id	sid	tid	token	lemma	pos
ijpds-4231	1	1	sanjay	sanjay	PROPN
ijpds-4231	1	2	s	s	PART
ijpds-4231	1	3	s	s	NOUN
ijpds-4231	1	4	patents	patent	NOUN
ijpds-4231	1	5	disclosed	disclose	VERB
ijpds-4231	1	6	synthetic	synthetic	ADJ
ijpds-4231	1	7	overview	overview	NOUN
ijpds-4231	1	8	of	of	ADP
ijpds-4231	1	9	rasagiline	rasagiline	ADJ
ijpds-4231	1	10	vol	vol	NOUN
ijpds-4231	1	11	2	2	NUM
ijpds-4231	1	12	|	|	ADV
ijpds-4231	1	13	issue	issue	VERB
ijpds-4231	1	14	4	4	NUM
ijpds-4231	1	15	|	|	ADV
ijpds-4231	1	16	oct	oct	PROPN
ijpds-4231	1	17	–	–	PUNCT
ijpds-4231	1	18	dec	dec	PROPN
ijpds-4231	1	19	2023	2023	NUM
ijpds-4231	1	20	indian	indian	PROPN
ijpds-4231	1	21	j	j	PROPN
ijpds-4231	1	22	pharm	pharm	PROPN
ijpds-4231	1	23	drug	drug	PROPN
ijpds-4231	1	24	studies	study	NOUN
ijpds-4231	1	25	|	|	ADV
ijpds-4231	1	26	132	132	NUM
ijpds-4231	1	27	review	review	NOUN
ijpds-4231	1	28	article	article	NOUN
ijpds-4231	1	29	an	an	DET
ijpds-4231	1	30	overview	overview	NOUN
ijpds-4231	1	31	of	of	ADP
ijpds-4231	1	32	prior	prior	ADJ
ijpds-4231	1	33	patents	patent	NOUN
ijpds-4231	1	34	for	for	ADP
ijpds-4231	1	35	the	the	DET
ijpds-4231	1	36	sequential	sequential	ADJ
ijpds-4231	1	37	progress	progress	NOUN
ijpds-4231	1	38	in	in	ADP
ijpds-4231	1	39	the	the	DET
ijpds-4231	1	40	synthetic	synthetic	ADJ
ijpds-4231	1	41	approaches	approach	NOUN
ijpds-4231	1	42	of	of	ADP
ijpds-4231	1	43	rasagiline	rasagiline	NOUN
ijpds-4231	1	44	,	,	PUNCT
ijpds-4231	1	45	its	its	PRON
ijpds-4231	1	46	salts	salt	NOUN
ijpds-4231	1	47	,	,	PUNCT
ijpds-4231	1	48	crystallographic	crystallographic	ADJ
ijpds-4231	1	49	forms	form	NOUN
ijpds-4231	1	50	and	and	CCONJ
ijpds-4231	1	51	impurities	impurity	NOUN
ijpds-4231	1	52	sanjay	sanjay	PROPN
ijpds-4231	1	53	sukumar	sukumar	PROPN
ijpds-4231	1	54	saralaya	saralaya	PROPN
ijpds-4231	1	55	from	from	ADP
ijpds-4231	1	56	,	,	PUNCT
ijpds-4231	1	57	assistant	assistant	NOUN
ijpds-4231	1	58	professor	professor	NOUN
ijpds-4231	1	59	,	,	PUNCT
ijpds-4231	1	60	department	department	NOUN
ijpds-4231	1	61	of	of	ADP
ijpds-4231	1	62	chemistry	chemistry	NOUN
ijpds-4231	1	63	,	,	PUNCT
ijpds-4231	1	64	sri	sri	PROPN
ijpds-4231	1	65	dharmasthala	dharmasthala	PROPN
ijpds-4231	1	66	manjunatheshwara	manjunatheshwara	PROPN
ijpds-4231	1	67	,	,	PUNCT
ijpds-4231	1	68	institute	institute	NOUN
ijpds-4231	1	69	of	of	ADP
ijpds-4231	1	70	technology	technology	NOUN
ijpds-4231	1	71	,	,	PUNCT
ijpds-4231	1	72	[	[	X
ijpds-4231	1	73	affiliated	affiliate	VERB
ijpds-4231	1	74	to	to	AUX
ijpds-4231	1	75	visvesvaraya	visvesvaraya	VERB
ijpds-4231	1	76	technological	technological	ADJ
ijpds-4231	1	77	university	university	NOUN
ijpds-4231	1	78	,	,	PUNCT
ijpds-4231	1	79	belagavi	belagavi	VERB
ijpds-4231	1	80	]	]	PUNCT
ijpds-4231	1	81	,	,	PUNCT
ijpds-4231	1	82	ujire	ujire	NOUN
ijpds-4231	1	83	,	,	PUNCT
ijpds-4231	1	84	belthangady	belthangady	NOUN
ijpds-4231	1	85	taluk	taluk	NOUN
ijpds-4231	1	86	,	,	PUNCT
ijpds-4231	1	87	dakshina	dakshina	PROPN
ijpds-4231	1	88	kannada	kannada	PROPN
ijpds-4231	1	89	,	,	PUNCT
ijpds-4231	1	90	karnataka	karnataka	PROPN
ijpds-4231	1	91	,	,	PUNCT
ijpds-4231	1	92	india	india	PROPN
ijpds-4231	1	93	.	.	PUNCT
ijpds-4231	2	1	pin	pin	PROPN
ijpds-4231	2	2	code	code	VERB
ijpds-4231	2	3	574	574	NUM
ijpds-4231	2	4	240	240	NUM
ijpds-4231	2	5	.	.	PUNCT
ijpds-4231	3	1	abstract	abstract	ADJ
ijpds-4231	3	2	this	this	DET
ijpds-4231	3	3	review	review	NOUN
ijpds-4231	3	4	work	work	NOUN
ijpds-4231	3	5	was	be	AUX
ijpds-4231	3	6	intended	intend	VERB
ijpds-4231	3	7	to	to	PART
ijpds-4231	3	8	provide	provide	VERB
ijpds-4231	3	9	the	the	DET
ijpds-4231	3	10	essential	essential	ADJ
ijpds-4231	3	11	details	detail	NOUN
ijpds-4231	3	12	disclosed	disclose	VERB
ijpds-4231	3	13	in	in	ADP
ijpds-4231	3	14	prior	prior	ADJ
ijpds-4231	3	15	patents	patent	NOUN
ijpds-4231	3	16	on	on	ADP
ijpds-4231	3	17	the	the	DET
ijpds-4231	3	18	synthesis	synthesis	NOUN
ijpds-4231	3	19	of	of	ADP
ijpds-4231	3	20	rasagiline	rasagiline	NOUN
ijpds-4231	3	21	,	,	PUNCT
ijpds-4231	3	22	its	its	PRON
ijpds-4231	3	23	salts	salt	NOUN
ijpds-4231	3	24	(	(	PUNCT
ijpds-4231	3	25	as	as	ADP
ijpds-4231	3	26	crystalline	crystalline	ADJ
ijpds-4231	3	27	or	or	CCONJ
ijpds-4231	3	28	amorphous	amorphous	ADJ
ijpds-4231	3	29	forms	form	NOUN
ijpds-4231	3	30	)	)	PUNCT
ijpds-4231	3	31	and	and	CCONJ
ijpds-4231	3	32	a	a	DET
ijpds-4231	3	33	few	few	ADJ
ijpds-4231	3	34	impurities	impurity	NOUN
ijpds-4231	3	35	.	.	PUNCT
ijpds-4231	4	1	quite	quite	DET
ijpds-4231	4	2	a	a	DET
ijpds-4231	4	3	high	high	ADJ
ijpds-4231	4	4	number	number	NOUN
ijpds-4231	4	5	of	of	ADP
ijpds-4231	4	6	patents	patent	NOUN
ijpds-4231	4	7	were	be	AUX
ijpds-4231	4	8	published	publish	VERB
ijpds-4231	4	9	in	in	ADP
ijpds-4231	4	10	various	various	ADJ
ijpds-4231	4	11	patent	patent	NOUN
ijpds-4231	4	12	trademark	trademark	NOUN
ijpds-4231	4	13	offices	office	NOUN
ijpds-4231	4	14	around	around	ADP
ijpds-4231	4	15	the	the	DET
ijpds-4231	4	16	world	world	NOUN
ijpds-4231	4	17	regarding	regard	VERB
ijpds-4231	4	18	the	the	DET
ijpds-4231	4	19	synthesis	synthesis	NOUN
ijpds-4231	4	20	of	of	ADP
ijpds-4231	4	21	rasagiline	rasagiline	NOUN
ijpds-4231	4	22	.	.	PUNCT
ijpds-4231	5	1	among	among	ADP
ijpds-4231	5	2	them	they	PRON
ijpds-4231	5	3	,	,	PUNCT
ijpds-4231	5	4	the	the	DET
ijpds-4231	5	5	patents	patent	NOUN
ijpds-4231	5	6	which	which	PRON
ijpds-4231	5	7	fall	fall	VERB
ijpds-4231	5	8	under	under	ADP
ijpds-4231	5	9	the	the	DET
ijpds-4231	5	10	similar	similar	ADJ
ijpds-4231	5	11	family	family	NOUN
ijpds-4231	5	12	are	be	AUX
ijpds-4231	5	13	excluded	exclude	VERB
ijpds-4231	5	14	to	to	PART
ijpds-4231	5	15	prevent	prevent	VERB
ijpds-4231	5	16	the	the	DET
ijpds-4231	5	17	possible	possible	ADJ
ijpds-4231	5	18	duplication	duplication	NOUN
ijpds-4231	5	19	of	of	ADP
ijpds-4231	5	20	the	the	DET
ijpds-4231	5	21	information	information	NOUN
ijpds-4231	5	22	.	.	PUNCT
ijpds-4231	6	1	the	the	DET
ijpds-4231	6	2	remaining	remain	VERB
ijpds-4231	6	3	distinct	distinct	ADJ
ijpds-4231	6	4	patents	patent	NOUN
ijpds-4231	6	5	were	be	AUX
ijpds-4231	6	6	carefully	carefully	ADV
ijpds-4231	6	7	reviewed	review	VERB
ijpds-4231	6	8	and	and	CCONJ
ijpds-4231	6	9	the	the	DET
ijpds-4231	6	10	particulars	particular	NOUN
ijpds-4231	6	11	are	be	AUX
ijpds-4231	6	12	grouped	group	VERB
ijpds-4231	6	13	in	in	ADP
ijpds-4231	6	14	chronological	chronological	ADJ
ijpds-4231	6	15	order	order	NOUN
ijpds-4231	6	16	.	.	PUNCT
ijpds-4231	7	1	moreover	moreover	ADV
ijpds-4231	7	2	,	,	PUNCT
ijpds-4231	7	3	this	this	DET
ijpds-4231	7	4	initiative	initiative	NOUN
ijpds-4231	7	5	can	can	AUX
ijpds-4231	7	6	provide	provide	VERB
ijpds-4231	7	7	an	an	DET
ijpds-4231	7	8	essential	essential	ADJ
ijpds-4231	7	9	backyard	backyard	NOUN
ijpds-4231	7	10	for	for	ADP
ijpds-4231	7	11	the	the	DET
ijpds-4231	7	12	global	global	ADJ
ijpds-4231	7	13	researchers	researcher	NOUN
ijpds-4231	7	14	and	and	CCONJ
ijpds-4231	7	15	the	the	DET
ijpds-4231	7	16	organizations	organization	NOUN
ijpds-4231	7	17	to	to	PART
ijpds-4231	7	18	get	get	VERB
ijpds-4231	7	19	the	the	DET
ijpds-4231	7	20	details	detail	NOUN
ijpds-4231	7	21	on	on	ADP
ijpds-4231	7	22	the	the	DET
ijpds-4231	7	23	methodological	methodological	ADJ
ijpds-4231	7	24	flourish	flourish	NOUN
ijpds-4231	7	25	of	of	ADP
ijpds-4231	7	26	rasagiline	rasagiline	NOUN
ijpds-4231	7	27	.	.	PUNCT
ijpds-4231	8	1	more	more	ADV
ijpds-4231	8	2	importantly	importantly	ADV
ijpds-4231	8	3	,	,	PUNCT
ijpds-4231	8	4	the	the	DET
ijpds-4231	8	5	work	work	NOUN
ijpds-4231	8	6	forms	form	VERB
ijpds-4231	8	7	a	a	DET
ijpds-4231	8	8	firm	firm	ADJ
ijpds-4231	8	9	basis	basis	NOUN
ijpds-4231	8	10	for	for	ADP
ijpds-4231	8	11	to	to	PART
ijpds-4231	8	12	invent	invent	VERB
ijpds-4231	8	13	/	/	PUNCT
ijpds-4231	8	14	innovate	innovate	VERB
ijpds-4231	8	15	a	a	DET
ijpds-4231	8	16	few	few	ADJ
ijpds-4231	8	17	more	more	ADV
ijpds-4231	8	18	new	new	ADJ
ijpds-4231	8	19	strategies	strategy	NOUN
ijpds-4231	8	20	to	to	PART
ijpds-4231	8	21	commercialize	commercialize	VERB
ijpds-4231	8	22	rasagiline	rasagiline	NOUN
ijpds-4231	8	23	in	in	ADP
ijpds-4231	8	24	its	its	PRON
ijpds-4231	8	25	pharmaceutically	pharmaceutically	ADV
ijpds-4231	8	26	suitable	suitable	ADJ
ijpds-4231	8	27	and	and	CCONJ
ijpds-4231	8	28	stable	stable	ADJ
ijpds-4231	8	29	forms	form	NOUN
ijpds-4231	8	30	.	.	PUNCT
ijpds-4231	9	1	additionally	additionally	ADV
ijpds-4231	9	2	,	,	PUNCT
ijpds-4231	9	3	researchers	researcher	NOUN
ijpds-4231	9	4	can	can	AUX
ijpds-4231	9	5	avail	avail	VERB
ijpds-4231	9	6	the	the	DET
ijpds-4231	9	7	information	information	NOUN
ijpds-4231	9	8	about	about	ADP
ijpds-4231	9	9	the	the	DET
ijpds-4231	9	10	organizations	organization	NOUN
ijpds-4231	9	11	which	which	PRON
ijpds-4231	9	12	are	be	AUX
ijpds-4231	9	13	behind	behind	ADP
ijpds-4231	9	14	the	the	DET
ijpds-4231	9	15	continuous	continuous	ADJ
ijpds-4231	9	16	process	process	NOUN
ijpds-4231	9	17	improvement	improvement	NOUN
ijpds-4231	9	18	on	on	ADP
ijpds-4231	9	19	various	various	ADJ
ijpds-4231	9	20	aspects	aspect	NOUN
ijpds-4231	9	21	of	of	ADP
ijpds-4231	9	22	rasagiline	rasagiline	NOUN
ijpds-4231	9	23	.	.	PUNCT
ijpds-4231	10	1	key	key	ADJ
ijpds-4231	10	2	words	word	NOUN
ijpds-4231	10	3	:	:	PUNCT
ijpds-4231	10	4	rasagiline	rasagiline	NOUN
ijpds-4231	10	5	base	base	NOUN
ijpds-4231	10	6	,	,	PUNCT
ijpds-4231	10	7	rasagiline	rasagiline	NOUN
ijpds-4231	10	8	mesylate	mesylate	NOUN
ijpds-4231	10	9	,	,	PUNCT
ijpds-4231	10	10	propargylation	propargylation	NOUN
ijpds-4231	10	11	,	,	PUNCT
ijpds-4231	10	12	n	n	CCONJ
ijpds-4231	10	13	-	-	PUNCT
ijpds-4231	10	14	alkylation	alkylation	NOUN
ijpds-4231	10	15	,	,	PUNCT
ijpds-4231	10	16	racemization	racemization	NOUN
ijpds-4231	10	17	.	.	PUNCT
ijpds-4231	11	1	he	he	PRON
ijpds-4231	11	2	popular	popular	ADJ
ijpds-4231	11	3	drug	drug	NOUN
ijpds-4231	11	4	,	,	PUNCT
ijpds-4231	11	5	rasagiline	rasagiline	NOUN
ijpds-4231	11	6	is	be	AUX
ijpds-4231	11	7	an	an	DET
ijpds-4231	11	8	irreversible	irreversible	ADJ
ijpds-4231	11	9	inhibitor	inhibitor	NOUN
ijpds-4231	11	10	of	of	ADP
ijpds-4231	11	11	monoamine	monoamine	ADJ
ijpds-4231	11	12	oxidase	oxidase	NOUN
ijpds-4231	11	13	.	.	PUNCT
ijpds-4231	12	1	it	it	PRON
ijpds-4231	12	2	is	be	AUX
ijpds-4231	12	3	used	use	VERB
ijpds-4231	12	4	widely	widely	ADV
ijpds-4231	12	5	as	as	ADP
ijpds-4231	12	6	a	a	DET
ijpds-4231	12	7	monotherapy	monotherapy	NOUN
ijpds-4231	12	8	during	during	ADP
ijpds-4231	12	9	the	the	DET
ijpds-4231	12	10	initial	initial	ADJ
ijpds-4231	12	11	stages	stage	NOUN
ijpds-4231	12	12	of	of	ADP
ijpds-4231	12	13	parkinson	parkinson	NOUN
ijpds-4231	12	14	's	's	PART
ijpds-4231	12	15	disease	disease	NOUN
ijpds-4231	12	16	or	or	CCONJ
ijpds-4231	12	17	as	as	ADP
ijpds-4231	12	18	an	an	DET
ijpds-4231	12	19	adjunct	adjunct	ADJ
ijpds-4231	12	20	therapy	therapy	NOUN
ijpds-4231	12	21	in	in	ADP
ijpds-4231	12	22	more	more	ADV
ijpds-4231	12	23	advanced	advanced	ADJ
ijpds-4231	12	24	scenarios	scenario	NOUN
ijpds-4231	12	25	[	[	X
ijpds-4231	12	26	1	1	NUM
ijpds-4231	12	27	,	,	PUNCT
ijpds-4231	12	28	2	2	NUM
ijpds-4231	12	29	]	]	PUNCT
ijpds-4231	12	30	.	.	PUNCT
ijpds-4231	13	1	nh	nh	PROPN
ijpds-4231	13	2	h	h	PROPN
ijpds-4231	13	3	s	s	PART
ijpds-4231	13	4	o	o	NOUN
ijpds-4231	13	5	o	o	X
ijpds-4231	13	6	oh1	oh1	NOUN
ijpds-4231	13	7	rasagiline	rasagiline	NOUN
ijpds-4231	13	8	mesylate	mesylate	NOUN
ijpds-4231	13	9	(	(	PUNCT
ijpds-4231	13	10	c13h17no3s	c13h17no3s	PROPN
ijpds-4231	13	11	)	)	PUNCT
ijpds-4231	13	12	1	1	NUM
ijpds-4231	13	13	has	have	VERB
ijpds-4231	13	14	the	the	DET
ijpds-4231	13	15	iupac	iupac	PROPN
ijpds-4231	13	16	name	name	NOUN
ijpds-4231	13	17	:	:	PUNCT
ijpds-4231	14	1	[	[	X
ijpds-4231	14	2	(	(	PUNCT
ijpds-4231	14	3	1r)-n-(prop-2	1r)-n-(prop-2	NUM
ijpds-4231	14	4	-	-	PUNCT
ijpds-4231	14	5	yn-1	yn-1	NOUN
ijpds-4231	14	6	-	-	PUNCT
ijpds-4231	14	7	yl)-2,3	yl)-2,3	NOUN
ijpds-4231	14	8	-	-	PUNCT
ijpds-4231	14	9	dihydro-1h	dihydro-1h	NOUN
ijpds-4231	14	10	-	-	PUNCT
ijpds-4231	14	11	inden-1	inden-1	NOUN
ijpds-4231	14	12	-	-	PUNCT
ijpds-4231	14	13	amine	amine	ADJ
ijpds-4231	14	14	methanesulfonate	methanesulfonate	NOUN
ijpds-4231	14	15	]	]	PUNCT
ijpds-4231	14	16	with	with	ADP
ijpds-4231	14	17	a	a	DET
ijpds-4231	14	18	cas	cas	PROPN
ijpds-4231	14	19	registry	registry	NOUN
ijpds-4231	14	20	number	number	NOUN
ijpds-4231	14	21	:	:	PUNCT
ijpds-4231	14	22	16173579	16173579	NUM
ijpds-4231	14	23	-	-	SYM
ijpds-4231	14	24	1	1	NUM
ijpds-4231	14	25	and	and	CCONJ
ijpds-4231	14	26	a	a	DET
ijpds-4231	14	27	molecular	molecular	ADJ
ijpds-4231	14	28	weight	weight	NOUN
ijpds-4231	14	29	:	:	PUNCT
ijpds-4231	14	30	267.34	267.34	NUM
ijpds-4231	14	31	g	g	NOUN
ijpds-4231	14	32	/	/	SYM
ijpds-4231	14	33	mol	mol	NOUN
ijpds-4231	14	34	.	.	PUNCT
ijpds-4231	15	1	it	it	PRON
ijpds-4231	15	2	is	be	AUX
ijpds-4231	15	3	commercially	commercially	ADV
ijpds-4231	15	4	marketed	market	VERB
ijpds-4231	15	5	under	under	ADP
ijpds-4231	15	6	the	the	DET
ijpds-4231	15	7	brand	brand	NOUN
ijpds-4231	15	8	/	/	SYM
ijpds-4231	15	9	trade	trade	NOUN
ijpds-4231	15	10	name	name	NOUN
ijpds-4231	15	11	azilect	azilect	PROPN
ijpds-4231	15	12	®	®	PROPN
ijpds-4231	15	13	.	.	PUNCT
ijpds-4231	16	1	rasagiline	rasagiline	PROPN
ijpds-4231	16	2	is	be	AUX
ijpds-4231	16	3	a	a	DET
ijpds-4231	16	4	renowned	renowned	ADJ
ijpds-4231	16	5	propargylamine	propargylamine	NOUN
ijpds-4231	16	6	access	access	NOUN
ijpds-4231	16	7	this	this	DET
ijpds-4231	16	8	article	article	NOUN
ijpds-4231	16	9	online	online	ADV
ijpds-4231	16	10	received	receive	VERB
ijpds-4231	16	11	–	–	PUNCT
ijpds-4231	16	12	24th	24th	ADJ
ijpds-4231	16	13	august	august	PROPN
ijpds-4231	16	14	2023	2023	NUM
ijpds-4231	16	15	initial	initial	ADJ
ijpds-4231	16	16	review	review	NOUN
ijpds-4231	16	17	–	–	PUNCT
ijpds-4231	16	18	09th	09th	ADJ
ijpds-4231	16	19	september	september	PROPN
ijpds-4231	16	20	2023	2023	NUM
ijpds-4231	16	21	accepted	accept	VERB
ijpds-4231	16	22	–	–	PUNCT
ijpds-4231	16	23	10th	10th	ADJ
ijpds-4231	16	24	october	october	PROPN
ijpds-4231	16	25	2023	2023	NUM
ijpds-4231	16	26	quick	quick	ADJ
ijpds-4231	16	27	response	response	NOUN
ijpds-4231	16	28	code	code	NOUN
ijpds-4231	16	29	derivative	derivative	NOUN
ijpds-4231	16	30	with	with	ADP
ijpds-4231	16	31	a	a	DET
ijpds-4231	16	32	good	good	ADJ
ijpds-4231	16	33	clinical	clinical	ADJ
ijpds-4231	16	34	efficacy	efficacy	NOUN
ijpds-4231	16	35	.	.	PUNCT
ijpds-4231	17	1	interestingly	interestingly	ADV
ijpds-4231	17	2	,	,	PUNCT
ijpds-4231	17	3	r(+)-enantiomer	r(+)-enantiomer	ADJ
ijpds-4231	17	4	is	be	AUX
ijpds-4231	17	5	therapeutically	therapeutically	ADV
ijpds-4231	17	6	active	active	ADJ
ijpds-4231	17	7	and	and	CCONJ
ijpds-4231	17	8	hence	hence	ADV
ijpds-4231	17	9	gained	gain	VERB
ijpds-4231	17	10	a	a	DET
ijpds-4231	17	11	wide	wide	ADJ
ijpds-4231	17	12	clinical	clinical	ADJ
ijpds-4231	17	13	importance	importance	NOUN
ijpds-4231	17	14	to	to	PART
ijpds-4231	17	15	treat	treat	VERB
ijpds-4231	17	16	parkinson	parkinson	NOUN
ijpds-4231	17	17	's	's	PART
ijpds-4231	17	18	disease	disease	NOUN
ijpds-4231	17	19	,	,	PUNCT
ijpds-4231	17	20	memory	memory	NOUN
ijpds-4231	17	21	disorders	disorder	NOUN
ijpds-4231	17	22	and	and	CCONJ
ijpds-4231	17	23	dementia	dementia	NOUN
ijpds-4231	17	24	of	of	ADP
ijpds-4231	17	25	the	the	DET
ijpds-4231	17	26	alzheimer	alzheimer	PROPN
ijpds-4231	17	27	type	type	NOUN
ijpds-4231	17	28	(	(	PUNCT
ijpds-4231	17	29	dat	dat	PROPN
ijpds-4231	17	30	)	)	PUNCT
ijpds-4231	17	31	,	,	PUNCT
ijpds-4231	17	32	depression	depression	NOUN
ijpds-4231	17	33	,	,	PUNCT
ijpds-4231	17	34	and	and	CCONJ
ijpds-4231	17	35	hyperactive	hyperactive	ADJ
ijpds-4231	17	36	syndrome	syndrome	NOUN
ijpds-4231	17	37	in	in	ADP
ijpds-4231	17	38	children	child	NOUN
ijpds-4231	17	39	[	[	X
ijpds-4231	17	40	3	3	NUM
ijpds-4231	17	41	]	]	PUNCT
ijpds-4231	17	42	.	.	PUNCT
ijpds-4231	18	1	the	the	DET
ijpds-4231	18	2	s-(-)-enantiomer	s-(-)-enantiomer	PROPN
ijpds-4231	18	3	of	of	ADP
ijpds-4231	18	4	rasagiline	rasagiline	NOUN
ijpds-4231	18	5	has	have	VERB
ijpds-4231	18	6	a	a	DET
ijpds-4231	18	7	bit	bit	NOUN
ijpds-4231	18	8	of	of	ADP
ijpds-4231	18	9	neuroprotective	neuroprotective	ADJ
ijpds-4231	18	10	properties	property	NOUN
ijpds-4231	18	11	but	but	CCONJ
ijpds-4231	18	12	the	the	DET
ijpds-4231	18	13	potency	potency	NOUN
ijpds-4231	18	14	of	of	ADP
ijpds-4231	18	15	r-(+)enantiomer	r-(+)enantiomer	NOUN
ijpds-4231	18	16	over	over	ADP
ijpds-4231	18	17	the	the	DET
ijpds-4231	18	18	monoamineoxidase	monoamineoxidase	ADJ
ijpds-4231	18	19	enzyme	enzyme	NOUN
ijpds-4231	18	20	(	(	PUNCT
ijpds-4231	18	21	mao	mao	NOUN
ijpds-4231	18	22	-	-	PUNCT
ijpds-4231	18	23	b	b	NOUN
ijpds-4231	18	24	)	)	PUNCT
ijpds-4231	18	25	is	be	AUX
ijpds-4231	18	26	around	around	ADV
ijpds-4231	18	27	1000	1000	NUM
ijpds-4231	18	28	-	-	NUM
ijpds-4231	18	29	fold	fold	VERB
ijpds-4231	18	30	higher	high	ADJ
ijpds-4231	18	31	.	.	PUNCT
ijpds-4231	19	1	however	however	ADV
ijpds-4231	19	2	,	,	PUNCT
ijpds-4231	19	3	the	the	DET
ijpds-4231	19	4	racemic	racemic	ADJ
ijpds-4231	19	5	rasagiline	rasagiline	NOUN
ijpds-4231	19	6	hydrochloride	hydrochloride	NOUN
ijpds-4231	19	7	was	be	AUX
ijpds-4231	19	8	discovered	discover	VERB
ijpds-4231	19	9	in	in	ADP
ijpds-4231	19	10	1970s	1970	NOUN
ijpds-4231	19	11	and	and	CCONJ
ijpds-4231	19	12	was	be	AUX
ijpds-4231	19	13	effectively	effectively	ADV
ijpds-4231	19	14	used	use	VERB
ijpds-4231	19	15	to	to	PART
ijpds-4231	19	16	treat	treat	VERB
ijpds-4231	19	17	hypertension	hypertension	NOUN
ijpds-4231	19	18	[	[	X
ijpds-4231	19	19	4	4	NUM
ijpds-4231	19	20	]	]	PUNCT
ijpds-4231	19	21	.	.	PUNCT
ijpds-4231	20	1	after	after	ADP
ijpds-4231	20	2	achieving	achieve	VERB
ijpds-4231	20	3	the	the	DET
ijpds-4231	20	4	resolution	resolution	NOUN
ijpds-4231	20	5	of	of	ADP
ijpds-4231	20	6	enantiomers	enantiomer	NOUN
ijpds-4231	20	7	,	,	PUNCT
ijpds-4231	20	8	it	it	PRON
ijpds-4231	20	9	was	be	AUX
ijpds-4231	20	10	found	find	VERB
ijpds-4231	20	11	that	that	SCONJ
ijpds-4231	20	12	r-(+)enantiomer	r-(+)enantiomer	NOUN
ijpds-4231	20	13	was	be	AUX
ijpds-4231	20	14	an	an	DET
ijpds-4231	20	15	active	active	ADJ
ijpds-4231	20	16	mao	mao	NOUN
ijpds-4231	20	17	-	-	PUNCT
ijpds-4231	20	18	b	b	NOUN
ijpds-4231	20	19	inhibitor	inhibitor	NOUN
ijpds-4231	20	20	with	with	ADP
ijpds-4231	20	21	a	a	DET
ijpds-4231	20	22	reasonably	reasonably	ADV
ijpds-4231	20	23	high	high	ADJ
ijpds-4231	20	24	degree	degree	NOUN
ijpds-4231	20	25	of	of	ADP
ijpds-4231	20	26	selectivity	selectivity	NOUN
ijpds-4231	20	27	.	.	PUNCT
ijpds-4231	21	1	meanwhile	meanwhile	ADV
ijpds-4231	21	2	,	,	PUNCT
ijpds-4231	21	3	s-(-)enantiomer	s-(-)enantiomer	PROPN
ijpds-4231	21	4	had	have	AUX
ijpds-4231	21	5	showed	show	VERB
ijpds-4231	21	6	relatively	relatively	ADV
ijpds-4231	21	7	very	very	ADV
ijpds-4231	21	8	low	low	ADJ
ijpds-4231	21	9	mao	mao	NOUN
ijpds-4231	21	10	-	-	PUNCT
ijpds-4231	21	11	b	b	NOUN
ijpds-4231	21	12	inhibitory	inhibitory	ADJ
ijpds-4231	21	13	activity	activity	NOUN
ijpds-4231	21	14	[	[	X
ijpds-4231	21	15	5	5	NUM
ijpds-4231	21	16	]	]	PUNCT
ijpds-4231	21	17	.	.	PUNCT
ijpds-4231	22	1	_	_	PUNCT
ijpds-4231	23	1	_	_	PUNCT
ijpds-4231	24	1	_	_	PUNCT
ijpds-4231	25	1	_	_	PUNCT
ijpds-4231	26	1	_	_	PUNCT
ijpds-4231	27	1	_	_	PUNCT
ijpds-4231	28	1	_	_	PUNCT
ijpds-4231	29	1	_	_	PUNCT
ijpds-4231	30	1	_	_	PUNCT
ijpds-4231	31	1	_	_	PUNCT
ijpds-4231	32	1	_	_	PUNCT
ijpds-4231	33	1	_	_	PUNCT
ijpds-4231	34	1	_	_	PUNCT
ijpds-4231	35	1	_	_	PUNCT
ijpds-4231	36	1	_	_	PUNCT
ijpds-4231	37	1	_	_	PUNCT
ijpds-4231	38	1	_	_	PUNCT
ijpds-4231	39	1	_	_	PUNCT
ijpds-4231	40	1	_	_	PUNCT
ijpds-4231	41	1	_	_	PUNCT
ijpds-4231	42	1	_	_	PUNCT
ijpds-4231	43	1	_	_	PUNCT
ijpds-4231	44	1	_	_	PUNCT
ijpds-4231	45	1	_	_	PUNCT
ijpds-4231	46	1	_	_	PUNCT
ijpds-4231	47	1	_	_	PUNCT
ijpds-4231	48	1	_	_	PUNCT
ijpds-4231	49	1	_	_	PUNCT
ijpds-4231	50	1	_	_	PUNCT
ijpds-4231	51	1	_	_	PUNCT
ijpds-4231	52	1	_	_	PUNCT
ijpds-4231	53	1	_	_	PUNCT
ijpds-4231	54	1	_	_	PUNCT
ijpds-4231	55	1	_	_	PUNCT
ijpds-4231	56	1	_	_	PUNCT
ijpds-4231	57	1	_	_	PUNCT
ijpds-4231	58	1	_	_	PUNCT
ijpds-4231	59	1	_	_	PUNCT
ijpds-4231	60	1	_	_	PUNCT
ijpds-4231	61	1	_	_	PUNCT
ijpds-4231	62	1	_	_	PUNCT
ijpds-4231	63	1	_	_	PUNCT
ijpds-4231	64	1	_	_	PUNCT
ijpds-4231	65	1	_	_	PUNCT
ijpds-4231	66	1	_	_	PUNCT
ijpds-4231	67	1	_	_	PUNCT
ijpds-4231	68	1	_	_	PUNCT
ijpds-4231	68	2	correspondence	correspondence	NOUN
ijpds-4231	68	3	to	to	ADP
ijpds-4231	68	4	:	:	PUNCT
ijpds-4231	68	5	sanjay	sanjay	PROPN
ijpds-4231	68	6	sukumar	sukumar	PROPN
ijpds-4231	68	7	saralaya	saralaya	PROPN
ijpds-4231	68	8	,	,	PUNCT
ijpds-4231	68	9	assistant	assistant	NOUN
ijpds-4231	68	10	professor	professor	NOUN
ijpds-4231	68	11	,	,	PUNCT
ijpds-4231	68	12	department	department	NOUN
ijpds-4231	68	13	of	of	ADP
ijpds-4231	68	14	chemistry	chemistry	NOUN
ijpds-4231	68	15	,	,	PUNCT
ijpds-4231	68	16	sri	sri	PROPN
ijpds-4231	68	17	dharmasthala	dharmasthala	PROPN
ijpds-4231	68	18	manjunatheshwara	manjunatheshwara	PROPN
ijpds-4231	68	19	,	,	PUNCT
ijpds-4231	68	20	institute	institute	NOUN
ijpds-4231	68	21	of	of	ADP
ijpds-4231	68	22	technology	technology	NOUN
ijpds-4231	68	23	,	,	PUNCT
ijpds-4231	68	24	[	[	X
ijpds-4231	68	25	affiliated	affiliate	VERB
ijpds-4231	68	26	to	to	AUX
ijpds-4231	68	27	visvesvaraya	visvesvaraya	VERB
ijpds-4231	68	28	technological	technological	ADJ
ijpds-4231	68	29	university	university	NOUN
ijpds-4231	68	30	,	,	PUNCT
ijpds-4231	68	31	belagavi	belagavi	VERB
ijpds-4231	68	32	]	]	PUNCT
ijpds-4231	68	33	,	,	PUNCT
ijpds-4231	68	34	ujire	ujire	NOUN
ijpds-4231	68	35	,	,	PUNCT
ijpds-4231	68	36	belthangady	belthangady	NOUN
ijpds-4231	68	37	taluk	taluk	NOUN
ijpds-4231	68	38	,	,	PUNCT
ijpds-4231	68	39	dakshina	dakshina	PROPN
ijpds-4231	68	40	kannada	kannada	PROPN
ijpds-4231	68	41	,	,	PUNCT
ijpds-4231	68	42	karnataka	karnataka	PROPN
ijpds-4231	68	43	,	,	PUNCT
ijpds-4231	68	44	india	india	PROPN
ijpds-4231	68	45	.	.	PUNCT
ijpds-4231	68	46	pincode	pincode	PROPN
ijpds-4231	68	47	574	574	NUM
ijpds-4231	68	48	240	240	NUM
ijpds-4231	68	49	.	.	PUNCT
ijpds-4231	69	1	email	email	NOUN
ijpds-4231	69	2	:	:	PUNCT
ijpds-4231	69	3	sanjay.saralaya@gmail.com	sanjay.saralaya@gmail.com	X
ijpds-4231	69	4	.	.	PROPN
ijpds-4231	70	1	t	t	PROPN
ijpds-4231	70	2	mailto:sanjay.saralaya@gmail.com	mailto:sanjay.saralaya@gmail.com	PROPN
ijpds-4231	70	3	sanjay	sanjay	PROPN
ijpds-4231	70	4	s	s	PROPN
ijpds-4231	70	5	s	s	NOUN
ijpds-4231	70	6	patents	patent	NOUN
ijpds-4231	70	7	disclosed	disclose	VERB
ijpds-4231	70	8	synthetic	synthetic	ADJ
ijpds-4231	70	9	overview	overview	NOUN
ijpds-4231	70	10	of	of	ADP
ijpds-4231	70	11	rasagiline	rasagiline	ADJ
ijpds-4231	70	12	vol	vol	NOUN
ijpds-4231	70	13	2	2	NUM
ijpds-4231	70	14	|	|	ADV
ijpds-4231	70	15	issue	issue	VERB
ijpds-4231	70	16	4	4	NUM
ijpds-4231	70	17	|	|	ADV
ijpds-4231	70	18	oct	oct	PROPN
ijpds-4231	70	19	–	–	PUNCT
ijpds-4231	70	20	dec	dec	PROPN
ijpds-4231	70	21	2023	2023	NUM
ijpds-4231	70	22	indian	indian	PROPN
ijpds-4231	70	23	j	j	PROPN
ijpds-4231	70	24	pharm	pharm	PROPN
ijpds-4231	70	25	drug	drug	PROPN
ijpds-4231	70	26	studies	study	NOUN
ijpds-4231	70	27	|	|	ADV
ijpds-4231	70	28	133	133	NUM
ijpds-4231	70	29	literature	literature	NOUN
ijpds-4231	70	30	review	review	VERB
ijpds-4231	70	31	a	a	DET
ijpds-4231	70	32	chronological	chronological	ADJ
ijpds-4231	70	33	flow	flow	NOUN
ijpds-4231	70	34	was	be	AUX
ijpds-4231	70	35	maintained	maintain	VERB
ijpds-4231	70	36	in	in	ADP
ijpds-4231	70	37	this	this	DET
ijpds-4231	70	38	review	review	NOUN
ijpds-4231	70	39	initiative	initiative	NOUN
ijpds-4231	70	40	to	to	PART
ijpds-4231	70	41	tabulate	tabulate	VERB
ijpds-4231	70	42	all	all	DET
ijpds-4231	70	43	the	the	DET
ijpds-4231	70	44	essential	essential	ADJ
ijpds-4231	70	45	process	process	NOUN
ijpds-4231	70	46	centric	centric	ADJ
ijpds-4231	70	47	details	detail	NOUN
ijpds-4231	70	48	disclosed	disclose	VERB
ijpds-4231	70	49	in	in	ADP
ijpds-4231	70	50	the	the	DET
ijpds-4231	70	51	prior	prior	ADJ
ijpds-4231	70	52	patents	patent	NOUN
ijpds-4231	70	53	regarding	regard	VERB
ijpds-4231	70	54	the	the	DET
ijpds-4231	70	55	synthesis	synthesis	NOUN
ijpds-4231	70	56	,	,	PUNCT
ijpds-4231	70	57	racemization	racemization	NOUN
ijpds-4231	70	58	,	,	PUNCT
ijpds-4231	70	59	purification	purification	NOUN
ijpds-4231	70	60	,	,	PUNCT
ijpds-4231	70	61	impurity	impurity	NOUN
ijpds-4231	70	62	profiling	profiling	NOUN
ijpds-4231	70	63	,	,	PUNCT
ijpds-4231	70	64	various	various	ADJ
ijpds-4231	70	65	stable	stable	ADJ
ijpds-4231	70	66	salts	salt	NOUN
ijpds-4231	70	67	of	of	ADP
ijpds-4231	70	68	rasagiline	rasagiline	NOUN
ijpds-4231	70	69	and	and	CCONJ
ijpds-4231	70	70	its	its	PRON
ijpds-4231	70	71	crystallograhic	crystallograhic	ADJ
ijpds-4231	70	72	forms	form	NOUN
ijpds-4231	70	73	.	.	PUNCT
ijpds-4231	71	1	nh2	nh2	NOUN
ijpds-4231	71	2	2	2	NUM
ijpds-4231	71	3	br	br	PROPN
ijpds-4231	71	4	3	3	NUM
ijpds-4231	71	5	n4	n4	PROPN
ijpds-4231	71	6	cl	cl	PROPN
ijpds-4231	71	7	5	5	NUM
ijpds-4231	71	8	nh2	nh2	NOUN
ijpds-4231	71	9	6	6	NUM
ijpds-4231	71	10	cl	cl	NOUN
ijpds-4231	71	11	7	7	NUM
ijpds-4231	72	1	oh13	oh13	PROPN
ijpds-4231	72	2	s	s	PART
ijpds-4231	72	3	o	o	NOUN
ijpds-4231	72	4	o	o	X
ijpds-4231	72	5	s	s	X
ijpds-4231	73	1	o	o	NOUN
ijpds-4231	73	2	o	o	X
ijpds-4231	73	3	o	o	NOUN
ijpds-4231	73	4	14	14	NUM
ijpds-4231	73	5	s	s	NOUN
ijpds-4231	73	6	o	o	NOUN
ijpds-4231	73	7	oo	oo	INTJ
ijpds-4231	73	8	8	8	NUM
ijpds-4231	73	9	o	o	NOUN
ijpds-4231	73	10	nh9	nh9	NOUN
ijpds-4231	73	11	11	11	NUM
ijpds-4231	73	12	cl12	cl12	PROPN
ijpds-4231	73	13	nh2	nh2	PROPN
ijpds-4231	73	14	10	10	NUM
ijpds-4231	73	15	huebner	huebner	PROPN
ijpds-4231	73	16	cf	cf	PROPN
ijpds-4231	73	17	.	.	PROPN
ijpds-4231	73	18	,	,	PUNCT
ijpds-4231	73	19	in	in	ADP
ijpds-4231	73	20	1966	1966	NUM
ijpds-4231	73	21	,	,	PUNCT
ijpds-4231	73	22	had	have	AUX
ijpds-4231	73	23	reported	report	VERB
ijpds-4231	73	24	the	the	DET
ijpds-4231	73	25	condensation	condensation	NOUN
ijpds-4231	73	26	of	of	ADP
ijpds-4231	73	27	1amino	1amino	NUM
ijpds-4231	73	28	-	-	PUNCT
ijpds-4231	73	29	indane	indane	NOUN
ijpds-4231	73	30	2	2	NUM
ijpds-4231	73	31	with	with	ADP
ijpds-4231	73	32	propargyl	propargyl	PROPN
ijpds-4231	73	33	bromide	bromide	NOUN
ijpds-4231	73	34	3	3	NUM
ijpds-4231	73	35	in	in	ADP
ijpds-4231	73	36	the	the	DET
ijpds-4231	73	37	presence	presence	NOUN
ijpds-4231	73	38	of	of	ADP
ijpds-4231	73	39	sodium	sodium	NOUN
ijpds-4231	73	40	carbonate	carbonate	NOUN
ijpds-4231	73	41	and	and	CCONJ
ijpds-4231	73	42	acetone	acetone	NOUN
ijpds-4231	73	43	to	to	PART
ijpds-4231	73	44	isolate	isolate	VERB
ijpds-4231	73	45	1-(n	1-(n	NUM
ijpds-4231	73	46	,	,	PUNCT
ijpds-4231	73	47	ndipropargyl	ndipropargyl	NOUN
ijpds-4231	73	48	-	-	PUNCT
ijpds-4231	73	49	amino)-indane	amino)-indane	PROPN
ijpds-4231	73	50	hydrochloride	hydrochloride	NOUN
ijpds-4231	73	51	4	4	NUM
ijpds-4231	73	52	with	with	ADP
ijpds-4231	73	53	a	a	DET
ijpds-4231	73	54	melting	melting	NOUN
ijpds-4231	73	55	point	point	NOUN
ijpds-4231	73	56	of	of	ADP
ijpds-4231	73	57	160	160	NUM
ijpds-4231	73	58	-	-	PUNCT
ijpds-4231	73	59	163oc	163oc	NOUN
ijpds-4231	73	60	(	(	PUNCT
ijpds-4231	73	61	yield	yield	NOUN
ijpds-4231	73	62	:	:	PUNCT
ijpds-4231	73	63	11.82	11.82	NUM
ijpds-4231	73	64	%	%	NOUN
ijpds-4231	73	65	,	,	PUNCT
ijpds-4231	73	66	recrystallized	recrystallize	VERB
ijpds-4231	73	67	from	from	ADP
ijpds-4231	73	68	ethyl	ethyl	PROPN
ijpds-4231	73	69	alcohol	alcohol	PROPN
ijpds-4231	73	70	)	)	PUNCT
ijpds-4231	73	71	.	.	PUNCT
ijpds-4231	74	1	furthermore	furthermore	ADV
ijpds-4231	74	2	,	,	PUNCT
ijpds-4231	74	3	the	the	DET
ijpds-4231	74	4	condensation	condensation	NOUN
ijpds-4231	74	5	of	of	ADP
ijpds-4231	74	6	1	1	NUM
ijpds-4231	74	7	-	-	PUNCT
ijpds-4231	74	8	chloroindane	chloroindane	NOUN
ijpds-4231	74	9	5	5	NUM
ijpds-4231	74	10	with	with	ADP
ijpds-4231	74	11	propargylamine	propargylamine	NOUN
ijpds-4231	74	12	6	6	NUM
ijpds-4231	74	13	was	be	AUX
ijpds-4231	74	14	achieved	achieve	VERB
ijpds-4231	74	15	in	in	ADP
ijpds-4231	74	16	isopropyl	isopropyl	NOUN
ijpds-4231	74	17	alcohol	alcohol	NOUN
ijpds-4231	74	18	to	to	PART
ijpds-4231	74	19	isolate	isolate	VERB
ijpds-4231	74	20	the	the	DET
ijpds-4231	74	21	racemic	racemic	ADJ
ijpds-4231	74	22	rasagiline	rasagiline	NOUN
ijpds-4231	74	23	hydrochloride	hydrochloride	NOUN
ijpds-4231	74	24	with	with	ADP
ijpds-4231	74	25	a	a	DET
ijpds-4231	74	26	melting	melting	NOUN
ijpds-4231	74	27	point	point	NOUN
ijpds-4231	74	28	of	of	ADP
ijpds-4231	74	29	178	178	NUM
ijpds-4231	74	30	-	-	PUNCT
ijpds-4231	74	31	179oc	179oc	NOUN
ijpds-4231	74	32	(	(	PUNCT
ijpds-4231	74	33	yield	yield	NOUN
ijpds-4231	74	34	:	:	PUNCT
ijpds-4231	74	35	22.27	22.27	NUM
ijpds-4231	74	36	%	%	NOUN
ijpds-4231	74	37	,	,	PUNCT
ijpds-4231	74	38	recrystallized	recrystallize	VERB
ijpds-4231	74	39	from	from	ADP
ijpds-4231	74	40	ethyl	ethyl	PROPN
ijpds-4231	74	41	alcohol	alcohol	NOUN
ijpds-4231	74	42	)	)	PUNCT
ijpds-4231	75	1	[	[	X
ijpds-4231	75	2	6	6	NUM
ijpds-4231	75	3	]	]	PUNCT
ijpds-4231	75	4	.	.	PUNCT
ijpds-4231	76	1	maurice	maurice	PROPN
ijpds-4231	76	2	wg	wg	PROPN
ijpds-4231	76	3	,	,	PUNCT
ijpds-4231	76	4	et	et	PROPN
ijpds-4231	76	5	al	al	PROPN
ijpds-4231	76	6	.	.	PROPN
ijpds-4231	76	7	,	,	PUNCT
ijpds-4231	76	8	in	in	ADP
ijpds-4231	76	9	1968	1968	NUM
ijpds-4231	76	10	&	&	CCONJ
ijpds-4231	76	11	1970	1970	NUM
ijpds-4231	76	12	,	,	PUNCT
ijpds-4231	76	13	had	have	AUX
ijpds-4231	76	14	demonstrated	demonstrate	VERB
ijpds-4231	76	15	synthesis	synthesis	NOUN
ijpds-4231	76	16	and	and	CCONJ
ijpds-4231	76	17	applications	application	NOUN
ijpds-4231	76	18	of	of	ADP
ijpds-4231	76	19	n	n	ADV
ijpds-4231	76	20	-	-	PUNCT
ijpds-4231	76	21	substituted	substitute	VERB
ijpds-4231	76	22	1aminoindanes	1aminoindane	NOUN
ijpds-4231	76	23	.	.	PUNCT
ijpds-4231	77	1	the	the	DET
ijpds-4231	77	2	condensation	condensation	NOUN
ijpds-4231	77	3	of	of	ADP
ijpds-4231	77	4	5	5	NUM
ijpds-4231	77	5	with	with	ADP
ijpds-4231	77	6	6	6	NUM
ijpds-4231	77	7	was	be	AUX
ijpds-4231	77	8	executed	execute	VERB
ijpds-4231	77	9	in	in	ADP
ijpds-4231	77	10	the	the	DET
ijpds-4231	77	11	presence	presence	NOUN
ijpds-4231	77	12	of	of	ADP
ijpds-4231	77	13	sodium	sodium	NOUN
ijpds-4231	77	14	iodide	iodide	NOUN
ijpds-4231	77	15	in	in	ADP
ijpds-4231	77	16	ethyl	ethyl	PROPN
ijpds-4231	77	17	alcohol	alcohol	NOUN
ijpds-4231	77	18	to	to	PART
ijpds-4231	77	19	isolate	isolate	VERB
ijpds-4231	77	20	the	the	DET
ijpds-4231	77	21	racemic	racemic	ADJ
ijpds-4231	77	22	rasagiline	rasagiline	NOUN
ijpds-4231	77	23	hydrochloride	hydrochloride	NOUN
ijpds-4231	77	24	with	with	ADP
ijpds-4231	77	25	a	a	DET
ijpds-4231	77	26	melting	melting	NOUN
ijpds-4231	77	27	point	point	NOUN
ijpds-4231	77	28	of	of	ADP
ijpds-4231	77	29	185	185	NUM
ijpds-4231	77	30	-	-	PUNCT
ijpds-4231	77	31	187oc	187oc	NOUN
ijpds-4231	77	32	(	(	PUNCT
ijpds-4231	77	33	recrystallized	recrystallize	VERB
ijpds-4231	77	34	from	from	ADP
ijpds-4231	77	35	isopropyl	isopropyl	NOUN
ijpds-4231	77	36	alcohol	alcohol	NOUN
ijpds-4231	77	37	)	)	PUNCT
ijpds-4231	77	38	.	.	PUNCT
ijpds-4231	78	1	it	it	PRON
ijpds-4231	78	2	was	be	AUX
ijpds-4231	78	3	believed	believe	VERB
ijpds-4231	78	4	that	that	SCONJ
ijpds-4231	78	5	,	,	PUNCT
ijpds-4231	78	6	n	n	CCONJ
ijpds-4231	78	7	,	,	PUNCT
ijpds-4231	78	8	n	n	CCONJ
ijpds-4231	78	9	-	-	PUNCT
ijpds-4231	78	10	di(1	di(1	NOUN
ijpds-4231	78	11	-	-	PUNCT
ijpds-4231	78	12	indanyl)-propargyl	indanyl)-propargyl	ADJ
ijpds-4231	78	13	amine	amine	ADJ
ijpds-4231	78	14	hydrochloride	hydrochloride	NOUN
ijpds-4231	78	15	(	(	PUNCT
ijpds-4231	78	16	dimer	dimer	NOUN
ijpds-4231	78	17	)	)	PUNCT
ijpds-4231	78	18	had	have	AUX
ijpds-4231	78	19	formed	form	VERB
ijpds-4231	78	20	as	as	ADP
ijpds-4231	78	21	an	an	DET
ijpds-4231	78	22	intermediate	intermediate	ADJ
ijpds-4231	79	1	[	[	X
ijpds-4231	79	2	4,7	4,7	NUM
ijpds-4231	79	3	]	]	PUNCT
ijpds-4231	79	4	.	.	PUNCT
ijpds-4231	80	1	youdim	youdim	PROPN
ijpds-4231	80	2	mbh	mbh	PROPN
ijpds-4231	80	3	,	,	PUNCT
ijpds-4231	80	4	et	et	PROPN
ijpds-4231	80	5	al	al	PROPN
ijpds-4231	80	6	.	.	PROPN
ijpds-4231	80	7	,	,	PUNCT
ijpds-4231	80	8	in	in	ADP
ijpds-4231	80	9	1991	1991	NUM
ijpds-4231	80	10	,	,	PUNCT
ijpds-4231	80	11	1995	1995	NUM
ijpds-4231	80	12	&	&	CCONJ
ijpds-4231	80	13	1996	1996	NUM
ijpds-4231	80	14	,	,	PUNCT
ijpds-4231	80	15	had	have	AUX
ijpds-4231	80	16	illustrated	illustrate	VERB
ijpds-4231	80	17	the	the	DET
ijpds-4231	80	18	synthesis	synthesis	NOUN
ijpds-4231	80	19	and	and	CCONJ
ijpds-4231	80	20	effective	effective	ADJ
ijpds-4231	80	21	resolution	resolution	NOUN
ijpds-4231	80	22	of	of	ADP
ijpds-4231	80	23	the	the	DET
ijpds-4231	80	24	racemic	racemic	ADJ
ijpds-4231	80	25	rasagiline	rasagiline	NOUN
ijpds-4231	80	26	base	base	NOUN
ijpds-4231	80	27	.	.	PUNCT
ijpds-4231	81	1	rasagiline	rasagiline	PROPN
ijpds-4231	81	2	base	base	PROPN
ijpds-4231	81	3	was	be	AUX
ijpds-4231	81	4	prepared	prepare	VERB
ijpds-4231	81	5	by	by	ADP
ijpds-4231	81	6	treating	treat	VERB
ijpds-4231	81	7	2	2	NUM
ijpds-4231	81	8	with	with	ADP
ijpds-4231	81	9	propargyl	propargyl	PROPN
ijpds-4231	81	10	chloride	chloride	PROPN
ijpds-4231	81	11	7	7	NUM
ijpds-4231	81	12	in	in	ADP
ijpds-4231	81	13	the	the	DET
ijpds-4231	81	14	presence	presence	NOUN
ijpds-4231	81	15	of	of	ADP
ijpds-4231	81	16	potassium	potassium	NOUN
ijpds-4231	81	17	carbonate	carbonate	NOUN
ijpds-4231	81	18	and	and	CCONJ
ijpds-4231	81	19	acetonitrile	acetonitrile	NOUN
ijpds-4231	81	20	.	.	PUNCT
ijpds-4231	82	1	the	the	DET
ijpds-4231	82	2	isolated	isolated	ADJ
ijpds-4231	82	3	rasagiline	rasagiline	NOUN
ijpds-4231	82	4	base	base	NOUN
ijpds-4231	82	5	was	be	AUX
ijpds-4231	82	6	treated	treat	VERB
ijpds-4231	82	7	with	with	ADP
ijpds-4231	82	8	ethereal	ethereal	ADJ
ijpds-4231	82	9	hydrochloride	hydrochloride	NOUN
ijpds-4231	82	10	(	(	PUNCT
ijpds-4231	82	11	hcl	hcl	PROPN
ijpds-4231	82	12	gas	gas	NOUN
ijpds-4231	82	13	purged	purge	VERB
ijpds-4231	82	14	to	to	ADP
ijpds-4231	82	15	diethyl	diethyl	NOUN
ijpds-4231	82	16	ether	ether	NOUN
ijpds-4231	82	17	)	)	PUNCT
ijpds-4231	82	18	to	to	PART
ijpds-4231	82	19	isolate	isolate	VERB
ijpds-4231	82	20	the	the	DET
ijpds-4231	82	21	rasagiline	rasagiline	ADJ
ijpds-4231	82	22	hydrochloride	hydrochloride	NOUN
ijpds-4231	82	23	with	with	ADP
ijpds-4231	82	24	a	a	DET
ijpds-4231	82	25	melting	melting	NOUN
ijpds-4231	82	26	point	point	NOUN
ijpds-4231	82	27	of	of	ADP
ijpds-4231	82	28	182	182	NUM
ijpds-4231	82	29	-	-	PUNCT
ijpds-4231	82	30	184oc	184oc	NOUN
ijpds-4231	82	31	(	(	PUNCT
ijpds-4231	82	32	yield	yield	NOUN
ijpds-4231	82	33	:	:	PUNCT
ijpds-4231	82	34	46.82	46.82	NUM
ijpds-4231	82	35	%	%	NOUN
ijpds-4231	82	36	,	,	PUNCT
ijpds-4231	82	37	recrystallized	recrystallize	VERB
ijpds-4231	82	38	from	from	ADP
ijpds-4231	82	39	isopropyl	isopropyl	NOUN
ijpds-4231	82	40	alcohol).the	alcohol).the	DET
ijpds-4231	82	41	racemic	racemic	ADJ
ijpds-4231	82	42	mixture	mixture	NOUN
ijpds-4231	82	43	of	of	ADP
ijpds-4231	82	44	rasagiline	rasagiline	NOUN
ijpds-4231	82	45	base	base	NOUN
ijpds-4231	82	46	was	be	AUX
ijpds-4231	82	47	resolved	resolve	VERB
ijpds-4231	82	48	in	in	ADP
ijpds-4231	82	49	a	a	DET
ijpds-4231	82	50	preparative	preparative	ADJ
ijpds-4231	82	51	hplc	hplc	NOUN
ijpds-4231	82	52	(	(	PUNCT
ijpds-4231	82	53	high	high	ADJ
ijpds-4231	82	54	performance	performance	NOUN
ijpds-4231	82	55	liquid	liquid	NOUN
ijpds-4231	82	56	chromatography	chromatography	NOUN
ijpds-4231	82	57	)	)	PUNCT
ijpds-4231	82	58	column	column	NOUN
ijpds-4231	82	59	and	and	CCONJ
ijpds-4231	82	60	converted	convert	VERB
ijpds-4231	82	61	to	to	ADP
ijpds-4231	82	62	s-(-)enantiomer	s-(-)enantiomer	NOUN
ijpds-4231	82	63	hydrochloride	hydrochloride	NOUN
ijpds-4231	82	64	with	with	ADP
ijpds-4231	82	65	a	a	DET
ijpds-4231	82	66	melting	melting	NOUN
ijpds-4231	82	67	point	point	NOUN
ijpds-4231	82	68	of	of	ADP
ijpds-4231	82	69	182184oc	182184oc	NOUN
ijpds-4231	82	70	(	(	PUNCT
ijpds-4231	82	71	isolated	isolate	VERB
ijpds-4231	82	72	from	from	ADP
ijpds-4231	82	73	diethyl	diethyl	NOUN
ijpds-4231	82	74	ether	ether	NOUN
ijpds-4231	82	75	)	)	PUNCT
ijpds-4231	82	76	.	.	PUNCT
ijpds-4231	83	1	similarly	similarly	ADV
ijpds-4231	83	2	,	,	PUNCT
ijpds-4231	83	3	r-(+)enantiomer	r-(+)enantiomer	NOUN
ijpds-4231	83	4	hydrochloride	hydrochloride	NOUN
ijpds-4231	83	5	was	be	AUX
ijpds-4231	83	6	isolated	isolate	VERB
ijpds-4231	83	7	with	with	ADP
ijpds-4231	83	8	a	a	DET
ijpds-4231	83	9	melting	melting	NOUN
ijpds-4231	83	10	point	point	NOUN
ijpds-4231	83	11	of	of	ADP
ijpds-4231	83	12	179	179	NUM
ijpds-4231	83	13	-	-	PUNCT
ijpds-4231	83	14	181oc	181oc	ADJ
ijpds-4231	83	15	(	(	PUNCT
ijpds-4231	83	16	isolated	isolate	VERB
ijpds-4231	83	17	from	from	ADP
ijpds-4231	83	18	diethyl	diethyl	NOUN
ijpds-4231	83	19	ether	ether	NOUN
ijpds-4231	83	20	)	)	PUNCT
ijpds-4231	83	21	.	.	PUNCT
ijpds-4231	84	1	moreover	moreover	ADV
ijpds-4231	84	2	,	,	PUNCT
ijpds-4231	84	3	the	the	DET
ijpds-4231	84	4	work	work	NOUN
ijpds-4231	84	5	extends	extend	VERB
ijpds-4231	84	6	to	to	PART
ijpds-4231	84	7	report	report	VERB
ijpds-4231	84	8	the	the	DET
ijpds-4231	84	9	reaction	reaction	NOUN
ijpds-4231	84	10	of	of	ADP
ijpds-4231	84	11	r-(-)enantiomer	r-(-)enantiomer	NOUN
ijpds-4231	84	12	of	of	ADP
ijpds-4231	84	13	2	2	NUM
ijpds-4231	84	14	with	with	ADP
ijpds-4231	84	15	7	7	NUM
ijpds-4231	84	16	in	in	ADP
ijpds-4231	84	17	the	the	DET
ijpds-4231	84	18	presence	presence	NOUN
ijpds-4231	84	19	of	of	ADP
ijpds-4231	84	20	potassium	potassium	NOUN
ijpds-4231	84	21	carbonate	carbonate	NOUN
ijpds-4231	84	22	and	and	CCONJ
ijpds-4231	84	23	acetonitrile	acetonitrile	NOUN
ijpds-4231	84	24	to	to	PART
ijpds-4231	84	25	isolate	isolate	VERB
ijpds-4231	84	26	r-(+)-enantiomer	r-(+)-enantiomer	NOUN
ijpds-4231	84	27	of	of	ADP
ijpds-4231	84	28	rasagiline	rasagiline	ADJ
ijpds-4231	84	29	hydrochloride	hydrochloride	NOUN
ijpds-4231	84	30	with	with	ADP
ijpds-4231	84	31	a	a	DET
ijpds-4231	84	32	melting	melting	NOUN
ijpds-4231	84	33	point	point	NOUN
ijpds-4231	84	34	of	of	ADP
ijpds-4231	84	35	183185oc	183185oc	NOUN
ijpds-4231	84	36	(	(	PUNCT
ijpds-4231	84	37	yield	yield	NOUN
ijpds-4231	84	38	:	:	PUNCT
ijpds-4231	84	39	35.18	35.18	NUM
ijpds-4231	84	40	%	%	NOUN
ijpds-4231	84	41	,	,	PUNCT
ijpds-4231	84	42	recrystallized	recrystallize	VERB
ijpds-4231	84	43	from	from	ADP
ijpds-4231	84	44	isopropyl	isopropyl	NOUN
ijpds-4231	84	45	alcohol	alcohol	NOUN
ijpds-4231	84	46	)	)	PUNCT
ijpds-4231	84	47	.	.	PUNCT
ijpds-4231	85	1	under	under	ADP
ijpds-4231	85	2	the	the	DET
ijpds-4231	85	3	similar	similar	ADJ
ijpds-4231	85	4	context	context	NOUN
ijpds-4231	85	5	,	,	PUNCT
ijpds-4231	85	6	s-(+)-enantiomer	s-(+)-enantiomer	NUM
ijpds-4231	85	7	of	of	ADP
ijpds-4231	85	8	2	2	NUM
ijpds-4231	85	9	was	be	AUX
ijpds-4231	85	10	reacted	react	VERB
ijpds-4231	85	11	with	with	ADP
ijpds-4231	85	12	7	7	NUM
ijpds-4231	85	13	to	to	PART
ijpds-4231	85	14	get	get	VERB
ijpds-4231	85	15	s-(-)-enantiomer	s-(-)-enantiomer	PROPN
ijpds-4231	85	16	of	of	ADP
ijpds-4231	85	17	rasagiline	rasagiline	ADJ
ijpds-4231	85	18	hydrochloride	hydrochloride	NOUN
ijpds-4231	85	19	with	with	ADP
ijpds-4231	85	20	a	a	DET
ijpds-4231	85	21	melting	melting	NOUN
ijpds-4231	85	22	point	point	NOUN
ijpds-4231	85	23	of	of	ADP
ijpds-4231	85	24	183	183	NUM
ijpds-4231	85	25	-	-	PUNCT
ijpds-4231	85	26	185oc	185oc	NOUN
ijpds-4231	85	27	(	(	PUNCT
ijpds-4231	85	28	recrystallized	recrystallize	VERB
ijpds-4231	85	29	from	from	ADP
ijpds-4231	85	30	isopropyl	isopropyl	NOUN
ijpds-4231	85	31	alcohol	alcohol	NOUN
ijpds-4231	85	32	)	)	PUNCT
ijpds-4231	85	33	.	.	PUNCT
ijpds-4231	86	1	furthermore	furthermore	ADV
ijpds-4231	86	2	,	,	PUNCT
ijpds-4231	86	3	r(+)-rasagiline	r(+)-rasagiline	ADJ
ijpds-4231	86	4	base	base	NOUN
ijpds-4231	86	5	was	be	AUX
ijpds-4231	86	6	treated	treat	VERB
ijpds-4231	86	7	with	with	ADP
ijpds-4231	86	8	l	l	ADJ
ijpds-4231	86	9	-	-	ADJ
ijpds-4231	86	10	tartaric	tartaric	ADJ
ijpds-4231	86	11	acid	acid	NOUN
ijpds-4231	86	12	to	to	PART
ijpds-4231	86	13	isolate	isolate	VERB
ijpds-4231	86	14	r-(+)-di	r-(+)-di	NOUN
ijpds-4231	86	15	-	-	ADJ
ijpds-4231	86	16	rasagiline	rasagiline	NOUN
ijpds-4231	86	17	tartarate	tartarate	NOUN
ijpds-4231	86	18	with	with	ADP
ijpds-4231	86	19	a	a	DET
ijpds-4231	86	20	melting	melting	NOUN
ijpds-4231	86	21	point	point	NOUN
ijpds-4231	86	22	of	of	ADP
ijpds-4231	86	23	175	175	NUM
ijpds-4231	86	24	-	-	PUNCT
ijpds-4231	86	25	177oc	177oc	NOUN
ijpds-4231	86	26	(	(	PUNCT
ijpds-4231	86	27	yield	yield	NOUN
ijpds-4231	86	28	:	:	PUNCT
ijpds-4231	86	29	46.59	46.59	NUM
ijpds-4231	86	30	%	%	NOUN
ijpds-4231	86	31	,	,	PUNCT
ijpds-4231	86	32	isolated	isolate	VERB
ijpds-4231	86	33	from	from	ADP
ijpds-4231	86	34	methyl	methyl	NOUN
ijpds-4231	86	35	alcohol	alcohol	NOUN
ijpds-4231	86	36	)	)	PUNCT
ijpds-4231	86	37	.	.	PUNCT
ijpds-4231	87	1	in	in	ADP
ijpds-4231	87	2	an	an	DET
ijpds-4231	87	3	illustration	illustration	NOUN
ijpds-4231	87	4	,	,	PUNCT
ijpds-4231	87	5	propargyl	propargyl	PROPN
ijpds-4231	87	6	benzenesulfonate	benzenesulfonate	VERB
ijpds-4231	87	7	8	8	NUM
ijpds-4231	87	8	was	be	AUX
ijpds-4231	87	9	reacted	react	VERB
ijpds-4231	87	10	with	with	ADP
ijpds-4231	87	11	racemic	racemic	ADJ
ijpds-4231	87	12	2	2	NUM
ijpds-4231	87	13	in	in	ADP
ijpds-4231	87	14	the	the	DET
ijpds-4231	87	15	presence	presence	NOUN
ijpds-4231	87	16	of	of	ADP
ijpds-4231	87	17	aqueous	aqueous	ADJ
ijpds-4231	87	18	sodium	sodium	NOUN
ijpds-4231	87	19	hydroxide	hydroxide	NOUN
ijpds-4231	87	20	in	in	ADP
ijpds-4231	87	21	toluene	toluene	NOUN
ijpds-4231	87	22	to	to	PART
ijpds-4231	87	23	isolate	isolate	VERB
ijpds-4231	87	24	r-(+)-di	r-(+)-di	NOUN
ijpds-4231	87	25	-	-	ADJ
ijpds-4231	87	26	rasagiline	rasagiline	NOUN
ijpds-4231	87	27	tartarate	tartarate	NOUN
ijpds-4231	87	28	.	.	PUNCT
ijpds-4231	88	1	it	it	PRON
ijpds-4231	88	2	was	be	AUX
ijpds-4231	88	3	treated	treat	VERB
ijpds-4231	88	4	with	with	ADP
ijpds-4231	88	5	methanesulfonic	methanesulfonic	ADJ
ijpds-4231	88	6	acid	acid	NOUN
ijpds-4231	88	7	in	in	ADP
ijpds-4231	88	8	isopropyl	isopropyl	NOUN
ijpds-4231	88	9	alcohol	alcohol	NOUN
ijpds-4231	88	10	to	to	PART
ijpds-4231	88	11	isolate	isolate	VERB
ijpds-4231	88	12	1	1	NUM
ijpds-4231	88	13	with	with	ADP
ijpds-4231	88	14	a	a	DET
ijpds-4231	88	15	melting	melting	NOUN
ijpds-4231	88	16	point	point	NOUN
ijpds-4231	88	17	of	of	ADP
ijpds-4231	88	18	157oc	157oc	NOUN
ijpds-4231	88	19	.	.	PUNCT
ijpds-4231	89	1	[	[	X
ijpds-4231	89	2	5,8	5,8	NUM
ijpds-4231	89	3	-	-	SYM
ijpds-4231	89	4	11	11	NUM
ijpds-4231	89	5	]	]	PUNCT
ijpds-4231	89	6	.	.	PUNCT
ijpds-4231	90	1	gutman	gutman	PROPN
ijpds-4231	90	2	al	al	PROPN
ijpds-4231	90	3	,	,	PUNCT
ijpds-4231	90	4	et	et	PROPN
ijpds-4231	90	5	al	al	PROPN
ijpds-4231	90	6	.	.	PROPN
ijpds-4231	90	7	,	,	PUNCT
ijpds-4231	90	8	in	in	ADP
ijpds-4231	90	9	2002	2002	NUM
ijpds-4231	90	10	,	,	PUNCT
ijpds-4231	90	11	had	have	AUX
ijpds-4231	90	12	reported	report	VERB
ijpds-4231	90	13	the	the	DET
ijpds-4231	90	14	condensation	condensation	NOUN
ijpds-4231	90	15	of	of	ADP
ijpds-4231	90	16	2,3	2,3	NUM
ijpds-4231	90	17	-	-	ADJ
ijpds-4231	90	18	dihydro-1h-1	dihydro-1h-1	ADJ
ijpds-4231	90	19	-	-	PUNCT
ijpds-4231	90	20	indanone	indanone	NOUN
ijpds-4231	90	21	9	9	NUM
ijpds-4231	90	22	with	with	ADP
ijpds-4231	90	23	benzylamine	benzylamine	NOUN
ijpds-4231	90	24	10	10	NUM
ijpds-4231	90	25	in	in	ADP
ijpds-4231	90	26	the	the	DET
ijpds-4231	90	27	presence	presence	NOUN
ijpds-4231	90	28	of	of	ADP
ijpds-4231	90	29	acetic	acetic	ADJ
ijpds-4231	90	30	acid	acid	NOUN
ijpds-4231	90	31	and	and	CCONJ
ijpds-4231	90	32	benzene	benzene	NOUN
ijpds-4231	90	33	to	to	PART
ijpds-4231	90	34	form	form	VERB
ijpds-4231	90	35	the	the	DET
ijpds-4231	90	36	important	important	ADJ
ijpds-4231	90	37	imine	imine	ADJ
ijpds-4231	90	38	intermediate	intermediate	NOUN
ijpds-4231	90	39	.	.	PUNCT
ijpds-4231	91	1	it	it	PRON
ijpds-4231	91	2	was	be	AUX
ijpds-4231	91	3	reduced	reduce	VERB
ijpds-4231	91	4	using	use	VERB
ijpds-4231	91	5	sodium	sodium	NOUN
ijpds-4231	91	6	borohydride	borohydride	NOUN
ijpds-4231	91	7	in	in	ADP
ijpds-4231	91	8	ethyl	ethyl	PROPN
ijpds-4231	91	9	alcohol	alcohol	NOUN
ijpds-4231	91	10	and	and	CCONJ
ijpds-4231	91	11	treated	treat	VERB
ijpds-4231	91	12	with	with	ADP
ijpds-4231	91	13	sodium	sodium	NOUN
ijpds-4231	91	14	hydroxide	hydroxide	NOUN
ijpds-4231	91	15	solution	solution	NOUN
ijpds-4231	91	16	to	to	PART
ijpds-4231	91	17	isolate	isolate	VERB
ijpds-4231	91	18	the	the	DET
ijpds-4231	91	19	racemic	racemic	ADJ
ijpds-4231	91	20	n	n	CCONJ
ijpds-4231	91	21	-	-	PUNCT
ijpds-4231	91	22	benzyl-2,3dihydro-1h	benzyl-2,3dihydro-1h	NOUN
ijpds-4231	91	23	-	-	PUNCT
ijpds-4231	91	24	inden-1	inden-1	NOUN
ijpds-4231	91	25	-	-	PUNCT
ijpds-4231	91	26	amine	amine	ADJ
ijpds-4231	91	27	11	11	NUM
ijpds-4231	91	28	with	with	ADP
ijpds-4231	91	29	a	a	DET
ijpds-4231	91	30	boiling	boiling	NOUN
ijpds-4231	91	31	point	point	NOUN
ijpds-4231	91	32	of	of	ADP
ijpds-4231	91	33	125135oc	125135oc	NOUN
ijpds-4231	91	34	(	(	PUNCT
ijpds-4231	91	35	yield	yield	NOUN
ijpds-4231	91	36	:	:	PUNCT
ijpds-4231	91	37	82	82	NUM
ijpds-4231	91	38	%	%	NOUN
ijpds-4231	91	39	,	,	PUNCT
ijpds-4231	91	40	purity	purity	NOUN
ijpds-4231	91	41	:	:	PUNCT
ijpds-4231	91	42	95.9	95.9	NUM
ijpds-4231	91	43	%	%	NOUN
ijpds-4231	91	44	by	by	ADP
ijpds-4231	91	45	gas	gas	NOUN
ijpds-4231	91	46	chromatographyhttps://patents.google.com/?inventor=huebner+charles+ferdinand	chromatographyhttps://patents.google.com/?inventor=huebner+charles+ferdinand	NOUN
ijpds-4231	91	47	sanjay	sanjay	PROPN
ijpds-4231	91	48	s	s	PART
ijpds-4231	91	49	s	s	NOUN
ijpds-4231	91	50	patents	patent	NOUN
ijpds-4231	91	51	disclosed	disclose	VERB
ijpds-4231	91	52	synthetic	synthetic	ADJ
ijpds-4231	91	53	overview	overview	NOUN
ijpds-4231	91	54	of	of	ADP
ijpds-4231	91	55	rasagiline	rasagiline	ADJ
ijpds-4231	91	56	vol	vol	NOUN
ijpds-4231	91	57	2	2	NUM
ijpds-4231	91	58	|	|	ADV
ijpds-4231	91	59	issue	issue	VERB
ijpds-4231	91	60	4	4	NUM
ijpds-4231	91	61	|	|	ADV
ijpds-4231	91	62	oct	oct	PROPN
ijpds-4231	91	63	–	–	PUNCT
ijpds-4231	92	1	dec	dec	PROPN
ijpds-4231	92	2	2023	2023	NUM
ijpds-4231	92	3	indian	indian	PROPN
ijpds-4231	92	4	j	j	PROPN
ijpds-4231	92	5	pharm	pharm	PROPN
ijpds-4231	92	6	drug	drug	PROPN
ijpds-4231	92	7	studies	study	NOUN
ijpds-4231	92	8	|	|	ADV
ijpds-4231	92	9	134	134	NUM
ijpds-4231	92	10	gc	gc	NOUN
ijpds-4231	92	11	)	)	PUNCT
ijpds-4231	92	12	.	.	PUNCT
ijpds-4231	93	1	in	in	ADP
ijpds-4231	93	2	an	an	DET
ijpds-4231	93	3	alternate	alternate	ADJ
ijpds-4231	93	4	pathway	pathway	NOUN
ijpds-4231	93	5	,	,	PUNCT
ijpds-4231	93	6	that	that	PRON
ijpds-4231	93	7	involved	involve	VERB
ijpds-4231	93	8	the	the	DET
ijpds-4231	93	9	condensation	condensation	NOUN
ijpds-4231	93	10	of	of	ADP
ijpds-4231	93	11	1	1	NUM
ijpds-4231	93	12	-	-	PUNCT
ijpds-4231	93	13	chloro-2,3	chloro-2,3	NOUN
ijpds-4231	93	14	-	-	ADJ
ijpds-4231	93	15	dihydro-1h	dihydro-1h	NOUN
ijpds-4231	93	16	-	-	PUNCT
ijpds-4231	93	17	indene	indene	NOUN
ijpds-4231	93	18	12	12	NUM
ijpds-4231	93	19	with	with	ADP
ijpds-4231	93	20	10	10	NUM
ijpds-4231	93	21	in	in	ADP
ijpds-4231	93	22	acetonitrile	acetonitrile	NOUN
ijpds-4231	93	23	to	to	PART
ijpds-4231	93	24	isolate	isolate	VERB
ijpds-4231	93	25	racemic	racemic	NOUN
ijpds-4231	93	26	11	11	NUM
ijpds-4231	93	27	with	with	ADP
ijpds-4231	93	28	a	a	DET
ijpds-4231	93	29	boiling	boiling	NOUN
ijpds-4231	93	30	point	point	NOUN
ijpds-4231	93	31	of	of	ADP
ijpds-4231	93	32	125	125	NUM
ijpds-4231	93	33	-	-	PUNCT
ijpds-4231	93	34	135oc	135oc	NOUN
ijpds-4231	93	35	(	(	PUNCT
ijpds-4231	93	36	yield	yield	NOUN
ijpds-4231	93	37	:	:	PUNCT
