Jtam-A4.dvi JOURNAL OF THEORETICAL AND APPLIED MECHANICS 54, 2, pp. 489-501, Warsaw 2016 DOI: 10.15632/jtam-pl.54.2.489 EXPERIMENTAL INVESTIGATIONS OF ELASTIC-PLASTIC STRAIN STATES ON VARIOUS STAGES OF MATERIAL PLASTIFYING Barbara Kozłowska Warsaw University of Technology, Faculty of Mechatronical Engineering, Warsaw, Poland e-mail: b.kozlowska@mchtr.pw.edu.pl In the paper, the possibility of application of various experimental methods to the analy- sis of elastic-plastic states at different levels of material plastifying is presented. For tests carried out on two-dimensional elements with different stress concentrators and loaded by tensile stresses, three experimental methods have been selected: Moiré method, method of photoelastic coating and the thermography method. On the basis of the tests results, the range of the applicability of chosenmethods and their suitability to the elastic-plastic strain analysis at the development ofmaterial plastifying has been determined. The strain compo- nents distribution obtained from theMoiré method and themethod of photoelastic coating has been compared. The possibility of increasing the accuracy of strain determination for theMoiré method by additional tests at the grid rotated by an angle of 45◦ with respect to the direction of tensile stress has been shown. The results of the investigations have been discussed. Keywords: mechanics of solids, experimental methods, elastic-plastic states 1. Introduction and the experimental method selection The analysis of elastic-plastic states finds many basic applications in engineering design, espe- cially nowadays, since the economical trend towards building more lightweight and cheaper structures accepts partial material plastifying during exploitation. Experimental studies on a great variety of non-linear problems are conducted inmany rese- arch centers all over the world. These problems, like non-linear material characteristics, partial material plastifying, large deformation, material with imperfections, etc, always cause difficul- ties associatedwith themodelling of constructionalmaterials. In such circumstances, thewidely nowadays applied numericalmethods as FEMstill need final experimental verification. Especial- ly the experimental methods which give information about the real object without any model simplification can be very useful as a good verification tool of theoretical and numerical design. The experimentalmethodsmost commonly used to researchwork on elastic-plastic problems are: photoelasticity, especially the method of photoelastic coating (Pacey et al., 2005; Foust et al., 2011; Lamberson et al., 2012; Diaz et al., 2010),Moiré methods (Min et al., 2006; Livieri and Nicoletto, 2003; Guo et al., 2006), holographic interferometry (Lin, 2000; Balalov et al., 2007), electronic speckle pattern interferometrymethod (ESPI) (Diaz et al., 2001; Schajer et al., 2005), digital image correlation method (DIC) (Vural et al., 2011; Diaz et al., 2004; Tarigopula et al., 2008), strain gauge technique (Rasty et al., 2007; Olmi, 2010), thermography (Pieczyska et al., 2006; Connesson et al., 2011). The selection of the experimental method to study plastic “in-plane” deformation depends on several elements: the ability and accuracy of the method, the ease of its use in practice, the character of the obtained results and the possibility of their work out, etc. The greatest potential taking into account a variety of research techniques and a diversity of the analyzed problems, create the photoelasticity andMoiré method. 490 B. Kozłowska To study elastic-plastic states, much more suitable is the method of photoelastic coating than a traditional photoelasticity which requires the use of optically active materials having characteristics corresponding to material characteristics of the tested element also in the non- linear range. Similarly, among various Moiré techniques – the best applicability to study elastic-plastic states has the classical geometric Moiré method. The frequently nowadays applied interferen- tial Moiré method has a very high sensitivity (density of the grid is here of several thousand lines/mm) and is used to the analysis of small areas. Its additional disadvantage is the necessity of coherent (laser) light application. Holographic interferometry, which bases on phenomena occurring during the coherent light interference, can be used directly for measurement of displacement (or shape) of the structure. It shows good accuracy (strain measurement with an accuracy of 0.1 · 10−4-1 · 10−4), but has a high mechanical sensitivity, and the result analysis is labor-consuming. It requires also laser light. Making use of coherent light requires also one of the modern experimental methods – elec- tronic speckle pattern interferometry (ESPI). It has a lot of advantages – non-contact measu- rement, high sensitivity, resolution