	4	metler	metler	NOUN
ijpds-3748	44	5	tolendo	tolendo	NOUN
ijpds-3748	44	6	was	be	AUX
ijpds-3748	44	7	used	use	VERB
ijpds-3748	44	8	for	for	ADP
ijpds-3748	44	9	weighing	weigh	VERB
ijpds-3748	44	10	purposes	purpose	NOUN
ijpds-3748	44	11	.	.	PUNCT
ijpds-3748	45	1	ph	ph	ADJ
ijpds-3748	45	2	meter	meter	NOUN
ijpds-3748	45	3	was	be	AUX
ijpds-3748	45	4	served	serve	VERB
ijpds-3748	45	5	for	for	ADP
ijpds-3748	45	6	the	the	DET
ijpds-3748	45	7	adjustment	adjustment	NOUN
ijpds-3748	45	8	of	of	ADP
ijpds-3748	45	9	the	the	DET
ijpds-3748	45	10	ph	ph	NOUN
ijpds-3748	45	11	of	of	ADP
ijpds-3748	45	12	the	the	DET
ijpds-3748	45	13	buffer	buffer	NOUN
ijpds-3748	45	14	for	for	ADP
ijpds-3748	45	15	the	the	DET
ijpds-3748	45	16	mobile	mobile	ADJ
ijpds-3748	45	17	phase	phase	NOUN
ijpds-3748	45	18	.	.	PUNCT
ijpds-3748	46	1	a	a	DET
ijpds-3748	46	2	neutronic	neutronic	PROPN
ijpds-3748	46	3	photostability	photostability	NOUN
ijpds-3748	46	4	chamber	chamber	NOUN
ijpds-3748	46	5	was	be	AUX
ijpds-3748	46	6	used	use	VERB
ijpds-3748	46	7	for	for	ADP
ijpds-3748	46	8	the	the	DET
ijpds-3748	46	9	photostability	photostability	NOUN
ijpds-3748	46	10	study	study	NOUN
ijpds-3748	46	11	,	,	PUNCT
ijpds-3748	46	12	and	and	CCONJ
ijpds-3748	46	13	thermal	thermal	ADJ
ijpds-3748	46	14	degradation	degradation	NOUN
ijpds-3748	46	15	was	be	AUX
ijpds-3748	46	16	checked	check	VERB
ijpds-3748	46	17	using	use	VERB
ijpds-3748	46	18	a	a	DET
ijpds-3748	46	19	memart	memart	NOUN
ijpds-3748	46	20	oven	oven	VERB
ijpds-3748	46	21	.	.	PUNCT
ijpds-3748	47	1	an	an	DET
ijpds-3748	47	2	ultrasonic	ultrasonic	ADJ
ijpds-3748	47	3	bath	bath	NOUN
ijpds-3748	47	4	was	be	AUX
ijpds-3748	47	5	used	use	VERB
ijpds-3748	47	6	to	to	PART
ijpds-3748	47	7	dissolve	dissolve	VERB
ijpds-3748	47	8	the	the	DET
ijpds-3748	47	9	samples	sample	NOUN
ijpds-3748	47	10	.	.	PUNCT
ijpds-3748	48	1	chromatographic	chromatographic	ADJ
ijpds-3748	48	2	conditions	condition	NOUN
ijpds-3748	48	3	:	:	PUNCT
ijpds-3748	48	4	in	in	ADP
ijpds-3748	48	5	the	the	DET
ijpds-3748	48	6	isocratic	isocratic	ADJ
ijpds-3748	48	7	mobile	mobile	ADJ
ijpds-3748	48	8	phase	phase	NOUN
ijpds-3748	48	9	,	,	PUNCT
ijpds-3748	48	10	the	the	DET
ijpds-3748	48	11	mixture	mixture	NOUN
ijpds-3748	48	12	of	of	ADP
ijpds-3748	48	13	phosphate	phosphate	ADJ
ijpds-3748	48	14	buffer	buffer	NOUN
ijpds-3748	48	15	ph	ph	VERB
ijpds-3748	48	16	3.0	3.0	NUM
ijpds-3748	48	17	and	and	CCONJ
ijpds-3748	48	18	methanol	methanol	NOUN
ijpds-3748	48	19	in	in	ADP
ijpds-3748	48	20	the	the	DET
ijpds-3748	48	21	ratio	ratio	NOUN
ijpds-3748	48	22	of	of	ADP
ijpds-3748	48	23	70:30	70:30	NUM
ijpds-3748	48	24	with	with	ADP
ijpds-3748	48	25	a	a	DET
ijpds-3748	48	26	flow	flow	NOUN
ijpds-3748	48	27	rate	rate	NOUN
ijpds-3748	48	28	of	of	ADP
ijpds-3748	48	29	1.0	1.0	NUM
ijpds-3748	48	30	ml	ml	NOUN
ijpds-3748	48	31	/	/	SYM
ijpds-3748	48	32	minute	minute	NOUN
ijpds-3748	48	33	and	and	CCONJ
ijpds-3748	48	34	column	column	NOUN
ijpds-3748	48	35	temperature	temperature	NOUN
ijpds-3748	48	36	of	of	ADP
ijpds-3748	48	37	30	30	NUM
ijpds-3748	48	38	°	°	NUM
ijpds-3748	48	39	c	c	NOUN
ijpds-3748	48	40	was	be	AUX
ijpds-3748	48	41	used	use	VERB
ijpds-3748	48	42	.	.	PUNCT
ijpds-3748	49	1	the	the	DET
ijpds-3748	49	2	flow	flow	NOUN
ijpds-3748	49	3	rate	rate	NOUN
ijpds-3748	49	4	was	be	AUX
ijpds-3748	49	5	set	set	VERB
ijpds-3748	49	6	at	at	ADP
ijpds-3748	49	7	1.0	1.0	NUM
ijpds-3748	49	8	ml	ml	NOUN
ijpds-3748	49	9	/	/	SYM
ijpds-3748	49	10	minute	minute	NOUN
ijpds-3748	49	11	and	and	CCONJ
ijpds-3748	49	12	the	the	DET
ijpds-3748	49	13	column	column	NOUN
ijpds-3748	49	14	temperature	temperature	NOUN
ijpds-3748	49	15	was	be	AUX
ijpds-3748	49	16	kept	keep	VERB
ijpds-3748	49	17	at	at	ADP
ijpds-3748	49	18	30	30	NUM
ijpds-3748	49	19	°	°	NOUN
ijpds-3748	49	20	c	c	NOUN
ijpds-3748	49	21	.	.	PUNCT
ijpds-3748	50	1	we	we	PRON
ijpds-3748	50	2	kept	keep	VERB
ijpds-3748	50	3	the	the	DET
ijpds-3748	50	4	injection	injection	NOUN
ijpds-3748	50	5	volume	volume	NOUN
ijpds-3748	50	6	at	at	ADP
ijpds-3748	50	7	20	20	NUM
ijpds-3748	50	8	µl	µl	NOUN
ijpds-3748	50	9	.	.	PUNCT
ijpds-3748	51	1	the	the	DET
ijpds-3748	51	2	mobile	mobile	ADJ
ijpds-3748	51	3	phase	phase	NOUN
ijpds-3748	51	4	was	be	AUX
ijpds-3748	51	5	also	also	ADV
ijpds-3748	51	6	used	use	VERB
ijpds-3748	51	7	as	as	ADP
ijpds-3748	51	8	diluent	diluent	NOUN
ijpds-3748	51	9	and	and	CCONJ
ijpds-3748	51	10	chromatograms	chromatogram	NOUN
ijpds-3748	51	11	were	be	AUX
ijpds-3748	51	12	recorded	record	VERB
ijpds-3748	51	13	at	at	ADP
ijpds-3748	51	14	224	224	NUM
ijpds-3748	51	15	nm	nm	NOUN
ijpds-3748	51	16	.	.	PUNCT
ijpds-3748	52	1	the	the	DET
ijpds-3748	52	2	summary	summary	NOUN
ijpds-3748	52	3	of	of	ADP
ijpds-3748	52	4	chromatographic	chromatographic	ADJ
ijpds-3748	52	5	conditions	condition	NOUN
ijpds-3748	52	6	is	be	AUX
ijpds-3748	52	7	mentioned	mention	VERB
ijpds-3748	52	8	in	in	ADP
ijpds-3748	52	9	table	table	NOUN
ijpds-3748	52	10	1	1	NUM
ijpds-3748	52	11	.	.	PUNCT
ijpds-3748	52	12	table	table	NOUN
ijpds-3748	52	13	1	1	NUM
ijpds-3748	52	14	–	–	PUNCT
ijpds-3748	52	15	chromatographic	chromatographic	ADJ
ijpds-3748	52	16	conditions	condition	NOUN
ijpds-3748	52	17	preparation	preparation	NOUN
ijpds-3748	52	18	of	of	ADP
ijpds-3748	52	19	solutions	solution	NOUN
ijpds-3748	52	20	preparation	preparation	NOUN
ijpds-3748	52	21	of	of	ADP
ijpds-3748	52	22	mobile	mobile	ADJ
ijpds-3748	52	23	phase	phase	NOUN
ijpds-3748	52	24	:	:	PUNCT
ijpds-3748	52	25	6.8	6.8	NUM
ijpds-3748	52	26	grams	gram	NOUN
ijpds-3748	52	27	of	of	ADP
ijpds-3748	52	28	monobasic	monobasic	NOUN
ijpds-3748	52	29	potassium	potassium	NOUN
ijpds-3748	52	30	phosphate	phosphate	NOUN
ijpds-3748	52	31	was	be	AUX
ijpds-3748	52	32	dissolved	dissolve	VERB
ijpds-3748	52	33	in	in	ADP
ijpds-3748	52	34	900	900	NUM
ijpds-3748	52	35	ml	ml	ADV
ijpds-3748	52	36	deionized	deionize	VERB
ijpds-3748	52	37	water	water	NOUN
ijpds-3748	52	38	in	in	ADP
ijpds-3748	52	39	a	a	DET
ijpds-3748	52	40	1000ml	1000ml	ADJ
ijpds-3748	52	41	volumetric	volumetric	ADJ
ijpds-3748	52	42	flask	flask	NOUN
ijpds-3748	52	43	,	,	PUNCT
ijpds-3748	52	44	the	the	DET
ijpds-3748	52	45	ph	ph	NOUN
ijpds-3748	52	46	was	be	AUX
ijpds-3748	52	47	adjusted	adjust	VERB
ijpds-3748	52	48	to	to	ADP
ijpds-3748	52	49	3.0	3.0	NUM
ijpds-3748	52	50	with	with	ADP
ijpds-3748	52	51	orthophosphoric	orthophosphoric	ADJ
ijpds-3748	52	52	acid	acid	NOUN
ijpds-3748	52	53	and	and	CCONJ
ijpds-3748	52	54	the	the	DET
ijpds-3748	52	55	solution	solution	NOUN
ijpds-3748	52	56	was	be	AUX
ijpds-3748	52	57	filtered	filter	VERB
ijpds-3748	52	58	through	through	ADP
ijpds-3748	52	59	a	a	DET
ijpds-3748	52	60	0.5	0.5	NUM
ijpds-3748	52	61	-	-	PUNCT
ijpds-3748	52	62	micron	micron	NOUN
ijpds-3748	52	63	filter	filter	NOUN
ijpds-3748	52	64	and	and	CCONJ
ijpds-3748	52	65	degassed	degassed	ADJ
ijpds-3748	52	66	.	.	PUNCT
ijpds-3748	53	1	then	then	ADV
ijpds-3748	53	2	phosphate	phosphate	ADJ
ijpds-3748	53	3	buffer	buffer	NOUN
ijpds-3748	53	4	and	and	CCONJ
ijpds-3748	53	5	methanol	methanol	NOUN
ijpds-3748	53	6	were	be	AUX
ijpds-3748	53	7	mixed	mix	VERB
ijpds-3748	53	8	in	in	ADP
ijpds-3748	53	9	a	a	DET
ijpds-3748	53	10	ratio	ratio	NOUN
ijpds-3748	53	11	of	of	ADP
ijpds-3748	53	12	70:30	70:30	NUM
ijpds-3748	53	13	to	to	PART
ijpds-3748	53	14	make	make	VERB
ijpds-3748	53	15	the	the	DET
ijpds-3748	53	16	isocratic	isocratic	ADJ
ijpds-3748	53	17	mobile	mobile	ADJ
ijpds-3748	53	18	phase	phase	NOUN
ijpds-3748	53	19	.	.	PUNCT
ijpds-3748	54	1	preparation	preparation	NOUN
ijpds-3748	54	2	of	of	ADP
ijpds-3748	54	3	standard	standard	ADJ
ijpds-3748	54	4	solution	solution	NOUN
ijpds-3748	54	5	:	:	PUNCT
ijpds-3748	54	6	after	after	ADP
ijpds-3748	54	7	weighing	weigh	VERB
ijpds-3748	54	8	carefully	carefully	ADV
ijpds-3748	54	9	,	,	PUNCT
ijpds-3748	54	10	the	the	DET
ijpds-3748	54	11	empagliflozin	empagliflozin	PROPN
ijpds-3748	54	12	working	work	VERB
ijpds-3748	54	13	standard	standard	PROPN
ijpds-3748	54	14	equivalent	equivalent	ADJ
ijpds-3748	54	15	to	to	ADP
ijpds-3748	54	16	25	25	NUM
ijpds-3748	54	17	mg	mg	PROPN
ijpds-3748	54	18	,	,	PUNCT
ijpds-3748	54	19	was	be	AUX
ijpds-3748	54	20	dissolved	dissolve	VERB
ijpds-3748	54	21	in	in	ADP
ijpds-3748	54	22	a	a	DET
ijpds-3748	54	23	diluent	diluent	NOUN
ijpds-3748	54	24	in	in	ADP
ijpds-3748	54	25	50	50	NUM
ijpds-3748	54	26	ml	ml	NOUN
ijpds-3748	54	27	volumetric	volumetric	ADJ
ijpds-3748	54	28	flask	flask	NOUN
ijpds-3748	54	29	.	.	PUNCT
ijpds-3748	55	1	the	the	DET
ijpds-3748	55	2	solution	solution	NOUN
ijpds-3748	55	3	was	be	AUX
ijpds-3748	55	4	filtered	filter	VERB
ijpds-3748	55	5	and	and	CCONJ
ijpds-3748	55	6	2ml	2ml	NOUN
ijpds-3748	55	7	of	of	ADP
ijpds-3748	55	8	the	the	DET
ijpds-3748	55	9	filtrate	filtrate	NOUN
ijpds-3748	55	10	was	be	AUX
ijpds-3748	55	11	taken	take	VERB
ijpds-3748	55	12	to	to	ADP
ijpds-3748	55	13	50	50	NUM
ijpds-3748	55	14	ml	ml	NOUN
ijpds-3748	55	15	volumetric	volumetric	ADJ
ijpds-3748	55	16	flask	flask	NOUN
ijpds-3748	55	17	,	,	PUNCT
ijpds-3748	55	18	mixed	mix	VERB
ijpds-3748	55	19	well	well	ADV
ijpds-3748	55	20	,	,	PUNCT
ijpds-3748	55	21	and	and	CCONJ
ijpds-3748	55	22	the	the	DET
ijpds-3748	55	23	volume	volume	NOUN
ijpds-3748	55	24	was	be	AUX
ijpds-3748	55	25	made	make	VERB
ijpds-3748	55	26	with	with	ADP
ijpds-3748	55	27	diluent	diluent	NOUN
ijpds-3748	55	28	to	to	ADP
ijpds-3748	55	29	50	50	NUM
ijpds-3748	55	30	ml	ml	NOUN
ijpds-3748	55	31	and	and	CCONJ
ijpds-3748	55	32	sonicated	sonicate	VERB
ijpds-3748	55	33	for	for	ADP
ijpds-3748	55	34	5.0	5.0	NUM
ijpds-3748	55	35	minutes	minute	NOUN
ijpds-3748	55	36	.	.	PUNCT
ijpds-3748	56	1	preparation	preparation	NOUN
ijpds-3748	56	2	of	of	ADP
ijpds-3748	56	3	sample	sample	NOUN
ijpds-3748	56	4	solution	solution	NOUN
ijpds-3748	56	5	:	:	PUNCT
ijpds-3748	56	6	we	we	PRON
ijpds-3748	56	7	took	take	VERB
ijpds-3748	56	8	20	20	NUM
ijpds-3748	56	9	tablets	tablet	NOUN
ijpds-3748	56	10	,	,	PUNCT
ijpds-3748	56	11	weighed	weigh	VERB
ijpds-3748	56	12	,	,	PUNCT
ijpds-3748	56	13	and	and	CCONJ
ijpds-3748	56	14	powdered	powder	VERB
ijpds-3748	56	15	them	they	PRON
ijpds-3748	56	16	.	.	PUNCT
ijpds-3748	57	1	then	then	ADV
ijpds-3748	57	2	the	the	DET
ijpds-3748	57	3	powder	powder	NOUN
ijpds-3748	57	4	equivalent	equivalent	ADJ
ijpds-3748	57	5	to	to	ADP
ijpds-3748	57	6	25	25	NUM
ijpds-3748	57	7	mg	mg	PROPN
ijpds-3748	57	8	empagliflozin	empagliflozin	PROPN
ijpds-3748	57	9	was	be	AUX
ijpds-3748	57	10	dissolved	dissolve	VERB
ijpds-3748	57	11	in	in	ADP
ijpds-3748	57	12	diluent	diluent	NOUN
ijpds-3748	57	13	and	and	CCONJ
ijpds-3748	57	14	the	the	DET
ijpds-3748	57	15	volume	volume	NOUN
ijpds-3748	57	16	was	be	AUX
ijpds-3748	57	17	made	make	VERB
ijpds-3748	57	18	up	up	ADP
ijpds-3748	57	19	to	to	PART
ijpds-3748	57	20	50	50	NUM
ijpds-3748	57	21	ml	ml	NOUN
ijpds-3748	57	22	in	in	ADP
ijpds-3748	57	23	the	the	DET
ijpds-3748	57	24	volumetric	volumetric	NOUN
ijpds-3748	57	25	flask	flask	NOUN
ijpds-3748	57	26	.	.	PUNCT
ijpds-3748	58	1	after	after	ADP
ijpds-3748	58	2	filtration	filtration	NOUN
ijpds-3748	58	3	,	,	PUNCT
ijpds-3748	58	4	2.0	2.0	NUM
ijpds-3748	58	5	ml	ml	NOUN
ijpds-3748	58	6	of	of	ADP
ijpds-3748	58	7	this	this	DET
ijpds-3748	58	8	solution	solution	NOUN
ijpds-3748	58	9	was	be	AUX
ijpds-3748	58	10	transferred	transfer	VERB
ijpds-3748	58	11	to	to	ADP
ijpds-3748	58	12	another	another	DET
ijpds-3748	58	13	50	50	NUM
ijpds-3748	58	14	ml	ml	NOUN
ijpds-3748	58	15	volumetric	volumetric	ADJ
ijpds-3748	58	16	flask	flask	NOUN
ijpds-3748	58	17	,	,	PUNCT
ijpds-3748	58	18	mixed	mix	VERB
ijpds-3748	58	19	well	well	ADV
ijpds-3748	58	20	with	with	ADP
ijpds-3748	58	21	diluent	diluent	NOUN
ijpds-3748	58	22	,	,	PUNCT
ijpds-3748	58	23	and	and	CCONJ
ijpds-3748	58	24	sonicated	sonicate	VERB
ijpds-3748	58	25	for	for	ADP
ijpds-3748	58	26	5.0	5.0	NUM
ijpds-3748	58	27	minutes	minute	NOUN
ijpds-3748	58	28	.	.	PUNCT
ijpds-3748	59	1	method	method	PROPN
ijpds-3748	59	2	development	development	NOUN
ijpds-3748	59	3	:	:	PUNCT
ijpds-3748	59	4	we	we	PRON
ijpds-3748	59	5	performed	perform	VERB
ijpds-3748	59	6	some	some	DET
ijpds-3748	59	7	preliminary	preliminary	ADJ
ijpds-3748	59	8	tests	test	NOUN
ijpds-3748	59	9	for	for	ADP
ijpds-3748	59	10	the	the	DET
ijpds-3748	59	11	development	development	NOUN
ijpds-3748	59	12	of	of	ADP
ijpds-3748	59	13	a	a	DET
ijpds-3748	59	14	stable	stable	ADJ
ijpds-3748	59	15	and	and	CCONJ
ijpds-3748	59	16	effective	effective	ADJ
ijpds-3748	59	17	method	method	NOUN
ijpds-3748	59	18	for	for	ADP
ijpds-3748	59	19	qualitative	qualitative	ADJ
ijpds-3748	59	20	and	and	CCONJ
ijpds-3748	59	21	quantitative	quantitative	ADJ
ijpds-3748	59	22	estimation	estimation	NOUN
ijpds-3748	59	23	of	of	ADP
ijpds-3748	59	24	empagliflozin	empagliflozin	PROPN
ijpds-3748	59	25	.	.	PUNCT
ijpds-3748	60	1	first	first	ADV
ijpds-3748	60	2	,	,	PUNCT
ijpds-3748	60	3	the	the	DET
ijpds-3748	60	4	wavelength	wavelength	NOUN
ijpds-3748	60	5	was	be	AUX
ijpds-3748	60	6	detected	detect	VERB
ijpds-3748	60	7	using	use	VERB
ijpds-3748	60	8	a	a	DET
ijpds-3748	60	9	uv	uv	NOUN
ijpds-3748	60	10	-	-	PUNCT
ijpds-3748	60	11	visible	visible	ADJ
ijpds-3748	60	12	spectrophotometer	spectrophotometer	NOUN
ijpds-3748	60	13	by	by	ADP
ijpds-3748	60	14	scanning	scan	VERB
ijpds-3748	60	15	the	the	DET
ijpds-3748	60	16	sample	sample	NOUN
ijpds-3748	60	17	and	and	CCONJ