ijpds-4231	93	38	64	64	NUM
ijpds-4231	93	39	%	%	NOUN
ijpds-4231	93	40	)	)	PUNCT
ijpds-4231	94	1	[	[	X
ijpds-4231	94	2	12	12	NUM
ijpds-4231	94	3	]	]	PUNCT
ijpds-4231	94	4	.	.	PUNCT
ijpds-4231	95	1	it	it	PRON
ijpds-4231	95	2	was	be	AUX
ijpds-4231	95	3	resolved	resolve	VERB
ijpds-4231	95	4	under	under	ADP
ijpds-4231	95	5	the	the	DET
ijpds-4231	95	6	influence	influence	NOUN
ijpds-4231	95	7	of	of	ADP
ijpds-4231	95	8	r	r	NOUN
ijpds-4231	95	9	,	,	PUNCT
ijpds-4231	95	10	r	r	NOUN
ijpds-4231	95	11	-	-	PUNCT
ijpds-4231	95	12	tartaric	tartaric	ADJ
ijpds-4231	95	13	acid	acid	NOUN
ijpds-4231	95	14	in	in	ADP
ijpds-4231	95	15	water	water	NOUN
ijpds-4231	95	16	to	to	PART
ijpds-4231	95	17	isolate	isolate	VERB
ijpds-4231	95	18	the	the	DET
ijpds-4231	95	19	crude	crude	ADJ
ijpds-4231	95	20	salt	salt	NOUN
ijpds-4231	95	21	.	.	PUNCT
ijpds-4231	96	1	it	it	PRON
ijpds-4231	96	2	was	be	AUX
ijpds-4231	96	3	recrystallized	recrystallize	VERB
ijpds-4231	96	4	from	from	ADP
ijpds-4231	96	5	water	water	NOUN
ijpds-4231	96	6	to	to	PART
ijpds-4231	96	7	isolate	isolate	VERB
ijpds-4231	96	8	the	the	DET
ijpds-4231	96	9	r	r	NOUN
ijpds-4231	96	10	,	,	PUNCT
ijpds-4231	96	11	rtartarate	rtartarate	VERB
ijpds-4231	96	12	salt	salt	NOUN
ijpds-4231	96	13	of	of	ADP
ijpds-4231	96	14	11	11	NUM
ijpds-4231	96	15	with	with	ADP
ijpds-4231	96	16	a	a	DET
ijpds-4231	96	17	melting	melting	NOUN
ijpds-4231	96	18	point	point	NOUN
ijpds-4231	96	19	of	of	ADP
ijpds-4231	96	20	135	135	NUM
ijpds-4231	96	21	-	-	PUNCT
ijpds-4231	96	22	144oc	144oc	NOUN
ijpds-4231	96	23	(	(	PUNCT
ijpds-4231	96	24	yield	yield	NOUN
ijpds-4231	96	25	:	:	PUNCT
ijpds-4231	96	26	32	32	NUM
ijpds-4231	96	27	%	%	NOUN
ijpds-4231	96	28	)	)	PUNCT
ijpds-4231	96	29	.	.	PUNCT
ijpds-4231	97	1	s	s	X
ijpds-4231	97	2	-	-	PUNCT
ijpds-4231	97	3	isomer	isomer	ADJ
ijpds-4231	97	4	of	of	ADP
ijpds-4231	97	5	11	11	NUM
ijpds-4231	97	6	was	be	AUX
ijpds-4231	97	7	recovered	recover	VERB
ijpds-4231	97	8	and	and	CCONJ
ijpds-4231	97	9	resolved	resolve	VERB
ijpds-4231	97	10	using	use	VERB
ijpds-4231	97	11	potassium	potassium	NOUN
ijpds-4231	97	12	-	-	PUNCT
ijpds-4231	97	13	t	t	NOUN
ijpds-4231	97	14	-	-	PUNCT
ijpds-4231	97	15	butoxide	butoxide	NOUN
ijpds-4231	97	16	in	in	ADP
ijpds-4231	97	17	dimethylsulfoxide	dimethylsulfoxide	ADV
ijpds-4231	97	18	to	to	PART
ijpds-4231	97	19	isolate	isolate	VERB
ijpds-4231	97	20	11	11	NUM
ijpds-4231	97	21	(	(	PUNCT
ijpds-4231	97	22	yield	yield	NOUN
ijpds-4231	97	23	:	:	PUNCT
ijpds-4231	97	24	80	80	NUM
ijpds-4231	97	25	%	%	NOUN
ijpds-4231	97	26	)	)	PUNCT
ijpds-4231	97	27	.	.	PUNCT
ijpds-4231	98	1	r	r	X
ijpds-4231	98	2	,	,	PUNCT
ijpds-4231	98	3	r	r	NOUN
ijpds-4231	98	4	-	-	PUNCT
ijpds-4231	98	5	tartarate	tartarate	ADJ
ijpds-4231	98	6	salt	salt	NOUN
ijpds-4231	98	7	of	of	ADP
ijpds-4231	98	8	11	11	NUM
ijpds-4231	98	9	was	be	AUX
ijpds-4231	98	10	reduced	reduce	VERB
ijpds-4231	98	11	using	use	VERB
ijpds-4231	98	12	palladium	palladium	NOUN
ijpds-4231	98	13	-	-	PUNCT
ijpds-4231	98	14	carbon	carbon	NOUN
ijpds-4231	98	15	in	in	ADP
ijpds-4231	98	16	water	water	NOUN
ijpds-4231	98	17	to	to	PART
ijpds-4231	98	18	isolate	isolate	VERB
ijpds-4231	98	19	r	r	NOUN
ijpds-4231	98	20	-	-	PUNCT
ijpds-4231	98	21	isomer	isomer	NOUN
ijpds-4231	98	22	of	of	ADP
ijpds-4231	98	23	2	2	NUM
ijpds-4231	98	24	with	with	ADP
ijpds-4231	98	25	a	a	DET
ijpds-4231	98	26	boiling	boiling	NOUN
ijpds-4231	98	27	point	point	NOUN
ijpds-4231	98	28	of	of	ADP
ijpds-4231	98	29	130	130	NUM
ijpds-4231	98	30	-	-	PUNCT
ijpds-4231	98	31	140oc	140oc	NOUN
ijpds-4231	98	32	(	(	PUNCT
ijpds-4231	98	33	yield	yield	NOUN
ijpds-4231	98	34	:	:	PUNCT
ijpds-4231	98	35	72	72	NUM
ijpds-4231	98	36	%	%	NOUN
ijpds-4231	98	37	)	)	PUNCT
ijpds-4231	98	38	.	.	PUNCT
ijpds-4231	99	1	this	this	PRON
ijpds-4231	99	2	can	can	AUX
ijpds-4231	99	3	also	also	ADV
ijpds-4231	99	4	be	be	AUX
ijpds-4231	99	5	treated	treat	VERB
ijpds-4231	99	6	with	with	ADP
ijpds-4231	99	7	3	3	NUM
ijpds-4231	99	8	or	or	CCONJ
ijpds-4231	99	9	7	7	NUM
ijpds-4231	99	10	to	to	PART
ijpds-4231	99	11	isolate	isolate	VERB
ijpds-4231	99	12	rasagiline	rasagiline	NOUN
ijpds-4231	99	13	base	base	NOUN
ijpds-4231	99	14	as	as	ADP
ijpds-4231	99	15	per	per	ADP
ijpds-4231	99	16	the	the	DET
ijpds-4231	99	17	past	past	ADJ
ijpds-4231	99	18	disclosures	disclosure	NOUN
ijpds-4231	99	19	[	[	X
ijpds-4231	99	20	12	12	NUM
ijpds-4231	99	21	]	]	PUNCT
ijpds-4231	99	22	.	.	PUNCT
ijpds-4231	100	1	lee	lee	PROPN
ijpds-4231	100	2	tb	tb	PROPN
ijpds-4231	100	3	,	,	PUNCT
ijpds-4231	100	4	et	et	PROPN
ijpds-4231	100	5	al	al	PROPN
ijpds-4231	100	6	.	.	PROPN
ijpds-4231	100	7	,	,	PUNCT
ijpds-4231	100	8	in	in	ADP
ijpds-4231	100	9	2006	2006	NUM
ijpds-4231	100	10	,	,	PUNCT
ijpds-4231	100	11	had	have	AUX
ijpds-4231	100	12	demonstrated	demonstrate	VERB
ijpds-4231	100	13	the	the	DET
ijpds-4231	100	14	condensation	condensation	NOUN
ijpds-4231	100	15	of	of	ADP
ijpds-4231	100	16	s-1	s-1	NOUN
ijpds-4231	100	17	-	-	PUNCT
ijpds-4231	100	18	indanol	indanol	NOUN
ijpds-4231	100	19	13	13	NUM
ijpds-4231	100	20	with	with	ADP
ijpds-4231	100	21	6	6	NUM
ijpds-4231	100	22	in	in	ADP
ijpds-4231	100	23	the	the	DET
ijpds-4231	100	24	presence	presence	NOUN
ijpds-4231	100	25	of	of	ADP
ijpds-4231	100	26	methanesulfonyl	methanesulfonyl	NOUN
ijpds-4231	100	27	anhydride	anhydride	NOUN
ijpds-4231	100	28	14	14	NUM
ijpds-4231	100	29	and	and	CCONJ
ijpds-4231	100	30	triethylamine	triethylamine	NOUN
ijpds-4231	100	31	in	in	ADP
ijpds-4231	100	32	dichloromethane	dichloromethane	NOUN
ijpds-4231	100	33	to	to	PART
ijpds-4231	100	34	isolate	isolate	VERB
ijpds-4231	100	35	the	the	DET
ijpds-4231	100	36	r	r	NOUN
ijpds-4231	100	37	-	-	PUNCT
ijpds-4231	100	38	rasagiline	rasagiline	NOUN
ijpds-4231	100	39	base	base	NOUN
ijpds-4231	100	40	(	(	PUNCT
ijpds-4231	100	41	yield	yield	NOUN
ijpds-4231	100	42	:	:	PUNCT
ijpds-4231	100	43	68	68	NUM
ijpds-4231	100	44	%	%	NOUN
ijpds-4231	100	45	,	,	PUNCT
ijpds-4231	100	46	as	as	ADP
ijpds-4231	100	47	brown	brown	ADJ
ijpds-4231	100	48	liquid	liquid	NOUN
ijpds-4231	100	49	)	)	PUNCT
ijpds-4231	101	1	[	[	X
ijpds-4231	101	2	13	13	NUM
ijpds-4231	101	3	]	]	PUNCT
ijpds-4231	101	4	.	.	PUNCT
ijpds-4231	102	1	anton	anton	PROPN
ijpds-4231	102	2	f	f	PROPN
ijpds-4231	102	3	,	,	PUNCT
ijpds-4231	102	4	et	et	PROPN
ijpds-4231	102	5	al	al	PROPN
ijpds-4231	102	6	.	.	PROPN
ijpds-4231	102	7	,	,	PUNCT
ijpds-4231	102	8	in	in	ADP
ijpds-4231	102	9	2007	2007	NUM
ijpds-4231	102	10	&	&	CCONJ
ijpds-4231	102	11	2009	2009	NUM
ijpds-4231	102	12	,	,	PUNCT
ijpds-4231	102	13	had	have	AUX
ijpds-4231	102	14	illustrated	illustrate	VERB
ijpds-4231	102	15	the	the	DET
ijpds-4231	102	16	reaction	reaction	NOUN
ijpds-4231	102	17	of	of	ADP
ijpds-4231	102	18	2	2	NUM
ijpds-4231	102	19	with	with	ADP
ijpds-4231	102	20	8	8	NUM
ijpds-4231	102	21	in	in	ADP
ijpds-4231	102	22	the	the	DET
ijpds-4231	102	23	presence	presence	NOUN
ijpds-4231	102	24	of	of	ADP
ijpds-4231	102	25	aqueous	aqueous	ADJ
ijpds-4231	102	26	sodium	sodium	NOUN
ijpds-4231	102	27	hydroxide	hydroxide	NOUN
ijpds-4231	102	28	in	in	ADP
ijpds-4231	102	29	toluene	toluene	NOUN
ijpds-4231	102	30	to	to	PART
ijpds-4231	102	31	isolate	isolate	VERB
ijpds-4231	102	32	rasagiline	rasagiline	NOUN
ijpds-4231	102	33	base	base	NOUN
ijpds-4231	102	34	through	through	ADP
ijpds-4231	102	35	the	the	DET
ijpds-4231	102	36	extraction	extraction	NOUN
ijpds-4231	102	37	method	method	NOUN
ijpds-4231	102	38	(	(	PUNCT
ijpds-4231	102	39	yield	yield	NOUN
ijpds-4231	102	40	:	:	PUNCT
ijpds-4231	102	41	66.71	66.71	NUM
ijpds-4231	102	42	%	%	NOUN
ijpds-4231	102	43	,	,	PUNCT
ijpds-4231	102	44	as	as	ADP
ijpds-4231	102	45	brown	brown	ADJ
ijpds-4231	102	46	oil	oil	NOUN
ijpds-4231	102	47	)	)	PUNCT
ijpds-4231	102	48	.	.	PUNCT
ijpds-4231	103	1	it	it	PRON
ijpds-4231	103	2	was	be	AUX
ijpds-4231	103	3	treated	treat	VERB
ijpds-4231	103	4	with	with	ADP
ijpds-4231	103	5	l	l	ADJ
ijpds-4231	103	6	-	-	ADJ
ijpds-4231	103	7	tartaric	tartaric	ADJ
ijpds-4231	103	8	acid	acid	NOUN
ijpds-4231	103	9	in	in	ADP
ijpds-4231	103	10	isopropyl	isopropyl	NOUN
ijpds-4231	103	11	alcohol	alcohol	NOUN
ijpds-4231	103	12	to	to	PART
ijpds-4231	103	13	isolate	isolate	VERB
ijpds-4231	103	14	r	r	NOUN
ijpds-4231	103	15	-	-	PUNCT
ijpds-4231	103	16	rasagiline	rasagiline	NOUN
ijpds-4231	103	17	tartarate	tartarate	NOUN
ijpds-4231	103	18	with	with	ADP
ijpds-4231	103	19	a	a	DET
ijpds-4231	103	20	melting	melting	NOUN
ijpds-4231	103	21	point	point	NOUN
ijpds-4231	103	22	of	of	ADP
ijpds-4231	103	23	176.3176.8oc	176.3176.8oc	NUM
ijpds-4231	103	24	(	(	PUNCT
ijpds-4231	103	25	yield	yield	NOUN
ijpds-4231	103	26	:	:	PUNCT
ijpds-4231	103	27	28.8	28.8	NUM
ijpds-4231	103	28	%	%	NOUN
ijpds-4231	103	29	,	,	PUNCT
ijpds-4231	103	30	s	s	NOUN
ijpds-4231	103	31	-	-	PUNCT
ijpds-4231	103	32	isomer	isomer	ADJ
ijpds-4231	103	33	:	:	PUNCT
ijpds-4231	103	34	approx	approx	PROPN
ijpds-4231	103	35	.	.	PUNCT
ijpds-4231	104	1	4	4	NUM
ijpds-4231	104	2	%	%	NOUN
ijpds-4231	104	3	)	)	PUNCT
ijpds-4231	104	4	.	.	PUNCT
ijpds-4231	105	1	with	with	ADP
ijpds-4231	105	2	the	the	DET
ijpds-4231	105	3	use	use	NOUN
ijpds-4231	105	4	of	of	ADP
ijpds-4231	105	5	similar	similar	ADJ
ijpds-4231	105	6	key	key	ADJ
ijpds-4231	105	7	reagents	reagent	NOUN
ijpds-4231	105	8	,	,	PUNCT
ijpds-4231	105	9	an	an	DET
ijpds-4231	105	10	additional	additional	ADJ
ijpds-4231	105	11	two	two	NUM
ijpds-4231	105	12	illustrations	illustration	NOUN
ijpds-4231	105	13	were	be	AUX
ijpds-4231	105	14	reported	report	VERB
ijpds-4231	105	15	.	.	PUNCT
ijpds-4231	106	1	they	they	PRON
ijpds-4231	106	2	are	be	AUX
ijpds-4231	106	3	,	,	PUNCT
ijpds-4231	106	4	direct	direct	ADJ
ijpds-4231	106	5	and	and	CCONJ
ijpds-4231	106	6	prolonged	prolonged	ADJ
ijpds-4231	106	7	precipitation	precipitation	NOUN
ijpds-4231	106	8	methods	method	NOUN
ijpds-4231	106	9	to	to	PART
ijpds-4231	106	10	isolate	isolate	VERB
ijpds-4231	106	11	rasagiline	rasagiline	NOUN
ijpds-4231	106	12	tartarate	tartarate	NOUN
ijpds-4231	106	13	with	with	ADP
ijpds-4231	106	14	the	the	DET
ijpds-4231	106	15	melting	melting	NOUN
ijpds-4231	106	16	points	point	NOUN
ijpds-4231	106	17	in	in	ADP
ijpds-4231	106	18	the	the	DET
ijpds-4231	106	19	range	range	NOUN
ijpds-4231	106	20	of	of	ADP
ijpds-4231	106	21	160.8	160.8	NUM
ijpds-4231	106	22	-	-	SYM
ijpds-4231	106	23	163.2oc	163.2oc	NUM
ijpds-4231	106	24	having	have	VERB
ijpds-4231	106	25	the	the	DET
ijpds-4231	106	26	s	s	NOUN
ijpds-4231	106	27	-	-	PUNCT
ijpds-4231	106	28	isomer	isomer	ADJ
ijpds-4231	106	29	content	content	NOUN
ijpds-4231	106	30	to	to	ADP
ijpds-4231	106	31	about	about	ADV
ijpds-4231	106	32	4	4	NUM
ijpds-4231	106	33	-	-	SYM
ijpds-4231	106	34	16	16	NUM
ijpds-4231	106	35	%	%	NOUN
ijpds-4231	106	36	.	.	PUNCT
ijpds-4231	107	1	the	the	DET
ijpds-4231	107	2	work	work	NOUN
ijpds-4231	107	3	had	have	AUX
ijpds-4231	107	4	even	even	ADV
ijpds-4231	107	5	disclosed	disclose	VERB
ijpds-4231	107	6	a	a	DET
ijpds-4231	107	7	few	few	ADJ
ijpds-4231	107	8	other	other	ADJ
ijpds-4231	107	9	precipitation	precipitation	NOUN
ijpds-4231	107	10	methods	method	NOUN
ijpds-4231	107	11	such	such	ADJ
ijpds-4231	107	12	as	as	ADP
ijpds-4231	107	13	,	,	PUNCT
ijpds-4231	107	14	rasagiline	rasagiline	ADJ
ijpds-4231	107	15	sulfate	sulfate	NOUN
ijpds-4231	107	16	isolation	isolation	NOUN
ijpds-4231	107	17	,	,	PUNCT
ijpds-4231	107	18	recrystallization	recrystallization	NOUN
ijpds-4231	107	19	of	of	ADP
ijpds-4231	107	20	rasagiline	rasagiline	NOUN
ijpds-4231	107	21	salts	salt	NOUN
ijpds-4231	107	22	from	from	ADP
ijpds-4231	107	23	solvents	solvent	NOUN
ijpds-4231	107	24	/	/	SYM
ijpds-4231	107	25	water	water	NOUN
ijpds-4231	107	26	and	and	CCONJ
ijpds-4231	107	27	salt	salt	NOUN
ijpds-4231	107	28	inter	inter	NOUN
ijpds-4231	107	29	-	-	NOUN
ijpds-4231	107	30	conversions	conversion	NOUN
ijpds-4231	107	31	etc	etc	X
ijpds-4231	108	1	[	[	X
ijpds-4231	108	2	14	14	NUM
ijpds-4231	108	3	,	,	PUNCT
ijpds-4231	108	4	15	15	NUM
ijpds-4231	108	5	]	]	PUNCT
ijpds-4231	108	6	.	.	PUNCT
ijpds-4231	109	1	n	n	PRON
ijpds-4231	110	1	oh	oh	NUM
ijpds-4231	110	2	15	15	NUM
ijpds-4231	110	3	n16	n16	NOUN
ijpds-4231	110	4	nh	nh	PROPN
ijpds-4231	110	5	nh17	nh17	PROPN
ijpds-4231	110	6	18	18	NUM
ijpds-4231	110	7	nh	nh	NOUN
ijpds-4231	110	8	o	o	PROPN
ijpds-4231	110	9	19	19	NUM
ijpds-4231	110	10	luo	luo	PROPN
ijpds-4231	110	11	jh	jh	PROPN
ijpds-4231	110	12	.	.	PROPN
ijpds-4231	110	13	,	,	PUNCT
ijpds-4231	110	14	in	in	ADP
ijpds-4231	110	15	2007	2007	NUM
ijpds-4231	110	16	,	,	PUNCT
ijpds-4231	110	17	had	have	AUX
ijpds-4231	110	18	reported	report	VERB
ijpds-4231	110	19	the	the	DET
ijpds-4231	110	20	reduction	reduction	NOUN
ijpds-4231	110	21	of	of	ADP
ijpds-4231	110	22	2,3dihydro-1h-1	2,3dihydro-1h-1	NUM
ijpds-4231	110	23	-	-	PUNCT
ijpds-4231	110	24	indanone	indanone	NOUN
ijpds-4231	110	25	oxime	oxime	NOUN
ijpds-4231	110	26	15	15	NUM
ijpds-4231	110	27	using	use	VERB
ijpds-4231	110	28	alumino	alumino	NOUN
ijpds-4231	110	29	-	-	PUNCT
ijpds-4231	110	30	nickel	nickel	NOUN
ijpds-4231	110	31	catalyst	catalyst	NOUN
ijpds-4231	110	32	in	in	ADP
ijpds-4231	110	33	the	the	DET
ijpds-4231	110	34	presence	presence	NOUN
ijpds-4231	110	35	of	of	ADP
ijpds-4231	110	36	sodium	sodium	NOUN
ijpds-4231	110	37	hydroxide	hydroxide	NOUN
ijpds-4231	110	38	solution	solution	NOUN
ijpds-4231	110	39	and	and	CCONJ
ijpds-4231	110	40	ethyl	ethyl	PROPN
ijpds-4231	110	41	alcohol	alcohol	PROPN
ijpds-4231	110	42	to	to	PART
ijpds-4231	110	43	isolate	isolate	VERB
ijpds-4231	110	44	2	2	NUM
ijpds-4231	110	45	(	(	PUNCT
ijpds-4231	110	46	yield	yield	NOUN
ijpds-4231	110	47	:	:	PUNCT
ijpds-4231	110	48	80.11	80.11	NUM
ijpds-4231	110	49	%	%	NOUN
ijpds-4231	110	50	,	,	PUNCT
ijpds-4231	110	51	as	as	ADP
ijpds-4231	110	52	oily	oily	ADJ
ijpds-4231	110	53	mass	mass	NOUN
ijpds-4231	110	54	)	)	PUNCT
ijpds-4231	110	55	.	.	PUNCT
ijpds-4231	111	1	in	in	ADP
ijpds-4231	111	2	another	another	DET
ijpds-4231	111	3	experiment	experiment	NOUN
ijpds-4231	111	4	,	,	PUNCT
ijpds-4231	111	5	9	9	NUM
ijpds-4231	111	6	was	be	AUX
ijpds-4231	111	7	treated	treat	VERB
ijpds-4231	111	8	with	with	ADP
ijpds-4231	111	9	oxammonium	oxammonium	NOUN
ijpds-4231	111	10	hydrochloride	hydrochloride	NOUN
ijpds-4231	111	11	in	in	ADP
ijpds-4231	111	12	the	the	DET
ijpds-4231	111	13	presence	presence	NOUN
ijpds-4231	111	14	of	of	ADP
ijpds-4231	111	15	sodium	sodium	NOUN
ijpds-4231	111	16	hydroxide	hydroxide	NOUN
ijpds-4231	111	17	solution	solution	NOUN
ijpds-4231	111	18	and	and	CCONJ
ijpds-4231	111	19	ethyl	ethyl	PROPN
ijpds-4231	111	20	alcohol	alcohol	PROPN
ijpds-4231	111	21	.	.	PUNCT
ijpds-4231	112	1	later	later	ADV
ijpds-4231	112	2	to	to	ADP
ijpds-4231	112	3	the	the	DET
ijpds-4231	112	4	reaction	reaction	NOUN
ijpds-4231	112	5	mixture	mixture	NOUN
ijpds-4231	112	6	added	add	VERB
ijpds-4231	112	7	alumino	alumino	NOUN
ijpds-4231	112	8	-	-	PUNCT
ijpds-4231	112	9	nickel	nickel	NOUN
ijpds-4231	112	10	catalyst	catalyst	NOUN
ijpds-4231	112	11	and	and	CCONJ
ijpds-4231	112	12	worked	work	VERB
ijpds-4231	112	13	up	up	ADP
ijpds-4231	112	14	to	to	PART
ijpds-4231	112	15	isolate	isolate	VERB
ijpds-4231	112	16	the	the	DET
ijpds-4231	112	17	hydrochloride	hydrochloride	NOUN
ijpds-4231	112	18	of	of	ADP
ijpds-4231	112	19	2	2	NUM
ijpds-4231	112	20	with	with	ADP
ijpds-4231	112	21	a	a	DET
ijpds-4231	112	22	melting	melting	NOUN
ijpds-4231	112	23	point	point	NOUN
ijpds-4231	112	24	of	of	ADP
ijpds-4231	112	25	208.4	208.4	NUM
ijpds-4231	112	26	-	-	SYM
ijpds-4231	112	27	209.5oc	209.5oc	NUM
ijpds-4231	112	28	(	(	PUNCT
ijpds-4231	112	29	yield	yield	NOUN
ijpds-4231	112	30	:	:	PUNCT
ijpds-4231	112	31	76.68	76.68	NUM
ijpds-4231	112	32	%	%	NOUN
ijpds-4231	112	33	,	,	PUNCT
ijpds-4231	112	34	purity	purity	NOUN
ijpds-4231	112	35	:	:	PUNCT
ijpds-4231	112	36	98.64	98.64	NUM
ijpds-4231	112	37	%	%	NOUN
ijpds-4231	112	38	by	by	ADP
ijpds-4231	112	39	hplc	hplc	NOUN
ijpds-4231	112	40	,	,	PUNCT
ijpds-4231	112	41	as	as	ADP
ijpds-4231	112	42	white	white	ADJ
ijpds-4231	112	43	crystals	crystal	NOUN
ijpds-4231	112	44	)	)	PUNCT
ijpds-4231	112	45	.	.	PUNCT
ijpds-4231	113	1	it	it	PRON
ijpds-4231	113	2	was	be	AUX
ijpds-4231	113	3	treated	treat	VERB
ijpds-4231	113	4	with	with	ADP
ijpds-4231	113	5	8	8	NUM
ijpds-4231	113	6	in	in	ADP
ijpds-4231	113	7	the	the	DET
ijpds-4231	113	8	presence	presence	NOUN
ijpds-4231	113	9	of	of	ADP
ijpds-4231	113	10	sodium	sodium	NOUN
ijpds-4231	113	11	hydroxide	hydroxide	NOUN
ijpds-4231	113	12	solution	solution	NOUN
ijpds-4231	113	13	and	and	CCONJ
ijpds-4231	113	14	toluene	toluene	NOUN
ijpds-4231	113	15	to	to	PART
ijpds-4231	113	16	isolate	isolate	VERB
ijpds-4231	113	17	the	the	DET
ijpds-4231	113	18	racemic	racemic	ADJ
ijpds-4231	113	19	rasagiline	rasagiline	NOUN
ijpds-4231	113	20	base	base	NOUN
ijpds-4231	113	21	(	(	PUNCT
ijpds-4231	113	22	yield	yield	NOUN
ijpds-4231	113	23	:	:	PUNCT
ijpds-4231	113	24	79.07	79.07	NUM
ijpds-4231	113	25	%	%	NOUN
ijpds-4231	113	26	,	,	PUNCT
ijpds-4231	113	27	purity	purity	NOUN
ijpds-4231	113	28	:	:	PUNCT
ijpds-4231	113	29	93.08	93.08	NUM
ijpds-4231	113	30	%	%	NOUN
ijpds-4231	113	31	by	by	ADP
ijpds-4231	113	32	hplc	hplc	NOUN
ijpds-4231	113	33	,	,	PUNCT
ijpds-4231	113	34	as	as	ADP
ijpds-4231	113	35	brown	brown	ADJ
ijpds-4231	113	36	oily	oily	ADJ
ijpds-4231	113	37	mass	mass	NOUN
ijpds-4231	113	38	)	)	PUNCT
ijpds-4231	113	39	.	.	PUNCT
ijpds-4231	114	1	in	in	ADP
ijpds-4231	114	2	another	another	DET
ijpds-4231	114	3	instance	instance	NOUN
ijpds-4231	114	4	,	,	PUNCT
ijpds-4231	114	5	15	15	NUM
ijpds-4231	114	6	was	be	AUX
ijpds-4231	114	7	dissolved	dissolve	VERB
ijpds-4231	114	8	in	in	ADP
ijpds-4231	114	9	ethyl	ethyl	PROPN
ijpds-4231	114	10	alcohol	alcohol	NOUN
ijpds-4231	114	11	and	and	CCONJ
ijpds-4231	114	12	treated	treat	VERB
ijpds-4231	114	13	with	with	ADP
ijpds-4231	114	14	sodium	sodium	NOUN
ijpds-4231	114	15	hydroxide	hydroxide	NOUN
ijpds-4231	114	16	solution	solution	NOUN
ijpds-4231	114	17	.	.	PUNCT
ijpds-4231	115	1	to	to	ADP
ijpds-4231	115	2	the	the	DET
ijpds-4231	115	3	reaction	reaction	NOUN
ijpds-4231	115	4	mixture	mixture	NOUN
ijpds-4231	115	5	added	add	VERB
ijpds-4231	115	6	alumino	alumino	NOUN
ijpds-4231	115	7	-	-	PUNCT
ijpds-4231	115	8	nickel	nickel	NOUN
ijpds-4231	115	9	catalyst	catalyst	NOUN
ijpds-4231	115	10	for	for	ADP
ijpds-4231	115	11	the	the	DET
ijpds-4231	115	12	reduction	reduction	NOUN
ijpds-4231	115	13	and	and	CCONJ
ijpds-4231	115	14	later	later	ADV
ijpds-4231	115	15	added	add	VERB
ijpds-4231	115	16	8	8	NUM
ijpds-4231	115	17	to	to	PART
ijpds-4231	115	18	isolate	isolate	VERB
ijpds-4231	115	19	the	the	DET
ijpds-4231	115	20	racemic	racemic	ADJ
ijpds-4231	115	21	rasagiline	rasagiline	NOUN
ijpds-4231	115	22	base	base	NOUN
ijpds-4231	115	23	(	(	PUNCT
ijpds-4231	115	24	yield	yield	NOUN
ijpds-4231	115	25	:	:	PUNCT
ijpds-4231	115	26	64.89	64.89	NUM
ijpds-4231	115	27	%	%	NOUN
ijpds-4231	115	28	,	,	PUNCT
ijpds-4231	115	29	purity	purity	NOUN
ijpds-4231	115	30	:	:	PUNCT
ijpds-4231	115	31	90.45	90.45	NUM
ijpds-4231	115	32	%	%	NOUN
ijpds-4231	115	33	by	by	ADP
ijpds-4231	115	34	hplc	hplc	NOUN
ijpds-4231	115	35	,	,	PUNCT
ijpds-4231	115	36	as	as	ADP
ijpds-4231	115	37	brown	brown	ADJ
ijpds-4231	115	38	oily	oily	ADJ
ijpds-4231	115	39	mass	mass	NOUN
ijpds-4231	115	40	)	)	PUNCT
ijpds-4231	115	41	.	.	PUNCT
ijpds-4231	116	1	in	in	ADP
ijpds-4231	116	2	another	another	DET
ijpds-4231	116	3	example	example	NOUN
ijpds-4231	116	4	,	,	PUNCT
ijpds-4231	116	5	9	9	NUM
ijpds-4231	116	6	was	be	AUX
ijpds-4231	116	7	treated	treat	VERB
ijpds-4231	116	8	with	with	ADP
ijpds-4231	116	9	oxammonium	oxammonium	NOUN
ijpds-4231	116	10	hydrochloride	hydrochloride	NOUN
ijpds-4231	116	11	in	in	ADP
ijpds-4231	116	12	the	the	DET
ijpds-4231	116	13	presence	presence	NOUN
ijpds-4231	116	14	of	of	ADP
ijpds-4231	116	15	sodium	sodium	NOUN
ijpds-4231	116	16	hydroxide	hydroxide	NOUN
ijpds-4231	116	17	solution	solution	NOUN
ijpds-4231	116	18	and	and	CCONJ
ijpds-4231	116	19	ethyl	ethyl	PROPN
ijpds-4231	116	20	alcohol	alcohol	PROPN
ijpds-4231	116	21	.	.	PUNCT
ijpds-4231	117	1	to	to	ADP
ijpds-4231	117	2	it	it	PRON
ijpds-4231	117	3	,	,	PUNCT
ijpds-4231	117	4	added	add	VERB
ijpds-4231	117	5	alumino	alumino	NOUN
ijpds-4231	117	6	-	-	PUNCT
ijpds-4231	117	7	nickel	nickel	NOUN
ijpds-4231	117	8	catalyst	catalyst	NOUN
ijpds-4231	117	9	for	for	ADP
ijpds-4231	117	10	the	the	DET
ijpds-4231	117	11	reduction	reduction	NOUN
ijpds-4231	117	12	and	and	CCONJ
ijpds-4231	117	13	then	then	ADV
ijpds-4231	117	14	added	add	VERB
ijpds-4231	117	15	8	8	NUM
ijpds-4231	117	16	to	to	PART
ijpds-4231	117	17	isolate	isolate	VERB
ijpds-4231	117	18	racemic	racemic	ADJ
ijpds-4231	117	19	rasagiline	rasagiline	NOUN
ijpds-4231	117	20	base	base	NOUN
ijpds-4231	117	21	(	(	PUNCT
ijpds-4231	117	22	yield	yield	NOUN
ijpds-4231	117	23	:	:	PUNCT
ijpds-4231	117	24	62.3	62.3	NUM
ijpds-4231	117	25	%	%	NOUN
ijpds-4231	117	26	,	,	PUNCT
ijpds-4231	117	27	purity	purity	NOUN
ijpds-4231	117	28	:	:	PUNCT
ijpds-4231	117	29	92.03	92.03	NUM
ijpds-4231	117	30	%	%	NOUN
ijpds-4231	117	31	by	by	ADP
ijpds-4231	117	32	hplc	hplc	NOUN
ijpds-4231	117	33	,	,	PUNCT
ijpds-4231	117	34	as	as	ADP
ijpds-4231	117	35	pale	pale	ADJ
ijpds-4231	117	36	brown	brown	ADJ
ijpds-4231	117	37	oily	oily	ADJ
ijpds-4231	117	38	mass	mass	NOUN
ijpds-4231	117	39	)	)	PUNCT
ijpds-4231	117	40	.	.	PUNCT
ijpds-4231	118	1	in	in	ADP
ijpds-4231	118	2	a	a	DET
ijpds-4231	118	3	few	few	ADJ
ijpds-4231	118	4	separate	separate	ADJ
ijpds-4231	118	5	experiments	experiment	NOUN
ijpds-4231	118	6	,	,	PUNCT
ijpds-4231	118	7	racemic	racemic	ADJ
ijpds-4231	118	8	rasagiline	rasagiline	NOUN
ijpds-4231	118	9	base	base	NOUN
ijpds-4231	118	10	was	be	AUX
ijpds-4231	118	11	treated	treat	VERB
ijpds-4231	118	12	with	with	ADP
ijpds-4231	118	13	l	l	NOUN
ijpds-4231	118	14	-	-	NOUN
ijpds-4231	118	15	tartarate	tartarate	NOUN
ijpds-4231	118	16	in	in	ADP
ijpds-4231	118	17	isopropyl	isopropyl	NOUN
ijpds-4231	118	18	alcohol	alcohol	NOUN
ijpds-4231	118	19	to	to	PART
ijpds-4231	118	20	get	get	VERB
ijpds-4231	118	21	the	the	DET
ijpds-4231	118	22	crude	crude	NOUN
ijpds-4231	118	23	solid	solid	NOUN
ijpds-4231	118	24	,	,	PUNCT
ijpds-4231	118	25	which	which	PRON
ijpds-4231	118	26	was	be	AUX
ijpds-4231	118	27	recrystallized	recrystallize	VERB
ijpds-4231	118	28	in	in	ADP
ijpds-4231	118	29	isopropyl	isopropyl	NOUN
ijpds-4231	118	30	alcohol	alcohol	NOUN
ijpds-4231	118	31	to	to	PART
ijpds-4231	118	32	isolate	isolate	VERB
ijpds-4231	118	33	r	r	NOUN
ijpds-4231	118	34	-	-	PUNCT
ijpds-4231	118	35	di-(rasagiline	di-(rasagiline	NOUN
ijpds-4231	118	36	)	)	PUNCT
ijpds-4231	118	37	tartarate	tartarate	NOUN
ijpds-4231	118	38	with	with	ADP
ijpds-4231	118	39	the	the	DET
ijpds-4231	118	40	melting	melting	NOUN
ijpds-4231	118	41	points	point	NOUN
ijpds-4231	118	42	in	in	ADP
ijpds-4231	118	43	the	the	DET
ijpds-4231	118	44	range	range	NOUN
ijpds-4231	118	45	of	of	ADP
ijpds-4231	118	46	174.2	174.2	NUM
ijpds-4231	118	47	-	-	PUNCT
ijpds-4231	118	48	177oc	177oc	NOUN
ijpds-4231	118	49	(	(	PUNCT
ijpds-4231	118	50	yield	yield	NOUN
ijpds-4231	118	51	range	range	NOUN
ijpds-4231	118	52	:	:	PUNCT
ijpds-4231	118	53	20	20	NUM
ijpds-4231	118	54	-	-	SYM
ijpds-4231	118	55	26	26	NUM
ijpds-4231	118	56	%	%	NOUN
ijpds-4231	118	57	,	,	PUNCT
ijpds-4231	118	58	purity	purity	NOUN
ijpds-4231	118	59	range	range	NOUN
ijpds-4231	118	60	:	:	PUNCT
ijpds-4231	118	61	97.46	97.46	NUM
ijpds-4231	118	62	-	-	SYM
ijpds-4231	118	63	98.54	98.54	NUM
ijpds-4231	118	64	%	%	NOUN
ijpds-4231	118	65	by	by	ADP
ijpds-4231	118	66	hplc	hplc	NOUN
ijpds-4231	118	67	,	,	PUNCT
ijpds-4231	118	68	as	as	ADP
ijpds-4231	118	69	white	white	ADJ
ijpds-4231	118	70	puffy	puffy	ADJ
ijpds-4231	118	71	crystals	crystal	NOUN
ijpds-4231	118	72	)	)	PUNCT
ijpds-4231	118	73	.	.	PUNCT
ijpds-4231	119	1	it	it	PRON
ijpds-4231	119	2	was	be	AUX
ijpds-4231	119	3	treated	treat	VERB
ijpds-4231	119	4	with	with	ADP
ijpds-4231	119	5	methanesulfonic	methanesulfonic	ADJ
ijpds-4231	119	6	acid	acid	NOUN
ijpds-4231	119	7	in	in	ADP
ijpds-4231	119	8	isopropyl	isopropyl	NOUN
ijpds-4231	119	9	alcohol	alcohol	NOUN
ijpds-4231	119	10	to	to	PART
ijpds-4231	119	11	isolate	isolate	VERB
ijpds-4231	119	12	1	1	NUM
ijpds-4231	119	13	with	with	ADP
ijpds-4231	119	14	a	a	DET
ijpds-4231	119	15	melting	melting	NOUN
ijpds-4231	119	16	point	point	NOUN
ijpds-4231	119	17	of	of	ADP
ijpds-4231	119	18	155155.8oc	155155.8oc	PROPN
ijpds-4231	119	19	(	(	PUNCT
ijpds-4231	119	20	purity	purity	NOUN
ijpds-4231	119	21	:	:	PUNCT
ijpds-4231	119	22	99.85	99.85	NUM
ijpds-4231	119	23	%	%	NOUN
ijpds-4231	119	24	by	by	ADP
ijpds-4231	119	25	hplc	hplc	NOUN
ijpds-4231	119	26	,	,	PUNCT
ijpds-4231	119	27	as	as	ADP
ijpds-4231	119	28	white	white	ADJ
ijpds-4231	119	29	crystals	crystal	NOUN
ijpds-4231	119	30	)	)	PUNCT
ijpds-4231	120	1	[	[	X
ijpds-4231	120	2	16	16	NUM
ijpds-4231	120	3	]	]	PUNCT
ijpds-4231	120	4	.	.	PUNCT
ijpds-4231	121	1	feng	feng	PROPN
ijpds-4231	121	2	q.	q.	PROPN
ijpds-4231	121	3	,	,	PUNCT
ijpds-4231	121	4	in	in	ADP
ijpds-4231	121	5	2007	2007	NUM
ijpds-4231	121	6	,	,	PUNCT
ijpds-4231	121	7	had	have	AUX
ijpds-4231	121	8	demonstrated	demonstrate	VERB
ijpds-4231	121	9	a	a	DET
ijpds-4231	121	10	simple	simple	ADJ
ijpds-4231	121	11	process	process	NOUN
ijpds-4231	121	12	to	to	PART
ijpds-4231	121	13	isolate	isolate	VERB
ijpds-4231	121	14	the	the	DET
ijpds-4231	121	15	reacemic	reacemic	ADJ
ijpds-4231	121	16	rasagiline	rasagiline	NOUN
ijpds-4231	121	17	base	base	NOUN
ijpds-4231	121	18	by	by	ADP
ijpds-4231	121	19	reacting	react	VERB
ijpds-4231	121	20	9	9	NUM
ijpds-4231	121	21	in	in	ADP
ijpds-4231	121	22	ethyl	ethyl	PROPN
ijpds-4231	121	23	alcohol	alcohol	NOUN
ijpds-4231	121	24	with	with	ADP
ijpds-4231	121	25	6	6	NUM
ijpds-4231	121	26	in	in	ADP
ijpds-4231	121	27	the	the	DET
ijpds-4231	121	28	presence	presence	NOUN
ijpds-4231	121	29	of	of	ADP
ijpds-4231	121	30	sodium	sodium	NOUN
ijpds-4231	121	31	borohydride	borohydride	NOUN
ijpds-4231	121	32	/	/	SYM
ijpds-4231	121	33	palladium	palladium	NOUN
ijpds-4231	121	34	-	-	PUNCT
ijpds-4231	121	35	carbon	carbon	NOUN
ijpds-4231	121	36	.	.	PUNCT
ijpds-4231	122	1	around	around	ADP
ijpds-4231	122	2	six	six	NUM
ijpds-4231	122	3	illustrations	illustration	NOUN
ijpds-4231	122	4	were	be	AUX
ijpds-4231	122	5	reported	report	VERB
ijpds-4231	122	6	with	with	ADP
ijpds-4231	122	7	a	a	DET
ijpds-4231	122	8	slight	slight	ADJ
ijpds-4231	122	9	modulated	modulate	VERB
ijpds-4231	122	10	reaction	reaction	NOUN
ijpds-4231	122	11	conditions	condition	NOUN
ijpds-4231	122	12	and	and	CCONJ
ijpds-4231	122	13	isolation	isolation	NOUN
ijpds-4231	122	14	procedures	procedure	NOUN
ijpds-4231	122	15	with	with	ADP
ijpds-4231	122	16	good	good	ADJ
ijpds-4231	122	17	yield	yield	NOUN
ijpds-4231	122	18	(	(	PUNCT
ijpds-4231	122	19	60.19	60.19	NUM
ijpds-4231	122	20	-	-	SYM
ijpds-4231	122	21	73.10	73.10	NUM
ijpds-4231	122	22	%	%	NOUN
ijpds-4231	122	23	)	)	PUNCT
ijpds-4231	123	1	[	[	X
ijpds-4231	123	2	17	17	NUM
ijpds-4231	123	3	]	]	PUNCT
ijpds-4231	123	4	.	.	PUNCT
ijpds-4231	124	1	n21	n21	PROPN
ijpds-4231	124	2	nh22	nh22	PROPN
ijpds-4231	124	3	nh2	nh2	PROPN
ijpds-4231	124	4	20	20	NUM
ijpds-4231	125	1	sanjay	sanjay	NOUN
ijpds-4231	125	2	s	s	PART
ijpds-4231	125	3	s	s	NOUN
ijpds-4231	125	4	patents	patent	NOUN
ijpds-4231	125	5	disclosed	disclose	VERB
ijpds-4231	125	6	synthetic	synthetic	ADJ
ijpds-4231	125	7	overview	overview	NOUN
ijpds-4231	125	8	of	of	ADP
ijpds-4231	125	9	rasagiline	rasagiline	ADJ
ijpds-4231	125	10	vol	vol	NOUN
ijpds-4231	125	11	2	2	NUM
ijpds-4231	125	12	|	|	ADV
ijpds-4231	125	13	issue	issue	VERB
ijpds-4231	125	14	4	4	NUM
ijpds-4231	125	15	|	|	ADV
ijpds-4231	125	16	oct	oct	PROPN
ijpds-4231	125	17	–	–	PUNCT
ijpds-4231	125	18	dec	dec	PROPN
ijpds-4231	125	19	2023	2023	NUM
ijpds-4231	125	20	indian	indian	PROPN
ijpds-4231	125	21	j	j	PROPN
ijpds-4231	125	22	pharm	pharm	PROPN
ijpds-4231	125	23	drug	drug	PROPN
ijpds-4231	125	24	studies	study	NOUN
ijpds-4231	125	25	|	|	ADV
ijpds-4231	125	26	135	135	NUM
ijpds-4231	125	27	zongxuan	zongxuan	PROPN
ijpds-4231	125	28	s	s	PROPN
ijpds-4231	125	29	,	,	PUNCT
ijpds-4231	125	30	et	et	PROPN
ijpds-4231	125	31	al	al	PROPN
ijpds-4231	125	32	.	.	PROPN
ijpds-4231	125	33	,	,	PUNCT
ijpds-4231	125	34	in	in	ADP
ijpds-4231	125	35	2008	2008	NUM
ijpds-4231	125	36	,	,	PUNCT
ijpds-4231	125	37	had	have	AUX
ijpds-4231	125	38	illustrated	illustrate	VERB
ijpds-4231	125	39	the	the	DET
ijpds-4231	125	40	condensation	condensation	NOUN
ijpds-4231	125	41	of	of	ADP
ijpds-4231	125	42	9	9	NUM
ijpds-4231	125	43	in	in	ADP
ijpds-4231	125	44	isopropyl	isopropyl	NOUN
ijpds-4231	125	45	acetate	acetate	NOUN
ijpds-4231	125	46	with	with	ADP
ijpds-4231	125	47	s-(-)-1phenylethylamine	s-(-)-1phenylethylamine	NOUN
ijpds-4231	125	48	20	20	NUM
ijpds-4231	125	49	in	in	ADP
ijpds-4231	125	50	the	the	DET
ijpds-4231	125	51	presence	presence	NOUN
ijpds-4231	125	52	of	of	ADP
ijpds-4231	125	53	p	p	NOUN
ijpds-4231	125	54	-	-	PUNCT
ijpds-4231	125	55	toluene	toluene	NOUN
ijpds-4231	125	56	-	-	PUNCT
ijpds-4231	125	57	sulfonic	sulfonic	ADJ
ijpds-4231	125	58	acid	acid	NOUN
ijpds-4231	125	59	monohydrate	monohydrate	NOUN
ijpds-4231	125	60	to	to	PART
ijpds-4231	125	61	form	form	NOUN
ijpds-4231	125	62	(	(	PUNCT
ijpds-4231	125	63	1z)-n	1z)-n	NUM
ijpds-4231	125	64	-	-	PUNCT
ijpds-4231	125	65	phenyl-2,3	phenyl-2,3	NOUN
ijpds-4231	125	66	-	-	PUNCT
ijpds-4231	125	67	dihydro-1hinden-1	dihydro-1hinden-1	NOUN
ijpds-4231	125	68	-	-	PUNCT
ijpds-4231	125	69	imine	imine	NOUN
ijpds-4231	125	70	21	21	NUM
ijpds-4231	125	71	(	(	PUNCT
ijpds-4231	125	72	82.5	82.5	NUM
ijpds-4231	125	73	%	%	NOUN
ijpds-4231	125	74	)	)	PUNCT
ijpds-4231	125	75	.	.	PUNCT
ijpds-4231	126	1	it	it	PRON
ijpds-4231	126	2	was	be	AUX
ijpds-4231	126	3	reduced	reduce	VERB
ijpds-4231	126	4	under	under	ADP
ijpds-4231	126	5	the	the	DET
ijpds-4231	126	6	impact	impact	NOUN
ijpds-4231	126	7	of	of	ADP
ijpds-4231	126	8	raney	raney	NOUN
ijpds-4231	126	9	-	-	PUNCT
ijpds-4231	126	10	nickel	nickel	NOUN
ijpds-4231	126	11	in	in	ADP
ijpds-4231	126	12	isopropyl	isopropyl	NOUN
ijpds-4231	126	13	acetate	acetate	NOUN
ijpds-4231	126	14	to	to	PART
ijpds-4231	126	15	isolate	isolate	VERB
ijpds-4231	126	16	n	n	CCONJ
ijpds-4231	126	17	-	-	PUNCT
ijpds-4231	126	18	phenyl2,3	phenyl2,3	PROPN
ijpds-4231	126	19	-	-	PUNCT
ijpds-4231	126	20	dihydro-1h	dihydro-1h	NOUN
ijpds-4231	126	21	-	-	PUNCT
ijpds-4231	126	22	inden-1	inden-1	NOUN
ijpds-4231	126	23	-	-	PUNCT
ijpds-4231	126	24	amine	amine	ADJ
ijpds-4231	126	25	22	22	NUM
ijpds-4231	126	26	(	(	PUNCT
ijpds-4231	126	27	yield	yield	NOUN
ijpds-4231	126	28	:	:	PUNCT
ijpds-4231	126	29	88	88	NUM
ijpds-4231	126	30	%	%	NOUN
ijpds-4231	126	31	)	)	PUNCT
ijpds-4231	126	32	.	.	PUNCT
ijpds-4231	127	1	it	it	PRON
ijpds-4231	127	2	was	be	AUX
ijpds-4231	127	3	dissolved	dissolve	VERB
ijpds-4231	127	4	in	in	ADP
ijpds-4231	127	5	tetrahydrofuran	tetrahydrofuran	NOUN
ijpds-4231	127	6	and	and	CCONJ
ijpds-4231	127	7	treated	treat	VERB
ijpds-4231	127	8	with	with	ADP
ijpds-4231	127	9	phosphorus	phosphorus	NOUN
ijpds-4231	127	10	pentachloride	pentachloride	ADV
ijpds-4231	127	11	in	in	ADP
ijpds-4231	127	12	the	the	DET
ijpds-4231	127	13	presence	presence	NOUN
ijpds-4231	127	14	of	of	ADP
ijpds-4231	127	15	triethylamine	triethylamine	NOUN
ijpds-4231	127	16	and	and	CCONJ
ijpds-4231	127	17	then	then	ADV
ijpds-4231	127	18	treated	treat	VERB
ijpds-4231	127	19	with	with	ADP
ijpds-4231	127	20	oxammonium	oxammonium	NOUN
ijpds-4231	127	21	hydrochloride	hydrochloride	NOUN
ijpds-4231	127	22	to	to	PART
ijpds-4231	127	23	isolate	isolate	VERB
ijpds-4231	127	24	risomer	risomer	NOUN
ijpds-4231	127	25	of	of	ADP
ijpds-4231	127	26	2	2	NUM
ijpds-4231	127	27	(	(	PUNCT
ijpds-4231	127	28	as	as	ADP
ijpds-4231	127	29	free	free	ADJ
ijpds-4231	127	30	base	base	NOUN
ijpds-4231	127	31	or	or	CCONJ
ijpds-4231	127	32	its	its	PRON
ijpds-4231	127	33	hydrochloride	hydrochloride	NOUN
ijpds-4231	127	34	salt	salt	NOUN
ijpds-4231	127	35	,	,	PUNCT
ijpds-4231	127	36	yield	yield	NOUN
ijpds-4231	127	37	:	:	PUNCT
ijpds-4231	127	38	70	70	NUM
ijpds-4231	127	39	-	-	SYM
ijpds-4231	127	40	90	90	NUM
ijpds-4231	127	41	%	%	NOUN
ijpds-4231	127	42	)	)	PUNCT
ijpds-4231	127	43	.	.	PUNCT
ijpds-4231	128	1	hydrochloride	hydrochloride	NOUN
ijpds-4231	128	2	salt	salt	NOUN
ijpds-4231	128	3	of	of	ADP
ijpds-4231	128	4	2	2	NUM
ijpds-4231	128	5	in	in	ADP
ijpds-4231	128	6	acetonitrile	acetonitrile	NOUN
ijpds-4231	128	7	was	be	AUX
ijpds-4231	128	8	treated	treat	VERB
ijpds-4231	128	9	with	with	ADP
ijpds-4231	128	10	3	3	NUM
ijpds-4231	128	11	in	in	ADP
ijpds-4231	128	12	the	the	DET
ijpds-4231	128	13	presence	presence	NOUN
ijpds-4231	128	14	of	of	ADP
ijpds-4231	128	15	potassium	potassium	NOUN
ijpds-4231	128	16	carbonate	carbonate	NOUN
ijpds-4231	128	17	followed	follow	VERB
ijpds-4231	128	18	by	by	ADP
ijpds-4231	128	19	the	the	DET
ijpds-4231	128	20	addition	addition	NOUN
ijpds-4231	128	21	of	of	ADP
ijpds-4231	128	22	methanesulfonic	methanesulfonic	ADJ
ijpds-4231	128	23	acid	acid	NOUN
ijpds-4231	128	24	in	in	ADP
ijpds-4231	128	25	diethyl	diethyl	NOUN
ijpds-4231	128	26	ether	ether	NOUN
ijpds-4231	128	27	to	to	PART
ijpds-4231	128	28	obtain	obtain	VERB
ijpds-4231	128	29	1	1	NUM
ijpds-4231	128	30	with	with	ADP
ijpds-4231	128	31	a	a	DET
ijpds-4231	128	32	melting	melting	NOUN
ijpds-4231	128	33	point	point	NOUN
ijpds-4231	128	34	of	of	ADP
ijpds-4231	128	35	156	156	NUM
ijpds-4231	128	36	-	-	PUNCT
ijpds-4231	128	37	158oc	158oc	NOUN
ijpds-4231	129	1	[	[	X
ijpds-4231	129	2	18	18	NUM
ijpds-4231	129	3	]	]	PUNCT
ijpds-4231	129	4	.	.	PUNCT
ijpds-4231	130	1	bosch	bosch	PROPN
ijpds-4231	130	2	ilj	ilj	PROPN
ijpds-4231	130	3	,	,	PUNCT
ijpds-4231	130	4	et	et	PROPN
ijpds-4231	130	5	al	al	PROPN
ijpds-4231	130	6	.	.	PROPN
ijpds-4231	130	7	,	,	PUNCT
ijpds-4231	130	8	in	in	ADP
ijpds-4231	130	9	2009	2009	NUM
ijpds-4231	130	10	,	,	PUNCT
ijpds-4231	130	11	had	have	AUX
ijpds-4231	130	12	reported	report	VERB
ijpds-4231	130	13	a	a	DET
ijpds-4231	130	14	few	few	ADJ
ijpds-4231	130	15	reactions	reaction	NOUN
ijpds-4231	130	16	of	of	ADP
ijpds-4231	130	17	r	r	NOUN
ijpds-4231	130	18	-	-	PUNCT
ijpds-4231	130	19	isomer	isomer	NOUN
ijpds-4231	130	20	of	of	ADP
ijpds-4231	130	21	2	2	NUM
ijpds-4231	130	22	in	in	ADP
ijpds-4231	130	23	toluene	toluene	NOUN
ijpds-4231	130	24	with	with	ADP
ijpds-4231	130	25	8	8	NUM
ijpds-4231	130	26	in	in	ADP
ijpds-4231	130	27	the	the	DET
ijpds-4231	130	28	presence	presence	NOUN
ijpds-4231	130	29	of	of	ADP
ijpds-4231	130	30	sodium	sodium	NOUN
ijpds-4231	130	31	hydroxide	hydroxide	NOUN
ijpds-4231	130	32	solution	solution	NOUN
ijpds-4231	130	33	to	to	PART
ijpds-4231	130	34	get	get	VERB
ijpds-4231	130	35	r	r	NOUN
ijpds-4231	130	36	-	-	PUNCT
ijpds-4231	130	37	rasagiline	rasagiline	NOUN
ijpds-4231	130	38	base	base	NOUN
ijpds-4231	130	39	(	(	PUNCT
ijpds-4231	130	40	yield	yield	NOUN
ijpds-4231	130	41	:	:	PUNCT
ijpds-4231	130	42	67.8272.49	67.8272.49	NUM
ijpds-4231	130	43	%	%	NOUN
ijpds-4231	130	44	)	)	PUNCT
ijpds-4231	130	45	.	.	PUNCT
ijpds-4231	131	1	it	it	PRON
ijpds-4231	131	2	was	be	AUX
ijpds-4231	131	3	treated	treat	VERB
ijpds-4231	131	4	with	with	ADP
ijpds-4231	131	5	methanesulfonic	methanesulfonic	ADJ
ijpds-4231	131	6	acid	acid	NOUN
ijpds-4231	131	7	in	in	ADP
ijpds-4231	131	8	toluene	toluene	NOUN
ijpds-4231	131	9	or	or	CCONJ
ijpds-4231	131	10	acetonitrile	acetonitrile	NOUN
ijpds-4231	131	11	to	to	PART
ijpds-4231	131	12	isolate	isolate	VERB
ijpds-4231	131	13	the	the	DET
ijpds-4231	131	14	crude	crude	ADJ
ijpds-4231	131	15	1	1	NUM
ijpds-4231	131	16	(	(	PUNCT
ijpds-4231	131	17	yield	yield	NOUN
ijpds-4231	131	18	:	:	PUNCT
ijpds-4231	131	19	85.5497.39	85.5497.39	NUM
ijpds-4231	131	20	%	%	NOUN
ijpds-4231	131	21	,	,	PUNCT
ijpds-4231	131	22	purity	purity	NOUN
ijpds-4231	131	23	:	:	PUNCT
ijpds-4231	131	24	79.65	79.65	NUM
ijpds-4231	131	25	-	-	SYM
ijpds-4231	131	26	93.32	93.32	NUM
ijpds-4231	131	27	%	%	NOUN
ijpds-4231	131	28	by	by	ADP
ijpds-4231	131	29	hplc	hplc	NOUN
ijpds-4231	131	30	)	)	PUNCT
ijpds-4231	131	31	.	.	PUNCT
ijpds-4231	132	1	furthermore	furthermore	ADV
ijpds-4231	132	2	,	,	PUNCT
ijpds-4231	132	3	a	a	DET
ijpds-4231	132	4	double	double	ADJ
ijpds-4231	132	5	recrystallization	recrystallization	NOUN
ijpds-4231	132	6	of	of	ADP
ijpds-4231	132	7	crude	crude	ADJ
ijpds-4231	132	8	1	1	NUM
ijpds-4231	132	9	was	be	AUX
ijpds-4231	132	10	done	do	VERB
ijpds-4231	132	11	from	from	ADP
ijpds-4231	132	12	acetonitrile	acetonitrile	NOUN
ijpds-4231	132	13	and	and	CCONJ
ijpds-4231	132	14	then	then	ADV
ijpds-4231	132	15	the	the	DET
ijpds-4231	132	16	solid	solid	ADJ
ijpds-4231	132	17	obtained	obtain	VERB
ijpds-4231	132	18	was	be	AUX
ijpds-4231	132	19	suspended	suspend	VERB
ijpds-4231	132	20	in	in	ADP
ijpds-4231	132	21	acetonitrile	acetonitrile	ADJ
ijpds-4231	132	22	/	/	SYM
ijpds-4231	132	23	water	water	NOUN
ijpds-4231	132	24	mixture	mixture	NOUN
ijpds-4231	132	25	to	to	PART
ijpds-4231	132	26	get	get	VERB
ijpds-4231	132	27	1	1	NUM
ijpds-4231	132	28	(	(	PUNCT
ijpds-4231	132	29	overall	overall	ADJ
ijpds-4231	132	30	yield	yield	NOUN
ijpds-4231	132	31	:	:	PUNCT
ijpds-4231	132	32	22	22	NUM
ijpds-4231	132	33	-	-	SYM
ijpds-4231	132	34	33	33	NUM
ijpds-4231	132	35	%	%	NOUN
ijpds-4231	132	36	,	,	PUNCT
ijpds-4231	132	37	purity	purity	NOUN
ijpds-4231	132	38	:	:	PUNCT
ijpds-4231	132	39	99	99	NUM
ijpds-4231	132	40	-	-	SYM
ijpds-4231	132	41	100	100	NUM
ijpds-4231	132	42	%	%	NOUN
ijpds-4231	132	43	by	by	ADP
ijpds-4231	132	44	hplc	hplc	NOUN
ijpds-4231	132	45	)	)	PUNCT
ijpds-4231	132	46	.	.	PUNCT
ijpds-4231	133	1	they	they	PRON
ijpds-4231	133	2	had	have	AUX
ijpds-4231	133	3	reported	report	VERB
ijpds-4231	133	4	the	the	DET
ijpds-4231	133	5	recrystallization	recrystallization	NOUN
ijpds-4231	133	6	of	of	ADP
ijpds-4231	133	7	1	1	NUM
ijpds-4231	133	8	in	in	ADP
ijpds-4231	133	9	isopropyl	isopropyl	NOUN
ijpds-4231	133	10	alcohol	alcohol	NOUN
ijpds-4231	133	11	,	,	PUNCT
ijpds-4231	133	12	but	but	CCONJ
ijpds-4231	133	13	the	the	DET
ijpds-4231	133	14	final	final	ADJ
ijpds-4231	133	15	product	product	NOUN
ijpds-4231	133	16	and	and	CCONJ
ijpds-4231	133	17	the	the	DET
ijpds-4231	133	18	filtrate	filtrate	NOUN
ijpds-4231	133	19	had	have	VERB
ijpds-4231	133	20	isopropyl	isopropyl	NOUN
ijpds-4231	133	21	mesylate	mesylate	NOUN
ijpds-4231	133	22	traces	trace	NOUN
ijpds-4231	133	23	as	as	ADP
ijpds-4231	133	24	an	an	DET
ijpds-4231	133	25	impurity	impurity	NOUN
ijpds-4231	133	26	(	(	PUNCT
ijpds-4231	133	27	by	by	ADP
ijpds-4231	133	28	gc	gc	PROPN
ijpds-4231	133	29	analysis	analysis	NOUN
ijpds-4231	133	30	)	)	PUNCT
ijpds-4231	134	1	[	[	X
ijpds-4231	134	2	19	19	NUM
ijpds-4231	134	3	]	]	PUNCT
ijpds-4231	134	4	.	.	PUNCT
ijpds-4231	135	1	frenkel	frenkel	PROPN
ijpds-4231	135	2	a	a	PRON
ijpds-4231	135	3	,	,	PUNCT
ijpds-4231	135	4	et	et	PROPN
ijpds-4231	135	5	al	al	PROPN
ijpds-4231	135	6	.	.	PROPN
ijpds-4231	135	7	,	,	PUNCT
ijpds-4231	135	8	in	in	ADP
ijpds-4231	135	9	2009	2009	NUM
ijpds-4231	135	10	,	,	PUNCT
ijpds-4231	135	11	had	have	AUX
ijpds-4231	135	12	demonstrated	demonstrate	VERB
ijpds-4231	135	13	the	the	DET
ijpds-4231	135	14	isolation	isolation	NOUN
ijpds-4231	135	15	of	of	ADP
ijpds-4231	135	16	crystalline	crystalline	NOUN
ijpds-4231	135	17	solid	solid	ADJ
ijpds-4231	135	18	r	r	NOUN
ijpds-4231	135	19	-	-	PUNCT
ijpds-4231	135	20	rasagiline	rasagiline	NOUN
ijpds-4231	135	21	base	base	NOUN
ijpds-4231	135	22	(	(	PUNCT
ijpds-4231	135	23	yield	yield	NOUN
ijpds-4231	135	24	:	:	PUNCT
ijpds-4231	135	25	70	70	NUM
ijpds-4231	135	26	-	-	SYM
ijpds-4231	135	27	90	90	NUM
ijpds-4231	135	28	%	%	NOUN
ijpds-4231	135	29	)	)	PUNCT
ijpds-4231	135	30	from	from	ADP
ijpds-4231	135	31	its	its	PRON
ijpds-4231	135	32	mesylate	mesylate	NOUN
ijpds-4231	135	33	or	or	CCONJ
ijpds-4231	135	34	tartarate	tartarate	NOUN
ijpds-4231	135	35	by	by	ADP
ijpds-4231	135	36	a	a	DET
ijpds-4231	135	37	few	few	ADJ
ijpds-4231	135	38	methods	method	NOUN
ijpds-4231	135	39	like	like	ADP
ijpds-4231	135	40	splitting	splitting	NOUN
ijpds-4231	135	41	,	,	PUNCT
ijpds-4231	135	42	extraction	extraction	NOUN
ijpds-4231	135	43	,	,	PUNCT
ijpds-4231	135	44	water	water	NOUN
ijpds-4231	135	45	crystallization	crystallization	NOUN
ijpds-4231	135	46	,	,	PUNCT
ijpds-4231	135	47	melt	melt	VERB
ijpds-4231	135	48	crystallization	crystallization	NOUN
ijpds-4231	135	49	,	,	PUNCT
ijpds-4231	135	50	quenching	quench	VERB
ijpds-4231	135	51	to	to	PART
ijpds-4231	135	52	water	water	NOUN
ijpds-4231	135	53	,	,	PUNCT
ijpds-4231	135	54	reverse	reverse	ADJ
ijpds-4231	135	55	quenching	quenching	NOUN
ijpds-4231	135	56	,	,	PUNCT
ijpds-4231	135	57	seeding	seed	VERB
ijpds-4231	135	58	crystallization	crystallization	NOUN
ijpds-4231	135	59	etc	etc	X
ijpds-4231	135	60	.	.	X
ijpds-4231	136	1	under	under	ADP
ijpds-4231	136	2	the	the	DET
ijpds-4231	136	3	usual	usual	ADJ
ijpds-4231	136	4	conditions	condition	NOUN
ijpds-4231	136	5	,	,	PUNCT
ijpds-4231	136	6	rrasagiline	rrasagiline	ADJ
ijpds-4231	136	7	base	base	NOUN
ijpds-4231	136	8	would	would	AUX
ijpds-4231	136	9	be	be	AUX
ijpds-4231	136	10	used	use	VERB
ijpds-4231	136	11	in	in	ADP
ijpds-4231	136	12	its	its	PRON
ijpds-4231	136	13	crude	crude	ADJ
ijpds-4231	136	14	form	form	NOUN
ijpds-4231	136	15	as	as	ADP
ijpds-4231	136	16	an	an	DET
ijpds-4231	136	17	oily	oily	ADJ
ijpds-4231	136	18	liquid	liquid	NOUN
ijpds-4231	136	19	.	.	PUNCT
ijpds-4231	137	1	the	the	DET
ijpds-4231	137	2	work	work	NOUN
ijpds-4231	137	3	had	have	AUX
ijpds-4231	137	4	reported	report	VERB
ijpds-4231	137	5	the	the	DET
ijpds-4231	137	6	isolation	isolation	NOUN
ijpds-4231	137	7	of	of	ADP
ijpds-4231	137	8	the	the	DET
ijpds-4231	137	9	solid	solid	ADJ
ijpds-4231	137	10	form	form	NOUN
ijpds-4231	137	11	of	of	ADP
ijpds-4231	137	12	r	r	NOUN
ijpds-4231	137	13	-	-	PUNCT
ijpds-4231	137	14	rasagiline	rasagiline	NOUN
ijpds-4231	137	15	base	base	NOUN
ijpds-4231	137	16	by	by	ADP
ijpds-4231	137	17	various	various	ADJ
ijpds-4231	137	18	crystallization	crystallization	NOUN
ijpds-4231	137	19	approaches	approach	NOUN
ijpds-4231	137	20	with	with	ADP
ijpds-4231	137	21	a	a	DET
ijpds-4231	137	22	melting	melting	NOUN
ijpds-4231	137	23	point	point	NOUN
ijpds-4231	137	24	of	of	ADP
ijpds-4231	137	25	15	15	NUM
ijpds-4231	137	26	-	-	PUNCT
ijpds-4231	137	27	20oc	20oc	NOUN
ijpds-4231	137	28	(	(	PUNCT
ijpds-4231	137	29	isolated	isolate	VERB
ijpds-4231	137	30	from	from	ADP
ijpds-4231	137	31	toluene	toluene	NOUN
ijpds-4231	137	32	)	)	PUNCT
ijpds-4231	137	33	,	,	PUNCT
ijpds-4231	137	34	38.2	38.2	NUM
ijpds-4231	137	35	-	-	SYM
ijpds-4231	137	36	38.4oc	38.4oc	NOUN
ijpds-4231	137	37	(	(	PUNCT
ijpds-4231	137	38	isolated	isolate	VERB
ijpds-4231	137	39	from	from	ADP
ijpds-4231	137	40	water	water	NOUN
ijpds-4231	137	41	)	)	PUNCT
ijpds-4231	137	42	,	,	PUNCT
ijpds-4231	137	43	39.0	39.0	NUM
ijpds-4231	137	44	-	-	SYM
ijpds-4231	137	45	39.2oc	39.2oc	NUM
ijpds-4231	137	46	(	(	PUNCT
ijpds-4231	137	47	isolated	isolate	VERB
ijpds-4231	137	48	from	from	ADP
ijpds-4231	137	49	isopropyl	isopropyl	NOUN
ijpds-4231	137	50	alcohol	alcohol	PROPN
ijpds-4231	137	51	)	)	PUNCT
ijpds-4231	137	52	,	,	PUNCT
ijpds-4231	137	53	40.8oc	40.8oc	NOUN
ijpds-4231	137	54	(	(	PUNCT
ijpds-4231	137	55	isolated	isolate	VERB
ijpds-4231	137	56	from	from	ADP
ijpds-4231	137	57	isopropyl	isopropyl	NOUN
ijpds-4231	137	58	alcohol	alcohol	NOUN
ijpds-4231	137	59	/	/	SYM
ijpds-4231	137	60	water	water	NOUN
ijpds-4231	137	61	by	by	ADP
ijpds-4231	137	62	seeded	seeded	ADJ
ijpds-4231	137	63	emulsion	emulsion	NOUN
ijpds-4231	137	64	)	)	PUNCT
ijpds-4231	137	65	and	and	CCONJ
ijpds-4231	137	66	41.3oc	41.3oc	NUM
ijpds-4231	137	67	(	(	PUNCT
ijpds-4231	137	68	isolated	isolate	VERB
ijpds-4231	137	69	from	from	ADP
ijpds-4231	137	70	isopropyl	isopropyl	NOUN
ijpds-4231	137	71	alcohol	alcohol	NOUN
ijpds-4231	137	72	/	/	SYM
ijpds-4231	137	73	water	water	NOUN
ijpds-4231	137	74	by	by	ADP
ijpds-4231	137	75	seeding	seed	VERB
ijpds-4231	137	76	crystallization	crystallization	NOUN
ijpds-4231	137	77	)	)	PUNCT
ijpds-4231	138	1	[	[	X
ijpds-4231	138	2	20	20	NUM
ijpds-4231	138	3	-	-	SYM
ijpds-4231	138	4	22	22	NUM
ijpds-4231	138	5	]	]	PUNCT
ijpds-4231	138	6	.	.	PUNCT
ijpds-4231	139	1	gore	gore	PROPN
ijpds-4231	139	2	v	v	PROPN
ijpds-4231	139	3	,	,	PUNCT
ijpds-4231	139	4	et	et	PROPN
ijpds-4231	139	5	al	al	PROPN
ijpds-4231	139	6	.	.	PROPN
ijpds-4231	139	7	,	,	PUNCT
ijpds-4231	139	8	in	in	ADP
ijpds-4231	139	9	2009	2009	NUM
ijpds-4231	139	10	,	,	PUNCT
ijpds-4231	139	11	had	have	AUX
ijpds-4231	139	12	disclosed	disclose	VERB
ijpds-4231	139	13	a	a	DET
ijpds-4231	139	14	process	process	NOUN
ijpds-4231	139	15	to	to	PART
ijpds-4231	139	16	get	get	VERB
ijpds-4231	139	17	enantiomerically	enantiomerically	ADV
ijpds-4231	139	18	pure	pure	ADJ
ijpds-4231	139	19	r	r	NOUN
ijpds-4231	139	20	-	-	PUNCT
ijpds-4231	139	21	isomer	isomer	NOUN
ijpds-4231	139	22	of	of	ADP
ijpds-4231	139	23	2	2	NUM
ijpds-4231	139	24	by	by	ADP
ijpds-4231	139	25	treating	treat	VERB
ijpds-4231	139	26	racemic	racemic	ADJ
ijpds-4231	139	27	2	2	NUM
ijpds-4231	139	28	with	with	ADP
ijpds-4231	139	29	2,3,4,6	2,3,4,6	NUM
ijpds-4231	139	30	-	-	PUNCT
ijpds-4231	139	31	di	di	NOUN
ijpds-4231	139	32	-	-	ADJ
ijpds-4231	139	33	o	o	NOUN
ijpds-4231	139	34	-	-	PUNCT
ijpds-4231	139	35	isopropylidene-2	isopropylidene-2	NUM
ijpds-4231	139	36	-	-	PUNCT
ijpds-4231	139	37	keto	keto	NOUN
ijpds-4231	139	38	-	-	PUNCT
ijpds-4231	139	39	l	l	NOUN
ijpds-4231	139	40	-	-	PUNCT
ijpds-4231	139	41	gulonic	gulonic	ADJ
ijpds-4231	139	42	acid	acid	NOUN
ijpds-4231	139	43	monohydrate	monohydrate	NOUN
ijpds-4231	139	44	in	in	ADP
ijpds-4231	139	45	methyl	methyl	NOUN
ijpds-4231	139	46	alcohol	alcohol	NOUN
ijpds-4231	139	47	to	to	PART
ijpds-4231	139	48	isolate	isolate	VERB
ijpds-4231	139	49	the	the	DET
ijpds-4231	139	50	crude	crude	ADJ
ijpds-4231	139	51	salt	salt	NOUN
ijpds-4231	139	52	.	.	PUNCT
ijpds-4231	140	1	it	it	PRON
ijpds-4231	140	2	was	be	AUX
ijpds-4231	140	3	dissolved	dissolve	VERB
ijpds-4231	140	4	in	in	ADP
ijpds-4231	140	5	aqueous	aqueous	ADJ
ijpds-4231	140	6	methyl	methyl	NOUN
ijpds-4231	140	7	alcohol	alcohol	NOUN
ijpds-4231	140	8	and	and	CCONJ
ijpds-4231	140	9	crystallized	crystallize	VERB
ijpds-4231	140	10	to	to	PART
ijpds-4231	140	11	isolate	isolate	VERB
ijpds-4231	140	12	the	the	DET
ijpds-4231	140	13	salt	salt	NOUN
ijpds-4231	140	14	.	.	PUNCT
ijpds-4231	141	1	pure	pure	ADJ
ijpds-4231	141	2	r	r	NOUN
ijpds-4231	141	3	-	-	PUNCT
ijpds-4231	141	4	isomer	isomer	NOUN
ijpds-4231	141	5	of	of	ADP
ijpds-4231	141	6	2	2	NUM
ijpds-4231	141	7	(	(	PUNCT
ijpds-4231	141	8	yield	yield	NOUN
ijpds-4231	141	9	:	:	PUNCT
ijpds-4231	141	10	40	40	NUM
ijpds-4231	141	11	-	-	SYM
ijpds-4231	141	12	42	42	NUM
ijpds-4231	141	13	%	%	NOUN
ijpds-4231	141	14	,	,	PUNCT
ijpds-4231	141	15	chiral	chiral	ADJ
ijpds-4231	141	16	purity	purity	NOUN
ijpds-4231	141	17	:	:	PUNCT
ijpds-4231	141	18	96	96	NUM
ijpds-4231	141	19	-	-	SYM
ijpds-4231	141	20	97	97	NUM
ijpds-4231	141	21	%	%	NOUN
ijpds-4231	141	22	by	by	ADP
ijpds-4231	141	23	hplc	hplc	NOUN
ijpds-4231	141	24	,	,	PUNCT
ijpds-4231	141	25	as	as	ADP
ijpds-4231	141	26	light	light	ADJ
ijpds-4231	141	27	green	green	ADJ
ijpds-4231	141	28	oily	oily	ADJ
ijpds-4231	141	29	liquid	liquid	NOUN
ijpds-4231	141	30	)	)	PUNCT
ijpds-4231	141	31	was	be	AUX
ijpds-4231	141	32	isolated	isolate	VERB
ijpds-4231	141	33	by	by	ADP
ijpds-4231	141	34	salt	salt	NOUN
ijpds-4231	141	35	breaking	break	VERB
ijpds-4231	141	36	method	method	NOUN
ijpds-4231	141	37	in	in	ADP
ijpds-4231	141	38	the	the	DET
