Jtam-A4.dvi JOURNAL OF THEORETICAL SHORT RESEARCH COMMUNICATION AND APPLIED MECHANICS 56, 1, pp. 323-328, Warsaw 2018 DOI: 10.15632/jtam-pl.56.1.323 MODIFIED SPLIT HOPKINSON PRESSURE BAR FOR INVESTIGATIONS OF DYNAMIC BEHAVIOUR OF MAGNETORHEOLOGICAL MATERIALS Leszek J. Frąś, Ryszard B. Pęcherski Institute of Fundamental Technological Research of the Polish Academy of Science, Warsaw, Poland e-mail: lfras@ippt.pan.pl The magnetorheological fluid is a functional material that is changing its rheological pro- perties and finally solidifies in amagnetic field. The dynamic behaviour, testedwith the use of the Split Hopkinson Pressure Bar is an important issue for description of this material, which is commonly used in different kinds of shock absorbers. This note presents a new idea how to modify the known SHPB set up in order to investigate dynamic properties of magnetorheological materials. Keywords: Split Hopkinson Pressure Bar (SHPB), Magnetorheological Fluid (MRF), dyna- mic behaviour, solidification in magnetic field, ferroelements 1. Introduction The magnetorheological fluid (MRF) is a material which is composed of microsized (less than 10µmdiameter) magnetoactive carbonyl iron particles immersed in a carrier fluid, e.g. oil. The influence of the magnetic field changes properties of the MRF. The ferroelements are joined together and form characteristic shapes – braids, which are created along the magnetic field lines. The braids are concentrating in the process of sticking together. The applied magnetic field is changing the state of thematerial leading to solidification. Then the yield shear strength appears the important material parameter, the value of which is dependent on strength of the magnetic field. The aim of the paper is to present the idea how to investigate the behaviour of the solidified magnetorheological fluid under high strain rates. The experimental tests are carried out with application of the own construction of a laboratory test stand – the modified Split Hopkinson Pressure Bar (SHPB). The Hopkinson Pressure bar was not only used to test metallic materials or brittle solids at high strain rates. Kenner (1980) adopted the split Hopkinson pressure bar to test pressure pulses in different kinds of fluids – ethyl alcohol, distilled water, glycerin and two kinds of oil. The experimental results help one to evaluate the one dimensional representation of pulse trans- mission and reflection at a solid-fluid interface. The results of experimental investigations make a basis for creation of amathematical expression describing the pressure pulse distributed in the fluid. Another attempt to use the SHPB to test fluids was presented by Lim et al. (2009). The authors tested Cannon N4000 and N5100 fluids consisting 100% polybutene. The experimental part was prepared with use of the SHPB furnished with aluminum bars and the fluid container was specially prepared. This part was machined of soft and flexible rubber and was tested with respect to fluid expansion in the radial direction. The dynamical tests of the polymermaterials were considered by Siviour and Jordan (2016) where the behaviour of the rearrangement of mi- crostructure of amorphous polymers was reviewed. The preliminary information about testing magnetorehological fluid under high strain rates was announced by Frąś (2015). There was pre- sented a proposal of the laboratory set-up and an attempt to use the Perzyna viscoplasticity 324 L.J. Frąś, R.B. Pęcherski model to describe the behavior ofmagnetorheological fluids. Another attempt of testingmagne- tically controlled materials was presented by Wang (2016). The authors tested a self-prepared material with content of 75% carbonyl iron particles in several magnetic fields – form 95 to 382kA/m. During those experiments, stress values from 5 to almost 16MPa (for maximal ma- gnetic field value)were obtained.Another attempt to use the SplitHopkinsonPressureBarwith magnetically controlled materials to test magnetorheological elastomers was presented by Liao et al. (2013). The authors used for several magnetic field strengths – maximally 320kA/m and received in a dynamic compression test maximal stress values about 6MPa with velocity of the striker about 30m/s. Themicrosized ferroelements in themagnetic field created the structure of viscoplastic solids. The structural rearrangements controlled by themagnetic field in the course of deformation can be investigated experimentally due to the recent developments of MEMS devices designed by Jarząbek et al. (2015). 