ijpds-3748	60	18	standard	standard	ADJ
ijpds-3748	60	19	solution	solution	NOUN
ijpds-3748	60	20	between	between	ADP
ijpds-3748	60	21	200	200	NUM
ijpds-3748	60	22	nm	nm	NOUN
ijpds-3748	60	23	to	to	ADP
ijpds-3748	60	24	400	400	NUM
ijpds-3748	60	25	nm	nm	NOUN
ijpds-3748	60	26	.	.	PUNCT
ijpds-3748	61	1	a	a	DET
ijpds-3748	61	2	major	major	ADJ
ijpds-3748	61	3	peak	peak	NOUN
ijpds-3748	61	4	of	of	ADP
ijpds-3748	61	5	empagliflozin	empagliflozin	PROPN
ijpds-3748	61	6	was	be	AUX
ijpds-3748	61	7	observed	observe	VERB
ijpds-3748	61	8	at	at	ADP
ijpds-3748	61	9	224	224	NUM
ijpds-3748	61	10	nm	nm	NOUN
ijpds-3748	61	11	(	(	PUNCT
ijpds-3748	61	12	figure	figure	NOUN
ijpds-3748	61	13	2	2	NUM
ijpds-3748	61	14	)	)	PUNCT
ijpds-3748	61	15	.	.	PUNCT
ijpds-3748	62	1	figure	figure	NOUN
ijpds-3748	62	2	2	2	NUM
ijpds-3748	62	3	–	–	PUNCT
ijpds-3748	62	4	uv	uv	NOUN
ijpds-3748	62	5	spectrum	spectrum	NOUN
ijpds-3748	62	6	of	of	ADP
ijpds-3748	62	7	empagliflozin	empagliflozin	PROPN
ijpds-3748	62	8	mobile	mobile	NOUN
ijpds-3748	62	9	phase	phase	NOUN
ijpds-3748	62	10	phosphate	phosphate	NOUN
ijpds-3748	62	11	buffer	buffer	NOUN
ijpds-3748	62	12	:	:	PUNCT
ijpds-3748	62	13	methanol	methanol	NOUN
ijpds-3748	62	14	(	(	PUNCT
ijpds-3748	62	15	70:30%v	70:30%v	NUM
ijpds-3748	62	16	/	/	SYM
ijpds-3748	62	17	v	v	NOUN
ijpds-3748	62	18	)	)	PUNCT
ijpds-3748	62	19	ph	ph	NOUN
ijpds-3748	62	20	adjusted	adjust	VERB
ijpds-3748	62	21	to	to	ADP
ijpds-3748	62	22	3.0	3.0	NUM
ijpds-3748	62	23	column	column	NOUN
ijpds-3748	62	24	ods	ods	PROPN
ijpds-3748	62	25	c18	c18	NOUN
ijpds-3748	62	26	,	,	PUNCT
ijpds-3748	62	27	250×4.6	250×4.6	PROPN
ijpds-3748	62	28	mm	mm	NOUN
ijpds-3748	62	29	,	,	PUNCT
ijpds-3748	62	30	5μ	5μ	NOUN
ijpds-3748	62	31	wavelength	wavelength	VERB
ijpds-3748	62	32	224	224	NUM
ijpds-3748	62	33	nm	nm	ADJ
ijpds-3748	62	34	flow	flow	NOUN
ijpds-3748	62	35	rate	rate	NOUN
ijpds-3748	62	36	1.0	1.0	NUM
ijpds-3748	62	37	ml	ml	NOUN
ijpds-3748	62	38	/	/	SYM
ijpds-3748	62	39	min	min	NOUN
ijpds-3748	62	40	injection	injection	NOUN
ijpds-3748	62	41	volume	volume	NOUN
ijpds-3748	62	42	20	20	NUM
ijpds-3748	62	43	μl	μl	ADP
ijpds-3748	62	44	run	run	VERB
ijpds-3748	62	45	time	time	NOUN
ijpds-3748	62	46	10	10	NUM
ijpds-3748	62	47	min	min	NOUN
ijpds-3748	62	48	diluent	diluent	NOUN
ijpds-3748	62	49	phosphate	phosphate	NOUN
ijpds-3748	62	50	buffer	buffer	NOUN
ijpds-3748	62	51	:	:	PUNCT
ijpds-3748	62	52	methanol	methanol	NOUN
ijpds-3748	62	53	(	(	PUNCT
ijpds-3748	62	54	70:30%v	70:30%v	NUM
ijpds-3748	62	55	/	/	SYM
ijpds-3748	62	56	v	v	NOUN
ijpds-3748	62	57	)	)	PUNCT
ijpds-3748	62	58	ph	ph	NOUN
ijpds-3748	62	59	adjusted	adjust	VERB
ijpds-3748	62	60	to	to	ADP
ijpds-3748	62	61	3.0	3.0	NUM
ijpds-3748	62	62	ahmad	ahmad	NOUN
ijpds-3748	62	63	et	et	PROPN
ijpds-3748	62	64	al	al	PROPN
ijpds-3748	62	65	rp	rp	PROPN
ijpds-3748	62	66	-	-	PUNCT
ijpds-3748	62	67	hplc	hplc	NOUN
ijpds-3748	62	68	method	method	NOUN
ijpds-3748	62	69	validation	validation	NOUN
ijpds-3748	62	70	of	of	ADP
ijpds-3748	62	71	empagliflozin	empagliflozin	PROPN
ijpds-3748	62	72	vol	vol	NOUN
ijpds-3748	62	73	2	2	NUM
ijpds-3748	63	1	|	|	NOUN
ijpds-3748	63	2	issue	issue	NOUN
ijpds-3748	63	3	2	2	NUM
ijpds-3748	63	4	|	|	ADV
ijpds-3748	63	5	apr	apr	ADV
ijpds-3748	63	6	–	–	PUNCT
ijpds-3748	63	7	jun	jun	PROPN
ijpds-3748	63	8	2023	2023	NUM
ijpds-3748	63	9	indian	indian	PROPN
ijpds-3748	63	10	j	j	PROPN
ijpds-3748	63	11	pharm	pharm	PROPN
ijpds-3748	63	12	drug	drug	PROPN
ijpds-3748	63	13	studies	study	NOUN
ijpds-3748	63	14	|	|	ADV
ijpds-3748	64	1	78	78	NUM
ijpds-3748	64	2	then	then	ADV
ijpds-3748	64	3	many	many	ADJ
ijpds-3748	64	4	injections	injection	NOUN
ijpds-3748	64	5	of	of	ADP
ijpds-3748	64	6	the	the	DET
ijpds-3748	64	7	sample	sample	NOUN
ijpds-3748	64	8	were	be	AUX
ijpds-3748	64	9	applied	apply	VERB
ijpds-3748	64	10	on	on	ADP
ijpds-3748	64	11	hplc	hplc	NOUN
ijpds-3748	64	12	using	use	VERB
ijpds-3748	64	13	water	water	NOUN
ijpds-3748	64	14	,	,	PUNCT
ijpds-3748	64	15	methanol	methanol	NOUN
ijpds-3748	64	16	and	and	CCONJ
ijpds-3748	64	17	acetonitrile	acetonitrile	NOUN
ijpds-3748	64	18	,	,	PUNCT
ijpds-3748	64	19	and	and	CCONJ
ijpds-3748	64	20	phosphate	phosphate	ADJ
ijpds-3748	64	21	buffer	buffer	NOUN
ijpds-3748	64	22	in	in	ADP
ijpds-3748	64	23	different	different	ADJ
ijpds-3748	64	24	compositions	composition	NOUN
ijpds-3748	64	25	(	(	PUNCT
ijpds-3748	64	26	to	to	PART
ijpds-3748	64	27	determine	determine	VERB
ijpds-3748	64	28	the	the	DET
ijpds-3748	64	29	optimal	optimal	ADJ
ijpds-3748	64	30	mobile	mobile	ADJ
ijpds-3748	64	31	phase	phase	NOUN
ijpds-3748	64	32	combination	combination	NOUN
ijpds-3748	64	33	)	)	PUNCT
ijpds-3748	64	34	as	as	ADP
ijpds-3748	64	35	mobile	mobile	ADJ
ijpds-3748	64	36	phase	phase	NOUN
ijpds-3748	64	37	.	.	PUNCT
ijpds-3748	65	1	the	the	DET
ijpds-3748	65	2	mobile	mobile	ADJ
ijpds-3748	65	3	phases	phase	NOUN
ijpds-3748	65	4	tested	test	VERB
ijpds-3748	65	5	included	include	VERB
ijpds-3748	65	6	methanol	methanol	NOUN
ijpds-3748	65	7	and	and	CCONJ
ijpds-3748	65	8	acetonitrile	acetonitrile	NOUN
ijpds-3748	65	9	in	in	ADP
ijpds-3748	65	10	the	the	DET
ijpds-3748	65	11	ratios	ratio	NOUN
ijpds-3748	65	12	of	of	ADP
ijpds-3748	65	13	60:40	60:40	NUM
ijpds-3748	65	14	and	and	CCONJ
ijpds-3748	65	15	70:30	70:30	NUM
ijpds-3748	65	16	,	,	PUNCT
ijpds-3748	65	17	phosphate	phosphate	ADJ
ijpds-3748	65	18	buffer	buffer	NOUN
ijpds-3748	65	19	,	,	PUNCT
ijpds-3748	65	20	and	and	CCONJ
ijpds-3748	65	21	methanol	methanol	NOUN
ijpds-3748	65	22	with	with	ADP
ijpds-3748	65	23	65:35	65:35	NUM
ijpds-3748	65	24	,	,	PUNCT
ijpds-3748	65	25	60:40	60:40	NUM
ijpds-3748	65	26	,	,	PUNCT
ijpds-3748	65	27	and	and	CCONJ
ijpds-3748	65	28	70:30	70:30	NUM
ijpds-3748	65	29	ratios	ratio	NOUN
ijpds-3748	65	30	to	to	PART
ijpds-3748	65	31	observe	observe	VERB
ijpds-3748	65	32	the	the	DET
ijpds-3748	65	33	separation	separation	NOUN
ijpds-3748	65	34	and	and	CCONJ
ijpds-3748	65	35	characteristics	characteristic	NOUN
ijpds-3748	65	36	of	of	ADP
ijpds-3748	65	37	the	the	DET
ijpds-3748	65	38	peak	peak	NOUN
ijpds-3748	65	39	.	.	PUNCT
ijpds-3748	66	1	it	it	PRON
ijpds-3748	66	2	was	be	AUX
ijpds-3748	66	3	observed	observe	VERB
ijpds-3748	66	4	that	that	SCONJ
ijpds-3748	66	5	the	the	DET
ijpds-3748	66	6	best	good	ADJ
ijpds-3748	66	7	symmetry	symmetry	NOUN
ijpds-3748	66	8	of	of	ADP
ijpds-3748	66	9	peak	peak	NOUN
ijpds-3748	66	10	with	with	ADP
ijpds-3748	66	11	less	less	ADJ
ijpds-3748	66	12	retention	retention	NOUN
ijpds-3748	66	13	time	time	NOUN
ijpds-3748	66	14	and	and	CCONJ
ijpds-3748	66	15	low	low	ADJ
ijpds-3748	66	16	pressure	pressure	NOUN
ijpds-3748	66	17	of	of	ADP
ijpds-3748	66	18	hplc	hplc	NOUN
ijpds-3748	66	19	pump	pump	NOUN
ijpds-3748	66	20	was	be	AUX
ijpds-3748	66	21	achieved	achieve	VERB
ijpds-3748	66	22	using	use	VERB
ijpds-3748	66	23	phosphate	phosphate	ADJ
ijpds-3748	66	24	buffer	buffer	NOUN
ijpds-3748	66	25	and	and	CCONJ
ijpds-3748	66	26	methanol	methanol	NOUN
ijpds-3748	66	27	in	in	ADP
ijpds-3748	66	28	the	the	DET
ijpds-3748	66	29	ratio	ratio	NOUN
ijpds-3748	66	30	of	of	ADP
ijpds-3748	66	31	70:30	70:30	NUM
ijpds-3748	66	32	as	as	ADP
ijpds-3748	66	33	mobile	mobile	ADJ
ijpds-3748	66	34	phase	phase	NOUN
ijpds-3748	66	35	.	.	PUNCT
ijpds-3748	67	1	the	the	DET
ijpds-3748	67	2	optimum	optimum	ADJ
ijpds-3748	67	3	flow	flow	NOUN
ijpds-3748	67	4	rate	rate	NOUN
ijpds-3748	67	5	selected	select	VERB
ijpds-3748	67	6	after	after	ADP
ijpds-3748	67	7	hit	hit	NOUN
ijpds-3748	67	8	and	and	CCONJ
ijpds-3748	67	9	trial	trial	NOUN
ijpds-3748	67	10	basis	basis	NOUN
ijpds-3748	67	11	was	be	AUX
ijpds-3748	67	12	1.0	1.0	NUM
ijpds-3748	67	13	ml	ml	NOUN
ijpds-3748	67	14	per	per	ADP
ijpds-3748	67	15	minute	minute	NOUN
ijpds-3748	67	16	.	.	PUNCT
ijpds-3748	68	1	system	system	NOUN
ijpds-3748	68	2	suitability	suitability	NOUN
ijpds-3748	68	3	:	:	PUNCT
ijpds-3748	68	4	a	a	DET
ijpds-3748	68	5	suitability	suitability	NOUN
ijpds-3748	68	6	study	study	NOUN
ijpds-3748	68	7	of	of	ADP
ijpds-3748	68	8	the	the	DET
ijpds-3748	68	9	system	system	NOUN
ijpds-3748	68	10	was	be	AUX
ijpds-3748	68	11	conducted	conduct	VERB
ijpds-3748	68	12	to	to	PART
ijpds-3748	68	13	confirm	confirm	VERB
ijpds-3748	68	14	its	its	PRON
ijpds-3748	68	15	performance	performance	NOUN
ijpds-3748	68	16	.	.	PUNCT
ijpds-3748	69	1	figure	figure	NOUN
ijpds-3748	69	2	3	3	NUM
ijpds-3748	69	3	–	–	PUNCT
ijpds-3748	69	4	suitability	suitability	NOUN
ijpds-3748	69	5	chromatogram	chromatogram	VERB
ijpds-3748	69	6	all	all	DET
ijpds-3748	69	7	critical	critical	ADJ
ijpds-3748	69	8	parameters	parameter	NOUN
ijpds-3748	69	9	including	include	VERB
ijpds-3748	69	10	percentage	percentage	NOUN
ijpds-3748	69	11	relative	relative	ADJ
ijpds-3748	69	12	standard	standard	ADJ
ijpds-3748	69	13	deviation	deviation	NOUN
ijpds-3748	69	14	(	(	PUNCT
ijpds-3748	69	15	rsd	rsd	NOUN
ijpds-3748	69	16	)	)	PUNCT
ijpds-3748	69	17	,	,	PUNCT
ijpds-3748	69	18	tailing	tail	VERB
ijpds-3748	69	19	factor	factor	NOUN
ijpds-3748	69	20	,	,	PUNCT
ijpds-3748	69	21	usp	usp	NOUN
ijpds-3748	69	22	plate	plate	NOUN
ijpds-3748	69	23	count	count	NOUN
ijpds-3748	69	24	,	,	PUNCT
ijpds-3748	69	25	and	and	CCONJ
ijpds-3748	69	26	usp	usp	NOUN
ijpds-3748	69	27	resolution	resolution	NOUN
ijpds-3748	69	28	were	be	AUX
ijpds-3748	69	29	verified	verify	VERB
ijpds-3748	69	30	by	by	ADP
ijpds-3748	69	31	injecting	inject	VERB
ijpds-3748	69	32	six	six	NUM
ijpds-3748	69	33	injections	injection	NOUN
ijpds-3748	69	34	of	of	ADP
ijpds-3748	69	35	standard	standard	ADJ
ijpds-3748	69	36	solution	solution	NOUN
ijpds-3748	69	37	.	.	PUNCT
ijpds-3748	70	1	the	the	DET
ijpds-3748	70	2	results	result	NOUN
ijpds-3748	70	3	of	of	ADP
ijpds-3748	70	4	system	system	NOUN
ijpds-3748	70	5	suitability	suitability	NOUN
ijpds-3748	70	6	are	be	AUX
ijpds-3748	70	7	depicted	depict	VERB
ijpds-3748	70	8	in	in	ADP
ijpds-3748	70	9	table	table	NOUN
ijpds-3748	70	10	2	2	NUM
ijpds-3748	70	11	.	.	PUNCT
ijpds-3748	70	12	table	table	NOUN
ijpds-3748	70	13	2	2	NUM
ijpds-3748	70	14	–	–	PUNCT
ijpds-3748	70	15	system	system	NOUN
ijpds-3748	70	16	suitability	suitability	NOUN
ijpds-3748	70	17	figure	figure	NOUN
ijpds-3748	70	18	4	4	NUM
ijpds-3748	70	19	–	–	PUNCT
ijpds-3748	70	20	specificity	specificity	NOUN
ijpds-3748	70	21	chromatogram	chromatogram	NOUN
ijpds-3748	70	22	specificity	specificity	NOUN
ijpds-3748	70	23	:	:	PUNCT
ijpds-3748	70	24	the	the	DET
ijpds-3748	70	25	analytical	analytical	ADJ
ijpds-3748	70	26	method	method	NOUN
ijpds-3748	70	27	should	should	AUX
ijpds-3748	70	28	have	have	VERB
ijpds-3748	70	29	the	the	DET
ijpds-3748	70	30	ability	ability	NOUN
ijpds-3748	70	31	to	to	PART
ijpds-3748	70	32	resolve	resolve	VERB
ijpds-3748	70	33	all	all	DET
ijpds-3748	70	34	its	its	PRON
ijpds-3748	70	35	process	process	NOUN
ijpds-3748	70	36	impurities	impurity	NOUN
ijpds-3748	70	37	,	,	PUNCT
ijpds-3748	70	38	known	known	ADJ
ijpds-3748	70	39	and	and	CCONJ
ijpds-3748	70	40	unknown	unknown	ADJ
ijpds-3748	70	41	degradation	degradation	NOUN
ijpds-3748	70	42	impurities	impurity	NOUN
ijpds-3748	70	43	during	during	ADP
ijpds-3748	70	44	stress	stress	NOUN
ijpds-3748	70	45	study	study	NOUN
ijpds-3748	70	46	.	.	PUNCT
ijpds-3748	71	1	a	a	DET
ijpds-3748	71	2	placebo	placebo	NOUN
ijpds-3748	71	3	should	should	AUX
ijpds-3748	71	4	not	not	PART
ijpds-3748	71	5	interfere	interfere	VERB
ijpds-3748	71	6	with	with	ADP
ijpds-3748	71	7	the	the	DET
ijpds-3748	71	8	retention	retention	NOUN
ijpds-3748	71	9	times	time	NOUN
ijpds-3748	71	10	of	of	ADP
ijpds-3748	71	11	active	active	ADJ
ijpds-3748	71	12	drugs	drug	NOUN
ijpds-3748	71	13	and	and	CCONJ
ijpds-3748	71	14	impurities	impurity	NOUN
ijpds-3748	71	15	.	.	PUNCT
ijpds-3748	72	1	the	the	DET
ijpds-3748	72	2	specificity	specificity	NOUN
ijpds-3748	72	3	of	of	ADP
ijpds-3748	72	4	the	the	DET
ijpds-3748	72	5	method	method	NOUN
ijpds-3748	72	6	was	be	AUX
ijpds-3748	72	7	confirmed	confirm	VERB
ijpds-3748	72	8	by	by	ADP
ijpds-3748	72	9	injecting	inject	VERB
ijpds-3748	72	10	the	the	DET
ijpds-3748	72	11	blank	blank	NOUN
ijpds-3748	72	12	,	,	PUNCT
ijpds-3748	72	13	placebo	placebo	NOUN
ijpds-3748	72	14	,	,	PUNCT
ijpds-3748	72	15	and	and	CCONJ
ijpds-3748	72	16	standard	standard	ADJ
ijpds-3748	72	17	solution	solution	NOUN
ijpds-3748	72	18	.	.	PUNCT
ijpds-3748	73	1	linearity	linearity	NOUN
ijpds-3748	73	2	:	:	PUNCT
ijpds-3748	73	3	the	the	DET
ijpds-3748	73	4	linearity	linearity	NOUN
ijpds-3748	73	5	of	of	ADP
ijpds-3748	73	6	the	the	DET
ijpds-3748	73	7	method	method	NOUN
ijpds-3748	73	8	was	be	AUX
ijpds-3748	73	9	checked	check	VERB
ijpds-3748	73	10	by	by	ADP
ijpds-3748	73	11	injecting	inject	VERB
ijpds-3748	73	12	5	5	NUM
ijpds-3748	73	13	standard	standard	ADJ
ijpds-3748	73	14	solutions	solution	NOUN
ijpds-3748	73	15	of	of	ADP
ijpds-3748	73	16	concentration	concentration	NOUN
ijpds-3748	73	17	ranging	range	VERB
ijpds-3748	73	18	from	from	ADP
ijpds-3748	73	19	25	25	NUM
ijpds-3748	73	20	µg	µg	NOUN
ijpds-3748	73	21	/	/	SYM
ijpds-3748	73	22	ml	ml	NOUN
ijpds-3748	73	23	to	to	ADP
ijpds-3748	73	24	125	125	NUM
ijpds-3748	73	25	µg	µg	NOUN
ijpds-3748	73	26	/	/	SYM
ijpds-3748	73	27	ml	ml	NOUN
ijpds-3748	73	28	.	.	PUNCT
ijpds-3748	74	1	then	then	ADV
ijpds-3748	74	2	the	the	DET
ijpds-3748	74	3	graph	graph	NOUN
ijpds-3748	74	4	was	be	AUX
ijpds-3748	74	5	plotted	plot	VERB
ijpds-3748	74	6	between	between	ADP