ijpds-4231	141	39	presence	presence	NOUN
ijpds-4231	141	40	of	of	ADP
ijpds-4231	141	41	sodium	sodium	NOUN
ijpds-4231	141	42	carbonate	carbonate	NOUN
ijpds-4231	141	43	solution	solution	NOUN
ijpds-4231	141	44	and	and	CCONJ
ijpds-4231	141	45	extracting	extract	VERB
ijpds-4231	141	46	the	the	DET
ijpds-4231	141	47	free	free	ADJ
ijpds-4231	141	48	base	base	NOUN
ijpds-4231	141	49	to	to	PART
ijpds-4231	141	50	dichloromethane	dichloromethane	VERB
ijpds-4231	141	51	[	[	X
ijpds-4231	141	52	23	23	NUM
ijpds-4231	141	53	]	]	PUNCT
ijpds-4231	141	54	.	.	PUNCT
ijpds-4231	142	1	the	the	DET
ijpds-4231	142	2	reported	report	VERB
ijpds-4231	142	3	work	work	NOUN
ijpds-4231	142	4	was	be	AUX
ijpds-4231	142	5	much	much	ADV
ijpds-4231	142	6	superior	superior	ADJ
ijpds-4231	142	7	to	to	ADP
ijpds-4231	142	8	the	the	DET
ijpds-4231	142	9	past	past	NOUN
ijpds-4231	142	10	disclosed	disclose	VERB
ijpds-4231	142	11	resolving	resolve	VERB
ijpds-4231	142	12	techniques	technique	NOUN
ijpds-4231	142	13	[	[	X
ijpds-4231	142	14	12,24	12,24	NUM
ijpds-4231	142	15	]	]	PUNCT
ijpds-4231	142	16	.	.	PUNCT
ijpds-4231	143	1	frenkel	frenkel	PROPN
ijpds-4231	143	2	a	a	PRON
ijpds-4231	143	3	&	&	CCONJ
ijpds-4231	143	4	koltai	koltai	PROPN
ijpds-4231	143	5	t.	t.	PROPN
ijpds-4231	143	6	,	,	PUNCT
ijpds-4231	143	7	in	in	ADP
ijpds-4231	143	8	2009	2009	NUM
ijpds-4231	143	9	,	,	PUNCT
ijpds-4231	143	10	had	have	AUX
ijpds-4231	143	11	illustrated	illustrate	VERB
ijpds-4231	143	12	a	a	DET
ijpds-4231	143	13	process	process	NOUN
ijpds-4231	143	14	to	to	PART
ijpds-4231	143	15	manufacture	manufacture	VERB
ijpds-4231	143	16	of	of	ADP
ijpds-4231	143	17	rasagiline	rasagiline	NOUN
ijpds-4231	143	18	tannate	tannate	NOUN
ijpds-4231	143	19	.	.	PUNCT
ijpds-4231	144	1	rasagiline	rasagiline	PROPN
ijpds-4231	144	2	base	base	PROPN
ijpds-4231	144	3	was	be	AUX
ijpds-4231	144	4	treated	treat	VERB
ijpds-4231	144	5	with	with	ADP
ijpds-4231	144	6	tannic	tannic	ADJ
ijpds-4231	144	7	acid	acid	NOUN
ijpds-4231	144	8	solution	solution	NOUN
ijpds-4231	144	9	to	to	PART
ijpds-4231	144	10	obtain	obtain	VERB
ijpds-4231	144	11	the	the	DET
ijpds-4231	144	12	first	first	ADJ
ijpds-4231	144	13	mixture	mixture	NOUN
ijpds-4231	144	14	.	.	PUNCT
ijpds-4231	145	1	a	a	DET
ijpds-4231	145	2	partial	partial	ADJ
ijpds-4231	145	3	removal	removal	NOUN
ijpds-4231	145	4	of	of	ADP
ijpds-4231	145	5	the	the	DET
ijpds-4231	145	6	liquid	liquid	NOUN
ijpds-4231	145	7	from	from	ADP
ijpds-4231	145	8	the	the	DET
ijpds-4231	145	9	first	first	ADJ
ijpds-4231	145	10	mixture	mixture	NOUN
ijpds-4231	145	11	and	and	CCONJ
ijpds-4231	145	12	the	the	DET
ijpds-4231	145	13	addition	addition	NOUN
ijpds-4231	145	14	of	of	ADP
ijpds-4231	145	15	a	a	DET
ijpds-4231	145	16	polar	polar	ADJ
ijpds-4231	145	17	water	water	NOUN
ijpds-4231	145	18	soluble	soluble	ADJ
ijpds-4231	145	19	solvent	solvent	NOUN
ijpds-4231	145	20	(	(	PUNCT
ijpds-4231	145	21	ethyl	ethyl	PROPN
ijpds-4231	145	22	alcohol	alcohol	PROPN
ijpds-4231	145	23	)	)	PUNCT
ijpds-4231	145	24	had	have	AUX
ijpds-4231	145	25	resulted	result	VERB
ijpds-4231	145	26	in	in	ADP
ijpds-4231	145	27	the	the	DET
ijpds-4231	145	28	formation	formation	NOUN
ijpds-4231	145	29	of	of	ADP
ijpds-4231	145	30	second	second	ADJ
ijpds-4231	145	31	mixture	mixture	NOUN
ijpds-4231	145	32	.	.	PUNCT
ijpds-4231	146	1	furthermore	furthermore	ADV
ijpds-4231	146	2	,	,	PUNCT
ijpds-4231	146	3	liquid	liquid	NOUN
ijpds-4231	146	4	/	/	SYM
ijpds-4231	146	5	solvent	solvent	NOUN
ijpds-4231	146	6	was	be	AUX
ijpds-4231	146	7	removed	remove	VERB
ijpds-4231	146	8	completely	completely	ADV
ijpds-4231	146	9	at	at	ADP
ijpds-4231	146	10	ambient	ambient	ADJ
ijpds-4231	146	11	temperature	temperature	NOUN
ijpds-4231	146	12	to	to	PART
ijpds-4231	146	13	isolate	isolate	VERB
ijpds-4231	146	14	the	the	DET
ijpds-4231	146	15	tannate	tannate	NOUN
ijpds-4231	146	16	salt	salt	NOUN
ijpds-4231	146	17	.	.	PUNCT
ijpds-4231	147	1	the	the	DET
ijpds-4231	147	2	isolated	isolated	ADJ
ijpds-4231	147	3	rasagiline	rasagiline	NOUN
ijpds-4231	147	4	tannate	tannate	NOUN
ijpds-4231	147	5	had	have	VERB
ijpds-4231	147	6	the	the	DET
ijpds-4231	147	7	water	water	NOUN
ijpds-4231	147	8	content	content	NOUN
ijpds-4231	147	9	of	of	ADP
ijpds-4231	147	10	below	below	ADP
ijpds-4231	147	11	10	10	NUM
ijpds-4231	147	12	%	%	NOUN
ijpds-4231	147	13	and	and	CCONJ
ijpds-4231	147	14	the	the	DET
ijpds-4231	147	15	rasagiline	rasagiline	NOUN
ijpds-4231	147	16	content	content	NOUN
ijpds-4231	147	17	was	be	AUX
ijpds-4231	147	18	got	get	VERB
ijpds-4231	147	19	varied	varied	ADJ
ijpds-4231	147	20	around	around	ADV
ijpds-4231	147	21	in	in	ADP
ijpds-4231	147	22	the	the	DET
ijpds-4231	147	23	range	range	NOUN
ijpds-4231	147	24	of	of	ADP
ijpds-4231	147	25	3	3	NUM
ijpds-4231	147	26	-	-	SYM
ijpds-4231	147	27	64	64	NUM
ijpds-4231	147	28	%	%	NOUN
ijpds-4231	147	29	.	.	PUNCT
ijpds-4231	148	1	the	the	DET
ijpds-4231	148	2	work	work	NOUN
ijpds-4231	148	3	had	have	AUX
ijpds-4231	148	4	disclosed	disclose	VERB
ijpds-4231	148	5	the	the	DET
ijpds-4231	148	6	cleavage	cleavage	NOUN
ijpds-4231	148	7	of	of	ADP
ijpds-4231	148	8	1	1	NUM
ijpds-4231	148	9	to	to	PART
ijpds-4231	148	10	isolate	isolate	VERB
ijpds-4231	148	11	rasagiline	rasagiline	NOUN
ijpds-4231	148	12	base	base	NOUN
ijpds-4231	148	13	as	as	ADP
ijpds-4231	148	14	an	an	DET
ijpds-4231	148	15	oily	oily	ADJ
ijpds-4231	148	16	mass	mass	NOUN
ijpds-4231	148	17	and	and	CCONJ
ijpds-4231	148	18	its	its	PRON
ijpds-4231	148	19	crystallization	crystallization	NOUN
ijpds-4231	148	20	to	to	PART
ijpds-4231	148	21	isolate	isolate	VERB
ijpds-4231	148	22	in	in	ADP
ijpds-4231	148	23	the	the	DET
ijpds-4231	148	24	solid	solid	ADJ
ijpds-4231	148	25	form	form	NOUN
ijpds-4231	148	26	with	with	ADP
ijpds-4231	148	27	a	a	DET
ijpds-4231	148	28	melting	melting	NOUN
ijpds-4231	148	29	point	point	NOUN
ijpds-4231	148	30	of	of	ADP
ijpds-4231	148	31	39	39	NUM
ijpds-4231	148	32	-	-	PUNCT
ijpds-4231	148	33	39.3oc	39.3oc	NOUN
ijpds-4231	148	34	.	.	PUNCT
ijpds-4231	149	1	it	it	PRON
ijpds-4231	149	2	was	be	AUX
ijpds-4231	149	3	then	then	ADV
ijpds-4231	149	4	treated	treat	VERB
ijpds-4231	149	5	with	with	ADP
ijpds-4231	149	6	tannic	tannic	ADJ
ijpds-4231	149	7	acid	acid	NOUN
ijpds-4231	149	8	solution	solution	NOUN
ijpds-4231	149	9	in	in	ADP
ijpds-4231	149	10	various	various	ADJ
ijpds-4231	149	11	methods	method	NOUN
ijpds-4231	149	12	to	to	PART
ijpds-4231	149	13	isolate	isolate	VERB
ijpds-4231	149	14	the	the	DET
ijpds-4231	149	15	tannate	tannate	NOUN
ijpds-4231	149	16	salt	salt	NOUN
ijpds-4231	149	17	.	.	PUNCT
ijpds-4231	150	1	an	an	DET
ijpds-4231	150	2	improved	improve	VERB
ijpds-4231	150	3	rasagiline	rasagiline	NOUN
ijpds-4231	150	4	tannate	tannate	NOUN
ijpds-4231	150	5	salt	salt	NOUN
ijpds-4231	150	6	formation	formation	NOUN
ijpds-4231	150	7	was	be	AUX
ijpds-4231	150	8	observed	observe	VERB
ijpds-4231	150	9	in	in	ADP
ijpds-4231	150	10	polar	polar	ADJ
ijpds-4231	150	11	solvents	solvent	NOUN
ijpds-4231	150	12	than	than	ADP
ijpds-4231	150	13	in	in	ADP
ijpds-4231	150	14	non	non	ADJ
ijpds-4231	150	15	-	-	ADJ
ijpds-4231	150	16	polar	polar	ADJ
ijpds-4231	150	17	solvents	solvent	NOUN
ijpds-4231	150	18	(	(	PUNCT
ijpds-4231	150	19	ethyl	ethyl	PROPN
ijpds-4231	150	20	acetate	acetate	NOUN
ijpds-4231	150	21	and	and	CCONJ
ijpds-4231	150	22	hexane	hexane	NOUN
ijpds-4231	150	23	)	)	PUNCT
ijpds-4231	151	1	[	[	X
ijpds-4231	151	2	25	25	NUM
ijpds-4231	151	3	]	]	PUNCT
ijpds-4231	151	4	.	.	PUNCT
ijpds-4231	152	1	caigu	caigu	PROPN
ijpds-4231	152	2	h	h	PROPN
ijpds-4231	152	3	&	&	CCONJ
ijpds-4231	152	4	huimin	huimin	PROPN
ijpds-4231	152	5	h.	h.	PROPN
ijpds-4231	152	6	,	,	PUNCT
ijpds-4231	152	7	in	in	ADP
ijpds-4231	152	8	2009	2009	NUM
ijpds-4231	152	9	,	,	PUNCT
ijpds-4231	152	10	had	have	AUX
ijpds-4231	152	11	reported	report	VERB
ijpds-4231	152	12	the	the	DET
ijpds-4231	152	13	process	process	NOUN
ijpds-4231	152	14	to	to	PART
ijpds-4231	152	15	isolate	isolate	VERB
ijpds-4231	152	16	the	the	DET
ijpds-4231	152	17	crystal	crystal	NOUN
ijpds-4231	152	18	form	form	NOUN
ijpds-4231	152	19	-	-	PUNCT
ijpds-4231	152	20	i	i	PRON
ijpds-4231	152	21	of	of	ADP
ijpds-4231	152	22	1	1	NUM
ijpds-4231	152	23	.	.	PUNCT
ijpds-4231	153	1	it	it	PRON
ijpds-4231	153	2	was	be	AUX
ijpds-4231	153	3	prepared	prepare	VERB
ijpds-4231	153	4	by	by	ADP
ijpds-4231	153	5	taking	take	VERB
ijpds-4231	153	6	1	1	NUM
ijpds-4231	153	7	in	in	ADP
ijpds-4231	153	8	(	(	PUNCT
ijpds-4231	153	9	ethyl	ethyl	PROPN
ijpds-4231	153	10	acetate	acetate	PROPN
ijpds-4231	153	11	/	/	SYM
ijpds-4231	153	12	ethyl	ethyl	PROPN
ijpds-4231	153	13	alcohol	alcohol	PROPN
ijpds-4231	153	14	)	)	PUNCT
ijpds-4231	153	15	or	or	CCONJ
ijpds-4231	153	16	(	(	PUNCT
ijpds-4231	153	17	acetone	acetone	NOUN
ijpds-4231	153	18	/	/	SYM
ijpds-4231	153	19	ethyl	ethyl	PROPN
ijpds-4231	153	20	alcohol	alcohol	PROPN
ijpds-4231	153	21	)	)	PUNCT
ijpds-4231	153	22	or	or	CCONJ
ijpds-4231	153	23	acetonitrile	acetonitrile	NOUN
ijpds-4231	153	24	or	or	CCONJ
ijpds-4231	153	25	isopropyl	isopropyl	NOUN
ijpds-4231	153	26	alcohol	alcohol	NOUN
ijpds-4231	153	27	.	.	PUNCT
ijpds-4231	154	1	the	the	DET
ijpds-4231	154	2	isolated	isolate	VERB
ijpds-4231	154	3	solid	solid	NOUN
ijpds-4231	154	4	had	have	AUX
ijpds-4231	154	5	exhibited	exhibit	VERB
ijpds-4231	154	6	a	a	DET
ijpds-4231	154	7	prominent	prominent	ADJ
ijpds-4231	154	8	dsc	dsc	NOUN
ijpds-4231	154	9	endotherm	endotherm	NOUN
ijpds-4231	154	10	at	at	ADP
ijpds-4231	154	11	157	157	NUM
ijpds-4231	154	12	-	-	SYM
ijpds-4231	154	13	157.5oc	157.5oc	NUM
ijpds-4231	154	14	[	[	X
ijpds-4231	154	15	26	26	NUM
ijpds-4231	154	16	]	]	PUNCT
ijpds-4231	154	17	.	.	PUNCT
ijpds-4231	155	1	stephen	stephen	PROPN
ijpds-4231	155	2	bdw	bdw	PROPN
ijpds-4231	155	3	.	.	PROPN
ijpds-4231	155	4	,	,	PUNCT
ijpds-4231	155	5	in	in	ADP
ijpds-4231	155	6	2009	2009	NUM
ijpds-4231	155	7	,	,	PUNCT
ijpds-4231	155	8	had	have	AUX
ijpds-4231	155	9	reported	report	VERB
ijpds-4231	155	10	the	the	DET
ijpds-4231	155	11	synthetic	synthetic	ADJ
ijpds-4231	155	12	pathway	pathway	NOUN
ijpds-4231	155	13	to	to	PART
ijpds-4231	155	14	isolate	isolate	VERB
ijpds-4231	155	15	the	the	DET
ijpds-4231	155	16	crystal	crystal	NOUN
ijpds-4231	155	17	form	form	NOUN
ijpds-4231	155	18	-	-	PUNCT
ijpds-4231	155	19	i	i	PRON
ijpds-4231	155	20	of	of	ADP
ijpds-4231	155	21	1	1	NUM
ijpds-4231	155	22	.	.	PUNCT
ijpds-4231	156	1	the	the	DET
ijpds-4231	156	2	work	work	NOUN
ijpds-4231	156	3	had	have	AUX
ijpds-4231	156	4	employed	employ	VERB
ijpds-4231	156	5	various	various	ADJ
ijpds-4231	156	6	solvents	solvent	NOUN
ijpds-4231	156	7	to	to	PART
ijpds-4231	156	8	dissolve	dissolve	VERB
ijpds-4231	156	9	1	1	NUM
ijpds-4231	156	10	and	and	CCONJ
ijpds-4231	156	11	isolate	isolate	VERB
ijpds-4231	156	12	the	the	DET
ijpds-4231	156	13	crystal	crystal	NOUN
ijpds-4231	156	14	form	form	NOUN
ijpds-4231	156	15	-	-	PUNCT
ijpds-4231	156	16	i	i	PRON
ijpds-4231	156	17	at	at	ADP
ijpds-4231	156	18	25	25	NUM
ijpds-4231	156	19	-	-	PUNCT
ijpds-4231	156	20	70oc	70oc	NOUN
ijpds-4231	157	1	[	[	X
ijpds-4231	157	2	27	27	NUM
ijpds-4231	157	3	]	]	PUNCT
ijpds-4231	157	4	.	.	PUNCT
ijpds-4231	158	1	patil	patil	PROPN
ijpds-4231	158	2	ns	ns	PROPN
ijpds-4231	158	3	,	,	PUNCT
ijpds-4231	158	4	et	et	PROPN
ijpds-4231	158	5	al	al	PROPN
ijpds-4231	158	6	.	.	PROPN
ijpds-4231	158	7	,	,	PUNCT
ijpds-4231	158	8	in	in	ADP
ijpds-4231	158	9	2009	2009	NUM
ijpds-4231	158	10	,	,	PUNCT
ijpds-4231	158	11	had	have	AUX
ijpds-4231	158	12	demonstrated	demonstrate	VERB
ijpds-4231	158	13	a	a	DET
ijpds-4231	158	14	process	process	NOUN
ijpds-4231	158	15	to	to	PART
ijpds-4231	158	16	prepare	prepare	VERB
ijpds-4231	158	17	1	1	NUM
ijpds-4231	158	18	with	with	ADP
ijpds-4231	158	19	90	90	NUM
ijpds-4231	158	20	volumepercent	volumepercent	NOUN
ijpds-4231	158	21	of	of	ADP
ijpds-4231	158	22	the	the	DET
ijpds-4231	158	23	particles	particle	NOUN
ijpds-4231	158	24	(	(	PUNCT
ijpds-4231	158	25	d-90	d-90	ADV
ijpds-4231	158	26	)	)	PUNCT
ijpds-4231	158	27	with	with	ADP
ijpds-4231	158	28	a	a	DET
ijpds-4231	158	29	size	size	NOUN
ijpds-4231	158	30	of	of	ADP
ijpds-4231	158	31	about	about	ADP
ijpds-4231	158	32	(	(	PUNCT
ijpds-4231	158	33	6001500	6001500	NUM
ijpds-4231	158	34	microns	micron	NOUN
ijpds-4231	158	35	)	)	PUNCT
ijpds-4231	158	36	and	and	CCONJ
ijpds-4231	158	37	(	(	PUNCT
ijpds-4231	158	38	255	255	NUM
ijpds-4231	158	39	-	-	SYM
ijpds-4231	158	40	1500	1500	NUM
ijpds-4231	158	41	microns	micron	NOUN
ijpds-4231	158	42	)	)	PUNCT
ijpds-4231	158	43	.	.	PUNCT
ijpds-4231	159	1	it	it	PRON
ijpds-4231	159	2	was	be	AUX
ijpds-4231	159	3	prepared	prepare	VERB
ijpds-4231	159	4	from	from	ADP
ijpds-4231	159	5	1	1	NUM
ijpds-4231	159	6	or	or	CCONJ
ijpds-4231	159	7	rasagiline	rasagiline	NOUN
ijpds-4231	159	8	base	base	NOUN
ijpds-4231	159	9	using	use	VERB
ijpds-4231	159	10	the	the	DET
ijpds-4231	159	11	suitable	suitable	ADJ
ijpds-4231	159	12	solvents	solvent	NOUN
ijpds-4231	159	13	[	[	X
ijpds-4231	159	14	28	28	NUM
ijpds-4231	159	15	]	]	PUNCT
ijpds-4231	159	16	.	.	PUNCT
ijpds-4231	160	1	s	s	PART
ijpds-4231	160	2	o	o	X
ijpds-4231	160	3	o	o	X
ijpds-4231	160	4	cl	cl	NOUN
ijpds-4231	161	1	n	n	NOUN
ijpds-4231	161	2	o	o	NOUN
ijpds-4231	161	3	o	o	NOUN
ijpds-4231	162	1	23	23	NUM
ijpds-4231	162	2	nh	nh	INTJ
ijpds-4231	163	1	so	so	ADV
ijpds-4231	163	2	o	o	PROPN
ijpds-4231	163	3	n	n	CCONJ
ijpds-4231	163	4	o	o	NOUN
ijpds-4231	163	5	o	o	NOUN
ijpds-4231	163	6	24	24	NUM
ijpds-4231	164	1	n	n	NOUN
ijpds-4231	164	2	so	so	ADV
ijpds-4231	164	3	o	o	PROPN
ijpds-4231	165	1	n	n	CCONJ
ijpds-4231	165	2	o	o	NOUN
ijpds-4231	165	3	o	o	NOUN
ijpds-4231	165	4	25	25	NUM
ijpds-4231	165	5	sanjay	sanjay	NOUN
ijpds-4231	165	6	s	s	PART
ijpds-4231	165	7	s	s	NOUN
ijpds-4231	165	8	patents	patent	NOUN
ijpds-4231	165	9	disclosed	disclose	VERB
ijpds-4231	165	10	synthetic	synthetic	ADJ
ijpds-4231	165	11	overview	overview	NOUN
ijpds-4231	165	12	of	of	ADP
ijpds-4231	165	13	rasagiline	rasagiline	ADJ
ijpds-4231	165	14	vol	vol	NOUN
ijpds-4231	165	15	2	2	NUM
ijpds-4231	165	16	|	|	ADV
ijpds-4231	165	17	issue	issue	VERB
ijpds-4231	165	18	4	4	NUM
ijpds-4231	165	19	|	|	ADV
ijpds-4231	165	20	oct	oct	PROPN
ijpds-4231	165	21	–	–	PUNCT
ijpds-4231	165	22	dec	dec	PROPN
ijpds-4231	165	23	2023	2023	NUM
ijpds-4231	165	24	indian	indian	PROPN
ijpds-4231	165	25	j	j	PROPN
ijpds-4231	165	26	pharm	pharm	PROPN
ijpds-4231	165	27	drug	drug	PROPN
ijpds-4231	165	28	studies	study	NOUN
ijpds-4231	165	29	|	|	ADV
ijpds-4231	165	30	136	136	NUM
ijpds-4231	165	31	qiandong	qiandong	NOUN
ijpds-4231	165	32	l	l	NOUN
ijpds-4231	165	33	,	,	PUNCT
ijpds-4231	165	34	et	et	PROPN
ijpds-4231	165	35	al	al	PROPN
ijpds-4231	165	36	.	.	PROPN
ijpds-4231	165	37	,	,	PUNCT
ijpds-4231	165	38	in	in	ADP
ijpds-4231	165	39	2009	2009	NUM
ijpds-4231	165	40	,	,	PUNCT
ijpds-4231	165	41	had	have	AUX
ijpds-4231	165	42	demonstrated	demonstrate	VERB
ijpds-4231	165	43	the	the	DET
ijpds-4231	165	44	condensation	condensation	NOUN
ijpds-4231	165	45	of	of	ADP
ijpds-4231	165	46	r	r	NOUN
ijpds-4231	165	47	-	-	PUNCT
ijpds-4231	165	48	isomer	isomer	NOUN
ijpds-4231	165	49	of	of	ADP
ijpds-4231	165	50	2	2	NUM
ijpds-4231	165	51	in	in	ADP
ijpds-4231	165	52	dichloromethane	dichloromethane	NOUN
ijpds-4231	165	53	with	with	ADP
ijpds-4231	165	54	onitro	onitro	NOUN
ijpds-4231	165	55	-	-	PUNCT
ijpds-4231	165	56	benzene	benzene	NOUN
ijpds-4231	165	57	-	-	PUNCT
ijpds-4231	165	58	sulfonyl	sulfonyl	NOUN
ijpds-4231	165	59	chloride	chloride	NOUN
ijpds-4231	165	60	23	23	NUM
ijpds-4231	165	61	in	in	ADP
ijpds-4231	165	62	the	the	DET
ijpds-4231	165	63	presence	presence	NOUN
ijpds-4231	165	64	of	of	ADP
ijpds-4231	165	65	triethylamine	triethylamine	NOUN
ijpds-4231	165	66	to	to	PART
ijpds-4231	165	67	isolate	isolate	VERB
ijpds-4231	165	68	r	r	NOUN
ijpds-4231	165	69	-	-	PUNCT
ijpds-4231	165	70	n-(2	n-(2	NOUN
ijpds-4231	165	71	-	-	PUNCT
ijpds-4231	165	72	nitro	nitro	NOUN
ijpds-4231	165	73	)	)	PUNCT
ijpds-4231	165	74	benzenesulfonyl-1indenamine	benzenesulfonyl-1indenamine	PROPN
ijpds-4231	165	75	24	24	NUM
ijpds-4231	165	76	(	(	PUNCT
ijpds-4231	165	77	yield	yield	NOUN
ijpds-4231	165	78	:	:	PUNCT
ijpds-4231	165	79	95	95	NUM
ijpds-4231	165	80	%	%	NOUN
ijpds-4231	165	81	,	,	PUNCT
ijpds-4231	165	82	as	as	ADP
ijpds-4231	165	83	white	white	X
ijpds-4231	165	84	solid	solid	ADJ
ijpds-4231	165	85	)	)	PUNCT
ijpds-4231	165	86	.	.	PUNCT
ijpds-4231	166	1	it	it	PRON
ijpds-4231	166	2	was	be	AUX
ijpds-4231	166	3	dissolved	dissolve	VERB
ijpds-4231	166	4	in	in	ADP
ijpds-4231	166	5	toluene	toluene	NOUN
ijpds-4231	166	6	and	and	CCONJ
ijpds-4231	166	7	treated	treat	VERB
ijpds-4231	166	8	with	with	ADP
ijpds-4231	166	9	3	3	NUM
ijpds-4231	166	10	in	in	ADP
ijpds-4231	166	11	the	the	DET
ijpds-4231	166	12	presence	presence	NOUN
ijpds-4231	166	13	of	of	ADP
ijpds-4231	166	14	sodium	sodium	NOUN
ijpds-4231	166	15	hydroxide	hydroxide	NOUN
ijpds-4231	166	16	and	and	CCONJ
ijpds-4231	166	17	catalytic	catalytic	ADJ
ijpds-4231	166	18	amount	amount	NOUN
ijpds-4231	166	19	of	of	ADP
ijpds-4231	166	20	tetrabutylammonium	tetrabutylammonium	NOUN
ijpds-4231	166	21	bromide	bromide	NOUN
ijpds-4231	166	22	to	to	PART
ijpds-4231	166	23	get	get	VERB
ijpds-4231	166	24	r	r	NOUN
ijpds-4231	166	25	-	-	PUNCT
ijpds-4231	166	26	n	n	CCONJ
ijpds-4231	166	27	-	-	PUNCT
ijpds-4231	166	28	propargyl	propargyl	NOUN
ijpds-4231	166	29	-	-	PUNCT
ijpds-4231	166	30	n-(2nitro)-benzenesulfonyl-1	n-(2nitro)-benzenesulfonyl-1	NOUN
ijpds-4231	166	31	-	-	PUNCT
ijpds-4231	166	32	indenamine	indenamine	NOUN
ijpds-4231	166	33	25	25	NUM
ijpds-4231	166	34	(	(	PUNCT
ijpds-4231	166	35	yield	yield	NOUN
ijpds-4231	166	36	:	:	PUNCT
ijpds-4231	166	37	81	81	NUM
ijpds-4231	166	38	%	%	NOUN
ijpds-4231	166	39	,	,	PUNCT
ijpds-4231	166	40	as	as	ADP
ijpds-4231	166	41	pale	pale	ADJ
ijpds-4231	166	42	yellow	yellow	NOUN
ijpds-4231	166	43	solid	solid	ADJ
ijpds-4231	166	44	)	)	PUNCT
ijpds-4231	166	45	.	.	PUNCT
ijpds-4231	167	1	n	n	CCONJ
ijpds-4231	167	2	,	,	PUNCT
ijpds-4231	167	3	n	n	CCONJ
ijpds-4231	167	4	-	-	PUNCT
ijpds-4231	167	5	dimethylformamide	dimethylformamide	NOUN
ijpds-4231	167	6	,	,	PUNCT
ijpds-4231	167	7	lithium	lithium	NOUN
ijpds-4231	167	8	hydroxide	hydroxide	NOUN
ijpds-4231	167	9	monohydrate	monohydrate	NOUN
ijpds-4231	167	10	and	and	CCONJ
ijpds-4231	167	11	mercapto	mercapto	NOUN
ijpds-4231	167	12	-	-	PUNCT
ijpds-4231	167	13	propionic	propionic	ADJ
ijpds-4231	167	14	acid	acid	NOUN
ijpds-4231	167	15	were	be	AUX
ijpds-4231	167	16	added	add	VERB
ijpds-4231	167	17	to	to	ADP
ijpds-4231	167	18	25	25	NUM
ijpds-4231	167	19	to	to	PART
ijpds-4231	167	20	isolate	isolate	VERB
ijpds-4231	167	21	r	r	NOUN
ijpds-4231	167	22	-	-	PUNCT
ijpds-4231	167	23	rasagiline	rasagiline	NOUN
ijpds-4231	167	24	base	base	NOUN
ijpds-4231	167	25	(	(	PUNCT
ijpds-4231	167	26	yield	yield	NOUN
ijpds-4231	167	27	:	:	PUNCT
ijpds-4231	167	28	96	96	NUM
ijpds-4231	167	29	%	%	NOUN
ijpds-4231	167	30	,	,	PUNCT
ijpds-4231	167	31	as	as	ADV
ijpds-4231	167	32	yellow	yellow	ADJ
ijpds-4231	167	33	oily	oily	ADJ
ijpds-4231	167	34	liquid	liquid	NOUN
ijpds-4231	167	35	)	)	PUNCT
ijpds-4231	167	36	.	.	PUNCT
ijpds-4231	168	1	the	the	DET
ijpds-4231	168	2	work	work	NOUN
ijpds-4231	168	3	had	have	AUX
ijpds-4231	168	4	also	also	ADV
ijpds-4231	168	5	reported	report	VERB
ijpds-4231	168	6	the	the	DET
ijpds-4231	168	7	use	use	NOUN
ijpds-4231	168	8	of	of	ADP
ijpds-4231	168	9	racemic	racemic	ADJ
ijpds-4231	168	10	2	2	NUM
ijpds-4231	168	11	for	for	ADP
ijpds-4231	168	12	the	the	DET
ijpds-4231	168	13	above	above	ADJ
ijpds-4231	168	14	steps	step	NOUN
ijpds-4231	168	15	to	to	PART
ijpds-4231	168	16	get	get	VERB
ijpds-4231	168	17	racemic	racemic	ADJ
ijpds-4231	168	18	rasagiline	rasagiline	NOUN
ijpds-4231	168	19	base	base	NOUN
ijpds-4231	168	20	,	,	PUNCT
ijpds-4231	168	21	which	which	PRON
ijpds-4231	168	22	was	be	AUX
ijpds-4231	168	23	treated	treat	VERB
ijpds-4231	168	24	with	with	ADP
ijpds-4231	168	25	l	l	ADJ
ijpds-4231	168	26	-	-	ADJ
ijpds-4231	168	27	tartaric	tartaric	ADJ
ijpds-4231	168	28	acid	acid	NOUN
ijpds-4231	168	29	in	in	ADP
ijpds-4231	168	30	isopropyl	isopropyl	NOUN
ijpds-4231	168	31	alcohol	alcohol	NOUN
ijpds-4231	168	32	to	to	PART
ijpds-4231	168	33	isolate	isolate	VERB
ijpds-4231	168	34	the	the	DET
ijpds-4231	168	35	salt	salt	NOUN
ijpds-4231	168	36	.	.	PUNCT
ijpds-4231	169	1	it	it	PRON
ijpds-4231	169	2	was	be	AUX
ijpds-4231	169	3	dissociated	dissociate	VERB
ijpds-4231	169	4	further	far	ADV
ijpds-4231	169	5	to	to	PART
ijpds-4231	169	6	isolate	isolate	VERB
ijpds-4231	169	7	the	the	DET
ijpds-4231	169	8	r	r	NOUN
ijpds-4231	169	9	-	-	PUNCT
ijpds-4231	169	10	rasagiline	rasagiline	NOUN
ijpds-4231	169	11	base	base	NOUN
ijpds-4231	169	12	(	(	PUNCT
ijpds-4231	169	13	as	as	ADP
ijpds-4231	169	14	yellow	yellow	ADJ
ijpds-4231	169	15	brown	brown	ADJ
ijpds-4231	169	16	oil	oil	NOUN
ijpds-4231	169	17	)	)	PUNCT
ijpds-4231	170	1	[	[	X
ijpds-4231	170	2	29	29	NUM
ijpds-4231	170	3	]	]	PUNCT
ijpds-4231	170	4	.	.	PUNCT
ijpds-4231	171	1	huang	huang	PROPN
ijpds-4231	171	2	c	c	PROPN
ijpds-4231	171	3	&	&	CCONJ
ijpds-4231	171	4	he	he	PRON
ijpds-4231	171	5	h	h	VERB
ijpds-4231	171	6	,	,	PUNCT
ijpds-4231	171	7	in	in	ADP
ijpds-4231	171	8	2009	2009	NUM
ijpds-4231	171	9	,	,	PUNCT
ijpds-4231	171	10	had	have	AUX
ijpds-4231	171	11	disclosed	disclose	VERB
ijpds-4231	171	12	the	the	DET
ijpds-4231	171	13	preparation	preparation	NOUN
ijpds-4231	171	14	of	of	ADP
ijpds-4231	171	15	form	form	NOUN
ijpds-4231	171	16	-	-	PUNCT
ijpds-4231	171	17	i	i	PRON
ijpds-4231	171	18	of	of	ADP
ijpds-4231	171	19	1	1	NUM
ijpds-4231	171	20	from	from	ADP
ijpds-4231	171	21	various	various	ADJ
ijpds-4231	171	22	solvents	solvent	NOUN
ijpds-4231	171	23	like	like	ADP
ijpds-4231	171	24	isopropyl	isopropyl	NOUN
ijpds-4231	171	25	alcohol	alcohol	PROPN
ijpds-4231	171	26	,	,	PUNCT
ijpds-4231	171	27	ethyl	ethyl	PROPN
ijpds-4231	171	28	alcohol	alcohol	PROPN
ijpds-4231	171	29	,	,	PUNCT
ijpds-4231	171	30	acetone	acetone	NOUN
ijpds-4231	171	31	,	,	PUNCT
ijpds-4231	171	32	ethyl	ethyl	PROPN
ijpds-4231	171	33	acetate	acetate	NOUN
ijpds-4231	171	34	and	and	CCONJ
ijpds-4231	171	35	acetonitrile	acetonitrile	NOUN
ijpds-4231	171	36	.	.	PUNCT
ijpds-4231	172	1	the	the	DET
ijpds-4231	172	2	crystal	crystal	NOUN
ijpds-4231	172	3	form	form	NOUN
ijpds-4231	172	4	-	-	PUNCT
ijpds-4231	172	5	i	i	PRON
ijpds-4231	172	6	had	have	AUX
ijpds-4231	172	7	showed	show	VERB
ijpds-4231	172	8	the	the	DET
ijpds-4231	172	9	characteristic	characteristic	ADJ
ijpds-4231	172	10	endothermic	endothermic	NOUN
ijpds-4231	172	11	peak	peak	NOUN
ijpds-4231	172	12	at	at	ADP
ijpds-4231	172	13	about	about	ADV
ijpds-4231	172	14	157.07oc	157.07oc	NUM
ijpds-4231	172	15	[	[	SYM
ijpds-4231	172	16	30	30	NUM
ijpds-4231	172	17	]	]	PUNCT
ijpds-4231	172	18	.	.	PUNCT
ijpds-4231	173	1	cherukupally	cherukupally	ADV
ijpds-4231	173	2	p	p	X
ijpds-4231	173	3	,	,	PUNCT
ijpds-4231	173	4	et	et	PROPN
ijpds-4231	173	5	al	al	PROPN
ijpds-4231	173	6	.	.	PROPN
ijpds-4231	173	7	,	,	PUNCT
ijpds-4231	173	8	in	in	ADP
ijpds-4231	173	9	2010	2010	NUM
ijpds-4231	173	10	,	,	PUNCT
ijpds-4231	173	11	had	have	AUX
ijpds-4231	173	12	illustrated	illustrate	VERB
ijpds-4231	173	13	the	the	DET
ijpds-4231	173	14	reaction	reaction	NOUN
ijpds-4231	173	15	of	of	ADP
ijpds-4231	173	16	9	9	NUM
ijpds-4231	173	17	in	in	ADP
ijpds-4231	173	18	methyl	methyl	NOUN
ijpds-4231	173	19	alcohol	alcohol	NOUN
ijpds-4231	173	20	with	with	ADP
ijpds-4231	173	21	6	6	NUM
ijpds-4231	173	22	to	to	PART
ijpds-4231	173	23	isolate	isolate	VERB
ijpds-4231	173	24	hydrochloride	hydrochloride	NOUN
ijpds-4231	173	25	salt	salt	NOUN
ijpds-4231	173	26	of	of	ADP
ijpds-4231	173	27	(	(	PUNCT
ijpds-4231	173	28	1z)-n-(prop-2	1z)-n-(prop-2	NUM
ijpds-4231	173	29	-	-	PUNCT
ijpds-4231	173	30	yn-1	yn-1	NOUN
ijpds-4231	173	31	-	-	PUNCT
ijpds-4231	173	32	yl)-2,3	yl)-2,3	NOUN
ijpds-4231	173	33	-	-	PUNCT
ijpds-4231	173	34	dihydro-1h	dihydro-1h	NOUN
ijpds-4231	173	35	-	-	PUNCT
ijpds-4231	173	36	inden-1	inden-1	NOUN
ijpds-4231	173	37	-	-	PUNCT
ijpds-4231	173	38	imine	imine	ADJ
ijpds-4231	173	39	16	16	NUM
ijpds-4231	173	40	.	.	PUNCT
ijpds-4231	174	1	it	it	PRON
ijpds-4231	174	2	was	be	AUX
ijpds-4231	174	3	then	then	ADV
ijpds-4231	174	4	reduced	reduce	VERB
ijpds-4231	174	5	using	use	VERB
ijpds-4231	174	6	sodium	sodium	NOUN
ijpds-4231	174	7	borohydride	borohydride	NOUN
ijpds-4231	174	8	in	in	ADP
ijpds-4231	174	9	methyl	methyl	NOUN
ijpds-4231	174	10	alcohol	alcohol	NOUN
ijpds-4231	174	11	to	to	PART
ijpds-4231	174	12	get	get	VERB
ijpds-4231	174	13	the	the	DET
ijpds-4231	174	14	crude	crude	ADJ
ijpds-4231	174	15	racemic	racemic	ADJ
ijpds-4231	174	16	rasagiline	rasagiline	NOUN
ijpds-4231	174	17	base	base	NOUN
ijpds-4231	174	18	.	.	PUNCT
ijpds-4231	175	1	it	it	PRON
ijpds-4231	175	2	was	be	AUX
ijpds-4231	175	3	treated	treat	VERB
ijpds-4231	175	4	with	with	ADP
ijpds-4231	175	5	isopropyl	isopropyl	NOUN
ijpds-4231	175	6	alcohol	alcohol	PROPN
ijpds-4231	175	7	/	/	SYM
ijpds-4231	175	8	hcl	hcl	PROPN
ijpds-4231	175	9	(	(	PUNCT
ijpds-4231	175	10	18	18	NUM
ijpds-4231	175	11	%	%	NOUN
ijpds-4231	175	12	)	)	PUNCT
ijpds-4231	175	13	to	to	PART
ijpds-4231	175	14	get	get	VERB
ijpds-4231	175	15	the	the	DET
ijpds-4231	175	16	racemic	racemic	ADJ
ijpds-4231	175	17	rasagiline	rasagiline	NOUN
ijpds-4231	175	18	hydrochloride	hydrochloride	NOUN
ijpds-4231	175	19	.	.	PUNCT
ijpds-4231	176	1	moreover	moreover	ADV
ijpds-4231	176	2	,	,	PUNCT
ijpds-4231	176	3	the	the	DET
ijpds-4231	176	4	salt	salt	NOUN
ijpds-4231	176	5	cleavage	cleavage	NOUN
ijpds-4231	176	6	had	have	AUX
ijpds-4231	176	7	resulted	result	VERB
ijpds-4231	176	8	in	in	ADP
ijpds-4231	176	9	the	the	DET
ijpds-4231	176	10	formation	formation	NOUN
ijpds-4231	176	11	of	of	ADP
ijpds-4231	176	12	rasagiline	rasagiline	NOUN
ijpds-4231	176	13	base	base	NOUN
ijpds-4231	176	14	.	.	PUNCT
ijpds-4231	177	1	the	the	DET
ijpds-4231	177	2	work	work	NOUN
ijpds-4231	177	3	also	also	ADV
ijpds-4231	177	4	had	have	AUX
ijpds-4231	177	5	reported	report	VERB
ijpds-4231	177	6	the	the	DET
ijpds-4231	177	7	use	use	NOUN
ijpds-4231	177	8	of	of	ADP
ijpds-4231	177	9	a	a	DET
ijpds-4231	177	10	few	few	ADJ
ijpds-4231	177	11	suitable	suitable	ADJ
ijpds-4231	177	12	reducing	reduce	VERB
ijpds-4231	177	13	agents	agent	NOUN
ijpds-4231	177	14	like	like	ADP
ijpds-4231	177	15	raney	raney	NOUN
ijpds-4231	177	16	nickel	nickel	NOUN
ijpds-4231	177	17	,	,	PUNCT
ijpds-4231	177	18	palladium	palladium	NOUN
ijpds-4231	177	19	on	on	ADP
ijpds-4231	177	20	carbon	carbon	NOUN
ijpds-4231	177	21	,	,	PUNCT
ijpds-4231	177	22	and	and	CCONJ
ijpds-4231	177	23	platinum	platinum	NOUN
ijpds-4231	177	24	dioxide	dioxide	NOUN
ijpds-4231	177	25	;	;	PUNCT
ijpds-4231	177	26	lithium	lithium	NOUN
ijpds-4231	177	27	aluminium	aluminium	NOUN
ijpds-4231	177	28	hydride	hydride	NOUN
ijpds-4231	177	29	;	;	PUNCT
ijpds-4231	177	30	sodium	sodium	NOUN
ijpds-4231	177	31	borohydride	borohydride	NOUN
ijpds-4231	177	32	;	;	PUNCT
ijpds-4231	177	33	sodium	sodium	NOUN
ijpds-4231	177	34	cyanoborohydride	cyanoborohydride	NOUN
ijpds-4231	177	35	;	;	PUNCT
ijpds-4231	177	36	sodium	sodium	NOUN
ijpds-4231	177	37	borohydride	borohydride	NOUN
ijpds-4231	177	38	in	in	ADP
ijpds-4231	177	39	acidic	acidic	ADJ
ijpds-4231	177	40	conditions	condition	NOUN
ijpds-4231	177	41	;	;	PUNCT
ijpds-4231	177	42	and	and	CCONJ
ijpds-4231	177	43	sodium	sodium	NOUN
ijpds-4231	177	44	bis(2methoxyethoxy)-aluminum	bis(2methoxyethoxy)-aluminum	ADJ
ijpds-4231	177	45	hydride	hydride	NOUN
ijpds-4231	177	46	(	(	PUNCT
ijpds-4231	177	47	vitride	vitride	NOUN
ijpds-4231	177	48	®	®	PROPN
ijpds-4231	177	49	)	)	PUNCT
ijpds-4231	177	50	to	to	PART
ijpds-4231	177	51	isolate	isolate	VERB
ijpds-4231	177	52	16	16	NUM
ijpds-4231	177	53	in	in	ADP
ijpds-4231	177	54	reasonably	reasonably	ADV
ijpds-4231	177	55	high	high	ADJ
ijpds-4231	177	56	yields	yield	NOUN
ijpds-4231	177	57	.	.	PUNCT
ijpds-4231	178	1	a	a	DET
ijpds-4231	178	2	few	few	ADJ
ijpds-4231	178	3	suitable	suitable	ADJ
ijpds-4231	178	4	chiral	chiral	ADJ
ijpds-4231	178	5	resolving	resolve	VERB
ijpds-4231	178	6	agents	agent	NOUN
ijpds-4231	178	7	were	be	AUX
ijpds-4231	178	8	used	use	VERB
ijpds-4231	178	9	like	like	ADP
ijpds-4231	178	10	l-(+)-tartaric	l-(+)-tartaric	ADJ
ijpds-4231	178	11	acid	acid	NOUN
ijpds-4231	178	12	and	and	CCONJ
ijpds-4231	178	13	(	(	PUNCT
ijpds-4231	178	14	-)-di	-)-di	ADJ
ijpds-4231	178	15	-	-	ADJ
ijpds-4231	178	16	ptoluoyltartaric	ptoluoyltartaric	ADJ
ijpds-4231	178	17	acid	acid	NOUN
ijpds-4231	178	18	(	(	PUNCT
ijpds-4231	178	19	dptta	dptta	PROPN
ijpds-4231	178	20	)	)	PUNCT
ijpds-4231	178	21	to	to	PART
ijpds-4231	178	22	isolate	isolate	VERB
ijpds-4231	178	23	the	the	DET
ijpds-4231	178	24	required	require	VERB
ijpds-4231	178	25	risomer	risomer	NOUN
ijpds-4231	178	26	.	.	PUNCT
ijpds-4231	179	1	with	with	ADP
ijpds-4231	179	2	the	the	DET
ijpds-4231	179	3	use	use	NOUN
ijpds-4231	179	4	of	of	ADP
ijpds-4231	179	5	these	these	DET
ijpds-4231	179	6	reagents	reagent	NOUN
ijpds-4231	179	7	,	,	PUNCT
ijpds-4231	179	8	enantiomerically	enantiomerically	ADV
ijpds-4231	179	9	pure	pure	ADJ
ijpds-4231	179	10	salts	salt	NOUN
ijpds-4231	179	11	of	of	ADP
ijpds-4231	179	12	rasagiline	rasagiline	NOUN
ijpds-4231	179	13	(	(	PUNCT
ijpds-4231	179	14	hydrochloride	hydrochloride	NOUN
ijpds-4231	179	15	/	/	SYM
ijpds-4231	179	16	tartarate	tartarate	NOUN
ijpds-4231	179	17	/	/	SYM
ijpds-4231	179	18	mesylate	mesylate	NOUN
ijpds-4231	179	19	)	)	PUNCT
ijpds-4231	179	20	were	be	AUX
ijpds-4231	179	21	prepared	prepare	VERB
ijpds-4231	179	22	with	with	ADP
ijpds-4231	179	23	good	good	ADJ
ijpds-4231	179	24	yields	yield	NOUN
ijpds-4231	179	25	.	.	PUNCT
ijpds-4231	180	1	furthermore	furthermore	ADV
ijpds-4231	180	2	,	,	PUNCT
ijpds-4231	180	3	the	the	DET
ijpds-4231	180	4	work	work	NOUN
ijpds-4231	180	5	provides	provide	VERB
ijpds-4231	180	6	a	a	DET
ijpds-4231	180	7	process	process	NOUN
ijpds-4231	180	8	for	for	ADP
ijpds-4231	180	9	the	the	DET
ijpds-4231	180	10	preparation	preparation	NOUN
ijpds-4231	180	11	of	of	ADP
ijpds-4231	180	12	1	1	NUM
ijpds-4231	180	13	having	have	VERB
ijpds-4231	180	14	d90	d90	NOUN
ijpds-4231	180	15	below	below	ADP
ijpds-4231	180	16	6	6	NUM
ijpds-4231	180	17	μm	μm	NOUN
ijpds-4231	180	18	.	.	PUNCT
ijpds-4231	181	1	it	it	PRON
ijpds-4231	181	2	was	be	AUX
ijpds-4231	181	3	done	do	VERB
ijpds-4231	181	4	by	by	ADP
ijpds-4231	181	5	adding	add	VERB
ijpds-4231	181	6	the	the	DET
ijpds-4231	181	7	solution	solution	NOUN
ijpds-4231	181	8	of	of	ADP
ijpds-4231	181	9	1	1	NUM
ijpds-4231	181	10	in	in	ADP
ijpds-4231	181	11	isopropyl	isopropyl	NOUN
ijpds-4231	181	12	alcohol	alcohol	NOUN
ijpds-4231	181	13	to	to	ADP
ijpds-4231	181	14	chilled	chill	VERB
ijpds-4231	181	15	methyl	methyl	NOUN
ijpds-4231	181	16	-	-	PUNCT
ijpds-4231	181	17	t	t	NOUN
ijpds-4231	181	18	-	-	PUNCT
ijpds-4231	181	19	butyl	butyl	NOUN
ijpds-4231	181	20	ether	ether	NOUN
ijpds-4231	181	21	.	.	PUNCT
ijpds-4231	182	1	the	the	DET
ijpds-4231	182	2	work	work	NOUN
ijpds-4231	182	3	involved	involve	VERB
ijpds-4231	182	4	the	the	DET
ijpds-4231	182	5	isolation	isolation	NOUN
ijpds-4231	182	6	of	of	ADP
ijpds-4231	182	7	rasagiline	rasagiline	NOUN
ijpds-4231	182	8	&	&	CCONJ
ijpds-4231	182	9	its	its	PRON
ijpds-4231	182	10	salts	salt	NOUN
ijpds-4231	182	11	which	which	PRON
ijpds-4231	182	12	are	be	AUX
ijpds-4231	182	13	significantly	significantly	ADV
ijpds-4231	182	14	free	free	ADJ
ijpds-4231	182	15	from	from	ADP
ijpds-4231	182	16	the	the	DET
ijpds-4231	182	17	critical	critical	ADJ
ijpds-4231	182	18	impurities	impurity	NOUN
ijpds-4231	182	19	like	like	ADP
ijpds-4231	182	20	n	n	CCONJ
ijpds-4231	182	21	,	,	PUNCT
ijpds-4231	182	22	ndi(prop-2	ndi(prop-2	PROPN
ijpds-4231	182	23	-	-	PUNCT
ijpds-4231	182	24	yn-1	yn-1	NOUN
ijpds-4231	182	25	-	-	PUNCT
ijpds-4231	182	26	yl)-2,3	yl)-2,3	NOUN
ijpds-4231	182	27	-	-	PUNCT
ijpds-4231	182	28	dihydro-1h	dihydro-1h	NOUN
ijpds-4231	182	29	-	-	PUNCT
ijpds-4231	182	30	inden-1	inden-1	NOUN
ijpds-4231	182	31	-	-	PUNCT
ijpds-4231	182	32	amine	amine	ADJ
ijpds-4231	182	33	4	4	NUM
ijpds-4231	182	34	,	,	PUNCT
ijpds-4231	182	35	n(prop-2	n(prop-2	NOUN
ijpds-4231	182	36	-	-	PUNCT
ijpds-4231	182	37	en-1	en-1	ADV
ijpds-4231	182	38	-	-	PUNCT
ijpds-4231	182	39	yl)-2,3	yl)-2,3	PROPN
ijpds-4231	182	40	-	-	PROPN
ijpds-4231	182	41	dihydro-1h	dihydro-1h	NOUN
ijpds-4231	182	42	-	-	PUNCT
ijpds-4231	182	43	inden-1	inden-1	NOUN
ijpds-4231	182	44	-	-	PUNCT
ijpds-4231	182	45	amine	amine	ADJ
ijpds-4231	182	46	17	17	NUM
ijpds-4231	182	47	,	,	PUNCT
ijpds-4231	182	48	npropyl-2,3	npropyl-2,3	PROPN
ijpds-4231	182	49	-	-	PUNCT
ijpds-4231	182	50	dihydro-1h	dihydro-1h	NOUN
ijpds-4231	182	51	-	-	PUNCT
ijpds-4231	182	52	inden-1	inden-1	NOUN
ijpds-4231	182	53	-	-	PUNCT
ijpds-4231	182	54	amine	amine	ADJ
ijpds-4231	182	55	18	18	NUM
ijpds-4231	182	56	&	&	CCONJ
ijpds-4231	182	57	3-(prop-2	3-(prop-2	PROPN
ijpds-4231	182	58	-	-	PUNCT
ijpds-4231	182	59	yn1	yn1	NOUN
ijpds-4231	182	60	-	-	PUNCT
ijpds-4231	182	61	ylamino)-2,3	ylamino)-2,3	ADJ
ijpds-4231	182	62	-	-	PROPN
ijpds-4231	182	63	dihydro-1h	dihydro-1h	NOUN
ijpds-4231	182	64	-	-	PUNCT
ijpds-4231	182	65	inden-1	inden-1	NOUN
ijpds-4231	182	66	-	-	PUNCT
ijpds-4231	182	67	one	one	NUM
ijpds-4231	182	68	19	19	NUM
ijpds-4231	182	69	[	[	X
ijpds-4231	182	70	31	31	NUM
ijpds-4231	182	71	]	]	PUNCT
ijpds-4231	182	72	.	.	PUNCT
ijpds-4231	183	1	o	o	NOUN
ijpds-4231	184	1	oh	oh	INTJ
ijpds-4231	185	1	26	26	NUM
ijpds-4231	185	2	s	s	NOUN
ijpds-4231	185	3	o	o	NOUN
ijpds-4231	185	4	nh2	nh2	NOUN
ijpds-4231	185	5	30	30	NUM
ijpds-4231	185	6	nh	nh	PROPN
ijpds-4231	185	7	s	s	PART
ijpds-4231	185	8	o	o	NOUN
ijpds-4231	185	9	31	31	NUM
ijpds-4231	185	10	n	n	PROPN
ijpds-4231	185	11	s	s	PART
ijpds-4231	185	12	o	o	NOUN
ijpds-4231	185	13	32	32	NUM
ijpds-4231	185	14	br	br	NOUN
ijpds-4231	185	15	27	27	NUM
ijpds-4231	185	16	nh28	nh28	PROPN
ijpds-4231	186	1	oh	oh	INTJ
ijpds-4231	187	1	oh	oh	INTJ
ijpds-4231	187	2	o	o	INTJ
ijpds-4231	188	1	o	o	INTJ
ijpds-4231	188	2	nh	nh	INTJ
ijpds-4231	188	3	br	br	NOUN
ijpds-4231	188	4	br	br	PROPN
ijpds-4231	188	5	29	29	NUM
ijpds-4231	188	6	br	br	PROPN
ijpds-4231	188	7	nh	nh	PROPN
ijpds-4231	188	8	nh	nh	PROPN
ijpds-4231	188	9	br	br	PROPN
ijpds-4231	188	10	33	33	NUM
ijpds-4231	188	11	34	34	NUM
ijpds-4231	188	12	marras	marra	NOUN
ijpds-4231	188	13	g	g	PROPN
ijpds-4231	188	14	,	,	PUNCT
ijpds-4231	188	15	et	et	PROPN
ijpds-4231	188	16	al	al	PROPN
ijpds-4231	188	17	.	.	PROPN
ijpds-4231	188	18	,	,	PUNCT
ijpds-4231	188	19	in	in	ADP
ijpds-4231	188	20	2010	2010	NUM
ijpds-4231	188	21	,	,	PUNCT
ijpds-4231	188	22	had	have	AUX
ijpds-4231	188	23	disclosed	disclose	VERB
ijpds-4231	188	24	a	a	DET
ijpds-4231	188	25	multi	multi	ADJ
ijpds-4231	188	26	-	-	ADJ
ijpds-4231	188	27	step	step	ADJ
ijpds-4231	188	28	process	process	NOUN
ijpds-4231	188	29	starting	start	VERB
ijpds-4231	188	30	from	from	ADP
ijpds-4231	188	31	(	(	PUNCT
ijpds-4231	188	32	±)-2	±)-2	PROPN
ijpds-4231	188	33	,	,	PUNCT
ijpds-4231	188	34	3	3	NUM
ijpds-4231	188	35	-	-	PUNCT
ijpds-4231	188	36	dihydro	dihydro	NOUN
ijpds-4231	188	37	-	-	PUNCT
ijpds-4231	188	38	lh	lh	NOUN
ijpds-4231	188	39	-	-	PUNCT
ijpds-4231	188	40	indene	indene	NOUN
ijpds-4231	188	41	-	-	PUNCT
ijpds-4231	188	42	lcarboxylic	lcarboxylic	ADJ
ijpds-4231	188	43	acid	acid	NOUN
ijpds-4231	188	44	26	26	NUM
ijpds-4231	188	45	to	to	PART
ijpds-4231	188	46	isolate	isolate	VERB
ijpds-4231	188	47	r	r	NOUN
ijpds-4231	188	48	-	-	PUNCT
ijpds-4231	188	49	rasagiline	rasagiline	NOUN
ijpds-4231	188	50	base	base	NOUN
ijpds-4231	188	51	(	(	PUNCT
ijpds-4231	188	52	as	as	ADP
ijpds-4231	188	53	light	light	ADJ
ijpds-4231	188	54	green	green	ADJ
ijpds-4231	188	55	oily	oily	ADJ
ijpds-4231	188	56	mass	mass	NOUN
ijpds-4231	188	57	)	)	PUNCT
ijpds-4231	188	58	.	.	PUNCT
ijpds-4231	189	1	the	the	DET
ijpds-4231	189	2	process	process	NOUN
ijpds-4231	189	3	had	have	AUX
ijpds-4231	189	4	involved	involve	VERB
ijpds-4231	189	5	a	a	DET
ijpds-4231	189	6	series	series	NOUN
ijpds-4231	189	7	of	of	ADP
ijpds-4231	189	8	reaction	reaction	NOUN
ijpds-4231	189	9	steps	step	NOUN
ijpds-4231	189	10	like	like	ADP
ijpds-4231	189	11	curtius	curtius	NOUN
ijpds-4231	189	12	rearrangement	rearrangement	NOUN
ijpds-4231	189	13	,	,	PUNCT
ijpds-4231	189	14	resolution	resolution	NOUN
ijpds-4231	189	15	,	,	PUNCT
ijpds-4231	189	16	hydrolysis	hydrolysis	NOUN
ijpds-4231	189	17	,	,	PUNCT
ijpds-4231	189	18	de	de	NOUN
ijpds-4231	189	19	-	-	NOUN
ijpds-4231	189	20	protection	protection	NOUN
ijpds-4231	189	21	etc	etc	NOUN
ijpds-4231	189	22	to	to	PART
ijpds-4231	189	23	isolate	isolate	VERB
ijpds-4231	189	24	the	the	DET
ijpds-4231	189	25	intended	intend	VERB
ijpds-4231	189	26	product	product	NOUN
ijpds-4231	189	27	[	[	X
ijpds-4231	189	28	32	32	NUM
ijpds-4231	189	29	]	]	PUNCT
ijpds-4231	189	30	.	.	PUNCT
ijpds-4231	190	1	allegrini	allegrini	PROPN
ijpds-4231	190	2	p	p	PROPN
ijpds-4231	190	3	,	,	PUNCT
ijpds-4231	190	4	et	et	PROPN
ijpds-4231	190	5	al	al	PROPN
ijpds-4231	190	6	.	.	PROPN
ijpds-4231	190	7	,	,	PUNCT
ijpds-4231	190	8	in	in	ADP
ijpds-4231	190	9	2010	2010	NUM
ijpds-4231	190	10	,	,	PUNCT
ijpds-4231	190	11	had	have	AUX
ijpds-4231	190	12	illustrated	illustrate	VERB
ijpds-4231	190	13	the	the	DET
ijpds-4231	190	14	condensation	condensation	NOUN
ijpds-4231	190	15	of	of	ADP
ijpds-4231	190	16	6	6	NUM
ijpds-4231	190	17	and	and	CCONJ
ijpds-4231	190	18	9	9	NUM
ijpds-4231	190	19	in	in	ADP
ijpds-4231	190	20	the	the	DET
ijpds-4231	190	21	presence	presence	NOUN
ijpds-4231	190	22	of	of	ADP
ijpds-4231	190	23	sodium	sodium	NOUN
ijpds-4231	190	24	borohydride	borohydride	NOUN
ijpds-4231	190	25	in	in	ADP
ijpds-4231	190	26	tetrahydrofuran	tetrahydrofuran	NOUN
ijpds-4231	190	27	to	to	PART
ijpds-4231	190	28	isolate	isolate	VERB
ijpds-4231	190	29	the	the	DET
ijpds-4231	190	30	racemic	racemic	ADJ
ijpds-4231	190	31	rasagiline	rasagiline	NOUN
ijpds-4231	190	32	base	base	NOUN
ijpds-4231	190	33	(	(	PUNCT
ijpds-4231	190	34	yield	yield	NOUN
ijpds-4231	190	35	:	:	PUNCT
ijpds-4231	190	36	91	91	NUM
ijpds-4231	190	37	%	%	NOUN
ijpds-4231	190	38	)	)	PUNCT
ijpds-4231	190	39	.	.	PUNCT
ijpds-4231	191	1	it	it	PRON
ijpds-4231	191	2	was	be	AUX
ijpds-4231	191	3	treated	treat	VERB
ijpds-4231	191	4	with	with	ADP
ijpds-4231	191	5	l-(+)tartaric	l-(+)tartaric	ADJ
ijpds-4231	191	6	acid	acid	NOUN
ijpds-4231	191	7	in	in	ADP
ijpds-4231	191	8	ethyl	ethyl	PROPN
ijpds-4231	191	9	alcohol	alcohol	NOUN
ijpds-4231	191	10	to	to	PART
ijpds-4231	191	11	get	get	VERB
ijpds-4231	191	12	r	r	NOUN
ijpds-4231	191	13	-	-	PUNCT
ijpds-4231	191	14	rasagiline	rasagiline	NOUN
ijpds-4231	191	15	tartarate	tartarate	NOUN
ijpds-4231	191	16	.	.	PUNCT
ijpds-4231	192	1	it	it	PRON
ijpds-4231	192	2	was	be	AUX
ijpds-4231	192	3	cleaved	cleave	VERB
ijpds-4231	192	4	under	under	ADP
ijpds-4231	192	5	nitrogen	nitrogen	NOUN
ijpds-4231	192	6	atmosphere	atmosphere	NOUN
ijpds-4231	192	7	using	use	VERB
ijpds-4231	192	8	sodium	sodium	NOUN
ijpds-4231	192	9	bicarbonate	bicarbonate	NOUN
ijpds-4231	192	10	solution	solution	NOUN
ijpds-4231	192	11	and	and	CCONJ
ijpds-4231	192	12	ethyl	ethyl	PROPN
ijpds-4231	192	13	acetate	acetate	PROPN
ijpds-4231	192	14	to	to	PART
ijpds-4231	192	15	isolate	isolate	VERB
ijpds-4231	192	16	rsanjay	rsanjay	VERB
ijpds-4231	192	17	s	s	PART
ijpds-4231	192	18	s	s	NOUN
ijpds-4231	192	19	patents	patent	NOUN
ijpds-4231	192	20	disclosed	disclose	VERB
ijpds-4231	192	21	synthetic	synthetic	ADJ
ijpds-4231	192	22	overview	overview	NOUN
ijpds-4231	192	23	of	of	ADP
ijpds-4231	192	24	rasagiline	rasagiline	ADJ
ijpds-4231	192	25	vol	vol	NOUN
ijpds-4231	192	26	2	2	NUM
ijpds-4231	192	27	|	|	ADV
ijpds-4231	192	28	issue	issue	VERB
ijpds-4231	192	29	4	4	NUM
ijpds-4231	192	30	|	|	ADV
ijpds-4231	192	31	oct	oct	PROPN
ijpds-4231	192	32	–	–	PUNCT
ijpds-4231	193	1	dec	dec	PROPN
ijpds-4231	193	2	2023	2023	NUM
ijpds-4231	193	3	indian	indian	PROPN
ijpds-4231	193	4	j	j	PROPN
ijpds-4231	193	5	pharm	pharm	PROPN
ijpds-4231	193	6	drug	drug	PROPN
ijpds-4231	193	7	studies	study	NOUN
ijpds-4231	193	8	|	|	ADV
ijpds-4231	193	9	137	137	NUM
ijpds-4231	193	10	rasagiline	rasagiline	NOUN
ijpds-4231	193	11	base	base	NOUN
ijpds-4231	193	12	(	(	PUNCT
ijpds-4231	193	13	as	as	ADP
ijpds-4231	193	14	an	an	DET
ijpds-4231	193	15	oily	oily	ADJ
ijpds-4231	193	16	liquid	liquid	NOUN
ijpds-4231	193	17	)	)	PUNCT
ijpds-4231	193	18	.	.	PUNCT
ijpds-4231	194	1	it	it	PRON
ijpds-4231	194	2	was	be	AUX
ijpds-4231	194	3	taken	take	VERB
ijpds-4231	194	4	in	in	ADP
ijpds-4231	194	5	isopropyl	isopropyl	NOUN
ijpds-4231	194	6	alcohol	alcohol	NOUN
ijpds-4231	194	7	and	and	CCONJ
ijpds-4231	194	8	treated	treat	VERB
ijpds-4231	194	9	with	with	ADP
ijpds-4231	194	10	methanesulfonic	methanesulfonic	ADJ
ijpds-4231	194	11	acid	acid	NOUN
ijpds-4231	194	12	to	to	PART
ijpds-4231	194	13	isolate	isolate	VERB
ijpds-4231	194	14	1	1	NUM
ijpds-4231	194	15	(	(	PUNCT
ijpds-4231	194	16	yield	yield	NOUN
ijpds-4231	194	17	:	:	PUNCT
ijpds-4231	194	18	89	89	NUM
ijpds-4231	194	19	%	%	NOUN
ijpds-4231	194	20	from	from	ADP
ijpds-4231	194	21	its	its	PRON
ijpds-4231	194	22	tartarate	tartarate	ADJ
ijpds-4231	194	23	salt	salt	NOUN
ijpds-4231	194	24	)	)	PUNCT
ijpds-4231	194	25	.	.	PUNCT
ijpds-4231	195	1	the	the	DET
ijpds-4231	195	2	work	work	NOUN
ijpds-4231	195	3	was	be	AUX
ijpds-4231	195	4	extended	extend	VERB
ijpds-4231	195	5	further	far	ADV
ijpds-4231	195	6	to	to	PART
ijpds-4231	195	7	provide	provide	VERB
ijpds-4231	195	8	the	the	DET
ijpds-4231	195	9	procedure	procedure	NOUN
ijpds-4231	195	10	to	to	PART
ijpds-4231	195	11	isolate	isolate	VERB
ijpds-4231	195	12	the	the	DET
ijpds-4231	195	13	crystalline	crystalline	ADJ
ijpds-4231	195	14	form	form	NOUN
ijpds-4231	195	15	of	of	ADP
ijpds-4231	195	16	r	r	NOUN
ijpds-4231	195	17	-	-	PUNCT
ijpds-4231	195	18	rasagiline	rasagiline	NOUN
ijpds-4231	195	19	base	base	NOUN
ijpds-4231	195	20	with	with	ADP
ijpds-4231	195	21	a	a	DET
ijpds-4231	195	22	melting	melting	NOUN
ijpds-4231	195	23	of	of	ADP
ijpds-4231	195	24	4041oc	4041oc	PROPN
ijpds-4231	195	25	[	[	X
ijpds-4231	195	26	33	33	NUM
ijpds-4231	195	27	]	]	PUNCT
ijpds-4231	195	28	.	.	PUNCT
ijpds-4231	196	1	phull	phull	PROPN
ijpds-4231	196	2	ms	ms	PROPN
ijpds-4231	196	3	,	,	PUNCT
ijpds-4231	196	4	et	et	PROPN
ijpds-4231	196	5	al	al	PROPN
ijpds-4231	196	6	.	.	PROPN
ijpds-4231	196	7	,	,	PUNCT
ijpds-4231	196	8	in	in	ADP
ijpds-4231	196	9	2010	2010	NUM
ijpds-4231	196	10	,	,	PUNCT
ijpds-4231	196	11	had	have	AUX
ijpds-4231	196	12	reported	report	VERB
ijpds-4231	196	13	a	a	DET
ijpds-4231	196	14	multi	multi	ADJ
ijpds-4231	196	15	-	-	ADJ
ijpds-4231	196	16	step	step	ADJ
ijpds-4231	196	17	process	process	NOUN
ijpds-4231	196	18	to	to	PART
ijpds-4231	196	19	isolate	isolate	VERB
ijpds-4231	196	20	1	1	NUM
ijpds-4231	196	21	.	.	PUNCT
ijpds-4231	197	1	in	in	ADP
ijpds-4231	197	2	an	an	DET
ijpds-4231	197	3	example	example	NOUN
ijpds-4231	197	4	,	,	PUNCT
ijpds-4231	197	5	9	9	NUM
ijpds-4231	197	6	was	be	AUX
ijpds-4231	197	7	reacted	react	VERB
ijpds-4231	197	8	with	with	ADP
ijpds-4231	197	9	allyl	allyl	ADJ
ijpds-4231	197	10	bromide	bromide	NOUN
ijpds-4231	197	11	27	27	NUM
ijpds-4231	197	12	in	in	ADP
ijpds-4231	197	13	the	the	DET
ijpds-4231	197	14	presence	presence	NOUN
ijpds-4231	197	15	of	of	ADP
ijpds-4231	197	16	potassium	potassium	NOUN
ijpds-4231	197	17	carbonate	carbonate	NOUN
ijpds-4231	197	18	in	in	ADP
ijpds-4231	197	19	acetonitrile	acetonitrile	NOUN
ijpds-4231	197	20	and	and	CCONJ
ijpds-4231	197	21	then	then	ADV
ijpds-4231	197	22	treated	treat	VERB
ijpds-4231	197	23	with	with	ADP
ijpds-4231	197	24	oxalic	oxalic	NOUN
ijpds-4231	197	25	acid	acid	NOUN
ijpds-4231	197	26	to	to	PART
ijpds-4231	197	27	obtain	obtain	VERB
ijpds-4231	197	28	r-()-n	r-()-n	VERB
ijpds-4231	197	29	-	-	PUNCT
ijpds-4231	197	30	allyl-1	allyl-1	NUM
ijpds-4231	197	31	-	-	PUNCT
ijpds-4231	197	32	aminoindan	aminoindan	NOUN
ijpds-4231	197	33	oxalate	oxalate	PROPN
ijpds-4231	197	34	28	28	NUM
ijpds-4231	197	35	.	.	PUNCT
ijpds-4231	198	1	it	it	PRON
ijpds-4231	198	2	was	be	AUX
ijpds-4231	198	3	de	de	ADJ
ijpds-4231	198	4	-	-	VERB
ijpds-4231	198	5	oxalated	oxalated	ADJ
ijpds-4231	198	6	and	and	CCONJ
ijpds-4231	198	7	then	then	ADV
ijpds-4231	198	8	brominated	brominate	VERB
ijpds-4231	198	9	(	(	PUNCT
ijpds-4231	198	10	by	by	ADP
ijpds-4231	198	11	bromine	bromine	NOUN
ijpds-4231	198	12	)	)	PUNCT
ijpds-4231	198	13	in	in	ADP
ijpds-4231	198	14	dichloromethane	dichloromethane	NOUN
ijpds-4231	198	15	to	to	PART
ijpds-4231	198	16	isolate	isolate	VERB
ijpds-4231	198	17	r-(-)-n-(2,3	r-(-)-n-(2,3	NOUN
ijpds-4231	198	18	-	-	PUNCT
ijpds-4231	198	19	dibromo	dibromo	NOUN
ijpds-4231	198	20	-	-	PUNCT
ijpds-4231	198	21	propyl)-1	propyl)-1	NOUN
ijpds-4231	198	22	-	-	PUNCT
ijpds-4231	198	23	aminoindan	aminoindan	NOUN
ijpds-4231	198	24	29	29	NUM
ijpds-4231	198	25	.	.	PUNCT
ijpds-4231	199	1	it	it	PRON
ijpds-4231	199	2	was	be	AUX
ijpds-4231	199	3	hydrolyzed	hydrolyze	VERB
ijpds-4231	199	4	using	use	VERB
ijpds-4231	199	5	potassium	potassium	NOUN
ijpds-4231	199	6	hydroxide	hydroxide	NOUN
ijpds-4231	199	7	solution	solution	NOUN
ijpds-4231	199	8	in	in	ADP
ijpds-4231	199	9	ethyl	ethyl	PROPN
ijpds-4231	199	10	alcohol	alcohol	NOUN
ijpds-4231	199	11	to	to	PART
ijpds-4231	199	12	isolate	isolate	VERB
ijpds-4231	199	13	r	r	NOUN
ijpds-4231	199	14	-	-	PUNCT
ijpds-4231	199	15	rasagiline	rasagiline	NOUN
ijpds-4231	199	16	oxalate	oxalate	NOUN
ijpds-4231	199	17	.	.	PUNCT
ijpds-4231	200	1	under	under	ADP
ijpds-4231	200	2	the	the	DET
ijpds-4231	200	3	similar	similar	ADJ
ijpds-4231	200	4	conditions	condition	NOUN
ijpds-4231	200	5	,	,	PUNCT
ijpds-4231	200	6	racemic	racemic	ADJ
ijpds-4231	200	7	29	29	NUM
ijpds-4231	200	8	was	be	AUX
ijpds-4231	200	9	synthesized	synthesize	VERB
ijpds-4231	200	10	and	and	CCONJ
ijpds-4231	200	11	hydrolyzed	hydrolyze	VERB
ijpds-4231	200	12	.	.	PUNCT
ijpds-4231	201	1	it	it	PRON
ijpds-4231	201	2	was	be	AUX
ijpds-4231	201	3	then	then	ADV
ijpds-4231	201	4	treated	treat	VERB
ijpds-4231	201	5	with	with	ADP
ijpds-4231	201	6	l	l	ADJ
ijpds-4231	201	7	-	-	ADJ
ijpds-4231	201	8	tartaric	tartaric	ADJ
ijpds-4231	201	9	acid	acid	NOUN
ijpds-4231	201	10	to	to	PART
ijpds-4231	201	11	isolate	isolate	VERB
ijpds-4231	201	12	the	the	DET
ijpds-4231	201	13	crude	crude	NOUN
ijpds-4231	201	14	solid	solid	ADJ
ijpds-4231	201	15	.	.	PUNCT
ijpds-4231	202	1	it	it	PRON
ijpds-4231	202	2	was	be	AUX
ijpds-4231	202	3	then	then	ADV
ijpds-4231	202	4	de	de	ADJ
ijpds-4231	202	5	-	-	VERB
ijpds-4231	202	6	tartarated	tartarate	VERB
ijpds-4231	202	7	by	by	ADP
ijpds-4231	202	8	treating	treat	VERB
ijpds-4231	202	9	with	with	ADP
ijpds-4231	202	10	sodium	sodium	NOUN
ijpds-4231	202	11	hydroxide	hydroxide	NOUN
ijpds-4231	202	12	solution	solution	NOUN
ijpds-4231	202	13	and	and	CCONJ
ijpds-4231	202	14	mesylated	mesylate	VERB
ijpds-4231	202	15	by	by	ADP
ijpds-4231	202	16	the	the	DET
ijpds-4231	202	17	addition	addition	NOUN
ijpds-4231	202	18	of	of	ADP
ijpds-4231	202	19	methanesulfonic	methanesulfonic	ADJ
ijpds-4231	202	20	acid	acid	NOUN
ijpds-4231	202	21	in	in	ADP
ijpds-4231	202	22	isopropyl	isopropyl	NOUN
ijpds-4231	202	23	alcohol	alcohol	NOUN
ijpds-4231	202	24	to	to	PART
ijpds-4231	202	25	obtain	obtain	VERB
ijpds-4231	202	26	1	1	NUM
ijpds-4231	202	27	(	(	PUNCT
ijpds-4231	202	28	purity	purity	NOUN
ijpds-4231	202	29	:	:	PUNCT
ijpds-4231	202	30	99.8	99.8	NUM
ijpds-4231	202	31	%	%	NOUN
ijpds-4231	202	32	,	,	PUNCT
ijpds-4231	202	33	chiral	chiral	ADJ
ijpds-4231	202	34	purity	purity	NOUN
ijpds-4231	202	35	:	:	PUNCT
ijpds-4231	202	36	99.5	99.5	NUM