and accuracy; it gives surface images of displacement and strain components. However, ESPImethod has also very serious limitations – high susceptibility on conditions in which experiment is performed, sensitivity to even slight movements. It is also not suitable for large deformations and requires the researcher to have high skills and a lot of experience. The second modern experimental method, the digital image correlation method (DIC) also allows non-contact measurement and gives surface images of displacement and strain compo- nents. Compared to the ESPImethod, it has a biggermeasurement range, but lower resolution. The surface of the element needs special preparation and the results require a lot of calculations. In contrast to modern experimental methods, one of the oldest commonly known but still most often used experimental technique is the strain gauge measurement. It enables one to get strain values with a very high accuracy (∼ 1 · 10−6), but only in several points. That is why it is usually used in combination with other experimental methods, after determining the most loaded parts of a structure. An auxiliary character has also usually the thermography method which is often used to detectmaterial defects. Its accuracy is difficult to determine anddependsmostly on temperature resolution of a thermovision camera and external conditions. However, the method allows one to observe thermal processes taking place in the material, what is a great advantage, especially concerning the elastic-plastic problems. Taking into account advantages and disadvantages of various experimental methods and abilities of their application regarding to the elastic-plastic states analysis, the simplicity of their use in practice, equipment availability, etc., for further experimental testing, threemethods have been selected: a method of photoelastic coating, Moiré method and the thermographymethod. All the threemethods give information about deformation of thewhole tested area (not only at several points). They can be used to investigate real structure elementsmade of anymaterial, in working conditions, even under heavy loading causing partial material plastifying. Their advantage is also excellent visualization of the process of progressive material plastifying. In particular, themethods of photoelastic coating and thermographyallowdirect observation of the process of formation and development of plastic zones, changes (expansion) of their boundaries and the direction of propagation. The first two methods are optical methods, although each of them gives information about different physical quantities (method of photoelastic coating – strain,Moiré method – displace- ment).Theyare also comparable in termsof the level of accuracy (measurementordetermination of strain with an accuracy ∼ 1 ·10−4). The third method – thermography is based on a quite Experimental investigations of elastic-plastic strain states... 491 different physical phenomenon (emission of infrared radiation from the surface of the tested element), which allows, to a certain degree, verification of the results obtained from the first two methods. Theadditional advantage of thephotoelastic coatingmethod is thepossibility of direct strain measurement. The disadvantage is the dependence of the obtained results on the properties of the tested material (using the analytical method of strain separation). TheMoiré method has a purely geometrical character (measurement of the displacements is direct and does not depend on the properties of the tested material), determination of strain, however, requires differentiation of the obtained displacement values. The photoelastic coating method and the Moiré method are methods very often used in worldwide research works, thus their choice seems to be themost evident and proper. Thermo- graphy, though less precise and giving results more qualitative than quantitative, can provide a useful and interesting complement to the first two methods, particularly for solving certain elastic-plastic problems. 2. Experimental testing The experimental investigation of elastic-plastic states has been performed on two-dimensional models of structural elements weakened by different stress concentrators (holes) and subjected to tensile stresses. The elements of this type and loaded in such a way are often used inmodern structures, particularly as different construction joints. The areas of the elements weakened by cut-outs are parts of structures which require special and accurate checking (Wung et al., 2001; Olmi, 2010; Foust et al., 2011). Shapes of stress concentrators have been designed on the basis of literature data and engineering practice (single central holes of various shapes and groups of circular holes of various configurations). The objects of discussion presented in the work are three of the models – Fig. 1. The