ijpds-3748	74	7	concentration	concentration	NOUN
ijpds-3748	74	8	and	and	CCONJ
ijpds-3748	74	9	peak	peak	NOUN
ijpds-3748	74	10	areas	area	NOUN
ijpds-3748	74	11	.	.	PUNCT
ijpds-3748	75	1	a	a	DET
ijpds-3748	75	2	straight	straight	ADJ
ijpds-3748	75	3	line	line	NOUN
ijpds-3748	75	4	was	be	AUX
ijpds-3748	75	5	obtained	obtain	VERB
ijpds-3748	75	6	which	which	PRON
ijpds-3748	75	7	confirmed	confirm	VERB
ijpds-3748	75	8	the	the	DET
ijpds-3748	75	9	linear	linear	ADJ
ijpds-3748	75	10	response	response	NOUN
ijpds-3748	75	11	of	of	ADP
ijpds-3748	75	12	the	the	DET
ijpds-3748	75	13	method	method	NOUN
ijpds-3748	75	14	(	(	PUNCT
ijpds-3748	75	15	fig	fig	NOUN
ijpds-3748	75	16	.	.	PUNCT
ijpds-3748	76	1	5	5	NUM
ijpds-3748	76	2	)	)	PUNCT
ijpds-3748	76	3	.	.	PUNCT
ijpds-3748	77	1	figure	figure	NOUN
ijpds-3748	77	2	5	5	NUM
ijpds-3748	77	3	–	–	PUNCT
ijpds-3748	77	4	linearity	linearity	NOUN
ijpds-3748	77	5	curve	curve	VERB
ijpds-3748	77	6	the	the	DET
ijpds-3748	77	7	intercept	intercept	NOUN
ijpds-3748	77	8	,	,	PUNCT
ijpds-3748	77	9	slope	slope	NOUN
ijpds-3748	77	10	,	,	PUNCT
ijpds-3748	77	11	correlation	correlation	NOUN
ijpds-3748	77	12	coefficient	coefficient	NOUN
ijpds-3748	77	13	of	of	ADP
ijpds-3748	77	14	regression	regression	NOUN
ijpds-3748	77	15	,	,	PUNCT
ijpds-3748	77	16	and	and	CCONJ
ijpds-3748	77	17	sum	sum	NOUN
ijpds-3748	77	18	of	of	ADP
ijpds-3748	77	19	squares	square	NOUN
ijpds-3748	77	20	were	be	AUX
ijpds-3748	77	21	calculated	calculate	VERB
ijpds-3748	77	22	.	.	PUNCT
ijpds-3748	78	1	the	the	DET
ijpds-3748	78	2	linearity	linearity	NOUN
ijpds-3748	78	3	results	result	NOUN
ijpds-3748	78	4	are	be	AUX
ijpds-3748	78	5	presented	present	VERB
ijpds-3748	78	6	in	in	ADP
ijpds-3748	78	7	table	table	NOUN
ijpds-3748	78	8	3	3	NUM
ijpds-3748	78	9	.	.	PUNCT
ijpds-3748	78	10	precision	precision	NOUN
ijpds-3748	78	11	a	a	DET
ijpds-3748	78	12	)	)	PUNCT
ijpds-3748	78	13	repeatability	repeatability	NOUN
ijpds-3748	78	14	:	:	PUNCT
ijpds-3748	78	15	for	for	ADP
ijpds-3748	78	16	repeatability	repeatability	NOUN
ijpds-3748	78	17	testing	testing	NOUN
ijpds-3748	78	18	,	,	PUNCT
ijpds-3748	78	19	we	we	PRON
ijpds-3748	78	20	applied	apply	VERB
ijpds-3748	78	21	six	six	NUM
ijpds-3748	78	22	replicate	replicate	ADJ
ijpds-3748	78	23	injections	injection	NOUN
ijpds-3748	78	24	of	of	ADP
ijpds-3748	78	25	the	the	DET
ijpds-3748	78	26	same	same	ADJ
ijpds-3748	78	27	concentration	concentration	NOUN
ijpds-3748	78	28	of	of	ADP
ijpds-3748	78	29	sample	sample	NOUN
ijpds-3748	78	30	solution	solution	NOUN
ijpds-3748	78	31	on	on	ADP
ijpds-3748	78	32	the	the	DET
ijpds-3748	78	33	same	same	ADJ
ijpds-3748	78	34	day	day	NOUN
ijpds-3748	78	35	.	.	PUNCT
ijpds-3748	79	1	all	all	DET
ijpds-3748	79	2	the	the	DET
ijpds-3748	79	3	parameters	parameter	NOUN
ijpds-3748	79	4	including	include	VERB
ijpds-3748	79	5	percentage	percentage	NOUN
ijpds-3748	79	6	rsd	rsd	NOUN
ijpds-3748	79	7	,	,	PUNCT
ijpds-3748	79	8	tailing	tail	VERB
ijpds-3748	79	9	factor	factor	NOUN
ijpds-3748	79	10	and	and	CCONJ
ijpds-3748	79	11	usp	usp	NOUN
ijpds-3748	79	12	plate	plate	NOUN
ijpds-3748	79	13	were	be	AUX
ijpds-3748	79	14	checked	check	VERB
ijpds-3748	79	15	and	and	CCONJ
ijpds-3748	79	16	are	be	AUX
ijpds-3748	79	17	mentioned	mention	VERB
ijpds-3748	79	18	in	in	ADP
ijpds-3748	79	19	table	table	NOUN
ijpds-3748	80	1	4	4	NUM
ijpds-3748	80	2	.	.	PUNCT
ijpds-3748	80	3	accuracy	accuracy	NOUN
ijpds-3748	80	4	:	:	PUNCT
ijpds-3748	80	5	the	the	DET
ijpds-3748	80	6	accuracy	accuracy	NOUN
ijpds-3748	80	7	of	of	ADP
ijpds-3748	80	8	a	a	DET
ijpds-3748	80	9	method	method	NOUN
ijpds-3748	80	10	describes	describe	VERB
ijpds-3748	80	11	how	how	SCONJ
ijpds-3748	80	12	close	close	ADJ
ijpds-3748	80	13	the	the	DET
ijpds-3748	80	14	results	result	NOUN
ijpds-3748	80	15	are	be	AUX
ijpds-3748	80	16	to	to	ADP
ijpds-3748	80	17	a	a	DET
ijpds-3748	80	18	true	true	ADJ
ijpds-3748	80	19	value	value	NOUN
ijpds-3748	80	20	.	.	PUNCT
ijpds-3748	81	1	the	the	DET
ijpds-3748	81	2	accuracy	accuracy	NOUN
ijpds-3748	81	3	study	study	NOUN
ijpds-3748	81	4	was	be	AUX
ijpds-3748	81	5	conducted	conduct	VERB
ijpds-3748	81	6	by	by	ADP
ijpds-3748	81	7	calculating	calculate	VERB
ijpds-3748	81	8	the	the	DET
ijpds-3748	81	9	percentage	percentage	NOUN
ijpds-3748	81	10	recovery	recovery	NOUN
ijpds-3748	81	11	of	of	ADP
ijpds-3748	81	12	empagliflozin	empagliflozin	PROPN
ijpds-3748	81	13	.	.	PUNCT
ijpds-3748	82	1	it	it	PRON
ijpds-3748	82	2	was	be	AUX
ijpds-3748	82	3	processed	process	VERB
ijpds-3748	82	4	by	by	ADP
ijpds-3748	82	5	injecting	inject	VERB
ijpds-3748	82	6	three	three	NUM
ijpds-3748	82	7	replicates	replicate	NOUN
ijpds-3748	82	8	of	of	ADP
ijpds-3748	82	9	three	three	NUM
ijpds-3748	82	10	different	different	ADJ
ijpds-3748	82	11	concentrations	concentration	NOUN
ijpds-3748	82	12	of	of	ADP
ijpds-3748	82	13	the	the	DET
ijpds-3748	82	14	analyte	analyte	NOUN
ijpds-3748	82	15	.	.	PUNCT
ijpds-3748	83	1	in	in	ADP
ijpds-3748	83	2	the	the	DET
ijpds-3748	83	3	end	end	NOUN
ijpds-3748	83	4	,	,	PUNCT
ijpds-3748	83	5	the	the	DET
ijpds-3748	83	6	percentage	percentage	NOUN
ijpds-3748	83	7	recovery	recovery	NOUN
ijpds-3748	83	8	of	of	ADP
ijpds-3748	83	9	the	the	DET
ijpds-3748	83	10	analyte	analyte	NOUN
ijpds-3748	83	11	was	be	AUX
ijpds-3748	83	12	determined	determine	VERB
ijpds-3748	83	13	to	to	PART
ijpds-3748	83	14	confirm	confirm	VERB
ijpds-3748	83	15	the	the	DET
ijpds-3748	83	16	accuracy	accuracy	NOUN
ijpds-3748	83	17	of	of	ADP
ijpds-3748	83	18	the	the	DET
ijpds-3748	83	19	system	system	NOUN
ijpds-3748	83	20	and	and	CCONJ
ijpds-3748	83	21	depicted	depict	VERB
ijpds-3748	83	22	in	in	ADP
ijpds-3748	83	23	table	table	NOUN
ijpds-3748	83	24	6	6	NUM
ijpds-3748	83	25	.	.	PUNCT
ijpds-3748	83	26	table	table	NOUN
ijpds-3748	83	27	3	3	NUM
ijpds-3748	83	28	–	–	PUNCT
ijpds-3748	83	29	linearity	linearity	NOUN
ijpds-3748	83	30	y	y	PROPN
ijpds-3748	83	31	=	=	SYM
ijpds-3748	83	32	845241x	845241x	PROPN
ijpds-3748	83	33	r²	r²	NOUN
ijpds-3748	83	34	=	=	PUNCT
ijpds-3748	84	1	0.9976	0.9976	NUM
ijpds-3748	84	2	0	0	NUM
ijpds-3748	84	3	1000000	1000000	NUM
ijpds-3748	84	4	2000000	2000000	NUM
ijpds-3748	84	5	3000000	3000000	NUM
ijpds-3748	84	6	4000000	4000000	NUM
ijpds-3748	84	7	5000000	5000000	NUM
ijpds-3748	84	8	6000000	6000000	NUM
ijpds-3748	84	9	0	0	NUM
ijpds-3748	84	10	1	1	NUM
ijpds-3748	84	11	2	2	NUM
ijpds-3748	84	12	3	3	NUM
ijpds-3748	84	13	4	4	NUM
ijpds-3748	84	14	5	5	NUM
ijpds-3748	84	15	6	6	NUM
ijpds-3748	84	16	7	7	NUM
ijpds-3748	84	17	ahmad	ahmad	NOUN
ijpds-3748	84	18	et	et	PROPN
ijpds-3748	84	19	al	al	PROPN
ijpds-3748	84	20	rp	rp	PROPN
ijpds-3748	84	21	-	-	PUNCT
ijpds-3748	84	22	hplc	hplc	NOUN
ijpds-3748	84	23	method	method	NOUN
ijpds-3748	84	24	validation	validation	NOUN
ijpds-3748	84	25	of	of	ADP
ijpds-3748	84	26	empagliflozin	empagliflozin	PROPN
ijpds-3748	84	27	vol	vol	NOUN
ijpds-3748	84	28	2	2	NUM
ijpds-3748	85	1	|	|	NOUN
ijpds-3748	85	2	issue	issue	NOUN
ijpds-3748	85	3	2	2	NUM
ijpds-3748	85	4	|	|	ADV
ijpds-3748	85	5	apr	apr	ADV
ijpds-3748	85	6	–	–	PUNCT
ijpds-3748	85	7	jun	jun	PROPN
ijpds-3748	85	8	2023	2023	NUM
ijpds-3748	85	9	indian	indian	PROPN
ijpds-3748	85	10	j	j	PROPN
ijpds-3748	85	11	pharm	pharm	PROPN
ijpds-3748	85	12	drug	drug	PROPN
ijpds-3748	85	13	studies	study	NOUN
ijpds-3748	85	14	|	|	ADV
ijpds-3748	85	15	79	79	NUM
ijpds-3748	85	16	table	table	NOUN
ijpds-3748	85	17	4	4	NUM
ijpds-3748	85	18	repeatability	repeatability	NOUN
ijpds-3748	85	19	table	table	NOUN
ijpds-3748	85	20	5	5	NUM
ijpds-3748	85	21	–	–	PUNCT
ijpds-3748	85	22	intermediate	intermediate	ADJ
ijpds-3748	85	23	precision	precision	NOUN
ijpds-3748	85	24	figure	figure	NOUN
ijpds-3748	85	25	6	6	NUM
ijpds-3748	85	26	–	–	PUNCT
ijpds-3748	85	27	accuracy	accuracy	NOUN
ijpds-3748	85	28	chromatogram	chromatogram	NOUN
ijpds-3748	85	29	limit	limit	NOUN
ijpds-3748	85	30	of	of	ADP
ijpds-3748	85	31	detection	detection	NOUN
ijpds-3748	85	32	(	(	PUNCT
ijpds-3748	85	33	lod	lod	PROPN
ijpds-3748	85	34	)	)	PUNCT
ijpds-3748	85	35	&	&	CCONJ
ijpds-3748	85	36	limit	limit	NOUN
ijpds-3748	85	37	of	of	ADP
ijpds-3748	85	38	quantitation	quantitation	NOUN
ijpds-3748	85	39	(	(	PUNCT
ijpds-3748	85	40	loq	loq	PROPN
ijpds-3748	85	41	):	):	PUNCT
ijpds-3748	85	42	qualitative	qualitative	ADJ
ijpds-3748	85	43	analysis	analysis	NOUN
ijpds-3748	85	44	of	of	ADP
ijpds-3748	85	45	an	an	DET
ijpds-3748	85	46	analyte	analyte	NOUN
ijpds-3748	85	47	in	in	ADP
ijpds-3748	85	48	a	a	DET
ijpds-3748	85	49	tablet	tablet	NOUN
ijpds-3748	85	50	at	at	ADP
ijpds-3748	85	51	the	the	DET
ijpds-3748	85	52	lowest	low	ADJ
ijpds-3748	85	53	possible	possible	ADJ
ijpds-3748	85	54	concentration	concentration	NOUN
ijpds-3748	85	55	is	be	AUX
ijpds-3748	85	56	called	call	VERB
ijpds-3748	85	57	the	the	DET
ijpds-3748	85	58	limit	limit	NOUN
ijpds-3748	85	59	of	of	ADP
ijpds-3748	85	60	detection	detection	NOUN
ijpds-3748	85	61	.	.	PUNCT
ijpds-3748	86	1	it	it	PRON
ijpds-3748	86	2	can	can	AUX
ijpds-3748	86	3	be	be	AUX
ijpds-3748	86	4	calculated	calculate	VERB
ijpds-3748	86	5	by	by	ADP
ijpds-3748	86	6	the	the	DET
ijpds-3748	86	7	formula	formula	NOUN
ijpds-3748	86	8	lod	lod	NOUN
ijpds-3748	86	9	=	=	SYM
ijpds-3748	86	10	3.3σ	3.3σ	NUM
ijpds-3748	86	11	/	/	SYM
ijpds-3748	86	12	s	s	NOUN
ijpds-3748	86	13	,	,	PUNCT
ijpds-3748	86	14	where	where	SCONJ
ijpds-3748	86	15	σ	σ	PROPN
ijpds-3748	86	16	is	be	AUX
ijpds-3748	86	17	the	the	DET
ijpds-3748	86	18	standard	standard	ADJ
ijpds-3748	86	19	deviation	deviation	NOUN
ijpds-3748	86	20	of	of	ADP
ijpds-3748	86	21	response	response	NOUN
ijpds-3748	86	22	and	and	CCONJ
ijpds-3748	86	23	s	s	NOUN
ijpds-3748	86	24	is	be	AUX
ijpds-3748	86	25	the	the	DET
ijpds-3748	86	26	slope	slope	NOUN
ijpds-3748	86	27	of	of	ADP
ijpds-3748	86	28	the	the	DET
ijpds-3748	86	29	calibration	calibration	NOUN
ijpds-3748	86	30	curve	curve	NOUN
ijpds-3748	86	31	.	.	PUNCT
ijpds-3748	87	1	whereas	whereas	SCONJ
ijpds-3748	87	2	the	the	DET
ijpds-3748	87	3	lowest	low	ADJ
ijpds-3748	87	4	possible	possible	ADJ
ijpds-3748	87	5	concentration	concentration	NOUN
ijpds-3748	87	6	of	of	ADP
ijpds-3748	87	7	an	an	DET
ijpds-3748	87	8	active	active	ADJ
ijpds-3748	87	9	ingredient	ingredient	NOUN
ijpds-3748	87	10	in	in	ADP
ijpds-3748	87	11	a	a	DET
ijpds-3748	87	12	tablet	tablet	NOUN
ijpds-3748	87	13	that	that	PRON
ijpds-3748	87	14	can	can	AUX
ijpds-3748	87	15	be	be	AUX
ijpds-3748	87	16	detected	detect	VERB
ijpds-3748	87	17	quantitatively	quantitatively	ADV
ijpds-3748	87	18	is	be	AUX
ijpds-3748	87	19	called	call	VERB
ijpds-3748	87	20	the	the	DET
ijpds-3748	87	21	limit	limit	NOUN
ijpds-3748	87	22	of	of	ADP
ijpds-3748	87	23	quantitation	quantitation	NOUN
ijpds-3748	87	24	.	.	PUNCT
ijpds-3748	88	1	in	in	ADP
ijpds-3748	88	2	the	the	DET
ijpds-3748	88	3	recent	recent	ADJ
ijpds-3748	88	4	study	study	NOUN
ijpds-3748	88	5	,	,	PUNCT
ijpds-3748	88	6	the	the	DET
ijpds-3748	88	7	limit	limit	NOUN
ijpds-3748	88	8	of	of	ADP
ijpds-3748	88	9	quantitation	quantitation	NOUN
ijpds-3748	88	10	was	be	AUX
ijpds-3748	88	11	calculated	calculate	VERB
ijpds-3748	88	12	in	in	ADP
ijpds-3748	88	13	the	the	DET
ijpds-3748	88	14	sample	sample	NOUN
ijpds-3748	88	15	with	with	ADP
ijpds-3748	88	16	acceptable	acceptable	ADJ
ijpds-3748	88	17	precision	precision	NOUN
ijpds-3748	88	18	and	and	CCONJ
ijpds-3748	88	19	accuracy	accuracy	NOUN
ijpds-3748	88	20	limits	limit	NOUN
ijpds-3748	88	21	by	by	ADP
ijpds-3748	88	22	the	the	DET
ijpds-3748	88	23	formula	formula	NOUN
ijpds-3748	88	24	loq=10σ	loq=10σ	PROPN
ijpds-3748	88	25	/	/	SYM
ijpds-3748	88	26	s.	s.	PROPN
ijpds-3748	88	27	the	the	DET
ijpds-3748	88	28	results	result	NOUN
ijpds-3748	88	29	of	of	ADP
ijpds-3748	88	30	the	the	DET
ijpds-3748	88	31	limit	limit	NOUN
ijpds-3748	88	32	of	of	ADP
ijpds-3748	88	33	detection	detection	NOUN
ijpds-3748	88	34	of	of	ADP
ijpds-3748	88	35	empagliflozin	empagliflozin	PROPN
ijpds-3748	88	36	calculated	calculate	VERB
ijpds-3748	88	37	in	in	ADP
ijpds-3748	88	38	xr	xr	PROPN
ijpds-3748	88	39	tablets	tablet	NOUN
ijpds-3748	88	40	were	be	AUX
ijpds-3748	88	41	found	find	VERB
ijpds-3748	88	42	to	to	PART
ijpds-3748	88	43	be	be	AUX
ijpds-3748	88	44	0.068μg	0.068μg	NOUN
ijpds-3748	88	45	/	/	SYM
ijpds-3748	88	46	ml	ml	NOUN
ijpds-3748	88	47	while	while	SCONJ
ijpds-3748	88	48	the	the	DET
ijpds-3748	88	49	limit	limit	NOUN
ijpds-3748	88	50	of	of	ADP
ijpds-3748	88	51	quantitation	quantitation	NOUN
ijpds-3748	88	52	came	come	VERB
ijpds-3748	88	53	out	out	ADP
ijpds-3748	88	54	to	to	PART
ijpds-3748	88	55	be	be	AUX
ijpds-3748	88	56	0.35	0.35	NUM
ijpds-3748	88	57	μg	μg	NOUN
ijpds-3748	88	58	/	/	SYM
ijpds-3748	88	59	ml	ml	PROPN
ijpds-3748	88	60	.	.	PUNCT
ijpds-3748	89	1	figure	figure	VERB
ijpds-3748	89	2	7	7	NUM
ijpds-3748	89	3	–	–	PUNCT
ijpds-3748	89	4	limit	limit	NOUN
ijpds-3748	89	5	of	of	ADP
ijpds-3748	89	6	detection	detection	NOUN
ijpds-3748	89	7	figure	figure	NOUN
ijpds-3748	89	8	8	8	NUM
ijpds-3748	89	9	–	–	PUNCT
ijpds-3748	89	10	limit	limit	NOUN
ijpds-3748	89	11	of	of	ADP
ijpds-3748	89	12	quantitation	quantitation	NOUN
ijpds-3748	89	13	robustness	robustness	NOUN
ijpds-3748	89	14	:	:	PUNCT
ijpds-3748	89	15	the	the	DET
ijpds-3748	89	16	robustness	robustness	NOUN
ijpds-3748	89	17	of	of	ADP
ijpds-3748	89	18	the	the	DET
ijpds-3748	89	19	analytical	analytical	ADJ
ijpds-3748	89	20	method	method	NOUN