ijpds-4231	202	37	%	%	NOUN
ijpds-4231	202	38	)	)	PUNCT
ijpds-4231	202	39	.	.	PUNCT
ijpds-4231	203	1	the	the	DET
ijpds-4231	203	2	resolving	resolving	NOUN
ijpds-4231	203	3	process	process	NOUN
ijpds-4231	203	4	can	can	AUX
ijpds-4231	203	5	be	be	AUX
ijpds-4231	203	6	adapted	adapt	VERB
ijpds-4231	203	7	to	to	ADP
ijpds-4231	203	8	racemic	racemic	ADJ
ijpds-4231	203	9	28	28	NUM
ijpds-4231	203	10	using	use	VERB
ijpds-4231	203	11	ltartaric	ltartaric	ADJ
ijpds-4231	203	12	acid	acid	NOUN
ijpds-4231	203	13	or	or	CCONJ
ijpds-4231	203	14	it	it	PRON
ijpds-4231	203	15	can	can	AUX
ijpds-4231	203	16	be	be	AUX
ijpds-4231	203	17	effectively	effectively	ADV
ijpds-4231	203	18	implemented	implement	VERB
ijpds-4231	203	19	to	to	ADP
ijpds-4231	203	20	racemic	racemic	VERB
ijpds-4231	203	21	29	29	NUM
ijpds-4231	203	22	using	use	VERB
ijpds-4231	203	23	l	l	NOUN
ijpds-4231	203	24	-	-	ADJ
ijpds-4231	203	25	tartaric	tartaric	ADJ
ijpds-4231	203	26	acid	acid	NOUN
ijpds-4231	203	27	.	.	PUNCT
ijpds-4231	204	1	the	the	DET
ijpds-4231	204	2	work	work	NOUN
ijpds-4231	204	3	had	have	AUX
ijpds-4231	204	4	provided	provide	VERB
ijpds-4231	204	5	an	an	DET
ijpds-4231	204	6	improved	improved	ADJ
ijpds-4231	204	7	process	process	NOUN
ijpds-4231	204	8	by	by	ADP
ijpds-4231	204	9	eliminating	eliminate	VERB
ijpds-4231	204	10	the	the	DET
ijpds-4231	204	11	drawbacks	drawback	NOUN
ijpds-4231	204	12	of	of	ADP
ijpds-4231	204	13	past	past	ADJ
ijpds-4231	204	14	disclosures	disclosure	NOUN
ijpds-4231	204	15	[	[	X
ijpds-4231	204	16	34	34	NUM
ijpds-4231	204	17	]	]	PUNCT
ijpds-4231	204	18	.	.	PUNCT
ijpds-4231	205	1	stahl	stahl	PROPN
ijpds-4231	205	2	hp	hp	PROPN
ijpds-4231	205	3	.	.	PROPN
ijpds-4231	205	4	,	,	PUNCT
ijpds-4231	205	5	in	in	ADP
ijpds-4231	205	6	2010	2010	NUM
ijpds-4231	205	7	,	,	PUNCT
ijpds-4231	205	8	had	have	AUX
ijpds-4231	205	9	demonstrated	demonstrate	VERB
ijpds-4231	205	10	the	the	DET
ijpds-4231	205	11	preparation	preparation	NOUN
ijpds-4231	205	12	,	,	PUNCT
ijpds-4231	205	13	solubility	solubility	NOUN
ijpds-4231	205	14	profile	profile	NOUN
ijpds-4231	205	15	,	,	PUNCT
ijpds-4231	205	16	and	and	CCONJ
ijpds-4231	205	17	hygroscopicity	hygroscopicity	NOUN
ijpds-4231	205	18	details	detail	NOUN
ijpds-4231	205	19	of	of	ADP
ijpds-4231	205	20	two	two	NUM
ijpds-4231	205	21	new	new	ADJ
ijpds-4231	205	22	salts	salt	NOUN
ijpds-4231	205	23	of	of	ADP
ijpds-4231	205	24	rasagiline	rasagiline	NOUN
ijpds-4231	205	25	.	.	PUNCT
ijpds-4231	206	1	rasagiline	rasagiline	PROPN
ijpds-4231	206	2	base	base	NOUN
ijpds-4231	206	3	was	be	AUX
ijpds-4231	206	4	taken	take	VERB
ijpds-4231	206	5	in	in	ADP
ijpds-4231	206	6	isopropyl	isopropyl	NOUN
ijpds-4231	206	7	alcohol	alcohol	NOUN
ijpds-4231	206	8	and	and	CCONJ
ijpds-4231	206	9	ethanedisulfonic	ethanedisulfonic	ADJ
ijpds-4231	206	10	acid	acid	NOUN
ijpds-4231	206	11	was	be	AUX
ijpds-4231	206	12	added	add	VERB
ijpds-4231	206	13	to	to	PART
ijpds-4231	206	14	isolate	isolate	VERB
ijpds-4231	206	15	rasagiline	rasagiline	ADJ
ijpds-4231	206	16	edisilate	edisilate	NOUN
ijpds-4231	206	17	with	with	ADP
ijpds-4231	206	18	a	a	DET
ijpds-4231	206	19	melting	melting	NOUN
ijpds-4231	206	20	point	point	NOUN
ijpds-4231	206	21	of	of	ADP
ijpds-4231	206	22	201oc	201oc	NOUN
ijpds-4231	206	23	(	(	PUNCT
ijpds-4231	206	24	yield	yield	NOUN
ijpds-4231	206	25	:	:	PUNCT
ijpds-4231	206	26	56.3	56.3	NUM
ijpds-4231	206	27	%	%	NOUN
ijpds-4231	206	28	)	)	PUNCT
ijpds-4231	206	29	.	.	PUNCT
ijpds-4231	207	1	under	under	ADP
ijpds-4231	207	2	the	the	DET
ijpds-4231	207	3	similar	similar	ADJ
ijpds-4231	207	4	conditions	condition	NOUN
ijpds-4231	207	5	,	,	PUNCT
ijpds-4231	207	6	rasagiline	rasagiline	NOUN
ijpds-4231	207	7	base	base	NOUN
ijpds-4231	207	8	was	be	AUX
ijpds-4231	207	9	treated	treat	VERB
ijpds-4231	207	10	with	with	ADP
ijpds-4231	207	11	oxalic	oxalic	NOUN
ijpds-4231	207	12	acid	acid	NOUN
ijpds-4231	207	13	in	in	ADP
ijpds-4231	207	14	isopropyl	isopropyl	NOUN
ijpds-4231	207	15	alcohol	alcohol	NOUN
ijpds-4231	207	16	to	to	PART
ijpds-4231	207	17	obtain	obtain	VERB
ijpds-4231	207	18	rasagiline	rasagiline	NOUN
ijpds-4231	207	19	oxalate	oxalate	NOUN
ijpds-4231	207	20	with	with	ADP
ijpds-4231	207	21	a	a	DET
ijpds-4231	207	22	melting	melting	NOUN
ijpds-4231	207	23	point	point	NOUN
ijpds-4231	207	24	of	of	ADP
ijpds-4231	207	25	204oc	204oc	NOUN
ijpds-4231	207	26	(	(	PUNCT
ijpds-4231	207	27	yield	yield	NOUN
ijpds-4231	207	28	:	:	PUNCT
ijpds-4231	207	29	93.1	93.1	NUM
ijpds-4231	207	30	%	%	NOUN
ijpds-4231	207	31	)	)	PUNCT
ijpds-4231	208	1	[	[	X
ijpds-4231	208	2	35	35	NUM
ijpds-4231	208	3	]	]	PUNCT
ijpds-4231	208	4	.	.	PUNCT
ijpds-4231	209	1	frenkel	frenkel	PROPN
ijpds-4231	209	2	a	a	PRON
ijpds-4231	209	3	,	,	PUNCT
ijpds-4231	209	4	et	et	PROPN
ijpds-4231	209	5	al	al	PROPN
ijpds-4231	209	6	.	.	PROPN
ijpds-4231	209	7	,	,	PUNCT
ijpds-4231	209	8	in	in	ADP
ijpds-4231	209	9	2010	2010	NUM
ijpds-4231	209	10	,	,	PUNCT
ijpds-4231	209	11	had	have	AUX
ijpds-4231	209	12	reported	report	VERB
ijpds-4231	209	13	the	the	DET
ijpds-4231	209	14	isolation	isolation	NOUN
ijpds-4231	209	15	of	of	ADP
ijpds-4231	209	16	mono	mono	NOUN
ijpds-4231	209	17	-	-	PUNCT
ijpds-4231	209	18	rasagiline	rasagiline	NOUN
ijpds-4231	209	19	citrate	citrate	NOUN
ijpds-4231	209	20	,	,	PUNCT
ijpds-4231	209	21	di	di	NOUN
ijpds-4231	209	22	-	-	PUNCT
ijpds-4231	209	23	rasagiline	rasagiline	NOUN
ijpds-4231	209	24	citrate	citrate	NOUN
ijpds-4231	209	25	or	or	CCONJ
ijpds-4231	209	26	trirasagiline	trirasagiline	VERB
ijpds-4231	209	27	citrate	citrate	NOUN
ijpds-4231	209	28	or	or	CCONJ
ijpds-4231	209	29	a	a	DET
ijpds-4231	209	30	mixture	mixture	NOUN
ijpds-4231	209	31	of	of	ADP
ijpds-4231	209	32	all	all	DET
ijpds-4231	209	33	them	they	PRON
ijpds-4231	209	34	.	.	PUNCT
ijpds-4231	210	1	these	these	DET
ijpds-4231	210	2	salts	salt	NOUN
ijpds-4231	210	3	or	or	CCONJ
ijpds-4231	210	4	salt	salt	NOUN
ijpds-4231	210	5	mixtures	mixture	NOUN
ijpds-4231	210	6	were	be	AUX
ijpds-4231	210	7	prepared	prepare	VERB
ijpds-4231	210	8	by	by	ADP
ijpds-4231	210	9	treating	treat	VERB
ijpds-4231	210	10	rasagiline	rasagiline	NOUN
ijpds-4231	210	11	base	base	NOUN
ijpds-4231	210	12	(	(	PUNCT
ijpds-4231	210	13	solid	solid	ADJ
ijpds-4231	210	14	)	)	PUNCT
ijpds-4231	210	15	with	with	ADP
ijpds-4231	210	16	citric	citric	ADJ
ijpds-4231	210	17	acid	acid	NOUN
ijpds-4231	210	18	in	in	ADP
ijpds-4231	210	19	ethyl	ethyl	PROPN
ijpds-4231	210	20	alcohol	alcohol	NOUN
ijpds-4231	210	21	or	or	CCONJ
ijpds-4231	210	22	a	a	DET
ijpds-4231	210	23	few	few	ADJ
ijpds-4231	210	24	other	other	ADJ
ijpds-4231	210	25	solvents	solvent	NOUN
ijpds-4231	210	26	/	/	SYM
ijpds-4231	210	27	water	water	NOUN
ijpds-4231	210	28	[	[	X
ijpds-4231	210	29	36	36	NUM
ijpds-4231	210	30	]	]	PUNCT
ijpds-4231	210	31	.	.	PUNCT
ijpds-4231	211	1	stephen	stephen	PROPN
ijpds-4231	211	2	bdw	bdw	PROPN
ijpds-4231	211	3	,	,	PUNCT
ijpds-4231	211	4	et	et	PROPN
ijpds-4231	211	5	al	al	PROPN
ijpds-4231	211	6	.	.	PROPN
ijpds-4231	211	7	,	,	PUNCT
ijpds-4231	211	8	in	in	ADP
ijpds-4231	211	9	2010	2010	NUM
ijpds-4231	211	10	,	,	PUNCT
ijpds-4231	211	11	had	have	AUX
ijpds-4231	211	12	illustrated	illustrate	VERB
ijpds-4231	211	13	a	a	DET
ijpds-4231	211	14	few	few	ADJ
ijpds-4231	211	15	more	more	ADJ
ijpds-4231	211	16	rasagiline	rasagiline	NOUN
ijpds-4231	211	17	salts	salt	NOUN
ijpds-4231	211	18	such	such	ADJ
ijpds-4231	211	19	as	as	ADP
ijpds-4231	211	20	tartrate	tartrate	NOUN
ijpds-4231	211	21	with	with	ADP
ijpds-4231	211	22	a	a	DET
ijpds-4231	211	23	melting	melting	NOUN
ijpds-4231	211	24	point	point	NOUN
ijpds-4231	211	25	of	of	ADP
ijpds-4231	211	26	176.2	176.2	NUM
ijpds-4231	211	27	-	-	PUNCT
ijpds-4231	211	28	177.3oc	177.3oc	NUM
ijpds-4231	211	29	,	,	PUNCT
ijpds-4231	211	30	maleate	maleate	NOUN
ijpds-4231	211	31	with	with	ADP
ijpds-4231	211	32	a	a	DET
ijpds-4231	211	33	melting	melting	NOUN
ijpds-4231	211	34	point	point	NOUN
ijpds-4231	211	35	of	of	ADP
ijpds-4231	211	36	87.287.8oc	87.287.8oc	NUM
ijpds-4231	211	37	,	,	PUNCT
ijpds-4231	211	38	sulphate	sulphate	VERB
ijpds-4231	211	39	with	with	ADP
ijpds-4231	211	40	a	a	DET
ijpds-4231	211	41	melting	melting	NOUN
ijpds-4231	211	42	point	point	NOUN
ijpds-4231	211	43	of	of	ADP
ijpds-4231	211	44	159.4	159.4	NUM
ijpds-4231	211	45	-	-	PUNCT
ijpds-4231	211	46	161.1oc	161.1oc	NUM
ijpds-4231	211	47	,	,	PUNCT
ijpds-4231	211	48	hydrochloride	hydrochloride	NOUN
ijpds-4231	211	49	with	with	ADP
ijpds-4231	211	50	a	a	DET
ijpds-4231	211	51	melting	melting	NOUN
ijpds-4231	211	52	point	point	NOUN
ijpds-4231	211	53	of	of	ADP
ijpds-4231	211	54	177.0	177.0	NUM
ijpds-4231	211	55	-	-	PUNCT
ijpds-4231	211	56	180.0oc	180.0oc	PROPN
ijpds-4231	211	57	,	,	PUNCT
ijpds-4231	211	58	tosylate	tosylate	VERB
ijpds-4231	211	59	with	with	ADP
ijpds-4231	211	60	a	a	DET
ijpds-4231	211	61	melting	melting	NOUN
ijpds-4231	211	62	point	point	NOUN
ijpds-4231	211	63	of	of	ADP
ijpds-4231	211	64	129.3	129.3	NUM
ijpds-4231	211	65	-	-	SYM
ijpds-4231	211	66	129.9oc	129.9oc	NUM
ijpds-4231	211	67	,	,	PUNCT
ijpds-4231	211	68	fumarate	fumarate	NOUN
ijpds-4231	211	69	with	with	ADP
ijpds-4231	211	70	a	a	DET
ijpds-4231	211	71	melting	melting	NOUN
ijpds-4231	211	72	point	point	NOUN
ijpds-4231	211	73	of	of	ADP
ijpds-4231	211	74	125.4	125.4	NUM
ijpds-4231	211	75	-	-	SYM
ijpds-4231	211	76	126.2oc	126.2oc	NUM
ijpds-4231	211	77	,	,	PUNCT
ijpds-4231	211	78	phosphate	phosphate	VERB
ijpds-4231	211	79	with	with	ADP
ijpds-4231	211	80	a	a	DET
ijpds-4231	211	81	melting	melting	NOUN
ijpds-4231	211	82	point	point	NOUN
ijpds-4231	211	83	of	of	ADP
ijpds-4231	211	84	109.5	109.5	NUM
ijpds-4231	211	85	-	-	SYM
ijpds-4231	211	86	110.4oc	110.4oc	NUM
ijpds-4231	211	87	,	,	PUNCT
ijpds-4231	211	88	acetate	acetate	NOUN
ijpds-4231	211	89	with	with	ADP
ijpds-4231	211	90	a	a	DET
ijpds-4231	211	91	melting	melting	NOUN
ijpds-4231	211	92	point	point	NOUN
ijpds-4231	211	93	of	of	ADP
ijpds-4231	211	94	69.2	69.2	NUM
ijpds-4231	211	95	-	-	PUNCT
ijpds-4231	211	96	69.7oc	69.7oc	NOUN
ijpds-4231	211	97	,	,	PUNCT
ijpds-4231	211	98	besylate	besylate	ADJ
ijpds-4231	211	99	,	,	PUNCT
ijpds-4231	211	100	tannate	tannate	NOUN
ijpds-4231	211	101	,	,	PUNCT
ijpds-4231	211	102	benzoate	benzoate	NOUN
ijpds-4231	211	103	,	,	PUNCT
ijpds-4231	211	104	galactarate	galactarate	NOUN
ijpds-4231	211	105	,	,	PUNCT
ijpds-4231	211	106	gluconate	gluconate	NOUN
ijpds-4231	211	107	,	,	PUNCT
ijpds-4231	211	108	glucuronate	glucuronate	ADJ
ijpds-4231	211	109	,	,	PUNCT
ijpds-4231	211	110	succinate	succinate	NOUN
ijpds-4231	211	111	,	,	PUNCT
ijpds-4231	211	112	hetartarate	hetartarate	NOUN
ijpds-4231	211	113	etc	etc	X
ijpds-4231	211	114	from	from	ADP
ijpds-4231	211	115	rasagiline	rasagiline	NOUN
ijpds-4231	211	116	base	base	NOUN
ijpds-4231	211	117	using	use	VERB
ijpds-4231	211	118	various	various	ADJ
ijpds-4231	211	119	suitable	suitable	ADJ
ijpds-4231	211	120	solvents	solvent	NOUN
ijpds-4231	211	121	/	/	SYM
ijpds-4231	211	122	water	water	NOUN
ijpds-4231	211	123	.	.	PUNCT
ijpds-4231	212	1	some	some	PRON
ijpds-4231	212	2	of	of	ADP
ijpds-4231	212	3	those	those	DET
ijpds-4231	212	4	salts	salt	NOUN
ijpds-4231	212	5	were	be	AUX
ijpds-4231	212	6	isolated	isolate	VERB
ijpds-4231	212	7	in	in	ADP
ijpds-4231	212	8	their	their	PRON
ijpds-4231	212	9	crystalline	crystalline	NOUN
ijpds-4231	212	10	forms	form	NOUN
ijpds-4231	212	11	(	(	PUNCT
ijpds-4231	212	12	form	form	VERB
ijpds-4231	212	13	i	i	PROPN
ijpds-4231	212	14	/	/	SYM
ijpds-4231	212	15	ii	ii	PROPN
ijpds-4231	212	16	)	)	PUNCT
ijpds-4231	212	17	and	and	CCONJ
ijpds-4231	212	18	a	a	DET
ijpds-4231	212	19	few	few	ADJ
ijpds-4231	212	20	salts	salt	NOUN
ijpds-4231	212	21	in	in	ADP
ijpds-4231	212	22	their	their	PRON
ijpds-4231	212	23	amorphous	amorphous	ADJ
ijpds-4231	212	24	form	form	NOUN
ijpds-4231	212	25	[	[	X
ijpds-4231	212	26	37	37	NUM
ijpds-4231	212	27	]	]	PUNCT
ijpds-4231	212	28	.	.	PUNCT
ijpds-4231	213	1	thomas	thomas	PROPN
ijpds-4231	213	2	t	t	PROPN
ijpds-4231	213	3	,	,	PUNCT
ijpds-4231	213	4	et	et	PROPN
ijpds-4231	213	5	al	al	PROPN
ijpds-4231	213	6	.	.	PROPN
ijpds-4231	213	7	,	,	PUNCT
ijpds-4231	213	8	in	in	ADP
ijpds-4231	213	9	2011	2011	NUM
ijpds-4231	213	10	,	,	PUNCT
ijpds-4231	213	11	had	have	AUX
ijpds-4231	213	12	reported	report	VERB
ijpds-4231	213	13	the	the	DET
ijpds-4231	213	14	preparation	preparation	NOUN
ijpds-4231	213	15	and	and	CCONJ
ijpds-4231	213	16	advantages	advantage	NOUN
ijpds-4231	213	17	of	of	ADP
ijpds-4231	213	18	a	a	DET
ijpds-4231	213	19	few	few	ADJ
ijpds-4231	213	20	salts	salt	NOUN
ijpds-4231	213	21	of	of	ADP
ijpds-4231	213	22	rasagiline	rasagiline	NOUN
ijpds-4231	213	23	such	such	ADJ
ijpds-4231	213	24	as	as	ADP
ijpds-4231	213	25	gluconate	gluconate	NOUN
ijpds-4231	213	26	,	,	PUNCT
ijpds-4231	213	27	l	l	NOUN
ijpds-4231	213	28	-	-	NOUN
ijpds-4231	213	29	aspartate	aspartate	ADJ
ijpds-4231	213	30	,	,	PUNCT
ijpds-4231	213	31	citrate	citrate	NOUN
ijpds-4231	213	32	,	,	PUNCT
ijpds-4231	213	33	dl	dl	NOUN
ijpds-4231	213	34	-	-	PUNCT
ijpds-4231	213	35	lactate	lactate	NOUN
ijpds-4231	213	36	,	,	PUNCT
ijpds-4231	213	37	saccharinate	saccharinate	ADJ
ijpds-4231	213	38	,	,	PUNCT
ijpds-4231	213	39	docusate	docusate	NOUN
ijpds-4231	213	40	,	,	PUNCT
ijpds-4231	213	41	lauryl	lauryl	NOUN
ijpds-4231	213	42	sulphate	sulphate	NOUN
ijpds-4231	213	43	,	,	PUNCT
ijpds-4231	213	44	4	4	NUM
ijpds-4231	213	45	-	-	PUNCT
ijpds-4231	213	46	dodecylbenzenesulfonate	dodecylbenzenesulfonate	ADJ
ijpds-4231	213	47	,	,	PUNCT
ijpds-4231	213	48	linoleate	linoleate	ADJ
ijpds-4231	213	49	,	,	PUNCT
ijpds-4231	213	50	pentanoate	pentanoate	ADJ
ijpds-4231	213	51	,	,	PUNCT
ijpds-4231	213	52	propanoate	propanoate	NOUN
ijpds-4231	213	53	,	,	PUNCT
ijpds-4231	213	54	acetate	acetate	NOUN
ijpds-4231	213	55	,	,	PUNCT
ijpds-4231	213	56	decanoate	decanoate	ADJ
ijpds-4231	213	57	,	,	PUNCT
ijpds-4231	213	58	octanoate	octanoate	NOUN
ijpds-4231	213	59	,	,	PUNCT
ijpds-4231	213	60	hexanoate	hexanoate	NOUN
ijpds-4231	213	61	and	and	CCONJ
ijpds-4231	213	62	oleate	oleate	NOUN
ijpds-4231	213	63	.	.	PUNCT
ijpds-4231	214	1	these	these	DET
ijpds-4231	214	2	salts	salt	NOUN
ijpds-4231	214	3	were	be	AUX
ijpds-4231	214	4	prepared	prepare	VERB
ijpds-4231	214	5	from	from	ADP
ijpds-4231	214	6	rasagiline	rasagiline	NOUN
ijpds-4231	214	7	base	base	NOUN
ijpds-4231	214	8	using	use	VERB
ijpds-4231	214	9	appropriate	appropriate	ADJ
ijpds-4231	214	10	solvents	solvent	NOUN
ijpds-4231	214	11	[	[	X
ijpds-4231	214	12	38	38	NUM
ijpds-4231	214	13	]	]	PUNCT
ijpds-4231	214	14	.	.	PUNCT
ijpds-4231	215	1	patil	patil	PROPN
ijpds-4231	215	2	ns	ns	PROPN
ijpds-4231	215	3	,	,	PUNCT
ijpds-4231	215	4	et	et	PROPN
ijpds-4231	215	5	al	al	PROPN
ijpds-4231	215	6	.	.	PROPN
ijpds-4231	215	7	,	,	PUNCT
ijpds-4231	215	8	in	in	ADP
ijpds-4231	215	9	2011	2011	NUM
ijpds-4231	215	10	,	,	PUNCT
ijpds-4231	215	11	had	have	AUX
ijpds-4231	215	12	demonstrated	demonstrate	VERB
ijpds-4231	215	13	the	the	DET
ijpds-4231	215	14	isolation	isolation	NOUN
ijpds-4231	215	15	of	of	ADP
ijpds-4231	215	16	a	a	DET
ijpds-4231	215	17	few	few	ADJ
ijpds-4231	215	18	rasagiline	rasagiline	NOUN
ijpds-4231	215	19	salts	salt	NOUN
ijpds-4231	215	20	.	.	PUNCT
ijpds-4231	216	1	the	the	DET
ijpds-4231	216	2	salts	salt	NOUN
ijpds-4231	216	3	reported	report	VERB
ijpds-4231	216	4	are	be	AUX
ijpds-4231	216	5	maleate	maleate	NOUN
ijpds-4231	216	6	(	(	PUNCT
ijpds-4231	216	7	form	form	NOUN
ijpds-4231	216	8	-	-	PUNCT
ijpds-4231	216	9	ii	ii	NOUN
ijpds-4231	216	10	)	)	PUNCT
ijpds-4231	216	11	,	,	PUNCT
ijpds-4231	216	12	mandelate	mandelate	NOUN
ijpds-4231	216	13	(	(	PUNCT
ijpds-4231	216	14	form	form	NOUN
ijpds-4231	216	15	-	-	PUNCT
ijpds-4231	216	16	i	i	NOUN
ijpds-4231	216	17	)	)	PUNCT
ijpds-4231	216	18	and	and	CCONJ
ijpds-4231	216	19	salicylate	salicylate	NOUN
ijpds-4231	216	20	(	(	PUNCT
ijpds-4231	216	21	form	form	NOUN
ijpds-4231	216	22	-	-	PUNCT
ijpds-4231	216	23	i	i	NOUN
ijpds-4231	216	24	)	)	PUNCT
ijpds-4231	216	25	,	,	PUNCT
ijpds-4231	216	26	surprisingly	surprisingly	ADV
ijpds-4231	216	27	these	these	DET
ijpds-4231	216	28	salts	salt	NOUN
ijpds-4231	216	29	had	have	VERB
ijpds-4231	216	30	good	good	ADJ
ijpds-4231	216	31	purity	purity	NOUN
ijpds-4231	216	32	and	and	CCONJ
ijpds-4231	216	33	had	have	AUX
ijpds-4231	216	34	exhibited	exhibit	VERB
ijpds-4231	216	35	an	an	DET
ijpds-4231	216	36	adequate	adequate	ADJ
ijpds-4231	216	37	stability	stability	NOUN
ijpds-4231	216	38	,	,	PUNCT
ijpds-4231	216	39	good	good	ADJ
ijpds-4231	216	40	flowability	flowability	NOUN
ijpds-4231	216	41	and	and	CCONJ
ijpds-4231	216	42	a	a	DET
ijpds-4231	216	43	good	good	ADJ
ijpds-4231	216	44	dissolution	dissolution	NOUN
ijpds-4231	216	45	properties	property	NOUN
ijpds-4231	216	46	[	[	X
ijpds-4231	216	47	39	39	NUM
ijpds-4231	216	48	]	]	PUNCT
ijpds-4231	216	49	.	.	PUNCT
ijpds-4231	217	1	dongwei	dongwei	PROPN
ijpds-4231	218	1	c	c	X
ijpds-4231	218	2	,	,	PUNCT
ijpds-4231	218	3	et	et	PROPN
ijpds-4231	218	4	al	al	PROPN
ijpds-4231	218	5	.	.	PROPN
ijpds-4231	218	6	,	,	PUNCT
ijpds-4231	218	7	in	in	ADP
ijpds-4231	218	8	2011	2011	NUM
ijpds-4231	218	9	,	,	PUNCT
ijpds-4231	218	10	had	have	AUX
ijpds-4231	218	11	illustrated	illustrate	VERB
ijpds-4231	218	12	a	a	DET
ijpds-4231	218	13	multi	multi	ADJ
ijpds-4231	218	14	-	-	ADJ
ijpds-4231	218	15	step	step	ADJ
ijpds-4231	218	16	process	process	NOUN
ijpds-4231	218	17	to	to	PART
ijpds-4231	218	18	isolate	isolate	VERB
ijpds-4231	218	19	1	1	NUM
ijpds-4231	218	20	.	.	PUNCT
ijpds-4231	219	1	the	the	DET
ijpds-4231	219	2	reaction	reaction	NOUN
ijpds-4231	219	3	of	of	ADP
ijpds-4231	219	4	9	9	NUM
ijpds-4231	219	5	with	with	ADP
ijpds-4231	219	6	t	t	PROPN
ijpds-4231	219	7	-	-	PUNCT
ijpds-4231	219	8	butylsulfinamide	butylsulfinamide	NOUN
ijpds-4231	219	9	30	30	NUM
ijpds-4231	219	10	was	be	AUX
ijpds-4231	219	11	carried	carry	VERB
ijpds-4231	219	12	out	out	ADP
ijpds-4231	219	13	under	under	ADP
ijpds-4231	219	14	the	the	DET
ijpds-4231	219	15	catalytic	catalytic	ADJ
ijpds-4231	219	16	impact	impact	NOUN
ijpds-4231	219	17	of	of	ADP
ijpds-4231	219	18	isopropyl	isopropyl	NOUN
ijpds-4231	219	19	titanate	titanate	NOUN
ijpds-4231	219	20	in	in	ADP
ijpds-4231	219	21	tetrahydrofuran	tetrahydrofuran	NOUN
ijpds-4231	219	22	to	to	PART
ijpds-4231	219	23	get	get	VERB
ijpds-4231	219	24	n-(2,3dihydro-1h	n-(2,3dihydro-1h	PROPN
ijpds-4231	219	25	-	-	PUNCT
ijpds-4231	219	26	inden-1	inden-1	PROPN
ijpds-4231	219	27	-	-	PUNCT
ijpds-4231	219	28	yl)-2	yl)-2	NOUN
ijpds-4231	219	29	-	-	PUNCT
ijpds-4231	219	30	methylpropane-2	methylpropane-2	NOUN
ijpds-4231	219	31	-	-	PUNCT
ijpds-4231	219	32	sulfinamide	sulfinamide	NOUN
ijpds-4231	219	33	31	31	NUM
ijpds-4231	219	34	(	(	PUNCT
ijpds-4231	219	35	yield	yield	NOUN
ijpds-4231	219	36	:	:	PUNCT
ijpds-4231	219	37	59	59	NUM
ijpds-4231	219	38	%	%	NOUN
ijpds-4231	219	39	)	)	PUNCT
ijpds-4231	219	40	.	.	PUNCT
ijpds-4231	220	1	it	it	PRON
ijpds-4231	220	2	was	be	AUX
ijpds-4231	220	3	dissolved	dissolve	VERB
ijpds-4231	220	4	in	in	ADP
ijpds-4231	220	5	dimethyl	dimethyl	NOUN
ijpds-4231	220	6	formamide	formamide	ADV
ijpds-4231	220	7	and	and	CCONJ
ijpds-4231	220	8	reacted	react	VERB
ijpds-4231	220	9	with	with	ADP
ijpds-4231	220	10	sodium	sodium	NOUN
ijpds-4231	220	11	-	-	PUNCT
ijpds-4231	220	12	t	t	NOUN
ijpds-4231	220	13	-	-	PUNCT
ijpds-4231	220	14	butoxide	butoxide	NOUN
ijpds-4231	220	15	.	.	PUNCT
ijpds-4231	221	1	to	to	ADP
ijpds-4231	221	2	the	the	DET
ijpds-4231	221	3	reaction	reaction	NOUN
ijpds-4231	221	4	mass	mass	PROPN
ijpds-4231	221	5	,	,	PUNCT
ijpds-4231	221	6	7	7	NUM
ijpds-4231	221	7	was	be	AUX
ijpds-4231	221	8	added	add	VERB
ijpds-4231	221	9	to	to	PART
ijpds-4231	221	10	isolate	isolate	VERB
ijpds-4231	221	11	n-(2,3	n-(2,3	ADJ
ijpds-4231	221	12	-	-	PUNCT
ijpds-4231	221	13	dihydro-1h	dihydro-1h	NOUN
ijpds-4231	221	14	-	-	PUNCT
ijpds-4231	221	15	inden-1	inden-1	NOUN
ijpds-4231	221	16	-	-	PUNCT
ijpds-4231	221	17	yl)-2methyl	yl)-2methyl	NOUN
ijpds-4231	221	18	-	-	PUNCT
ijpds-4231	221	19	n-(prop-2	n-(prop-2	NUM
ijpds-4231	221	20	-	-	PUNCT
ijpds-4231	221	21	yn-1	yn-1	NOUN
ijpds-4231	221	22	-	-	PUNCT
ijpds-4231	221	23	yl)propane-2	yl)propane-2	NOUN
ijpds-4231	221	24	-	-	PUNCT
ijpds-4231	221	25	sulfinamide	sulfinamide	NOUN
ijpds-4231	221	26	32	32	NUM
ijpds-4231	221	27	(	(	PUNCT
ijpds-4231	221	28	yield	yield	NOUN
ijpds-4231	221	29	:	:	PUNCT
ijpds-4231	221	30	51	51	NUM
ijpds-4231	221	31	%	%	NOUN
ijpds-4231	221	32	from	from	ADP
ijpds-4231	221	33	9	9	NUM
ijpds-4231	221	34	)	)	PUNCT
ijpds-4231	221	35	.	.	PUNCT
ijpds-4231	222	1	the	the	DET
ijpds-4231	222	2	solution	solution	NOUN
ijpds-4231	222	3	of	of	ADP
ijpds-4231	222	4	methanesulfonic	methanesulfonic	ADJ
ijpds-4231	222	5	acid	acid	NOUN
ijpds-4231	222	6	in	in	ADP
ijpds-4231	222	7	diethyl	diethyl	NOUN
ijpds-4231	222	8	ether	ether	NOUN
ijpds-4231	222	9	was	be	AUX
ijpds-4231	222	10	added	add	VERB
ijpds-4231	222	11	to	to	ADP
ijpds-4231	222	12	the	the	DET
ijpds-4231	222	13	solution	solution	NOUN
ijpds-4231	222	14	of	of	ADP
ijpds-4231	222	15	32	32	NUM
ijpds-4231	222	16	in	in	ADP
ijpds-4231	222	17	methyl	methyl	NOUN
ijpds-4231	222	18	alcohol	alcohol	NOUN
ijpds-4231	222	19	to	to	PART
ijpds-4231	222	20	isolate	isolate	VERB
ijpds-4231	222	21	the	the	DET
ijpds-4231	222	22	enantiomerically	enantiomerically	ADV
ijpds-4231	222	23	pure	pure	ADJ
ijpds-4231	222	24	1	1	NUM
ijpds-4231	222	25	with	with	ADP
ijpds-4231	222	26	a	a	DET
ijpds-4231	222	27	melting	melting	NOUN
ijpds-4231	222	28	point	point	NOUN
ijpds-4231	222	29	of	of	ADP
ijpds-4231	222	30	156	156	NUM
ijpds-4231	222	31	-	-	PUNCT
ijpds-4231	222	32	158oc	158oc	NOUN
ijpds-4231	222	33	(	(	PUNCT
ijpds-4231	222	34	yield	yield	NOUN
ijpds-4231	222	35	:	:	PUNCT
ijpds-4231	222	36	46	46	NUM
ijpds-4231	222	37	%	%	NOUN
ijpds-4231	222	38	from	from	ADP
ijpds-4231	222	39	9	9	NUM
ijpds-4231	222	40	,	,	PUNCT
ijpds-4231	222	41	as	as	ADP
ijpds-4231	222	42	white	white	ADJ
ijpds-4231	222	43	crystals	crystal	NOUN
ijpds-4231	222	44	,	,	PUNCT
ijpds-4231	222	45	isolated	isolate	VERB
ijpds-4231	222	46	from	from	ADP
ijpds-4231	222	47	methyl	methyl	NOUN
ijpds-4231	222	48	-	-	PUNCT
ijpds-4231	222	49	t	t	NOUN
ijpds-4231	222	50	-	-	PUNCT
ijpds-4231	222	51	butyl	butyl	NOUN
ijpds-4231	222	52	ether	ether	NOUN
ijpds-4231	222	53	)	)	PUNCT
ijpds-4231	223	1	[	[	X
ijpds-4231	223	2	40	40	NUM
ijpds-4231	223	3	]	]	PUNCT
ijpds-4231	223	4	.	.	PUNCT
ijpds-4231	224	1	chi	chi	PROPN
ijpds-4231	224	2	-	-	PUNCT
ijpds-4231	224	3	hsiang	hsiang	PROPN
ijpds-4231	224	4	y	y	PROPN
ijpds-4231	224	5	&	&	CCONJ
ijpds-4231	224	6	tsung	tsung	PROPN
ijpds-4231	224	7	-	-	PUNCT
ijpds-4231	224	8	ting	ting	PROPN
ijpds-4231	224	9	c.	c.	PROPN
ijpds-4231	224	10	,	,	PUNCT
ijpds-4231	224	11	in	in	ADP
ijpds-4231	224	12	2011	2011	NUM
ijpds-4231	224	13	,	,	PUNCT
ijpds-4231	224	14	had	have	AUX
ijpds-4231	224	15	reported	report	VERB
ijpds-4231	224	16	the	the	DET
ijpds-4231	224	17	condensation	condensation	NOUN
ijpds-4231	224	18	of	of	ADP
ijpds-4231	224	19	9	9	NUM
ijpds-4231	224	20	with	with	ADP
ijpds-4231	224	21	6	6	NUM
ijpds-4231	224	22	in	in	ADP
ijpds-4231	224	23	methyl	methyl	NOUN
ijpds-4231	224	24	-	-	PUNCT
ijpds-4231	224	25	t	t	NOUN
ijpds-4231	224	26	-	-	PUNCT
ijpds-4231	224	27	butyl	butyl	NOUN
ijpds-4231	224	28	ether	ether	NOUN
ijpds-4231	224	29	using	use	VERB
ijpds-4231	224	30	ptoluene	ptoluene	PROPN
ijpds-4231	224	31	sulfonic	sulfonic	ADJ
ijpds-4231	224	32	acid	acid	NOUN
ijpds-4231	224	33	to	to	PART
ijpds-4231	224	34	form	form	VERB
ijpds-4231	224	35	the	the	DET
ijpds-4231	224	36	intermediate	intermediate	ADJ
ijpds-4231	224	37	16	16	NUM
ijpds-4231	224	38	.	.	PUNCT
ijpds-4231	225	1	it	it	PRON
ijpds-4231	225	2	was	be	AUX
ijpds-4231	225	3	effectively	effectively	ADV
ijpds-4231	225	4	reduced	reduce	VERB
ijpds-4231	225	5	using	use	VERB
ijpds-4231	225	6	20	20	NUM
ijpds-4231	225	7	%	%	NOUN
ijpds-4231	225	8	di	di	NOUN
ijpds-4231	225	9	-	-	NOUN
ijpds-4231	225	10	isobutyl	isobutyl	NOUN
ijpds-4231	225	11	-	-	PUNCT
ijpds-4231	225	12	aluminumhydride	aluminumhydride	NOUN
ijpds-4231	225	13	(	(	PUNCT
ijpds-4231	225	14	dibal	dibal	ADJ
ijpds-4231	225	15	-	-	PUNCT
ijpds-4231	225	16	h	h	NOUN
ijpds-4231	225	17	)	)	PUNCT
ijpds-4231	225	18	in	in	ADP
ijpds-4231	225	19	hexane	hexane	NOUN
ijpds-4231	225	20	to	to	PART
ijpds-4231	225	21	isolate	isolate	VERB
ijpds-4231	225	22	the	the	DET
ijpds-4231	225	23	racemic	racemic	ADJ
ijpds-4231	225	24	rasagiline	rasagiline	NOUN
ijpds-4231	225	25	base	base	NOUN
ijpds-4231	225	26	(	(	PUNCT
ijpds-4231	225	27	yield	yield	NOUN
ijpds-4231	225	28	:	:	PUNCT
ijpds-4231	225	29	81	81	NUM
ijpds-4231	225	30	%	%	NOUN
ijpds-4231	225	31	)	)	PUNCT
ijpds-4231	225	32	.	.	PUNCT
ijpds-4231	226	1	it	it	PRON
ijpds-4231	226	2	was	be	AUX
ijpds-4231	226	3	treated	treat	VERB
ijpds-4231	226	4	with	with	ADP
ijpds-4231	226	5	s-(+)mandelic	s-(+)mandelic	ADJ
ijpds-4231	226	6	acid	acid	NOUN
ijpds-4231	226	7	in	in	ADP
ijpds-4231	226	8	methyl	methyl	NOUN
ijpds-4231	226	9	-	-	PUNCT
ijpds-4231	226	10	t	t	NOUN
ijpds-4231	226	11	-	-	PUNCT
ijpds-4231	226	12	butyl	butyl	NOUN
ijpds-4231	226	13	ether	ether	NOUN
ijpds-4231	226	14	to	to	PART
ijpds-4231	226	15	isolate	isolate	VERB
ijpds-4231	226	16	rrasagiline	rrasagiline	ADJ
ijpds-4231	226	17	mandelate	mandelate	NOUN
ijpds-4231	226	18	(	(	PUNCT
ijpds-4231	226	19	yield	yield	NOUN
ijpds-4231	226	20	:	:	PUNCT
ijpds-4231	226	21	45	45	NUM
ijpds-4231	226	22	%	%	NOUN
ijpds-4231	226	23	)	)	PUNCT
ijpds-4231	226	24	.	.	PUNCT
ijpds-4231	227	1	de	de	X
ijpds-4231	227	2	-	-	PUNCT
ijpds-4231	227	3	salting	salt	VERB
ijpds-4231	227	4	it	it	PRON
ijpds-4231	227	5	with	with	ADP
ijpds-4231	227	6	2	2	NUM
ijpds-4231	227	7	%	%	NOUN
ijpds-4231	227	8	sodium	sodium	NOUN
ijpds-4231	227	9	hydroxide	hydroxide	NOUN
ijpds-4231	227	10	solution	solution	NOUN
ijpds-4231	227	11	gave	give	VERB
ijpds-4231	227	12	r	r	NOUN
ijpds-4231	227	13	-	-	PUNCT
ijpds-4231	227	14	rasagiline	rasagiline	NOUN
ijpds-4231	227	15	base	base	NOUN
ijpds-4231	227	16	(	(	PUNCT
ijpds-4231	227	17	yield	yield	NOUN
ijpds-4231	227	18	:	:	PUNCT
ijpds-4231	227	19	90	90	NUM
ijpds-4231	227	20	%	%	NOUN
ijpds-4231	227	21	)	)	PUNCT
ijpds-4231	227	22	.	.	PUNCT
ijpds-4231	228	1	it	it	PRON
ijpds-4231	228	2	was	be	AUX
ijpds-4231	228	3	treated	treat	VERB
ijpds-4231	228	4	with	with	ADP
ijpds-4231	228	5	methanesulfonic	methanesulfonic	ADJ
ijpds-4231	228	6	acid	acid	NOUN
ijpds-4231	228	7	in	in	ADP
ijpds-4231	228	8	isopropyl	isopropyl	NOUN
ijpds-4231	228	9	alcohol	alcohol	NOUN
ijpds-4231	228	10	to	to	PART
ijpds-4231	228	11	isolate	isolate	VERB
ijpds-4231	228	12	1	1	NUM
ijpds-4231	228	13	(	(	PUNCT
ijpds-4231	228	14	yield	yield	NOUN
ijpds-4231	228	15	:	:	PUNCT
ijpds-4231	228	16	80	80	NUM
ijpds-4231	228	17	%	%	NOUN
ijpds-4231	228	18	)	)	PUNCT
ijpds-4231	229	1	[	[	X
ijpds-4231	229	2	41	41	NUM
ijpds-4231	229	3	]	]	PUNCT
ijpds-4231	229	4	.	.	PUNCT
ijpds-4231	230	1	gore	gore	PROPN
ijpds-4231	230	2	v	v	PROPN
ijpds-4231	230	3	,	,	PUNCT
ijpds-4231	230	4	et	et	PROPN
ijpds-4231	230	5	al	al	PROPN
ijpds-4231	230	6	.	.	PROPN
ijpds-4231	230	7	,	,	PUNCT
ijpds-4231	230	8	in	in	ADP
ijpds-4231	230	9	2011	2011	NUM
ijpds-4231	230	10	,	,	PUNCT
ijpds-4231	230	11	had	have	AUX
ijpds-4231	230	12	illustrated	illustrate	VERB
ijpds-4231	230	13	the	the	DET
ijpds-4231	230	14	condensation	condensation	NOUN
ijpds-4231	230	15	of	of	ADP
ijpds-4231	230	16	r	r	NOUN
ijpds-4231	230	17	-	-	PUNCT
ijpds-4231	230	18	isomer	isomer	NOUN
ijpds-4231	230	19	of	of	ADP
ijpds-4231	230	20	2	2	NUM
ijpds-4231	230	21	with	with	ADP
ijpds-4231	230	22	8	8	NUM
ijpds-4231	230	23	under	under	ADP
ijpds-4231	230	24	the	the	DET
ijpds-4231	230	25	influence	influence	NOUN
ijpds-4231	230	26	of	of	ADP
ijpds-4231	230	27	1,8diazabicyclo-[5,4,0]-undec-7	1,8diazabicyclo-[5,4,0]-undec-7	ADJ
ijpds-4231	230	28	-	-	PUNCT
ijpds-4231	230	29	ene	ene	NOUN
ijpds-4231	230	30	(	(	PUNCT
ijpds-4231	230	31	dbu	dbu	PROPN
ijpds-4231	230	32	)	)	PUNCT
ijpds-4231	230	33	in	in	ADP
ijpds-4231	230	34	tetrahydrofuran	tetrahydrofuran	NOUN
ijpds-4231	230	35	to	to	PART
ijpds-4231	230	36	get	get	VERB
ijpds-4231	230	37	r	r	NOUN
ijpds-4231	230	38	-	-	PUNCT
ijpds-4231	230	39	rasagiline	rasagiline	NOUN
ijpds-4231	230	40	base	base	NOUN
ijpds-4231	230	41	(	(	PUNCT
ijpds-4231	230	42	yield	yield	NOUN
ijpds-4231	230	43	:	:	PUNCT
ijpds-4231	230	44	80	80	NUM
ijpds-4231	230	45	-	-	SYM
ijpds-4231	230	46	82	82	NUM
ijpds-4231	230	47	%	%	NOUN
ijpds-4231	230	48	,	,	PUNCT
ijpds-4231	230	49	sanjay	sanjay	PROPN
ijpds-4231	230	50	s	s	PROPN
ijpds-4231	230	51	s	s	NOUN
ijpds-4231	230	52	patents	patent	NOUN
ijpds-4231	230	53	disclosed	disclose	VERB
ijpds-4231	230	54	synthetic	synthetic	ADJ
ijpds-4231	230	55	overview	overview	NOUN
ijpds-4231	230	56	of	of	ADP
ijpds-4231	230	57	rasagiline	rasagiline	ADJ
ijpds-4231	230	58	vol	vol	NOUN
ijpds-4231	230	59	2	2	NUM
ijpds-4231	230	60	|	|	ADV
ijpds-4231	230	61	issue	issue	VERB
ijpds-4231	230	62	4	4	NUM
ijpds-4231	230	63	|	|	ADV
ijpds-4231	230	64	oct	oct	PROPN
ijpds-4231	230	65	–	–	PUNCT
ijpds-4231	230	66	dec	dec	PROPN
ijpds-4231	230	67	2023	2023	NUM
ijpds-4231	230	68	indian	indian	PROPN
ijpds-4231	230	69	j	j	PROPN
ijpds-4231	230	70	pharm	pharm	PROPN
ijpds-4231	230	71	drug	drug	PROPN
ijpds-4231	230	72	studies	study	NOUN
ijpds-4231	230	73	|	|	ADV
ijpds-4231	230	74	138	138	NUM
ijpds-4231	230	75	purity	purity	NOUN
ijpds-4231	230	76	:	:	PUNCT
ijpds-4231	230	77	64.33	64.33	NUM
ijpds-4231	230	78	%	%	NOUN
ijpds-4231	230	79	by	by	ADP
ijpds-4231	230	80	hplc	hplc	NOUN
ijpds-4231	230	81	,	,	PUNCT
ijpds-4231	230	82	as	as	ADP
ijpds-4231	230	83	yellow	yellow	ADJ
ijpds-4231	230	84	oily	oily	ADJ
ijpds-4231	230	85	mass	mass	NOUN
ijpds-4231	230	86	)	)	PUNCT
ijpds-4231	230	87	.	.	PUNCT
ijpds-4231	231	1	it	it	PRON
ijpds-4231	231	2	was	be	AUX
ijpds-4231	231	3	treated	treat	VERB
ijpds-4231	231	4	with	with	ADP
ijpds-4231	231	5	methanesulfonic	methanesulfonic	ADJ
ijpds-4231	231	6	acid	acid	NOUN
ijpds-4231	231	7	in	in	ADP
ijpds-4231	231	8	isopropyl	isopropyl	NOUN
ijpds-4231	231	9	alcohol	alcohol	NOUN
ijpds-4231	231	10	to	to	PART
ijpds-4231	231	11	isolate	isolate	VERB
ijpds-4231	231	12	1	1	NUM
ijpds-4231	231	13	(	(	PUNCT
ijpds-4231	231	14	yield	yield	NOUN
ijpds-4231	231	15	:	:	PUNCT
ijpds-4231	231	16	47	47	NUM
ijpds-4231	231	17	%	%	NOUN
ijpds-4231	231	18	,	,	PUNCT
ijpds-4231	231	19	purity	purity	NOUN
ijpds-4231	231	20	:	:	PUNCT
ijpds-4231	231	21	99.84	99.84	NUM
ijpds-4231	231	22	%	%	NOUN
ijpds-4231	231	23	,	,	PUNCT
ijpds-4231	231	24	chiral	chiral	ADJ
ijpds-4231	231	25	purity	purity	NOUN
ijpds-4231	231	26	:	:	PUNCT
ijpds-4231	231	27	100	100	NUM
ijpds-4231	231	28	%	%	NOUN
ijpds-4231	231	29	by	by	ADP
ijpds-4231	231	30	hplc	hplc	NOUN
ijpds-4231	231	31	)	)	PUNCT
ijpds-4231	232	1	[	[	X
ijpds-4231	232	2	42	42	NUM
ijpds-4231	232	3	]	]	PUNCT
ijpds-4231	232	4	.	.	PUNCT
ijpds-4231	233	1	thanedar	thanedar	PROPN
ijpds-4231	233	2	aa	aa	INTJ
ijpds-4231	233	3	,	,	PUNCT
ijpds-4231	233	4	et	et	PROPN
ijpds-4231	233	5	al	al	PROPN
ijpds-4231	233	6	.	.	PROPN
ijpds-4231	233	7	,	,	PUNCT
ijpds-4231	233	8	in	in	ADP
ijpds-4231	233	9	2011	2011	NUM
ijpds-4231	233	10	,	,	PUNCT
ijpds-4231	233	11	had	have	AUX
ijpds-4231	233	12	demonstrated	demonstrate	VERB
ijpds-4231	233	13	a	a	DET
ijpds-4231	233	14	comparative	comparative	ADJ
ijpds-4231	233	15	example	example	NOUN
ijpds-4231	233	16	to	to	PART
ijpds-4231	233	17	condense	condense	VERB
ijpds-4231	233	18	racemic	racemic	ADJ
ijpds-4231	233	19	2	2	NUM
ijpds-4231	233	20	in	in	ADP
ijpds-4231	233	21	acetonitrile	acetonitrile	NOUN
ijpds-4231	233	22	with	with	ADP
ijpds-4231	233	23	7	7	NUM
ijpds-4231	233	24	in	in	ADP
ijpds-4231	233	25	the	the	DET
ijpds-4231	233	26	presence	presence	NOUN
ijpds-4231	233	27	of	of	ADP
ijpds-4231	233	28	potassium	potassium	NOUN
ijpds-4231	233	29	carbonate	carbonate	NOUN
ijpds-4231	233	30	to	to	PART
ijpds-4231	233	31	isolate	isolate	VERB
ijpds-4231	233	32	racemic	racemic	ADJ
ijpds-4231	233	33	rasagiline	rasagiline	NOUN
ijpds-4231	233	34	base	base	NOUN
ijpds-4231	233	35	(	(	PUNCT
ijpds-4231	233	36	yield	yield	NOUN
ijpds-4231	233	37	:	:	PUNCT
ijpds-4231	233	38	101	101	NUM
ijpds-4231	233	39	%	%	NOUN
ijpds-4231	233	40	,	,	PUNCT
ijpds-4231	233	41	purity	purity	NOUN
ijpds-4231	233	42	:	:	PUNCT
ijpds-4231	233	43	72.33	72.33	NUM
ijpds-4231	233	44	%	%	NOUN
ijpds-4231	233	45	by	by	ADP
ijpds-4231	233	46	hplc	hplc	NOUN
ijpds-4231	233	47	,	,	PUNCT
ijpds-4231	233	48	as	as	ADP
ijpds-4231	233	49	oily	oily	ADJ
ijpds-4231	233	50	residue	residue	NOUN
ijpds-4231	233	51	)	)	PUNCT
ijpds-4231	233	52	.	.	PUNCT
ijpds-4231	234	1	it	it	PRON
ijpds-4231	234	2	was	be	AUX
ijpds-4231	234	3	done	do	VERB
ijpds-4231	234	4	as	as	ADP
ijpds-4231	234	5	per	per	ADP
ijpds-4231	234	6	the	the	DET
ijpds-4231	234	7	previous	previous	ADJ
ijpds-4231	234	8	disclosure	disclosure	NOUN
ijpds-4231	234	9	[	[	X
ijpds-4231	234	10	10	10	NUM
ijpds-4231	234	11	]	]	PUNCT
ijpds-4231	234	12	.	.	PUNCT
ijpds-4231	235	1	in	in	ADP
ijpds-4231	235	2	another	another	DET
ijpds-4231	235	3	example	example	NOUN
ijpds-4231	235	4	,	,	PUNCT
ijpds-4231	235	5	9	9	NUM
ijpds-4231	235	6	in	in	ADP
ijpds-4231	235	7	ethyl	ethyl	PROPN
ijpds-4231	235	8	alcohol	alcohol	NOUN
ijpds-4231	235	9	was	be	AUX
ijpds-4231	235	10	reacted	react	VERB
ijpds-4231	235	11	with	with	ADP
ijpds-4231	235	12	6	6	NUM
ijpds-4231	235	13	in	in	ADP
ijpds-4231	235	14	the	the	DET
ijpds-4231	235	15	presence	presence	NOUN
ijpds-4231	235	16	of	of	ADP
ijpds-4231	235	17	titanium	titanium	NOUN
ijpds-4231	235	18	(	(	PUNCT
ijpds-4231	235	19	iv	iv	NOUN
ijpds-4231	235	20	)	)	PUNCT
ijpds-4231	235	21	isopropoxide	isopropoxide	NOUN
ijpds-4231	235	22	to	to	PART
ijpds-4231	235	23	form	form	VERB
ijpds-4231	235	24	the	the	DET
ijpds-4231	235	25	respective	respective	ADJ
ijpds-4231	235	26	titanium	titanium	NOUN
ijpds-4231	235	27	complex	complex	NOUN
ijpds-4231	235	28	.	.	PUNCT
ijpds-4231	236	1	it	it	PRON
ijpds-4231	236	2	was	be	AUX
ijpds-4231	236	3	reduced	reduce	VERB
ijpds-4231	236	4	by	by	ADP
ijpds-4231	236	5	sodium	sodium	NOUN
ijpds-4231	236	6	borohydride	borohydride	NOUN
ijpds-4231	236	7	and	and	CCONJ
ijpds-4231	236	8	performed	perform	VERB
ijpds-4231	236	9	acid	acid	NOUN
ijpds-4231	236	10	-	-	PUNCT
ijpds-4231	236	11	base	base	NOUN
ijpds-4231	236	12	isolation	isolation	NOUN
ijpds-4231	236	13	to	to	PART
ijpds-4231	236	14	get	get	VERB
ijpds-4231	236	15	racemic	racemic	ADJ
ijpds-4231	236	16	rasagiline	rasagiline	NOUN
ijpds-4231	236	17	base	base	NOUN
ijpds-4231	236	18	(	(	PUNCT
ijpds-4231	236	19	yield	yield	NOUN
ijpds-4231	236	20	:	:	PUNCT
ijpds-4231	236	21	22.57	22.57	NUM
ijpds-4231	236	22	%	%	NOUN
ijpds-4231	236	23	,	,	PUNCT
ijpds-4231	236	24	purity	purity	NOUN
ijpds-4231	236	25	:	:	PUNCT
ijpds-4231	236	26	98	98	NUM
ijpds-4231	236	27	%	%	NOUN
ijpds-4231	236	28	by	by	ADP
ijpds-4231	236	29	hplc	hplc	NOUN
ijpds-4231	236	30	)	)	PUNCT
ijpds-4231	236	31	.	.	PUNCT
ijpds-4231	237	1	it	it	PRON
ijpds-4231	237	2	was	be	AUX
ijpds-4231	237	3	resolved	resolve	VERB
ijpds-4231	237	4	using	use	VERB
ijpds-4231	237	5	l-(+)-tartaric	l-(+)-tartaric	ADJ
ijpds-4231	237	6	acid	acid	NOUN
ijpds-4231	237	7	in	in	ADP
ijpds-4231	237	8	isopropyl	isopropyl	NOUN
ijpds-4231	237	9	alcohol	alcohol	NOUN
ijpds-4231	237	10	to	to	PART
ijpds-4231	237	11	isolate	isolate	VERB
ijpds-4231	237	12	the	the	DET
ijpds-4231	237	13	crude	crude	ADJ
ijpds-4231	237	14	salt	salt	NOUN
ijpds-4231	237	15	.	.	PUNCT
ijpds-4231	238	1	it	it	PRON
ijpds-4231	238	2	was	be	AUX
ijpds-4231	238	3	recrystallized	recrystallize	VERB
ijpds-4231	238	4	from	from	ADP
ijpds-4231	238	5	methyl	methyl	NOUN
ijpds-4231	238	6	alcohol	alcohol	NOUN
ijpds-4231	238	7	to	to	PART
ijpds-4231	238	8	isolate	isolate	VERB
ijpds-4231	238	9	r	r	NOUN
ijpds-4231	238	10	-	-	PUNCT
ijpds-4231	238	11	rasagiline	rasagiline	NOUN
ijpds-4231	238	12	tartarate	tartarate	NOUN
ijpds-4231	238	13	(	(	PUNCT
ijpds-4231	238	14	recovery	recovery	NOUN
ijpds-4231	238	15	:	:	PUNCT
ijpds-4231	238	16	80	80	NUM
ijpds-4231	238	17	%	%	NOUN
ijpds-4231	238	18	,	,	PUNCT
ijpds-4231	238	19	purity	purity	NOUN
ijpds-4231	238	20	:	:	PUNCT
ijpds-4231	238	21	99.89	99.89	NUM
ijpds-4231	238	22	%	%	NOUN
ijpds-4231	238	23	by	by	ADP
ijpds-4231	238	24	hplc	hplc	NOUN
ijpds-4231	238	25	)	)	PUNCT
ijpds-4231	238	26	.	.	PUNCT
ijpds-4231	239	1	it	it	PRON
ijpds-4231	239	2	was	be	AUX
ijpds-4231	239	3	de	de	ADJ
ijpds-4231	239	4	-	-	VERB
ijpds-4231	239	5	salted	salt	VERB
ijpds-4231	239	6	and	and	CCONJ
ijpds-4231	239	7	treated	treat	VERB
ijpds-4231	239	8	with	with	ADP
ijpds-4231	239	9	methanesulfonic	methanesulfonic	ADJ
ijpds-4231	239	10	acid	acid	NOUN
ijpds-4231	239	11	in	in	ADP
ijpds-4231	239	12	acetone	acetone	NOUN
ijpds-4231	239	13	to	to	PART
ijpds-4231	239	14	isolate	isolate	VERB
ijpds-4231	239	15	1	1	NUM
ijpds-4231	239	16	(	(	PUNCT
ijpds-4231	239	17	yield	yield	NOUN
ijpds-4231	239	18	:	:	PUNCT
ijpds-4231	239	19	72.12	72.12	NUM
ijpds-4231	239	20	%	%	NOUN
ijpds-4231	239	21	,	,	PUNCT
ijpds-4231	239	22	purity	purity	NOUN
ijpds-4231	239	23	:	:	PUNCT
ijpds-4231	239	24	99.97	99.97	NUM
ijpds-4231	239	25	%	%	NOUN
ijpds-4231	239	26	by	by	ADP
ijpds-4231	239	27	hplc	hplc	PROPN
ijpds-4231	239	28	)	)	PUNCT
ijpds-4231	239	29	.	.	PUNCT
ijpds-4231	240	1	a	a	DET
ijpds-4231	240	2	direct	direct	ADJ
ijpds-4231	240	3	conversion	conversion	NOUN
ijpds-4231	240	4	process	process	NOUN
ijpds-4231	240	5	of	of	ADP
ijpds-4231	240	6	tartarate	tartarate	ADJ
ijpds-4231	240	7	salt	salt	NOUN
ijpds-4231	240	8	to	to	ADP
ijpds-4231	240	9	1	1	NUM
ijpds-4231	240	10	(	(	PUNCT
ijpds-4231	240	11	yield	yield	NOUN
ijpds-4231	240	12	:	:	PUNCT
ijpds-4231	240	13	88.14	88.14	NUM
ijpds-4231	240	14	%	%	NOUN
ijpds-4231	240	15	,	,	PUNCT
ijpds-4231	240	16	purity	purity	NOUN
ijpds-4231	240	17	:	:	PUNCT
ijpds-4231	240	18	99.5	99.5	NUM
ijpds-4231	240	19	%	%	NOUN
ijpds-4231	240	20	,	,	PUNCT
ijpds-4231	240	21	chiral	chiral	ADJ
ijpds-4231	240	22	purity	purity	NOUN
ijpds-4231	240	23	:	:	PUNCT
ijpds-4231	240	24	99.9	99.9	NUM
ijpds-4231	240	25	%	%	NOUN
ijpds-4231	240	26	by	by	ADP
ijpds-4231	240	27	hplc	hplc	PROPN
ijpds-4231	240	28	)	)	PUNCT
ijpds-4231	240	29	was	be	AUX
ijpds-4231	240	30	also	also	ADV
ijpds-4231	240	31	reported	report	VERB
ijpds-4231	240	32	[	[	X
ijpds-4231	240	33	43	43	NUM
ijpds-4231	240	34	]	]	PUNCT
ijpds-4231	240	35	.	.	PUNCT
ijpds-4231	241	1	selic	selic	PROPN
ijpds-4231	241	2	l.	l.	PROPN
ijpds-4231	241	3	,	,	PUNCT
ijpds-4231	241	4	in	in	ADP
ijpds-4231	241	5	2011	2011	NUM
ijpds-4231	241	6	,	,	PUNCT
ijpds-4231	241	7	had	have	AUX
ijpds-4231	241	8	disclosed	disclose	VERB
ijpds-4231	241	9	the	the	DET
ijpds-4231	241	10	preparation	preparation	NOUN
ijpds-4231	241	11	of	of	ADP
ijpds-4231	241	12	a	a	DET
ijpds-4231	241	13	few	few	ADJ
ijpds-4231	241	14	salts	salt	NOUN
ijpds-4231	241	15	of	of	ADP
ijpds-4231	241	16	rasagiline	rasagiline	NOUN
ijpds-4231	241	17	and	and	CCONJ
ijpds-4231	241	18	those	those	PRON
ijpds-4231	241	19	are	be	AUX
ijpds-4231	241	20	exclusively	exclusively	ADV
ijpds-4231	241	21	used	use	VERB
ijpds-4231	241	22	to	to	PART
ijpds-4231	241	23	resolve	resolve	VERB
ijpds-4231	241	24	racemic	racemic	ADJ
ijpds-4231	241	25	rasagiline	rasagiline	NOUN
ijpds-4231	241	26	base	base	NOUN
ijpds-4231	241	27	.	.	PUNCT
ijpds-4231	242	1	the	the	DET
ijpds-4231	242	2	major	major	ADJ
ijpds-4231	242	3	salts	salt	NOUN
ijpds-4231	242	4	reported	report	VERB
ijpds-4231	242	5	are	be	AUX
ijpds-4231	242	6	rasagiline	rasagiline	ADJ
ijpds-4231	242	7	-	-	PUNCT
ijpds-4231	242	8	l	l	NOUN
ijpds-4231	242	9	-	-	NOUN
ijpds-4231	242	10	mandelate	mandelate	ADJ
ijpds-4231	242	11	,	,	PUNCT
ijpds-4231	242	12	rasagiline	rasagiline	NOUN
ijpds-4231	242	13	-	-	ADJ
ijpds-4231	242	14	d	d	NOUN
ijpds-4231	242	15	-	-	NOUN
ijpds-4231	242	16	mandelate	mandelate	ADJ
ijpds-4231	242	17	,	,	PUNCT
ijpds-4231	242	18	rasagiline	rasagiline	NOUN
ijpds-4231	242	19	-	-	PUNCT
ijpds-4231	242	20	r	r	NOUN
ijpds-4231	242	21	-	-	PUNCT
ijpds-4231	242	22	mandelate	mandelate	NOUN
ijpds-4231	242	23	(	(	PUNCT
ijpds-4231	242	24	yield	yield	NOUN
ijpds-4231	242	25	:	:	PUNCT
ijpds-4231	242	26	33	33	NUM
ijpds-4231	242	27	%	%	NOUN
ijpds-4231	242	28	,	,	PUNCT
ijpds-4231	242	29	with	with	ADP
ijpds-4231	242	30	a	a	DET
ijpds-4231	242	31	melting	melting	NOUN
ijpds-4231	242	32	point	point	NOUN
ijpds-4231	242	33	of	of	ADP
ijpds-4231	242	34	107	107	NUM
ijpds-4231	242	35	-	-	PUNCT
ijpds-4231	242	36	111oc	111oc	NOUN
ijpds-4231	242	37	)	)	PUNCT
ijpds-4231	242	38	,	,	PUNCT
ijpds-4231	242	39	r	r	NOUN
ijpds-4231	242	40	-	-	PUNCT
ijpds-4231	242	41	rasagiline-(+)-camphor-10	rasagiline-(+)-camphor-10	NOUN
ijpds-4231	242	42	-	-	NOUN
ijpds-4231	242	43	sulfonate	sulfonate	ADJ
ijpds-4231	242	44	(	(	PUNCT
ijpds-4231	242	45	yield	yield	NOUN
ijpds-4231	242	46	:	:	PUNCT
ijpds-4231	242	47	27	27	NUM
ijpds-4231	242	48	%	%	NOUN
ijpds-4231	242	49	,	,	PUNCT
ijpds-4231	242	50	with	with	ADP
ijpds-4231	242	51	a	a	DET
ijpds-4231	242	52	melting	melting	NOUN
ijpds-4231	242	53	point	point	NOUN
ijpds-4231	242	54	of	of	ADP
ijpds-4231	242	55	167	167	NUM
ijpds-4231	242	56	-	-	PUNCT
ijpds-4231	242	57	170oc	170oc	PROPN
ijpds-4231	242	58	)	)	PUNCT
ijpds-4231	242	59	,	,	PUNCT
ijpds-4231	242	60	rasagiline	rasagiline	NOUN
ijpds-4231	242	61	orotate	orotate	NOUN
ijpds-4231	242	62	,	,	PUNCT
ijpds-4231	242	63	rasagiline	rasagiline	NOUN
ijpds-4231	242	64	cinnamate	cinnamate	NOUN
ijpds-4231	242	65	,	,	PUNCT
ijpds-4231	242	66	rasagiline-1hydroxy-2	rasagiline-1hydroxy-2	NOUN
ijpds-4231	242	67	-	-	PUNCT
ijpds-4231	242	68	naftoate	naftoate	NOUN
ijpds-4231	242	69	,	,	PUNCT
ijpds-4231	242	70	rasagiline	rasagiline	NOUN
ijpds-4231	242	71	fumarate	fumarate	NOUN
ijpds-4231	242	72	,	,	PUNCT
ijpds-4231	242	73	rasagiline	rasagiline	NOUN
ijpds-4231	242	74	benzoate	benzoate	NOUN
ijpds-4231	242	75	and	and	CCONJ
ijpds-4231	242	76	rasagiline-(-)-camphor-10	rasagiline-(-)-camphor-10	PROPN
ijpds-4231	242	77	-	-	NOUN
ijpds-4231	242	78	sulfonate	sulfonate	NOUN
ijpds-4231	242	79	.	.	PUNCT
ijpds-4231	243	1	the	the	DET
ijpds-4231	243	2	work	work	NOUN
ijpds-4231	243	3	also	also	ADV
ijpds-4231	243	4	had	have	AUX
ijpds-4231	243	5	disclosed	disclose	VERB
ijpds-4231	243	6	the	the	DET
ijpds-4231	243	7	recrystallization	recrystallization	NOUN
ijpds-4231	243	8	methods	method	NOUN
ijpds-4231	243	9	of	of	ADP
ijpds-4231	243	10	those	those	DET
ijpds-4231	243	11	salts	salt	NOUN
ijpds-4231	243	12	along	along	ADP
ijpds-4231	243	13	with	with	ADP
ijpds-4231	243	14	an	an	DET
ijpds-4231	243	15	efficient	efficient	ADJ
ijpds-4231	243	16	analysis	analysis	NOUN
ijpds-4231	243	17	method	method	NOUN
ijpds-4231	243	18	[	[	X
ijpds-4231	243	19	44	44	NUM
ijpds-4231	243	20	]	]	PUNCT
ijpds-4231	243	21	.	.	PUNCT
ijpds-4231	244	1	zope	zope	PROPN
ijpds-4231	244	2	ss	ss	PROPN
ijpds-4231	244	3	,	,	PUNCT
ijpds-4231	244	4	et	et	PROPN
ijpds-4231	244	5	al	al	PROPN
ijpds-4231	244	6	.	.	PROPN
ijpds-4231	244	7	,	,	PUNCT
ijpds-4231	244	8	in	in	ADP
ijpds-4231	244	9	2011	2011	NUM
ijpds-4231	244	10	,	,	PUNCT
ijpds-4231	244	11	had	have	AUX
ijpds-4231	244	12	demonstrated	demonstrate	VERB
ijpds-4231	244	13	the	the	DET
ijpds-4231	244	14	synthesis	synthesis	NOUN
ijpds-4231	244	15	of	of	ADP
ijpds-4231	244	16	some	some	DET
ijpds-4231	244	17	rasagiline	rasagiline	NOUN
ijpds-4231	244	18	salts	salt	NOUN
ijpds-4231	244	19	like	like	VERB
ijpds-4231	244	20	,	,	PUNCT
ijpds-4231	244	21	r	r	NOUN
ijpds-4231	244	22	-	-	PUNCT
ijpds-4231	244	23	rasagiline	rasagiline	NOUN
ijpds-4231	244	24	phosphate	phosphate	NOUN
ijpds-4231	244	25	(	(	PUNCT
ijpds-4231	244	26	purity	purity	NOUN
ijpds-4231	244	27	:	:	PUNCT
ijpds-4231	244	28	99.96	99.96	NUM
ijpds-4231	244	29	%	%	NOUN
ijpds-4231	244	30	)	)	PUNCT
ijpds-4231	244	31	,	,	PUNCT
ijpds-4231	244	32	r	r	NOUN
ijpds-4231	244	33	-	-	PUNCT
ijpds-4231	244	34	rasagiline	rasagiline	NOUN
ijpds-4231	244	35	benzoate	benzoate	NOUN
ijpds-4231	244	36	(	(	PUNCT
ijpds-4231	244	37	yield	yield	NOUN
ijpds-4231	244	38	:	:	PUNCT
ijpds-4231	244	39	78	78	NUM
ijpds-4231	244	40	%	%	NOUN
ijpds-4231	244	41	,	,	PUNCT
ijpds-4231	244	42	purity	purity	NOUN
ijpds-4231	244	43	:	:	PUNCT
ijpds-4231	244	44	99.94	99.94	NUM
ijpds-4231	244	45	%	%	NOUN
ijpds-4231	244	46	)	)	PUNCT
ijpds-4231	244	47	,	,	PUNCT
ijpds-4231	244	48	r	r	NOUN
ijpds-4231	244	49	-	-	PUNCT
ijpds-4231	244	50	rasagiline	rasagiline	NOUN
ijpds-4231	244	51	mandelate	mandelate	NOUN
ijpds-4231	244	52	(	(	PUNCT
ijpds-4231	244	53	yield	yield	NOUN
ijpds-4231	244	54	:	:	PUNCT
ijpds-4231	244	55	61	61	NUM
ijpds-4231	244	56	%	%	NOUN
ijpds-4231	244	57	,	,	PUNCT
ijpds-4231	244	58	purity	purity	NOUN
ijpds-4231	244	59	:	:	PUNCT
ijpds-4231	244	60	99.89	99.89	NUM
ijpds-4231	244	61	%	%	NOUN
ijpds-4231	244	62	)	)	PUNCT
ijpds-4231	244	63	and	and	CCONJ
ijpds-4231	244	64	r	r	NOUN
ijpds-4231	244	65	-	-	PUNCT
ijpds-4231	244	66	rasagiline	rasagiline	NOUN
ijpds-4231	244	67	oxalate	oxalate	NOUN
ijpds-4231	244	68	(	(	PUNCT
ijpds-4231	244	69	purity	purity	NOUN
ijpds-4231	244	70	:	:	PUNCT
ijpds-4231	244	71	99.9	99.9	NUM
ijpds-4231	244	72	%	%	NOUN
ijpds-4231	244	73	)	)	PUNCT
ijpds-4231	244	74	from	from	ADP
ijpds-4231	244	75	rrasagiline	rrasagiline	ADJ
ijpds-4231	244	76	free	free	ADJ
ijpds-4231	244	77	base	base	NOUN
ijpds-4231	244	78	in	in	ADP
ijpds-4231	244	79	isopropyl	isopropyl	NOUN
ijpds-4231	244	80	alcohol	alcohol	NOUN
ijpds-4231	244	81	[	[	X
ijpds-4231	244	82	45	45	NUM
ijpds-4231	244	83	]	]	PUNCT
ijpds-4231	244	84	.	.	PUNCT
ijpds-4231	245	1	sun	sun	PROPN
ijpds-4231	245	2	j	j	PROPN
ijpds-4231	245	3	,	,	PUNCT
ijpds-4231	245	4	et	et	PROPN
ijpds-4231	245	5	al	al	PROPN
ijpds-4231	245	6	.	.	PROPN
ijpds-4231	245	7	,	,	PUNCT
ijpds-4231	245	8	in	in	ADP
ijpds-4231	245	9	2011	2011	NUM
ijpds-4231	245	10	,	,	PUNCT
ijpds-4231	245	11	had	have	AUX
ijpds-4231	245	12	reported	report	VERB
ijpds-4231	245	13	a	a	DET
ijpds-4231	245	14	method	method	NOUN
ijpds-4231	245	15	to	to	PART
ijpds-4231	245	16	prepare	prepare	VERB
ijpds-4231	245	17	rrasagiline	rrasagiline	ADJ
ijpds-4231	245	18	base	base	NOUN
ijpds-4231	245	19	starting	start	VERB
ijpds-4231	245	20	from	from	ADP
ijpds-4231	245	21	racemic	racemic	ADJ
ijpds-4231	245	22	2	2	NUM
ijpds-4231	245	23	as	as	ADP
ijpds-4231	245	24	the	the	DET
ijpds-4231	245	25	raw	raw	ADJ
ijpds-4231	245	26	material	material	NOUN
ijpds-4231	245	27	through	through	ADP
ijpds-4231	245	28	enzyme	enzyme	NOUN
ijpds-4231	245	29	-	-	PUNCT
ijpds-4231	245	30	catalyzed	catalyze	VERB
ijpds-4231	245	31	asymmetric	asymmetric	ADJ
ijpds-4231	245	32	acylation	acylation	NOUN
ijpds-4231	245	33	reaction	reaction	NOUN
ijpds-4231	245	34	,	,	PUNCT
ijpds-4231	245	35	hydrolysis	hydrolysis	NOUN
ijpds-4231	245	36	and	and	CCONJ
ijpds-4231	245	37	n	n	CCONJ
ijpds-4231	245	38	-	-	PUNCT
ijpds-4231	245	39	propargylation	propargylation	NOUN
ijpds-4231	245	40	reactions	reaction	NOUN
ijpds-4231	245	41	.	.	PUNCT
ijpds-4231	246	1	the	the	DET
ijpds-4231	246	2	r	r	NOUN
ijpds-4231	246	3	-	-	PUNCT
ijpds-4231	246	4	isomer	isomer	NOUN
ijpds-4231	246	5	of	of	ADP
ijpds-4231	246	6	2	2	NUM
ijpds-4231	246	7	in	in	ADP
ijpds-4231	246	8	isopropyl	isopropyl	NOUN
ijpds-4231	246	9	ether	ether	NOUN
ijpds-4231	246	10	was	be	AUX
ijpds-4231	246	11	reacted	react	VERB
ijpds-4231	246	12	with	with	ADP
ijpds-4231	246	13	8	8	NUM
ijpds-4231	246	14	in	in	ADP
ijpds-4231	246	15	the	the	DET
ijpds-4231	246	16	presence	presence	NOUN
ijpds-4231	246	17	of	of	ADP
ijpds-4231	246	18	sodium	sodium	NOUN
ijpds-4231	246	19	carbonate	carbonate	NOUN
ijpds-4231	246	20	solution	solution	NOUN
ijpds-4231	246	21	to	to	PART
ijpds-4231	246	22	isolate	isolate	VERB
ijpds-4231	246	23	the	the	DET