first two models with one central hole have the same area of themostweakened cross-section in thex axis of symmetry (the effective cross-section) anddiffer only in shape of the hole. The thirdmodel is weakened by five circular holes cut symmetrically not only on the axis of symmetry x. Fig. 1. Models of constructional elements 492 B. Kozłowska Themodels have beenmade of a duralumin sheet 3mm thick, fromwhich stripes of 100mm in width and 450mm in length have been cut out. The length of the stripes was taken large enough to compensate potential non-uniformity of tensile stresses distribution applied at their ends. The characteristic of thematerial (aluminumalloy EN-AW-2024) has been determined expe- rimentally on the basis of a standard static uniaxial tensile test and it is shown in Fig. 2. Fig. 2. Material characteristic After mechanical working and special surface preparation, the models have been covered with: a cross-type grid of 20 lines/mm (for the Moiré method) with a 2mm thick photoelastic coating of strain constant: fε =1.114·10 −3 1/fringe order (for the photoelastic coatingmethod) andwith a layer of graphite (for the thermographymethod). Next, different holes have been cut out in the way which allowed avoiding creation of plastic strains as a result of machining. The models have been loaded at their ends with uniformly distributed tensile stresses p. As the measure of the loading intensity, the ‘loading factor’ s has been accepted. It has been calculated as the ratio of the average tensile stresses at the cross-section weakened by the hole on the axis of symmetry perpendicular to the stretching direction in relation to the offset yield strengthR0.2 =182MPa (taken from thematerial characteristic). The loading of the models has been increased step by step within the over-elastic range of the material. At selected levels of loading, images of the Moiré pattern (for the displacement u(x,y) and v(x,y)) and isochromatic pattern (for dark- and light-field polariscope) have been registered. For the thermographymethod, the loading of themodels increased continuously and the temperature changes on the specimen surface have been recorded by a thermovision camera. On the basis of the experimental data obtained from the Moiré method and the method of photoelastic coating, quantitative analysis of theelastic-plastic strainandstress aroundthe stress concentrators has beenmade (Kozłowska, 2008, 2013). Due to low resolution of thermal images obtained from the infrared camera, the thermograms have given only qualitative information about deformation of the elements (Kozłowska, 2012). 3. Determination of the suitability of selected experimental methods to elastic-plastic analysis in dependence on the material plastifying level The experiment has been performed within a wide range of the loading – from the moment of occurring first plastic deformations to the elements failure. But not at every level of loading all of the selected methods have been equally useful. As proved byan experiment, photoelastic coatingmethod allows analysis of the plastic strain starting from the beginning of their occurring in the material – level of about s ≈ 0.5 (tensile stress p≈ 45MPa) for the models with a single hole or s≈ 0.3 (tensile stress p≈ 44MPa) for the model with five holes. At that loading level, the Moiré method is not very useful (to low Experimental investigations of elastic-plastic strain states... 493 number ofMoiré fringes). Exemplary images of isochromatic andMoiré patterns at thediscussed loading level for the area around the stress concentrator of model III are shown in Fig. 3. Fig. 3. Model III (s=0.495) – isochromatic pattern: (a) dark-field polariscope, (b) light-field polariscope;Moiré fringe pattern: (c) u(x,y) surface, (d) v(x,y) surface For significant plastic deformation, for a loading level over s≈ 1 (tensile stress p≈ 91MPa) for themodels with a single hole or s≈ 0.8 (tensile stress p≈ 116MPa) for the model with five holes, the method of photoelastic coating is no longer useful. It is so because the photoelastic coating can crack (Fig. 4), come off the base (Fig. 5) or (in the best case) isochromatic fringes in the most plastified areas become quite unreadable (Fig. 6). TheMoiré method, however, at the same loading level or even higher, enables proper analysis of elastic-plastic states (Figs. 4-6). Fig. 4. Model II (s=1.136) – isochromatic pattern: (a) dark-field polariscope, (b) light-field polariscope;Moiré fringe pattern: (c) u(x,y) surface, (d) v(x,y) surface Fig. 5. Model III (s=1.136) – isochromatic pattern: (a) dark-field polariscope, (b) light-field polariscope;Moiré fringe pattern: (c) u(x,y) surface, (d) v(x,y) surface The discussed examples show an approximate range of the application of theMoiré method and the method of photoelastic coating depending on the level of plastic deformation of