2. Magnetorheological fluid The magnetorheological fluid contains microsized ferroelements. The particles are spherically shaped and their diameter is less than 10µm.Themagnetoactive ferroelements are coated with a silicon shield and immersed in the carrying fluid, e.g. mineral oil. The silicon coating prevents from aggregation of particles which are made of a carbonyl iron material. The influence of the magnetic field forces the ferroelements to connect together into characteristic linear shapes – the braids. The linearly-shaped elements made of ferroelements are sticking together and create the solid structure of the material. Fig. 1. The ferroelements in neutral state (a) and under the influence of a magnetic field (b) The ferroelements can freelymove in the carrying fluid. Figure 1b shows the influence of the magnetic field on the way how the ferroelements are connected. The magnetoactive particles are sticking together creating characteristic braids parallel to the line of themagnetic field. The whole rearrangement of the structureduring thedeformation process canbedescribedby tearing off a single ferroelement from the braid. The structure is deformed in the course of taking off from the sequence of separate braids. The rearrangement of ferrorelements under the external force tends to swap the neighboring element. The particle is shifted and this produces a shear angle. The interaction energy of two particles is given as follows (Jolly et al., 1996) E12 = |m2|(1−3cos2θ) 4πµ1µ0r 3 (2.1) where m is mass of the particle, θ corresponds to the angle of shear, r denotes the distance between particles and µ1 is the relative permeability, µ0 is vacuum permability. The shift of a Short Research Communication – Modified Split Hopkinson Pressure Bar for... 325 Fig. 2. The rearrangement of the structure, F – external force,H –magnetic flux single ferroelement produces migration of the braid. The refreshable features of the magneto- rheological fluid allow one to use them as an energy absorptionmaterial. The shifting of a single ferroelement by some external force causes reorganization of the skeleton structure. 3. The laboratory test stand The testing stand is made on the basis of the Split Hopkison Pressure Bar with 7075 alloy aluminum bars. Their length is 1000mm and diameter 20mm. The strain gauges are cemented in themiddle – four on the each bar, and they are working as a quarter bridge sub systemwith the signal amplifier. Themain idea is to modify the present laboratory device and prepare it to test the magnetorheological fluid – LORDMRF-140CG in amagnetic field at high strain rates by using the prepared coil – the resitivity of used copper 0.7mmwire is 180Ohm. It generates a 120kA/m magnetic flux with a 360V and 2A direct current power supply. The coil with inner diameter 30mmand length 50mmhas 80 turns of thewire. The power line is realized byEA-PS 8360-30 and the maximum voltage is 360V while the current is 50A. The laboratory device to investigate magnetorheological materials is subjected tomodification. The idea of the proposed modification is presented in Fig. 3. Fig. 3. 1 – striker, 2 – laser sensor to measure velocity, 3 – incident bar, 4 – strain gauges, 5 – glue, 6 – deformable hose, 7 – MR fluid, 8 – coil cover, 9 – coil , 10 – glue, 11 – transmitter bar, 12 – spring, 13 – momentum trap, 14 – velocitymeasure system, 15 – signal amplifier , 16 – oscilloscope, 17 – power supply for coils The novelty of the proposed laboratory test stand is the application of coils for the sleeves shown in Fig. 3 to induce a constantmagnetic field. Also a new shear testing device is designed. Due to this, the dynamic axial compression and shear tests of the solidified magnetorheological material is possible. The theory of measurement of the axial strain and determination of the axial stresswith theuse of theSHPBwas presentedbyKlepaczko (2007). The striker accelerated by the gas gun achieves velocity V0 which is measured by a matrix of diodes and photodiodes. In the case of impact by the striker against an incident bar shockwave is triggered. It has length ϕ = 2L, where L is length of the striker. The time period of this wave is T = 2L/C0, where C0 is the velocity of the sound wave inside the bar. 326 L.J. Frąś, R.B. Pęcherski 4. Results During the experiment, the MR fluid solidified under the magnetic field responds to the stress waves. The effect of the compressive longitudinal incident pulse and the reflected pulse can be observed in Fig. 4b. Fig. 4. (a) The deformable hose with theMR fluid before the test, (b) the observed wave forms of the tested material The MR