ijpds-4231	246	24	desired	desire	VERB
ijpds-4231	246	25	propargylated	propargylate	VERB
ijpds-4231	246	26	product	product	NOUN
ijpds-4231	246	27	(	(	PUNCT
ijpds-4231	246	28	yield	yield	NOUN
ijpds-4231	246	29	:	:	PUNCT
ijpds-4231	246	30	82.5	82.5	NUM
ijpds-4231	246	31	%	%	NOUN
ijpds-4231	246	32	,	,	PUNCT
ijpds-4231	246	33	as	as	ADV
ijpds-4231	246	34	yellow	yellow	ADJ
ijpds-4231	246	35	oily	oily	ADJ
ijpds-4231	246	36	liquid	liquid	NOUN
ijpds-4231	246	37	)	)	PUNCT
ijpds-4231	247	1	[	[	X
ijpds-4231	247	2	46	46	NUM
ijpds-4231	247	3	]	]	PUNCT
ijpds-4231	247	4	.	.	PUNCT
ijpds-4231	248	1	dwivedi	dwivedi	PROPN
ijpds-4231	248	2	sd	sd	PROPN
ijpds-4231	248	3	,	,	PUNCT
ijpds-4231	248	4	et	et	PROPN
ijpds-4231	248	5	al	al	PROPN
ijpds-4231	248	6	.	.	PROPN
ijpds-4231	248	7	,	,	PUNCT
ijpds-4231	248	8	in	in	ADP
ijpds-4231	248	9	2011	2011	NUM
ijpds-4231	248	10	,	,	PUNCT
ijpds-4231	248	11	had	have	AUX
ijpds-4231	248	12	illustrated	illustrate	VERB
ijpds-4231	248	13	the	the	DET
ijpds-4231	248	14	synthesis	synthesis	NOUN
ijpds-4231	248	15	of	of	ADP
ijpds-4231	248	16	many	many	ADJ
ijpds-4231	248	17	salts	salt	NOUN
ijpds-4231	248	18	of	of	ADP
ijpds-4231	248	19	rasagiline	rasagiline	NOUN
ijpds-4231	248	20	from	from	ADP
ijpds-4231	248	21	its	its	PRON
ijpds-4231	248	22	base	base	NOUN
ijpds-4231	248	23	using	use	VERB
ijpds-4231	248	24	the	the	DET
ijpds-4231	248	25	suitable	suitable	ADJ
ijpds-4231	248	26	solvents	solvent	NOUN
ijpds-4231	248	27	.	.	PUNCT
ijpds-4231	249	1	the	the	DET
ijpds-4231	249	2	salts	salt	NOUN
ijpds-4231	249	3	reported	report	VERB
ijpds-4231	249	4	are	be	AUX
ijpds-4231	249	5	r	r	NOUN
ijpds-4231	249	6	-	-	PUNCT
ijpds-4231	249	7	rasagiline	rasagiline	NOUN
ijpds-4231	249	8	hydrobromide	hydrobromide	NOUN
ijpds-4231	249	9	form	form	NOUN
ijpds-4231	249	10	-	-	PUNCT
ijpds-4231	249	11	i	i	NOUN
ijpds-4231	249	12	,	,	PUNCT
ijpds-4231	249	13	amorphous	amorphous	ADJ
ijpds-4231	249	14	rasagiline	rasagiline	NOUN
ijpds-4231	249	15	hydrobromide	hydrobromide	NOUN
ijpds-4231	249	16	,	,	PUNCT
ijpds-4231	249	17	r	r	NOUN
ijpds-4231	249	18	-	-	PUNCT
ijpds-4231	249	19	rasagiline	rasagiline	NOUN
ijpds-4231	249	20	hydrogen	hydrogen	NOUN
ijpds-4231	249	21	phosphate	phosphate	NOUN
ijpds-4231	249	22	,	,	PUNCT
ijpds-4231	249	23	1	1	NUM
ijpds-4231	249	24	from	from	ADP
ijpds-4231	249	25	r	r	NOUN
ijpds-4231	249	26	-	-	PUNCT
ijpds-4231	249	27	rasagiline	rasagiline	NOUN
ijpds-4231	249	28	hydrobromide	hydrobromide	NOUN
ijpds-4231	249	29	form	form	NOUN
ijpds-4231	249	30	-	-	PUNCT
ijpds-4231	249	31	i	i	NOUN
ijpds-4231	249	32	,	,	PUNCT
ijpds-4231	249	33	form	form	NOUN
ijpds-4231	249	34	-	-	PUNCT
ijpds-4231	249	35	i	i	PRON
ijpds-4231	249	36	of	of	ADP
ijpds-4231	249	37	1	1	NUM
ijpds-4231	249	38	,	,	PUNCT
ijpds-4231	249	39	rrasagiline	rrasagiline	ADJ
ijpds-4231	249	40	1,2	1,2	NUM
ijpds-4231	249	41	-	-	PUNCT
ijpds-4231	249	42	edisylate	edisylate	ADJ
ijpds-4231	249	43	form	form	NOUN
ijpds-4231	249	44	-	-	PUNCT
ijpds-4231	249	45	ii	ii	NOUN
ijpds-4231	249	46	,	,	PUNCT
ijpds-4231	249	47	crystalline	crystalline	ADJ
ijpds-4231	249	48	r	r	NOUN
ijpds-4231	249	49	-	-	PUNCT
ijpds-4231	249	50	rasagiline2	rasagiline2	NOUN
ijpds-4231	249	51	-	-	PUNCT
ijpds-4231	249	52	napsylate	napsylate	NOUN
ijpds-4231	249	53	,	,	PUNCT
ijpds-4231	249	54	r	r	X
ijpds-4231	249	55	-	-	PUNCT
ijpds-4231	249	56	rasagiline-1,5	rasagiline-1,5	ADJ
ijpds-4231	249	57	-	-	PUNCT
ijpds-4231	249	58	dinapsylate	dinapsylate	NOUN
ijpds-4231	249	59	form	form	NOUN
ijpds-4231	249	60	-	-	PUNCT
ijpds-4231	249	61	i	i	NOUN
ijpds-4231	249	62	,	,	PUNCT
ijpds-4231	249	63	rrasagiline	rrasagiline	VERB
ijpds-4231	249	64	1,5	1,5	NUM
ijpds-4231	249	65	-	-	PUNCT
ijpds-4231	249	66	dinapsylate	dinapsylate	NOUN
ijpds-4231	249	67	form	form	NOUN
ijpds-4231	249	68	-	-	PUNCT
ijpds-4231	249	69	ii	ii	NOUN
ijpds-4231	249	70	,	,	PUNCT
ijpds-4231	249	71	crystalline	crystalline	ADJ
ijpds-4231	249	72	rrasagiline	rrasagiline	ADJ
ijpds-4231	249	73	-	-	PUNCT
ijpds-4231	249	74	l	l	NOUN
ijpds-4231	249	75	-	-	PUNCT
ijpds-4231	249	76	napsylatate	napsylatate	ADJ
ijpds-4231	249	77	,	,	PUNCT
ijpds-4231	249	78	r	r	NOUN
ijpds-4231	249	79	-	-	PUNCT
ijpds-4231	249	80	rasagiline	rasagiline	NOUN
ijpds-4231	249	81	ascorbate	ascorbate	NOUN
ijpds-4231	249	82	,	,	PUNCT
ijpds-4231	249	83	amorphous	amorphous	ADJ
ijpds-4231	249	84	rasagiline	rasagiline	NOUN
ijpds-4231	249	85	ascorbate	ascorbate	NOUN
ijpds-4231	249	86	[	[	X
ijpds-4231	249	87	47	47	NUM
ijpds-4231	249	88	]	]	PUNCT
ijpds-4231	249	89	.	.	PUNCT
ijpds-4231	250	1	sathe	sathe	PROPN
ijpds-4231	250	2	dg	dg	PROPN
ijpds-4231	250	3	,	,	PUNCT
ijpds-4231	250	4	et	et	PROPN
ijpds-4231	250	5	al	al	PROPN
ijpds-4231	250	6	.	.	PROPN
ijpds-4231	250	7	,	,	PUNCT
ijpds-4231	250	8	in	in	ADP
ijpds-4231	250	9	2011	2011	NUM
ijpds-4231	250	10	,	,	PUNCT
ijpds-4231	250	11	had	have	AUX
ijpds-4231	250	12	demonstrated	demonstrate	VERB
ijpds-4231	250	13	the	the	DET
ijpds-4231	250	14	reaction	reaction	NOUN
ijpds-4231	250	15	of	of	ADP
ijpds-4231	250	16	r-(-)-isomer	r-(-)-isomer	PROPN
ijpds-4231	250	17	of	of	ADP
ijpds-4231	250	18	2	2	NUM
ijpds-4231	250	19	hydrochloride	hydrochloride	NOUN
ijpds-4231	250	20	with	with	ADP
ijpds-4231	250	21	8	8	NUM
ijpds-4231	250	22	in	in	ADP
ijpds-4231	250	23	the	the	DET
ijpds-4231	250	24	presence	presence	NOUN
ijpds-4231	250	25	of	of	ADP
ijpds-4231	250	26	sodium	sodium	NOUN
ijpds-4231	250	27	hydroxide	hydroxide	NOUN
ijpds-4231	250	28	solution	solution	NOUN
ijpds-4231	250	29	and	and	CCONJ
ijpds-4231	250	30	tetra	tetra	NOUN
ijpds-4231	250	31	-	-	PUNCT
ijpds-4231	250	32	butyl	butyl	NOUN
ijpds-4231	250	33	-	-	PUNCT
ijpds-4231	250	34	ammoniumbromide	ammoniumbromide	NOUN
ijpds-4231	250	35	to	to	PART
ijpds-4231	250	36	get	get	VERB
ijpds-4231	250	37	the	the	DET
ijpds-4231	250	38	crude	crude	ADJ
ijpds-4231	250	39	r	r	NOUN
ijpds-4231	250	40	-	-	PUNCT
ijpds-4231	250	41	rasagiline	rasagiline	NOUN
ijpds-4231	250	42	base	base	NOUN
ijpds-4231	250	43	(	(	PUNCT
ijpds-4231	250	44	yield	yield	NOUN
ijpds-4231	250	45	:	:	PUNCT
ijpds-4231	250	46	60	60	NUM
ijpds-4231	250	47	%	%	NOUN
ijpds-4231	250	48	,	,	PUNCT
ijpds-4231	250	49	as	as	ADP
ijpds-4231	250	50	an	an	DET
ijpds-4231	250	51	oily	oily	ADJ
ijpds-4231	250	52	mass	mass	NOUN
ijpds-4231	250	53	)	)	PUNCT
ijpds-4231	250	54	.	.	PUNCT
ijpds-4231	251	1	it	it	PRON
ijpds-4231	251	2	was	be	AUX
ijpds-4231	251	3	subjected	subject	VERB
ijpds-4231	251	4	to	to	ADP
ijpds-4231	251	5	column	column	NOUN
ijpds-4231	251	6	chromatography	chromatography	NOUN
ijpds-4231	251	7	to	to	PART
ijpds-4231	251	8	isolate	isolate	VERB
ijpds-4231	251	9	r	r	NOUN
ijpds-4231	251	10	-	-	PUNCT
ijpds-4231	251	11	rasagiline	rasagiline	NOUN
ijpds-4231	251	12	base	base	NOUN
ijpds-4231	251	13	(	(	PUNCT
ijpds-4231	251	14	recovery	recovery	NOUN
ijpds-4231	251	15	:	:	PUNCT
ijpds-4231	251	16	90	90	NUM
ijpds-4231	251	17	%	%	NOUN
ijpds-4231	251	18	)	)	PUNCT
ijpds-4231	251	19	.	.	PUNCT
ijpds-4231	252	1	the	the	DET
ijpds-4231	252	2	unreacted	unreacted	ADJ
ijpds-4231	252	3	r-(-)-isomer	r-(-)-isomer	PROPN
ijpds-4231	252	4	of	of	ADP
ijpds-4231	252	5	2	2	NUM
ijpds-4231	252	6	was	be	AUX
ijpds-4231	252	7	recovered	recover	VERB
ijpds-4231	252	8	by	by	ADP
ijpds-4231	252	9	the	the	DET
ijpds-4231	252	10	basification	basification	NOUN
ijpds-4231	252	11	and	and	CCONJ
ijpds-4231	252	12	extraction	extraction	NOUN
ijpds-4231	252	13	processes	process	NOUN
ijpds-4231	252	14	.	.	PUNCT
ijpds-4231	253	1	r	r	X
ijpds-4231	253	2	-	-	PUNCT
ijpds-4231	253	3	rasagiline	rasagiline	NOUN
ijpds-4231	253	4	base	base	NOUN
ijpds-4231	253	5	was	be	AUX
ijpds-4231	253	6	treated	treat	VERB
ijpds-4231	253	7	with	with	ADP
ijpds-4231	253	8	methanesulfonic	methanesulfonic	ADJ
ijpds-4231	253	9	acid	acid	NOUN
ijpds-4231	253	10	in	in	ADP
ijpds-4231	253	11	isopropyl	isopropyl	NOUN
ijpds-4231	253	12	alcohol	alcohol	NOUN
ijpds-4231	253	13	to	to	PART
ijpds-4231	253	14	isolate	isolate	VERB
ijpds-4231	253	15	1	1	NUM
ijpds-4231	253	16	(	(	PUNCT
ijpds-4231	253	17	yield	yield	NOUN
ijpds-4231	253	18	:	:	PUNCT
ijpds-4231	253	19	83	83	NUM
ijpds-4231	253	20	%	%	NOUN
ijpds-4231	253	21	)	)	PUNCT
ijpds-4231	253	22	.	.	PUNCT
ijpds-4231	254	1	the	the	DET
ijpds-4231	254	2	work	work	NOUN
ijpds-4231	254	3	was	be	AUX
ijpds-4231	254	4	extended	extend	VERB
ijpds-4231	254	5	further	far	ADV
ijpds-4231	254	6	to	to	PART
ijpds-4231	254	7	provide	provide	VERB
ijpds-4231	254	8	the	the	DET
ijpds-4231	254	9	preparation	preparation	NOUN
ijpds-4231	254	10	methods	method	NOUN
ijpds-4231	254	11	of	of	ADP
ijpds-4231	254	12	rasagiline	rasagiline	NOUN
ijpds-4231	254	13	hydrochloride	hydrochloride	NOUN
ijpds-4231	254	14	,	,	PUNCT
ijpds-4231	254	15	form	form	NOUN
ijpds-4231	254	16	-	-	PUNCT
ijpds-4231	254	17	i	i	PRON
ijpds-4231	254	18	and	and	CCONJ
ijpds-4231	254	19	form	form	NOUN
ijpds-4231	254	20	-	-	PUNCT
ijpds-4231	254	21	ii	ii	NOUN
ijpds-4231	254	22	,	,	PUNCT
ijpds-4231	254	23	rasagiline	rasagiline	ADJ
ijpds-4231	254	24	hydrobromide	hydrobromide	NOUN
ijpds-4231	254	25	,	,	PUNCT
ijpds-4231	254	26	rasagiline	rasagiline	NOUN
ijpds-4231	254	27	palmitate	palmitate	NOUN
ijpds-4231	254	28	.	.	PUNCT
ijpds-4231	255	1	furthermore	furthermore	ADV
ijpds-4231	255	2	,	,	PUNCT
ijpds-4231	255	3	the	the	DET
ijpds-4231	255	4	work	work	NOUN
ijpds-4231	255	5	reported	report	VERB
ijpds-4231	255	6	the	the	DET
ijpds-4231	255	7	route	route	NOUN
ijpds-4231	255	8	to	to	PART
ijpds-4231	255	9	synthesize	synthesize	VERB
ijpds-4231	255	10	and	and	CCONJ
ijpds-4231	255	11	isolate	isolate	VERB
ijpds-4231	255	12	the	the	DET
ijpds-4231	255	13	impurities	impurity	NOUN
ijpds-4231	255	14	like	like	ADP
ijpds-4231	255	15	33	33	NUM
ijpds-4231	255	16	(	(	PUNCT
ijpds-4231	255	17	impurity	impurity	NOUN
ijpds-4231	255	18	a	a	NOUN
ijpds-4231	255	19	)	)	PUNCT
ijpds-4231	255	20	and	and	CCONJ
ijpds-4231	255	21	34	34	NUM
ijpds-4231	255	22	(	(	PUNCT
ijpds-4231	255	23	impurity	impurity	NOUN
ijpds-4231	255	24	b	b	NOUN
ijpds-4231	255	25	)	)	PUNCT
ijpds-4231	256	1	[	[	X
ijpds-4231	256	2	48	48	NUM
ijpds-4231	256	3	]	]	PUNCT
ijpds-4231	256	4	.	.	PUNCT
ijpds-4231	257	1	sanjay	sanjay	PROPN
ijpds-4231	257	2	s	s	PART
ijpds-4231	258	1	s	s	NOUN
ijpds-4231	258	2	patents	patent	NOUN
ijpds-4231	258	3	disclosed	disclose	VERB
ijpds-4231	258	4	synthetic	synthetic	ADJ
ijpds-4231	258	5	overview	overview	NOUN
ijpds-4231	258	6	of	of	ADP
ijpds-4231	258	7	rasagiline	rasagiline	ADJ
ijpds-4231	258	8	vol	vol	NOUN
ijpds-4231	258	9	2	2	NUM
ijpds-4231	258	10	|	|	ADV
ijpds-4231	258	11	issue	issue	VERB
ijpds-4231	258	12	4	4	NUM
ijpds-4231	258	13	|	|	ADV
ijpds-4231	258	14	oct	oct	PROPN
ijpds-4231	258	15	–	–	PUNCT
ijpds-4231	258	16	dec	dec	PROPN
ijpds-4231	258	17	2023	2023	NUM
ijpds-4231	258	18	indian	indian	PROPN
ijpds-4231	258	19	j	j	PROPN
ijpds-4231	258	20	pharm	pharm	PROPN
ijpds-4231	258	21	drug	drug	PROPN
ijpds-4231	258	22	studies	study	NOUN
ijpds-4231	258	23	|	|	ADV
ijpds-4231	258	24	139	139	NUM
ijpds-4231	258	25	elffrink	elffrink	NOUN
ijpds-4231	258	26	wwj	wwj	ADV
ijpds-4231	258	27	,	,	PUNCT
ijpds-4231	258	28	in	in	ADP
ijpds-4231	258	29	2011	2011	NUM
ijpds-4231	258	30	,	,	PUNCT
ijpds-4231	258	31	had	have	AUX
ijpds-4231	258	32	disclosed	disclose	VERB
ijpds-4231	258	33	the	the	DET
ijpds-4231	258	34	techniques	technique	NOUN
ijpds-4231	258	35	to	to	PART
ijpds-4231	258	36	synthesize	synthesize	VERB
ijpds-4231	258	37	a	a	DET
ijpds-4231	258	38	few	few	ADJ
ijpds-4231	258	39	crystallographic	crystallographic	ADJ
ijpds-4231	258	40	forms	form	NOUN
ijpds-4231	258	41	of	of	ADP
ijpds-4231	258	42	rasagiline	rasagiline	NOUN
ijpds-4231	258	43	hydrochloride	hydrochloride	NOUN
ijpds-4231	258	44	like	like	ADP
ijpds-4231	258	45	form	form	NOUN
ijpds-4231	258	46	-	-	PUNCT
ijpds-4231	258	47	i	i	PRON
ijpds-4231	258	48	(	(	PUNCT
ijpds-4231	258	49	as	as	ADP
ijpds-4231	258	50	per	per	ADP
ijpds-4231	258	51	the	the	DET
ijpds-4231	258	52	past	past	ADJ
ijpds-4231	258	53	disclosures	disclosure	NOUN
ijpds-4231	258	54	)	)	PUNCT
ijpds-4231	258	55	,	,	PUNCT
ijpds-4231	258	56	form	form	NOUN
ijpds-4231	258	57	-	-	PUNCT
ijpds-4231	258	58	ii	ii	NOUN
ijpds-4231	258	59	and	and	CCONJ
ijpds-4231	258	60	form	form	NOUN
ijpds-4231	258	61	-	-	PUNCT
ijpds-4231	258	62	iii	iii	NOUN
ijpds-4231	258	63	(	(	PUNCT
ijpds-4231	258	64	by	by	ADP
ijpds-4231	258	65	the	the	DET
ijpds-4231	258	66	use	use	NOUN
ijpds-4231	258	67	of	of	ADP
ijpds-4231	258	68	an	an	DET
ijpds-4231	258	69	inert	inert	ADJ
ijpds-4231	258	70	solvent	solvent	NOUN
ijpds-4231	258	71	for	for	ADP
ijpds-4231	258	72	a	a	DET
ijpds-4231	258	73	sufficient	sufficient	ADJ
ijpds-4231	258	74	time	time	NOUN
ijpds-4231	258	75	to	to	PART
ijpds-4231	258	76	attain	attain	VERB
ijpds-4231	258	77	the	the	DET
ijpds-4231	258	78	conversion	conversion	NOUN
ijpds-4231	258	79	)	)	PUNCT
ijpds-4231	259	1	[	[	X
ijpds-4231	259	2	49	49	NUM
ijpds-4231	259	3	]	]	PUNCT
ijpds-4231	259	4	.	.	PUNCT
ijpds-4231	260	1	bohumil	bohumil	PROPN
ijpds-4231	260	2	d.	d.	PROPN
ijpds-4231	260	3	,	,	PUNCT
ijpds-4231	260	4	in	in	ADP
ijpds-4231	260	5	2012	2012	NUM
ijpds-4231	260	6	,	,	PUNCT
ijpds-4231	260	7	had	have	AUX
ijpds-4231	260	8	illustrated	illustrate	VERB
ijpds-4231	260	9	the	the	DET
ijpds-4231	260	10	resolution	resolution	NOUN
ijpds-4231	260	11	of	of	ADP
ijpds-4231	260	12	racemic	racemic	ADJ
ijpds-4231	260	13	2	2	NUM
ijpds-4231	260	14	in	in	ADP
ijpds-4231	260	15	methanol	methanol	NOUN
ijpds-4231	260	16	using	use	VERB
ijpds-4231	260	17	l-(+)-aspartic	l-(+)-aspartic	ADJ
ijpds-4231	260	18	acid	acid	NOUN
ijpds-4231	260	19	,	,	PUNCT
ijpds-4231	260	20	l-(-)malic	l-(-)malic	ADJ
ijpds-4231	260	21	acid	acid	NOUN
ijpds-4231	260	22	and	and	CCONJ
ijpds-4231	260	23	(	(	PUNCT
ijpds-4231	260	24	2r	2r	NUM
ijpds-4231	260	25	,	,	PUNCT
ijpds-4231	260	26	3r)-tartaric	3r)-tartaric	NUM
ijpds-4231	260	27	acid	acid	NOUN
ijpds-4231	260	28	.	.	PUNCT
ijpds-4231	261	1	the	the	DET
ijpds-4231	261	2	work	work	NOUN
ijpds-4231	261	3	had	have	AUX
ijpds-4231	261	4	reported	report	VERB
ijpds-4231	261	5	the	the	DET
ijpds-4231	261	6	conversion	conversion	NOUN
ijpds-4231	261	7	of	of	ADP
ijpds-4231	261	8	s	s	NOUN
ijpds-4231	261	9	-	-	PUNCT
ijpds-4231	261	10	isomer	isomer	ADJ
ijpds-4231	261	11	of	of	ADP
ijpds-4231	261	12	2	2	NUM
ijpds-4231	261	13	to	to	ADP
ijpds-4231	261	14	its	its	PRON
ijpds-4231	261	15	r	r	NOUN
ijpds-4231	261	16	-	-	PUNCT
ijpds-4231	261	17	isomer	isomer	NOUN
ijpds-4231	261	18	(	(	PUNCT
ijpds-4231	261	19	yield	yield	NOUN
ijpds-4231	261	20	:	:	PUNCT
ijpds-4231	261	21	94	94	NUM
ijpds-4231	261	22	%	%	NOUN
ijpds-4231	261	23	,	,	PUNCT
ijpds-4231	261	24	purity	purity	NOUN
ijpds-4231	261	25	:	:	PUNCT
ijpds-4231	261	26	96	96	NUM
ijpds-4231	261	27	%	%	NOUN
ijpds-4231	261	28	by	by	ADP
ijpds-4231	261	29	hplc	hplc	NOUN
ijpds-4231	261	30	)	)	PUNCT
ijpds-4231	261	31	in	in	ADP
ijpds-4231	261	32	the	the	DET
ijpds-4231	261	33	presence	presence	NOUN
ijpds-4231	261	34	of	of	ADP
ijpds-4231	261	35	potassium	potassium	NOUN
ijpds-4231	261	36	-	-	PUNCT
ijpds-4231	261	37	tert	tert	NOUN
ijpds-4231	261	38	-	-	PUNCT
ijpds-4231	261	39	butoxide	butoxide	NOUN
ijpds-4231	261	40	in	in	ADP
ijpds-4231	261	41	dimethyl	dimethyl	NOUN
ijpds-4231	261	42	sulfoxide	sulfoxide	NOUN
ijpds-4231	261	43	.	.	PUNCT
ijpds-4231	262	1	it	it	PRON
ijpds-4231	262	2	also	also	ADV
ijpds-4231	262	3	extends	extend	VERB
ijpds-4231	262	4	to	to	PART
ijpds-4231	262	5	report	report	VERB
ijpds-4231	262	6	the	the	DET
ijpds-4231	262	7	condensation	condensation	NOUN
ijpds-4231	262	8	of	of	ADP
ijpds-4231	262	9	r	r	NOUN
ijpds-4231	262	10	-	-	PUNCT
ijpds-4231	262	11	isomer	isomer	NOUN
ijpds-4231	262	12	of	of	ADP
ijpds-4231	262	13	2	2	NUM
ijpds-4231	262	14	hydrochloride	hydrochloride	NOUN
ijpds-4231	262	15	with	with	ADP
ijpds-4231	262	16	3	3	NUM
ijpds-4231	262	17	in	in	ADP
ijpds-4231	262	18	the	the	DET
ijpds-4231	262	19	presence	presence	NOUN
ijpds-4231	262	20	of	of	ADP
ijpds-4231	262	21	sodium	sodium	NOUN
ijpds-4231	262	22	hydroxide	hydroxide	NOUN
ijpds-4231	262	23	solution	solution	NOUN
ijpds-4231	262	24	under	under	ADP
ijpds-4231	262	25	the	the	DET
ijpds-4231	262	26	toluene	toluene	NOUN
ijpds-4231	262	27	medium	medium	NOUN
ijpds-4231	262	28	to	to	PART
ijpds-4231	262	29	form	form	VERB
ijpds-4231	262	30	rasagiline	rasagiline	NOUN
ijpds-4231	262	31	base	base	NOUN
ijpds-4231	262	32	(	(	PUNCT
ijpds-4231	262	33	not	not	PART
ijpds-4231	262	34	isolated	isolate	VERB
ijpds-4231	262	35	)	)	PUNCT
ijpds-4231	262	36	.	.	PUNCT
ijpds-4231	263	1	to	to	ADP
ijpds-4231	263	2	the	the	DET
ijpds-4231	263	3	rasagiline	rasagiline	NOUN
ijpds-4231	263	4	base	base	NOUN
ijpds-4231	263	5	dissolved	dissolve	VERB
ijpds-4231	263	6	in	in	ADP
ijpds-4231	263	7	toluene	toluene	NOUN
ijpds-4231	263	8	,	,	PUNCT
ijpds-4231	263	9	added	add	VERB
ijpds-4231	263	10	methanesulfonic	methanesulfonic	ADJ
ijpds-4231	263	11	acid	acid	NOUN
ijpds-4231	263	12	in	in	ADP
ijpds-4231	263	13	isopropyl	isopropyl	NOUN
ijpds-4231	263	14	alcohol	alcohol	NOUN
ijpds-4231	263	15	to	to	PART
ijpds-4231	263	16	isolate	isolate	VERB
ijpds-4231	263	17	1	1	NUM
ijpds-4231	263	18	(	(	PUNCT
ijpds-4231	263	19	purity	purity	NOUN
ijpds-4231	263	20	:	:	PUNCT
ijpds-4231	263	21	99.86	99.86	NUM
ijpds-4231	263	22	%	%	NOUN
ijpds-4231	263	23	,	,	PUNCT
ijpds-4231	263	24	chiral	chiral	ADJ
ijpds-4231	263	25	purity	purity	NOUN
ijpds-4231	263	26	:	:	PUNCT
ijpds-4231	263	27	100	100	NUM
ijpds-4231	263	28	%	%	NOUN
ijpds-4231	263	29	,	,	PUNCT
ijpds-4231	263	30	by	by	ADP
ijpds-4231	263	31	hplc	hplc	NOUN
ijpds-4231	263	32	)	)	PUNCT
ijpds-4231	264	1	[	[	X
ijpds-4231	264	2	50	50	NUM
ijpds-4231	264	3	]	]	PUNCT
ijpds-4231	264	4	.	.	PUNCT
ijpds-4231	265	1	liu	liu	PROPN
ijpds-4231	265	2	g	g	PROPN
ijpds-4231	265	3	,	,	PUNCT
ijpds-4231	265	4	et	et	PROPN
ijpds-4231	265	5	al	al	PROPN
ijpds-4231	265	6	,	,	PUNCT
ijpds-4231	265	7	in	in	ADP
ijpds-4231	265	8	2012	2012	NUM
ijpds-4231	265	9	,	,	PUNCT
ijpds-4231	265	10	had	have	AUX
ijpds-4231	265	11	reported	report	VERB
ijpds-4231	265	12	the	the	DET
ijpds-4231	265	13	condensation	condensation	NOUN
ijpds-4231	265	14	of	of	ADP
ijpds-4231	265	15	risomer	risomer	NOUN
ijpds-4231	265	16	of	of	ADP
ijpds-4231	265	17	2	2	NUM
ijpds-4231	265	18	with	with	ADP
ijpds-4231	265	19	methyl	methyl	NOUN
ijpds-4231	265	20	trifluoroacetate	trifluoroacetate	NOUN
ijpds-4231	265	21	35	35	NUM
ijpds-4231	265	22	in	in	ADP
ijpds-4231	265	23	methyl	methyl	NOUN
ijpds-4231	265	24	alcohol	alcohol	NOUN
ijpds-4231	265	25	to	to	PART
ijpds-4231	265	26	isolate	isolate	VERB
ijpds-4231	265	27	n-[(1r)-2,3	n-[(1r)-2,3	ADJ
ijpds-4231	265	28	-	-	PUNCT
ijpds-4231	265	29	dihydro-1h	dihydro-1h	NOUN
ijpds-4231	265	30	-	-	PUNCT
ijpds-4231	265	31	inden-1	inden-1	NOUN
ijpds-4231	265	32	-	-	PUNCT
ijpds-4231	265	33	yl]2,2,2	yl]2,2,2	NOUN
ijpds-4231	265	34	-	-	PUNCT
ijpds-4231	265	35	trifluoroacetamide	trifluoroacetamide	NOUN
ijpds-4231	265	36	38	38	NUM
ijpds-4231	265	37	(	(	PUNCT
ijpds-4231	265	38	yield	yield	NOUN
ijpds-4231	265	39	:	:	PUNCT
ijpds-4231	265	40	96	96	NUM
ijpds-4231	265	41	%	%	NOUN
ijpds-4231	265	42	,	,	PUNCT
ijpds-4231	265	43	purity	purity	NOUN
ijpds-4231	265	44	:	:	PUNCT
ijpds-4231	265	45	99.5	99.5	NUM
ijpds-4231	265	46	%	%	NOUN
ijpds-4231	265	47	by	by	ADP
ijpds-4231	265	48	hplc	hplc	NOUN
ijpds-4231	265	49	)	)	PUNCT
ijpds-4231	265	50	.	.	PUNCT
ijpds-4231	266	1	similarly	similarly	ADV
ijpds-4231	266	2	,	,	PUNCT
ijpds-4231	266	3	ethyl	ethyl	PROPN
ijpds-4231	266	4	trifluoroacetate	trifluoroacetate	VERB
ijpds-4231	266	5	36	36	NUM
ijpds-4231	266	6	in	in	ADP
ijpds-4231	266	7	ethyl	ethyl	PROPN
ijpds-4231	266	8	alcohol	alcohol	NOUN
ijpds-4231	266	9	was	be	AUX
ijpds-4231	266	10	used	use	VERB
ijpds-4231	266	11	to	to	PART
ijpds-4231	266	12	isolate	isolate	VERB
ijpds-4231	266	13	38	38	NUM
ijpds-4231	266	14	(	(	PUNCT
ijpds-4231	266	15	yield	yield	NOUN
ijpds-4231	266	16	:	:	PUNCT
ijpds-4231	266	17	98	98	NUM
ijpds-4231	266	18	%	%	NOUN
ijpds-4231	266	19	,	,	PUNCT
ijpds-4231	266	20	purity	purity	NOUN
ijpds-4231	266	21	:	:	PUNCT
ijpds-4231	266	22	99.7	99.7	NUM
ijpds-4231	266	23	%	%	NOUN
ijpds-4231	266	24	by	by	ADP
ijpds-4231	266	25	hplc	hplc	NOUN
ijpds-4231	266	26	)	)	PUNCT
ijpds-4231	266	27	.	.	PUNCT
ijpds-4231	267	1	additionally	additionally	ADV
ijpds-4231	267	2	,	,	PUNCT
ijpds-4231	267	3	butyl	butyl	NOUN
ijpds-4231	267	4	-	-	PUNCT
ijpds-4231	267	5	trifluoroacetate	trifluoroacetate	NOUN
ijpds-4231	267	6	37	37	NUM
ijpds-4231	267	7	in	in	ADP
ijpds-4231	267	8	pentyl	pentyl	NOUN
ijpds-4231	267	9	alcohol	alcohol	NOUN
ijpds-4231	267	10	or	or	CCONJ
ijpds-4231	267	11	tetrahydrofuran	tetrahydrofuran	NOUN
ijpds-4231	267	12	was	be	AUX
ijpds-4231	267	13	used	use	VERB
ijpds-4231	267	14	to	to	PART
ijpds-4231	267	15	get	get	VERB
ijpds-4231	267	16	38	38	NUM
ijpds-4231	267	17	(	(	PUNCT
ijpds-4231	267	18	yield	yield	NOUN
ijpds-4231	267	19	:	:	PUNCT
ijpds-4231	267	20	94	94	NUM
ijpds-4231	267	21	%	%	NOUN
ijpds-4231	267	22	,	,	PUNCT
ijpds-4231	267	23	purity	purity	NOUN
ijpds-4231	267	24	:	:	PUNCT
ijpds-4231	267	25	99.2	99.2	NUM
ijpds-4231	267	26	%	%	NOUN
ijpds-4231	267	27	by	by	ADP
ijpds-4231	267	28	hplc	hplc	NOUN
ijpds-4231	267	29	)	)	PUNCT
ijpds-4231	267	30	.	.	PUNCT
ijpds-4231	268	1	in	in	ADP
ijpds-4231	268	2	the	the	DET
ijpds-4231	268	3	next	next	ADJ
ijpds-4231	268	4	step	step	NOUN
ijpds-4231	268	5	,	,	PUNCT
ijpds-4231	268	6	38	38	NUM
ijpds-4231	268	7	was	be	AUX
ijpds-4231	268	8	treated	treat	VERB
ijpds-4231	268	9	with	with	ADP
ijpds-4231	268	10	7	7	NUM
ijpds-4231	268	11	in	in	ADP
ijpds-4231	268	12	the	the	DET
ijpds-4231	268	13	presence	presence	NOUN
ijpds-4231	268	14	of	of	ADP
ijpds-4231	268	15	n	n	CCONJ
ijpds-4231	268	16	,	,	PUNCT
ijpds-4231	268	17	n	n	CCONJ
ijpds-4231	268	18	-	-	PUNCT
ijpds-4231	268	19	dimethylformamide	dimethylformamide	NOUN
ijpds-4231	268	20	and	and	CCONJ
ijpds-4231	268	21	sodium	sodium	NOUN
ijpds-4231	268	22	hydroxide	hydroxide	NOUN
ijpds-4231	268	23	solution	solution	NOUN
ijpds-4231	268	24	to	to	PART
ijpds-4231	268	25	obtain	obtain	VERB
ijpds-4231	268	26	n-[(1r)-2,3	n-[(1r)-2,3	NOUN
ijpds-4231	268	27	-	-	PUNCT
ijpds-4231	268	28	dihydro1h	dihydro1h	PROPN
ijpds-4231	268	29	-	-	PUNCT
ijpds-4231	268	30	inden-1	inden-1	PROPN
ijpds-4231	268	31	-	-	PUNCT
ijpds-4231	268	32	yl]-2,2,2	yl]-2,2,2	NUM
ijpds-4231	268	33	-	-	PUNCT
ijpds-4231	268	34	trifluoro	trifluoro	ADP
ijpds-4231	268	35	-	-	PUNCT
ijpds-4231	268	36	n-(prop-2	n-(prop-2	NOUN
ijpds-4231	268	37	-	-	PUNCT
ijpds-4231	268	38	yn-1yl)acetamide	yn-1yl)acetamide	PROPN
ijpds-4231	268	39	39	39	NUM
ijpds-4231	268	40	(	(	PUNCT
ijpds-4231	268	41	yield	yield	NOUN
ijpds-4231	268	42	:	:	PUNCT
ijpds-4231	268	43	86	86	NUM
ijpds-4231	268	44	%	%	NOUN
ijpds-4231	268	45	,	,	PUNCT
ijpds-4231	268	46	purity	purity	NOUN
ijpds-4231	268	47	:	:	PUNCT
ijpds-4231	268	48	99.1	99.1	NUM
ijpds-4231	268	49	%	%	NOUN
ijpds-4231	268	50	by	by	ADP
ijpds-4231	268	51	hplc	hplc	PROPN
ijpds-4231	268	52	)	)	PUNCT
ijpds-4231	268	53	.	.	PUNCT
ijpds-4231	269	1	a	a	DET
ijpds-4231	269	2	slight	slight	ADJ
ijpds-4231	269	3	process	process	NOUN
ijpds-4231	269	4	modification	modification	NOUN
ijpds-4231	269	5	was	be	AUX
ijpds-4231	269	6	done	do	VERB
ijpds-4231	269	7	to	to	PART
ijpds-4231	269	8	condense	condense	VERB
ijpds-4231	269	9	3	3	NUM
ijpds-4231	269	10	to	to	NOUN
ijpds-4231	269	11	with	with	ADP
ijpds-4231	269	12	38	38	NUM
ijpds-4231	269	13	to	to	PART
ijpds-4231	269	14	obtain	obtain	VERB
ijpds-4231	269	15	39	39	NUM
ijpds-4231	269	16	(	(	PUNCT
ijpds-4231	269	17	yield	yield	NOUN
ijpds-4231	269	18	:	:	PUNCT
ijpds-4231	269	19	90	90	NUM
ijpds-4231	269	20	%	%	NOUN
ijpds-4231	269	21	,	,	PUNCT
ijpds-4231	269	22	purity	purity	NOUN
ijpds-4231	269	23	:	:	PUNCT
ijpds-4231	269	24	99.7	99.7	NUM
ijpds-4231	269	25	%	%	NOUN
ijpds-4231	269	26	by	by	ADP
ijpds-4231	269	27	hplc	hplc	PROPN
ijpds-4231	269	28	)	)	PUNCT
ijpds-4231	269	29	.	.	PUNCT
ijpds-4231	270	1	a	a	DET
ijpds-4231	270	2	few	few	ADJ
ijpds-4231	270	3	different	different	ADJ
ijpds-4231	270	4	reagents	reagent	NOUN
ijpds-4231	270	5	and	and	CCONJ
ijpds-4231	270	6	solvents	solvent	NOUN
ijpds-4231	270	7	were	be	AUX
ijpds-4231	270	8	used	use	VERB
ijpds-4231	270	9	to	to	PART
ijpds-4231	270	10	condense	condense	VERB
ijpds-4231	270	11	3	3	NUM
ijpds-4231	270	12	or	or	CCONJ
ijpds-4231	270	13	7	7	NUM
ijpds-4231	270	14	with	with	ADP
ijpds-4231	270	15	38	38	NUM
ijpds-4231	270	16	to	to	PART
ijpds-4231	270	17	isolate	isolate	VERB
ijpds-4231	270	18	39	39	NUM
ijpds-4231	270	19	with	with	ADP
ijpds-4231	270	20	good	good	ADJ
ijpds-4231	270	21	optical	optical	ADJ
ijpds-4231	270	22	purity	purity	NOUN
ijpds-4231	270	23	.	.	PUNCT
ijpds-4231	271	1	hydrolysis	hydrolysis	NOUN
ijpds-4231	271	2	of	of	ADP
ijpds-4231	271	3	39	39	NUM
ijpds-4231	271	4	under	under	ADP
ijpds-4231	271	5	the	the	DET
ijpds-4231	271	6	suitable	suitable	ADJ
ijpds-4231	271	7	alkaline	alkaline	NOUN
ijpds-4231	271	8	conditions	condition	NOUN
ijpds-4231	271	9	had	have	AUX
ijpds-4231	271	10	resulted	result	VERB
ijpds-4231	271	11	in	in	ADP
ijpds-4231	271	12	the	the	DET
ijpds-4231	271	13	formation	formation	NOUN
ijpds-4231	271	14	of	of	ADP
ijpds-4231	271	15	r	r	NOUN
ijpds-4231	271	16	-	-	PUNCT
ijpds-4231	271	17	rasagiline	rasagiline	NOUN
ijpds-4231	271	18	base	base	NOUN
ijpds-4231	271	19	(	(	PUNCT
ijpds-4231	271	20	yield	yield	NOUN
ijpds-4231	271	21	:	:	PUNCT
ijpds-4231	271	22	8696	8696	NUM
ijpds-4231	271	23	%	%	NOUN
ijpds-4231	271	24	,	,	PUNCT
ijpds-4231	271	25	purity	purity	NOUN
ijpds-4231	271	26	:	:	PUNCT
ijpds-4231	271	27	99.8	99.8	NUM
ijpds-4231	271	28	-	-	SYM
ijpds-4231	271	29	99.3	99.3	NUM
ijpds-4231	271	30	%	%	NOUN
ijpds-4231	271	31	)	)	PUNCT
ijpds-4231	271	32	.	.	PUNCT
ijpds-4231	272	1	it	it	PRON
ijpds-4231	272	2	was	be	AUX
ijpds-4231	272	3	treated	treat	VERB
ijpds-4231	272	4	with	with	ADP
ijpds-4231	272	5	methanesulfonic	methanesulfonic	ADJ
ijpds-4231	272	6	acid	acid	NOUN
ijpds-4231	272	7	in	in	ADP
ijpds-4231	272	8	diethyl	diethyl	NOUN
ijpds-4231	272	9	ether	ether	NOUN
ijpds-4231	272	10	to	to	PART
ijpds-4231	272	11	get	get	VERB
ijpds-4231	272	12	1	1	NUM
ijpds-4231	272	13	(	(	PUNCT
ijpds-4231	272	14	yield	yield	NOUN
ijpds-4231	272	15	:	:	PUNCT
ijpds-4231	272	16	82	82	NUM
ijpds-4231	272	17	%	%	NOUN
ijpds-4231	272	18	,	,	PUNCT
ijpds-4231	272	19	purity	purity	NOUN
ijpds-4231	272	20	:	:	PUNCT
ijpds-4231	272	21	99.3	99.3	NUM
ijpds-4231	272	22	%	%	NOUN
ijpds-4231	272	23	)	)	PUNCT
ijpds-4231	273	1	[	[	X
ijpds-4231	273	2	51	51	NUM
ijpds-4231	273	3	]	]	PUNCT
ijpds-4231	273	4	.	.	PUNCT
ijpds-4231	274	1	oemer	oemer	NOUN
ijpds-4231	274	2	r	r	NOUN
ijpds-4231	274	3	,	,	PUNCT
ijpds-4231	274	4	et	et	PROPN
ijpds-4231	274	5	al	al	PROPN
ijpds-4231	274	6	,	,	PUNCT
ijpds-4231	274	7	in	in	ADP
ijpds-4231	274	8	2012	2012	NUM
ijpds-4231	274	9	,	,	PUNCT
ijpds-4231	274	10	had	have	AUX
ijpds-4231	274	11	demonstrated	demonstrate	VERB
ijpds-4231	274	12	a	a	DET
ijpds-4231	274	13	high	high	ADJ
ijpds-4231	274	14	yield	yield	NOUN
ijpds-4231	274	15	method	method	NOUN
ijpds-4231	274	16	for	for	ADP
ijpds-4231	274	17	the	the	DET
ijpds-4231	274	18	synthesis	synthesis	NOUN
ijpds-4231	274	19	of	of	ADP
ijpds-4231	274	20	1	1	NUM
ijpds-4231	274	21	by	by	ADP
ijpds-4231	274	22	the	the	DET
ijpds-4231	274	23	alkylation	alkylation	NOUN
ijpds-4231	274	24	of	of	ADP
ijpds-4231	274	25	39	39	NUM
ijpds-4231	274	26	.	.	PUNCT
ijpds-4231	275	1	the	the	DET
ijpds-4231	275	2	trifluoroacetyl	trifluoroacetyl	PROPN
ijpds-4231	275	3	protection	protection	PROPN
ijpds-4231	275	4	had	have	AUX
ijpds-4231	275	5	enabled	enable	VERB
ijpds-4231	275	6	to	to	PART
ijpds-4231	275	7	carry	carry	VERB
ijpds-4231	275	8	out	out	ADP
ijpds-4231	275	9	an	an	DET
ijpds-4231	275	10	alkylation	alkylation	NOUN
ijpds-4231	275	11	of	of	ADP
ijpds-4231	275	12	38	38	NUM
ijpds-4231	275	13	with	with	ADP
ijpds-4231	275	14	a	a	DET
ijpds-4231	275	15	high	high	ADJ
ijpds-4231	275	16	yield	yield	NOUN
ijpds-4231	275	17	and	and	CCONJ
ijpds-4231	275	18	purity	purity	NOUN
ijpds-4231	275	19	under	under	ADP
ijpds-4231	275	20	very	very	ADV
ijpds-4231	275	21	mild	mild	ADJ
ijpds-4231	275	22	conditions	condition	NOUN
ijpds-4231	275	23	with	with	ADP
ijpds-4231	275	24	a	a	DET
ijpds-4231	275	25	wide	wide	ADJ
ijpds-4231	275	26	range	range	NOUN
ijpds-4231	275	27	of	of	ADP
ijpds-4231	275	28	reaction	reaction	NOUN
ijpds-4231	275	29	conditions	condition	NOUN
ijpds-4231	275	30	and	and	CCONJ
ijpds-4231	275	31	reagent	reagent	ADJ
ijpds-4231	275	32	selection	selection	NOUN
ijpds-4231	275	33	.	.	PUNCT
ijpds-4231	276	1	r	r	X
ijpds-4231	276	2	-	-	PUNCT
ijpds-4231	276	3	isomer	isomer	NOUN
ijpds-4231	276	4	of	of	ADP
ijpds-4231	276	5	2	2	NUM
ijpds-4231	276	6	hydrochloride	hydrochloride	NOUN
ijpds-4231	276	7	was	be	AUX
ijpds-4231	276	8	treated	treat	VERB
ijpds-4231	276	9	with	with	ADP
ijpds-4231	276	10	trifluoroacetic	trifluoroacetic	ADJ
ijpds-4231	276	11	anhydride	anhydride	NOUN
ijpds-4231	276	12	40	40	NUM
ijpds-4231	276	13	in	in	ADP
ijpds-4231	276	14	the	the	DET
ijpds-4231	276	15	presence	presence	NOUN
ijpds-4231	276	16	of	of	ADP
ijpds-4231	276	17	pyridine	pyridine	NOUN
ijpds-4231	276	18	and	and	CCONJ
ijpds-4231	276	19	dichloromethane	dichloromethane	NOUN
ijpds-4231	276	20	to	to	PART
ijpds-4231	276	21	isolate	isolate	VERB
ijpds-4231	276	22	38	38	NUM
ijpds-4231	276	23	(	(	PUNCT
ijpds-4231	276	24	yield	yield	NOUN
ijpds-4231	276	25	:	:	PUNCT
ijpds-4231	276	26	95	95	NUM
ijpds-4231	276	27	%	%	NOUN
ijpds-4231	276	28	,	,	PUNCT
ijpds-4231	276	29	purity	purity	NOUN
ijpds-4231	276	30	:	:	PUNCT
ijpds-4231	276	31	99.5	99.5	NUM
ijpds-4231	276	32	%	%	NOUN
ijpds-4231	276	33	by	by	ADP
ijpds-4231	276	34	hplc	hplc	NOUN
ijpds-4231	276	35	)	)	PUNCT
ijpds-4231	276	36	.	.	PUNCT
ijpds-4231	277	1	it	it	PRON
ijpds-4231	277	2	was	be	AUX
ijpds-4231	277	3	alkylated	alkylate	VERB
ijpds-4231	277	4	with	with	ADP
ijpds-4231	277	5	3	3	NUM
ijpds-4231	277	6	in	in	ADP
ijpds-4231	277	7	the	the	DET
ijpds-4231	277	8	presence	presence	NOUN
ijpds-4231	277	9	of	of	ADP
ijpds-4231	277	10	cesium	cesium	NOUN
ijpds-4231	277	11	carbonate	carbonate	NOUN
ijpds-4231	277	12	in	in	ADP
ijpds-4231	277	13	acetonitrile	acetonitrile	NOUN
ijpds-4231	277	14	to	to	PART
ijpds-4231	277	15	isolate	isolate	VERB
ijpds-4231	277	16	39	39	NUM
ijpds-4231	277	17	(	(	PUNCT
ijpds-4231	277	18	purity	purity	NOUN
ijpds-4231	277	19	:	:	PUNCT
ijpds-4231	277	20	97.8	97.8	NUM
ijpds-4231	277	21	%	%	NOUN
ijpds-4231	277	22	by	by	ADP
ijpds-4231	277	23	hplc	hplc	NOUN
ijpds-4231	277	24	)	)	PUNCT
ijpds-4231	277	25	and	and	CCONJ
ijpds-4231	277	26	then	then	ADV
ijpds-4231	277	27	hydrolyzed	hydrolyze	VERB
ijpds-4231	277	28	in	in	ADP
ijpds-4231	277	29	the	the	DET
ijpds-4231	277	30	presence	presence	NOUN
ijpds-4231	277	31	of	of	ADP
ijpds-4231	277	32	potassium	potassium	NOUN
ijpds-4231	277	33	hydroxide	hydroxide	NOUN
ijpds-4231	277	34	solution	solution	NOUN
ijpds-4231	277	35	and	and	CCONJ
ijpds-4231	277	36	methyl	methyl	NOUN
ijpds-4231	277	37	alcohol	alcohol	NOUN
ijpds-4231	277	38	to	to	PART
ijpds-4231	277	39	get	get	VERB
ijpds-4231	277	40	r	r	NOUN
ijpds-4231	277	41	-	-	PUNCT
ijpds-4231	277	42	rasagiline	rasagiline	NOUN
ijpds-4231	277	43	base	base	NOUN
ijpds-4231	277	44	(	(	PUNCT
ijpds-4231	277	45	purity	purity	NOUN
ijpds-4231	277	46	:	:	PUNCT
ijpds-4231	277	47	99.5	99.5	NUM
ijpds-4231	277	48	%	%	NOUN
ijpds-4231	277	49	by	by	ADP
ijpds-4231	277	50	hplc	hplc	NOUN
ijpds-4231	277	51	)	)	PUNCT
ijpds-4231	277	52	.	.	PUNCT
ijpds-4231	278	1	it	it	PRON
ijpds-4231	278	2	was	be	AUX
ijpds-4231	278	3	taken	take	VERB
ijpds-4231	278	4	in	in	ADP
ijpds-4231	278	5	isopropyl	isopropyl	NOUN
ijpds-4231	278	6	alcohol	alcohol	NOUN
ijpds-4231	278	7	and	and	CCONJ
ijpds-4231	278	8	added	add	VERB
ijpds-4231	278	9	methanesulfonic	methanesulfonic	ADJ
ijpds-4231	278	10	acid	acid	NOUN
ijpds-4231	278	11	to	to	PART
ijpds-4231	278	12	get	get	VERB
ijpds-4231	278	13	1	1	NUM
ijpds-4231	278	14	(	(	PUNCT
ijpds-4231	278	15	yield	yield	NOUN
ijpds-4231	278	16	:	:	PUNCT
ijpds-4231	278	17	88	88	NUM
ijpds-4231	278	18	%	%	NOUN
ijpds-4231	278	19	,	,	PUNCT
ijpds-4231	278	20	purity	purity	NOUN
ijpds-4231	278	21	:	:	PUNCT
ijpds-4231	278	22	100	100	NUM
ijpds-4231	278	23	%	%	NOUN
ijpds-4231	278	24	by	by	ADP
ijpds-4231	278	25	hplc	hplc	NOUN
ijpds-4231	278	26	,	,	PUNCT
ijpds-4231	278	27	as	as	ADP
ijpds-4231	278	28	white	white	ADJ
ijpds-4231	278	29	crystals	crystal	NOUN
ijpds-4231	278	30	)	)	PUNCT
ijpds-4231	279	1	[	[	X
ijpds-4231	279	2	52	52	NUM
ijpds-4231	279	3	]	]	PUNCT
ijpds-4231	279	4	.	.	PUNCT
ijpds-4231	280	1	yao	yao	PROPN
ijpds-4231	280	2	q	q	PROPN
ijpds-4231	280	3	&	&	CCONJ
ijpds-4231	280	4	chen	chen	PROPN
ijpds-4231	281	1	z	z	PROPN
ijpds-4231	281	2	,	,	PUNCT
ijpds-4231	281	3	in	in	ADP
ijpds-4231	281	4	2012	2012	NUM
ijpds-4231	281	5	,	,	PUNCT
ijpds-4231	281	6	had	have	AUX
ijpds-4231	281	7	illustrated	illustrate	VERB
ijpds-4231	281	8	the	the	DET
ijpds-4231	281	9	condensation	condensation	NOUN
ijpds-4231	281	10	of	of	ADP
ijpds-4231	281	11	9	9	NUM
ijpds-4231	281	12	with	with	ADP
ijpds-4231	281	13	6	6	NUM
ijpds-4231	281	14	in	in	ADP
ijpds-4231	281	15	the	the	DET
ijpds-4231	281	16	presence	presence	NOUN
ijpds-4231	281	17	of	of	ADP
ijpds-4231	281	18	p	p	ADJ
ijpds-4231	281	19	-	-	PUNCT
ijpds-4231	281	20	toluenesulfonic	toluenesulfonic	ADJ
ijpds-4231	281	21	acid	acid	NOUN
ijpds-4231	281	22	in	in	ADP
ijpds-4231	281	23	methyl	methyl	NOUN
ijpds-4231	281	24	-	-	PUNCT
ijpds-4231	281	25	t	t	NOUN
ijpds-4231	281	26	-	-	PUNCT
ijpds-4231	281	27	butyl	butyl	NOUN
ijpds-4231	281	28	ether	ether	NOUN
ijpds-4231	281	29	to	to	PART
ijpds-4231	281	30	form	form	VERB
ijpds-4231	281	31	16	16	NUM
ijpds-4231	281	32	.	.	PUNCT
ijpds-4231	282	1	it	it	PRON
ijpds-4231	282	2	was	be	AUX
ijpds-4231	282	3	dissolved	dissolve	VERB
ijpds-4231	282	4	in	in	ADP
ijpds-4231	282	5	-	-	PUNCT
ijpds-4231	282	6	situ	situ	NOUN
ijpds-4231	282	7	in	in	ADP
ijpds-4231	282	8	toluene	toluene	NOUN
ijpds-4231	282	9	and	and	CCONJ
ijpds-4231	282	10	added	add	VERB
ijpds-4231	282	11	20	20	NUM
ijpds-4231	282	12	%	%	NOUN
ijpds-4231	282	13	di	di	NOUN
ijpds-4231	282	14	-	-	ADJ
ijpds-4231	282	15	isobutylaluminum	isobutylaluminum	ADJ
ijpds-4231	282	16	hydride	hydride	NOUN
ijpds-4231	282	17	solution	solution	NOUN
ijpds-4231	282	18	(	(	PUNCT
ijpds-4231	282	19	dibal	dibal	ADJ
ijpds-4231	282	20	-	-	PUNCT
ijpds-4231	282	21	h	h	NOUN
ijpds-4231	282	22	dissolved	dissolve	VERB
ijpds-4231	282	23	in	in	ADP
ijpds-4231	282	24	n	n	CCONJ
ijpds-4231	282	25	-	-	PUNCT
ijpds-4231	282	26	hexane	hexane	NOUN
ijpds-4231	282	27	)	)	PUNCT
ijpds-4231	282	28	and	and	CCONJ
ijpds-4231	282	29	worked	work	VERB
ijpds-4231	282	30	up	up	ADP
ijpds-4231	282	31	to	to	PART
ijpds-4231	282	32	isolate	isolate	VERB
ijpds-4231	282	33	racemic	racemic	ADJ
ijpds-4231	282	34	rasagiline	rasagiline	NOUN
ijpds-4231	282	35	base	base	NOUN
ijpds-4231	282	36	(	(	PUNCT
ijpds-4231	282	37	yield	yield	NOUN
ijpds-4231	282	38	:	:	PUNCT
ijpds-4231	282	39	81	81	NUM
ijpds-4231	282	40	%	%	NOUN
ijpds-4231	282	41	)	)	PUNCT
ijpds-4231	282	42	.	.	PUNCT
ijpds-4231	283	1	it	it	PRON
ijpds-4231	283	2	was	be	AUX
ijpds-4231	283	3	resolved	resolve	VERB
ijpds-4231	283	4	by	by	ADP
ijpds-4231	283	5	converting	convert	VERB
ijpds-4231	283	6	to	to	ADP
ijpds-4231	283	7	its	its	PRON
ijpds-4231	283	8	mandelate	mandelate	ADJ
ijpds-4231	283	9	salt	salt	NOUN
ijpds-4231	283	10	(	(	PUNCT
ijpds-4231	283	11	yield	yield	NOUN
ijpds-4231	283	12	:	:	PUNCT
ijpds-4231	283	13	45	45	NUM
ijpds-4231	283	14	%	%	NOUN
ijpds-4231	283	15	)	)	PUNCT
ijpds-4231	283	16	to	to	PART
ijpds-4231	283	17	isolate	isolate	VERB
ijpds-4231	283	18	the	the	DET
ijpds-4231	283	19	required	required	ADJ
ijpds-4231	283	20	r	r	NOUN
ijpds-4231	283	21	-	-	PUNCT
ijpds-4231	283	22	isomer	isomer	NOUN
ijpds-4231	283	23	.	.	PUNCT
ijpds-4231	284	1	it	it	PRON
ijpds-4231	284	2	was	be	AUX
ijpds-4231	284	3	subjected	subject	VERB
ijpds-4231	284	4	to	to	ADP
ijpds-4231	284	5	desaltation	desaltation	NOUN
ijpds-4231	284	6	(	(	PUNCT
ijpds-4231	284	7	yield	yield	NOUN
ijpds-4231	284	8	:	:	PUNCT
ijpds-4231	284	9	90	90	NUM
ijpds-4231	284	10	%	%	NOUN
ijpds-4231	284	11	)	)	PUNCT
ijpds-4231	284	12	using	use	VERB
ijpds-4231	284	13	sodium	sodium	NOUN
ijpds-4231	284	14	hydroxide	hydroxide	NOUN
ijpds-4231	284	15	solution	solution	NOUN
ijpds-4231	284	16	and	and	CCONJ
ijpds-4231	284	17	then	then	ADV
ijpds-4231	284	18	treated	treat	VERB
ijpds-4231	284	19	with	with	ADP
ijpds-4231	284	20	methanesulfonic	methanesulfonic	ADJ
ijpds-4231	284	21	acid	acid	NOUN
ijpds-4231	284	22	in	in	ADP
ijpds-4231	284	23	isopropyl	isopropyl	NOUN
ijpds-4231	284	24	alcohol	alcohol	NOUN
ijpds-4231	284	25	to	to	PART
ijpds-4231	284	26	obtain	obtain	VERB
ijpds-4231	284	27	1	1	NUM
ijpds-4231	284	28	(	(	PUNCT
ijpds-4231	284	29	yield	yield	NOUN
ijpds-4231	284	30	:	:	PUNCT
ijpds-4231	284	31	80	80	NUM
ijpds-4231	284	32	%	%	NOUN
ijpds-4231	284	33	)	)	PUNCT
ijpds-4231	285	1	[	[	X
ijpds-4231	285	2	53	53	NUM
ijpds-4231	285	3	]	]	PUNCT
ijpds-4231	285	4	.	.	PUNCT
ijpds-4231	285	5	tang	tang	PROPN
ijpds-4231	285	6	l	l	PROPN
ijpds-4231	285	7	,	,	PUNCT
ijpds-4231	285	8	et	et	PROPN
ijpds-4231	285	9	al	al	PROPN
ijpds-4231	285	10	.	.	PROPN
ijpds-4231	285	11	,	,	PUNCT
ijpds-4231	285	12	in	in	ADP
ijpds-4231	285	13	2012	2012	NUM
ijpds-4231	285	14	,	,	PUNCT
ijpds-4231	285	15	had	have	AUX
ijpds-4231	285	16	reported	report	VERB
ijpds-4231	285	17	the	the	DET
ijpds-4231	285	18	treatment	treatment	NOUN
ijpds-4231	285	19	of	of	ADP
ijpds-4231	285	20	15	15	NUM
ijpds-4231	285	21	in	in	ADP
ijpds-4231	285	22	aqueous	aqueous	ADJ
ijpds-4231	285	23	ethyl	ethyl	PROPN
ijpds-4231	285	24	alcohol	alcohol	NOUN
ijpds-4231	285	25	with	with	SCONJ
ijpds-4231	285	26	aluminium	aluminium	NOUN
ijpds-4231	285	27	-	-	PUNCT
ijpds-4231	285	28	amalgum	amalgum	NOUN
ijpds-4231	285	29	to	to	PART
ijpds-4231	285	30	isolate	isolate	VERB
ijpds-4231	285	31	racemic	racemic	ADJ
ijpds-4231	285	32	2	2	NUM
ijpds-4231	285	33	(	(	PUNCT
ijpds-4231	285	34	purity	purity	NOUN
ijpds-4231	285	35	:	:	PUNCT
ijpds-4231	285	36	98.9	98.9	NUM
ijpds-4231	285	37	-	-	SYM
ijpds-4231	285	38	99.9	99.9	NUM
ijpds-4231	285	39	%	%	NOUN
ijpds-4231	285	40	)	)	PUNCT
ijpds-4231	285	41	.	.	PUNCT
ijpds-4231	286	1	it	it	PRON
ijpds-4231	286	2	was	be	AUX
ijpds-4231	286	3	condensed	condense	VERB
ijpds-4231	286	4	with	with	ADP
ijpds-4231	286	5	8	8	NUM
ijpds-4231	286	6	in	in	ADP
ijpds-4231	286	7	the	the	DET
ijpds-4231	286	8	presence	presence	NOUN
ijpds-4231	286	9	of	of	ADP
ijpds-4231	286	10	sodium	sodium	NOUN
ijpds-4231	286	11	hydroxide	hydroxide	NOUN
ijpds-4231	286	12	solution	solution	NOUN
ijpds-4231	286	13	and	and	CCONJ
ijpds-4231	286	14	dichloromethane	dichloromethane	NOUN
ijpds-4231	286	15	to	to	PART
ijpds-4231	286	16	form	form	VERB
ijpds-4231	286	17	racemic	racemic	ADJ
ijpds-4231	286	18	rasagiline	rasagiline	NOUN
ijpds-4231	286	19	base	base	NOUN
ijpds-4231	286	20	.	.	PUNCT
ijpds-4231	287	1	it	it	PRON
ijpds-4231	287	2	was	be	AUX
ijpds-4231	287	3	resolved	resolve	VERB
ijpds-4231	287	4	by	by	ADP
ijpds-4231	287	5	the	the	DET
ijpds-4231	287	6	formation	formation	NOUN
ijpds-4231	287	7	of	of	ADP
ijpds-4231	287	8	tartarate	tartarate	ADJ
ijpds-4231	287	9	salt	salt	NOUN
ijpds-4231	287	10	in	in	ADP
ijpds-4231	287	11	isopropyl	isopropyl	NOUN
ijpds-4231	287	12	alcohol	alcohol	NOUN
ijpds-4231	287	13	to	to	PART
ijpds-4231	287	14	isolate	isolate	VERB
ijpds-4231	287	15	r	r	NOUN
ijpds-4231	287	16	-	-	PUNCT
ijpds-4231	287	17	rasagiline	rasagiline	NOUN
ijpds-4231	287	18	tartarate	tartarate	NOUN
ijpds-4231	287	19	with	with	ADP
ijpds-4231	287	20	a	a	DET
ijpds-4231	287	21	melting	melt	VERB
ijpds-4231	287	22	sanjay	sanjay	NOUN
ijpds-4231	287	23	s	s	PART
ijpds-4231	287	24	s	s	NOUN
ijpds-4231	287	25	patents	patent	NOUN
ijpds-4231	287	26	disclosed	disclose	VERB
ijpds-4231	287	27	synthetic	synthetic	ADJ
ijpds-4231	287	28	overview	overview	NOUN
ijpds-4231	287	29	of	of	ADP
ijpds-4231	287	30	rasagiline	rasagiline	ADJ
ijpds-4231	287	31	vol	vol	NOUN
ijpds-4231	287	32	2	2	NUM
ijpds-4231	287	33	|	|	ADV
ijpds-4231	287	34	issue	issue	VERB
ijpds-4231	287	35	4	4	NUM
ijpds-4231	287	36	|	|	ADV
ijpds-4231	287	37	oct	oct	PROPN
ijpds-4231	287	38	–	–	PUNCT
ijpds-4231	288	1	dec	dec	PROPN
ijpds-4231	288	2	2023	2023	NUM
ijpds-4231	288	3	indian	indian	PROPN
ijpds-4231	288	4	j	j	PROPN
ijpds-4231	288	5	pharm	pharm	PROPN
ijpds-4231	288	6	drug	drug	PROPN
ijpds-4231	288	7	studies	study	NOUN
ijpds-4231	288	8	|	|	ADV
ijpds-4231	288	9	140	140	NUM
ijpds-4231	288	10	point	point	NOUN
ijpds-4231	288	11	of	of	ADP
ijpds-4231	288	12	174.9	174.9	NUM
ijpds-4231	288	13	-	-	SYM
ijpds-4231	288	14	176.3oc	176.3oc	NUM
ijpds-4231	288	15	(	(	PUNCT
ijpds-4231	288	16	yield	yield	NOUN
ijpds-4231	288	17	:	:	PUNCT
ijpds-4231	288	18	41.05	41.05	NUM
ijpds-4231	288	19	%	%	NOUN
ijpds-4231	288	20	)	)	PUNCT
ijpds-4231	288	21	.	.	PUNCT
ijpds-4231	289	1	it	it	PRON
ijpds-4231	289	2	was	be	AUX
ijpds-4231	289	3	dissolved	dissolve	VERB
ijpds-4231	289	4	in	in	ADP
ijpds-4231	289	5	isopropyl	isopropyl	NOUN
ijpds-4231	289	6	alcohol	alcohol	NOUN
ijpds-4231	289	7	and	and	CCONJ
ijpds-4231	289	8	treated	treat	VERB
ijpds-4231	289	9	with	with	ADP
ijpds-4231	289	10	methanesulfonic	methanesulfonic	ADJ
ijpds-4231	289	11	acid	acid	NOUN
ijpds-4231	289	12	to	to	PART
ijpds-4231	289	13	obtain	obtain	VERB
ijpds-4231	289	14	1	1	NUM
ijpds-4231	289	15	with	with	ADP
ijpds-4231	289	16	a	a	DET
ijpds-4231	289	17	melting	melting	NOUN
ijpds-4231	289	18	point	point	NOUN
ijpds-4231	289	19	of	of	ADP
ijpds-4231	289	20	150.1	150.1	NUM
ijpds-4231	289	21	-	-	PUNCT
ijpds-4231	289	22	151oc	151oc	NOUN
ijpds-4231	289	23	(	(	PUNCT
ijpds-4231	289	24	yield	yield	NOUN
ijpds-4231	289	25	:	:	PUNCT
ijpds-4231	289	26	81	81	NUM
ijpds-4231	289	27	%	%	NOUN
ijpds-4231	289	28	)	)	PUNCT
ijpds-4231	290	1	[	[	X
ijpds-4231	290	2	54	54	NUM
ijpds-4231	290	3	]	]	PUNCT
ijpds-4231	290	4	.	.	PUNCT
ijpds-4231	291	1	nagarajan	nagarajan	PROPN
ijpds-4231	291	2	k	k	PROPN
ijpds-4231	291	3	,	,	PUNCT
ijpds-4231	291	4	et	et	PROPN
ijpds-4231	291	5	al	al	PROPN
ijpds-4231	291	6	.	.	PROPN
ijpds-4231	291	7	,	,	PUNCT
ijpds-4231	291	8	in	in	ADP
ijpds-4231	291	9	2012	2012	NUM
ijpds-4231	291	10	,	,	PUNCT
ijpds-4231	291	11	had	have	AUX
ijpds-4231	291	12	demonstrated	demonstrate	VERB
ijpds-4231	291	13	a	a	DET
ijpds-4231	291	14	process	process	NOUN
ijpds-4231	291	15	to	to	PART
ijpds-4231	291	16	isolate	isolate	VERB
ijpds-4231	291	17	1	1	NUM
ijpds-4231	291	18	with	with	ADP
ijpds-4231	291	19	a	a	DET
ijpds-4231	291	20	particle	particle	NOUN
ijpds-4231	291	21	size	size	NOUN
ijpds-4231	291	22	of	of	ADP
ijpds-4231	291	23	about	about	ADV
ijpds-4231	291	24	255	255	NUM
ijpds-4231	291	25	-	-	SYM
ijpds-4231	291	26	590	590	NUM
ijpds-4231	291	27	microns	micron	NOUN
ijpds-4231	291	28	.	.	PUNCT
ijpds-4231	292	1	it	it	PRON
ijpds-4231	292	2	was	be	AUX
ijpds-4231	292	3	achieved	achieve	VERB
ijpds-4231	292	4	by	by	ADP
ijpds-4231	292	5	the	the	DET
ijpds-4231	292	6	crystallization	crystallization	NOUN
ijpds-4231	292	7	from	from	ADP
ijpds-4231	292	8	isopropyl	isopropyl	NOUN
ijpds-4231	292	9	alcohol	alcohol	NOUN
ijpds-4231	292	10	and	and	CCONJ
ijpds-4231	292	11	the	the	DET
ijpds-4231	292	12	disclosed	disclose	VERB
ijpds-4231	292	13	method	method	NOUN
ijpds-4231	292	14	was	be	AUX
ijpds-4231	292	15	devoid	devoid	ADJ
ijpds-4231	292	16	of	of	ADP
ijpds-4231	292	17	routine	routine	ADJ
ijpds-4231	292	18	comminution	comminution	NOUN
ijpds-4231	292	19	techniques	technique	NOUN
ijpds-4231	292	20	to	to	PART
ijpds-4231	292	21	control	control	VERB
ijpds-4231	292	22	the	the	DET
ijpds-4231	292	23	particle	particle	NOUN
ijpds-4231	292	24	size	size	NOUN
ijpds-4231	292	25	of	of	ADP
ijpds-4231	292	26	1	1	NUM
ijpds-4231	293	1	[	[	X
ijpds-4231	293	2	55	55	NUM
ijpds-4231	293	3	]	]	PUNCT
ijpds-4231	293	4	.	.	PUNCT
ijpds-4231	294	1	dwivedi	dwivedi	PROPN
ijpds-4231	294	2	sd	sd	PROPN
ijpds-4231	294	3	,	,	PUNCT
ijpds-4231	294	4	et	et	PROPN
ijpds-4231	294	5	al	al	PROPN
ijpds-4231	294	6	.	.	PROPN
ijpds-4231	294	7	,	,	PUNCT
ijpds-4231	294	8	in	in	ADP
ijpds-4231	294	9	2011	2011	NUM
ijpds-4231	294	10	,	,	PUNCT
ijpds-4231	294	11	had	have	AUX
ijpds-4231	294	12	illustrated	illustrate	VERB
ijpds-4231	294	13	the	the	DET
ijpds-4231	294	14	process	process	NOUN
ijpds-4231	294	15	to	to	PART
ijpds-4231	294	16	isolate	isolate	VERB
ijpds-4231	294	17	r	r	NOUN
ijpds-4231	294	18	-	-	PUNCT
ijpds-4231	294	19	rasagiline	rasagiline	NOUN
ijpds-4231	294	20	besylate	besylate	ADJ
ijpds-4231	294	21	form	form	NOUN
ijpds-4231	294	22	-	-	PUNCT
ijpds-4231	294	23	i	i	PRON
ijpds-4231	294	24	with	with	ADP
ijpds-4231	294	25	the	the	DET
ijpds-4231	294	26	larger	large	ADJ
ijpds-4231	294	27	particle	particle	NOUN
ijpds-4231	294	28	size	size	NOUN
ijpds-4231	294	29	by	by	ADP
ijpds-4231	294	30	treating	treat	VERB
ijpds-4231	294	31	rasagiline	rasagiline	NOUN
ijpds-4231	294	32	base	base	NOUN
ijpds-4231	294	33	with	with	ADP
ijpds-4231	294	34	benzene	benzene	NOUN
ijpds-4231	294	35	sulfonic	sulfonic	ADJ
ijpds-4231	294	36	acid	acid	NOUN
ijpds-4231	294	37	solution	solution	NOUN
ijpds-4231	294	38	in	in	ADP
ijpds-4231	294	39	ethyl	ethyl	PROPN
ijpds-4231	294	40	acetate	acetate	NOUN
ijpds-4231	294	41	.	.	PUNCT
ijpds-4231	295	1	similarly	similarly	ADV
ijpds-4231	295	2	,	,	PUNCT
ijpds-4231	295	3	a	a	DET
ijpds-4231	295	4	few	few	ADJ
ijpds-4231	295	5	other	other	ADJ
ijpds-4231	295	6	salts	salt	NOUN
ijpds-4231	295	7	were	be	AUX
ijpds-4231	295	8	also	also	ADV
ijpds-4231	295	9	prepared	prepare	VERB
ijpds-4231	295	10	like	like	ADP
ijpds-4231	295	11	r	r	NOUN
ijpds-4231	295	12	-	-	PUNCT
ijpds-4231	295	13	rasagiline	rasagiline	NOUN
ijpds-4231	295	14	hydrobromide	hydrobromide	NOUN
ijpds-4231	295	15	form	form	NOUN
ijpds-4231	295	16	-	-	PUNCT
ijpds-4231	295	17	i	i	PRON
ijpds-4231	295	18	and	and	CCONJ
ijpds-4231	295	19	its	its	PRON
ijpds-4231	295	20	larger	large	ADJ
ijpds-4231	295	21	particle	particle	NOUN
ijpds-4231	295	22	size	size	NOUN
ijpds-4231	295	23	,	,	PUNCT
ijpds-4231	295	24	amorphous	amorphous	ADJ
ijpds-4231	295	25	rasagiline	rasagiline	NOUN
ijpds-4231	295	26	hydrobromide	hydrobromide	NOUN
ijpds-4231	295	27	,	,	PUNCT
ijpds-4231	295	28	r	r	NOUN
ijpds-4231	295	29	-	-	PUNCT
ijpds-4231	295	30	rasagiline	rasagiline	NOUN
ijpds-4231	295	31	hydrogen	hydrogen	NOUN
ijpds-4231	295	32	phosphate	phosphate	NOUN
ijpds-4231	295	33	form	form	NOUN
ijpds-4231	295	34	-	-	PUNCT
ijpds-4231	295	35	i	i	PRON
ijpds-4231	295	36	and	and	CCONJ
ijpds-4231	295	37	form	form	NOUN
ijpds-4231	295	38	-	-	PUNCT
ijpds-4231	295	39	i	i	PRON
ijpds-4231	295	40	of	of	ADP
ijpds-4231	295	41	1	1	NUM
ijpds-4231	295	42	.	.	PUNCT
ijpds-4231	296	1	the	the	DET
ijpds-4231	296	2	reaction	reaction	NOUN
ijpds-4231	296	3	of	of	ADP
ijpds-4231	296	4	9	9	NUM
ijpds-4231	296	5	in	in	ADP
ijpds-4231	296	6	methyl	methyl	NOUN
ijpds-4231	296	7	alcohol	alcohol	NOUN
ijpds-4231	296	8	with	with	ADP
ijpds-4231	296	9	hydroxylamine	hydroxylamine	ADJ
ijpds-4231	296	10	hydrochloride	hydrochloride	NOUN
ijpds-4231	296	11	was	be	AUX
ijpds-4231	296	12	carried	carry	VERB
ijpds-4231	296	13	out	out	ADP
ijpds-4231	296	14	in	in	ADP
ijpds-4231	296	15	the	the	DET
ijpds-4231	296	16	presence	presence	NOUN
ijpds-4231	296	17	of	of	ADP
ijpds-4231	296	18	sodium	sodium	NOUN
ijpds-4231	296	19	hydroxide	hydroxide	NOUN
ijpds-4231	296	20	solution	solution	NOUN
ijpds-4231	296	21	to	to	PART
ijpds-4231	296	22	obtain	obtain	VERB
ijpds-4231	296	23	15	15	NUM
ijpds-4231	296	24	.	.	PUNCT
ijpds-4231	297	1	it	it	PRON
ijpds-4231	297	2	was	be	AUX
ijpds-4231	297	3	reduced	reduce	VERB