the material. This rangemaybe changed to some extent because the sensitivity of these twomethods depends on the selection of the proper “measuring element”. Greater possibilities creates here 494 B. Kozłowska Fig. 6. Model V (s=0.778) – isochromatic pattern: (a) dark-field polariscope, (b) light-field polariscope;Moiré fringe pattern: (c) u(x,y) surface, (d) v(x,y) surface theMoirémethodbychangingdensity of thegrids – for thegeometricMoirémethod, thenumber of lines per millimeter may vary from a few to several tens (most commonly from 20 to 40). The change in sensitivity of themethod of photoelastic coating can be achieved by variation of thickness of an optically active layer, but in amuch smaller range.Usually, the thickness of the applied photoelastic coating is 1 to 3mm, although you can find one of 0.25mm.A thicker layer causes stiffening of the element and introduces toomuch ofmeasurement inaccuracy (averaging over the thickness). The upper limit of the capabilities of the photoelastic coatingmethod is the layer cracking or its coming off the base at higher loading levels. This disadvantage doesnot applies to theMoirémethod,because even if the grid is imprinted to a photographic film and is affixed to the surface of the element, it forms a flexible thin layer, very strongly connected with the base. In the case of a grid applied directly to the surface of the element (e.g. etched), the problem of the grid coming off does not exist at all. For the grids used in experimental testing (20 lines per millimeter), the range of measured strain was ∼ 0.2% to 1.5%, while for the photoelastic coating of 2mm thick, the maximum determined plastic strain was up to∼ 0.9%. The thermal images obtained from infrared camera did not give sufficiently precise informa- tion about the temperature distribution on the surface of the tested element. The accuracy of temperature measurement by an infrared camera, however, depended mainly on its resolution, and that increases with the technical possibilities. Even if the thermograms do not allow one to obtain the values of strain components, they show directly the full development of plastic zones, from the beginning of their creation to the failure of the element as e.g. in model III (Fig. 7) Fig. 7. Thermograms (model III) for loading levels: (a) s=0.989, (b) s=1.172, (c) s=1.304 (first cracks), (d) s> 1.355 (element failure) The method of thermography has also no limitations resulting from the properties of the layer covering model (graphite), as it is in the case of the photoelastic coating method (the optically active layer) or even in the Moiré method, when the grid is affixed to the surface of Experimental investigations of elastic-plastic strain states... 495 the model. Thus, this method can be used, both as a preliminary tool to select an area of the element to be tested with a more accurate method (the formation of plastic zones) as well as a way to observe the mechanism of plastic material failure in the range already out of reach for other experimental methods. 4. The accuracy of the determination of strain components by selected experimental methods Although the Moiré method and the method of photoelastic coating have different ranges of the best suitability for quantitative analysis of the elastic-plastic strain and stress components, there is a certain range of loading level for which bothmethods can be properly used. To compare the accuracy of the Moiré method and the method of photoelastic coating, the loading levels for which both methods give results freely allowing one to determine the strain components have been chosen. The analysis of model II and III has been carried out at the loading level s=0.952, which corresponds to tensile stresses p=87MPa. The average stress on the x axis was then σav = 173MPa (average strain – εav = 0.38%). For model V the loading level accepted for analysis, was s = 0.687 (tensile stress p = 100MPa), for which the average stress on the axis of symmetry x – was σav =125MPa (average strain – εav =0.15%). At the chosen loading levels, a quite significant plastification of thematerial already occurred around the stress concentrators, on the one hand large enough to enable measurement by the Moiré method, on the other hand, still allowing using themethod of photoelastic coating. The analysis of the elastic-plastic strain state for the models with one hole is shown on the example ofmodel III, forwhich the images of isochromatic andMoiré patterns around the stress concentrator at the loading level s=0.952 are presented in Fig. 8. Fig. 8. Isochromatic pattern for model III – s=0.952: (a) dark-field polariscope, (b) light-field polariscope;Moiré fringe pattern – (c) u(x,y) surface, (d) v(x,y) surface To compare the results obtained from the Moiré method and the method of photoelastic coating, the strain components distribution on a