ijpds-3748	89	21	is	be	AUX
ijpds-3748	89	22	the	the	DET
ijpds-3748	89	23	capacity	capacity	NOUN
ijpds-3748	89	24	to	to	PART
ijpds-3748	89	25	remain	remain	VERB
ijpds-3748	89	26	unchanged	unchanged	ADJ
ijpds-3748	89	27	by	by	ADP
ijpds-3748	89	28	a	a	DET
ijpds-3748	89	29	small	small	ADJ
ijpds-3748	89	30	change	change	NOUN
ijpds-3748	89	31	in	in	ADP
ijpds-3748	89	32	conditions	condition	NOUN
ijpds-3748	89	33	.	.	PUNCT
ijpds-3748	90	1	high	high	ADJ
ijpds-3748	90	2	system	system	NOUN
ijpds-3748	90	3	robustness	robustness	NOUN
ijpds-3748	90	4	ensures	ensure	VERB
ijpds-3748	90	5	a	a	DET
ijpds-3748	90	6	positive	positive	ADJ
ijpds-3748	90	7	indication	indication	NOUN
ijpds-3748	90	8	in	in	ADP
ijpds-3748	90	9	normal	normal	ADJ
ijpds-3748	90	10	use	use	NOUN
ijpds-3748	90	11	.	.	PUNCT
ijpds-3748	91	1	the	the	DET
ijpds-3748	91	2	robustness	robustness	NOUN
ijpds-3748	91	3	of	of	ADP
ijpds-3748	91	4	the	the	DET
ijpds-3748	91	5	method	method	NOUN
ijpds-3748	91	6	was	be	AUX
ijpds-3748	91	7	checked	check	VERB
ijpds-3748	91	8	by	by	ADP
ijpds-3748	91	9	making	make	VERB
ijpds-3748	91	10	minor	minor	ADJ
ijpds-3748	91	11	changes	change	NOUN
ijpds-3748	91	12	in	in	ADP
ijpds-3748	91	13	the	the	DET
ijpds-3748	91	14	composition	composition	NOUN
ijpds-3748	91	15	of	of	ADP
ijpds-3748	91	16	the	the	DET
ijpds-3748	91	17	mobile	mobile	ADJ
ijpds-3748	91	18	phase	phase	NOUN
ijpds-3748	91	19	,	,	PUNCT
ijpds-3748	91	20	flow	flow	NOUN
ijpds-3748	91	21	rate	rate	NOUN
ijpds-3748	91	22	,	,	PUNCT
ijpds-3748	91	23	temperature	temperature	NOUN
ijpds-3748	91	24	of	of	ADP
ijpds-3748	91	25	the	the	DET
ijpds-3748	91	26	column	column	NOUN
ijpds-3748	91	27	,	,	PUNCT
ijpds-3748	91	28	and	and	CCONJ
ijpds-3748	91	29	the	the	DET
ijpds-3748	91	30	ph	ph	NOUN
ijpds-3748	91	31	of	of	ADP
ijpds-3748	91	32	the	the	DET
ijpds-3748	91	33	buffer	buffer	NOUN
ijpds-3748	91	34	.	.	PUNCT
ijpds-3748	92	1	it	it	PRON
ijpds-3748	92	2	was	be	AUX
ijpds-3748	92	3	confirmed	confirm	VERB
ijpds-3748	92	4	that	that	SCONJ
ijpds-3748	92	5	no	no	DET
ijpds-3748	92	6	significant	significant	ADJ
ijpds-3748	92	7	changes	change	NOUN
ijpds-3748	92	8	occur	occur	VERB
ijpds-3748	92	9	after	after	ADP
ijpds-3748	92	10	deliberately	deliberately	ADV
ijpds-3748	92	11	changing	change	VERB
ijpds-3748	92	12	the	the	DET
ijpds-3748	92	13	system	system	NOUN
ijpds-3748	92	14	conditions	condition	NOUN
ijpds-3748	92	15	.	.	PUNCT
ijpds-3748	93	1	the	the	DET
ijpds-3748	93	2	robustness	robustness	NOUN
ijpds-3748	93	3	results	result	NOUN
ijpds-3748	93	4	are	be	AUX
ijpds-3748	93	5	depicted	depict	VERB
ijpds-3748	93	6	in	in	ADP
ijpds-3748	93	7	table	table	NOUN
ijpds-3748	93	8	7	7	NUM
ijpds-3748	93	9	.	.	PUNCT
ijpds-3748	93	10	table	table	NOUN
ijpds-3748	93	11	6	6	NUM
ijpds-3748	93	12	–	–	PUNCT
ijpds-3748	93	13	accuracy	accuracy	NOUN
ijpds-3748	93	14	of	of	ADP
ijpds-3748	93	15	the	the	DET
ijpds-3748	93	16	system	system	NOUN
ijpds-3748	93	17	ahmad	ahmad	PROPN
ijpds-3748	93	18	et	et	PROPN
ijpds-3748	93	19	al	al	PROPN
ijpds-3748	93	20	rp	rp	PROPN
ijpds-3748	93	21	-	-	PUNCT
ijpds-3748	93	22	hplc	hplc	NOUN
ijpds-3748	93	23	method	method	NOUN
ijpds-3748	93	24	validation	validation	NOUN
ijpds-3748	93	25	of	of	ADP
ijpds-3748	93	26	empagliflozin	empagliflozin	PROPN
ijpds-3748	93	27	vol	vol	NOUN
ijpds-3748	93	28	2	2	NUM
ijpds-3748	93	29	|	|	NOUN
ijpds-3748	93	30	issue	issue	NOUN
ijpds-3748	93	31	2	2	NUM
ijpds-3748	93	32	|	|	ADV
ijpds-3748	93	33	apr	apr	ADV
ijpds-3748	93	34	–	–	PUNCT
ijpds-3748	93	35	jun	jun	PROPN
ijpds-3748	93	36	2023	2023	NUM
ijpds-3748	93	37	indian	indian	PROPN
ijpds-3748	93	38	j	j	PROPN
ijpds-3748	93	39	pharm	pharm	PROPN
ijpds-3748	93	40	drug	drug	PROPN
ijpds-3748	93	41	studies	study	NOUN
ijpds-3748	93	42	|	|	ADV
ijpds-3748	93	43	80	80	NUM
ijpds-3748	93	44	table	table	NOUN
ijpds-3748	93	45	7	7	NUM
ijpds-3748	93	46	–	–	PUNCT
ijpds-3748	93	47	robustness	robustness	NOUN
ijpds-3748	93	48	of	of	ADP
ijpds-3748	93	49	the	the	DET
ijpds-3748	93	50	method	method	NOUN
ijpds-3748	93	51	table	table	NOUN
ijpds-3748	93	52	8	8	NUM
ijpds-3748	93	53	–	–	PUNCT
ijpds-3748	93	54	stress	stress	NOUN
ijpds-3748	93	55	stability	stability	NOUN
ijpds-3748	93	56	study	study	NOUN
ijpds-3748	93	57	stress	stress	NOUN
ijpds-3748	93	58	stability	stability	NOUN
ijpds-3748	93	59	study	study	NOUN
ijpds-3748	93	60	:	:	PUNCT
ijpds-3748	93	61	this	this	DET
ijpds-3748	93	62	study	study	NOUN
ijpds-3748	93	63	was	be	AUX
ijpds-3748	93	64	conducted	conduct	VERB
ijpds-3748	93	65	to	to	PART
ijpds-3748	93	66	assess	assess	VERB
ijpds-3748	93	67	the	the	DET
ijpds-3748	93	68	stability	stability	NOUN
ijpds-3748	93	69	of	of	ADP
ijpds-3748	93	70	the	the	DET
ijpds-3748	93	71	method	method	NOUN
ijpds-3748	93	72	under	under	ADP
ijpds-3748	93	73	stressed	stress	VERB
ijpds-3748	93	74	conditions	condition	NOUN
ijpds-3748	93	75	.	.	PUNCT
ijpds-3748	94	1	the	the	DET
ijpds-3748	94	2	forced	force	VERB
ijpds-3748	94	3	degradation	degradation	NOUN
ijpds-3748	94	4	parameters	parameter	NOUN
ijpds-3748	94	5	like	like	ADP
ijpds-3748	94	6	acid	acid	NOUN
ijpds-3748	94	7	,	,	PUNCT
ijpds-3748	94	8	alkali	alkali	ADJ
ijpds-3748	94	9	,	,	PUNCT
ijpds-3748	94	10	oxidative	oxidative	ADJ
ijpds-3748	94	11	,	,	PUNCT
ijpds-3748	94	12	photolytic	photolytic	ADJ
ijpds-3748	94	13	,	,	PUNCT
ijpds-3748	94	14	thermal	thermal	ADJ
ijpds-3748	94	15	,	,	PUNCT
ijpds-3748	94	16	and	and	CCONJ
ijpds-3748	94	17	hydrolytic	hydrolytic	ADJ
ijpds-3748	94	18	analyses	analysis	NOUN
ijpds-3748	94	19	were	be	AUX
ijpds-3748	94	20	carried	carry	VERB
ijpds-3748	94	21	out	out	ADP
ijpds-3748	94	22	under	under	ADP
ijpds-3748	94	23	the	the	DET
ijpds-3748	94	24	scope	scope	NOUN
ijpds-3748	94	25	of	of	ADP
ijpds-3748	94	26	this	this	DET
ijpds-3748	94	27	study	study	NOUN
ijpds-3748	94	28	.	.	PUNCT
ijpds-3748	95	1	acid	acid	ADJ
ijpds-3748	95	2	degradation	degradation	NOUN
ijpds-3748	95	3	study	study	NOUN
ijpds-3748	95	4	:	:	PUNCT
ijpds-3748	95	5	in	in	ADP
ijpds-3748	95	6	the	the	DET
ijpds-3748	95	7	acid	acid	NOUN
ijpds-3748	95	8	degradation	degradation	NOUN
ijpds-3748	95	9	study	study	NOUN
ijpds-3748	95	10	,	,	PUNCT
ijpds-3748	95	11	1ml	1ml	NOUN
ijpds-3748	95	12	of	of	ADP
ijpds-3748	95	13	2n	2n	NUM
ijpds-3748	95	14	hcl	hcl	PROPN
ijpds-3748	95	15	was	be	AUX
ijpds-3748	95	16	added	add	VERB
ijpds-3748	95	17	to	to	ADP
ijpds-3748	95	18	1ml	1ml	NOUN
ijpds-3748	95	19	of	of	ADP
ijpds-3748	95	20	stock	stock	NOUN
ijpds-3748	95	21	solution	solution	NOUN
ijpds-3748	95	22	of	of	ADP
ijpds-3748	95	23	empagliflozin	empagliflozin	PROPN
ijpds-3748	95	24	and	and	CCONJ
ijpds-3748	95	25	the	the	DET
ijpds-3748	95	26	mixture	mixture	NOUN
ijpds-3748	95	27	was	be	AUX
ijpds-3748	95	28	refluxed	refluxe	VERB
ijpds-3748	95	29	for	for	ADP
ijpds-3748	95	30	30	30	NUM
ijpds-3748	95	31	minutes	minute	NOUN
ijpds-3748	95	32	at	at	ADP
ijpds-3748	95	33	60	60	NUM
ijpds-3748	95	34	°	°	NOUN
ijpds-3748	95	35	c	c	NOUN
ijpds-3748	95	36	.	.	PUNCT
ijpds-3748	96	1	the	the	DET
ijpds-3748	96	2	resultant	resultant	NOUN
ijpds-3748	96	3	solution	solution	NOUN
ijpds-3748	96	4	was	be	AUX
ijpds-3748	96	5	diluted	dilute	VERB
ijpds-3748	96	6	with	with	ADP
ijpds-3748	96	7	diluent	diluent	NOUN
ijpds-3748	96	8	to	to	ADP
ijpds-3748	96	9	5	5	NUM
ijpds-3748	96	10	µg	µg	ADV
ijpds-3748	96	11	/	/	SYM
ijpds-3748	96	12	ml	ml	NOUN
ijpds-3748	96	13	.	.	PUNCT
ijpds-3748	97	1	then	then	ADV
ijpds-3748	97	2	three	three	NUM
ijpds-3748	97	3	replicate	replicate	ADJ
ijpds-3748	97	4	injections	injection	NOUN
ijpds-3748	97	5	of	of	ADP
ijpds-3748	97	6	10	10	NUM
ijpds-3748	97	7	μl	μl	NOUN
ijpds-3748	97	8	solution	solution	NOUN
ijpds-3748	97	9	were	be	AUX
ijpds-3748	97	10	injected	inject	VERB
ijpds-3748	97	11	into	into	ADP
ijpds-3748	97	12	the	the	DET
ijpds-3748	97	13	chromatograph	chromatograph	NOUN
ijpds-3748	97	14	and	and	CCONJ
ijpds-3748	97	15	chromatograms	chromatogram	NOUN
ijpds-3748	97	16	were	be	AUX
ijpds-3748	97	17	observed	observe	VERB
ijpds-3748	97	18	to	to	PART
ijpds-3748	97	19	check	check	VERB
ijpds-3748	97	20	the	the	DET
ijpds-3748	97	21	stability	stability	NOUN
ijpds-3748	97	22	of	of	ADP
ijpds-3748	97	23	the	the	DET
ijpds-3748	97	24	solution	solution	NOUN
ijpds-3748	97	25	.	.	PUNCT
ijpds-3748	98	1	the	the	DET
ijpds-3748	98	2	percentage	percentage	NOUN
ijpds-3748	98	3	degradation	degradation	NOUN
ijpds-3748	98	4	was	be	AUX
ijpds-3748	98	5	checked	check	VERB
ijpds-3748	98	6	by	by	ADP
ijpds-3748	98	7	comparing	compare	VERB
ijpds-3748	98	8	the	the	DET
ijpds-3748	98	9	results	result	NOUN
ijpds-3748	98	10	with	with	ADP
ijpds-3748	98	11	the	the	DET
ijpds-3748	98	12	standard	standard	NOUN
ijpds-3748	98	13	.	.	PUNCT
ijpds-3748	99	1	alkali	alkali	ADJ
ijpds-3748	99	2	degradation	degradation	NOUN
ijpds-3748	99	3	study	study	NOUN
ijpds-3748	99	4	:	:	PUNCT
ijpds-3748	99	5	this	this	DET
ijpds-3748	99	6	study	study	NOUN
ijpds-3748	99	7	was	be	AUX
ijpds-3748	99	8	conducted	conduct	VERB
ijpds-3748	99	9	by	by	ADP
ijpds-3748	99	10	taking	take	VERB
ijpds-3748	99	11	1ml	1ml	NOUN
ijpds-3748	99	12	of	of	ADP
ijpds-3748	99	13	stock	stock	NOUN
ijpds-3748	99	14	solution	solution	NOUN
ijpds-3748	99	15	and	and	CCONJ
ijpds-3748	99	16	1ml	1ml	NOUN
ijpds-3748	99	17	of	of	ADP
ijpds-3748	99	18	2n	2n	NUM
ijpds-3748	99	19	naoh	naoh	NOUN
ijpds-3748	99	20	solution	solution	NOUN
ijpds-3748	99	21	and	and	CCONJ
ijpds-3748	99	22	the	the	DET
ijpds-3748	99	23	mixture	mixture	NOUN
ijpds-3748	99	24	was	be	AUX
ijpds-3748	99	25	refluxed	refluxe	VERB
ijpds-3748	99	26	for	for	ADP
ijpds-3748	99	27	30	30	NUM
ijpds-3748	99	28	minutes	minute	NOUN
ijpds-3748	99	29	at	at	ADP
ijpds-3748	99	30	60	60	NUM
ijpds-3748	99	31	°	°	NOUN
ijpds-3748	99	32	c	c	NOUN
ijpds-3748	99	33	.	.	PUNCT
ijpds-3748	100	1	then	then	ADV
ijpds-3748	100	2	the	the	DET
ijpds-3748	100	3	solution	solution	NOUN
ijpds-3748	100	4	was	be	AUX
ijpds-3748	100	5	diluted	dilute	VERB
ijpds-3748	100	6	to	to	ADP
ijpds-3748	100	7	5	5	NUM
ijpds-3748	100	8	µg	µg	ADV
ijpds-3748	100	9	/	/	SYM
ijpds-3748	100	10	ml	ml	NOUN
ijpds-3748	100	11	.	.	PUNCT
ijpds-3748	101	1	three	three	NUM
ijpds-3748	101	2	replicate	replicate	ADJ
ijpds-3748	101	3	injections	injection	NOUN
ijpds-3748	101	4	of	of	ADP
ijpds-3748	101	5	10	10	NUM
ijpds-3748	101	6	μl	μl	NOUN
ijpds-3748	101	7	solution	solution	NOUN
ijpds-3748	101	8	were	be	AUX
ijpds-3748	101	9	then	then	ADV
ijpds-3748	101	10	injected	inject	VERB
ijpds-3748	101	11	into	into	ADP
ijpds-3748	101	12	the	the	DET
ijpds-3748	101	13	chromatograph	chromatograph	NOUN
ijpds-3748	101	14	and	and	CCONJ
ijpds-3748	101	15	the	the	DET
ijpds-3748	101	16	behavior	behavior	NOUN
ijpds-3748	101	17	of	of	ADP
ijpds-3748	101	18	the	the	DET
ijpds-3748	101	19	peak	peak	NOUN
ijpds-3748	101	20	area	area	NOUN
ijpds-3748	101	21	was	be	AUX
ijpds-3748	101	22	observed	observe	VERB
ijpds-3748	101	23	.	.	PUNCT
ijpds-3748	102	1	this	this	DET
ijpds-3748	102	2	peak	peak	NOUN
ijpds-3748	102	3	area	area	NOUN
ijpds-3748	102	4	was	be	AUX
ijpds-3748	102	5	then	then	ADV
ijpds-3748	102	6	compared	compare	VERB
ijpds-3748	102	7	with	with	ADP
ijpds-3748	102	8	that	that	PRON
ijpds-3748	102	9	of	of	ADP
ijpds-3748	102	10	the	the	DET
ijpds-3748	102	11	standard	standard	NOUN
ijpds-3748	102	12	.	.	PUNCT
ijpds-3748	103	1	dry	dry	ADJ
ijpds-3748	103	2	heat	heat	NOUN
ijpds-3748	103	3	degradation	degradation	NOUN
ijpds-3748	103	4	study	study	NOUN
ijpds-3748	103	5	:	:	PUNCT
ijpds-3748	103	6	thermal	thermal	ADJ
ijpds-3748	103	7	degradation	degradation	NOUN
ijpds-3748	103	8	was	be	AUX
ijpds-3748	103	9	carried	carry	VERB
ijpds-3748	103	10	out	out	ADP
ijpds-3748	103	11	by	by	ADP
ijpds-3748	103	12	placing	place	VERB
ijpds-3748	103	13	powder	powder	NOUN
ijpds-3748	103	14	of	of	ADP
ijpds-3748	103	15	empagliflozin	empagliflozin	PROPN
ijpds-3748	103	16	in	in	ADP
ijpds-3748	103	17	a	a	DET
ijpds-3748	103	18	petri	petri	ADJ
ijpds-3748	103	19	dish	dish	NOUN
ijpds-3748	103	20	at	at	ADP
ijpds-3748	103	21	105	105	NUM
ijpds-3748	103	22	°	°	ADP
ijpds-3748	103	23	c	c	NOUN
ijpds-3748	103	24	for	for	ADP
ijpds-3748	103	25	1	1	NUM
ijpds-3748	103	26	hour	hour	NOUN
ijpds-3748	103	27	.	.	PUNCT
ijpds-3748	104	1	then	then	ADV
ijpds-3748	104	2	5	5	NUM
ijpds-3748	104	3	µg	µg	ADJ
ijpds-3748	104	4	/	/	SYM
ijpds-3748	104	5	ml	ml	NOUN
ijpds-3748	104	6	solution	solution	NOUN
ijpds-3748	104	7	of	of	ADP
ijpds-3748	104	8	empagliflozin	empagliflozin	PROPN
ijpds-3748	104	9	was	be	AUX
ijpds-3748	104	10	made	make	VERB
ijpds-3748	104	11	and	and	CCONJ
ijpds-3748	104	12	triplicate	triplicate	VERB
ijpds-3748	104	13	injections	injection	NOUN
ijpds-3748	104	14	were	be	AUX
ijpds-3748	104	15	applied	apply	VERB
ijpds-3748	104	16	to	to	ADP
ijpds-3748	104	17	the	the	DET
ijpds-3748	104	18	chromatograph	chromatograph	NOUN
ijpds-3748	104	19	and	and	CCONJ
ijpds-3748	104	20	the	the	DET
ijpds-3748	104	21	degradation	degradation	NOUN
ijpds-3748	104	22	was	be	AUX
ijpds-3748	104	23	observed	observe	VERB
ijpds-3748	104	24	by	by	ADP
ijpds-3748	104	25	comparing	compare	VERB
ijpds-3748	104	26	the	the	DET
ijpds-3748	104	27	peak	peak	NOUN
ijpds-3748	104	28	areas	area	NOUN
ijpds-3748	104	29	with	with	ADP
ijpds-3748	104	30	the	the	DET
ijpds-3748	104	31	standard	standard	ADJ
ijpds-3748	104	32	solution	solution	NOUN
ijpds-3748	104	33	.	.	PUNCT
ijpds-3748	105	1	photo	photo	NOUN
ijpds-3748	105	2	stability	stability	NOUN