ijpds-4231	297	4	under	under	ADP
ijpds-4231	297	5	the	the	DET
ijpds-4231	297	6	catalytic	catalytic	ADJ
ijpds-4231	297	7	impact	impact	NOUN
ijpds-4231	297	8	of	of	ADP
ijpds-4231	297	9	raney	raney	NOUN
ijpds-4231	297	10	-	-	PUNCT
ijpds-4231	297	11	nickel	nickel	NOUN
ijpds-4231	297	12	(	(	PUNCT
ijpds-4231	297	13	with	with	ADP
ijpds-4231	297	14	5	5	NUM
ijpds-4231	297	15	kg	kg	NOUN
ijpds-4231	297	16	of	of	ADP
ijpds-4231	297	17	hydrogen	hydrogen	NOUN
ijpds-4231	297	18	pressure	pressure	NOUN
ijpds-4231	297	19	)	)	PUNCT
ijpds-4231	297	20	in	in	ADP
ijpds-4231	297	21	the	the	DET
ijpds-4231	297	22	presence	presence	NOUN
ijpds-4231	297	23	of	of	ADP
ijpds-4231	297	24	ammoniacal	ammoniacal	ADJ
ijpds-4231	297	25	methyl	methyl	NOUN
ijpds-4231	297	26	alcohol	alcohol	NOUN
ijpds-4231	297	27	to	to	PART
ijpds-4231	297	28	get	get	VERB
ijpds-4231	297	29	racemic	racemic	ADJ
ijpds-4231	297	30	2	2	NUM
ijpds-4231	297	31	.	.	PUNCT
ijpds-4231	298	1	it	it	PRON
ijpds-4231	298	2	was	be	AUX
ijpds-4231	298	3	treated	treat	VERB
ijpds-4231	298	4	with	with	ADP
ijpds-4231	298	5	7	7	NUM
ijpds-4231	298	6	in	in	ADP
ijpds-4231	298	7	the	the	DET
ijpds-4231	298	8	presence	presence	NOUN
ijpds-4231	298	9	of	of	ADP
ijpds-4231	298	10	potassium	potassium	NOUN
ijpds-4231	298	11	carbonate	carbonate	NOUN
ijpds-4231	298	12	and	and	CCONJ
ijpds-4231	298	13	sodium	sodium	NOUN
ijpds-4231	298	14	hydroxide	hydroxide	NOUN
ijpds-4231	298	15	using	use	VERB
ijpds-4231	298	16	the	the	DET
ijpds-4231	298	17	solvent	solvent	ADJ
ijpds-4231	298	18	dimethyl	dimethyl	NOUN
ijpds-4231	298	19	formamide	formamide	ADV
ijpds-4231	298	20	to	to	PART
ijpds-4231	298	21	isolate	isolate	VERB
ijpds-4231	298	22	the	the	DET
ijpds-4231	298	23	racemic	racemic	ADJ
ijpds-4231	298	24	rasagiline	rasagiline	NOUN
ijpds-4231	298	25	base	base	NOUN
ijpds-4231	298	26	(	(	PUNCT
ijpds-4231	298	27	as	as	ADP
ijpds-4231	298	28	yellow	yellow	ADJ
ijpds-4231	298	29	oil	oil	NOUN
ijpds-4231	298	30	)	)	PUNCT
ijpds-4231	298	31	.	.	PUNCT
ijpds-4231	299	1	the	the	DET
ijpds-4231	299	2	isolated	isolated	ADJ
ijpds-4231	299	3	base	base	NOUN
ijpds-4231	299	4	was	be	AUX
ijpds-4231	299	5	resolved	resolve	VERB
ijpds-4231	299	6	using	use	VERB
ijpds-4231	299	7	l-(+)-tartaric	l-(+)-tartaric	ADJ
ijpds-4231	299	8	acid	acid	NOUN
ijpds-4231	299	9	and	and	CCONJ
ijpds-4231	299	10	desalted	desalt	VERB
ijpds-4231	299	11	to	to	PART
ijpds-4231	299	12	isolate	isolate	VERB
ijpds-4231	299	13	r	r	NOUN
ijpds-4231	299	14	-	-	PUNCT
ijpds-4231	299	15	rasagiline	rasagiline	NOUN
ijpds-4231	299	16	base	base	NOUN
ijpds-4231	299	17	(	(	PUNCT
ijpds-4231	299	18	as	as	ADP
ijpds-4231	299	19	oil	oil	NOUN
ijpds-4231	299	20	)	)	PUNCT
ijpds-4231	299	21	and	and	CCONJ
ijpds-4231	299	22	then	then	ADV
ijpds-4231	299	23	converted	convert	VERB
ijpds-4231	299	24	to	to	ADP
ijpds-4231	299	25	required	require	VERB
ijpds-4231	299	26	salt	salt	NOUN
ijpds-4231	299	27	forms	form	NOUN
ijpds-4231	299	28	[	[	X
ijpds-4231	299	29	56	56	NUM
ijpds-4231	299	30	]	]	PUNCT
ijpds-4231	299	31	.	.	PUNCT
ijpds-4231	300	1	zhang	zhang	PROPN
ijpds-4231	300	2	r	r	PROPN
ijpds-4231	300	3	,	,	PUNCT
ijpds-4231	300	4	et	et	PROPN
ijpds-4231	300	5	al	al	PROPN
ijpds-4231	300	6	.	.	PROPN
ijpds-4231	300	7	,	,	PUNCT
ijpds-4231	300	8	in	in	ADP
ijpds-4231	300	9	2012	2012	NUM
ijpds-4231	300	10	,	,	PUNCT
ijpds-4231	300	11	had	have	AUX
ijpds-4231	300	12	disclosed	disclose	VERB
ijpds-4231	300	13	the	the	DET
ijpds-4231	300	14	condensation	condensation	NOUN
ijpds-4231	300	15	of	of	ADP
ijpds-4231	300	16	r	r	NOUN
ijpds-4231	300	17	-	-	PUNCT
ijpds-4231	300	18	isomer	isomer	NOUN
ijpds-4231	300	19	of	of	ADP
ijpds-4231	300	20	2	2	NUM
ijpds-4231	300	21	in	in	ADP
ijpds-4231	300	22	acetonitrile	acetonitrile	NOUN
ijpds-4231	300	23	with	with	ADP
ijpds-4231	300	24	propargyl	propargyl	PROPN
ijpds-4231	300	25	methanesulfonate	methanesulfonate	PROPN
ijpds-4231	300	26	44	44	NUM
ijpds-4231	300	27	to	to	PART
ijpds-4231	300	28	isolate	isolate	VERB
ijpds-4231	300	29	1	1	NUM
ijpds-4231	300	30	with	with	ADP
ijpds-4231	300	31	a	a	DET
ijpds-4231	300	32	melting	melting	NOUN
ijpds-4231	300	33	point	point	NOUN
ijpds-4231	300	34	of	of	ADP
ijpds-4231	300	35	156	156	NUM
ijpds-4231	300	36	-	-	PUNCT
ijpds-4231	300	37	158oc	158oc	NOUN
ijpds-4231	300	38	(	(	PUNCT
ijpds-4231	300	39	yield	yield	NOUN
ijpds-4231	300	40	:	:	PUNCT
ijpds-4231	300	41	97.8	97.8	NUM
ijpds-4231	300	42	%	%	NOUN
ijpds-4231	300	43	)	)	PUNCT
ijpds-4231	300	44	.	.	PUNCT
ijpds-4231	301	1	the	the	DET
ijpds-4231	301	2	isolation	isolation	NOUN
ijpds-4231	301	3	of	of	ADP
ijpds-4231	301	4	1	1	NUM
ijpds-4231	301	5	in	in	ADP
ijpds-4231	301	6	different	different	ADJ
ijpds-4231	301	7	scales	scale	NOUN
ijpds-4231	301	8	as	as	ADP
ijpds-4231	301	9	above	above	ADV
ijpds-4231	301	10	was	be	AUX
ijpds-4231	301	11	reported	report	VERB
ijpds-4231	301	12	via	via	ADP
ijpds-4231	301	13	one	one	NUM
ijpds-4231	301	14	-	-	PUNCT
ijpds-4231	301	15	pot	pot	NOUN
ijpds-4231	301	16	processes	process	NOUN
ijpds-4231	301	17	(	(	PUNCT
ijpds-4231	301	18	yield	yield	NOUN
ijpds-4231	301	19	:	:	PUNCT
ijpds-4231	301	20	85	85	NUM
ijpds-4231	301	21	-	-	SYM
ijpds-4231	301	22	92	92	NUM
ijpds-4231	301	23	%	%	NOUN
ijpds-4231	301	24	)	)	PUNCT
ijpds-4231	301	25	along	along	ADP
ijpds-4231	301	26	with	with	ADP
ijpds-4231	301	27	a	a	DET
ijpds-4231	301	28	few	few	ADJ
ijpds-4231	301	29	comparative	comparative	ADJ
ijpds-4231	301	30	examples	example	NOUN
ijpds-4231	301	31	as	as	ADP
ijpds-4231	301	32	per	per	ADP
ijpds-4231	301	33	the	the	DET
ijpds-4231	301	34	past	past	ADJ
ijpds-4231	301	35	disclosures	disclosure	NOUN
ijpds-4231	301	36	[	[	X
ijpds-4231	301	37	57	57	NUM
ijpds-4231	301	38	]	]	PUNCT
ijpds-4231	301	39	.	.	PUNCT
ijpds-4231	302	1	bahar	bahar	PROPN
ijpds-4231	302	2	e	e	PROPN
ijpds-4231	302	3	,	,	PUNCT
ijpds-4231	302	4	et	et	PROPN
ijpds-4231	302	5	al	al	PROPN
ijpds-4231	302	6	.	.	PROPN
ijpds-4231	302	7	,	,	PUNCT
ijpds-4231	302	8	2012	2012	NUM
ijpds-4231	302	9	,	,	PUNCT
ijpds-4231	302	10	had	have	AUX
ijpds-4231	302	11	demonstrated	demonstrate	VERB
ijpds-4231	302	12	the	the	DET
ijpds-4231	302	13	synthesis	synthesis	NOUN
ijpds-4231	302	14	and	and	CCONJ
ijpds-4231	302	15	applications	application	NOUN
ijpds-4231	302	16	of	of	ADP
ijpds-4231	302	17	deuterated	deuterate	VERB
ijpds-4231	302	18	rasagiline	rasagiline	NOUN
ijpds-4231	302	19	,	,	PUNCT
ijpds-4231	302	20	its	its	PRON
ijpds-4231	302	21	salts	salt	NOUN
ijpds-4231	302	22	.	.	PUNCT
ijpds-4231	303	1	the	the	DET
ijpds-4231	303	2	work	work	NOUN
ijpds-4231	303	3	was	be	AUX
ijpds-4231	303	4	primarily	primarily	ADV
ijpds-4231	303	5	focused	focus	VERB
ijpds-4231	303	6	on	on	ADP
ijpds-4231	303	7	the	the	DET
ijpds-4231	303	8	varied	varied	ADJ
ijpds-4231	303	9	metabolic	metabolic	NOUN
ijpds-4231	303	10	profile	profile	NOUN
ijpds-4231	303	11	of	of	ADP
ijpds-4231	303	12	deuterated	deuterate	VERB
ijpds-4231	303	13	forms	form	NOUN
ijpds-4231	303	14	of	of	ADP
ijpds-4231	303	15	rasagiline	rasagiline	NOUN
ijpds-4231	303	16	than	than	ADP
ijpds-4231	303	17	the	the	DET
ijpds-4231	303	18	protonated	protonate	VERB
ijpds-4231	303	19	forms	form	NOUN
ijpds-4231	303	20	.	.	PUNCT
ijpds-4231	304	1	to	to	PART
ijpds-4231	304	2	substantiate	substantiate	VERB
ijpds-4231	304	3	it	it	PRON
ijpds-4231	304	4	,	,	PUNCT
ijpds-4231	304	5	phase	phase	NOUN
ijpds-4231	304	6	-	-	PUNCT
ijpds-4231	304	7	i	i	PRON
ijpds-4231	304	8	bio	bio	NOUN
ijpds-4231	304	9	-	-	PUNCT
ijpds-4231	304	10	trasformations	trasformation	NOUN
ijpds-4231	304	11	of	of	ADP
ijpds-4231	304	12	deuterated	deuterate	VERB
ijpds-4231	304	13	rasagiline	rasagiline	NOUN
ijpds-4231	304	14	was	be	AUX
ijpds-4231	304	15	conducted	conduct	VERB
ijpds-4231	304	16	with	with	ADP
ijpds-4231	304	17	encouraging	encourage	VERB
ijpds-4231	304	18	results	result	NOUN
ijpds-4231	304	19	[	[	X
ijpds-4231	304	20	58	58	NUM
ijpds-4231	304	21	]	]	PUNCT
ijpds-4231	304	22	.	.	PUNCT
ijpds-4231	305	1	ulanenko	ulanenko	PROPN
ijpds-4231	305	2	k	k	PROPN
ijpds-4231	305	3	,	,	PUNCT
ijpds-4231	305	4	et	et	PROPN
ijpds-4231	305	5	al	al	PROPN
ijpds-4231	305	6	.	.	PROPN
ijpds-4231	305	7	,	,	PUNCT
ijpds-4231	305	8	in	in	ADP
ijpds-4231	305	9	2013	2013	NUM
ijpds-4231	305	10	,	,	PUNCT
ijpds-4231	305	11	had	have	AUX
ijpds-4231	305	12	reported	report	VERB
ijpds-4231	305	13	the	the	DET
ijpds-4231	305	14	synthesis	synthesis	NOUN
ijpds-4231	305	15	of	of	ADP
ijpds-4231	305	16	2-(2-((2	2-(2-((2	NUM
ijpds-4231	305	17	,	,	PUNCT
ijpds-4231	305	18	3	3	NUM
ijpds-4231	305	19	-	-	PUNCT
ijpds-4231	305	20	dihydro	dihydro	NOUN
ijpds-4231	305	21	-	-	PUNCT
ijpds-4231	305	22	li/-inden	li/-inden	PROPN
ijpds-4231	305	23	-	-	PUNCT
ijpds-4231	305	24	l	l	NOUN
ijpds-4231	305	25	-	-	PUNCT
ijpds-4231	305	26	yl)(prop-2	yl)(prop-2	NOUN
ijpds-4231	305	27	-	-	PUNCT
ijpds-4231	305	28	ynyl)amino)-2oxoethyl)-2	ynyl)amino)-2oxoethyl)-2	NOUN
ijpds-4231	305	29	-	-	PUNCT
ijpds-4231	305	30	hydroxysucckiic	hydroxysucckiic	NOUN
ijpds-4231	305	31	acid	acid	NOUN
ijpds-4231	305	32	42	42	NUM
ijpds-4231	305	33	from	from	ADP
ijpds-4231	305	34	citric	citric	ADJ
ijpds-4231	305	35	acid	acid	NOUN
ijpds-4231	305	36	41	41	NUM
ijpds-4231	305	37	.	.	PUNCT
ijpds-4231	306	1	in	in	ADP
ijpds-4231	306	2	the	the	DET
ijpds-4231	306	3	first	first	ADJ
ijpds-4231	306	4	step	step	NOUN
ijpds-4231	306	5	,	,	PUNCT
ijpds-4231	306	6	41	41	NUM
ijpds-4231	306	7	was	be	AUX
ijpds-4231	306	8	esterified	esterify	VERB
ijpds-4231	306	9	to	to	PART
ijpds-4231	306	10	form	form	VERB
ijpds-4231	306	11	trimethyl	trimethyl	NUM
ijpds-4231	306	12	citrate	citrate	NOUN
ijpds-4231	306	13	.	.	PUNCT
ijpds-4231	307	1	it	it	PRON
ijpds-4231	307	2	was	be	AUX
ijpds-4231	307	3	then	then	ADV
ijpds-4231	307	4	converted	convert	VERB
ijpds-4231	307	5	to	to	ADP
ijpds-4231	307	6	1	1	NUM
ijpds-4231	307	7	,	,	PUNCT
ijpds-4231	307	8	2	2	NUM
ijpds-4231	307	9	-	-	PUNCT
ijpds-4231	307	10	dimethyl	dimethyl	NOUN
ijpds-4231	307	11	citrate	citrate	NOUN
ijpds-4231	307	12	by	by	ADP
ijpds-4231	307	13	a	a	DET
ijpds-4231	307	14	selective	selective	ADJ
ijpds-4231	307	15	stearically	stearically	ADV
ijpds-4231	307	16	controlled	control	VERB
ijpds-4231	307	17	saponification	saponification	NOUN
ijpds-4231	307	18	.	.	PUNCT
ijpds-4231	308	1	in	in	ADP
ijpds-4231	308	2	the	the	DET
ijpds-4231	308	3	next	next	ADJ
ijpds-4231	308	4	step	step	NOUN
ijpds-4231	308	5	,	,	PUNCT
ijpds-4231	308	6	an	an	DET
ijpds-4231	308	7	amidation	amidation	NOUN
ijpds-4231	308	8	reaction	reaction	NOUN
ijpds-4231	308	9	was	be	AUX
ijpds-4231	308	10	conducted	conduct	VERB
ijpds-4231	308	11	between	between	ADP
ijpds-4231	308	12	r	r	NOUN
ijpds-4231	308	13	-	-	PUNCT
ijpds-4231	308	14	rasagiline	rasagiline	NOUN
ijpds-4231	308	15	base	base	NOUN
ijpds-4231	308	16	and	and	CCONJ
ijpds-4231	308	17	1	1	NUM
ijpds-4231	308	18	,	,	PUNCT
ijpds-4231	308	19	2	2	NUM
ijpds-4231	308	20	-	-	PUNCT
ijpds-4231	308	21	dimethyl	dimethyl	NOUN
ijpds-4231	308	22	citramide	citramide	NOUN
ijpds-4231	308	23	and	and	CCONJ
ijpds-4231	308	24	finally	finally	ADV
ijpds-4231	308	25	the	the	DET
ijpds-4231	308	26	esters	ester	NOUN
ijpds-4231	308	27	were	be	AUX
ijpds-4231	308	28	hydrolyzed	hydrolyze	VERB
ijpds-4231	308	29	to	to	PART
ijpds-4231	308	30	isolate	isolate	VERB
ijpds-4231	308	31	42	42	NUM
ijpds-4231	308	32	(	(	PUNCT
ijpds-4231	308	33	yield	yield	NOUN
ijpds-4231	308	34	:	:	PUNCT
ijpds-4231	308	35	3.5	3.5	NUM
ijpds-4231	308	36	%	%	NOUN
ijpds-4231	308	37	)	)	PUNCT
ijpds-4231	309	1	[	[	X
ijpds-4231	309	2	59	59	NUM
ijpds-4231	309	3	]	]	PUNCT
ijpds-4231	309	4	.	.	PUNCT
ijpds-4231	310	1	santosh	santosh	PROPN
ijpds-4231	310	2	vp	vp	PROPN
ijpds-4231	310	3	,	,	PUNCT
ijpds-4231	310	4	et	et	PROPN
ijpds-4231	310	5	al	al	PROPN
ijpds-4231	310	6	.	.	PROPN
ijpds-4231	310	7	,	,	PUNCT
ijpds-4231	310	8	in	in	ADP
ijpds-4231	310	9	2013	2013	NUM
ijpds-4231	310	10	,	,	PUNCT
ijpds-4231	310	11	had	have	AUX
ijpds-4231	310	12	reported	report	VERB
ijpds-4231	310	13	the	the	DET
ijpds-4231	310	14	condensation	condensation	NOUN
ijpds-4231	310	15	of	of	ADP
ijpds-4231	310	16	r-(-)-isomer	r-(-)-isomer	PROPN
ijpds-4231	310	17	of	of	ADP
ijpds-4231	310	18	2	2	NUM
ijpds-4231	310	19	hydrochloride	hydrochloride	NOUN
ijpds-4231	310	20	in	in	ADP
ijpds-4231	310	21	acetonitrile	acetonitrile	NOUN
ijpds-4231	310	22	with	with	ADP
ijpds-4231	310	23	7	7	NUM
ijpds-4231	310	24	in	in	ADP
ijpds-4231	310	25	the	the	DET
ijpds-4231	310	26	presence	presence	NOUN
ijpds-4231	310	27	of	of	ADP
ijpds-4231	310	28	potassium	potassium	NOUN
ijpds-4231	310	29	carbonate	carbonate	NOUN
ijpds-4231	310	30	to	to	PART
ijpds-4231	310	31	isolate	isolate	VERB
ijpds-4231	310	32	crude	crude	ADJ
ijpds-4231	310	33	base	base	NOUN
ijpds-4231	310	34	.	.	PUNCT
ijpds-4231	311	1	it	it	PRON
ijpds-4231	311	2	was	be	AUX
ijpds-4231	311	3	purified	purify	VERB
ijpds-4231	311	4	by	by	ADP
ijpds-4231	311	5	the	the	DET
ijpds-4231	311	6	selective	selective	ADJ
ijpds-4231	311	7	ph	ph	NOUN
ijpds-4231	311	8	adjustment	adjustment	NOUN
ijpds-4231	311	9	and	and	CCONJ
ijpds-4231	311	10	selective	selective	ADJ
ijpds-4231	311	11	extraction	extraction	NOUN
ijpds-4231	311	12	to	to	ADP
ijpds-4231	311	13	suitable	suitable	ADJ
ijpds-4231	311	14	solvents	solvent	NOUN
ijpds-4231	311	15	to	to	PART
ijpds-4231	311	16	isolate	isolate	VERB
ijpds-4231	311	17	rrasagiline	rrasagiline	ADJ
ijpds-4231	311	18	base	base	NOUN
ijpds-4231	311	19	(	(	PUNCT
ijpds-4231	311	20	purity	purity	NOUN
ijpds-4231	311	21	:	:	PUNCT
ijpds-4231	311	22	99.82	99.82	NUM
ijpds-4231	311	23	%	%	NOUN
ijpds-4231	311	24	by	by	ADP
ijpds-4231	311	25	hplc	hplc	NOUN
ijpds-4231	311	26	,	,	PUNCT
ijpds-4231	311	27	as	as	ADP
ijpds-4231	311	28	oily	oily	ADJ
ijpds-4231	311	29	mass	mass	NOUN
ijpds-4231	311	30	)	)	PUNCT
ijpds-4231	311	31	.	.	PUNCT
ijpds-4231	312	1	it	it	PRON
ijpds-4231	312	2	was	be	AUX
ijpds-4231	312	3	treated	treat	VERB
ijpds-4231	312	4	with	with	ADP
ijpds-4231	312	5	methanesulfonic	methanesulfonic	ADJ
ijpds-4231	312	6	acid	acid	NOUN
ijpds-4231	312	7	in	in	ADP
ijpds-4231	312	8	isopropyl	isopropyl	NOUN
ijpds-4231	312	9	alcohol	alcohol	NOUN
ijpds-4231	312	10	to	to	PART
ijpds-4231	312	11	obtain	obtain	VERB
ijpds-4231	312	12	1	1	NUM
ijpds-4231	312	13	(	(	PUNCT
ijpds-4231	312	14	purity	purity	NOUN
ijpds-4231	312	15	:	:	PUNCT
ijpds-4231	312	16	99.99	99.99	NUM
ijpds-4231	312	17	%	%	NOUN
ijpds-4231	312	18	by	by	ADP
ijpds-4231	312	19	hplc	hplc	PROPN
ijpds-4231	312	20	)	)	PUNCT
ijpds-4231	312	21	.	.	PUNCT
ijpds-4231	313	1	an	an	DET
ijpds-4231	313	2	optional	optional	ADJ
ijpds-4231	313	3	isolation	isolation	NOUN
ijpds-4231	313	4	of	of	ADP
ijpds-4231	313	5	free	free	ADJ
ijpds-4231	313	6	base	base	NOUN
ijpds-4231	313	7	was	be	AUX
ijpds-4231	313	8	reported	report	VERB
ijpds-4231	313	9	by	by	ADP
ijpds-4231	313	10	converting	convert	VERB
ijpds-4231	313	11	in	in	ADP
ijpds-4231	313	12	-	-	PUNCT
ijpds-4231	313	13	situ	situ	NOUN
ijpds-4231	313	14	to	to	ADP
ijpds-4231	313	15	1	1	NUM
ijpds-4231	313	16	with	with	ADP
ijpds-4231	313	17	good	good	ADJ
ijpds-4231	313	18	purity	purity	NOUN
ijpds-4231	313	19	.	.	PUNCT
ijpds-4231	314	1	this	this	DET
ijpds-4231	314	2	work	work	NOUN
ijpds-4231	314	3	avoids	avoid	VERB
ijpds-4231	314	4	the	the	DET
ijpds-4231	314	5	tedious	tedious	ADJ
ijpds-4231	314	6	and	and	CCONJ
ijpds-4231	314	7	timeconsuming	timeconsuming	ADJ
ijpds-4231	314	8	column	column	NOUN
ijpds-4231	314	9	chromatographic	chromatographic	ADJ
ijpds-4231	314	10	purification	purification	NOUN
ijpds-4231	314	11	method	method	NOUN
ijpds-4231	314	12	&	&	CCONJ
ijpds-4231	314	13	the	the	DET
ijpds-4231	314	14	solvent	solvent	NOUN
ijpds-4231	314	15	recrystallization	recrystallization	NOUN
ijpds-4231	314	16	techniques	technique	NOUN
ijpds-4231	314	17	to	to	PART
ijpds-4231	314	18	get	get	VERB
ijpds-4231	314	19	pure	pure	ADJ
ijpds-4231	314	20	free	free	ADJ
ijpds-4231	314	21	base	base	NOUN
ijpds-4231	314	22	,	,	PUNCT
ijpds-4231	314	23	instead	instead	ADV
ijpds-4231	314	24	had	have	AUX
ijpds-4231	314	25	incorporated	incorporate	VERB
ijpds-4231	314	26	a	a	DET
ijpds-4231	314	27	simple	simple	ADJ
ijpds-4231	314	28	workup	workup	ADJ
ijpds-4231	314	29	techniques	technique	NOUN
ijpds-4231	314	30	to	to	PART
ijpds-4231	314	31	get	get	VERB
ijpds-4231	314	32	the	the	DET
ijpds-4231	314	33	r	r	NOUN
ijpds-4231	314	34	-	-	PUNCT
ijpds-4231	314	35	rasagiline	rasagiline	NOUN
ijpds-4231	314	36	base	base	NOUN
ijpds-4231	314	37	with	with	ADP
ijpds-4231	314	38	high	high	ADJ
ijpds-4231	314	39	purity	purity	NOUN
ijpds-4231	314	40	.	.	PUNCT
ijpds-4231	315	1	[	[	X
ijpds-4231	315	2	60	60	NUM
ijpds-4231	315	3	]	]	PUNCT
ijpds-4231	315	4	.	.	PUNCT
ijpds-4231	316	1	gade	gade	PROPN
ijpds-4231	316	2	sr	sr	PROPN
ijpds-4231	316	3	,	,	PUNCT
ijpds-4231	316	4	et	et	PROPN
ijpds-4231	316	5	al	al	PROPN
ijpds-4231	316	6	.	.	PROPN
ijpds-4231	316	7	,	,	PUNCT
ijpds-4231	316	8	in	in	ADP
ijpds-4231	316	9	2013	2013	NUM
ijpds-4231	316	10	,	,	PUNCT
ijpds-4231	316	11	had	have	AUX
ijpds-4231	316	12	demonstrated	demonstrate	VERB
ijpds-4231	316	13	the	the	DET
ijpds-4231	316	14	treatment	treatment	NOUN
ijpds-4231	316	15	of	of	ADP
ijpds-4231	316	16	rasagiline	rasagiline	NOUN
ijpds-4231	316	17	base	base	NOUN
ijpds-4231	316	18	with	with	ADP
ijpds-4231	316	19	l-(+)-tartaric	l-(+)-tartaric	ADJ
ijpds-4231	316	20	acid	acid	NOUN
ijpds-4231	316	21	in	in	ADP
ijpds-4231	316	22	methyl	methyl	NOUN
ijpds-4231	316	23	alcohol	alcohol	NOUN
ijpds-4231	316	24	to	to	PART
ijpds-4231	316	25	isolate	isolate	VERB
ijpds-4231	316	26	rasagiline	rasagiline	PROPN
ijpds-4231	316	27	hemi	hemi	NOUN
ijpds-4231	316	28	-	-	PUNCT
ijpds-4231	316	29	tartarate	tartarate	NOUN
ijpds-4231	316	30	(	(	PUNCT
ijpds-4231	316	31	yield	yield	NOUN
ijpds-4231	316	32	:	:	PUNCT
ijpds-4231	316	33	70	70	NUM
ijpds-4231	316	34	-	-	SYM
ijpds-4231	316	35	75	75	NUM
ijpds-4231	316	36	%	%	NOUN
ijpds-4231	316	37	,	,	PUNCT
ijpds-4231	316	38	purity	purity	NOUN
ijpds-4231	316	39	:	:	PUNCT
ijpds-4231	316	40	99.91	99.91	NUM
ijpds-4231	316	41	-	-	SYM
ijpds-4231	316	42	99.98	99.98	NUM
ijpds-4231	316	43	%	%	NOUN
ijpds-4231	316	44	by	by	ADP
ijpds-4231	316	45	hplc	hplc	NOUN
ijpds-4231	316	46	)	)	PUNCT
ijpds-4231	317	1	[	[	X
ijpds-4231	317	2	61	61	NUM
ijpds-4231	317	3	]	]	PUNCT
ijpds-4231	317	4	.	.	PUNCT
ijpds-4231	318	1	sanjay	sanjay	PROPN
ijpds-4231	318	2	s	s	PART
ijpds-4231	319	1	s	s	NOUN
ijpds-4231	319	2	patents	patent	NOUN
ijpds-4231	319	3	disclosed	disclose	VERB
ijpds-4231	319	4	synthetic	synthetic	ADJ
ijpds-4231	319	5	overview	overview	NOUN
ijpds-4231	319	6	of	of	ADP
ijpds-4231	319	7	rasagiline	rasagiline	ADJ
ijpds-4231	319	8	vol	vol	NOUN
ijpds-4231	319	9	2	2	NUM
ijpds-4231	319	10	|	|	ADV
ijpds-4231	319	11	issue	issue	VERB
ijpds-4231	319	12	4	4	NUM
ijpds-4231	319	13	|	|	ADV
ijpds-4231	319	14	oct	oct	PROPN
ijpds-4231	319	15	–	–	PUNCT
ijpds-4231	319	16	dec	dec	PROPN
ijpds-4231	319	17	2023	2023	NUM
ijpds-4231	319	18	indian	indian	PROPN
ijpds-4231	319	19	j	j	PROPN
ijpds-4231	319	20	pharm	pharm	PROPN
ijpds-4231	319	21	drug	drug	PROPN
ijpds-4231	319	22	studies	study	NOUN
ijpds-4231	319	23	|	|	ADV
ijpds-4231	319	24	141	141	NUM
ijpds-4231	319	25	sun	sun	PROPN
ijpds-4231	319	26	y	y	PROPN
ijpds-4231	319	27	,	,	PUNCT
ijpds-4231	319	28	et	et	PROPN
ijpds-4231	319	29	al	al	PROPN
ijpds-4231	319	30	.	.	PROPN
ijpds-4231	319	31	,	,	PUNCT
ijpds-4231	319	32	in	in	ADP
ijpds-4231	319	33	2014	2014	NUM
ijpds-4231	319	34	,	,	PUNCT
ijpds-4231	319	35	had	have	AUX
ijpds-4231	319	36	demonstrated	demonstrate	VERB
ijpds-4231	319	37	a	a	DET
ijpds-4231	319	38	one	one	NUM
ijpds-4231	319	39	-	-	PUNCT
ijpds-4231	319	40	pot	pot	NOUN
ijpds-4231	319	41	synthetic	synthetic	ADJ
ijpds-4231	319	42	process	process	NOUN
ijpds-4231	319	43	to	to	PART
ijpds-4231	319	44	condense	condense	VERB
ijpds-4231	319	45	r-(-)-isomer	r-(-)-isomer	PROPN
ijpds-4231	319	46	of	of	ADP
ijpds-4231	319	47	2	2	NUM
ijpds-4231	319	48	in	in	ADP
ijpds-4231	319	49	acetonitrile	acetonitrile	NOUN
ijpds-4231	319	50	or	or	CCONJ
ijpds-4231	319	51	n	n	CCONJ
ijpds-4231	319	52	,	,	PUNCT
ijpds-4231	319	53	n	n	CCONJ
ijpds-4231	319	54	-	-	PUNCT
ijpds-4231	319	55	dimethyl	dimethyl	NOUN
ijpds-4231	319	56	formamide	formamide	ADV
ijpds-4231	319	57	with	with	ADP
ijpds-4231	319	58	propargyl	propargyl	NOUN
ijpds-4231	319	59	-	-	PUNCT
ijpds-4231	319	60	ptoluenesulfonate	ptoluenesulfonate	VERB
ijpds-4231	319	61	43	43	NUM
ijpds-4231	319	62	or	or	CCONJ
ijpds-4231	319	63	44	44	NUM
ijpds-4231	319	64	in	in	ADP
ijpds-4231	319	65	the	the	DET
ijpds-4231	319	66	presence	presence	NOUN
ijpds-4231	319	67	of	of	ADP
ijpds-4231	319	68	sodium	sodium	NOUN
ijpds-4231	319	69	carbonate	carbonate	NOUN
ijpds-4231	319	70	or	or	CCONJ
ijpds-4231	319	71	potassium	potassium	NOUN
ijpds-4231	319	72	carbonate	carbonate	NOUN
ijpds-4231	319	73	or	or	CCONJ
ijpds-4231	319	74	triethylamine	triethylamine	NOUN
ijpds-4231	319	75	to	to	PART
ijpds-4231	319	76	form	form	VERB
ijpds-4231	319	77	an	an	DET
ijpds-4231	319	78	intermediate	intermediate	NOUN
ijpds-4231	319	79	.	.	PUNCT
ijpds-4231	320	1	it	it	PRON
ijpds-4231	320	2	was	be	AUX
ijpds-4231	320	3	not	not	PART
ijpds-4231	320	4	isolated	isolate	VERB
ijpds-4231	320	5	,	,	PUNCT
ijpds-4231	320	6	but	but	CCONJ
ijpds-4231	320	7	immediately	immediately	ADV
ijpds-4231	320	8	treated	treat	VERB
ijpds-4231	320	9	with	with	ADP
ijpds-4231	320	10	methanesulfonic	methanesulfonic	ADJ
ijpds-4231	320	11	acid	acid	NOUN
ijpds-4231	320	12	to	to	PART
ijpds-4231	320	13	isolate	isolate	VERB
ijpds-4231	320	14	the	the	DET
ijpds-4231	320	15	crude	crude	NOUN
ijpds-4231	320	16	solid	solid	ADJ
ijpds-4231	320	17	.	.	PUNCT
ijpds-4231	321	1	it	it	PRON
ijpds-4231	321	2	was	be	AUX
ijpds-4231	321	3	recrystallized	recrystallize	VERB
ijpds-4231	321	4	in	in	ADP
ijpds-4231	321	5	isopropyl	isopropyl	NOUN
ijpds-4231	321	6	alcohol	alcohol	NOUN
ijpds-4231	321	7	to	to	PART
ijpds-4231	321	8	isolate	isolate	VERB
ijpds-4231	321	9	1	1	NUM
ijpds-4231	321	10	with	with	ADP
ijpds-4231	321	11	a	a	DET
ijpds-4231	321	12	melting	melting	NOUN
ijpds-4231	321	13	point	point	NOUN
ijpds-4231	321	14	of	of	ADP
ijpds-4231	321	15	156	156	NUM
ijpds-4231	321	16	-	-	PUNCT
ijpds-4231	321	17	157oc	157oc	NOUN
ijpds-4231	321	18	(	(	PUNCT
ijpds-4231	321	19	yield	yield	NOUN
ijpds-4231	321	20	:	:	PUNCT
ijpds-4231	321	21	approximately	approximately	ADV
ijpds-4231	321	22	40	40	NUM
ijpds-4231	321	23	-	-	SYM
ijpds-4231	321	24	50	50	NUM
ijpds-4231	321	25	%	%	NOUN
ijpds-4231	321	26	,	,	PUNCT
ijpds-4231	321	27	purity	purity	NOUN
ijpds-4231	321	28	:	:	PUNCT
ijpds-4231	321	29	more	more	ADJ
ijpds-4231	321	30	than	than	ADP
ijpds-4231	321	31	99.5	99.5	NUM
ijpds-4231	321	32	%	%	NOUN
ijpds-4231	321	33	by	by	ADP
ijpds-4231	321	34	hplc	hplc	PROPN
ijpds-4231	321	35	)	)	PUNCT
ijpds-4231	321	36	.	.	PUNCT
ijpds-4231	322	1	the	the	DET
ijpds-4231	322	2	work	work	NOUN
ijpds-4231	322	3	was	be	AUX
ijpds-4231	322	4	extended	extend	VERB
ijpds-4231	322	5	further	far	ADV
ijpds-4231	322	6	to	to	PART
ijpds-4231	322	7	isolate	isolate	VERB
ijpds-4231	322	8	a	a	DET
ijpds-4231	322	9	few	few	ADJ
ijpds-4231	322	10	impurities	impurity	NOUN
ijpds-4231	322	11	like	like	ADP
ijpds-4231	322	12	prop2	prop2	NOUN
ijpds-4231	322	13	-	-	PUNCT
ijpds-4231	322	14	yn-1	yn-1	NOUN
ijpds-4231	322	15	-	-	NOUN
ijpds-4231	322	16	yl	yl	NOUN
ijpds-4231	322	17	(	(	PUNCT
ijpds-4231	322	18	1r)-2,3	1r)-2,3	ADJ
ijpds-4231	322	19	-	-	PUNCT
ijpds-4231	322	20	dihydro-1h	dihydro-1h	NOUN
ijpds-4231	322	21	-	-	PUNCT
ijpds-4231	322	22	inden-1	inden-1	NOUN
ijpds-4231	322	23	-	-	PUNCT
ijpds-4231	322	24	ylcarbamate	ylcarbamate	ADJ
ijpds-4231	322	25	45	45	NUM
ijpds-4231	322	26	and	and	CCONJ
ijpds-4231	322	27	prop-2	prop-2	NUM
ijpds-4231	322	28	-	-	PUNCT
ijpds-4231	322	29	yn-1	yn-1	PRON
ijpds-4231	322	30	-	-	PUNCT
ijpds-4231	322	31	yl-(1r)-2,3	yl-(1r)-2,3	ADJ
ijpds-4231	322	32	-	-	PUNCT
ijpds-4231	322	33	dihydro-1h	dihydro-1h	NOUN
ijpds-4231	322	34	-	-	PUNCT
ijpds-4231	322	35	inden-1	inden-1	NOUN
ijpds-4231	322	36	-	-	PUNCT
ijpds-4231	322	37	yl-(prop2	yl-(prop2	NOUN
ijpds-4231	322	38	-	-	PUNCT
ijpds-4231	322	39	yn-1	yn-1	NOUN
ijpds-4231	322	40	-	-	NOUN
ijpds-4231	322	41	yl)carbamate	yl)carbamate	NOUN
ijpds-4231	322	42	46	46	NUM
ijpds-4231	322	43	from	from	ADP
ijpds-4231	322	44	the	the	DET
ijpds-4231	322	45	filtrate	filtrate	NOUN
ijpds-4231	322	46	by	by	ADP
ijpds-4231	322	47	the	the	DET
ijpds-4231	322	48	column	column	NOUN
ijpds-4231	322	49	chromatography	chromatography	NOUN
ijpds-4231	322	50	technique	technique	NOUN
ijpds-4231	322	51	[	[	X
ijpds-4231	322	52	62	62	NUM
ijpds-4231	322	53	]	]	PUNCT
ijpds-4231	322	54	.	.	PUNCT
ijpds-4231	323	1	sun	sun	PROPN
ijpds-4231	323	2	y	y	PROPN
ijpds-4231	323	3	,	,	PUNCT
ijpds-4231	323	4	et	et	PROPN
ijpds-4231	323	5	al	al	PROPN
ijpds-4231	323	6	.	.	PROPN
ijpds-4231	323	7	,	,	PUNCT
ijpds-4231	323	8	in	in	ADP
ijpds-4231	323	9	2014	2014	NUM
ijpds-4231	323	10	,	,	PUNCT
ijpds-4231	323	11	had	have	AUX
ijpds-4231	323	12	illustrated	illustrate	VERB
ijpds-4231	323	13	the	the	DET
ijpds-4231	323	14	isolation	isolation	NOUN
ijpds-4231	323	15	and	and	CCONJ
ijpds-4231	323	16	analysis	analysis	NOUN
ijpds-4231	323	17	methods	method	NOUN
ijpds-4231	323	18	of	of	ADP
ijpds-4231	323	19	45	45	NUM
ijpds-4231	323	20	,	,	PUNCT
ijpds-4231	323	21	46	46	NUM
ijpds-4231	323	22	and	and	CCONJ
ijpds-4231	323	23	r	r	NOUN
ijpds-4231	323	24	-	-	PUNCT
ijpds-4231	323	25	mesylate	mesylate	NOUN
ijpds-4231	323	26	of	of	ADP
ijpds-4231	323	27	4	4	NUM
ijpds-4231	323	28	.	.	PUNCT
ijpds-4231	324	1	the	the	DET
ijpds-4231	324	2	lcms	lcms	PROPN
ijpds-4231	324	3	data	datum	NOUN
ijpds-4231	324	4	of	of	ADP
ijpds-4231	324	5	isolated	isolated	ADJ
ijpds-4231	324	6	impurities	impurity	NOUN
ijpds-4231	324	7	are	be	AUX
ijpds-4231	324	8	[	[	X
ijpds-4231	324	9	m+h]+	m+h]+	PROPN
ijpds-4231	324	10	216.1	216.1	NUM
ijpds-4231	324	11	for	for	ADP
ijpds-4231	324	12	45	45	NUM
ijpds-4231	324	13	,	,	PUNCT
ijpds-4231	324	14	[	[	X
ijpds-4231	324	15	m+h]+	m+h]+	X
ijpds-4231	324	16	254.1	254.1	NUM
ijpds-4231	324	17	for	for	ADP
ijpds-4231	324	18	46	46	NUM
ijpds-4231	324	19	and	and	CCONJ
ijpds-4231	324	20	[	[	X
ijpds-4231	324	21	m+h]+	m+h]+	PROPN
ijpds-4231	324	22	210.1	210.1	NUM
ijpds-4231	324	23	for	for	ADP
ijpds-4231	324	24	mesylate	mesylate	NOUN
ijpds-4231	324	25	of	of	ADP
ijpds-4231	324	26	4	4	NUM
ijpds-4231	324	27	[	[	SYM
ijpds-4231	324	28	63	63	NUM
ijpds-4231	324	29	]	]	PUNCT
ijpds-4231	324	30	.	.	PUNCT
ijpds-4231	325	1	prudic	prudic	PROPN
ijpds-4231	325	2	d	d	PROPN
ijpds-4231	325	3	,	,	PUNCT
ijpds-4231	325	4	et	et	PROPN
ijpds-4231	325	5	al	al	PROPN
ijpds-4231	325	6	.	.	PROPN
ijpds-4231	325	7	,	,	PUNCT
ijpds-4231	325	8	in	in	ADP
ijpds-4231	325	9	2015	2015	NUM
ijpds-4231	325	10	&	&	CCONJ
ijpds-4231	325	11	2016	2016	NUM
ijpds-4231	325	12	,	,	PUNCT
ijpds-4231	325	13	had	have	AUX
ijpds-4231	325	14	reported	report	VERB
ijpds-4231	325	15	a	a	DET
ijpds-4231	325	16	process	process	NOUN
ijpds-4231	325	17	for	for	ADP
ijpds-4231	325	18	the	the	DET
ijpds-4231	325	19	preparation	preparation	NOUN
ijpds-4231	325	20	of	of	ADP
ijpds-4231	325	21	optically	optically	ADV
ijpds-4231	325	22	pure	pure	ADJ
ijpds-4231	325	23	r	r	NOUN
ijpds-4231	325	24	-	-	PUNCT
ijpds-4231	325	25	isomer	isomer	NOUN
ijpds-4231	325	26	of	of	ADP
ijpds-4231	325	27	2	2	NUM
ijpds-4231	325	28	by	by	ADP
ijpds-4231	325	29	a	a	DET
ijpds-4231	325	30	diastereomeric	diastereomeric	ADJ
ijpds-4231	325	31	resolution	resolution	NOUN
ijpds-4231	325	32	of	of	ADP
ijpds-4231	325	33	racemic	racemic	ADJ
ijpds-4231	325	34	2	2	NUM
ijpds-4231	325	35	using	use	VERB
ijpds-4231	325	36	n	n	CCONJ
ijpds-4231	325	37	-	-	PUNCT
ijpds-4231	325	38	acetyl	acetyl	NOUN
ijpds-4231	325	39	-	-	PUNCT
ijpds-4231	325	40	lglutamic	lglutamic	ADJ
ijpds-4231	325	41	acid	acid	NOUN
ijpds-4231	325	42	47	47	NUM
ijpds-4231	325	43	as	as	ADP
ijpds-4231	325	44	an	an	DET
ijpds-4231	325	45	effective	effective	ADJ
ijpds-4231	325	46	resolving	resolving	NOUN
ijpds-4231	325	47	agent	agent	NOUN
ijpds-4231	325	48	.	.	PUNCT
ijpds-4231	326	1	the	the	DET
ijpds-4231	326	2	formation	formation	NOUN
ijpds-4231	326	3	of	of	ADP
ijpds-4231	326	4	diastereomeric	diastereomeric	ADJ
ijpds-4231	326	5	salts	salt	NOUN
ijpds-4231	326	6	of	of	ADP
ijpds-4231	326	7	r	r	NOUN
ijpds-4231	326	8	-	-	PUNCT
ijpds-4231	326	9	isomer	isomer	NOUN
ijpds-4231	326	10	of	of	ADP
ijpds-4231	326	11	2	2	NUM
ijpds-4231	326	12	with	with	ADP
ijpds-4231	326	13	47	47	NUM
ijpds-4231	326	14	and	and	CCONJ
ijpds-4231	326	15	their	their	PRON
ijpds-4231	326	16	use	use	NOUN
ijpds-4231	326	17	in	in	ADP
ijpds-4231	326	18	the	the	DET
ijpds-4231	326	19	synthesis	synthesis	NOUN
ijpds-4231	326	20	of	of	ADP
ijpds-4231	326	21	optically	optically	ADV
ijpds-4231	326	22	enriched	enrich	VERB
ijpds-4231	326	23	rasagiline	rasagiline	NOUN
ijpds-4231	326	24	base	base	NOUN
ijpds-4231	326	25	was	be	AUX
ijpds-4231	326	26	also	also	ADV
ijpds-4231	326	27	reported	report	VERB
ijpds-4231	326	28	.	.	PUNCT
ijpds-4231	327	1	rasagiline	rasagiline	PROPN
ijpds-4231	327	2	base	base	PROPN
ijpds-4231	327	3	was	be	AUX
ijpds-4231	327	4	treated	treat	VERB
ijpds-4231	327	5	with	with	ADP
ijpds-4231	327	6	methanesulfonic	methanesulfonic	ADJ
ijpds-4231	327	7	acid	acid	NOUN
ijpds-4231	327	8	in	in	ADP
ijpds-4231	327	9	isopropyl	isopropyl	NOUN
ijpds-4231	327	10	alcohol	alcohol	NOUN
ijpds-4231	327	11	to	to	PART
ijpds-4231	327	12	obtain	obtain	VERB
ijpds-4231	327	13	1	1	NUM
ijpds-4231	327	14	(	(	PUNCT
ijpds-4231	327	15	yield	yield	NOUN
ijpds-4231	327	16	:	:	PUNCT
ijpds-4231	327	17	76.6	76.6	NUM
ijpds-4231	327	18	%	%	NOUN
ijpds-4231	327	19	,	,	PUNCT
ijpds-4231	327	20	purity	purity	NOUN
ijpds-4231	327	21	:	:	PUNCT
ijpds-4231	327	22	100	100	NUM
ijpds-4231	327	23	%	%	NOUN
ijpds-4231	327	24	by	by	ADP
ijpds-4231	327	25	hplc	hplc	NOUN
ijpds-4231	327	26	)	)	PUNCT
ijpds-4231	327	27	.	.	PUNCT
ijpds-4231	328	1	the	the	DET
ijpds-4231	328	2	reaction	reaction	NOUN
ijpds-4231	328	3	of	of	ADP
ijpds-4231	328	4	9	9	NUM
ijpds-4231	328	5	with	with	ADP
ijpds-4231	328	6	hydroxylamine	hydroxylamine	ADJ
ijpds-4231	328	7	hydrochloride	hydrochloride	NOUN
ijpds-4231	328	8	was	be	AUX
ijpds-4231	328	9	carried	carry	VERB
ijpds-4231	328	10	out	out	ADP
ijpds-4231	328	11	in	in	ADP
ijpds-4231	328	12	ethyl	ethyl	PROPN
ijpds-4231	328	13	alcohol	alcohol	NOUN
ijpds-4231	328	14	to	to	PART
ijpds-4231	328	15	get	get	VERB
ijpds-4231	328	16	15	15	NUM
ijpds-4231	328	17	(	(	PUNCT
ijpds-4231	328	18	yield	yield	NOUN
ijpds-4231	328	19	:	:	PUNCT
ijpds-4231	328	20	91.6	91.6	NUM
ijpds-4231	328	21	%	%	NOUN
ijpds-4231	328	22	)	)	PUNCT
ijpds-4231	328	23	.	.	PUNCT
ijpds-4231	329	1	it	it	PRON
ijpds-4231	329	2	was	be	AUX
ijpds-4231	329	3	reduced	reduce	VERB
ijpds-4231	329	4	by	by	ADP
ijpds-4231	329	5	raney	raney	NOUN
ijpds-4231	329	6	-	-	PUNCT
ijpds-4231	329	7	nickel	nickel	NOUN
ijpds-4231	329	8	in	in	ADP
ijpds-4231	329	9	the	the	DET
ijpds-4231	329	10	presence	presence	NOUN
ijpds-4231	329	11	of	of	ADP
ijpds-4231	329	12	ammonia	ammonia	NOUN
ijpds-4231	329	13	enriched	enrich	VERB
ijpds-4231	329	14	methyl	methyl	NOUN
ijpds-4231	329	15	alcohol	alcohol	NOUN
ijpds-4231	329	16	to	to	PART
ijpds-4231	329	17	isolate	isolate	VERB
ijpds-4231	329	18	racemic	racemic	ADJ
ijpds-4231	329	19	2	2	NUM
ijpds-4231	329	20	(	(	PUNCT
ijpds-4231	329	21	yield	yield	NOUN
ijpds-4231	329	22	:	:	PUNCT
ijpds-4231	329	23	100	100	NUM
ijpds-4231	329	24	%	%	NOUN
ijpds-4231	329	25	)	)	PUNCT
ijpds-4231	330	1	[	[	X
ijpds-4231	330	2	64	64	NUM
ijpds-4231	330	3	,	,	PUNCT
ijpds-4231	330	4	65	65	NUM
ijpds-4231	330	5	]	]	PUNCT
ijpds-4231	330	6	.	.	PUNCT
ijpds-4231	331	1	frenkel	frenkel	PROPN
ijpds-4231	331	2	a	a	PRON
ijpds-4231	331	3	,	,	PUNCT
ijpds-4231	331	4	et	et	PROPN
ijpds-4231	331	5	al	al	PROPN
ijpds-4231	331	6	.	.	PROPN
ijpds-4231	331	7	,	,	PUNCT
ijpds-4231	331	8	in	in	ADP
ijpds-4231	331	9	2015	2015	NUM
ijpds-4231	331	10	,	,	PUNCT
ijpds-4231	331	11	had	have	AUX
ijpds-4231	331	12	reported	report	VERB
ijpds-4231	331	13	the	the	DET
ijpds-4231	331	14	synthesis	synthesis	NOUN
ijpds-4231	331	15	of	of	ADP
ijpds-4231	331	16	19	19	NUM
ijpds-4231	331	17	from	from	ADP
ijpds-4231	331	18	n-(2,3	n-(2,3	ADJ
ijpds-4231	331	19	-	-	PUNCT
ijpds-4231	331	20	dihydro-1h	dihydro-1h	NOUN
ijpds-4231	331	21	-	-	PUNCT
ijpds-4231	331	22	inden-1	inden-1	NOUN
ijpds-4231	331	23	-	-	PUNCT
ijpds-4231	331	24	yl)acetamide	yl)acetamide	NOUN
ijpds-4231	331	25	48	48	NUM
ijpds-4231	331	26	.	.	PUNCT
ijpds-4231	332	1	impurity	impurity	NOUN
ijpds-4231	332	2	19	19	NUM
ijpds-4231	332	3	was	be	AUX
ijpds-4231	332	4	formed	form	VERB
ijpds-4231	332	5	during	during	ADP
ijpds-4231	332	6	the	the	DET
ijpds-4231	332	7	production	production	NOUN
ijpds-4231	332	8	of	of	ADP
ijpds-4231	332	9	1	1	NUM
ijpds-4231	332	10	under	under	ADP
ijpds-4231	332	11	certain	certain	ADJ
ijpds-4231	332	12	specific	specific	ADJ
ijpds-4231	332	13	conditions	condition	NOUN
ijpds-4231	332	14	.	.	PUNCT
ijpds-4231	333	1	the	the	DET
ijpds-4231	333	2	work	work	NOUN
ijpds-4231	333	3	was	be	AUX
ijpds-4231	333	4	extended	extend	VERB
ijpds-4231	333	5	further	far	ADV
ijpds-4231	333	6	to	to	PART
ijpds-4231	333	7	contribute	contribute	VERB
ijpds-4231	333	8	a	a	DET
ijpds-4231	333	9	commercial	commercial	ADJ
ijpds-4231	333	10	process	process	NOUN
ijpds-4231	333	11	to	to	PART
ijpds-4231	333	12	get	get	VERB
ijpds-4231	333	13	1	1	NUM
ijpds-4231	333	14	with	with	ADP
ijpds-4231	333	15	very	very	ADV
ijpds-4231	333	16	low	low	ADJ
ijpds-4231	333	17	content	content	NOUN
ijpds-4231	333	18	of	of	ADP
ijpds-4231	333	19	19	19	NUM
ijpds-4231	333	20	.	.	PUNCT
ijpds-4231	334	1	racemic	racemic	ADJ
ijpds-4231	334	2	2	2	NUM
ijpds-4231	334	3	was	be	AUX
ijpds-4231	334	4	treated	treat	VERB
ijpds-4231	334	5	with	with	ADP
ijpds-4231	334	6	8	8	NUM
ijpds-4231	334	7	in	in	ADP
ijpds-4231	334	8	the	the	DET
ijpds-4231	334	9	presence	presence	NOUN
ijpds-4231	334	10	of	of	ADP
ijpds-4231	334	11	sodium	sodium	NOUN
ijpds-4231	334	12	hydroxide	hydroxide	NOUN
ijpds-4231	334	13	solution	solution	NOUN
ijpds-4231	334	14	to	to	PART
ijpds-4231	334	15	isolate	isolate	VERB
ijpds-4231	334	16	racemic	racemic	ADJ
ijpds-4231	334	17	rasagiline	rasagiline	NOUN
ijpds-4231	334	18	base	base	NOUN
ijpds-4231	334	19	.	.	PUNCT
ijpds-4231	335	1	it	it	PRON
ijpds-4231	335	2	was	be	AUX
ijpds-4231	335	3	treated	treat	VERB
ijpds-4231	335	4	with	with	ADP
ijpds-4231	335	5	l	l	ADJ
ijpds-4231	335	6	-	-	ADJ
ijpds-4231	335	7	tartaric	tartaric	ADJ
ijpds-4231	335	8	acid	acid	NOUN
ijpds-4231	335	9	in	in	ADP
ijpds-4231	335	10	isopropyl	isopropyl	NOUN
ijpds-4231	335	11	alcohol	alcohol	NOUN
ijpds-4231	335	12	to	to	PART
ijpds-4231	335	13	isolate	isolate	VERB
ijpds-4231	335	14	r	r	NOUN
ijpds-4231	335	15	-	-	PUNCT
ijpds-4231	335	16	rasagiline	rasagiline	NOUN
ijpds-4231	335	17	tartarate	tartarate	NOUN
ijpds-4231	335	18	,	,	PUNCT
ijpds-4231	335	19	it	it	PRON
ijpds-4231	335	20	was	be	AUX
ijpds-4231	335	21	then	then	ADV
ijpds-4231	335	22	de	de	ADJ
ijpds-4231	335	23	-	-	VERB
ijpds-4231	335	24	salted	salt	VERB
ijpds-4231	335	25	and	and	CCONJ
ijpds-4231	335	26	treated	treat	VERB
ijpds-4231	335	27	further	far	ADV
ijpds-4231	335	28	with	with	ADP
ijpds-4231	335	29	methane	methane	NOUN
ijpds-4231	335	30	sulfonic	sulfonic	ADJ
ijpds-4231	335	31	acid	acid	NOUN
ijpds-4231	335	32	to	to	PART
ijpds-4231	335	33	isolate	isolate	VERB
ijpds-4231	335	34	1	1	NUM
ijpds-4231	335	35	(	(	PUNCT
ijpds-4231	335	36	with	with	ADP
ijpds-4231	335	37	around	around	ADV
ijpds-4231	335	38	0.01	0.01	NUM
ijpds-4231	335	39	-	-	PUNCT
ijpds-4231	335	40	0.02	0.02	NUM
ijpds-4231	335	41	%	%	NOUN
ijpds-4231	335	42	of	of	ADP
ijpds-4231	335	43	19	19	NUM
ijpds-4231	335	44	content	content	NOUN
ijpds-4231	335	45	)	)	PUNCT
ijpds-4231	336	1	[	[	X
ijpds-4231	336	2	66	66	NUM
ijpds-4231	336	3	]	]	PUNCT
ijpds-4231	336	4	.	.	PUNCT
ijpds-4231	337	1	chen	chen	PROPN
ijpds-4231	337	2	j	j	PROPN
ijpds-4231	337	3	,	,	PUNCT
ijpds-4231	337	4	et	et	PROPN
ijpds-4231	337	5	al	al	PROPN
ijpds-4231	337	6	.	.	PROPN
ijpds-4231	337	7	,	,	PUNCT
ijpds-4231	337	8	in	in	ADP
ijpds-4231	337	9	2019	2019	NUM
ijpds-4231	337	10	,	,	PUNCT
ijpds-4231	337	11	had	have	AUX
ijpds-4231	337	12	demonstrated	demonstrate	VERB
ijpds-4231	337	13	the	the	DET
ijpds-4231	337	14	reaction	reaction	NOUN
ijpds-4231	337	15	of	of	ADP
ijpds-4231	337	16	r-(-)-isomer	r-(-)-isomer	PROPN
ijpds-4231	337	17	of	of	ADP
ijpds-4231	337	18	2	2	NUM
ijpds-4231	337	19	with	with	ADP
ijpds-4231	337	20	propynoic	propynoic	ADJ
ijpds-4231	337	21	acid	acid	NOUN
ijpds-4231	337	22	49	49	NUM
ijpds-4231	337	23	in	in	ADP
ijpds-4231	337	24	dichloromethane	dichloromethane	NOUN
ijpds-4231	337	25	under	under	ADP
ijpds-4231	337	26	the	the	DET
ijpds-4231	337	27	presence	presence	NOUN
ijpds-4231	337	28	of	of	ADP
ijpds-4231	337	29	suitable	suitable	ADJ
ijpds-4231	337	30	acid	acid	NOUN
ijpds-4231	337	31	amine	amine	ADJ
ijpds-4231	337	32	coupling	couple	VERB
ijpds-4231	337	33	agents	agent	NOUN
ijpds-4231	337	34	like	like	ADP
ijpds-4231	337	35	dicyclohexylcarbazone/	dicyclohexylcarbazone/	NUM
ijpds-4231	337	36	4dimethylaminopyridine	4dimethylaminopyridine	NUM
ijpds-4231	337	37	to	to	PART
ijpds-4231	337	38	get	get	VERB
ijpds-4231	337	39	n-[(1r)-2,3	n-[(1r)-2,3	NOUN
ijpds-4231	337	40	-	-	PUNCT
ijpds-4231	337	41	dihydro-1hinden-1	dihydro-1hinden-1	NOUN
ijpds-4231	337	42	-	-	PUNCT
ijpds-4231	337	43	yl]but-3	yl]but-3	NOUN
ijpds-4231	337	44	-	-	PUNCT
ijpds-4231	337	45	ynamide	ynamide	NOUN
ijpds-4231	337	46	50	50	NUM
ijpds-4231	337	47	(	(	PUNCT
ijpds-4231	337	48	yield	yield	NOUN
ijpds-4231	337	49	:	:	PUNCT
ijpds-4231	337	50	97.7	97.7	NUM
ijpds-4231	337	51	%	%	NOUN
ijpds-4231	337	52	,	,	PUNCT
ijpds-4231	337	53	purity	purity	NOUN
ijpds-4231	337	54	:	:	PUNCT
ijpds-4231	337	55	96.76	96.76	NUM
ijpds-4231	337	56	%	%	NOUN
ijpds-4231	337	57	by	by	ADP
ijpds-4231	337	58	hplc	hplc	NOUN
ijpds-4231	337	59	)	)	PUNCT
ijpds-4231	337	60	.	.	PUNCT
ijpds-4231	338	1	similarly	similarly	ADV
ijpds-4231	338	2	,	,	PUNCT
ijpds-4231	338	3	the	the	DET
ijpds-4231	338	4	use	use	NOUN
ijpds-4231	338	5	of	of	ADP
ijpds-4231	338	6	1hydroxybenzotriazole/	1hydroxybenzotriazole/	NUM
ijpds-4231	338	7	1-(3	1-(3	NUM
ijpds-4231	338	8	-	-	PUNCT
ijpds-4231	338	9	dimethylaminopropyl)-3ethylcarbodiimide	dimethylaminopropyl)-3ethylcarbodiimide	ADJ
ijpds-4231	338	10	hydrochloride	hydrochloride	NOUN
ijpds-4231	338	11	in	in	ADP
ijpds-4231	338	12	tetrahydrofuran	tetrahydrofuran	NOUN
ijpds-4231	338	13	gave	give	VERB
ijpds-4231	338	14	50	50	NUM
ijpds-4231	338	15	(	(	PUNCT
ijpds-4231	338	16	yield	yield	NOUN
ijpds-4231	338	17	:	:	PUNCT
ijpds-4231	338	18	95.2	95.2	NUM
ijpds-4231	338	19	%	%	NOUN
ijpds-4231	338	20	,	,	PUNCT
ijpds-4231	338	21	purity	purity	NOUN
ijpds-4231	338	22	:	:	PUNCT
ijpds-4231	338	23	96.59	96.59	NUM
ijpds-4231	338	24	%	%	NOUN
ijpds-4231	338	25	by	by	ADP
ijpds-4231	338	26	hplc	hplc	NOUN
ijpds-4231	338	27	)	)	PUNCT
ijpds-4231	338	28	.	.	PUNCT
ijpds-4231	339	1	the	the	DET
ijpds-4231	339	2	use	use	NOUN
ijpds-4231	339	3	of	of	ADP
ijpds-4231	339	4	(	(	PUNCT
ijpds-4231	339	5	azabenzotriazol-1	azabenzotriazol-1	NOUN
ijpds-4231	339	6	-	-	PUNCT
ijpds-4231	339	7	yl)-n	yl)-n	ADJ
ijpds-4231	339	8	,	,	PUNCT
ijpds-4231	339	9	n	n	CCONJ
ijpds-4231	339	10	,	,	PUNCT
ijpds-4231	339	11	n',n'-tetramethyluroniumhexafluorophosphate/	n',n'-tetramethyluroniumhexafluorophosphate/	ADV
ijpds-4231	339	12	di	di	NOUN
ijpds-4231	339	13	-	-	NOUN
ijpds-4231	339	14	isopropylethylamine	isopropylethylamine	NOUN
ijpds-4231	339	15	in	in	ADP
ijpds-4231	339	16	2methyltetrahydrofuran	2methyltetrahydrofuran	NUM
ijpds-4231	339	17	had	have	AUX
ijpds-4231	339	18	resulted	result	VERB
ijpds-4231	339	19	in	in	ADP
ijpds-4231	339	20	the	the	DET
ijpds-4231	339	21	formation	formation	NOUN
ijpds-4231	339	22	of	of	ADP
ijpds-4231	339	23	50	50	NUM
ijpds-4231	339	24	(	(	PUNCT
ijpds-4231	339	25	yield	yield	NOUN
ijpds-4231	339	26	:	:	PUNCT
ijpds-4231	339	27	96.8	96.8	NUM
ijpds-4231	339	28	%	%	NOUN
ijpds-4231	339	29	,	,	PUNCT
ijpds-4231	339	30	purity	purity	NOUN
ijpds-4231	339	31	:	:	PUNCT
ijpds-4231	339	32	96.84	96.84	NUM
ijpds-4231	339	33	%	%	NOUN
ijpds-4231	339	34	by	by	ADP
ijpds-4231	339	35	hplc	hplc	NOUN
ijpds-4231	339	36	)	)	PUNCT
ijpds-4231	339	37	.	.	PUNCT
ijpds-4231	340	1	it	it	PRON
ijpds-4231	340	2	was	be	AUX
ijpds-4231	340	3	dissolved	dissolve	VERB
ijpds-4231	340	4	in	in	ADP
ijpds-4231	340	5	toluene	toluene	PROPN
ijpds-4231	340	6	/	/	SYM
ijpds-4231	340	7	xylene	xylene	NOUN
ijpds-4231	340	8	/	/	SYM
ijpds-4231	340	9	benzene	benzene	NOUN
ijpds-4231	340	10	and	and	CCONJ
ijpds-4231	340	11	treated	treat	VERB
ijpds-4231	340	12	with	with	ADP
ijpds-4231	340	13	diphenylsilane	diphenylsilane	NOUN
ijpds-4231	340	14	/	/	SYM
ijpds-4231	340	15	triphenylsilane	triphenylsilane	NOUN
ijpds-4231	340	16	/	/	SYM
ijpds-4231	340	17	diphenylmethylsilane	diphenylmethylsilane	NOUN
ijpds-4231	340	18	and	and	CCONJ
ijpds-4231	340	19	di	di	NOUN
ijpds-4231	340	20	-	-	ADJ
ijpds-4231	340	21	o	o	NOUN
ijpds-4231	340	22	-	-	ADJ
ijpds-4231	340	23	chlorophenylboronic	chlorophenylboronic	ADJ
ijpds-4231	340	24	acid/	acid/	NUM
ijpds-4231	340	25	bis	bis	ADJ
ijpds-4231	340	26	-	-	ADJ
ijpds-4231	340	27	fluorophenylboronic	fluorophenylboronic	ADJ
ijpds-4231	340	28	acid	acid	NOUN
ijpds-4231	340	29	to	to	PART
ijpds-4231	340	30	isolate	isolate	VERB
ijpds-4231	340	31	rasagiline	rasagiline	NOUN
ijpds-4231	340	32	base	base	NOUN
ijpds-4231	340	33	(	(	PUNCT
ijpds-4231	340	34	yield	yield	NOUN
ijpds-4231	340	35	:	:	PUNCT
ijpds-4231	340	36	59.4	59.4	NUM
ijpds-4231	340	37	-	-	SYM
ijpds-4231	340	38	60.7	60.7	NUM
ijpds-4231	340	39	%	%	NOUN
ijpds-4231	340	40	,	,	PUNCT
ijpds-4231	340	41	purity	purity	NOUN
ijpds-4231	340	42	:	:	PUNCT
ijpds-4231	340	43	99.72	99.72	NUM
ijpds-4231	340	44	-	-	SYM
ijpds-4231	340	45	99.77	99.77	NUM
ijpds-4231	340	46	%	%	NOUN
ijpds-4231	340	47	by	by	ADP
ijpds-4231	340	48	hplc	hplc	NOUN
ijpds-4231	340	49	)	)	PUNCT
ijpds-4231	340	50	.	.	PUNCT
ijpds-4231	341	1	it	it	PRON
ijpds-4231	341	2	was	be	AUX
ijpds-4231	341	3	diluted	dilute	VERB
ijpds-4231	341	4	in	in	ADP
ijpds-4231	341	5	isopropyl	isopropyl	NOUN
ijpds-4231	341	6	alcohol	alcohol	NOUN
ijpds-4231	341	7	and	and	CCONJ
ijpds-4231	341	8	treated	treat	VERB
ijpds-4231	341	9	with	with	ADP
ijpds-4231	341	10	methanesulfonic	methanesulfonic	ADJ
ijpds-4231	341	11	acid	acid	NOUN
ijpds-4231	341	12	to	to	PART
ijpds-4231	341	13	obtain	obtain	VERB
ijpds-4231	341	14	1	1	NUM
ijpds-4231	341	15	(	(	PUNCT
ijpds-4231	341	16	yield	yield	NOUN
ijpds-4231	341	17	:	:	PUNCT
ijpds-4231	341	18	58.5	58.5	NUM
ijpds-4231	341	19	%	%	NOUN
ijpds-4231	341	20	,	,	PUNCT
ijpds-4231	341	21	purity	purity	NOUN
ijpds-4231	341	22	:	:	PUNCT
ijpds-4231	341	23	99.89	99.89	NUM
ijpds-4231	341	24	%	%	NOUN
ijpds-4231	341	25	by	by	ADP
ijpds-4231	341	26	hplc	hplc	NOUN
ijpds-4231	341	27	)	)	PUNCT
ijpds-4231	342	1	[	[	X
ijpds-4231	342	2	67	67	NUM
ijpds-4231	342	3	]	]	PUNCT
ijpds-4231	342	4	.	.	PUNCT
ijpds-4231	343	1	li	li	PROPN
ijpds-4231	343	2	j	j	PROPN
ijpds-4231	343	3	,	,	PUNCT
ijpds-4231	343	4	et	et	PROPN
ijpds-4231	343	5	al	al	PROPN
ijpds-4231	343	6	.	.	PROPN
ijpds-4231	343	7	,	,	PUNCT
ijpds-4231	343	8	in	in	ADP
ijpds-4231	343	9	2020	2020	NUM
ijpds-4231	343	10	,	,	PUNCT
ijpds-4231	343	11	had	have	AUX
ijpds-4231	343	12	reported	report	VERB
ijpds-4231	343	13	a	a	DET
ijpds-4231	343	14	one	one	NUM
ijpds-4231	343	15	-	-	PUNCT
ijpds-4231	343	16	pot	pot	NOUN
ijpds-4231	343	17	synthetic	synthetic	ADJ
ijpds-4231	343	18	procedure	procedure	NOUN
ijpds-4231	343	19	to	to	PART
ijpds-4231	343	20	isolate	isolate	VERB
ijpds-4231	343	21	rasagiline	rasagiline	NOUN
ijpds-4231	343	22	base	base	NOUN
ijpds-4231	343	23	by	by	ADP
ijpds-4231	343	24	the	the	DET
ijpds-4231	343	25	condensation	condensation	NOUN
ijpds-4231	343	26	of	of	ADP
ijpds-4231	343	27	sanjay	sanjay	PROPN
ijpds-4231	343	28	s	s	PART
ijpds-4231	343	29	s	s	NOUN
ijpds-4231	343	30	patents	patent	NOUN
ijpds-4231	343	31	disclosed	disclose	VERB
ijpds-4231	343	32	synthetic	synthetic	ADJ
ijpds-4231	343	33	overview	overview	NOUN
ijpds-4231	343	34	of	of	ADP
ijpds-4231	343	35	rasagiline	rasagiline	ADJ
ijpds-4231	343	36	vol	vol	NOUN
ijpds-4231	343	37	2	2	NUM
ijpds-4231	343	38	|	|	ADV
ijpds-4231	343	39	issue	issue	VERB
ijpds-4231	343	40	4	4	NUM
ijpds-4231	343	41	|	|	ADV
ijpds-4231	343	42	oct	oct	PROPN
ijpds-4231	343	43	–	–	PUNCT
ijpds-4231	343	44	dec	dec	PROPN
ijpds-4231	343	45	2023	2023	NUM
ijpds-4231	343	46	indian	indian	PROPN
ijpds-4231	343	47	j	j	PROPN
ijpds-4231	343	48	pharm	pharm	PROPN
ijpds-4231	343	49	drug	drug	PROPN
ijpds-4231	343	50	studies	study	NOUN
ijpds-4231	343	51	|	|	ADV
ijpds-4231	343	52	142	142	NUM
ijpds-4231	343	53	9	9	NUM
ijpds-4231	343	54	with	with	ADP
ijpds-4231	343	55	6	6	NUM
ijpds-4231	343	56	in	in	ADP
ijpds-4231	343	57	the	the	DET
ijpds-4231	343	58	presence	presence	NOUN
ijpds-4231	343	59	of	of	ADP
ijpds-4231	343	60	a	a	DET
ijpds-4231	343	61	suitable	suitable	ADJ
ijpds-4231	343	62	dehydrating	dehydrate	VERB
ijpds-4231	343	63	agent	agent	NOUN
ijpds-4231	343	64	/	/	SYM
ijpds-4231	343	65	s	s	X
ijpds-4231	343	66	(	(	PUNCT
ijpds-4231	343	67	sodium	sodium	NOUN
ijpds-4231	343	68	borohydride	borohydride	NOUN
ijpds-4231	343	69	,	,	PUNCT
ijpds-4231	343	70	glacial	glacial	ADJ
ijpds-4231	343	71	acetic	acetic	ADJ
ijpds-4231	343	72	acid	acid	NOUN
ijpds-4231	343	73	and	and	CCONJ
ijpds-4231	343	74	tetraisopropyl	tetraisopropyl	NOUN
ijpds-4231	343	75	titanate	titanate	NOUN
ijpds-4231	343	76	)	)	PUNCT
ijpds-4231	343	77	in	in	ADP
ijpds-4231	343	78	tetrahydrofuran	tetrahydrofuran	NOUN
ijpds-4231	343	79	to	to	PART
ijpds-4231	343	80	isolate	isolate	VERB
ijpds-4231	343	81	racemic	racemic	ADJ
ijpds-4231	343	82	rasagiline	rasagiline	NOUN
ijpds-4231	343	83	base	base	NOUN
ijpds-4231	343	84	(	(	PUNCT
ijpds-4231	343	85	yield	yield	NOUN
ijpds-4231	343	86	:	:	PUNCT
ijpds-4231	343	87	93.6	93.6	NUM
ijpds-4231	343	88	%	%	NOUN
ijpds-4231	343	89	,	,	PUNCT
ijpds-4231	343	90	purity	purity	NOUN
ijpds-4231	343	91	:	:	PUNCT
ijpds-4231	343	92	95.67	95.67	NUM
ijpds-4231	343	93	%	%	NOUN
ijpds-4231	343	94	by	by	ADP
ijpds-4231	343	95	hplc	hplc	NOUN
ijpds-4231	343	96	,	,	PUNCT
ijpds-4231	343	97	as	as	ADP
ijpds-4231	343	98	red	red	ADJ
ijpds-4231	343	99	-	-	PUNCT
ijpds-4231	343	100	brown	brown	ADJ
ijpds-4231	343	101	oily	oily	ADJ
ijpds-4231	343	102	liquid	liquid	NOUN
ijpds-4231	343	103	)	)	PUNCT
ijpds-4231	343	104	.	.	PUNCT
ijpds-4231	344	1	it	it	PRON
ijpds-4231	344	2	was	be	AUX
ijpds-4231	344	3	resolved	resolve	VERB
ijpds-4231	344	4	by	by	ADP
ijpds-4231	344	5	the	the	DET
ijpds-4231	344	6	use	use	NOUN
ijpds-4231	344	7	of	of	ADP
ijpds-4231	344	8	l(+)-tartaric	l(+)-tartaric	ADJ
ijpds-4231	344	9	acid	acid	NOUN
ijpds-4231	344	10	to	to	PART
ijpds-4231	344	11	get	get	VERB
ijpds-4231	344	12	r	r	NOUN
ijpds-4231	344	13	-	-	PUNCT
ijpds-4231	344	14	rasagiline	rasagiline	NOUN
ijpds-4231	344	15	tartarate	tartarate	NOUN
ijpds-4231	344	16	(	(	PUNCT
ijpds-4231	344	17	yield	yield	NOUN
ijpds-4231	344	18	:	:	PUNCT
ijpds-4231	344	19	39	39	NUM
ijpds-4231	344	20	%	%	NOUN
ijpds-4231	344	21	,	,	PUNCT
ijpds-4231	344	22	purity	purity	NOUN
ijpds-4231	344	23	:	:	PUNCT
ijpds-4231	344	24	99.46	99.46	NUM
ijpds-4231	344	25	%	%	NOUN
ijpds-4231	344	26	by	by	ADP
ijpds-4231	344	27	hplc	hplc	NOUN
ijpds-4231	344	28	,	,	PUNCT
ijpds-4231	344	29	as	as	SCONJ
ijpds-4231	344	30	off	off	ADP
ijpds-4231	344	31	-	-	PUNCT
ijpds-4231	344	32	while	while	NOUN
ijpds-4231	344	33	solid	solid	ADJ
ijpds-4231	344	34	)	)	PUNCT
ijpds-4231	344	35	.	.	PUNCT
ijpds-4231	345	1	it	it	PRON