specimen is closed in a deformable hose made of latex with carefully prepared dimensions – 10mm long and 20mm in the external diameter of the bars, which allows one to keep about 3.2ml of the fluid injected with a syringe – Fig. 4a. It provides free deformation of the solidifiedMR fluid. The specially designed coil is generating a 120kA/mmagnetic flux and is responsible for sticking the ferroelements together. The generated field is parallel to the axis of incident – the transmitted bars what keeps the solidified ferroelements between the bars. The magnetoactive particles are arranged along the lines of themagnetic field. The deformable hose presented in Fig. 4 a with the MR fluid inside allows free deformation during the dynamical tests. The influence of the thin rubber hose on the longitudinal stress waves can be neglected. The results of experimental investigation are presented below. Fig. 5. The results of the experiment, the nominal stress-strain curve The results presented in Fig. 5 are obtained during experimental investigation. Thematerial has been tested with a 300mm long striker and with two velocities 18m/s and 10m/s±0.1m/s. Short Research Communication – Modified Split Hopkinson Pressure Bar for... 327 During the experiment aluminum bars without the shaper placed between the striker and the incident bar were used. Themeasured values were multiplied 200 times by the signal amplifier. For this reason, the obtained transmittedwave had an amplitude about 0.08Vwith the velocity of the striker about 18m/s and about 0.035V for∼ 10m/s. 5. Conclusions TheSplitHopkinsonPressureBar has been adopted to test themagnetorheological fluid at high strain rates. The material was tested for two velocities of the striker to test and evaluate the laboratory set-up. The obtained results can be compared with the results ofWang et al. (2016) who tested similar materials but with a lower content of iron particles 74% versus 84% in our case.Wang et al. (2016) obtained for 200mT (159kA/m) and the strain rate 6000s−1 the stress values in the range of 10-17MPa. The material structure of Wang et al. (2016) was completely different (74% of carbonyl irons and several another additions closed into the gel structure) but the order of magnitude was similar to tested LORDMRF-140CG (84% of carbonyl irons). The the effect of dispersion can play an essential role in the interpretation of the experimental data. The dispersion effect in the aluminium bars is not significant due to the large ratio of wavelength to the bar diameter, however, it has not been analysed yet and requires further studies. The comparison of our preliminary results confirms the validity of the concept of the proposed laboratory set-up and gives a promising perspective for a more detailed investigation aiming at the identification of Perzyna model. Acknowledgment This work was supported by the NCN (National Science Centre Poland) Research Project: 2015/17/N/ST8/02018. References 1. FrąśL.J., 2015,ThePerzynaviscoplasticmodel in dynamic behaviour ofmagnetorheologicalfluid under high strain rates,Engineering Transactions (Rozprawy Inżynierskie), ISSN: 0867-888X, 63, 2, 233-243 2. JarząbekD.M.,ChmielewskiM.,WojciechowskiT., 2015,Themeasurementof theadhesion force between ceramic particles and metal matrix in ceramic reinforced-metal matrix composites, Composites Part A – Applied Science and Manufacturing, 76, 124-130 3. JollyM.R.,CarlsonJ.D.,MunozB.C., 1996,Amodel of the behaviour ofmagnetorheological materials, Smart Materials and Structures, 5, 607-614 4. Kenner V.H., 1980, The fluid Hopkinson bar,Experimental Mechanics, 20, 7, 226-232 5. Klepaczko J.R., 2007, Introduction to Experimental Techniques for Materials Testing at High Strain Rates, Institute of Aviation,Warsaw 6. Liao G., Gong X., Xuan S., 2913,Magnetic field-induced compressive property of magnetorhe- ological elastomer under high strain rate, Industrial and Engineering Chemistry Research, 52, 25, 8445-8453 7. Lim A.S., Lopatnikov S.L., Gillespie Jr. J.W., 2009, Phenomenological modelling of the response of a dense colloidal suspension under dynamic squeezing flow, Polymer Testing, 28, 891-900 328 L.J. Frąś, R.B. Pęcherski 8. Siviour C.R., Jordan J.L., 2016, High strain rate mechanics of polymers: a review, Dynamic Behavior of Materials, 2, 15-32 9. WangY.,Wang S., XuC., Xuan S., JiangW.,GongX., 2016,Dynamic behavior ofmagne- tically responsive shear-stiffening gel under high strain rate, Composites Science and Technology, 127, 169-176 Manuscript received August 24, 2017; accepted for print November 3, 2017