ijpds-3748	105	3	:	:	PUNCT
ijpds-3748	105	4	for	for	ADP
ijpds-3748	105	5	photolytic	photolytic	ADJ
ijpds-3748	105	6	degradation	degradation	NOUN
ijpds-3748	105	7	,	,	PUNCT
ijpds-3748	105	8	a	a	DET
ijpds-3748	105	9	standard	standard	ADJ
ijpds-3748	105	10	stock	stock	NOUN
ijpds-3748	105	11	solution	solution	NOUN
ijpds-3748	105	12	of	of	ADP
ijpds-3748	105	13	empagliflozin	empagliflozin	PROPN
ijpds-3748	105	14	was	be	AUX
ijpds-3748	105	15	placed	place	VERB
ijpds-3748	105	16	in	in	ADP
ijpds-3748	105	17	a	a	DET
ijpds-3748	105	18	photostability	photostability	NOUN
ijpds-3748	105	19	chamber	chamber	NOUN
ijpds-3748	105	20	for	for	ADP
ijpds-3748	105	21	5	5	NUM
ijpds-3748	105	22	days	day	NOUN
ijpds-3748	105	23	.	.	PUNCT
ijpds-3748	106	1	then	then	ADV
ijpds-3748	106	2	after	after	ADP
ijpds-3748	106	3	5	5	NUM
ijpds-3748	106	4	days	day	NOUN
ijpds-3748	106	5	,	,	PUNCT
ijpds-3748	106	6	the	the	DET
ijpds-3748	106	7	powder	powder	NOUN
ijpds-3748	106	8	was	be	AUX
ijpds-3748	106	9	diluted	dilute	VERB
ijpds-3748	106	10	to	to	PART
ijpds-3748	106	11	make	make	VERB
ijpds-3748	106	12	the	the	DET
ijpds-3748	106	13	concentration	concentration	NOUN
ijpds-3748	106	14	of	of	ADP
ijpds-3748	106	15	about	about	ADV
ijpds-3748	106	16	5	5	NUM
ijpds-3748	106	17	µg	µg	ADV
ijpds-3748	106	18	/	/	SYM
ijpds-3748	106	19	ml	ml	NOUN
ijpds-3748	106	20	and	and	CCONJ
ijpds-3748	106	21	then	then	ADV
ijpds-3748	106	22	triplicate	triplicate	VERB
ijpds-3748	106	23	injections	injection	NOUN
ijpds-3748	106	24	were	be	AUX
ijpds-3748	106	25	applied	apply	VERB
ijpds-3748	106	26	to	to	ADP
ijpds-3748	106	27	the	the	DET
ijpds-3748	106	28	chromatograph	chromatograph	NOUN
ijpds-3748	106	29	and	and	CCONJ
ijpds-3748	106	30	the	the	DET
ijpds-3748	106	31	results	result	NOUN
ijpds-3748	106	32	for	for	ADP
ijpds-3748	106	33	possible	possible	ADJ
ijpds-3748	106	34	degradation	degradation	NOUN
ijpds-3748	106	35	were	be	AUX
ijpds-3748	106	36	observed	observe	VERB
ijpds-3748	106	37	.	.	PUNCT
ijpds-3748	107	1	the	the	DET
ijpds-3748	107	2	standard	standard	ADJ
ijpds-3748	107	3	solution	solution	NOUN
ijpds-3748	107	4	kept	keep	VERB
ijpds-3748	107	5	in	in	ADP
ijpds-3748	107	6	normal	normal	ADJ
ijpds-3748	107	7	condition	condition	NOUN
ijpds-3748	107	8	was	be	AUX
ijpds-3748	107	9	studied	study	VERB
ijpds-3748	107	10	versus	versus	ADP
ijpds-3748	107	11	the	the	DET
ijpds-3748	107	12	photolytic	photolytic	ADJ
ijpds-3748	107	13	standard	standard	ADJ
ijpds-3748	107	14	solution	solution	NOUN
ijpds-3748	107	15	and	and	CCONJ
ijpds-3748	107	16	then	then	ADV
ijpds-3748	107	17	the	the	DET
ijpds-3748	107	18	percentage	percentage	NOUN
ijpds-3748	107	19	degradation	degradation	NOUN
ijpds-3748	107	20	was	be	AUX
ijpds-3748	107	21	calculated	calculate	VERB
ijpds-3748	107	22	.	.	PUNCT
ijpds-3748	108	1	the	the	DET
ijpds-3748	108	2	results	result	NOUN
ijpds-3748	108	3	of	of	ADP
ijpds-3748	108	4	degradation	degradation	NOUN
ijpds-3748	108	5	studies	study	NOUN
ijpds-3748	108	6	were	be	AUX
ijpds-3748	108	7	depicted	depict	VERB
ijpds-3748	108	8	in	in	ADP
ijpds-3748	108	9	table	table	NOUN
ijpds-3748	108	10	8	8	NUM
ijpds-3748	108	11	.	.	PUNCT
ijpds-3748	108	12	results	result	NOUN
ijpds-3748	108	13	and	and	CCONJ
ijpds-3748	108	14	discussion	discussion	NOUN
ijpds-3748	108	15	with	with	ADP
ijpds-3748	108	16	the	the	DET
ijpds-3748	108	17	advancements	advancement	NOUN
ijpds-3748	108	18	in	in	ADP
ijpds-3748	108	19	technology	technology	NOUN
ijpds-3748	108	20	and	and	CCONJ
ijpds-3748	108	21	instrumentation	instrumentation	NOUN
ijpds-3748	108	22	,	,	PUNCT
ijpds-3748	108	23	there	there	PRON
ijpds-3748	108	24	comes	come	VERB
ijpds-3748	108	25	the	the	DET
ijpds-3748	108	26	requirement	requirement	NOUN
ijpds-3748	108	27	to	to	PART
ijpds-3748	108	28	design	design	VERB
ijpds-3748	108	29	an	an	DET
ijpds-3748	108	30	efficient	efficient	ADJ
ijpds-3748	108	31	,	,	PUNCT
ijpds-3748	108	32	dependable	dependable	ADJ
ijpds-3748	108	33	,	,	PUNCT
ijpds-3748	108	34	and	and	CCONJ
ijpds-3748	108	35	selective	selective	ADJ
ijpds-3748	108	36	quantification	quantification	NOUN
ijpds-3748	108	37	approach	approach	NOUN
ijpds-3748	108	38	for	for	ADP
ijpds-3748	108	39	active	active	ADJ
ijpds-3748	108	40	pharmaceutical	pharmaceutical	ADJ
ijpds-3748	108	41	components	component	NOUN
ijpds-3748	108	42	.	.	PUNCT
ijpds-3748	109	1	though	though	SCONJ
ijpds-3748	109	2	numerous	numerous	ADJ
ijpds-3748	109	3	analytical	analytical	ADJ
ijpds-3748	109	4	techniques	technique	NOUN
ijpds-3748	109	5	have	have	AUX
ijpds-3748	109	6	been	be	AUX
ijpds-3748	109	7	employed	employ	VERB
ijpds-3748	109	8	to	to	PART
ijpds-3748	109	9	estimate	estimate	VERB
ijpds-3748	109	10	drugs	drug	NOUN
ijpds-3748	109	11	,	,	PUNCT
ijpds-3748	109	12	researchers	researcher	NOUN
ijpds-3748	109	13	continue	continue	VERB
ijpds-3748	109	14	to	to	PART
ijpds-3748	109	15	develop	develop	VERB
ijpds-3748	109	16	alternative	alternative	ADJ
ijpds-3748	109	17	and	and	CCONJ
ijpds-3748	109	18	more	more	ADV
ijpds-3748	109	19	efficient	efficient	ADJ
ijpds-3748	109	20	hplc	hplc	NOUN
ijpds-3748	109	21	methods	method	NOUN
ijpds-3748	109	22	to	to	PART
ijpds-3748	109	23	quantify	quantify	VERB
ijpds-3748	109	24	a	a	DET
ijpds-3748	109	25	wide	wide	ADJ
ijpds-3748	109	26	range	range	NOUN
ijpds-3748	109	27	of	of	ADP
ijpds-3748	109	28	compounds	compound	NOUN
ijpds-3748	109	29	.	.	PUNCT
ijpds-3748	110	1	we	we	PRON
ijpds-3748	110	2	also	also	ADV
ijpds-3748	110	3	employed	employ	VERB
ijpds-3748	110	4	a	a	DET
ijpds-3748	110	5	novel	novel	ADJ
ijpds-3748	110	6	method	method	NOUN
ijpds-3748	110	7	for	for	ADP
ijpds-3748	110	8	the	the	DET
ijpds-3748	110	9	pharmaceutical	pharmaceutical	ADJ
ijpds-3748	110	10	assay	assay	NOUN
ijpds-3748	110	11	of	of	ADP
ijpds-3748	110	12	empagliflozin	empagliflozin	PROPN
ijpds-3748	110	13	tablets	tablet	NOUN
ijpds-3748	110	14	.	.	PUNCT
ijpds-3748	111	1	we	we	PRON
ijpds-3748	111	2	developed	develop	VERB
ijpds-3748	111	3	an	an	DET
ijpds-3748	111	4	accurate	accurate	ADJ
ijpds-3748	111	5	,	,	PUNCT
ijpds-3748	111	6	simple	simple	ADJ
ijpds-3748	111	7	,	,	PUNCT
ijpds-3748	111	8	and	and	CCONJ
ijpds-3748	111	9	stable	stable	ADJ
ijpds-3748	111	10	reverse	reverse	NOUN
ijpds-3748	111	11	phase	phase	NOUN
ijpds-3748	111	12	hplc	hplc	NOUN
ijpds-3748	111	13	method	method	NOUN
ijpds-3748	111	14	for	for	ADP
ijpds-3748	111	15	both	both	CCONJ
ijpds-3748	111	16	qualitative	qualitative	ADJ
ijpds-3748	111	17	and	and	CCONJ
ijpds-3748	111	18	quantitative	quantitative	ADJ
ijpds-3748	111	19	estimation	estimation	NOUN
ijpds-3748	111	20	of	of	ADP
ijpds-3748	111	21	empagliflozin	empagliflozin	NOUN
ijpds-3748	111	22	using	use	VERB
ijpds-3748	111	23	different	different	ADJ
ijpds-3748	111	24	ratios	ratio	NOUN
ijpds-3748	111	25	of	of	ADP
ijpds-3748	111	26	mobile	mobile	ADJ
ijpds-3748	111	27	phase	phase	NOUN
ijpds-3748	111	28	,	,	PUNCT
ijpds-3748	111	29	different	different	ADJ
ijpds-3748	111	30	chromatographic	chromatographic	ADJ
ijpds-3748	111	31	conditions	condition	NOUN
ijpds-3748	111	32	,	,	PUNCT
ijpds-3748	111	33	diluents	diluent	NOUN
ijpds-3748	111	34	,	,	PUNCT
ijpds-3748	111	35	and	and	CCONJ
ijpds-3748	111	36	flow	flow	NOUN
ijpds-3748	111	37	rates	rate	NOUN
ijpds-3748	111	38	for	for	ADP
ijpds-3748	111	39	analysis	analysis	NOUN
ijpds-3748	111	40	.	.	PUNCT
ijpds-3748	112	1	in	in	ADP
ijpds-3748	112	2	optimal	optimal	ADJ
ijpds-3748	112	3	conditions	condition	NOUN
ijpds-3748	112	4	of	of	ADP
ijpds-3748	112	5	isocratic	isocratic	ADJ
ijpds-3748	112	6	mobile	mobile	ADJ
ijpds-3748	112	7	phase	phase	NOUN
ijpds-3748	112	8	with	with	ADP
ijpds-3748	112	9	the	the	DET
ijpds-3748	112	10	combination	combination	NOUN
ijpds-3748	112	11	of	of	ADP
ijpds-3748	112	12	phosphate	phosphate	ADJ
ijpds-3748	112	13	buffer	buffer	NOUN
ijpds-3748	112	14	ph	ph	VERB
ijpds-3748	112	15	3.0	3.0	NUM
ijpds-3748	112	16	and	and	CCONJ
ijpds-3748	112	17	methanol	methanol	NOUN
ijpds-3748	112	18	(	(	PUNCT
ijpds-3748	112	19	70:30	70:30	NUM
ijpds-3748	112	20	)	)	PUNCT
ijpds-3748	112	21	,	,	PUNCT
ijpds-3748	112	22	c18	c18	NOUN
ijpds-3748	112	23	column	column	NOUN
ijpds-3748	112	24	(	(	PUNCT
ijpds-3748	112	25	150x4.6	150x4.6	NOUN
ijpds-3748	112	26	mm	mm	NOUN
ijpds-3748	112	27	)	)	PUNCT
ijpds-3748	112	28	with	with	ADP
ijpds-3748	112	29	particle	particle	NOUN
ijpds-3748	112	30	size	size	NOUN
ijpds-3748	112	31	5μm	5μm	ADJ
ijpds-3748	112	32	and	and	CCONJ
ijpds-3748	112	33	flow	flow	NOUN
ijpds-3748	112	34	rate	rate	NOUN
ijpds-3748	112	35	of	of	ADP
ijpds-3748	112	36	1.0	1.0	NUM
ijpds-3748	112	37	ml	ml	NOUN
ijpds-3748	112	38	per	per	ADP
ijpds-3748	112	39	minute	minute	NOUN
ijpds-3748	112	40	,	,	PUNCT
ijpds-3748	112	41	accurate	accurate	ADJ
ijpds-3748	112	42	and	and	CCONJ
ijpds-3748	112	43	precise	precise	ADJ
ijpds-3748	112	44	results	result	NOUN
ijpds-3748	112	45	were	be	AUX
ijpds-3748	112	46	obtained	obtain	VERB
ijpds-3748	112	47	.	.	PUNCT
ijpds-3748	113	1	the	the	DET
ijpds-3748	113	2	results	result	NOUN
ijpds-3748	113	3	of	of	ADP
ijpds-3748	113	4	system	system	NOUN
ijpds-3748	113	5	suitability	suitability	NOUN
ijpds-3748	113	6	,	,	PUNCT
ijpds-3748	113	7	specificity	specificity	NOUN
ijpds-3748	113	8	,	,	PUNCT
ijpds-3748	113	9	linearity	linearity	NOUN
ijpds-3748	113	10	,	,	PUNCT
ijpds-3748	113	11	and	and	CCONJ
ijpds-3748	113	12	robustness	robustness	NOUN
ijpds-3748	113	13	were	be	AUX
ijpds-3748	113	14	all	all	ADV
ijpds-3748	113	15	within	within	ADP
ijpds-3748	113	16	good	good	ADJ
ijpds-3748	113	17	acceptable	acceptable	ADJ
ijpds-3748	113	18	limits	limit	NOUN
ijpds-3748	113	19	.	.	PUNCT
ijpds-3748	114	1	there	there	PRON
ijpds-3748	114	2	was	be	VERB
ijpds-3748	114	3	no	no	DET
ijpds-3748	114	4	interaction	interaction	NOUN
ijpds-3748	114	5	of	of	ADP
ijpds-3748	114	6	solvents	solvent	NOUN
ijpds-3748	114	7	like	like	ADP
ijpds-3748	114	8	mobile	mobile	ADJ
ijpds-3748	114	9	phase	phase	NOUN
ijpds-3748	114	10	,	,	PUNCT
ijpds-3748	114	11	diluents	diluent	NOUN
ijpds-3748	114	12	,	,	PUNCT
ijpds-3748	114	13	and	and	CCONJ
ijpds-3748	114	14	excipients	excipient	NOUN
ijpds-3748	114	15	with	with	ADP
ijpds-3748	114	16	the	the	DET
ijpds-3748	114	17	peak	peak	NOUN
ijpds-3748	114	18	of	of	ADP
ijpds-3748	114	19	empagliflozin	empagliflozin	PROPN
ijpds-3748	114	20	.	.	PUNCT
ijpds-3748	115	1	additionally	additionally	ADV
ijpds-3748	115	2	,	,	PUNCT
ijpds-3748	115	3	statistical	statistical	ADJ
ijpds-3748	115	4	analysis	analysis	NOUN
ijpds-3748	115	5	revealed	reveal	VERB
ijpds-3748	115	6	negligible	negligible	ADJ
ijpds-3748	115	7	differences	difference	NOUN
ijpds-3748	115	8	between	between	ADP
ijpds-3748	115	9	the	the	DET
ijpds-3748	115	10	peak	peak	NOUN
ijpds-3748	115	11	areas	area	NOUN
ijpds-3748	115	12	during	during	ADP
ijpds-3748	115	13	precision	precision	NOUN
ijpds-3748	115	14	,	,	PUNCT
ijpds-3748	115	15	suitability	suitability	NOUN
ijpds-3748	115	16	,	,	PUNCT
ijpds-3748	115	17	and	and	CCONJ
ijpds-3748	115	18	repeatability	repeatability	NOUN
ijpds-3748	115	19	studies	study	NOUN
ijpds-3748	115	20	.	.	PUNCT
ijpds-3748	116	1	a	a	DET
ijpds-3748	116	2	fit	fit	ADJ
ijpds-3748	116	3	value	value	NOUN
ijpds-3748	116	4	of	of	ADP
ijpds-3748	116	5	0.9996	0.9996	NUM
ijpds-3748	116	6	was	be	AUX
ijpds-3748	116	7	obtained	obtain	VERB
ijpds-3748	116	8	for	for	ADP
ijpds-3748	116	9	the	the	DET
ijpds-3748	116	10	regression	regression	NOUN
ijpds-3748	116	11	equation	equation	NOUN
ijpds-3748	116	12	y	y	PROPN
ijpds-3748	116	13	=	=	SYM
ijpds-3748	116	14	845241x	845241x	PROPN
ijpds-3748	116	15	,	,	PUNCT
ijpds-3748	116	16	indicating	indicate	VERB
ijpds-3748	116	17	a	a	DET
ijpds-3748	116	18	strong	strong	ADJ
ijpds-3748	116	19	correlation	correlation	NOUN
ijpds-3748	116	20	.	.	PUNCT
ijpds-3748	117	1	it	it	PRON
ijpds-3748	117	2	was	be	AUX
ijpds-3748	117	3	discovered	discover	VERB
ijpds-3748	117	4	that	that	SCONJ
ijpds-3748	117	5	the	the	DET
ijpds-3748	117	6	minimal	minimal	ADJ
ijpds-3748	117	7	detection	detection	NOUN
ijpds-3748	117	8	and	and	CCONJ
ijpds-3748	117	9	quantification	quantification	NOUN
ijpds-3748	117	10	limits	limit	NOUN
ijpds-3748	117	11	were	be	AUX
ijpds-3748	117	12	0.068	0.068	NUM
ijpds-3748	117	13	µg	µg	NOUN
ijpds-3748	117	14	/	/	SYM
ijpds-3748	117	15	ml	ml	NOUN
ijpds-3748	117	16	and	and	CCONJ
ijpds-3748	117	17	0.35	0.35	NUM
ijpds-3748	117	18	µg	µg	NOUN
ijpds-3748	117	19	/	/	SYM
ijpds-3748	117	20	ml	ml	NOUN
ijpds-3748	117	21	,	,	PUNCT
ijpds-3748	117	22	respectively	respectively	ADV
ijpds-3748	117	23	.	.	PUNCT
ijpds-3748	118	1	due	due	ADP
ijpds-3748	118	2	to	to	ADP
ijpds-3748	118	3	the	the	DET
ijpds-3748	118	4	proper	proper	ADJ
ijpds-3748	118	5	selection	selection	NOUN
ijpds-3748	118	6	and	and	CCONJ
ijpds-3748	118	7	composition	composition	NOUN
ijpds-3748	118	8	of	of	ADP
ijpds-3748	118	9	the	the	DET
ijpds-3748	118	10	mobile	mobile	ADJ
ijpds-3748	118	11	phase	phase	NOUN
ijpds-3748	118	12	,	,	PUNCT
ijpds-3748	118	13	the	the	DET
ijpds-3748	118	14	reduced	reduced	ADJ
ijpds-3748	118	15	detection	detection	NOUN
ijpds-3748	118	16	values	value	NOUN
ijpds-3748	118	17	in	in	ADP
ijpds-3748	118	18	our	our	PRON
ijpds-3748	118	19	investigation	investigation	NOUN
ijpds-3748	118	20	were	be	AUX
ijpds-3748	118	21	noted	note	VERB
ijpds-3748	118	22	.	.	PUNCT
ijpds-3748	119	1	lower	low	ADJ
ijpds-3748	119	2	standard	standard	ADJ
ijpds-3748	119	3	deviations	deviation	NOUN