ijpds-4231	345	2	was	be	AUX
ijpds-4231	345	3	desalted	desalt	VERB
ijpds-4231	345	4	and	and	CCONJ
ijpds-4231	345	5	treated	treat	VERB
ijpds-4231	345	6	with	with	ADP
ijpds-4231	345	7	methanesulfonic	methanesulfonic	ADJ
ijpds-4231	345	8	acid	acid	NOUN
ijpds-4231	345	9	in	in	ADP
ijpds-4231	345	10	isopropyl	isopropyl	NOUN
ijpds-4231	345	11	alcohol	alcohol	NOUN
ijpds-4231	345	12	to	to	PART
ijpds-4231	345	13	get	get	VERB
ijpds-4231	345	14	1	1	NUM
ijpds-4231	345	15	(	(	PUNCT
ijpds-4231	345	16	yield	yield	NOUN
ijpds-4231	345	17	:	:	PUNCT
ijpds-4231	345	18	87.6	87.6	NUM
ijpds-4231	345	19	%	%	NOUN
ijpds-4231	345	20	,	,	PUNCT
ijpds-4231	345	21	purity	purity	NOUN
ijpds-4231	345	22	:	:	PUNCT
ijpds-4231	345	23	99.80	99.80	NUM
ijpds-4231	345	24	%	%	NOUN
ijpds-4231	345	25	by	by	ADP
ijpds-4231	345	26	hplc	hplc	NOUN
ijpds-4231	345	27	)	)	PUNCT
ijpds-4231	346	1	[	[	X
ijpds-4231	346	2	68	68	NUM
ijpds-4231	346	3	]	]	PUNCT
ijpds-4231	346	4	.	.	PUNCT
ijpds-4231	347	1	ma	ma	PROPN
ijpds-4231	347	2	y	y	PROPN
ijpds-4231	347	3	,	,	PUNCT
ijpds-4231	347	4	et	et	PROPN
ijpds-4231	347	5	al	al	PROPN
ijpds-4231	347	6	.	.	PROPN
ijpds-4231	347	7	,	,	PUNCT
ijpds-4231	347	8	in	in	ADP
ijpds-4231	347	9	2020	2020	NUM
ijpds-4231	347	10	,	,	PUNCT
ijpds-4231	347	11	had	have	AUX
ijpds-4231	347	12	demonstrated	demonstrate	VERB
ijpds-4231	347	13	the	the	DET
ijpds-4231	347	14	condensation	condensation	NOUN
ijpds-4231	347	15	of	of	ADP
ijpds-4231	347	16	r-(-)-isomer	r-(-)-isomer	PROPN
ijpds-4231	347	17	of	of	ADP
ijpds-4231	347	18	2	2	NUM
ijpds-4231	347	19	with	with	ADP
ijpds-4231	347	20	3	3	NUM
ijpds-4231	347	21	in	in	ADP
ijpds-4231	347	22	the	the	DET
ijpds-4231	347	23	presence	presence	NOUN
ijpds-4231	347	24	of	of	ADP
ijpds-4231	347	25	n	n	CCONJ
ijpds-4231	347	26	,	,	PUNCT
ijpds-4231	347	27	ndiisopropylethylamine	ndiisopropylethylamine	NOUN
ijpds-4231	347	28	in	in	ADP
ijpds-4231	347	29	acetonitrile	acetonitrile	NOUN
ijpds-4231	347	30	to	to	PART
ijpds-4231	347	31	isolate	isolate	VERB
ijpds-4231	347	32	rrasagiline	rrasagiline	ADJ
ijpds-4231	347	33	base	base	NOUN
ijpds-4231	347	34	(	(	PUNCT
ijpds-4231	347	35	yield	yield	NOUN
ijpds-4231	347	36	:	:	PUNCT
ijpds-4231	347	37	45.3	45.3	NUM
ijpds-4231	347	38	-	-	SYM
ijpds-4231	347	39	58	58	NUM
ijpds-4231	347	40	%	%	NOUN
ijpds-4231	347	41	,	,	PUNCT
ijpds-4231	347	42	purity	purity	NOUN
ijpds-4231	347	43	:	:	PUNCT
ijpds-4231	347	44	91.4	91.4	NUM
ijpds-4231	347	45	-	-	SYM
ijpds-4231	347	46	97.54	97.54	NUM
ijpds-4231	347	47	%	%	NOUN
ijpds-4231	347	48	by	by	ADP
ijpds-4231	347	49	hplc	hplc	NOUN
ijpds-4231	347	50	)	)	PUNCT
ijpds-4231	347	51	.	.	PUNCT
ijpds-4231	348	1	it	it	PRON
ijpds-4231	348	2	was	be	AUX
ijpds-4231	348	3	dissolved	dissolve	VERB
ijpds-4231	348	4	in	in	ADP
ijpds-4231	348	5	isopropyl	isopropyl	NOUN
ijpds-4231	348	6	alcohol	alcohol	NOUN
ijpds-4231	348	7	and	and	CCONJ
ijpds-4231	348	8	added	add	VERB
ijpds-4231	348	9	methanesulfonic	methanesulfonic	ADJ
ijpds-4231	348	10	acid	acid	NOUN
ijpds-4231	348	11	to	to	PART
ijpds-4231	348	12	isolate	isolate	VERB
ijpds-4231	348	13	1	1	NUM
ijpds-4231	348	14	(	(	PUNCT
ijpds-4231	348	15	yield	yield	NOUN
ijpds-4231	348	16	:	:	PUNCT
ijpds-4231	348	17	83.1	83.1	NUM
ijpds-4231	348	18	%	%	NOUN
ijpds-4231	348	19	,	,	PUNCT
ijpds-4231	348	20	purity	purity	NOUN
ijpds-4231	348	21	:	:	PUNCT
ijpds-4231	348	22	99.3	99.3	NUM
ijpds-4231	348	23	%	%	NOUN
ijpds-4231	348	24	by	by	ADP
ijpds-4231	348	25	hplc	hplc	PROPN
ijpds-4231	348	26	)	)	PUNCT
ijpds-4231	348	27	.	.	PUNCT
ijpds-4231	349	1	the	the	DET
ijpds-4231	349	2	work	work	NOUN
ijpds-4231	349	3	had	have	AUX
ijpds-4231	349	4	even	even	ADV
ijpds-4231	349	5	covered	cover	VERB
ijpds-4231	349	6	the	the	DET
ijpds-4231	349	7	process	process	NOUN
ijpds-4231	349	8	to	to	PART
ijpds-4231	349	9	recover	recover	VERB
ijpds-4231	349	10	the	the	DET
ijpds-4231	349	11	un	un	PROPN
ijpds-4231	349	12	-	-	ADJ
ijpds-4231	349	13	reacted	react	VERB
ijpds-4231	349	14	2	2	NUM
ijpds-4231	349	15	from	from	ADP
ijpds-4231	349	16	the	the	DET
ijpds-4231	349	17	filtrate	filtrate	NOUN
ijpds-4231	349	18	(	(	PUNCT
ijpds-4231	349	19	recovery	recovery	NOUN
ijpds-4231	349	20	:	:	PUNCT
ijpds-4231	349	21	32	32	NUM
ijpds-4231	349	22	%	%	NOUN
ijpds-4231	349	23	,	,	PUNCT
ijpds-4231	349	24	purity	purity	NOUN
ijpds-4231	349	25	:	:	PUNCT
ijpds-4231	349	26	81	81	NUM
ijpds-4231	349	27	%	%	NOUN
ijpds-4231	349	28	by	by	ADP
ijpds-4231	349	29	hplc	hplc	NOUN
ijpds-4231	349	30	)	)	PUNCT
ijpds-4231	350	1	[	[	X
ijpds-4231	350	2	69	69	NUM
ijpds-4231	350	3	]	]	PUNCT
ijpds-4231	350	4	.	.	PUNCT
ijpds-4231	351	1	ma	ma	PROPN
ijpds-4231	351	2	y	y	PROPN
ijpds-4231	351	3	,	,	PUNCT
ijpds-4231	351	4	et	et	PROPN
ijpds-4231	351	5	al	al	PROPN
ijpds-4231	351	6	.	.	PROPN
ijpds-4231	351	7	,	,	PUNCT
ijpds-4231	351	8	in	in	ADP
ijpds-4231	351	9	2021	2021	NUM
ijpds-4231	351	10	,	,	PUNCT
ijpds-4231	351	11	had	have	AUX
ijpds-4231	351	12	illustrated	illustrate	VERB
ijpds-4231	351	13	the	the	DET
ijpds-4231	351	14	synthesis	synthesis	NOUN
ijpds-4231	351	15	of	of	ADP
ijpds-4231	351	16	a	a	DET
ijpds-4231	351	17	few	few	ADJ
ijpds-4231	351	18	critical	critical	ADJ
ijpds-4231	351	19	genotoxic	genotoxic	ADJ
ijpds-4231	351	20	impurities	impurity	NOUN
ijpds-4231	351	21	like	like	ADP
ijpds-4231	351	22	(	(	PUNCT
ijpds-4231	351	23	1r)-n-(2	1r)-n-(2	NUM
ijpds-4231	351	24	-	-	PUNCT
ijpds-4231	351	25	chloroprop-2en-1	chloroprop-2en-1	PRON
ijpds-4231	351	26	-	-	PUNCT
ijpds-4231	351	27	yl)-2,3	yl)-2,3	NOUN
ijpds-4231	351	28	-	-	PUNCT
ijpds-4231	351	29	dihydro-1h	dihydro-1h	NOUN
ijpds-4231	351	30	-	-	PUNCT
ijpds-4231	351	31	inden-1	inden-1	NOUN
ijpds-4231	351	32	-	-	PUNCT
ijpds-4231	351	33	amine	amine	ADJ
ijpds-4231	351	34	51	51	NUM
ijpds-4231	351	35	(	(	PUNCT
ijpds-4231	351	36	purity	purity	NOUN
ijpds-4231	351	37	:	:	PUNCT
ijpds-4231	351	38	84.6	84.6	NUM
ijpds-4231	351	39	%	%	NOUN
ijpds-4231	351	40	by	by	ADP
ijpds-4231	351	41	hplc	hplc	NOUN
ijpds-4231	351	42	,	,	PUNCT
ijpds-4231	351	43	as	as	ADP
ijpds-4231	351	44	light	light	ADJ
ijpds-4231	351	45	yellow	yellow	ADJ
ijpds-4231	351	46	oil	oil	NOUN
ijpds-4231	351	47	)	)	PUNCT
ijpds-4231	351	48	,	,	PUNCT
ijpds-4231	351	49	(	(	PUNCT
ijpds-4231	351	50	1r)-n-[(2e)-3	1r)-n-[(2e)-3	NUM
ijpds-4231	351	51	-	-	PUNCT
ijpds-4231	351	52	chloroprop2	chloroprop2	NOUN
ijpds-4231	351	53	-	-	PUNCT
ijpds-4231	351	54	en-1	en-1	NOUN
ijpds-4231	351	55	-	-	PUNCT
ijpds-4231	351	56	yl]-2,3	yl]-2,3	NOUN
ijpds-4231	351	57	-	-	PUNCT
ijpds-4231	351	58	dihydro-1h	dihydro-1h	NOUN
ijpds-4231	351	59	-	-	PUNCT
ijpds-4231	351	60	inden-1	inden-1	NOUN
ijpds-4231	351	61	-	-	PUNCT
ijpds-4231	351	62	amine	amine	ADJ
ijpds-4231	351	63	52	52	NUM
ijpds-4231	351	64	(	(	PUNCT
ijpds-4231	351	65	yield	yield	NOUN
ijpds-4231	351	66	:	:	PUNCT
ijpds-4231	351	67	89.3	89.3	NUM
ijpds-4231	351	68	%	%	NOUN
ijpds-4231	351	69	by	by	ADP
ijpds-4231	351	70	hplc	hplc	NOUN
ijpds-4231	351	71	,	,	PUNCT
ijpds-4231	351	72	as	as	ADP
ijpds-4231	351	73	yellow	yellow	ADJ
ijpds-4231	351	74	oil	oil	NOUN
ijpds-4231	351	75	)	)	PUNCT
ijpds-4231	351	76	,	,	PUNCT
ijpds-4231	351	77	(	(	PUNCT
ijpds-4231	351	78	1r)-n-[(2z)-3chloroprop-2	1r)-n-[(2z)-3chloroprop-2	NUM
ijpds-4231	351	79	-	-	PUNCT
ijpds-4231	351	80	en-1	en-1	NOUN
ijpds-4231	351	81	-	-	PUNCT
ijpds-4231	351	82	yl]-2,3	yl]-2,3	NOUN
ijpds-4231	351	83	-	-	PUNCT
ijpds-4231	351	84	dihydro-1h	dihydro-1h	NOUN
ijpds-4231	351	85	-	-	PUNCT
ijpds-4231	351	86	inden-1	inden-1	NOUN
ijpds-4231	351	87	-	-	PUNCT
ijpds-4231	351	88	amine	amine	ADJ
ijpds-4231	351	89	53	53	NUM
ijpds-4231	351	90	(	(	PUNCT
ijpds-4231	351	91	purity	purity	NOUN
ijpds-4231	351	92	:	:	PUNCT
ijpds-4231	351	93	88.4	88.4	NUM
ijpds-4231	351	94	%	%	NOUN
ijpds-4231	351	95	by	by	ADP
ijpds-4231	351	96	hplc	hplc	NOUN
ijpds-4231	351	97	,	,	PUNCT
ijpds-4231	351	98	as	as	ADP
ijpds-4231	351	99	yellow	yellow	ADJ
ijpds-4231	351	100	oil	oil	NOUN
ijpds-4231	351	101	)	)	PUNCT
ijpds-4231	351	102	,	,	PUNCT
ijpds-4231	351	103	(	(	PUNCT
ijpds-4231	351	104	1r)-n	1r)-n	NUM
ijpds-4231	351	105	-	-	PUNCT
ijpds-4231	351	106	nitroso	nitroso	NOUN
ijpds-4231	351	107	-	-	PUNCT
ijpds-4231	351	108	n(prop-2	n(prop-2	NOUN
ijpds-4231	351	109	-	-	PUNCT
ijpds-4231	351	110	yn-1	yn-1	NOUN
ijpds-4231	351	111	-	-	PUNCT
ijpds-4231	351	112	yl)-2,3	yl)-2,3	NOUN
ijpds-4231	351	113	-	-	PUNCT
ijpds-4231	351	114	dihydro-1h	dihydro-1h	NOUN
ijpds-4231	351	115	-	-	PUNCT
ijpds-4231	351	116	inden-1	inden-1	NOUN
ijpds-4231	351	117	-	-	PUNCT
ijpds-4231	351	118	amine	amine	ADJ
ijpds-4231	351	119	54	54	NUM
ijpds-4231	351	120	(	(	PUNCT
ijpds-4231	351	121	purity	purity	NOUN
ijpds-4231	351	122	:	:	PUNCT
ijpds-4231	351	123	88	88	NUM
ijpds-4231	351	124	-	-	SYM
ijpds-4231	351	125	8.9	8.9	NUM
ijpds-4231	351	126	%	%	NOUN
ijpds-4231	351	127	by	by	ADP
ijpds-4231	351	128	hplc	hplc	PROPN
ijpds-4231	351	129	,	,	PUNCT
ijpds-4231	351	130	red	red	ADJ
ijpds-4231	351	131	-	-	PUNCT
ijpds-4231	351	132	brown	brown	ADJ
ijpds-4231	351	133	oil	oil	NOUN
ijpds-4231	351	134	)	)	PUNCT
ijpds-4231	351	135	and	and	CCONJ
ijpds-4231	351	136	n-[(1r)2,3	n-[(1r)2,3	PROPN
ijpds-4231	351	137	-	-	PROPN
ijpds-4231	351	138	dihydro-1h	dihydro-1h	NOUN
ijpds-4231	351	139	-	-	PUNCT
ijpds-4231	351	140	inden-1	inden-1	NOUN
ijpds-4231	351	141	-	-	PUNCT
ijpds-4231	351	142	yl]-n	yl]-n	ADJ
ijpds-4231	351	143	-	-	ADJ
ijpds-4231	351	144	nitroso-2,3	nitroso-2,3	ADJ
ijpds-4231	351	145	-	-	PUNCT
ijpds-4231	351	146	dihydro-1hinden-1	dihydro-1hinden-1	NOUN
ijpds-4231	351	147	-	-	PUNCT
ijpds-4231	351	148	amine	amine	ADJ
ijpds-4231	351	149	55	55	NUM
ijpds-4231	351	150	(	(	PUNCT
ijpds-4231	351	151	purity	purity	NOUN
ijpds-4231	351	152	:	:	PUNCT
ijpds-4231	351	153	75	75	NUM
ijpds-4231	351	154	-	-	SYM
ijpds-4231	351	155	79.8	79.8	NUM
ijpds-4231	351	156	%	%	NOUN
ijpds-4231	351	157	by	by	ADP
ijpds-4231	351	158	hplc	hplc	NOUN
ijpds-4231	351	159	,	,	PUNCT
ijpds-4231	351	160	as	as	SCONJ
ijpds-4231	351	161	brownblack	brownblack	VERB
ijpds-4231	351	162	oil	oil	NOUN
ijpds-4231	351	163	)	)	PUNCT
ijpds-4231	351	164	.	.	PUNCT
ijpds-4231	352	1	these	these	PRON
ijpds-4231	352	2	are	be	AUX
ijpds-4231	352	3	the	the	DET
ijpds-4231	352	4	process	process	NOUN
ijpds-4231	352	5	related	relate	VERB
ijpds-4231	352	6	impurities	impurity	NOUN
ijpds-4231	352	7	of	of	ADP
ijpds-4231	352	8	1	1	NUM
ijpds-4231	352	9	,	,	PUNCT
ijpds-4231	352	10	and	and	CCONJ
ijpds-4231	352	11	are	be	AUX
ijpds-4231	352	12	synthesized	synthesize	VERB
ijpds-4231	352	13	by	by	ADP
ijpds-4231	352	14	the	the	DET
ijpds-4231	352	15	suitable	suitable	ADJ
ijpds-4231	352	16	reagents	reagent	NOUN
ijpds-4231	352	17	under	under	ADP
ijpds-4231	352	18	the	the	DET
ijpds-4231	352	19	favorable	favorable	ADJ
ijpds-4231	352	20	reaction	reaction	NOUN
ijpds-4231	352	21	conditions	condition	NOUN
ijpds-4231	352	22	.	.	PUNCT
ijpds-4231	353	1	the	the	DET
ijpds-4231	353	2	work	work	NOUN
ijpds-4231	353	3	had	have	AUX
ijpds-4231	353	4	even	even	ADV
ijpds-4231	353	5	extended	extend	VERB
ijpds-4231	353	6	to	to	PART
ijpds-4231	353	7	provide	provide	VERB
ijpds-4231	353	8	the	the	DET
ijpds-4231	353	9	characterization	characterization	NOUN
ijpds-4231	353	10	details	detail	NOUN
ijpds-4231	353	11	of	of	ADP
ijpds-4231	353	12	impurities	impurity	NOUN
ijpds-4231	353	13	and	and	CCONJ
ijpds-4231	353	14	their	their	PRON
ijpds-4231	353	15	detection	detection	NOUN
ijpds-4231	353	16	methods	method	NOUN
ijpds-4231	353	17	in	in	ADP
ijpds-4231	353	18	the	the	DET
ijpds-4231	353	19	finished	finished	ADJ
ijpds-4231	353	20	product	product	NOUN
ijpds-4231	353	21	[	[	X
ijpds-4231	353	22	70,71	70,71	NUM
ijpds-4231	353	23	]	]	X
ijpds-4231	353	24	.	.	PUNCT
ijpds-4231	354	1	hu	hu	PROPN
ijpds-4231	355	1	a	a	PRON
ijpds-4231	355	2	,	,	PUNCT
ijpds-4231	355	3	et	et	PROPN
ijpds-4231	355	4	al	al	PROPN
ijpds-4231	355	5	.	.	PROPN
ijpds-4231	355	6	,	,	PUNCT
ijpds-4231	355	7	in	in	ADP
ijpds-4231	355	8	2022	2022	NUM
ijpds-4231	355	9	,	,	PUNCT
ijpds-4231	355	10	had	have	AUX
ijpds-4231	355	11	demonstrated	demonstrate	VERB
ijpds-4231	355	12	an	an	DET
ijpds-4231	355	13	electroreduction	electroreduction	NOUN
ijpds-4231	355	14	synthetic	synthetic	ADJ
ijpds-4231	355	15	pathway	pathway	NOUN
ijpds-4231	355	16	(	(	PUNCT
ijpds-4231	355	17	a	a	DET
ijpds-4231	355	18	green	green	ADJ
ijpds-4231	355	19	chemistry	chemistry	NOUN
ijpds-4231	355	20	approach	approach	NOUN
ijpds-4231	355	21	)	)	PUNCT
ijpds-4231	355	22	to	to	PART
ijpds-4231	355	23	isolate	isolate	VERB
ijpds-4231	355	24	racemic	racemic	ADJ
ijpds-4231	355	25	2	2	NUM
ijpds-4231	355	26	hydrochloride	hydrochloride	NOUN
ijpds-4231	355	27	.	.	PUNCT
ijpds-4231	356	1	the	the	DET
ijpds-4231	356	2	reduction	reduction	NOUN
ijpds-4231	356	3	of	of	ADP
ijpds-4231	356	4	15	15	NUM
ijpds-4231	356	5	under	under	ADP
ijpds-4231	356	6	electrolytic	electrolytic	ADJ
ijpds-4231	356	7	conditions	condition	NOUN
ijpds-4231	356	8	(	(	PUNCT
ijpds-4231	356	9	alkaline	alkaline	NOUN
ijpds-4231	356	10	)	)	PUNCT
ijpds-4231	356	11	was	be	AUX
ijpds-4231	356	12	performed	perform	VERB
ijpds-4231	356	13	in	in	ADP
ijpds-4231	356	14	the	the	DET
ijpds-4231	356	15	presence	presence	NOUN
ijpds-4231	356	16	of	of	ADP
ijpds-4231	356	17	an	an	DET
ijpds-4231	356	18	organic	organic	ADJ
ijpds-4231	356	19	solvent	solvent	NOUN
ijpds-4231	356	20	to	to	PART
ijpds-4231	356	21	obtain	obtain	VERB
ijpds-4231	356	22	racemic	racemic	ADJ
ijpds-4231	356	23	2	2	NUM
ijpds-4231	356	24	hydrochloride	hydrochloride	NOUN
ijpds-4231	356	25	with	with	ADP
ijpds-4231	356	26	a	a	DET
ijpds-4231	356	27	melting	melting	NOUN
ijpds-4231	356	28	point	point	NOUN
ijpds-4231	356	29	of	of	ADP
ijpds-4231	356	30	210	210	NUM
ijpds-4231	356	31	-	-	PUNCT
ijpds-4231	356	32	212oc	212oc	NOUN
ijpds-4231	356	33	(	(	PUNCT
ijpds-4231	356	34	yield	yield	NOUN
ijpds-4231	356	35	:	:	PUNCT
ijpds-4231	356	36	90.6	90.6	NUM
ijpds-4231	356	37	%	%	NOUN
ijpds-4231	356	38	,	,	PUNCT
ijpds-4231	356	39	as	as	ADP
ijpds-4231	356	40	a	a	DET
ijpds-4231	356	41	white	white	X
ijpds-4231	356	42	solid	solid	NOUN
ijpds-4231	356	43	)	)	PUNCT
ijpds-4231	357	1	[	[	X
ijpds-4231	357	2	72	72	NUM
ijpds-4231	357	3	]	]	PUNCT
ijpds-4231	357	4	.	.	PUNCT
ijpds-4231	358	1	tang	tang	PROPN
ijpds-4231	358	2	h	h	PROPN
ijpds-4231	358	3	,	,	PUNCT
ijpds-4231	358	4	et	et	PROPN
ijpds-4231	358	5	al	al	PROPN
ijpds-4231	358	6	.	.	PROPN
ijpds-4231	358	7	,	,	PUNCT
ijpds-4231	358	8	in	in	ADP
ijpds-4231	358	9	2023	2023	NUM
ijpds-4231	358	10	,	,	PUNCT
ijpds-4231	358	11	had	have	AUX
ijpds-4231	358	12	reported	report	VERB
ijpds-4231	358	13	the	the	DET
ijpds-4231	358	14	cyclization	cyclization	NOUN
ijpds-4231	358	15	of	of	ADP
ijpds-4231	358	16	3phenylpropanoic	3phenylpropanoic	NUM
ijpds-4231	358	17	acid	acid	NOUN
ijpds-4231	358	18	56	56	NUM
ijpds-4231	358	19	in	in	ADP
ijpds-4231	358	20	the	the	DET
ijpds-4231	358	21	presence	presence	NOUN
ijpds-4231	358	22	of	of	ADP
ijpds-4231	358	23	trifluoromethanesulfonic	trifluoromethanesulfonic	ADJ
ijpds-4231	358	24	acid	acid	NOUN
ijpds-4231	358	25	and	and	CCONJ
ijpds-4231	358	26	trifluoromethanesulfonic	trifluoromethanesulfonic	ADJ
ijpds-4231	358	27	anhydride	anhydride	NOUN
ijpds-4231	358	28	to	to	PART
ijpds-4231	358	29	isolate	isolate	VERB
ijpds-4231	358	30	15	15	NUM
ijpds-4231	358	31	(	(	PUNCT
ijpds-4231	358	32	yield	yield	NOUN
ijpds-4231	358	33	:	:	PUNCT
ijpds-4231	358	34	86.84	86.84	NUM
ijpds-4231	358	35	%	%	NOUN
ijpds-4231	358	36	,	,	PUNCT
ijpds-4231	358	37	purity	purity	NOUN
ijpds-4231	358	38	:	:	PUNCT
ijpds-4231	358	39	99.37	99.37	NUM
ijpds-4231	358	40	%	%	NOUN
ijpds-4231	358	41	by	by	ADP
ijpds-4231	358	42	hplc	hplc	NOUN
ijpds-4231	358	43	)	)	PUNCT
ijpds-4231	358	44	.	.	PUNCT
ijpds-4231	359	1	it	it	PRON
ijpds-4231	359	2	was	be	AUX
ijpds-4231	359	3	dissolved	dissolve	VERB
ijpds-4231	359	4	in	in	ADP
ijpds-4231	359	5	tetrahydrofuran	tetrahydrofuran	NOUN
ijpds-4231	359	6	and	and	CCONJ
ijpds-4231	359	7	treated	treat	VERB
ijpds-4231	359	8	with	with	ADP
ijpds-4231	359	9	sodium	sodium	NOUN
ijpds-4231	359	10	triacetoxyborohydride	triacetoxyborohydride	NOUN
ijpds-4231	359	11	and	and	CCONJ
ijpds-4231	359	12	added	add	VERB
ijpds-4231	359	13	the	the	DET
ijpds-4231	359	14	solution	solution	NOUN
ijpds-4231	359	15	of	of	ADP
ijpds-4231	359	16	6	6	NUM
ijpds-4231	359	17	in	in	ADP
ijpds-4231	359	18	tetrahydrofuran	tetrahydrofuran	NOUN
ijpds-4231	359	19	to	to	PART
ijpds-4231	359	20	obtain	obtain	VERB
ijpds-4231	359	21	racemic	racemic	ADJ
ijpds-4231	359	22	rasagiline	rasagiline	NOUN
ijpds-4231	359	23	hydrochloride	hydrochloride	NOUN
ijpds-4231	359	24	(	(	PUNCT
ijpds-4231	359	25	yield	yield	NOUN
ijpds-4231	359	26	:	:	PUNCT
ijpds-4231	359	27	79	79	NUM
ijpds-4231	359	28	%	%	NOUN
ijpds-4231	359	29	,	,	PUNCT
ijpds-4231	359	30	purity	purity	NOUN
ijpds-4231	359	31	:	:	PUNCT
ijpds-4231	359	32	99.67	99.67	NUM
ijpds-4231	359	33	%	%	NOUN
ijpds-4231	359	34	by	by	ADP
ijpds-4231	359	35	hplc	hplc	NOUN
ijpds-4231	359	36	)	)	PUNCT
ijpds-4231	359	37	.	.	PUNCT
ijpds-4231	360	1	it	it	PRON
ijpds-4231	360	2	was	be	AUX
ijpds-4231	360	3	de	de	ADJ
ijpds-4231	360	4	-	-	VERB
ijpds-4231	360	5	salted	salt	VERB
ijpds-4231	360	6	and	and	CCONJ
ijpds-4231	360	7	resolved	resolve	VERB
ijpds-4231	360	8	using	use	VERB
ijpds-4231	360	9	l	l	PROPN
ijpds-4231	360	10	-	-	ADJ
ijpds-4231	360	11	tartaric	tartaric	ADJ
ijpds-4231	360	12	acid	acid	NOUN
ijpds-4231	360	13	in	in	ADP
ijpds-4231	360	14	methyl	methyl	NOUN
ijpds-4231	360	15	alcohol	alcohol	NOUN
ijpds-4231	360	16	to	to	PART
ijpds-4231	360	17	isolate	isolate	VERB
ijpds-4231	360	18	r	r	NOUN
ijpds-4231	360	19	-	-	PUNCT
ijpds-4231	360	20	rasagiline	rasagiline	NOUN
ijpds-4231	360	21	tartarate	tartarate	NOUN
ijpds-4231	360	22	(	(	PUNCT
ijpds-4231	360	23	yield	yield	NOUN
ijpds-4231	360	24	:	:	PUNCT
ijpds-4231	360	25	34.38	34.38	NUM
ijpds-4231	360	26	%	%	NOUN
ijpds-4231	360	27	,	,	PUNCT
ijpds-4231	360	28	purity	purity	NOUN
ijpds-4231	360	29	:	:	PUNCT
ijpds-4231	360	30	98.83	98.83	NUM
ijpds-4231	360	31	%	%	NOUN
ijpds-4231	360	32	)	)	PUNCT
ijpds-4231	360	33	.	.	PUNCT
ijpds-4231	361	1	it	it	PRON
ijpds-4231	361	2	was	be	AUX
ijpds-4231	361	3	treated	treat	VERB
ijpds-4231	361	4	with	with	ADP
ijpds-4231	361	5	methanesulfonic	methanesulfonic	ADJ
ijpds-4231	361	6	acid	acid	NOUN
ijpds-4231	361	7	in	in	ADP
ijpds-4231	361	8	isopropyl	isopropyl	NOUN
ijpds-4231	361	9	alcohol	alcohol	NOUN
ijpds-4231	361	10	to	to	PART
ijpds-4231	361	11	isolate	isolate	VERB
ijpds-4231	361	12	1	1	NUM
ijpds-4231	361	13	(	(	PUNCT
ijpds-4231	361	14	yield	yield	NOUN
ijpds-4231	361	15	:	:	PUNCT
ijpds-4231	361	16	94.97	94.97	NUM
ijpds-4231	361	17	%	%	NOUN
ijpds-4231	361	18	,	,	PUNCT
ijpds-4231	361	19	purity	purity	NOUN
ijpds-4231	361	20	:	:	PUNCT
ijpds-4231	361	21	100	100	NUM
ijpds-4231	361	22	%	%	NOUN
ijpds-4231	361	23	,	,	PUNCT
ijpds-4231	361	24	chiral	chiral	ADJ
ijpds-4231	361	25	purity	purity	NOUN
ijpds-4231	361	26	:	:	PUNCT
ijpds-4231	361	27	100	100	NUM
ijpds-4231	361	28	%	%	NOUN
ijpds-4231	361	29	by	by	ADP
ijpds-4231	361	30	hplc	hplc	PROPN
ijpds-4231	361	31	)	)	PUNCT
ijpds-4231	361	32	.	.	PUNCT
ijpds-4231	362	1	the	the	DET
ijpds-4231	362	2	disclosed	disclose	VERB
ijpds-4231	362	3	initiative	initiative	NOUN
ijpds-4231	362	4	was	be	AUX
ijpds-4231	362	5	proved	prove	VERB
ijpds-4231	362	6	to	to	PART
ijpds-4231	362	7	be	be	AUX
ijpds-4231	362	8	an	an	DET
ijpds-4231	362	9	industrially	industrially	ADV
ijpds-4231	362	10	feasible	feasible	ADJ
ijpds-4231	362	11	process	process	NOUN
ijpds-4231	362	12	involving	involve	VERB
ijpds-4231	362	13	cyclization	cyclization	NOUN
ijpds-4231	362	14	,	,	PUNCT
ijpds-4231	362	15	reductive	reductive	ADJ
ijpds-4231	362	16	amination	amination	NOUN
ijpds-4231	362	17	,	,	PUNCT
ijpds-4231	362	18	resolution	resolution	NOUN
ijpds-4231	362	19	and	and	CCONJ
ijpds-4231	362	20	salification	salification	NOUN
ijpds-4231	362	21	using	use	VERB
ijpds-4231	362	22	the	the	DET
ijpds-4231	362	23	readily	readily	ADV
ijpds-4231	362	24	available	available	ADJ
ijpds-4231	362	25	starting	start	VERB
ijpds-4231	362	26	materials	material	NOUN
ijpds-4231	362	27	,	,	PUNCT
ijpds-4231	362	28	simple	simple	ADJ
ijpds-4231	362	29	reagents	reagent	NOUN
ijpds-4231	362	30	and	and	CCONJ
ijpds-4231	362	31	solvents	solvent	NOUN
ijpds-4231	363	1	[	[	X
ijpds-4231	363	2	73	73	NUM
ijpds-4231	363	3	]	]	PUNCT
ijpds-4231	363	4	.	.	PUNCT
ijpds-4231	364	1	57	57	NUM
ijpds-4231	364	2	s	s	NOUN
ijpds-4231	364	3	o	o	NOUN
ijpds-4231	364	4	o	o	X
ijpds-4231	364	5	nh	nh	NOUN
ijpds-4231	364	6	n	n	ADV
ijpds-4231	364	7	o	o	NOUN
ijpds-4231	365	1	o	o	X
ijpds-4231	365	2	s	s	X
ijpds-4231	365	3	o	o	X
ijpds-4231	365	4	o	o	NOUN
ijpds-4231	365	5	n	n	INTJ
ijpds-4231	365	6	no	no	INTJ
ijpds-4231	365	7	o	o	NOUN
ijpds-4231	365	8	58	58	NUM
ijpds-4231	365	9	wu	wu	NOUN
ijpds-4231	365	10	g	g	PROPN
ijpds-4231	365	11	,	,	PUNCT
ijpds-4231	365	12	et	et	PROPN
ijpds-4231	365	13	al	al	PROPN
ijpds-4231	365	14	.	.	PROPN
ijpds-4231	365	15	,	,	PUNCT
ijpds-4231	365	16	in	in	ADP
ijpds-4231	365	17	2023	2023	NUM
ijpds-4231	365	18	,	,	PUNCT
ijpds-4231	365	19	had	have	AUX
ijpds-4231	365	20	illustrated	illustrate	VERB
ijpds-4231	365	21	the	the	DET
ijpds-4231	365	22	use	use	NOUN
ijpds-4231	365	23	of	of	ADP
ijpds-4231	365	24	9	9	NUM
ijpds-4231	365	25	as	as	ADP
ijpds-4231	365	26	the	the	DET
ijpds-4231	365	27	starting	starting	NOUN
ijpds-4231	365	28	material	material	NOUN
ijpds-4231	365	29	to	to	PART
ijpds-4231	365	30	obtain	obtain	VERB
ijpds-4231	365	31	s	s	NOUN
ijpds-4231	365	32	-	-	NOUN
ijpds-4231	365	33	isomer	isomer	ADJ
ijpds-4231	365	34	of	of	ADP
ijpds-4231	365	35	13	13	NUM
ijpds-4231	365	36	(	(	PUNCT
ijpds-4231	365	37	yield	yield	NOUN
ijpds-4231	365	38	:	:	PUNCT
ijpds-4231	365	39	75.6	75.6	NUM
ijpds-4231	365	40	-	-	SYM
ijpds-4231	365	41	82	82	NUM
ijpds-4231	365	42	%	%	NOUN
ijpds-4231	365	43	,	,	PUNCT
ijpds-4231	365	44	purity	purity	NOUN
ijpds-4231	365	45	:	:	PUNCT
ijpds-4231	365	46	98.3	98.3	NUM
ijpds-4231	365	47	-	-	SYM
ijpds-4231	365	48	98.6	98.6	NUM
ijpds-4231	365	49	%	%	NOUN
ijpds-4231	365	50	by	by	ADP
ijpds-4231	365	51	hplc	hplc	NOUN
ijpds-4231	365	52	)	)	PUNCT
ijpds-4231	365	53	in	in	ADP
ijpds-4231	365	54	high	high	ADJ
ijpds-4231	365	55	purity	purity	NOUN
ijpds-4231	365	56	through	through	ADP
ijpds-4231	365	57	the	the	DET
ijpds-4231	365	58	asymmetric	asymmetric	ADJ
ijpds-4231	365	59	reduction	reduction	NOUN
ijpds-4231	365	60	of	of	ADP
ijpds-4231	365	61	a	a	DET
ijpds-4231	365	62	chiral	chiral	ADJ
ijpds-4231	365	63	auxiliary	auxiliary	NOUN
ijpds-4231	365	64	and	and	CCONJ
ijpds-4231	365	65	borane	borane	NOUN
ijpds-4231	365	66	intermediate	intermediate	NOUN
ijpds-4231	365	67	.	.	PUNCT
ijpds-4231	366	1	it	it	PRON
ijpds-4231	366	2	was	be	AUX
ijpds-4231	366	3	dissolved	dissolve	VERB
ijpds-4231	366	4	in	in	ADP
ijpds-4231	366	5	tetrahydrofuran	tetrahydrofuran	NOUN
ijpds-4231	366	6	and	and	CCONJ
ijpds-4231	366	7	treated	treat	VERB
ijpds-4231	366	8	with	with	ADP
ijpds-4231	366	9	2	2	NUM
ijpds-4231	366	10	-	-	PUNCT
ijpds-4231	366	11	nitro	nitro	NOUN
ijpds-4231	366	12	-	-	PUNCT
ijpds-4231	366	13	n-(prop-2	n-(prop-2	NUM
ijpds-4231	366	14	-	-	PUNCT
ijpds-4231	366	15	yn-1yl)benzenesulfonamide	yn-1yl)benzenesulfonamide	NUM
ijpds-4231	366	16	57	57	NUM
ijpds-4231	366	17	,	,	PUNCT
ijpds-4231	366	18	triphenylphosphine	triphenylphosphine	NOUN
ijpds-4231	366	19	and	and	CCONJ
ijpds-4231	366	20	diisopropyl	diisopropyl	NOUN
ijpds-4231	366	21	azodicarboxylate	azodicarboxylate	NOUN
ijpds-4231	366	22	under	under	ADP
ijpds-4231	366	23	the	the	DET
ijpds-4231	366	24	nitrogen	nitrogen	NOUN
ijpds-4231	366	25	atmosphere	atmosphere	NOUN
ijpds-4231	366	26	to	to	PART
ijpds-4231	366	27	isolate	isolate	VERB
ijpds-4231	366	28	n-[(1r)-2,3	n-[(1r)-2,3	ADJ
ijpds-4231	366	29	-	-	PUNCT
ijpds-4231	366	30	dihydro-1h	dihydro-1h	NOUN
ijpds-4231	366	31	-	-	PUNCT
ijpds-4231	366	32	inden-1	inden-1	NOUN
ijpds-4231	366	33	-	-	PUNCT
ijpds-4231	366	34	yl]-2	yl]-2	PROPN
ijpds-4231	366	35	-	-	PUNCT
ijpds-4231	366	36	nitro	nitro	NOUN
ijpds-4231	366	37	-	-	PUNCT
ijpds-4231	366	38	n(prop-2	n(prop-2	NOUN
ijpds-4231	366	39	-	-	PUNCT
ijpds-4231	366	40	yn-1	yn-1	NOUN
ijpds-4231	366	41	-	-	NOUN
ijpds-4231	366	42	yl)benzenesulfonamide	yl)benzenesulfonamide	NOUN
ijpds-4231	366	43	58	58	NUM
ijpds-4231	366	44	(	(	PUNCT
ijpds-4231	366	45	yield	yield	NOUN
ijpds-4231	366	46	:	:	PUNCT
ijpds-4231	366	47	81.5	81.5	NUM
ijpds-4231	366	48	-	-	SYM
ijpds-4231	366	49	85	85	NUM
ijpds-4231	366	50	%	%	NOUN
ijpds-4231	366	51	,	,	PUNCT
ijpds-4231	366	52	purity	purity	NOUN
ijpds-4231	366	53	:	:	PUNCT
ijpds-4231	366	54	98	98	NUM
ijpds-4231	366	55	-	-	SYM
ijpds-4231	366	56	98.8	98.8	NUM
ijpds-4231	366	57	%	%	NOUN
ijpds-4231	366	58	by	by	ADP
ijpds-4231	366	59	hplc	hplc	NOUN
ijpds-4231	366	60	)	)	PUNCT
ijpds-4231	366	61	.	.	PUNCT
ijpds-4231	367	1	in	in	ADP
ijpds-4231	367	2	this	this	DET
ijpds-4231	367	3	step	step	NOUN
ijpds-4231	367	4	,	,	PUNCT
ijpds-4231	367	5	a	a	DET
ijpds-4231	367	6	chiral	chiral	ADJ
ijpds-4231	367	7	amine	amine	NOUN
ijpds-4231	367	8	was	be	AUX
ijpds-4231	367	9	constructed	construct	VERB
ijpds-4231	367	10	in	in	ADP
ijpds-4231	367	11	a	a	DET
ijpds-4231	367	12	simple	simple	ADJ
ijpds-4231	367	13	pathway	pathway	NOUN
ijpds-4231	367	14	and	and	CCONJ
ijpds-4231	367	15	the	the	DET
ijpds-4231	367	16	amino	amino	NOUN
ijpds-4231	367	17	group	group	NOUN
ijpds-4231	367	18	was	be	AUX
ijpds-4231	367	19	protected	protect	VERB
ijpds-4231	367	20	by	by	ADP
ijpds-4231	367	21	the	the	DET
ijpds-4231	367	22	nitro	nitro	NOUN
ijpds-4231	367	23	sulfonyl	sulfonyl	NOUN
ijpds-4231	367	24	group	group	NOUN
ijpds-4231	367	25	.	.	PUNCT
ijpds-4231	368	1	the	the	DET
ijpds-4231	368	2	reported	report	VERB
ijpds-4231	368	3	work	work	NOUN
ijpds-4231	368	4	successfully	successfully	ADV
ijpds-4231	368	5	avoids	avoid	VERB
ijpds-4231	368	6	the	the	DET
ijpds-4231	368	7	formation	formation	NOUN
ijpds-4231	368	8	of	of	ADP
ijpds-4231	368	9	unwanted	unwanted	ADJ
ijpds-4231	368	10	polysubstituted	polysubstitute	VERB
ijpds-4231	368	11	byproducts	byproduct	NOUN
ijpds-4231	368	12	.	.	PUNCT
ijpds-4231	369	1	intermediate	intermediate	ADJ
ijpds-4231	369	2	58	58	NUM
ijpds-4231	369	3	was	be	AUX
ijpds-4231	369	4	dissolved	dissolve	VERB
ijpds-4231	369	5	in	in	ADP
ijpds-4231	369	6	dimethylformamide	dimethylformamide	NOUN
ijpds-4231	369	7	and	and	CCONJ
ijpds-4231	369	8	treated	treat	VERB
ijpds-4231	369	9	with	with	ADP
ijpds-4231	369	10	lithium	lithium	NOUN
ijpds-4231	369	11	hydroxide	hydroxide	NOUN
ijpds-4231	369	12	solution	solution	NOUN
ijpds-4231	369	13	.	.	PUNCT
ijpds-4231	370	1	to	to	ADP
ijpds-4231	370	2	the	the	DET
ijpds-4231	370	3	mixture	mixture	NOUN
ijpds-4231	370	4	,	,	PUNCT
ijpds-4231	370	5	mercaptopropionic	mercaptopropionic	ADJ
ijpds-4231	370	6	acid	acid	NOUN
ijpds-4231	370	7	in	in	ADP
ijpds-4231	370	8	dimethyl	dimethyl	PROPN
ijpds-4231	370	9	formamide	formamide	ADV
ijpds-4231	370	10	was	be	AUX
ijpds-4231	370	11	added	add	VERB
ijpds-4231	370	12	drop	drop	NOUN
ijpds-4231	370	13	-	-	PUNCT
ijpds-4231	370	14	wise	wise	ADJ
ijpds-4231	370	15	and	and	CCONJ
ijpds-4231	370	16	worked	work	VERB
ijpds-4231	370	17	-	-	PUNCT
ijpds-4231	370	18	up	up	NOUN
ijpds-4231	370	19	by	by	ADP
ijpds-4231	370	20	ph	ph	ADJ
ijpds-4231	370	21	adjustment	adjustment	NOUN
ijpds-4231	370	22	to	to	PART
ijpds-4231	370	23	obtain	obtain	VERB
ijpds-4231	370	24	r	r	NOUN
ijpds-4231	370	25	-	-	PUNCT
ijpds-4231	370	26	rasagiline	rasagiline	NOUN
ijpds-4231	370	27	base	base	NOUN
ijpds-4231	370	28	(	(	PUNCT
ijpds-4231	370	29	yield	yield	NOUN
ijpds-4231	370	30	:	:	PUNCT
ijpds-4231	370	31	92	92	NUM
ijpds-4231	370	32	%	%	NOUN
ijpds-4231	370	33	,	,	PUNCT
ijpds-4231	370	34	97.5	97.5	NUM
ijpds-4231	370	35	%	%	NOUN
ijpds-4231	370	36	by	by	ADP
ijpds-4231	370	37	hplc	hplc	NOUN
ijpds-4231	370	38	)	)	PUNCT
ijpds-4231	370	39	.	.	PUNCT
ijpds-4231	371	1	upon	upon	SCONJ
ijpds-4231	371	2	the	the	DET
ijpds-4231	371	3	use	use	NOUN
ijpds-4231	371	4	of	of	ADP
ijpds-4231	371	5	lithium	lithium	NOUN
ijpds-4231	371	6	hydroxide	hydroxide	NOUN
ijpds-4231	371	7	solution	solution	NOUN
ijpds-4231	371	8	in	in	ADP
ijpds-4231	371	9	dimethyl	dimethyl	PROPN
ijpds-4231	371	10	acetamide	acetamide	PROPN
ijpds-4231	371	11	and	and	CCONJ
ijpds-4231	371	12	mercapto	mercapto	NOUN
ijpds-4231	371	13	-	-	PUNCT
ijpds-4231	371	14	acetic	acetic	ADJ
ijpds-4231	371	15	acid	acid	NOUN
ijpds-4231	371	16	,	,	PUNCT
ijpds-4231	371	17	1	1	NUM
ijpds-4231	371	18	was	be	AUX
ijpds-4231	371	19	isolated	isolate	VERB
ijpds-4231	371	20	with	with	ADP
ijpds-4231	371	21	relatively	relatively	ADV
ijpds-4231	371	22	good	good	ADJ
ijpds-4231	371	23	purity	purity	NOUN
ijpds-4231	371	24	(	(	PUNCT
ijpds-4231	371	25	yield	yield	NOUN
ijpds-4231	371	26	:	:	PUNCT
ijpds-4231	371	27	84.4	84.4	NUM
ijpds-4231	371	28	%	%	NOUN
ijpds-4231	371	29	,	,	PUNCT
ijpds-4231	371	30	purity	purity	NOUN
ijpds-4231	371	31	:	:	PUNCT
ijpds-4231	371	32	97.1	97.1	NUM
ijpds-4231	371	33	%	%	NOUN
ijpds-4231	371	34	by	by	ADP
ijpds-4231	371	35	hplc	hplc	NOUN
ijpds-4231	371	36	)	)	PUNCT
ijpds-4231	371	37	.	.	PUNCT
ijpds-4231	372	1	in	in	ADP
ijpds-4231	372	2	another	another	DET
ijpds-4231	372	3	experiment	experiment	NOUN
ijpds-4231	372	4	,	,	PUNCT
ijpds-4231	372	5	lithiumbistrimethylsilylamide	lithiumbistrimethylsilylamide	NOUN
ijpds-4231	372	6	in	in	ADP
ijpds-4231	372	7	n	n	CCONJ
ijpds-4231	372	8	-	-	PUNCT
ijpds-4231	372	9	methyl	methyl	NOUN
ijpds-4231	372	10	pyrrolidone	pyrrolidone	NOUN
ijpds-4231	372	11	and	and	CCONJ
ijpds-4231	372	12	thioglycolic	thioglycolic	ADJ
ijpds-4231	372	13	acid	acid	NOUN
ijpds-4231	372	14	was	be	AUX
ijpds-4231	372	15	used	use	VERB
ijpds-4231	372	16	to	to	PART
ijpds-4231	372	17	isolate	isolate	VERB
ijpds-4231	372	18	1	1	NUM
ijpds-4231	372	19	in	in	ADP
ijpds-4231	372	20	reasonably	reasonably	ADV
ijpds-4231	372	21	good	good	ADJ
ijpds-4231	372	22	purity	purity	NOUN
ijpds-4231	372	23	(	(	PUNCT
ijpds-4231	372	24	yield	yield	NOUN
ijpds-4231	372	25	:	:	PUNCT
ijpds-4231	372	26	77	77	NUM
ijpds-4231	372	27	%	%	NOUN
ijpds-4231	372	28	,	,	PUNCT
ijpds-4231	372	29	purity	purity	NOUN
ijpds-4231	372	30	:	:	PUNCT
ijpds-4231	372	31	95.8	95.8	NUM
ijpds-4231	372	32	%	%	NOUN
ijpds-4231	372	33	by	by	ADP
ijpds-4231	372	34	hplc	hplc	NOUN
ijpds-4231	372	35	)	)	PUNCT
ijpds-4231	373	1	[	[	X
ijpds-4231	373	2	74	74	NUM
ijpds-4231	373	3	]	]	PUNCT
ijpds-4231	373	4	.	.	PUNCT
ijpds-4231	374	1	summary	summary	VERB
ijpds-4231	374	2	numerous	numerous	ADJ
ijpds-4231	374	3	researchers	researcher	NOUN
ijpds-4231	374	4	(	(	PUNCT
ijpds-4231	374	5	inventors	inventor	NOUN
ijpds-4231	374	6	)	)	PUNCT
ijpds-4231	374	7	associated	associate	VERB
ijpds-4231	374	8	to	to	ADP
ijpds-4231	374	9	various	various	ADJ
ijpds-4231	374	10	global	global	ADJ
ijpds-4231	374	11	organizations	organization	NOUN
ijpds-4231	374	12	(	(	PUNCT
ijpds-4231	374	13	assignees	assignee	NOUN
ijpds-4231	374	14	)	)	PUNCT
ijpds-4231	374	15	had	have	AUX
ijpds-4231	374	16	contributed	contribute	VERB
ijpds-4231	374	17	to	to	PART
ijpds-4231	374	18	commercialize	commercialize	VERB
ijpds-4231	374	19	rasagiline	rasagiline	NOUN
ijpds-4231	374	20	,	,	PUNCT
ijpds-4231	374	21	its	its	PRON
ijpds-4231	374	22	salts	salt	NOUN
ijpds-4231	374	23	and	and	CCONJ
ijpds-4231	374	24	crystallographic	crystallographic	ADJ
ijpds-4231	374	25	forms	form	NOUN
ijpds-4231	374	26	.	.	PUNCT
ijpds-4231	375	1	sanjay	sanjay	PROPN
ijpds-4231	375	2	s	s	PART
ijpds-4231	376	1	s	s	NOUN
ijpds-4231	376	2	patents	patent	NOUN
ijpds-4231	376	3	disclosed	disclose	VERB
ijpds-4231	376	4	synthetic	synthetic	ADJ
ijpds-4231	376	5	overview	overview	NOUN
ijpds-4231	376	6	of	of	ADP
ijpds-4231	376	7	rasagiline	rasagiline	ADJ
ijpds-4231	376	8	vol	vol	NOUN
ijpds-4231	376	9	2	2	NUM
ijpds-4231	376	10	|	|	ADV
ijpds-4231	376	11	issue	issue	VERB
ijpds-4231	376	12	4	4	NUM
ijpds-4231	376	13	|	|	ADV
ijpds-4231	376	14	oct	oct	PROPN
ijpds-4231	376	15	–	–	PUNCT
ijpds-4231	376	16	dec	dec	PROPN
ijpds-4231	376	17	2023	2023	NUM
ijpds-4231	376	18	indian	indian	PROPN
ijpds-4231	376	19	j	j	PROPN
ijpds-4231	376	20	pharm	pharm	PROPN
ijpds-4231	376	21	drug	drug	PROPN
ijpds-4231	376	22	studies	study	NOUN
ijpds-4231	376	23	|	|	ADV
ijpds-4231	376	24	143	143	NUM
ijpds-4231	376	25	the	the	DET
ijpds-4231	376	26	information	information	NOUN
ijpds-4231	376	27	regarding	regard	VERB
ijpds-4231	376	28	the	the	DET
ijpds-4231	376	29	assignee	assignee	NOUN
ijpds-4231	376	30	of	of	ADP
ijpds-4231	376	31	all	all	DET
ijpds-4231	376	32	the	the	DET
ijpds-4231	376	33	disclosures	disclosure	NOUN
ijpds-4231	376	34	till	till	SCONJ
ijpds-4231	376	35	date	date	NOUN
ijpds-4231	376	36	was	be	AUX
ijpds-4231	376	37	revealed	reveal	VERB
ijpds-4231	376	38	in	in	ADP
ijpds-4231	376	39	table	table	NOUN
ijpds-4231	376	40	1	1	NUM
ijpds-4231	376	41	.	.	PUNCT
ijpds-4231	376	42	to	to	ADP
ijpds-4231	376	43	the	the	DET
ijpds-4231	376	44	context	context	NOUN
ijpds-4231	376	45	,	,	PUNCT
ijpds-4231	376	46	“	"	PUNCT
ijpds-4231	376	47	teva	teva	ADJ
ijpds-4231	376	48	pharma	pharma	PROPN
ijpds-4231	376	49	”	"	PUNCT
ijpds-4231	376	50	leads	lead	VERB
ijpds-4231	376	51	under	under	ADP
ijpds-4231	376	52	the	the	DET
ijpds-4231	376	53	category	category	NOUN
ijpds-4231	376	54	of	of	ADP
ijpds-4231	376	55	publication	publication	NOUN
ijpds-4231	376	56	of	of	ADP
ijpds-4231	376	57	patents	patent	NOUN
ijpds-4231	376	58	on	on	ADP
ijpds-4231	376	59	various	various	ADJ
ijpds-4231	376	60	aspects	aspect	NOUN
ijpds-4231	376	61	of	of	ADP
ijpds-4231	376	62	rasagiline	rasagiline	NOUN
ijpds-4231	376	63	and	and	CCONJ
ijpds-4231	376	64	its	its	PRON
ijpds-4231	376	65	close	close	ADJ
ijpds-4231	376	66	related	relate	VERB
ijpds-4231	376	67	compounds	compound	NOUN
ijpds-4231	376	68	.	.	PUNCT
ijpds-4231	377	1	table	table	NOUN
ijpds-4231	377	2	1	1	NUM
ijpds-4231	377	3	.	.	X
ijpds-4231	377	4	list	list	NOUN
ijpds-4231	377	5	of	of	ADP
ijpds-4231	377	6	organizations	organization	NOUN
ijpds-4231	377	7	/	/	SYM
ijpds-4231	377	8	institutions	institution	NOUN
ijpds-4231	377	9	behind	behind	ADP
ijpds-4231	377	10	the	the	DET
ijpds-4231	377	11	disclosed	disclose	VERB
ijpds-4231	377	12	work	work	NOUN
ijpds-4231	377	13	(	(	PUNCT
ijpds-4231	377	14	patent	patent	NOUN
ijpds-4231	377	15	/	/	SYM
ijpds-4231	377	16	s	s	VERB
ijpds-4231	377	17	applied	apply	VERB
ijpds-4231	377	18	by	by	ADP
ijpds-4231	377	19	/	/	SYM
ijpds-4231	377	20	assignee	assignee	NOUN
ijpds-4231	377	21	)	)	PUNCT
ijpds-4231	377	22	ref	ref	NOUN
ijpds-4231	377	23	.	.	PUNCT
ijpds-4231	378	1	no	no	INTJ
ijpds-4231	378	2	.	.	PUNCT
ijpds-4231	379	1	patent	patent	NOUN
ijpds-4231	379	2	no	no	PROPN
ijpds-4231	379	3	.	.	PUNCT
ijpds-4231	380	1	applicant	applicant	PROPN
ijpds-4231	380	2	/	/	SYM
ijpds-4231	380	3	s	s	PART
ijpds-4231	380	4	or	or	CCONJ
ijpds-4231	380	5	assignee	assignee	NOUN
ijpds-4231	380	6	organization	organization	NOUN
ijpds-4231	380	7	/	/	SYM
ijpds-4231	380	8	s	s	PART
ijpds-4231	381	1	[	[	X
ijpds-4231	381	2	4	4	NUM
ijpds-4231	381	3	]	]	PUNCT
ijpds-4231	381	4	,	,	PUNCT
ijpds-4231	382	1	[	[	X
ijpds-4231	382	2	7	7	NUM
ijpds-4231	382	3	]	]	PUNCT
ijpds-4231	382	4	.	.	PUNCT
ijpds-4231	383	1	us3513244a	us3513244a	ADJ
ijpds-4231	383	2	de1443403a1	de1443403a1	PROPN
ijpds-4231	383	3	aspro	aspro	ADJ
ijpds-4231	383	4	nicholas	nicholas	PROPN
ijpds-4231	383	5	ltd	ltd	PROPN
ijpds-4231	384	1	[	[	X
ijpds-4231	384	2	5	5	NUM
ijpds-4231	384	3	]	]	PUNCT
ijpds-4231	384	4	,	,	PUNCT
ijpds-4231	384	5	[	[	X
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ijpds-4231	384	8	,	,	PUNCT
ijpds-4231	384	9	[	[	X
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ijpds-4231	384	11	]	]	PUNCT
ijpds-4231	384	12	,	,	PUNCT
ijpds-4231	384	13	[	[	X
ijpds-4231	384	14	10	10	NUM
ijpds-4231	384	15	]	]	PUNCT
ijpds-4231	384	16	.	.	PUNCT
ijpds-4231	385	1	us5453446a	us5453446a	PROPN
ijpds-4231	385	2	,	,	PUNCT
ijpds-4231	385	3	ep0436492a2	ep0436492a2	PROPN
ijpds-4231	385	4	,	,	PUNCT
ijpds-4231	385	5	wo9511016a1	wo9511016a1	PROPN
ijpds-4231	385	6	,	,	PUNCT
ijpds-4231	385	7	us5532415a	us5532415a	PROPN
ijpds-4231	385	8	teva	teva	PROPN
ijpds-4231	385	9	pharma	pharma	PROPN
ijpds-4231	385	10	[	[	X
ijpds-4231	385	11	il	il	PROPN
ijpds-4231	385	12	]	]	X
ijpds-4231	385	13	;	;	PUNCT
ijpds-4231	385	14	technion	technion	PROPN
ijpds-4231	385	15	res	res	PROPN
ijpds-4231	385	16	&	&	CCONJ
ijpds-4231	385	17	dev	dev	PROPN
ijpds-4231	385	18	foundation	foundation	PROPN
ijpds-4231	386	1	[	[	X
ijpds-4231	386	2	il	il	X
ijpds-4231	386	3	]	]	X
ijpds-4231	387	1	[	[	X
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ijpds-4231	387	3	]	]	PUNCT
ijpds-4231	387	4	.	.	PUNCT
ijpds-4231	388	1	us3253037a	us3253037a	PROPN
ijpds-4231	389	1	ciba	ciba	PROPN
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ijpds-4231	389	3	corp	corp	PROPN
ijpds-4231	390	1	[	[	X
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ijpds-4231	390	3	]	]	PUNCT
ijpds-4231	390	4	.	.	PUNCT
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ijpds-4231	392	1	[	[	X
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ijpds-4231	393	1	[	[	X
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ijpds-4231	393	3	]	]	PUNCT
ijpds-4231	393	4	.	.	PUNCT
ijpds-4231	394	1	wo02068376a1	wo02068376a1	VERB
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ijpds-4231	395	1	[	[	X
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ijpds-4231	395	3	]	]	X
ijpds-4231	396	1	[	[	X
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ijpds-4231	396	3	]	]	PUNCT
ijpds-4231	396	4	,	,	PUNCT
ijpds-4231	396	5	[	[	X
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ijpds-4231	396	8	,	,	PUNCT
ijpds-4231	396	9	[	[	X
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ijpds-4231	396	12	,	,	PUNCT
ijpds-4231	396	13	[	[	X
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ijpds-4231	396	16	,	,	PUNCT
ijpds-4231	396	17	[	[	X
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ijpds-4231	396	20	,	,	PUNCT
ijpds-4231	396	21	[	[	X
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ijpds-4231	396	24	,	,	PUNCT
ijpds-4231	397	1	[	[	X
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ijpds-4231	397	3	]	]	PUNCT
ijpds-4231	397	4	.	.	PUNCT
ijpds-4231	398	1	us	us	PROPN
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ijpds-4231	398	3	,	,	PUNCT
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ijpds-4231	398	5	,	,	PUNCT
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ijpds-4231	398	7	,	,	PUNCT
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ijpds-4231	398	9	,	,	PUNCT
ijpds-4231	398	10	us	us	PROPN
ijpds-4231	398	11	7547806b2	7547806b2	NOUN
ijpds-4231	398	12	,	,	PUNCT
ijpds-4231	398	13	us7855233b2	us7855233b2	X
ijpds-4231	398	14	ep2939669a1	ep2939669a1	ADJ
ijpds-4231	398	15	teva	teva	ADJ
ijpds-4231	398	16	pharma	pharma	PROPN
ijpds-4231	399	1	[	[	X
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ijpds-4231	400	1	[	[	X
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ijpds-4231	400	3	]	]	PUNCT
ijpds-4231	400	4	.	.	PUNCT
ijpds-4231	401	1	cn101062897a	cn101062897a	AUX
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ijpds-4231	402	1	[	[	X
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ijpds-4231	403	1	[	[	X
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ijpds-4231	403	3	]	]	PUNCT
ijpds-4231	403	4	.	.	PUNCT
ijpds-4231	404	1	cn1990455a	cn1990455a	ADP
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ijpds-4231	404	3	d	d	PROPN
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ijpds-4231	404	5	pharm	pharm	NOUN
ijpds-4231	404	6	tech	tech	NOUN
ijpds-4231	405	1	[	[	X
ijpds-4231	405	2	cn	cn	X
ijpds-4231	405	3	]	]	X
ijpds-4231	406	1	[	[	X
ijpds-4231	406	2	18	18	NUM
ijpds-4231	406	3	]	]	PUNCT
ijpds-4231	406	4	.	.	PUNCT
ijpds-4231	407	1	cn101260048a	cn101260048a	PROPN
ijpds-4231	407	2	suzhou	suzhou	PROPN
ijpds-4231	407	3	chireach	chireach	PROPN
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ijpds-4231	407	5	tec	tec	NOUN
ijpds-4231	408	1	[	[	X
ijpds-4231	408	2	cn	cn	X
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ijpds-4231	408	4	[	[	X
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ijpds-4231	408	6	]	]	PUNCT
ijpds-4231	408	7	,	,	PUNCT
ijpds-4231	408	8	[	[	X
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ijpds-4231	408	11	,	,	PUNCT
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ijpds-4231	409	1	us2009292141a1	us2009292141a1	PROPN
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ijpds-4231	409	3	wo2009118657a2	wo2009118657a2	VERB
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ijpds-4231	409	5	medichem	medichem	NOUN
ijpds-4231	409	6	sa	sa	PROPN
ijpds-4231	410	1	[	[	X
ijpds-4231	410	2	es	es	X
ijpds-4231	410	3	]	]	X
ijpds-4231	410	4	[	[	X
ijpds-4231	410	5	21	21	NUM
ijpds-4231	410	6	]	]	PUNCT
ijpds-4231	410	7	,	,	PUNCT
ijpds-4231	411	1	[	[	X
ijpds-4231	411	2	22	22	NUM
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ijpds-4231	411	4	,	,	PUNCT
ijpds-4231	411	5	[	[	X
ijpds-4231	411	6	53	53	NUM
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ijpds-4231	411	8	,	,	PUNCT
ijpds-4231	411	9	[	[	X
ijpds-4231	411	10	58	58	NUM
ijpds-4231	411	11	]	]	PUNCT
ijpds-4231	411	12	,	,	PUNCT
ijpds-4231	411	13	[	[	X
ijpds-4231	411	14	59	59	NUM
ijpds-4231	411	15	]	]	PUNCT
ijpds-4231	411	16	.	.	PUNCT
ijpds-4231	412	1	wo2009154777a	wo2009154777a	PROPN
ijpds-4231	412	2	,	,	PUNCT
ijpds-4231	412	3	wo2009154782a1	wo2009154782a1	PROPN
ijpds-4231	412	4	,	,	PUNCT
ijpds-4231	412	5	wo2012058219a2	wo2012058219a2	X
ijpds-4231	412	6	,	,	PUNCT
ijpds-4231	412	7	wo2012058219a2	wo2012058219a2	SCONJ
ijpds-4231	412	8	wo2013055684a1	wo2013055684a1	PROPN
ijpds-4231	412	9	teva	teva	PROPN
ijpds-4231	412	10	pharma	pharma	PROPN
ijpds-4231	412	11	[	[	X
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ijpds-4231	412	13	]	]	X
ijpds-4231	412	14	;	;	PUNCT
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ijpds-4231	412	16	pharma	pharma	PROPN
ijpds-4231	413	1	[	[	X
ijpds-4231	413	2	us	we	PRON
ijpds-4231	413	3	]	]	X
ijpds-4231	413	4	[	[	X
ijpds-4231	413	5	23	23	NUM
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ijpds-4231	413	7	.	.	PUNCT
ijpds-4231	414	1	ca2723869a1	ca2723869a1	PROPN
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ijpds-4231	414	3	uk	uk	PROPN
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ijpds-4231	415	1	[	[	X
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ijpds-4231	416	4	.	.	PUNCT
ijpds-4231	417	1	ep0235590a2	ep0235590a2	PROPN
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ijpds-4231	417	3	lambert	lambert	PROPN
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ijpds-4231	418	2	us	we	PRON
ijpds-4231	418	3	]	]	X
ijpds-4231	419	1	[	[	X
ijpds-4231	419	2	26	26	NUM
ijpds-4231	419	3	]	]	PUNCT
ijpds-4231	419	4	.	.	PUNCT
ijpds-4231	420	1	cn101486655a	cn101486655a	PROPN
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ijpds-4231	420	3	jiangxi	jiangxi	PROPN
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ijpds-4231	420	5	co	co	NOUN
ijpds-4231	421	1	[	[	X
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ijpds-4231	422	1	[	[	X
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ijpds-4231	422	3	]	]	PUNCT
ijpds-4231	422	4	,	,	PUNCT
ijpds-4231	422	5	[	[	X
ijpds-4231	422	6	39	39	NUM
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ijpds-4231	422	8	.	.	PUNCT
ijpds-4231	423	1	wo2009122301a2	wo2009122301a2	NOUN
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ijpds-4231	423	3	actavis	actavis	PROPN
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ijpds-4231	423	5	ptc	ptc	PROPN
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ijpds-4231	424	1	[	[	X
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ijpds-4231	424	3	]	]	PUNCT
ijpds-4231	424	4	[	[	X
ijpds-4231	424	5	29	29	NUM
ijpds-4231	424	6	]	]	PUNCT
ijpds-4231	424	7	.	.	PUNCT
ijpds-4231	425	1	cn101381314a	cn101381314a	PROPN
ijpds-4231	426	1	chengdu	chengdu	PROPN
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ijpds-4231	426	3	pharmaceuticals	pharmaceuticals	PROPN
ijpds-4231	427	1	[	[	X
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ijpds-4231	427	3	]	]	X
ijpds-4231	428	1	[	[	X
ijpds-4231	428	2	30	30	NUM
ijpds-4231	428	3	]	]	PUNCT
ijpds-4231	428	4	.	.	PUNCT
ijpds-4231	429	1	cn101486655a	cn101486655a	PROPN
ijpds-4231	429	2	meide	meide	PROPN
ijpds-4231	429	3	jiangxi	jiangxi	PROPN
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ijpds-4231	430	1	[	[	X
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ijpds-4231	430	7	.	.	PUNCT
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ijpds-4231	432	4	;	;	PUNCT
ijpds-4231	432	5	dr	dr	PROPN
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ijpds-4231	432	8	lab	lab	PROPN
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ijpds-4231	433	1	[	[	X
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ijpds-4231	434	4	.	.	PUNCT
ijpds-4231	435	1	wo2010049379a1	wo2010049379a1	PROPN
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ijpds-4231	435	4	sa	sa	PROPN
ijpds-4231	436	1	[	[	X
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ijpds-4231	437	1	[	[	X
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ijpds-4231	437	3	]	]	PUNCT
ijpds-4231	437	4	.	.	PUNCT
ijpds-4231	438	1	us2010029987a1	us2010029987a1	PROPN
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ijpds-4231	440	1	[	[	X
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ijpds-4231	443	4	[	[	X
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ijpds-4231	443	7	,	,	PUNCT
ijpds-4231	443	8	[	[	X
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ijpds-4231	443	11	.	.	PUNCT
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ijpds-4231	444	8	[	[	X
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ijpds-4231	444	11	.	.	PUNCT
ijpds-4231	445	1	cn102010353a	cn102010353a	PROPN
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ijpds-4231	445	7	ltd	ltd	PROPN
ijpds-4231	445	8	[	[	X
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ijpds-4231	445	10	]	]	PUNCT
ijpds-4231	445	11	.	.	PUNCT
ijpds-4231	446	1	us2011218361a1	us2011218361a1	PROPN
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ijpds-4231	447	1	[	[	X
ijpds-4231	447	2	us	we	PRON
ijpds-4231	447	3	]	]	X
ijpds-4231	448	1	[	[	X
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ijpds-4231	448	3	]	]	PUNCT
ijpds-4231	448	4	.	.	PUNCT
ijpds-4231	449	1	cn102203053a	cn102203053a	PROPN
ijpds-4231	449	2	generics	generics	PROPN
ijpds-4231	449	3	uk	uk	PROPN
ijpds-4231	449	4	ltd	ltd	PROPN
ijpds-4231	450	1	[	[	X
ijpds-4231	450	2	43	43	NUM
ijpds-4231	450	3	]	]	PUNCT
ijpds-4231	450	4	,	,	PUNCT
ijpds-4231	450	5	[	[	X
ijpds-4231	450	6	45	45	NUM
ijpds-4231	450	7	]	]	PUNCT
ijpds-4231	450	8	.	.	PUNCT
ijpds-4231	451	1	wo2011048612a2	wo2011048612a2	ADJ
ijpds-4231	451	2	,	,	PUNCT
ijpds-4231	451	3	wo2011095985a2	wo2011095985a2	ADV
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ijpds-4231	451	5	generics	generics	PROPN
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ijpds-4231	452	1	[	[	X
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ijpds-4231	452	3	]	]	X
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ijpds-4231	452	7	.	.	PUNCT
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ijpds-4231	454	7	.	.	PUNCT
ijpds-4231	455	1	cn102154432a	cn102154432a	PROPN
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ijpds-4231	456	1	bbca	bbca	PROPN
ijpds-4231	456	2	medicine	medicine	PROPN
ijpds-4231	456	3	science	science	PROPN
ijpds-4231	456	4	dev	dev	PROPN