horizontal axis of symmetry x perpendicular to the loading direction (segment AB – Fig. 1) have been assumed. In addition, on the same diagram it is also shown the distribution of strain εx and εy obtained from numerical (FEM) calculations (Fig. 9). Formodel V (with five circular holes), the images of isochromatic andMoiré pattern around the stress concentrators at the loading level s=0.687 are shown in Fig. 10. To compare the results obtained from the Moiré method and the method of photoelastic coating, the strain components distribution in the horizontal axis of symmetry x perpendicular to the loading direction (segment AB – Fig. 1) has been assumed (Fig. 11). For this model, FEM calculations have not been performed. As follows from the presented diagrams, the strain components εx and εy distribution in the axis of symmetry x (segmentAB) for the chosen loading level obtained from theMoiré method and themethod of photoelastic coating are approximate. The differences between the calculated 496 B. Kozłowska Fig. 9. Strain components distribution in the axis of symmetry x for model III – s=0.952: (1) Moiré method, (2) method of photoelastic coating, (3) FEM calculations Fig. 10. Isochromatic pattern for model V – s=0.687: (a) dark-field polariscope, (b) light-field polariscope;Moiré fringe pattern – (c) u(x,y) surface, (d) v(x,y) surface Fig. 11. Strain components distribution in the axis of symmetry x for model V – s=0.687: (1) Moiré method, (2) method of photoelastic coating values of strain components do not exceed a few percent (6% to 8%).A higher divergence occurs between the experimental results and numerical calculations, but even there it does not exceed 10% to 12%. 5. The influence of grid configuration on the accuracy of determination of strain components distribution The strain components obtained on the basis of the Moiré fringes at the traditionally affixed grid (in accordance with the axes of symmetry of the model – the direction of tension) can be determined accurately not in every part of the testedmodel.Where the surfaces of deformation are not much diversified in the direction of the axis of the coordinate system (directions of differentiation), the derivatives can be calculated with a certain error. Experimental investigations of elastic-plastic strain states... 497 As it has been said, the measurement sensitivity of the Moiré method may be increased by changing density of used grids. It is not always convenient, when the increasing of the accuracy is neededonly in thepart of the tested element. In suchacase, an improvement of themeasurement accuracymay be achieved by performing additional tests with grids rotated with respect to the direction of the basic grid by a certain angle. Fig. 12. The grid affixed according to the direction of tensile stresses (a), grid rotated by an angle of 45◦ (b) In order to verify the possibility of increasing accuracy of determination of the elastic-plastic strain distribution around stress concentrators, additional tests have been performed at the grid rotated by an angle of 45◦ with respect to the direction of tensile stress (coordinate system x-y) – Fig. 12. An exemplary comparison of the strain components obtained by grids arranged in different ways is shown for model V with five holes at the loading level s= 0.778, for which, the strain state has been already determined using a traditionally affixed grid (Kozłowska, 2008). The images ofMoiré fringes at the grids affixed in different ways are shown in Fig. 13, where one can see a larger number of Moiré fringes in selected areas at the rotated grid than at the grid affixed in the direction of tensile stress. Fig. 13.Moiré pattern for model V (s=0.778) – grid affixed according to the direction of tension: (a) u(x,y), (b) v(x,y); grid rotated by an angle of 45◦: (c) clockwise, (d) counter-clockwise The analysis for the rotated grid has been carried out as in previous cases (because of the double symmetry of themodel and loading) for one-quarter of the tested area (Kozłowska, 2007) – Fig. 14. For strain analysis, the coordinate system x-y associated with an element under tension and a traditionally affixed grid has been rotated by an angle of 45◦ to forma coordinate system x′-y′ associated with a rotated grid (Fig. 12). On the basis of the displacement obtained fromMoiré fringes at the rotated grid, the strain components have been determined in the new coordinate system (x′,y′) bymeans of analytical differentiation. 