ijpds-3748	119	4	and	and	CCONJ
ijpds-3748	119	5	coefficients	coefficient	NOUN
ijpds-3748	119	6	of	of	ADP
ijpds-3748	119	7	variation	variation	NOUN
ijpds-3748	119	8	were	be	AUX
ijpds-3748	119	9	found	find	VERB
ijpds-3748	119	10	in	in	ADP
ijpds-3748	119	11	the	the	DET
ijpds-3748	119	12	drug	drug	NOUN
ijpds-3748	119	13	assay	assay	NOUN
ijpds-3748	119	14	results	result	NOUN
ijpds-3748	119	15	,	,	PUNCT
ijpds-3748	119	16	indicating	indicate	VERB
ijpds-3748	119	17	good	good	ADJ
ijpds-3748	119	18	procedure	procedure	NOUN
ijpds-3748	119	19	accuracy	accuracy	NOUN
ijpds-3748	119	20	.	.	PUNCT
ijpds-3748	120	1	the	the	DET
ijpds-3748	120	2	peak	peak	NOUN
ijpds-3748	120	3	purity	purity	NOUN
ijpds-3748	120	4	of	of	ADP
ijpds-3748	120	5	a	a	DET
ijpds-3748	120	6	sample	sample	NOUN
ijpds-3748	120	7	depends	depend	VERB
ijpds-3748	120	8	on	on	ADP
ijpds-3748	120	9	the	the	DET
ijpds-3748	120	10	selectivity	selectivity	NOUN
ijpds-3748	120	11	and	and	CCONJ
ijpds-3748	120	12	specificity	specificity	NOUN
ijpds-3748	120	13	of	of	ADP
ijpds-3748	120	14	an	an	DET
ijpds-3748	120	15	analyte	analyte	NOUN
ijpds-3748	120	16	.	.	PUNCT
ijpds-3748	121	1	for	for	ADP
ijpds-3748	121	2	confirmation	confirmation	NOUN
ijpds-3748	121	3	of	of	ADP
ijpds-3748	121	4	peak	peak	NOUN
ijpds-3748	121	5	purity	purity	NOUN
ijpds-3748	121	6	,	,	PUNCT
ijpds-3748	121	7	the	the	DET
ijpds-3748	121	8	drug	drug	NOUN
ijpds-3748	121	9	solution	solution	NOUN
ijpds-3748	121	10	was	be	AUX
ijpds-3748	121	11	also	also	ADV
ijpds-3748	121	12	tested	test	VERB
ijpds-3748	121	13	against	against	ADP
ijpds-3748	121	14	a	a	DET
ijpds-3748	121	15	placebo	placebo	NOUN
ijpds-3748	121	16	mixture	mixture	NOUN
ijpds-3748	121	17	(	(	PUNCT
ijpds-3748	121	18	with	with	ADP
ijpds-3748	121	19	excipients	excipient	NOUN
ijpds-3748	121	20	used	use	VERB
ijpds-3748	121	21	in	in	ADP
ijpds-3748	121	22	tablet	tablet	NOUN
ijpds-3748	121	23	formulations).a	formulations).a	PROPN
ijpds-3748	121	24	lack	lack	NOUN
ijpds-3748	121	25	of	of	ADP
ijpds-3748	121	26	co	co	NOUN
ijpds-3748	121	27	-	-	NOUN
ijpds-3748	121	28	elution	elution	NOUN
ijpds-3748	121	29	peaks	peak	NOUN
ijpds-3748	121	30	during	during	ADP
ijpds-3748	121	31	the	the	DET
ijpds-3748	121	32	drug	drug	NOUN
ijpds-3748	121	33	sample	sample	NOUN
ijpds-3748	121	34	's	's	PART
ijpds-3748	121	35	retention	retention	NOUN
ijpds-3748	121	36	time	time	NOUN
ijpds-3748	121	37	indicated	indicate	VERB
ijpds-3748	121	38	that	that	SCONJ
ijpds-3748	121	39	the	the	DET
ijpds-3748	121	40	current	current	ADJ
ijpds-3748	121	41	approach	approach	NOUN
ijpds-3748	121	42	was	be	AUX
ijpds-3748	121	43	suggestive	suggestive	ADJ
ijpds-3748	121	44	of	of	ADP
ijpds-3748	121	45	both	both	CCONJ
ijpds-3748	121	46	selectivity	selectivity	NOUN
ijpds-3748	121	47	and	and	CCONJ
ijpds-3748	121	48	specificity	specificity	NOUN
ijpds-3748	121	49	.	.	PUNCT
ijpds-3748	122	1	since	since	SCONJ
ijpds-3748	122	2	there	there	PRON
ijpds-3748	122	3	was	be	VERB
ijpds-3748	122	4	no	no	DET
ijpds-3748	122	5	peak	peak	NOUN
ijpds-3748	122	6	of	of	ADP
ijpds-3748	122	7	any	any	DET
ijpds-3748	122	8	additive	additive	NOUN
ijpds-3748	122	9	during	during	ADP
ijpds-3748	122	10	the	the	DET
ijpds-3748	122	11	analytical	analytical	ADJ
ijpds-3748	122	12	run	run	NOUN
ijpds-3748	122	13	of	of	ADP
ijpds-3748	122	14	empagliflozin	empagliflozin	PROPN
ijpds-3748	122	15	,	,	PUNCT
ijpds-3748	122	16	the	the	DET
ijpds-3748	122	17	devised	devise	VERB
ijpds-3748	122	18	method	method	NOUN
ijpds-3748	122	19	can	can	AUX
ijpds-3748	122	20	be	be	AUX
ijpds-3748	122	21	effectively	effectively	ADV
ijpds-3748	122	22	used	use	VERB
ijpds-3748	122	23	to	to	PART
ijpds-3748	122	24	quantify	quantify	VERB
ijpds-3748	122	25	the	the	DET
ijpds-3748	122	26	medicine	medicine	NOUN
ijpds-3748	122	27	in	in	ADP
ijpds-3748	122	28	the	the	DET
ijpds-3748	122	29	marketed	market	VERB
ijpds-3748	122	30	tablets	tablet	NOUN
ijpds-3748	122	31	.	.	PUNCT
ijpds-3748	123	1	the	the	DET
ijpds-3748	123	2	underlying	underlying	ADJ
ijpds-3748	123	3	methodology	methodology	NOUN
ijpds-3748	123	4	was	be	AUX
ijpds-3748	123	5	confirmed	confirm	VERB
ijpds-3748	123	6	to	to	PART
ijpds-3748	123	7	be	be	AUX
ijpds-3748	123	8	reliable	reliable	ADJ
ijpds-3748	123	9	because	because	SCONJ
ijpds-3748	123	10	no	no	DET
ijpds-3748	123	11	concentration	concentration	NOUN
ijpds-3748	123	12	change	change	NOUN
ijpds-3748	123	13	was	be	AUX
ijpds-3748	123	14	seen	see	VERB
ijpds-3748	123	15	when	when	SCONJ
ijpds-3748	123	16	the	the	DET
ijpds-3748	123	17	flow	flow	NOUN
ijpds-3748	123	18	rate	rate	NOUN
ijpds-3748	123	19	,	,	PUNCT
ijpds-3748	123	20	column	column	NOUN
ijpds-3748	123	21	temperature	temperature	NOUN
ijpds-3748	123	22	,	,	PUNCT
ijpds-3748	123	23	or	or	CCONJ
ijpds-3748	123	24	mobile	mobile	ADJ
ijpds-3748	123	25	phase	phase	NOUN
ijpds-3748	123	26	composition	composition	NOUN
ijpds-3748	123	27	ahmad	ahmad	NOUN
ijpds-3748	123	28	et	et	PROPN
ijpds-3748	123	29	al	al	PROPN
ijpds-3748	123	30	rp	rp	PROPN
ijpds-3748	123	31	-	-	PUNCT
ijpds-3748	123	32	hplc	hplc	NOUN
ijpds-3748	123	33	method	method	NOUN
ijpds-3748	123	34	validation	validation	NOUN
ijpds-3748	123	35	of	of	ADP
ijpds-3748	123	36	empagliflozin	empagliflozin	PROPN
ijpds-3748	123	37	vol	vol	NOUN
ijpds-3748	123	38	2	2	NUM
ijpds-3748	123	39	|	|	NOUN
ijpds-3748	123	40	issue	issue	NOUN
ijpds-3748	123	41	2	2	NUM
ijpds-3748	123	42	|	|	ADV
ijpds-3748	123	43	apr	apr	ADV
ijpds-3748	123	44	–	–	PUNCT
ijpds-3748	123	45	jun	jun	PROPN
ijpds-3748	123	46	2023	2023	NUM
ijpds-3748	123	47	indian	indian	PROPN
ijpds-3748	123	48	j	j	PROPN
ijpds-3748	123	49	pharm	pharm	PROPN
ijpds-3748	123	50	drug	drug	PROPN
ijpds-3748	123	51	studies	study	NOUN
ijpds-3748	123	52	|	|	ADV
ijpds-3748	123	53	81	81	NUM
ijpds-3748	123	54	was	be	AUX
ijpds-3748	123	55	changed	change	VERB
ijpds-3748	123	56	.	.	PUNCT
ijpds-3748	124	1	previous	previous	ADJ
ijpds-3748	124	2	studies	study	NOUN
ijpds-3748	124	3	also	also	ADV
ijpds-3748	124	4	confirmed	confirm	VERB
ijpds-3748	124	5	the	the	DET
ijpds-3748	124	6	reliability	reliability	NOUN
ijpds-3748	124	7	of	of	ADP
ijpds-3748	124	8	analytical	analytical	ADJ
ijpds-3748	124	9	methods	method	NOUN
ijpds-3748	124	10	,	,	PUNCT
ijpds-3748	124	11	frequently	frequently	ADV
ijpds-3748	124	12	by	by	ADP
ijpds-3748	124	13	altering	alter	VERB
ijpds-3748	124	14	the	the	DET
ijpds-3748	124	15	solvent	solvent	NOUN
ijpds-3748	124	16	composition	composition	NOUN
ijpds-3748	124	17	,	,	PUNCT
ijpds-3748	124	18	flow	flow	NOUN
ijpds-3748	124	19	rate	rate	NOUN
ijpds-3748	124	20	,	,	PUNCT
ijpds-3748	124	21	and	and	CCONJ
ijpds-3748	124	22	column	column	NOUN
ijpds-3748	124	23	temperature	temperature	NOUN
ijpds-3748	124	24	to	to	ADP
ijpds-3748	124	25	a	a	DET
ijpds-3748	124	26	limited	limited	ADJ
ijpds-3748	124	27	extent	extent	NOUN
ijpds-3748	124	28	[	[	X
ijpds-3748	124	29	22	22	NUM
ijpds-3748	124	30	]	]	PUNCT
ijpds-3748	124	31	.	.	PUNCT
ijpds-3748	125	1	based	base	VERB
ijpds-3748	125	2	on	on	ADP
ijpds-3748	125	3	the	the	DET
ijpds-3748	125	4	results	result	NOUN
ijpds-3748	125	5	,	,	PUNCT
ijpds-3748	125	6	it	it	PRON
ijpds-3748	125	7	can	can	AUX
ijpds-3748	125	8	be	be	AUX
ijpds-3748	125	9	concluded	conclude	VERB
ijpds-3748	125	10	that	that	SCONJ
ijpds-3748	125	11	the	the	DET
ijpds-3748	125	12	present	present	ADJ
ijpds-3748	125	13	method	method	NOUN
ijpds-3748	125	14	can	can	AUX
ijpds-3748	125	15	be	be	AUX
ijpds-3748	125	16	employed	employ	VERB
ijpds-3748	125	17	in	in	ADP
ijpds-3748	125	18	pharmaceutical	pharmaceutical	NOUN
ijpds-3748	125	19	labs	lab	NOUN
ijpds-3748	125	20	for	for	ADP
ijpds-3748	125	21	routine	routine	ADJ
ijpds-3748	125	22	quality	quality	NOUN
ijpds-3748	125	23	control	control	NOUN
ijpds-3748	125	24	testing	testing	NOUN
ijpds-3748	125	25	and	and	CCONJ
ijpds-3748	125	26	can	can	AUX
ijpds-3748	125	27	serve	serve	VERB
ijpds-3748	125	28	as	as	ADP
ijpds-3748	125	29	a	a	DET
ijpds-3748	125	30	basis	basis	NOUN
ijpds-3748	125	31	for	for	ADP
ijpds-3748	125	32	further	further	ADJ
ijpds-3748	125	33	modifications	modification	NOUN
ijpds-3748	125	34	in	in	ADP
ijpds-3748	125	35	the	the	DET
ijpds-3748	125	36	method	method	NOUN
ijpds-3748	125	37	in	in	ADP
ijpds-3748	125	38	the	the	DET
ijpds-3748	125	39	future	future	NOUN
ijpds-3748	125	40	.	.	PUNCT
ijpds-3748	126	1	conclusion	conclusion	NOUN
ijpds-3748	126	2	validation	validation	NOUN
ijpds-3748	126	3	parameters	parameter	NOUN
ijpds-3748	126	4	mentioned	mention	VERB
ijpds-3748	126	5	in	in	ADP
ijpds-3748	126	6	the	the	DET
ijpds-3748	126	7	recent	recent	ADJ
ijpds-3748	126	8	study	study	NOUN
ijpds-3748	126	9	were	be	AUX
ijpds-3748	126	10	checked	check	VERB
ijpds-3748	126	11	according	accord	VERB
ijpds-3748	126	12	to	to	ADP
ijpds-3748	126	13	ich	ich	NOUN
ijpds-3748	126	14	guidelines	guideline	NOUN
ijpds-3748	126	15	and	and	CCONJ
ijpds-3748	126	16	satisfactory	satisfactory	ADJ
ijpds-3748	126	17	results	result	NOUN
ijpds-3748	126	18	were	be	AUX
ijpds-3748	126	19	obtained	obtain	VERB
ijpds-3748	126	20	.	.	PUNCT
ijpds-3748	127	1	a	a	DET
ijpds-3748	127	2	stress	stress	NOUN
ijpds-3748	127	3	stability	stability	NOUN
ijpds-3748	127	4	study	study	NOUN
ijpds-3748	127	5	confirmed	confirm	VERB
ijpds-3748	127	6	that	that	SCONJ
ijpds-3748	127	7	the	the	DET
ijpds-3748	127	8	method	method	NOUN
ijpds-3748	127	9	is	be	AUX
ijpds-3748	127	10	stability	stability	NOUN
ijpds-3748	127	11	-	-	PUNCT
ijpds-3748	127	12	indicating	indicate	VERB
ijpds-3748	127	13	.	.	PUNCT
ijpds-3748	128	1	therefore	therefore	ADV
ijpds-3748	128	2	,	,	PUNCT
ijpds-3748	128	3	based	base	VERB
ijpds-3748	128	4	on	on	ADP
ijpds-3748	128	5	the	the	DET
ijpds-3748	128	6	study	study	NOUN
ijpds-3748	128	7	conducted	conduct	VERB
ijpds-3748	128	8	it	it	PRON
ijpds-3748	128	9	can	can	AUX
ijpds-3748	128	10	be	be	AUX
ijpds-3748	128	11	ensured	ensure	VERB
ijpds-3748	128	12	that	that	SCONJ
ijpds-3748	128	13	the	the	DET
ijpds-3748	128	14	method	method	NOUN
ijpds-3748	128	15	can	can	AUX
ijpds-3748	128	16	be	be	AUX
ijpds-3748	128	17	applied	apply	VERB
ijpds-3748	128	18	to	to	ADP
ijpds-3748	128	19	the	the	DET
ijpds-3748	128	20	pharmaceutical	pharmaceutical	ADJ
ijpds-3748	128	21	lab	lab	NOUN
ijpds-3748	128	22	for	for	ADP
ijpds-3748	128	23	routine	routine	ADJ
ijpds-3748	128	24	analysis	analysis	NOUN
ijpds-3748	128	25	of	of	ADP
ijpds-3748	128	26	tablet	tablet	ADJ
ijpds-3748	128	27	dosage	dosage	NOUN
ijpds-3748	128	28	form	form	NOUN
ijpds-3748	128	29	.	.	PUNCT
ijpds-3748	129	1	references	reference	NOUN
ijpds-3748	129	2	1	1	NUM
ijpds-3748	129	3	.	.	PUNCT
ijpds-3748	130	1	frampton	frampton	PROPN
ijpds-3748	130	2	je	je	PROPN
ijpds-3748	130	3	.	.	PUNCT
ijpds-3748	130	4	empagliflozin	empagliflozin	PROPN
ijpds-3748	130	5	.	.	PUNCT
ijpds-3748	131	1	a	a	DET
ijpds-3748	131	2	review	review	NOUN
ijpds-3748	131	3	in	in	ADP
ijpds-3748	131	4	type	type	NOUN
ijpds-3748	131	5	2	2	NUM
ijpds-3748	131	6	diabetes	diabetes	NOUN
ijpds-3748	131	7	.	.	PUNCT
ijpds-3748	132	1	drugs	drug	NOUN
ijpds-3748	133	1	[	[	X
ijpds-3748	133	2	internet	internet	NOUN
ijpds-3748	133	3	]	]	PUNCT
ijpds-3748	133	4	.	.	PUNCT
ijpds-3748	134	1	2018	2018	NUM
ijpds-3748	134	2	;	;	PUNCT
ijpds-3748	134	3	78	78	NUM
ijpds-3748	134	4	(	(	PUNCT
ijpds-3748	134	5	10):1037–48	10):1037–48	NUM
ijpds-3748	134	6	.	.	NOUN
ijpds-3748	135	1	2	2	NUM
ijpds-3748	135	2	.	.	X
ijpds-3748	135	3	lamos	lamos	PROPN
ijpds-3748	135	4	em	em	PRON
ijpds-3748	135	5	,	,	PUNCT
ijpds-3748	135	6	younk	younk	NOUN
ijpds-3748	135	7	lm	lm	PROPN
ijpds-3748	135	8	,	,	PUNCT
ijpds-3748	135	9	davis	davis	PROPN
ijpds-3748	135	10	sn	sn	PROPN
ijpds-3748	135	11	.	.	PUNCT
ijpds-3748	136	1	empagliflozin	empagliflozin	PROPN
ijpds-3748	136	2	,	,	PUNCT
ijpds-3748	136	3	a	a	DET
ijpds-3748	136	4	sodium	sodium	NOUN
ijpds-3748	136	5	glucose	glucose	NOUN
ijpds-3748	136	6	co	co	NOUN
ijpds-3748	136	7	-	-	NOUN
ijpds-3748	136	8	transporter	transporter	ADJ
ijpds-3748	136	9	2	2	NUM
ijpds-3748	136	10	inhibitor	inhibitor	NOUN
ijpds-3748	136	11	,	,	PUNCT
ijpds-3748	136	12	in	in	ADP
ijpds-3748	136	13	the	the	DET
ijpds-3748	136	14	treatment	treatment	NOUN
ijpds-3748	136	15	of	of	ADP
ijpds-3748	136	16	type	type	NOUN
ijpds-3748	136	17	1	1	NUM
ijpds-3748	136	18	diabetes	diabetes	NOUN
ijpds-3748	136	19	.	.	PUNCT
ijpds-3748	137	1	expert	expert	NOUN
ijpds-3748	137	2	opin	opin	NOUN
ijpds-3748	137	3	investig	investig	NOUN
ijpds-3748	137	4	drugs	drug	NOUN
ijpds-3748	137	5	.	.	PUNCT
ijpds-3748	138	1	2014	2014	NUM
ijpds-3748	138	2	;	;	PUNCT
ijpds-3748	138	3	23(6	23(6	NUM
ijpds-3748	138	4	):	):	PUNCT
ijpds-3748	138	5	875–82	875–82	NOUN
ijpds-3748	138	6	.	.	PUNCT
ijpds-3748	139	1	3	3	X
ijpds-3748	139	2	.	.	X
ijpds-3748	139	3	empagliflozin	empagliflozin	PROPN
ijpds-3748	139	4	monograph	monograph	PROPN
ijpds-3748	139	5	for	for	ADP
ijpds-3748	139	6	professionals	professional	NOUN
ijpds-3748	139	7	"	"	PUNCT
ijpds-3748	139	8	.	.	PUNCT
ijpds-3748	140	1	drugs.com	drugs.com	X
ijpds-3748	140	2	.	.	PROPN
ijpds-3748	140	3	ahfs	ahfs	PROPN
ijpds-3748	140	4	.	.	PUNCT
ijpds-3748	141	1	retrieved	retrieve	VERB
ijpds-3748	141	2	dec	dec	PROPN
ijpds-3748	141	3	2018	2018	NUM
ijpds-3748	141	4	.	.	PUNCT
ijpds-3748	142	1	4	4	X
ijpds-3748	142	2	.	.	X
ijpds-3748	142	3	davies	davies	PROPN
ijpds-3748	142	4	mj	mj	PROPN
ijpds-3748	142	5	,	,	PUNCT
ijpds-3748	142	6	d’alessio	d’alessio	PROPN