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ijpds-4231	456	6	ltd	ltd	PROPN
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ijpds-4231	457	8	.	.	PUNCT
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ijpds-4231	460	4	.	.	PUNCT
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ijpds-4231	462	1	[	[	X
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ijpds-4231	463	1	[	[	X
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ijpds-4231	463	4	,	,	PUNCT
ijpds-4231	463	5	[	[	X
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ijpds-4231	463	8	,	,	PUNCT
ijpds-4231	463	9	[	[	X
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ijpds-4231	463	12	.	.	PUNCT
ijpds-4231	464	1	wo2011012140a2	wo2011012140a2	NOUN
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ijpds-4231	465	4	[	[	X
ijpds-4231	465	5	51	51	NUM
ijpds-4231	465	6	]	]	PUNCT
ijpds-4231	465	7	.	.	PUNCT
ijpds-4231	466	1	cn102464589a	cn102464589a	ADP
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ijpds-4231	467	4	.	.	PUNCT
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ijpds-4231	472	8	.	.	PUNCT
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ijpds-4231	474	3	]	]	X
ijpds-4231	475	1	[	[	X
ijpds-4231	475	2	52	52	NUM
ijpds-4231	475	3	]	]	PUNCT
ijpds-4231	475	4	.	.	PUNCT
ijpds-4231	476	1	cn102786422a	cn102786422a	PROPN
ijpds-4231	476	2	topharman	topharman	ADJ
ijpds-4231	476	3	shanghai	shanghai	PROPN
ijpds-4231	476	4	co	co	PROPN
ijpds-4231	476	5	ltd	ltd	PROPN
ijpds-4231	476	6	;	;	PUNCT
ijpds-4231	476	7	shanghai	shanghai	PROPN
ijpds-4231	476	8	inst	inst	PROPN
ijpds-4231	476	9	materia	materia	PROPN
ijpds-4231	476	10	medica	medica	PROPN
ijpds-4231	476	11	;	;	PUNCT
ijpds-4231	476	12	shandong	shandong	PROPN
ijpds-4231	476	13	topharman	topharman	PROPN
ijpds-4231	476	14	medical	medical	ADJ
ijpds-4231	476	15	raw	raw	ADJ
ijpds-4231	476	16	material	material	NOUN
ijpds-4231	476	17	co	co	X
ijpds-4231	476	18	ltd	ltd	PROPN
ijpds-4231	477	1	[	[	X
ijpds-4231	477	2	61	61	NUM
ijpds-4231	477	3	]	]	PUNCT
ijpds-4231	477	4	.	.	PUNCT
ijpds-4231	478	1	ep2610239a1	ep2610239a1	PROPN
ijpds-4231	478	2	dr	dr	PROPN
ijpds-4231	478	3	.	.	PROPN
ijpds-4231	478	4	reddys	reddys	PROPN
ijpds-4231	478	5	lab	lab	PROPN
ijpds-4231	478	6	ltd	ltd	PROPN
ijpds-4231	479	1	[	[	X
ijpds-4231	479	2	in	in	ADP
ijpds-4231	479	3	]	]	X
ijpds-4231	480	1	[	[	X
ijpds-4231	480	2	62	62	NUM
ijpds-4231	480	3	]	]	PUNCT
ijpds-4231	480	4	,	,	PUNCT
ijpds-4231	480	5	[	[	X
ijpds-4231	480	6	63	63	NUM
ijpds-4231	480	7	]	]	PUNCT
ijpds-4231	480	8	.	.	PUNCT
ijpds-4231	481	1	cn103804200a	cn103804200a	PROPN
ijpds-4231	481	2	,	,	PUNCT
ijpds-4231	481	3	cn103864646a	cn103864646a	PUNCT
ijpds-4231	482	1	changzhou	changzhou	PROPN
ijpds-4231	482	2	no	no	DET
ijpds-4231	482	3	4	4	NUM
ijpds-4231	482	4	pharmaceutical	pharmaceutical	NOUN
ijpds-4231	482	5	factory	factory	NOUN
ijpds-4231	482	6	co	co	PROPN
ijpds-4231	482	7	ltd	ltd	PROPN
ijpds-4231	483	1	[	[	X
ijpds-4231	483	2	64	64	NUM
ijpds-4231	483	3	]	]	PUNCT
ijpds-4231	483	4	,	,	PUNCT
ijpds-4231	484	1	[	[	X
ijpds-4231	484	2	65	65	NUM
ijpds-4231	484	3	]	]	PUNCT
ijpds-4231	484	4	.	.	PUNCT
ijpds-4231	485	1	wo2015070995a	wo2015070995a	PROPN
ijpds-4231	485	2	,	,	PUNCT
ijpds-4231	485	3	wo2016116607a1	wo2016116607a1	PROPN
ijpds-4231	485	4	farma	farma	PROPN
ijpds-4231	485	5	grs	grs	PROPN
ijpds-4231	486	1	d	d	NOUN
ijpds-4231	486	2	o	o	X
ijpds-4231	487	1	o	o	X
ijpds-4231	488	1	[	[	X
ijpds-4231	488	2	si	si	X
ijpds-4231	488	3	]	]	X
ijpds-4231	488	4	[	[	X
ijpds-4231	488	5	67	67	NUM
ijpds-4231	488	6	]	]	PUNCT
ijpds-4231	488	7	.	.	PUNCT
ijpds-4231	489	1	cn109180499a	cn109180499a	PROPN
ijpds-4231	489	2	shanghai	shanghai	PROPN
ijpds-4231	489	3	bocimed	bocime	VERB
ijpds-4231	489	4	pharmaceutical	pharmaceutical	PROPN
ijpds-4231	489	5	co	co	PROPN
ijpds-4231	489	6	ltd	ltd	PROPN
ijpds-4231	490	1	[	[	X
ijpds-4231	490	2	68	68	NUM
ijpds-4231	490	3	]	]	PUNCT
ijpds-4231	490	4	.	.	PUNCT
ijpds-4231	491	1	cn110776429a	cn110776429a	VERB
ijpds-4231	492	1	qilu	qilu	VERB
ijpds-4231	492	2	pharmaceutical	pharmaceutical	PROPN
ijpds-4231	492	3	co	co	PROPN
ijpds-4231	492	4	ltd	ltd	PROPN
ijpds-4231	493	1	[	[	X
ijpds-4231	493	2	69	69	NUM
ijpds-4231	493	3	]	]	PUNCT
ijpds-4231	493	4	,	,	PUNCT
ijpds-4231	494	1	[	[	X
ijpds-4231	494	2	70	70	NUM
ijpds-4231	494	3	]	]	PUNCT
ijpds-4231	494	4	,	,	PUNCT
ijpds-4231	494	5	[	[	X
ijpds-4231	494	6	71	71	NUM
ijpds-4231	494	7	]	]	PUNCT
ijpds-4231	494	8	.	.	PUNCT
ijpds-4231	495	1	cn111333517a	cn111333517a	PROPN
ijpds-4231	495	2	,	,	PUNCT
ijpds-4231	495	3	cn113030283a	cn113030283a	PROPN
ijpds-4231	495	4	,	,	PUNCT
ijpds-4231	495	5	cn113045456a	cn113045456a	PROPN
ijpds-4231	495	6	shanghai	shanghai	PROPN
ijpds-4231	495	7	aobo	aobo	PROPN
ijpds-4231	495	8	pharmtech	pharmtech	PROPN
ijpds-4231	495	9	inc	inc	PROPN
ijpds-4231	495	10	ltd	ltd	PROPN
ijpds-4231	495	11	;	;	PUNCT
ijpds-4231	495	12	zhejiang	zhejiang	PROPN
ijpds-4231	495	13	huahai	huahai	PROPN
ijpds-4231	495	14	pharm	pharm	PROPN
ijpds-4231	495	15	co	co	PROPN
ijpds-4231	495	16	ltd	ltd	PROPN
ijpds-4231	496	1	[	[	X
ijpds-4231	496	2	72	72	NUM
ijpds-4231	496	3	]	]	PUNCT
ijpds-4231	496	4	.	.	PUNCT
ijpds-4231	497	1	cn114438531a	cn114438531a	PROPN
ijpds-4231	497	2	univ	univ	PROPN
ijpds-4231	497	3	hunan	hunan	PROPN
ijpds-4231	498	1	[	[	X
ijpds-4231	498	2	73	73	NUM
ijpds-4231	498	3	]	]	PUNCT
ijpds-4231	498	4	.	.	PUNCT
ijpds-4231	499	1	cn115838333a	cn115838333a	PROPN
ijpds-4231	499	2	jiangsu	jiangsu	PROPN
ijpds-4231	499	3	szyy	szyy	PROPN
ijpds-4231	499	4	pharmaceutical	pharmaceutical	PROPN
ijpds-4231	499	5	res	res	PROPN
ijpds-4231	499	6	institute	institute	PROPN
ijpds-4231	499	7	co	co	PROPN
ijpds-4231	499	8	ltd	ltd	PROPN
ijpds-4231	500	1	[	[	X
ijpds-4231	500	2	74	74	NUM
ijpds-4231	500	3	]	]	PUNCT
ijpds-4231	500	4	.	.	PUNCT
ijpds-4231	501	1	cn115947675a	cn115947675a	PROPN
ijpds-4231	501	2	boji	boji	NOUN
ijpds-4231	501	3	medical	medical	ADJ
ijpds-4231	501	4	technology	technology	PROPN
ijpds-4231	501	5	co	co	PROPN
ijpds-4231	501	6	ltd	ltd	PROPN
ijpds-4231	501	7	conclusion	conclusion	NOUN
ijpds-4231	501	8	this	this	DET
ijpds-4231	501	9	work	work	NOUN
ijpds-4231	501	10	was	be	AUX
ijpds-4231	501	11	primarily	primarily	ADV
ijpds-4231	501	12	aimed	aim	VERB
ijpds-4231	501	13	to	to	PART
ijpds-4231	501	14	cover	cover	VERB
ijpds-4231	501	15	the	the	DET
ijpds-4231	501	16	disclosures	disclosure	NOUN
ijpds-4231	501	17	in	in	ADP
ijpds-4231	501	18	prior	prior	ADJ
ijpds-4231	501	19	patents	patent	NOUN
ijpds-4231	501	20	for	for	ADP
ijpds-4231	501	21	the	the	DET
ijpds-4231	501	22	synthetic	synthetic	ADJ
ijpds-4231	501	23	approaches	approach	NOUN
ijpds-4231	501	24	on	on	ADP
ijpds-4231	501	25	rasagiline	rasagiline	NOUN
ijpds-4231	501	26	,	,	PUNCT
ijpds-4231	501	27	its	its	PRON
ijpds-4231	501	28	salts	salt	NOUN
ijpds-4231	501	29	(	(	PUNCT
ijpds-4231	501	30	in	in	ADP
ijpds-4231	501	31	crystalline	crystalline	NOUN
ijpds-4231	501	32	or	or	CCONJ
ijpds-4231	501	33	amorphous	amorphous	ADJ
ijpds-4231	501	34	forms	form	NOUN
ijpds-4231	501	35	)	)	PUNCT
ijpds-4231	501	36	and	and	CCONJ
ijpds-4231	501	37	a	a	DET
ijpds-4231	501	38	few	few	ADJ
ijpds-4231	501	39	impurities	impurity	NOUN
ijpds-4231	501	40	.	.	PUNCT
ijpds-4231	502	1	numerous	numerous	ADJ
ijpds-4231	502	2	patents	patent	NOUN
ijpds-4231	502	3	were	be	AUX
ijpds-4231	502	4	published	publish	VERB
ijpds-4231	502	5	at	at	ADP
ijpds-4231	502	6	various	various	ADJ
ijpds-4231	502	7	patent	patent	NOUN
ijpds-4231	502	8	trademark	trademark	NOUN
ijpds-4231	502	9	offices	office	NOUN
ijpds-4231	502	10	over	over	ADP
ijpds-4231	502	11	the	the	DET
ijpds-4231	502	12	years	year	NOUN
ijpds-4231	502	13	covering	cover	VERB
ijpds-4231	502	14	many	many	ADJ
ijpds-4231	502	15	aspects	aspect	NOUN
ijpds-4231	502	16	of	of	ADP
ijpds-4231	502	17	the	the	DET
ijpds-4231	502	18	drug	drug	NOUN
ijpds-4231	502	19	,	,	PUNCT
ijpds-4231	502	20	rasagiline	rasagiline	NOUN
ijpds-4231	502	21	.	.	PUNCT
ijpds-4231	503	1	to	to	ADP
ijpds-4231	503	2	the	the	DET
ijpds-4231	503	3	context	context	NOUN
ijpds-4231	503	4	,	,	PUNCT
ijpds-4231	503	5	the	the	DET
ijpds-4231	503	6	patents	patent	NOUN
ijpds-4231	503	7	with	with	ADP
ijpds-4231	503	8	attempts	attempt	NOUN
ijpds-4231	503	9	/	/	SYM
ijpds-4231	503	10	explorings	exploring	NOUN
ijpds-4231	503	11	on	on	ADP
ijpds-4231	503	12	the	the	DET
ijpds-4231	503	13	synthesis	synthesis	NOUN
ijpds-4231	503	14	,	,	PUNCT
ijpds-4231	503	15	impurity	impurity	NOUN
ijpds-4231	503	16	profiling	profiling	NOUN
ijpds-4231	503	17	,	,	PUNCT
ijpds-4231	503	18	salt	salt	NOUN
ijpds-4231	503	19	formation	formation	NOUN
ijpds-4231	503	20	(	(	PUNCT
ijpds-4231	503	21	in	in	ADP
ijpds-4231	503	22	crystalline	crystalline	NOUN
ijpds-4231	503	23	or	or	CCONJ
ijpds-4231	503	24	amorphous	amorphous	ADJ
ijpds-4231	503	25	form	form	NOUN
ijpds-4231	503	26	)	)	PUNCT
ijpds-4231	503	27	of	of	ADP
ijpds-4231	503	28	rasagiline	rasagiline	NOUN
ijpds-4231	503	29	were	be	AUX
ijpds-4231	503	30	considered	consider	VERB
ijpds-4231	503	31	,	,	PUNCT
ijpds-4231	503	32	as	as	SCONJ
ijpds-4231	503	33	retrieved	retrieve	VERB
ijpds-4231	503	34	from	from	ADP
ijpds-4231	503	35	the	the	DET
ijpds-4231	503	36	web	web	NOUN
ijpds-4231	503	37	search	search	NOUN
ijpds-4231	503	38	tools	tool	NOUN
ijpds-4231	503	39	/	/	SYM
ijpds-4231	503	40	databases	database	NOUN
ijpds-4231	503	41	like	like	ADP
ijpds-4231	503	42	google	google	PROPN
ijpds-4231	503	43	patents	patent	NOUN
ijpds-4231	503	44	,	,	PUNCT
ijpds-4231	503	45	uspto	uspto	PROPN
ijpds-4231	503	46	(	(	PUNCT
ijpds-4231	503	47	united	united	PROPN
ijpds-4231	503	48	states	states	PROPN
ijpds-4231	503	49	patent	patent	PROPN
ijpds-4231	503	50	and	and	CCONJ
ijpds-4231	503	51	trademark	trademark	NOUN
ijpds-4231	503	52	office	office	NOUN
ijpds-4231	503	53	)	)	PUNCT
ijpds-4231	503	54	and	and	CCONJ
ijpds-4231	503	55	espacenet	espacenet	NOUN
ijpds-4231	503	56	(	(	PUNCT
ijpds-4231	503	57	european	european	PROPN
ijpds-4231	503	58	patent	patent	NOUN
ijpds-4231	503	59	office	office	PROPN
ijpds-4231	503	60	)	)	PUNCT
ijpds-4231	503	61	.	.	PUNCT
ijpds-4231	504	1	this	this	DET
ijpds-4231	504	2	review	review	NOUN
ijpds-4231	504	3	work	work	NOUN
ijpds-4231	504	4	provides	provide	VERB
ijpds-4231	504	5	the	the	DET
ijpds-4231	504	6	essential	essential	ADJ
ijpds-4231	504	7	information	information	NOUN
ijpds-4231	504	8	regarding	regard	VERB
ijpds-4231	504	9	the	the	DET
ijpds-4231	504	10	key	key	ADJ
ijpds-4231	504	11	starting	starting	NOUN
ijpds-4231	504	12	material	material	NOUN
ijpds-4231	504	13	/	/	SYM
ijpds-4231	504	14	s	s	NOUN
ijpds-4231	504	15	,	,	PUNCT
ijpds-4231	504	16	reagents	reagent	NOUN
ijpds-4231	504	17	and	and	CCONJ
ijpds-4231	504	18	solvents	solvent	NOUN
ijpds-4231	504	19	employed	employ	VERB
ijpds-4231	504	20	to	to	PART
ijpds-4231	504	21	obtain	obtain	VERB
ijpds-4231	504	22	rasagiline	rasagiline	NOUN
ijpds-4231	504	23	and	and	CCONJ
ijpds-4231	504	24	its	its	PRON
ijpds-4231	504	25	salts	salt	NOUN
ijpds-4231	504	26	.	.	PUNCT
ijpds-4231	505	1	the	the	DET
ijpds-4231	505	2	present	present	ADJ
ijpds-4231	505	3	review	review	NOUN
ijpds-4231	505	4	initiative	initiative	NOUN
ijpds-4231	505	5	can	can	AUX
ijpds-4231	505	6	assist	assist	VERB
ijpds-4231	505	7	global	global	ADJ
ijpds-4231	505	8	researchers	researcher	NOUN
ijpds-4231	505	9	to	to	PART
ijpds-4231	505	10	venture	venture	VERB
ijpds-4231	505	11	further	far	ADV
ijpds-4231	505	12	on	on	ADP
ijpds-4231	505	13	the	the	DET
ijpds-4231	505	14	synthetic	synthetic	ADJ
ijpds-4231	505	15	aspects	aspect	NOUN
ijpds-4231	505	16	and	and	CCONJ
ijpds-4231	505	17	reaction	reaction	NOUN
ijpds-4231	505	18	optimization	optimization	NOUN
ijpds-4231	505	19	studies	study	NOUN
ijpds-4231	505	20	to	to	PART
ijpds-4231	505	21	isolate	isolate	VERB
ijpds-4231	505	22	rasagiline	rasagiline	NOUN
ijpds-4231	505	23	and	and	CCONJ
ijpds-4231	505	24	its	its	PRON
ijpds-4231	505	25	clinically	clinically	ADV
ijpds-4231	505	26	acceptable	acceptable	ADJ
ijpds-4231	505	27	salts	salt	NOUN
ijpds-4231	505	28	.	.	PUNCT
ijpds-4231	506	1	racemization	racemization	NOUN
ijpds-4231	506	2	,	,	PUNCT
ijpds-4231	506	3	recovery	recovery	NOUN
ijpds-4231	506	4	of	of	ADP
ijpds-4231	506	5	s	s	NOUN
ijpds-4231	506	6	-	-	NOUN
ijpds-4231	506	7	isomer	isomer	ADJ
ijpds-4231	506	8	and	and	CCONJ
ijpds-4231	506	9	its	its	PRON
ijpds-4231	506	10	effective	effective	ADJ
ijpds-4231	506	11	reuse	reuse	NOUN
ijpds-4231	506	12	are	be	AUX
ijpds-4231	506	13	the	the	DET
ijpds-4231	506	14	key	key	ADJ
ijpds-4231	506	15	process	process	NOUN
ijpds-4231	506	16	bottle	bottle	NOUN
ijpds-4231	506	17	-	-	PUNCT
ijpds-4231	506	18	necks	neck	NOUN
ijpds-4231	506	19	either	either	CCONJ
ijpds-4231	506	20	at	at	ADP
ijpds-4231	506	21	the	the	DET
ijpds-4231	506	22	initial	initial	ADJ
ijpds-4231	506	23	phase	phase	NOUN
ijpds-4231	506	24	or	or	CCONJ
ijpds-4231	506	25	at	at	ADP
ijpds-4231	506	26	the	the	DET
ijpds-4231	506	27	end	end	NOUN
ijpds-4231	506	28	.	.	PUNCT
ijpds-4231	507	1	an	an	DET
ijpds-4231	507	2	optimized	optimize	VERB
ijpds-4231	507	3	process	process	NOUN
ijpds-4231	507	4	with	with	ADP
ijpds-4231	507	5	the	the	DET
ijpds-4231	507	6	use	use	NOUN
ijpds-4231	507	7	of	of	ADP
ijpds-4231	507	8	commercially	commercially	ADV
ijpds-4231	507	9	viable	viable	ADJ
ijpds-4231	507	10	starting	starting	NOUN
ijpds-4231	507	11	material	material	NOUN
ijpds-4231	507	12	/	/	SYM
ijpds-4231	507	13	s	s	NOUN
ijpds-4231	507	14	and	and	CCONJ
ijpds-4231	507	15	the	the	DET
ijpds-4231	507	16	use	use	NOUN
ijpds-4231	507	17	of	of	ADP
ijpds-4231	507	18	green	green	ADJ
ijpds-4231	507	19	solvents/	solvents/	NUM
ijpds-4231	507	20	reagents	reagent	NOUN
ijpds-4231	507	21	under	under	ADP
ijpds-4231	507	22	mild	mild	ADJ
ijpds-4231	507	23	reaction	reaction	NOUN
ijpds-4231	507	24	conditions	condition	NOUN
ijpds-4231	507	25	would	would	AUX
ijpds-4231	507	26	favor	favor	VERB
ijpds-4231	507	27	the	the	DET
ijpds-4231	507	28	large	large	ADJ
ijpds-4231	507	29	scale	scale	NOUN
ijpds-4231	507	30	manufacturing	manufacturing	NOUN
ijpds-4231	507	31	of	of	ADP
ijpds-4231	507	32	rasagiline	rasagiline	NOUN
ijpds-4231	507	33	and	and	CCONJ
ijpds-4231	507	34	its	its	PRON
ijpds-4231	507	35	stable	stable	ADJ
ijpds-4231	507	36	salts	salt	NOUN
ijpds-4231	507	37	.	.	PUNCT
ijpds-4231	508	1	references	reference	NOUN
ijpds-4231	508	2	1	1	NUM
ijpds-4231	508	3	.	.	PUNCT
ijpds-4231	508	4	akao	akao	PROPN
ijpds-4231	508	5	y	y	PROPN
ijpds-4231	508	6	,	,	PUNCT
ijpds-4231	508	7	maruyama	maruyama	PROPN
ijpds-4231	508	8	w	w	PROPN
ijpds-4231	508	9	,	,	PUNCT
ijpds-4231	508	10	yi	yi	PROPN
ijpds-4231	508	11	h	h	NOUN
ijpds-4231	508	12	,	,	PUNCT
ijpds-4231	508	13	et	et	PROPN
ijpds-4231	508	14	al	al	PROPN
ijpds-4231	508	15	.	.	PUNCT
ijpds-4231	509	1	an	an	DET
ijpds-4231	509	2	anti	anti	ADJ
ijpds-4231	509	3	-	-	ADJ
ijpds-4231	509	4	parkinson	parkinson	ADJ
ijpds-4231	509	5	’s	’s	PART
ijpds-4231	509	6	disease	disease	NOUN
ijpds-4231	509	7	drug	drug	NOUN
ijpds-4231	509	8	,	,	PUNCT
ijpds-4231	509	9	n	n	CCONJ
ijpds-4231	509	10	-	-	PUNCT
ijpds-4231	509	11	propargyl-1(r)-aminoindan	propargyl-1(r)-aminoindan	NOUN
ijpds-4231	509	12	(	(	PUNCT
ijpds-4231	509	13	rasagiline	rasagiline	NOUN
ijpds-4231	509	14	)	)	PUNCT
ijpds-4231	509	15	,	,	PUNCT
ijpds-4231	509	16	enhances	enhance	VERB
ijpds-4231	509	17	expression	expression	NOUN
ijpds-4231	509	18	of	of	ADP
ijpds-4231	509	19	anti	anti	ADJ
ijpds-4231	509	20	-	-	ADJ
ijpds-4231	509	21	apoptotic	apoptotic	ADJ
ijpds-4231	509	22	bcl-2	bcl-2	NOUN
ijpds-4231	509	23	in	in	ADP
ijpds-4231	509	24	human	human	ADJ
ijpds-4231	509	25	dopaminergic	dopaminergic	ADJ
ijpds-4231	509	26	sh	sh	NOUN
ijpds-4231	509	27	-	-	PUNCT
ijpds-4231	509	28	sy5y	sy5y	PROPN
ijpds-4231	509	29	cells	cell	NOUN
ijpds-4231	509	30	.	.	PUNCT
ijpds-4231	510	1	neurosci	neurosci	PROPN
ijpds-4231	510	2	lett	lett	PROPN
ijpds-4231	510	3	.	.	PUNCT
ijpds-4231	511	1	2002;326(2):105–8	2002;326(2):105–8	NUM
ijpds-4231	511	2	.	.	PUNCT
ijpds-4231	512	1	available	available	ADJ
ijpds-4231	512	2	from	from	ADP
ijpds-4231	512	3	:	:	PUNCT
ijpds-4231	512	4	http://dx.doi.org	http://dx.doi.org	NUM
ijpds-4231	512	5	/10.1016	/10.1016	ADJ
ijpds-4231	512	6	/	/	SYM
ijpds-4231	512	7	s0304	s0304	ADJ
ijpds-4231	512	8	-	-	PUNCT
ijpds-4231	512	9	3940(02)00332	3940(02)00332	NUM
ijpds-4231	512	10	-	-	PUNCT
ijpds-4231	512	11	4	4	NUM
ijpds-4231	512	12	2	2	NUM
ijpds-4231	512	13	.	.	PUNCT
ijpds-4231	513	1	oldfield	oldfield	PROPN
ijpds-4231	513	2	v	v	PROPN
ijpds-4231	513	3	,	,	PUNCT
ijpds-4231	513	4	keating	keating	PROPN
ijpds-4231	513	5	gm	gm	PROPN
ijpds-4231	513	6	,	,	PUNCT
ijpds-4231	513	7	perry	perry	PROPN
ijpds-4231	513	8	cm	cm	PROPN
ijpds-4231	513	9	.	.	PUNCT
ijpds-4231	513	10	rasagiline	rasagiline	PROPN
ijpds-4231	513	11	:	:	PUNCT
ijpds-4231	513	12	a	a	DET
ijpds-4231	513	13	review	review	NOUN
ijpds-4231	513	14	of	of	ADP
ijpds-4231	513	15	its	its	PRON
ijpds-4231	513	16	use	use	NOUN
ijpds-4231	513	17	in	in	ADP
ijpds-4231	513	18	the	the	DET
ijpds-4231	513	19	management	management	NOUN
ijpds-4231	513	20	of	of	ADP
ijpds-4231	513	21	parkinson??s	parkinson??s	PROPN
ijpds-4231	513	22	disease	disease	NOUN
ijpds-4231	513	23	.	.	PUNCT
ijpds-4231	514	1	drugs	drug	NOUN
ijpds-4231	514	2	.	.	PUNCT
ijpds-4231	515	1	2007;67(12):1725–47	2007;67(12):1725–47	NUM
ijpds-4231	515	2	.	.	PUNCT
ijpds-4231	515	3	available	available	ADJ
ijpds-4231	515	4	from	from	ADP
ijpds-4231	515	5	:	:	PUNCT
ijpds-4231	515	6	http://dx.doi.org/	http://dx.doi.org/	PROPN
ijpds-4231	515	7	10.2165/00003495	10.2165/00003495	NUM
ijpds-4231	515	8	-	-	SYM
ijpds-4231	515	9	200767120	200767120	NUM
ijpds-4231	515	10	-	-	SYM
ijpds-4231	515	11	00006	00006	NUM
ijpds-4231	515	12	3	3	NUM
ijpds-4231	515	13	.	.	PUNCT
ijpds-4231	515	14	lakhan	lakhan	PROPN
ijpds-4231	515	15	se	se	PROPN
ijpds-4231	515	16	.	.	PROPN
ijpds-4231	516	1	from	from	ADP
ijpds-4231	516	2	a	a	DET
ijpds-4231	516	3	parkinson	parkinson	NOUN
ijpds-4231	516	4	’s	’s	PART
ijpds-4231	516	5	disease	disease	NOUN
ijpds-4231	516	6	expert	expert	NOUN
ijpds-4231	516	7	:	:	PUNCT
ijpds-4231	516	8	rasagiline	rasagiline	NOUN
ijpds-4231	516	9	and	and	CCONJ
ijpds-4231	516	10	the	the	DET
ijpds-4231	516	11	future	future	NOUN
ijpds-4231	516	12	of	of	ADP
ijpds-4231	516	13	therapy	therapy	NOUN
ijpds-4231	516	14	.	.	PUNCT
ijpds-4231	517	1	mol	mol	ADP
ijpds-4231	517	2	neurodegener	neurodegener	NOUN
ijpds-4231	517	3	.	.	PUNCT
ijpds-4231	518	1	2007;2(1):13	2007;2(1):13	X
ijpds-4231	518	2	.	.	PUNCT
ijpds-4231	518	3	available	available	ADJ
ijpds-4231	518	4	from	from	ADP
ijpds-4231	518	5	:	:	PUNCT
ijpds-4231	518	6	http://dx.doi.org/10.1186/1750-1326-2-13	http://dx.doi.org/10.1186/1750-1326-2-13	ADP
ijpds-4231	518	7	4	4	NUM
ijpds-4231	518	8	.	.	PUNCT
ijpds-4231	518	9	maurice	maurice	PROPN
ijpds-4231	518	10	wg	wg	PROPN
ijpds-4231	518	11	,	,	PUNCT
ijpds-4231	518	12	john	john	PROPN
ijpds-4231	518	13	wj	wj	PROPN
ijpds-4231	518	14	,	,	PUNCT
ijpds-4231	518	15	leslie	leslie	PROPN
ijpds-4231	518	16	fw	fw	PROPN
ijpds-4231	518	17	.	.	PROPN
ijpds-4231	518	18	methods	method	NOUN
ijpds-4231	518	19	of	of	ADP
ijpds-4231	518	20	lowering	lower	VERB
ijpds-4231	518	21	blood	blood	NOUN
ijpds-4231	518	22	pressure	pressure	NOUN
ijpds-4231	518	23	in	in	ADP
ijpds-4231	518	24	animals	animal	NOUN
ijpds-4231	518	25	by	by	ADP
ijpds-4231	518	26	administering	administer	VERB
ijpds-4231	518	27	secondary	secondary	ADJ
ijpds-4231	518	28	and	and	CCONJ
ijpds-4231	518	29	tertiary	tertiary	ADJ
ijpds-4231	518	30	amines	amine	NOUN
ijpds-4231	518	31	.	.	PUNCT
ijpds-4231	519	1	1970	1970	NUM
ijpds-4231	519	2	.	.	PUNCT
ijpds-4231	520	1	available	available	ADJ
ijpds-4231	520	2	from	from	ADP
ijpds-4231	520	3	:	:	PUNCT
ijpds-4231	520	4	https://worldwide	https://worldwide	NUM
ijpds-4231	520	5	.	.	PUNCT
ijpds-4231	520	6	espacenet.com/patent/search/family/010332675/publication/	espacenet.com/patent/search/family/010332675/publication/	PROPN
ijpds-4231	520	7	us3513244a?q	us3513244a?q	PUNCT
ijpds-4231	520	8	=	=	ADJ
ijpds-4231	520	9	us3513244a	us3513244a	ADJ
ijpds-4231	520	10	http://dx.doi.org/%2010.2165/00003495-200767120-00006	http://dx.doi.org/%2010.2165/00003495-200767120-00006	NOUN
ijpds-4231	520	11	http://dx.doi.org/%2010.2165/00003495-200767120-00006	http://dx.doi.org/%2010.2165/00003495-200767120-00006	NOUN
ijpds-4231	520	12	http://dx.doi.org/10.1186/1750-1326-2-13	http://dx.doi.org/10.1186/1750-1326-2-13	NOUN
ijpds-4231	520	13	sanjay	sanjay	NOUN
ijpds-4231	520	14	s	s	PART
ijpds-4231	520	15	s	s	NOUN
ijpds-4231	520	16	patents	patent	NOUN
ijpds-4231	520	17	disclosed	disclose	VERB
ijpds-4231	520	18	synthetic	synthetic	ADJ
ijpds-4231	520	19	overview	overview	NOUN
ijpds-4231	520	20	of	of	ADP
ijpds-4231	520	21	rasagiline	rasagiline	ADJ
ijpds-4231	520	22	vol	vol	NOUN
ijpds-4231	520	23	2	2	NUM
ijpds-4231	520	24	|	|	ADV
ijpds-4231	520	25	issue	issue	VERB
ijpds-4231	520	26	4	4	NUM
ijpds-4231	520	27	|	|	ADV
ijpds-4231	520	28	oct	oct	PROPN
ijpds-4231	520	29	–	–	PUNCT
ijpds-4231	520	30	dec	dec	PROPN
ijpds-4231	520	31	2023	2023	NUM
ijpds-4231	520	32	indian	indian	PROPN
ijpds-4231	520	33	j	j	PROPN
ijpds-4231	520	34	pharm	pharm	PROPN
ijpds-4231	520	35	drug	drug	PROPN
ijpds-4231	520	36	studies	study	NOUN
ijpds-4231	520	37	|	|	ADV
ijpds-4231	520	38	145	145	NUM
ijpds-4231	520	39	5	5	NUM
ijpds-4231	520	40	.	.	PUNCT
ijpds-4231	521	1	youdim	youdim	PROPN
ijpds-4231	521	2	mbh	mbh	PROPN
ijpds-4231	521	3	,	,	PUNCT
ijpds-4231	521	4	finberg	finberg	PROPN
ijpds-4231	521	5	jpm	jpm	PROPN
ijpds-4231	521	6	,	,	PUNCT
ijpds-4231	521	7	levy	levy	NOUN
ijpds-4231	521	8	r	r	NOUN
ijpds-4231	521	9	,	,	PUNCT
ijpds-4231	521	10	et	et	PROPN
ijpds-4231	521	11	al	al	PROPN
ijpds-4231	521	12	.	.	PUNCT
ijpds-4231	522	1	use	use	NOUN
ijpds-4231	522	2	of	of	ADP
ijpds-4231	522	3	the	the	DET
ijpds-4231	522	4	renantiomers	renantiomer	NOUN
ijpds-4231	522	5	of	of	ADP
ijpds-4231	522	6	n	n	CCONJ
ijpds-4231	522	7	-	-	PUNCT
ijpds-4231	522	8	propargyl	propargyl	NOUN
ijpds-4231	522	9	1	1	NUM
ijpds-4231	522	10	-	-	PUNCT
ijpds-4231	522	11	aminoindan	aminoindan	NOUN
ijpds-4231	522	12	compounds	compound	NOUN
ijpds-4231	522	13	for	for	ADP
ijpds-4231	522	14	treating	treat	VERB
ijpds-4231	522	15	parkinson	parkinson	NOUN
ijpds-4231	522	16	's	's	PART
ijpds-4231	522	17	disease	disease	NOUN
ijpds-4231	522	18	.	.	PUNCT
ijpds-4231	523	1	1995	1995	NUM
ijpds-4231	523	2	.	.	PUNCT
ijpds-4231	524	1	available	available	ADJ
ijpds-4231	524	2	from	from	ADP
ijpds-4231	524	3	:	:	PUNCT
ijpds-4231	524	4	https://worldwide.espacenet.com/patent/search/family/01106	https://worldwide.espacenet.com/patent/search/family/01106	NOUN
ijpds-4231	524	5	0756	0756	NUM
ijpds-4231	524	6	/	/	SYM
ijpds-4231	524	7	publication	publication	NOUN
ijpds-4231	524	8	/	/	SYM
ijpds-4231	524	9	us5453446a?q	us5453446a?q	NOUN
ijpds-4231	524	10	=	=	NOUN
ijpds-4231	524	11	us5453446a	us5453446a	NOUN
ijpds-4231	524	12	6	6	NUM
ijpds-4231	524	13	.	.	PUNCT
ijpds-4231	525	1	huebner	huebner	PROPN
ijpds-4231	525	2	cf	cf	PROPN
ijpds-4231	525	3	.	.	PUNCT
ijpds-4231	526	1	n-2	n-2	NOUN
ijpds-4231	526	2	-	-	PUNCT
ijpds-4231	526	3	alkynyl	alkynyl	NOUN
ijpds-4231	526	4	-	-	PUNCT
ijpds-4231	526	5	amino	amino	NOUN
ijpds-4231	526	6	-	-	PUNCT
ijpds-4231	526	7	benzocylo	benzocylo	NOUN
ijpds-4231	526	8	-	-	PUNCT
ijpds-4231	526	9	alkanes	alkane	NOUN
ijpds-4231	526	10	.	.	PUNCT
ijpds-4231	527	1	1966	1966	NUM
ijpds-4231	527	2	.	.	PUNCT
ijpds-4231	528	1	available	available	ADJ
ijpds-4231	528	2	from	from	ADP
ijpds-4231	528	3	:	:	PUNCT
ijpds-4231	528	4	https://worldwide.espacenet.com/patent/	https://worldwide.espacenet.com/patent/	PROPN
ijpds-4231	528	5	search	search	NOUN
ijpds-4231	528	6	/	/	SYM
ijpds-4231	528	7	family/027394548	family/027394548	NOUN
ijpds-4231	528	8	/	/	SYM
ijpds-4231	528	9	publication	publication	NOUN
ijpds-4231	528	10	/	/	SYM
ijpds-4231	528	11	us3253037a?q	us3253037a?q	PROPN
ijpds-4231	528	12	=	=	PROPN
ijpds-4231	528	13	us32	us32	PROPN
ijpds-4231	528	14	53037a	53037a	NUM
ijpds-4231	528	15	7	7	NUM
ijpds-4231	528	16	.	.	PUNCT
ijpds-4231	529	1	maurice	maurice	PROPN
ijpds-4231	529	2	wg	wg	PROPN
ijpds-4231	529	3	,	,	PUNCT
ijpds-4231	529	4	john	john	PROPN
ijpds-4231	529	5	wj	wj	PROPN
ijpds-4231	529	6	,	,	PUNCT
ijpds-4231	529	7	langley	langley	PROPN
ijpds-4231	529	8	b	b	PROPN
ijpds-4231	529	9	et	et	PROPN
ijpds-4231	529	10	al	al	PROPN
ijpds-4231	529	11	.	.	PROPN
ijpds-4231	529	12	process	process	NOUN
ijpds-4231	529	13	for	for	ADP
ijpds-4231	529	14	the	the	DET
ijpds-4231	529	15	preparation	preparation	NOUN
ijpds-4231	529	16	of	of	ADP
ijpds-4231	529	17	therapeutically	therapeutically	ADV
ijpds-4231	529	18	utilizable	utilizable	ADJ
ijpds-4231	529	19	n	n	CCONJ
ijpds-4231	529	20	-	-	PUNCT
ijpds-4231	529	21	substituted	substitute	VERB
ijpds-4231	529	22	-1aminoindanes	-1aminoindanes	PROPN
ijpds-4231	529	23	.	.	NOUN
ijpds-4231	529	24	1968	1968	NUM
ijpds-4231	529	25	.	.	PUNCT
ijpds-4231	530	1	available	available	ADJ
ijpds-4231	530	2	from	from	ADP
ijpds-4231	530	3	:	:	PUNCT
ijpds-4231	530	4	https://worldwide	https://worldwide	NUM
ijpds-4231	530	5	.	.	PUNCT
ijpds-4231	530	6	espacenet.com/patent/search/family/010313839/publication/	espacenet.com/patent/search/family/010313839/publication/	PUNCT
ijpds-4231	531	1	de1443403a1?q	de1443403a1?q	PROPN
ijpds-4231	531	2	=	=	PROPN
ijpds-4231	531	3	pn%3dde1443403a1	pn%3dde1443403a1	NOUN
ijpds-4231	531	4	8	8	NUM
ijpds-4231	531	5	.	.	PUNCT
ijpds-4231	531	6	youdim	youdim	PROPN
ijpds-4231	531	7	mbh	mbh	PROPN
ijpds-4231	531	8	,	,	PUNCT
ijpds-4231	531	9	finberg	finberg	PROPN
ijpds-4231	531	10	jpm	jpm	PROPN
ijpds-4231	531	11	,	,	PUNCT
ijpds-4231	531	12	levy	levy	NOUN
ijpds-4231	531	13	r	r	NOUN
ijpds-4231	531	14	,	,	PUNCT
ijpds-4231	531	15	et	et	PROPN
ijpds-4231	531	16	al	al	PROPN
ijpds-4231	531	17	.	.	PUNCT
ijpds-4231	532	1	r	r	X
ijpds-4231	532	2	-	-	PUNCT
ijpds-4231	532	3	enantiomer	enantiomer	NOUN
ijpds-4231	532	4	of	of	ADP
ijpds-4231	532	5	n	n	CCONJ
ijpds-4231	532	6	-	-	PUNCT
ijpds-4231	532	7	propargyl-1	propargyl-1	NOUN
ijpds-4231	532	8	-	-	PUNCT
ijpds-4231	532	9	aminoindan	aminoindan	NOUN
ijpds-4231	532	10	,	,	PUNCT
ijpds-4231	532	11	its	its	PRON
ijpds-4231	532	12	preparation	preparation	NOUN
ijpds-4231	532	13	and	and	CCONJ
ijpds-4231	532	14	pharmaceutical	pharmaceutical	NOUN
ijpds-4231	532	15	compositions	composition	NOUN
ijpds-4231	532	16	containing	contain	VERB
ijpds-4231	532	17	it	it	PRON
ijpds-4231	532	18	.	.	PUNCT
ijpds-4231	533	1	1991	1991	NUM
ijpds-4231	533	2	.	.	PUNCT
ijpds-4231	534	1	available	available	ADJ
ijpds-4231	534	2	from	from	ADP
ijpds-4231	534	3	:	:	PUNCT
ijpds-4231	534	4	https://worldwide.espacenet.com/patent/search/family/	https://worldwide.espacenet.com/patent/search/family/	NUM
ijpds-4231	534	5	011060756	011060756	NUM
ijpds-4231	534	6	/	/	SYM
ijpds-4231	534	7	publication	publication	NOUN
ijpds-4231	534	8	/	/	SYM
ijpds-4231	534	9	ep0436492a2?q	ep0436492a2?q	PROPN
ijpds-4231	534	10	=	=	PROPN
ijpds-4231	534	11	ep0436492a2	ep0436492a2	PROPN
ijpds-4231	534	12	9	9	NUM
ijpds-4231	534	13	.	.	PUNCT
ijpds-4231	534	14	youdim	youdim	PROPN
ijpds-4231	534	15	mbh	mbh	PROPN
ijpds-4231	534	16	,	,	PUNCT
ijpds-4231	534	17	finberg	finberg	PROPN
ijpds-4231	534	18	jpm	jpm	PROPN
ijpds-4231	534	19	,	,	PUNCT
ijpds-4231	534	20	levy	levy	NOUN
ijpds-4231	534	21	r	r	NOUN
ijpds-4231	534	22	,	,	PUNCT
ijpds-4231	534	23	et	et	PROPN
ijpds-4231	534	24	al	al	PROPN
ijpds-4231	534	25	.	.	PUNCT
ijpds-4231	535	1	r	r	X
ijpds-4231	535	2	-	-	PUNCT
ijpds-4231	535	3	enantiomer	enantiomer	NOUN
ijpds-4231	535	4	of	of	ADP
ijpds-4231	535	5	n	n	CCONJ
ijpds-4231	535	6	-	-	PUNCT
ijpds-4231	535	7	propargyl-1	propargyl-1	NOUN
ijpds-4231	535	8	-	-	PUNCT
ijpds-4231	535	9	aminoindan	aminoindan	NOUN
ijpds-4231	535	10	,	,	PUNCT
ijpds-4231	535	11	salts	salt	NOUN
ijpds-4231	535	12	,	,	PUNCT
ijpds-4231	535	13	compositions	composition	NOUN
ijpds-4231	535	14	and	and	CCONJ
ijpds-4231	535	15	uses	use	VERB
ijpds-4231	535	16	thereof	thereof	ADV
ijpds-4231	535	17	.	.	PUNCT
ijpds-4231	536	1	1995	1995	NUM
ijpds-4231	536	2	.	.	PUNCT
ijpds-4231	537	1	available	available	ADJ
ijpds-4231	537	2	from	from	ADP
ijpds-4231	537	3	:	:	PUNCT
ijpds-4231	537	4	https://worldwide.espacenet	https://worldwide.espacenet	PROPN
ijpds-4231	537	5	.	.	PUNCT
ijpds-4231	537	6	com	com	NOUN
ijpds-4231	537	7	/	/	SYM
ijpds-4231	537	8	patent	patent	NOUN
ijpds-4231	537	9	/	/	SYM
ijpds-4231	537	10	search	search	NOUN
ijpds-4231	537	11	/	/	SYM
ijpds-4231	537	12	family/022487049	family/022487049	NOUN
ijpds-4231	537	13	/	/	SYM
ijpds-4231	537	14	publication	publication	NOUN
ijpds-4231	537	15	/	/	SYM
ijpds-4231	537	16	wo951101	wo951101	NOUN
ijpds-4231	537	17	6a1?q	6a1?q	PROPN
ijpds-4231	538	1	=	=	SYM
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ijpds-4231	538	4	.	.	PUNCT
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ijpds-4231	539	2	mbh	mbh	PROPN
ijpds-4231	539	3	,	,	PUNCT
ijpds-4231	539	4	finberg	finberg	PROPN
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ijpds-4231	539	6	,	,	PUNCT
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ijpds-4231	540	1	r	r	X
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ijpds-4231	540	15	uses	use	VERB
ijpds-4231	540	16	thereof	thereof	ADV
ijpds-4231	540	17	.	.	PUNCT
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ijpds-4231	541	2	.	.	PUNCT
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ijpds-4231	542	14	publication	publication	NOUN
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ijpds-4231	542	16	us5532415	us5532415	NOUN
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ijpds-4231	542	18	=	=	NOUN
ijpds-4231	542	19	us5532415a	us5532415a	X
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ijpds-4231	542	21	.	.	PUNCT
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ijpds-4231	543	2	mbh	mbh	PROPN
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ijpds-4231	543	6	,	,	PUNCT
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ijpds-4231	543	12	.	.	PROPN
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ijpds-4231	543	17	r	r	NOUN
ijpds-4231	543	18	-	-	PUNCT
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ijpds-4231	543	22	-	-	PUNCT
ijpds-4231	543	23	propargyl-1	propargyl-1	NUM
ijpds-4231	543	24	-	-	PUNCT
ijpds-4231	543	25	aminoindan	aminoindan	NOUN
ijpds-4231	543	26	compounds	compound	NOUN
ijpds-4231	543	27	.	.	PUNCT
ijpds-4231	544	1	1996	1996	NUM
ijpds-4231	544	2	.	.	PUNCT
ijpds-4231	545	1	available	available	ADJ
ijpds-4231	545	2	from	from	ADP
ijpds-4231	545	3	:	:	PUNCT
ijpds-4231	545	4	https://worldwide	https://worldwide	NUM
ijpds-4231	545	5	.	.	PUNCT
ijpds-4231	545	6	espacenet.com/patent/search/family/036764609/publication/c	espacenet.com/patent/search/family/036764609/publication/c	PUNCT
ijpds-4231	546	1	n1031995c?q	n1031995c?q	PROPN
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ijpds-4231	547	9	,	,	PUNCT
ijpds-4231	547	10	et	et	PROPN
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ijpds-4231	547	12	.	.	PROPN
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ijpds-4231	547	18	rasagiline	rasagiline	NOUN
ijpds-4231	547	19	and	and	CCONJ
ijpds-4231	547	20	its	its	PRON
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ijpds-4231	547	22	.	.	PUNCT
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ijpds-4231	548	2	.	.	PUNCT
ijpds-4231	549	1	available	available	ADJ
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ijpds-4231	549	5	5183	5183	NUM
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ijpds-4231	549	9	wo02068376a1?q	wo02068376a1?q	PROPN
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ijpds-4231	550	14	enantomeric	enantomeric	ADJ
ijpds-4231	550	15	indanylamine	indanylamine	ADJ
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ijpds-4231	552	5	4953	4953	NUM
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ijpds-4231	552	7	publication	publication	NOUN
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ijpds-4231	552	9	us2006199974a1?q	us2006199974a1?q	PROPN
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ijpds-4231	552	11	us%202006%2f019	us%202006%2f019	PROPN
ijpds-4231	552	12	9974a1	9974a1	PROPN
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ijpds-4231	552	14	.	.	PUNCT
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ijpds-4231	553	10	al	al	PROPN
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ijpds-4231	553	15	propargylated	propargylated	ADJ
ijpds-4231	553	16	aminoindans	aminoindan	NOUN
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ijpds-4231	555	3	:	:	PUNCT
ijpds-4231	555	4	https://	https://	PROPN
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ijpds-4231	555	6	ublication	ublication	PROPN
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ijpds-4231	555	8	us2007112217a1?q	us2007112217a1?q	PROPN
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ijpds-4231	556	1	anton	anton	PROPN
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ijpds-4231	556	5	lh	lh	PROPN
ijpds-4231	556	6	,	,	PUNCT
ijpds-4231	556	7	eduard	eduard	PROPN
ijpds-4231	556	8	g	g	PROPN
ijpds-4231	556	9	et	et	PROPN
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ijpds-4231	556	11	.	.	PROPN
ijpds-4231	556	12	methods	method	NOUN
ijpds-4231	556	13	for	for	ADP
ijpds-4231	556	14	isolating	isolate	VERB
ijpds-4231	556	15	propargylated	propargylated	ADJ
ijpds-4231	556	16	aminoindans	aminoindan	NOUN
ijpds-4231	556	17	.	.	PUNCT
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ijpds-4231	557	2	.	.	PUNCT
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ijpds-4231	558	8	us7491847b2?q	us7491847b2?q	ADJ
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ijpds-4231	558	10	pn%3dus7491847b2	pn%3dus7491847b2	NOUN
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ijpds-4231	559	7	preparing	prepare	VERB
ijpds-4231	559	8	2,3	2,3	NUM
ijpds-4231	559	9	-	-	PUNCT
ijpds-4231	559	10	dihydro-1hindenes-1	dihydro-1hindenes-1	NOUN
ijpds-4231	559	11	-	-	PUNCT
ijpds-4231	559	12	amine	amine	NOUN
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ijpds-4231	561	9	cn101062897a?q	cn101062897a?q	PROPN
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ijpds-4231	561	12	2897a	2897a	NUM
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ijpds-4231	562	1	feng	feng	PROPN
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ijpds-4231	562	6	process	process	NOUN
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ijpds-4231	563	1	2007	2007	NUM
ijpds-4231	563	2	.	.	PUNCT
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ijpds-4231	564	5	.	.	PUNCT
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ijpds-4231	566	3	:	:	PUNCT
ijpds-4231	566	4	https://	https://	PROPN
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ijpds-4231	566	6	ublication	ublication	NOUN
ijpds-4231	566	7	/	/	SYM
ijpds-4231	566	8	cn101260048a?q	cn101260048a?q	X
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ijpds-4231	569	5	search	search	PROPN
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ijpds-4231	569	8	/	/	SYM
ijpds-4231	569	9	publication	publication	NOUN
ijpds-4231	569	10	/	/	SYM
ijpds-4231	569	11	us2009292141a1?q	us2009292141a1?q	PROPN
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ijpds-4231	572	5	search	search	PROPN
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ijpds-4231	607	2	https://worldwide.espacenet.com/patent/%20search/family/039536623/publication/ep2101569b1?q=pn%3dep2101569b1	https://worldwide.espacenet.com/patent/%20search/family/039536623/publication/ep2101569b1?q=pn%3dep2101569b1	SCONJ
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ijpds-4231	635	2	from	from	ADP
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ijpds-4231	635	4	https://	https://	PROPN
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ijpds-4231	635	9	=	=	SYM
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ijpds-4231	642	1	espacenet.com/patent/search/family/044144855/publication/	espacenet.com/patent/search/family/044144855/publication/	X
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ijpds-4231	644	1	=	=	PRON
ijpds-4231	644	2	pn%3dwo2011080589a2	pn%3dwo2011080589a2	NOUN
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ijpds-4231	651	1	=	=	SYM
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ijpds-4231	655	9	cn102203053a?q	cn102203053a?q	X
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ijpds-4231	718	5	048082617	048082617	NUM
ijpds-4231	718	6	/	/	SYM
ijpds-4231	718	7	publication	publication	NOUN
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ijpds-4231	718	9	wo2013054346a2?q	wo2013054346a2?q	PROPN
ijpds-4231	718	10	=	=	PROPN
ijpds-4231	718	11	pn%3dwo20	pn%3dwo20	X
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ijpds-4231	718	13	61	61	NUM
ijpds-4231	718	14	.	.	PUNCT
ijpds-4231	719	1	gade	gade	PROPN
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ijpds-4231	719	4	adla	adla	NOUN
ijpds-4231	719	5	vk	vk	PROPN
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ijpds-4231	719	7	vempati	vempati	NOUN
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ijpds-4231	719	9	preparation	preparation	NOUN
ijpds-4231	719	10	of	of	ADP
ijpds-4231	719	11	rasagiline	rasagiline	NOUN
ijpds-4231	719	12	hemitartrate	hemitartrate	NOUN
ijpds-4231	719	13	.	.	PUNCT
ijpds-4231	720	1	2013	2013	NUM
ijpds-4231	720	2	.	.	PUNCT
ijpds-4231	721	1	available	available	ADJ
ijpds-4231	721	2	from	from	ADP
ijpds-4231	721	3	:	:	PUNCT
ijpds-4231	721	4	https://worldwide	https://worldwide	NUM
ijpds-4231	721	5	.	.	PUNCT
ijpds-4231	722	1	espacenet.com/patent/search/family/047559035/publication/e	espacenet.com/patent/search/family/047559035/publication/e	NOUN
ijpds-4231	722	2	p2610239a1?q	p2610239a1?q	NOUN
ijpds-4231	722	3	=	=	PROPN
ijpds-4231	722	4	pn%3dep2610239a1	pn%3dep2610239a1	ADJ
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ijpds-4231	722	6	.	.	PUNCT
ijpds-4231	723	1	sun	sun	PROPN
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ijpds-4231	723	3	,	,	PUNCT
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ijpds-4231	723	7	feng	feng	PROPN
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ijpds-4231	723	9	,	,	PUNCT
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ijpds-4231	723	12	.	.	PUNCT
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ijpds-4231	723	18	analogue	analogue	NOUN
ijpds-4231	723	19	thereof	thereof	ADV
ijpds-4231	723	20	.	.	PUNCT
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ijpds-4231	724	2	.	.	PUNCT
ijpds-4231	725	1	available	available	ADJ
ijpds-4231	725	2	from	from	ADP
ijpds-4231	725	3	:	:	PUNCT
ijpds-4231	725	4	https	https	NOUN
ijpds-4231	725	5	:	:	PUNCT
ijpds-4231	725	6	//worldwide.espacenet.com	//worldwide.espacenet.com	X
ijpds-4231	725	7	/	/	SYM
ijpds-4231	725	8	patent	patent	NOUN
ijpds-4231	725	9	/	/	SYM
ijpds-4231	725	10	search	search	NOUN
ijpds-4231	725	11	/	/	SYM
ijpds-4231	725	12	family/050701641/	family/050701641/	PROPN
ijpds-4231	725	13	publication	publication	NOUN
ijpds-4231	725	14	/	/	SYM
ijpds-4231	725	15	cn103804200a?q	cn103804200a?q	NOUN
ijpds-4231	725	16	=	=	NOUN
ijpds-4231	725	17	pn%3dcn103804200a	pn%3dcn103804200a	PROPN
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ijpds-4231	725	19	.	.	PUNCT
ijpds-4231	726	1	sun	sun	PROPN
ijpds-4231	726	2	y	y	PROPN
ijpds-4231	726	3	,	,	PUNCT
ijpds-4231	726	4	yan	yan	PROPN
ijpds-4231	726	5	y	y	PROPN
ijpds-4231	726	6	,	,	PUNCT
ijpds-4231	726	7	feng	feng	PROPN
ijpds-4231	726	8	x	x	PROPN
ijpds-4231	726	9	,	,	PUNCT
ijpds-4231	726	10	et	et	PROPN
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ijpds-4231	726	12	.	.	PUNCT
ijpds-4231	726	13	preparation	preparation	NOUN
ijpds-4231	726	14	and	and	CCONJ
ijpds-4231	726	15	analysis	analysis	NOUN
ijpds-4231	726	16	method	method	NOUN
ijpds-4231	726	17	of	of	ADP
ijpds-4231	726	18	impurity	impurity	NOUN
ijpds-4231	726	19	of	of	ADP
ijpds-4231	726	20	rasagiline	rasagiline	NOUN
ijpds-4231	726	21	mesylate	mesylate	NOUN
ijpds-4231	726	22	.	.	PUNCT
ijpds-4231	727	1	2014	2014	NUM
ijpds-4231	727	2	.	.	PUNCT
ijpds-4231	728	1	available	available	ADJ
ijpds-4231	728	2	from	from	ADP
ijpds-4231	728	3	:	:	PUNCT
ijpds-4231	728	4	https://worldwide.espacenet.com/patent/search/family/	https://worldwide.espacenet.com/patent/search/family/	NUM
ijpds-4231	728	5	050903722	050903722	NUM
ijpds-4231	728	6	/	/	SYM
ijpds-4231	728	7	publication	publication	NOUN
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ijpds-4231	728	9	cn103864646a?q	cn103864646a?q	PROPN
ijpds-4231	728	10	=	=	PROPN
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ijpds-4231	728	12	4646a	4646a	NUM
ijpds-4231	728	13	64	64	NUM
ijpds-4231	728	14	.	.	PUNCT
ijpds-4231	729	1	prudic	prudic	PROPN
ijpds-4231	729	2	d	d	PROPN
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ijpds-4231	729	4	ruzic	ruzic	PROPN
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ijpds-4231	729	6	,	,	PUNCT
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ijpds-4231	729	9	,	,	PUNCT
ijpds-4231	729	10	et	et	PROPN
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ijpds-4231	729	16	preparation	preparation	NOUN
ijpds-4231	729	17	of	of	ADP
ijpds-4231	729	18	enatiomerically	enatiomerically	ADV
ijpds-4231	729	19	pure	pure	ADJ
ijpds-4231	729	20	1	1	NUM
ijpds-4231	729	21	-	-	PUNCT
ijpds-4231	729	22	aminoindan	aminoindan	NOUN
ijpds-4231	729	23	.	.	PUNCT
ijpds-4231	730	1	2015	2015	NUM
ijpds-4231	730	2	.	.	PUNCT
ijpds-4231	731	1	available	available	ADJ
ijpds-4231	731	2	from	from	ADP
ijpds-4231	731	3	:	:	PUNCT
ijpds-4231	731	4	https://worldwide.espacenet.com/patent/	https://worldwide.espacenet.com/patent/	PROPN
ijpds-4231	731	5	search	search	NOUN
ijpds-4231	731	6	/	/	SYM
ijpds-4231	731	7	family/051266306	family/051266306	NOUN
ijpds-4231	731	8	/	/	SYM
ijpds-4231	731	9	publication	publication	NOUN
ijpds-4231	731	10	/	/	SYM
ijpds-4231	731	11	wo2015070995a1?q=	wo2015070995a1?q=	NOUN
ijpds-4231	731	12	pn%3dwo2015070995a1	pn%3dwo2015070995a1	VERB
ijpds-4231	731	13	65	65	NUM
ijpds-4231	731	14	.	.	PUNCT
ijpds-4231	732	1	ruzic	ruzic	PROPN
ijpds-4231	732	2	m	m	PROPN
ijpds-4231	732	3	,	,	PUNCT
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ijpds-4231	732	5	d	d	PROPN
ijpds-4231	732	6	,	,	PUNCT
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ijpds-4231	732	8	a	a	X
ijpds-4231	732	9	,	,	PUNCT
ijpds-4231	732	10	et	et	PROPN
ijpds-4231	732	11	al	al	PROPN
ijpds-4231	732	12	.	.	PROPN
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ijpds-4231	732	18	racemization	racemization	NOUN
ijpds-4231	732	19	of	of	ADP
ijpds-4231	732	20	enantiomerically	enantiomerically	ADV
ijpds-4231	732	21	enriched	enrich	VERB
ijpds-4231	732	22	1aminoindane	1aminoindane	NUM
ijpds-4231	732	23	.	.	PROPN
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ijpds-4231	732	25	.	.	PUNCT
ijpds-4231	733	1	available	available	ADJ
ijpds-4231	733	2	from	from	ADP
ijpds-4231	733	3	:	:	PUNCT
ijpds-4231	733	4	https://worldwide	https://worldwide	PROPN
ijpds-4231	733	5	.	.	PUNCT
ijpds-4231	733	6	espacenet.com/patent/search/family/055221430/publication/	espacenet.com/patent/search/family/055221430/publication/	NOUN
ijpds-4231	733	7	wo2016116607a1?q	wo2016116607a1?q	PROPN
ijpds-4231	733	8	=	=	SYM
ijpds-4231	733	9	pn%3dwo2016116607a	pn%3dwo2016116607a	PROPN
ijpds-4231	733	10	66	66	NUM
ijpds-4231	733	11	.	.	PUNCT
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ijpds-4231	734	3	,	,	PUNCT
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ijpds-4231	734	6	,	,	PUNCT
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ijpds-4231	734	8	e.	e.	PROPN
ijpds-4231	734	9	3	3	PROPN
ijpds-4231	734	10	-	-	PUNCT
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ijpds-4231	734	12	-	-	PUNCT
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ijpds-4231	734	14	-	-	PUNCT
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ijpds-4231	734	18	.	.	PUNCT
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ijpds-4231	735	3	:	:	PUNCT
ijpds-4231	735	4	https://worldwide	https://worldwide	NUM
ijpds-4231	735	5	.	.	PUNCT
ijpds-4231	736	1	espacenet.com/patent/search/family/044151964/publication/e	espacenet.com/patent/search/family/044151964/publication/e	VERB
ijpds-4231	736	2	p2939669a1?q	p2939669a1?q	PROPN
ijpds-4231	737	1	=	=	NUM
ijpds-4231	737	2	pn%3dep2939669a1	pn%3dep2939669a1	NOUN
ijpds-4231	737	3	67	67	NUM
ijpds-4231	737	4	.	.	PUNCT
ijpds-4231	738	1	chen	chen	PROPN
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ijpds-4231	738	12	rasagiline	rasagiline	NOUN
ijpds-4231	738	13	mesylate	mesylate	NOUN
ijpds-4231	738	14	and	and	CCONJ
ijpds-4231	738	15	intermediate	intermediate	ADJ
ijpds-4231	738	16	thereof	thereof	ADV
ijpds-4231	738	17	.	.	PUNCT
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ijpds-4231	739	2	.	.	PUNCT
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ijpds-4231	740	2	from	from	ADP
ijpds-4231	740	3	:	:	PUNCT
ijpds-4231	740	4	htt	htt	NOUN
ijpds-4231	740	5	ps://worldwide.espacenet.com/patent/search/family/0649374	ps://worldwide.espacenet.com/patent/search/family/0649374	ADV
ijpds-4231	740	6	95	95	NUM
ijpds-4231	740	7	/	/	SYM
ijpds-4231	740	8	publication	publication	NOUN
ijpds-4231	740	9	/	/	SYM
ijpds-4231	740	10	cn109180499a?q	cn109180499a?q	NOUN
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ijpds-4231	741	8	c	c	PROPN
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ijpds-4231	743	3	:	:	PUNCT
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ijpds-4231	743	5	:	:	PUNCT
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ijpds-4231	743	11	/	/	SYM
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ijpds-4231	743	13	publication	publication	NOUN
ijpds-4231	743	14	/	/	SYM
ijpds-4231	743	15	cn110776429a?q	cn110776429a?q	PROPN
ijpds-4231	743	16	=	=	NOUN
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ijpds-4231	745	2	.	.	PUNCT
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ijpds-4231	746	3	:	:	PUNCT
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ijpds-4231	746	5	.	.	PUNCT
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ijpds-4231	746	7	n111333517a?q	n111333517a?q	PROPN
ijpds-4231	747	1	=	=	NOUN
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ijpds-4231	749	2	.	.	PUNCT
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ijpds-4231	750	2	from	from	ADP
ijpds-4231	750	3	:	:	PUNCT
ijpds-4231	750	4	https://worldwide	https://worldwide	PROPN
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ijpds-4231	750	7	n113030283a?q	n113030283a?q	PROPN
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ijpds-4231	750	9	pn%3dcn113030283a	pn%3dcn113030283a	PROPN
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ijpds-4231	765	5	087288402	087288402	NUM
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ijpds-4231	769	12	https://worldwide.espacenet.com/patent/search/family/046939731/publication/wo2012153349a2?q=pn%3dwo2012153349a2	https://worldwide.espacenet.com/patent/search/family/046939731/publication/wo2012153349a2?q=pn%3dwo2012153349a2	PROPN
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ijpds-4231	769	21	https://worldwide.espacenet.com/patent/%20search/family/050701641/publication/cn103804200a?q=pn%3dcn103804200a	https://worldwide.espacenet.com/patent/%20search/family/050701641/publication/cn103804200a?q=pn%3dcn103804200a	ADV
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