498 B. Kozłowska Fig. 14.Moiré pattern for the analyzed area of model V (s=0.778) – grid rotated by an angle of 45◦: (a) clockwise, (b) counter-clockwise Then the values of strain εx and εy in the basic coordinate system (x,y) have been calculated bymakinguseof formulas enablingconverting the strain statedescribed inonecoordinate system to another (rotated) one (1), where α=45◦, Fig. 15 εx = εx′ cos 2α+εy′ sin 2α+γx′y′ sinαcosα εy = εx′ sin 2α+εy′ cos 2α−γx′y′ sinαcosα 1 2 γxy =(εx′ −εy′)sinαcosα+ 1 2 γx′y′(sin 2α−cos2α) (5.1) Fig. 15. Strain state transformation To compare the obtained results with those from the analysis of Moiré images at the grid affixed according to the direction of the tensile stresses, the strain components distribution in the horizontal axis of symmetry x has been assumed (Fig. 16). In the diagram, the correction of strain components calculation resulting from the larger number ofMoiré fringes (selected areas) is shown. The analysis of strain components for model V (model with five holes) shows that in its horizontal axis of symmetry x, where the data obtained at the grid affixed traditionally are relatively inaccurate (low number ofMoiré fringes), the information found from the rotated grid allows one to increase the accuracy of strain determination and to correct errors resulting from differentiation of surfaces of deformation. Experimental investigations of elastic-plastic strain states... 499 Fig. 16. Strain distribution in the axis of symmetry x (model V – s=0.778): (1) grid affixed according to the direction of tension, (2) grid rotated by an angle of 45◦ 6. Conclusions The review of experimental methods used in mechanics of solids carried out in terms of elastic- plastic analysis resulted in the selection of three of them for further investigations: the Moiré method, the method of photoelastic coating and the method of thermography. The choice has been dictated not only by their measuring capabilities in the over-elastic range of the material characteristics, but also by the simplicity of their use in practice and the availability of the equipment. The main advantage of all three methods is the ability to conduct an experiment on real structures in working conditions, also under loading causing partial plastifying of the mate- rial and to obtain information about the strain state of the whole tested object. An additional advantage of the chosen methods (especially the method of photoelastic coating and the ther- mography method) is excellent visualization of the process of progressive material plastifying. The advantage of theMoiré method is also the simplicity of measurements and the work out of the experimental results. TheMoiré method and themethod of photoelastic coating enable a relatively easy and quick quantitative analysis of the strain state around stress concentrators on the basis of experimental data. Thermographic tests have shown that this method allows rather getting a general view of the distribution of plastic strain components than their precise quantitative determination. The conducted tests and detailed analysis of experimental data enabled definition of the range of applicability of each of the selected methods and determination of their capabilities in termsof theaccuracyof calculation of strain components atvarious stages ofmaterial plastifying. The range of application of the method of photoelastic coating (for an 2mm thick optically active layer used in the testing of duralumin elements) is up to the maximum plastic strain ∼ 0.9%. TheMoirémethodallowes testing of the elements in awider range of thematerial plastifying. For the used grids of 20 lines permillimeter, plastic strain can bemeasured up to∼ 1.5%, while determination of the strain less than∼ 0.2% causes difficulties due to the low number of Moiré fringes. The measurement sensitivity of the Moiré method can be locally increased by affixing the grids at different angles. Such a possibility has been verified by additional tests performed at the grid rotated by an angle of 45◦ to the axis of symmetry of themodel. That gave an effect similar to applying the rosette of strain gauges and showed that the accuracy of the elastic- plastic strain distribution around stress concentrators could be increased in the areas where the number of Moiré fringes is low. The comparison of the strain components distribution in the horizontal axis of symmetry x (perpendicular to the direction of tension) obtained from theMoiré method and themethod of 500 B. Kozłowska photoelastic coating for the range of material plastifying, for which both of them are applica- ble, shows that the differences between results are about a few percent. The comparison with numerical calculations (FEM) also shows good agreement of the results. The quantitative analysis of strain and stress components in the whole area around stress concentrators proves that theMoiré method is a little more useful. Themethod of photoelastic coating is more labor-consuming due to the necessity of analytical strain separation (solving of the system of partial differential equations, Kozłowska, 2013) and converting the obtained results from irregular grid nodes to the rectangular grid. 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