ijpds-3748	142	7	da	da	PROPN
ijpds-3748	142	8	,	,	PUNCT
ijpds-3748	142	9	fradkin	fradkin	PROPN
ijpds-3748	142	10	j	j	PROPN
ijpds-3748	142	11	,	,	PUNCT
ijpds-3748	142	12	et	et	PROPN
ijpds-3748	142	13	al	al	PROPN
ijpds-3748	142	14	.	.	PUNCT
ijpds-3748	142	15	management	management	NOUN
ijpds-3748	142	16	of	of	ADP
ijpds-3748	142	17	hyperglycemia	hyperglycemia	NOUN
ijpds-3748	142	18	in	in	ADP
ijpds-3748	142	19	type	type	NOUN
ijpds-3748	142	20	2	2	NUM
ijpds-3748	142	21	diabetes	diabete	NOUN
ijpds-3748	142	22	,	,	PUNCT
ijpds-3748	142	23	2018	2018	NUM
ijpds-3748	142	24	.	.	PUNCT
ijpds-3748	143	1	a	a	DET
ijpds-3748	143	2	consensus	consensus	NOUN
ijpds-3748	143	3	report	report	NOUN
ijpds-3748	143	4	by	by	ADP
ijpds-3748	143	5	the	the	DET
ijpds-3748	143	6	american	american	ADJ
ijpds-3748	143	7	diabetes	diabetes	PROPN
ijpds-3748	143	8	association	association	PROPN
ijpds-3748	143	9	(	(	PUNCT
ijpds-3748	143	10	ada	ada	PROPN
ijpds-3748	143	11	)	)	PUNCT
ijpds-3748	143	12	and	and	CCONJ
ijpds-3748	143	13	the	the	DET
ijpds-3748	143	14	european	european	PROPN
ijpds-3748	143	15	association	association	PROPN
ijpds-3748	143	16	for	for	ADP
ijpds-3748	143	17	the	the	DET
ijpds-3748	143	18	study	study	NOUN
ijpds-3748	143	19	of	of	ADP
ijpds-3748	143	20	diabetes	diabetes	NOUN
ijpds-3748	143	21	(	(	PUNCT
ijpds-3748	143	22	easd	easd	NOUN
ijpds-3748	143	23	)	)	PUNCT
ijpds-3748	143	24	.	.	PUNCT
ijpds-3748	144	1	diabetes	diabetes	NOUN
ijpds-3748	144	2	care	care	NOUN
ijpds-3748	144	3	.	.	PUNCT
ijpds-3748	145	1	2018	2018	NUM
ijpds-3748	145	2	;	;	PUNCT
ijpds-3748	145	3	41(12):2669–701	41(12):2669–701	X
ijpds-3748	145	4	.	.	NOUN
ijpds-3748	146	1	5	5	X
ijpds-3748	146	2	.	.	X
ijpds-3748	146	3	kinduryte	kinduryte	PROPN
ijpds-3748	146	4	schorling	schorle	VERB
ijpds-3748	146	5	o	o	PROPN
ijpds-3748	146	6	,	,	PUNCT
ijpds-3748	146	7	clark	clark	PROPN
ijpds-3748	146	8	d	d	PROPN
ijpds-3748	146	9	,	,	PUNCT
ijpds-3748	146	10	zwiener	zwiener	PROPN
ijpds-3748	146	11	i	i	PROPN
ijpds-3748	146	12	,	,	PUNCT
ijpds-3748	146	13	et	et	PROPN
ijpds-3748	146	14	al	al	PROPN
ijpds-3748	146	15	.	.	PROPN
ijpds-3748	146	16	pooled	pool	VERB
ijpds-3748	146	17	safety	safety	NOUN
ijpds-3748	146	18	and	and	CCONJ
ijpds-3748	146	19	tolerability	tolerability	NOUN
ijpds-3748	146	20	analysis	analysis	NOUN
ijpds-3748	146	21	of	of	ADP
ijpds-3748	146	22	empagliflozin	empagliflozin	PROPN
ijpds-3748	146	23	in	in	ADP
ijpds-3748	146	24	patients	patient	NOUN
ijpds-3748	146	25	with	with	ADP
ijpds-3748	146	26	type	type	NOUN
ijpds-3748	146	27	2	2	NUM
ijpds-3748	146	28	diabetes	diabetes	NOUN
ijpds-3748	146	29	mellitus	mellitus	NOUN
ijpds-3748	146	30	.	.	PUNCT
ijpds-3748	147	1	adv	adv	INTJ
ijpds-3748	147	2	ther	ther	ADV
ijpds-3748	147	3	.	.	PUNCT
ijpds-3748	148	1	2020	2020	NUM
ijpds-3748	148	2	;	;	PUNCT
ijpds-3748	148	3	37(8):3463–84	37(8):3463–84	NUM
ijpds-3748	148	4	.	.	PUNCT
ijpds-3748	149	1	6	6	NUM
ijpds-3748	149	2	.	.	PUNCT
ijpds-3748	149	3	kinch	kinch	PROPN
ijpds-3748	149	4	ms	ms	PROPN
ijpds-3748	149	5	,	,	PUNCT
ijpds-3748	149	6	griesenauer	griesenauer	PROPN
ijpds-3748	149	7	rh	rh	PROPN
ijpds-3748	149	8	.	.	PROPN
ijpds-3748	149	9	2018	2018	NUM
ijpds-3748	149	10	in	in	ADP
ijpds-3748	149	11	review	review	NOUN
ijpds-3748	149	12	:	:	PUNCT
ijpds-3748	149	13	fda	fda	PROPN
ijpds-3748	149	14	approvals	approval	NOUN
ijpds-3748	149	15	of	of	ADP
ijpds-3748	149	16	new	new	ADJ
ijpds-3748	149	17	molecular	molecular	ADJ
ijpds-3748	149	18	entities	entity	NOUN
ijpds-3748	149	19	.	.	PUNCT
ijpds-3748	150	1	drug	drug	NOUN
ijpds-3748	150	2	discov	discov	PROPN
ijpds-3748	150	3	today	today	NOUN
ijpds-3748	150	4	.	.	PUNCT
ijpds-3748	151	1	2019	2019	NUM
ijpds-3748	151	2	;	;	PUNCT
ijpds-3748	152	1	24(9):1710–4	24(9):1710–4	X
ijpds-3748	152	2	.	.	NOUN
ijpds-3748	152	3	7	7	X
ijpds-3748	152	4	.	.	X
ijpds-3748	152	5	ayoub	ayoub	PROPN
ijpds-3748	152	6	b	b	PROPN
ijpds-3748	152	7	,	,	PUNCT
ijpds-3748	152	8	el	el	PROPN
ijpds-3748	152	9	zahar	zahar	PROPN
ijpds-3748	152	10	n	n	PROPN
ijpds-3748	152	11	,	,	PUNCT
ijpds-3748	152	12	michel	michel	PROPN
ijpds-3748	152	13	h	h	PROPN
ijpds-3748	152	14	,	,	PUNCT
ijpds-3748	152	15	et	et	PROPN
ijpds-3748	152	16	al	al	PROPN
ijpds-3748	152	17	.	.	PUNCT
ijpds-3748	153	1	economic	economic	ADJ
ijpds-3748	153	2	spectrofluorometric	spectrofluorometric	ADJ
ijpds-3748	153	3	bioanalysis	bioanalysis	NOUN
ijpds-3748	153	4	of	of	ADP
ijpds-3748	153	5	empagliflozin	empagliflozin	PROPN
ijpds-3748	153	6	in	in	ADP
ijpds-3748	153	7	rats	rat	NOUN
ijpds-3748	153	8	’	'	PUNCT
ijpds-3748	153	9	plasma	plasma	NOUN
ijpds-3748	153	10	.	.	PUNCT
ijpds-3748	154	1	j	j	PROPN
ijpds-3748	154	2	anal	anal	ADJ
ijpds-3748	154	3	methods	method	NOUN
ijpds-3748	154	4	chem	chem	NOUN
ijpds-3748	155	1	[	[	X
ijpds-3748	155	2	internet	internet	NOUN
ijpds-3748	155	3	]	]	X
ijpds-3748	155	4	.	.	PUNCT
ijpds-3748	155	5	2021	2021	NUM
ijpds-3748	155	6	;	;	PUNCT
ijpds-3748	155	7	2021	2021	NUM
ijpds-3748	155	8	:	:	PUNCT
ijpds-3748	155	9	9983477	9983477	NUM
ijpds-3748	155	10	.	.	PUNCT
ijpds-3748	156	1	doi	doi	NOUN
ijpds-3748	156	2	:	:	PUNCT
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ijpds-3748	156	4	8	8	NUM
ijpds-3748	156	5	.	.	PUNCT
ijpds-3748	157	1	antypenko	antypenko	ADJ
ijpds-3748	157	2	om	om	PROPN
ijpds-3748	157	3	,	,	PUNCT
ijpds-3748	157	4	kovalenko	kovalenko	PROPN
ijpds-3748	157	5	si	si	NOUN
ijpds-3748	157	6	,	,	PUNCT
ijpds-3748	157	7	zhernova	zhernova	X
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ijpds-3748	157	9	.	.	PUNCT
ijpds-3748	158	1	search	search	VERB
ijpds-3748	158	2	for	for	ADP
ijpds-3748	158	3	compounds	compound	NOUN
ijpds-3748	158	4	with	with	ADP
ijpds-3748	158	5	hypoglycemic	hypoglycemic	ADJ
ijpds-3748	158	6	activity	activity	NOUN
ijpds-3748	158	7	in	in	ADP
ijpds-3748	158	8	the	the	DET
ijpds-3748	158	9	series	series	NOUN
ijpds-3748	158	10	of	of	ADP
ijpds-3748	158	11	1-[2-(1htetrazol-5	1-[2-(1htetrazol-5	PROPN
ijpds-3748	158	12	-	-	PUNCT
ijpds-3748	158	13	yl)-r(1)-phenyl]-3	yl)-r(1)-phenyl]-3	NOUN
ijpds-3748	158	14	-	-	PUNCT
ijpds-3748	158	15	r(2)-phenyl(ethyl)ureas	r(2)-phenyl(ethyl)ureas	PROPN
ijpds-3748	158	16	and	and	CCONJ
ijpds-3748	158	17	r(1)tetrazolo[1,5	r(1)tetrazolo[1,5	NOUN
ijpds-3748	158	18	-	-	PUNCT
ijpds-3748	158	19	c]quinazolin-5(6h)-ones	c]quinazolin-5(6h)-one	NOUN
ijpds-3748	158	20	.	.	PUNCT
ijpds-3748	159	1	sci	sci	PROPN
ijpds-3748	159	2	pharm	pharm	PROPN
ijpds-3748	159	3	.	.	PUNCT
ijpds-3748	160	1	2016	2016	NUM
ijpds-3748	160	2	;	;	PUNCT
ijpds-3748	160	3	84:233	84:233	NUM
ijpds-3748	160	4	–	–	PUNCT
ijpds-3748	160	5	54	54	NUM
ijpds-3748	160	6	.	.	NOUN
ijpds-3748	161	1	9	9	NUM
ijpds-3748	161	2	.	.	X
ijpds-3748	161	3	scheen	scheen	PROPN
ijpds-3748	161	4	aj	aj	PROPN
ijpds-3748	161	5	.	.	PROPN
ijpds-3748	162	1	pharmacokinetic	pharmacokinetic	ADJ
ijpds-3748	162	2	and	and	CCONJ
ijpds-3748	162	3	pharmacodynamic	pharmacodynamic	ADJ
ijpds-3748	162	4	profile	profile	NOUN
ijpds-3748	162	5	of	of	ADP
ijpds-3748	162	6	empagliflozin	empagliflozin	PROPN
ijpds-3748	162	7	,	,	PUNCT
ijpds-3748	162	8	a	a	DET
ijpds-3748	162	9	sodium	sodium	NOUN
ijpds-3748	162	10	glucose	glucose	NOUN
ijpds-3748	162	11	co	co	NOUN
ijpds-3748	162	12	-	-	NOUN
ijpds-3748	162	13	transporter	transporter	ADJ
ijpds-3748	162	14	2	2	NUM
ijpds-3748	162	15	inhibitor	inhibitor	NOUN
ijpds-3748	162	16	.	.	PUNCT
ijpds-3748	163	1	clin	clin	PROPN
ijpds-3748	163	2	pharmacokinet	pharmacokinet	PROPN
ijpds-3748	163	3	.	.	PUNCT
ijpds-3748	163	4	2014	2014	NUM
ijpds-3748	163	5	;	;	PUNCT
ijpds-3748	163	6	53(3	53(3	NUM
ijpds-3748	163	7	):	):	PUNCT
ijpds-3748	163	8	213	213	NUM
ijpds-3748	163	9	-	-	SYM
ijpds-3748	163	10	25	25	NUM
ijpds-3748	163	11	.	.	PUNCT
ijpds-3748	164	1	doi	doi	NOUN
ijpds-3748	164	2	:	:	PUNCT
ijpds-3748	164	3	10.1007	10.1007	NUM
ijpds-3748	164	4	/	/	SYM
ijpds-3748	164	5	s40262	s40262	PROPN
ijpds-3748	164	6	-	-	PUNCT
ijpds-3748	164	7	0130126	0130126	NUM
ijpds-3748	164	8	-	-	PUNCT
ijpds-3748	164	9	x	x	SYM
ijpds-3748	164	10	10	10	NUM
ijpds-3748	164	11	.	.	PUNCT
ijpds-3748	165	1	shubrook	shubrook	PROPN
ijpds-3748	165	2	j	j	PROPN
ijpds-3748	165	3	,	,	PUNCT
ijpds-3748	165	4	baradar	baradar	NOUN
ijpds-3748	165	5	-	-	PUNCT
ijpds-3748	165	6	bokaie	bokaie	PROPN
ijpds-3748	165	7	b	b	PROPN
ijpds-3748	165	8	,	,	PUNCT
ijpds-3748	165	9	adkins	adkins	PROPN
ijpds-3748	165	10	s.	s.	PROPN
ijpds-3748	165	11	empagliflozin	empagliflozin	PROPN
ijpds-3748	165	12	in	in	ADP
ijpds-3748	165	13	the	the	DET
ijpds-3748	165	14	treatment	treatment	NOUN
ijpds-3748	165	15	of	of	ADP
ijpds-3748	165	16	type	type	NOUN
ijpds-3748	165	17	2	2	NUM
ijpds-3748	165	18	diabetes	diabetes	NOUN
ijpds-3748	165	19	:	:	PUNCT
ijpds-3748	165	20	evidence	evidence	NOUN
ijpds-3748	165	21	to	to	ADP
ijpds-3748	165	22	date	date	NOUN
ijpds-3748	165	23	.	.	PUNCT
ijpds-3748	166	1	drug	drug	NOUN
ijpds-3748	166	2	des	des	PROPN
ijpds-3748	166	3	devel	devel	NOUN
ijpds-3748	166	4	ther	ther	PROPN
ijpds-3748	167	1	[	[	X
ijpds-3748	167	2	internet	internet	NOUN
ijpds-3748	167	3	]	]	PUNCT
ijpds-3748	167	4	.	.	PUNCT
ijpds-3748	168	1	2015	2015	NUM
ijpds-3748	168	2	;	;	PUNCT
ijpds-3748	168	3	5793	5793	NUM
ijpds-3748	168	4	.	.	PUNCT
ijpds-3748	169	1	11	11	NUM
ijpds-3748	169	2	.	.	PUNCT
ijpds-3748	170	1	kiran	kiran	PROPN
ijpds-3748	170	2	tnr	tnr	PROPN
ijpds-3748	170	3	,	,	PUNCT
ijpds-3748	170	4	parvathi	parvathi	PROPN
ijpds-3748	170	5	p	p	PROPN
ijpds-3748	170	6	,	,	PUNCT
ijpds-3748	170	7	kumar	kumar	PROPN
ijpds-3748	170	8	jns	jns	PROPN
ijpds-3748	170	9	.	.	PUNCT
ijpds-3748	170	10	development	development	NOUN
ijpds-3748	170	11	and	and	CCONJ
ijpds-3748	170	12	validation	validation	NOUN
ijpds-3748	170	13	of	of	ADP
ijpds-3748	170	14	rp	rp	NOUN
ijpds-3748	170	15	-	-	PUNCT
ijpds-3748	170	16	hplc	hplc	NOUN
ijpds-3748	170	17	method	method	NOUN
ijpds-3748	170	18	for	for	ADP
ijpds-3748	170	19	the	the	DET
ijpds-3748	170	20	simultaneous	simultaneous	ADJ
ijpds-3748	170	21	estimation	estimation	NOUN
ijpds-3748	170	22	of	of	ADP
ijpds-3748	170	23	linagliptin	linagliptin	PROPN
ijpds-3748	170	24	,	,	PUNCT
ijpds-3748	170	25	empagliflozin	empagliflozin	PROPN
ijpds-3748	170	26	and	and	CCONJ
ijpds-3748	170	27	metformin	metformin	NOUN
ijpds-3748	170	28	in	in	ADP
ijpds-3748	170	29	solid	solid	ADJ
ijpds-3748	170	30	dosage	dosage	NOUN
ijpds-3748	170	31	forms	form	NOUN
ijpds-3748	170	32	.	.	PUNCT
ijpds-3748	171	1	asian	asian	PROPN
ijpds-3748	171	2	j	j	PROPN
ijpds-3748	171	3	pharm	pharm	PROPN
ijpds-3748	171	4	anal	anal	PROPN
ijpds-3748	172	1	[	[	X
ijpds-3748	172	2	internet	internet	NOUN
ijpds-3748	172	3	]	]	PUNCT
ijpds-3748	172	4	.	.	PUNCT
ijpds-3748	173	1	2020	2020	NUM
ijpds-3748	173	2	;	;	PUNCT
ijpds-3748	174	1	10(3):117	10(3):117	NUM
ijpds-3748	174	2	.	.	PUNCT
ijpds-3748	174	3	available	available	ADJ
ijpds-3748	174	4	from	from	ADP
ijpds-3748	174	5	:	:	PUNCT
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ijpds-3748	174	7	.	.	PUNCT
ijpds-3748	175	1	12	12	NUM
ijpds-3748	175	2	.	.	PUNCT
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ijpds-3748	176	2	kr	kr	PROPN
ijpds-3748	176	3	,	,	PUNCT
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ijpds-3748	176	5	p	p	NOUN
ijpds-3748	176	6	,	,	PUNCT
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ijpds-3748	176	8	s.	s.	PROPN
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ijpds-3748	176	10	ultraperformance	ultraperformance	ADJ
ijpds-3748	176	11	liquid	liquid	ADJ
ijpds-3748	176	12	chromatography	chromatography	NOUN
ijpds-3748	176	13	method	method	NOUN
ijpds-3748	176	14	development	development	NOUN
ijpds-3748	176	15	and	and	CCONJ
ijpds-3748	176	16	validation	validation	NOUN
ijpds-3748	176	17	for	for	ADP
ijpds-3748	176	18	simultaneous	simultaneous	ADJ
ijpds-3748	176	19	estimation	estimation	NOUN
ijpds-3748	176	20	of	of	ADP
ijpds-3748	176	21	metformin	metformin	NOUN
ijpds-3748	176	22	,	,	PUNCT
ijpds-3748	176	23	linagliptin	linagliptin	ADJ
ijpds-3748	176	24	,	,	PUNCT
ijpds-3748	176	25	and	and	CCONJ
ijpds-3748	176	26	empagliflozin	empagliflozin	PROPN
ijpds-3748	176	27	in	in	ADP
ijpds-3748	176	28	bulk	bulk	NOUN
ijpds-3748	176	29	and	and	CCONJ
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ijpds-3748	176	31	dosage	dosage	NOUN
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ijpds-3748	176	33	.	.	PUNCT
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ijpds-3748	177	2	chromatogr	chromatogr	NOUN
ijpds-3748	178	1	[	[	X
ijpds-3748	178	2	internet	internet	NOUN
ijpds-3748	178	3	]	]	X
ijpds-3748	178	4	.	.	PUNCT
ijpds-3748	179	1	2021	2021	NUM
ijpds-3748	179	2	;	;	PUNCT
ijpds-3748	179	3	35(4	35(4	NUM
ijpds-3748	179	4	)	)	PUNCT
ijpds-3748	179	5	.	.	PUNCT
ijpds-3748	180	1	13	13	NUM
ijpds-3748	180	2	.	.	X
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ijpds-3748	180	14	-	-	PUNCT
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ijpds-3748	180	16	rp	rp	NOUN
ijpds-3748	180	17	-	-	PUNCT
ijpds-3748	180	18	hplc	hplc	NOUN
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ijpds-3748	180	23	of	of	ADP
ijpds-3748	180	24	metformin	metformin	PROPN
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ijpds-3748	180	26	and	and	CCONJ
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ijpds-3748	180	28	in	in	ADP
ijpds-3748	180	29	fixed	fix	VERB
ijpds-3748	180	30	-	-	PUNCT
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ijpds-3748	180	32	combination	combination	NOUN
ijpds-3748	180	33	.	.	PUNCT
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ijpds-3748	181	4	[	[	X
ijpds-3748	181	5	internet	internet	NOUN
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ijpds-3748	181	7	.	.	PUNCT
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ijpds-3748	181	9	;	;	PUNCT
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ijpds-3748	181	11	:	:	PUNCT
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ijpds-3748	182	2	.	.	PUNCT
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ijpds-3748	183	9	.	.	PUNCT
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ijpds-3748	183	17	-	-	PUNCT
ijpds-3748	183	18	hplc	hplc	NOUN
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ijpds-3748	183	22	.	.	PUNCT
ijpds-3748	184	1	asian	asian	PROPN
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ijpds-3748	184	4	anal	anal	PROPN
ijpds-3748	185	1	[	[	X
ijpds-3748	185	2	internet	internet	NOUN
ijpds-3748	185	3	]	]	X
ijpds-3748	185	4	.	.	PUNCT
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ijpds-3748	186	2	;	;	PUNCT
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ijpds-3748	186	4	.	.	PUNCT
ijpds-3748	187	1	doi	doi	NOUN
ijpds-3748	187	2	:	:	PUNCT
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ijpds-3748	187	4	-	-	PUNCT
ijpds-3748	187	5	5675.2016.00030.2	5675.2016.00030.2	NUM
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ijpds-3748	187	7	.	.	PUNCT
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ijpds-3748	188	7	,	,	PUNCT
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ijpds-3748	188	13	.	.	PUNCT
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ijpds-3748	188	15	:	:	PUNCT
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ijpds-3748	188	19	method	method	NOUN
ijpds-3748	188	20	development	development	NOUN
ijpds-3748	188	21	and	and	CCONJ
ijpds-3748	188	22	application	application	NOUN
ijpds-3748	188	23	to	to	ADP
ijpds-3748	188	24	pharmaceutical	pharmaceutical	ADJ
ijpds-3748	188	25	raw	raw	ADJ
ijpds-3748	188	26	material	material	NOUN
ijpds-3748	188	27	and	and	CCONJ
ijpds-3748	188	28	dosage	dosage	NOUN
ijpds-3748	188	29	form	form	NOUN
ijpds-3748	188	30	.	.	PUNCT
ijpds-3748	189	1	pak	pak	PROPN
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ijpds-3748	189	5	.	.	PROPN
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ijpds-3748	189	7	;	;	PUNCT
ijpds-3748	189	8	34(3	34(3	PRON
ijpds-3748	189	9	(	(	PUNCT
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ijpds-3748	189	11	):	):	PUNCT
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ijpds-3748	189	13	.	.	NOUN
ijpds-3748	190	1	16	16	NUM
ijpds-3748	190	2	.	.	PUNCT
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ijpds-3748	190	4	,	,	PUNCT
ijpds-3748	190	5	p	p	X
ijpds-3748	190	6	,	,	PUNCT
ijpds-3748	190	7	reddy	reddy	PROPN
ijpds-3748	190	8	rm	rm	PROPN
ijpds-3748	190	9	,	,	PUNCT
ijpds-3748	190	10	devanna	devanna	PROPN
ijpds-3748	190	11	n.	n.	PROPN
ijpds-3748	190	12	rphplc	rphplc	PROPN
ijpds-3748	190	13	method	method	PROPN
ijpds-3748	190	14	development	development	NOUN
ijpds-3748	190	15	and	and	CCONJ
ijpds-3748	190	16	validation	validation	NOUN
ijpds-3748	190	17	for	for	ADP
ijpds-3748	190	18	simultaneous	simultaneous	ADJ
ijpds-3748	190	19	determination	determination	NOUN
ijpds-3748	190	20	of	of	ADP
ijpds-3748	190	21	linagliptin	linagliptin	ADJ
ijpds-3748	190	22	and	and	CCONJ
ijpds-3748	190	23	empagliflozine	empagliflozine	ADJ
ijpds-3748	190	24	in	in	ADP
ijpds-3748	190	25	tablet	tablet	ADJ
ijpds-3748	190	26	dosage	dosage	NOUN
ijpds-3748	190	27	form	form	NOUN
ijpds-3748	190	28	.	.	PUNCT
ijpds-3748	191	1	int	int	NOUN
ijpds-3748	191	2	advanced	advanced	ADJ
ijpds-3748	191	3	res	re	NOUN
ijpds-3748	191	4	j	j	PROPN
ijpds-3748	191	5	sci	sci	PROPN
ijpds-3748	191	6	eng	eng	PROPN
ijpds-3748	191	7	technol	technol	NOUN
ijpds-3748	191	8	.	.	PROPN
ijpds-3748	191	9	2015	2015	NUM
ijpds-3748	191	10	;	;	PUNCT
ijpds-3748	191	11	2	2	NUM
ijpds-3748	191	12	:	:	SYM
ijpds-3748	191	13	95	95	NUM
ijpds-3748	191	14	-	-	SYM
ijpds-3748	191	15	99	99	NUM
ijpds-3748	191	16	.	.	PUNCT
ijpds-3748	191	17	17	17	NUM
ijpds-3748	191	18	.	.	PUNCT
ijpds-3748	192	1	hussain	hussain	PROPN
ijpds-3748	192	2	bj	bj	PROPN
ijpds-3748	192	3	,	,	PUNCT
ijpds-3748	192	4	karuppasamy	karuppasamy	NOUN
ijpds-3748	192	5	c	c	PROPN
ijpds-3748	192	6	,	,	PUNCT
ijpds-3748	192	7	suresh	suresh	PROPN
ijpds-3748	192	8	y	y	PROPN
ijpds-3748	192	9	,	,	PUNCT
ijpds-3748	192	10	et	et	PROPN
ijpds-3748	192	11	al	al	PROPN
ijpds-3748	192	12	.	.	PROPN
ijpds-3748	192	13	method	method	PROPN
ijpds-3748	192	14	development	development	NOUN
ijpds-3748	192	15	and	and	CCONJ
ijpds-3748	192	16	validation	validation	NOUN
ijpds-3748	192	17	of	of	ADP
ijpds-3748	192	18	metformin	metformin	NOUN
ijpds-3748	192	19	and	and	CCONJ
ijpds-3748	192	20	empagliflozin	empagliflozin	PROPN
ijpds-3748	192	21	in	in	ADP
ijpds-3748	192	22	the	the	DET
ijpds-3748	192	23	pharmaceutical	pharmaceutical	ADJ
ijpds-3748	192	24	dosage	dosage	NOUN
ijpds-3748	192	25	form	form	NOUN
ijpds-3748	192	26	in	in	ADP
ijpds-3748	192	27	rp	rp	NOUN
ijpds-3748	192	28	-	-	PUNCT
ijpds-3748	192	29	hplc	hplc	NOUN
ijpds-3748	192	30	.	.	PUNCT
ijpds-3748	193	1	asian	asian	PROPN
ijpds-3748	193	2	j	j	PROPN
ijpds-3748	193	3	res	res	PROPN
ijpds-3748	193	4	chem	chem	NOUN
ijpds-3748	193	5	pharma	pharma	PROPN
ijpds-3748	193	6	sci	sci	PROPN
ijpds-3748	193	7	.	.	PROPN
ijpds-3748	193	8	2016	2016	NUM
ijpds-3748	193	9	;	;	PUNCT
ijpds-3748	193	10	4	4	NUM
ijpds-3748	193	11	:	:	SYM
ijpds-3748	193	12	91	91	NUM
ijpds-3748	193	13	-	-	SYM
ijpds-3748	193	14	100	100	NUM
ijpds-3748	193	15	.	.	PUNCT
ijpds-3748	193	16	18	18	NUM
ijpds-3748	193	17	.	.	PUNCT
ijpds-3748	193	18	abdel	abdel	PROPN
ijpds-3748	193	19	-	-	PUNCT
ijpds-3748	193	20	ghany	ghany	PROPN
ijpds-3748	193	21	mf	mf	PROPN
ijpds-3748	193	22	,	,	PUNCT
ijpds-3748	193	23	abdel	abdel	PROPN
ijpds-3748	193	24	-	-	PUNCT
ijpds-3748	193	25	aziz	aziz	PROPN
ijpds-3748	193	26	o	o	PROPN
ijpds-3748	193	27	,	,	PUNCT
ijpds-3748	193	28	ayad	ayad	PROPN
ijpds-3748	193	29	mf	mf	PROPN
ijpds-3748	193	30	,	,	PUNCT
ijpds-3748	193	31	et	et	PROPN
ijpds-3748	193	32	al	al	PROPN
ijpds-3748	193	33	.	.	PROPN
ijpds-3748	193	34	pharmaceutical	pharmaceutical	ADJ
ijpds-3748	193	35	analysis	analysis	NOUN
ijpds-3748	193	36	of	of	ADP
ijpds-3748	193	37	linagliptin	linagliptin	NOUN
ijpds-3748	193	38	and	and	CCONJ
ijpds-3748	193	39	empagliflozin	empagliflozin	NOUN
ijpds-3748	193	40	using	use	VERB
ijpds-3748	193	41	lc	lc	PROPN
ijpds-3748	193	42	-	-	PUNCT
ijpds-3748	193	43	ms	ms	PROPN
ijpds-3748	193	44	/	/	SYM
ijpds-3748	193	45	ms	ms	PROPN
ijpds-3748	193	46	.	.	PROPN
ijpds-3748	193	47	pharma	pharma	PROPN
ijpds-3748	193	48	chem	chem	NOUN
ijpds-3748	193	49	.	.	PUNCT
ijpds-3748	194	1	2016	2016	NUM
ijpds-3748	194	2	;	;	PUNCT
ijpds-3748	194	3	8	8	NUM
ijpds-3748	194	4	:	:	SYM
ijpds-3748	194	5	186	186	NUM
ijpds-3748	194	6	-	-	SYM
ijpds-3748	194	7	189	189	NUM
ijpds-3748	194	8	.	.	NOUN
ijpds-3748	194	9	19	19	NUM
ijpds-3748	194	10	.	.	PROPN
ijpds-3748	194	11	united	united	PROPN
ijpds-3748	194	12	states	states	PROPN
ijpds-3748	194	13	pharmacopoeia	pharmacopoeia	PROPN
ijpds-3748	194	14	.	.	PUNCT
ijpds-3748	195	1	general	general	ADJ
ijpds-3748	195	2	chapter	chapter	NOUN
ijpds-3748	195	3	<	<	PROPN
ijpds-3748	195	4	621	621	NUM
ijpds-3748	195	5	>	>	PRON
ijpds-3748	195	6	“	"	PUNCT
ijpds-3748	195	7	chromatography	chromatography	NOUN
ijpds-3748	195	8	”	"	PUNCT
ijpds-3748	195	9	,	,	PUNCT
ijpds-3748	195	10	usp	usp	PROPN
ijpds-3748	195	11	37	37	NUM
ijpds-3748	195	12	,	,	PUNCT
ijpds-3748	195	13	nf	nf	NOUN
ijpds-3748	195	14	32	32	NUM
ijpds-3748	195	15	;	;	PUNCT
ijpds-3748	195	16	2014	2014	NUM
ijpds-3748	195	17	.	.	PUNCT
ijpds-3748	196	1	20	20	NUM
ijpds-3748	196	2	.	.	PUNCT
ijpds-3748	197	1	moid	moid	PROPN
ijpds-3748	197	2	m	m	PROPN
ijpds-3748	197	3	,	,	PUNCT
ijpds-3748	197	4	afzal	afzal	PROPN
ijpds-3748	197	5	s	s	PROPN
ijpds-3748	197	6	,	,	PUNCT
ijpds-3748	197	7	rahim	rahim	PROPN
ijpds-3748	197	8	n	n	PRON
ijpds-3748	197	9	,	,	PUNCT
ijpds-3748	197	10	et	et	PROPN
ijpds-3748	197	11	al	al	PROPN
ijpds-3748	197	12	.	.	PROPN
ijpds-3748	197	13	high	high	ADJ
ijpds-3748	197	14	-	-	PUNCT
ijpds-3748	197	15	performance	performance	NOUN
ijpds-3748	197	16	liquid	liquid	ADJ
ijpds-3748	197	17	chromatographic	chromatographic	ADJ
ijpds-3748	197	18	method	method	NOUN
ijpds-3748	197	19	validation	validation	NOUN
ijpds-3748	197	20	for	for	ADP
ijpds-3748	197	21	determination	determination	NOUN
ijpds-3748	197	22	of	of	ADP
ijpds-3748	197	23	rosuvastatin	rosuvastatin	ADJ
ijpds-3748	197	24	calcium	calcium	NOUN
ijpds-3748	197	25	in	in	ADP
ijpds-3748	197	26	tablet	tablet	ADJ
ijpds-3748	197	27	dosage	dosage	NOUN
ijpds-3748	197	28	forms	form	NOUN
ijpds-3748	197	29	.	.	PUNCT
ijpds-3748	198	1	pak	pak	PROPN
ijpds-3748	198	2	.	.	PUNCT
ijpds-3748	199	1	j.pharm	j.pharm	PROPN
ijpds-3748	199	2	.	.	PUNCT
ijpds-3748	200	1	sci	sci	PROPN
ijpds-3748	200	2	.	.	PROPN
ijpds-3748	200	3	2018	2018	NUM
ijpds-3748	200	4	;	;	PUNCT
ijpds-3748	200	5	31(4	31(4	NUM
ijpds-3748	200	6	):	):	PUNCT
ijpds-3748	200	7	1577	1577	NUM
ijpds-3748	200	8	-	-	SYM
ijpds-3748	200	9	1582	1582	NUM
ijpds-3748	200	10	.	.	PUNCT
ijpds-3748	201	1	21	21	NUM
ijpds-3748	201	2	.	.	PUNCT
ijpds-3748	202	1	international	international	ADJ
ijpds-3748	202	2	conference	conference	NOUN
ijpds-3748	202	3	on	on	ADP
ijpds-3748	202	4	harmonization	harmonization	NOUN
ijpds-3748	202	5	,	,	PUNCT
ijpds-3748	202	6	q1b	q1b	PROPN
ijpds-3748	202	7	(	(	PUNCT
ijpds-3748	202	8	r2	r2	PROPN
ijpds-3748	202	9	)	)	PUNCT
ijpds-3748	202	10	stability	stability	NOUN
ijpds-3748	202	11	testing	testing	NOUN
ijpds-3748	202	12	:	:	PUNCT
ijpds-3748	202	13	photostability	photostability	NOUN
ijpds-3748	202	14	testing	testing	NOUN
ijpds-3748	202	15	in	in	ADP
ijpds-3748	202	16	new	new	ADJ
ijpds-3748	202	17	drug	drug	NOUN
ijpds-3748	202	18	substances	substance	NOUN
ijpds-3748	202	19	and	and	CCONJ
ijpds-3748	202	20	products	product	NOUN
ijpds-3748	202	21	;	;	PUNCT
ijpds-3748	202	22	1996	1996	NUM
ijpds-3748	202	23	.	.	PUNCT
ijpds-3748	203	1	22	22	NUM
ijpds-3748	203	2	.	.	PUNCT
ijpds-3748	204	1	international	international	ADJ
ijpds-3748	204	2	conference	conference	NOUN
ijpds-3748	204	3	on	on	ADP
ijpds-3748	204	4	harmonization	harmonization	NOUN
ijpds-3748	204	5	,	,	PUNCT
ijpds-3748	204	6	q2	q2	NOUN
ijpds-3748	204	7	(	(	PUNCT
ijpds-3748	204	8	r1	r1	PROPN
ijpds-3748	204	9	)	)	PUNCT
ijpds-3748	204	10	validation	validation	NOUN
ijpds-3748	204	11	of	of	ADP
ijpds-3748	204	12	analytical	analytical	ADJ
ijpds-3748	204	13	procedures	procedure	NOUN
ijpds-3748	204	14	:	:	PUNCT
ijpds-3748	204	15	text	text	NOUN
ijpds-3748	204	16	and	and	CCONJ
ijpds-3748	204	17	methodology	methodology	NOUN
ijpds-3748	204	18	2005	2005	NUM
ijpds-3748	204	19	.	.	PUNCT
ijpds-3748	205	1	how	how	SCONJ
ijpds-3748	205	2	to	to	PART
ijpds-3748	205	3	cite	cite	VERB
ijpds-3748	205	4	this	this	DET
ijpds-3748	205	5	article	article	NOUN
ijpds-3748	205	6	:	:	PUNCT
ijpds-3748	205	7	ahmad	ahmad	PROPN
ijpds-3748	205	8	a.	a.	PROPN
ijpds-3748	205	9	zahra	zahra	PROPN
ijpds-3748	205	10	m.	m.	PROPN
ijpds-3748	205	11	development	development	PROPN
ijpds-3748	205	12	and	and	CCONJ
ijpds-3748	205	13	validation	validation	NOUN
ijpds-3748	205	14	of	of	ADP
ijpds-3748	205	15	novel	novel	ADJ
ijpds-3748	205	16	stability	stability	NOUN
ijpds-3748	205	17	indicating	indicate	VERB
ijpds-3748	205	18	rp	rp	ADP
ijpds-3748	205	19	hplc	hplc	NOUN
ijpds-3748	205	20	method	method	NOUN
ijpds-3748	205	21	for	for	ADP
ijpds-3748	205	22	quantitative	quantitative	ADJ
ijpds-3748	205	23	estimation	estimation	NOUN
ijpds-3748	205	24	of	of	ADP
ijpds-3748	205	25	empagliflozin	empagliflozin	PROPN
ijpds-3748	205	26	in	in	ADP
ijpds-3748	205	27	tablets	tablet	NOUN
ijpds-3748	205	28	.	.	PUNCT
ijpds-3748	206	1	indian	indian	PROPN
ijpds-3748	206	2	j	j	PROPN
ijpds-3748	206	3	pharm	pharm	PROPN
ijpds-3748	206	4	drug	drug	PROPN
ijpds-3748	206	5	studies	study	NOUN
ijpds-3748	206	6	.	.	PUNCT
ijpds-3748	207	1	2023	2023	NUM
ijpds-3748	207	2	:	:	PUNCT
ijpds-3748	207	3	2(2	2(2	NUM
ijpds-3748	207	4	)	)	PUNCT
ijpds-3748	207	5	;	;	PUNCT
ijpds-3748	207	6	76	76	NUM
ijpds-3748	207	7	-	-	SYM
ijpds-3748	207	8	81	81	NUM
ijpds-3748	207	9	.	.	PUNCT
ijpds-3748	208	1	funding	funding	NOUN
ijpds-3748	208	2	:	:	PUNCT
ijpds-3748	208	3	none	none	NOUN
ijpds-3748	208	4	conflict	conflict	NOUN
ijpds-3748	208	5	of	of	ADP
ijpds-3748	208	6	interest	interest	NOUN
ijpds-3748	208	7	:	:	PUNCT
ijpds-3748	208	8	none	none	NOUN
ijpds-3748	208	9	stated	state	VERB
ijpds-3748	208	10	https://www.drugs.com/monograph/empagliflozin.html	https://www.drugs.com/monograph/empagliflozin.html	X
ijpds-3748	208	11	http://dx.doi.org/10.1155/2021/9983477	http://dx.doi.org/10.1155/2021/9983477	NOUN
ijpds-3748	208	12	http://dx.doi.org/10.1007/s40262-013-0126-x	http://dx.doi.org/10.1007/s40262-013-0126-x	NOUN
ijpds-3748	208	13	http://dx.doi.org/10.1007/s40262-013-0126-x	http://dx.doi.org/10.1007/s40262-013-0126-x	PROPN
ijpds-3748	208	14	http://dx.doi.org/10.5958/2231-5675.2020.00021.6	http://dx.doi.org/10.5958/2231-5675.2020.00021.6	NOUN
ijpds-3748	208	15	http://dx.doi.org/10.5958/2231-5675.2016.00030.2	http://dx.doi.org/10.5958/2231-5675.2016.00030.2	VERB